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HomeMy WebLinkAboutNCG030027_MONITORING INFO_20190618STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ I o 1 YYYYM M D D Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 CERTIFICATE OF COVERAGE NO. NCG03 0 0 2 7 FACILITYNAME Eaton Corporation COUNTY Person PERSON COLLECTING SAMPLES Dustin LeClair LABORATORY PACE National Date submitted Lab Cent. # ENV375/DW21704/B10041 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or 0 Monthly' June (month) DISCHARGING TO CLASS ❑ORW ❑HC(W ❑Trout ❑PNA ❑Zero -flow [:]Watersupply [_]SA *Other WS-III: NSW PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 � ❑ No discharge this Period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics= Benchmarks - - 100 mg/Lor 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 Tool Room Trench (005) 06/18/2019 0.22 7.37 8.5 0.00792 0.002 (ND) 0.0315 0.806 (ND) 0.127 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Dustin LaClair Name (Print name) EHS Manager Titl ri (tY}LIe/���/ • W 0-1 IIAI TAI Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES 0 NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑ REGIONAL OFFICE CONTACT NAME: D..,Ss iID Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware t+f thSPTai a significant pprf%4 fWsubmitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Permit Date: 11/1/2018-05/31/2021 O? 1 b 70 164 Date SWU-245, last revised 11/1/2018 Page 3 of 3 2019-06-18-001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dale/lime: 05/18/19 14:30 L1110945 Additional Information Result Units Analyte PH (On Site) 8.5 so Temperature (on -site) 25.5 Deg C Gravimetric Analysis by Method 2540 D-2011 Result Oumifier MDL RDL Dilution Analysis Batch Analyle mg/I mg4 mg4 date/time Suspended Solids 7.37 0.462 3,30 1 06/25/201918:15 WG1301085 Wet Chemistry by Method 1664E Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg4 mg/I mg/l date/time TPH - Oil & Grease U 0.806 5.56 1 06/3020191140 WG1304002 Metals (ICIO) by Method 200.7 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Copper 0,00792 J 0.00700 0-0100 1 06/26/201903:00 WG1300332 Lead U 0,00200 0.00500 1 06/261201903:00 WG1300332 Zinc 0.0315 J 0,00340 0.0500 1 06/26/201903'.00 WG1300332 Volatile Organic Compounds (GC/MS) by Method 624.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ri mg/I mg/I date/time Acrolein U 0.00887 0,0500 1 06/21201919:08 WG1300040 Acrylonitrile - U 0,00187 0QdGO .1 06/21201919:08 WG1300040 Benzene U 0.000331 0,00100 1 06/21/201916:08 WG1300040 Bromodlchloromethane U 0.000380 0.00100 1 06/21/201919:08 WG1300040 Bromoform U 0.000469 0.00100 1 06/21/201919:08 WG1300040 Bromomothane - U 0.000866 0.00500 1 06/21/201919:08 WG1300040 Carbon tetrachloride U 0.000379 0.00100 1 06/21/201919:08 WG1300040 Chlorobenzene U 0,000348 0.00100 1 06/21201919:08 WG1300040 Cflood ibromomethane U 0.000327 0.00160 1 O6/21/20191908 WG1300040 Chloroethane - U 0.000453 0.00500 1 06/21/201919:08 WG1300040 2-broroethyl vinyl ether U 0.00301 0.0500 1 06/21/201919:08 WG1300040 Chloroform 0,000339 J, 0,000324 0.00500 1 06/21/201919:68 WG1300040 Chloromethane U 0.000276 0.00250 1 06/21/201919:08 WG1300040 1.2-6lchlorobenzene U 0.000349 0.00100 1 66/21/201919:68 WG1300040 13-Dichlorobenzene U 0.000220 0.00100 1 06121201919:08 WG1300040 1,4471chlorobe-nzene U 0.000274 0.00160 1 66/21/2016 im: WG1300040 Dichlorodifluoromethane U 0.000551 0.00500 1 06/21/201919:08 WG1300040 1,17Dichloroethane U 0.000259 0.00100 1 66/21/201919:08 WG1300040 1,2-Dichloroethane U 0.000361 0,00100 1 06/21/2019 19:08 WG1300040 - 1,1-fichloroethene - � U 0.000398 0.00100 - 1 06/21/201919:68 - WG1300040 trans-1,2-Dichloroethene U 0.000396 0.00100 1 06/21/201919:08 WG1300040 1.2-61chloropropane U - 0.000306 0.00100 1 661T201919:08 WG1300040 cis-1,3-Dichloropropene U 0.000418 0.00100 1 06/21/201919:08 WG1300040 trans-6 Dichloropropene U 0.000419 0.00100 1 06/21/2019 19:08 W61300640 Ethylbenzene U 0,000384 0.00100 1 06/21/201919:08 WG1300040 Methylene Chloride -U 0.00100 6.Oo500 1 66/21/201619M WG1300040 1,1,2,2.Tetrachloroethane U 0.000130 0.00100 1 06/21/201919:08 WG1300040 Tetrachloroethene 0.00187 0.000372 0.00100 1 0621/201919:68 WG1300040 Toluene U 0.000412 0,00100 1 0621/201919:08 WG1300040 _., . .. _. 1,1,1-Trichloroethane� . - . . . U .. 19 0.000319 ..... 0.00100 1 _ .. 06/21/201919:06 WG1300040 11,2-Trichloroethane U 0.000383 0.00100 1 06121/201919:08 WG1300040 ACCOUNT: PROJECT: SOG DATE/TIME: PAGE: Eaton Corporation 28091.R L1110945 07/02/19 09:02 5 of 26 2019-06-18-001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 06118/19 14:30 L1110945 Volatile Organic Compounds (GC/MS) by Method 624.1 RP Result Qualifier MDL RDL Dilution Analysis Batch mg/I al mind date/lime Trichloroothene 0.000780 J 0.000398 0.00100 1 06/21/201919:08 WG1300040 ITC Trichlorolluoromethane U 0.00120 0.00500 1 06/21/201919:08 WG1300040 Vinyl chloride U 0,000259 0,00100 1 06/21/201919:08 WG1300040 a (S)Toluene-d8 99.7 800-120 06121201919.08 WG1300040 SS (5)0.a,a-Tri/luarotoluene 0.000 12 800-120 06/21/10191908 W61300040 (S)4-Bromolluorobenzene 79.6 J2 80.0-120 061211.201919:08 WG1300040 Cn (S) 7,2-Dichloroethana-d4 99.6 70.0-130 0621/207919:08 W61300040 Pesticides (GC) by Method EPA 608.3 Result Oualifer MDL RDL Dilution Analysis Batch 5 Analyse mg/I ri mg/I date Itime QC Aldrin U 0,00000813 0.0000500 1 06/23/201914:26 WG1299470 Alpha BHC U 0.0000166 0.0000500. 1 06/23/201914:26 WG1299470 7GI Beta BHC U 0.0000184 00000500 1 06/23/201914.26 WG1299470 Delta BHC U 0.0000197 0.0000500 1 06/23/201914 26 WG1299470 e Gamma BHC U 0.0000176 0,0000500 1 06/23/20191426 WG1299470 [Al Chlordane U - 0.0000977 0.000500 1 06/2 3/2019 14:26 WG1299470 4,4-DDD U 0.0000170 0.0000500 1 06/23/201914:26 WG1299470 9 qC 4,4-DDE U _ 0.0000164 0.0000500 1 06R3R01914:26 WG1299470 4,4-DDT U 0,0000177 0.0000500 1 06/23/201914:26 WG1299470 Dieldrin U 0.00000751 0.0000500 1 06/23/2019 14:26 WG12994111 707 Endosullan I U 0.0000179 0.0000500 1 06/23/201914:26 WG1299470 Endosullan ll U 0.0000176 0.0000500. - 1 06/23/201914:26 WG1299470 - Endosulfan sulfate U 0,0000196 0.0000500 1 06/23/201914:26 WG1299470 Endrin U 0.0000189 0.0000500 1 06123120191426 WG1299476 Endrin aldehyde U 0.0000142 0.0000500 1 06f23/201914:26 WG1299470 Endrin ketone : U - 0.0000170 0.0000500 • 1 06123/2019 14:26 WG1299470 Heptachlor U 0.0000108 0.0000500 1 06/23/201914:26 VIG1299470 - Heptachlor epoxide U .. - 0.0000175 .. 0.0000500 1 . _.. 06/23/20191426 -- . . WG1299470 Hexachlorobenzene U 0,0000134 0.0000500 1 06/23/20191426 WG1299470 Methoxychlor U 0.0000193 0.0000500 1 06123/20191426 W61299470 Toxaphene U 0,000168 0.000500 1 06123/201914:26 WG1299470 /SJDecachloiobiphenyl 59.3 - 10.0-144 0623120191426 WG1299470 (S)Tetrachloro-m-xylene 61.4 10.0-135 06123120191426 WG1299470 Polychlorinated Biphenyls (GC) by Method EPA-608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyle mg4 mg/I mgll date/time PCB 1016 U 0,000100 0.000500 1 06124/201908:51 WG1299470 PCB 1221 U 0.0000730 0.000500 - 1 06/24/201908:51 WG1299470 - PCB 1232 U 0.0000420 0.000500 1 06/24/2019 08:51 WG1299470 PCB 1242 U 0.0000470 0.000500 1 06/24/2019 08:51 WG1299470 PCB 1248 U 0.0000360 0.000500 1 06/24/2019 08:51 WG1299470 PCB 1254 U 0.000070 0.000560 1 06/24/2019 08:51 WG1299470 PC81260 U 0.000120 0.000500 1 06/24/2019 08:51 WG1299470 (SJ Decochlorobiphenyl 579 100144 06124120190851 WG1299470 (S Tetrachloro-m-xylene 56.6 10.0-135 061241201908.51 WG1299470 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Oualifier MDL RDL Dilution Analysis Batch Analyse mg/I mg/I mgll date/time Acenaphthene U 0,000316 0.00100 1 06/25/201915:03 WG1300466 Acenaphtiiylene U - 0.000309 0.00100 1 06/25I201915:03 WG1300466 Anthracene U 0,000291 0.00100 1 06/25/201915:03 WG1300466 Denzil U 0.00432 0.0100 1 66/25/20196:03 WG1300466 ACCOUNT: .PROJECT: SDG: DATEMME: PAGE' Eaton Corporation _ 28091-R L1110945 07/02/19 09:02 6 of 26 2019-06-18-001 SAMPLE RESULTS - 01 ONE LAS. NATIONWIDE. Collected dateltime: 06/18/19 14:30 L1110945 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Analyte Result mg/1 Oualifer MDL mg/I RDL mg/I Dilution Analysis date/lime Batch Benzo(a(anthracene U 0.0000975 0.00100 1 06/251201915:03 WG1300466 Benzo(b(fluoranthene J 0.0000896 0.00100 1 06125/201915:03 WG1300466 Benzo(k(fluoranthene U 0.000355 0,00100 1 06/25n01915:03 WG1300466 Benzo(g,h,ilperylene U - 6.600161 0.00100 1 06/251201915:03 WG1300466 Benzo(a)pyrene U 0,000340 0.00100 1 06/25/201915:03 WG1300466 Bis(2-chlorethoxy)methane U 0.000329 0DI00 1 06/25n01915-03 WG1300466 Bis(2-chloroethy;)ether U 0.00162 0.0100 1 06125/201915:03 WG1300466 B142-chloroisopropyl)ether U - 0.000445 0.0100 1 - 06125/201915:03 WG1300466 4 Bromophenyl-phenylether U 0,000335 0.0100 1 06125/201915:03 .WG1300466 2-Chloronaphihalene _ U J4 0.000330 0.00100 1 66/25/201915:03 WG1300466 4 Chlorophenyl-phenylether J 0.000303 0,0100 1 06125/201915.03 WG1300466 Chrysene -U 0.000332 0.00100 •1 06/25I201915:03 WG1300466 Dibenz(a,h(anthrncene U 0.000279 0,00100 1 06/25/2019 15:03 WG1300466 3,3-Dichlorobenzidine U 0.06202 0.0100 1 0605/201915:03 WG1300466 24 Dinitrotoluene J 0.00165 0,0100 1 06/25/20191503 WG1300466 2,6-61nilrotoluene - U 0.000279 0.0100 1 06/25/201915:03 WG1300466 1,2 Diphenylhydrazine U 0.000318 0.0100 1 06/251201915:03 WG1300466 Flucenthene U 0.000310 0.00100 1 06/25/201915:03 WG1300466 Fluorene U 0,000323 0.00100 1 06/25/201915:03 WG1300466 Hexachlorobenzene U 6.000341F 0.00100 1 06/25n0191503 WG1300466 Hexachloro-1,3-butadiene U 0.000329 0.0100 1 06/25/201915:03 WG1300466 Hexachlorocydopen adiene U 0.00233 0.0100 1 06I25/201915:03 WG1300466 Hexachloroethane U J4 0.000365 0.0100 1 06125/201915:03 WG130G466 Indeno(1,2,3td(pyrehe If 0.000279 0.00100 1 66/25n01915:03 WG1300466 Isophorone U 0,000272 0.0100 1 06/25/201915:03 .. WG1300466 _ Naphthalene � U � . ..... 0.000372 _ .. _ 0.00100 .. 1 . 06125/2019 15:03 WG1300466 Nitrobenzene U 0.000367 0.0100 1 06125/2019 is 03 WG1300466 n-Nilrosddimethylamine U 0.00126 0.0100 1 06I25I201915:03 WG1300466 n-Nilrosodiphenylamine U 0.00119 0.0100 1 061251201915:03 WG1300466 n-Nitrosodl n-propylamine U - 0.000403 0.0100 1 06/25I201915:03 WG1300466 Phenanthrene U 0.000366 0.00100 1 06/25n01915:03 WG1300466 Beniylbutyl phthalate O.000Z75 0-00300 1 06/25n01)15:03 WG1300466 Bis(2- ethyl hexyl)phthalate U 0.000709 0,00300 1 06/25/201915:03 WG1300466 . ..__.. _._.__ .. . .... Din -butyl phthalate .. .. .. U .. 0.000266 66 - ..___ 0.00300 - 1 _ ... 06/25/2019 i5:03 ... .. WG13004fi6 Diethyl phthalate U 0.000282 0.00300 1 06125/201915:03 WG1300466 _. .. Dinletbyl phthalate - U _. .... _._ 0.000283 0.00300 _. 1 06/25/201915:03 .. .. WG1300466 Di-n-octyl phthalate U 0.000278 0,00300 1 06125/201915.03 WG1300466 Pyrene U omi:330 0.00100 1 06/251201915:03 WG1300466 1,2,4-Trichlorobenzene U J4 0.000355 0,0100 1 06/251201915:03 WG1300466 4-Chloro-3:methylphenol U 0.000263 0.0100 1 06/251201915:03 WG1300466 2-Chlorophenol U 0,000283 0.0100 1 06/25/201915:03 WG1300466 2,4-Dichlorophenol U 0.000284 0.0100 1 06/25/201915:03 WG1300466 24 Dimethylphenol U 0.000624 0,0100 1 06125/201915:03 WG1300466 4,6-6initro-2-methyl0enol U 0.00262 0.0100 1 06/251201915:03 WG1300466 2,4-Dinitrophenol U 0.00325 0.0100 1 06/251201915:03 WG1300466 2-Nitrophenol U 0.000320 0.0100 1 06/25/201915:03 WG1300466 4-Nitrophenol U 0.00201 0.0100 1 06/25/201915:03 WG1300466 Pentachlorophenol U 0.000313 0.0100 1 06/251201915:03 WG1300466 Phenol 0.00176 J 0.000334 0.0100 1 06/25/201915:03 WG1300466 2,4,6-Trichlorophenol J . 0.000297 0,6100 1 06M/201915:03 WG1300466 /5/2-Fluorophenol 18.2 10.0-120 062WO1915.03 WG1300466 (5)Phenol-d5 115 - 800-424 66125120791503 WG1300466 (S) Nitrobenzene-d5 33.7 15,0-314 0625201915.03 WG1300466 (S)2-Fluoroblphenyl 38.7 22.0d27 067257201915:03 WG1300466 (S)2,4,6-Fribromophenol 535 1a0-153 05/2520191503 WG1300466 (S)p-Ferphenybdl4 . 58.5 29.0-141 06725/201915.03 WG1300466 ACCOUNT: PROJECT: SDG: DATE/TIME: Eaton Corporation 28091-R 1-1110945 07/02/1909.02 PAGE: 7 of 26 2019-06-18-005 SAMPLE RESULTS - 02 ONeLAe NATIONWIDE. Collected date/lime: 06/18/19 14:45 L1110945 Additional Information Result Units pH (On Site) 8 so Temperartue (on -site) 317 Deg C Gravimetric Analysis by Method 2540 D-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/l mg/I mg/l date/time Suspended Solids 711 0.420 3,00 1 06/25/201918:15 WG1301085 Wet Chemistry by Method 1664B Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time TPH - Oil R Grease U 1.45 10.0 1 06/3020191140 WG1304002 Metals (ICP) by Method 200.7 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgll mg/I mg/I date/time Copper 0.0148 0,00700 0.0100 1 06126/201903:03 WG1300332 Lead 000241 1 0.00200 - 0.00500 - 1 06/26/201903:03 WG1300332 Zinc 0.0336 J 0.00340 06500 1 0666/201903:03 WG1300332 Volatile Organic Compounds (GC/MS) by Method 624.1 Analyte Result mg/I Qualifier MDL iii RDL mg/I Dilution Analysis date/time Batch Acrolein U 0.00887 0.0500 1 06121120191929 WG1300040 Acrylonitrile - 'U 0.00187 0.0100 1 06/21/201919:29. WG1300040 Benzene U 0.060331 0.00100 1 06/21I20191929 WG1300040 Bromodichloromethane U 0,000380 0.00100 1 06121/201919:29 WG1300040 Bromoform U 0.060469 0.00100 1 0621/201919:29 WG1300040 Bromomethane U - 0.000866 0.00500 1 06121/201919:29 WG1300040 Carbon tetrachloride U 0.000379 0.00100 1 06/21/201919:29 WGI300040 Chlorobenzene 11 GD00348 .0.00100 1 06/2l/201919:29 WG1300040 Chlorodibromomethane U 0.000327 0.00106 1 06121/201919:29 WG1300040 Chloroethane - U 0,000453 0.00500 1 06/21/201919:29 WG1300040 2-Chloroelhyl vinyl ether U 0.00301 0.0500 1 06/21/201919:29 WG1300040 Chloroform u 0.000324 OA0500, 1 0601/201919:29 WG1300040 Chloromethane U 0.000276 0.00250 1 06/21/201919:29 WGI300040 1,2-Dichlorobenzene u 0.000349 0.00100 1 06/21120191929 WG1300040 13 Dichlorobenzene U 0.000220 0.00100 1 06/21/201919:29 WG1300040 1,4-61chlorobenzene u 0,000274 0,00100 1 06/21/201919:29 WG1306040 Dichlorodifluoromethane U 0,000551 0.00500 1 06/211201919:29 WG1300040 1,1-Dichloroethane _ u 0.060259 Ob0100 1 06121/201919:29 WG1300040 1,2-Dichloroethane U 0.000361 0.00100 1 06/21/201919:29 WG1300040 1,1-Dichloroethene u O.o00398 0.00100 1 106/21/201916:29 W31300040 trans-1,2-Dichloroethene u 0.000396 0.00100 1 06/21/201919:29 WG1300040 1,2-Dichloropropane - u 0,060306 0.00100 1 06/21/2019 19:29 WGI300040 cis-1,3-Dichloropropene U 0.000418 0.00100 1 06121/201919:29 WG1300040 trans-1,3-Dichloropropene U 0.000419 0.00100 - 1 06/21/201919:29 WG1300040 Elhylbenzene u 0.000384 0.00100 1 062V201919:29 WG1300040 Methylene Chloride u - - 0.00100 0.60500 1 661211201919:29 WG1300040 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 06/21/201919:29 WG1300040 Tetrachloroetfiene U 0.060372 6.00100 1 06/2V201919i29 WG1300040 Toluene U 0.000412 0.00100 1 06/21/201919:29 WG1300040 1,1,1-Trichloroethane U 0.000319 0.00100 1 06/21/201919:29 W67300040 11,2-Trichloroethane u 0.000383 0.00100 1 06/21/201919:29 WG1300040 9 ACCOUNT: PROJECT: 90G: - DATE/TIME' - PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09,02 8 of 26 2019-06-18-005 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected daleltlme: 06/18/19 14:45 L1110945 Volatile Organic Compounds (GC/MS) by Method 624.1 1 Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/I mg/1 mg/I date/time Trichloroethene U 0.000398 0.00100 1 06/211201919:29 WG1300040 FTC] Trichlarofluarome[hane U 0.00120 0.00500 1 O6/21/201919:29 WG1300040 Vinyl chloride U 0.o00259 0,00100 1 0601/201919:29 WG1300040 a (S)Toluene-d8 96.5 80.0-120 0672201919.29 WG1300040 $5 (S)a.o,a- Trilluorotoluene 0000 J2 80.6-120 06211201919:29 WG7300040 (S)4-Bromol7uombenzene 74.4 J2 80.0-120 06211201919.29 WG1300040 ° S) l2-Dichloroethane-dal 99.2 70.0-130 OkV201919.29 WG1300040 Pesticides (GC) by Method EPA 608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyze mg/I mg/I mg/I date/time Aldrin U 0.00000813 0.0000500 1 06/23/201914:38 WG1299470 Alpha BHC U 0.0000iis 0.0o00500 1 06M/201914:38 WG1299470 Beta BHC U 0.0000184 0.0000500 1 06/231201914:36 WG1299470 Delta BHC U 0.0000197 0.0000500 1 06/23/201914:38 WG1299470 Gamma BHC U 0.0000176 0.0000500 1 06/23/2019 14 38 WG1299470 Chlordane U 0.0000977 0.000500 1 06I23I201914:38 WG7299470 4,4-DDD U 0.0000170 0.0000500 1 06123/201914:38 WG1299470 4,4;6DE U 0.0000164 0.0000500 1 06/23/201914:M WG1299470. _ 4,4-DDT U 0.0000177 0.0000500 1 06MMB)14:38 WG1299470 Oieldrin -U O.000OO75T 0.0000500 1 061231201914:38 WG1299410 EndosulfanI U 0.0000179 0.0000500 1 06/231201914:38 WG1299470 Endosulfan II U 0.0000176 0.0000500 1 06/231201914:38 WG1299470 Erdosultan sulfate U 0.0000196 0,0000500 1 06/231201914:38 WG1299470 Endrin U 0.0000189 0.0000500 1 06I2300191446 WG1299470 Endrin aldehyde U 0.0000142 0.0000500 1 06/23/201914:38 WG1299470 Endrin ketone 0.0000170 0.0000500 1 06/23I201914:36 W61299470 ' Heptachlor U 0,0000108 0.0000500 1 06/23/2019 14:38 WG1299470 Heptachlor epoxide U 0.0000175 0.0000500 1 06123R01914:38 WG7299470 Hexachlorobenzene U 0.0000134 0.0000500 1 061231201914:38 WG1299470 _.. . ... -- Methdxychlor U .. . . 0.0000193 -- o- -' 0.0000500 _ - 1 ..._. _ 06R3/201914:38 ... WG1299470 Toxaphene U 0.000168 0.000500 1 06/23/201914:38 WG1299470 (S/Decachldrabiphenyl 75.6 10.0-744 0623/10191438 WG1299470 (S)Tetrochloro-m-Mene 71.8 10.0-135 061231201914.38 WG1299470 Polychlorinated Biphenyls (GC) by Method EPA-608.3 Analyze Result mgll OualiBer MDL mg/I RDL mgll Dilution Analysis date/time Batch PCB 1016 U 0.000100 0.000500 1 06/24/201909:05 WG1299470 PCB 1221 - U 0.0000730 0.000500 1 06/241261909:05 WG1299470 PCB 1232 U 0.0000420 0.000500 1 06/24/201909:05 WG1299470 PCB 1242 U 0.0000470 0.000500 1 06124/201909:05 WG1299470 PCB 1248 U 0,0000860 0.000500 1 06124/2019 09:05 WG1299470 PCB 1254 U 0.0000470 0.000500 1 06/24/2019 09:05 WG1299470 PCB 1260 U 0.000120 0,000500 1 06124120190905 WG1299470 (5) 0emchldiobiphenyl 70.1 . 70.0-144 06241201909:05 WG1299470 (S) Tetrachloro-m-xylene 65.1 10.0-135 061241201909:05 WG1299470 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Acenaphthene U 0.000316 0.00100 1 06/24/201914:53 WG1300466 Acenaphthylene U. _ 0.000309 0.00100 1 061241201914:53 WG1300466 Anthracene U 0.000291 0.00100 1 06124/201914:53 WG1300466 Benzidine U 0.00432 0.0100 1 06/24/2019 14:53 WG1300466 FOCI 7GI aAl 9SC ACCOUNT: PROJECT: SDG' DATE/TIME: PAGE: Eaton Corporation 26091-R L1110945 07/02/19 09.02 9 of 26 2019-06-18-005 SAMPLE RESULTS 02 ONE LAB. NATIONWIDE. � Collected dale/lime: 06118/1914:45 L1110645 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Analyte Result mg/I Qualifier MDL nal RDL mg/I Dilution Analysis date/time Batch Cp Benzo(a)anthraceno U 0.0000975 0.00100 1 06124/2019 14:53 WG1300466 a Tcthehe Benzo(b)fluoran - U � � 0.0000896 0.00100 1 06/241201914:53 WG73004fi6 Benzo(k)fluoranthene U 0.000355 0.00100 1 06/24/2019 14:53 WG1300466 aSS] Benzo(g,h.i)perylene U 6.600161 0.00100 1 06/24001914:53 WG1300466 Benzo(a)pyrene U 0.000340 0.00100 1 O6/24/2019 14:53 WG1300466 Bis(2-chlorethoxy)methane U _ 0.000329 0.0100 1 06/241201914:53 WG1300466 4 Cn Bis(2-chloroethypether U 0.00162 � 0.0100 1 06/24/2019 14:53 WG1300466 Bls(2-chlorolsopropy)ether U 0.006445 0.0100 1 013/24I2019 14:53 WG1300466 4-Bromophenyl-phenylether U 0,000335 0.0100 1 06/24/2019 14:53 WG1300466 2-Chloromplamalene U J4 0.000330 0.06100 1 06124/201914:53 WGI300466 4-Chlorophenyl-phenylether U 0.000303 0.0100 1 06/241201914:53 WG1300466 5 Chrysene U � 0.000332 0.00700 1 O6/24201914:53 WG1300466 Dibenz(a,h)anthracene U 0.000279 0.00100 1 06/24/2019 14:53 WG1300466 z 3,3 Dichlorobenzidine .. U, 0.00202� 0,0100 1 . 06124/201914:53 WG1300466 GI 2A Dinitrotoluene U 0.00165 0.0100 1 06/24/2019 14:53 WG1300466 _ .. . 2.6-Dimtrotaluene U 0.000279 ... .. 0.0100 1 ...__- _ .. Ofi/24120191453 WG7300466 aAl 1,2-Diphenylhydrazine U 0,000318 0.0100 1 06/241201914:53 WG1300466 Fluoranthene U - 0.000316 0.00100 1 06/24/201914:53 WG130046.6 s Fluarene U 0.000323 0.00100 1 06/241201914:53 WG1300466 SC HexachIchobonzene U 0.000341 O.o0100. 1 06/240019 14:53 W61300466 Hexachloro-13-buediene U 0.000329 0,0100 1 06/2412019 14:53 WG1300466 --....e_._. Hexachlorocydopentaoiene ... ._ .. U ... .. ._ .. 0.00233 _. _......... - 0.0160 1 06/24/2019 14:53 .. .. WG1300466 Hexachloroethane U J4 0,000365 0.0100 1 06/24I201914:53 WG1300466 Indeno(1),3td)pyrene - U 0.000279 0.00100 1 06/2412019114:53 - WG1300466 Isophorone U 0.000272 0.0100 1 06/24/2019 14:53 WG1300466 Naphthalene - U 0 000372 6.00100 - 1 06/241201914:53 WG1300466 Nitrobenzene U 0.000367 0.0100 1 06/24/2019 14:53 WG1300466 .. n-Nitrosodimethylamihe U 000126 26 ... 0.0100 _ 1 _._. _ �O6/24201914.53 53 _ ... WG1300466 n-Nitrosodiphenylamine U 0.00119 0.0100 1 06124/201914:53 WG1300466 n-Nitrosodi-n-propylamme U 0.000403 0.0100 1 06%24201914:53 W61300466 Phenanthrene U 0.000366 0.00100 1 06124/201914:53 WG1300466 Benzylbutyl phthalate, U 6600275 0.00300 1 06124/201914:53 W(31300466� - Bis(2-ethylhexyl)phlhalate U 0.000709 0.00300 1 0624/201914:53 WG1300466 Di-n-butyl phthalate 0.000310 J ' 0.000266 0.00300 1 06/24/20191453 WG7300466 Dlethyl phthalate U 0.000282 0.00300 1 06/241201914:53 WG1300466 Dlmethyl phthalate U 6.000283 0.00300 1 06/24/201914:53 W61300466 Di-n-octyl phthalate U 0,000278 0.00300 1 06/24/2019 14:53 WG1300466 Pyrene U .. 0.000330 000100 1 0124/201914:53 WG1300466 . 1,2,4-Trichlorobenzene U J4 0.000355 0.0100 1 06/241201914:53 WG1300466 4-Chloro-3-methylphenol U 0.000263 0.0100 1 06/241201914:53 'WG1300466 2-Chlorophenol U 0,000283 0.0100 1 06124/201914:53 WG1300466 2,4-Dichlor6phehol - U 0.000284 0.0100 1 06/24/2019 14:53 WG1300466 - 2,4-Dimethylphenol U 0.000624 0.0100 1 06/241201914:53 WG1300466 4,6-Dinitro-2-methylphenol U _ 0,00262 0.0100 1 06/241201914:53 WG1300466 2,4-Dinitrophenol U 0.00325 0,0100 1 06/24/2019 14:53 WG1300466 2-Nitrophenol U 0.000320 0.0100 1 06/24/2019 14:53 WG1300466 4-Nitrophenol U 0,00201 0,0100 1 06/241201914:53 WG1300466 Pentachlorophenol U 0.000313 0.0160 1 06/24/2019 14:53 WG1300466 Phenol 0,00164 J 0,000334 0.0100 1 06/24/2019 14:53 WG1300466 2 A,6-Trichlorophenol U - 0.000297 0.0100 1 06/24/201914:53 WG1300466 (S)1-Fluorophenol 19.3 10.0-120 0612412019 14 53 WGI300466 (S)Phendf-d5 12.8 8.00-424 06/24201914:53 W61360466 (S) Nitrobenzene-d5 33.6 150-314 06124201914,53 WG1300466 /S/2-Fluorobiphenyl 39.3 22.0-127 06241701914.53 WG1300466 (S)2,4,6-Tribromophenol 540 10.0-153 06241201914:53 WG1300466 (5/p-Terp6enyl-d14 543 29.0-141. ' 06/24/201914:53 WG1300466 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporallon 28091-R L1110945 07/02/19 09.02 10 of 26 ONE LAB. NATIONWIDE. WG1301085 QUALITY CONTROL.SUMMARY � Gravimetrlc Analysis by Method 2540 D-2011 _ _ L1110945-.01.02: - - Method Blank (MB) C (MB) R3424936-1 06/25/1918:15 a 2 MB Result MB Oualifier M8 MOIL MB ROL Analyte mg/I mg)] mg/I Tc Suspended Solids U 0.350 2.50 aSs 4Cn L111O831-01 Original Sample (OS) • Duplicate (DUP) (OS) L1110831-01 06/25/1918:15 • (DUP) R3424936-3 06/25/1918:15 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits s Sr Analyte mg/I mg/I % % Suspended Solids 58.8 61.2 1 4.00 5 Q L111O911-01 Original Sample (OS) • Duplicate (DUP) 7GI (OS) L1110911-01 06/25/1918:15 • (DUP) R3424936-4 06/25/1918:15 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPO Limits a [Al Analyte mg/I mg/I % % Suspended Solids 21.2 22.6 1 6.39 Pt 5 Sc Laboratory Control Sample (LCS) (LCS) R3424936-2 06/25/19 18:15 Spike Amount LCS Result LCS Red. Red. Limits LCS Oualifier Analyte mg/I mg/I % % Suspended Solids 773 780 101 85.0-115 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09:02 11 of 26 WG1304002 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. ! Wet Chemistry -.by Matti. - 71110945-01:02 Method Blank (MB) (MB) R3426189-1 06/30/191140 Cp MB Result MB Qualifier MB MOIL MB ROL Analyte mgh mg/I mg/1 TPH -Oil&Grease U 0,725 5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3426189-2 06/30/1911:40 • (LCSD) R3426189-3 06/30/19 1140 Spike Amount LCS Result LCSD Result Analyte mg/1 mg/1 mg/I LCS Rec. LCSD Rec. % % Rec. Limits % LCS Qualifier LCSD Qualifier RPD % RPD Limits % TPH -Oil&Grease 20.0 22.1 23.9 ill 120 64.0-132 T83 34 ACCOUNT: PROJECT:. SDG: DATEITME: PAGE: Eaton Corporation - 28091-R 'L1110945 07/02/19 09'02 12 of 26 WG1300332 QUALITY CONTROL SUMMARY ONELAB:NATIONWIDE. Metals (ICP) by.Method 200.7. L1110945-01,02 .. Method Blank (MB) C (MB) R3424691-1 06/26/19 02:18 ❑ 2 MB Result MB Qualifier MB MDL MR RDL Analyte mg/I mg/I mg/I TC Copper U 0.00700 0.0100 Lead U - 0.00200 0.00500 a SS Zinc U 0.00340 0.0500 4Cn Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3424691-2 06/26/19 02:21 • (LCSD) R3424691-3 06/26/19 02:24 5 Sf Spike Amount LCS Result LCSD Result LCS Res. LCSD Res. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyze mg/I mg/I mgA % % % % % Copper 1.00 7.01 0.978 101 97.8 85.0-115 2.80 20 Lead 1.00 1.02 0.994 102 99A HD-115 2.36 20 7 Zinc 1.00 0.995 0.973 99.5 97.3 85.0-115 2.23 20 Gi $AI L1110970-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1110970-01 06/26/19 02:27 • (MS) R3424691-5 06/26/19 02:32 • (MSD) R3424691-6 06/26/19 02:35 e Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Sc Analyte mg/1 mg/I mgA mg/1 % % % % % Copper 1.00 NO 0.967 0.978 96.7 97.8 1 70D-130 1.18 20 Lead. 1.00 . ND '1.01 _ 1.01 101 101 1 70.0-130 - 0.0756 20 Zinc 1.00 ND 0.980 0.979 97.5 97.4 1 70.0-130 0.0258 20 L1111035-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1111035-01 06/26/19 02:38 • (MS) R3424691-7 06/26/19 02:40 • (MSD) P3424691-8 06/26/19 02:43 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mgA mgA mg/I % % % % % Copper 1.00 NO 0.972 0.996 97.2 99.6 1 70.0-130 249 20 Lead 1.00 ND 0.991 1.03 99.1 103 1 70.0-130 4.30 20 Zinc 1.00 NO 0.962 1.00 96.2 100 1 70.0-130 4.06 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09:02 13 of 26 WG1300040 QUALITY CONTROL SUMMARY ONELAB.NATIONWIOE, -Volatile Organic Compounds (GC/MS) by Method 624.1 L1110945-01,02 .. _. Method Blank (MB) (MB) R3423681-1 06/21/191702 Cp MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I TC Acrolein U 0.00887 0.0500 Acrylonitrile " _ U. 6.00187 0.0100 Benzene U 0.000331 000100 SS BromodichloromethaneU' Bromoform U 0.000360 0,000469 0.00100 000100 4 CT1 Bromomethane U. 0.000866 0,00500 Carbon tetrachloride U 0000379 0.00100 SST .Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U :Chloroethane U 0.000327 0.000453 0.00100 0.00500 - 2-Chloroethyl vinyl ether U 0.00301 0,0500 Chloroform U. . . _ 0.000324 0-00500 Chloromethane U - 0.000276 0A0250 G 1,2-Dichlorobenzene U. 1,3-Dichlorobenzene U 6,060349 0.000220 0.00100 0.00100 - a A 1 4-Dichlorobenzene U 0.000274 0.00100 Dichlorodifluoromethane U 0.000551 0.00500 9SC 1.1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0,00100 1,1-Dichloroethene U 0.000398 0.00100 trans-1,2-Dichloroethene U 0,000396 0,00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0,00100 trans-1,3-Dichloropropene U 0.000419 0.00100 - Ethylbenzene U 0.000384 0.00100 .Methylene Chloride U 0.00100 0.00500 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 7etrachloroethene U 0.000372 0.00100 Toluene U 0.000412 0.00100 1,1,1-Trichloroethane U 0.000319. 0.00700 11,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 - Trichlorofluoromethane U 0.00120 0.00500 .Vinyl chloride, U 0.000259 0.00100 , (S) Toluene-d8 102 80.0-120 (S)a,a,a-Trifluorotaluene .0.000 J2 80.0-120 (S)4-BromoDuorobenzene 83.2 80.0-120 (S)1,2-Dichloroethane-d4 976 700-130 - ACCOUNT: PROJECT: - SDG:. DATE/TIME: PAGE: Eaton Corporation 28091-R iL1110945 - 07/02/19 09.02 14 of 26, WG1300040 QUALITY CONTROL SUMMARY ONE LAB. . NATIONWIDE. � Volatile Organic Compounds.(GC/MS) by Method 624.1 - _ L1110945-01,02 Laboratory Control Sample (LCS) Cp (LCS) R3423681-2 06121/1917:23 Spike Amount LCS Result LCS Red. Red. Limits LCS Qualifier z Analyze mg/I mg/I % % ITC Acrolein 0.125 0.118 94.6 60.0-140 Acrylonitrile - 0.125 0159 127 60:0.140 Benzene 0,0250 0.0255 102 65.0-135 Bromodichloromethane 0.0250 0.0243 97.2 - 70.0-135 4 Bromoform 0,0250 0.0287 115 70.0-130 Cn Bromomethane 0.0250 0.0157 - 62.7 15.0-185 Carbon tetrachloride 0.0250 0.0239 95.7 700-130 5 Chlorobenzene - 0.0250 0.0266 106 650-135 Chlorodibromomethane 0.0250 0.0284 114 70.0-135 Chloroethane 6.0250 o.0145 57.9 40.0-160 2-Chloroethyl vinyl ether 0.125 0.116 93.0 0.100-225 Chloroform. 0.0250 0.0224 89.5 70.6-135 - 7GI Chloromethane 0.0250 0.0326 130 0,100-205 1I2Dichlorobenzene 0.0250 0.0222 88.8 65.0-135 8A1 1,3-Dichlorobenzene 0.0250 0,0223 89.2 70.0-130 1,4.Dlchlorobenzene 0.0250 .0,0225 89.9 65.0-135 Dichlorodifluoromethane 0.0250 0.0235 94.0 49.0-155 _ SC 1.1-Dichloroethane 0.0250 00246 98.5 70.0-130 1.2-Dichloroethane 0.0250 0.0264 105 70.0-130 1,1-Dichioroethene 0.0250 0.0187 74.7 50.0-150 trans-1,2-Dichioroethene 0.0250 0.0226 90.4 70.0-130 _1.2-Dichloropropane 0.0250 0.0257 .103 35.0-165 cis-1,3-Dichloropropene 0.0250 0,0274 110 25.0-175 trans-1,3-Dichloropropene 0.0250 0.0292 117 50.0-150 Ethylbenzene 0.0250 0,0243 97.0 60.0-140 Methylene Chloride 0.0250 0.0223 89.1 60.0-140 1.1,2,2-Tetrachloroethane 0.0250 0.0266 106 60.0-140 Tetrachloroethene 0.0250 0.0306 122 70.0-130 Toluene 0.0250 0.0256 102 70.0-130 _ 1,1,1-Trichloroethane 0.0250 0.0226 90.4 70.0-130 1,7,2-Trichloroethane 0.0250 0.0260 104 70.0-130 Trichloroethene 0.0250 0.0269 107 65.0135 Trichlorolluoromethane 0,0250 0.0188 75.1 50.0-150 Vinyl chloride 0.0250 0.0204 81.5 5.00-195 (S) Toluene-d8 101 80.0-120 (S)a,o,0-r itluorotolueoe 0.000 80.0-170 J2 (S)4-Bromolluorobenzene 84.5 80.0-120 (S)12-Dichloroethane-d4 105 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09:02 15 of 26 WG1299470 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides.(GC) by'Method EPA 606.3 1-1110945-01,02 Method Blank (MB) (MB) R3423788-2 06/23/191132 Cp AB Result MIS Qualifier Analyte Mg/1 AB mq/l MB mg/l TC Aldrin U 0.00000813 0.0000500 -- Alpha BHC U 0.0000166 �0.0000500 a $8 Beta BHC U 0.0000184 0.0000500 Delta BHC U 0.0000197 - 0.6000500 - 4 Gamma BHC U 0,0000176 0.0000500 Cn 4,4-DDD U 0.0000170 0.0000500 - 4,4-DDE U 0.0000164 0.0000500 6 _ _... ._ 4,4-DDT U � 0.0000177- _. ... 0.0000500 Dieldnn U 0.00000751 0,0000500 i Endosulfan I U 0.0000179 0.0000500 Endosulfan II U 0.0000176 0,0000500 Endosulfan sulfate U - 0.0000196 0.0000500 Endrin U 0.0000189 0.0000500 :Endrin aldehyde U 0.0000142 0.0000500 - .. 6 Endrin ketone U 0.0000170 0.0000500 A Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0,0000500 9 SC _... Hexachlorobenzene U 0.0000134 _ .. _. .. .._ 0.0000500 ... .. .. .. _ Methoxychlor U 0,0000193 0.0000500 Chlordane U 0.0000977 -0.000500 Toxaphene U 0.000168 0,000500 (S) Decachlorabiphenyb 43.1 10.0-144 - (S) Tetrochlam-m-xylene 89.5 100435 Laboratory Control Sample (LCS) (LCS) R3423788-1 06/23/19 11:19 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mgA % % Aldrin 0.00100 0.000961 96.1 42.0-140 Alpha BHC 0.00100 0.00115 115 37.0-140' Bela BHC 0.00100 0.00106 105 17.0-147 Delta BHC 0.00100 0.00113 113 IM-140 Gamma BHC 0.00100 0.00112 112 32.0-140 4,4-DDD 0,60100 0.00106 106 31.0-W 4,4-DDE 0,00100 0.000948 94.8 30.0-145 4,4-DDT 0.00100 0.000866 86.6 25.0-160 - Dieldrin 0.00100 0.00107 107 36.0-146 4ntlosulfaril. 0.00700 0.00103 103 45.0-753 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09:02 16 of 26 WG1299470 QUALITY CONTROL SUM 'IMARY ONE LAS, NATIONWIDE. ' Pesticides (GC) by. Method EPA 608.3 _ _ : L1110945-01,62 -_ - Laboratory Control Sample (LCS) Cp (LCS) R3423788-1 06/23/191119 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Ouarfer 7 Analyte mg/I mg/I % % TC Endosulfan 11 OD0100 0.00100 100 1.00-202 Endosulfan sulfate 0.00100 0.00110 110 26.0-144 a SS Endrin 0.00100 0.00108 108 30.0-147 Endrin aldehyde 0,00100 0.00102 107 5UT28 n Endrin ketone 0.00100 0,00109 109 54.0-142 Cn Heptachlor 0.00100 0.00100 100 34.0-140 Heptachlor epoxide 0.00100 0.00106 106 37.0-142 _ s Hexachlorobenzene 0.00100 0:600964 96.4 35.0-120 - Methoxychlor 0.00102 102 44.0-160 _--0.00100 (S)Decochlorobiphenyl 45.8 10.0-144 (5) Tetrachlons-m-xylene 94.3 10.0435 TGI eAl 9Sc ACCOUNT: PROJECT: SOG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09:02 17 of 26 WG1299470 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Polychlorinated Blphenyls (GC) by Method-EPA-608.3 L1110945-01,02 . Method Blank (MB) (MB) R3423901-1 06/23/191530 Cp MB Result Analyte mg4 MB Qualifier M8 MDL mg/I MB RDL mg/I TC PCB 1260 U 0.000120 0.000500 PCB 1016 U 0.000100- 0.000500 aS5 PCB 1221 U 0.0000730 0.000500 PCB 1232 - U PCB 1242 U 0.0000420. 0,0000470 0.000500' 0.000500 4 Cn PCB 1248 U 0.0606860 - 0.000500 PCB 1254 U 0.0000470 0.000500 s _. __.. ... (S) Decachlorobiphenyl 56.1 __. 10.0-144 (S) Tetrachloro-m-xylene 710 10.0-135 Laboratory Control Sample (LCS) (LCS) R3423901-2 06/23/1915:45 Spike Amount LCS Result LCS Rec. Rec. Limits LCS OualiFler Analyte mg/I mg/I % % PCB 1260 0.00250 0.00192 76.8 8.00-140 PCB 1016 0.00250 0.00219 87.6 50.0-140 (S) Decachlorobiphenyl 44.9 10.0-144 . (S) Tetrachloro-m-xylene .. 94.9 __. 10.0-135 L1110533-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1110533-02 06/24/19 08:10 • (MS) R3423999-1 06/24/19 08:24 • (MSD) R3423999-2 06/24/19 08:38 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Ouallfer MSD Qualifier RPD RPD Limits Analyte mg/I mg4 mg/I mg/I % % % % % PCB 1260 0,00250 NO 0.00137 0.00133 54.8 53.2 1 8.00-140 2A6 38 PCB 1016 6,00250 NO 0.00197 0.00189 78.8 75.6 1 50.0-140 4.15 36 (S)Decochlorobiphenyl 374 354 10.0-144 (S)Telrochloro-m-xylene 62.4 60.3 70.0-135 ' ACCOUNT: PROJECT: SDG: - DATE7TIME: PAGE: Eaton Corporation 28091-R L1110945 07/02/19 09:02 18 of 26 WG1300466 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. .k '. Semi Volatile: Organic Compounds (GC/MS) by Method 625.1 'L1110945-0T,02 _. Method Blank (MB) Cp (MB) R3424171-2 06124/1913:52 MB Result MB Qualifier MB MOIL MB RDL z Analyte mg/I mg/I mg/I - TC Acenaphthene U 0.000316 0.00100 Acenaphthylene - U '0.606309 0.00160 aSS Anthracene U 0.000291 0.00100 Azobenzene U 0.000318 0,0100 4 Benzidine U 0.00432 0,0100 _ _ _ - -.- _ _ - _,- - Cn Benzo(a)anthracene U 0.0000975 0,00100 _ _ _. _ Benzo(b)fluoranthene U 0.0000896 0.00100 s ;Benzo(k)fluoranthene U 0.000355 0.00100: Benzo(g,h,gperylene U 0.000161 0.00100 Benzo(a)pyrene U 0.000340 6.00700 - Bis(2-chlorethoxy)methane U Bis)2-chloroethygether U 0.000329 0.00162 0.0100 0.0100 7GI Bis(2-chloroisopropyl)ether U 0.000445 0.0100 4-Bromophenyl-phenylether U 0.006335 ao100. - BA 2-Chloronaphthalene U 0.000330 0.00100 4-Chlorophenyl-phenylether U 0.000303 0.0100 Chrysene U 0.000332 0.00100 z Dibenz(a,nanthracene ,U 0.000279 0.00100 3,3-Dichlorobenzidine U 0.00202 0.0100 2,4-Dinitrotoluene U 0.00165 0.0100 2,6-Dinitrotoluene U 0.000279 0.0100 Fluoranthene U 0.00610 6.00160 - - Fluorene U 0.000323 0.00100 _ Hexachlorobenzene U 0.000341 0.00100 Hexachloro-1,3-butadiene U 0,000329 a0loo Hexachlorocyclopentadiene U 0.00233 0,0100 Hexachloroethane U 0.000365 0.0100 Indeno(1,2,3-cd)pyrene U 0,000279 0.00100 Isophorone U 0.000272 0.0100 , Naphthalene U 0.000372 o.001o0 . Nitrobenzene U 0.00D367 0.0100 n-Nitrosodimethylamine U 0.00126 0.0100 n-Nitrosodiphenylamine U 0,00119 0.0100 . n-Nltrosodi-n-propylamine U 0.000403 0.0100. Phenanthrene U 0.000366 0.00100 _ Benzylbutyl phthalate U 0.006275 0.00300 Bis(2-ethylhexy1)phthalate U 0.000709 0.00300 Di-n-butyl phthalate U 0.000266 0.00300 Diethyl phthalate U 0,000282 0.00300 Dimethyl phthalate U a000283 0.00300 ACCOUNT: 'PROJECT: SDG: DATE/TIME: PAGE: Eaton. Corporation 28091-R 1_7110945 07/02/1909:02 19 of 26 WG1.300466 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1110945-01,02 „- Method Blank (MB) (MB)R3424171-2 06/24/191352 Cp MB Result Analyte Trill MB Qualifier MB MDL mg/I MB moll TC Di-n-ocryl phthalate U 0.000278 0.00300 - - Pyrene. U� 0.000330 0.00700 - 3 t2 4-Trichlorobenzene U 0,000355 0.0100 $9 4 Chloro-3-methylphenol U 0.000263 0.0100 4 2-Chlorophenol U 0.000283 00100 Cn 2,4-Dichlorophenol U 0.000264 0.0100 ' 2,4-Dimethylphenol U 0.000624 _ 0.0100 U 0.00262 0.0100 Fri 2,4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol U 0.00201 0,0100 Pentachlorophenol U 0.000313 0.0100 - 7G1 Phenol U 0,0100 2,4,6-Trlchlorophenol. U (S)Nitrobenzene-d5 49.7 .0.000334 0.000297 0.0100 15.0-314 AI -(S)2-Fluorobiphenyl 640 22.0-727- (Ap-Terphenyl-dN 83.6 29.0-141 9SC (S) Phenol-d5 16.5 8.00-424 (S) 2-Fluorophenol 277 10.0-120 (5) 2,4,6-Tribromophenol 74.5 10.0153 - Laboratory Control Sample (LCS) (LCS) R3424171-1 06/24/19 13:32 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I % % Acenaphthene 0.0500 0.0350 70.0 47.0-145 Acenaphthylene 0.0500 0.0367 73A 330-145 Anthracene 0.0500 0.0379 75.8 27.0-133 Azobenzene 0.0500 o.0395 79.0 37.0-125 Benzibine 0.100 0,0190 19.0 100-120 Benzo(a)anthracene .. 0.0500 0.0417 83.4 33.0-143 Benzo(b)fluoranthene 0.0500 0.0422 84.4 24.0-159 Benzo(k)fluoranthene 0.0500 - 0,0467 81.4 11.0-162 - Benzo(g,h,iJperylene 0.0500 0.0410 82.0 1.00-219 Benzo)a)pyrene 0.0500 0.0417 83.4 17.0-163 Bis(2-chlorethoxy)methane 0.0500 0.0294 58.8 1.00-219 Bis(2-chloroethyl)ether 0.0500 0.0673 135 33.0-185 Bis(2-chloroisopropyl)ether 0,0500 0.0305 61.0 36.0-166 ACCOUNT: PROJECT: Eaton Corporation 28091-R SDG: L1110945 DATMIME:. PAGE: 07/02/19 09:02 20 of 26 WG1300466 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Seml,Valatlle Organic Compounds (GC/MS) by Method 625.1 L1110945-01.02 Laboratory Control Sample (LCS) Cp (LCS) R3424171-1 06/24/191332 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier FTC Analyte mg/I mgA % % 4-Bromophenyl-phenylether 0.0500 0.0369 73.8 53.0-127 2-Chloronaphihalene 0.0500 0.0299 59.8 60.0-120 34 a .4-Chlorophenyl-phenylether 0.0500 0.0359 71.8 25.0-156 Chrysene 0.0500 0.0381 76.2 - - 17.0-168 -1.00-227 - - - - - 4 -0 benzla,hlanthracene 0.0500 0.0397 79.4 ,.. _ _- . Cf1 3,3-Dichlorobenzidine 0.100 0.0895 89.5 1.00-262 -2,4-Dinitrotoluene 0,0506 6.0414 82.8 39.0-139 2,6-Dinitrotoluene 0,0500 HESS 79.0 50.0-158 Fluoranthene 0,0500 0.0409 81.8 26.0137. - Fluorene 0.0500 0.0373 74.6 59.0-121 Hexachlorobenzene 0.0500 HERS 77.0 1.00-152 Hexachloro-1,3-butadiene 0.0500 0.0129 25.8 24.0-120 7G Hexachlorocyclopentadiene 0.0500 0.0131 26.2 _ 10.0-120 Hexachloroethane 0.0500 0.0143 28.6 40.0-120 J4 BAl Indeno(1,2,3-cd)pyrene 0.0500 0.0414 82.8 1.00-171 Isophorone 0.0500 0.0306 61.2 21.0-196 Naphthalene 0.0500 6.0267 53.4 21.0-133 Nitrobenzene 0.0500 0.0292 58.4 35.0-180 n-Nitrosodimethylamine 0.0500 0.0213 42.6 10.0-120 n-Nitrosodiphenylamine 0.0500 0.0384 76.8 44.0-120 n-Nitrosodi-n-propylamine 0.0500 0,0314 62.8 1:00-230 Phenanthrene 0.0500 0.0375 75.0 54.0-120 Benzylbutyl phthalate 0.0500 0.0408 81.6 1.00-152 Bis(2-ethylhexyl)phthalate 0.0500 0.0398 79.6 8.00-158 Di-n-butyl phthalate 0.0500 0.0428 85.6 1.00-120 Diethyl phthalate 0.0500 0.0426 85.2 1.00-120 Dimethyl phthalate 0.0500 0.0407 81.4 1.00-120 Di-n-octyl phthalate 0.0500 0.0412 82.4 4.00-146 Pyrene 0.0500 0.0392 78.4 52.0-120 1,2,4-TrichIand benzene 0.0500 0.0200 40.0 44.0-142 J4 4-Chloro-3-methylphenol 0.0500 0.0359 71.8 22.0-147. 2-Chlorophenol 0.0500 0.0271 54.2 23.0-134 2,4-Dichlorophenol 0.0500 0,0314 62.8 39.0-135 2,4-Dimethylphenol 0.0500 0.0324 64.8 32.0-120 4,6-Dinitro-2-methylphenol a0500 0.0483 96.6 1.00-181 2,4-Dinitrophenol 0.0500 0.0552 110 1.00-191 2--Nitrophenol 0.0500 0.0350 70.0 29.0-182 4-Nitrophenol 0.0500 0.0195 39.0 1.00-132 Pentachlorophenol 0.0500 6.6446 89.2 14.0-176 Phenol 0.0500 0.0115 23.0 5.00-120 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R 'L1110945 07/02/19 09:02 21 of 26 WG1300466 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Semi Volatile Organic. Compounds (GC/MS).by Method 625.1 L1110945-01:02' _ Laboratory Control Sample (LCS) (LCS) R3424171-1 06/24/191332 Spike Amount LCS Result Analyte mg/I mg/I 2,4,6-Trichlorophenol 0.0500. 0.0395 /5J Nitrobenzene-d5 /5/ 2-Fluoroblphenyl (S)p-Terphenyl-d14 (S) Phenol-d5 (S) 2-Fluorophenol (S)2,4,6-Tr1bromopheno1 - LCS Rec. Rec. Limits LCS Qualifier 79.0 37.0-144 52.2 15.0-314 68.9 22.0-127 ' 78.8 29.0-141 23.4 8.004241:. 33.9 100-120 935 100-153 - L1111094-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1111094-01 06/24/19 17:16 • (MS) R3424171-3 06/24/19 17:37 • (MSD) R3424171-4 06/24/1917:57 Spike Amount Original Result MS Result MSD Result MS Rec. Analyte mgA mg/I mgA mgA % MSD Rec. % Dilution Rec. Limits % MS Qualifier MSD Qualifier RPD % RPD Limits % Acenaphthene 0.0500 U 0.0359 0.0329 71.8 65.8 1 4Z0-145 8.72 48 Acenaphthylene 0.0500 U 0.0372 0.0342 74.4 68.4 1 33.0-145 8.40 74 Anthracene 0.0500 U 0,0381 0.0369 76.2 73.8 1 27.0-133 3.20 66 Benzo(a)anthracene 0.0500 U 0.0414 0.0407- - 82.8 814 1. 733.0-143 1.71 6 Benzo(b)fluoranthene 0,0500 U 0.0440 0.0433 88.0 86.6 1 24.0-159 1,60 71 1,2-Diphenylhytlratine 0.0500 U 0.0404. 0.0375 80.8 75.0 T '.78:0-156 7.45 34 Benzo(k)fluoranthene 0.0500 U 0.0426 0.0412 85.2 82A 1 110-162 3,34 63 8enzo(g,h;i)perylene 0.0500 U 0.0409 0.0390 81.8 78.0 T 1,00:219 4,76 97 Senzo(a)pyrene 0,0500 U 0.0430 0.0420 86.0 84D 1 17D-163 2.35 72 8is(2-chlorethoxy)methane 0.0500 U 0.0289 DOM 57.8 54.6 1 33.0-184 5,69 54 Bis(2-chloroethyl)ether 0.0500 U 0.0444 0.0587 88.8 117 1 12.0-158 277 108 Benzidine 0.100 U 0.0323 0.0473 32.3 47.3 1 1.00-120 377 40 Bis(2-chloroisopropyl)ether 0.0500 U 0.0309 0.0301 61.8 60.2 1 36.0-166 2.62 76 4-Bromophenyl-phenylether 0.0500 U 0.0390 0.0372 78.0 74.4 1 53.0-127 4.72 43 2-Chloronaphthalene 0.0500 U 0.0308 0.0280 6i.6 56.0 1 60.0-120 J6 9.52 24 4-Chlorophenyl-phenylether 0.0500 U 0.0386 0.0357 77.2 714 1 25.0-158 7.81 61 Chrysene 0.0500 U 0.0386 0.0378 77.2 75.6 1 17.0-168 2,09 87 Dibenz(a,h)anthracene 0,0500 U 0.0396 0.6386 79.2 .772. 1 1.00-227 _256 126 33-DichlorobenzIdine 0.100 U 0.0817 0.0858 81.7 85.8 1 1.00-262 4.90 108 -2,4-0initrotoluene 0.0500 U 0.0415 0.0389 83.0 77.8 1 39.0-139 6,47 42 2,6-Dinitrotoluene 0.0500 U 0.0410 0.0384 82.0 76.8 1 50.0-158 6,55 48 Fluoranthene 0.0500 U 0.0413 0.6397 82.6 79.4 1 26.0-137 355 66 Fluorene 0.0500 U 0.0388 0.0358 77.6 71.6 1 59.0-121 8.04 38 Hexachlorobenzene 0.0500 U 0.0418 0.0400 83.6 80.0 1 1..00-152 4.40 55 Hexachloro-1,3-butadiene 0,0500 U 0.0151 0.0112 30.2 22.4 1 24.0-120 J6 29.7 62 Hexachlorocyciopentadiene 0.0500 - U 0.0195 0.0150 39.0 30.0 1 10.0-146 261 34 - Cp TC aSs 4Cn SSr 7GI BAI 95C ACCOUNT: PROJECT: SDG: DATE/TIME PAGE: Eaton Corporation 28091-R L111094507/02/19 09D2 22 of 26 WG1300466 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 't1110945-01,02 L1111O94-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) C p (OS) L1111094-01 06/24/19 17:16 • (MS) R3424171-3 06/24/1917:37 • (MSD) R3424171-4 06/24/19 17:57 Spike Amount Original Result MS Result MSD Result MS Rec. M51) Rec Dilution Rec. Limits MS Qualifier MSD Oualifier RPD RPD Limits z Analyte mg/I mgh mg/I mg/I % % % % % TC Hexachloroethane L. - _.__.. ___..�...- ndeno(12,3-cdlpyrene 0.0500 ._ _ . 6.0500 U U . 0,0160 __ _ M389 0.0128 0.0377 320 778 25.6 74.4 1 1 40.0-120 J6 .--.._ _.__ _. .. 1.00-17T J6 22.2 --_ _._ .-_�_.- 4.47 52 -. .. _. _ _...__-.___ 99 3 55 Isophorone 0.0500 U 0.0305 0.0287 610 57.4 1 21.0-196 6.08 93 Naphthalene 0,0500 U 0.0261 0.0248 52.2 49.6. 1 21.0-133 - 5.11 65 < Nitrobenzene 0.0500 U 0.0292 0.0275 58.4 55.0 1 35.0-180 6.00 62 Cn n-Nitrosod imethyla mine 0.0500 U 0.0208 0.0197 41.6 39.4 1 10.0-120 5.43 40 s$f n-Nitrosodiphenylamine 0.0500 U 0.0405 0.0388 81.0 776 1 16.0-160 429 28 - _ ._ n-Nitmsodi-n-propylamine 0.0500 U 0.0311, 0.0297 62.2 59A 1 1.00-230 4.61 87 Phenanthrene 0,0500 U 0.0381 0.0366 76.2 73.2 1 54.0-120 4.02 39 Benzylbutyl phthalate 0.0500 U 0.0429 00419 85.8 -83.8 - 1 1.00-152 2.36 60 31s(2-ethylhexyI)phthalate 0.0500 U 0.0414 0.0411 82.8 82.2 1 8.00-158 0.727 82 Di-n-butyl phthalate 6.0500 0.0434 0.0431 86.8 86.2 1 .1.00-120 0.694. 47 G Diethyl phthalate 0.0500 U 0.0425 0.0410 85.0 82.0 1 1.00-120 - 3.59 100 Dime[hyl phthalate 0.0500 U 0.0411 0.0387 822 774 1 1.00-120 6.07 183 IF e Di-n-octyl phthalate 0.0500 U 0.0424 0.0412 84.8 82A 1 4.00-146 2,87 69 . __ Pyrene 0.0500 U 0.0403 .0397 80.6 79.4 �� 1 52.0-120 150 49 1,2,4-Trichlorobenzene 0.0500 U 0.0209 0.0181 41.8 36.2 1 44.0-142 J6 J6 14A 50 s Sc 4-Chloro-3.methylphenol 0,0500 U 0.0350 0.0321 70.6 64.2 1 22.0-147 8.64 73 2-Chlorophenol 0,0500 U 0.0298 0.0273 59.6 54.6 1 23.0-134 _ 8.76 61 2,4-Dichlorophenol 0.0500 U 0.0314 0.0303 62.8 60.6 4 39.0-135 - 3.0 50 2,4-Dimethylphenol 0.0500 U 0.0322 0.0304 64.4 60.8 1 32.0-120 5.75 58 4,6-Dinitro2-methyl phenol 0.0500 U- 0.6443 0.0465 88.6 93.0 1 1.00-181 - 4.85 203 24-Dinitrophenol 0.0500 U 0.0517 0.0523 103 105 1 1.00-191 1,15 132 - 2-Nilrophenol 0.0500 U 0.0345 0.0333 69.6 66.6 1 290-182 4.41 55 4-Nitrophenol 0.0500 U 0.0158 OD169 31.6 33.8 1 1,00-132 6.73 131 Pentachlorophenof 0.0500 U 0.0429 0.0428 85.8 85.6 1 14.0-176 0A3 86 Phenol 0.0500 U 0.0115 0.0111 23.0 22.2 1 5.00-120 3.54 64 2,4,6-Trichlorophenol 0.0500 U 0.0393 0.0377 78.6 75A - 1 37.0444 .4.16 58 (S) Nitrobenzene-d5 53.5 50.6 15.0-314 (S)2-Fluorobiphenyl 72.3 66.2 22.0427 (S)p-Terphenyl-d14 SOS 80.2 29.0-141 (S)Phenol-d5 24A- 22.1 8.60-424 (S)2-Fluoraphenal 38.0 34.7 10.0-120 (S)2.4,6-Trlbromophenol 95.0 870 100-153 - ACCOUNT: PROJECT: SOG: DATUTIME: PAGE: Eaton Corporation 28091-R L1110945 07/02n9 09:02 23 of 26 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. 0 Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit, ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. - - RPD Relative Percent Difference. SDG - Sample Delivery Group., Surrogate (Surrogate Standard) - Analyzes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analyzes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution - standard, or if concentrations of analyzes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample maybe diluted for analysis. If a value different than I is used in this fela, the result reported has already been corrected for this factor. These are the target %recovery ranges or %difference value that the laboratory has historically determined as normal Limits for the method and analyze being reported. Successful QC Sample analysis will target all analyzes recovered or duplicated within these ranges. Original. Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RED) from a quality control sample. The Original Sample may not be included within the. reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative If applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyze, the result in this column may state -ND" (Not Detected) or -BDL- Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection. Limit) that defines the lowest value that the laboratory could detect or report for this analyze. Uncertainty ma. Confidence level of 2 sigma. g A brief discussion about the included sample results, Including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receiptby the laboratory fromThe field or during the analytical process. f.present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (So) chainof custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/oranalysis. - Qualifier Description J The identification of the analyze is acceptable; the reported value is an estimate. J2 Surrogate recovery limits have been exceeded; values are outside lower control limits. J4 The associated batch OC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination: spike value is low. PI RPD value not applicable for sample concentrations less than 5 times the reporting limit. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R 1-1110945 07/0219 09.02 24 of 26 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National Is the only environmental laboratory accreditedlcertifed to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories In our Industry. The most significant benefit to our one location design Is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported In the attached report. ' Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. State Accreditations Alabama 40660 Alaska -__ --__ 17_026 Arizona A70612 Arkansas 88-0469_-__-_-___.-__„__ _ California -__- _ 2932 oolarado -------PH-0197 TN00003 ---_-----_— Connecticut Florida _. E87487 Georgia NELAP Georgia' _ 923 Idaho TN00003 Illlnnis 200008 Iowa 364 Kansas E-10277 Kentucky i° _ 90010 Kentucky ° 16 Louisiana A130792 Louisiana LA180010 Maine TN0002 Maryland 324 Massachusetts M-TNO03 Minnesota 047-999-395 Mlssisslppl TN00003 CERT0086 Third Party Federal Accreditations Nebraska NE-OS-15 05 Nevada _ IN 03.2002-34 _ New Hampshire 2975 New Jersey-NELAP TNO02 _ _ New Mexico' me New York 11742 North Carolina Env375 North Carolina' DW21704 North Carolina ° 41 Ohlo-VAP CL0069 Oklahoma 9915 Oregon TN200002 Pennsylvania 6802979 Rhode Island LA000356 South Carolina 84004 South Dakota Na Tennessee " 2006 Texas T10470424518 15 Texas° LA90152 Vermont W2006 Virginia 460132 Washington C847 West Virginia 233 Wisconsin 9980939910 A2LA-ISO 17025 1461.01 AIHA LAP,LLC EMLAP 100789 A2LA-ISO 17025' 1461.02 DOD 146101 Canada 1461.01 USDA P330-15-00234 EPA-Crypto TN00003 'Drinking Water ° Underground Storage Tanks 3Aquatic Toxiciry'ChemicallMicroblological "Mold °Wastewater Na Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. ACCOUNT: - PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091 R L1110945 07/02/19 09,02 25 of 26 - Billing Information: Analysis/Contai ner/Preserv Eaton Corporation NA Financial Services Center - 1009 Pres PO Box 816024 ChkAnatyticA2564 �al Durham Road Cleveland, OH 44181.8024 s)aa.nxm -Anar Roxboro, NC27573 � - ) - 11WS1 baron NO O%FEE Report to: Email To: dustiniaclair@eaton.com Dustin La CIa Ir - r' "A lull-7 PJ : go, 8.8858 1 Pbe go, In. Project City/Stale Description: Eaton Corp Semi -Annual Stormwater Collected: r GIs 7sases9 - , m - Phone: :.. 2' Client Project A. Lab Project A Ln Fax: 28091-R EATONRNC-28091SW o z a v , z Collected Facility ID # -- Site/Rush? 1FKKC,,. ROXBORO, NC 148703 R Q Acnnum EATONRNC``'1 (�) ) Collected by(si nature; (Lab MUST Be Notill Quoteq - u� Q ,. _ b: ' 4E. E t Semplate:T99967 ... -' . ,Q Same Day _Five Day 1' E: ��' �' W:. E (/�;: �" Prelogin P686424 •' .- _ �_ -� _ Nert Day _ 5 Day Only) Date Results Needed 0 w `J Wa .- TSR 873 �_ eathe 1 Wain ImmcdiatelY X. -- Two Day--^--1D DaY tRad ONy) No. _..._-.. _ .., .___ E C' C N O _ Q /f Packed on Ice N _ Y _ Three DaY .. S_ f , o Do Q.._ -� - -� O= _ H �' PB D 0 - Sample In Comp/Grab Matrix ' Depth Date Tin e �nvs Shipped ':Fed XGroun&, Re us) samolea pabaoNl ,V ,. i- r > 1., l— Q - - - Do 1 Grad WW ��l a .�X - X `X • X X X r'�1� • pmo �019 06-/8'-cos - -WW Ig�I Y50'n 9 xz -X X. X X X Ko 31.7 6 A. k y - • Matrix: 55-Soil Remarks: <a•+dt a c + b r_.ack1.52 .' AIR - Air F-Filter - PH Temp oC Sea "Pzesout/Into c: RP � y' GW-Groundwater B-Bloassay W +•, Cr GCI� Q.S COC Sx9 ed/Beta za e _NI ea eWater ` rnPV' flow Other -- t DW-Drinking Water .. OT - Other -Other Sam les returned na: - - t1P5 ✓Fedu f Trackingp � ( loaner T- ' J> _p- x� �fl7U•_ -��� a. _, I -, -_ .._ 2esoryoeadsoace le cable v vox -.- P se va :cn o cc%CAecced: 2Y _N Relinquished by: (Signature) Date: Time: Received by: (Signature) � Trip Blank Received: - No '-- - p\ [' IJ __ I /MedH- Y"k T iBR Relinquished by: (Signature) - Date: Time: Received by: (Signature) - Temp: C . Battles Received: _ If preservation required by Login: Date/Time Relinquished by (Signature) Date: Time: Received for lab by (Signature) Date: Time; - Condill - )) ,y _Hold NCF ative Chain of Custody Page_ol � Fm,T*N July 16, 2019 Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attn: DWQ Central Files Dustin A. LaClair Environmental, Health & Safety Manager RE: June 2019 Monthly Tier III Discharge Monitoring Report (336) 503-6538 (office) (336) 503-6562 (fax) d usti n I acla ir(a)eaton. com RECFIVED JUL 18 Z019 CDRAIL FILES SECTION Attached are the analytical results and associated chain of custody for the June 18, 2019 monthly Tier III stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility. Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North Carolina Division of Water Quality (NCDWQ). I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with the system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or other persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Sinc X232 Dustin A. LaClair EHS Manager Attachments