HomeMy WebLinkAboutNCG030027_MONITORING INFO_20190918TR/D
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ QUO v I i u
YYYYMMDD
F I
AnTeN
September 12, 2019
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attn: DWQ Central Files
Dustin A. LaClair
Environmental, Health & Safety Manager
(336) 503-6538 (office)
(336) 503-6562 (fax)
d usti n lacl a i rneato n. com
REeEi V ED
SEP 18 2019
CENTL FILES
DNNR SECTION
RE: August 2019 Monthly Tier III Discharge Monitoring Report
Attached are the analytical results and associated chain of custody for the August 7, 2019 monthly Tier III
stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater
General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility.
Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North
Carolina Division of Water Quality (NCDWQ).
I certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with the system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or other persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are
significant penalties for submitting false information, including the possibility of fine and imprisonment for
knowing violations.
Since yy
Dustin A. LaClair
EHS Manager
Attachments
Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted 09/13/2019
CERTIFICATE OF COVERAGE NO. NCG03 o 0 2 7
FACILITYNAME Eaton Corporation
COUNTY Person County
PERSON COLLECTING SAMPLES Dustin LeClair
LABORATORY Pace National Lab Cert. # ENv975/Dw21704/610041
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or Q Monthly' August (monthl
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow [:]WaterSupply ❑SA
❑O Other ws-ul; Nsw
RECEIVED
SEP 18 Z019 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 i
CENTRAL FILES
DWR SECTION ❑ No discharge this period?'
OutfalLNo.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
.Standard units
'. -.
Total Copper
Total.Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks
-
-
100 mg/L or 50mg/L4
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Tool Room Trench (005)
08/07/19
0.37
17.0
7.2
0.104
0.0108
0.0210
0.815
0.03
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
Signature
Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage ..Petroleum
Non -Polar O&G/ Total
Hydrocarbons
Total Suspended
-Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50*mg/L4'
Parameter Code
-
46529
NCOIL
00552
CO530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCE5 IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES 0 NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑
REGIONAL OFFICE CONTACT NAME: Danny Smith
Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results for at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am awarftlNt thV-c,�re significany,J ajties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Permit Date: 11/1/2018-05/31/2021
OR L ZolI
Date
SWU-245, last revised 11/1/2018
Page 3 of 3
aceAnalytical
N(�
ational Center for TesGrp 8lnrwe00n
ANALYTICAL REPORT
August 19, 2019
Eaton Corporation
Sample Delivery Group:
Samples Received:
Project Number:
Description:
Site:
Report To:
L1127117
08/09/2019
28091-R
Eaton Corp Monthly Stormwater
ROXBORO,NC
Dustin LaClair
2564 Durham Road
Roxboro, NC 27573
Entire Report Reviewed By: 4�A
Heather J Wagner
Project Manager
'rounded-.
t a
are
Results red.excetolheilems ithout ed orcalibrated andelaboratory aserepvable, sampling
conductedyPac r<
port she [I not be
reproduced. N final i in fulerf rmed per
rguida approval of in laboratory. Where applicable, procedures
es ENV- O by Pace
Analytical National is performed piing conce ducted by the customer,
results relate
to to the accuracy
of
ENV-SOP-0067 and
4.
ENV dOPMTR-00 are recce sampling conducted by the Nstomer, results relate to the accuracy Onhe information provided, G
and as the samples are received.
j 41 i' i
�'
11
ACCOUNT: PROJECT: SDG: DATE/TIME:
Eaton Corporation 28091-R L1127117 08/19/1914:11.
PAGE:
1 of23_
TABLE OF CONTENTS ONELAB.NATIONWIDE.
Cp: Cover Page
1
Tc: Table of Contents
2
RP
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
3
Ss
2019-08-07-005 L1127117.01
5
Oc: Quality Control Summary
8
Cn
Gravimetric Analysis by Method 2540 D-2011
8
SSr
Wet Chemistry by Method 1664E
9
Metals (ICP) by Method 200.7
10
6
Qc
Volatile Organic Compounds (GC/MS) by Method 624.1
11
GI
Pesticides (GC) by Method EPA 608.3
13
Polychlorinated Biphenyls (GC) by Method EPA-608.3
15
Al
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
16
GI: Glossary of Terms
21
9
Sc
Al: Accreditations & Locations
22
Sc: Sample Chain of Custody
23
ACCOUNT:
PROJECT:
SDG
DATE/TIME:
PAGE:
Eaton Corporation
28091-R
L1127117
08/19/1914:11
2 of 23
SAMPLE SUMMARY ONE LAB. NATIONWIDE,
2019-08-07-005 L1127117-01 WW
Collected by
Colin Betchan
Collected date/time
08/07/1913:50
Received dateltime
08/09119 08 45
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
dale/lime
dateltime
Gravimetric Analysis by Method 2540 D-2011
WG1326774
1
08/11/1912:58
08111/1913:58
Tit
Mt. Juliet, TN
Wet Chemistry by Method 1664E
WG1328082
1
08113/1915:23
09/15/19 00,19
MBP
Mt. Juliet, TN
Metals (ICP) by Method 200.7
WG1326494
1
08/11119 07:07
08/12/19 07.40
CCE
Mt. Juliet, TN
Volatile Organic Compounds (GCIMS) by Method 6241
WG1326382
1
08/10/1913:27
08110/19 13 27
BMA
Mt. Juliet, TN
Pesticides (GC) by Method EPA 608.3
WG1326828
1
08/13/19 23:54
08/14/1913:17
LEE
Mt. Juliet, TN
Polychlorinated Biphenyls (GC) by Method EPA-608.3
WG1326828
1
08/13/19 23:54
08/14/19 21,31
RP
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG1328408
1
08/14/1916:36
08117/1912:11
AO
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Eaton Corporation 28091-R L1127117 08/19/19 14 11 3 of 23
CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
Ir
l-P
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
TC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
SS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
SSr
}�uwE,l
6QC
" V
FI
Heather J Wagner
aAl
Project Manager
BSc
ACCOUNT: PROJECT: EGG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1127117 08/19/1914:11 4 of 23
2019-08-07-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 08/07119 13:50 L1127117
Additional Information
Result
Units
Cp
Analyte
2
pH (On Site)
7.2
so
TC
Temperature (on -site)
25.5
Deg C
-
Gravimetric Analysis
by Method
2540 D-2011
aSS
Result
Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyte
mg/I
MO
mg/I
date/time
Cn
Suspended Solids
17.0
0.700
5,00
1
08/11/201913,58
WG1326774
Wet Chemistry by
Method 16646
Result
Qualifier
MDL
RDL
Dilution
Analysis
Batch
6
QC
Analyte
nigh
mg/I
wed
date/time
TPH-Oil 8 Grease
U
0.815
5.62
1
08/15/201900.19
WG1328082
7Gl
Metals (ICID) by Method 200.7
a
Result
Qualifier
MDL
RDL
Dilution
Analysis
Batch
A
Analyte
mg/I
mgA
mgn
dale/time
9
Copper
0.104
0.00700
0.0100
1
08/12/201907:40
-
WG1326494
SC
Lead
0.0108
0.00200
0.00500
1
68/12/2019 07.46
WG1326494
Zinc
0.210
0,00340
0.0500
1
08112/2019 NAB
WG1326494
Volatile Organic Compounds
(GC/MS) by Method 624.1
Result
Oualiner
MDL
RDL
Dilution
Analysis
Batch
Analyte
mgn
mg/I
mgll
date/time
Acrolein
U
J3
0.00887
0.0500
1
08/101201913:27
WG1326382
Acrylonitnio
U
0.00187
0.0100
1
08110120191327
WG1326382 .. _
Benzene
U
0.000331
0.00100
1
08/10/201913:27
WG1326382
Bromodichloromethane
U
0,000386
0.00100
1
08/10/201913:27
WG1326382
Bromoform
U
0.000469
0.00100
1
08110/201913:27
WG1326382
Bromomethane
U
J3
0,006866
6.00500
1
08110/201913:27
WG1326382 -
Carbontetrachloride
U
_
J3
0,000379
0.00100
1
08/10/20191327
WG1326382
Chlorohenzene
U
0,000348
0.00100
1
08/10/201913:27
WG1326382
Chlorodibromomethane
U
0.000327
0.00100
1
68116120191327
WG1326382
Chlorhethane
U
J3
0.000453
0.00500
1
08110120191327
WG7326382
2-Chloroethyl vinyl ether
U
J3
0.00301
0.0500
1
08/10/201913:27
WG1326382
Chloroform
U
0.000324
0.00500
I _
08IV201913:V
WG1326382
Chloromethane
U
J3
0.000276
0.00250
1
08/10/201913:27
WG1326382
1,2-Dichlorobenzene
U
0.000349
0.00100
1
08/101261g 13:27 _
WG1326382
1,3-Dichlorobenzene
U
J3
0.000220
0.00100
1
08/10/201913:27
WG1326382
14-Dichlorobenzene
U
0.000274
0.00100
1
081161201913:27
WG1326382
Dichlorodinuoromethane
U
J3
0.000551
0.00500
1
08/10/201913:27
WG1326382
1,1-Dichloroethane
U
0.000259
0.00100
1
08/16201913:27
WG1326382
1,2-Dichloroethane
U
J3
0.000361
0,00100
1
08/10/201913:27
WG1326382
1,1-Dichloroethene
U
J3
0.000398
0.00100
1
68/16261913:27
WG1326382
trans-1,2-Dichloroethene
U
J3
0000396
0.00100
1
68/161201913:27
WG1326382
9,2-Dichloropropane
U
0.000306
0.00100
1
08110120191127
WG1326382 -
cis-1.3-Dlchloropropene
U
J3
0,000418
0.00100
1
08/10/201913:27
WG1326382
trans-1,3.Dichloropropene
U
0.000419
0.00100
1
09/10/2019 13 :27
WG1326382
Ethylbenzene
U
0.000384
0.00100
1
08/10/201913:27
WG1326382
Methylene Chloride
U
J3
0,00100
0.00500
1
08/10R01913:2-7
WG1326382 _
L 2,2-Tetrachloroethane
U
0.000130
0.00100
1
08/10/201913:27
WG1326382
Tetrachloraethene
U
0.000372
-
0.00100
1
.. 08I10I20191327
..
WG1326382 ,
Toluene
U
0.000412
0.00100
1
081101201913:27
WG1326382
11,1-Trlchloroethane
U
A
0.600319
om16o
1
08/10120191327
WG1326382 -
1,1,2-Trichlorcethane
U
0.000383
0.00100
1
081101201913:27
WG1326382
ACCOUNT: PROJECT: SDG' DATE/TIME: PAGE:
Eaton Corporation 28091 R L1127117 08/19/1914:11 5 of 23
2019-08-07-005
SAMPLE
RESULTS - 01
ONE LAB. NATIONWIDE.
Collected tlateltlme: 08/07/19 13:50
L1127117
Volatile Organic Compounds
(GC/MS)
by Method 624.1
Gp
Result
Qualifier
MDL RDL
Dilution Analysis
Batch
Analyze mg/I
rol mg/l
date/lime
Trichloroethene U
0,000398 0.00100
1 08/101201913.27
WG1326382
z `- Tc
Trichlorolluoromethane U
J3
0.00120 0.00500
1 08/10/201913:27
WG1326382
Vinyl chloride U
J3
0.000259 0.00100
1 08/10/201913:27
WG1326382
3
(S)7aluene-d8 116
80.0-120
08/1020191327
WG1326382
SS
(S)o,gaThduorOtaluene 0.000
J2
80.0-120
08/10/20191327
WG1326382
(S)4-Bromolluorobenzene 99,3
80.0-120
08/1020191327
WG1326382
Cn
(S) 1,2 Dichloroethone-d4 102
70.0-130
08/102019 7377
W61326362
Pesticides (GC) by Method EPA 608.3
Result Qualifier
MDL
RDL
Dilution
Analysis
Batch
a
Analyle
mg/1
mgll
mg/1
date/time
Qe
Aldrin
U
0.00000813
0.0000500
1
08/141201913:17
WG1326829
Alpha BHC
U
0.0000166
0.0000500
1
08/14/201913:17
W66A826
7GI
Beta BHC
U
0.0000184
0.0000500
_
1
08114/201913:17
WG1326828
Delta BHC
U
0.0000197
0.0000500
1
_ .. _.
08/t4/201913:17
WG1326828,
e
Gamma BHC
U
0.0000176
0,0000500
1
08114/201913:17
WG1326828
Al
'Chlordane
U
o.0000977
o.000500
1
08/14/26161317
WG1326828
44-DDD
U
0.0000170
0.0000500
1
08/141201913:17
WG7326828
SC
44-DDE
U
0.0000164
0.0000500
1
08114/201913:17
WG1326828
,
4,4-DDT
U
0.0000177
0.0000500
1
08/141201913:17
WG1326828
upland
U
0.00000751
o.0oo0500
1
68/14120191*317
WG1326828
Endosulfan I
u
0.0060179
0,0000506
1
08/14120191317
WG1326828
Endosulfan II
u
0.0000176
0.0000500
1
68/14/201913:17
WG7326828
Endosulfan sulfate
U
0.0000196
6.0060506
1
08114/20191317
WG1326828
Endrin
U
0.0000189
0.0000500
1
08/141201613:17
WG7326828
Endrin aldehyde
U
0.0000142
0.0000500
1
08/14/201913:17
WG1326828
Endrin ketone
u
o.0000170
o.0000500
1
08/14/20191317
WG7326828
Heptachlor
U
0.0000108
0.0000500
1
08Y14/201913:17
WG1326828
Heptachlor epoxide
U-
0.000O175
0.0000500
1
08114/26191317
WG7326828
Hexachlorobenzene
U
0.0000134
0.0000500
1
08114/201913:17
WG1326828
'Methoxychlor
U
0.0000193
0.0000500
1
08/14/201913:17
WG7326828
Toxaphene
u
0.000168
0.000500
1
08114/201913:17
WG1326828
(5) Demchlordbiphenyl
69.9
10.0444
08/142019 i397
WG7326828
'
IS) Tetrochloro-m-xylene
7i6
10.0-135
08114201913.17
WG1326828
Polychlorinated Biphenyls
(GC) by Method EPA-608.3
Result Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyle
mg4
mg/I
r ll
date/time
PCB 1016
U
0.000100
0.000500
1
08/14/2019 21:31
WG1326828
PCB 1221
u
0.0000730
0.000500
1
08114/2019 2131
WG1326828
PCB 1232
U
0.0000420
0.000500
1
08114/2019 21:31
WG1326828
PCB 12Q
U
o.0060470
0.000500
1
08114/2019 21:31
WG1326828
PC81246
U
0.0000860
0.000500
1
OB114/20192131
WG1326828
PCB 1254
U
0.0000470
6.006500
1
0811412619 2131
WG1326828
PCB 1260
U
0.000120
0.000500
1
08/14/2019 2131
WG1326828
(S)Decochlorr iphenyl
73.0
10.0-144
08114201921,*31
WG1326828
QTetrochloro-m-xylene
82..9
100-135
081141207927,31
WG1326828
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyle
mg/I
mg/I
mg/1
date/time
Acenaphthene
U
0.000316
0.00100
1
08/17/201912:11
WG1328408
Acenaph[hylene
U .
0.000309
0.00100
1
_.
08/17/201912:11
WG1326406
Anthracene
U
0.000291
0.00100
1
08/17/201912:11
WG1328408
Benzidine
U
6.00432
0.0100
1
0M7/201912:11
M1328408
ACCOUNT:
PROJECT:
5DG
DATE/TME: _
PAGE:
Eaton Corporation
28091-R
L1127117
08/19/19 14:11
6 of 23
2019-08-07-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/lime: 08/07119 13:50 L1127117
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Oualifer 14DL
RDL
Dilution
Analysis
Batch
Analyle
mg/I
mg/I
mg/I
date/time
Benzo(a)anlhracene
U
0,0000975
0,00100
1
08/17/201912:11
WG1328408
Benzo(b)fluoranthene
U
0.0000896
0.00100
1
08/17/201912:11
WG1328408
Benzo(k)fluoranthene
U
0.000355
0.00100
1
08/17/201912:11
WG1328408
Senzo(g,h,i)perylene
U
0.000161
0.00100
1
08117/2019 12:11
WG1328408
6enzo(a)pyrene
U
0.000340
0,00100
1
08/17/2019 1211
WG1328408
Bis(2-chlorethoxy)melhane
U
0,000329
0.0100
1
08117/261912:11
WG1321I
Bis(2-chloroethyl)ether
U
0,00162
0,0100
1
08117/201912:11
WG1328408
Bis(2-chloroisopropyl)e[her
U
0.000445
0.0100
1
08/17/2019 1 2:11
WG1328468
4-Bromophenyl-phenylether
U
0.000335
0.0100
1
08/17/201912:11
WG1328408
2-Chloronaphthalene
U
J4 0,000330
0.00100
1
08/17/2019 12:11
WG1328408 -
4-Chlorophenyhphenylether
U
0.000303
0.0100
1
08117/201912:11
WG1328408
Chrysene
U
0.000332
0,00100
1
68117/201912.*N
WG1328408
Dibenz(a,h)anthracene
U
0,000279
0.00100
1
09/171201912:11
WG1328408
3,3 Dichlorobenzidine
U
0.00202
0.0106
1
08/17/201912,11
WG1328408
2.4-Dinitrotoluene
U
0.00165
0.0100
1
08/17/201912:11
WG1328408
2,6-Dinitrotoluene
U
0.000279
0.0100
1
.
08/17I201912:11
..
W61328408
1,2-Diphenylhydrazine
U
0.000318
0.0100
1
08/17/201912:11
WG1328408
Fluoranthene
U
0,000316
0.00100
1
08117/261912:11
WG1328408 - -
Fluorene
U
0.000323
0.00100
1
08/17/201912:11
WG1328408
Hexachlorobenzene
U
0.000341
0.00100
1
08/171201912:11
WG1328408
Hexachloro-1.3-butadiene
U
0.000329
0.0100
1
08/17/201912:11
WG1328408
Hexachlorocyclopentaoiene
U
6,00233
0.0100
1
08/1712616 i2:11
WG1328401i
Hexachloroethane
U
0,000365
0.0100
1
08/17/201912:11
WG1328408
Indeno(1,2,3-cd)pyrene
U
0.000279
0.00100
1
08I17501972:71
WG7328408
Isophorone
U
0,000272
0.0106
1
08/171201912:11
WG1328408
Naphthalene
U
0.000372
0.00100
1
08I17/201912:11
WG7328408
Nitrobenzene
U
0.000367
0.0100
1
08117/201912:11
WG1328408
nZarosodimethylamine
U
0.00126
0.0100
1
08/17/201912:11
WG1328408
n-Nitrosodiphenytamine
U
0.00119
0,0100
1
08/171201912:11
WG1328408
n-Nitrosodi-n-propylamine
U
- 0.000403
0,0100
1
08/17/201912:11
WGI328408
Phenanthrene
U
0,000366
0.00100
1
08/17/201912:11
WG1328408
Seniylbutyl phthalate
U
0.000275
0.00300
1
08/17/201912:11
WG1328408
Bis(2-ethy1hexypphthalate
U
0,006709
0.00300
1
08/17/201912:11
WG1328408
Dimbulyl phthalate
U
0.000266
0.00300
1
08/17I20191211
WG1328408
Diethyl phthalate
U
0.000282
0.00300
1
08117/201912:It
WG1328408
Dimethyl phthalate
U
0.000283
0.00300
1
08/17/201912.11
WGI328408
Di-moctyl phthalate
U
6.600278
0,00300
1
08/17/201912:11
WG1328408
Pyrene
U
0.000330
0.00100
1
U/17001912:11
WG1328408
1,2,4-Trichlorobenzene
U
0,000355
0.0100
1
08/17/201912:11
WG1328408
4-Chloro3-methylphenol
U
0.600263
0.0106
1
Cilh7/20191211
WG1328408 -
2-Chlorophenol
U
0.000283
0.0100
1
081171201912:11
WG1328408
2,4.Dichlorophenol
U
/ 0.000284
0.0100
1
08/17/2019 1211
WG1328408
2,4-Dimethylphenol
U
0.000624
0.0100
1
08/17/201912:11
WG1328408
4,6-Dlnitro-2-methylphenol
U
0.00262
0.0100
1
081171201912:11
WG1328408
24-Dinitrophenol
U
0.00325
0,0100
1
08117/201912:11
WG1328408
2-Nitrophenol
U
o.000320
viioo
1
08/1D201912:11
W(37328408
4-Nitrophenol
U
0,00201
0.0100
1
08/17/201912,11
WG1328408
Pentachlorophenol
U
0.000313
0.0100
1
08/17/2019 12.11
WG1328408
Phenol
0.000799
J 0.000334
0.0100
1
08/17/201912:11
WG1328408
2,4,6-Trichlorophenol
U
0.000297
0.0100
1
080/201912:11
WG1328408
(5)2-Fluorophenol
11.6
0.0-120
0811712019 12 IF
WG1328408
IS)Phenol-d5
13.9
800-424
087177201912.11
WG132JR408
/5/Nitrobenzene-d5
39.2
15.0-314
081171201912: 11
WG1328408
(S)2-Fluoroblphenyl
42.7
22.0-127
087177201912:11
WM1 itl08 -
(S)2,4,6-Fribromophenol
50.1
10.0-153
081171201912.17
WG1328408
(S)p-Terphenyl-d14
50.5
29.0-741
08h77201912. 11
WG132840§
ACCOUNT: PROJECT: SDG DATE/TIME: PAGE:
Eaton Corporation 28091-R L1127117 08/19/19 14.11 7 of 23
WG1326774 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE,
Gravimetric Analysis by Method 2540 'D-2011 L1127117 01 _
Method Blank (MB)
(MB) R3439484-1 08/11/19 13:38
MB Result M8 Qualifier MB MOIL MB RDL
Analyte mg/I mgA mg/I
Suspended Solids U
0.350 2.50
L1127118-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1127118-01 08/11/19 13:58 - (DUP) R3439484-3 08/11/19 13:58
Original Result
DUP Result
Dilution DUP RPD
DUPOualifier DUP RPD
Limits
Analyte mg/I
III
%
%
Suspended Solids 72.0
80.0
1 10.5
P1 5
L1127126-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1127126-01 08/11/19 13:58 - (DUP) R3439484-4 08/11/1913:58
Original Result DUP Result Dilution DUPRPD DUP Qualifier DUPRPD
Limits
Analyze mg/I mg/1 % %
Suspended Solids 42.0 43.0 1 2.35 5
Laboratory Control Sample (LCS)
(LCS) R3439484-2 08/11/19 13:58
Spike Amount LCS Result LCS Red. Red. Limits LCS Qualifier
Analyze mg/1 mgA % %
Suspended Solids 773 872 113 85.0-115
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE:
Eaton Corporation 28091-R L1127117 08/19/19 14 11 8 of 23
WG1328082
QUALITY
CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Wet Chemistry by Method 16648
L1127117-01. -
Method Blank (MB)
C
(MB) R3440594-1 08/15/19 0019
p
M8 Result MB Qualifier MB MDL
MB ROL
2
Analyle mg/I mg/I
mg/I
TC
TPH - Oil & Grease U 0.725
5.00
ass
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
4Cn
(LCS) R3440594-2 08/15/19 00:19 • (LCSD) R3440594-3 08/15/19 0019
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec.
Rec. Limits LCS Oualifier LCSD Oualifier RPD RPD Limits
s
Analyte mgA mg/I mgA
% %
% % %
$r
TPH -Oil&Grease 20.0 15.0 15.5
75.0 77.5
64.0-132 3.28 34
7G1
8AI
9$C
ACCOUNTPROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporatlon - 28091-R' L1127117 08/1911914:11 - 9 of 23
WG1326494 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
_Metals (ICP) by _Method 200.7 L1127117-01
Method Blank (MB)
(MB) R3439540-1 08/12/19 07:32
Cp
2
MB Result MB Qualifier MB MDL MB RDL
Analyse mg/I mg4 mg/I
TC
Copper U 0.00700 0.0100
Lead 0 OA0200 0.00500
a
SS
Zinc 0.00386 J 0,00340 0.0500
4Cn
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3439540-2 08/12/19 07:34 • (LCSD) R3439540-3 08/12/19 07:37
FriSpike
Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyse mg/I mg/I mg/I % % %
%
%
Copper 1.00 1.00 1.02 100 102 85.0-115
240
20
Lead 1A0 1.04 LOS 104 105 85.0-115
1,40
20
7
Zinc 1.00 1.02 1.04 102 104 89.0-115
1.80
20
G
L1127117-01 Original Sample Matrix Spike Matrix Spike Duplicate
8AI
(OS) • (MS) • (MSD)
(OS) L1127117-01 08/12/19 07:40 • (MS) R3439540-5 08/12/19 07:45 • (MSD) R3439540-6 08/12/19 07:47
y
Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec
Dilution Rec Limits
MS Qualifier
MSD Qualifier
RPD
RPD Limits
SC
Analyte mg/1 mg/I mg/I mg/I % %
%
%
%
Copper 1.00 0.104 1.21 1L23 ill 112
1 70.0-130
1,09
20
Lead 1.00 0.0108 1.09 1.09 107 108
1 70.0-130
0.570
20
Zinc 1.00 0.210 1.26 1.27 105 106
1 70.0-130
0.658
20
L1126775-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1126775-01 08/12/19 07:50 • (MS) R3439540-7 08/12/19 07:52 • (MSD) R3439540-8 08/12/19 07:55
Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec.
Dilution Rec Limits
MS Qualifier
MSD Qualifier
RPD
RPD Limits
Analyse mg11 mg0 mg/I mg/I % %
%
%
%
Copper 1.00 0.0156 1A7 L07 105 105
1 70.0-130
0.00703
20
Lead 1.00 ND 108 LOU1707�- 107
1. 70.0-130
0.388
20
Zinc 1,00 ND 109 1.09 105 105
1 70.0-130
0.442
20
ACCOUNT: PROJECT:. - SDG: - DATE/TIME PAGE:
Eaton Corporation 28091-R L1127117'. 08/19/1914:11 10 of 23
WG1326382
QUALITY
CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Volatile, Organic Compounds (GC/MS)
by Method 624.1
L1127117-01
Method Blank (MB)
CP
(MB) R3439212-3 08/10/1910:26
MB Result
MB Oualifer MB MDL
MB RDL
2
Analyte mg/I
thigh
mg/I
TC
Acrolein U
0.00887
0.0500
Acrylonitrile U
0.00187
0.0100
a
SS
Benzene U
0.000331
0.00100
Bromodichloromethane U
0.000380
0.00100
4
Bromoform U
0.000469
0.00100
Cn
Bromomemane U
0.000866
0.00500
Carbon tetrachloride U
0.000379
0.00100
a
Sr
Chlorobenzene U
0.000348
0MI00
Chlorodibromomethane U
_
0.000327
0A0100
Chloroethane U
0A00453
0.00500
2-Chioroethyl vinyl ether U
U0301
0.0500
Chloroform U
0.000324
aomo0
7G�
Chloromethane U
0.000276
0.00250
1,2-Dichlorobenzene U
- 0.000349
0.00100
e
1,3-Dichlorobenzene U
0.000220
0.00100
A�
1,4-Dichlorobenzene U
0.000274
0.00100
_
DichlorodiRuoromethane U
0.000551
0M500
s
SC
1,1-Dichloroethane U
_
0.000259
.0.00700 _
1,2-Dichloroethane U
0.000361
0.00100
1,1-Dichloroethene U
0.000398
_ 0.00100
trans-1,2-Dichloroethene U
0.000396
0.00100
'1.2-Dichloropropane U
0.000306
0.00100
cis-1,3-Dichloropropene U
0.000418
0.00100
.trans-1,3-Dichloropropene U
0.000419
.0.00100
Ethylbenzene U
0.000384
0.00100
Methylene Chloride U
Owif:0
0.00500.
-
71,2,2-Tetrachloroethane U
0.000130
0.00100
Tetrachloroethene U
0A00372
0.00100
Toluene U
0.000412
0.00100
1,1,1-Trichloroethane U
0A00319
0.00100
_
1,1,2-Trichloroethane U
OA00383
0.00100
Trichloroethene U
0.000398
OA0100
Trichlorof uoromethane U
0,00120
0,00500
Vinyl chloride U
_ 0.000259
OM100
(S)Toluene-dB 998
80.0-120
(S)a,o,o-Tri7luorozDfuene 0..060
J2
80.0-120
(S)1,2-Dichlooethane-d4 104
70 0-130
(S)4-BromDOuorobenzene 93.3
80.0-120
ACCOUNT:
PROJECT: -
SDG:
DATMIME_ PAGE-
-Eaton Corporation
.28091-R'
-L1127117
08119/1914:11 11 of 23
WG1326382 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic. Compounds_(GC/MS by Method 524.1 L1127117-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3439212-1 08/10/19 09:26 •
(LCSD) R3439212-2 08/10/19 09:46
Spike Amount
LCS Result
LCSD Result
LCS Red.
LCSD Rec.
Red. Limits
LCS Oualifer LCSD Oualifler
RPD
RPD Limits
Analyte
mg/I
mg/I
mgA
%
%
%
%
%
Acroleln
0.125
0.0996
0.124
79.7
99.5
60.0-140
J3
22.1
20
Acrylomtrile
0.125
0.118
0.124
94.7
99.6
60.0-140
5.03
20
Benzene
0.0250
0.0213
0.0256
85.3
102
65.0-135
BK4
20
Bromobichloromethane
0.0250
0.0193
0.0236
77.2
94.2
70.0-135
19.9
20
Bromoform
0.0250
0.0205
0.0190
82.0
76.2
70.0-130
7.39
20
Bromomethane
0.0250
�0,0154
0.0208
61.7
83.2
15.0-185
J3
29.6
20
Carbon tetrachloride
0.0250
0,0207
0.0268
82.8
107
70.0-130
J3
25.8
20
Chlorobenzene
0.0250
0.0230
0.0251
92.0
100
65.0-135
8.64
20
Chlorodibromomethane
0.0250
0.0234
0.0221
934
88.4
70.0-135
5,59
20
Chloroethane
0.0250
0.0217
0.0300
86.8
120
40.0-160
J3
32.1
20
2-Chloroethyl vinyl ether
0.125
0.104
0129
83.3
103
0.100-225
J3
21.5
20
Chloroform
0.0250
0,0219
BMW
87.5
104
70.0-135
17.1,
20
Chloromethane
0.0250
0.0274
0.0386
110
155
0.160-205
J3
34.0
20
1;2-Dichlorobenzene
0.0250
0,0226
0.0262
90.5
105
65.0-135
14.5
20
1,3-Dichlorobenzene
0.0250
0.0227
0.0285
90.8
114
70.0-130
J3
22.5
20
1,4-Dichlorobenzene
0.0250
0.0225
0.0267
89.9
107
650-135
17.3
20
Dichlorodilluoromethane
0,0250
0,0190
0,0270
76.2
108
49.0-155
J3
34.7
20
1,14Jichloroethane
0.0250
0.0222
0,0263
kO
105
70.0-130
16.7
20
1.2-Dichloroethane
0.0250
0,0222
0.0279
89.0
112
70.0-130
J3
22.5
20
1,1-Dichloroethene
O.o250
0,0214
0.0308
85.7
123
50.0-150
.J3
35.9
20
trans-1,2-Dichloroethene
0.0250
0.0224
0,0295
89.6
118
70.0-130
J3
27.4
20
1,2-Dichloropropane
0.0250
0.0210
0,0257
84.0
103
35.0-165
_
20.0
20
cis-1,3-Dichloropropene
0.0250
0.0166
0,0243
66.3
97.1
25.0-175
J3
37.7
20
trans-1,3-Dichloropropene
0.0250
0.0185
0.0M
74.2
76.7
50.0-150
3.25
20
Ethylbenzene
0.0250
0.0231
0,0252
92.5
101
60.0-140
8,65
20
Methylene Chloride 0.0250 0.0215 0.0295 85.9 118 60.0-140 J3 31.4 20
1,1,2,2-Tetrachloroethane
0.0250
0,0195
0.0225
7T9
90.0
60.0-140
Tebachlomethene
0.0250
0.0249
0.6255
99.7
102
70.0-130
Toluene
0,0250
0.0242
0.0237
9C7
94.7
70.0-130
771-Trichloroethane
0,0250
0.0211
0.0269
8T5
108
70.0-130
1,1,2-Trichloroethane
0.0250
0.0217
0,0245
86.9
97.9
70.0-130
Trichloroethene
0.0250
0.0219
BMW
87.6
103
65:0-135
Trichlorofluoromethane
0.0250
0.0242
0-0331
96.8
133
50.0-150
'Vinyl chloride
0.0250.
0.0214
0.0287
85.8
115,
5.00-195
(S) Toluene-d8
117
95.8
80.0420
(S)¢o,o-TriOuorotoluene
-
0.000
0.000,
80.0420 J2
(S) 1,2-Dichloroethene-d4
96.1
IN
70.0-130
(S) 4-Bromolluorobenzene
100
102" `
"80.0-120
14.4
20
2.10
20
2.13
20
J3
-�
24.1; -
20
11.8
20
15.8
20 - - -
J3
31.2
20
J3
- 28.8
20
- J2
ACCOUNT: PROJECT:
Eaton Corporation 28091-R
SDG:
L1127117
DATE/TIME: PAGE:
08/19/19 14:11 12 of 23
WG1326828 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Pesticides (GC) by Method .EPA 608.3 L1127117.01
Method Blank (MB) C
(ME) R3440198-2 08/14/19
Analyte
08:51
MB Result MB Oualifer
mg/I
MB MDL
mg/I
MB RDL
mg/I
Aldrin
U
0.00000813
O.0000500
Alpha BHC
U
0.0000166
0.0000500
Beta BHC
U
0.0000184
0,0000500
Delta BHC
U
0,0060197
0.0000500
Gamma BHC
U
0,0000176
0.0000500
4,4-DOD
U
0.0000170
0.0006500
4,4-DDE
U
0.0000164
0.0000500
4,4-DDT -
U - -
0.0060177
0.0000500
Dieldrin
U
0.00000751
0.0000500
Endosulfan I
U
o.0o00179
o.0000500
Endosulfan II
U
H000176
0.0000500
. Endosulfan sulfate
U
0.0000196
0.0000500
Endrin
U
0.0000189
0.0000500
Endrin aldehyde
U
0,0000142
0.0000500
Endrin ketone
U
0,0000170
0,0000500
Heptachlor
U
0:0000108
0.0000500
Heptachlor epoxide
U
0.0000175
0,0000500
Hexachlorobenzene
U
0.0000134.
0,0000500
Methoxychlor
U
0.0000193
H000500
Chlordane -
U
0MG0977
0.000500
Toxaphene
U
OM0168
O.000500
(S) Decochlorobiphenyl.
74.6
_
10:0-144 -
(S)Telmchloro-m-xylene
93.9
10.0-135
Laboratory Control Sample (LCS)
(LCS) R3440198-1 08/14/19 08:36
Spike Amount
LCS Result
-CS Rec.
Rec. Limlts LCS Oualifer
Analyte
mg/I
mgll
%
%
Aldrin
0.00100
0.000907
90.7
42.0-140
Alpha BHC
- 0.00100'
0A00987-
- 96.7 - -
37.0-140
Beta BHC
0.00100
O.000946
94.6
17.0-147
Delta BHC
0.00100
0A00986-
96.6
19.0-140
Gamma BHC
0.00100
O.000959
95.9
32.0-140
4,4-DDD
0.00100`
0,000997-
99.7
31.0-141
4,4-DDE
0.00100
0,00104
104
30.0-145
4,4-DDT
0,00100
OA00983
_ 98.3 _
25.0-160-
Dieldnn
0.00100
OA00976
9T6
36.0-146
Endosulfadl
0.00100
0.000954
95.4
45.0-153
ACCOUNT:.
PROJECT:,
Eaton Corporation
28091-R
SDG:. DATETTIME: PAGE:
L1127117 08/19/19 14:11 13 of 23
WG1326828 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. 410
Pesticides (GC) by Method EPA 608.3. L1127117.01 _
Laboratory Control Sample (LCS)
(LCS) R3440198-1 08/14/19
0636
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Oualifier
Analyte
mgll
mgA
%
%
Endosulfan II
0.00100
0,000945
94.5
1.00-202
Endosulfan sulfate
0.00100
0.000922
92.2
26.0-144
Endrin
0.00100
0.00100
100
30.0-147
Endrin aldehyde -
-0.00100
0,000928
92.8
56.6-128
Endrin ketone
0.00100
0.000917
91.7
54.0-142
Heptachlor
0.00100
0.000970
97.0
34.0-140
Heptachlor epoxide
0.00100
0.00103
103
37.0-142
Hexachlorobenzene
0.00100
0,000929
92.9
35.0-120-
Methoxychlor
0.00100
0,000992
99.2
44.0-160
(S) Decochlorobiphenyl
82.7
10.0-144
(S) Tetrochloro-m-xylene
90.5
10.0-135
L1126776-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1126776-01 08/14/19 12:03 • (MS) R3440198-3 08/14/1912:18 •
(MSD) R3440198-4 08/14/19 12:33
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Bee.
Dilution Bee Limits
MS Oualifier
MSD Oualifier
RPD
RPD Limits
Analyte
mgA
mgA
mgA
mg/I
%
%
%
%
%
Aldrin
0.00100
U
0.000142
0.000195
14.2
19.5
1 42.0-140
J6
J6
31.5
35
Alpha BHC
0,00100
U
0.000209
0.000217
20.9
21.7
1-.37.0-140
J6
J6
3.76
36
Beta BHC
0.00100
U
0.0000686
0.0000992
6.86
9.92
1 17.0-147
J6
J6
36.5
44
Delta BHC
0.00100
U
0.000380
0.006572
38.0
5T2
1 19,0-140
P
P
40.3
52
Gamma BHC
0.00100
U
0.0000902
0.000133
9.02
13.3
1 32.0-140
J6
J6
38.4
39
4,4-DDD _
0.00100
U
0.000208
0.000239
20.8
23.9
1 31.0-141-
J6 P._
J6 P
13.9
39
4,4-DDE
0.00100
U
0,0000882
0,000127
8.82
12.7
1 30.0-145
J6
J3 J6
36.1
35
4,4-DDT
0.00100
U
0,000130
0.000178
13.0
17.8
1. 25.0-160
J6
J6
31.2
42
Dieldrin
0.00100
U
0,000120
0.000182
12.0
18.2
1 36.0-146
J6
J6
41.1
49
Endosulfan )
0.00100
U
0.000107
0.000158
10.7
15.8
1 45.0-153
J6 P.
J3 J6P
38.5
28
Endosulfan II
0.00100
U
0.000111
0.000155
11.1
15.5
1 1.00-202
33.1
53
Endosulfan sulfate
0.00100
U
0.000158
0.000166
15.8
-16.6
1 26.0-144
J6
J6
4.94
38
Endrin
0.00100
U
0.000125
0.000163
12.5
16.3
1 30.0-147
J6P
J6
26.4
48
Endrin aldehyde
0.00100
U
0.000109
0.000115
10.9 -
11.5.
1 56.0-128
J6
J6
5.36
20
Endrin ketone
0.00100
U
0.000353
0.000382
35.3
38.2
1 54.0-142
J6 P
J6 P
7.89
20
Heptachlor
0.00100
U
0.000159
0.000286
.15-9
26.6
1 34.0-140•
J6
J3 J6
57.1'
43
Heptachlor epoxide
0.00100
U
0.000159
0.000205
15.9
20.5
1 37.0-142
J6
J6
25.3
26
-Hexachlorobenzene
0.00100
U
0.000133
0.000190-
13.3 -
19.0.
_ 1;. 35.0-120;:
J6
J3:J6.
35.3
25
Methoxychlor
0.00100
U
0.000140
0.000209
14D
20R
1 44.0-160
J6 P
J3 J6
39.5
22
(S) Decochlorobiphenyl
-
- _
_
14.7
19.1
10.0-144-
(S) Tetrochlara-m-xylerre
_
11.8
17.0
10.0735
ACCOUNT: PROJECT: SDG DATEriIME: PAGE
Eaton Corporation 28091-R - L1127117.' 08/19/1914:11 14 of 23
WG1326828
QUALITY CONTROL SUMMARY
ONE LAB, NATIONWIDE.
Polychlorinated Biphenyls (GC) by Method EPA-608.3
L1127117 01 -
Method Blank (MB)
1C
(Me) R3440274-1 08/14/19 09:27
p
i
MB Result MB Qualifier MB MOIL MB ROL
Analyte mgA
mgA
mgA
TC
PCB 1260 U
0.000120
0.000500
PCB 1016 U
0.000100
0.000500
a
SS
PCB 1221 U
0.0006730
0.600500
PC131232 U
0.0000420
0.000500 _
n
PCB 1242 U
0.0000470
0.000500
Cn
PCB 1248 U
0.0000860
0.000500
_
PCB 1254 U
0.0600470
0-000500
s
Sr
(S)Decachlorobiphenyl 947
10.0-144
(S) Tetrochloro-m-xylene 111
10.0-135
Laboratory Control Sample (LCS)
7GI
(LCS) R3440274-2 08/14/19 09:33
aAl
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg11 mgA
%
%
PCB 1260 0.00250 0.00270
PCB 1016 OD0250 0.00280
108
112
8.00-140
50.0-140
9$C
(5) Decochlorobiphenyl
116
10.0-144
(S) Tetrochloro-m-xylene
110
10.0-135
L1126776-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1126776-01 08/15/19 08:19 - (MS) R3440770-1 08/15/19 08:32 - (MSD) R3440770-2 O8/15/19 08:44
Analyze
Spike Amount
mg/I
Original Result
mg/I
MS Result
mgA
MSD Result
mgA
MS Rec.
%
MSD Red.
%
Dilution Rec. Limits
%
MS Oualifier
MSD Qualifier RPD
%
RPD Limits
%
PCB 1260
0.00250
U
0.00212
0.00273
84.8
109
1 8.00-140
P
252
38
PCB 1016
0.00250
U
D00716
0.0104
286
416
1 50.0-140
J5
J3 J5 36.9
36
/S) Decochlorobiphenyl
16.5
193
100-144
'
(S) retrochloro-m-xylene
12.3
170
.10,0-135
ACCOUNT:
Eaton Corporation
"PROJECT:' - - SDG
28091-R L1127117
DATErFIME:
O8/19/19 14:11
PAGE:
15 of 23
WG1328408
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS)'by Method 625.1
L1127117-01
Method Blank (MB)
CP
❑
(MB) R3441432-2 08/16/1917:04
MB Result
MB Oualifter MB MDL
M8 RDL
7
Analyte
mg/I
mg/I
mg/I
TC
Acenaphthene
U
0.000316
0.00100
Acenaphthylene
U
0.000309
0.00100
3
SS
Anthracene
U
0.000291
0.00100
Benzitline
U
0.00432
0.0100
Benzo(a)anthracene
U
0.0000975
0.00100
Cn
Benzo(b)fluoranthene
U
0.0000896
0.00100
Benzo(k)fluoranthene
U
0.000355
_
0.00100
Benzo(g,h,Qperylene
U
0.000161
0.00100
Benzo(a)pyrene
U
0,000340
0.00100
Bis(2-chlorethoxy)methane
U
0.000329
0.0100
-
Bis(2-chloroethygether
U
0.00162
0.0100
Bis(2-chloroisopropyl)ether
U
0.000445
0.0100
7G
4-Bromophenyl-phenylether
U
0.000335
0.0100
2-Chloronaphthalene
U
0.000330
0.00100 _
a
4-Chlorophenyl-phenyle[her
U
0.000303
0.0100
AI
Chysene
U
0.000332
0.00100
Dibenz(a,h)amhracene
U
0,000279
0.00100
SC
3,3-Dichlorobenzidine
U
0.00202
0.0100 _
2,4-Dinitrotoluene
U
0.00165
0.0100
2,6-Dinitrotoluene
U
0.000279
0.0100
_
Fluoranthene
U
0.000310
0.00100
Fluorene
U
0.000323
0,00100
Hexachlorobenzene
U
0.000341
0.00100
Hexachloro-13-butadiene
U
0.000329
0.0100
Hexachlorocyclopentadiene
U
0,00233
0.0100
'Hexachloroethane
U
0.000365 _
0.0100
Indeno(1,2,3-cd)pyrene
U
0.000279
0.00100
Isophorone
U
0.000272
0,0100 _
Naphthalene
U
0.000372
0.00100
Nitrobenzene -
U
0.000367
0.0100 _
n-Nitrosodimethylamine
U
0.00126
0.0100
n-Nitrosotliphenylamine
U
0.00119
0.0100 .
n-NiImsod1-n-propylamine
U
0,000403
0,0100
Phenanthrene
U
0.000366
0.00100
Benzylbutyl phthalate
U
0.000275
0.00300
Bis(2-ethylhexyf)phihalate
U
0.000709
0.00300
Di-n-butyl phthalate
U
0.000266
0.00300
.Diethyl phthalate
U
0.000282
.0.00300
Dimethyl phthalate
U
0.000283
0.00300 -
Dl-n-octyl phthalate
U:
- 0.000278
'0.00300 `
ACCOUNT: PROJECT: 'SDG 'DATE,71ME: PAGE:
Eaton Corporation 28091-R L1127117 08/19/1914:11 16.123
WG1328408
QUALITY CONTROL SUMMARY
ONE LAB.NATIONwi0F.
Semi Volatile. Organic Compounds
(GC/MS) by Method 625.1
L1127117-01
Method Blank (MB)
Cp
(MB) R3441432-2 08/16/1917:04
MB Result
MB Oualifier MB MDL
MB RDL
z
Analyze mg/I
mgA
mgll
TC
Pyrene U
0.000330
0,00100
1,2,4-Trichlorobenzene U
0.000355
0,0100
a
SS
L2-Diphenylhydrazine U
0.000318
0.0100
4-Chloro-3-methylphenol U
0.000263
0.0100
y
2-Chiorophenol U
0.000283
0.0100
Cn
2-Nitrophenol . U
0.000320
0.0100
4-Nitrophenol U
0.00201
0.0100
s
Sr
Pentachlorophenol U
0.000313
0.0100
Phenol U
0.000334
0.0100
2,4,6-Trichlorophenol U
0.000297
0.0100
2,4-Dichlorophenol U
0.000284
0.0100
2,4-Dimethyiphenol U
0.000624
0.0100
- 7G1
4,6-Dinitro-2-methylphenol U
0.00262
0.0100
2,4-Dinitrophenol U
0.0.0325
0.0100
- -
_ -
a
(S) Nltrobenzened5 45.9
15.0-314
A
(S) 2-Fluorobiphenyl 56.5
22.0-127 -
(S)p-Terphenyl-dM 53.8
29.0-141
9SC
(S)Phenol-d5 '15.7
-.
8004A
(S) 2-Fluorophenol 275
10.0-120
(S) Z,4,6-Tribromophenol 48.3
10.0-153
Laboratory Control Sample (LCS)
(LCS) R3441432-1 08/16/19
16:43
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Oualifer
Analyte
mg/I
mg/I
%
%
Acenaphthene
0.0500
0.0290
58.0
47.0-145
Acenaphthylene
0.0500
0.0301
60.2
33.0-145
Anthracene
0.0500
0.0298
59.6
27.0-133
Benzidine
0.100
0.00753
T53
1.00-120
Benzo(a)anthracene
0.0500
0.0259
51.8
33.0-143
Benzo(b)fluoranthene
. 0.0500
0:0263
52.6
24.0-159
_
Benzo(k)fluoranthene
0.0500
0.0261
52.2
11.0-162
,Benzo(g,h,i)peryiene
-0.0506
0.0249
49.8.
- 1:00-219
Benzo(a)pyrene
0.0500
0.0260
52.0
17.0-163
,Bis(bchlorethoxy)methane
0.0500
0.0249
49.8
1.00-219
Bis(2-chloroethyl)ether
0,0500
0,0254
50.8
33.0-185
Bis(2-chloroisopropyl)ether
0,0500
0.0265
53.0
36.0-166 _
4-Bromophenyl-phenylether
0.0500
0,0295
59.0
53.0-127
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation - 28091-R L1127117 08119/191411 17 of 23
WG1328408 QUALITY CONTROL SUMMARY
Semi Volatile Organlc Compounds (GC/MS) by Method 625.1 L1127117-01
Laboratory Control Sample (LCS)
(LCS) R3441432-1 08/16/19 16:43
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Oualifer
Analyte
mg/I
mgA
%
%
2-Chloronaphthalene
0.0500
0.0287
57.4
60.0-120 J4
4-Chlorophenyhphenylethei
0.0500
0.0299
59.8
25.0-158
Chrysene
0.0500
0.0258 "
51.6
1Z0-168
Dibenz(ah)anthracene
0.0500
0.0251
502
1.00-227
3,3-Dichlorobenzidine
0.100
0.0515
51.5
1.00-262
24-Dinitrotoluene
0,0500
0.0323
64.6
39.0-139
2,6-Dinitrotoluene
0.0500
0.0303
60.6
50.0-158
Fluoranthene
0.0500
0.0303
60.6
26.0-137
Fluorene
0.0500
0,0306
61.2
59.0-121
Hexachlorobenzene
0.0500
0.0248
49.6
1,00-152
Hexachlow 1,3-butadiene
0.0500
0.0258
51.6
24.0-120
Hexachlorocyclopentadiene
0.0500
0.0233
46.6
10.0-120
Hexachloroethane
0.0500
0.0265
53.0
40.0-120
Indeno(1,2,3-cd)pyrene
0.0500
0.0242
48A
1.00-171
Isophorone
0.0500
0.0257
51.41
21.0-196
Naphthalene
0.0500
0.0258
51.6
2tO-133
Nitrobenzene
0.0500
0.0252
50.4
35.0-180
n-Nitrosodimethylamine
0,0500
0.0115
23.0
10.0-120
n-Nitrosodiphenylamine
0.0500
0.0200
50.0
44.0920
n-Nitrosodi-n-propylamine
0,0500
0.0278
55.6
1.00-230
Phenanthrene -
0,0500
0.0300
60.0
54.0-120
Benzylbutyl phthalate
0.0500
0.0289
57.8
1.00-152
Bis(2-ethylheayl)phthalate
0.0500
0.0254,
50.8
8.00-158
Di-n-butyl phthalate
0.0500
0.0330
66.0
1.00-120
Diethyl phthalate
ao500
0,0331:
66.2
1.00-120
Dimethyl phthalate
0.0500
EMU
63.4
t00-120
Di-n-octyl phthalate
0.0500
0.0232
46.4
4.00-146
Pyrene
0.0500
0,0299
59.8
52D-120
1,24-Trichlorobenzene
0.0500
0.0264
52.2
4410-142
1,2-Diphenylhydrazine
0.0500
0.0297
59A
37.0-125
4-Chloro-3-methylphenol
0.0500 -
0.0227
45A
22:0-147
2-Chlorophenol
0.0500
0.0213
42.6
23.0-134
24-Dichlorophenol
0.050o
0.0230,
46.0.
39.0-135
2,4-Dimethylphenol
0.0500
0.0206
41.2
32.0-120
4,6-Dinitro-2-methylphenol
0.0500
0.0280
5U
100-181
2,4-Dinitrophenol
0.0500
0.0247
49 A
1.00-191
2-Nitrophenol
0.0500
0,0M
50.6
29.0-182
4-Nitrophenol
0.0500
0.0117
23.4
1.00-132
Pentachlorophenol
0.0500
0,0302
60A
14:0-176
Phenol
0,0500
0.00729
14.6
5,00-120
ACCOUNT:
PROJECT:
Eaton
Corporation
28091-R
SDG: DATE/TIME:
L1127117 08/19/1914:11
ONE LAB. NATIONWIDE.
1Cp
�Tc
aSs
4Cn
eSr
7GI
aAl
9Sc
PAGE:
18 of 23
WG1328408 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC7MS) by Method 625.1 L1127117-01
Laboratory Control Sample (LCS)
(LCS) R3441432-1 08/16/1916:43
Cp
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
LCS Qualifier
2
Analyze
mgA
mg/I
%
%
TC
2,4,6-Trichlorophenol
0.0500
0.0280
56.0
37.0-144
(S) Nitrobenzene-d5
67.3
15.0-314
17-1
a
$5
(S) 2-Fluorobiphenyl'
-_ _
574 -
12.0-127
(S)p-Terphenyl-dN
519
29.0-141
4Cn
(S) Phenol-d5
14.1
8.00-424
(S) 2-Fluorophenol
25.4
10.0-120
(S) 2,4,6-Tabromophenol
60.6
10.0-153
s
$f
L1127343-01 Original Sample (OS) • Matrix Spike (MS)
• Matrix
Spike Duplicate
(MSD)
a
(OS) L1127343-01 08/16/19 21:05 • (MS) R3441432-3 08/16/19
21:26
• (MSD) R3441432-4 08/16/19 21:46
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec .
Dilution
Rec Limits
MS Qualifier
MSD Qualifier
RPD
RPD Limits
7GI
Analyte
mg/I
mgA
mgA
mgA
%
%
%
%
%
Acenaphthene
0,0500
U
0.0180
0.0274
36.0
54.8
1
47.0-145
J6
414
48
-Acenaphthylene
0.0500
U
0.0196
0.0283
39.2
56.6
1
.33.0-145
36.3
74
Anlhracene
Benzidine
0.0500
0.100
U
U
0.0168
0.00537-
0.0292
ND
33.6
5.37
584
0.000.
1
1
27.0-133
7.00-120
J3 J6
53.9
200
66
40
9
$C
Benzo(a)anthracene
0,0500
U
0,0124
0.0240
24.8
48.0
1
33.0-143
J6
J3
633
53
Benzo(b)8uoranthene
0.0500
U
0,0113
0.0224
22.6
44.8
1
24.0-159
J6
65.9
71
Benzo(k)8uoranthene
0.0500
U
0.0112
0.0220
22A
44.0
1
11.0-162
J3
65.1
63
8enzo(g,h,i)pery1ene
0.0500
U
0.0120
0.0259 _
24.0
51.8:
1
1.00-219
73.4
97
Benzo(a)pyrene
0.0500
U
0.0120
0.0245
24.0
49.0
1
17.0-163
_
_
68.5
72
Bis(2-chlorethoxy)methane
0.0500
U
0.0233
0.0328
46.6
666
1
33.0-184
33.9
54
Bis(2-chloraethyl)ether
0.0500
U
0.0572
0.0805
114
161
1
12.0-158
J5
33.8
108
Bis(2-chloroisopropyl)ether
0.0500
U
0.0181
0.0268
36.2
53.6
1
-36.0-166
38.8
76
4-Bromophenyl-phenylether
0.0500
U
0.0167
0.0290
33.4
58.0
1
53.0-127
J6
J3
53.8
43
2-Chloronaphthalene
0.0500
U
0,0176
0.0274
35.2
54.8
1
60.0-120
J6
J3 J6.
43.6
24
4-Chlorophenyl-phenylether
0.0500
U
0.0170
0.0285
34D
57.0
1
25.0-158
50.5
61
Chrysene
0.0500
U
0.0124-
0.0239
24.8
47.9
1
170-168
63.4
87 -
Dibenz(a h)anthracene
0.0500
U
0.0112
0.0239
22.4
47.8
1
100-227
72A
126
3,3-Dichlorobenzidine
0.100
U
0.00300
0.00556
3.00
5.56.
1
L00-262
59.8
108
2,4-Dinitrotoluene
0.0500
U
0.0229
0,0341
45.6
68.2
1
39.0-139
39.7
42
,2,6-Dinitrotoluene
0.0500
:U
0.0297
0,0355
59,4
no
1.
50.0-158
ITS
48
Fluoranthene
0,0500
U
0.0154
0.0282
30.8
564
1
26.0-137
583
66
_ ..
'Fluorene
0.0500
At
0.0187
0.0287
. _
37.4
57.4
1
59.0-121
J6
J3 J6
42.2
38
Hexachlorobenzene
0.0500
U
0.0135
0.0262
27.0
524
1
1,00-152
J3
64.0
55
Hexachloro-1,3-butadiene
0.0500
U
0.0124
0.0212
24.8
42.4 -
1
24.0-120
52A
62
Hexachlorocyclopentadiene
0.0500
U
0.00457
0.0140
9.14
28.0
1
10.0-146
J6
J3
102
34
Hexachlomethane
0.0500
U
0.0162
0.0252
32.4
50.4
1
40.0-120
J6 ..
-43.5
52
ACCOUNT:' - PROJECT: SOG: DATE/TIME: PAGE:
Eaton Corporation 28091-R - L1127117 08/19/1914.11 19 of 23
WG1328408 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE,
Semi Volatile Organic Compounds (GC/MS) by Method 625.1- L1127117.01 -
L1127343-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1127343-01 08/16/19 21:05 - (MS) R3441432-3 08/16/19 21:26
- (MSD) R3441432-4 08/16/19 21:46
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution
Rec. Limits
MS Qualifier
MSD Qualirer
RPD
RPD Limits
Analyze
mgA
mgA
mgA
mgA
%
%
%
%
%
Indeno(1,2,3-cd)pyrene
0.0500
U
0.0120
0.0260
24.0
52.0
1
1.00-171
73.7
99
9sophorone
0.0500
U
6.0291
0.0435
58.2
87.0
1
21.0-196
393
93
Naphthalene
0.0500
U
0.0202
0.0281
40.4
56.2
1
21.0-133
323
65
Nitrobenzene
0.0500
U
0.0182
0.0252
364
50.4
1
35.0-180
323
62
n-Nitrosodimethylamine
0,0500
U
0,0102
0.0227
20.4
45.4
1
10.0-120
J3
76.0
40
n-Nitrosodiphenylamine
0.0500,
U
0.0201
0.0313
40.2
62.6
1
16,0-160
J3
43.6
28
n-Nitrosodi-n-propylamine
0.0500
U
0.0278
0.0401
55.6
80.2
1
1.00-230
36.2
87
Phenanthrene
0.0500
U
0.0171
OM88
34.2
57.6
1
54.0-120
J6
J3
51.0
39
Ben2ybutyl phthalate
0.0500
U
0,0153
0.0269
30.6
53.8
1
1.00-152
55.0
60
Bis(2-ethylhexypphthalate
0.0500
0.00261
0.0118
0.0244
18.4
43.6
T
8.00-158
69.6
82
Di-n-butyl phthalate
0.0500
U
0.0176
0.0297
35.2
59A
1
1.00-120
J3
5L2
47
Diethyl phthalate
0.0500
U
0.0233
0.0336 _
46.6
67.2
1
1,00-120
362
100
Dimethyl phthalate
0.0500
U
0.0222
0.0317
44.4
63.4
1
1.00-120
35.3
183
Di-n-octyl phthalate
0.0500
U
0.00992
0.0183
19.6
36.6
7
4.00-146
59.4
69
Pyrene
0.0500
U
0.0148
0.0275
29.6
55.0
1
52.0-120
J6
J3
60.0
49
12,4-Trichlorobenzene
0.0500
U
0.0164
.0.0237
32.8
47.4
1
44.0-142
J6
364
50
1,2-Diphenylhydrazine
0.0500
U
0.0188
0.0281
3T6
56.2
1
18.0-156
J3
39.7
34
4-Chloro-3-methylphenoi
0.0500
U
0.0405
0.0594
81.0
119
1
22.0-147
3T8
73
2-Chlorophenol
0.0500
U
0.0161
0.0259
32.2
51.8
1
23.0-134
46.7
61
2,4-Dichlorophenol
0.0500
U
0.0187
'0.0291
37.4
58.2
1
39.0-135
J6 .'
43.5.
50
2,4-Dimethylphenol
0,0500
U
0.0174
0.0261
34.8
52.2
1
32.0-120
40.0
58
4,6-Dinitro-2-methylphenol
0,0500
U
0.0186
0.0261
37.2
52.2
1
1.00-181
33.6
203
2,4-Dinitrophenol
0,0500
U
0,0206
0.0292
41.2
58.4
1
L00-191
34.5
132
2-Nitrophenol
0.0500
U
0,0187
0.0263
37.4
52.6
1
29.0-182
33.8
55
4-Nitrophenol
0.0500
U
ND
0.0117
0.000
23A
1
L0i
J6
J3
200
131
Pentachlorophenol
0.0500
U
0.0196
0.0312
39.2
62.4
1
14.0-176
-
453
86
Phenol
0.0500
0.0281
0.0353
0.0703
14.4
84.4
1
5.00-120
J3
66.3
64
2,4,6-Trichlorophenol
0.0500
U
0.0208
- 0.0306
41.6
61.2
1
37.0-144
_
38.1
5.8
(S) Nitrobenzene45
50.3
66.9
15.0-314
(S)2-Fluorobiphenyl
358
52.0 _
-
22.0-127
(S)p-Terphenyl-d14
263
51.4
29.0-141
J2
(S) Phenol-d5
12.4
19.0
_
8.00424
(S) 2-Fluorophenol
18.4
32.8
10.0-120
(S) 2,4,6-rrsbromophenol
45.1
74.0
10.0-153-
.
.ACCOUNT PROJECT: SDG: DATE/TIME PAGE:
Eaton Corporation 28091-R L1127117 08/19/1914:11 20 0( 23
GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. 0
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer- Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Datesrfimes, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit,
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Red. Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
Surrogate (Surrogate Standard) - Analyzes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyze
The name of the particular compound or analysis performed, Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample. preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or %difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful CC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state -No- (Not Detected) or'BDL'
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol ,
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical, process. If present, there will -
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the Feld when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
PI RPD value not applicable for sample concentrations less than 5 times the reporting limit.
1CP
ZTc
3Ss
4Cn
SSr
sQC
BAI
9Sc
ACCOUNT: PROJECT: .SDG: DATEITIME: PAGE'
Eaton Corporation 28091.R L1127117 08/19/19 14:11 21 of 23
ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accreddedlcertified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our Industry. The most significant benefit to our one location design Is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turnaround time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
'Not all certifications held by the laboratoryare applicable to the results reported in the attached report.
'Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
Alabama 40660
Alaska
17-026
Arizona
AZO612
Arkansas
88-0469
California
2932
Colorado
TN00003
Connecticut
PH_019]
Florida
E87487
Georgia
NELAP_
Georgia
923
Idaho
TN00003
Illinois
200008
Indiana
_
C-TN-01
Kentucky "
90010
Kentucky'
16
Louisiana
-Louisiana '—__----_�_-_--__
Maine
A130792 _
_-__--LA180010__—_--
TN0002
Maryland
324
Massachusetts
M TNO03
Michigan
_ _
9958
_ _
Minnesota
047-999395
MISSISSIPPI
Missouri _
_ _ _
TN00003
340
Montana
CERT0086
Third Party Federal Accreditations
A21LA - ISO 17025
1461.01
A2LA-ISO 17025'
1461.02
Canada
_ 1461.01
EPA-Crypto
TN00003
Nebraska
NE-OS-15-05
Nevada
TN-03-2002-34
New Hampshire
2975
New Jersey_NELAP
TNO02
New Mexico'
Na
New York
11742
North Carolina
Emv375
North Carolina'
DW21704_
North Carolinas
_
41
North Dakota
R-140
Ohlo-VAP CLOO69
Oklahoma 9915
Pennsylvania
68 02979
Rhode Island
LAOOD356
South Carolina
84004
South Dakota
n/a___
Tennessee1°
-
2006
- -_-_�
Texas
- __ _
T10470424548 IS
Texas'
_-
_-_-_ _--_
LA80152
Utah
_
TN00003
Vermont
_ W2006
Virginia
_
--- 460132
Washington
C847 ___--
West Virginia
233
Wisconsin
9980939910
AIHA4AP,LLC EMLAP 100789
DOD 1461.01 _
USDA P330-15-00234
'Drinking Water ' Underground Storage Tanks 3Aquatic Toxicity 'Chemicald, icrobiological s Mold ` Wastewater ma Accreditation not applicable
Our Locations
Pace National has sixty four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
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ACCOUNT: PROJECT: SOG' DATErrIME:
Eaton Corporation 28091-R L1127117 08/19M914:11
ME
PAGE:
22 of 23
Billing Information:
Analysis/Container/Preservative
Chain of Custody Page _a'_
Eaton Corporation
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NA Financial Services Center • 1009 Gres
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PO Box 818024 Chk
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