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HomeMy WebLinkAboutNCG030027_MONITORING INFO_202001102ZL) STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. IV U& n 3 b GO-% DOC TYPE ❑ HISTORICAL FILE ❑� MONITORING REPORTS DOC DATE ❑ 03 U b( 1 YYYYM M D D DOC TYPE 1 ❑ HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE 1 ❑ YYYYM M DD Fm,T*N January 3, 2020 Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attn: DWQ Central Files Colin W. Betchan Environmental, Health & Safety Supervisor (919) 702-3703 (mobile) (336) 503-6562 (fax) colinwbetchan(@eaton.com RECEIVED RE: December 2019 Monthly Tier III Discharge Monitoring Report JAN 10 2020 CENTRAL FILES DWR SECTION Attached are the analytical results and associated chain of custody for the December 13, 2019, monthly Tier III stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility. Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North Carolina Division of Water Quality (NCDWQ). I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with the system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or other persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Sincerely, Colin W. Betch AXt EHS Supervisor Attachments Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 CERTIFICATE OF COVERAGE NO. N0003 0 0 2 7 FACILITY NAME Eaton Corporation COUNTY Person County PERSON COLLECTING SAMPLES Colin Betchan LABORATORY Pace National Date submitted 01/03/2020 Lab Cert. fi ENV375/DW21704/BI0041 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD Jan -June 0 July -Dec or Q Monthly' December (month) ECEIVp4MCHARGINGTOCLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA JAN 10 2020 ❑I1 Other WS-III; NSW 'ENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DW'R SECTION n No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Hydrocarbons Total Toxic Benchmarks - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46S29 C0530 00400 01119 01051 01094 00552 78141 Tool Room Trench (005) 12/13/19 0.30 4.60 8.9 0.0181 0.00200 0.126 4.40 0.03365 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufactu"re electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 - — - - - - - - -..- -- - --- -- - - - Page 1 of 3 -- Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Colin Betchan Name (Print name) EHS Supervisor Title (Print title) Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2of3__=. - - FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART If SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES 0 NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO[] . REGIONAL OFFICE CONTACT NAME: Dannysmith Mail an oriainal coov of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 -- - — - - - - - - - - - _ - - -- - Page of - _. aceAnalytical° ANALYTICAL REPORT Melionel Cmterior Testing 8lnno-than December 23, 2019 R Eaton Corporation Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L1170973 12/14/2019 28091-R Eaton Corp Monthly Stormwater ROXBORO,NC Dustin LaClair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: 4�� Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without wrlllen approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National Is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTIL-0067 and . ! ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the Information provided, and as the samples are received. J." E ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1170973 12/23/1909A7 1of 25 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1❑ Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 3SS Sr: Sample Results 5 2019-12-13-005 L1170973-01 5 Oc: Quality Control Summary g Cn Gravimetric Analysis by Method 2540 D-2011 9 s Sr Wet Chemistry by Method 1664E 10 6QC Metals (ICP) by Method 200.7 11 Volatile Organic Compounds (GC/MS) by Method 624.1 12 7GI Pesticides (GC) by Method EPA 608.3 15 Polychlorinated Biphenyls (GC) by Method EPA-608.3 17 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 18 Gl: Glossary of Terms 23 Sc Al: Accreditations & Locations 24 Sc: Sample Chain of Custody 25 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1170973 12/23/19 09 47 2 of 25 SAMPLE SUMMARY ONE LAB. NATIONWIDE. x Collected by Collected dateltlme Received dateltime 2019-12-13-005 L117O973-01 WW Colin Betchan 12/1311909:30 12/14/1909:00 C p Method Batch Dilution Preparation Analysis Analyst Location date/time dateltime FTC Gravlmetric Analysis by Method 2540 D-2011 WG1399308 1 12179/1906:47 7211911911:24 TH Mt. Juliel, TN Wet CheMslry by Method 1664B W61399727 1 12119/1907:39 12/19/1921.06 MOP Mt. Jullel, TN Metals (ICP) by Method 2003 WG1396282 1 12/16/19 07:21 12/17M910:25 TRB Mt. Juliet, TN Volatile Organic Compounds (GCJMS) by Method 624.1 WG1397047 1 12116/1913:39 12/16M913*39 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 6241 WG1397531 1 12116/19 2112 12/16/19 2112 JHH Mt. Juliet, TN ° Cn Pesticides (GC) by Method EPA 608.3 WG1397445 1 72/17/1907:37 12117/1915:26 HMH Mt. Juliet, TN Polychlorinated Biphenyls)GC) by Method EPA-608.3 WG1397445 1 12/17/1907:31 12/17/1918:16 MTJ Mt. Juliet, TN s Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1398261 1 12/1811916:37 12119/19 00:54 AO Mt. Juliet, TN ST 6^C 7G1 eAl jl 9SC ACCOUNT: i PROJECT: SDG: DATE/TIME' PAGE: Eaton Corporation 28091-R L1170973 12/2319 09:47 3 of 25 U CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the Cp appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples TC have been corrected for the dilution factor used In the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my SS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information of data have been knowingly withheld that would affect the quality of the data. SSr 7GI Heather J Wagner c Project Manager A� 9Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1170973 12123P9 09:47 4 of 25 319-12-13-005 SAMPLE RESULTS - 01 ONELAB.NATIONWoE. lected dale/time: 12/13119 09:30 L1170973 Additional Information Result Units Cp Analyze pH (On Site) 8.9 su Temperature (on -site) 5 Deg C Gravimetric Analysis by Method 2540 D-2011 Result Qualifier MDL ROL Dilution Analysis Batch Analyle mg4 mgn mgA date/time Suspended Solids 4.60 J 0,700 5.00 1 12/19/20191124 WG1399308 Sample Narrative: L1170973-01 WG1399308: Reporting limit determined by filtrate volume. Wet Chemistry by Method 1664E Result Qualifier MDL RDL Dilution Analysis Batch Analyte all mg/I mg/I date/time TPH - Oil & Grease 4.40 J 0.863 5,95 1 12/19/2019 21:06 WG1399727 Metals (ICP) by Method 200.7 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgll mg/I mg/I date/time copper 0.0181 0.00700 0.0100 1 121171201910:25 WG1396282 Leatl U 0.06200 0.00500 1 12/17/201910:25 WG1396282 n Zinc 0.126 0.00340 0,0500 1 12/17/201910:25 WG1396282 Organic Compounds (GC/MS) by Method 624.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg4 mg/I mg4 date/time Acelten U 0.00887 0.0500 1 12/16/201921:12 WG1397531 Acrylonitrile U 0.06187 0,0100 1 12/16/201913:39 WG1397047 Benzene U 0,000331 000100 1 12116/201913:39 WG1397047 Bromodlchloromethane U 0000380 000100 1 12/16/201913:39 WG1397047 Bromotorm U 0000469 000100 1 12/16/201913:39 WG1397047 Bromomemane U 0.000866 0.00500 1 12/161201913:39 WG1397047 Carbon tetrachloride U 0.000379 0.00100 1 12I16I201913:39 WG1397047 2hlorobenzene U 0.000348 0.00100 1 12/16/M1913:39 WG1397047 sr Chlorodibromomethane U 0000327 0.00100 1 12116/201913:39 WG1397047 Chloroethane r U 0.000453 0.00500 1 12I76I201913:39 W61397047 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 12/16201913:39 WG1397047 1. Chloroform U 0.000324 0,00500 1 12/161201913:39 WG1397047 CMoromethane U 0.000276 0.00250 1 12116/201913:39 WG1397047 1.2-Dichlerobenzene U 0.000349 0.00100 1 12/16/201913:39 WG1397047 1,3-Dichlorobenzene U 0000220 0.00100 1 121161201913:39 WG1397047 1 '1,4-Dichlorobenzene U 0.000274 0.00100 1 12I16/201913:39 WG1397047 Dichlorodlfluoromethane U 0.000551 0.00500 1 12/16/201913t39 WG1397047 11-Dichloroethane U 0.000259 0.00100 1 12/16/201913:39 WG1397047 il 1,2-Dichloroethane U 0.000361 0.00100 1 12116/201913:39 WG1397047 1,1-aDichloroethene U 0.000398 0.00100 1 12/16/201913:39 WG1397047 trans-1,2-Dichloroethene U 0.000396 0.00100 1 121161201913:39 WG1397047 ,1,2 Dlchloropmpane U 0.000306 0.00100 1 12I16I201913:39 WG1397047 cis-1,3-Dichloropropene U 0.000418 0,00100 1 12/161201913:39 WG1397047 its ns-1,3-Dichloropropene U 0.000419 0.00100 1 121161201913:39 WG1397047 Ethylbenzene U 0,000384 000100 1 12/16/201913:39 WG1397047 'Methylene Chloride U 000100 000500 1 121161201913:39 WG1397047 1,1,2,2-Telrachloroethane U 0.000130 0.00700 1 12/76/201913:39 WG7397047 Tet U 0.000372 0.00100 1 12/16/201913:39 WG1397047 itrachloroethene ACCOUNT: PROJECT: SDG: DATETIME: PAGE: it Eaton ll Corporation 28091-R L1170973 12/23d909:47 5of 25 2019-12-13-005 SAMPLE RESULTS - 01 ONE LAB, NATIONWIDE, Collected date/time. 12/13/19 09:30 L1170973 Volatile Organic Compounds (GC/MS) by Method 624.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyze mg/I mg/I mg/I date/time Toluene U 0.000412 0,00100 1 12/16/201913:39 WGI397047 1,L7-1 richlmoethane U 0.000319 0.00100 1 12/16/201913.39 WG1397047 11.2-1 rich lorcethane U 0,000383 0.00100 1 12116/201913,39 WG1397047 Trichloroethene U 0-000398 0.00100 1 121161201913:39 WG1397047 Trichlorofluoromethane U 0.00120 0,00500 1 12/16/201913:39 WG1397047 Vinyl chloride - U 0000259 0.00100 1 12/16/201913:39 WG1397047 (5)Tohene-d8 98.1 80,0120 127161201913,39 WG1397047 (S) Toluene-d8 103 80.0-120 1211612019 21,12 WG1397531 (S) 4-13mmolluorobenzene 923 80.0 120 121161201913.39 WG1397047 (S) 4 Bromolluorobenzene 95.5 800120 1211612019202 WG1397531 (5)1,2-01-d4 969 70.0-130 121161201913,79 WGI397047 (5) 12-Dichloroelhone-d4 85.9 70.0430 1211612019 21.12 WG1397531 Pesticides (GC) by Method EPA 608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgll mg/I mg/l date/time Aldrin U 0.00000813 0.0000500 1 12/17/201915:26 WG1397445 Alpha BHC U 0.0000166 (0000500 1 12117/20191526 WG1397445 Beta BFIC U 00000184 0,0000500 1 12/17/201)15.26 WG1397445 Delta BHC U J4 0.0000197 0-0000500 1 12/17/201915.26 WG1397445 Gamma BHC U 00000176 0.0000500 1 12/17/201915:26 WG1397445 Chlordane U 0,0000977 0.000500 1 12YI71201915:26 WG1397445 44-1)f7D It 00000170 0.0000500 1 12/17/201915:26 WG1397445 4,4-DDE U 00000164 00000500 1 12/17/201915:26 WG1397445 44-DDT U 0.0000177 0,0000500 1 12/17/201915.26 WG1397445 Dieldrin U 0.00000751 0.0000500 1 12/17/201915:26 WG1397445 EndosullanI U 00000179 0.0000500 1 12/17/201915:26 WG1397445 Endosulfan ll U 00000176 0.0000500 1 12/17/201915:26 WG1397445 Endosulfan sulfate U 0.0000196 0.0000500 1 12/17/201915:26 WG1397445 Endrin U 00000189 0.0000500 1 12/17/201915:26 WG1397445 Endrin aldehyde U 0.0000142 0.0000500 1 12/17/201915:26 WGI397445 Endrin ketone U 00000170 0.0000500 1 12/17/201915:26 WG1397445 Heptachlor U J4 00000108 0.0000500 1 12/171201915:26 WG1397445 Heptachlor epoxide U 0.0000175 0.0000500 1 12/17/201915:26 WG1397445 Hexachlolobenzene U 0,0000134 0.0000500 1 12/17/2019 15:26 WG1397445 MClhoxychlor U 0.0000193 0,0000500 1 12/17/201915:26 WGI397445 Toxaphene U 0 000168 0.000500 1 12/17/201915:26 WG1397445 (S) Decochlorobiphenyl 615 10.0-744 721171201915,26 WG1397445 (5) 7elrochloro-m-xylene 69.3 10.0-135 121771207915.26 WG1397445 Polychlorinated Biphenyls (GC) by Method EPA-608.3 Result Oualifier MDL RDL Dilution Analysis Analyze mg/I mg/I al date/time PCB 1016 U 0000100 0.000500 1 12/171201918:16 PCB 1221 U 00000730 0.000500 1 12117/20191816 PCB 1232 U 00000420 0000500 1 12117/201918:16 PCB 1242 U 0.0000470 0.000500 1 12/17/201918:16 PCB 1248 U 00000860 0.000500 1 12/17/201918:16 PCB 1254 U 00000470 0000500 1 12/17/201918,16 PCB 1260 tl 0.000120 0.000500 1 12/17/2019 18 16 (S) Decochlorobiphenyl 78 1 10.0444 12117201918.16 (S) Terrochli ru-xylene 69.7 10.0 135 1211712019 18.76 Batch WG1397445 WG1397445 WGI397445 WG1397445 WG1397445 WGI397445 WG1397445 WG1397445 WG1397445 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L1170973 DATEMME: PAGE: 12/23A9 09:47 6 of 25 2019-12-13-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dale/rlme: 12/13/19 09.30 L1170973 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyze ni mg/I mgll date/lime Acenaphthene U 0.000316 0.00100 1 12/19/2019 00:54 WG1398261 Attenaphlhylene U 0000309 0.00100 1 12I791201900:54 WG1398261 Anthracene U 0.000291 0.00100 1 12/19/2019 00:54 WG1398261 Benzidine U 0.06432 0.0100 1 12119/2019 00:54 WG1398261 Ben2o(a)anthracene U 0.0000975 0.00100 1 12I19/2019 00:54 WG1398261 8a.wo(h)fluoranthene .1 U 0.0000896 0.00100 1 12/19/201900:54 WG1398261 Benzo(kltluoranthene U 0.000355 0.00100 1 12/19/2019 00:54 WG1398261 .Ben2a(g,hj)pmylene it U 0.000161 0.00100 1 12AM01900:54 WG1398261 Benzo(a)pyrene U 0.000340 0.00100 1 12/19/2019 00:54 WG1398261 Bil(2-chlorethoxy)melhane U 0,000329 0.0100 1 12A912019 00:54 WG1398261 - B1s(2-chloroelhygether U 0.00162 0.0100 1 12/19/2019 00:54 WG1398261 BIs(2-chloroisopropylielhel U 6.060445 0.0100 1 1L19I2019 00:54 WG1398261 4-Bromophenyl-phenylether U 0.000335 0.0100 1 12/19/2019 00:54 WG1398261 2 -Chloronaphihalene U 0.000330 0.00100 1 12/19/2019 60:54 WG1398261 4.Chlorophenyl-phenylether U 0.000303 0.0100 1 12/19)2019 00:54 WG1398261 Chrysene U 0.000332 0.00100 1 12/19/201900:54 WG1398261 Dibenz(a,h(amhmcene U 0.000279 0,00100 1 12/19/201900:54 WG1398261 3,3-Dich1orobenz1d1ne U 0.00202 aovio 1 12/19/2019 00:54 WG1398261 2,4-Dinitrotoluene U 0.00165 0,0160 1 12/191201900:54 WG1398261 2 ,'6-Dinitrotoluene U 0000279 0.0100 1 12119/2019 00:54 WG1398261 11-Diphenylhydrazine a, U 0,000318 0.0100 1 12/19/2019 00:54 WG1398261 Pluoranthene U .. 0.000310 0.00100 1 12119/2019 0054 -. WGI398261 Fluorene U 0.000323 0,00100 1 12/19/2019 00:54 WG1398261 Hezachlorohenzene U 0.000341 0.00100 1 12119/2019 00:54 WG1398261 Hezachloro-1,3-huladiene U 0.000329 0.0100 1 129/201900:54 WG1398261 He}achlorocyclopentadiene U 6,06233 0.0100 1 12/19/201900:54 WG1398261 Hexachloroethane U 0.000365 0.0100 1 12/19/2019 00:54 WG1398261 Indeno(1,2,3-cd)pyrene U 0.000279 0.06100 1 12P91201900:54 WG1398261 Isophorone U 0.000272 0.0100 1 121191201900:54 WG1398261 Naphthalene U 0,000372 0.00100 1 12/19/2019 00:54 WG1398261 Nitrobenzene U 0.000367 0.0100 1 12119/2019 00:54 WG1398261 n-Nithosodimethylamine U 0.00126 0.0100 1 12/19/2019 00:54 WG13682161 n-Niuosodiphenylamine U 0.00119 0.0100 1 12119/2019 00:54 WG1398261 n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 121160 WG1398261 Phenanthrene U 0.000366 0.00100 1 12119/2019 00:54 WG1398261 Bezylbutyl phthalate U 0,000275 0.00300 1 12/19/2019 00:54 WG1398261 Pisj2-ethylhexygphthalate U 0.000709 0.00300 1 12/19/201900:54 WG1398261 Di ri phthalate U 0.000266 0.OMO 1 12A91201900:54 WG1398261 Diethyl phthalate U 0.000282 0.00300 1 121191201900:54 WG1398261 Dimelhyl phthalate U 0.000283 0.00300 1 121191201900:54 WG1396261 Di,n-octyl phthalate U 0.000278 0.00300 1 12/19/201900:54 WG1398261 p1re U 0.000330 0.06106 1 12/19/201900:54 WG1398261 12,4-Trichlorohenzene U 0.000355 0.0100 1 12119/201900:54 WG1398261 4-Chloro-3-methyl phenol U 0.000263 0.0100 1 12119/201900:54 WG1398261 2-Chlorophenol U 0 000283 0.0100 1 12/19/2019 00:54 WG1398261 2,41DIchlorophenol U 0.0002V 0.0100 1 12/19/2019 0054 WG1398261 2,4=Dimethylpheri U 0A00624 0.0100 1 12/19/2019 00:54 WG1398261 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 121191201900*54 WG1398261 2,47Dinitrophenol U 000325 0.0100 1 12/19/2019 00:54 WGI398261 2-Nilrophenol U 0.000320 0.0100 1 12P9/2019 00:54 WC31398261 4-Nilrophenol U 0.00201 0,0100 1 12119/201900:54 WGI396261 .Pentachlorophenol U 0.000313 0.0100 1 12/1912019 00:54 WG1398261 Phenol 0.00172 J 0,000334 0.0100 1 12/191201900:54 WG1398261 ,a - 2,4,6-Tdchlorophenol U 0.000297 0.0100 1 12/19/2019 00:54 WG1398261 SJ2-Fluorophenol 40.1 100-120 1279120190054 WG1398261 (S)Phenol-d5 27.2 8,00-424 12/19201900.54 WG1398261 ACCOUNT: PROJECT: SDG: DATEMME: PAGE' Eaton Corporation 28091-R L1170973 12/23/19 09:47 7 of 25 2019-12-13-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected datOtlme: 12/13M9 09:30 L1170973 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Analyte mgfl mgll mgll (S) Nitrobenzene-d5 64.9 15,0314 (S) 2-Fluorob ohcnyl 72.8 22.0-127 (S) 2,4, 6-hibromophenol 915 100153 (5)p-7erphenybd14 787 290-141 Dilution Analysis Batch date / time 1211912,00 00,54 WG1398261 12719201900:54 WG1398261 12119201900.54 WG1398261 121191201900:54 WG1398261 ACCOUNT: PROJECT. SDG: DATERIME' Eaton Corporation 28091-R 1-1170973 12/23/1909:47 PAGE: 8 of 25 WG1399308 QUALITY CONTROL SUMMARY ONELAB.NATIONWIDE. Gravimetric. Analysis by Method 2540 D-2011 L1170973-01 Method Blank (MB) (MB) R3484476-1 12/19/191124 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Suspended Solids U 0.350 250 L1171O73-01 Original Sample (OS) • Duplicate (DUP) (OS) L1171073-01 12/19/19 11:24 • (DUP) R3484476-3 12/19/19 11:24 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD 9 Limits Analyte mg/I mg4 % % Suspended Solids 142 158 1 103 P1 5 L1171O85-01 Original Sample (OS) • Duplicate (DUP) (OS) L1171085-01 12/19/19 11:24 • (DUP) R3484476-4 12/19/19 1124 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUPRPD Limits Analyte mg4 mg4 % % Suspended Solids 98.0 104 1 5.94 P1 5 Laboratory Control Sample (LCS) (LCS) R3484476-2 12/19/19 11:24 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg4 mg/I % % Suspended Solids 773 864 112 85.0-115 ACCOUNT^ '^ PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1170973 12/23/19 09:47 9 of 25 WG1399727 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Wet Chemistry by Method 1664B L1170973-01 Method Blank IMB) (MB) R3484360-1 12/19/19 2106 MB Result MB Oualifier MB MDL MB RDL Analyte mg/I mg/I mg/I TPH -Oil &Grease U G 725 —5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3484360-2 12/19/19 21:06 • (LCSD) R3484360-3 12/19/19 21:06 -- Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rea, Rec. Limits LCS Qualifier LCSD oualifier RPD RPD Limits TPAnalyte mg/I mg/I mg/I % % % % % H-011&Grease 20.0 13.9 17.1 69.5 B5.5 64.0 -132 20.6 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE' Eaton Corporation 28091-R L1170973 2/23/19 09:47 10 0` 25 WG1396282 QUALITY CONTROL SUMMARY ONELAB.NATIONWIDE. Metals (ICP) by Method 200.7 L1170973-01 _ Method Blank (MB) (ME) R3483077-1 12/17/19 09:05 ME Result ME Qualifier ME MDL ME ROL Analyte men ni mg/1 Copper U 0.00700 0.0100 Lead U 0.00200 0.00500 Zinc 0.00420 J 0.00340 0.0500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3483077-2 12/17/19 09:08 • (LCSD) R3483077-3 12/17/19 09:10 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I moil mg/I % % % % % Copper 1.00 0.959 0.972 95.9 97.2 85.0-115 140 20 Lead 1.00 0.955 0.968 95.5 96.8 85.0-115 1.34 20 Zinc 1.00 0.928 0.943 92.8 94.3 85.0-115 1.64 20 L1169794-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1169794-01 12/17/19 09:13 • (MS) R3483077-5 12/17/19 09:16 • (MSD) R3483077-6 12/17/19 09:21 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec Limits ME Qualifier MSD Qualifier RPD RPD Limits AnaMe moil moll mgA mg/I % % % % % Copper 1.00 NO 0.976 0.966 97.6 96.6 1 70.0-130 0.996 20 Lead 1.00 NO 0.972 0.971 972 97.1 1 70.0-130 0.0587 20 Zinc 1.00 NO 0.945 0.943 945 94.3 1 70.0-130 0181 20 L1169895-01 Original. Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1169895-01 12/17/19 09:23 • (MS) R3483077-7 12/17/19 09:26 • (MSD) R3483077-8 12/17/19 09:28 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I moll % % % % % Copper 1.00 NO 0.971 0.983 97.1 98.3 1 70.0-130 1.18 20 Lead 1.00 NO 0.970 0.991 97.0 SEA 1 70.0-130 2.19 20 , Zinc 1.00 NO 0.939 0A57 93.9 95.7 1 70.0-130 1.96 20 ACCOUNT PROJECT SDG: DATE/TIME: PAGE: Eason Corporation 28091-R a170973 12/23A9 09:47 11 of 25 WG1397047 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE, Volatile Organic Compounds (GC/MS1 by Method 624A L1170973-01 Method Blank (MB) (MB) R3482890-3 12/16/19 08,59 MB Result MB Oualifier MB MDL MB RDL Analyte mg/I ma/I mg/I Acrylonitrile U 0,00187 0,0100 Benzene U 0,000331 0,00100 Bromodichloromethane U 0.000380 0.00100 BrDMOfernl U 0.000469 0.00100 Bromomethane U 0.000866 0.00500 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0,00100 Chlorodibromomethane U 0.000327 0.00100 Chlorcethane U 0,000453 0,00500 2-Chloroethyl vinyl ether U 0,00301 0.0500 Chloroform U 0000324 0.00500 Chloromethane U 0000276 0.00250 1.2-Dichlorobenzene U 0000349 MOM 1,3-Dichlorobenzene U 0.000220 0,00100 14-Dichlorobenzene U 0000274 MOM Dichlorodifluoromethane U 0.000551 0.00500 1,i-Dichloreethane U 0.000259 0.00i00 1,2-Dichloroethane U 0,000361 0,00100 it-Dichloroethene U 0.000398 0.00100 trans-1,2-Dichloroethene U 0.000396 How 1,2-Dichloropropane U 0.000306 0.MOO cis-i,3-Dichloropropene U 0000418 MOM trans-1,3-Dichloropropene U 0,000419 0,00100 Ethylbenzene U 0.000384 0.00100 Methylene Chloride U 0,00100 0.00500 11,2,2-Tetrachloroethane U 0,000130 0,00100 Tetrachloroethene U 0000372 HMO Toluene U 0000412 0,00100 1.1,1-Trichloroethane U 0000319 CALM 11,2-Trichloroethane U 0.000383 0,00100 Trichloroethene U 0000398 0,00100 Tdchlorofluoromethane U 0.00120 0.00500 Vinyl chloride U 0.000259 0.00100 (S)Toluene-d8 974 80,0-120 (S)4-Bromolluorobenzeae 901 800-120 (S)1.2-Dichloroebbone-d4 95A 70.0-130 ACCOUNT: PROJECT: Eaton Corporation 28091-R SDG: L1170973 DATE/TIME: 12/23/19 09:47 PAGE: 12 of 25 WG1397047 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds.(GC/MS) by Method 624.1 L1170973-01, - Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3482890-1 12/16/19 Analyte 07:59 • (LCSD) R3482890-2 Spike Amount LCS Result man mgll 12/16/19 08:18 LCSD Result mgn LCS Rec. % LCSD Rec. % Rec. Limits % LCS Qualifier LCSD Qualifier RPD % RPD Limits % Acrylonitrile 0.0250 0.0192 0.0185 76.8 74.0 60.0-140 371 20 Benzene 0.00500 0.00550 0.00551 110 110 65.0-135 0.182 20 Bromodichloromethane 0.00500 0.00553 0.00534 Ili 107 70.0-05 350 20 Sromoform noso0 0.00407 0.00406 814 81.2 70.0-130 0.246 20 Bromomethane 0.00500 0.00432 0.00467 96.4 93A 15.0-185 316 20 Carbon tetrachloride 0.00500 0.00555 0.00568 Ili 114 70.0-130 2.32 2D Chlorobenzene 0.00500 0.00522 0.00521 104 104 65.0-135 0192 20 Chlorodibromomethane 0.00500 0.00477 000490 95A 98.0 70.0-135 2.69 20 Chloroethane 0,00500 0.00407 0.00443 81.4 88.6 40.0-160 8.47 20 2-Chloroethyl vinyl ether 0,0250 0.0251 0.0239 100 95.6 0.100-225 4.90 20 Chloroform 000500 0.00561 0.00558 112 112 70.0-135 0,536 20 Chloromethane 0,00500 0.00550 0.00551 110 110 0.100-205 0.182 20 1,2-Dichlorobenzene 0.00500 0.00546 0.60502 109 100 65.0-135 840 20 1,3-Dichlorobenzene 0.00500 0.00562 0.00531 112 106 70.0-130 5,67 20 14-Dichlorobenzene 0.00500 0.00542 0.00521 108 104 65.0-135 3.95 20 Dichlorodifluoromethane 0.00500 0.00588 0.00570 118 114 49.0-155 311 20 1,1-Dichloroethane 0,00500 0.00550 0.00540 110 108 70.0-130 1,83 20 1,2-Dichloroethane 0,00500 0.00518 0.00511 104 102 70.0-130 1.36 20 1,1-Dichloroethene 0,00500 0.00467 0,00482 93A 964 50.0-150 316 20 trans-1.2-Dichloroethene 0.00500 0.00491 0.00490 9B.2 98.0 70.0-130 0.204 20 1,2-Dichloropropane 0.00500 0.00581 0.00553 116 111 35.0-165 4.94 20 cis-1.3-Dichloropropene 0.00500 0.00550 0.00525 110 105 25.0-175 4,65 20 trans-1,3-Dichloropropene 0,00500 0.00518 0.00522 104 104 50.0-150 0.769 20 Ethylbenzene 0,00500 0.00495 0.00517 99.2 103 60.0-140 415 20 _ Methylene Chloride 0.00500 0.00498 0.00486 99.6 9T2 60.0-140 2.44 20 1,1,2,2-Tetrachloroethane 0,00500 000450 0.00410 90.0 82.0 %0-140 9.30 20 Tetrachloroethene 0,00500 0.00505 0.00502 101 100 70.0-130 0,596 20 Toluene 0.00500 000511 0,00521 102 104 70.0-130 1.94 20 1,1,1-Trichloroethane 0.00500 0.00544 000551 109 110 70.0-130 US 20 1,1,2-Trichloroethane 0.00500 0.00476 0.00478 95.2 95.6 70.0-130 0.419 20 Trichloroethene 0.00500 000537 0,00530 107 106 65.0-135 1.31 20 Trichlorofluoromelhane 0,00500 0.00543 0.00536 109 107 50.0-150 1.30 20 Vinyl chloride 0.00500 0.00485 0.00515 97.0 103 5.00-195 6.00 20 (S) Toluene-d8 97.2 98.6 80.0-120 _ (S) 4-Bromof uorobenzene 93.1 96.0 80.0-120 (8)12-Dichloroethane-d4 98.0 96.1 70.0-130 ACCOUNT PROJECT: SDG: DATETIME: PAGE: Eaton Corporation 28091-R L1170973 1223/19 09:47 13 of 25 WG1397531 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624.1 L1170973-01 Method Blank (MB) 17-7-1 (Mb) HJ4831Bb-2 12/lb/19 20'.31 MB Result Analyte - _ mg/I Acrolein U (S) Toluene-d8 103 (S4-BromolWorobenzene 976 (S)1,2-Dichlleroethone-d4 863 MB Qualifier MS MDL MB RDL mg/I mall 0.00887 0.0500 80.0-120 80.0-120 70.0-130 Laboratory Control Sample (LCS) IL(.D) HJ4d,51bb-1 12/1b/1919: 54 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte - mg/I mg/I % % Acrolein 0.0250 00185 74.0 60.0-140 (S) Toluene-d8 103 80.0-120 (S) 4-BromoOuorobenzene 98.1 80.0-120 /S) 1,2-Dichloroethone-d4 88.6 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1170973 12/23/19 09 47 14 of 25 WG1397445 QUALITY CONTROL SUMMARY ONELAB.NATIONWDE. Pesticides (GC) by Method EPA 608.3 L1170973-01 Method Blank (MB) (MB) R3483328-1 12/17/1912:32 MB Result Analyte mg/I MB Qualifier MB MDL mg/I MB RDL mg/l Aldrin U 0.00000813 0.0000500 Alpha BHC U 0.0000166 0,0600500 Beta BHC U 0.0000194 00000500 Delta BHC U 0.0000197 0.0000500 Gamma BHC U 0.0000176 0.0000500 4,4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT U 0.0000177 0.000D500 Dieldrin U O,000O0751 0.0000500 Endosulfan I U 0,0000179 0.0000500 Endosulfan 11 U 0.0000176 0,0000500 Endosulfan sulfate U 0.0000196 0.0000500 Endrin U 0.0000189 0.0000500 Endrin aldehyde U 0.0000142 0.0000500 Endrin ketone U 0.0000170 0.0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0.0000500 Hexachlorobenzene U 0.0000134 0.0000500 Methoxychlor U 0.0000193 0,0000500 Chlordane U 0.0000977 0.000500 _ Toxaphene U 0,000168 0.000500 (5) Decochlorobiphenyl 80.6 10.0-144 (5)Tetrochloro-m-xylene 74.7 10.0-135 Laboratory Control Sample (LCS) (LCS) R3483328-2 12/17/19 12:45 Spike Amount Analyze mg/I LCS Result MO LCS Rec. % Rec. Limits LCS Qualifier % Aldrin 0.00100 0.000943 94.3 420-140 _ Alpha BHC 0.00100 0,00103 103 37.0-140 Beta BHC 0.00100 0,00i0B 108 17.0-147 Delta BHC 0.00100 0.00i95 195 19.0-140 J4 P Gamma BHC 0.00100 000iO3 103 32.0-140 4,4-DDD 0.00100 0.00107 107 31.0-141 4,4-DDE 0.00100 0.000970 97.0 30.0-145 4,4-DDT 0.00100 0000941 94.1 25.0-160 Dieldrin 0.00i00 oboiO4 104 36.0-146 Ertl 1 0.00100 0.000962 96.2 45.0-153 ACCOUNT. PROJECT SDG: DATEITIME: PAGE: Eaton Corporation 28091-R L1170973 12/23/19 09:47 15 of 25 WG1397445 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Pesti Gibes (GC) by Method EPA 608.3 L1170973-01 Laboratory Control Sample (LCS) (LCS) P3483328-2 12/17/19 1245 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Endosulfan II 0.00100 0,000867 861 1,00-202 Endosulfan sulfate 0.00100 0.00104 104 26.0-144 Endrin 0.00100 0.000976 97.6 30.0-147 Endrin aldehyde 0.00100 0.000983 98.3 56.0-128 Endrin ketone 0,00100 0.000995 99.5 54.0-142 Heptachlor O.00i00 0.00212 212 34.0-140 J4P Heptachlor epoxide O.00i00 0.000957 957 37.0-142 Hexachlorobenzene 0.00100 0.000796 79.6 35.0-120 Methoxychlor 0.001D0 0.000989 98.9 44.0-160 (5) Demchlorobiphenyl 83.5 10.0-144 (5) Tebachloro-m-xylene 82,0 10.0-135 L1171043-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1171043-01 12/17/19 15:39 • (MS) R3483328-3 12/17/19 15:55 • (MSD) R3483328-4 12/17/19 16:08 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Rec Limits Analyte mg/I mg4 mg/I mg/I % % % Aldric 0.00100 U O.000812 0.000925 81.2 82.5 1 42.0-140 Alpha BHC 0.00100 U 0.000934 0,000954 934 954 1 37.0-140 Beta BHC 0.00100 U 0.000975 0,00101 97.5 10i 1 17.0-147 Delta BHC 0.00000 U 0,00175 0.00183 175 193 1 19.0-140 Gamma SHC 0,00100 U 0.000898 0,000943 89.8 94.3 1 32.0-140 4,4-DDD 0,00100 U O.00131 0.00137 131 137 1 31.0-141 44-DDE 0.00100 U 0.000911 0.000949 91.1 94.9 1 30.0-145 4 4-DDT 0.00100 U 0.000848 0,000879 84.8 879 1 25.0-160 Dieldrin 0.00100 U 0.000973 0.0010i 97.3 101 1 36.0-146 Endosulfan) 0,00100 U 0.000876 0.000903 87.6 903 1 45.0-153 Endosulfan II 0.00100 U 0.000868 0.000904 86.8 90A 1 1.00-202 Endosulfan sulfate 0,00100 U 0.000882 0.000938 88.2 93.8 1 26.0-144 Endrin O.00 OO U 0,000927 0.000953 927 953 i 30.0-147 Endrin aldehyde 0.00100 U 0,000877 0,000928 873 92.8 1 56.0-128 Endrin ketone 0,00100 U 0.000806 0.000872 80.6 87.2 1 54.0-142 Heptachlor 0,00100 U 0,00191 0.00200 191 200 1 34.0-140 Heptachlor epoxide O.00i00 U 0.000855 0.000892 85.5 892 i 370-142 Hexachlorobenzene 0.00100 U 0.0007i5 0,000699 71.5 699 1 35.0-120 Melhoxychlor 0,00100 U 0.000899 0.000951 89.9 951 1 44.0-160 (5) Decochlorobiphenyl 45.6 58.3 10.0-144 (5) Tetroch/oro-m-xylene 70.7 713 10.0-135 MS Qualifier MSD Qualifier RPD J5 P J5 P J5 P J5 P 1.59 12 3.53 4.47 4.89 448 4.09 3,59 3,73 3.04 4,06 6,15 2.77 5.65 7.37 4.60 4.24 2,26 5.62 RED Limits 35 36 44 52 39 39 35 42 49 28 53 38 48 20 20 43 26 25 22 ACCOUNT: PROJECT: SDG: DA T E/TIME: PAGE: Eaton Corporation 28091-R 11170973 12/23/19 09:47 16 of 25 WG1397445 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. ' Polychlorinated 8lphenyls (GC) by Method EPA-608.3 L1170973-01 .. Method Blank (MB) Cp (MB) R3483245-1 12/17/19 13:55 M8 Result MS Qualifier MB MOIL MB RDL �TC Analyte mg/I mg/1 mg/1 PCB 1260 U PCB 1016 U 0.000120 0.000100 0.000500 _ 0.000500 Lis PCB 1221 U 0.0000730 0.000500 PCB 1232 U 0.0000420 0.000500 4 PCB 1242 U 0.0000470 0000500 Cn PCB 1248 U PCB 1254 U 0.0000860 0.0000470 0.000500 0000500 s $r (S) Demchlorobiphenyl 77.0 10.0-144 (S)Tetrochloro-m-xylene 670 100435 Laboratory Control Sample (LCS) (LCS) R3483245-2 12/17/1914:23 Spike Amount LCS Result Anayte PCB 1260 PCB 1016 (S) Decachlorobiphenyl (S Tetrochloro-m-xylene 0,00250 0.00216 0.60250 0.00249 7GI LCS Rec. Rec Limits LCS Qualifier 864 8.00-140 9 99.6 50.0-140 Sc 84.8 10.0144 73.2 10.0135 L1171043-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) IOS) L1171043-Ot 12/17/1915:04 • (MS) R3483245-3 12/17/19 15:18 • (MSD) R3483245-4 12/17/1915:31 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Anayte mgn ni mgp mgp % % % % % PCB 1260 0.00250 U 0.00207 000220 82.8 88.0 1 8.00-140 6.09 38 PCB 1016 0.00250 U 0.00270 0.00279 108 112 i 50.0-140 3.28 36 (S) Decochlorobipherryl 77.1 78.8 10.0144 (S) retrochloro-m-xylene 68.5 73.2 10.0-135 ACCOUNT. PROJECT: SDG: Eaton Corporation 28091-R L1170973 DATE/TIME: 1223/19 09:47 PAGE: 17 of 25 WG1398261 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC7MS) by Method 625.1 L1170973-01 Method Blank IMB) (Md) R3483946-2 12/18/19 2356 ME Result ME Qualifier MBIADL MIS RDL Analyte mg/I mg/1 mg/I Acenaphihene U 0.000315 0.00700 Acenaphthylene U 0.000309 0.00100 Anthracene U 0.000291 0.00000 Azobenzene U 0.000318 0,0100 Ber idine U 0.00432 0.0100 Benzo(a)anthracene U 0.0000975 0.00100 Benzo@Ifluoranthene U 0.0000896 0.00i00 Benzo(k)fluoranihene U 0.000355 0,00100 Benzo(g,h i)perylene U 0.000161 0,00100 Benzo(a)pyrene U 0,000340 0,00100 Bis(2-chlorethexy(methane U 0,000329 D.0100 Bls(2-chloroethyl)ether U 0,00162 0,0100 Bis(2-ch1oroisooropyl)ether U 0.000445 0.0100 4-Bromophenyl-phenylether U 0,000335 Hi00 2-Chloronaphthalene U 0.000330 0.00100 4-Chlorophenyl-phenylether U 0,000303 0.0100 Chrysene U 0.000332 MOM Dibenz(a,h)anth race ne U 0.000279 0.00100 3.3-Dlchlorobenzidlne U 0,00202 0.0100 2,4-Dinitrotoluene U 0,00165 0,0100 2,6-Dinitrololuene U 0.000279 0.0100 Fluoranthene U 0.000310 0.00100 Fluorene U 0.000323 0,00100 Hexachlorobenzene U 0.000341 0.0010o Hexachlolo-13-butadiene U 0.000329 0.0100 Hexacblorocyclopentadiene U 0.00233 0.0100 Hexachlomethane U 0.000365 0.0100 Indeno(1,2,3-cdpyrene U 0,000279 0.00100 Isophorone U 0,000272 0,0100 Naphthalene U 0.000372 0.00100 Nitrobenzene U 0.000367 0.0100 n-Narosodimethylamine U 1 0,0100 n-Nitrosodiphenylamine U 0.00119 0.0100 n-Nitrosodi-n-propylamine U 0.000403 0.0100 Phenanthrene U 0.000366 0.00100 Benzylbutyl phthalate U 0.000275 0.00300 BIs(2-ethylhexyl)phtha1ate U 0,000709 0.00300 Di-n-butyl phthalate U 0.000266 0.00300 Diethyl phthalate U 0,000282 0,00300 Dimethyl phthalate U 0.000283 0.00300 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 22091-R L1170973 12/23/19 09:47 18 of 25 WG1398261 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Semi Volatile Organic Compounds 1GC/MS) by Method 625.1 L1170973-01 Method Blank (MB) (MB) R3483946-2 12/18/19 2356 MB Result Analyte mg/I MB Oualifer MB MDL mg4 MB RDL mg/I Di-n-octyl phthalate U 0.000278 0.00300 Pyrene U 0,000330 0.00100 1,2,4.Trichlorobenzene U 0.000355 0.0100 4-Chloro-3-methylphenol U 0.000263 0.0100 2-Chlorophenol U 0.000283 0.0100 2,4-Dichlorophenol U 0.000284 0.0100 2,4-Dimethylphenol U 0.000624 0.0100 4.6-Dinitro-2-methylphenol U 0.00262 0.0100 2.4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0Jy00 4-Nitrophenol U 0.00201 0.0100 Pentachlorophenol U 0.000313 0.0100 Phenol U 0.000334 0.0100 2,4.6-Trlchlorophenol U 0.000297 0.0100 (S)Nilrobenzene-d5 5L7 15.0-314 (S) 2-Fluorobiphenyl 6L7 22.0-127 (S)p-Terphenyl-dl4 73.1 29.0141 (S)PhenoFd5 21.7 8.00424 (S) 2-Fluorophenol 33.2 10.0-120 (S) 24,5-Tribromophenol 61.5 10.0-153 Method Blank (MB) (MB) P3483958-1 12/16/19 23:14 Acolyte MB Result mg/I MB Oualifer MB MDL mg4 MB RDL mg/I Acenaphthene U 0.000316 0.0010o Acenaphthylene U 0.000309 0.00100 Anthracene U 0.000291 0.00100 Azobenzene U 0.000318 idol Benzidine U 0,00432 0.0100 Benzo(a)anthracene U 0,0000975 0.00100 Benzo(b)Ruoranthene U 0,0000896 0.00100 Benzo(k)fluoranthene U 0,000355 0.00100 Benzo(g.h,i)perylene U 0.000161 0.00100 Benzo(a)pyrene U 0.000340 0.00100 Bis(2-chlorethoxy)methane U 0.000329 0.0100 Bis(2-chloroethyl)ether U 000162 0.0100 Bisl2-chloroisopropygether U 0.000445 0.0100 ACCOUNT. PROJECT SDG: DATE/TIME PAGE: Eaton Corporation 28091-R L1170973 1223/19 09:47 19.f25 WG1398261 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Metho^ 625.1 L1170973-01 Method Blank (MB) (ME) M.34b,iEb6-1 12118/i9 23:14 MB Result MB Oualifer MB MDL MB RDL Analyte mg/I me/I ni 4-Bromophenyl-phenylether U 0.000335 0.0100 2-Chloronaphfhalene U 0.000330 0,00100 4-Chlorophenyl-phenylether U 0.000303 0.0100 Chrysene U 0.000332 0.00100 Mori nth race ne U 0.000279 0,00100 3.3-Dichlorobenzidine U 0,00202 0,0100 2,4-Dinitrotoluene U 0.00i65 0.0100 2.6-Dinitrotoluene U 0.000279 0.0i00 Fluoranthene U 0,000310 0,00100 Fluorene U 0.000323 0.00100 Hexachlorobenzene U 0.000341 0.00100 Hexachloro-i3-butadiene U 0,000329 00100 Hexachlorocyclopentadiene U 0,00233 0.0100 Hexachloroethane U 0.000365 0,0100 Indeno(1,2,3-cd)pyrene U 0.000279 000100 Isophorone U 0000272 Mi00 Naphthalene U 0.000372 0,00100 N arobenzene U 0,000367 0.0100 n-Nitrosodimethylamine U 0.00126 0,0100 n-Nitrosodiphenylamine U 0,00119 0.0100 n-Nitrosodi-n-propylamine U 0.000403 0,0100 Phenanthrene U 0.000366 0.00100 Benzylbutyl phthalate U 0.000275 0.00300 Bis(2-ethylhexypphthalate U 0.000709 0.00300 Di-n-butyl phthalate U 0.000266 0.00300 Diethyl phthalate U 0.000282 0.00300 Dimeihyl phthalate U 0.000283 0,00300 Di-n-octyl phthalate U 0,000273 0.00300 Pyrene U 0.000330 000100 1.2,4-Tiichlorobenzene U 0.000355 0.0100 4-Chloro-3-methylphenol U 0,000263 0.0100 2-Chlorophenol U 0.000283 0.0100 2,4-Dichlorophenol U 0,000284 0.0100 2,4-Dimethylphenol U 0.000624 0.0100 4.6-Dinitio-2-methylphenol U 0.00262 0,0100 2,4-Dlnitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol IJ 0.0020i 0.0i00 Pentachlorophenol IJ 0.000313 0,0100 Phenol U 0.000334 0.0100 ACCOUNT: PROJECT: Eaton Corporation 26091-R SDG: L1170973 DATEMME: 12/23/19 09,47 PAGE: 20 of 25 WG1398261 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1170973-01 Method Blank (MB) (MB) R3483958-1 12/18/19 23:14 Cp MB Result MB Oualifer MB MDL MB RDL Analyte mg/I mg/1 mgn 2,4,6-Trich lomphenol U - 0.000297 0.0100 (S)Nitrobenzene-d5 H2 15.0-314 (S) 2-Fluorobiphenyl 62.0 22.0-127 (S)p-Terphenyl-d14 80.5 29.4141 (S)Phenol-d5 21.5 8,00-424 (5) 2-Fluorophenol 33.2 10.0-120 (S) 2,4,6-Tribromophenol 71.0 10.0-153 Laboratory Control Sample (LCS) (LCS) R3483946-1 12/18/19 Analyte 2336 Spike Amount mg/I LCS Result mg4 LCS Rec. % Rec. Limits LCS OualiBer % Acenaphthene 0.0500 00327 654 47.0-145 Acenaphthylene 0.0500 0.0348 69.6 33.0-145 Anthracene 0.0500 0.0359 71.8 27.0-133 Azobenzene 0.0500 0.0308 61.6 37.0-125 Benzidine 0.100 0,0587 58.7 1.00-120 Benzo(a)anthracene 0.0500 0,0345 69.0 33.0-143 Benzo(b)8uoranthene 0.0500 0.0355 71.0 24.0-159 Benzo(k)luoranthene 0.0500 0.0344 68.8 11.0-162 Benzolg.h,pperylene 0.0500 0.0334 76.8 100-219 Benzo(a)pyrene 0.0500 0.0373 74.6 17.0-163 Bis(2-chlorethoxy)methane 0.0500 0.0294 58.8 1.00-219 Bis(2-chloroethyl)ether 0.0500 0.0310 62.0 33.0-185 Bis(2-chloroisopropyl)ether 0,0500 0.0302 60A 36.0-166 4-Bromophenyl-phenylether 0.0500 0.0356 71.2 53.0-127 2-Chloronaphthalene 0,0500 0.0336 67.2 60.0-120 4-Chlorophenyl-phenylether 0,0500 0.0334 66.8 25.0-158 Chrysene 0.0500 0.0354 70.8 17.0-168 Dibenz(a,h)anthracene 0.0500 0.0374 74.8 1.00-227 3,3-Dichlorobenzidine 0100 0.0785 78.5 100-262 2,4-Dinitrotoluene 0.0500 0.0350 70.0 39.0-139 2,6-Dinitrotoluene 0.0500 0.0334 66.8 50.0-158 Fluoranthene 0.0500 0.0360 72.0 26.0-137 Fluorene 0.0500 0.0331 66.2 59.0-121 Hexachlorobenzene 0.0500 0.0338 67.6 1.00-152 Hexachloro-1,3-butadiene 0.0500 0.0262 52.4 24.0-120 Hexachlorocyclopentadiene 0.0500 00271 SU 10.0-120 ACCOUNT. _'__`__ PROJECT. - -_. _- ----SDGi_"-.: __._ _ _ __ _ - _DATE/1-IME ..-... _ _.__._ __ _- -=-. PAGE' . ---. - Eaton Corporation 28091-R L117O973 12/23/19 09:47 21 of 25 WG1398261 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1170973-01 Laboratory Control Sample (LCS) (LCS) H3483946-1 12/18/19 23:36 Spike Amount LCS Result LCS Rec. Rec. Limits Analytic mg/I mg/1 % % Hexachloroethane 0.0500 00264� 528 40.0-120 Indeno(7.2,3-cd)pyrene 0.0500 00369 73.8 1,00-171 Isophorone 0.0500 00291 582 21.0-196 Naphthalene 0.0500 00283 56.6 21.0-133 Nitrobenzene 0,0500 0,0277 554 35.0-180 n-Nitrosodimethylamine 0,0500 0.0182 364 10.0-120 n-Nitrosodiphenylamine 0.0500 0,0355 71.0 44.0-120 n-Nitrosodi-n-propylamine 0,0500 0.0314 62.8 1.00-230 Phenanthrene 0.0500 00367 73A 54.0-120 Benzylbutyl phthalate 0.0500 00334 66.8 1.00-152 BIsl2-ethylhexyl)phthalate 0,0500 0 0325 65.0 8.00-158 Di-n-butyl phthalate 0,0500 0.0355 71.0 1.00-120 Diethyl phthalate 00500 00327 65.4 1.00-120 Dimethyl phthalate 00500 0.0341 68.2 1.00-120 Di-n-octyl ohthalate 00500 0.0341 68.2 4.00-146 Pyrene 0,0500 0.0385 77.0 52.0-120 1,24-Trlchlorobenzcne 0,0500 0.0272 544 44.0-142 4-Chloro-3-methylphenol 0.0500 0,0272 544 22.0-147 2-Chlorophenol 0.0500 0,0287 574 23.0-134 2,4-Dichlorophenol 0!0500 0.0291 58.2 39.0-135 24-Dimethylphenol 00500 0.0276 55.2 32.0-120 4,6-Dinitro-2-methylphenol 0.0500 0.0352 70,4 1.00-0 24-Dlnitrophenol 0-0500 0.0327 65.4 1.00-191 2-Nitrophenol 00500 0.0303 60.6 29.0-192 4-Nitrophenol 00500 0.0141 28.2 i.00-132 Pentachloroohenol 00500 0,0363 72.6 14.0-176 Phenol 0.0500 0.0130 26.0 5.00-i20 2,4,6-Trichlorophenol 0.0500 0.0322 644 37.0-144 (S) Nitrobenzene-d5 43.4 15.0-314 (5)2-Fluorobiphenyl 62.7 22.0-127 (S)p-Terohemhd74 82.0 29.0741 (S)Phenol-d5 25.4 800-424 (S) 2-Fluorophenal 39.7 10-0-120 (S) 2,4, 6-Tribromopheno' 67.0 10.0-153 LCS Oualifier ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R 1-1170973 DATErIME: 12/23/19 09:47 PAGE: 22 of 25 GLOSSARY OF TERMS ONE LAB, NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not Cp intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer- Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, TC Sample D. Sample Matrix, Sample Preservation. Field Blanks, Field Spikes. Field Duplicates, On -Site Data, Sampling Collection Datesrrimes, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions aSs MDL NO Method Detection Limit. Not detected at the Reporting Limit (or MDL where applicable). a Cn RDL Reported Detection Limit. Red. Recovery. s RPD Relative Percent Difference. Sr SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analyses added to every blank, sample, Laboratory Control Sample/Duplicate and 6 QC (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyle The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ Gom the a AI Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor 6 These are the target %recovery ranges or %difference value that the laboratory has historically determined as normal SC Limits for the method and analyte being reported. Successful CC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RED) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was no measurable result returned for a specific analylc, the result in this column may slate 'ND" (Not Detected) or "BOL' Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyle. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (CC) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample D. including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J4 The associated batch OC was outside the established quality control range for accuracy. JS The sample matrix interfered with the ability to make any accurate determination; spike value is high. P BPI) between the primary and confirmatory analysis exceeded 40%. Pi RED value not applicable for sample concentrations less than 5 times the reporting limit. ACCOUNT: PROJECT: SDG: DATErrIME: PAGE: Eaton Corporation 28091-R L1170973 12/23n9 09:47 23 of 25 li ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. � Pace National is the only environmental laboratory accreditedkerliBed to support your work nationwide from one location. One phone call, one paint of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. Tire most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing RP time, and prevenling cross contamination, thus protecting sample In tegdty. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. ' Not all certifications held by the laboratory are applicable to the results reported In the attached report. ' Accreditation is only applicable to the test methods specified on each scope, of accreditation held by Pace National. ,TC State Accreditations Alabama 40660 Nebraska NE-OS-15-05 3 S Alaska 17-026 Nevada TN-03-2002-34 S Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 4 Cn California 2932 New Mexico' n/a Colorado TN00003 New York 11742 Connecticut PH-0797 North Carolina Env375 Sr f forum E87487 North Carolina' DW21704 Georgia NELAP North Carolina41 Georgia' 923 North Dakota R-140 6 Idaho TN00003 Ohio—VAP QGDfi9 QC Illinois 200008 Oklahoma 9915 Indiana _ C-TN-01 Oregon TN200002 7Cj1 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky1B 90010 South Carolina 84004 Kentucky' 16 South Dakota Wo Louisiana A130792 Tennosseer 2006 Louisiana' LA180010 Texas Maine TN0002 4246-18-15 JSC texasLABO15 ' LAB0152 Maryland _ 324 Utah TN00003 Massachusetts M-TNO03 Vermont W2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 _ Wyoming A21-A Third Party Federal Accieditations A2LA—ISO 17025 1461.01 AIHA-LAP, LLC EMLAP 100789 A2LA—ISO 17025° 1461.02 DOD 1461.01 Canada 146101 USDA P330-15-00234 EPA—Crypto TN00003 'Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological s Mold s Wastewater n/a Accreditation not applicable Out Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. T wA �l R 'IT NO rate v— OR MN t ID SD t VAN .� NY _ MI t t NV T NE IAt t PA t t UT t COT IL all OH � S T KS MO t yA IT p KY t T YN t Tit L t� Nor Olt AR T SC IT \` T rx MS AT GA T l.A �T T --tiJ o AK T �L O 0F$ • B O HI ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1170973 12/23/19 09:47 24 of 25 ,' . Billing Information:, _ Main Page Of _�, .• ..r: Eaton Corporation q NA Financial Services Center -1D09 Pres r - J,�/�� PO Box 818024 -"- Chit ,. - ceAnallical E N.a..•o.n:e , r 2564 Durham Road , Cleveland OH 44181 8024 Roxboro, NC 27573 -:, 3 `.� r ,�. ,,. a i ls-r' t' 1, ,, { _ 3 s <� 12mtew `rid, Q Q ' «.yn Report to. Email To: o .� E r t'rsl ,q?,a �. 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