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HomeMy WebLinkAboutWQ0009477_Residual Annual Report 2019_20200225CW cascades Date: Feb 18 ,2020 Cascades Tissue Group — North Carolina A Division of Cascades Holding US Inc. 805 Midway Road, P.O. Box 578, Rockingham, NC 28380 USA Phone: (910) 895-4033 Fax: (910) 895-9887 www.cascades.com * Info@cascades.com To: State of North Carolina Department of Environment and Division of Water Quality Aquifer Protection Section Land Application Unit 512 N Salisbury St. Raleigh, North Carolina 27604 1-919-807-6300 Natural Resources From: Karen Bellamy-ORC and Preparer of 2019 Annual Report Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. 805 Midway Road Rockingham, NC 28379 1-910-895-4033 EXT 74280 1-910-895-1877 Fax Karen Bel lamy(o),Cascades.com Permit # WQ0009477 Subject: Land Application Annual Report Cover Letter Forms Included: Cover Letter and Compliance inspection Letter from DEQ �QoO� �1�C���Go ti0 g e F� O�SGraV��� Qe Annual Land Application Certification Form DENR Form ACF Letter from E. D. Black on Application and email concerning issues with Jan lab results. Excel Spreadsheets on Farmers, Field #, Address, Rain Data, Crops, If K Soil, % Solids, Acres, Wet Tons, Dry Tons, Dry tons per Acre, Long and Latitudes DENR Form DMSDF and Additional Supplemental DENR Form RSSF DENR Form RSSF-B Lab Results TCLP, Ignitability, Reactivity, & Corrosivity DENR Form PVRF 503 Letter on Vector Reduction Page 1 of 2 Subject: Land Application Annual Report Cover Letter. Cascades has 1 ORC and 2 Backup ORC. Karen Bellamy ORC and (David Sheppard and Corey Wyand as Backup). Field Inspections where conducted, equipment calibration, PM work on equipment and ORC and backup ORC performed required inspections for the year. Corey Wyand, David Sheppard and Karen Bellamy attended Rural Water Association Training in 2019 for our Continuing Education Contact Hours. Dr. Elwood Black continues to work closely with our land application Program. Advanced Residuals had No incidents in 2019. 2019- Challenging year(2018 with Hurricane Florence and all the additional rain. We were able to stay in compliance of the 60 day spread time for 2018, but had to ask for an extension in Jan 2019. Worst weather and field conditions , since I started in 1994. We stayed in touch with Tony Honeycutt and we were able to complete fields in the 60 day extension time line. Advanced Residuais has worked hard to have a good program. Cascades and Advanced Residuals has vorked hard to make sure we have a good program that is Environmentally Friendly and also benefits the armers. We have gotten a lot of positive feedback from farmers. Duke Goodwin is the Project Manager for Advanced Residuals project at Cascades. Mr. Goodwin has been a farmer for several years and also has worked at the City of Rockingham WWTP, so he is very familiar with regulations. Duke Goodwin also received his certification for Land Application in 2016 . Mr. Goodwin also received his continuing Ed hours for 2019. Pathogen and Vector Reduction aren't required on by our Permit. Several of the heavy metals have also been removed from our permit, since levels have been extremely low for over 10 years. During our inspection from Tony Honeycutt in 2019. We discussed issues with our testing lab for So of our Jan test results. We also have testing performed by Department of Agronomics so the farms can have access to information. So we know these results aren't valid. New lab rep and also test changed from one lab to another. Elwood Black commented on Jan 2019 test results with email. ********Cascades intends to renew our Land Application Permit in ,tOY COOPER Gmernor MICHAEL S. REGAN Secretary LINDA CULPEPPER Director NORTH CAROLINA Environmental Quality October 01, 2019 Karen V. Bellamy Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc PO Box 578 Rockingham, NC 28380-0578 SUBJECT: Compliance Inspection Report Rockingham FiberClay Distribution Program Non -discharge Permit No. WQ0009477 Richmond County Dear Permittee: The North Carolina Division of Water Resources conducted an inspection of the Rockingham FiberClay Distribution Program on 9/24/2019. This inspection was conducted to verify that the facility is operating in compliance with the conditions and limitations specified in Non -discharge Permit No. WQ0009477. The findings and comments noted during this inspection are provided in the enclosed copy of the inspection report entitled "Compliance Inspection Report". If you should have any questions, please do not hesitate to contact Tony Honeycutt with the Water Quality Regional Operations Section in the Fayetteville Regional Office at 910-433-3300 or via email at tony.honeycutt@ncdenr.gov. Sincerely, DocuSigned Cby: ��°." 5189C2D3DD5C42B. J. Trent Allen, Regional Supervisor Water Quality Regional Operations Section Fayetteville Regional Office Division of Water Resources, NCDEQ Cc: Karen Bellamy - ORC WQS Fayetteville Regional Office — (TH) Central Files D_Eq2, NortnCar� naDepart mentof-tn.vicArnente'Qua"Y I DvsonOfWit erResrurcas Farettev a Reg ona, Off ce 1225 G:een Street. Su to 714 1 Fa ettev !e, N:rth Caro na 28301 Compliance Inspection Report Permit: W00009477 Effective: 01/01/16 Expiration: 12/31/20 Owner: Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc SOC: Effective: Expiration: Facility: Rockingham FiberClay Distribution Program County: Richmond 805 Midway Rd Region: Fayetteville Rockingham NC 283794101 Contact Person: Mickey Lee Title: Phone: 910-895-4033 Directions to Facility: Travel US Hwy. 74 to US Hwy. 1 intersection. Follow US Hwy. 1 interchange. Turn west onto Midway Road. The plant is approximately two miles from this turn System Classifications: LA, Primary ORC: Karen V Bellamy Certification: 19197 Phone: 910-895-4033 Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 09/24/2019 e}uTi AW Iby10::OOA��M��} Primary Inspector: Tony W Honeycutt �" �kt'9*,..-d_--„ Secondary Inspector(s): WE697DUCF4cz.. Exit Time: 12:OOPM Reason for Inspection: Routine Inspection Type Permit Inspection Type: Distribution of Residual Solids (503 Exempt) Facility Status: Compliant Not Compliant Question Areas: Miscellaneous Questions Record Keeping (See attachment summary) Phone: 910-433-3339 Compliance Evaluation Page 1 of 3 Permit: WQ0009477 Owner - Facility: Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc Inspection Date: 09/24/2019 Inspection Type : Compliance Evaluation Reason for Visit: Routine Inspection Summary: Cascades produces a class "A" material. Facility records were up to date and available for review. Ms. Bellamy is doing a good job managing the facilities land application program. No additional problems noted. Page 2 of 3 Permit: WQ0009477 Owner - Facility: Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc Inspection Date: 09/24/2019 Inspection Type: Compliance Evaluation Reason for Visit: Routine Tvpe Yes No NA NE Distribution and Marketing ❑ Land Application Record Keeping Yes No NA NE Is GW monitoring being conducted, if required? ❑ ❑ N ❑ Are GW samples from all MWs sampled for all required parameters? ❑ ❑ 0 ❑ Are there any GW quality violations? ❑ ❑ N ❑ Is GW-59A certification form completed for facility? ❑ ❑ E ❑ Is a copy of current permit on -site? 0 ❑ ❑ ❑ Are current metals and nutrient analysis available? E ❑ ❑ ❑ Are nutrient and metal loading calculating most limiting parameters? 0 ❑ ❑ ❑ a. TCLP analysis? E ❑ ❑ ❑ b. SSFA (Standard Soil Fertility Analysis)? E ❑ ❑ ❑ Are PAN balances being maintained? 0 ❑ ❑ ❑ Are PAN balances within permit limits? 0 ❑ ❑ ❑ Has land application equipment been calibrated? ❑ ❑ ❑ Are there pH records for alkaline stabilization? ❑ ❑ 0 ❑ Are there pH records for the land application site? ❑ ❑ 0 ❑ Are nutrient/crop removal practices in place? 0 ❑ ❑ ❑ Do lab sheets support data reported on Residual Analysis Summary? 0 ❑ ❑ ❑ Are hauling records available? E ❑ ❑ ❑ Are hauling records maintained and up-to-date? E ❑ ❑ ❑ # Has permittee been free of public complaints in last 12 months? 0 ❑ ❑ ❑ Has application occurred during Seasonal Restriction window? ❑ ❑ 0 ❑ Comment Page 3 of 3 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0009477 County: Richmond Year: 2019 Facility Name (as shown on permit): Land Application Operator: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. Karen V. Bellamy Phone: 910-895-4033 Ext 74280 Lan application of residuals as allowed by the permit occurred during the past calendar year? Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the ermit: Total number of fields utilized for land application during the year: Total amount of dry tons applied during the year for all application sites: 23302.42205 Total number of acres utilizes for land application during the year: Part B - Annual Compiance Statement: Facility was compliant during calendar year 2019 with all conditions of the land applic tion permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. YYes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Karen V. Bellamy Environmental Manager Permittee Namy and Title (type or print) Signature Date Date Land Applier (if different from Permittee) (if different from Permittee and Preparer) * Prenarer is defined in 40 CTR Part S01.9 (r)and 15A NCAC.. 09T 1109 (96) nFNR FORM Ar..F 119/9(1m February 9, 2020 Cascades Tissue Group POB 578 Rockingham, NC 28380 Attention: Karen Bellamy - Technical Director Dear Ms Bellamy: From January 1, 2019 thru December 31, 2019, FiberClay was distributed only to agricultural land. No farm field received FiberClay in a continuous year-to-year application as defined by the North Carolina Department of Environmental Quality respective to permit WQ0009477. These statements are based on information reported by Advanced Residuals Management. Sincerely: Elwood Black, Ph.D. - Soils Karen Bellamy From: Eblack@nc.rr.com Sent: Wednesday, February 19, 20201:47 PM To: Karen Bellamy Subject: PAN calculation The Plant Available Nitrogen (PAN) calculation is widely used to estimate the N that will be available to a crop from the biosolids. The carbon to nitrogen ratio in biosolids is commonly less than 20:1 and net mineralization of N from the biosolids occurs. For materials with a C:N of less than 20:1 the PAN provides a good estimate of the N that may be available to the plant. However for materials like the Cascades soil additive, which have a C:N greater than 30:1, the PAN calculation is not appropriate. Instead of mineralization, N immobilization occurs. As a result farmers need to apply additional N to off set the N that will be immobilized as the soil microorganisms assimilate the fiber. The PAN should be 0. Elwood Black, Ph.D. - Soils Sent from my iPhone Cascades - ATTENTION: Ce courriel provient de 1'exterieur de ('organisation. Ne pas cliquey sur les liens et ne pas ouvrir les pieces jointes sauf si vous reconnaissez 1'expediteur et que vous etes sur que le contenu est Iegitime. Cascades - CAUTION: This email is from outside the organization. Do not click on links or open attachments unless you recognize the sender and you are sure the content is safe. 2019 i i I ITons Tons Month Field I P.I. Acres D Use An Good NK,NW,Y S, YD,NP, 7I31/2018 RC YF 42.50% 49 a 3139.532N 7914.196W 545 Burl.! h Rd Pembroke NC 28372 .. ,.:.:„. ,,. YK,NW,N P,Y0. 11/6/2017 - RC 3NSNF 42.50% 25 a 3518.159N 8012.539 W 36083 Western Rd. Alb emrade NC 28001 NKYW- r' 2,NF,NS, 1O/17/2017 ,. _ . _ RC NP YD 42.5016 i 1 a 34 /9.562N 79 5.622W 5274 Old Lo Rd. Shannon NC 28387 J NK YW,N .,,.... F,NS,NP, W T/2017 RC YD-2 42.50% 39 a 3f 50.034W787.264W 5274 Old Lc Rd. Shannon NC 28387 NK,YW- 2,NF,NS, 70/77/2017 RC NP YD-5 42.50% 46 a 34 49.682N 79 7.520 W 5274 Old Lo Rd. Shannon NC 28387 NK YW,Y F,NS,NP, 10/17/2017 5 RC YD 42.50% 35 a 34 49.488N 79 7.799 W 5274 OW LoweryRd. Shannon NC 28387 NK,NW,Y F,NS,NP, 8/29/2018 RC YD 42.50% 29 a 34 37.872N 7912.582 W 170 Elaroe Rd. Pembroke NC 28372 NKYW- 3,NP,YD- 8131/2018 _, Grass 4 NS NF 42.50% 19 a 34 35.667N 7914.235W 650 Bridges Rd. Rowland NC 28383 KYW- 2, YF, YS, YP-7,YD- 1/2/2018 07H7H9 RC 10 42.50% 400 a 351L191N 8015.818W 29710 Hollvbrook. DR. albermaNe NC 28001 Nk,YW- lia 3,NF,NS, 10H1/2018 Grass YP Y0.4 42.50% 134 a 34 26.747N 79 8A40W 1199 Mill Branch Rd. Faimwunt NC 28340 NKYW,N F,NS,NP, 10H8/2017 RC YD-242.50X 18 3132.026N 7911.970 W 1927 GereWs Rd. Rowland NC NKNW,N F,NS,NP, 10H8/2017 RC YD-2 42.50% 17 No 34 32.112N 7912.117W 1927 Geraids Rd. Rowland NC Nk,NF,N W, NS,NP,Y 10H8/2017 RC D-3 42.50% 59 a 34 33.111N 79 6.260W 1927 Gwaids Rd. Rowland NC _ Nk,YW,N F,NS,NP, 8/3/2018 RC YD 42.50'/. 1I 34 26.086N 79 .735W 2648 Marietta Marian NC 28362 NK, YW,N F,NS,YP, 10/18/2017 RC YD-3 42.50% 21 34 25.852N 79 7.898W ra 1927 Geralds Rd. Rowland NC NK YW,N P,Y0. 8/29Q018 RC 4 NS NF 42.50% 77 34 42.102N 79 13.561 W 170 Elarce Rd. Pembroke NC 28372 NK,nW,Y F,NS, MP, H/29/201H RC YD-2 42.50% 43 a 34 37.747N 7912.408W 170 Elarce Rd. Pombroke NC 28372 NK,YW. 4,NF,NS, H/29Q01H - RC NPYD-5 42.50% 28 all 34 39.723N 79 11.882 W 170 Elarce Rd. Pembroke NC 28372 NK,NW,N F,NS,NP, 812912078 Grass YD 42.50' i6 3/ 40.132N 79 8.878 W 170 Elarce Rd. Pembroke NC 28372 NK, YW- 2,YP- 2,NS,NF, f0/23/1018 RC YD-f0 42.50% 113 a 34 34.597N 79 81.155W 1384 School Rd Fairmont NC 28340 NK, YW,N P,YD- 1012312018 RC 4 NS NF 42.50% 102 a 34 35.363N 78 4.856 W 1384 School Rd Fal mont NC 28340 YK. YW,N P,YD- 1/2/2018 RC 3 NS NF 42.50% 65 3515.566N 80.21.870W 29716 Holh, Brook Dr. Albermarle NC 28001 NK,NW,N P,YD- 11/9/Z018 RC 3 NS NF 42.50% d6 a 3/ 45.531N 7917.785W 343 W.L Moore Maxton NC 28364 NK, YW. $NF,NS, Hl31/201H RC NPYD4 42.50% 57 a 34 42.418N 7914.024W 343 W.L. Moore Maxton NC 28364 .... NK,YW- 2.NF,NS, 52 a 34 39.544N 79 11.234 W 343 W.L Moore Maxton NC 28364 NK,NW,N S, YD,NP, 7/31/2018 Grass YF 42.50% 15 a 34 38.287N 7913.783W 545 Budei h Rd P mbroke NC 28372 NK, YW. ... 2,NP,YD. 9MO18 Grass 2 NS NF 42.W% 27 34 42.849N 79 6.788W 2811YndellMd. Lumberton NC 26360 Nk,NW,N F,NS,NP, " 10n8/Z017 RC YD-3 42.50% 32 5 34 28.482N 7914.742N 1927 Gera/ds Rd. Rowland. NC NK,YW,N F,NS,NP, ion8/2017 RC YD-3 42.50% 119 3/ 28.403N 7915d83W 1927 Geralds Rd. Rowland NC NK,YW,N 10/Z312078 RC PNS,NF 42.5051 21 34 35.952N 79 5.514 W 1384 School Rd Fairmont NC 28340 NK,NW,N lWzj 2018 RC P,NS,NF 42.50% 39 a 34 35.727N 79 4.772W 1384 School Rd Fairmont NC 28340 NK,NW,Y F,NS,Np, 10/23/201H RC YD4 42.50% 44 a 34 38.653N 79 7338W 1384 School Rd Fairmont. NC 28340 NK,YW,N _ P, Y- f0/23/2018 RC 4,NS NF 42.. 23 a 1384 School Rd Fairmont NC 28340 NKYW 2,NF,NS, 8/3012018 _ RC YP YD-4 42.50% 130 a 34 43.851N 7915.941W 2702 Preston Rd Marton NC 28364 NKNW,N F,NS,NP, 3/2/2016 RC M2 42.50% 113 a 3418.101 N 7918.770W 2702 Preston Rd Heston NC 28364 NK,NP,Y W,NF,NS, 3/7/2016 RC YD-3 42.50% 83 a 34 32.998N 7915.814W 2702 Preston Rd Heston NC 28364 NKNW,N F,NS,NP, 3121, B RC YD-3 42.5016 50 a 3445.076N 7917.481W 2702 Preston Rd Marton NC 28364 NKYW 2,YP,NF, 3R/2016 RC NS YDJ 42.50% 113 a 3415.129N 7817.155W _ 2702 Preston Rd Marton NC 28364 _ ... - ... NKYW,Y P,NS, Y& 31=018 ^° ' ° ^' w' ' RC 1 NF 42.50% 8H a 3! 45.412N 79 17.002W 2702 Preston Rd Melton NC 28364 NKNF.N W,NS,NP RC YD 42.50% 38 a 134 25.714N 79 7.191 W 26{8 Medana Madefb NC 28362 _ NK YW. 2,NP,YD- 1/7/2019 RC 2 NS NF 42.50% 43 a 34 46.0161179 5302 OM Red SwInas Rd. Macron NC 28364 M_ NKYW- 3,NP,YD 1/7/1019 RC 4 YS NF 42.50% 29 a 34 45.776N 7914.223W 5302 Old Red Springs Rd. Marton NC 28364 NK,YW- Y,YP,YD 1/7/T019 RC 2 NSNF 42.50% 23 a 34 45.296N 7914.269 W 5302 ON Red Swings Rd. Marton NC 28364 NK YW. 2,NP,YD- 1/7/2019 RC 5 YS NF 42.50% 18 34 45.492N 7913.986 W 5302 Old Ratl Springs Rd. Marton NC 283" _ NKYW- 6,NP,YD- i!7/2019 _ RC 8 YS NF 42.50% 79 a 34 4S157N 7913.595W 5302 OW Red Spring. Rd. Marton NC 28364 _ NK YW $NF,NS, 1/24l2019 Gress NP YD 42.50% 28 34 48.N7N 79 8.260W 3811 MeD CroaW Rd Lumberton NC 28360 NK, YW,N P,YD,NS, 1/21/2019 RC NF 42.50% 98 a 314B.361N 78 4.363 W 3811 McDuffv Crossing Rd Lumberton NC 28360 NKYW,N P, YD,NS, 1/1N2019 Grass NF 42.50% 12 a 34 45.300N 79 4.690W _ 3811 AkDuffy Crossing Rd Lumberton NC 28360 NK,YW,N P,YD- 1R4/2018 RC 1 NS NF 42.50% 12 a 34 45.372N 79 4.840 3811 McDuffy Crossing Rd Lumberton NC 28360 NK YW2, P, YD•2, 1/24/2019 -- RC NS NF 42.50% 20 a 3415.4/7N 791.459W 3811 McDuffv Crossina Rd Lumberton NC 28360 1/24/2019 34 45.086N 79 4.513W _ RC NKYW,Y- 2,NP,NS, NF 42.50% 18 a 3811 McDuffv Crossina Rd Lumberton NC 28360 1/2412019 34 44.305N 79 3.501W RC NKYW,Y P,YD- 2 NS YF 42.50% N a 1/24/2019 3611 AkDuMl CrOssina Rd Lumberton NC 28360 34 44.318N 79 2.787W RC NKYW,N P,YD- 2 NS YF 42.50% 31 1/24/2019 3811 AfcDuffv Crossina Rd Lumberton NC 28360 3/ H.38/N 78 2.815W �— RC NKYW 4,NP,YD- 5 NS YF 42.50.6 34 a 3811 A(cDuffv Crossina Rd Lumberton NC 28360 a Month 1 4752.82000 2019.9050 2019 Tons Tons MonthZJ Field Raln Acres D Usa Nk,YW,N F,YS,NP, 10/17/2017 RC YD-2 42.30% 48 a 34 49.215N 79 6.181W 5274 Old Lowe Rd. Shannon NC 28386 NK, YW,N F,NS,NP, 812912018 --- RC YD-3 42.30% 22 a 34 47.997N 79 8.027W 170 Elarce Rd Pembroke NC 28372 K,YW- 4 2, YF, YS, 1/2/2018 RC YPYD-10 42.30% 400 a 3517.191N 8015.818W 29716 Holl brook DR. albennade NC 28001 NK,YW 4,YP,D- 10/23/2018 RC 4 NS NF 42.30% 39 a 34 33.326N 79 8.708W 1384 School Rd Fahmont NC 28340 NK,NW,N F,NS,NP, 10/23/2018 _ RC YD-2 42.80% 15 a 34 33.237N 79 7.503 W 1384 School Rd Fahmon NC 28340 _ NK, YW- 2,YX 2,NS,NF, 10123/2018 RC YD•f0 42.30% 113 a _ 34 34.597N 79 81.155W 1384 School Rd Falmtont NC 28340 YK. YW,N P,YD- IIW018 RC 3 NS NF 42.30% 85 a 3515.566N 80.21.870W 29716 Hol Brook Dr. AlbemarleNC 28001 _ NK,NW,N 23415.531N F,NS,NP, 11r9/2018 RC YD-3 42.30% IB a 79 17.785 W 345 W.L. Moore Marron NC 28361 NK, Y W 2,NP,NF, 10/23/2018 RC NS YD-4 42.30% 35 a 34 32.895N 79 8.060 W 1384 School Rd Fahrnont NC 28340 NK,YW- 2,NF,NS, 3/2/2018 RC YP YD4 42.30% M a 34 43.302N 7918.770W 2702 Preston Rd Marron NC 28364 NK,YW,N F,NS,NP, 3/2/2016 RC YD4 42.30% 73 a 34 44.588N 7917.624W 2702 Preston Rd Marron NC 28364 NK,NW,Y F,NS,YP, 3/2/2016 RC YD 42.30-A 32 a 341I.588N 7917.624 W 2702 Preston Rd Marton NC 28364 NK,YW 2,NF,NS, 12/27/2018 RC NP 42.30% 42 a 31 49.072N 79 20.498W 179 Elmor Drive Marron NC 28364 NK,YW- 2, YF, NS,NP,Y 12/27/2018 RC D-5 42.30% SB a 34 49.072N 79 20.960 W 179 Elmor Drive Maxron NC 28364 NK, YW,N P,NS,NF, 1212712018 RC YD4 42.30% 24 a 34 47.447N 079 19.873W 854 b ant Circle Maxton NC 28364 NK,YW,N 1H8R019 RC S NP NF 42.30% 18 a 3133.328N 79 8.708W 37 Disne Dr. Maxton NC 28364 i024 W Nk,Y 2,NF,NS, 8R8/2018 RC NP YD-3 42.30% I7 a 38.957N 79 7.487W 170 Elarce Rd. Pembroke NC 28372 NK, YW,Y P, YD. 1/24/2019 RC 2 NS YF 42.30% W a 34 44.305N 79 3.50' 3811 AkDuffy Crossina Rd Lumberton NC 28360 NK,YW- 4,NP,YD- 1/21/2019 RC 5 NS YF 4230% 34 34 44.384N 79 2.915W 3811 McD Crossin Rd Lumberton NC 28360 Fa NK,YW- 2,YP,YD- 112412019 RC 2 NSNF 42.30% I2 3443.411N 794.191W 3811 kkD Crossln Rd Lumberton NC 28360 NK,YW,N P,YD- 1/24/T019 RC 3 NS NF 42.30% 26 a 34 43.039N 79 4.213W 3811 McD Cross) Rd Lumberton NC 28360 NK,YW,N P,YD- 1/21/2018 RC 3 NS NF 42.30% 20 a 34 43.124N 79 4.102W 2811 MeD Crossin Rd Lumberton NC 28360 NK,YW,Y F,YS,NP, 1/2I@019 RC YDd 42.30% 48 a 34 42.856N 79 2,984 W 3811 UcDuffy Crossina Rd Lumberton NC 28360 NK,NW,N F,NS,NP, 1/2//2019 RC YD-2 42.30% 35 a 3142.599N 793.007W 3811 McDuffv Crossina Rd Lumberton NC 28360 NK,YW,N F,NS,NP, 1/14/2019 RC YD-2 42.30% 31 a 34 42.71N 79 2.547W 3811 ?AcDuffv Crossing Rd Lumberton NC 28360 NK,YW- $NF,NS, 1/24/t019 RC YP YD-7 42.30% 89 34 38.876N 79 2.065W 3811 UcDuffv Crossim Rd Lumberton NC 28360 NK,YW,N F,NS,NP, 1/24/2019 RC YD 42.30% 49 a 34 38.235N 79 2.320W 3811 McDuf& Crossina Rd Lumberton NC 28360 NK,YW,N F,NS,NP, 1/2I/2018 RC YD-2 42.30% 18 34 29.949N 79 9.158 W 3811 kkDuffv Crossina Rd Lumberton NC 28360 NK,NW,N P, YD- 1/29/2018 RC 1 NS NF 42.30% 1 a 34 30.338N 79 8.453W 5338 H 130East Rowland NC 28383 NK,Y W- 2,NF,NS, 1/29/2018 RC NPYD-5 42,30% 105 a 34 19.949N 79 9.15BW 5338 H 130East Rowland NC 28383 NK,YW,N F,NS,NP, 1/29/2018 RC YD-2 42.30% 21 a 34 30.219N 79 8.950W 5338 H 130East Rowland NC 28383 Nk, YW,N P,YD- 1R9/1018 RC 3 NS NF 42.30% 55 a 134 30.382N 79 9.018 W 5338 Hwy 130East Rowland NC 28383 NK,YW,N F,NS,NP, 112941018 34 30.677N 79 9.046 W RC YD3 42.30% iH a 5338 HWV 130East Rowland NC 28383 NK,YW,N P,YD- 1/29/2018 3f 30.873N 79 8.808W RC 2 NS NF 42.30% 98 a 5338 Hwy 130East Rowland NC 28383 NK, YW,N F,YS,NP, 1/29R018 RC YD-6 42.30% 4H a 3/ 30.902N 79 10.101W Eaat Rowfand NC 28383 NK,YW,N F,NS,NP, 21WO19 10.684W 0349379.117W RC YD-2 42.30% 30 a Shop Rd. Moron NC 28384 NK,YW,N F,NS,NP, 216 20019 RC YD-4 42.30% 11 a 581 Cabinet Shop Rd. Maxron NC 28364 NK, YW,N F,NS,NP, 2H/2019 RC YD-2 42.30% 16 a 34 31.232N 7910.382W 581 Cabinet Shop Rd. Mahon NC 28364 _ NK,NW,N F,NS,NP, 2/I/2019 RC YD-2 42.30% 88 a 3147.017N 7917.490W 2139 Oak G— CMuch Rd. Lumberton NC 28360 a I-OFn—thI 3019.37000 1 1277.19351 2019 Tons I Tons Monts ' . " FIGN I Rain Acres D Use Mar Nk,NW,N F,NS,NP, 10/18/2017 RC YD-5 41.10% 47 a 34 36.286N 7914.933W 1927 Geralds Rd. Rowland NC 3 Nk,NW,N ` PI P,YD,NS 8/22/2018 ^°� RC NF 41.10% 46 a 34 45.820N 7915.769W 1312 J.L Rd Marton NC 28364 NK, YW,N P,YD- 8/L2018 RC 4NS NF 41.f0% 53 a 34 41.696N 7918.477W 1312 J.I. Rd Marton NC 28364 NK, YW,N F, NS,NP,Y f0lI7/2017 RC D-2 41.10% 39 a 34 50.034N 79 7.184W 5274 Old Lo Rd. Shannon NC 28386 NK,YW- 2,NF,NS, 10/17l2017 RC NP YD-3 N.fO% 46 a 3I {9.882N 797.SZOW 5274 Old Lowwy Rd. Shannon NC 28386 NK,YW,N F,NS,YP, 812912018 RC YD-3 41.10-A 27 a 34 47.214N 79 4.654 W 170 Elarce Rd. Pembroke NC 28372 YK,NW,N F, YS,NP, f0/2/2018 RC YD3 41.10% 12 a 35 2.471N 8013.409W 2317HwV218 Pesehland NC 28133 NK, YW,N P,YD- 8Q9/2018 RC INS NF 41.10% 77 a 3442A02N 7913.561W 170 Elam Rd. Pembroke NC 28372 YK,YW,N F,NS,NP, lar, RC YD3 41.1. 65 a 3515.566N 80 21.870 W 29716 Nol brook DR. alb -le NC 28001 NK,YW,N P,YD- 11/9/201B RC 2NSNF 41.10% 30 a 3445.523N 7918.201W 343 W.L. Moore Marton NC 283" NK,NW,N P, YD-2 11/9l2018 RC NS NF 41.10% 29 a 3412.463N 7915.125W 343 W.L. Moore Marton NC 28364 Nk,YW,N F,NS,YP, 813012018 RC YD-4 41.10% 130 a 3143.854N 7915.941W 2702 Preston Rd Marton NC 28384 NK,NW,N F,NS,NP, 3/2/201B RC YD-2 41.,. 113 a 34 46.101N 7916.770W 2702 Preston Rd Marron NC 28364 Nk,YW- 2,NF,NS, 3/2/2018 RC NP YD3 41.10% 33 a 34 43.479N 7915.373W 2702 Preston Rd Maxfon NC 28364 Nk,YW- 2,NF,NS, 3/S/2016 RC NP YD-2 41.10% 46 a 3413.311N 7915.051W 2702 Preston Rd Marton NC 28364 NK,YW- 2,NF,NS, 3/2/2016 RC NP YD 41.10% 42 a 34 43.203N 79 17.528W 2702 Preston Rd Marron NC 28364 NKYW,N P,NS,ND, 3lLT018 RC NF 41J0% 2B a 34I5.573N 7818.441W 2702 Preston Rd Marron NC 28364 NKYW- 2,YP,NF, 3/2/2016 RC NS YD4 41.f0% 113 a 34 45.129N 7917.155W 2702 Preston Rd Maxton NC 28364 NK YW,Y P,NS, Y0. 3/2/Z018 RC 2 NF H.f0% 88 a 34 45.412N 7917.002W 2702 Preston Rd Moron NC 28364 yD- 3,NKYW- 2,NF,NS, 1/2I/1019 RC YP 41.10% 131 34 W.910N 79 0.561W 3811 McD Crv, In Rd Lumberton NC 28300 YK YW,N F,NS,NP, 7712912077 RC YD-2 41.10% 22 a 35 2.142N 80.18.326W 2746 Dee Springs Church Rd. Peachland NC 28133 YKW Y,N F,YS,YP, 11/29/2017 RC YD-3 41.10% 29 35 2.403N 8016.283W 2748 Springs Church Rd. Peachland NC 28133 YKNW,N ga F,NS,NP 1112912017 RC YD 41.10% 8 35 2.81 SN 8016.314W 2746 Dee rin s Church Rd. Peachland NC 28133 YKW, YN F,NS,NP, 1112912017 RC YD-2 41.10% 12 35 3.OBSN 8016.477W 2746 Deep Springs Church Rd. Peachland NC 28133 NKYW- 2,NF,NS, 1/7/2019 RC NP YD-2 41.10% 43 a 3148.01BN 7914.457W 5302 Old Red Springs Rd. Maxton NC 28364 NK,YW- 3,NF,NS, 1/7/2018 RC NPYS4 41.10% 29 a 3445.776N 7914.223W 5302 Old Red Springs Rd. Maxton NC 28364 NKYW- 2,NF,NS, 1/7lM19 RC YP YO-2 41.10% T3 a 34 45.286N 7913.986W 5302 Old Red Springs Rd. Maxton NC 28364 NKYW- 2,NF,NS, 1/7/2019 RC NP YD-5 41.10% 26 a 34 45.492N 7913.986 W 5302 Old Red Springs Rd. Maxton NC 28364 NK,YW- 6,NF,NS, 1/7/7079 RC NP YD-8 41.10% 79 34 45.157N 7913.595W 5302 Old Red S rings Rd. Maxton NC 28364 NKNW,N F,NS,NP, 1/7/2019 RC YD-2 41.10% 25 a 34 44.846N 7912.263W 5302 Old Red Springs Rd. Maxton NC 28364 NKYW,N F, YS, YP, 1/7/2019 RC YD-2 41.10% 35 a 34 45.217N 7911.210W 5302 Old Red Springs Rd. Maxton NC 28364 K,YW- 2,NF,NS, YP-3, Y0. 1B/2019 RC 7 41.10% 110 a 35 2.979N 80 29.383W 117275 Merlin Rd Monroe NC 28110 K,YW- 3,NF,NS, 1Bl1019 RC P Y0.T 11.,. 23 a 117275 Merlin Rd Monroe NC 28110 KYW- 4, YF,NYS ,YP3,YD- RC 8 41.10% 109 a 35 2.325N 80 30.218 W 117275 Merlin Rd Monroe NC 28110 YK,YW- 2,NF,NS, 1/8/2019 RC YP YD-5 41.10% 86 a 351.974N 80 29.807W 117275 Merlin Rd MonroeNC 28110 _ YKYW- 2,NF,NS, 1/8/2019 RC NP YD-3 41.10% 18 ao 351.987N 80 29.230W 117275 Merlin Rd Monroe NC 28110 YK,YW- 2,NF,NS, 1/5/2018 RC NP YD-3 41.10% 29 all 35 5.917N 80 18.268W 5407 Pleasant Hill Chruch Rd Marshville NC 28103 Yk,YW- 2,NF,YS, 1/8/2019 RC NP YD-2 41.10% 32 a 351.890N 80 30.382W 117275 Merlin Rd MonroeNC 28110 YK,YW,N F,NS,YP, 1/S@018 RC YD 41.10% 36 a 35 8.314N 80 16.310W 5407 Pleasant Hill Chruch Rd Marshville NC 28103 YKYW,N F, YS, NP, 1/5/2018 RC YD-2 41.f0% 23 a 35 5.907N 8016.883W 5407 Pleasant HIII Chruch Rd Marshville NC 28103 YK,NW,N F,NS, YP, 1/5/2018 RC YD 41.10% 21 a 35 3.589N 8013.594W 5407 Pleasant Hill Chruch Rd Marshvllle NC 28103 YKNW,N F,NS,NP, 1/5/2078 RC YD-2 41.10% 19 a 35 3.367N 8013.648 W U07 Pleasant Hill Chruch Rd Marshville NC 28103 YK YW,N F,NS,NP, 1151201E RC YD.S 41.10% 11 a 353.171N 8013.587W 5407 Pleasant Hill Chruch Rd Marahville NC 28103 YK,NW,N F,NS,NP, 11512018 RC YD-2 41.10% e a 35 3.913N B0 15.189W - 5407 Pleasant Hill Chruch Rd Marshville NC 28103 YK,NW,N F,YS,NP, 1/5/2018 RC YD-2 41.10% 24 a 35 4.018N 8015.357W 5407 Pleasant Hill Chruch Rd Marshvllle NC 28103 NK,NW,N F,NS,NP, 10/18/2017 RC YD-5 41.10% 79 34 37.404N 7918.229W 1927 Geralds Rd. Rowland NC NK,YW- 2,NF,NS, 1/24/2019 RC YP YD-2 41.10% 20 a 3! 45.417N 79 4.159W 2139 Oak Grove Church Rd. Lumberton NC 28360 NKYW- 2,NF,NS, 2/20/1019 RC YP YD-4 41.10% !1 a 34 55.520N 79 1 3.583W 2139 Oak Grove Church Rd. Lumberton NC 28360 2/20/2019 34 52.549N 79 9.850W RC NK,YW- 2,NF,NS, NP YD-4 41.10% 3T a 2/20/2019 2139 Oak Grow Church Rd. Lumberton NC 28360 34 47.017N 7917.490W RC NK,YW,N P,YD- 2 NS NF 41.10% 6H a 2/20/2019 2139 Oak Grow Church Rd. Lumberton NC 28360 34 26.963N 79 9.363 W RC d Grass NK,YW- 2,NF,YN, YP YD4 41.10% 38 a 2/20/2078 465 Mill Branch Rd. Fairmont NC 28340 34 27.012N 79 8.815W RC NK, YW,N F,YS,NP, YD-2 41.10% 8 a 2/20/2019 4B5 Mill Branch Rd. Fairmont NC 28340 34 27.031N 79 B.9TBW RC NK,YW,N F,YS,NP, YD-3 41.10% 18 a 465 Mill Branch I Fairmont NC 2". a Mon. 4721.89000 1 1940.69679 NK, YW,Y P,NF,NS, 2121/2018 Grass YD-3 42.90% 137 34 53.170N 80 7.677W 2842 Horton Rd. Wadesboro NC 28170 YK,YW- Va 2,NF,YS, 119/L017 RC NP YD-3 42.90% 54 3514.594N 8017.498W 14348 McLester Rd. Oakboro NC 28129 YK,NW,N 119/2017 RC F. NS YP /2.9014 17 a 351L415N 8017.920W 14348 McLester Rd. Oakboro NC 28129 YK,YW- 2,NF,NS, 1199017 RC NP YD-2 42.90% 15 a 3514.125N 8017.872W 14348 McLester Rd, Oakboro NC 28129 YK,YW- 2,NF,NS, 11r9/2017 RC NP YD-3 42.90% I9 a 35 17.822N 80 18.943W 14348 McLester Rd. Oakboro NC 28129 YK, YW,Y F,YS,NP, 119/2017 RC YD-4 42.90% 39 a 3515.917N 8015.738W 14348 McLester Rd. Oakboro NC 28129 K, YIN, YF, YS,NP,D- 10/2/2018 Grass 3 42.90% 82 a 351.453N 8013.377W 10963 Willow Rd. Norwood NC 28128 K, YW, YF, YS,YP,D- 10/2/2018 Gress 3 42.90% 59 a 35 2.136N 8013.377W 10963 Willow Rd. Norwood NC 28128 NK,YW- 2,NF,NS, 1!M/2019 RC NP YD-2 42.90% 27 a 34I2.984N 791.718W 2139 Oak Grove Church Rd. Lumberton NC 28360 NK,YW- 3,NF,YS, YP-2,YD- 19U2019 RC 6 42.90% 99 a 3143.025N 791.BBO W 2139 Oak Grove Church Rd. Lumberton NC 28360 NK,YW- 2,NF,NS, 1124/2019 Grass NP YD 42.90% 40 a 3I {2.BOBN 791.8BOW 2139 Oak Gmm Church Rd. Lumberton NC 28360 NK,YW- 2,NF,NS, 194/2019 RC NP YD-4 42.90% 2d a 34 41.456N 79 2.015W 2139 Oak Grove Church Rd. Lumberton NC 28360 NK,YW- $NF,NS, 1/24/2019 RC NP YD-3 42.90% 17 34 41.472N 79 2.169 W 2139 Oak Grove Church Rd. Lumberton NC 28360 NK,YW- 2,NF,NS, 1/24PL019 RC NP YD-2 42.90% 31 a 34 41.545N 79 2.738W 2139 Oak Grove Church Rd. Lumberton NC 28360 NK,YW- 2,NF,NS, 19I12019 RC YP YD.3 42.90% 131 a 34 50.910N 79 0.561W 2139 Oak Grove Church Rd. Lumberton NC 28360 NK,YW- 2,NF,NS, 1/24/2019 RC YP YD-7 42.90% 69 a 34 38.878N 79 2.OBSW 2139 Oak Grove Church Rd. Lumberton NC 28360 NK, YW- 2,NF, YS, 24/1019 RC NP YD-2 42.90% 55 a 34 4788.1N 791.385W 979 Co Rd. Saint Paul's NC 28384 NK,YW- 2,NF,NS, 2/4/2019 RC YP YD•2 42.90% 18 a 34 50.772N 79 4.135W 979 Co Rd. Saint Pauls NC 28384 NK,YW- 2,NF,NS, 2///2018 RC NP YD 42.90% 72 a 3112.135N 79 B.B72W 2139 Oak Grow Church Rd. Lumberton NC 28360 NK, YW,N F,YS,NP, 2/4/1019 RC YD-2 42.90% 50 a 3I 11.718N 79 6.872 W 2139 Oak Grove Church Rd. Lumberton NC 28360 NK, YW,Y P,YD,NS, dN/2019 Grass IF 42.90'.L 32 a 34 50.670N 79 36.244 W 280 Dirt Rd. Hamlet NC 28345 YK,YW- $NF,NS, 311312018 Grass YP Y0 4 42.90-A 81 a 351L112N 807.821N 11204 Hw 145 South Woman. NC 28119 a a Month 3654.39000 1567.7333f 2019 Tons Tons Month Field Rain Acres D Use YK,YW- IS 2,YF,YS, 9l17/2017 Grass YP D-4 43.60% 180 a o /.487N 8018.007W 5815 Ansonville Rd. Marshville NC 28103 K,YW,NF, YS,NP,Y 11r9/2017 3515.817N 8018.9I3W RC D-4 43.60% 39 a 14348 McLester Rd. Oakboro NC 28129 K, YW, YF, YS,NP,Y 1/5/2018 RC D-3 43.60% 63 a 35 8.541N 80 16.360W 5407 Pleasant Hill Chruch Rd Marshville NC 28103 NK,YW,N F,NS,YP, 2/i1/2018 3{ 53.170N 80 7.8771 W Grass YD-3 43.60% 737 a 2842 Horton Rd. Wadesboro NC 28170 W K, Y,NF, YS,NP,Y 10/21Q018 RC D-3 13.80% 119 35 2.874N 8015.363W 10963 Willow Rd. Norwood NC 28128 K, YW, YF, YS,NP,D- 10/2/2018 Grass 3 43.80•/. 82 351.453N 8013.377W 10963 Willow Rd. Norwood NC 28128 NK,YW,Y 12130/2018 3/ 56.090N 7913.791W Grass F YS YP 43.60% 50 a o 284 Baldwin Rd. Rockingham, NC 28379 K,YW,NF, NS,YP,Y 3/7/1019 35 17.691N 80 12.412W Grass D-2 43.60•r6 29 a 64610 Malbry Rd. Albemarle NC 28001 K,YW,NF, YS, YP,Y 3/7/2019 Grass D-3 43.6056 12 a 35 16.749N 80 12.583W 64610 Mabry Rd. Albemarle NC 28001 K,NW,NF ,YS,NP,Y 3/7/2019 Grass D-2 43.60% 11 e 35 16.618N 80 12.708W 64610 Mabw Rd, Albemarle NC 28001 YIN. 3/7/L079 Grass YP YDA 43.60% 77 a 35 16.530N 80 12.555W 64610 Mabry Rd. Albemarle NC 28001 YIN. YP, YS, 5/22019 RC YD-3 NF 43.60% df a 35 2.T39N 80 21.018W 4723 Ansonville Rd. Marshville NC 28103 K,YW,NF, NS,YP,Y �1/2019 RC D-3 43.60% f36 a 34 57.593N 80 22.620 W 4723 Ansonville Rd. Marshville NC 28103 YK,NW,N F,NS,YP, 5?/2019 Grass YD 43.60% 1/ a 34 57.l11N 8011.70IW 4723 Ansonville Rd. Marshville NC 28103 YK,YW- 2,YP,YD- 5/1/2019 RC 4 YS NF 43.60% 66 35 4.013N 80 14.191W 4723 Ansonville Rd. Marshville NC 28103 :aE YW, YF, YS,YP,D- 5/2/2019 Grass Grass 6 43.60% 59 35 3.855N 80 MOM 35 4.405N 80 17.546W 4723 An�vllle Rd. Marshville, NC 2810 �358.421NBOSMIW 5815 An"nville Rd. Marshvllle,NC 28103 met"'�.4k 7"7�WEi KNW,NF ,NS,NP,Y 9H8!/077 Grass D 43.30% {2 Jb b.066N 80 9.69/W 3513 Amonville PolktonRd. Wadesboro NC 28170 KYW,NF, NS,NP,Y 9/20R017 Grass D-2 43.30% 54 35 2.543N 8011.329W PO BOX 84 PoBcton NC 38135 KYW,NF, NS,YP,Y 9,20/2017 Grass D-2 43.30-A 65 35 4.182N 8016. f25W PO BOX 84 PolMon NC 38135 KYw- 2, YP- 2,NF,NS, 9/20/2017 Grass YD-3 43.30% 57 a 35 3.898N 80 16.074W PO BOX 84 Polkton NC 38135 YKYw- 2, YF, YS. 8lt7l2017 Grass YPD4 43.30% ISO a 33l.167N 80 18.007W 5815 Ansonville Rd. Marshville NC 28103 KYw 2,NP,NS, 29/T019 Grass ND NF 43.30% 28 a 35 7.427N 80 10.723W ' 3655 Randall Rd. PolMon NC 28135 K YW, YP, YD,NS,N 2/9/2019 Grans F YD-4 43.30% 180 35 8.904N 80 8.634W 3655 Rantlall Rtl. Polkton NC 28135 KYS, YP- 2,YW YD- ?/9Q018 Grass 3 NF 43.30% 69 35 6.744N 80 7.687W 3655 Rantlall Rtl. Polkton NC 28135 YKYW,Y F,NS,NP, 5/?/2019 Grass 62 43.30% 28 35 3.801N 80 19.564W 5815 Ansonville Rd. Marshville NC 28103 KYW,NF, NS, YP,Y 5/2/2019 Grass D-2 43.30% 38 33 4.778N 8018.912W 5815 Ansonville Rd. Marshville NC 28103 Y YKW- 2,NF,YS, 5/2lL019 Grass YP YD4 13.. 83 36 4.405N 8017.546W a 4723 An-nvllle Rd. Marshville NC 28103 KYW,NF, YS,YP,D- YL2018 Grass 3 43.30% 40 35 2.719N 80 21.321W 5815 Aneonville Rd. Marshville NC 28103 YKYW,N F, YS, YP, YtR019 Grass D3 43.30% 42 35l.b0lN 8016.1{{W 5816 AnSd-ille Rd. MamhvilleNC 28103 YKYW,N F,NS,YP, YV1018 Grass YD-2 13.30X p a 35 2.749N 80 24.324W 5815 Ansonville Rd. Marshville NC 28103 KYW YF, YS,YP,D- Sr2Q019 Grass 2 43.30% f7 35 5.888N 80 20.260W 5815 Ansonville Rd. Marshville NC 28103 YK,YW- 2,NF,VS, 8!3/2019 Grass YP YD3 43.30% M 35 4.001 N 80 17.435W 7024 Thanny Helms Rd. Marshville NC 28103 YKYW,N F, YS, YP, e/J/2019 Gass YD-2 43.30% 17 3S 3.824N 8017.885W a 7024 Thannv Helms Rd. Marshville NC 28103 YKYW,N F,NS,NP, 1/52018 RC YD4 43.30% 89 11 35 5.781 N BO 17.O18W e 5407 Pleasant Hill Chmch Rd Marshville NC 28103 YK YW,Y P,NS,YD- 9Q0/2019 Grass 3 NF 43.30% 31 a 35 1.533N 80 12.069W PO BOX 84 Polkton NC 38135 KYW- 3,NP,NS, 9120lL019 Grass YD-2 NF 43.30% 28 a 35 2.837N 80 11.126W PO BOX 84 Polkton NC 38135 KYW,NP ,NS,YD- 1/i/2018 Grass 3 NF 43.30% 18 35 3.564N 8017.809W a 7024 Thannv Helms Rd. Marshville NC 28103 KYW-2, YP, YS,Y 9/20l2019 Grass D-2 NF 43.30% 23 35 922W 3.721N 80 15. a PO BOX 84 Polkton NC 38135 a e -- Month 4889.44000 2021.86752 2019 1Tone Tona Month T 8. Fls/d Rain 'ii. Use K,YW- 2,YP- 9i10/2017 2,NF,NS, 35 3.898N 80 16.074W Gross YD-3 41.20% 57 a PO BOX 84 Polkton NC 38135 K,YW- 11R1/2017 3,YP,YD- 35 5.334N 80 19.741 W Grass 6 YS YF 41.20% 172 a 9406 Olive Branch Rd, Marshville NC Nil K, YP, YIN, f0/2/2018 .;Jim NF, YS,Y 35 2 064N 80 14 532W Gross D-3 41.20% 38 a 2317 H 218 Peachland NC 28133 KYW,NP 7orb 18 ,YD,NS,N 35 2.258N 80 14.034W Gross F 41.20% 34 a 2317 218 Peachland NC 28133 KYW,YP, Z9/2019 YD- 35 8.904N 80 8.634W Gross 4 NS NF 41.20% 180 3655 Randall Rd. Polkton NC 28135 KYW,NF, 2/9R019 YS,YP- 35 6.744N 80 7.687W Grass 2 YD-3 41.20% 55 3655 Randall Rd. Polkton NC 28135 K,YW- eH7R019 2,NF,YS, 34 57.957N 80 24.929W Gross YP YD-2 41.20% BS a 4918 Old Monroe Manhville NC 28103 KYW,MF 6H7/2019 'YS'YP'Y 34 58.402N 8019.151W Grass 0.2 41.20% 85 2512 Old Pa eland Marshville Rd. Marshville NC 28103 K,YW,NF, 7/2019 YS, YP,Y 58.987N 34 8019.068W Gross D-3 11.20% 58 a 2512 Old Pa elaM Marshville Rd. Marshville NC 28103 KYW- 8/17/2019 2,NF,NS, 34 59.125N 8019.323 W Gross YP Y0.3 41.20% 67 a 2512 Old Pa eland Marshville Rd, Marshville NC 28103 KYW 6/21/2015 3,NFYS, 34 53.123N 80 22.419W Grass YP YD-4 41.20% 85 a 4103 Philadeohia Rd. Mamhville NC 28103 YK, YW,N 612712 F,NS,YP- 35 1.818N 80 23.004W Grass 2 YD-2 41.2. 65 a 5131 Dustv Lane Mamhville NC 28103 KNW,NF 79/t019 ,YS, YP,Y 35 6.335N 80 8.303W Gross D 41.20% 80 a 162 Hill Rd. Ansonville NC 28007 KYW- 7H5/2019 3,NF,YS, 35 7.502N 80 9.604W Gross YPYD-3 41.2. I8 a 38255 Harciv Rd Norwood NC 28128 K YW, YP, 7/19/2019 YD- 35 5.5764N 8010.156W Gross 4 YS NF 41.20% 29 a 740 Buffalo Creek Rd. Wadesboro NC 28170 KYW- 7/18/2018 2,NP,YD- 35 6.181 N 80 10.064W Gross 3 NS NF 41.2. 1{ a 740 Buffalo Creek Rd. Wadesboro NC 28170 KYW 2,NF, YS, 711912019 YP4, Y0. 35 6.161 N 80 9.600W Grass 5 41.20% 1, a 740 Buffalo Creek Rd. Wadesboro NC 28170 KYW- 7M9/2019 2,NPYD- 35 6.242N 8010.424W Gress 2 NS NF 41.20% 12 a 740 Buffalo Creek Rd. Wadesboro NC 28170 K YIN, YP, 7/79/2019 YD,NS,N 35 0.077N BO 5.841 W Gress F 41.20% 38 a 740 Buffalo Creek Rd, Wadesboro NC 28170 K. YIN, YP, 7/79,2019 Y0. 35 8.l21N 80 5.406W Gress 4 NS YF 41.20% 50 a 740 Buffalo Creek Rd. Wadesboro NC 28170 KYW,YP, 7..0" Y0. 35 5.188W 3.016N 80 Grass 2 NS NF 4/.20% q a 171 Po Road Wadesboro NC28170 a Month 4770.67000 1985.51604 Elwood 2019 soil I ITons Tons Month Tons FeTlei Field Rain T K Acres Wet Use Auo I Good YK,YW- 2,NF,YS, 10/5/1017 Grass YP YD-1 43.40% 70 3151.759N 80 29.887W a 6219 Ram Rd. Monme NC 28112 K,YW- 2,NF,NS, f0/S/1017 Grass YP YD-T 43.40% 57 34 53.295N 80 29.49W 6218 Ram Rd. Monme NC 28112 K, YW. 3, YP, YD- 1112112017 Grass 6 YS YF 43.40% TiT 35 5.334N 80 19.741W 9406 Olive Branch Rd. Marshville NC k YW- 2,NFYS, 3/11/2018 Grass YP YD-3 43.40% 81 M 32.445N 80 0.893W 550 Rodahaven Rd Morvan NC28119 K,YW- 1,NF,YS, 5/T/T019 Grass YP YD-2 43.40% 39 351.282N 8019.389W 4723 Ansonville Rd Marshville NC K,YW- 2,NF,YS, 5/2/2019 Grass YP YD-2 43.40% 21 35 09.48N 80 21.515W 1723 Ansonville Rd Marshville NC K,YW,NF, 6/2/2019 Grass NS, YP, YD 43.40% 24 J/ 55.151N 80 2J.593W 1723 Ansonvilla Rd Marshville NC YK,YW,N F,YS,NP, 5/2/2019 Grass YD 43.40% 1H s 34 52.988N 80 24.633W 4723 Ansonville Rd Marshville NC YK,YW- 4,NF,YS, 5/2/T019 Grass NP YD-2 43.40% 26 11 3151218N 80 23.831W 1723 Ansonville Rd Marshville NC YK,YW,N F,NS,NP, 6/21/2019 Grass YD-2 48 34 52.201 N 8018.002W 4103 Philadel hia Church Rd. Marshville NC 28103 K, Y- 2,NF,NS, 6121/1019 Grass YP YO.3 43.40% 25 74 50.889N 80 23.522W 4103 Philadelphia Church Rd. Marshville NC 28103 YK, YW,N F,NS,YP- 6/27/2019 Grass 2 YD-2 43.40% 31 34 56.073N 80 20.820W 5131 Dusty Lane Marshville NC 28103 K,YW,NF, YS, YP,Y 6/T7/2019 Gress D-3 43.40% 30 34 56.077N 80 20.737W 5131 Dusty Lana Marshville NC 28103 K, YW,NF, NS,NP,N 612712019 Grass F 43.40% 15 35 2.I29N 80 22.BSBW 5131 Dusty Lana Marshville NC 28103 K,YW,NF, YS, YP,Y 6/27/2019 Grass D 43.40% 18 75 2.258N 80 23.082W 5131 Dusty Lane Marshville NC 28103 K,YW- 2, NF, YS, 7BlL019 Grass YP YD-3 43A0% 92 35 5.847 N 80 21.753W 1611 Stewart Farm Rd. Marshville NC 28103 YK,YW- 2,NF, YS, 7/26/2019 Grass YP YD-3 43.40% 18S p 35 4.584N 80 9.483W 5/Z2019 2512 Red Hill Mt Vernon Rd. Wadesboro NC 28170 35 3.892N 80 20.971 W RC K,YW,NF, NS, YP, Y- 4 43.40% M a 4723 Ansonvllle Rd Marshvllle NC 28103 5/2/2019 35 4.038N 80 20.839W RC YK,YW,N F,NS, YP, YD 43AM 18 a SS/2019 4723 Ansonville Rd Marshville NC 28103 35 4.451N 80 20.480W RC YK,YW- 2,NF, YS, NP YM2 43.40% 106 a 5/L201B 4723 Ansonvllle Rd Marshville NC 28103 35 3.388N 80 20.850W RC K, YW,NF, NS,NP,N D 43.40% 25 a WZ17019 4723 Ansonvllle Rd. Marshvllle NC 28103 351.008N 80 18.940W RC K,NW,YS ,YF,NP,Y D-2 43.40% 156 a 4723 Ansonvllle Rd Marshville NC 28103 a Month 4915.17000 1 2133.18378 YKYw- $NF,YS, IM57017 34 51.758N 80 29.887W Gross YP YD-2 I4.00% 70 a 6218 Roos Rd. Monroe NC 28112 KYW- 2,NF,NS, 10/5/2017 Grass YPYD3 44,00% 68 a 34 52.O66N 80 33.634W _ 6218 Roos Rd. Monroe NC 28112 K YW- 2,NF,YS, 5/2/1019 Grass YP YD-2 44.00% 39 a 354.282N 8019.SBBW _ Rd Marshville NC KYW,NF, _ NS,NP,N 6/27/2019 Asew =352.256N Grass F ND 44.00% 15 a Dusty e Marshville NC 28103 KYW,NF, YS,YP,Y 6/27/2019 Grass D 44.00% 18 a 082W _ 5131 Dusty Lane Marshvllle NC 28103 YKYW- 2,NF,YS, Grass YP YD3 44.00% 185 35 4.564N 80 9.483W _ 2512 Red Hill Mt Vernon Rd. Wadesboro NC 28170 _ ... _. ,.. YKYW- 2,NF,YS, 5/2/2019 4153 35 4.451 N 80 20.460W RC NP YD-2 44.00% f08 a 4723 Ansonville Rd Marshvllle NC 28103 ,.. — K YW 2 YP YS 51212019 4161 35 01.812N 80 16.379W Grass NF YD-2 44.00% 33 a 4723 Ansonville Rd Marshvllle NC 28103 _ K,NW,YS ,YF,NP,Y 5/2/2019 RC D-2 44.00% 158 a 351.00BN 8018.940W _ 4723 Ansonvllle Rd. Marshvllle NC 28103 r YKYW,N F, YS, Old 1212812015 _ 34 58.182N BO 22.133W RC PYD 44.00% 43 a 4723 Ansonville Rd Marshvllle NC 28103 K YW, YS, NF, YP,Y 12/28/2015 RC D-3 44.00% 58 a 34 58.132N 80 22.899W 4723 Ansonville Rd. Marshville NC 28103 KYW,NF, YS,NP,Y 12/28/2018 RC D-2 44.00% 88 a 34 57.195N 80 22.775W 4723 Ansonville Rd Marshvllle NC 28103 K YIN, YF, YS,NP,Y 12/28/2015 RC D-2 44.00% 76 a 34 58.948N 80 23.061 W 4723 Ansonville Rd Marshville NC 28103 — — K YW 2,NF,YS, 5/2/2019 RC NP YD3 44.00% 56 a 351.055N 8019.403W 4723 Ansonvllle Rd Marshville NC 28103 YK,YIN. 2,NF,YS, Y-2P,YD- 8/29/2019 RC 4 44.00% 135 _ 34 49.208N 80 30.113W 5818 Cox Rd. Monroe NC 28112 YK,YW,N F,YS,YP- 8/2912019 RC i 2 YD-3 H.00% 125 a 34 49.325N 80 31.202W 5818 Cox Rd. Monroe NC 28112 1,4 34 52.MN 80 31.43OW 5818 COX Rd. Monr", NC 28112 EMMA =1 E1Wood 2019 Sob Tons Tons Monts Two I Farmer Field Rain T K Acres et D Use K,YW,NF, Grass YS, YP,Y D 40.00% 130 12M8/2018 3854 34 48.794N 80 6.253W 377 Can! Rd. an NC 28119YK,YW,N =Ea F, YS, YP, RC YD-84000% 34 51.593N 80 32.658W 5818 Cox Rd. Monroe NC 28112 0 YK,YW.2, NF,YS,OI 8lt9lM1D RC dP, YD-4 40.00% 134 a 34 51.841 N 80 J1.J11 W 5 118 Cox Rd. Monroe NC 28112 K,YW,NF, YS, YP,Y B/29/2019 RC D-J 40.00% 325 a 34 52.328N BO 31.130W 5818 Cox Rd. Monroe NC 28112 YK, YW. 2,NF,YS, 8/29/2019 RC NP YD-4 40.00°h 274 a 34 49.208N 80 30.1 t3W 5818 Cox Rd. Monroe NC 28112 YK,YW,N F,NS,NP, 812912019 RC YD 40.00% 34 a 34 49.325N 80 31.202W 5818 Cox Rd. Monroe NC 28112 K,YW- 2, NF, YS, 8/2W2079 RC YP YD-3 40.00% 19B09 34 54.403N 80 32.912W 5818 Cox Rd. Monroe NC 28112 YK, YW,Y F,YS,NP, 8/29/2019 4190 RC YD 40.00% 217 34 54.358N 80 32.295W 5818 Cox Rd. Monroe NC 28112 K,YW- 1,NF,NS, 8/29/2019 RC YP YD-4 40.00% 175 34 58.179N 80 22.443W Wia Cox Rd. Monroe NC 28112 K,YW- 3,NF,YS, H/29/2019 RC YP YD-3 40.00 % 81 34 58.140N 80 20.929W 5818 Cox Rd. Monroe NC 28112 K,YW- 2,NF,NS, 8/29/2019 RC NP, YD 40.00% 2H 34 51.BSON 80 31.879W 5818 Cox Rd. Monroe NC 28112 YK, YW- 2,YP,YD- RC 4 YS NF 40.00% 148 34 52.033N 80 28.025W 5818 Cox Rd. Monroe NC 28112 K, YW, NF, NS, YP,Y 1012512019 RC D 40.00% 11 >• 52.439N 80 27.802W 4302 Stock Rd. Monroe NC 2812 K,YW,NF, NS,NP,N 10/15/2019 RC D 40.00% 12 34 52.579N 80 27.878W 4302 Stack Rd. Monroe NC 2812 K,YW,NF, NS,NP,Y 10/25/2019 RC D-2 40.00% 13 a 34 52.843N 80 27.542W 4W2 Stack Rd. Monroe NC 2812 K,YW,NF, NS, YP,Y 1012512019 RC D 40.00% 9 34 52.523N 80 27.258 W ��� �� 1 l`. 2019 1Tons Tons Monty x Fleld Rain Acres D use KYW,NF, YS,YP,Y 12H8lL018 3854 Grass D 45.20% 130 a 34 48.794N 80 6.253W 377 CmlPe Rd. Morgan. NC 28119 YK, YW,N SWO19 4270 RC F NS NP 45.20% f02 ao 35 3.958N 80 20.301 W 4723 Ansonvllle Rd. Marshville NC YK,YW,N 1212&2018 4174 RC FNSNp 45.20% 83 a 35 5.315N 80 18.919W 117275 Merlin Rd Monroe NC 28110 YK YW,N F,YS,NP, 81291, RC YD-2 45.20% 133 a 34 53.227N 80 33.109W 5818 Cox Rd. Monroe NC 28112 W KY $NF, YS, 8l29/2019 RC YP YD3 45.20% i 34 54.403N 80 32.912W 5818 Cox Rd. Monroe NC 28112 M YK YW,Y F,YS,NP, 8/29/2019 4190 RC YD 45.20% 217 34 54.358N 80 32.295W 5818 Cox Rd. Monroe NC 28112 812912019 4191 0 11107119 0.3", 11101119 .7',111=19 RC YK YW,Y F YS NP 45.20% 582 a J4 57.781 N 80 27.530W 5818 Cox Rd. Monroe NC 28112 YK,YW,N 1012&2019 4220 RC F NS NP 45.20% 12 a 34 51.934N 80 29.175W 4302 Stack Rd. Monroe NC 2812 K YW,NF, NS,NP,Y 1012512019 RC D-2 45.20% 13 a 34 52.BpN 80 27.542W 4302 Stack Rd. Monroe NC 2812 K YW, YP, YS,YD,Y 5/2/2019 4235 RC F 45.20% 185 a 350.524N 80 19.099W 4723 Ansonvllle Rd.Marshville NC 28103 YK YW,Y P,NS,YD, 5/2lt019 4237 RC NF 45.20% 92 a 351.155N 8018.574W 4723 Ansonvllle Rd.Marshville NC 28103 NK YW,N IZ12312019 Grass F NS YP 45.20% 31 a 35 4.481 N 7912.738W 2589GIbson Rd. Nurse Rd. Ellerbe NC 28338 NKYW- 4,NF,NS, 1213Q019 Grass NP YD 45.20% 38 a 35 2.281 N 79 43.042W 2589GIbwn Rd. Nurser Rd. Ellerbe NC 28338 NK YW,N F,NS,YP 12/23/2019 4269 Gress YD /5.20% 77 a 35 8.619N 79 38.984W 2589GIbson Rd. Nursery Rd. Ellerbe NC 28338 NKNW,N F,NS,NP, i 7/22R019 RC YD 45.20% 15 a 34 58.432N 79 40.853W 805 Mldvre Rd. Rockin ham NC 28379 NK YW,Y F,YS,YP, 2N6/L017 RC YD 45.20% 82 a 34 42.068N 7915.389W 1373 Harpsis Fer Rd. Pembroke NC 283 r2 E 9F--- �53 ig[M 'r, N M I IM�aaaaaallLL-L- NK,YW,N F,YS,NP, 2d3/2019 3976 RC YD 44.80% 51 a 34 32.988N 78 6.3BQW 1892 Honn Comp Rd. Fairmont NC Nk, YW,N 11/23/2018 I2I8 Grass F NS NP 44.80% 20 a 35 5,307N 79 40.137W 2589GIbson Rd. Nursery Rd. Ellerbe NC 28338 NK,NW,N F, YS,NP, IWIO12017 {253 RC YD 44.80% 13 a 34 31.307N 79 9.385W 1927 Geral Rd. Rowland NC NK,YW,N F,NS,NP, 10/1&2017 4255 RC YD 4/.80% 40 a 34 31.572N 79 6.745W Za 1927 Geral Rd. Rowland NC NK,YW,N fOHB/2017 IT57 RC FNSNP 44.80% 126 34 30.080N 79 9.871 W 1927 Gerald Rtl. Rowland NC NK,YW,N IZ23/2018 Grass FNS YP 44.80% TO a 35 6.336N 79 40.003W 2589Gibson Rd. NurseryRd. Ellerbe NC 28338 NK,YW,N 1112=019 RC F NS YP 44.80% 15 34 56.432N 79 40,653W 805 MidwayRd. Rockin ham NC 28379 NK,YW- 2,NF,NS, THB/2017 RC YP YD-3 44.80% 82 a 34 42.OBBN 7915.389W 1373 Nar is FerryRd. Pembroke NC 28372 NK,YW,N F,NS,NP, 11/29/2019 4281 RC YD 44.80% IO a 34 33.062N 79 9.801 W 652 Stone Rd FairmontNC 28340 NK,NW,N F,YS,NP, 11/29/2019 4284 RC YD 44.80% 71 34 32.651 N 79 9.204W 852 Slone Rd Fairmon NC 28340 NK, YW< NF, YS,Y 11/29/2019 4285 RC P YD M.80% 151 a 34 32.308N 7910.872W 662 Stone Rd FairmontNC 28340 NK, YW,N 11/29/2019 4288 RC F NS NP 44.80% 112 a 34 33.435N 7912.094W NK, YW,N F,NS,NP, 11/29/2019 RC YD-6 44.80% 151 a 34 31.906N 7916.495W 652 Stoll Rd Fairmon NC 28340 NK,YW,Y 12/23/L016 Grass P NF NS 44.8014 T8 a 35 3.681 N 79 45.604W 2589 gibscm Nursery Rd. Ellerbe NC 28338 NK,YW,N 17l10/T019 4290 Gnss F NS YP 44.80% 79 34 49.447N 79 46.998W 127 Saron Church Rd. Ellerbe NC 28338 NK,YW,N F,NS, YP, 12,20/2019 4291 Gross ND 44.8011 24 a 35 5.889N 79 43.873W 601 Crawford Rd. Ellerbe NC I.M R"T nT, I :c, m 4 1 rmn 35 30.358N 79 4% 914W 232 Cagle Rd Somrove, NC 37341 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): � Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) Distribution anarketing (complete Parts A, B, and C) Was the facility in operation during the past calendar near? Yes No ❑ -► If No skin Darts A. B. C and certify form helnw Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January WQ0009477 2019.94850 2019.94850 See Attached 2019.94850 Agricultural February WQ0009477 1277.19351 1277.19351 1277.19351 Agricultural March WQ0009477 1940.69679 1940.69679 1940.69679 Agricultural April WQ0009477 1567.73331 1567.73331 1567.73331 Agricultural May WQ0009477 2166.00004 2166.00004 2166.00004 Agricultural June WQ0009477 2021.86752 2021.86752 2021.86752 Agricultural July WQ0009477 1965.51604 1965.51604 1965.51604 Agricultural August WQ0009477 2133.18378 2133.18378 2133.18378 Agricultural September WQ0009477 2151.86400 2151.86400 2151.86400 Agricultural October WQ0009477 2044.75200 2044.75200 2044.75200 Agricultural November WQ0009477 2217.18656 1 2217.18656 2217.18656 Agricultural December WQ0009477 1796.48000 1 1796.48000 1796.48000 Agricultural Total from FORM DMSDF (sup) 0 23302.42205 23302.42205 23302.42205 Totals: Annual (dry tons): 0 23302.42205 23302.42205 23302.42205 Amendment(s) used: Bulking Agent(s) used: (supp)): Total Number of Form DMSDF (Supp)l 7 * If more space is required, attach additional information sheets (FORM DMSDF rar< %-: Facility was compliant during the past calendar year with all conditions of the land application permit Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. Z. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature ofPermittee Date Signature ofPreparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nFNR FnRan nancnF ti9i9nnai CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): ❑ rface Disposal (complete Part A -"Month", "Source(s)" and "Residual In" columns only) Distribution and Marketing (complete Parts A, and B) Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) Jan WQ0009477 10.28075 10.28075 Ronnie Bralock 10.28075 ag WQ0009477 21.063 21.063 Richard Hays 21.063 ag WQ0009477 306.63750 306.63750 Andura Hunt 306.63750 ag WQ0009477 191.70475 191.70475 James Ray Locklear 191.70475 ag WQ0009477 10.60800 10.60800 Wendall Locklear 10.60800 ag WQ0009477 193.82975 193.82975 L&R Moore 193.82975 ag WQ0009477 31.44150 31.44150 Lycurous Lowery 31.44150 ag WQ0009477 115.55750 115.55750 Jessie Oxendine 115.55750 ag WQ0009477 62.36025 62.36025 Roger Oxendine 62.36025 ag WQ0009477 23.07325 23.07325 Johnathan Scott 23.07325 ag WQ0009477 166.01350 166.01350 David Underwood 166.01350 ag WQ0009477 10.50600 10.50600 Mike Willoughby 10.50600 ag WQ0009477 334.15200 334.15200 Odell Wilkins 334.15200 ag WQ0009477 172.01875 172.01875 Robert Wilkins 172.01875 ag WQ0009477 370.702 370.702 Lee Grady Lowery 370.702 ag 0 Feb WQ0009477 197.33373 197.33373 Aundra Hunt 197.33373 ag WQ0009477 51.16608 51.16608 Jimmy Hunt 51.16608 ag WQ0009477 10.35081 9.72900 29.16585 21.30651 30.19797 10.35081 9.72900 29.16585 21.30651 30.19797 L&R Moore Farm Daniel Locklear Jerry Locklear Phillip Locklear Lee Grady Lowery 10.35081 9.72900 29.16585 21.30651 30.19797 ag ag ag a WQ0009477 WQ0009477 WQ0009477 WQ0009477 ag Totals: Annual (dry tons): 0 2369.19845 2369.19845 2369.19845 rvnendmentts) used: I I hulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)r 7 DENR FORM DMSDF (Supp) (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Distribution and Marketino tcmmnlete Porte A_ end R1 Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name (s) Volume (dry tons) Intended use(s) .e 2Gontin'uerl W00009477 71.14437 71.14437 Jessie Oxendine 71.14437 ag W00009477 19.44954 19.44954 Peter Duel Oxendine 19.44954 a W00009477 478.78947 478.78947 Rex Oxendine 478.78947 a W00009477 20.0079 20.0079 David Undenvood 20.0079 ag W00009477 329.27589 329.27589 Odell Wilkins 329.27589 a W00009477 9.27639 9.27639 Robert Wilkins 9.27639 a Mar W00009477 241.61046 241.61046 Jamie Austin 241.61046 a WQ0009477 70.78653 70.78653 Kevin Buie 70.78653 a WQ0009477 10.00374 10.00374 JeffGriffin 10.00374 a W00009477 117.01992 177.01992 Wilber Hams 177.01992 a W00009477 81.74379 81.74379 L&R Moore Farm 81.74379 a W00009477 133.33251 133.33251 James Ray Locklear 133.33251 a W00009477 226.96242 226.96242 Lee Grady Lowery 226.96242 ag W00009477 69.05211 69.05211 Jessie Oxendine 69.05211 ag W00009477 127.96485 127.96485 Peter Duel Oxendine 127.96485 a W00009477 157.21161 157.21161 Roger Oxendine 157.21161 a W00009477 90.38712 90.38712 Glen Phiefer 90.38712 a W00009477 432.28158 432.28158 Tony Taylor 432.28158 a W00009477 30.29892 30.29892 David Underwood 30.29892 ag WQ0009477 133.40649 133.40649 Odell Wilkins 133.40649 a W00009477 18.63474 18.63474 Robert Wilkins 18.63474 a Totals: Annual (dry tons): 0 2868.64035 2928.64035:•; ;*..,*""; : •'.'.'.'.'..::::::: 2928.64035 .................................... Amendment(s) used: Bulking Agent(s) used: • It more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 7 927.94356 1940.69679 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Distribution and Marketing (complete Parts A, and B) Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) April W00009477 238.54545 238.54545 Jason Blackwelder 238.54545 ag WQ0009477 161.86170 161.86170 Bruce Cuddy 161.86170 ag WQ0009477 63.00294 63.00294 Tony Helton 63.00294 ag WQ0009477 204.58152 204.58152 Lee Farm 204.58152 ag WQ0009477 126.72231 126.72231 Talton Locklear 126.72231 ag WQ0009477 146.24610 146.24610 Mike Preslar 146.24610 ag WQ0009477 105.74850 105.74850 Peter Duel Orendine 105.74850 ag WQ0009477 521.02479 521.02479 Odell Wilkins 521.02479 ag 6 Sg May W00009477 86.91224 86.91224 James Austin 86.91224 ag WQ0009477 11.46244 11.46244 Jason Blackwelder 11.46244 ag WQ0009477 11.72404 11.72404 Lee Farm 11.72404 ag WQ0009477 573.13508 573.13508 David Hill 573.13508 ag WQ0009477 233.44312 233.44312 Clifford Kinrey 233.44312 ag WQ0009477 488.20228 488.20228 Mike Preslar 488.20228 ag WQ0009477 661.29428 661.29428 Mark Lynn Thomas 661.29428 ag WQ0009477 99.82656 99.82656 Tony Williams 99.82656 ag 1 6+ OOQ4 Totals: Annual (dry tons): 0 3733.73335 3733.73335 :: 3733.73335 Amendment(s) used: I Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1 7 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT N: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-8954033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Dktrihutinn and Mnrk.fno (-.W. P"rrr A ,...a Ru Part A": Part B•• Month Sources(s) (include NPDES N if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use s ( ) June W00009477 95.42021 95.42021 Jamie Austin 95.42021 ag W00009477 182.42290 182.42290 David Hill 182.42290 ag W00009477 503.60065 503.60065 Buck Meeks 503.60065 ag W00009477 199.47011 199.47011 Henry Nance 199.47011 ag W00009477 520.18022 520.18022 Bruce Shankle 520.18022 ag W00009477 419.21328 419.21328 Mark Lynn Thomas 419.21328 ag W00009477 101.56015 101.56015 Lavon Tyson 105.56015 ag July W00009477 411 28724 411,28724 Ralph Blevems 411.28724 ag W00009477 83.1416 83.1416 Stevie Carpenter 83.1416 ag W00009477 123.50936 123.50936 Jeff Griffin 123.50936 ag W00009477 156.76188 156.76188 Lane Haigler 156.76188 ag W00009477 146.13228 146.13228 Paulett Helms 146.13228 ag W00009477 171.04180 171.04180 Donnie Honeycutt 171.04180 ag W00009477 402.98132 402.98132 Fincher Martin 402.98132 ag W00009477 10.3734 20.3734 Bruce Meeks 20.3734 ag W00009477 39.81568 39.81568 Bruce Shankle 39.81568 ag W00009477 175.66856 175.66856 Ed Staton 175.66856 ag W00009477 111.27296 111.27296 Tommy Staton 111.27296 ag W00009477 123.52996 123.52996 Andy Williams 123.52996 ag Totals: Annual (dry tons): 0 3987.3836 3987.3836 :• 3991.3836 Amendment(s) used: Bulking Agent(s) used: • It more space is required, attach additional untormatuon sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)� 1965.51604 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT N: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-8954033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Distribution and Marketine (comnlete Parts A. and R) Part A': Part B": Month Sources(s) (include NPDES N if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) Aug .... W00009477 150.31156 150.31156 Lane Haigler 150.31156 ag .. .- . _.- 0009477 W Q 369.8982 369.8982 BuckHarrinton 369.8982 ag W00009477 180.87818 180.87818 JefPLong 180.87818 ag W00009477 175.3143 175.3143 George Short 175.3143 ag W00009477 252.8484 252.8484 Ed Staton 252.8484 ag W00009477 176.55554 176.55554 Tommy Staton 176.55554 ag W00009477 207.65598 207.65598 Bryan Stewart 207.65598 ag W00009477 619.721621 619.72162 Mark Lynn Thomas 619.72162 ag Set W00009477 1298.18480 1298.18480 Cox & Watson 1298.18480 ag W00009477 79.04160 79.04160 Buck Harrinton 79.04160 ag W00009477 133.74240 133.74240 Jeff Long 133.74240 ag W00009477 22.26840 22.26840 Tommy Staton 22.26840 ag W00009477 618.62680 618.62680 Mark Lynn Thomas 618.62680 ag W00009477 ag W00009477 ag W00009477 ag WQ0009477 ag W00009477 ag W00009477 ag W00009477 ag W00009477 ag W00009477 ag WQ0009477 ag Totals: Annual (dry tons): 0 4285.04778 4285.04778 ;;;;'''''•'''''''.'.'.'.'.'. 4285.04778 ............. Amendment(s) used: I Bulking Agent(s) used: It more space is required, attach additional mtorrnatton sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)1 7 133.18378 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: W00009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-895-4033 7428E COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) X Distribution and Marketing tmmnlete Pnrtc A_ -1 R1 Part A": Part B": Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) Oct W00009477 1782.16000 1782.16000 Cox And Watson 1782.16000 ag W00009477 152.25600 152.25600 Michael Canipe 152.25600 ag W00009477 110.33600 110,33600 Thomas Farms 110.33600 ag Nov W00009477 373.67292 373.67292 Mark & Lynn Thomas 373.67292 ag W00009477 192,32148 192,32148 Michael Canipe 192.32148 ag W00009477 22.23388 22.23388 Thomas Farms 22.23388 ag W00009477 11.39040 11.39040 John Quick 11.39040 ag W00009477 332.04824 332.04824 Steve Reams 332.04824 ag W00009477 231.93024 231.93024 Ronald Strickland 231.93024 ag W00009477 89.60448 89.60448 Tony Taylor 89.60448 ag W00009477 963.98492 963.98492 Cox & Watson 963.98492 ag ag Totals: Annual (dry tons): 1 0 4261.93856 4261.93856. >ii:::•: is }}}??:: ii}}}:' 4261.93856 Amendment(s) used: I Bulking Agent(s) used: it more space is required, attach additional information sheets (1-UKM UMJUF (supp)): Total Number of Form DMSDF (Supp)I 1044.75200 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT H: WQ0009477 FACILITY NAME: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. PHONE: 910-8954033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy FACILITY TYPE (please check one): Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) x .nd Ma,kaq nn ann ie.e o.,_.- . Part A": Part B*: Month Sources(s) (include NPDES N if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) Dec-19 W00009477 162.36864 162.36864 Henry Currie 162.36864 ag W00009477 74.20672 74.20672 Joe Grooms 74.20672 ag W00009477 65.60960 65.60960 Jimmy Hunt 65.60960 ag W00009477 108.36224 108.36224 Alan Locklear 108.36224 ag W00009477 279.09504 279.09504 Lee McFarland 279.09504 ag W00009477 677.65376 677.65376 Mitch & Garrison 677.65376 ag W00009477 276.80128 1 276.80128 Roger Oxendine 276.80128 ag W00009477 20.31232 20.31232 John Quick 20.31232 ag W00009477 122.30848 122.30848 Steve Reams 122.30848 a W00009477 9.76192 9.76192 Ronald Strickland 9.76192 ag :use 4e. a Totals: Annual (dry tons): 0 1796.480001 1796.48000::::::::_._..:.. i:: >::-:::-:-i:::: 1796.48 ................. .......... Amendment(s) used: Bulking Agent(s) used: i more space is requires, attach aaaltionai mtormation sheets (FURM DMSDF (supp)): Total Number of Form DMSDF (Supp)� ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0009477 Cascades Tissue Group -North Carolina, a Facility Name: division of Cascades Holdings US Inc. Residual Source WQ # or WQ0009477 NPDES #: WWTP Name: Residual Analvsis Data Laboratory: 1) Pace Analytical Services LLC. 2) Waypoint Analytical 3) Summit 4) 5) Parameter (mg/kg) Ceiling Conc. Limit (m /k )a Sample or Composite Date 01/17/19 02/07/19 03/07/19 04/09/19 05/09/19 06/11/19 07/15/19 08/13/19 09/10/19 10/10/19 11/07/19 12/10/19 Percent Solids (%) NA 42.50 42.3 41.10 1 42.9 43.6 43.3 41.2 43.4 44 40 45.2 44.8 Arsenic 75 0.081 0.064 1.4 0.75 0.62 I 1.1 0.77 0.72 1.1 0.85 1.1 Cadmium 85 Not Permit Required Copper 4,300 17.6 13.2 15.3 15.2 13.7 17.5 15.9 15.7 24 18.1 17.6 16.2 Chromium NA Not Permit Required Lead 840 Not Permit Required Mercury 57 Not Permit Required Molybdenum 75 Not Permit Required Nickel 420 1.2 1.1 1.4 1.50 1.2 1.5 1.2 1.7 1.1 1.50 5.2 11.8 Selenium 100 Not Permit Required Zinc 7,500 62.8 67.6 57.9 120 48.5 92.6 84.2 107 65.3 76.6 81.7 61.8 Total Phosphorus NA Not Permit Required TKN NA 3380 1430 2290 1040 1320 1310 1900 1810 1730 1960 1400 1530 Ammonia -Nitrogen NA 290 22.7 20.6 19.4 20.5 20.3 23.3 22.6 21 18.6 22.1 21.9 Nitrate and Nitrite NA 4.76 4.7 4.8 4.6 4 4.5 4.8 4.5 4.4 4.9 4.3 4.4 rui su,iauc u,sPwai iac,iiues ine cenmg concentration limits Listed in this Corm are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penaltie f r submitting false i9foppition, including the possibility of fines and imprisonment for knowing violations." Si nature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00009477 Cascades Tissue Group -North Carolina, a division of Facility Name: Cascades Holding US Inc. Residual Source NPDES # or WQ#: WWTP Name: Recidnal Analvcic nota WQ0009477 Laboratory: 1) Pace Analytical Services, LLC 2) Waypoint Analytical 3) Summit ample or Composite Date 01/17/19 02/07/19 03/07/19 04/09/19 05/09/19 06/11/19 07/15/19 08/13/19 09/10/19 10/10/19 11/07/19 12/10/19 Parameter (mg/kg) Pan Cal 2709 429 687 312 396 393 570 543 519 588 420 459 Aluminum Not Permit Required Carbon/Nitrogen Ratio 86 10 81 330 150 81 61 63 99 42 51.5 27 Calcium Carbonate Equivalency Not Permit Required PH 6.6 7 7.1 7.4 8.10 6.9 7.1 7 6.8 6.9 6.9 7.3 Magnesium 1410 1450 1240 1400 1770 1550 1590 1360 1770 1790 1600 1620 Sodium Not Permit Required Potassium Not Permit Required Calcium 150000 159000 122000 141000 199000 156000 163000 170000 188000 193000 169000 159000 Non- Ignitablilty- Summit 04/22/19 Flammable ND-0.495 mg/kg Cyanide ND-25.0 mg/KG Reactivity Summit 04/22/19 Sulfide Corrosivity Summit 04/22/19 7.2 Total Nitrogen 3380 1430 2290 1040 1320 1310 1900 1810 1730 1960 1400 1530 TOC 29200 299000 367000 322000 281000 284000 306000 307000 295000 285000 275000 651000 Volatile Solids 503000 514000 631000 554000 483000 489000 526000 528000 508000 491000 473000 494000 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprison�en�tr knowing ions." '?o Sign a a Prepare, * Date •Preparer is defined in 40 CFR Part 503.9(r) and 15A C 2T .1102 (26) DENR FORM RSSF - B (12/2006) aceAnalytical www.pacelabs.com February 18, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92414423 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on January 17, 2019. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. A revised report is being submitted on 2/18/19 to include a revised subcontract report. If you have any questions concerning this report, please feel free to contact me. Sincerely, o, q�l ; `T✓=' N' Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 19 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92414423 Sample: Monthly Sludge Lab ID: 92414423001 Collected: 01/17/19 07:40 Received: 01/17/19 08:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601OD Preparation Method: EPA3050B Arsenic ND mg/kg 1.6 0.81 1 01/18/19 09:23 01/21/19 04:45 7440-38-2 Calcium 150000 mg/kg 161 80.6 10 01/18/19 09:23 01/21/19 23:36 7440-70-2 Copper 17.6 mg/kg 0.81 0.40 1 01/18/19 09:23 01/21/19 04:45 7440-50-8 Magnesium 1410 mg/kg 16.1 0.40 1 01/18/19 09:23 01/21/19 04:45 7439-95-4 Nickel 1.2 mg/kg 0.81 0.40 1 01/18/19 09:23 01/21/19 04:45 7440-02-0 Zinc 62.8 mg/kg 1.6 0.81 1 01/18/19 09:23 01/21/19 04:45 7440-66-6 254OG Total Percent Solids Analytical Method: SM 254OG-2011 Total Solids 42.5 % 0.10 0.000010 1 01/17/19 18:00 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 57.5 % 0.10 0.10 1 01/17/19 17:55 9045 pH Soil Analytical Method: EPA 9045D pH at 25 Degrees C 6.6 Std. Units 0.10 0.10 1 01/23/19 16:57 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/18/2019 09:26 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 19 Report Number: 19-022-9206 •(M Account Number: 05734 ��ypO' �� . 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : Sludge - 92414423001 ANGELA BAIONI 9800 KINCEY AVENUE SUITE 100 HUNTERSVILLE , NC 28078 REPORT OF ANALYSIS Date Sampled: 1/17/2019 07:40:00 Lab Number: 64501 Date Received: 01/22/2019 00:00 Sample Id : Sludge - 92414423001 Revised Report Date : 02/18/2019 Total Solids 41.40 414000 100.0 CJR 01/24/2019 15:44 SM-2540G Moisture' 58.60 100.0 CJR 01/24/2019 15:44 SM-2540G Total Kjeldahl Nitrogen 0.34 3380 250 CLP 01/31/2019 14:30 SM-4500-NH3C-TKN Total Nitrogen 0.34 3380 250 01/31/2019 14:30 CALCULATION Ammonia Nitrogen 0.03 290 100 ZBD 02/06/2019 10:30 SM-4500-NH3C Organic N 0.31 3090 0.025 CLP 02/18/2019 09:14 CALCULATION Nitrate+Nitrite-N <4.76 4.76 ZBD 02/06/201915:54 4500NO3F-2011 Calcium Carbonate Equivalent 46.10 461000 1000 DXT 01/29/2019 16:00 AOAC 955.01 Total Volatile Solids 50.30 503000 100.0 CJR 01/24/2019 15:44 SM-2540G C/N RATIO' 86 0 01/24/2019 15:44 CALCULATION Carbon (TOC)' 29.20 292000 100 01/24/2019 15:44 CALCULATION Comments: PAN = 2709 mg/kg All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. pll« mC lo"r, Pauric McGroary Agronomist Page 17 of 19 Page 3 of 5 _ aceAnalytical wwwpacelabs.com February 21, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92416938 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on February 07, 2019. The results relate only to the samples included in this report Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, O- q�l Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 11ceAnalXical' www.pacelabs.cwn ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92416938 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Monthly Sludge Lab ID: 92416938001 Collected: 02/07/19 08:00 Received: 02/07/19 09:40 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 02/21/2019 08:30 AM Analytical Method: EPA 601 OD Preparation Method: EPA 3050B ND mg/kg 1.3 0.64 1 02/18/19 09:27 02/19/19 14:27 7440-38-2 159000 mg/kg 1270 635 100 02/18/19 09:27 02/20/19 19:11 7440-70-2 13.2 mg/kg 0.64 0.32 1 02/18/19 09:27 02/19/19 14:27 7440-50-8 1450 mg/kg 12.7 0.32 1 02/18/19 09:27 02/19/19 14:27 7439-95-4 1.1 mg/kg 0.64 0.32 1 02/18/19 09:27 02/19/19 14:27 7440-02-0 67.6 mg/kg 1.3 0.64 1 02/18/19 09:27 02/19/19 14:27 7440-66-6 Analytical Method: SM 254OG-2011 42.3 1 % 0.10 0.000010 1 02/07/1917:16 Analytical Method: ASTM D2974-87 57.7 % 0.10 0.10 1 02/07/1917:06 Analytical Method: EPA 9045D 7.0 Std. Units 0.10 0.10 1 02/18/19 11:35 Analytical Method: SM 271OB-2011 429 mg/kg 0.12 0.12 1 02/18/1911:00 Analytical Method: TKN+NO3+NO2 Calculation 1430 mg/kg 40.0 20.0 1 02/19/1910:53 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 22.7 22.7 1 02/14/1911:06 02/14/1914:19 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1430 mg/kg 103 51.4 1 02/13/19 16:00 02/14/19 00:38 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 4.7 4.7 1 02/09/19 04:09 02/09/19 05:33 ND mg/kg 4.7 4.7 1 02/09/19 04:09 02/09/19 05:33 14797-55-8 ND mg/kg 2.3 2.3 1 02/09/19 04:09 02/09/19 05:33 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. H3 N2 M1 Page 5 of 21 Report Number: 19-043-0219 Account Number: 05734 Waypoint,(D ANALYTICAL Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : 92416938001 ANGELA BAIONI 9800 KINCEYAVENUE SUITE 100 HUNTERSVILLE , NC 28078 Lab Number: 64738 Sample Id : 92416938001 Total Solids Moisture * Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO * Carbon (TOC) Comments: REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 2/7/2019 08:00:00 Date Received: 02/12/2019 00:00 Date Reported: 02/20/2019 42.30 423000 100.0 CJR 02/14/201914:10 SM-2540G 57.70 100.0 CJR 02/14/201914:10 SM-2540G 3.07 30700 250 CLIP 02/19/201912:30 SM-4500-NH3C-TKN 12.90 129000 1000 DXT 02/18/2019 10:20 AOAC 955.01 51.40 514000 100.0 CJR 02/14/201914:10 SM-2540G 10 0 02/14/201914:10 CALCULATION 29.90 299000 100 02/14/201914:10 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pofie' #1 C 1011r" Pauric McGroary Agronomist Page 19 of 21 Page 3 of 5 _ 2ce Analytical www.pacelabs.com March 29, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92420580 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on March 08, 2019. The results relate only to the samples included in this report Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, 1-fr'� Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 aceAnalytical www.pacefabs coin ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pace Project No.: 92420580 Sample: Monthly Sludge Lab ID: 92420580001 Collected: 03/07/19 08:30 Received: 03/08/19 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050E Arsenic ND mg/kg 1.4 0.72 1 03/15/19 16:22 03/21/19 04:15 7440-38-2 Calcium 122000 mg/kg 145 72.4 10 03/15/19 16:22 03/21/1915:57 7440-70-2 Copper 15.3 mg/kg 0.72 0.36 1 03/15/19 16:22 03/21/19 04:15 7440-50-8 Magnesium 1240 mg/kg 14.5 0.36 1 03/15/19 16:22 03/21/19 04:15 7439-95-4 Nickel 1.4 mg/kg 0.72 0.36 1 03/15/19 16:22 03/21/19 04:15 7440-02-0 Zinc 57.9 mg/kg 1.4 0.72 1 03/15/19 16:22 03/21/19 04:15 7440-66-6 254OG Total Percent Solids Analytical Method: SM 254OG-2011 Total Solids 41A % 0.10 0.000010 1 03/08/19 17:22 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 58.9 % 0.10 0.10 1 03/08/19 17:12 9045 pH Soil Analytical Method: EPA 9045D pH at 25 Degrees C 7.1 Std. Units 0.10 0.10 1 03/13/19 22:09 H3 Plant Available Nitrogen Analytical Method: SM 271 OB-2011 Plant Available Nitrogen 687 mg/kg 0.12 0.12 1 03/20/19 16:51 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 2290 mg/kg 40.0 20.0 1 03/26/1915:37 7727-37-9 350A Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Nitrogen, Ammonia ND mg/kg 20.6 20.6 1 03/18/19 15:02 03/19/19 15:01 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 2290 mg/kg 106 52.9 1 03/14/19 02:20 03/14/19 09:08 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg/kg 9.6 4.8 1 03/08/19 22:46 03/09/19 01:24 Nitrogen, Nitrate ND mg/kg 9.6 4.8 1 03/08/19 22:46 03/09/19 01:24 14797-55-8 Nitrogen, Nitrite ND mg/kg 9.6 2.4 1 03/08/19 22:46 03/09/19 01:24 14797-65-0 Date: 03/29/2019 12:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 21 Report Number: 19-071-0204 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Lab Number: 65222 Sample Id : 92420580001 Waypoint(2) ANALYTICAL Project : 92420580001 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 3/7/2019 08:30:00 Date Received: 03/12/2019 00:00 Date Reported: 03/20/2019 Total Solids * 39.90 399000 100.0 CJR 03/14/2019 16:10 SM-2540G Moisture * 60.10 100.0 CJR 03/14/2019 16:10 SM-2540G Total Kjeldahl Nitrogen 0.45 4540 250 CLP 03/18/2019 12:30 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 28.10 281000 1000 DXT 03/19/2019 11:58 AOAC 955.01 Total Volatile Solids 63.10 631000 100.0 CJR 03/14/2019 16:10 SM-2540G C/N RATIO * 81 0 03/14/2019 16:10 CALCULATION Carbon (TOC) * 36.70 367000 100 03/14/2019 16:10 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time I ttiG • / i�c 10441 Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 19 of 21 Page 3 of 5 1�;a'ceAnalXicalo www.pacelabs.com April 23, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: SLUDGE Pace Project No.: 92424617 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on April 09, 2019. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 ace Analytical' www.pacelabs.cwn ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: SLUDGE Pace Project No.: 92424617 Sample: MONTHLY SLUDGE Lab ID: 92424617001 Collected: 04/09/19 09:46 Received: 04/09/19 09:50 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050E Arsenic ND mg/kg 1.5 0.75 1 04/22/19 13:30 04/22/19 23:31 7440-38-2 Calcium 141000 mg/kg 299 149 20 04/22/19 13:30 04/23/1912:52 7440-70-2 M6 Copper 15.2 mg/kg 0.75 0.37 1 04/22/19 13:30 04/22/19 23:31 7440-50-8 Magnesium 1400 mg/kg 14.9 0.37 1 04/22/19 13:30 04/22/19 23:31 7439-95-4 Nickel 1.5 mg/kg 0.75 0.37 1 04/22/19 13:30 04/22/19 23:31 7440-02-0 Zinc 120 mg/kg 1.5 0.75 1 04/22/19 13:30 04/22/19 23:31 7440-66-6 BC, M 1 254OG Total Percent Solids Analytical Method: SM 254OG-2011 Total Solids 42.9 % 0.10 0.000010 1 04/09/19 18:07 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 57.1 % 0.10 0.10 1 04/09/19 18:03 9045 pH Soil Analytical Method: EPA 9045D pH at 25 Degrees C 7.4 Std. Units 0.10 0.10 1 04/22/19 15:28 1-11 Plant Available Nitrogen Analytical Method: SM 271OB-2011 Plant Available Nitrogen 312 mg/kg 0.12 0.12 1 04/22/19 15:58 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1040 mg/kg 40.0 20.0 1 04/22/1917:18 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Nitrogen, Ammonia ND mg/kg 19.4 19.4 1 04/14/19 14:54 04/14/19 16:46 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 1040 mg/kg 66.6 33.3 1 04/16/19 06:29 04/16/19 16:55 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg/kg 9.3 4.6 1 04/10/19 01:09 04/10/19 07:10 Nitrogen, Nitrate ND mg/kg 9.3 4.6 1 04/10/19 01:09 04/10/19 07:10 14797-55-8 Nitrogen, Nitrite ND mg/kg 9.3 2.3 1 04/10/19 01:09 04/10/19 07:10 14797-65-0 Date: 04/23/2019 06:08 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 21 Report Number: 19-102-0201 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Lab Number: 65858 Sample Id : 92424617001 Monthly Sludge Total Solids Moisture * Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO * Carbon (TOC) Comments: Waypoint,(D Project : 92424617001 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 4/9/2019 09:46:00 Date Received: 04/12/2019 00:00 Date Reported: 04/22/2019 42.50 425000 100.0 ADM 04/19/201916:20 SM-2540G 57.50 100.0 ADM 04/19/201916:20 SM-2540G 0.10 965 250 CLP 04/18/201913:30 SM-4500-NH3C-TKN 37.00 370000 1000 DXT 04/19/2019 09:37 AOAC 955.01 55.40 554000 100.0 ADM 04/19/201916:20 SM-254OG 330 0 04/18/201913:30 CALCULATION 32.20 322000 100 04/19/201916:20 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Poficl mC 6ew Pauric McGroary Page 19 of 21 Agronomist Page 3 of 5 acivAnalyticaf wwwpacelabs.com May 23, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92428638 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on May 09, 2019. The results relate only to the samples included in this report Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 acmnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92428638 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Monthly Sludge Lab ID: 92428638001 Collected: 05/09/19 07:20 Received: 05/09/19 08:32 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 05/23/2019 12:19 PM Analytical Method: EPA 6010 Preparation Method: EPA 3050 ND mg/kg 1.2 0.62 1 05/22/19 07:13 05/22/19 13:09 7440-38-2 199000 mg/kg 3080 1540 50 05/22/19 07:13 05/22/19 22:30 7440-70-2 13.7 mg/kg 0.62 0.31 1 05/22/19 07:13 05/22/19 13:09 7440-50-8 1770 mg/kg 61.6 30.8 1 05/22/19 07:13 05/22/19 13:09 7439-95-4 1.2 mg/kg 0.62 0.31 1 05/22/19 07:13 05/22/19 13:09 7440-02-0 48.5 mg/kg 2.5 1.2 1 05/22/19 07:13 05/22/19 13:09 7440-66-6 Analytical Method- SM 2540G-2011 43.6 % 0.10 0.000010 1 05/10/1916:43 Analytical Method: ASTM D2974-87 56.4 % 0.10 0.10 1 05/10/1916:29 Analytical Method: EPA 9045D 8.1 Std. Units 0.10 0.10 1 05/13/19 15:34 H1 Analytical Method: SM 271 OB-2011 396 mg/kg 0.12 0.12 1 05/22/1911:28 N2 Analytical Method: TKN+NO3+NO2 Calculation 1320 mg/kg 40.0 20.0 1 05/21/1914:57 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod ND mg/kg 20.5 20.5 1 05/13/19 23:30 05/14/19 02:57 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1320 mg/kg 115 57.4 1 05/19/1915:08 05/20/1913:16 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 7.9 4.0 1 05/10/1914:02 05/11/1911:15 H1 ND mg/kg 7.9 4.0 1 05/1011914:02 05/11/1911:15 14797-55-8 ND mg/kg 7.9 2.0 1 05/10/1914:02 05/11/1911:15 14797-65-0 H1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC Page 5 of 21 Report Number: 19-133-0202 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Lab Number: 66318 Sample Id : 92428638001 Waypoint(2) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Sludge-92428638001 REPORT OFANALYSIS Date Sampled: 5/9/2019 07:20:00 Date Received: 05/13/2019 00:00 Date Reported: 05/20/2019 Total Solids 43.30 433000 100.0 CJR 05/15/2019 15:11 SM-254OG Moisture' 56.70 100.0 CJR 05/15/2019 15:11 SM-2540G Total Kjeldahl Nitrogen 0.19 1920 250 JPJ 05/17/2019 14:00 SM-4500-NH3C-TKN Calcium Carbonate Equivalent 26.50 265000 1000 DXT 05/17/2019 16:20 AOAC 955.01 Total Volatile Solids 48.30 483000 100.0 CJR 05/15/2019 15:11 SM-2540G C/N RATIO' 150 0 05/15/2019 15:11 CALCULATION Carbon (TOC)' 28.10 281000 100 05/15/2019 15:11 CALCULATION Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 19 of 21 Page 3 of 5 aceAnalXical www.pacelabs.com July 08, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92433055 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on June 13, 2019. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, nn In Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92433055 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Monthly Sludge Lab ID: 92433055001 Collected: 06/11/19 14:30 Received: 06/13/19 09:58 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 07/08/2019 11:38 AM Analytical Method: EPA 6010D Preparation Method: EPA 3050B ND mg/kg 2.1 1.0 1 06/25/19 11:53 06/25/19 23:18 7440-38-2 156000 mg/kg 206 103 10 06/25/19 11:53 06/26/1911:52 7440-70-2 BC 17.5 mg/kg 1.0 0.52 1 06/25/19 11:53 06/25/19 23:18 7440-50-8 1550 mg/kg 20.6 0.52 1 06/25/19 11:53 06/25/19 23:18 7439-95-4 1.5 mg/kg 1.0 0.52 1 06/25/19 11:53 06/25/19 23:18 7440-02-0 92.6 mg/kg 2.1 1.0 1 06/25/19 11:53 06/26/1914:00 7440-66-6 Analytical Method: SM 2540G-2011 43.3 % 0.10 0.000010 1 06/14/1917:17 Analytical Method: ASTM D2974-87 56.7 % 0.10 0.10 1 06/14/1917:09 Analytical Method: EPA9045D 6.9 Std. Units 0.10 0.10 1 06/24/19 14.26 H3 Analytical Method: SM 271 OB-2011 393 mg/kg 0.12 0.12 1 06/24/1914:10 N2 Analytical Method: TKN+NO3+NO2 Calculation 1310 mg/kg 40.0 20.0 1 06/27/1915:56 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 20.3 20.3 1 06/19/19 17:46 06/20/19 00:21 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1310 mg/kg 110 55.0 1 06/18/19 13:41 06/19/19 01:50 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 9.1 4.5 1 06/14/19 02:10 06/14/19 11:19 H1,H2 ND mg/kg 9.1 4.5 1 06/14/19 02:10 06/14/19 11:19 14797-55-8 H1 ND mg/kg 9.1 2.3 1 06/14/19 02:10 06/14/19 11:19 14797-65-0 H1,1-12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 21 Report Number: 19-179-0200 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Lab Number: 66915 Sample Id : 92433055001 Total Solids Moisture * Total Kjeldahl Nitrogen Total Volatile Solids C/N RATIO * Carbon (TOC) Comments: Waypoint(2) ANALYTICAL Project : 92433055001 Sludge REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° fax 804-271-6446 www.waypointanalytical.com Date Sampled: 6/11/2019 14:30:00 Date Received: 06/28/2019 00:00 Date Reported: 07/08/2019 42.70 CJR 07/01/201915:34 SM-254OG 57.30 CJR 07/01/201915:34 SM-2540G 0.35 3490 250 JPJ 07/02/2019 09:00 SM-4500-NH3C-TKN 48.90 CJR 07/01/201915:34 SM-2540G 81 0 07/01/201915:34 CALCULATION 28.40 284000 100 07/01/201915:34 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Page 19 of 21 Agronomist Page 3 of 5 aceAnalytical www.paw1abs.com July 30, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: SLUDGE Pace Project No.: 92437021 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on July 16, 2019. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, nql--s— Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 22 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: SLUDGE Pace Project No.: 92437021 Sample: MONTHLY SLUDGE Lab ID: 92437021001 Collected: 07/15/19 15-15 Received: 07/16/19 08:50 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601OD Preparation Method: EPA3050B Arsenic ND mg/kg 2.3 1.1 1 07/29/19 16:50 07/29/19 20:20 7440-38-2 Calcium 163000 mg/kg 1140 572 50 07/29/19 16:50 07/3011915:31 7440-70-2 Copper 15.9 mg/kg 1.1 0.57 1 07/29/19 16:50 07/29/19 20:20 7440-50-8 Magnesium 1690 mg/kg 22.9 0.57 1 07/29/19 16:50 07/29/19 20:20 7439-95-4 Nickel 1.2 mg/kg 1.1 0.57 1 07/29/19 16:50 07/29/19 20.20 7440-02-0 Zinc 84.2 mg/kg 2.3 1.1 1 07/29/19 16:50 07/29/19 20:20 7440-66-6 254OG Total Percent Solids Analytical Method: SM 2540G-2011 Total Solids 41.2 % 0.10 0.000010 1 07/16/19 17:41 Percent Moisture Analytical Method: ASTM D2974-87 ' Percent Moisture 58.8 % 0.10 0.10 1 07/16/19 17:39 9045 pH Soil Analytical Method: EPA9045D pH at 25 Degrees C 7.1 Std. Units 0.10 010 1 07/22/19 18:28 H3 Plant Available Nitrogen Analytical Method: SM 271OB-2011 Plant Available Nitrogen 570 mg/kg 0.12 0.12 1 07/29/19 17:07 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1900 mg/kg 40.0 20.0 1 07/29/1917:08 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2 0 1993 Mod Nitrogen, Ammonia ND mg/kg 23.3 23.3 1 07/18/19 07:18 07/18/19 12:29 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2 0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 1900 mg/kg 106 52.8 1 07/23/19 05:17 07/25/19 03:37 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg/kg 9.5 4.8 1 07/16/19 22:10 07/17/19 00:13 Nitrogen, Nitrate ND mg/kg 9.5 4.8 1 07/16/19 22:10 07/17/19 00:13 14797-55-8 Nitrogen, Nitrite ND mg/kg 9.5 2.4 1 07/16/19 22:10 07/17/19 00:13 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/30/2019 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 22 Report Number: 19-199-0009 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Lab Number: 67424 Sample Id : 92437021001 Total Solids Moisture * Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO * Carbon (TOC) Comments: WaypRint(DYTICAL Project : 92437021001 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 7/15/2019 15:15:00 Date Received: 07/18/2019 00:00 Date Reported: 07/24/2019 41.00 ADM 07/19/201915:52 SM-254OG 59.00 ADM 07/19/201915:52 SM-2540G 0.50 4980 250 JPJ 07/24/201910:00 SM-4500-NH3C-TKN 35.50 355000 1000 DXT 07/23/2019 06:10 AOAC 955.01 52.60 ADM 07/19/201915:52 SM-2540G 61 0 07/19/201915:52 CALCULATION 30.60 306000 100 07/19/201915:52 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Page 18 of 22 Agronomist Page 2 of 6 1'7,'Ia.c,- eaAnalytical www.pacelabs.com August 27, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92441201 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on August 13, 2019. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 aceAnalytical • "Mpacelaba.corn ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92441201 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Lab ID: 92441201001 Collected: 08/13/19 08:20 Received: 08/13/19 11:40 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 08/27/2019 10:57 AM Analytical Method: EPA 601OD Preparation Method: EPA 3050E ND mg/kg 1.5 0.77 1 08/15/19 00:10 08/16/19 23:43 7440-38-2 170000 mg/kg 307 154 20 08/15/19 00:10 08/17/19 15:12 7440-70-2 15.7 mg/kg 0.77 0.38 1 08/15/19 00:10 08/16/19 23:43 7440-50-8 1360 mg/kg 15.4 0.38 1 08/15/19 00:10 08/16/19 23:43 7439-95-4 1.7 mg/kg 0.77 0.38 1 08/15/19 00:10 08/16/19 23:43 7440-02-0 107 mg/kg 1.5 0.77 1 08/15/19 00:10 08/16/19 23:43 7440-66-6 Analytical Method: SM 254OG-2011 43.4 % 0.10 0.000010 1 08/13/1917:31 Analytical Method: ASTM D2974-87 56.6 % 0.10 0.10 1 08/13/1917:28 Analytical Method: EPA9045D 7.0 Std. Units 0.10 0.10 1 08/19/19 15:27 H3 Analytical Method: SM 271OB-2011 643 mg/kg 0.12 0.12 1 08/26/1915:18 N2 Analytical Method: TKN+NO3+NO2 Calculation 1810 mg/kg 40.0 20.0 1 08/17/1910:56 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 22.6 22.6 1 08/22/19 22:23 08/22/19 23:07 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1810 mg/kg 105 52.4 1 08/14/19 17:29 08/15/19 04:56 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 9.1 4.5 1 08/14/1909:31 08/14/1911:49 M1,R1 ND mg/kg 9.1 4.5 1 08/14/1909:31 08/14/1911:49 14797-55-8 M1,R1 ND mg/kg 9.1 2.3 1 08/14/1909:31 08/14/1911:49 14797-65-0 M1,R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 21 Report Number: 19-227-0009 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Lab Number: 67838 Sample Id : 92441201 Total Solids Moisture * Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO * Carbon (TOC) Comments: Waypoint(D ANALYTICAL Project : 92441201 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 8/13/2019 08:20:00 Date Received: 08/15/2019 00:00 Date Reported: 08/22/2019 44.80 ADM 08/16/201916:20 SM-2540G 55.20 ADM 08/16/201916:20 SM-2540G 0.48 4840 250 JPJ 08/20/201913:00 SM-4500-NH3C-TKN 28.80 288000 1000 DXT 08/22/2019 06:38 AOAC 955.01 52.80 ADM 08/16/201916:20 SM-2540G 63 0 08/16/201916:20 CALCULATION 30.70 307000 100 08/16/201916:20 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Page 19 of 21 Agronomist Page 3 of 5 aceAnalytical www.pacelabs.com September 23, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: SLUDGE Pace Project No.: 92444794 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on September 10, 2019. The results relate only to the samples included in this report_ Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 20 aceAnalytical *W..pacetabs.com { ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: SLUDGE Pace Project No.: 92444794 Sample: SLUDGE Lab ID: 92444794001 Collected: 09/10/19 07:10 Received: 09/10/19 09:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050B Arsenic ND mg/kg 1.4 0.72 1 09/12/1911:15 09/14/1916:55 7440-38-2 Calcium 188000 mg/kg 719 359 50 09/12/19 11:15 09/14/19 23:19 7440-70-2 Copper 24.0 mg/kg 0.72 0.36 1 09/12/1911:15 09/14/1916:55 7440-50-8 Magnesium 1770 mg/kg 14.4 0.36 1 09/12/1911:15 09/14/1916:55 7439-95-4 Nickel 1.1 mg/kg 0.72 0.36 1 09/12/1911:15 09/14/1916:55 7440-02-0 Zinc 65.3 mg/kg 1.4 0.72 1 09/12/1911:15 09/14/1916:55 7440-66-6 254OG Total Percent Solids Analytical Method: SM 254OG-2011 Total Solids 44.0 % 0.10 0.000010 1 09/10/19 16:44 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 56.0 % 0.10 0.10 1 09/10/19 16:37 9045 pH Soil Analytical Method: EPA 9045D pH at 25 Degrees C 6.8 Std. Units 0.10 0.10 1 09/19/19 21:22 Plant Available Nitrogen Analytical Method: SM 271OB-2011 Plant Available Nitrogen 519 mg/kg 0.12 0.12 1 09/23/19 14:14 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 1730 mg/kg 40.0 20.0 1 09/16/1915:18 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Nitrogen, Ammonia ND mg/kg 21.0 21.0 1 09/18/19 23:45 09/19/19 21:35 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 1730 mg/kg 90.9 45.4 1 09/12/19 05:48 09/13/19 04:47 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg/kg 8.8 4.4 1 09/10/19 22:37 09/10/19 23:40 Nitrogen, Nitrate ND mg/kg 8.8 4.4 1 09/10/19 22:37 09/10/19 23:40 14797-55-8 Nitrogen, Nitrite ND mg/kg 8.8 2.2 1 09/10/19 22:37 09/10/19 23:40 14797-65-0 Date: 09/23/2019 02:25 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. H3 I&, Page 5 of 20 Report Number: 19-255-0003 Account Number: 11769 Send To: Pace Analytical Labs Charlotte Tyriek Hooks 9800 Kindey Ave Huntersville , NC 28078 Lab Number: 68174 Sample Id : 92444794001 Total Solids Moisture Total Kjeldahl Nitrogen Calcium Carbonate Equivalent Total Volatile Solids C/N RATIO Carbon (TOC) Comments: Waypoint,(2) ANALYTICAL Project : 92444794001 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 9/10/2019 07:10:00 Date Received: 09/12/2019 00:00 Date Reported: 09/19/2019 45.30 ADM 09/13/201916:17 SM-2540G 54.70 ADM 09/13/201916:17 SM-254OG 0.30 2980 250 JPJ 09/18/201912:30 SM-4500-NH3C-TKN 57.40 574000 1000 DXT 09/18/2019 15:02 AOAC 955.01 50.80 ADM 09/13/201916:17 SM-2540G 99 0 09/13/201916:17 CALCULATION 29.50 295000 100 09/13/201916:17 CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results. or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization. ?oft` mC Pauric McGroary Page 18 of 20 Agronomist Page 3 of 5 aceAnalytical www.pacelabs.com October 24, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 RE: Project: Sludge Monthly Testing Pace Project No.: 92449220 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on October 10, 2019. The results relate only to the samples included in this report Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 23 aceAnalytical 1 www.parelabs.corn ANALYTICAL RESULTS Project: Sludge Monthly Testing Pace Project No.: 92449220 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Monthly Testing Lab ID: 92449220001 Collected: 10/10/19 07:25 Received: 10/10/19 12:00 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 10/24/2019 04:43 PM Analytical Method: EPA 601 OD Preparation Method: EPA 3050E ND mg/kg 2.2 1.1 1 10/15/19 12:07 10/18/19 01:33 7440-38-2 193000 mg/kg 223 112 10 10/15/19 12:07 10/18/19 20:10 7440-70-2 18.1 mg/kg 1.1 0.56 1 10/15/19 12:07 10/18/19 01:33 7440-50-8 1790 mg/kg 22.3 0.56 1 10/15/19 12:07 10/18/19 01:33 7439-95-4 1.5 mg/kg 1.1 0.56 1 10/15/19 12:07 10/18/19 01:33 7440-02-0 76.0 mg/kg 2.2 1.1 1 10/15/19 12:07 10/18/19 01:33 7440-66-6 Analytical Method: SM 254OG-2011 40.0 % 0.10 0.000010 1 10/10/1918:49 Analytical Method: ASTM D2974-87 60.0 % 0.10 0.10 1 10/10/1918:45 Analytical Method: EPA 9045D 6.9 Std. Units 0.10 0.10 1 10/21/19 15:45 H2 Analytical Method: SM 271OB-2011 588 mg/kg 0.12 0.12 1 10/22/19 08:41 N2 Analytical Method: TKN+NO3+NO2 Calculation 1960 mg/kg 40.0 20.0 1 10/21/1915:58 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 18.6 18.6 1 10/18/19 08:46 10/18/19 11:48 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1960 mg/kg 92.5 46.3 1 10/11/19 23:50 10/13/19 11:52 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 9.8 4.9 1 10/10/19 22:33 10/10/19 23:42 ND mg/kg 9.8 4.9 1 10/10/19 22:33 10/10/19 23:42 14797-55-8 M1 ND mg/kg 9.8 2.5 1 10/10/19 22:33 10/10/19 23:42 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 23 s P �' �� 7621 Whitepine Road, Richmond, VA 23237 Way Main 804-743-9401 ° fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 11769 Pace Analytical Labs Charlotte Tyriek Hooks Project 92449220001 Report Date : 10/23/2019 9800 Kindey Ave Information : Received : 10/15/2019 Huntersville , NC 28078 Pam•« m` (fet'�' Report Number :19-288-0006 REPORT OFANAL YSIS Pauric McGroary Agronomist Lab No : 68591 Matrix: Solids Sample ID : 92449220001 Sampled: 10/10/2019 7:25 Moisture 56.0 % 0.010 1 10/16/19 16:56 ADM SM-2540G Total Solids 44.0 % 0.010 1 10/16/19 16:56 ADM SM-2540G Total Kjeldahl Nitrogen 0.681 % - dry 0.056 1 10/21/19 09:00 JPJ ;M-4500-NH3C-TKP Calcium Carbonate Equivalent 55.3 % - dry 0.1 1 10/22/19 15:15 DXT AOAC 955.01 Total Volatile Solids 49.1 % 0.010 1 10/16/19 16:56 ADM SM-2540G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Carbon (TOC) 28.5 % 0.010 1 10/16/19 16:56 CALCULATION C/N RATIO 42 Ratio 0 1 10/16/19 16:56 CALCULATION Qualifiers/ B Analyte detected in blank Definitions H Beyond holding time Page 3 of 5 Page 21 of 23 /�;a'cieAnalXical www.pacelabs.com 1 i December 05, 2019 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Sludge Pace Project No.: 92452957 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on November 07, 2019. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Sludge Pace Project No.: 92452957 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Samples Lab ID: 92452957001 Collected: 11/07/19 09:20 Received: 11/07/19 15:20 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Calcium Copper Magnesium Nickel Zinc 254OG Total Percent Solids Total Solids Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 12/05/2019 04:54 PM Analytical Method: EPA 601 OD Preparation Method: EPA 3050B ND mg/kg 1.7 0.85 1 11/13/1913:50 11/15/1911:13 7440-38-2 169000 mg/kg 851 426 50 11/13/1913:50 11117/1919:34 7440-70-2 17.6 mg/kg 0.85 0.43 1 11/1311913:50 11/15/1911:13 7440-50-8 1600 mg/kg 17.0 0.43 1 11/13/1913:50 11/15/1911:13 7439-95-4 6.2 mg/kg 0.85 0.43 1 11/13/1913:50 11/15/1911:13 7440-02-0 81.7 mg/kg 1.7 0.85 1 11/13/1913:50 11/15/1911:13 7440-66-6 Analytical Method: SM 2540G-2011 45.2 % 0.10 0.000010 1 11/08/1914:22 Analytical Method: ASTM D2974-87 54.8 % 0.10 0.10 1 11/08/1914:15 Analytical Method: EPA9045D 6.9 Std. Units 0.10 0.10 1 11/26/19 10:48 H3 Analytical Method: SM 271OB-2011 420 mg/kg 0.12 0.12 1 11/20/1911:44 N2 Analytical Method: TKN+NO3+NO2 Calculation 1400 mg/kg 40.0 20.0 1 11/20/1911:57 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 22.1 22.1 1 11/12/19 16:15 11/12/19 22:34 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1400 mg/kg 96.2 48.1 1 11/19/19 15:10 11/20/19 02:59 7727-37-9 R1 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 8.6 4.3 1 11/08/19 22:18 11/08/19 23:35 M1 ND mg/kg 8.6 4.3 1 11/08/19 22:18 11/08/19 23:35 14797-55-8 ND mg/kg 8.6 2.2 1 11/08/19 22:18 11/08/19 23:35 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 21 • WayPAoint. NALYTICAL 11769 Pace Analytical Labs Charlotte 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Original Report Date : 11/19/2019 Tyriek Hooks Project 92452957001 Revised Report Date: 12/05/2019 9800 Kindey Ave Information : Received : 11/11/2019 Huntersville , NC 28078 Report Number :19-315-9004 REPORTOFANALYSIS Lab No : 69547 Matrix: Solids Sample ID : 92452957001 Sampled: 11/7/2019 9:20 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 54.7 % 0.010 1 11/13/19 17:03 ADM SM-2540G Calcium Carbonate Equivalent 48.5 % - dry 0.1 1 11/18/19 13:12 DXT AOAC 955.01 C/N RATIO 51.50 Ratio 0 1 11/13/19 17:03 CALCULATION Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Solids 45.3 % 0.010 1 11/13/19 17:03 ADM SM-2540G Total Volatile Solids 47.3 % 0.010 1 11/13/19 17:03 ADM SM-2540G Total Kjeldahl Nitrogen 5340 mg/Kg - dry 552 1 11/15/19 12:00 JPJ iM-4500-NH3C-TKP Carbon (TOC) 27.5 % 0.010 1 11/13/19 17:03 JM CALCULATION Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 19 of 21 Page 3 of 5 _. ;acie Analytical www.pacelabs.com January 14, 2020 Ms. Karen Bellamy Cascades Tissue Group -NC 805 Midway Road PO Box 578 Rockingham, NC 28380 RE: Project: Monthly Pace Project No.: 92456771 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Ms. Bellamy: Enclosed are the analytical results for sample(s) received by the laboratory on December 10, 2019. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Accounts Payable, Cascades Tissue Group -NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 23 aceAnalytical www.pacolabs.com ANALYTICAL RESULTS Project: Monthly Pace Project No.: 92456771 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Samples Lab ID: 92456771001 Collected: 12/10/19 08:33 Received: 12/10/19 13:22 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA6010D Preparation Method: EPA3050B Arsenic ND mg/kg 2.1 1.1 1 12/11/19 11:17 12/12/19 23:31 7440-38-2 Calcium 159000 mg/kg 211 105 10 12/11/19 11:17 12/13/1919:22 7440-70-2 Copper 16.2 mg/kg 1.1 0.53 1 12/11/19 11:17 12/12/19 23:31 7440-50-8 Magnesium 1620 mg/kg 21.1 0.53 1 12/11/19 11:17 12/12/19 23:31 7439-95-4 Nickel 11.8 mg/kg 1.1 0.53 1 12/11/19 11:17 12/12/19 23:31 7440-02-0 Zinc 61.8 mg/kg 2.1 1.1 1 12/11/19 11:17 12/12/19 23:31 7440-66-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 55.2 % 0.10 0.10 1 12/10/19 17-n3 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Total Nitrogen Calculation Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 363.2 Nitrogen, NO2/NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite Date: 01 /14/2020 11:33 AM Analytical Method: EPA 9045D 7.3 Std. Units 0.10 0.10 1 01/06/20 12:06 Analytical Method: SM 271OB-2011 459 mg/kg 0.12 0.12 1 12/17/1915:27 Analytical Method: TKN+NO3+NO2 Calculation 1530 mg/kg 40.0 20.0 1 12/13/1913:34 7727-37-9 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. ND mg/kg 21.9 21.9 1 12/17/19 09:57 12/17/19 13:53 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 1530 mg/kg 101 50.7 1 12/12/19 05:28 12/13/19 07:45 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 ND mg/kg 8.8 4.4 1 12/10/19 22:20 12/10/19 23:47 ND mg/kg 8.8 4.4 1 12/10/19 22:20 12/10/19 23:47 14797-55-8 ND mg/kg 8.8 2.2 1 12/10/19 22:20 12/10/19 23:47 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. H3 IPA Page 5 of 23 WayPAaint. • NALYTICAL 16254 Pace Analytical Sevices, Inc. -Carolinas 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Original Report Date : 12/26/2019 Mr. Craig Griffin Project Monthly Revised Report Date: 01/13/2020 9800 Kincey Ave Information : Workorder# 92456771 Received : 12/12/2019 Suite 100 Huntersville , NC 28078 Report Number :19-346-0054 REPORT OFANAL YSIS Lab No : 98658 Sample ID: Samples Matrix: Solids Sampled: 12/10/2019 8:33 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Total Volatile Solids 49.4 H % 0.010 1 01/10/20 17:42 ADM 2540G-2011 C/N RATIO 27 Ratio 0 1 01/01/00 00:00 CALCULATION — Neutralizing Value (%CCE) 49.7 % - dry 0.1 1 12/17/19 09:33 DXT AOAC 955.01 Carbon, Total 27.8 % 0.10 1 01/01/00 00:00 PMW LECO Total Organic Carbon 6.51 % 0.05 1 12/20/19 14:49 DXT WALK -BLACK Total N (Inorg+Org) <0.01 % 0.01 1 01/01/00 00:00 PMW LECO Qualifiers/ DF Dilution Factor H Beyond holding time Definitions L Limit Exceeded MQL Method Quantitation Limit Page 18 of 23 Page 4 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Quality Control Data Client ID: Pace Analytical Sevices, Inc. -Carolinas Project Description: Monthly Report No: 19-346-0054 QC Analytical Batch: L472403 Analysis Method: 2540G-2011 Analysis Description: Total, Fixed, and Volatile Solids Duplicate L 98658-DUP Result DUP RPD Max RPD Analyzed Parameter Units Result Total Volatile Solids % 49.4 49.3 0.2 15.0 01/10/20 17:42 Date: 01/13/2020 04:54 PM Pa9ePage f P 3 Page 5 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Quality Control Data Client ID: Pace Analytical Sevices, Inc. -Carolinas Project Description: Monthly Report No: 19-346-0054 QC Analytical Batch: L469167 Analysis Method: AOAC 955.01 Analysis Description: Neutralizing Value (%CCE) Duplicate E 69879-DUP Result DUP RPD Max RPD Analyzed Parameter Units Result Neutralizing Value (%CCE) % - dry 15.9 14.9 6.4 10.0 12/17/19 09:33 Date: 01/13/2020 04:54 PM PagPPage z 13 Page 6 of 9 SUMM111- Surrrnrit Environmental Technologies, Inc. 3310 Win St. ciiENVInON1AENTAL rECHNOLOGIBS, INC Cuyahoga Falls, Ohio 44223 AnaVical Laboratorles . TEL: (330) 253-8211 FAX. • (330) 253-4489 Website: http:/hvwtv.settek.com May 08, 2019 Karen Bellamy Cascades Tissue Group - North Carolina Inc 805 Midway Road Rockingham, NC 28379 TEL: 910-895-4033 FAX: 910-895-9887 RE: Waste Characterization Dear Karen Bellamy: Order No.: 19041884 Summit Environmental Technologies, Inc. received 1 sample(s) on 4/26/2019 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, =01 Holly Florea Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington C891 Page 1 of 35 Page 1 of 36 Inc S U M M I T Summit Environmental Technologies, 3310 Win StSt. Case Narrative . ENVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 44223 WO#: 19041884 Analytical Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 Website: hity.lAvwiv.settek.com Date: 5/8/2019 CLIENT: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization WorkOrder Narrative: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program Analytes Report" for accredited analytes list. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 19041884-001A MTL-TCLP-7(60 I OD): The following CCV exhibited a high recovery for lead, but the sample was non -detect. Therefore, the concentration of lead in the sample can be accepted. 19041884-001a tclp-SVOC-Herb_npw(8151): Low surrogate recovery likely due to excessive water in the extract (high humidity in extraction lab). Results could be biased accordingly. 19041884-001 a tclp-svoc-CPEST(8081 B): CCV exhibits high recovery for 4,4'-DDT and Methoxychlor. All reported samples are ND. Original Page 2 of 35 Page 2 of 36 Summit Environmental Technologies, Inc. prSUMMINt 3310 Win St. ENVIRONIVIENTAL TECHNOLAGIt S, INC Cuyahoga Falls, Ohio 44223 Analytical Laboralories TEL: (330) 253-8211 FAX.- (330) 253-4489 Websile: hgp.-1AvmP.settek.coni CLIENT: Cascades Tissue Group - North Carolina Inc Project: Waste Characterization Workorder Sample Summary WO#: 19041884 08-May-19 Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 19041884-001 Sludge 4/22/2019 6:10:00 AM 4/26/2019 2:44:00 PM Sludge Page 3 of 35 Page 3 of 36 Suuunit Environmental Technologies, Inc. Mzylooq SUMM111- 3310 Win St. ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Analytical Laboratories TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htto://wiviv.seuek.com WO#: 19041884 Date Reported: 5/8/2019 Company: Cascades Tissue Group - North Carolina I Address: 805 Midway Road Rockingham NC 28379 Received: 4/26/2019 Project#: Waste Characteri TCLP Metals Analysis (SW1311/6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 4/22/2019 TCLP Arsenic(As) 1.25 ND mg/L Sludge EPA 6010 1 5.00 5/1/2019 KMO D Sludge 001 4/22/2019 TCLP Barium(Ba) 12.5 ND mg/L Sludge EPA 6010 1 100 5/1/2019 KMO D Sludge 001 4/22/2019 TCLP Cadmium(Cd) 0.250 ND mg/L Sludge EPA 6010 1 1.00 5/1/2019 KMO D Sludge 001 4/22/2019 TCLP Chromium(Cr) 0.500 ND mg/L Sludge EPA 6010 1 5.00 5/1/2019 KMO D Sludge 001 4/22/2019 TCLP Lead(Pb) 1.25 ND mg/L Sludge EPA 6010 1 5.00 5/1/2019 KMO D Sludge 001 4/22/2019 TCLP Selenium(Se) 0.125 ND mg/L Sludge EPA 6010 1 1.00 5/1/2019 KMO D Sludge 001 4/22/2019 TCLP Silver(Ag) 1.25 ND mg/L Sludge EPA 6010 1 5.00 5/1/2019 KMO D TCLP Mercury Analysis (SW1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 4/22/2019 TCLP Mercury 0.00500 ND mg/L Sludge EPA 7470 A 1 0.200 5/1/2019 DNS TCLP Pesticides Analysis (SW1311/8081) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 4/22/2019 Chlordane, total 0.0250 ND mg/L Sludge EPA 8081 B 10 0.0300 5/4/2019 MES Sludge 001 4/22/2019 Toxaphene 0.0500 ND mg/L Sludge EPA 8081B 10 0.500 5/4/2019 MES Sludge 001 4/22/2019 Endrin 0.00500 ND mg/L Sludge EPA 8081B 10 0.0200 5/4/2019 MES Sludge 001 4/22/2019 gamma-BHC 0.00500 ND mg/L Sludge EPA 8081B 10 0.400 5/4/2019 MES Sludge 001 4/22/2019 Heptachlor 0.00500 ND mg/L Sludge EPA 8081B 10 0.00800 5/4/2019 MES Sludge 001 4/22/2019 Heptachlor epoxide 0.00500 ND mg/L Sludge EPA 8081E 10 0.00800 5/4/2019 MES Sludge 001 4/22/2019 Methoxychlor 0.00500 ND mg/L Sludge EPA 8081E 10 10.0 5/4/2019 MES Sludge 001 4/22/2019 Surr: TCMX 10-119 66.1 %Rec Sludge EPA 8081 B 10 5/4/2019 MES Sludge 001 4/22/2019 Surr:DCB 10-119 89.7 %Rec Sludge EPA 8081B 10 5/4/2019 MES SVOC SW-846: 8151 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 4/22/2019 2,4-D 0.0100 ND mg/L Sludge EPA 8151 1 10.0 5/3/2019 MES A Sludge 001 4/22/2019 2,4,5-TP 0.00500 ND mg/L Sludge EPA 8151 1 1.00 5/3/2019 MES A ludge 001 4/22/2019 Surr: DCAA 20-140 16.4 %Rec Sludge EPA 8151 1 5/3/2019 MES A Pa§m4 of 36 INI Environmental Technologies, Inc. 3310 Win St. WO#: 19041884 TSUMMSummit ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Date Reported: 5/8/2019 AnalyrIcai Lnbornforios TEL: (330) 253-8211 FAX. (330) 253-4489 Company: Cascades Tissue Group - North Carolina I Website: hno://iviviv.settek.coln Address: 805 Midway Road Rockingham NC 28379 Received: 4/26/2019 Project#: Waste Characteri TCLP Volatiles Analysis Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 4/22/2019 1,1-Dichloroethene 0.250 ND mg/L Sludge 001 4/22/2019 1,2-Dichloroethane 0.250 ND mg/L Sludge 001 4/22/2019 MEK 5.00 ND mg/L Sludge 001 4/22/2019 Benzene 0.250 ND mg/L Sludge 001 4/22/2019 Carbon tetrachloride 0.250 ND mg/L Sludge 001 4/22/2019 Chlorobenzene 2.50 ND mg/L Sludge 001 4/22/2019 Chloroform 0.250 ND mg/L Sludge 001 4/22/2019 Tetrachloroethene 0.250 ND mg/L Sludge 001 4/22/2019 Trichloroethene 0.250 ND mg/L Sludge 001 4/22/2019 Vinyl chloride 0.100 ND mg/L Sludge 001 4/22/2019 Surr:4- 70-130 99.0 %Rec Bromofluorobenzene Sludge 001 4/22/2019 Surr: 70-130 91.3 %Rec Dibromofluoromethane ludge 001 4/22/2019 Surr: Toluene-d8 70-130 99.6 %Rec Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 Sludge EPA 8260D 50 TCLP Semi-Volatiles Analysis (SW1311/8270) 0.700 4/30/2019 CTB 0.500 4/30/2019 CTB 200 4/30/2019 CTB 0.500 4/30/2019 CTB 0.500 4/30/2019 CTB 100 4/30/2019 CTB 6.00 4/30/2019 CTB 0.700 4/30/2019 CTB 0.500 4/30/2019 CTB 0.200 4/30/2019 CTB 4/30/2019 CTB 4/30/2019 CTB 4/30/2019 CTB Client ID# Lab ID# Collected Analyte Rep Lunt Result Units Matrix Method DF RegLvl Run Analyst Sludge 001 4/22/2019 IA-Dichlorobenzene 0.0800 ND mg/L Sludge 001 4/22/2019 2,4,5-Trichlorophenol 0.200 ND mg/L Sludge 001 4/22/2019 2,4,6-Trichlorophenol 0.200 ND mg/L Sludge 001 4/22/2019 2,4-Dinitrotoluene 0.0400 ND mg/L Sludge 001 4/22/2019 Cresols, Total 4.00 ND mg/L Sludge 001 4/22/2019 Hexachloro-1,3- 0.0160 ND mg/L butadiene Sludge 001 4/22/2019 Hexachlorobenzene 0.0400 ND mg/L Sludge 001 4/22/2019 Hexachloroethane 0.0800 ND mg/L Sludge 001 4/22/2019 Nitrobenzene 0.0800 ND mg/L Sludge 001 4/22/2019 Pentachlorophenol 0.200 ND mg/L Sludge 001 4/22/2019 Pyridine 0.200 ND mg/L Sludge 001 4/22/2019 Surr:2-Fluorophenol 10-109 54.5 %Rec Sludge 001 4/22/2019 Surr: Phenol-d6 10-109 64.3 %Rec Sludge 001 4/22/2019 Surr: Nitrobenzene- 19-120 56.9 %Rec d5 Sludge 001 4/22/2019 Surr:2,4,6- 10-120 82.8 %Rec Tribromophenol Sludge 001 4/22/2019 Surr: 2- 22-117 56.9 %Rec Fluorobiphenyl Sludge 001 4/22/2019 Surr: p-Terphenyl- 34-116 87.0 %Rec d14 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 Sludge EPA 8270E 2 7.50 5/1/2019 BJH 400 5/1/2019 BJH 2.00 5/1/2019 BJH 0.130 5/1/2019 BJH 200 5/1/2019 BJH 0.500 5/1/2019 BJH 0.130 5/1/2019 BJH 3.00 5/1/2019 BJH 2.00 5/1/2019 BJH 100 5/1/2019 BJH 5.00 5/1/2019 BJH 5/1/2019 BJH 5/1/2019 BJH 5/1/2019 BJH 5/1/2019 BJH 5/1/2019 BJH 5/1/2019 BJH Suulntif Environmental Technologies, Inc. frSUMMIT3310 Win St. Analytical Report ENVIRONMENTAL TECHNOLOGIFS, INC Cuyahoga Falls, Ohio 44223 (consolidated) Analytical Laboratories TEL: (330) 253-821 / FAX: (330) 253-4489 WO#: 19041884 Websile: huy.lAvivtv.settek.com Date Reported: 5/8/2019 CLIENT: Cascades Tissue Group - North Carolina Inc Collection Date: 4/22/2019 6:10:00 AM Project: Waste Characterization Lab ID: 19041884-001 Matrix: SLUDGE Client Sample ID Sludge Analyses Result PQL Qual Units DF Date Analyzed RCI-SOLID-W/ IGNITABILITY1030 SW9014 Analyst: MS REACTIVE CYANIDE (9014/7.3.3.2)-SOLID Cyanide, Reactive ND 0.495 mg/Kg 1 4/30/2019 5:20:00 PM RCI-SOLID-W/ IGNITABILITY1030 SW1030 Analyst: AJT IGNITABILITY OF SOLIDS (SW-846: 1030) Ignitability non-flammable 1 4/30/2019 1:00:00 PM RCI-SOLID-W/ IGNITABILITY1030 SW9046D Analyst: DHC PH (SW9045D) pH 7.2 s.u.@20.7C 1 5/3/2019 10:55:00 AM RCI-SOLID-W/ IGNITABILITY1030 SW9034 Analyst: MS REACTIVE SULFIDE (9034)/7.3.4.2 Sulfide, Reactive ND 25.0 mg/Kg 1 4/30/2019 5:20:00 PM Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response ND Not Detected PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit W Sample container temperature is out of littct as specified at testcode Original Page 6 of 35 Page 6 of 36 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. WQ Permit Number: WWTP Name: NPDES Number: WQ0009477 Monitoring Period: From 1/1/2019 To 12/31/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ElPasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion ❑ Anaerobic obic ' Dr e ' g soon If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density Number of Frequency 4 y Sample p na ytica in Sludge Excee- of Analysis Type Tech - Minimum Geo. Mean Maximum Units dences ni oue 2 x 10 to the MPN N/A N/A 6th power Fecal Coliform per gram of total solids CFU N/A N/A 1000 mpn per gram of total solid (dry N/A N/A weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry N/A C N/A coliform) weight) vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization [:I Alt 7 (Drying - Stable) ElAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) �/ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector 0.attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Karen V. Bellamy Environmental Manager Duke Goodwi roject Manager Preparer Naqfeand Ti tl ( p r print) Land Applie a d Title (if applicable)(type or pri ) 7 7c� Signature f Preparer* Date Signature of, Land Applier (if applicable) D to *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF sns (19/9nnFn (W Cascades Date: Feb 18, 2020 Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc. 805 Midway Road, Post Office Box 578 Rockingham, NC 28380 USA Phone: (910) 895-4033 Fax: (910) 895-9887 From: Karen Bellamy Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc. Po Box 578 805 Midway Rd. Rockingham, NC 28380 Phone 1-910-895-4033-Ext 74280 Fax 1-910-895-9887 Email: Karen BeIlamy(D.Cascades. com Permit: WQ0009477 Subject: Fecal Testing Cascades Material is a lime material, so we don't perform vector reduction. Should your office have any question please contact me at the above numbers or email. Karen V. Bellamy Environmental Manager Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.