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HomeMy WebLinkAboutNCG030027_MONITORING INFO_20200122T " STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. �jCG D3b0a'-7 DOC TYPE ❑ HISTORICAL FILE C MONITORING REPORTS D / a DOC DATE ❑ YYYYM M D D Um'T*N January 13, 2020 Colin W. Betchan Environmental, Health & Safety Supervisor (919) 702-3703 (mobile) (336) 503-6562 (fax) co l i nwbetch a n (a'Deaton. co m Division of Water Quality RECEIVED 1617 Mail Service Center JAN 2 Raleigh, North Carolina 27699-1617 2 2020 CENTRAL FILES Attn: DWQ Central Files DWR SECTIOP! RE: January 2020 Monthly Tier III Discharge Monitoring Report Attached are the analytical results and associated chain of custody for the January 3, 2020, monthly Tier III stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility. Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North Carolina Division of Water Quality (NCDWQ). The chain of custody lists rainfall as 0.24 inches, at the time of sample shipment to the laboratory. The total rainfall for the rain event was 0.96 inches. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with the system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or other persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Sincerely, y �j�' W—^� �lM�/�%%� Colin W. Betchan EHS Supervisor Attachments Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted 01/13/2020 CERTIFICATE OF COVERAGE NO. NCG03 o 0 2 7 FACILITYNAME Eaton Corporation COUNTY Person County PERSON COLLECTING SAMPLES Colin Betchan LabCert.q ENV375/OW217041aI[ 1.���\/�I r Comments on sample collection or analysis: mr IAN 2 2 N11 LABORATORY Pace National CENTRAL. FILE` Part A: Stormwater Benchmarks and Monitoring Results LWR �drCT10 SAMPLE COLLECTION YEAR 2020 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or E] Monthly' January (month) DISCHARGING TO CLASS ❑ORW ❑HC!W ❑Trout ❑PNA ❑Zero -flow [:]Watersupply [:]SA *Other WS-Ill: NSW PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks _ - 100 mg/L or 50 mg/0 6.0— 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 Tool Room Trench (005) 01/03/2020 0.96 17.4 8.4 0.0110 0.00288 0.0277 0.806 0.035395 / �, ,^r rt^ � _r•� r\ ^.Ivy . 1 1 -i -> l Monthly sampling (instead of semi-annual) musi,begin'with'the second consecutive benchmark exceedahce'for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Colin Betchan Name (Print name) EHS Supervisor Title (Print title) 64 hX_af 1113 aodo Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n Nn rlicrhnrnc Chic norinn02 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO 0 IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑ REGIONAL OFFICE CONTACT NAME: Danny Smuh Mail an original copv of this DMR, including all "No Discharqe" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee - Da` 1 Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 3 of 3 aceAnr ical® ANALYTICAL REPORT NaVonal Center for Testing a lnnave0on January 10, 2020 Eaton Corporation Sample Delivery Group: Samples Received: Project Number: Description: Site: L1176249 01/04/2020 28091-R Eaton Corp Monthly Stormwater ROXBORO,NC Report To: Dustin LaClair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Eaton Corporation 28091-R L1176249 0IM012011:39 1 of 23 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cl): Cover Page 1 Tc: Table of Contents 2 Cp Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 3S5 2020-01-03-005 L1176249-01 5 4Cn Oc: Quality Control Summary g Gravimetric Analysis by Method 2540 D-2011 8 SSr Wet Chemistry by Method 1664B g Metals (ICP) by Method 200.7 t0 C Volatile Organic Compounds (GC/MS) by Method 624.1 11 Pesticides (GC) by Method EPA 608.3 13 GI Polychlorinated Biphenyls (GC) by Method EPA-608.3 15 JAI Semi Volatile Organic Compounds (GC/MS) by Method 625.1 16 GI: Glossary of Terms 21 9Sc Al: Accreditations & Locations 22 Sc: Sample Chain of Custody 23 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE. Eamn Corporation 28091-R L1176249 01110201139 2 of 23 SAMPLE SUMMARY ONE LAB. NATIONWIDE. 1, Collected by Collected dateAime Received date/time 2020-01-03-005 L1176249-01 WW Colin Betchan 01103/2015:07 01/04/2008:30 Cp Method Batch Dilution Preparation Analysis Analyst Location datedime datedime ETC Gravimetric Analysis by Method 25400-2011 WG1406805 1 01/0712010:22 01/0712011:36 MMF Mt. Juliet, TN Wet Chemistry by Method 1664E WG1408114 1 01/08/2017AS 01109/2008:45 AMG Mt. Juliet, IN Metals (ICP( by Method 200.7 WG1406598 1 01/06/2018:27 01/07/20 03:08 TRB Mt. Juliet, TN Volatile Organic Compounds(GC/MS( by Method 624.1 WG1406126 1 0110512000:05 01/05/2000:05 BMB Mt. Juliet, TN Pesticides(GC) by Method EPA 608.3 WG1406117 1 0110512008:18 01/0612013:51 LEL Mt. Juliet, TN ° Cn Polychlorinated Biphenyls(GC) by Method EPA-608.3 WG1406117 1 01/05/2008:18 01/OSI2019:45 RP Mi. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1406113 1 01/05/20 08:02 01/05/20 20:48 AO Mt. Juliet, TN s Sr o�C 7G1 aAl 9Sc ACCOUNT: PROJECT: SDG: DATErNME: PAGE: �3 Eaton Corporation 28091-R L1176249 01/10/2011:39 3 of 23 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the Cp appropriate preservatives, and within method specified holding times, unless qualified of notated within the report. Where applicable, all MDL (LOD) and RDL (LOO) values reported for environmental samples �TC have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this Case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of mY 3Ss knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. SSr 5QC [GI Heather J Wagner Project Manager AI 9Sc ACCOUNT: PROJECT: SDG: DATEMME' PAGE: Eaton Cornoralion 28091-R L1176249 01/10/2011'.39 4 of 23 020-01-03-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Ilected datoltlme: 01103120 15:07 L1176249 Additional Information Result Units Cp Analyte z pH (On Site) 8.4 su TC Temperatuie(on-sile) 11.7 DegC aSs Gravimetric Analysis by Method 2540 D-2011 Result Oualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Cn Suspended Solids 174 0.539 3.85 1 01/07/20201136 WG1406805 Wet Chemistry by Method 1664B 6 QC Result Oualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mgll date/time TPH -Oil&Grease U 0.806 5.56 1 01/09/202008:45 WG1408114 Gl Metals (ICP) by Method 200.7 a Result Oualifier MDL RDL Dilution Analysis Batch AI Anzlyte mgll mg/I mg/I date/time 9 Copper 0.0110 0,00700 MIMI 1 01/07/202003:08 WG1406598 SC Lead 0.00288 1 0.06200 - 0.00500 1 01/67/202003:08 WG1406598 u Zinc 0.0277 J 0.00340 0.0500 1 01/07/2020 03:08 WG1406598 Volatile Organic Compounds (GC/MS) by Method 624.1 Analyte Result mgh Oualifief MDL mg/I RDL mgll Dilution Analysis date/time Batch Acrolein U 000887 0.0500 1 01/05/202000:05 WG1406126 Acrylonitrile U 0.00187 0.0100 1 01/05/202000:05 WG1406126 Benzene U 0.000331 0.00100 1 01/051202000:05 WG1406126 Sroinodichloromethane U 0000380 0.00100 1 01/05/202000.05 WG1406126 Bromoform U 0.000469 0,00100 1 01/05/2020 00:05 WG1406126 Broinomethane U 0.000866 000500 1 01105/202000:05 WG1406126 Carbon tetrachloride U 0.000379 0.00100 1 01/05/202000:05 WG1406126 'Chlombenzene U 0000348 0.00100 1 01105/202000:05 WG1406126 o Chlorotlibromomethane U 0.000327 0.00100 1 07/05I202000:05 WG1406126 Chlaroethane U 0.000453 0.00500 1 01165/202000:05 WG1406126 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 011051202000:05 WG1406126 Chloroform U 0.006324 0.00500 1 01/05/202000:05 WG1406126 a Chloromethane U 0.000276 0.00250 1 01105I2020 00:05 WG1406126 1.2-13ichlorobenzene U 0.000349 0.00106 1 01105/202000:05 WG1406126 1,3-Dichlorobenzene U 0.000220 0.00100 1 01/05/202000:05 WG1406126 1,4-Dichlorobenzene U 0.000274 0.00100 1 01/05/202000:05 WG1406126 Dichlorodifluoromethane U 0.000551 0,00500 1 01105/202000:05 WG1406126 11-6lchloroethane U 0.000259 0.00100 1 01/05/202000:05 WG1406126 1,2-Dichloroethane U 0.000361 0,00100 1 01/05/202000:05 WG1406126 '1,1-61'chloroethene U 0.600398 0.00100 1 01/05/202000:05 WG1406126 , r trans-1,2-Dlchloroethene U 0.000396 0.00100 1 01/05/202000:05 WG1406126 1,2-Dichloropropene U 0.000306 000100 1 01/05/202000:05 WG1406126 cis-1,3-Dichloropropene U 0.000418 0.00100 1 01105002000:05 WG1406126 trans-1,3-Dichloropropene U 0.000419 O.00l00 1 01/6S/202000:05 WG1406126 Ethylbenzene U 0000384 0,00100 1 01/05/2020 00:05 WG1406126 Methylene Chloride U 0.00160 0.00500 1 01/05/202600:05 WG1406126 1,1,2,2-Tetrachloroethane U 0.000130 000100 1 01105f202000:05 WG1406126 Telrachloroemone U 0.00o372 0.00100 1 01/05/202000:65 WG1406126 Toluene U 0000412 0.00100 1 01/05/202000:05 WG1406126 4,1,1-Trichloroethane U 0.000319 0.00100 1 01/05/202000:05 WG1406126 n 1,1,2-Trichloroethane U 0.000383 0.00100 1 011051202000:05 WG1406126 i ACCOUNT PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R Ln76249 Ot/1020 11:39 5 of 23 2020-01-03-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dateltlme: 01/03/20 15:07 L1176249 Volatile Organic Compounds (GC/MS) by Method 624.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyze mg/1 n1g/l mg/I date/time Lichloroethene U 0.000398 0,00100 1 OV05/202000:05 WG1406126 Inchlorofluoromethane U 0.00120 0.00500 1 01/05/202000.05 WG1406126 Vinyl chloride U 0,000259 0,00100 1 OV05/202000:05 WG1406126 (27oluene cig 101 80.0-120 011051202000: 05 WG1406126 (5)4-13romolluorobenzene 953 80.0-120 01705120200005 WG1406126 (5) 12 Oichloroethone-64 101 70G-130 0V05202000.05 W61406126 Pesticides (GC) by Method EPA 608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ni trgh mind date/lime Nddn U 0.00000813 0.0000500 1 01/06/202013:51 WG1406117 Alpha BHC U 0.0000166 0.0000500 1 01/06/202013:51 WG1406117 Beta BHC U 0.0000184 0D000500 1 01/06/202013:51 WG1406117 Delta BHC U 0.0000197 0.0000500 1 01/06/202013:51 WG1406117 Gamma BHC U 0,0000176 0.0000500 1 01/06/202013:51 WG1406117 Chlordane U 0.0000977 0.000500 1 01/06/202013,51 WG1406117 44-DDD U 0.0000170 0,0000500 1 01/06/202013:51 tYG1406117 4,4-DDi U 0.0000164 0.0000500 1 011061202013:51 WG1406117 4,4-DOT U 0.0000177 0.0000500 1 01/06/202013:51 WG1406117 Deland U 0,00000751 0.0000500 1 011061202013,51 WG1406117 Endosulfan I U 0.0000179 0.0000500 1 011061202013:51 WG1406117 Endosulfan II U 0.0000176 0,0000500 1 01/06/202013:51 WG1406117 Endosulfan sulfate U 0,0000196 0.0000500 1 OV06/2020 i3:51 WG1406117 Endrin U 0.0000189 0.0000500 1 01/06/202013:51 WG1406117 Enddn aldehyde U 0.0000142 0.0000500 1 01/06/202013:51 WG1406117 Endrm ketone U 0.0000170 0,0000500 1 01/06/202013:51 WG1406117 Heptachlor U 0.0000108 0.0000500 1 011061202013:51 LVG1406117 Heptachlorepoxide U 0.0000175 GD000500 1 01/06/202013:51 WG1406117 lexachloiobenzene U J3 0.0000134 0.0000500 1 01/06/202013:51 WG1406117 Methoxychlor U 0.0000193 0,0000500 1 01/06/202013:51 WG1406117 Toxaphene U 0000168 0,000500 1 01106/202013:51 WG1406117 (5) Decochloroblphcnyl 76.1 70.0-144 011061202013,51 WG1406117 (S Tehachloro-m xylene 676 10.0-135 011061202013,51 WG1406117 Polychlorinated Biphenyls (GC) by Method EPA-608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/1 date/time PCB 1016 U 0,000100 0.000500 1 01/05/202019:45 WG1406117 PCB 1221 U 0.0000730 0.000500 1 011051202019:45 WG1406117 PCB 1232 U 0.0000420 0.000500 1 01105/202019:45 WG1406117 PCB 1242 U 0.0000470 0.000500 1 01/05/202019,45 WG1406117 BOB 1248 U 0,0000860 0.000500 1 01/05/202019:45 WG1406117 PCB 1254 U 0,0000470 0,000500 1 OIJ05/202019:45 WG1406117 PCB 1260 U 0.000120 0.000500 1 01/05/202019:45 WG1406117 (S)Decochloroblphenyl 78.6 10.0744 071051202019.45 W61406117 (STesochloro-nr-xylene 72.4 10.0-135 011051202019,45 WG1406117 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyse mg/1 ri mglt date/time Acenaphnene U 0.000316 0.00100 1 01/05/2020 20:48 WG1406113 Aceniphthylene U 0-000309 0.00100 1 01/05/2020 2048. WG1406113 Anthracene U 0.00029i 0.00100 1 01/05/2020 20:48 WG1406113 Benzidine U 000432 0.0100 1 01/05/2020 20:48 WG1406113 Benzo(a)anlhiacene U 0.0000975 0,00100 1 01/05/2020 20:48 WG1406113 ACCOUNT: PROJECTSDG: DATEITIME: PAGE. Eaton Corporation 28091-R L1176249 01/10/2011:39 6 of 23 2020-01-03-005 SAMPLE RESULTS - 01 Collected date/lime: 01/03/20 15:07 L1176249 11 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MOIL ROL Dilution Analysis Batch Analyte mg4 mg/I mgll date/lime ONE LAB. NATIONWIDE. M Benzo(b(fluoranthene U 0.0000996 0.00100 1 01/05202020:48 WG1406113 Benzo(k)fluonnthenc U 0.000355 0.00100 1 01/05/202020:48 WG7406113 Benzo(g,h,1)pegene U 0.000161 0.00100 1 01/051202020:48 WG1406113 Benzo(alpyrene U 0.000340 0.00100 1 01/05/2020 20:48 WG1406113 Bls(2-chlorethoxylmethane U 0.000329 0.0100 1 01/05/2020 20:48 WG1406113 Bis(2-chloroethyl)ether U 0.00162 0.0100 1 01/05/2020 20:48 WG1406113 Bus(2-chloroisopropypethei U 0.000445 0,0100 1 61/05/202020:48 W61406113 4-Bromophenyl-phenylether U 0.000335 0.0100 1 01/05/2020 20:48 WG1406113 2FChloronaphthalene U 0.000330 0.00100 1 01/05/2020 20:48 WG1406113 4=Chlorophenyl-phenylether U 0.000303 0.0100 1 01/05/2020 20:48 WG1406113 ,Chrysene rr U 0,000332 0.00100 1 01/0512020 20:48 WG1406113 Aenz(a,h)anthracene U 0.000279 0.00100 1 01/052020 20:48 WG1406113 -3;3-Dichlorohenzidine U 0.00202 0.0100 1 01/05/202020:48 WG1406113 2,4-Dinitrololuene U 0.60165 0,0100 1 01/05/202020:48 WG1406113 26-Dinitrotoluene U 0.060279 0.0100 1 01/056020 20:48 WG1406113 0 1,2-Diphenylhydrazine U 0.000318 0.0100 1 01105/202020*48 WG1406113 Fluoranlhene U 0.060310 0.06160 1 _ 01/05202020:48 WGU06113 ' Fluoiene, U 0000323 0.00100 1 01/05/2020 20:48 WG1406113 Hexachlorobenzene U 0.000341 0.00100 1 O1/05/2020 20:48 WG1406113 Hexachloro-13-butadiene U 0.000329 0.0100 1 01/05/2020 20:48 WG1406113 Hexachlorocyclopentadiene ;r U 0.00233 6.6160 1 01I05/202026:48 WG140616 Hexachloroethane U 0.000365 0.0100 1 01/05/2020 20:48 WG1406113 Indeno(1,2,3td)pyrene U 0.0002A 0.00100 1 01/051202020:48 WG1406113 Isophorone U 0.060272 0.0100 1 01/65/2020 20:48 WG1406113 iNaphthalene U 0.000372 0.00100 1 01/0512620 20:48 WG1406113 Nitrobenzene U 0.000367 0.0100 1 01/05/2020 20:48 WG1406113 n-Nitrosodimethylamine U 0.00126 0.0100 1 01/05/202026:48 WG1406113 n-Nitrosodiphenylamine U 0.00119 0.0100 1 01105/20202048 WG1406113 .n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 01/05/20202048 WG1406113 Phenanthrene U 0.000366 0,00100 1 01/05/202020:48 WG1406113 Benzylbutyl phthalate U 0.000275 0.00300 1 01I0512020 2048 WG1406113Bis(2-ethylhexyllphthalate 0.00107 J 0.0 0070 9 0.003100 1 01/05/202020*48 WG1406113 Di-n-butyl phthalate 0.000360 J 0,000266 0.00300 1 01/05/2020 20:48 WG140616 Diethyl phthalate U 0000282 0.00300 1 01/65/202020:48 WG1406113 Dimethyl phthalate U 0.000283 0.00300 1 01/05/202020:48 WG1406113 . Di-n-octyl phthalate U 0.006278 0.00300 1 01105/202020:48 WG1406113 Pyrene U 0.006330 0.00100 1 01/05/202020:48 WG1406113 1,2,4-Trichlorobenzene U 0.000355 0.0100 1 01/051202020:49 WG1406113 4-Chloro-3-melhylphenol U 0.000263 0.0106 1 01/05/202020:48 WG1406113 2-Chlorophenol U 0.000283 0.0100 1 01JOW2020 20:48 WG1406113 2,4-Dichlarophenol U 0.006284 0.0100 1 01/05/2020 20:48 WG1406113 2,4-Dimethylphenol U 0,000624 0,0100 1 01/05/202020:48 WG1406113 4,6-Dinitro-2-melhylphenol U 0.00262 0.0100 1 01105/202020:48 WG1406113 2,4-Dinihophenol U 0.00325 0.0100 1 01105/202020:48 WG1406113 2-Nitrophenol U OM0320 0.0100 1 01/051202020:48 WG1406113 4-Nitrophenol U 0.00201 0.0100 1 01/05/202020:48 WG1406113 Pentachlorophenol U 0.006313 0,0100 1 01/056020 20:48 WG1406113 Phenol 0.00170 J 0.000334 0.0100 1 011051202020:48 WG1406113 2,4,6-Trichlorophenol U 0.060.297 0.0100 1 01/05/2020 20 48 WG1406113 (92-Fluorophenol 35.1 10.0-120 011051202020:48 WG1406113 (Sfrphenol-d5 25.4 8.60-424 01105/202020:48 WG1406113 (S) Nitrobenzene-d5 58.3 15.0-314 011051202020:48 WG1406113 (Sj2-Fluorobiphenyl 74.8 22.0-127 01165120202048 WG1406113 (5)24,6-Tfibromopheno) 60.5 10.0-153 01105120202OA8 WG1406113 (SJp-Terphenyl-M 90.4 29.0-141 OY651202020.48 WG1406113 } ACCOUNT: PROJECT: SDG: DATE/TIME: Eaton Corporation 28091-R L1176249 0111012011:39 PAGE: 7 of 23 WG1406805 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Gravlmetric Analysis by Method 2540 D-2011 L1176249-01 Method Blank (MB) (MB) R3468975-1 01/07/20 11.36 C p MB Result MB Qualifier PAB MDL ME RDL Analyte mg/I mg/I mg/I �.. _._�... _.__. Suspended Solids U 0 �50 2.50 ' TC L1176248-01 Original Sample (OS) • Duplicate (DUP) (UD) Lll/b24d-Ul Ul/U//ZU T:36 • (UUP) R3488975-3 01/07/2011:36 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Suspended Solids 315 316 1 0422 5 Laboratory Control Sample (LCS) (Li-J) ttS4Cby/b-L UVU112U 11: b Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyze me/I mg/I % % ____ _—_____ ___- _____ ------ Suspended Solltls 773 768 99 4 85.0-__ii" 3Ss r1 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE' Eaton Corporation 28091-R L1176249 01/10/201139 8 of 23 WG1408114 QUALITY CONTROL_ SUMMARY ONELAB.NATIONVADE Method Blank (MB) Cp (MB) P3489203-1 OV09/20 08:45 MB Result MB Qualifier MB MDL MB ROL Analyte n TPH - Oil& Grease U mg/I mgfl 0.725 5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3489203-2 01/09/20 08:45 - (LCSD) R3489203-3 01/09/20 08:45 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mgll TO mgli % % % % % TPH - Oil 8 Grease 20.0 1T5 18.7 ST5 93.5 64.0-132 6.63 34 ACCOUNT: - PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1176249 01/1012011:39 9 of 23 WG1406598 QUALITY CONTROL SUMMARY ONELAB.NATIONWIDE. Metals (ICP) by Method 200.7 L1176249-01 Method Blank (MB) (MB) R3488512-1 01/07/20 0218 Cp M8 Result MB Qualifier MB MOLL MB ROL Analyte mg/I mg/I mg/I Copper U 0.00700 -_ __. __- -_ -- - -_ _ 0.0100 _TC - -- Lead U 0.00200 0,00500 3 Zinc U 0.00340 O0500 SS Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (Lcb) R3488512-2 01/07/20 02:21 - (LCSD) R3488512-3 01/07/20 02:23 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Oualifier LCSD Oualifier RPD RPD Limits Analyze mg ri mg,l % % % % % Copper 1.00 0.967 .________._______________. 0.966 96.7 _..______________. 96.6 850-115 ___________.___.______________.__. _____. 0.117 ________ _____-- 20 Lead 1.00 0.972 0.968 97.2 96.8 250-115 0.394 20 Zinc 1.00 0.971 0.970 971 97D 850-LS 0.0824 20 L1176239-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (0S) 1-1176239-01 01/07/20 02:26 • (MS) P3488512-5 01/07/20 02:31 • (MSD) R3488512-6 01/07/20 0234 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Oualifier RPD Analyte mg/I mg/I _ mg/I mg/I % % % % Copper 1.00 ND 0.968 0.977 �95.& 97.7 70.0-130-�_--� - _ -� 0.996 Lead iDo ND 0.971 0.984 97.1 98A 1 700-130 1.34 Zinc 1.00 NO 1.01 1.02 96.1 97.5 1 70.0-130 144 L1176416-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) RPD Limits os -20 -- 20 20 (Us) Lll/64lb-01 O1/07/20 02:36 • (MS) R3488512-7 01/07/20 02:39 • (MSD) R3488512-8 01/07/20 0241 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec Limits MS Qualifier MSD Oualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Copper 1.00 NO 0.968 0.963 96.8 96.3 1 70.0-130 0.596 20 Lead 1.00 ND 0.974 0.965 974 96.5 1 70.0-130 0.980 20 Zinc i.00 ND 0971 0.961 971 96.i 1 70.0-130 0.984 20 ACCOUNT: PROJECT: EDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1176249 01/10/201139 10 of 23 WG1406126 QUALITY CONTROL SUMMARY_ ONE LAB. NATIONWIDE. =�VolatlleorganlNCompounds=(GC/MS)-by:MetK'6d 624.1 Method Blank (MB) Cp (MB) R3488076-2 01/04/20 21:21 MB Result MB Qualifier MB MDL MB RDL Anah¢e mg/I mg4 mg/I FC Acrotein U 0.00887 0.0500 a$5 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 Bromodichloromethane U 0.000380 0.00100 4 Bromoform U 0.000469 0.00100 Cn Bromomethane U 0.000866 0.00500 s Carbon tetrachloride U 0.000379 0,00100 Sr Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 _ ..... 2-Chloroethyl vinyl ether U 0.00301 0.0500 7GI Chloroform U 0.000324 0.00500 Chloromethane U 0,000276 0.00250 1,2-Dichlorobenzene U 0.000349 0.00100 " VAS 13-Dichlorobenzene U 0,000220 0.00100 14-Dichlorobenzene U 0.000274 MOW a Dichlorodifluoromethane U 0.000551 0.00500 SC 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1.2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 - Emylbenzene U 0.000384 0.00100 Methylene Chloride U 0.00100 0.00500 71,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000412 0.00100 1,1,1-Trtchloroethane U OT00319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0,00100 _ - Trichlofofluoromethane U 0.00120 0.00500 Vinyl chloride U 0000259 0,00100 (S) Toluene-d8 101 80.0-120 (S)4-Bromofluorobenzena 101 80.4110 - (S)12-Dichloroethane-d4 103 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton. Corporation 28091-R L1176249 01/10/2011:39: 11 of 23 WG1406126 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624A L1176249-01 Laboratory Control Sample (LCS) (LCS) R3488076-1 01/04/20 2040 Spike Amount LCS Result LCS Rec. Rec. Limits Analyze mg/l mg/I % % Acrolein 0,0250 0.0351 140 60.0-140 Acrylomaile 0.0250 00257 ion 50.0-i40 Benzene 0.00500 000494 98.8 65.0-135 Bra modich hap methane 0,00500 000518 104 70.0135 Bromororm 0.00500 000531 106 70.0-130 Bromomethane 0,00500 0.00503 i01 15.0-185 Carbon tetrachloride 0-00500 0.00570 114 70.0-130 Chlorobenzene 0.00500 0.00485 970 65.0-135 Chlorodibromomethane 0,00500 0.00488 97.6 70.0-135 Chloroethane 0.00500 0.00462 924 40.0-160 2-Chloroethyl vinyl ether 0.0250 0,0252 101 0 100-225 Chloroform 0.00500 0.00524 105 70.0-135 Chloromethane 0.00500 000437 874 0.100-205 1,2-Dichlorobenzene 0,00500 0,00498 99.6 65.0-135 1,3-Dichlorobenzene 0.00500 0,00467 934 70.0-120 1,4-Dichlorobenzene 0.00500 0.00495 99.0 65.0-135 Dichlorodinuoromethane 0.00500 0.00527 i0 49.0-155 1,1-Dichloroethane 0.00500 0.00497 99.4 70.0-130 1.2-Dichloroethane 0.00500 0.00541 109 70.0-130 i.i-Dichloroethene 0.00500 0.00524 i05 50.0-i50 trans-1,2-Dichloroethene 0.00500 0.00514 103 70.0-130 1.2-Dichloropropane 0.00500 0.00458 91.6 35.0-165 cis-1,3-Dichloropropene 0.00500 0.00523 105 25.0-175 trans-1,3-Dichloropropene 0.00500 0.00512 102 50.0-150 Ethylbenzene 0,00500 0,00515 103 60.0-140 Methylene Chloride 0.00500 000490 98.0 60.0.140 1,1,2,2-Tetrachloroethane 0.00500 000415 930 60-0-140 Tetrachloroethene 0.00500 000520 iO4 70.0-130 Toluene 0.00500 000475 95.0 70.0-130 1,U-Trichloroethane 0.00500 0.00567 113 70.0-130 11,2-Trichloroethane 0.00500 0,00506 101 70.0-130 Trichloroethene 0.00500 0,00524 105 65.0-135 Tnchlorofluoromethane 0,00500 0,00599 120 5D.0-150 Vinyl chloride 0.00500 0.00496 99.2 5.00-i95 (5)Toluene-d8 98.4 80.0-120 (5) 4-Bromalluorobenzene 101 80.0-120 (5)1,2-Dichloroelhone-d4 105 70.0-130 LCS 0ualifier ACCOUNT: Eaton Corporation PROJECT: 28091-R BOG: DATE/TIME L1176249 01/10/20 1139 PAGE: 12 of 23 WG1406117 QUALITY CONTROL SUMMARYONE LAB. NATIONWIDE _.- __T-pesticitles.(GC)-by'M ethotl'EPA'608`3 �-- - Method Blank (MB) Cp (MB) R3489389-1 OV06/20 Analyte 11:10 MB Result mg/I MB Qualifier MB MDL mg4 MB ROL mgn Aldrin U 0,00000813 0.0000500 Alpha BHC U 0.0000166 0.0000500 Beta BHC U 0.0000184 0.0000500 DeltaBHC U - 0.0000197 0.0000500 Gamma BHC U 0.0000176 0.0000500 4 4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT - U 0.0000177 0.0000500 Dieldrin U 0.00000751 0.0000500 Endosulfan) U 0.0000179 0.0000500- Endosulfan II U 0.0000176 0.0000500 Endosulfan sulfate U 0.0000196 0.0000500 Endrin U 0.0000189 0.0000500 Endrin aldehyde U 0.0000142 0.0000500, Endrin ketone U 0.0000170 0.0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0,0000500 Hexachlorobenzene U 0.0000134 0.0000500 Methoxychlor U 0.0000193 0.0000500 Chlordane U 0.0000977 0.000500 Toxaphene U 0.000168 0.000500 /S/ Decochlorobiphenyl 59.4 10.0-144 (S)Tetrochloro-m-xylene 26.6 10.0135 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3489389-2 Analyte 01/06/2011:35 • (LCSD) R3489389-3 Spike Amount LCS Result mg/I mg/1 01/06/20 11:47 LCSD Result moll LCS Rec. % LCSD Rec % Rec. Limits % LCS Qualifier LCSD Qualifier RPD % RPD Limits % Aldrin 0,00100 0.000797 0.000647 79.7 64.7 420-140 20.8 35 Alpha BHC 0.00100 0.000837 0.000726 83.7 72.6 37.0-140 14.2 36 Beta SHE 0.00100 0.000837 0.000773 83.7 T7.3 17.0-147 7.95 44 . Delta BHC 0.00100 0.000910 0.00083E 91.0 _ 83.8 19.0-140 8.24 52 Gamma BHC 0.00100 0.000827 0000745 62.7 74.5 32.0-140 10.4 39 4,4-6DD 0.00100 OA00907 0.000845 907 845 31.0-141 7.08 39 4,4-DDE 0.00100 0.00096E 0.000889 96.8 88.9 30.0-145 8,51 35 4.4-DDT 0.00100 0.000873 O.00O812 BZ3 K2 25.0-160 7.24 42 Dieldrin 0.00100 0.000858 0.000798 85.8 79.8 3U-146 7.25 49 Endosulfan I 0.00100 6,000848 0.000791 84.E 79.1 45.0-153 6.96 28 ACCOUNT: PROJECT: Eaton. Corporation 28091-R SDG: L1176249 DATEMME: 01/10/20 1139 PAGE: 13 of 23 WG1406117 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides (GC) by Method EPA 608.3 L1176249-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) piL�) HC4dydd9 -2 Ul/Ub2U 11:3b - (LCSU) H3489389-3 01/06/201147 Spike Amount -CS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RFD RPD Limits Analyte mg/I mo/I mg/1 % % % % Endosulfan 11 0.00000 0.000800 0.000742 80.0 74.2 �1.00-202 i 7.52 53 Endosulfan sulfate MOM 0.000882 0,000823 98.2 82.3 26.0-144 6.92 38 Endrin 0.00100 0,000893 0.000830 89.3 83.0 30.0-147 7.31 48 Endrin aldehyde 0.00100 0.000811 0.000752 81.1 75.2 56-0-128 7.55 20 Endrin ketone 0.00100 0000766 0.000720 76.6 72.0 54.0-142 6.19 20 Heptachlor 0.00100 0000802 0000644 301 64A 34.0-140 279 43 Heptachlor epoxide 0,00100 0,000841 0.000778 84.1 77.8 37.0-142 778 26 Hexachlombenzene 0.00100 0000726 0.000421 72.6 42.1 35.0-120 J3 53.2 25 Methoxychlor 000100 0.000763 0,000729 76.3 72.9 44.0-160 4.56 22 (S) Decochlorobiphenyl 829 72.6 100-144 (S)Ttrochloro-m- xylene 577 436 100-125 ACCOUNT: PROJECT: SDG: DATEfTIME: PAGE: Eaton Corporation 28091-R L1176249 01/10/201139 14 of 23 WG1406117 QUALITY CONTROL SUMMARY � ONE LAB. NATIONWIDE - P.olychlorinated;Biphenyls;(GC)_by-Melhod=EPA=608.3 _=- Method Blank (MB) (MB) R3488227-1 01/05/2016:39 Analyte MB Result mgh MB Qualifier MB MDL mg/I MB RDL mg/I PCB 1260 U 0.000120 0000500 _ PCB 1616 U 0.000100 0.000500 , PCB 1221 U 0.0000730 0,000500 PCB 1232 U 0.0000420 0.000500 PCB 1242 U 0.0000470 0.000500 PCB 1248 U 0.0000860 0.000500 _ PCB 1254 U 0.0000470 0.000500 (S) Decochlorobiphenyl 48.8 10.6-144 (S) Tetrochloro-m-xylene 28.2 10.0435 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R348B227-2 01105/2016:51 • (LCSD) R3488227-3 01/05/2017:03 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rea. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I Tell % % % % % PCB 1260 0.00250 0.00193 0.00208 77.2 83.2 8,00-140 P P 748 38 PCB 1016 0,00250 0.00181 MOM 72.4 64.0 50 0-140 12.3 36 (S) Decochlorobiphenyl 58.3 51.5 10.0-144 (S) Telrochloro-m-aylene 41.1 23.2 10.0-135 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L1176249 01/10/2011:39 15 of 23 WG1406113 QUALITY CONTROL SUMMARY ONELAB.NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1176249-01 Method Blank (MB) ii f<o42S IHbL UVUb/LU lb:bb MB Result MB Dualifier MB MDL MB RDL Analyte mg/1 mg/I mg/I Acenaphthene U 0,000316 0.00100 Acenaphthylene U 0.000309 0,00100 Anthracene IJ 0.000291 0.00100 Azobenzene U 0.000318 0.0100 Benzidine U 0.00432 0,0100 Benzo(a)anthracene U 0,0000975 0.00100 Benzo(b)fluoranthene U 0.0000896 OOOM Benzo(k)fluoranthene U 0,000355 0,00100 Benzo(g,h,i)perylene U 0.000161 0.00100 Benzo(a)pyrene U 0.000340 0,00100 Bisl2-chlorethcxy)methane U 0,000329 0.0100 Rrs(2-chloroethylether U O.00i62 0.0100 Bis(2-chloroisopropyllether U 0.000445 0,0100 4-Bromophenyl-phenylether U 0.000335 0.Oi00 2-Chloronaphthalene U 0.000230 0,00100 4-Chlorophenyl-phenylether U 0.000303 0,0100 Chrysene U 0.000332 0,00100 Dibenz(a,h)anthracene U 0.000279 0.00100 3,3-Dichlorobenzidine J D.00202 O0100 2 c-Dinitrotoluene J 000165 0.0100 2.6-Dinitrotoluene U 0.000279 00100 Fluoranthene U 0,000310 000 OO Fluorene U 0.000323 0.00100 Hexachlorobenzene U 0.000341 0,00100 Hexachloro-i,3-butadiene U 0.000329 0 0i0o Hexachlorocyclopentadlene J 0.00233 0.0100 Hexachloroethane U 0.000365 0,0100 Indeno(1,2,3-cd)pyrene J 0.000279 0.00100 Isophorone U 0,000272 0.0100 Naphthalene U 0.000372 0.00100 Nitrobenzene U 0.000367 0.0100 n-Nitrosodimethylamine U O,00126 0.0100 n-Nitrosodiphenylamine U 0.00119 0.0100 n-Nitrosodi-n-propvlamine U 0.000403 0,0100 Phenanthrene U 0.000366 0.00100 Benzylbulyl phthalate U 0.000275 0.00300 Bis(2-e1hylhexyl)ph!halate IJ 0.000709 0!00300 Di-n-butyl phthalate U 0.000266 0.00300 Diethyl phthalate J 0.000282 0.00300 Dimethyl phthalate U 0,000293 0.00300 Cp E FS 4Cn SSr rGl Al Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE' Eaton Corporation 26091-R L1176249 01/10201139 16 of 23 WG1406113 QUALITY CONTROL SUMMARY _ ONE LAS. NATIONWIDE,___ --- -- _ _ _ .. _ - "Semi VOIa11I2 Drgantc Compounds �(GC/MS) by Method 625.1 - Lil76249-01 Method Blank (MB) (MB) R3488192-2 01105/2016:55 MB Result Anah4e mgfl MB Qualifier MB MDL mgfl MB RDL mg/I Di-n-oayl phthalate U 0.000278 0,00300 - Pyrene U 0.000330 0.00100 1.2,4-Trichlorobenzene U 0.000355 0.0100 - 4-Chloro-3-methylphenol U 0.000263 0.0100 2-Chlorophenol U 0,000283 0.0100 2.4-Dichlorophenol U 0.000284 0.0100 24-Dimethylphenol U 0.000624 0.0100 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 2.4-Dinitrophenol U 0.00325 0.0100 2-Nltrophenol U 0.000320 0.0100 4-Nitrophenol U 0.0020i 0.0100 Pentachlorophenol U 0.000313 0.0100 - Phenol U 0.000334 0.0100 2,4.6-Trichlorophenol U 0.000297 0.0100- QMtrobenzene-d5 52.7 15.0-34 (S) 2-Fluomblphenyl 68.3 224127 (S)p-Terphenyl-d14 86.3 29.0-141 (S) Phenol-d5 25.9 8.00-424 (S) 2-Fluorophenol 378 10.0420 (S)2,4,6-Tribromophenol 68.5 10.0453 - - Laboratory Control Sample (LCS) (LCS) P3488192-1 OV05/2016:33 Spike Amount LCS Result Analyte Acenaphthene Acenaphthylene Anthracene Azobenzene Benzidine Benzo(a)anthracene. Benzo(b)fluoranthene Benzo(k)fluoramhene Benzo(g,ni)perylene Benzo(a)pyrene Bis(2-ch lorethoxy)metha ne Bisl2-chloroethyllether Bis(2-chloroisopropyl)ether 0.0500 0.0500 0.0500 0,0500 0.100 0.0500 0.0500 0.0560 0.0500 0.0500 0.0500 0.0500 0,0500 0.0380 6.0468 0.0416 0.0396 0.0262 0.0415 0.0451 6.0445 0.0453 0.0462 0.0336 0.0350 0.0355 LCS Rec. 76.0 81.6 83.2 79.2 26.2 83.0 90.2 99.0 90.6 92.4 67.2 70.0 71.0 Rec. Limits 47.0-145 33.0-145 27.0-133 37.0-125 1.00-120 33.0-143 24.0-159 11.0-162 1.00-219 T7:0-163 1.00-219 33.0-185 36.0-166 LCS Qualifier ACCOUNT: Eaton Corporation PROJECT: 28091-R SDG: DATE/TIME: L1176249 0110/2011:39 PAGE: 17 of 23 WG1406113 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1176249-01 Laboratory Control Sample (LCS) )LCS) R3488192-1 01/05/20 1633 Spike Amount LCS Result LCS Res. Rec. Limits Analyte mg/I mg/I % % 4-Bromophenyl-phenylether 0,0500 0.0433 86.6 53.0-127 2-Chloronaphihalene 0.0500 0.0370 74.0 60.0-120 4-Chlorophenyl-phenylether 0.0500 0.0425 85.0 25.0-158 Ch ysene 0.0500 0.0429 85.8 17.0--168 Dibenz(a,h)anthracene 0.0500 0,0394 78.8 1.00-227 3,3-Dichlorobenzidine 0,100 0.0846 84.6 1,00-262 2,4-Dinitrotoluene 0.0500 0,0454 90.8 39.0-139 2,6-Dinitrotoluene 0.0500 0.0445 89.0 50.0-158 Fluoranthene 0,0500 0,0445 89.0 26.0-137 Fluorene 0,0500 0.0423 84.6 59.0-121 Hexachlorobenzene 0.0500 0.0421 84.2 i.00-152 Hexachloro-13-butadiene 0.0500 0.0296 59.2 24.0-120 Hexachlorocyclopemadiene 0.0500 0.0276 55.2 10.0-120 Hexachloroelhane 0.0500 0.0297 59,4 40.0-120 Indeno(1,2,3-cd)pyrene 0.0500 0.0388 77.6 100-171 Isophorone 0.0500 0.0341 68,2 21.0-196 Naphthalene 0.0500 0.0316 63.2 21.0-133 Nitrobenzene 0.0500 0.0315 63.0 35.0-180 n-Nitrosodimethylamine 0.0500 0,0198 39.6 10.0-120 n-Nitrosodiphenylamine 0.0600 0.0416 83.2 44.0-120 n-Nitrosodl-n-propylamine 0,0500 0.0378 75.6 1.00-230 Phenamhrene 0.0500 0.0404 30.8 54.0-120 Benzylbutyl phthalate 0.0500 0.0400 80.0 1.00-152 9is(2-ethylhexyI)phthalale 0.0500 0.0379 75.8 8.00-158 Di-n-butyl phthalate 0,0500 0.0450 90.0 1.00-i20 Diethyl phthalate 0.0500 0.0441 88.2 1.00-120 Dimethyl phthalate 0.0500 0.0439 87.8 h00-120 Di-n-ociyl phthalate 0.0500 0.0372 74A 4,00-146 Pyrene 00500 0.0435 8Z0 52.0-120 1,2,4-Trichlorobenzene 0,0500 0.0298 59.6 44.0-142 4-Chloro-3-methylphenot 0.0500 0.0267 734 22.0-147 2-Chlorophenol 0.0500 0.0339 57.8 23.0-134 2,4-Dichlorophenol 00500 0.0348 69.6 39.0-135 2,4-Dimethylphenol 0.0500 00325 65.0 310-120 4,6-Di nitro-2-m ethyl phenol 0.0500 0.0442 88.4 t00-181 2,4-Diniaophenol 0.0500 0.0442 88.4 1.00-i91 2-Nitrophenol 0,0500 0.0348 69.6 29.0-132 4-Nitrophenol 00500 0.0222 44.4 1.00-132 Pentachiorophenoi 0.0500 0.0399 79.8 14.0-176 Phenol 00500 0.0163 32.6 5,00-120 LCS Oualifier ACCOUNT: PROJECTSDG: Eaton Corporation 26091-R L1176249 DATE/TIME: 01/10/201139 PAGE: 12 of 23 , WG1406113 _ __ QUALITY- CONTROL SUMMARY_ _ Y ONE LAB_ NATIONWIDE - -- - Semi Volatile`Organic`Com pounds (GC/M S) by Method 625.1 --' -� _._ L1176249-Ot- Laboratory Control Sample (LCS) Cp (LCS) R3488192-1 01/05/2016:33 Spike Amount LCS Result LCS Rec. Rec Limits LCS Qualifier ETC Analyte mg/I mgn % % 2,4,6-Trichlorophenol 0.0500 0.0383 76.6 37.0-144 a (S) Nitrobenzene-d5 50.4 15.0-314 $5 IS)2-Fluoroblphenyl 79.7 22.0-127 (S) p- Terphenyl-dM 89.0 29.0-141 _. _ _ a Cn (S)Phenol-d5 32.0 8.00-424 /SJ 2-Fluorophenol 44.6 10.0120 (S) 2,4,6-Tobromophenol 89.5 10.0.153 Fri L1176235-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1176235-01 01/07/20 02:18 - (MS) R3488555-1 01/07/20 02:40 - (MSD) R3488555-2 01/07/20 03:02 zGl Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec Limits ME Qualifier MSD Qualifier RPD RPD Limits Analyte mg4 mgn mgll mg4 % % % % % 13is(2-chlorethoxy)methane 0.0500 U 0.0378 0.0511 75.6 102 10 33.0-184 29.9 54 AI Bs-(2-chloroethyl)ether 0.0500 U 0.0373 6.6418 74:6 83.6 10 12.0-158 HA i08 Bisl2-chloraisopropyoether 0.0500 U 0.0823 0.0914 165 183 10 36.0-166 JS 10.5 76 4-Bromophenyl-phenylether 0.0500 U 0.0426 0.0446 85.2 89.2 10 53.0-127 4,59 43 SC 4-Chlorophenyl-phenylether 0,0500 U 0.0376 0.0422 75.2 84.4 10 25.0-158 its 61 .3,3-Dichlorobenzidine 0.100 U, NO ND 0.000 0.000 10 1.00-262 J6 J6 0.000 108 2,4-Dlnitrotoluene 0,0500 U 0.0420 0.0427 84.0 85.4 10 39.0-139 1.65 42 2,6-Dinitrotoluene 0.0500 U NO 0.0413 0.000 82.6 10 50.0-158 J6 J3 200 48 Hexachloro-1.3-butadiene 0,0500 U 0.0381 0.0575 76.2 115 10 24.0-120 40.6 62 Hexachlorocyclopentadiene 0.0500 U NO NO 0.000 0.000 10 10.0-146 J6 J6 0.000 34 Hexachlorcethane 0.0500 U 0.0314 0.0346 62.8 69.2 10 40.0-120 9,70 52 Isophorone 0,0500 U 0.0354 6.0849 76.8 170 10 21.0-196 82.3 93 Nitrobenzene 0.0500 U 0.0711 0.0994 142 199 10 35.0-180 J5 33.2 62 n-Nitrosodiphenylamine 0,0500 U D.0406 0.0451 K2 90.2 10 16.0-160 10.5 28 n-Nitrosodi-n-propylamine 0.0500 U 0.0483 0.155 96.6 310 i0 1.00-230 J3 J5 105 87 Benzylbulyl phthalate 0.0500 U 0.0534 0.0482 107 96.4 1D 1.00-152 10.2 60 Bisl2-ethylhexyl)phthalate 0.0500 U 0.0434 0.0431 86.8 86.2 10 8.00-158 0.694 82 Di-n-butyl phthalate 0.0500 U 0,0409 0.0421 819 84.2 10 00-120 2.89 47 Diethyl phthalate 0.0500 U 0.0376 0,0385 75.2 T7.0 10 1,00-120 2.37 100 Dimethyl phthalate 0.0500 U 0.0352 0.0374 70.4 74.8 10 1.00-120 6.06 183 Di-n-ocy phthalate CD500 U 0.0484 0.0481 96.8 96.2 10 400-146 0,622 69 4-Chloro-3-methylphenol 0.0500 U 0.00842 6.0130 16.8 26.6 10 22.0-147 J6 421 73- 2-Chlorophenol 0.0500 U 0.00687 0.00779 13.7 15.6 10 23.0-134 J6 J6 12.4 61 2,4-Dichlorophenol 0.0500 U 0.00338 0.00500.' 6.76 10.0 10 39.0-135 J6. J6 367 50 2,4-Dimethylphenol 0.0500 U 0.00751 0.0129 15.0 25.8 10 32.0-120 J6 J6 52.8 58 4,6-Dinitro-2-methylphenol 0.0500 U. 0.0909 0.0902 182 180 10 1.00-181 J5 0373 203 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton. Corporation 28091-R L11]6249 01/10/20 11:39 19 of 23 WG1406113 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GCrMS) by Method 625.1 L1176249-01 L1176235-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1176235-01 01/07/20 02,18 • (MS) R3488555-1 01/07/20 02:40 • (MSD) R3488555-2 01/07/20 03:02 CS' Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Red. Limits MS Oualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % TC 24-6initrophenol 0.0500 U 0.0554 0.0935 191 187 70 1.00-i91 2.01 132 v 2-Nitrophenol 0.0500 0.557 0.345 0.508 0.000 0.000 10 29.0-182 V V 38.2 55 s 4-Nltrophenol 0.0500 0.321 0.285 0.302 0000 0000 10 t00-132 V V 579 131 SS Pentachlorophenol 0.0500 U 0.0499 0.0545 99.8 109 10 14.0-176 8.8i 86 Phenol 0.0500 U 0.0575 0.0765 50.0 88.0 10 5,00-120 23.4 64 4 Cn Acenaphmene 0,0500 U 0,0359 0,0386 71.8 77.2 10 47.0-145 7,25 48 2,46-Trichlorophenol 0,0500 U 0.0345 0.0411 69.0 822 10 320-144 173 58 s Acendph[h)'lene 0.0500 U 0.0679 0.0223 35.8 44.6 10 33.0-i45 21.9 74 Sr Anthracene 0.0500 U 0.0341 0,0369 68.2 73.8 io 27.0-133 7.89 66 Benzidine 0.100 U NO ND 0.000 0.000 i0 1.00-120 J6 J6 0.000 4C Benzo(a)anihracene 0.0500 U 0.0387 0,0405 774 81.0 10 33.0-i43 455 53 Benzo(b)fluoranthene 0.0500 U 0.0399 0.0438 79-8 87.6 10 24.0-i59 932 71 7Gl 1,2-Diphenylhydrazine 0,0500 U 0.0524 0.0492 105 984 i0 18.0-156 6.30 �4 Benzo(k)fluoranthene 0,0500 U 0,0375 0.0404 75.0 80.8 10 11.0-162 745 63 Benzcrd,h,i)perylene 0,0500 J 0,0385 0.0400 77.0 80.0 10 1,00-219 3.82 97 A Benzo(a)pyrene 0.0500 U 0.037i 0.0410 74.2 82.0 i0 17.0-163 9,99 72 2-Chloronaphthalene 0,0500 U 00383 0.0407 76.6 31.4 i0 60.0120 6.08 24 CSC Chrysene 0,0500 U 0,0403 0.0412 80.6 82A 10 17.0-165 2.21 87 Dibenz(a,h)anthracene. 0.0500 U 0.0408 0.0416 81.6 83.2 10 1.00-227 1,94 126 Fluoranthene 0.0500 U 0.0370 0.0406 740 61.2 10 26.0-137 9.28 66 Fluorene 0.0500 U 00378 0.0399 75.6 79.8 10 59.0-121 541 38 Hexachlorobenzene 0.0500 U 0.0469 0.0438 93.9 87.6 10 1.00-152 6.84 55 Indemo(1,2,3-cd)pi 0.050C J 0.0423 0.0452 84.6 904 i0 i.00-171 6.63 99 Naphthalene 0.0500 U 0,0323 0,0453 64.6 9(1 10 21.0-133 33.5 6E n-Nitrosodimethylamine 0.0500 U 0.0918 0101 20.2 38.6 10 10.0-120 9.54 40 Phenanthrene 0.0500 U 0.0386 0.0417 77.2 83.4 10 54.0-120 7.72 39 Pyrene 0.0500 U 0.0434 0.0455 86 8 91.0 10 52.0-120 472 49 1,2,4-Trichlorobenzene 0.0500 U 0,0296 0,0433 59.2 86.5 10 44.0142 37.6 Sc (S Nihobenzene-d5 108 195 15.0-?c4 (S 2-Fluterobiphenyl 76.1 85.2 22.0-727 (S) p-Terphenyl-d74 26 6 106 25.0-141 (S)Phenol-d5 0,000 0.000 8.00-424 J2 J2 (S)2-Fluoropheno7 0,000 0000 10.0-120 J2 J2 (S)Z,1,6-Tnbromophenal HE 4Z3 700-153 Sample Narrative: OS. Dilution due to matrix. Surrogate failure due to matrix interference, ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1176249 01/10/2011:39 20 of 23 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. $ Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer- Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. No Not detected at the Reporting Limit (or MDL where applicable). ROL Reported Detection Limit. Rec. Recovery, RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard)- Analytes added to every blank, sample, Laboratory Can Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the ;Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or %difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND' (Not Detected) or "BDL" Result (Below DetectableLevels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and .Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (So) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. (Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyze is acceptable; the reported value is an estimate. J2 Surrogate recovery limits have been exceeded; values are outside lower control limits. J3 The associated batch QC was outside the established quality control range for precision. J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high. - J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. :P RED between the primary and confirmatory analysis exceeded 40%. v The sample concentration is too high to evaluate accurate spike recoveries. 'Cp RC ass 4Cn aSr aQC aAl 9Sc ACCOUNT:. PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1176249 01/10/20 It:39 21of23 ACCREDITATIONS & LOCATIONS ONE LAB, NATIONWIDE, Pace National is the only environmental laboratoryaccoss ited/certihed to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most signIDcant benefit to our one location design Is the design of our laboratory campus. The Total Is conducive to accelerated productivity decreasing turnaround time, and preventing cross contamination, thus protecting sample integrity. Our focus an premium quality and prompt service allows us to be YOUR LAB OF CHOICE- ' Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is onlyapplicable to the test methods specified on each scope ofacnedilation held by Pace National. 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Tennessee 1° 2006 Louisiana' LA180010 Texas T104704245-18-15 Maine TN0002 Texas' LAB0152 Maryland _ 324 Utah TN00003 Massachusetts M-TNO03 Vermont VY2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington Clio MBsissippl TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 _ Wyoming A21-A Third Party Federal Accreditations A2LA - 150 17025 146T01 AIHA LAP,LLC EMLAP 100789 A2LA-ISO 17025° 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15 00234 EPA-Crypto TN00003 'drinking Water ° Underground Storage Tanks ' Aquatic Toxicity 4 Chemical/Microbiological `Mold a Wastewater n/a Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office Pace National performs all testing at our central laboratory. T ` VVA R T NO 2 aE OR MN T 1D so T vv, NY MI � T NV T NE IA T T PA T T UT T T OH IL Ito T T �r 410 CO KS M10 lT � VAT TAZ ' Not 1J — T TX AK T 9 .O F Elf OVT AR T SC MS AI TGA LA FL ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Eaton Corporation 28091-R L1176249 0111012011:39 22 of 23 441 Billing information,.,- nt.1; I eg Chain of C=tody, -Page of-- `iit It Eaton Corporation NA Fina'Aw Services Center -:100;h res , Fo BOX9-1864 2564 Durharin Road, C1eve1an@"OlH 44181-8024 Roxboro,liC 27S73 t 12M Lebtran Rd Q. B Report w Email To: Dustin LeClair dustinlaclabiti m meaton.m,colinwbetchan@eaten.co Fam 61L7"-5859 Project City/State Please CIncIe:, Description: Eaton Corp Mcinthly.Stoh Collected: PT MIT CT4Er OY SDG Phone: cuent Project A Lab Project A 28091TR EATONRNC48091SW_ z E096 Fax: A z -w Collected by (print): p;.O. 4— 159838 xccir46EATONRNC�_ ROXBORO NC z temptate�*131J!602 Collected by (sig ii"VII Rush? (Lab MUST Be Notified) Quote W ft;E�� L z �E 10 �refoglr�. 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(Signature) Same$ Received: If presen radon required by Login: Date/Time, Relinquished by: (Signature) Date: Time: Received for tabby: (Signature) � -, �i - ", - Date - .. Time F : Hold- , Condition. _" NCF-- al