HomeMy WebLinkAboutNCG030027_MONITORING INFO_20190618STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ I o 1
YYYYM M D D
Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
CERTIFICATE OF COVERAGE NO. NCG03 0 0 2 7
FACILITYNAME Eaton Corporation
COUNTY Person
PERSON COLLECTING SAMPLES Dustin LeClair
LABORATORY PACE National
Date submitted
Lab Cent. # ENV375/DW21704/B10041
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or 0 Monthly' June (month)
DISCHARGING TO CLASS ❑ORW ❑HC(W ❑Trout ❑PNA
❑Zero -flow [:]Watersupply [_]SA
*Other WS-III: NSW
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 �
❑ No discharge this Period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics=
Benchmarks
-
-
100 mg/Lor 50 mg/L4
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Tool Room Trench (005)
06/18/2019
0.22
7.37
8.5
0.00792
0.002 (ND)
0.0315
0.806 (ND)
0.127
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Dustin LaClair
Name (Print name)
EHS Manager
Titl ri (tY}LIe/���/
• W 0-1 IIAI TAI
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
-
46529
NCOIL
00552
CO530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES 0 NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑
REGIONAL OFFICE CONTACT NAME: D..,Ss iID
Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware t+f thSPTai a significant pprf%4 fWsubmitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Permit Date: 11/1/2018-05/31/2021
O? 1 b 70 164
Date
SWU-245, last revised 11/1/2018
Page 3 of 3
2019-06-18-001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected dale/lime: 05/18/19 14:30 L1110945
Additional Information
Result Units
Analyte
PH (On Site) 8.5 so
Temperature (on -site) 25.5 Deg C
Gravimetric Analysis by Method 2540 D-2011
Result Oumifier MDL RDL Dilution Analysis Batch
Analyle mg/I mg4 mg4 date/time
Suspended Solids 7.37 0.462 3,30 1 06/25/201918:15 WG1301085
Wet Chemistry by Method 1664E
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte mg4
mg/I
mg/l
date/time
TPH - Oil & Grease U
0.806
5.56
1 06/3020191140
WG1304002
Metals (ICIO) by Method 200.7
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Copper 0,00792
J
0.00700
0-0100
1 06/26/201903:00
WG1300332
Lead U
0,00200
0.00500
1 06/261201903:00
WG1300332
Zinc 0.0315
J
0,00340
0.0500
1 06/26/201903'.00
WG1300332
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte
ri
mg/I
mg/I
date/time
Acrolein
U
0.00887
0,0500
1
06/21201919:08
WG1300040
Acrylonitrile -
U
0,00187
0QdGO
.1
06/21201919:08
WG1300040
Benzene
U
0.000331
0,00100
1
06/21/201916:08
WG1300040
Bromodlchloromethane
U
0.000380
0.00100
1
06/21/201919:08
WG1300040
Bromoform
U
0.000469
0.00100
1
06/21/201919:08
WG1300040
Bromomothane -
U
0.000866
0.00500
1
06/21/201919:08
WG1300040
Carbon tetrachloride
U
0.000379
0.00100
1
06/21/201919:08
WG1300040
Chlorobenzene
U
0,000348
0.00100
1
06/21201919:08
WG1300040
Cflood ibromomethane
U
0.000327
0.00160
1
O6/21/20191908
WG1300040
Chloroethane -
U
0.000453
0.00500
1
06/21/201919:08
WG1300040
2-broroethyl vinyl ether
U
0.00301
0.0500
1
06/21/201919:08
WG1300040
Chloroform
0,000339 J,
0,000324
0.00500
1
06/21/201919:68
WG1300040
Chloromethane
U
0.000276
0.00250
1
06/21/201919:08
WG1300040
1.2-6lchlorobenzene
U
0.000349
0.00100
1
66/21/201919:68
WG1300040
13-Dichlorobenzene
U
0.000220
0.00100
1
06121201919:08
WG1300040
1,4471chlorobe-nzene
U
0.000274
0.00160
1
66/21/2016 im:
WG1300040
Dichlorodifluoromethane
U
0.000551
0.00500
1
06/21/201919:08
WG1300040
1,17Dichloroethane
U
0.000259
0.00100
1
66/21/201919:08
WG1300040
1,2-Dichloroethane
U
0.000361
0,00100
1
06/21/2019 19:08
WG1300040
-
1,1-fichloroethene
- �
U
0.000398
0.00100 -
1
06/21/201919:68
- WG1300040
trans-1,2-Dichloroethene
U
0.000396
0.00100
1
06/21/201919:08
WG1300040
1.2-61chloropropane
U -
0.000306
0.00100
1
661T201919:08
WG1300040
cis-1,3-Dichloropropene
U
0.000418
0.00100
1
06/21/201919:08
WG1300040
trans-6 Dichloropropene
U
0.000419
0.00100
1
06/21/2019 19:08
W61300640
Ethylbenzene
U
0,000384
0.00100
1
06/21/201919:08
WG1300040
Methylene Chloride
-U
0.00100
6.Oo500
1
66/21/201619M
WG1300040
1,1,2,2.Tetrachloroethane
U
0.000130
0.00100
1
06/21/201919:08
WG1300040
Tetrachloroethene
0.00187
0.000372
0.00100
1
0621/201919:68
WG1300040
Toluene
U
0.000412
0,00100
1
0621/201919:08
WG1300040
_., . .. _.
1,1,1-Trichloroethane�
. - . . .
U
.. 19
0.000319
.....
0.00100
1
_ ..
06/21/201919:06
WG1300040
11,2-Trichloroethane
U
0.000383
0.00100
1
06121/201919:08
WG1300040
ACCOUNT: PROJECT: SOG DATE/TIME: PAGE:
Eaton Corporation 28091.R L1110945 07/02/19 09:02 5 of 26
2019-06-18-001
SAMPLE
RESULTS - 01
ONE LAB. NATIONWIDE.
Collected date/time: 06118/19
14:30
L1110945
Volatile Organic Compounds
(GC/MS)
by Method 624.1
RP
Result Qualifier
MDL
RDL
Dilution
Analysis
Batch
mg/I
al
mind
date/lime
Trichloroothene
0.000780 J
0.000398
0.00100
1
06/21/201919:08
WG1300040
ITC
Trichlorolluoromethane
U
0.00120
0.00500
1
06/21/201919:08
WG1300040
Vinyl chloride
U
0,000259
0,00100
1
06/21/201919:08
WG1300040
a
(S)Toluene-d8
99.7
800-120
06121201919.08
WG1300040
SS
(5)0.a,a-Tri/luarotoluene
0.000 12
800-120
06/21/10191908
W61300040
(S)4-Bromolluorobenzene
79.6 J2
80.0-120
061211.201919:08
WG1300040
Cn
(S) 7,2-Dichloroethana-d4
99.6
70.0-130
0621/207919:08
W61300040
Pesticides (GC) by Method EPA 608.3
Result Oualifer
MDL
RDL
Dilution
Analysis
Batch
5
Analyse
mg/I
ri
mg/I
date Itime
QC
Aldrin
U
0,00000813
0.0000500
1
06/23/201914:26
WG1299470
Alpha BHC
U
0.0000166
0.0000500.
1
06/23/201914:26
WG1299470
7GI
Beta BHC
U
0.0000184
00000500
1
06/23/201914.26
WG1299470
Delta BHC
U
0.0000197
0.0000500
1
06/23/201914 26
WG1299470
e
Gamma BHC
U
0.0000176
0,0000500
1
06/23/20191426
WG1299470
[Al
Chlordane
U -
0.0000977
0.000500
1
06/2 3/2019 14:26
WG1299470
4,4-DDD
U
0.0000170
0.0000500
1
06/23/201914:26
WG1299470
9
qC
4,4-DDE
U _
0.0000164
0.0000500
1
06R3R01914:26
WG1299470
4,4-DDT
U
0,0000177
0.0000500
1
06/23/201914:26
WG1299470
Dieldrin
U
0.00000751
0.0000500
1
06/23/2019 14:26
WG12994111 707
Endosullan I
U
0.0000179
0.0000500
1
06/23/201914:26
WG1299470
Endosullan ll
U
0.0000176
0.0000500. -
1
06/23/201914:26
WG1299470 -
Endosulfan sulfate
U
0,0000196
0.0000500
1
06/23/201914:26
WG1299470
Endrin
U
0.0000189
0.0000500
1
06123120191426
WG1299476
Endrin aldehyde
U
0.0000142
0.0000500
1
06f23/201914:26
WG1299470
Endrin ketone
: U
- 0.0000170
0.0000500 •
1
06123/2019 14:26
WG1299470
Heptachlor
U
0.0000108
0.0000500
1
06/23/201914:26
VIG1299470
-
Heptachlor epoxide
U
..
- 0.0000175
..
0.0000500
1
. _..
06/23/20191426
-- . .
WG1299470
Hexachlorobenzene
U
0,0000134
0.0000500
1
06/23/20191426
WG1299470
Methoxychlor
U
0.0000193
0.0000500
1
06123/20191426
W61299470
Toxaphene
U
0,000168
0.000500
1
06123/201914:26
WG1299470
/SJDecachloiobiphenyl
59.3
-
10.0-144
0623120191426
WG1299470
(S)Tetrachloro-m-xylene
61.4
10.0-135
06123120191426
WG1299470
Polychlorinated
Biphenyls
(GC) by Method EPA-608.3
Result
Qualifier MDL
RDL
Dilution
Analysis
Batch
Analyle
mg4
mg/I
mgll
date/time
PCB 1016
U
0,000100
0.000500
1
06124/201908:51
WG1299470
PCB 1221
U
0.0000730
0.000500 -
1
06/24/201908:51
WG1299470 -
PCB 1232
U
0.0000420
0.000500
1
06/24/2019 08:51
WG1299470
PCB 1242
U
0.0000470
0.000500
1
06/24/2019 08:51
WG1299470
PCB 1248
U
0.0000360
0.000500
1
06/24/2019 08:51
WG1299470
PCB 1254
U
0.000070
0.000560
1
06/24/2019 08:51
WG1299470
PC81260
U
0.000120
0.000500
1
06/24/2019 08:51
WG1299470
(SJ Decochlorobiphenyl
579
100144
06124120190851
WG1299470
(S Tetrachloro-m-xylene
56.6
10.0-135
061241201908.51
WG1299470
Semi Volatile Organic Compounds (GC/MS) by Method
625.1
Result
Oualifier MDL
RDL
Dilution
Analysis
Batch
Analyse
mg/I
mg/I
mgll
date/time
Acenaphthene
U
0,000316
0.00100
1
06/25/201915:03
WG1300466
Acenaphtiiylene
U -
0.000309
0.00100
1
06/25I201915:03
WG1300466
Anthracene
U
0,000291
0.00100
1
06/25/201915:03
WG1300466
Denzil
U
0.00432
0.0100
1
66/25/20196:03
WG1300466
ACCOUNT:
.PROJECT:
SDG:
DATEMME: PAGE'
Eaton
Corporation
_
28091-R
L1110945
07/02/19 09:02 6 of 26
2019-06-18-001 SAMPLE RESULTS - 01 ONE LAS. NATIONWIDE.
Collected dateltime: 06/18/19 14:30 L1110945
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Analyte
Result
mg/1
Oualifer
MDL
mg/I
RDL
mg/I
Dilution
Analysis
date/lime
Batch
Benzo(a(anthracene
U
0.0000975
0.00100
1
06/251201915:03
WG1300466
Benzo(b(fluoranthene
J
0.0000896
0.00100
1
06125/201915:03
WG1300466
Benzo(k(fluoranthene
U
0.000355
0,00100
1
06/25n01915:03
WG1300466
Benzo(g,h,ilperylene
U -
6.600161
0.00100
1
06/251201915:03
WG1300466
Benzo(a)pyrene
U
0,000340
0.00100
1
06/25/201915:03
WG1300466
Bis(2-chlorethoxy)methane
U
0.000329
0DI00
1
06/25n01915-03
WG1300466
Bis(2-chloroethy;)ether
U
0.00162
0.0100
1
06125/201915:03
WG1300466
B142-chloroisopropyl)ether
U
- 0.000445
0.0100
1 -
06125/201915:03
WG1300466
4 Bromophenyl-phenylether
U
0,000335
0.0100
1
06125/201915:03
.WG1300466
2-Chloronaphihalene _
U
J4
0.000330
0.00100
1
66/25/201915:03
WG1300466
4 Chlorophenyl-phenylether
J
0.000303
0,0100
1
06125/201915.03
WG1300466
Chrysene
-U
0.000332
0.00100
•1
06/25I201915:03
WG1300466
Dibenz(a,h(anthrncene
U
0.000279
0,00100
1
06/25/2019 15:03
WG1300466
3,3-Dichlorobenzidine
U
0.06202
0.0100
1
0605/201915:03
WG1300466
24 Dinitrotoluene
J
0.00165
0,0100
1
06/25/20191503
WG1300466
2,6-61nilrotoluene -
U
0.000279
0.0100
1
06/25/201915:03
WG1300466
1,2 Diphenylhydrazine
U
0.000318
0.0100
1
06/251201915:03
WG1300466
Flucenthene
U
0.000310
0.00100
1
06/25/201915:03
WG1300466
Fluorene
U
0,000323
0.00100
1
06/25/201915:03
WG1300466
Hexachlorobenzene
U
6.000341F
0.00100
1
06/25n0191503
WG1300466
Hexachloro-1,3-butadiene
U
0.000329
0.0100
1
06/25/201915:03
WG1300466
Hexachlorocydopen adiene
U
0.00233
0.0100
1
06I25/201915:03
WG1300466
Hexachloroethane
U
J4
0.000365
0.0100
1
06125/201915:03
WG130G466
Indeno(1,2,3td(pyrehe
If
0.000279
0.00100
1
66/25n01915:03
WG1300466
Isophorone
U
0,000272
0.0100
1
06/25/201915:03
..
WG1300466
_
Naphthalene �
U
�
. .....
0.000372
_ .. _
0.00100
..
1
.
06125/2019 15:03
WG1300466
Nitrobenzene
U
0.000367
0.0100
1
06125/2019 is 03
WG1300466
n-Nilrosddimethylamine
U
0.00126
0.0100
1
06I25I201915:03
WG1300466
n-Nilrosodiphenylamine
U
0.00119
0.0100
1
061251201915:03
WG1300466
n-Nitrosodl n-propylamine
U
-
0.000403
0.0100
1
06/25I201915:03
WG1300466
Phenanthrene
U
0.000366
0.00100
1
06/25n01915:03
WG1300466
Beniylbutyl phthalate
O.000Z75
0-00300
1
06/25n01)15:03
WG1300466
Bis(2- ethyl hexyl)phthalate
U
0.000709
0,00300
1
06/25/201915:03
WG1300466
. ..__.. _._.__ .. . ....
Din -butyl phthalate
.. .. ..
U
..
0.000266
66
- ..___
0.00300
-
1
_ ...
06/25/2019 i5:03
... ..
WG13004fi6
Diethyl phthalate
U
0.000282
0.00300
1
06125/201915:03
WG1300466
_.
..
Dinletbyl phthalate
-
U
_. ....
_._
0.000283
0.00300
_.
1
06/25/201915:03
.. ..
WG1300466
Di-n-octyl phthalate
U
0.000278
0,00300
1
06125/201915.03
WG1300466
Pyrene
U
omi:330
0.00100
1
06/251201915:03
WG1300466
1,2,4-Trichlorobenzene
U
J4
0.000355
0,0100
1
06/251201915:03
WG1300466
4-Chloro-3:methylphenol
U
0.000263
0.0100
1
06/251201915:03
WG1300466
2-Chlorophenol
U
0,000283
0.0100
1
06/25/201915:03
WG1300466
2,4-Dichlorophenol
U
0.000284
0.0100
1
06/25/201915:03
WG1300466
24 Dimethylphenol
U
0.000624
0,0100
1
06125/201915:03
WG1300466
4,6-6initro-2-methyl0enol
U
0.00262
0.0100
1
06/251201915:03
WG1300466
2,4-Dinitrophenol
U
0.00325
0.0100
1
06/251201915:03
WG1300466
2-Nitrophenol
U
0.000320
0.0100
1
06/25/201915:03
WG1300466
4-Nitrophenol
U
0.00201
0.0100
1
06/25/201915:03
WG1300466
Pentachlorophenol
U
0.000313
0.0100
1
06/251201915:03
WG1300466
Phenol
0.00176
J
0.000334
0.0100
1
06/25/201915:03
WG1300466
2,4,6-Trichlorophenol
J .
0.000297
0,6100
1
06M/201915:03
WG1300466
/5/2-Fluorophenol
18.2
10.0-120
062WO1915.03
WG1300466
(5)Phenol-d5
115
-
800-424
66125120791503
WG1300466
(S) Nitrobenzene-d5
33.7
15,0-314
0625201915.03
WG1300466
(S)2-Fluoroblphenyl
38.7
22.0d27
067257201915:03
WG1300466
(S)2,4,6-Fribromophenol
535
1a0-153
05/2520191503
WG1300466
(S)p-Ferphenybdl4 .
58.5
29.0-141
06725/201915.03
WG1300466
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Eaton
Corporation
28091-R
1-1110945
07/02/1909.02
PAGE:
7 of 26
2019-06-18-005 SAMPLE RESULTS - 02 ONeLAe NATIONWIDE.
Collected date/lime: 06/18/19 14:45 L1110945
Additional Information
Result Units
pH (On Site) 8 so
Temperartue (on -site) 317 Deg C
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier
MDL
RDL
Dilution Analysis Batch
Analyte mg/l
mg/I
mg/l
date/time
Suspended Solids 711
0.420
3,00
1 06/25/201918:15 WG1301085
Wet Chemistry by Method 1664B
Result
Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
TPH - Oil R Grease U
1.45
10.0
1
06/3020191140
WG1304002
Metals (ICP) by Method 200.7
Result
Qualifier
MDL
RDL
Dilution
Analysis
Batch
Analyte mgll
mg/I
mg/I
date/time
Copper 0.0148
0,00700
0.0100
1
06126/201903:03
WG1300332
Lead 000241
1
0.00200
- 0.00500
- 1
06/26/201903:03
WG1300332
Zinc 0.0336
J
0.00340
06500
1
0666/201903:03
WG1300332
Volatile Organic Compounds (GC/MS) by Method 624.1
Analyte
Result
mg/I
Qualifier MDL
iii
RDL
mg/I
Dilution
Analysis
date/time
Batch
Acrolein
U
0.00887
0.0500
1
06121120191929
WG1300040
Acrylonitrile -
'U
0.00187
0.0100
1
06/21/201919:29.
WG1300040
Benzene
U
0.060331
0.00100
1
06/21I20191929
WG1300040
Bromodichloromethane
U
0,000380
0.00100
1
06121/201919:29
WG1300040
Bromoform
U
0.060469
0.00100
1
0621/201919:29
WG1300040
Bromomethane
U
- 0.000866
0.00500
1
06121/201919:29
WG1300040
Carbon tetrachloride
U
0.000379
0.00100
1
06/21/201919:29
WGI300040
Chlorobenzene
11
GD00348
.0.00100
1
06/2l/201919:29
WG1300040
Chlorodibromomethane
U
0.000327
0.00106
1
06121/201919:29
WG1300040
Chloroethane -
U
0,000453
0.00500
1
06/21/201919:29
WG1300040
2-Chloroelhyl vinyl ether
U
0.00301
0.0500
1
06/21/201919:29
WG1300040
Chloroform
u
0.000324
OA0500,
1
0601/201919:29
WG1300040
Chloromethane
U
0.000276
0.00250
1
06/21/201919:29
WGI300040
1,2-Dichlorobenzene
u
0.000349
0.00100
1
06/21120191929
WG1300040
13 Dichlorobenzene
U
0.000220
0.00100
1
06/21/201919:29
WG1300040
1,4-61chlorobenzene
u
0,000274
0,00100
1
06/21/201919:29
WG1306040
Dichlorodifluoromethane
U
0,000551
0.00500
1
06/211201919:29
WG1300040
1,1-Dichloroethane
_ u
0.060259
Ob0100
1
06121/201919:29
WG1300040
1,2-Dichloroethane
U
0.000361
0.00100
1
06/21/201919:29
WG1300040
1,1-Dichloroethene
u
O.o00398
0.00100
1
106/21/201916:29
W31300040
trans-1,2-Dichloroethene
u
0.000396
0.00100
1
06/21/201919:29
WG1300040
1,2-Dichloropropane -
u
0,060306
0.00100
1
06/21/2019 19:29
WGI300040
cis-1,3-Dichloropropene
U
0.000418
0.00100
1
06121/201919:29
WG1300040
trans-1,3-Dichloropropene
U
0.000419
0.00100 -
1
06/21/201919:29
WG1300040
Elhylbenzene
u
0.000384
0.00100
1
062V201919:29
WG1300040
Methylene Chloride
u
- - 0.00100
0.60500
1
661211201919:29
WG1300040
1,1,2,2-Tetrachloroethane
U
0.000130
0.00100
1
06/21/201919:29
WG1300040
Tetrachloroetfiene
U
0.060372
6.00100
1
06/2V201919i29
WG1300040
Toluene
U
0.000412
0.00100
1
06/21/201919:29
WG1300040
1,1,1-Trichloroethane
U
0.000319
0.00100
1
06/21/201919:29
W67300040
11,2-Trichloroethane
u
0.000383
0.00100
1
06/21/201919:29
WG1300040
9
ACCOUNT: PROJECT: 90G: - DATE/TIME' - PAGE:
Eaton Corporation 28091-R L1110945 07/02/19 09,02 8 of 26
2019-06-18-005
SAMPLE
RESULTS - 02
ONE LAB. NATIONWIDE.
Collected daleltlme: 06/18/19 14:45
L1110945
Volatile Organic Compounds
(GC/MS) by Method 624.1
1
Result
Qualifier MDL RDL
Dilution Analysis
Batch
Cp
Analyte
mg/I
mg/1 mg/I
date/time
Trichloroethene
U
0.000398 0.00100
1 06/211201919:29
WG1300040
FTC]
Trichlarofluarome[hane
U
0.00120 0.00500
1 O6/21/201919:29
WG1300040
Vinyl chloride
U
0.o00259 0,00100
1 0601/201919:29
WG1300040
a
(S)Toluene-d8
96.5
80.0-120
0672201919.29
WG1300040
$5
(S)a.o,a- Trilluorotoluene
0000
J2 80.6-120
06211201919:29
WG7300040
(S)4-Bromol7uombenzene
74.4
J2 80.0-120
06211201919.29
WG1300040
°
S) l2-Dichloroethane-dal
99.2
70.0-130
OkV201919.29
WG1300040
Pesticides (GC) by Method EPA 608.3
Result
Qualifier MDL
RDL
Dilution
Analysis
Batch
Analyze
mg/I
mg/I
mg/I
date/time
Aldrin
U
0.00000813
0.0000500
1
06/23/201914:38
WG1299470
Alpha BHC
U
0.0000iis
0.0o00500
1
06M/201914:38
WG1299470
Beta BHC
U
0.0000184
0.0000500
1
06/231201914:36
WG1299470
Delta BHC
U
0.0000197
0.0000500
1
06/23/201914:38
WG1299470
Gamma BHC
U
0.0000176
0.0000500
1
06/23/2019 14 38
WG1299470
Chlordane
U
0.0000977
0.000500
1
06I23I201914:38
WG7299470
4,4-DDD
U
0.0000170
0.0000500
1
06123/201914:38
WG1299470
4,4;6DE
U
0.0000164
0.0000500
1
06/23/201914:M
WG1299470. _
4,4-DDT
U
0.0000177
0.0000500
1
06MMB)14:38
WG1299470
Oieldrin
-U
O.000OO75T
0.0000500
1
061231201914:38
WG1299410
EndosulfanI
U
0.0000179
0.0000500
1
06/231201914:38
WG1299470
Endosulfan II
U
0.0000176
0.0000500
1
06/231201914:38
WG1299470
Erdosultan sulfate
U
0.0000196
0,0000500
1
06/231201914:38
WG1299470
Endrin
U
0.0000189
0.0000500
1
06I2300191446
WG1299470
Endrin aldehyde
U
0.0000142
0.0000500
1
06/23/201914:38
WG1299470
Endrin ketone
0.0000170
0.0000500
1
06/23I201914:36
W61299470 '
Heptachlor
U
0,0000108
0.0000500
1
06/23/2019 14:38
WG1299470
Heptachlor epoxide
U
0.0000175
0.0000500
1
06123R01914:38
WG7299470
Hexachlorobenzene
U
0.0000134
0.0000500
1
061231201914:38
WG1299470
_.. . ... --
Methdxychlor
U
.. . .
0.0000193
-- o- -'
0.0000500
_ -
1
..._. _
06R3/201914:38
...
WG1299470
Toxaphene
U
0.000168
0.000500
1
06/23/201914:38
WG1299470
(S/Decachldrabiphenyl
75.6
10.0-744
0623/10191438
WG1299470
(S)Tetrochloro-m-Mene
71.8
10.0-135
061231201914.38
WG1299470
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Analyze
Result
mgll
OualiBer MDL
mg/I
RDL
mgll
Dilution Analysis
date/time
Batch
PCB 1016
U
0.000100
0.000500
1 06/24/201909:05
WG1299470
PCB 1221 -
U
0.0000730
0.000500
1 06/241261909:05
WG1299470
PCB 1232
U
0.0000420
0.000500
1 06/24/201909:05
WG1299470
PCB 1242
U
0.0000470
0.000500
1 06124/201909:05
WG1299470
PCB 1248
U
0,0000860
0.000500
1 06124/2019 09:05
WG1299470
PCB 1254
U
0.0000470
0.000500
1 06/24/2019 09:05
WG1299470
PCB 1260
U
0.000120
0,000500
1 06124120190905
WG1299470
(5) 0emchldiobiphenyl
70.1 .
70.0-144
06241201909:05
WG1299470
(S) Tetrachloro-m-xylene
65.1
10.0-135
061241201909:05
WG1299470
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier MDL
RDL
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Acenaphthene
U
0.000316
0.00100
1 06/24/201914:53
WG1300466
Acenaphthylene
U.
_ 0.000309
0.00100
1 061241201914:53
WG1300466
Anthracene
U
0.000291
0.00100
1 06124/201914:53
WG1300466
Benzidine
U
0.00432
0.0100
1 06/24/2019 14:53
WG1300466
FOCI
7GI
aAl
9SC
ACCOUNT: PROJECT: SDG' DATE/TIME: PAGE:
Eaton Corporation 26091-R L1110945 07/02/19 09.02 9 of 26
2019-06-18-005 SAMPLE RESULTS 02 ONE LAB. NATIONWIDE. �
Collected dale/lime: 06118/1914:45 L1110645
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Analyte
Result
mg/I
Qualifier
MDL
nal
RDL
mg/I
Dilution
Analysis
date/time
Batch
Cp
Benzo(a)anthraceno
U
0.0000975
0.00100
1
06124/2019 14:53
WG1300466
a
Tcthehe
Benzo(b)fluoran
- U �
�
0.0000896
0.00100
1
06/241201914:53
WG73004fi6
Benzo(k)fluoranthene
U
0.000355
0.00100
1
06/24/2019 14:53
WG1300466
aSS]
Benzo(g,h.i)perylene
U
6.600161
0.00100
1
06/24001914:53
WG1300466
Benzo(a)pyrene
U
0.000340
0.00100
1
O6/24/2019 14:53
WG1300466
Bis(2-chlorethoxy)methane
U
_
0.000329
0.0100
1
06/241201914:53
WG1300466
4
Cn
Bis(2-chloroethypether
U
0.00162 �
0.0100
1
06/24/2019 14:53
WG1300466
Bls(2-chlorolsopropy)ether
U
0.006445
0.0100
1
013/24I2019 14:53
WG1300466
4-Bromophenyl-phenylether
U
0,000335
0.0100
1
06/24/2019 14:53
WG1300466
2-Chloromplamalene
U
J4
0.000330
0.06100
1
06124/201914:53
WGI300466
4-Chlorophenyl-phenylether
U
0.000303
0.0100
1
06/241201914:53
WG1300466
5
Chrysene
U �
0.000332
0.00700
1
O6/24201914:53
WG1300466
Dibenz(a,h)anthracene
U
0.000279
0.00100
1
06/24/2019 14:53
WG1300466
z
3,3 Dichlorobenzidine ..
U,
0.00202�
0,0100
1 .
06124/201914:53
WG1300466
GI
2A Dinitrotoluene
U
0.00165
0.0100
1
06/24/2019 14:53
WG1300466
_
.. .
2.6-Dimtrotaluene
U
0.000279
... ..
0.0100
1
...__- _ ..
Ofi/24120191453
WG7300466
aAl
1,2-Diphenylhydrazine
U
0,000318
0.0100
1
06/241201914:53
WG1300466
Fluoranthene
U -
0.000316
0.00100
1
06/24/201914:53
WG130046.6
s
Fluarene
U
0.000323
0.00100
1
06/241201914:53
WG1300466
SC
HexachIchobonzene
U
0.000341
O.o0100.
1
06/240019 14:53
W61300466
Hexachloro-13-buediene
U
0.000329
0,0100
1
06/2412019 14:53
WG1300466
--....e_._.
Hexachlorocydopentaoiene
... ._ ..
U
... ..
._ ..
0.00233
_. _.........
- 0.0160
1
06/24/2019 14:53
.. ..
WG1300466
Hexachloroethane
U
J4
0,000365
0.0100
1
06/24I201914:53
WG1300466
Indeno(1),3td)pyrene
- U
0.000279
0.00100
1
06/2412019114:53
- WG1300466
Isophorone
U
0.000272
0.0100
1
06/24/2019 14:53
WG1300466
Naphthalene -
U
0 000372
6.00100 -
1
06/241201914:53
WG1300466
Nitrobenzene
U
0.000367
0.0100
1
06/24/2019 14:53
WG1300466
..
n-Nitrosodimethylamihe
U
000126 26
...
0.0100 _
1
_._. _
�O6/24201914.53 53
_ ...
WG1300466
n-Nitrosodiphenylamine
U
0.00119
0.0100
1
06124/201914:53
WG1300466
n-Nitrosodi-n-propylamme
U
0.000403
0.0100
1
06%24201914:53
W61300466
Phenanthrene
U
0.000366
0.00100
1
06124/201914:53
WG1300466
Benzylbutyl phthalate,
U
6600275
0.00300
1
06124/201914:53
W(31300466� -
Bis(2-ethylhexyl)phlhalate
U
0.000709
0.00300
1
0624/201914:53
WG1300466
Di-n-butyl phthalate
0.000310
J '
0.000266
0.00300
1
06/24/20191453
WG7300466
Dlethyl phthalate
U
0.000282
0.00300
1
06/241201914:53
WG1300466
Dlmethyl phthalate
U
6.000283
0.00300
1
06/24/201914:53
W61300466
Di-n-octyl phthalate
U
0,000278
0.00300
1
06/24/2019 14:53
WG1300466
Pyrene
U
..
0.000330
000100
1
0124/201914:53
WG1300466 .
1,2,4-Trichlorobenzene
U
J4
0.000355
0.0100
1
06/241201914:53
WG1300466
4-Chloro-3-methylphenol
U
0.000263
0.0100
1
06/241201914:53
'WG1300466
2-Chlorophenol
U
0,000283
0.0100
1
06124/201914:53
WG1300466
2,4-Dichlor6phehol -
U
0.000284
0.0100
1
06/24/2019 14:53
WG1300466
-
2,4-Dimethylphenol
U
0.000624
0.0100
1
06/241201914:53
WG1300466
4,6-Dinitro-2-methylphenol
U
_
0,00262
0.0100
1
06/241201914:53
WG1300466
2,4-Dinitrophenol
U
0.00325
0,0100
1
06/24/2019 14:53
WG1300466
2-Nitrophenol
U
0.000320
0.0100
1
06/24/2019 14:53
WG1300466
4-Nitrophenol
U
0,00201
0,0100
1
06/241201914:53
WG1300466
Pentachlorophenol
U
0.000313
0.0160
1
06/24/2019 14:53
WG1300466
Phenol
0,00164
J
0,000334
0.0100
1
06/24/2019 14:53
WG1300466
2 A,6-Trichlorophenol
U
-
0.000297
0.0100
1
06/24/201914:53
WG1300466
(S)1-Fluorophenol
19.3
10.0-120
0612412019 14 53
WGI300466
(S)Phendf-d5
12.8
8.00-424
06/24201914:53
W61360466
(S) Nitrobenzene-d5
33.6
150-314
06124201914,53
WG1300466
/S/2-Fluorobiphenyl
39.3
22.0-127
06241701914.53
WG1300466
(S)2,4,6-Tribromophenol
540
10.0-153
06241201914:53
WG1300466
(5/p-Terp6enyl-d14
543
29.0-141.
'
06/24/201914:53
WG1300466
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Eaton Corporallon
28091-R
L1110945
07/02/19 09.02
10 of 26
ONE LAB. NATIONWIDE.
WG1301085 QUALITY CONTROL.SUMMARY �
Gravimetrlc Analysis by Method 2540 D-2011 _ _ L1110945-.01.02: - -
Method Blank (MB) C
(MB) R3424936-1 06/25/1918:15
a
2
MB Result MB Oualifier M8 MOIL MB ROL
Analyte mg/I mg)]
mg/I
Tc
Suspended Solids U 0.350
2.50
aSs
4Cn
L111O831-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1110831-01 06/25/1918:15 • (DUP) R3424936-3 06/25/1918:15
Original Result DUP Result Dilution DUP
RPD
DUP Qualifier DUP RPD
Limits
s
Sr
Analyte mg/I mg/I %
%
Suspended Solids 58.8 61.2 1 4.00
5
Q
L111O911-01 Original Sample (OS) • Duplicate (DUP)
7GI
(OS) L1110911-01 06/25/1918:15 • (DUP) R3424936-4 06/25/1918:15
Original Result DUP Result Dilution DUP
RPD
DUP Qualifier DUP RPO
Limits
a
[Al
Analyte mg/I mg/I %
%
Suspended Solids 21.2 22.6 1 6.39
Pt 5
Sc
Laboratory Control Sample (LCS)
(LCS) R3424936-2 06/25/19 18:15
Spike Amount LCS Result LCS Red.
Red. Limits
LCS Oualifier
Analyte mg/I mg/I %
%
Suspended Solids 773 780 101
85.0-115
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Eaton Corporation 28091-R L1110945 07/02/19 09:02 11 of 26
WG1304002 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. !
Wet Chemistry -.by Matti. - 71110945-01:02
Method Blank (MB)
(MB) R3426189-1 06/30/191140 Cp
MB Result MB Qualifier MB MOIL MB ROL
Analyte mgh mg/I mg/1
TPH -Oil&Grease U 0,725 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3426189-2 06/30/1911:40 • (LCSD) R3426189-3 06/30/19 1140
Spike Amount LCS Result LCSD Result
Analyte mg/1 mg/1 mg/I
LCS Rec. LCSD Rec.
% %
Rec. Limits
%
LCS Qualifier LCSD Qualifier
RPD
%
RPD Limits
%
TPH -Oil&Grease 20.0 22.1 23.9
ill 120
64.0-132
T83
34
ACCOUNT:
PROJECT:.
SDG:
DATEITME: PAGE:
Eaton Corporation -
28091-R
'L1110945
07/02/19 09'02 12 of 26
WG1300332 QUALITY CONTROL SUMMARY ONELAB:NATIONWIDE.
Metals (ICP) by.Method 200.7. L1110945-01,02 ..
Method Blank (MB) C
(MB) R3424691-1 06/26/19 02:18
❑
2
MB Result MB Qualifier MB MDL MR RDL
Analyte mg/I mg/I mg/I
TC
Copper U 0.00700 0.0100
Lead U - 0.00200 0.00500
a
SS
Zinc U 0.00340 0.0500
4Cn
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3424691-2 06/26/19 02:21 • (LCSD) R3424691-3 06/26/19 02:24
5
Sf
Spike Amount LCS Result LCSD Result LCS Res. LCSD Res. Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyze mg/I mg/I mgA % % %
%
%
Copper 1.00 7.01 0.978 101 97.8 85.0-115
2.80
20
Lead 1.00 1.02 0.994 102 99A HD-115
2.36
20
7
Zinc 1.00 0.995 0.973 99.5 97.3 85.0-115
2.23
20
Gi
$AI
L1110970-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1110970-01 06/26/19 02:27 • (MS) R3424691-5 06/26/19 02:32 • (MSD) R3424691-6 06/26/19 02:35
e
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Dilution Rec. Limits
MS Qualifier
MSD Qualifier
RPD
RPD Limits
Sc
Analyte mg/1 mg/I mgA mg/1 % %
%
%
%
Copper 1.00 NO 0.967 0.978 96.7 97.8
1 70D-130
1.18
20
Lead. 1.00 . ND '1.01 _ 1.01 101 101
1 70.0-130
-
0.0756
20
Zinc 1.00 ND 0.980 0.979 97.5 97.4
1 70.0-130
0.0258
20
L1111035-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1111035-01 06/26/19 02:38 • (MS) R3424691-7 06/26/19 02:40 • (MSD) P3424691-8 06/26/19 02:43
Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec.
Dilution Rec Limits
MS Qualifier
MSD Qualifier
RPD
RPD Limits
Analyte mg/I mgA mgA mg/I % %
%
%
%
Copper 1.00 NO 0.972 0.996 97.2 99.6
1 70.0-130
249
20
Lead 1.00 ND 0.991 1.03 99.1 103
1 70.0-130
4.30
20
Zinc 1.00 NO 0.962 1.00 96.2 100
1 70.0-130
4.06
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1110945 07/02/19 09:02 13 of 26
WG1300040
QUALITY
CONTROL SUMMARY
ONELAB.NATIONWIOE,
-Volatile Organic Compounds (GC/MS)
by Method 624.1
L1110945-01,02 .. _.
Method Blank (MB)
(MB) R3423681-1 06/21/191702
Cp
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
TC
Acrolein U
0.00887
0.0500
Acrylonitrile " _ U.
6.00187
0.0100
Benzene U
0.000331
000100
SS
BromodichloromethaneU'
Bromoform U
0.000360
0,000469
0.00100
000100
4
CT1
Bromomethane U.
0.000866
0,00500
Carbon tetrachloride U
0000379
0.00100
SST
.Chlorobenzene U
0.000348
0.00100
Chlorodibromomethane U
:Chloroethane U
0.000327
0.000453
0.00100
0.00500
-
2-Chloroethyl vinyl ether U
0.00301
0,0500
Chloroform U. . .
_ 0.000324
0-00500
Chloromethane U
- 0.000276
0A0250
G
1,2-Dichlorobenzene U.
1,3-Dichlorobenzene U
6,060349
0.000220
0.00100
0.00100
- a
A
1 4-Dichlorobenzene U
0.000274
0.00100
Dichlorodifluoromethane U
0.000551
0.00500
9SC
1.1-Dichloroethane U
0.000259
0.00100
1,2-Dichloroethane U
0.000361
0,00100
1,1-Dichloroethene U
0.000398
0.00100
trans-1,2-Dichloroethene U
0,000396
0,00100
1,2-Dichloropropane U
0.000306
0.00100
cis-1,3-Dichloropropene U
0.000418
0,00100
trans-1,3-Dichloropropene U
0.000419
0.00100 -
Ethylbenzene U
0.000384
0.00100
.Methylene Chloride U
0.00100
0.00500
1,1,2,2-Tetrachloroethane U
0.000130
0.00100
7etrachloroethene U
0.000372
0.00100
Toluene U
0.000412
0.00100
1,1,1-Trichloroethane U
0.000319.
0.00700
11,2-Trichloroethane U
0.000383
0.00100
Trichloroethene U
0.000398
0.00100
-
Trichlorofluoromethane U
0.00120
0.00500
.Vinyl chloride, U
0.000259
0.00100
,
(S) Toluene-d8 102
80.0-120
(S)a,a,a-Trifluorotaluene .0.000
J2
80.0-120
(S)4-BromoDuorobenzene 83.2
80.0-120
(S)1,2-Dichloroethane-d4 976
700-130
-
ACCOUNT:
PROJECT:
- SDG:.
DATE/TIME: PAGE:
Eaton Corporation
28091-R
iL1110945 -
07/02/19 09.02 14 of 26,
WG1300040
QUALITY CONTROL
SUMMARY
ONE LAB. . NATIONWIDE. �
Volatile Organic Compounds.(GC/MS)
by Method 624.1
- _ L1110945-01,02
Laboratory Control Sample (LCS)
Cp
(LCS) R3423681-2 06121/1917:23
Spike Amount
LCS Result
LCS Red.
Red. Limits LCS Qualifier
z
Analyze mg/I
mg/I
%
%
ITC
Acrolein 0.125
0.118
94.6
60.0-140
Acrylonitrile - 0.125
0159
127
60:0.140
Benzene 0,0250
0.0255
102
65.0-135
Bromodichloromethane 0.0250
0.0243
97.2 -
70.0-135
4
Bromoform 0,0250
0.0287
115
70.0-130
Cn
Bromomethane 0.0250
0.0157 -
62.7
15.0-185
Carbon tetrachloride 0.0250
0.0239
95.7
700-130
5
Chlorobenzene - 0.0250
0.0266
106
650-135
Chlorodibromomethane 0.0250
0.0284
114
70.0-135
Chloroethane 6.0250
o.0145
57.9
40.0-160
2-Chloroethyl vinyl ether 0.125
0.116
93.0
0.100-225
Chloroform. 0.0250
0.0224
89.5
70.6-135
- 7GI
Chloromethane 0.0250
0.0326
130
0,100-205
1I2Dichlorobenzene 0.0250
0.0222
88.8
65.0-135
8A1
1,3-Dichlorobenzene 0.0250
0,0223
89.2
70.0-130
1,4.Dlchlorobenzene 0.0250
.0,0225
89.9
65.0-135
Dichlorodifluoromethane 0.0250
0.0235
94.0
49.0-155
_
SC
1.1-Dichloroethane 0.0250
00246
98.5
70.0-130
1.2-Dichloroethane 0.0250
0.0264
105
70.0-130
1,1-Dichioroethene 0.0250
0.0187
74.7
50.0-150
trans-1,2-Dichioroethene 0.0250
0.0226
90.4
70.0-130
_1.2-Dichloropropane 0.0250
0.0257
.103
35.0-165
cis-1,3-Dichloropropene 0.0250
0,0274
110
25.0-175
trans-1,3-Dichloropropene 0.0250
0.0292
117
50.0-150
Ethylbenzene 0.0250
0,0243
97.0
60.0-140
Methylene Chloride 0.0250
0.0223
89.1
60.0-140
1.1,2,2-Tetrachloroethane 0.0250
0.0266
106
60.0-140
Tetrachloroethene 0.0250
0.0306
122
70.0-130
Toluene 0.0250
0.0256
102
70.0-130
_
1,1,1-Trichloroethane 0.0250
0.0226
90.4
70.0-130
1,7,2-Trichloroethane 0.0250
0.0260
104
70.0-130
Trichloroethene 0.0250
0.0269
107
65.0135
Trichlorolluoromethane 0,0250
0.0188
75.1
50.0-150
Vinyl chloride 0.0250
0.0204
81.5
5.00-195
(S) Toluene-d8
101
80.0-120
(S)a,o,0-r itluorotolueoe
0.000
80.0-170 J2
(S)4-Bromolluorobenzene
84.5
80.0-120
(S)12-Dichloroethane-d4
105
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Eaton Corporation
28091-R
L1110945
07/02/19 09:02 15 of 26
WG1299470
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Pesticides.(GC) by'Method EPA 606.3
1-1110945-01,02
Method Blank (MB)
(MB) R3423788-2 06/23/191132
Cp
AB Result MIS Qualifier
Analyte Mg/1
AB
mq/l
MB
mg/l
TC
Aldrin U
0.00000813
0.0000500
--
Alpha BHC U
0.0000166
�0.0000500
a
$8
Beta BHC U
0.0000184
0.0000500
Delta BHC U
0.0000197
-
0.6000500 -
4
Gamma BHC U
0,0000176
0.0000500
Cn
4,4-DDD U
0.0000170
0.0000500 -
4,4-DDE U
0.0000164
0.0000500
6
_ _... ._
4,4-DDT U �
0.0000177-
_. ...
0.0000500
Dieldnn U
0.00000751
0,0000500
i
Endosulfan I U
0.0000179
0.0000500
Endosulfan II U
0.0000176
0,0000500
Endosulfan sulfate U -
0.0000196
0.0000500
Endrin U
0.0000189
0.0000500
:Endrin aldehyde U
0.0000142
0.0000500 - ..
6
Endrin ketone U
0.0000170
0.0000500
A
Heptachlor U
0.0000108
0.0000500
Heptachlor epoxide U
0.0000175
0,0000500
9
SC
_...
Hexachlorobenzene U
0.0000134
_ .. _. .. .._
0.0000500
... .. .. .. _
Methoxychlor U
0,0000193
0.0000500
Chlordane U
0.0000977
-0.000500
Toxaphene U
0.000168
0,000500
(S) Decachlorabiphenyb 43.1
10.0-144 -
(S) Tetrochlam-m-xylene 89.5
100435
Laboratory Control Sample (LCS)
(LCS) R3423788-1 06/23/19 11:19
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mgA
%
%
Aldrin 0.00100
0.000961
96.1
42.0-140
Alpha BHC 0.00100
0.00115
115
37.0-140'
Bela BHC 0.00100
0.00106
105
17.0-147
Delta BHC 0.00100
0.00113
113
IM-140
Gamma BHC 0.00100
0.00112
112
32.0-140
4,4-DDD 0,60100
0.00106
106
31.0-W
4,4-DDE 0,00100
0.000948
94.8
30.0-145
4,4-DDT 0.00100
0.000866
86.6
25.0-160 -
Dieldrin 0.00100
0.00107
107
36.0-146
4ntlosulfaril. 0.00700
0.00103
103
45.0-753
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation
28091-R L1110945 07/02/19 09:02 16 of 26
WG1299470
QUALITY CONTROL SUM 'IMARY
ONE LAS, NATIONWIDE. '
Pesticides (GC) by. Method EPA 608.3
_ _
: L1110945-01,62 -_
-
Laboratory Control Sample (LCS)
Cp
(LCS) R3423788-1 06/23/191119
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Ouarfer
7
Analyte mg/I mg/I
%
%
TC
Endosulfan 11 OD0100 0.00100
100
1.00-202
Endosulfan sulfate 0.00100 0.00110
110
26.0-144
a
SS
Endrin 0.00100 0.00108
108
30.0-147
Endrin aldehyde 0,00100 0.00102
107
5UT28
n
Endrin ketone 0.00100 0,00109
109
54.0-142
Cn
Heptachlor 0.00100 0.00100
100
34.0-140
Heptachlor epoxide 0.00100 0.00106
106
37.0-142
_
s
Hexachlorobenzene 0.00100 0:600964
96.4
35.0-120
-
Methoxychlor 0.00102
102
44.0-160
_--0.00100
(S)Decochlorobiphenyl
45.8
10.0-144
(5) Tetrachlons-m-xylene
94.3
10.0435
TGI
eAl
9Sc
ACCOUNT: PROJECT: SOG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1110945 07/02/19 09:02 17 of 26
WG1299470
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE,
Polychlorinated Blphenyls (GC) by Method-EPA-608.3
L1110945-01,02 .
Method Blank (MB)
(MB) R3423901-1 06/23/191530
Cp
MB Result
Analyte mg4
MB Qualifier M8 MDL
mg/I
MB RDL
mg/I
TC
PCB 1260 U
0.000120
0.000500
PCB 1016 U
0.000100-
0.000500
aS5
PCB 1221 U
0.0000730
0.000500
PCB 1232 - U
PCB 1242 U
0.0000420.
0,0000470
0.000500'
0.000500
4
Cn
PCB 1248 U
0.0606860
-
0.000500
PCB 1254 U
0.0000470
0.000500
s
_. __.. ...
(S) Decachlorobiphenyl 56.1
__.
10.0-144
(S) Tetrachloro-m-xylene 710
10.0-135
Laboratory Control Sample (LCS)
(LCS) R3423901-2 06/23/1915:45
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS OualiFler
Analyte
mg/I
mg/I
%
%
PCB 1260
0.00250
0.00192
76.8
8.00-140
PCB 1016
0.00250
0.00219
87.6
50.0-140
(S) Decachlorobiphenyl
44.9
10.0-144
.
(S) Tetrachloro-m-xylene
..
94.9
__.
10.0-135
L1110533-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1110533-02 06/24/19 08:10 • (MS) R3423999-1 06/24/19 08:24 • (MSD) R3423999-2 06/24/19 08:38
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Ouallfer MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg4
mg/I
mg/I
%
%
%
%
%
PCB 1260
0,00250
NO
0.00137
0.00133
54.8
53.2
1 8.00-140
2A6
38
PCB 1016
6,00250
NO
0.00197
0.00189
78.8
75.6
1 50.0-140
4.15
36
(S)Decochlorobiphenyl
374
354
10.0-144
(S)Telrochloro-m-xylene
62.4
60.3
70.0-135 '
ACCOUNT: PROJECT: SDG: - DATE7TIME: PAGE:
Eaton Corporation 28091-R L1110945 07/02/19 09:02 18 of 26
WG1300466
QUALITY
CONTROL SUMMARY
ONE LAB. NATIONWIDE. .k
'. Semi Volatile: Organic Compounds
(GC/MS) by Method 625.1
'L1110945-0T,02 _.
Method Blank (MB)
Cp
(MB) R3424171-2 06124/1913:52
MB Result
MB Qualifier MB MOIL
MB RDL
z
Analyte mg/I
mg/I
mg/I
-
TC
Acenaphthene U
0.000316
0.00100
Acenaphthylene - U
'0.606309
0.00160
aSS
Anthracene U
0.000291
0.00100
Azobenzene U
0.000318
0,0100
4
Benzidine U
0.00432
0,0100
_ _ _ - -.-
_ _ - _,- -
Cn
Benzo(a)anthracene U
0.0000975
0,00100
_ _ _.
_
Benzo(b)fluoranthene U
0.0000896
0.00100
s
;Benzo(k)fluoranthene U
0.000355
0.00100:
Benzo(g,h,gperylene U
0.000161
0.00100
Benzo(a)pyrene U
0.000340
6.00700
-
Bis(2-chlorethoxy)methane U
Bis)2-chloroethygether U
0.000329
0.00162
0.0100
0.0100
7GI
Bis(2-chloroisopropyl)ether U
0.000445
0.0100
4-Bromophenyl-phenylether U
0.006335
ao100.
-
BA
2-Chloronaphthalene U
0.000330
0.00100
4-Chlorophenyl-phenylether U
0.000303
0.0100
Chrysene U
0.000332
0.00100
z
Dibenz(a,nanthracene ,U
0.000279
0.00100
3,3-Dichlorobenzidine U
0.00202
0.0100
2,4-Dinitrotoluene U
0.00165
0.0100
2,6-Dinitrotoluene U
0.000279
0.0100
Fluoranthene U
0.00610
6.00160
- -
Fluorene U
0.000323
0.00100
_
Hexachlorobenzene U
0.000341
0.00100
Hexachloro-1,3-butadiene U
0,000329
a0loo
Hexachlorocyclopentadiene U
0.00233
0,0100
Hexachloroethane U
0.000365
0.0100
Indeno(1,2,3-cd)pyrene U
0,000279
0.00100
Isophorone U
0.000272
0.0100
,
Naphthalene U
0.000372
o.001o0
.
Nitrobenzene U
0.00D367
0.0100
n-Nitrosodimethylamine U
0.00126
0.0100
n-Nitrosodiphenylamine U
0,00119
0.0100
.
n-Nltrosodi-n-propylamine U
0.000403
0.0100.
Phenanthrene U
0.000366
0.00100
_
Benzylbutyl phthalate U
0.006275
0.00300
Bis(2-ethylhexy1)phthalate U
0.000709
0.00300
Di-n-butyl phthalate U
0.000266
0.00300
Diethyl phthalate U
0,000282
0.00300
Dimethyl phthalate U
a000283
0.00300
ACCOUNT:
'PROJECT:
SDG:
DATE/TIME: PAGE:
Eaton. Corporation
28091-R
1_7110945
07/02/1909:02 19 of 26
WG1.300466
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS) by Method 625.1
L1110945-01,02 „-
Method Blank (MB)
(MB)R3424171-2 06/24/191352
Cp
MB Result
Analyte Trill
MB Qualifier MB MDL
mg/I
MB
moll
TC
Di-n-ocryl phthalate U
0.000278
0.00300
- -
Pyrene. U�
0.000330
0.00700 -
3
t2 4-Trichlorobenzene U
0,000355
0.0100
$9
4 Chloro-3-methylphenol U
0.000263
0.0100
4
2-Chlorophenol U
0.000283
00100
Cn
2,4-Dichlorophenol U
0.000264
0.0100
'
2,4-Dimethylphenol U
0.000624
_
0.0100
U
0.00262
0.0100
Fri
2,4-Dinitrophenol U
0.00325
0.0100
2-Nitrophenol U
0.000320
0.0100
4-Nitrophenol U
0.00201
0,0100
Pentachlorophenol U
0.000313
0.0100 -
7G1
Phenol U
0,0100
2,4,6-Trlchlorophenol. U
(S)Nitrobenzene-d5 49.7
.0.000334
0.000297
0.0100
15.0-314
AI
-(S)2-Fluorobiphenyl 640
22.0-727-
(Ap-Terphenyl-dN 83.6
29.0-141
9SC
(S) Phenol-d5 16.5
8.00-424
(S) 2-Fluorophenol 277
10.0-120
(5) 2,4,6-Tribromophenol 74.5
10.0153
-
Laboratory Control Sample (LCS)
(LCS) R3424171-1 06/24/19 13:32
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
%
%
Acenaphthene
0.0500
0.0350
70.0
47.0-145
Acenaphthylene
0.0500
0.0367
73A
330-145
Anthracene
0.0500
0.0379
75.8
27.0-133
Azobenzene
0.0500
o.0395
79.0
37.0-125
Benzibine
0.100
0,0190
19.0
100-120
Benzo(a)anthracene ..
0.0500
0.0417
83.4
33.0-143
Benzo(b)fluoranthene
0.0500
0.0422
84.4
24.0-159
Benzo(k)fluoranthene
0.0500 -
0,0467
81.4
11.0-162 -
Benzo(g,h,iJperylene
0.0500
0.0410
82.0
1.00-219
Benzo)a)pyrene
0.0500
0.0417
83.4
17.0-163
Bis(2-chlorethoxy)methane
0.0500
0.0294
58.8
1.00-219
Bis(2-chloroethyl)ether
0.0500
0.0673
135
33.0-185
Bis(2-chloroisopropyl)ether
0,0500
0.0305
61.0
36.0-166
ACCOUNT:
PROJECT:
Eaton
Corporation
28091-R
SDG:
L1110945
DATMIME:. PAGE:
07/02/19 09:02 20 of 26
WG1300466
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Seml,Valatlle Organic Compounds
(GC/MS) by
Method 625.1
L1110945-01.02
Laboratory Control Sample (LCS)
Cp
(LCS) R3424171-1 06/24/191332
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
FTC
Analyte mg/I
mgA
%
%
4-Bromophenyl-phenylether 0.0500
0.0369
73.8
53.0-127
2-Chloronaphihalene 0.0500
0.0299
59.8
60.0-120 34
a
.4-Chlorophenyl-phenylether 0.0500
0.0359
71.8
25.0-156
Chrysene 0.0500
0.0381
76.2
- -
17.0-168
-1.00-227 - - -
- -
4
-0 benzla,hlanthracene 0.0500
0.0397
79.4
,..
_
_- .
Cf1
3,3-Dichlorobenzidine 0.100
0.0895
89.5
1.00-262
-2,4-Dinitrotoluene 0,0506
6.0414
82.8
39.0-139
2,6-Dinitrotoluene 0,0500
HESS
79.0
50.0-158
Fluoranthene 0,0500
0.0409
81.8
26.0137. -
Fluorene 0.0500
0.0373
74.6
59.0-121
Hexachlorobenzene 0.0500
HERS
77.0
1.00-152
Hexachloro-1,3-butadiene 0.0500
0.0129
25.8
24.0-120
7G
Hexachlorocyclopentadiene 0.0500
0.0131
26.2
_
10.0-120
Hexachloroethane 0.0500
0.0143
28.6
40.0-120 J4
BAl
Indeno(1,2,3-cd)pyrene 0.0500
0.0414
82.8
1.00-171
Isophorone 0.0500
0.0306
61.2
21.0-196
Naphthalene 0.0500
6.0267
53.4
21.0-133
Nitrobenzene 0.0500
0.0292
58.4
35.0-180
n-Nitrosodimethylamine 0.0500
0.0213
42.6
10.0-120
n-Nitrosodiphenylamine 0.0500
0.0384
76.8
44.0-120
n-Nitrosodi-n-propylamine 0.0500
0,0314
62.8
1:00-230
Phenanthrene 0.0500
0.0375
75.0
54.0-120
Benzylbutyl phthalate 0.0500
0.0408
81.6
1.00-152
Bis(2-ethylhexyl)phthalate 0.0500
0.0398
79.6
8.00-158
Di-n-butyl phthalate 0.0500
0.0428
85.6
1.00-120
Diethyl phthalate 0.0500
0.0426
85.2
1.00-120
Dimethyl phthalate 0.0500
0.0407
81.4
1.00-120
Di-n-octyl phthalate 0.0500
0.0412
82.4
4.00-146
Pyrene 0.0500
0.0392
78.4
52.0-120
1,2,4-TrichIand benzene 0.0500
0.0200
40.0
44.0-142 J4
4-Chloro-3-methylphenol 0.0500
0.0359
71.8
22.0-147.
2-Chlorophenol 0.0500
0.0271
54.2
23.0-134
2,4-Dichlorophenol 0.0500
0,0314
62.8
39.0-135
2,4-Dimethylphenol 0.0500
0.0324
64.8
32.0-120
4,6-Dinitro-2-methylphenol a0500
0.0483
96.6
1.00-181
2,4-Dinitrophenol 0.0500
0.0552
110
1.00-191
2--Nitrophenol 0.0500
0.0350
70.0
29.0-182
4-Nitrophenol 0.0500
0.0195
39.0
1.00-132
Pentachlorophenol 0.0500
6.6446
89.2
14.0-176
Phenol 0.0500
0.0115
23.0
5.00-120
ACCOUNT:
PROJECT:
SDG:
DATEMME: PAGE:
Eaton Corporation
28091-R
'L1110945
07/02/19 09:02 21 of 26
WG1300466 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE.
Semi Volatile Organic. Compounds (GC/MS).by Method 625.1 L1110945-01:02' _
Laboratory Control Sample (LCS)
(LCS) R3424171-1 06/24/191332
Spike Amount LCS Result
Analyte mg/I mg/I
2,4,6-Trichlorophenol 0.0500. 0.0395
/5J Nitrobenzene-d5
/5/ 2-Fluoroblphenyl
(S)p-Terphenyl-d14
(S) Phenol-d5
(S) 2-Fluorophenol
(S)2,4,6-Tr1bromopheno1 -
LCS Rec.
Rec. Limits LCS Qualifier
79.0
37.0-144
52.2
15.0-314
68.9
22.0-127 '
78.8
29.0-141
23.4
8.004241:.
33.9
100-120
935
100-153 -
L1111094-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1111094-01 06/24/19 17:16 • (MS) R3424171-3 06/24/19 17:37 • (MSD) R3424171-4 06/24/1917:57
Spike Amount Original Result MS Result MSD Result MS Rec.
Analyte mgA mg/I mgA mgA %
MSD Rec.
%
Dilution
Rec. Limits
%
MS Qualifier MSD Qualifier RPD
%
RPD Limits
%
Acenaphthene
0.0500
U
0.0359
0.0329
71.8
65.8
1
4Z0-145
8.72
48
Acenaphthylene
0.0500
U
0.0372
0.0342
74.4
68.4
1
33.0-145
8.40
74
Anthracene
0.0500
U
0,0381
0.0369
76.2
73.8
1
27.0-133
3.20
66
Benzo(a)anthracene
0.0500
U
0.0414
0.0407- -
82.8
814
1.
733.0-143
1.71
6
Benzo(b)fluoranthene
0,0500
U
0.0440
0.0433
88.0
86.6
1
24.0-159
1,60
71
1,2-Diphenylhytlratine
0.0500
U
0.0404.
0.0375
80.8
75.0
T
'.78:0-156
7.45
34
Benzo(k)fluoranthene
0.0500
U
0.0426
0.0412
85.2
82A
1
110-162
3,34
63
8enzo(g,h;i)perylene
0.0500
U
0.0409
0.0390
81.8
78.0
T
1,00:219
4,76
97
Senzo(a)pyrene
0,0500
U
0.0430
0.0420
86.0
84D
1
17D-163
2.35
72
8is(2-chlorethoxy)methane
0.0500
U
0.0289
DOM
57.8
54.6
1
33.0-184
5,69
54
Bis(2-chloroethyl)ether
0.0500
U
0.0444
0.0587
88.8
117
1
12.0-158
277
108
Benzidine
0.100
U
0.0323
0.0473
32.3
47.3
1
1.00-120
377
40
Bis(2-chloroisopropyl)ether
0.0500
U
0.0309
0.0301
61.8
60.2
1
36.0-166
2.62
76
4-Bromophenyl-phenylether
0.0500
U
0.0390
0.0372
78.0
74.4
1
53.0-127
4.72
43
2-Chloronaphthalene
0.0500
U
0.0308
0.0280
6i.6
56.0
1
60.0-120
J6 9.52
24
4-Chlorophenyl-phenylether
0.0500
U
0.0386
0.0357
77.2
714
1
25.0-158
7.81
61
Chrysene
0.0500
U
0.0386
0.0378
77.2
75.6
1
17.0-168
2,09
87
Dibenz(a,h)anthracene
0,0500
U
0.0396
0.6386
79.2
.772.
1
1.00-227
_256
126
33-DichlorobenzIdine
0.100
U
0.0817
0.0858
81.7
85.8
1
1.00-262
4.90
108
-2,4-0initrotoluene
0.0500
U
0.0415
0.0389
83.0
77.8
1
39.0-139
6,47
42
2,6-Dinitrotoluene
0.0500
U
0.0410
0.0384
82.0
76.8
1
50.0-158
6,55
48
Fluoranthene
0.0500
U
0.0413
0.6397
82.6
79.4
1
26.0-137
355
66
Fluorene
0.0500
U
0.0388
0.0358
77.6
71.6
1
59.0-121
8.04
38
Hexachlorobenzene
0.0500
U
0.0418
0.0400
83.6
80.0
1
1..00-152
4.40
55
Hexachloro-1,3-butadiene
0,0500
U
0.0151
0.0112
30.2
22.4
1
24.0-120
J6 29.7
62
Hexachlorocyciopentadiene
0.0500 -
U
0.0195
0.0150
39.0
30.0
1
10.0-146
261
34
- Cp
TC
aSs
4Cn
SSr
7GI
BAI
95C
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE:
Eaton Corporation 28091-R L111094507/02/19 09D2 22 of 26
WG1300466
QUALITY
CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic
Compounds
(GC/MS) by Method 625.1
't1110945-01,02
L1111O94-01 Original
Sample (OS) • Matrix
Spike (MS) • Matrix Spike Duplicate (MSD)
C p
(OS) L1111094-01 06/24/19 17:16 • (MS) R3424171-3 06/24/1917:37 •
(MSD) R3424171-4
06/24/19 17:57
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
M51) Rec
Dilution Rec. Limits MS Qualifier
MSD Oualifier RPD
RPD Limits
z
Analyte
mg/I
mgh
mg/I
mg/I
%
%
%
%
%
TC
Hexachloroethane
L. - _.__.. ___..�...-
ndeno(12,3-cdlpyrene
0.0500
._ _ .
6.0500
U
U .
0,0160
__ _
M389
0.0128
0.0377
320
778
25.6
74.4
1
1
40.0-120 J6
.--.._ _.__ _.
.. 1.00-17T
J6 22.2
--_ _._ .-_�_.-
4.47
52
-. .. _. _ _...__-.___
99
3
55
Isophorone
0.0500
U
0.0305
0.0287
610
57.4
1
21.0-196
6.08
93
Naphthalene
0,0500
U
0.0261
0.0248
52.2
49.6.
1
21.0-133 -
5.11
65
<
Nitrobenzene
0.0500
U
0.0292
0.0275
58.4
55.0
1
35.0-180
6.00
62
Cn
n-Nitrosod imethyla mine
0.0500
U
0.0208
0.0197
41.6
39.4
1
10.0-120
5.43
40
s$f
n-Nitrosodiphenylamine
0.0500
U
0.0405
0.0388
81.0
776
1
16.0-160
429
28 - _ ._
n-Nitmsodi-n-propylamine
0.0500
U
0.0311,
0.0297
62.2
59A
1
1.00-230
4.61
87
Phenanthrene
0,0500
U
0.0381
0.0366
76.2
73.2
1
54.0-120
4.02
39
Benzylbutyl phthalate
0.0500
U
0.0429
00419
85.8
-83.8 -
1
1.00-152
2.36
60
31s(2-ethylhexyI)phthalate
0.0500
U
0.0414
0.0411
82.8
82.2
1
8.00-158
0.727
82
Di-n-butyl phthalate
6.0500
0.0434
0.0431
86.8
86.2
1
.1.00-120
0.694.
47
G
Diethyl phthalate
0.0500
U
0.0425
0.0410
85.0
82.0
1
1.00-120 -
3.59
100
Dime[hyl phthalate
0.0500
U
0.0411
0.0387
822
774
1
1.00-120
6.07
183
IF e
Di-n-octyl phthalate
0.0500
U
0.0424
0.0412
84.8
82A
1
4.00-146
2,87
69 . __
Pyrene
0.0500
U
0.0403
.0397
80.6
79.4 ��
1
52.0-120
150
49
1,2,4-Trichlorobenzene
0.0500
U
0.0209
0.0181
41.8
36.2
1
44.0-142 J6
J6 14A
50
s
Sc
4-Chloro-3.methylphenol
0,0500
U
0.0350
0.0321
70.6
64.2
1
22.0-147
8.64
73
2-Chlorophenol
0,0500
U
0.0298
0.0273
59.6
54.6
1
23.0-134 _
8.76
61
2,4-Dichlorophenol
0.0500
U
0.0314
0.0303
62.8
60.6
4
39.0-135 -
3.0
50
2,4-Dimethylphenol
0.0500
U
0.0322
0.0304
64.4
60.8
1
32.0-120
5.75
58
4,6-Dinitro2-methyl phenol
0.0500
U-
0.6443
0.0465
88.6
93.0
1
1.00-181 -
4.85
203
24-Dinitrophenol
0.0500
U
0.0517
0.0523
103
105
1
1.00-191
1,15
132 -
2-Nilrophenol
0.0500
U
0.0345
0.0333
69.6
66.6
1
290-182
4.41
55
4-Nitrophenol
0.0500
U
0.0158
OD169
31.6
33.8
1
1,00-132
6.73
131
Pentachlorophenof
0.0500
U
0.0429
0.0428
85.8
85.6
1
14.0-176
0A3
86
Phenol
0.0500
U
0.0115
0.0111
23.0
22.2
1
5.00-120
3.54
64
2,4,6-Trichlorophenol
0.0500
U
0.0393
0.0377
78.6
75A -
1
37.0444
.4.16
58
(S) Nitrobenzene-d5
53.5
50.6
15.0-314
(S)2-Fluorobiphenyl
72.3
66.2
22.0427
(S)p-Terphenyl-d14
SOS
80.2
29.0-141
(S)Phenol-d5
24A-
22.1
8.60-424
(S)2-Fluoraphenal
38.0
34.7
10.0-120
(S)2.4,6-Trlbromophenol
95.0
870
100-153
-
ACCOUNT: PROJECT: SOG: DATUTIME: PAGE:
Eaton Corporation 28091-R L1110945 07/02n9 09:02 23 of 26
GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. 0
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL
Method Detection Limit,
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery. - -
RPD
Relative Percent Difference.
SDG -
Sample Delivery Group.,
Surrogate (Surrogate Standard) - Analyzes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analyzes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution -
standard, or if concentrations of analyzes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample maybe diluted for analysis. If a value different than I is used in this fela, the
result reported has already been corrected for this factor.
These are the target %recovery ranges or %difference value that the laboratory has historically determined as normal
Limits
for the method and analyze being reported. Successful QC Sample analysis will target all analyzes recovered or
duplicated within these ranges.
Original. Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RED) from a quality control
sample. The Original Sample may not be included within the. reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative If applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyze, the result in this column may state -ND" (Not Detected) or -BDL-
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection. Limit) that defines the lowest value that the laboratory could detect
or report for this analyze.
Uncertainty
ma. Confidence level of 2 sigma.
g
A brief discussion about the included sample results, Including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receiptby the laboratory fromThe field or during the analytical process. f.present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (So)
chainof custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/oranalysis. -
Qualifier Description
J The identification of the analyze is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch OC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination: spike value is low.
PI RPD value not applicable for sample concentrations less than 5 times the reporting limit.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R 1-1110945 07/0219 09.02 24 of 26
ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
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accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories In our Industry. The most significant benefit to our one location design Is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported In the attached report.
' Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
Alabama
40660
Alaska -__ --__
17_026
Arizona
A70612
Arkansas
88-0469_-__-_-___.-__„__
_ California
-__- _ 2932
oolarado
-------PH-0197
TN00003
---_-----_—
Connecticut
Florida _.
E87487
Georgia
NELAP
Georgia'
_ 923
Idaho
TN00003
Illlnnis
200008
Iowa
364
Kansas
E-10277
Kentucky i°
_
90010
Kentucky °
16
Louisiana
A130792
Louisiana
LA180010
Maine
TN0002
Maryland
324
Massachusetts
M-TNO03
Minnesota 047-999-395
Mlssisslppl TN00003
CERT0086
Third Party Federal Accreditations
Nebraska
NE-OS-15 05
Nevada
_
IN 03.2002-34
_
New Hampshire
2975
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TNO02 _
_
New Mexico'
me
New York
11742
North Carolina
Env375
North Carolina'
DW21704
North Carolina °
41
Ohlo-VAP
CL0069
Oklahoma
9915
Oregon
TN200002
Pennsylvania
6802979
Rhode Island
LA000356
South Carolina
84004
South Dakota
Na
Tennessee "
2006
Texas
T10470424518 15
Texas°
LA90152
Vermont
W2006
Virginia
460132
Washington
C847
West Virginia
233
Wisconsin
9980939910
A2LA-ISO 17025 1461.01 AIHA LAP,LLC EMLAP 100789
A2LA-ISO 17025' 1461.02 DOD 146101
Canada 1461.01 USDA P330-15-00234
EPA-Crypto TN00003
'Drinking Water ° Underground Storage Tanks 3Aquatic Toxiciry'ChemicallMicroblological "Mold °Wastewater Na Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
ACCOUNT: - PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091 R L1110945 07/02/19 09,02 25 of 26
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- r'
"A lull-7
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NCF
ative Chain of Custody Page_ol �
Fm,T*N
July 16, 2019
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attn: DWQ Central Files
Dustin A. LaClair
Environmental, Health & Safety Manager
RE: June 2019 Monthly Tier III Discharge Monitoring Report
(336) 503-6538 (office)
(336) 503-6562 (fax)
d usti n I acla ir(a)eaton. com
RECFIVED
JUL 18 Z019
CDRAIL FILES
SECTION
Attached are the analytical results and associated chain of custody for the June 18, 2019 monthly Tier III
stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater
General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility.
Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North
Carolina Division of Water Quality (NCDWQ).
I certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with the system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or other persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are
significant penalties for submitting false information, including the possibility of fine and imprisonment for
knowing violations.
Sinc X232
Dustin A. LaClair
EHS Manager
Attachments