HomeMy WebLinkAboutNCG030027_MONITORING INFO_20200122T "
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
�jCG D3b0a'-7
DOC TYPE
❑ HISTORICAL FILE
C MONITORING REPORTS
D / a
DOC DATE
❑
YYYYM M D D
Um'T*N
January 13, 2020
Colin W. Betchan
Environmental, Health & Safety Supervisor
(919) 702-3703 (mobile)
(336) 503-6562 (fax)
co l i nwbetch a n (a'Deaton. co m
Division of Water Quality RECEIVED
1617 Mail Service Center JAN 2
Raleigh, North Carolina 27699-1617 2 2020
CENTRAL FILES
Attn: DWQ Central Files DWR SECTIOP!
RE: January 2020 Monthly Tier III Discharge Monitoring Report
Attached are the analytical results and associated chain of custody for the January 3, 2020, monthly Tier
III stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater
General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility.
Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North
Carolina Division of Water Quality (NCDWQ). The chain of custody lists rainfall as 0.24 inches, at the time
of sample shipment to the laboratory. The total rainfall for the rain event was 0.96 inches.
I certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with the system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,
or other persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violations.
Sincerely, y �j�'
W—^� �lM�/�%%�
Colin W. Betchan
EHS Supervisor
Attachments
Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted 01/13/2020
CERTIFICATE OF COVERAGE NO. NCG03 o 0 2 7
FACILITYNAME Eaton Corporation
COUNTY Person County
PERSON COLLECTING SAMPLES Colin Betchan
LabCert.q ENV375/OW217041aI[ 1.���\/�I r
Comments on sample collection or analysis: mr
IAN 2 2 N11
LABORATORY Pace National
CENTRAL. FILE`
Part A: Stormwater Benchmarks and Monitoring Results LWR �drCT10
SAMPLE COLLECTION YEAR 2020
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or E] Monthly' January (month)
DISCHARGING TO CLASS ❑ORW ❑HC!W ❑Trout ❑PNA
❑Zero -flow [:]Watersupply [:]SA
*Other WS-Ill: NSW
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks
_
-
100 mg/L or 50 mg/0
6.0— 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Tool Room Trench (005)
01/03/2020
0.96
17.4
8.4
0.0110
0.00288
0.0277
0.806
0.035395
/
�, ,^r rt^ � _r•� r\ ^.Ivy
.
1 1 -i ->
l
Monthly sampling (instead of semi-annual) musi,begin'with'the second consecutive benchmark exceedahce'for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Colin Betchan
Name (Print name)
EHS Supervisor
Title (Print title)
64 hX_af 1113 aodo
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n Nn rlicrhnrnc Chic norinn02
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
-
46529
NCOIL
00552
CO530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO 0
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑
REGIONAL OFFICE CONTACT NAME: Danny Smuh
Mail an original copv of this DMR, including all "No Discharqe" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee -
Da` 1
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3
aceAnr ical® ANALYTICAL REPORT
NaVonal Center for Testing a lnnave0on January 10, 2020
Eaton Corporation
Sample Delivery Group:
Samples Received:
Project Number:
Description:
Site:
L1176249
01/04/2020
28091-R
Eaton Corp Monthly Stormwater
ROXBORO,NC
Report To: Dustin LaClair
2564 Durham Road
Roxboro, NC 27573
Entire Report Reviewed By:
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Eaton Corporation 28091-R L1176249 0IM012011:39 1 of 23
TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cl): Cover Page
1
Tc: Table of Contents
2
Cp
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
3S5
2020-01-03-005 L1176249-01
5
4Cn
Oc: Quality Control Summary
g
Gravimetric Analysis by Method 2540 D-2011
8
SSr
Wet Chemistry by Method 1664B
g
Metals (ICP) by Method 200.7
t0
C
Volatile Organic Compounds (GC/MS) by Method 624.1
11
Pesticides (GC) by Method EPA 608.3
13
GI
Polychlorinated Biphenyls (GC) by Method EPA-608.3
15
JAI
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
16
GI: Glossary of Terms
21
9Sc
Al: Accreditations & Locations
22
Sc: Sample Chain of Custody
23
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE.
Eamn Corporation 28091-R L1176249 01110201139 2 of 23
SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
1,
Collected by
Collected dateAime
Received date/time
2020-01-03-005 L1176249-01 WW
Colin Betchan
01103/2015:07
01/04/2008:30
Cp
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
datedime
datedime
ETC
Gravimetric Analysis by Method 25400-2011
WG1406805
1 01/0712010:22
01/0712011:36
MMF
Mt. Juliet, TN
Wet Chemistry by Method 1664E
WG1408114
1 01/08/2017AS
01109/2008:45
AMG
Mt. Juliet, IN
Metals (ICP( by Method 200.7
WG1406598
1 01/06/2018:27
01/07/20 03:08
TRB
Mt. Juliet, TN
Volatile Organic Compounds(GC/MS( by Method 624.1
WG1406126
1 0110512000:05
01/05/2000:05
BMB
Mt. Juliet, TN
Pesticides(GC) by Method EPA 608.3
WG1406117
1 0110512008:18
01/0612013:51
LEL
Mt. Juliet, TN
°
Cn
Polychlorinated Biphenyls(GC) by Method EPA-608.3
WG1406117
1 01/05/2008:18
01/OSI2019:45
RP
Mi. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG1406113
1 01/05/20 08:02
01/05/20 20:48
AO
Mt. Juliet, TN
s
Sr
o�C
7G1
aAl
9Sc
ACCOUNT: PROJECT: SDG: DATErNME: PAGE:
�3 Eaton Corporation 28091-R L1176249 01/10/2011:39 3 of 23
CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the Cp
appropriate preservatives, and within method specified holding times, unless qualified of notated within
the report. Where applicable, all MDL (LOD) and RDL (LOO) values reported for environmental samples �TC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this Case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of mY 3Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
SSr
5QC
[GI
Heather J Wagner
Project Manager AI
9Sc
ACCOUNT: PROJECT: SDG: DATEMME' PAGE:
Eaton Cornoralion 28091-R L1176249 01/10/2011'.39 4 of 23
020-01-03-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Ilected datoltlme: 01103120 15:07 L1176249
Additional Information
Result Units
Cp
Analyte
z
pH (On Site) 8.4 su
TC
Temperatuie(on-sile) 11.7 DegC
aSs
Gravimetric Analysis by Method 2540 D-2011
Result Oualifier MDL
RDL
Dilution Analysis
Batch
Analyte mg/I mg/I
mg/I
date/time
Cn
Suspended Solids 174 0.539
3.85
1 01/07/20201136
WG1406805
Wet Chemistry by Method 1664B
6
QC
Result Oualifier MDL
RDL
Dilution Analysis
Batch
Analyte mg/I mg/I
mgll
date/time
TPH -Oil&Grease U 0.806
5.56
1 01/09/202008:45
WG1408114
Gl
Metals (ICP) by Method 200.7
a
Result Oualifier MDL
RDL
Dilution Analysis
Batch
AI
Anzlyte mgll mg/I
mg/I
date/time
9
Copper 0.0110 0,00700
MIMI
1 01/07/202003:08
WG1406598
SC
Lead 0.00288 1 0.06200
-
0.00500
1 01/67/202003:08
WG1406598
u
Zinc 0.0277 J 0.00340
0.0500
1 01/07/2020 03:08
WG1406598
Volatile Organic Compounds (GC/MS) by Method 624.1
Analyte
Result
mgh
Oualifief MDL
mg/I
RDL
mgll
Dilution
Analysis
date/time
Batch
Acrolein
U
000887
0.0500
1
01/05/202000:05
WG1406126
Acrylonitrile
U
0.00187
0.0100
1
01/05/202000:05
WG1406126
Benzene
U
0.000331
0.00100
1
01/051202000:05
WG1406126
Sroinodichloromethane
U
0000380
0.00100
1
01/05/202000.05
WG1406126
Bromoform
U
0.000469
0,00100
1
01/05/2020 00:05
WG1406126
Broinomethane
U
0.000866
000500
1
01105/202000:05
WG1406126
Carbon tetrachloride
U
0.000379
0.00100
1
01/05/202000:05
WG1406126
'Chlombenzene
U
0000348
0.00100
1
01105/202000:05
WG1406126
o
Chlorotlibromomethane
U
0.000327
0.00100
1
07/05I202000:05
WG1406126
Chlaroethane
U
0.000453
0.00500
1
01165/202000:05
WG1406126
2-Chloroethyl vinyl ether
U
0.00301
0.0500
1
011051202000:05
WG1406126
Chloroform
U
0.006324
0.00500
1
01/05/202000:05
WG1406126
a
Chloromethane
U
0.000276
0.00250
1
01105I2020 00:05
WG1406126
1.2-13ichlorobenzene
U
0.000349
0.00106
1
01105/202000:05
WG1406126
1,3-Dichlorobenzene
U
0.000220
0.00100
1
01/05/202000:05
WG1406126
1,4-Dichlorobenzene
U
0.000274
0.00100
1
01/05/202000:05
WG1406126
Dichlorodifluoromethane
U
0.000551
0,00500
1
01105/202000:05
WG1406126
11-6lchloroethane
U
0.000259
0.00100
1
01/05/202000:05
WG1406126
1,2-Dichloroethane
U
0.000361
0,00100
1
01/05/202000:05
WG1406126
'1,1-61'chloroethene
U
0.600398
0.00100
1
01/05/202000:05
WG1406126 ,
r
trans-1,2-Dlchloroethene
U
0.000396
0.00100
1
01/05/202000:05
WG1406126
1,2-Dichloropropene
U
0.000306
000100
1
01/05/202000:05
WG1406126
cis-1,3-Dichloropropene
U
0.000418
0.00100
1
01105002000:05
WG1406126
trans-1,3-Dichloropropene
U
0.000419
O.00l00
1
01/6S/202000:05
WG1406126
Ethylbenzene
U
0000384
0,00100
1
01/05/2020 00:05
WG1406126
Methylene Chloride
U
0.00160
0.00500
1
01/05/202600:05
WG1406126
1,1,2,2-Tetrachloroethane
U
0.000130
000100
1
01105f202000:05
WG1406126
Telrachloroemone
U
0.00o372
0.00100
1
01/05/202000:65
WG1406126
Toluene
U
0000412
0.00100
1
01/05/202000:05
WG1406126
4,1,1-Trichloroethane
U
0.000319
0.00100
1
01/05/202000:05
WG1406126
n
1,1,2-Trichloroethane
U
0.000383
0.00100
1
011051202000:05
WG1406126
i ACCOUNT
PROJECT:
SDG:
DATEMME: PAGE:
Eaton Corporation
28091-R
Ln76249
Ot/1020 11:39 5 of 23
2020-01-03-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected dateltlme: 01/03/20 15:07 L1176249
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyze
mg/1
n1g/l
mg/I
date/time
Lichloroethene
U
0.000398
0,00100
1 OV05/202000:05
WG1406126
Inchlorofluoromethane
U
0.00120
0.00500
1 01/05/202000.05
WG1406126
Vinyl chloride
U
0,000259
0,00100
1 OV05/202000:05
WG1406126
(27oluene cig
101
80.0-120
011051202000: 05
WG1406126
(5)4-13romolluorobenzene
953
80.0-120
01705120200005
WG1406126
(5) 12 Oichloroethone-64
101
70G-130
0V05202000.05
W61406126
Pesticides (GC) by
Method EPA 608.3
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
ni
trgh
mind
date/lime
Nddn
U
0.00000813
0.0000500
1 01/06/202013:51
WG1406117
Alpha BHC
U
0.0000166
0.0000500
1 01/06/202013:51
WG1406117
Beta BHC
U
0.0000184
0D000500
1 01/06/202013:51
WG1406117
Delta BHC
U
0.0000197
0.0000500
1 01/06/202013:51
WG1406117
Gamma BHC
U
0,0000176
0.0000500
1 01/06/202013:51
WG1406117
Chlordane
U
0.0000977
0.000500
1 01/06/202013,51
WG1406117
44-DDD
U
0.0000170
0,0000500
1 01/06/202013:51
tYG1406117
4,4-DDi
U
0.0000164
0.0000500
1 011061202013:51
WG1406117
4,4-DOT
U
0.0000177
0.0000500
1 01/06/202013:51
WG1406117
Deland
U
0,00000751
0.0000500
1 011061202013,51
WG1406117
Endosulfan I
U
0.0000179
0.0000500
1 011061202013:51
WG1406117
Endosulfan II
U
0.0000176
0,0000500
1 01/06/202013:51
WG1406117
Endosulfan sulfate
U
0,0000196
0.0000500
1 OV06/2020 i3:51
WG1406117
Endrin
U
0.0000189
0.0000500
1 01/06/202013:51
WG1406117
Enddn aldehyde
U
0.0000142
0.0000500
1 01/06/202013:51
WG1406117
Endrm ketone
U
0.0000170
0,0000500
1 01/06/202013:51
WG1406117
Heptachlor
U
0.0000108
0.0000500
1 011061202013:51
LVG1406117
Heptachlorepoxide
U
0.0000175
GD000500
1 01/06/202013:51
WG1406117
lexachloiobenzene
U
J3 0.0000134
0.0000500
1 01/06/202013:51
WG1406117
Methoxychlor
U
0.0000193
0,0000500
1 01/06/202013:51
WG1406117
Toxaphene
U
0000168
0,000500
1 01106/202013:51
WG1406117
(5) Decochloroblphcnyl
76.1
70.0-144
011061202013,51
WG1406117
(S Tehachloro-m xylene
676
10.0-135
011061202013,51
WG1406117
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier MDL
RDL Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/1
date/time
PCB 1016
U
0,000100
0.000500 1
01/05/202019:45
WG1406117
PCB 1221
U
0.0000730
0.000500 1
011051202019:45
WG1406117
PCB 1232
U
0.0000420
0.000500 1
01105/202019:45
WG1406117
PCB 1242
U
0.0000470
0.000500 1
01/05/202019,45
WG1406117
BOB 1248
U
0,0000860
0.000500 1
01/05/202019:45
WG1406117
PCB 1254
U
0,0000470
0,000500 1
OIJ05/202019:45
WG1406117
PCB 1260
U
0.000120
0.000500 1
01/05/202019:45
WG1406117
(S)Decochloroblphenyl
78.6
10.0744
071051202019.45
W61406117
(STesochloro-nr-xylene
72.4
10.0-135
011051202019,45
WG1406117
Semi Volatile Organic Compounds
(GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyse
mg/1
ri
mglt
date/time
Acenaphnene
U
0.000316
0.00100
1 01/05/2020
20:48
WG1406113
Aceniphthylene
U
0-000309
0.00100
1 01/05/2020
2048.
WG1406113
Anthracene
U
0.00029i
0.00100
1 01/05/2020
20:48
WG1406113
Benzidine
U
000432
0.0100
1 01/05/2020
20:48
WG1406113
Benzo(a)anlhiacene
U
0.0000975
0,00100
1 01/05/2020
20:48
WG1406113
ACCOUNT: PROJECTSDG: DATEITIME: PAGE.
Eaton Corporation 28091-R L1176249 01/10/2011:39 6 of 23
2020-01-03-005 SAMPLE RESULTS - 01
Collected date/lime: 01/03/20 15:07 L1176249
11
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MOIL ROL Dilution Analysis Batch
Analyte mg4 mg/I mgll date/lime
ONE LAB. NATIONWIDE. M
Benzo(b(fluoranthene
U
0.0000996
0.00100 1
01/05202020:48
WG1406113
Benzo(k)fluonnthenc
U
0.000355
0.00100 1
01/05/202020:48
WG7406113
Benzo(g,h,1)pegene
U
0.000161
0.00100 1
01/051202020:48
WG1406113
Benzo(alpyrene
U
0.000340
0.00100 1
01/05/2020 20:48
WG1406113
Bls(2-chlorethoxylmethane
U
0.000329
0.0100 1
01/05/2020 20:48
WG1406113
Bis(2-chloroethyl)ether
U
0.00162
0.0100 1
01/05/2020 20:48
WG1406113
Bus(2-chloroisopropypethei
U
0.000445
0,0100 1
61/05/202020:48
W61406113
4-Bromophenyl-phenylether
U
0.000335
0.0100 1
01/05/2020 20:48
WG1406113
2FChloronaphthalene
U
0.000330
0.00100 1
01/05/2020 20:48
WG1406113
4=Chlorophenyl-phenylether
U
0.000303
0.0100 1
01/05/2020 20:48
WG1406113
,Chrysene
rr
U
0,000332
0.00100 1
01/0512020 20:48
WG1406113
Aenz(a,h)anthracene
U
0.000279
0.00100 1
01/052020 20:48
WG1406113
-3;3-Dichlorohenzidine
U
0.00202
0.0100 1
01/05/202020:48
WG1406113
2,4-Dinitrololuene
U
0.60165
0,0100 1
01/05/202020:48
WG1406113
26-Dinitrotoluene
U
0.060279
0.0100 1
01/056020 20:48
WG1406113
0
1,2-Diphenylhydrazine
U
0.000318
0.0100 1
01105/202020*48
WG1406113
Fluoranlhene
U
0.060310
0.06160 1
_ 01/05202020:48
WGU06113 '
Fluoiene,
U
0000323
0.00100 1
01/05/2020 20:48
WG1406113
Hexachlorobenzene
U
0.000341
0.00100 1
O1/05/2020 20:48
WG1406113
Hexachloro-13-butadiene
U
0.000329
0.0100 1
01/05/2020 20:48
WG1406113
Hexachlorocyclopentadiene
;r
U
0.00233
6.6160 1
01I05/202026:48
WG140616
Hexachloroethane
U
0.000365
0.0100 1
01/05/2020 20:48
WG1406113
Indeno(1,2,3td)pyrene
U
0.0002A
0.00100 1
01/051202020:48
WG1406113
Isophorone
U
0.060272
0.0100 1
01/65/2020 20:48
WG1406113
iNaphthalene
U
0.000372
0.00100 1
01/0512620 20:48
WG1406113
Nitrobenzene
U
0.000367
0.0100 1
01/05/2020 20:48
WG1406113
n-Nitrosodimethylamine
U
0.00126
0.0100 1
01/05/202026:48
WG1406113
n-Nitrosodiphenylamine
U
0.00119
0.0100 1
01105/20202048
WG1406113
.n-Nitrosodi-n-propylamine
U
0.000403
0.0100 1
01/05/20202048
WG1406113
Phenanthrene
U
0.000366
0,00100 1
01/05/202020:48
WG1406113
Benzylbutyl phthalate
U
0.000275
0.00300 1
01I0512020 2048
WG1406113Bis(2-ethylhexyllphthalate
0.00107 J
0.0 0070 9
0.003100 1
01/05/202020*48
WG1406113
Di-n-butyl phthalate
0.000360 J
0,000266
0.00300 1
01/05/2020 20:48
WG140616
Diethyl phthalate
U
0000282
0.00300 1
01/65/202020:48
WG1406113
Dimethyl phthalate
U
0.000283
0.00300 1
01/05/202020:48
WG1406113 .
Di-n-octyl phthalate
U
0.006278
0.00300 1
01105/202020:48
WG1406113
Pyrene
U
0.006330
0.00100 1
01/05/202020:48
WG1406113
1,2,4-Trichlorobenzene
U
0.000355
0.0100 1
01/051202020:49
WG1406113
4-Chloro-3-melhylphenol
U
0.000263
0.0106 1
01/05/202020:48
WG1406113
2-Chlorophenol
U
0.000283
0.0100 1
01JOW2020 20:48
WG1406113
2,4-Dichlarophenol
U
0.006284
0.0100 1
01/05/2020 20:48
WG1406113
2,4-Dimethylphenol
U
0,000624
0,0100 1
01/05/202020:48
WG1406113
4,6-Dinitro-2-melhylphenol
U
0.00262
0.0100 1
01105/202020:48
WG1406113
2,4-Dinihophenol
U
0.00325
0.0100 1
01105/202020:48
WG1406113
2-Nitrophenol
U
OM0320
0.0100 1
01/051202020:48
WG1406113
4-Nitrophenol
U
0.00201
0.0100 1
01/05/202020:48
WG1406113
Pentachlorophenol
U
0.006313
0,0100 1
01/056020 20:48
WG1406113
Phenol
0.00170 J
0.000334
0.0100 1
011051202020:48
WG1406113
2,4,6-Trichlorophenol
U
0.060.297
0.0100 1
01/05/2020 20 48
WG1406113
(92-Fluorophenol
35.1
10.0-120
011051202020:48
WG1406113
(Sfrphenol-d5
25.4
8.60-424
01105/202020:48
WG1406113
(S) Nitrobenzene-d5
58.3
15.0-314
011051202020:48
WG1406113
(Sj2-Fluorobiphenyl
74.8
22.0-127
01165120202048
WG1406113
(5)24,6-Tfibromopheno)
60.5
10.0-153
01105120202OA8
WG1406113
(SJp-Terphenyl-M
90.4
29.0-141
OY651202020.48
WG1406113
} ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Eaton Corporation
28091-R
L1176249
0111012011:39
PAGE:
7 of 23
WG1406805 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Gravlmetric Analysis by Method 2540 D-2011 L1176249-01
Method Blank (MB)
(MB) R3468975-1 01/07/20 11.36 C p
MB Result MB Qualifier PAB MDL ME RDL
Analyte mg/I mg/I mg/I �.. _._�... _.__.
Suspended Solids U 0 �50 2.50 ' TC
L1176248-01 Original Sample (OS) • Duplicate (DUP)
(UD) Lll/b24d-Ul Ul/U//ZU T:36 • (UUP) R3488975-3 01/07/2011:36
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Suspended Solids 315 316 1 0422 5
Laboratory Control Sample (LCS)
(Li-J) ttS4Cby/b-L UVU112U 11: b
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyze me/I mg/I % %
____ _—_____ ___-
_____ ------
Suspended Solltls 773 768 99 4 85.0-__ii"
3Ss
r1
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE'
Eaton Corporation 28091-R L1176249 01/10/201139 8 of 23
WG1408114 QUALITY CONTROL_ SUMMARY ONELAB.NATIONVADE
Method Blank (MB)
Cp
(MB) P3489203-1 OV09/20 08:45
MB Result MB Qualifier MB MDL MB ROL
Analyte n
TPH - Oil& Grease U
mg/I mgfl
0.725 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3489203-2 01/09/20 08:45 - (LCSD) R3489203-3 01/09/20 08:45
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mgll TO mgli % % % % %
TPH - Oil 8 Grease 20.0 1T5 18.7 ST5 93.5 64.0-132 6.63 34
ACCOUNT: - PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1176249 01/1012011:39 9 of 23
WG1406598
QUALITY CONTROL SUMMARY
ONELAB.NATIONWIDE.
Metals (ICP) by Method 200.7
L1176249-01
Method Blank (MB)
(MB) R3488512-1 01/07/20 0218
Cp
M8 Result
MB Qualifier MB MOLL
MB ROL
Analyte mg/I
mg/I
mg/I
Copper U
0.00700
-_ __. __- -_ -- - -_ _
0.0100
_TC
- --
Lead U
0.00200
0,00500
3
Zinc U
0.00340
O0500
SS
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(Lcb) R3488512-2 01/07/20 02:21
- (LCSD) R3488512-3 01/07/20 02:23
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Oualifier LCSD Oualifier RPD
RPD Limits
Analyze
mg
ri
mg,l
%
%
%
%
%
Copper
1.00
0.967
.________._______________.
0.966
96.7
_..______________.
96.6
850-115
___________.___.______________.__. _____.
0.117
________ _____--
20
Lead
1.00
0.972
0.968
97.2
96.8
250-115
0.394
20
Zinc
1.00
0.971
0.970
971
97D
850-LS
0.0824
20
L1176239-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(0S) 1-1176239-01 01/07/20 02:26 • (MS) P3488512-5 01/07/20 02:31
• (MSD) R3488512-6 01/07/20 0234
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Oualifier RPD
Analyte
mg/I
mg/I _
mg/I
mg/I
%
%
%
%
Copper
1.00
ND
0.968
0.977 �95.&
97.7
70.0-130-�_--�
- _ -� 0.996
Lead
iDo
ND
0.971
0.984
97.1
98A
1 700-130
1.34
Zinc
1.00
NO
1.01
1.02
96.1
97.5
1 70.0-130
144
L1176416-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
RPD Limits
os
-20 --
20
20
(Us) Lll/64lb-01 O1/07/20 02:36 • (MS) R3488512-7 01/07/20 02:39
• (MSD) R3488512-8 01/07/20 0241
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec Limits
MS Qualifier MSD Oualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
%
%
Copper
1.00
NO
0.968
0.963
96.8
96.3
1 70.0-130
0.596
20
Lead
1.00
ND
0.974
0.965
974
96.5
1 70.0-130
0.980
20
Zinc
i.00
ND
0971
0.961
971
96.i
1 70.0-130
0.984
20
ACCOUNT: PROJECT: EDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1176249 01/10/201139
10 of 23
WG1406126 QUALITY CONTROL SUMMARY_ ONE LAB. NATIONWIDE.
=�VolatlleorganlNCompounds=(GC/MS)-by:MetK'6d 624.1
Method Blank (MB) Cp
(MB) R3488076-2 01/04/20 21:21
MB Result MB Qualifier MB MDL MB RDL
Anah¢e
mg/I
mg4
mg/I
FC
Acrotein
U
0.00887
0.0500
a$5
Acrylonitrile
U
0.00187
0.0100
Benzene
U
0.000331
0.00100
Bromodichloromethane
U
0.000380
0.00100
4
Bromoform
U
0.000469
0.00100
Cn
Bromomethane
U
0.000866
0.00500
s
Carbon tetrachloride
U
0.000379
0,00100
Sr
Chlorobenzene
U
0.000348
0.00100
Chlorodibromomethane
U
0.000327
0.00100
Chloroethane
U
0.000453
0.00500
_ .....
2-Chloroethyl vinyl ether
U
0.00301
0.0500
7GI
Chloroform
U
0.000324
0.00500
Chloromethane
U
0,000276
0.00250
1,2-Dichlorobenzene
U
0.000349
0.00100
"
VAS
13-Dichlorobenzene
U
0,000220
0.00100
14-Dichlorobenzene
U
0.000274
MOW
a
Dichlorodifluoromethane
U
0.000551
0.00500
SC
1,1-Dichloroethane
U
0.000259
0.00100
1,2-Dichloroethane
U
0.000361
0.00100
1,1-Dichloroethene
U
0.000398
0.00100
trans-1,2-Dichloroethene
U
0.000396
0.00100
1.2-Dichloropropane
U
0.000306
0.00100
cis-1,3-Dichloropropene
U
0.000418
0.00100
trans-1,3-Dichloropropene
U
0.000419
0.00100
-
Emylbenzene
U
0.000384
0.00100
Methylene Chloride
U
0.00100
0.00500
71,2,2-Tetrachloroethane
U
0.000130
0.00100
Tetrachloroethene
U
0.000372
0.00100
Toluene
U
0.000412
0.00100
1,1,1-Trtchloroethane
U
OT00319
0.00100
1,1,2-Trichloroethane
U
0.000383
0.00100
Trichloroethene
U
0.000398
0,00100
_ -
Trichlofofluoromethane
U
0.00120
0.00500
Vinyl chloride
U
0000259
0,00100
(S) Toluene-d8
101
80.0-120
(S)4-Bromofluorobenzena
101
80.4110
-
(S)12-Dichloroethane-d4
103
70.0-130
ACCOUNT:
PROJECT:
SDG: DATE/TIME: PAGE:
Eaton.
Corporation
28091-R
L1176249 01/10/2011:39: 11 of 23
WG1406126 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 624A L1176249-01
Laboratory Control Sample (LCS)
(LCS) R3488076-1 01/04/20 2040
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyze
mg/l
mg/I
%
%
Acrolein
0,0250
0.0351
140
60.0-140
Acrylomaile
0.0250
00257
ion
50.0-i40
Benzene
0.00500
000494
98.8
65.0-135
Bra modich hap methane
0,00500
000518
104
70.0135
Bromororm
0.00500
000531
106
70.0-130
Bromomethane
0,00500
0.00503
i01
15.0-185
Carbon tetrachloride
0-00500
0.00570
114
70.0-130
Chlorobenzene
0.00500
0.00485
970
65.0-135
Chlorodibromomethane
0,00500
0.00488
97.6
70.0-135
Chloroethane
0.00500
0.00462
924
40.0-160
2-Chloroethyl vinyl ether
0.0250
0,0252
101
0 100-225
Chloroform
0.00500
0.00524
105
70.0-135
Chloromethane
0.00500
000437
874
0.100-205
1,2-Dichlorobenzene
0,00500
0,00498
99.6
65.0-135
1,3-Dichlorobenzene
0.00500
0,00467
934
70.0-120
1,4-Dichlorobenzene
0.00500
0.00495
99.0
65.0-135
Dichlorodinuoromethane
0.00500
0.00527
i0
49.0-155
1,1-Dichloroethane
0.00500
0.00497
99.4
70.0-130
1.2-Dichloroethane
0.00500
0.00541
109
70.0-130
i.i-Dichloroethene
0.00500
0.00524
i05
50.0-i50
trans-1,2-Dichloroethene
0.00500
0.00514
103
70.0-130
1.2-Dichloropropane
0.00500
0.00458
91.6
35.0-165
cis-1,3-Dichloropropene
0.00500
0.00523
105
25.0-175
trans-1,3-Dichloropropene
0.00500
0.00512
102
50.0-150
Ethylbenzene
0,00500
0,00515
103
60.0-140
Methylene Chloride
0.00500
000490
98.0
60.0.140
1,1,2,2-Tetrachloroethane
0.00500
000415
930
60-0-140
Tetrachloroethene
0.00500
000520
iO4
70.0-130
Toluene
0.00500
000475
95.0
70.0-130
1,U-Trichloroethane
0.00500
0.00567
113
70.0-130
11,2-Trichloroethane
0.00500
0,00506
101
70.0-130
Trichloroethene
0.00500
0,00524
105
65.0-135
Tnchlorofluoromethane
0,00500
0,00599
120
5D.0-150
Vinyl chloride
0.00500
0.00496
99.2
5.00-i95
(5)Toluene-d8
98.4
80.0-120
(5) 4-Bromalluorobenzene
101
80.0-120
(5)1,2-Dichloroelhone-d4
105
70.0-130
LCS 0ualifier
ACCOUNT:
Eaton Corporation
PROJECT:
28091-R
BOG: DATE/TIME
L1176249 01/10/20 1139
PAGE:
12 of 23
WG1406117 QUALITY CONTROL SUMMARYONE LAB. NATIONWIDE
_.-
__T-pesticitles.(GC)-by'M ethotl'EPA'608`3 �-- -
Method Blank (MB) Cp
(MB) R3489389-1 OV06/20
Analyte
11:10
MB Result
mg/I
MB Qualifier MB MDL
mg4
MB ROL
mgn
Aldrin
U
0,00000813
0.0000500
Alpha BHC
U
0.0000166
0.0000500
Beta BHC
U
0.0000184
0.0000500
DeltaBHC
U
- 0.0000197
0.0000500
Gamma BHC
U
0.0000176
0.0000500
4 4-DDD
U
0.0000170
0.0000500
4,4-DDE
U
0.0000164
0.0000500
4,4-DDT -
U
0.0000177
0.0000500
Dieldrin
U
0.00000751
0.0000500
Endosulfan)
U
0.0000179
0.0000500-
Endosulfan II
U
0.0000176
0.0000500
Endosulfan sulfate
U
0.0000196
0.0000500
Endrin
U
0.0000189
0.0000500
Endrin aldehyde
U
0.0000142
0.0000500,
Endrin ketone
U
0.0000170
0.0000500
Heptachlor
U
0.0000108
0.0000500
Heptachlor epoxide
U
0.0000175
0,0000500
Hexachlorobenzene
U
0.0000134
0.0000500
Methoxychlor
U
0.0000193
0.0000500
Chlordane
U
0.0000977
0.000500
Toxaphene
U
0.000168
0.000500
/S/ Decochlorobiphenyl
59.4
10.0-144
(S)Tetrochloro-m-xylene
26.6
10.0135
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3489389-2
Analyte
01/06/2011:35 • (LCSD) R3489389-3
Spike Amount LCS Result
mg/I mg/1
01/06/20 11:47
LCSD Result
moll
LCS Rec.
%
LCSD Rec
%
Rec. Limits
%
LCS Qualifier LCSD Qualifier RPD
%
RPD Limits
%
Aldrin
0,00100
0.000797
0.000647
79.7
64.7
420-140
20.8
35
Alpha BHC
0.00100
0.000837
0.000726
83.7
72.6
37.0-140
14.2
36
Beta SHE
0.00100
0.000837
0.000773
83.7
T7.3
17.0-147
7.95
44 .
Delta BHC
0.00100
0.000910
0.00083E
91.0
_
83.8
19.0-140
8.24
52
Gamma BHC
0.00100
0.000827
0000745
62.7
74.5
32.0-140
10.4
39
4,4-6DD
0.00100
OA00907
0.000845
907
845
31.0-141
7.08
39
4,4-DDE
0.00100
0.00096E
0.000889
96.8
88.9
30.0-145
8,51
35
4.4-DDT
0.00100
0.000873
O.00O812
BZ3
K2
25.0-160
7.24
42
Dieldrin
0.00100
0.000858
0.000798
85.8
79.8
3U-146
7.25
49
Endosulfan I
0.00100
6,000848
0.000791
84.E
79.1
45.0-153
6.96
28
ACCOUNT: PROJECT:
Eaton. Corporation 28091-R
SDG:
L1176249
DATEMME:
01/10/20 1139
PAGE:
13 of 23
WG1406117 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Pesticides (GC) by Method EPA 608.3 L1176249-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
piL�) HC4dydd9 -2 Ul/Ub2U 11:3b - (LCSU) H3489389-3
01/06/201147
Spike Amount
-CS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RFD
RPD Limits
Analyte
mg/I
mo/I
mg/1
%
%
%
%
Endosulfan 11
0.00000
0.000800
0.000742
80.0
74.2
�1.00-202
i 7.52
53
Endosulfan sulfate
MOM
0.000882
0,000823
98.2
82.3
26.0-144
6.92
38
Endrin
0.00100
0,000893
0.000830
89.3
83.0
30.0-147
7.31
48
Endrin aldehyde
0.00100
0.000811
0.000752
81.1
75.2
56-0-128
7.55
20
Endrin ketone
0.00100
0000766
0.000720
76.6
72.0
54.0-142
6.19
20
Heptachlor
0.00100
0000802
0000644
301
64A
34.0-140
279
43
Heptachlor epoxide
0,00100
0,000841
0.000778
84.1
77.8
37.0-142
778
26
Hexachlombenzene
0.00100
0000726
0.000421
72.6
42.1
35.0-120
J3 53.2
25
Methoxychlor
000100
0.000763
0,000729
76.3
72.9
44.0-160
4.56
22
(S) Decochlorobiphenyl
829
72.6
100-144
(S)Ttrochloro-m- xylene
577
436
100-125
ACCOUNT: PROJECT: SDG: DATEfTIME: PAGE:
Eaton Corporation 28091-R L1176249 01/10/201139 14 of 23
WG1406117
QUALITY
CONTROL SUMMARY �
ONE LAB. NATIONWIDE
-
P.olychlorinated;Biphenyls;(GC)_by-Melhod=EPA=608.3
_=-
Method Blank (MB)
(MB) R3488227-1 01/05/2016:39
Analyte
MB Result
mgh
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
PCB 1260
U
0.000120
0000500 _
PCB 1616
U
0.000100
0.000500 ,
PCB 1221
U
0.0000730
0,000500
PCB 1232
U
0.0000420
0.000500
PCB 1242
U
0.0000470
0.000500
PCB 1248
U
0.0000860
0.000500 _
PCB 1254
U
0.0000470
0.000500
(S) Decochlorobiphenyl
48.8
10.6-144
(S) Tetrochloro-m-xylene
28.2
10.0435
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R348B227-2 01105/2016:51 •
(LCSD) R3488227-3 01/05/2017:03
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rea.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
Tell
%
%
%
%
%
PCB 1260
0.00250
0.00193
0.00208
77.2
83.2
8,00-140
P P 748
38
PCB 1016
0,00250
0.00181
MOM
72.4
64.0
50 0-140
12.3
36
(S) Decochlorobiphenyl
58.3
51.5
10.0-144
(S) Telrochloro-m-aylene
41.1
23.2
10.0-135
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Eaton Corporation 28091-R L1176249 01/10/2011:39 15 of 23
WG1406113 QUALITY CONTROL SUMMARY ONELAB.NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1176249-01
Method Blank (MB)
ii f<o42S IHbL UVUb/LU lb:bb
MB Result
MB Dualifier MB MDL
MB RDL
Analyte
mg/1
mg/I
mg/I
Acenaphthene
U
0,000316
0.00100
Acenaphthylene
U
0.000309
0,00100
Anthracene
IJ
0.000291
0.00100
Azobenzene
U
0.000318
0.0100
Benzidine
U
0.00432
0,0100
Benzo(a)anthracene
U
0,0000975
0.00100
Benzo(b)fluoranthene
U
0.0000896
OOOM
Benzo(k)fluoranthene
U
0,000355
0,00100
Benzo(g,h,i)perylene
U
0.000161
0.00100
Benzo(a)pyrene
U
0.000340
0,00100
Bisl2-chlorethcxy)methane
U
0,000329
0.0100
Rrs(2-chloroethylether
U
O.00i62
0.0100
Bis(2-chloroisopropyllether
U
0.000445
0,0100
4-Bromophenyl-phenylether
U
0.000335
0.Oi00
2-Chloronaphthalene
U
0.000230
0,00100
4-Chlorophenyl-phenylether
U
0.000303
0,0100
Chrysene
U
0.000332
0,00100
Dibenz(a,h)anthracene
U
0.000279
0.00100
3,3-Dichlorobenzidine
J
D.00202
O0100
2 c-Dinitrotoluene
J
000165
0.0100
2.6-Dinitrotoluene
U
0.000279
00100
Fluoranthene
U
0,000310
000 OO
Fluorene
U
0.000323
0.00100
Hexachlorobenzene
U
0.000341
0,00100
Hexachloro-i,3-butadiene
U
0.000329
0 0i0o
Hexachlorocyclopentadlene
J
0.00233
0.0100
Hexachloroethane
U
0.000365
0,0100
Indeno(1,2,3-cd)pyrene
J
0.000279
0.00100
Isophorone
U
0,000272
0.0100
Naphthalene
U
0.000372
0.00100
Nitrobenzene
U
0.000367
0.0100
n-Nitrosodimethylamine
U
O,00126
0.0100
n-Nitrosodiphenylamine
U
0.00119
0.0100
n-Nitrosodi-n-propvlamine
U
0.000403
0,0100
Phenanthrene
U
0.000366
0.00100
Benzylbulyl phthalate
U
0.000275
0.00300
Bis(2-e1hylhexyl)ph!halate
IJ
0.000709
0!00300
Di-n-butyl phthalate
U
0.000266
0.00300
Diethyl phthalate
J
0.000282
0.00300
Dimethyl phthalate
U
0,000293
0.00300
Cp
E
FS
4Cn
SSr
rGl
Al
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE'
Eaton Corporation 26091-R
L1176249 01/10201139 16 of 23
WG1406113 QUALITY CONTROL SUMMARY _ ONE LAS. NATIONWIDE,___
--- -- _ _ _ .. _ -
"Semi VOIa11I2 Drgantc Compounds �(GC/MS) by Method 625.1 - Lil76249-01
Method Blank (MB)
(MB) R3488192-2 01105/2016:55
MB Result
Anah4e mgfl
MB Qualifier MB MDL
mgfl
MB RDL
mg/I
Di-n-oayl phthalate
U
0.000278
0,00300 -
Pyrene
U
0.000330
0.00100
1.2,4-Trichlorobenzene
U
0.000355
0.0100 -
4-Chloro-3-methylphenol
U
0.000263
0.0100
2-Chlorophenol
U
0,000283
0.0100
2.4-Dichlorophenol
U
0.000284
0.0100
24-Dimethylphenol
U
0.000624
0.0100
4,6-Dinitro-2-methylphenol
U
0.00262
0.0100
2.4-Dinitrophenol
U
0.00325
0.0100
2-Nltrophenol
U
0.000320
0.0100
4-Nitrophenol
U
0.0020i
0.0100
Pentachlorophenol
U
0.000313
0.0100 -
Phenol
U
0.000334
0.0100
2,4.6-Trichlorophenol
U
0.000297
0.0100-
QMtrobenzene-d5
52.7
15.0-34
(S) 2-Fluomblphenyl
68.3
224127
(S)p-Terphenyl-d14
86.3
29.0-141
(S) Phenol-d5
25.9
8.00-424
(S) 2-Fluorophenol
378
10.0420
(S)2,4,6-Tribromophenol
68.5
10.0453 - -
Laboratory Control Sample (LCS)
(LCS) P3488192-1 OV05/2016:33
Spike Amount LCS Result
Analyte
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
Benzo(a)anthracene.
Benzo(b)fluoranthene
Benzo(k)fluoramhene
Benzo(g,ni)perylene
Benzo(a)pyrene
Bis(2-ch lorethoxy)metha ne
Bisl2-chloroethyllether
Bis(2-chloroisopropyl)ether
0.0500
0.0500
0.0500
0,0500
0.100
0.0500
0.0500
0.0560
0.0500
0.0500
0.0500
0.0500
0,0500
0.0380
6.0468
0.0416
0.0396
0.0262
0.0415
0.0451
6.0445
0.0453
0.0462
0.0336
0.0350
0.0355
LCS Rec.
76.0
81.6
83.2
79.2
26.2
83.0
90.2
99.0
90.6
92.4
67.2
70.0
71.0
Rec. Limits
47.0-145
33.0-145
27.0-133
37.0-125
1.00-120
33.0-143
24.0-159
11.0-162
1.00-219
T7:0-163
1.00-219
33.0-185
36.0-166
LCS Qualifier
ACCOUNT:
Eaton Corporation
PROJECT:
28091-R
SDG: DATE/TIME:
L1176249 0110/2011:39
PAGE:
17 of 23
WG1406113 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1176249-01
Laboratory Control Sample (LCS)
)LCS) R3488192-1 01/05/20 1633
Spike Amount
LCS Result
LCS Res.
Rec. Limits
Analyte
mg/I
mg/I
%
%
4-Bromophenyl-phenylether
0,0500
0.0433
86.6
53.0-127
2-Chloronaphihalene
0.0500
0.0370
74.0
60.0-120
4-Chlorophenyl-phenylether
0.0500
0.0425
85.0
25.0-158
Ch ysene
0.0500
0.0429
85.8
17.0--168
Dibenz(a,h)anthracene
0.0500
0,0394
78.8
1.00-227
3,3-Dichlorobenzidine
0,100
0.0846
84.6
1,00-262
2,4-Dinitrotoluene
0.0500
0,0454
90.8
39.0-139
2,6-Dinitrotoluene
0.0500
0.0445
89.0
50.0-158
Fluoranthene
0,0500
0,0445
89.0
26.0-137
Fluorene
0,0500
0.0423
84.6
59.0-121
Hexachlorobenzene
0.0500
0.0421
84.2
i.00-152
Hexachloro-13-butadiene
0.0500
0.0296
59.2
24.0-120
Hexachlorocyclopemadiene
0.0500
0.0276
55.2
10.0-120
Hexachloroelhane
0.0500
0.0297
59,4
40.0-120
Indeno(1,2,3-cd)pyrene
0.0500
0.0388
77.6
100-171
Isophorone
0.0500
0.0341
68,2
21.0-196
Naphthalene
0.0500
0.0316
63.2
21.0-133
Nitrobenzene
0.0500
0.0315
63.0
35.0-180
n-Nitrosodimethylamine
0.0500
0,0198
39.6
10.0-120
n-Nitrosodiphenylamine
0.0600
0.0416
83.2
44.0-120
n-Nitrosodl-n-propylamine
0,0500
0.0378
75.6
1.00-230
Phenamhrene
0.0500
0.0404
30.8
54.0-120
Benzylbutyl phthalate
0.0500
0.0400
80.0
1.00-152
9is(2-ethylhexyI)phthalale
0.0500
0.0379
75.8
8.00-158
Di-n-butyl phthalate
0,0500
0.0450
90.0
1.00-i20
Diethyl phthalate
0.0500
0.0441
88.2
1.00-120
Dimethyl phthalate
0.0500
0.0439
87.8
h00-120
Di-n-ociyl phthalate
0.0500
0.0372
74A
4,00-146
Pyrene
00500
0.0435
8Z0
52.0-120
1,2,4-Trichlorobenzene
0,0500
0.0298
59.6
44.0-142
4-Chloro-3-methylphenot
0.0500
0.0267
734
22.0-147
2-Chlorophenol
0.0500
0.0339
57.8
23.0-134
2,4-Dichlorophenol
00500
0.0348
69.6
39.0-135
2,4-Dimethylphenol
0.0500
00325
65.0
310-120
4,6-Di nitro-2-m ethyl phenol
0.0500
0.0442
88.4
t00-181
2,4-Diniaophenol
0.0500
0.0442
88.4
1.00-i91
2-Nitrophenol
0,0500
0.0348
69.6
29.0-132
4-Nitrophenol
00500
0.0222
44.4
1.00-132
Pentachiorophenoi
0.0500
0.0399
79.8
14.0-176
Phenol
00500
0.0163
32.6
5,00-120
LCS Oualifier
ACCOUNT: PROJECTSDG:
Eaton Corporation 26091-R L1176249
DATE/TIME:
01/10/201139
PAGE:
12 of 23
,
WG1406113
_ __
QUALITY-
CONTROL
SUMMARY_
_ Y
ONE LAB_ NATIONWIDE
- --
- Semi Volatile`Organic`Com pounds
(GC/M S) by Method 625.1
--'
-� _._
L1176249-Ot-
Laboratory Control Sample (LCS)
Cp
(LCS) R3488192-1 01/05/2016:33
Spike Amount
LCS Result
LCS Rec.
Rec Limits
LCS Qualifier
ETC
Analyte mg/I
mgn
%
%
2,4,6-Trichlorophenol 0.0500
0.0383
76.6
37.0-144
a
(S) Nitrobenzene-d5
50.4
15.0-314
$5
IS)2-Fluoroblphenyl
79.7
22.0-127
(S) p- Terphenyl-dM
89.0
29.0-141
_.
_
_
a
Cn
(S)Phenol-d5
32.0
8.00-424
/SJ 2-Fluorophenol
44.6
10.0120
(S) 2,4,6-Tobromophenol
89.5
10.0.153
Fri
L1176235-01 Original Sample (OS) • Matrix Spike (MS) • Matrix
Spike Duplicate (MSD)
(OS) L1176235-01 01/07/20 02:18 - (MS) R3488555-1 01/07/20 02:40
- (MSD) R3488555-2
01/07/20 03:02
zGl
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec
Dilution
Rec Limits
ME Qualifier
MSD Qualifier
RPD
RPD Limits
Analyte mg4
mgn
mgll
mg4
%
%
%
%
%
13is(2-chlorethoxy)methane 0.0500
U
0.0378
0.0511
75.6
102
10
33.0-184
29.9
54
AI
Bs-(2-chloroethyl)ether 0.0500
U
0.0373
6.6418
74:6
83.6
10
12.0-158
HA
i08
Bisl2-chloraisopropyoether 0.0500
U
0.0823
0.0914
165
183
10
36.0-166
JS
10.5
76
4-Bromophenyl-phenylether 0.0500
U
0.0426
0.0446
85.2
89.2
10
53.0-127
4,59
43
SC
4-Chlorophenyl-phenylether 0,0500
U
0.0376
0.0422
75.2
84.4
10
25.0-158
its
61
.3,3-Dichlorobenzidine 0.100
U,
NO
ND
0.000
0.000
10
1.00-262
J6
J6
0.000
108
2,4-Dlnitrotoluene 0,0500
U
0.0420
0.0427
84.0
85.4
10
39.0-139
1.65
42
2,6-Dinitrotoluene 0.0500
U
NO
0.0413
0.000
82.6
10
50.0-158
J6
J3
200
48
Hexachloro-1.3-butadiene 0,0500
U
0.0381
0.0575
76.2
115
10
24.0-120
40.6
62
Hexachlorocyclopentadiene 0.0500
U
NO
NO
0.000
0.000
10
10.0-146
J6
J6
0.000
34
Hexachlorcethane 0.0500
U
0.0314
0.0346
62.8
69.2
10
40.0-120
9,70
52
Isophorone 0,0500
U
0.0354
6.0849
76.8
170
10
21.0-196
82.3
93
Nitrobenzene 0.0500
U
0.0711
0.0994
142
199
10
35.0-180
J5
33.2
62
n-Nitrosodiphenylamine 0,0500
U
D.0406
0.0451
K2
90.2
10
16.0-160
10.5
28
n-Nitrosodi-n-propylamine 0.0500
U
0.0483
0.155
96.6
310
i0
1.00-230
J3 J5
105
87
Benzylbulyl phthalate 0.0500
U
0.0534
0.0482
107
96.4
1D
1.00-152
10.2
60
Bisl2-ethylhexyl)phthalate 0.0500
U
0.0434
0.0431
86.8
86.2
10
8.00-158
0.694
82
Di-n-butyl phthalate 0.0500
U
0,0409
0.0421
819
84.2
10
00-120
2.89
47
Diethyl phthalate 0.0500
U
0.0376
0,0385
75.2
T7.0
10
1,00-120
2.37
100
Dimethyl phthalate 0.0500
U
0.0352
0.0374
70.4
74.8
10
1.00-120
6.06
183
Di-n-ocy phthalate CD500
U
0.0484
0.0481
96.8
96.2
10
400-146
0,622
69
4-Chloro-3-methylphenol 0.0500
U
0.00842
6.0130
16.8
26.6
10
22.0-147
J6
421
73-
2-Chlorophenol 0.0500
U
0.00687
0.00779
13.7
15.6
10
23.0-134
J6
J6
12.4
61
2,4-Dichlorophenol 0.0500
U
0.00338
0.00500.'
6.76
10.0
10
39.0-135
J6.
J6
367
50
2,4-Dimethylphenol 0.0500
U
0.00751
0.0129
15.0
25.8
10
32.0-120
J6
J6
52.8
58
4,6-Dinitro-2-methylphenol 0.0500
U.
0.0909
0.0902
182
180
10
1.00-181
J5
0373
203
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton. Corporation 28091-R L11]6249 01/10/20 11:39 19 of 23
WG1406113
QUALITY
CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic
Compounds
(GCrMS) by
Method 625.1
L1176249-01
L1176235-01 Original Sample
(OS) • Matrix
Spike (MS) • Matrix
Spike Duplicate
(MSD)
(OS) L1176235-01 01/07/20 02,18 • (MS) R3488555-1 01/07/20 02:40
• (MSD) R3488555-2
01/07/20 03:02
CS'
Spike Amount
Original Result
MS Result
MSD Result MS Rec.
MSD Rec.
Dilution Red. Limits
MS Oualifier
MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
%
%
TC
24-6initrophenol
0.0500
U
0.0554
0.0935
191
187
70
1.00-i91
2.01
132 v
2-Nitrophenol
0.0500
0.557
0.345
0.508
0.000
0.000
10
29.0-182
V
V 38.2
55
s
4-Nltrophenol
0.0500
0.321
0.285
0.302
0000
0000
10
t00-132
V
V 579
131
SS
Pentachlorophenol
0.0500
U
0.0499
0.0545
99.8
109
10
14.0-176
8.8i
86
Phenol
0.0500
U
0.0575
0.0765
50.0
88.0
10
5,00-120
23.4
64
4
Cn
Acenaphmene
0,0500
U
0,0359
0,0386
71.8
77.2
10
47.0-145
7,25
48
2,46-Trichlorophenol
0,0500
U
0.0345
0.0411
69.0
822
10
320-144
173
58
s
Acendph[h)'lene
0.0500
U
0.0679
0.0223
35.8
44.6
10
33.0-i45
21.9
74
Sr
Anthracene
0.0500
U
0.0341
0,0369
68.2
73.8
io
27.0-133
7.89
66
Benzidine
0.100
U
NO
ND
0.000
0.000
i0
1.00-120
J6
J6 0.000
4C
Benzo(a)anihracene
0.0500
U
0.0387
0,0405
774
81.0
10
33.0-i43
455
53
Benzo(b)fluoranthene
0.0500
U
0.0399
0.0438
79-8
87.6
10
24.0-i59
932
71
7Gl
1,2-Diphenylhydrazine
0,0500
U
0.0524
0.0492
105
984
i0
18.0-156
6.30
�4
Benzo(k)fluoranthene
0,0500
U
0,0375
0.0404
75.0
80.8
10
11.0-162
745
63
Benzcrd,h,i)perylene
0,0500
J
0,0385
0.0400
77.0
80.0
10
1,00-219
3.82
97
A
Benzo(a)pyrene
0.0500
U
0.037i
0.0410
74.2
82.0
i0
17.0-163
9,99
72
2-Chloronaphthalene
0,0500
U
00383
0.0407
76.6
31.4
i0
60.0120
6.08
24
CSC
Chrysene
0,0500
U
0,0403
0.0412
80.6
82A
10
17.0-165
2.21
87
Dibenz(a,h)anthracene.
0.0500
U
0.0408
0.0416
81.6
83.2
10
1.00-227
1,94
126
Fluoranthene
0.0500
U
0.0370
0.0406
740
61.2
10
26.0-137
9.28
66
Fluorene
0.0500
U
00378
0.0399
75.6
79.8
10
59.0-121
541
38
Hexachlorobenzene
0.0500
U
0.0469
0.0438
93.9
87.6
10
1.00-152
6.84
55
Indemo(1,2,3-cd)pi
0.050C
J
0.0423
0.0452
84.6
904
i0
i.00-171
6.63
99
Naphthalene
0.0500
U
0,0323
0,0453
64.6
9(1
10
21.0-133
33.5
6E
n-Nitrosodimethylamine
0.0500
U
0.0918
0101
20.2
38.6
10
10.0-120
9.54
40
Phenanthrene
0.0500
U
0.0386
0.0417
77.2
83.4
10
54.0-120
7.72
39
Pyrene
0.0500
U
0.0434
0.0455
86 8
91.0
10
52.0-120
472
49
1,2,4-Trichlorobenzene
0.0500
U
0,0296
0,0433
59.2
86.5
10
44.0142
37.6
Sc
(S Nihobenzene-d5
108
195
15.0-?c4
(S 2-Fluterobiphenyl
76.1
85.2
22.0-727
(S) p-Terphenyl-d74
26 6
106
25.0-141
(S)Phenol-d5
0,000
0.000
8.00-424
J2
J2
(S)2-Fluoropheno7
0,000
0000
10.0-120
J2
J2
(S)Z,1,6-Tnbromophenal
HE
4Z3
700-153
Sample Narrative:
OS. Dilution due to matrix. Surrogate failure due
to matrix interference,
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Eaton
Corporation
28091-R
L1176249
01/10/2011:39
20 of 23
GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. $
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer- Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
No
Not detected at the Reporting Limit (or MDL where applicable).
ROL
Reported Detection Limit.
Rec.
Recovery,
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard)- Analytes added to every blank, sample, Laboratory Can Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
;Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or %difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND' (Not Detected) or "BDL"
Result
(Below DetectableLevels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
.Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (So)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
(Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyze is acceptable; the reported value is an estimate.
J2
Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high. -
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
:P
RED between the primary and confirmatory analysis exceeded 40%.
v
The sample concentration is too high to evaluate accurate spike recoveries.
'Cp
RC
ass
4Cn
aSr
aQC
aAl
9Sc
ACCOUNT:. PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1176249 01/10/20 It:39 21of23
ACCREDITATIONS & LOCATIONS ONE LAB, NATIONWIDE,
Pace National is the only environmental laboratoryaccoss ited/certihed to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most signIDcant benefit to our one location design Is the design of our laboratory campus. The Total Is conducive to accelerated productivity decreasing
turnaround time, and preventing cross contamination, thus protecting sample integrity. Our focus an premium quality and prompt service allows us to be YOUR LAB OF CHOICE-
' Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is onlyapplicable to the test methods specified on each scope ofacnedilation held by Pace National.
State Accreditations
Alabama
40660
Nebraska
NE-0545-05
Alaska
77-026
Nevada
TN-03-200-34
Arizona
A20612
Nov, Hampshire
2975
Arkansas
88 0469
New Jersey-NELAP
TNO02
California
2932
New Mexico'
Colorado
TN00003
New York
117 11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
Hands Dakota
R-140
Idaho
TN00003
OhioVARCLOO69
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode island
LA000356
Kentucky's
90010
Sou1h Carolina
84004
Kentucky'
..
16
South Dakota
We
Louisiana
AI30792
_..
Tennessee 1°
2006
Louisiana'
LA180010
Texas
T104704245-18-15
Maine
TN0002
Texas'
LAB0152
Maryland _
324
Utah
TN00003
Massachusetts
M-TNO03
Vermont
VY2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
Clio
MBsissippl
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
_
Wyoming
A21-A
Third Party Federal Accreditations
A2LA - 150 17025
146T01
AIHA LAP,LLC EMLAP
100789
A2LA-ISO 17025°
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15 00234
EPA-Crypto
TN00003
'drinking Water ° Underground Storage Tanks
' Aquatic Toxicity 4 Chemical/Microbiological
`Mold a Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers
that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office Pace National performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Eaton Corporation 28091-R L1176249 0111012011:39 22 of 23
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