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WQ0001346_Residual Annual Report 2019_20200224
February 18, 2020 North Carolina Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: City of Monroe 2019 Land Application Annual Report Permit No: WQ00013463 Monroe North Carolina FEB 2 4 2020 DV"j SEGT!ON 1'NF0Rt-.1A7I0N PROCESSING UNIT City of Monroe personnel performed application events during 2019 on the permitted fields for the City of Monroe. A total of 6,386 Cubic Yards for a total of 1,918 dry tons of residual solids from the City of Monroe Wastewater and Water Treatment Facilities were land applied. If any further information is required regarding this land application report, please do not hesitate to contact Mr. Kyle Ketchum (704) 282-4612 or Steve Holden (704) 282-4679 with the City of Monroe. Sincerely, Russell Colbath, P.E. Director of Water Resources C: I: 8040 WWTP and Collection\ Land Application\2019\ annual report City, of Monroe • PO Box 69 • Monroe, NC 28111-0069 Tel: (704) 282-4500 • Fax: (704) 283-9098 www.monroenc.org -ram w FE8 "I on, -roe North Carolina RESIDUALS LAND APPLICATION PROGRAM CITY OF MONROE ANNUAL REPORT 2019 PERMIT NUMBER WQ0001346 E1VED!NCDEQ�DwR SEC FEB ;; � 2020 �on_plscn unit n9 Monroe North Carolina City of Monroe Water & Wastewater Residuals Land Application Program 2019 Annual Report Table of Contents 1. Certification Form & Annual Operations Summary 2. Annual Residual Sampling Summary Forms & Biosolids Analysis 3. TCLP Analysis 4. Field Summary Forms 5. Pathogen Reduction & Vector Attraction Reduction 6. Soil Analysis ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001346 County: Union Year: 2019 Facility Name (as shown on permit): Land Application Operator: City of Monroe Steve Holden, Land Residual Coordinator Phone: 704-282-4679 Land application of residuals as allowed by the permit occurred during the past calendar year? ❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary. Total number of application fields in thepermit: 35 Total number of fields utilized for land application during the year: 23 Total amount of dry tons applied during the year for all application sites: 1,918 Total number of acres utilizes for land application during the year: 1301.6 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Russell Colbath, P.E., Water Res. Director 7 • �$ Permittee Name and Title (type or print) Signature of Permittee Date O .111 ✓ li�-- %%31)oio -AO- Signature of Preparer* Date Signature of LannI Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) OPERATION SUMMARY Permit # W00001346 FIELDS USED IN 2019 NAME NO. GALS GALS YARDS YARDS DryTons Dry Tons PAN (lbs/ac) Calvin Morris ov 11.6 217 39.47 85.19 en 1 44. 54 Myers 732 135.00 68.37 NC-UN-18 225 40.94 22.98 119Nov 126 32.16 9.90 2 27.6 375 68.23 61.88 75 19.13 9.52 50 9.11 8.25 ov 2b 6,38 3.17 7-Jun 5.7 100 62.4073.32 19-Jun 42 5.4 4. -32 Wayne ep 6.7 117 21.58 72.75 McBride 3 19-Sep 14.6 225 41.49 64.20 19-Sep 75 11.24 merson9-Aug 16.4 75 113.83 . 5 McBride 19-Aug 120 27.58 16.83 NC-UN-26 19-Sep 19-Sep 14 2.57 3.56 39 8.97 5.47 2 19-Aug 6.5 114 21.03 73.06 19-Aug 14 3.22 4.95 3 19-Aug 11.3 175 32.27 64.51 19-Aug 84 19.31 17.20 4 19-Aug 25.6 259 47.77 42.15 6 19-Jul 14 256 47.22 76.17 u 5 William 1 - ay 4. 7. 19.33 51.18 Griffin 19-May 148 11.74 NC-UN-29 2 19-May 5.7 117 73.01 85.79 - pr 7.4 15'3 9b.46.4 om - ov 3.1 225 40.92 7 . Appenzeller 19-Nov 84 21.43 22.47 Henry ay 2.5 53 33.07 88.61 Myers 4 19-Jun 4.7 100 62.41 88.93 NC-UN-31 19-Jun 42 5.48 9.49 5 19-Apr 17.6 195 121.68 46.31 19-May 78 48.68 18.52 19-Sep 50 9.22 11.83 19-Sep 225 51.72 29.401 6 19-Apr 7.8 78 48.68 41.8 ep 75 17.25 22.11 Danny ay 19-May 15.5 190 118.5851.23 Baker 100 13.05 12.54 NC-UN-32 3 19-May 10 217 135.42 90.69 19-May 42 5.48 8.16 4 f PTa-y- 5 7 e un er ur 1- u 5 7 .5 7.4 NG-UN-33]E_�_ Totals WWTP- Metric Tons 1462.00 WTP- Metric Tons 277.72 Total Metric Tons 1739.73 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF B WQ Permit Number: WQ0001346 Facility Name: City of Monroe Residual Source WQ # or NCO024333 NPDES #: WWTP Name: Monroe WWTP (cake) Dav; iial A»olveie na*a Laboratory: 1) Contract Labs 2) 3) 4) 5) Parameter (mpg) Ceiling Conc. Limit Sample or Composite Date 1-8-19 4-1-19 7-1-19 10-1-19 Percent Solids (%) NA 14.2 74.1 21.9 21.6 Arsenic 75 8.77 9.75 10:9 < 23.1 Cadmium 85 1.16 1.01 < 1 < 4.63 Copper 4,300 331 268 304 293 Chromium NA 117 133 133 105 Lead 840 13.8 15.4 14.9 14.7 Mercury 57 0.202 0.162 0.199 0.528 Molybdenum 75 21.9 17.9 24 24.1 Nickel 420 53 66.3 58.2 77.8 Selenium 100 < 5.0 < 5.0 < 5.0 < 23.1 Zinc 7,500 719 565 704 750 Total Phosphorus NA 14200 14100 14200 17200 TKN NA 48900 10300 35200 38300 Ammonia -Nitrogen NA 6550 1270 3560 5090 Nitrate and Nitrite NA 40.8 < 4.66 21.2 9.68 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the -possibility of fines and imprisonment for knowing violations." 14 lw' 01%0}0 Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001346 Facility Name: Residual Source NPDES # or WQ#: WWTP Name: -Dna. lnol Anahreie Vfia+cs City of Monroe NCO024333 Monroe WWTP (cake) Laboratory: 1) 2) 3) 4) 5) Contract Labs Parameter (mg/kg)1-8-19 Sample or Composite Date 4-1-19 7-1-19 10-1-19 Potassium 1090 1020 1070 1170 Sulfur 7650 7420 7830 8800 Calcium 10600 8470 10200 12200 Magnesium 1620 1560 1450 2100 Sodium 731 447 555 < 1160 Iron 274000 113000 149000 120000 Aluminum 8030 10100 8180 9770 Manganese 1130 1270 1450 1800 Organic N 42350 9030 31640 33200 pH ( standard units) 7 7.6 7 7.2 Volitile Solids % 50.6 3.37 53.4 50.4 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001346 Laboratory: 1) Contract Labs Facility Name: City of Monroe 2) Residual Source WQ # or NCO024333 3) NPDES #: 4) WWTP Name: Monroe WTP (cake) 5) 1 .a.Anol Anolveie Yla+a Parameter (mg/kg) Ceiling Conc. Limit Sample or Composite Date 1-8-19 4-1-19 7-1-19 10-1-19 Percent Solids (%) NA 17 15.5 27.3 30.3 Arsenic 75 12 29.6 13.3 53.5 Cadmium 85 3.55 < 5.0. 1.27 < 3.30 Copper 4,300 479 491 308 337 Chromium NA 225 250 197 217 Lead 840 6.16 < 15.0 3.2 < 9.90 Mercury 57 0.0524 0.0524 0.0165 < .0524 . Molybdenum 75 39.7 43.5 37.4 52.1 Nickel 420 44.5 53.5 36 39.9 Selenium 100 < 5.0 < 25 < 25 < 16.5 Zinc 7,500 155 89.1 196 252 Total Phosphorus NA 3710 2670 2210 1640 TKN NA 21900 18100 12300 16900 Ammonia -Nitrogen NA 1120 903 769 1020 Nitrate and Nitrite NA 73.5 112 < 4.58 < 3.30 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." lylot- Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0001346 Facility Name: City of Monroe Residual Source NCO024333 NPDES # or WQ#: WWTP Name: Monroe WTP (cake) Racirinai Analvcic data Laboratory: 1) 2) 3) 4) 5) Contract Labs Parameter (mg/kg)1-8-19 Sample or Composite Date 4-1-19 7-1-19 10-1-19 Potassium 315 304 301 366 Sulfur 2250 2400 2880 2520 Calcium 2070 2060 3140 2300 Magnesium 539 524 470 538 Sodium 610 < 1250 368 < 825 Iron 358000 368000 295000 333000 Aluminum 6220 7600 2840 3930 Manganese 360 498 715 1080 Organic N 20780 17197 11531 15900 pH ( standard units) 5.4 5.9 5.9 6 Volitile Solids % 29.8 28.5 — 41.7 40.8 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) City of Monroe Reports of Lab Analysis I St 90 Days Report Number: 19-009-0217 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 64360 Sample Id : RAS Total Solids' Moisture ` Total Volatile Solids Comments: Waypoint(D ANALYTICAL Project : RAS REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/8/2019 09:58:00 Date Received: 01/09/2019 00:00 Date Reported: 01/14/2019 1.50 15000 100.0 CJR 01/10/201915:20 SM-2540G 98.50 100.0 CJR 01/10/201915:20 SM-2540G 66.50 665000 100.0 CJR 01/10/201915:20 SM-254OG All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced m whole or part, nor may any reference be made to the work, the results, or the company in any advertising. news release, or other public announcements without obtaining our prior written authorization. PIf« mt G0il� Pauric McGroary Agronomist Page 3 of 5 v CD a K Illlll lull llll 111111 illl lllli IIII IlIIII IIIII IIIII IIIII !Ili llll 06205 S A R- Crf; o1 Nk"w'- RRS 13:59 15 f OF CUSTODY Inc. 743-9401 OfficeTLon Customer Information Submitted By Charge To Copy To Project Steve Holden City of Monroe POB 69 Monroe NC 28111 Email sholden<cumonroenc.or Lab NumOnly) t Sample ID RA Container Type Glass (� or No) Sampled Date: Sam led Time. — — $ Date Recd: Time Recd: Plastic (Yes or" Sampled B : ecd B : eli(Signature) Date Time Received By: (Signature) Date Time 9 Please Place a "X" by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N x Cd Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Org-N Mo CI B Ba X SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B SOL NA 08G SP.GR. TSSjS::i:,vE.:#:2::0: e#60 Sieve#100 ASH CaO CaCO3 MgCO3 MgO C/N TOC Env I TOTAL P205 TOTAL K20 TN TKNW NH4W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA b¢ lc-_� Co e_ Special Instructions or Remarks Comments _ Report Number: 19-009-0215 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 64358 Sample Id : WWTP Cake Waypoint(D ANALYTICAL Project: WWTP Cake REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/8/2019 10:10:00 Date Received: 01/09/2019 00:00 Date Reported: 01/17/2019 Total Solids * 14.20 142000 100.0 CJR 01/10/2019 15:20 SM-2540G Moisture * 85.80 100.0 CJR 01/10/2019 15:20 SM-2540G Total Kjeldahl Nitrogen 4.89 48900 250 CLP 01/16/2019 13:50 SM-4500-NH3C-TKN Phosphorus 1.42 14200 50.0 CCR 01/14/201917:06 601OD Potassium 0.11 1090 50.0 CCR 01/14/201917:06 601OD Sulfur 0.77 7650 50.0 CCR 01/14/201917:06 601OD Calcium 1.06 10600 250 CCR 01/14/201917:06 6010D Magnesium 0.16 1620 50.0 CCR 01/14/201917:06 601OD Sodium 0.07 731 250 CCR 01/14/201917:06 601OD Iron 274000 500 KKM 01/15/201917:38 601OD Aluminum 8030 50.0 CCR 01/14/201917:06 601OD Manganese 1130 5.00 CCR 01/14/201917:06 6010D Copper 331 2.50 CCR 01/14/201917:06 6010D Zinc 719 12.5 CCR 01/14/201917:06 6010D Ammonia Nitrogen 0.66 6550 100 ZBD 01/16/2019 09:45 SM-4500-NH3C Organic N 4.23 42350 250 01/16/2019 09:45 CALCULATION Nitrate+Nitrite-N 40.8 4.56 ZBD 01/16/201913:56 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time PW« - / #1C 11411 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 3 of 6 7-7 Report Number: 19-009-0215 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 64358 Sample Id : WWTP Cake Waypoint(2) ANALYTICAL Project: WWTP Cake REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/8/2019 10:10:00 Date Received: 01/09/2019 00:00 Date Reported: 01/17/2019 Cadmium 1.16 1.00 CCR 01/14/201917:06 601OD Chromium 117 2.50 CCR 01/14/201917:06 601OD Nickel 53.0 2.50 CCR 01/14/201917:06 601OD Lead 13.8 3.00 CCR 01/14/201917:06 601OD Arsenic 8.77 5.00 CCR 01/14/201917:06 601OD Mercury 0.202 0.0138 TJS 01/14/201914:04 SW-7471B Selenium <5.00 5.00 CCR 01/14/201917:06 601OD pH " 7.0 JSL 01/15/2019 08:26 9045D Total Volatile Solids 50.60 506000 100.0 CJR 01/10/2019 15:20 SM-2540G Molybdenum 21.9 2.50 CCR 01/14/201917:06 601OD Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time pWi` #"C 60wr Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 4 of 6 SAMP 5 I�I�IIIII�I�II�II��I10ilI�II�I��III��III�IIII��II����II�� 46205 2019 1156 07 �itv of Monroe T CUSTODY 9401 on OfficerAcct# a ton Subrr �, a yC 1 Copy To Project Steve Holden City of Monroe POB 69Email - --- Monroe NC 28111 sholdcn(&.monrocnc-.orb 46 Lab Number (Lab Use Only) Sample ID Container Type Glass (*es or No) WWI P Cake Plastic (Yes or lie) Reli rshed ignature) Date Time - r.-/ A.34D Sampled Date: Sampled Time: Date Recd: Time Recd: Sampled B : j,J Received By: (Signature) _ Recd By: Date Time -- - — t- Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids °la TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N X X X X X X X X X X X X X X X Ni Pb As Hg Se pH CaCO3 E . % Volatile Solids % Org-N Mo Cl B �Ba Cd Cr X X X X X X X X X X X SO4 Ag Sb Co Sn Ti V Be ALK SS Avali P Sol K Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH Cao CaCO3 Pn CO3 t0 C1N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3w ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL _TCLP ICR I -- - — - State Certification Needed: -A NORTH CAROLINA �� L Instructions or Remarks Comments _ Report Number: 19-009-0216 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 64359 Sample Id : WTP Ferric Cake Waypoint(2) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 1/8/2019 10:05:00 Date Received: 01 /09/2019 00:00 Date Reported: 01/17/2019 Total Solids 17.00 170000 100.0 CJR 01/10/2019 15:20 SM-2540G Moisture' 83.00 100.0 CJR 01/10/201915:20 SM-2540G Total Kjeldahl Nitrogen 2.19 21900 250 CLP 01/16/2019 13:50 SM-4500-NH3C-TKN Phosphorus 0.37 3710 50.0 CCR 01/14/201917:12 601OD Potassium 0.03 315 50.0 KKM 01/15/201917:43 601OD Sulfur 0.23 2250 50.0 CCR 01/14/201917:12 601OD Calcium 0.21 2070 250 CCR 01/14/201917:12 601OD Magnesium 0.05 539 50.0 CCR 01/14/201917:12 601OD Sodium 0.06 610 250 CCR 01/14/201917:12 601OD Iron 358000 500 KKM 01/15/201917:49 601OD Aluminum 6220 50.0 CCR 01/14/201917:12 601OD Manganese 360 5.00 CCR 01/14/201917:12 6010D Copper 479 2.50 CCR 01/14/201917:12 6010D Zinc 155 12.5 CCR 01/14/201917:12 6010D Ammonia Nitrogen 0.11 1120 100 ZBD 01/16/2019 09:45 SM-4500-NI3C Organic N 2.08 20780 250 01/16/2019 09:45 CALCULATION Nitrate+Nitrite-N 73.5 4.97 ZBD 01/16/201913:58 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. ' B-Analyte detected in blank H - Beyond Holding Time POf« #1C ow r/ Our reports and letters are for the exclusive and confidential use of our clients, and n7ay not be reproduced in whole or part, nor may any reference be made Pau ric McGroary to the work the results, or the company in any adveilising, news release, or other public announcements without obtaining our phor written authorization. Agronomist Page 3 of 6 Report Number: 19-009-0216 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 64359 Sample Id : WTP Ferric Cake Waypoint(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 1/8/2019 10:05:00 Date Received: 01/09/2019 00:00 Date Reported: 01/17/2019 Cadmium 3.55 1.00 CCR 01/14/201917:12 601OD Chromium 225 2.50 CCR 01/14/201917:12 601OD Nickel 44.5 2.50 CCR 01/14/201917:12 601OD Lead 6.16 3.00 CCR 01/14/201917:12 601OD Arsenic 12.0 5.00 CCR 01/14/201917:12 601OD Mercury 0.0524 0.0155 TJS 01/14/201914:05 SW-7471B Selenium <5.00 5.00 CCR 01/14/201917:12 601OD pH " 5.4 JSL 01/15/2019 08:26 9045D Total Volatile Solids 29.80 298000 100.0 CJR 01/10/2019 15:20 SM-2540G Molybdenum 39.7 2.50 CCR 01/14/201917:12 601OD Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time VwiG 11C 101r'r Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 4 of 6 v CD a M SAMPLE' IIIII�IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIINIIIIIIIIIIIIIIIIIIIII16 p �19 W TP Ferric Cake '741 nAni USTODY Office Information Customer Information Rapt# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 ,hoidcn d monrocnc.or� Lab Number (Lab Use Only) Sample ID lContainer Tye Sampled Date: /- - / Date Recd: LA 3� WTP Ferric Cake Glass (`-egor No) Sampled Time: Time Recd: Plastic (Yes orAie) Sampled By: Recd By: Religauished Si nature) Date Time Received B (Signature) Date Time Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids % TKN P a K S Ca 'r Mg Na-, Fe Al Mn Cu Zn NH4-N NO3-N x x! x x x X X x; x x X X x x x Cd Cr Ni Pb As Hq Se - PH CaG03 Eq. % Volatile Soli8s % Or -N I Mo CI B Ba X X X X x X X X X ; x x " SO4 .: A -Sb : Co 'Sn '�-j- Ti I - �t` ! Be ALK,.. -_SS AvaiLP — Sot K Conti WIN SOL B f SOL NA O&G, . 'SP.GR. TSS Slgvetl20 Sieve#Bo Sieve#100 ;ASH "CaO `CaCO3 M CO3 M q C/N TOC Env i OTAIy, E�;., P208` T Q, At, q. =K2p ITN T< � KN1lIL:> h�dYV . ' -NQ3W R@�.. G1RG = .. :C RT A'a'4^r•4 *�y �CERT Sp'}. ^i: -0; PCBS �� : 'CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA m Special Instructions or Remarks Comments City of Monroe Reports of Lab Analysis 2nd 90 Days Report Number: 19-092-0217 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 65686 Sample Id : RAS Total Solids Moisture * Total Volatile Solids Comments: Waypoint,(D ANALYTICAL Project: RAS REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 4/1/2019 07:57:00 Date Received: 04/02/2019 00:00 Date Reported: 04/08/2019 0.71 7100 100.0 CJR 04/04/201918:06 SM-2540G 99.30 100.0 CJR 04/04/201918:06 SM-2540G 71.50 715000 100.0 CJR 04/04/201918:06 SM-2540G All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the won(, the results, or the company in any advertising. news release, or other public announcements without obtanung our prior written authorization. Pofi` mC 1Q°"r Pauric McGroary Agronomist Page 3 of 5 1111111P11111Iff1111ia,97 CUSTODY SAMPLI M°n`°" At RAS t 4 t t OZ 7621 11'111te nne Road Ricbnlum, Ul f Office Information Customer Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Email POB 69 Acct # shulden�irmtmroenc.or 46205 Monroe NC 28111 — Date Recd: Lab Number (Lab Use Only) Sample ID Container T pe Sampled Date: `Y"' 9 Time Recd: Glass (Yes or No) Sam led Time: Recd By: RAS Plastic (Yes or No) Sampled By: f nataI Time Received By: (Signature) Date Timu Please Place''a "X" by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe At Mn Cu Zn NH4-N NO3-N X GaCO3 Volatile H E % Solids % Org-N Mo CI B Ba Cd Cr Ni Pb SO4 Ag Sb Go SOL NA O&G SP.GR. TSS TOTAL TOTAL P205 K20 TN TKNW As Sn Sieve#20 NH4W Hg Ti Sieve#60 NO3W Se V 0-0 ORGN-W g x Be ALK SS Avail P Sol K Cond WIN SOL B ASHCa 0 CaCO3 C/N TOC Env --- PA CERT AZ CERT BTU PCBS REACT GN FECAL TCLP ICR State Certification Needed: I NORTH CAROLINA Sna! tat lnstnlctions or Remarks W, *1 Report Number: 19-092-0215 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 65684 Sample Id : WWTP Cake y ,h Waypoint ANALYTICAL Project: WWTP Cake REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 4/1/2019 08:09:00 Date Received: 04/02/2019 00:00 Date Reported: 04/09/2019 Total Solids 74.10 741000 100.0 ADM 04/08/2019 15:07 SM-2540G Moisture' 25.90 100.0 ADM 04/08/201915:07 SM-2540G Total Kjeldahl Nitrogen 1.03 10300 250 CLP 04/08/2019 13:30 SM-4500-NH3C-TKN Phosphorus 1.41 14100 50.0 BKN 04/06/2019 02:18 601 OD Potassium 0.10 1020 50.0 BKN 04/06/2019 02:18 601 OD Sulfur 0.74 7420 50.0 BKN 04/06/2019 02:18 601 OD Calcium 0.85 8470 250 BKN 04/06/2019 02:18 601 OD Magnesium 0.16 1560 50.0 BKN 04/06/2019 02:18 601 OD Sodium 0.04 447 250 BKN 04/08/201915:35 6010D Iron 113000 250 BKN 04/08/201915:40 601 OD Aluminum 10100 50.0 BKN 04/06/2019 02:18 601 OD Manganese 1270 5.00 BKN 04/06/2019 02:18 6010D Copper 268 2.50 BKN 04/06/2019 02:18 6010D Zinc 565 12.5 BKN 04/06/2019 02:18 6010D Ammonia Nitrogen 0.13 1270 100 JPJ 04/08/2019 09:30 SM-4500-NH3C Organic N 0.90 9030 250 04/08/2019 09:30 CALCULATION Nitrate+Nitrite-N <4.66 4.66 ZBD 04/08/201915:48 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time I Wic- mC G04N�' Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the won<, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 3 of 6 Report Number: 19-092-0215 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 65684 Sample Id : WWTP Cake Waypoint,(2) ANALYTICAL Project: WWTP Cake REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 4/1/2019 08:09:00 Date Received: 04/02/2019 00:00 Date Reported: 04/09/2019 Cadmium 1.01 1.00 BKN 04/06/2019 02:18 601 OD Chromium 133 2.50 BKN 04/06/2019 02:18 601 OD Nickel 66.3 2.50 BKN 04/06/2019 02:18 601 OD Lead 15.4 3.00 BKN 04/06/2019 02:18 601 OD Arsenic 9.75 5.00 BKN 04/06/2019 02:18 601 OD Mercury 0.162 0.0157 TJS 04/05/2019 13:43 SW-7471 B Selenium <5.00 5.00 BKN 04/06/2019 02:18 601 OD pH . 7.6 JSL 04/08/2019 06:40 9045D Total Volatile Solids 3.37 33700 100.0 ADM 04/08/2019 15:07 SM-2540G Molybdenum 17.9 2.50 BKN 04/06/2019 02:18 601 OD Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time pwiG #1 V06~,%/ Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the won(, the results, or the company in any advertising, news release, or other public announcements without obtaining out, prior written authorization. Agronomist Page 4 of 6 SAMPLE "TR AN SI I ����NN��� (�I �I���) Hill ����� �) ����� ��� ���N �I) ���� IN� 01909 4 - 0195 Y City of Monroe 1405,38 A&L JUWTPCake 7621 Wl1ite)ll7- -- _- Customer information Office Information Charge To Copy To Project Rept# Submitted By Steve Holden city of Monroe Email Acct # POB 69 Monroe NC 28111 ,holdcn(a�monroenc.or r 46205 Date Recd: Lab Number (Lab Use Only) Sample ID Container T pe Sampled Date: `�-�'� Time Recd: Glass (Yes or No) Sam led Time: Recd By: WWTP Cake Plastic (Yes or No) Sampled BY: d �� Re' wished natDate Time Received B : (Signature) Date f ime B (Sigure) 2 Internal Lab Code: SLMONR Please Place a "X" by Desired Tests K S Ca Mg Na Fe Al Mn Cu Zn NH4 N NO3-� ,, Solids % TKN P X X X X X x X X X X X X X X CaCO3 VolatilePb As H Se H Eq. % Solids % Or -N Mo C! B Ba, Cd Cr Ni X X X X X X X X X X X Be ALK =,' SS' Avail P' Sol K Cond WIN' SOL SO4 A Sb s, ,Sn :Tl u '' SOL NA O&G SP,GR, TSS Sieve#20 Sleve#80 Sieve41oo ASH CaO CaCO3 M CO3 M O CIN TOG Env REACT TOTAL TOTAL PCBS GN FECAL TCLP ICR F'205 K20 TN TKNW NH4W NO3W ORGN-W PA GERT AZ State Certification Needed: NORTH CAROLINA - Comments Special Instructions or Remarks T W. a) eT M 0- Report Number: 19-092-0216 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 65685 Sample Id : WTP Ferric Cake Waypoiint(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Project : WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 4/1/2019 08:06:00 Date Received: 04/02/2019 00:00 Date Reported: 04/09/2019 Total Solids 15.50 155000 100.0 ADM 04/08/2019 15:07 SM-2540G Moisture ' 84.50 100.0 ADM 04/08/2019 15:07 SM-2540G Total Kjeldahl Nitrogen 1.81 18100 250 CLIP 04/08/2019 13:30 SM-4500-NH3C-TKN Phosphorus 0.27 2670 250 BKN 04/08/201915:45 601OD Potassium 0.03 304 250 BKN 04/08/201915:45 601OD Sulfur 0.24 2400 250 BKN 04/08/201915:45 601OD Calcium 0.21 2060 1250 BKN 04/08/201915:45 601OD Magnesium 0.05 524 250 BKN 04/08/201915:45 601OD Sodium <0.13 <1250 1250 BKN 04/08/201915:45 601OD Iron 368000 250 BKN 04/08/201915:45 601OD Aluminum 7600 250 BKN 04/08/201915:45 601OD Manganese 498 25.0 BKN 04/08/201915:45 6010D Copper 491 12.5 BKN 04/08/201915:45 6010D Zinc 89.1 62.5 BKN 04/08/201915:45 6010D Ammonia Nitrogen 0.09 903 100 JPJ 04/08/2019 09:30 SM-4500-NI3C Organic N 1.72 17197 250 04/08/2019 09:30 CALCULATION Nitrate+Nitrite-N 112 4.77 ZBD 04/08/201915:49 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time ?Ofic mC 1011r Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the wort(, the results, or the company in any advertising, news release, or other public announcements wdhout obtarning our prior written authorization. Agronomist Page 3 of 6 Report Number: 19-092-0216 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 65685 Sample Id : WTP Ferric Cake Waypoiint,(2). ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 4/1/2019 08:06:00 Date Received: 04/02/2019 00:00 Date Reported: 04/09/2019 Cadmium <5.00 5.00 BKN 04/08/201915:45 601OD Chromium 250 12.5 BKN 04/08/201915:45 601OD Nickel 53.5 12.5 BKN 04/08/201915:45 601OD Lead <15.0 15.0 BKN 04/08/201915:45 601OD Arsenic 29.6 25.0 BKN 04/08/201915:45 601OD Mercury 0.0524 0.0139 TJS 04/05/2019 13:44 SW-7471 B Selenium <25.0 25.0 BKN 04/08/201915:45 6010D pH ` 5.9 JSL 04/08/2019 06:40 9045D Total Volatile Solids 28.50 285000 100.0 ADM 04/08/2019 15:07 SM-2540G Molybdenum 43.5 12.5 BKN 04/08/201915:45 601OD Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time ?Wl:6 mC If0N1 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the won<, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 4 of 6 SAMPLE TRANSMITTAL A&L Eastern 7621 Whitepine Road Richr IIBII I I I IIII (III III III I III IIII III I NIA NI I IIII I� 6205 6 2019 CrvofIvkmix' 14N36 W TP Fernc Cake n OE(La --- - - Submitted By Charge To Copy To Project Steve Holden Cityof Monroe POB 69 Email Monroe NC 28111 sholden(a rnonrocnc.org Lab nly) Sam le ID 11'T� Lori, C';1k: Container T pe Glass (Yes or No) Sampled Date: Sam led Time: / v Date Reed: Time Recd: Plastic (Yes or No) Sampled By: Recd By: Relinquished B Si nature Date Time Received By: (Signature) Date Time 2 Please Plac a "X" by Desired Tests Internal Lab Code: SLMONR SoUtJs °% TKN 'P x x :;Ca: M . Na Fe AI Mn Cu Zn NH4 N NO3-N x x x x x x x x x x x x x ed Cr Ni* L r -N Mo CI B Ba x x x x x x x x x x x s, SO4 A Sb :1 L '.WIN SOL B SOL NA O G ,S T ;, ,Stpve#20 yS{eve#6o Siev, .ASH a0 CaCO3 M CO3 M O, C/N TOC Env TOTAL K2D TN C. FECAL`, TCLP ICR OTAL. P205 State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments 1 w tm m o- City of Monroe Reports of Lab Analysis 3rd 90 Days Report Number: 19-183-0007 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 67217 Sample Id : RAS Total Solids Moisture * Total Volatile Solids Comments: D Waypoint,( ANALYTICAL Project : RAS REPORT OF ANALYSIS 1.20 ADM 98.80 ADM 75.40 ADM 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointa nalytical. corn Date Sampled: 7/1/2019 07:54:00 Date Received: 07/02/2019 00:00 Date Reported: 07/11/2019 07/05/201914:53 SM-254OG 07/05/201914:53 SM-254OG 07/05/201914:53 SM-2540G All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond holding time Our reports and letters are for the exclusive and confidential'use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. g',jr, r 6ewvr Pauric McGroary Agronomist Page 3 of 5 SEMI 11010111111111 0+ M 2019 C,1V "I m—w— 13:03:18 R A S 7F CUSTODY e{y Information cation Rept# Submitted By Charge To Copy To Project FOffice Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sitolden�u.mzxuvenc.��r Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: - J Date Recd: RAS Glass (Yes or No) Sampled Time: q Time Recd: Plastic (Yes or No) Sampled By: E Recd By: Relinquished y: (Signature) Date Time Received By: (Signature) Date Time Z 2- Please Place a "X" by Desired Tests Internal Lab Code Solids % TKN P K S Ca Mg Na Fe Al _Mn Cu Zn NH4-N NO3-N X Cd Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Or •N Mo CI B Ba X 304 Sb Co 311 Ti V Be ALK SS Avail P Sol K Cond I WIN SOL B --Ag SOL NA O&G P.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH CaO CaCO3 MgCO3 MgO C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments a Report Number: 19-183-0008 • Account Number: 46205 7621 Whitepine Road, Richmond, VA 23237 Waypoint, Main 804.743.9401 ° fax 804-271.6446 ANALYTICAL www.waypointanalyfical.com Send To: City of Monroe Project: WWTP Cake Steve Holden 775 Treeway Dr Monroe, NC 28110 REPORT OF ANALYSIS Date Sampled: 7/1/2019 09:09:00 Lab Number: 67218 Date Received: 07/02/2019 00:00 Sample Id : WWTP Cake Date Reported: 07/12/2019 Total Solids * 21.90 ADM 07/05/2019 14:53 SM-2540G Moisture * 78.10 ADM 07/05/2019 14:53 SM-254OG Total Kjeldahl Nitrogen 3.52 35200 250 JPJ 07/10/2019 10:00 SM-4500-NH3C-TKN Phosphorus 1.42 14200 50.0 BKN 07/10/201914A4 601OD Potassium 0.11 1070 50.0 BKN 07/10/201914:44 601OD Sulfur 0.78 7830 50.0 BKN 07/10/201914:44 6010D Calcium 1.02 10200 250 BKN 07/10/201914:44 601OD Magnesium 0.15 1450 50.0 BKN 07/10/201914:44 601OD Sodium 0.06 555 250 BKN 07/11/201913:31 601OD Iron 149000 250 BKN 07/10/201916:09 601OD Aluminum 8180 50.0 BKN 07/10/201914:44 601OD Manganese 1450 5.00 BKN 07/10/201914:44 6010D Copper 304 2.50 BKN 07/10/201914:44 6010D Zinc 704 12.5 BKN 07/10/201914:44 6010D Ammonia Nitrogen 0.36 3560 100 JPJ 07/10/2019 11:00 SM-4500-NH3C Organic N 3.16 31640 250 07/10/2019 10:00 CALCULATION Nitrate+Nitrite-N 21.2 4.61 ZBD 07/08/201915:23 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond holding time RliG 1 11 G0X1 Oct reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising; news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 3 of 6 Report Number: 19-183-0008 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 67218 Sample Id : WWTP Cake • Waypoint(2 .ANALYTICAL Project: W WTP Cake REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.cotn Date Sampled: 7/1/2019 09:09:00 Date Received: 07/02/2019 00:00 Date Reported: 07/12/2019 Cadmium <1.00 1.00 BKN 07/10/201914:44 601OD Chromium 133 2.50 BKN 07/10/201914:44 601OD Nickel 58.2 2.50 BKN 07/10/201914:44 601OD Lead 14.9 3.00 BKN 07/10/201914:44 6010D Arsenic 10.9 5.00 BKN 07/10/201914:44 6010D Mercury 0.199 0.0134 TJS 07/10/2019 10:48 SW-7471 B Selenium <5.00 5.00 BKN 07/10/201914:44 601OD pH " 7.0 JSL 07/08/2019 06:53 9045D Total Volatile Solids 53.40 ADM 07/05/2019 14:53 SM-254OG Molybdenum 24.0 2.50 BKN 07/10/201914:44 601OD Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time jpcwfic' oil GaON� Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 4 of 6 SAMPLE 11 I jI1 1111111I1 �2� 'USTODY i & 183�0008 Cwv Of MONOB 07-02-2019 130812 1NWTP Cake OF Office Information Rept# n Submitted By Charge To Copy To Project Steve Holden Cityof Monroe Acct # 46205 POB 69 Monroe NC 28111 Email sholden c�Monroc nc.orb Lab Number (Lab Use Only) i o�- Zip Sample ID W WTP Cake Container Type Glass (Yes or No) Sampled Date: Sampled Time: -7- �! Date Recd: Time Recd: Plastic (Yes or No) Sampled By:MM. Recd B lin uis ed By : (Si nature) Date Time Received B Si nature) Date Time / L/ 2' Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N x x x X x x x x X X x X X x x Cd Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Or -N Mo Cl B Ba x x x x x x x x x x X SO4 Ag Sb Co >,`w Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sleve#60 Steve#100 ASH Ca0 CaCO3 M CO3 MgO r C/N TOG Env TOTAL 113205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments ;0300 go Report Number: 19-183-0009 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 67219 Sample Id : WTP Feric Waypoint.(D ANALYTICAL Project : WTP Feric REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 7/1/2019 09:14:00 Date Received: 07/02/2019 00:00 Date Reported: 07/12/2019 Total Solids 27.30 ADM 07/05/2019 14:53 SM-2540G Moisture * 72.70 ADM 07/05/2019 14:53 SM-2540G Total Kjeldahl Nitrogen 1.23 12300 250 JPJ 07/10/2019 10:00 SM-4500-NH3C-TKN Phosphorus 0.22 2210 50.0 BKN 07/10/201914:49 601OD Potassium 0.03 301 50.0 BKN 07/10/201914:49 6010D Sulfur 0.29 2880 50.0 BKN 07/10/201914:49 6010D Calcium 0.31 3140 250 BKN 07/10/201914:49 601OD Magnesium 0.05 470 50.0 BKN 07/10/201914:49 6010D Sodium 0.04 368 250 BKN 07/11/201913:36 6010D Iron 295000 250 BKN 07/10/201916:14 601OD Aluminum 2840 50.0 BKN 07/10/201914:49 601OD Manganese 715 5.00 BKN 07/10/201914:49 6010D Copper 308 2.50 BKN 07/10/201914:49 6010D Zinc 196 12.5 BKN 07/10/201914:49 6010D Ammonia Nitrogen 0.08 769 100 JPJ 07/10/2019 11:00 SM-4500-NH3C Organic N 1.15 11531 250 DH 07/10/2019 10:00 CALCULATION Nitrate+Nitrite-N <4.58 4.58 ZBD 07/08/201915:25 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond holding time Runic it" G*Jl Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the won<, the results, or the company m any advertising. news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 4 of 7 Report Number: 19-183-0009 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 67219 Sample Id : WTP Feric i Waypoint.(2 ANALYTICAL Project : WTP Feric REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 7/1/2019 09:14:00 Date Received: 07/02/2019 00:00 Date Reported: 07/12/2019 Cadmium 1.27 1.00 BKN 07/10/201914:49 6010D Chromium 197 2.50 BKN 07/10/201914:49 601OD Nickel 36.0 2.50 BKN 07/10/201914:49 6010D Lead 3.20 3.00 BKN 07/10/201914:49 601OD Arsenic 13.3 5.00 BKN 07/10/201914:49 601OD Mercury 0.0165 0.0158 TJS 07/10/2019 10:49 SW-7471 B Selenium <25.0 25.0 BKN 07/10/201916:14 601OD pH * 5.9 JSL 07/08/2019 06:53 9045D Total Volatile Solids 41.70 ADM 07/05/2019 14:53 SM-2540G Molybdenum 37.4 2.50 BKN 07/10/201914:49 6010D Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time pwic X Vol Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the worts, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 5 of 7 AM1'( 19-1834)009 22 CAN of Mons 2019 13 11.33 WTP F,,,u; 'CUSTODY Office Information tlon Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden(&monmrocnc.org Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: — Date Recd: �j I WTP Feric Glass (Yes or No) Sample Time: �► Time Recd: Plastic (Yes or No) Sampled B Recd By: lin uished Bw (Signature) Date Time Received By: (Signature) Date Time J1.ftl� /Z 2= 156 Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids % TKN P K ' S Ca. ` Me a Fe Al Mn Cu Zn NH4-N NO3-N x x x x x x x EH x x x x x x x Cd Cr Ni Pb, As H ,Se - CaCO3 E . % Volatile Solids % Or -N Mo Cl B Ba x x x x x x x x x x x ':'304 A Sb Co Sn TI V Be ALK SS Avail P Sol K ''Cand WIN SOL B SOL NA O&G I SP.GR. TSS Steve#2o Sieve#6o sieve#100 ASH CaO CaCO3 M CO3 M O. C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W , ' NO3W ORGN-W PA CERT AZ CERT BTU PCBS, REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments •'. City of Monroe Reports of Lab Analysis 4th 90 Days Waypointo ANALYTICAL 46205 City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Report Number : 19-275-0004 Lab No : 68415 Sample ID: RAS Project RAS Information : 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OFANAL YSIS Report Date : 10/09/2019 Received : 10/02/2019 Pam, m` 60wr Pauric McGroary Agronomist Matrix: Solids Sampled: 10/1/2019 8:13 Moisture 99.0 % 0.010 1 10/03/19 16:58 ADM SM-2540G Total Solids 1.02 % 0.010 1 10/03/19 16:58 ADM SM-2540G Total Volatile Solids 74.9 % 0.010 1 10/03/19 16:58 ADM SM-2540G Qualifiers/ * Outside QC Limit Definitions B Analyte detected in blank Page 3 of 5 10 �°�SAMPLE TRANSMI 1111111111 IIIIN I 1111H IIIII IIIII III �11111 Gtv ul tv{onro.� A & L Ea RAS 133045 Office Information d Customer Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden(umcmrocnc.mz! Lab Number (Lab Use Only) Sample ID Container Type Sampled Date. J.0 Date Recd: R A S Glass (des or No) Sampled Time: , Time Recd: Plastic (Yes or Ne) Sampled By: Recd By: Relin uishe By: (Signature) Date Time Received By: (Signature) Date Time _ _ ____ to z Please Place a "X" by Desired Tests Internal Lab Code: Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N X Cd Cr Ni Pb As Hg Se pH CaCO3 Eq. % Volatile Solids % Org-N Mo Cl B Ba X SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond WIN SOL B i SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH CaO CaCO3 MgCO3 MgO C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR I State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments _ - --- 9/ — - — - - - - ---- - T Page 5 of 5 Waypoi to . 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project WWTP Cake 775 Treeway Dr Information Monroe, NC 28110 Report Number:19-275-0003 REPORT OFANAL YSIS Report Date: 10/10/2019 Received : 10/02/2019 Pod. m` 6awr Pauric McGroary Agronomist Lab No : 68414 Matrix: Solids Sample ID : WWTP Cake Sampled: 10/1/2019 8:24 Moisture 78.4 % 0.010 1 10/03/19 16:58 ADM SM-2540G Selenium <23.1 mg/Kg - dry 23.1 10 10/04/19 21:55 BKN 6010D Total Solids 21.6 % 0.010 1 10/03/19 16:58 ADM SM-2540G Total Kjeldahl Nitrogen 3.83 % - dry 0.115 1 10/09/19 10:00 JPJ ')M-4500-NH3C-TKP Phosphorus 17200 mg/Kg - dry 231 10 10/04/19 21:55 BKN 6010D Potassium 1170 mg/Kg - dry 231 10 10/04/19 21:55 BKN 6010D Sulfur 8800 mg/Kg - dry 231 10 10/04/19 21:55 BKN 6010D Calcium 12200 mg/Kg - dry 1160 10 10/04/19 21:55 BKN 6010D Magnesium 2100 mg/Kg - dry 231 10 10/04/19 21:55 BKN 6010D Iron 120000 mg/Kg - dry 231 10 10/04/19 21:55 BKN 6010D Manganese 1800 mg/Kg - dry 23.1 10 10/04/19 21:55 BKN 6010D Copper 293 mg/Kg - dry 11.6 10 10/04/19 21:55 BKN 6010D Organic N 3.32 % - dry 0.115 1 10/09/19 10:00 CALCULATION Nitrate+ N itrite-N 9.68 mg/Kg - dry 4.63 1 10/08/19 15:38 ZBD 4500NO3F-2011 Nickel 77.8 mg/Kg - dry 11.6 10 10/04/19 21:55 BKN 6010D Mercury 0.528 mg/Kg - dry 0.0722 1 10/08/19 13:18 TJS SW-7471B pH 7.2 S.U. 1 10/08/19 07:04 JSL 9045D Total Volatile Solids 50.4 % 0.010 1 10/03/19 16:58 ADM SM-2540G Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions C GCMS Confirmation Analysis E Result above cal range g GGA Outside QC Limits H Beyond holding time J Estimated value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q RPD >40% dual column results T Sample exhibits toxicity U Unconfirmed Refer to cover letter. Page 3 of 6 0 Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project WWTP Cake Report Date : 10/10/2019 775 Treeway Dr Information : Received : 10/02/2019 Monroe, NC 28110 Pauric McGroary Report Number :19-275-0003 REPORT Agronomist Lab No : 68414 Matrix: Solids Sample ID : WWTP Cake Sampled: 10/1/2019 8:24 Test Results Units MOIL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 0.509 % - dry 0.046 1 10/09/19 12:30 JPJ SM-4500-NH3C Aluminum 9770 mg/Kg - dry 231 10 10/04/19 21:55 BKN 6010D Arsenic <23.1 mg/Kg - dry 23.1 10 10/04/19 21:55 BKN 6010D Cadmium <4.63 mg/Kg - dry 4.63 10 10/04/19 21:55 BKN 6010D Chromium 105 mg/Kg - dry 11.6 10 10/04/19 21:55 BKN 6010D Lead 14.7 mg/Kg - dry 13.9 10 10/04/19 21:55 BKN 6010D Molybdenum 24.1 mg/Kg - dry 11.6 10 10/04/19 21:55 BKN 6010D Sodium <1160 mg/Kg - dry 1160 10 10/04/19 21:55 BKN 6010D Zinc 750 mg/Kg - dry 57.9 10 10/04/19 21:55 BKN 6010D Qualifiers/ B Analyte detected in blank H Beyond holding time Definitions Page 4 of 6 SAMPLE TRANSMIT' A&L East "7l.11 Whit—i— Q-1 Iilli1111�11111111111111111�111111111� 5 �99 City of Monroe WWTP Cake nformation .,..�..,���a1 inrormation "Rept# Submitted B Charge To Copy To Project teve Hoiden Cityof Monroe Acct # FLabNumber POB 69 VI Email 6205 Monroe NC 28111 sholden@monroenc.org (Lab Use Onlyle ID Container T e Sampled Date: _ — Date Recd: 9) q Glass (Yes or No) P Cake Plastic (Yes or No) Sampled Time: . Z Time Recd: Sam led B v f Recd By: Reli uished B i nature Date Time Received B (Signature) Date Time z Please Place al "Xif by Desired Tests Internal Lab Code SLMONR Solids % TKN P K S Ca Mg Na Fe AI Mn Cu Zn NH4-N NO3-N X X X X X X X X X X X X X X X Cd Cr Ni As H Se H CaCO3 Eq. % Volatile Solids % Or -N Mo Cl B Ba x X X Kb X X X X X XtSoI S04 Ag Sb Sn Ti V Be ALK SS Avail P Cond WIN SOL B SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH CaO CaCO3 M CO3 C/N TOC Env TOTAL P205 TOTAL K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS REACT CN FECAL TCLP ICR State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments -- v Page 6 of 6 0 7621 Whitepine Road, Richmond, VA 23237 Waypoint. Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project WTP Ferric Cake Report Date : 10/10/2019 775 Treeway Dr Information : Received : 10/02/2019 Monroe, NC 28110 Report Number : 19-275-0002 REPORT OPANAL YSIS Pauric McGroary Agronomist Lab No : 68413 Matrix: Solids Sample ID : WTP Ferric Cake Sampled: 10/1/2019 7:52 Moisture 69.7 % 0.010 1 10/03/19 16:58 ADM SM-2540G Selenium <16.5 mg/Kg - dry 16.5 10 10/04/19 21:50 BKN 6010D Total Solids 30.3 % 0.010 1 10/03/19 16:58 ADM SM-254OG Total Kjeldahl Nitrogen 1.69 % - dry 0.082 1 10/09/19 10:00 JPJ ;M-4500-NH3C-TKP Phosphorus 1640 mg/Kg - dry 165 10 10/04/19 21:50 BKN 6010D Potassium 366 mg/Kg - dry 165 10 10/04/19 21:50 BKN 6010D Sulfur 2520 mg/Kg - dry 165 10 10/04/19 21:50 BKN 6010D Calcium 2300 mg/Kg - dry 825 10 10/04/19 21:50 BKN 6010D Magnesium 538 mg/Kg - dry 165 10 10/04/19 21:50 BKN 6010D Iron 333000 mg/Kg - dry 1650 100 10/07/19 17:07 BKN 6010D Manganese 1080 mg/Kg - dry 16.5 10 10/04/19 21:50 BKN 6010D Copper 337 mg/Kg - dry 8.25 10 10/04/19 21:50 BKN 6010D Organic N 1.59 % - dry 0.082 1 10/09/19 10:00 CALCULATION Nitrate+ N itrite-N <3.30 mg/Kg - dry 3.30 1 10/08/19 15:37 ZBD 4500NO3F-2011 Nickel 39.9 mg/Kg - dry 8.25 10 10/04/19 21:50 BKN 6010D Mercury <0.0524 mg/Kg - dry 0.0524 1 10/08/19 13:16 TJS SW-7471B pH 6.0 S.U. 1 10/08/19 07:04 JSL 9045D Total Volatile Solids 40.8 % 0.010 1 10/03/19 16:58 ADM SM-2540G Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions C GCMS Confirmation Analysis E Result above cal range 9 GGA Outside QC Limits H Beyond holding time J Estimated value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q RPD >40% dual column results T Sample exhibits toxicity U Unconfirmed Refer to cover letter. Page 3 of 6 0 Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46205 City of Monroe Steve Holden Project WTP Ferric Cake Report Date : 10/10/2019 775 Treeway Dr Information : Received : 10/02/2019 Monroe, NC 28110 me Gawr Pauric McGroary Report Number :19-275-0002 REPORT OFANALYSIS Agronomist Lab No : 68413 Matrix: Solids Sample ID : WTP Ferric Cake Sampled: 10/1/2019 7:52 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 0.102 % - dry 0.033 1 10/09/19 12:30 JPJ SM-4500-NH3C Aluminum 3930 mg/Kg - dry 165 10 10/04/19 21:50 BKN 6010D Arsenic 53.5 mg/Kg - dry 16.5 10 10/04/19 21:50 BKN 6010D Cadmium <3.30 mg/Kg - dry 3.30 10 10/04/19 21:50 BKN 6010D Chromium 217 mg/Kg - dry 8.25 10 10/04/19 21:50 BKN 6010D Lead <9.90 mg/Kg - dry 9.90 10 10/04/19 21:50 BKN 6010D Molybdenum 52.1 mg/Kg - dry 8.25 10 10/04/19 21:50 BKN 6010D Sodium <825 mg/Kg - dry 825 10 10/04/19 21:50 BKN 6010D Zinc 252 mg/Kg - dry 41.3 10 10/04/19 21:50 BKN 6010D Qualifiers/ B Analyte detected in blank Definitions H Beyond holding time Page 4 of 6 SAMPLE TRA ��2 City 01 M nyo, 2 2019 A& VVTP Ferric Cake 132018 7/,) t UJt J Office Information Customer inTor111aL1v.. Rept# Submitted B Charge To Co To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden( monrocne.or Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: U -1 -i Date Recd: Aq I'� 4t'1 !' herrk� t :� Glass *eoor No) Sampled Time: Time Recd: Plastic (Yes orai* Sampled By: Aecd By: uishe ig nature) Date Time Received B (Signature) Date Time Please Place a "X" by Desired Tests Internal Lab Code: SLMONR Solids % TKN P - K ` S ".,Ca Mg Na Fe At Mn Cu Zn NH4-N NO3-N x x x x x x x x x I x x x x; x x Cd Cr Ni Pb As Hg Se H CaCO3 E . %Solids Volatile % Or -N Mo Cl 8 Ba X I x x { x I x x x x x x x E 04. A •Sb`: :. Co* Win : Tl ;` Vz` ; _Be AM: �SS �':Avail P,1:1 Sol K Cond WIN .. SOL B SQL NA SP.GR. TSS Sleve#20 jisieve#60 sieve#100 4iASH -i tlCaO iGaCO3 M CO3 MVO .' C/N TOC Env I TQTA�.. f'203 ` TC Al K2A TN* t iCN) ', . NH4W °° NO3W = m x i0Ri3NW PA, E ~ . r RTksTU.L;,wH;' k r AC 'CN ' FECAL TCLP ICR I State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Page 6 of 6 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis City of Monroe PO Box 69 Monroe, NC 28111 Attention: Steve Holden Project Name: Land Application Lot Number:UJ02066 Date Completed:10/11/2019 10/14/2019 2:58 PM Approved and released by: Project Manager: Kelly M. Nance 2�SQ PCCgE�!�OAAB TNI', ACCREDITED The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page I of 18 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Monroe Lot Number: UJ02066 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Samples -001 and -002 were not received in glass containers or in jars with septum caps for TCLP volatiles analysis, as required by the method. The pH analysis associated with the samples in this report were performed after the method recommended 15 minute holding time. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 18 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Monroe Lot Number: UJ02066 Sample Number Sample ID Matrix Date Sampled Date Received 001 WV TP CAKE Solid 10/02/2019 0819 10/02/2019 002 V TP CAKE Solid 10/02/2019 1004 10/02/2019 (2 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 18 Inorganic non-metals Client: City of Monroe Laboratory ID: UJ02066-001 Description: WWTP CAKE Matrix: Solid Date Sampled:1010212019 0819 % Solids: 15.9 10/03/2019 2322 Date Received:10/0212019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 10/11/2010 1203 SLC 31804 1 (Reactive Cya) 7.3.3 1 10/09/2019 0101 KFE 10/08/2019 1031 1 (Reactive Sul) 7.3.4 1 10/09/2019 1843 HET 10/08/2019 1031 1 (Soil pH meas) 9045D 1 10/07/2019 2210 HET 31236 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 ° F 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 Soil pH measured in water @ 18.1 ° C 9045D 7.5 su 1 LOD = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOCI N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 18 TCLP Volatiles Client: City of Monroe Laboratory ID: UJ02066-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/02/2019 0819 % Solids: 15.9 10/03/2019 2322 Date Received:10/02/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260D 10 10/09/2019 0325 JTH 31390 10/08/2019 0023 CAS Analytical Parameter Number Method Result Q LOQ Units Run Benzene 71-43-2 8260D ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260D ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260D ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260D ND 0.050 mg/L 1 Chloroform 67-66-3 8260D ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260D ND 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260D ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 8260D ND 0.050 mg/L 1 Trichloroethene 79-01-6 8260D ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260D ND 0.010 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 94 70-130 1,2-Dichloroethane-d4 99 70-130 Toluene-d8 102 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 18 TCLP Semivolatiles Client: City of Monroe Laboratory ID: UJ02066-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/02/2019 0819 % Solids: 15.9 10/03/2019 2322 Date Received:10/0212019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 10/07/20191222 JCG 10/04/20191701 31061 10/03/20191738 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 mg/L 1 Hexachlorobenzene 118-74-1 8270E ND 0.040 mg/L 1 Hexachlorobutadiene 87-68-3 8270E ND 0.040 mg/L 1 Hexachloroethane 67-72-1 8270E ND 0.040 mg/L 1 2-Methylphenol 95-48-7 8270E ND 0.040 mg/L 1 3+4-Methylphenol 106-44-5 8270E ND 0.040 mg/L 1 Nitrobenzene 98-95-3 8270E ND 0.040 mg/L 1 Pentachlorophenol 87-86-5 8270E ND 0.20 mg/L 1 Pyridine 110-86-1 8270E ND 0.040 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 74 37-129 2-Fluorophenol 39 24-127 Nitrobenzene-d5 80 38-127 Phenol-d5 61 28-128 Terphenyl-d14 85 10-148 2,4,6-Tribromophenol 78 41-144 LOD = Limit of CIuantitation B = Detected in the method blank E = Ouanlitation of compound exceeded the calibration range ND = Not detected at or above the LOCI N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 18 TCLP Herbicides Client: City of Monroe Laboratory ID: UJ02066-001 Description: WWTP CAKE Matrix: Solid Date Sampled:1010212019 0819 % Solids: 15.9 10/03/2019 2322 Date Received:10102/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 10/07/20191339 DAL1 10/06/20191941 31117 10/03/20191738 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 74 50-112 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 18 TCLP Pesticides Client: City of Monroe Laboratory ID:UJ02066-001 Description: WWTP CAKE Matrix: Solid Date Sampled:1010212019 0819 % Solids: 15.9 10/03/2019 2322 Date Received: 1010212019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 10/08/20191513 DAL1 10/04/20191701 31062 10/03/20191738 CAS Analytical Parameter Number Method Result Q LOCI Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 mg/L 1 Chlordane 57-74-9 8081 B ND 0.0040 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081 B ND 0.00040 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0016 mg/L 1 Toxaphene 8001-35-2 8081E ND 0.0080 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 56 20-131 Tetrachloro-m-xylene 60 26-132 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 18 TCLP Metals Client: City of Monroe Laboratory ID: UJ02066-001 Description: VW1/TP CAKE Matrix: Solid Date Sampled:10/02/2019 0819 % Solids: 15.9 10/03/2019 2322 Date Received:10/02/2019 Run Prep Method 1 1311/3010A 1 1311/7470A Analytical Method Dilution Analysis Date Analyst 601 OD 1 10/08/2019 0807 LLL 7470A 1 10/09/2019 1305 KSH2 Prep Date Batch Leachate Date 10/07/2019 1731 31192 10/03/2019 1738 10/08/2019 1538 31253 10/03/20191738 CAS Analytical Parameter Number Method Result Q LOQ Units Run Arsenic 7440-38-2 601OD ND 0.15 mg/L 1 Barium 7440-39-3 601OD ND 0.25 mg/L 1 Cadmium 7440-43-9 601OD ND 0.050 mg/L 1 Chromium 7440-47-3 6010D ND 0.10 mg/L 1 Lead 7439-92-1 601OD ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 mg/L 1 Selenium 7782-49-2 601OD ND 0.20 mg/L 1 Silver 7440-22-4 601OD ND 0.10 mg/L 1 LOQ = Limit of Quantitation 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 18 Inorganic non-metals Client: City of Monroe Laboratory ID: UJ02066-002 Description: WTP CAKE Matrix: Solid Date Sampled: 10/02/2019 1004 % Solids: 27.5 10/03/2019 0002 Date Received:10/02/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 10/11/2010 1319 SLC 31804 1 (Reactive Cya) 7.3.3 1 10/09/2019 0102 KFE 10/08/2019 1031 1 (Reactive Sul) 7.3.4 1 10/09/2019 1843 HET 10/08/2019 1031 1 (Soil pH meas) 9045D 1 10/07/2019 2213 HET 31236 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 - F 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 Soil pH measured in water @ 18.1 ° C 9045D 6.0 su 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 18 TCLP Volatiles Client: City of Monroe Laboratory I D: UJ02066-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/02/2019 1004 % Solids: 27.5 10/03/2019 0002 Date Received: 10/0212019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260D 10 10/09/2019 0348 JTH 31390 10/08/2019 0023 CAS Analytical Parameter Number Method Result Q LOQ Units Run Benzene 71-43-2 8260D ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260D ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260D ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260D ND 0.050 mg/L 1 Chloroform 67-66-3 8260D ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260D ND 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260D ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 8260D ND 0.050 mg/L 1 Trichloroethene 79-01-6 8260D ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260D ND 0.010 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 93 70-130 1,2-Dichloroethane-d4 99 70-130 Toluene-d8 103 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 18 TCLP Semivolatiles Client: City of Monroe Laboratory ID: UJ02066-002 Description: WTP CAKE Matrix: Solid Date Sampled:10102/2019 1004 % Solids: 27.5 10103/2019 0002 Date Received:10102/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 10/07/20191312 JCG 10/04/20191701 31061 10/03/20191738 CAS Analytical Parameter Number Method Result Q LOCI Units Run 1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 mg/L 1 Hexachloro benzene 118-74-1 8270E ND 0.040 mg/L 1 Hexachlorobutadiene 87-68-3 8270E ND 0.040 mg/L 1 Hexachloroethane 67-72-1 8270E ND 0.040 mg/L 1 2-Methylphenol 95-48-7 8270E ND 0.040 mg/L 1 3+4-Methylphenol 106-44-5 8270E ND 0.040 mg/L 1 Nitrobenzene 98-95-3 8270E ND 0.040 mg/L 1 Pentachlorophenol 87-86-5 8270E ND 0.20 mg/L 1 Pyridine 110-86-1 8270E ND 0.040 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 75 37-129 2-Fluorophenol 42 24-127 Nitrobenzene-d5 81 38-127 Phenol-d5 60 28-128 Terphenyl-d14 85 10-148 2,4,6-Tribromophenol 78 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 18 TCLP Herbicides Client: City of Monroe Laboratory ID: UJ02066-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/02/2019 1004 % Solids: 27.5 10/03/2019 0002 Date Received:10/02/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 10/07/20191425 DAL1 10/06/20191941 31117 10/03/20191738 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 79 50-112 LOO = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 18 TCLP Pesticides Client: City of Monroe Laboratory ID: UJ02066-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/02/2019 1004 % Solids: 27.5 10/03/2019 0002 )ate Received:10102/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 10/08/20191542 DAL1 10/04/20191701 31062 10/03120191738 CAS Analytical Parameter Number Method Result Q LOCI Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 mg/L 1 Chlordane 57-74-9 8081B ND 0.0040 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081 B ND 0.00040 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0016 mg/L 1 Toxaphene 8001-35-2 8081B ND 0.0080 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 52 20-131 Tetrachloro-m-xylene 64 26-132 LOO = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 14 of 18 TCLP Metals Client: City of Monroe Laboratory ID:UJ02066-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/02/2019 1004 % Solids: 27.5 10/03/2019 0002 )ate Received:10/02/2019 Run Prep Method 1 1311/3010A 1 1311/7470A Analytical Method Dilution Analysis Date Analyst 601 OD 1 10/08/2019 0812 LLL 7470A 1 10/09/2019 1308 KSH2 Prep Date Batch Leachate Date 10/07/2019 1731 31192 10/03/2019 1738 10/08/2019 1538 31253 10/03/2019 1738 CAS Analytical Parameter Number Method Result Q LOQ Units Run Arsenic 7440-38-2 601OD ND 0.15 mg/L 1 Barium 7440-39-3 601OD 0.30 0.25 mg/L 1 Cadmium 7440-43-9 601OD ND 0.050 mg/L 1 Chromium 7440-47-3 601OD ND 0.10 mg/L 1 Lead 7439-92-1 601OD ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 mg/L 1 Selenium 7782-49-2 601OD ND 0.20 mg/L 1 Silver 7440-22-4 601OD ND 0.10 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 15 of 18 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 16 of 18 00 ,N os � m m � C < CD 0 c, U) m m �3. �N aP 3 d n N 11? -4 N 0 -4 c4 0 0 x 0 V c0 CD fD � N xl 0 3 E a't CWA / NPDES SHEALY ENVIRONMENTAL SERVICES, INC. SUALY Chain of Custody Record 106 Vantage Point Nve •'WestCUlurnbia. SC 29172 Telephone N�. t8W) 79--97oo Fax No. vw') 79 -9ii I Y�r,< a,Mw-sheaiy(sn.com .^..'tent T ,1 s—K-171 JSQN12 f , Pf bvf'%.•m: Number 2 6 f -7 8 Fit3�d�v! A5 f:rrc•r�.f .. T�6� ifitxx: Pi0 f FflY NG- i Ell;aY "' �C ` J1i �iiSNa M.. _--. Ak_— sa�e.;; � st�.t'n:.n: WaybW1 Na r— - Arayp� (A'!saR i'at r rrndn- soars is �xrd'an J f rA7rfti .\'&t�R (+� t 7 iPib .pdYaClBR7r& t 9..�ryfi. Gnt4J r7i)fi ±'.Bn mmt6edhl cftck &M*t, u rib di : r"?e o7 rmN4i'A.g � Ty%�y �,�;R' Y • � J] '��y #FF. SfaAix-. byr'hxaarn9irr.! :4Yr f . � � JJ�, Y[�f�y i'� i.1^7MY!•':.l Mfa %rxi.4cY: •' � �'- i 6 � w� � � i S'W'wArll!i+`•'e1CrylnrHr (+ tYiL� .�F T ,y�y Y~ �j''� _ P i , V.l +� j� f UJ0U66 Ftrlil $r:51r 2 rP _� a-j. arm y �7t s� Froth ( ANn A.z+ nd raW P.egainrd jAw lab jp,s%%W id't•Y k, (tAr'.�GP?ITBG ?1Tj ;iar•yvb' rJ�yOaSaf Ch.^ Aew)ww.s f:Ggzm Ksia-:-J�-n/ rs Ais ispe'^ I L .4.-im fd Gikc! Yrns m-*by f- _ Y. Rnrv'-F'Lft lip DAN TS7tB t. Rcx'.tar_ by ffl-2-19 • / 2 P i nµ kcr7Ad Lek ?7 Tane 2 r?•.rriar y b L..- s. x�•�,�ed r;v �'- K.•«�+ tra'" � f{ t,nw 5 � ar:f,•�r�� ar a. i�elhut sf ertLy Date T.- a. t�8nx NxV rL:ffia4adby Nate: Ad stlr plus are ttit3tai.ted N- Sir L190ks from rece,W "AS � L'r unless other arrancjernen� sty r)k^rje. i . _ an ace (�e'e; :�� WSTRABUTtON: NNE & YELLOW -Reny rt rotaows4,ry mril gww..a(pi: Ptr.'rc Fb d Snz: Corn• *- , v. .� yf rl:? lce ©Q®0 7'o� At L P .S Pusrant. i _earl �lan Hmrc �-] harimiable 7 SW lift-. Nolme r- 1..vz Do I wing 0 DFre Ti'rt _ (%M Tare lA�cvrncrt.V.•rmfrf[ F-.a(�i 0.4! [riiOChn Dare y-G;-r7B Z X Z m Z D r cn m 0 VI Z n SHEALY ENVIRONMENTAL SERVICES, INC. Sheel.. Lit. 11vall enw Rervurc• Lc D='.i at19u.Aba-MW,1IEI'-N Sample Receipt Checklist (SRC) Paee i of CYf,^mv- Date A•::2018 ❑ Yes 0 Nol 0 NA 18. Were all will samples received at a pH > 12 and sulfide samples raceivM at a p14 > 9? ❑ Yes ❑ Na ®NA Were all applicable NH,r KN.cyanideiphcno i625 (c ) samples free o residual chlorine^ ❑ Yee ❑ No ® N:4 ev. were cuent rcm3irKs.'rvpes1S (l.c. requested dilutions, MSIMSI) designations, etc. t con•ccdy trwiwribcd from the COC into the comment section i» UMS? Yes N.'o 1. Was the quetv dumber hated on tilecontainer label? conlabel? If vesQuote k NA Santplc Preservation (Must be completed for any sample(s) incorrectly presaved or with htntdspace.) Sample(s) NA __ were received incorrectly p"crved and were adjusted aCutirrlingly in sample receiving with KA mL of circle rme: H2", HNO3, HCI, NaOH using SR 7 NA Time of pry wn-ttion NA if more than one preeservalivc is needed, plessso note in the comments helow. sunplcis) •+ _ __ were received with bubbatm; >6 mm in diameter. 11 NA were rmcived with TRC > 0.5 mgil. (if 419 is no ) an d w acre 11 i u 5: c accordingly in sample receiving with sodium thiosulrat e rN%S203) with Shealy m: NA JJSR h:u•cotie labels applied by: UMN _ pate; IOfO2?19 -I Comments: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 18 of 18 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 11.6 Land Owner: Calvin Morris Annual Dry Tons Applied: 39.4743 Site #: NC-AN-19 Acres Permitted: 11.6 Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity (non 503): N/A Crop 1 Name: Ftscue (past.) Crop 1 Max. PAN: 126 Crop 2 Name: Fescue (past.) Crop 2 Max. PAN: 50 ° y ° Ca Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. (Dry' Wet' Moist) Precip. Past 24 Hrs. inches D Ts o n * c N' * w o' 3 :n w m * N w TKN mg/kg Z a o 5 M C mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Nov-19 217 21.6 3.403 WWTPC D 0 S 0.5 0.3 38,300 5,090 9.68 85.194 NA Fescue 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: -2-17'f As Cd Cu Cr Pb Hg Mo Ni Se Zn P 85.194 0.000 Lime Applied Annuallbs/acre 0.157 0.032 1.994 0.715 0.100 0.004 0.164 0.530 0.157 5.105 117.063:::::::::::::::::::::::::::::::::::: .................. ........................... Date lbs/ac Prior Years Cumulative lbs/ac 1.44 0.228 18.926 24.412 3.011 0.094 2.678 4.78 0.54 88.792 Current Cumulative lbs/ac 1.597 0.260 20.920 25.127 3.111 0.098 2.842 5.310 0.697 93.897 Permitted C. P. L. R.**** 36 34 1 1338 X 1 267 1 15 X 1 374 1 89 2498 P rmit PAN Limit lst/2nd Cro e P 126 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incl ing the possibi ty of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface 0.5, Injection/incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report acility Name: 'ermit #: Operator: acres Used: City of Monroe WQ0001346 Calvin Morris Owner: 11.6 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 11.6 Site #: NC-AN-19 Field #: 39.47 N/A GoB-Goldston 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date 1 2 3 4 5 6 7 8 9 10 10/ 1 / 19 11 12 Solids 21.6 Arsenic 23.1 admium 4.63 Copper 293 hromium 105 Lead 14.7 Mercury 0.528 Molyb- denum 24.1 Nickel 77.8 Selenium 23.1 Zinc 750 Total Phos- horus 17200 knnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 11 2 3 4 5 6 7 8 9 10 3.40 11 12 H Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.157 0.000 0.000 1 0.157 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 0.000 0.000 0.032 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.994 0.000 0.000 1.994 'hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.715 0.000 0.000 0.715 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.100 0.000 0.000 0.100 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.164 0.000 0.000 0.164 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.530 0.000 0.000 0.530 Selenium 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.157 0.000 0.000 0.157 Zinc 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.105 0.000 0.000 5.105 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 117.063 0.000 0.000 117.063 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 44.6 Land Owner: Ben Myers Annual Dry Tons Applied: 228.1919 Site #: NC-UN18 Acres Permitted: 44.6 Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 +� Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs. inches a 4 `�? o w .� o• o %`� ° N' 4 7c w , r w * N TKN mg/kg z a " o a ao o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 June 19 154 15.5 0.451 WTPC D 0 S 0.5 0.4 18,100 903 112 6.709 NA Fescue July 19 732 21.9 3.027 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 68.371 NA Fescue Dec 19 225 21.6 0.918 WWTPC D 0 S 0.5 0.3 38,300 5,090 9.68 22.975 NA Fescue Dec 19 126 30.3 j 0.721 WTPC D 0 S 0.5 0.4 16,900 1,020 3.3 9.898 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 12371 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 107.9531 0.000 Lime Applied Annuallbs/acre 0.212 0.024 3.308 1.536 0.145 0.002 0.304 0.601 0.119 6.085 122.385.:::.::::::::::::::::::::::: ::::::::::::::::::::::::::.:::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.956 0.113 14.297 14.812 1.935 0.034 0.726 2.358 0.123 46.226 Current Cumulative lbs/ac 1.168 0.137 17.605 16.348 2.080 0.036 1.030 2.959 0.242 52.311 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 i t/2nd Crop Pe rmit PAN Limit 1 s p 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibDity of fines and imprisonment for knowing violations." Signature of Land Applier "� *Application Method: S - Surface, IN - Injection, INC - Incorporation 10-,V2 **Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: !acres Used: City of Monroe WQ0001346 Ben Myers Owner: 35.5 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 35.5 Site #: NC-UN18 Field #: 181.69 N/A BdB2-Badin 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 4/1/19 6 7 jL_j8 7/1/19 9 10 10/1/19 11 10/1/19 12 % Solids 15.5 21.9 21.6 30.3 Arsenic 29.6 10.9 23.1 53.5 Cadmium 5 1 4.63 3.3 Copper 491 304 293 337 Chromium 250 133 105 217 Lead 15 14.9 14.7 9.9 Mercury 0.0524 0.199 0.528 0.0524 Molyb- denum 43.5 24 24.1 52.1 Nickel 1 1 53.5 58.2 77.8 39.9 Selenium 25 5 23.1 16.5 Zinc 89.1 704 750 252 Total I Phos- horus 2670 14200 17200 1640 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ APP• Event 1 2 3 4 5 0.45 6 7 3.03 8 9 10 0.92 11 0.72 12 14 Arsenic 0.000 0.000 0.000 0.000 0.027 0.000 0.066 0.000 0.000 0.043 1 0.077 0.000 0.212 Cadmium 0.000 1 0.000 0.000 0.000 0.005 0.000 0.006 0.000 0.000 0.009 0.005 0.000 0.024 Copper 0.000 0.000 0.000 0.000 0.443 0.000 1.840 0.000 0.000 0.539 0.485 0.000 3.308 Mromium 0.000 0.000 0.000 0.000 0.226 0.000 0.805 0.000 0.000 0.193 0.312 0.000 1.536 Lead 0.000 0.000 0.000 0.000 0.014 0.000 0.090 0.000 0.000 0.027 0.014 0.000 0.145 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.001 0.000 0.000 0.002 Molyb- denum 0.000 0.000 0.000 0.000 0.039 0.000 0.145 0.000 0.000 0.044 0.075 0.000 0.304 Nickel 0.000 0.000 0.000 0.000 0.048 0.000 0.352 0.000 0.000 0.143 0.057 0.000 0.601 Selenium 0.000 0.000 0.000 0.000 0.023 0.000 0.030 1 0.000 0.000 0.043 0.024 0.000 0.119 Zinc 0.000 0.000 0.000 0.000 1 0.080 0.000 4.262 0.000 0.000 1.380 1 0.363 0.000 6.085 Total Phos- horus 0.000 0.000 0.000 0.000 2.408 0.000 85.967 0.000 0.000 31.648 2.362 0.000 122.385 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". SigVa-ture of Land Applier v-�,daJ Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Ben Myers Operator: Same WQ Permit #: WQ0001346 Field #: 2 Annual Dry Tons Applied: 102.8293 Site #: NC-UN18 Predominant Soil Series: GoB-Golston Acres Utilized: 27.6 Acres Permitted: 27.6 Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 `' = ° N >~ Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons "�o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources PDES #, W #, Q Fert., Animal Waste, etc) Soil Cond. D (Dry, e ' Moist) Precip. Past 24 Hrs. inches Y 410 co t? a 0 o o .._. * = 4 ;a 5 w ??, * a TKN mg/kg Z = q o (M o g w• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Oct 19 375 21.6 2.472 WWTPC D 0 S 0.5 0.3 38,300 5,090 9.68 61.877 NA Fescue Oct 19 75 30.3 0.693 WTPC D 0 S 0.5 0.4 16,900 1,020 3.3 9.521 NA Fescue Nov 19 50 21.6 0.330 WWTPC D 0 S 0.5 0.3 38,300 5,090 9.68 8.250 NA Fescue Nov 19 25 30.3 0.231 WTPC D 0 S 0.5 0.4 16,900 1,020 3.3 3.174 1 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 525 0::::::::::.:: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 82.822 uoo Lime Applied Annuallbs/acre 0.228 0.032 2.265 0.989 0.101 0.003 0.231 0.510 0.160 4.669 99.420 :: Date lbs/ac Prior Years Cumulative lbs/ac 4.685 0.442 25.8 18.944 5.094 1.439 3.629 4.555 2.293 61.987 Current Cumulative lbs/ac 4.913 0.474 28.065 19.933 5.195 1.442 3.860 5.065 2.453 66.656 Permitted C. P. L. R.**** 36 1 34 1 1338 1 X 267 1 15 1 X 1 374 1 89 1 2498 Permit PAN Limit 1 st/2nd Cro P 135 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: City of Monroe Total Dry Tons Applied (Annual): 102.84 WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Ben Myers Owner: Acres Used: 27.6 Acres Permitted: Same Predominant Soil Series 27.6 Site #: NC -UN 18 Field #: N/A GoB-Golston 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date L-IJ 2 3 4 5j 6j 7 8 9 10 10/1/19 11 10/1/19 12 % Solids 21.6 30.3 Arsenic 1 1 23.1 1 53.5 Cadmium 4.63 3.3 Copper 293 337 Chromium 105 217 Lead 14.7 9.9 Mercury 0.528 0.0524 Molyb- denum 24.1 52.1 Nickel 77.8 39.9 Selenium 23.1 16.5 Zinc 750 252 Total I Phos- horus 17200 1640 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 i 2 .._..-__, 3. __� 4 ^....., 5 ----- 6 7 8 9 10 2.80 11 ! 0.92 12 Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.129 0.099 0.000 0.228 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 0.006 0.000 0.032 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.642 0.623 0.000 2.265 Zhromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.588 0.401 0.000 0.989 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.082 0.018 0.000 0.101 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.135 0.096 0.000 0.231 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.436 0.074 0.000 0.510 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.129 0.030 0.000 0.160 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.203 1 0.466 0.000 4.669 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 96.389 3.031 0.000 99.42 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ignature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Ben Myers Operator: Same WQ Permit #: WQ0001346 Field #: 7 Acres Utilized: 5.7 Annual Dry Tons Applied: 67.8876 Site #: NC-UN18 Acres Permitted: 5.7 Predominant Soil Series: CmB-Cid Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 141 Cation Exchange Capacity (non 503): N/A Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 `' = ° Q0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources PDES #, W #, Fert., Animal Waste, etc) Soil Cond. D (Dry, Moist) Precip. Past 24 Hrs. inches a 4 b � d °n ^"w, ° o � ?» � * 70 m -� `D w * TKN mg/kg Z Y q o � mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application pp Crop 1 Crop 2 Crop 1 Crop 2 June 19 100 74.1 10.948 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 73.324 NA Fescue June 19 42 15.5 0.962 WTPC D 0 S 0.5 0.4 18,100 903 112 14.317 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): ................... TOTALS: 1421 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 87.641 0.00o Lime Applied Annuallbs/acre 0.270 0.032 6.813 3.393 0.366 0.004 0.476 1.555 0.158 12.543 313.871:::::::::::::::::::::::::::::::::::: .................. ........................... Date lbs/ac Prior Years Cumulative lbs/ac 0.401 0.083 9.468 2.968 0.649 0.014 0.704 1.142 0.143 19.281 Current Cumulative lbs/ac 0.671 0.115 16.281 6.361 1.015 0.018 1.180 2.697 0.301 31.824 Permitted C. P. L. R.**** 36 34 1 1338 1 X 1 267 1 15 X 374 89 2498 Permit PAN Limit lst/2nd Crop 141 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier W Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Monroe Total Dry Tons Applied (Annual): WQ0001346 Cation Exchange Capacity (non 503 only): Ben Myers Owner: Same 5.4 Acres Permitted: Predominant Soil Series: 5.4 Site #: NC -UN 18 Field #: 64.31 N/A CmB-Cid 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 2 3 4 4/1/19 5 4/1/19 6 7 8 9 10 11j 12 % Solids 74.1 1 15.5 Arsenic 9.75 29.6 Cadmium 1.01 5 Copper 268 491 Chromium 133 250 Lead 15.4 15 Mercury 0.162 0.0524 Molyb- denum 17.9 43.5 Nickel 66.3 53.5 Selenium 5 25 Zinc 565 89.1 Total I Phos- horus 14100 2670 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ APp• Event 1 2 3 4 10.95 5 0.96 6 7 8 9 10 11 12 y 0 L Arsenic 0.000 1 0.000 0.000 0.213 1 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.270 Cadmium 0.000 1 0.000 0.000 0.022 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Copper 0.000 0.000 0.000 5.868 0.945 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.813 �hromiurn 0.000 0.000 0.000 2.912 0.481 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.393 Lead 0.000 0.000 0.000 0.337 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.366 Mercury 0.000 0.000 0.000 0.004 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.392 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.476 Nickel 0.000 0.000 0.000 1.452 0.103 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1.555 Selenium 0.000 0.000 0.000 0.109 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.158 Zinc 0.000 0.000 0.000 12.371 1 0.171 0.000 0.000 0.000 0.000 0.000 0.000 0.000 12.543 Total Phos- horus L00 0.000 0.000 308.734 5.137 0.000 0.000 0.000 0.000 0.000 0.000 0.000 313.87 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Wayne McBride Operator: Same WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 6.7 Annual Dry Tons Applied: 21.5790 Site #: NC-UN25 Acres Permitted: 6.7 Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 137 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 s Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources PDES #, W #, Q Fert., Animal Waste, etc) Soil Cond. D Wet, Moist) Precip. Past 24 Hrs. inches Y b co t? �• c w + o ° o w t D `- * w ", �, w * w. TKN mg/kg Z. a q o � as o 0 w• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Sept 19 117 21.9 3.221 WWTPC D 0 S 1 0.5 0.3 35,200 3,560 21.2 72.745 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 117 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 72.745 0.000 Lime Applied Annuallbs/acre 0.070 0.006 1.958 0.857 0.096 0.001 0.155 0.375 0.032 4.535 91.476 :: ::: Date lbs/ac Prior Years Cumulative lbs/ac 1.048 0.121 18.87 13.711 1.566 0.043 2.009 2.421 0.133 39.796 Current Cumulative lbs/ac 1.118 0.127 20.828 14.568 1.662 0.044 2.164 2.796 0.165 44.331 Permitted C. P. L. R.**** 36 1 34 1338 X 1 267 1 15 X 374 89 2498 Permit PAN Limit lst/2nd Crop P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibilityof fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Wayne McBride Owner: kcres Used: 6.5 Acres Permitted: Same Predominant Soil Series: 6.5 Site #: NC-UN25 Field #: 20.94 N/A TaB-Tatum 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 21 3 4 5 6 7 7/ 1 / 19 8 9 101 IIJ 12 % Solids 21.9 Arsenic 10.9 Cadmium 1 Copper 304 Chromium 133 Lead 14.9 Mercury 0.199 Molyb- denum 24 Nickel 58.2 Selenium 5 Zinc 704 Total I Phos- horus 14200 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 L3 4 5j 6 7 3.22 8 9 10 11 12 y ° Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.070 0.000 0.000 0.000 1 0.000 0.000 0.070 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.000 0.000 0.000 0.000 0.000 0.006 Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.958 0.000 0.000 0.000 0.000 0.000 1.958 Mromium 0.000 0.000 0.000 0.000 0.000 0.000 0.857 0.000 0.000 0.000 0.000 0.000 0.857 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.096 0.000 0.000 0.000 0.000 0.000 0.096 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.155 0.000 0.000 0.000 0.000 0.000 0.155 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.375 0.000 0.000 0.000 0.000 0.000 0.375 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.032 0.000 0.000 0.000 0.000 0.000 0.032 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 4.535 1 0.000 0.000 0.000 0.000 0.000 4.535 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 91.476 0.000 0.000 0.000 0.000 0.000 91.476 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ignature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 3 Acres Utilized: 14.6 Land Owner: Wayne McBride Annual Dry Tons Applied: 58.7416 Site #: NC-UN25 Acres Permitted: 14.6 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 137 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 '~ ° Y Y oUP Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet' Moist) Precip. Past 24 Hrs. inches Y " z7 o a o %U ?» N' o' N TKN mg/kg z = o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop i Crop 2 Crop 1 Crop 2 Sept 19 225 21.9 2.842 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 64.198 NA Fescue Sept 19 75 27.3 1.181 WTPC D 0 S 0.5 0.4 12,300 769 4.58 11.814 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ......... .... ... ...... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):............... ................... ...... TOTALS: 3001 As Cd Cu Cr Pb 1-19 Mo Ni Se Zn P 76.012 0.000 Lime Applied Annuallbs/acre 0.093 0.009 2.454 1.220 0.092 0.001 0.225 0.416 0.087 4.461 85.872 :: Date lbs/ac Prior Years Cumulative lbs/ac 1.058 0.146 18.402 14.736 1.555 0.036 1.95 2.599 0.262 44.701 Current Cumulative lbs/ac 1.151 0.155 20.856 15.956 1.647 0.037 2.175 3.015 0.349 49.162 Permitted C. P. L. R.**** 36 34 1338 1 X 267 1 15 X 374 89 1 2498 n Permit PAN Limit 1 st/2 d Cr o P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Wayne McBride Owner: Same Predominant Soil Series: Acres Used: 14.1 Acres Permitted: 14.1 Site #: NC-UN25 Field #: 56.68 N/A TaB-Tatum 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 21 L3 j4 5 6 7 7/1/19 8 7/1/19 9j 10 11 12 % Solids 1 21.9 1 27.3 Arsenic 10.9 13.3 Cadmium 1 1.27 Copper 304 308 Chromium 133 197 Lead 14.9 3.2 Mercury 0.199 0.0165 Molyb- denum 24 37.4 Nickel 58.2 36 Selenium 1 5 25 Zinc 704 196 Total I Phos- horus 14200 2210 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 DT/Ac./ App- Event 11 2 3 4 5 6 7 2.84 8 1.18 9 10 11 12 14 Arsenic 0.000 1 0.000 0.000 0.000 0.000 0.000 0.062 0.031 0.000 0.000 1 0.000 0.000 0.093 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.003 0.000 0.000 0.000 0.000 0.009 Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.727 0.727 0.000 0.000 0.000 0.000 2.454 Zhromium 0.000 0.000 0.000 0.000 0.000 0.000 0.755 0.465 0.000 0.000 0.000 0.000 1.220 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.085 0.008 0.000 0.000 0.000 0.000 0.092 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.136 0.088 0.000 0.000 0.000 0.000 0.225 Nickel 0.000 0.000 0.000 0.000 0.000 1 0.000 0.331 0.085 0.000 0.000 0.000 0.000 0.416 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.028 0.059 0.000 0.000 0.000 0.000 0.087 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 3.999 0.463 0.000 0.000 0.000 0.000 4.461 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 80.656 5.216 0.000 0.000 0.000 0.000 85.872 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: W00001346 Field #: 1 Acres Utilized: 16.4 Land Owner: Emerson McBride Operator: Same Crop 1 Name: Fescue Annual Dry Tons Applied: 52.9710 Predominant Soil Series: TaB-Tatum Crop 1 Max. PAN: 137 Crop 2 Name: Site #: NC-UN26 Acres Permitted: 16.4 Cation Exchange Capacity (non 503): N/A Fescue Crop 2 Max. PAN: 50 Q 0 Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tans/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D- (Dry, Moist) Preci . p Past 24 Hrs. inches � ,� 'd 0- � +o ° C 0 w ' * N 3 77 = w �, >v TKN mg/kg Z a o ao o w• mg/kg Nitrate and Nitrite mg/kg PAN Applied pp ( lbs/acre) Name of CropType yp Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 Aug 19 75 21.9 0.843 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 19.051 NA Fescue Aug 19 120 27.3 1.682 WTPC D 0 S 0.5 0.4 12,300 769 4.58 16.828 NA Fescue Sept 19 14 21.9 0.157 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 3.556 NA Fescue Sept 19 39 27.3 0.547 WTPC D 0 S 0.5 0.4 12300 769 4.58 5.469 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 248 0:::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 44.904 0.000 Lime Applied Annuallbs/acre 0.081 0.008 1.982 1.145 0.044 0.000 0.215 0.277 0.122 2.282 38.257 :: :: Date lbs/ac Prior Years Cumulative lbs/ac 0.949 0.143 19.046 12.782 1.747 0.031 1.765 2.602 0.238 46.985 Current Cumulative lbs/ac 1.030 0.151 21.028 13.927 1.791 0.031 1.980 2.879 0.360 49.267 Permitted C. P. L. R.**** 36 1 34 1 1338 1 X 1 267 1 15 1 X 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Mowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 'ermit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Emerson Mcbride Owner: Same Predominant Soil Series: tcres Used: 16.4 Acres Permitted: 16.4 Site #: NC-UN26 Field #: 52.97 N/A TaB-Tatum 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date 1 11 L2J3j L4 51 6 7 7/1/19 8 7/1/19 9 10 11 12 % Solids 21.9 27.3 Arsenic 10.9 1 13.3 Cadmium 1 1.27 Copper 304 308 Chromium 133 197 Lead 14.9 3.2 Mercury 0.199 0.0165 Molyb- denum 24 37.4 Nickel 58.2 36 Selenium 5 25 Zinc 704 196 Total I Phos- horus 14200 2210 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 1 2 3 4 5 611 7 1.00 81 2.23 91 101 111112 14 Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.022 0.059 0.000 0.000 1 0.000 0.000 0.081 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.006 0.000 0.000 0.000 0.000 0.008 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.608 1.374 0.000 0.000 0.000 0.000 1.982 �hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.266 0.879 0.000 0.000 0.000 0.000 1.145 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.030 0.014 0.000 0.000 0.000 0.000 0.044 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.048 0.167 0.000 0.000 0.000 0.000 0.215 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.116 0.161 0.000 0.000 0.000 0.000 0.277 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.010 0.112 0.000 0.000 0.000 0.000 0.122 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 1.408 0.874 0.000 0.000 0.000 0.000 2.282 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 28.400 9.857 0.000 0.000 0.000 0.000 38.257 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ignature of Land Applier v7'/�� Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 2 Acres Utilized: 6.5 Land Owner: Emerson McBride Annual Dry Tons Applied: 24.2445 Site #: NC-UN26 Acres Permitted: 6.5 Operator: Same Predominant Soil Series: TaB2-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Precip. Past 24 Hrs. inches 4-0 ? c o C o w * 4 w * TKN mg/kg Z a �o ° �• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acpe) Name of CropType Yp Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 19 114 21.9 3.235 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 73.061 NA Fescue Aug 19 14 27.3 0.495 WTPC D 0 S 0.5 0.4 12,300 769 4.58 4.953 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 128 o :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 78.014 0.000 Lime Applied Annuallbs/acre 0.084 0.008 2.272 1.056 0.100 0.001 0.192 0.412 0.057 4.749 94.062 Date lbs/ac Prior Years Cumulative lbs/ac 0.817 0.119 17.267 10.991 1.826 0.03 1.51 2.561 0.22 48.732 Current Cumulative lbs/ac 0.901 0.127 19.539 12.047 1.926 0.031 1.702 2.973 0.277 53.481 Permitted C. P. L. R.**** 1 36 34 1 1338 1 X 1 267 1 15 1 X 1 374 1 89 2498 Permit PAN Limit lst/2nd Crop 13 7 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibifil of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation �vok-bZ'� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 24.25 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson McBride Owner: Same Predominant Soil Series: TaB2-Tatum kcres Used: 6.5 Acres Permitted: 6.5 Site #: NC-UN26 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 61 7 7/1/19 8 7/1/19 9 10 Ij 12 % Solids 21.9 27.3 Arsenic 10.9 1 13.3 Cadmium 1 1.27 Copper 304 308 Chromium 133 197 Lead 14.9 3.2 Mercury 0.199 0.0165 Molyb- denum 24 37.4 Nickel 58.2 36 Selenium 1 5 1 25 Zinc 704 196 Total I Phos- horus 14200 2210 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 11 2 3 4 5 6 7 3.24 8 0.50 9 10 Llj 12 y Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.071 0.013 0.000 0.000 0.000 0.000 0.084 Cadmium 0.000 1 0.000 0.000 0.000 0.000 0.000 0.006 0.001 0.000 0.000 0.000 0.000 0.008 Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.967 0.305 0.000 0.000 0.000 0.000 2.272 Zhromium 0.000 0.000 0.000 0.000 0.000 0.000 0.861 0.195 0.000 0.000 0.000 0.000 1.056 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.096 0.003 0.000 0.000 0.000 0.000 0.100 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.155 0.037 0.000 0.000 0.000 0.000 0.192 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.377 0.036 0.000 0.000 0.000 0.000 0.412 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.032 0.025 0.000 0.000 0.000 0.000 0.057 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 4.555 1 0.194 0.000 0.000 0.000 0.000 4.749 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 91.874 2.188 0.000 0.000 0.000 0.000 94.062 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". gnature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 3 Acres Utilized: 11.3 Land Owner: Emerson McBride Annual Dry Tons Applied: 51.5890 Site #: NC-UN26 Acres Permitted: 11.3 Operator: Same Crop 1 Name: Fescue Predominant Soil Series: TaB-Tatum Crop 1 Max. PAN: 137 Crop 2 Name: Cation Exchange Capacity (non 503): N/A Fescue Crop 2 Max. PAN: 50 '- +� Q Volume applied (enter one) Solids/ Liquid 9 Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. (Dry' Wet' Moist) Precip. Past 24 Hrs. inches a b o °� o 2 w = N' o' z w , N TKN mg/kg z Y q B o °4 2 w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 19 175 21.9 2.856 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 1 64.514 NA Fescue Aug 19 84 27.3 1.709 WTPC D 0 S 0.5 0.4 12,300 769 4.58 17.096 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ......... ....... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):....... ................... TOTALS: 2591 0 :::::::::::::: As Cd Cu I Cr Pb Hg Mo Ni Se Zn P 81.61TI 0.000 Lime Applied Annuallbs/acre 0.108 0.010 2.789 1.433 0.096 0.001 0.265 0.455 0.114 4.691 88.664 :: ::::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.984 0.154 20.82 17.484 2.042 0.036 1.886 3.01 0.229 54.885 July 18 2088 Current Cumulative lbs/ac 1.092 0.164 23.609 18.917 2.138 0.037 2.151 3.465 0.343 59.576 Permitted C. P. L. R.**** 36 1 34 1338 X 1 267 1 15 X 374 1. 89 1 2498 Permit a 1 PAN Lims t/2nd Crop 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility o fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation �a�vSJ,J **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report +acility Name: 'ermit #: Operator: kcres Used: City of Monroe Total Dry Tons Applied (Annual): WQ0001346 Cation Exchange Capacity (non 503 only): Emerson McBride Owner: Same Predominant Soil Series: 11.3 Acres Permitted: 11.3 Site #: NC-UN26 Field #: 51.58 N/A TaB-Tatum 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date L11 2 _3j L 4 5 L 6j L 7 7/1/19 81 7/1/19 9 10 Ill 1 12 % Solids 1 21.9 27.3 Arsenic 10.9 13.3 admium 1 1.27 Copper 304 308 Chromium 133 197 Lead 14.9 3.2 Mercury 0.199 0.0165 Molyb- denum 24 37.4 Nickel 58.2 36 Selenium 5 25 Zinc 704 196 Total Phos- horus 14200 2210 knnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 11 2 3 4 5 6 7 2.86 8 1.71 9 10 11 12 14 Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.062 0.045 0.000 0.000 0.000 0.000 0.108 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.004 0.000 0.000 0.000 0.000 0.010 Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.736 1.053 0.000 0.000 0.000 0.000 2.789 'hromi 0.000 0.000 0.000 0.000 0.000 0.000 0.760 0.673 0.000 0.000 0.000 0.000 1.433 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.085 0.011 0.000 0.000 0.000 0.000 0.096 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.137 0.128 0.000 0.000 0.000 0.000 0.265 Nickel 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.332 0.123 0.000 0.000 0.000 0.000 1 0.455 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.029 0.085 0.000 0.000 0.000 0.000 0.114 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 4.021 0.670 0.000 0.000 0.000 0.000 4.691 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 81.110 7.554 0.000 0.000 0.000 0.000 88.664 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ignature of Land Applier cP2�y-dv�J Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City Of Monroe WQ Permit #: WQ0001346 Field #: 4 Land Owner: Emerson McBride Annual Dry Tons Applied: 47.7689 Operator: Same Predominant Soil Series: TaB-Tatum Site #: NC-UN26 Acres Utilized: 25.6 Acres Permitted: 25.6 Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 �- O 0 Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons u /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ#, Fert., Animal Waste, etc) Soil Cond. D ( ry' Wet, Moist) Pre P. Past 24 Hrs. inches Y b : 'b �• a w o o m w - � w -+ W �, >y * w' « TKN mg/kg Z :, o vo o g mglkg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 19 259 21.9 1.866 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 42.146 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 259 0 ::::::::::::. As Cd Cu Cr Pb H Mo Ni Se Zn P 42.146 0.000 Lime A lied Annuallbs/acre 0.041 0.004 1.135 0.496 0.056 0.001 0.090 0.217 0.019 2.627 52.994 :::::::.....::::::::::::::::: ::• Date lbs/ac Prior Years Cumulative lbs/ac 1.042 0.154 22.774 13.41 2.142 0.037 2.039 3.08 0.282 55.654 Current Cumulative lbs/ac 1.083 0.158 23.909 13.906 2.198 0.038 2.129 3.297 0.301 58.281 Permitted C. P. L. R.**** 36 1 34 1 1338 X 1 267 1 15 1 X 1 374 1 89 2498 Permit PAN Limit lst/2nd Crop P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: kcres Used: City of Monroe Total Dry Tons Applied (Annual): 47.77 WQ0001346 Cation Exchange Capacity (non 503 only): N/A Emerson Mc Bride Owner: Same Predominant Soil Series: TaB-Tatum 25.6 Acres Permitted: 25.6 Site #: NC-UN26 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date LIJ L_?]31 4 5 6 7T/ 1 / 19 8 9 10 11 12 Vo Solids 21.9 Arsenic 10.9 Cadmium 1 Copper 304 Chromium 133 Lead 14.9 Mercury 0.199 Molyb- denum 24 Nickel 58.2 Selenium 5 Zinc 704 Total I Phos- horus 14200 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4 5 6 7 1.87 8 9 10 11 12 14 Arsenic 0.000 1 0.000 0.000 0.000 0.000 0.000 0.041 0.000 0.000 0.000 1 0.000 0.000 0.041 Cadmium 0.000 1 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.135 0.000 0.000 0.000 0.000 0.000 1.135 'hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.496 0.000 0.000 0.000 0.000 0.000 0.496 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.056 0.000 0.000 0.000 0.000 0.000 0.056 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.090 0.000 0.000 0.000 0.000 0.000 0.090 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.217 0.000 0.000 0.000 0.000 0.000 0.217 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.019 1 0.000 0.000 0.000 0.000 0.000 0.019 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 2.627 0.000 0.000 0.000 0.000 0.000 2.627 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 52.994 0.000 0.000 0.000 0.000 0.000 52.994 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". <�� 011141111��� .2 ignature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 6 Acres Utilized: 14 Land Owner: Emerson McBride Annual Dry Tons Applied: 60.0907 Site #: NC-UN26 Acres Permitted: 26.5 Operator: Same Predominant Soil Series: TaB2-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (hay) Crop 1 Max. PAN: 137 Crop 2 Name: Fescue (hay) Crop 2 Max. PAN: 50 '" .� ° ., ° s~ Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons oho Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, e ' Moist) Precip. Past 24 Hrs. inches Y 'b cc 'd a c ° o w _ * w' 7 -� �, w TKN mg/kg Z Y .; E3 o 5 ao o R. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 July 19 256 21.9 3.373 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 76.174 NA Fescue July 19 56 27.3 0.920 WTPC D 0 S 0.5 0.4 12,300 769 4.58 9.199 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 312 0 :::::::::::::: As Cd Cu Cr Pb Ha Mo Ni Se Zn P 85.373 0.000 Lime Applied Annuallbs/acre 0.098 0.009 2.618 1.260 0.106 0.001 0.231 0.459 0.080 5.110 99.860 :: Date lbs/ac Prior Years Cumulative lbs/ac 0.412 0.068 11.865 4.041 0.952 0.013 0.993 1.22 0.144 20.364 Current Cumulative lbs/ac 0.510 0.077 14.483 5.301 1.058 0.014 1.224 1.679 0.224 25.474 Permitted C. P. L. R.**** 36 34 1338 1 X 267 15 X 374 89 2498 Permit PAN Limit lst/2nd Crop 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." M Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 60.10 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson McBride Owner: Same Predominant Soil Series: TaB2-Tatum kcres Used: 14 Acres Permitted: 26.5 Site #: NC-UN-26 Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6 7T/ 1/19 8 7/1/19 9 10 1 1 12 % Solids 21.9 27.3 Arsenic 1 10.9 1 13.3 Cadmium 1 1.27 Copper 304 308 Chromium 133 197 Lead 14.9 3.2 Mercury 0.199 0.0165 Molyb- denum 24 37.4 Nickel 58.2 36 Selenium 5 25 Zinc 704 1 196 Total I Phos- horus 14200 2210 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 1 2j 3 4 5 6 71 3.37 8 0.92 9 10 111 12 H 14 Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.074 0.024 0.000 0.000 1 0.000 0.000 0.098 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.002 0.000 0.000 0.000 0.000 0.009 Copper 0.000 0.000 0.000 0.000 0.000 0.000 2.051 0.567 0.000 0.000 0.000 0.000 2.618 hromium 0.000 0.000 0.000 0.000 0.000 0.000 0.897 0.362 0.000 0.000 0.000 0.000 1.260 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.101 0.006 0.000 0.000 0.000 0.000 0.106 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.162 0.069 0.000 0.000 0.000 0.000 0.231 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.393 0.066 0.000 0.000 0.000 0.000 1 0.459 Selenium 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.034 0.046 0.000 0.000 0.000 0.000 1 0.080 Zinc 0.000 1 0.000 0.000 0.000 0.000 0.000 4.749 0.361 0.000 0.000 0.000 0.000 5.110 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 95.793 4.066 0.000 0.000 0.000 0.000 99.860 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ignature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 24.5 Land Owner: William Griffin Annual Dry Tons Applied: 206.5346 Site #: NC-UN29 Acres Permitted: 24.5 Operator: Same Predominant Soil Series: GoC-Golston Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 116 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 o c� O Volume applied (enter one) Solids/ Liquid Q Cu. Yds Gallons oho Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NpDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs. inches TD -. d o 8- _. o R N' R w -+ w * N w o o TKN mg/kg z o B ao o m' mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 19 300 74.1 7.641 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 51.177 NA Fescue May 19 148 15.5 0.789 WTPC D 0 S 0.5 0.4 18,100 903 112 11.737 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ........ ..... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):...... ................... .......... TOTALS: 448 o As Cd Cu Cr Pb H Mo Ni Se Zn P 62.914 0.000 Lime Applied Annuallbs/acre 0.196 0.023 4.870 2.427 0.259 0.003 0.342 1.098 0.116 8.775 219.689::::::::::::::::::::::::::::::... .................. ........................... Date lbs/ac Prior Years Cumulative lbs/ac 0.279 0.045 6.325 2.271 0.507 0.006 0.515 0.706 0.084 11.198 Current Cumulative lbs/ac 0.475 0.068 11.195 4.698 0.766 0.009 0.857 1.804 0.200 19.973 Permitted C. P. L. R.**** 1 36 34 1338 X 267 1 15 X 1 374 1 89 1 2498 n i PAN Limit lst/2 d Cr Permit op P 116 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation a **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: kcres Used: City of Monroe WQ0003146 William Griffin Owner: 24.5 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 24.5 Site #: NC-UN29 Field #: 206.54 N/A GoC-Golston 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): >ample or Com- posite Date 1 2 3 4 4/1/19 5 4/1/19 6 j 8 91 10 11 12 % Solids 74.1 1 15.5 Arsenic 9.75 29.6 Cadmium 1.01 5 Copper 268 491 Chromium 133 250 Lead 15.4 15 Mercury 0.162 0.0524 Molyb- denum 17.9 43.5 Nickel 1 66.3 53.5 Selenium 5 25 Zinc 565 89.1 Total I Phos- horus 14100 2670 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App . Event �.._i __2_i __3. i 4 7.64 5 J 0.79 6 j 8 9_1 10 11j 12 Arsenic 0.000 1 0.000 0.000 0.149 1 0.047 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.196 Cadmium 0.000 0.000 0.000 0.015 0.008 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.023 Copper 0.000 0.000 0.000 4.096 0.775 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.870 Zhromium 0.000 0.000 0.000 2.033 0.395 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.427 Lead 0.000 0.000 0.000 0.235 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.259 Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.274 0.069 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.342 Nickel 0.000 0.000 0.000 1.013 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.098 Selenium 0.000 0.000 0.000 0.076 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.116 Zinc 0.000 0.000 0.000 8.634 0.141 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 8.775 Total Phos- horus 0.000 0.000 0.000 215.476 4.213 0.000 0.000 0.000 0.000 0.000 0.000 0.000 219.689 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". -AV .34.3 v Sign-a_t'ure of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: William Griffin Operator: Same WQ Permit #: WQ0001346 Field #: 2 Annual Dry Tons Applied: 73.0139 Predominant Soil Series: GoC-Goldston Site #: NC-UN29 Acres Utilized: 5.7 Acres Permitted: 5.7 Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 116 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 $-. O y Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (DryTonslAc) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs inches Y b a 'b r . o w a, �• * � o ;0 w � * N' * w 4 w `; w � N * 0 TKN mg/kg Z > r: o El va o E. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 19 117 74.1 12.809 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 85.789 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 1171 As Cd Cu Cr Pb Hg Mo Ni I Se Zn P 85.789 1 0.000 Lime Applied Annuallbs/acre 0.250 0.026 6.866 3.407 0.395 0.004 0.459 1.698 0.128 14.474 361.214 ::::::::::::::::::::::::::: :.:' :.:. Date lbs/ac Prior Years Cumulative lbs/ac 0.505 0.08 11.462 3.141 0.92 0.013 0.997 0.984 0.122 16.324 July 18 2165 Current Cumulative lbs/ac 0.755 0.106 18.328 6.548 1.315 0.017 1.456 2.682 0.250 30.798 Permitted C. P. L. R.**** 36 34 1 1338 X 267 15 X 374 89 2498 Permit PAN Limit 1 stl2nd Crop P :. 116 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility pf fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation O��ay **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 73.01 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: William Griffin Owner: Same Predominant Soil Series: GoC-Goldston Acres Used: 5.7 Acres Permitted: 5.7 Site #: NC-UN29 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or, Com- posite Date 1 21 L3J4 4/1/19 5j 6 7 8j L 9j 10 11 J 12 % Solids 74.1 Arsenic 9.75 Cadmium 1.01 Copper 268 Chromium 133 Lead 15.4 Mercury 0.162 Molyb- denum 17.9 Nickel 66.3 Selenium 5 Zinc 565 Total I Phos- horus 14100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4 12.81 5 _6j 7 8 J 9] 1101 11 12 H in Arsenic 0.000 1 0.000 0.000 0.250 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.250 Cadmium 0.000 0.000 0.000 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Copper 0.000 0.000 0.000 6.866 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.866 Chromium 0.000 0.000 0.000 3.407 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.407 Lead 0.000 0.000 0.000 0.395 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.395 Mercury 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.459 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.459 Nickel 0.000 0.000 0.000 1.698 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.698 Selenium 0.000 0.000 0.000 0.128 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.128 Zinc 0.000 0.000 0.000 14.474 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 14.474 Total Phos- horus 0.000 0.000 0.000 361.214 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 361.214 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Si re of Land pplier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: William Griffin Operator: Same WQ Permit #: WQ0001346 Field #: 3 Annual Dry Tons Applied: 95.4797 Site #: NC-UN29 Predominant Soil Series: BaB-Badin Acres Utilized: 7.4 Acres Permitted: 7.4' Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 S. Ci Q 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources DES # W #, ( Q Fert., Animal Waste, etc) Soil Cond. D (Dry, Moist) Precip. Past 24 ems• inches Y 4 co � �. o c ] o � _ 7y R -+ �, w w TKN mg/kg z Y q o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 April19 153 74.1 12.903 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 86.413 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000• 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 153 0::,::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 86.413 0.000 Lime Applied Annuallbs/acre 0.252 0.026 6.916 3.432 0.397 0.004 0.462 1.711 0.129 14.580 363.865 ::::::::::::::::::::::::. •::: Date lbs/ac Prior Years Cumulative lbs/ac 0.615 0.101 16.372 6.146 0.888 0.019 1.387 1.735 0.739 23.21 Current Cumulative lbs/ac 0.867 0.127 23.288 9.578 1.285 0.023 1.849 3.446 0.868 37.790 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit lst/2nd Crop P 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report acility Name: 'ermit #: Operator: tires Used: City of Monroe Total Dry Tons Applied (Annual): WQ0001346 Cation Exchange Capacity (non 503 only): William Griffin Owner: 7.4 Acres Permitted: Same Predominant Soil Series: 7.4 Site #: NC-UN29 Field #: 95.48 N/A BaB-Badin 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date 1 2 3 4 4/1/19 5 6 7 8 9 Loj 11j 12 % Solids 74.1 Arsenic 9.75 admium 1.01 Copper 268 Chromium 133 Lead 15.4 Mercury 0.162 Molyb- denum 17.9 Nickel 66.3 Selenium 5 Zinc 565 Total I Phos- horus 14100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ APP• Event 11 21 3j 4j 12.90 5 6 7 8 9 10 11 12 H " Arsenic 0.000 1 0.000 0.000 0.252 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.252 Cadmium 0.000 0.000 0.000 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Copper 0.000 0.000 0.000 6.916 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.916 ,hromium 0.000 0.000 0.000 3.432 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.432 Lead 0.000 0.000 0.000 0.397 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.397 Mercury 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.462 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.462 Nickel 0.000 0.000 0.000 1.711 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.711 Selenium 0.000 0.000 0.000 0.129 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.129 Zinc 0.000 0.000 0.000 14.580 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 14.580 Total Phos- horus 0.000 0.000 0.000 363.865 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 363.865 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". nature of Land Applier v) /A7''v� J Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Tom Appenzeller Operator: William Griffin Crop 1 Name: Fescue (Past.) WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 13.1 Annual Dry Tons Applied: 62.3646 Site #: UN-UN30 Acres Permitted: 13.1 Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 $. 0 +� O Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, W #, Q Fert., Animal Waste, etc) Soil Cond. (Dry' Wet' Moist) Precip. Past 24 Hrs. inches Y 41� cc S o w * °� c ; ?» .- * N' o' 4 ;0 = m -, w * N TKN mg/kg z a .; B o El ao C w mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Nov 19 225 21.6 3.124 WWTPC D 0 S 0.5 0.3 38,300 5,090 9.68 78.220 NA Fescue Nov 19 1 84 30.3 1.636 WTPC D 0 S 0.5 0.4 16,900 1,020 3.3 22.467 NA Fescue 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 3091 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 100.6871 0.000 Lime Applied Annuallbs/acre 0.319 0.040 2.933 1.366 0.124 0.003 0.321 0.617 0.198 5.511 112.832 :::::::::::::::::::::::....:: Date lbs/ac Prior Years Cumulative lbs/ac 0.564 0.085 15.441 5.39 1.034 0.019 1.218 1.788 0.155 29.55 Current Cumulative lbs/ac 0.883 0.125 18.374 6.756 1.158 0.022 1.539 2.405 0.353 35.061 Permitted C. P. L. R.**** 36 34 1 1338 X 1 267 1 15 X 374 1 89 2498 Pet rmi PAN Limit 1st/2n d Crop p 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation c;� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 62.36 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Tom Appenzeller Owner: William Griffin Predominant Soil Series: BdB2-Badin Acres Used: 13.1 Acres Permitted: 13.1 Site #: NC-LJN30 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 2 3 4 5 _6j 7 8 9 101 10/1/19 111 10/1/19 12 % Solids 21.6 30.3 Arsenic 23.1 53.5 Cadmium 4.63 3.3 Copper 293 337 Chromium 105 217 Lead 14.7 9.9 Mercury 0.528 0.0524 Molyb- denum 24.1 52.1 Nickel 77.8 39.9 Selenium 23.1 16.5 Zinc 750 252 Total I Phos- horus 17200 1640 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4 5 6 7 8 9 10 3.12 11 1.64 12 „oy, y Arsenic 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.144 0.175 1 0.000 0.319 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 0.011 0.000 0.040 Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.831 1.103 0.000 2.933 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.656 0.710 0.000 1.366 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.092 0.032 0.000 0.124 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 1 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.151 0.170 0.000 0.321 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.486 0.131 0.000 0.617 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.144 0.054 0.000 0.198 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 4.686 0.825 0.000 5.511 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 107.466 5.366 0.000 112.832 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ;�%� > S' ature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Henry Myers Operator: Same Crop 1 Name: Fescue (Past.) WQ Permit #: WQ0001346 Field #: 3 Annual Dry Tons Applied: 33.0747 Site #: NC-UN31 Predominant Soil Series: BM-Badin Acres Utilized: 2.5 Acres Permitted: 2.5 Cation Exchange Capacity (non 503): N/A Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 y 0 Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, W #, Q Fert. Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs. inches Y ° '- o w a o. o w, K_ N' * w °� 5 w �* w * N• * C TKN mg/kg Z o w o � r, �. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 19 53 74.1 13.230 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 88.605 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 531 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 88.605 1 0.000 Lime Applied Annual lbs/acre 0.258 0.027 7.091 3.519 0.407 0.004 0.474 1.754 0.132 14.950 373.086 :::::::::::::::::::::::::.Date :: :: lbs/ac Prior Years Cumulative lbs/ac 0.71 0.076 11.201 9.399 1.338 0.24 1.141 1.919 1.38 34.469 July 18 2165 Current Cumulative lbs/ac 0.968 0.103 18.292 12.918 1.745 0.244 1.615 3.673 1.512 49.419 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 1 2498 Permit PAN Limit 1 st/2nd Crop P 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inSluding the possibility, of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report +acility Name: 'ermit #: Operator: kcres Used: City of Monroe Total Dry Tons Applied (Annual): WQ0001346 Cation Exchange Capacity (non 503 only): Henry Myers Owner: Same Predominant Soil Series: 2.5 Acres Permitted: 2.5 Site #: NC-UN31 Field #: 33.08 N/A BdB2-Badin 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date 1 2 3 4j 4/1/19 5 6 7 8 _9j LOJ 11 12 % Solids 74.1 Arsenic 1 9.75 admium 1.01 Copper 268 Chromium 133 Lead 15.4 Mercury 0.162 Molyb- denum 17.9 Nickel 66.3 Selenium 5 Zinc 565 Total I Phos- horus 14100 knnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4 13.23 5 j 7 8 9 1 o Ill 12 H Arsenic 0.000 1 0.000 0.000 0.258 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.258 Cadmium 0.000 0.000 0.000 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Copper 0.000 0.000 0.000 7.091 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.091 �hromiu 0.000 0.000 0.000 3.519 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.519 Lead 0.000 0.000 0.000 0.40 00.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.407 Mercury 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.474 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.474 Nickel 0.000 0.000 0.000 1.754 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.754 Selenium 0.000 0.000 0.000 0.132 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.132 Zinc 0.000 0.000 0.000 14.950 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 14.950 Total Phos- horus 0.000 0.000 0.000 373.086 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 373.09 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". gnature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Henry Myers Operator: Same WQ Permit #: WQ0001346 Field #: 4 Annual Dry Tons Applied: 67.8876 Site #: NC-UN31 Predominant Soil Series: BdB2-Badin Acres Utilized: 4.7 Acres Permitted: 4.7 Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 �. ° ° � Q 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D Wei Moist) Precip. Past 24 ems• inches a � c 'L? � F• a *cr Z o 7y P», c �. 0 w `� g * 0 TKN mg/kg Z o as o 0• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 June 19 100 74.1 13.278 WWTPC D 0 S 0.5 1 0.3 10,300 1,270 4.66 88.925 NA Fescue June 19 42 15.5 1.166 WTPC D 0 S 0.5 0.2 18,100 903 112 9.339 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): • TOTALS: 1421 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 98.264 1 o.000 Lime Applied Annuallbs/acre 0.328 0.038 8.262 4.115 0.444 0.004 0.577 1.885 0.191 15.212 380.666 .:. ::::::::::: :.:.: :: .: • • • • Date lbs/ac Prior Years Cumulative lbs/ac 0.77 0.077 12.803 10.477 1.496 0.027 1.306 2.149 0.195 39.706 2-17 1904 Current Cumulative lbs/ac 1.098 0.115 21.065 14.592 1.940 0.031 1.883 4.034 0.386 54.918 Permitted C. P. L. R.**** 36 34 1 1338 1 X 1 267 1 15 X 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 0 Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Henry Myers Owner: Same Predominant Soil Series: Acres Used: 4.7 Acres Permitted: 4.7 Site #: NC-UN31 Field #: 67.89 N/A BdB2-Badin 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 4/1/19 5 4/1/19 6 7 8 9 10 J 11 12 % Solids 74.1 15.5 Arsenic 1 9.75 1 29.6 Cadmium 1.01 5 Copper 268 491 Chromium 133 250 Lead 15.4 15 Mercury 0.162 0.0524 Molyb- denum 17.9 43.5 Nickel 1 66.3 53.5 Selenium 5 25 Zinc 565 1 89.1 Total I Phos- horus 14100 2670 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 21 3 3.28 rn 5 1.17 6 7 8 9 10 11 12 H y Arsenic 0.000 0.000 0.000 .259 0.069 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.328 Cadmium 0.000 0.000 0.000 0.027 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Copper 0.000 0.000 0.000 7.117 1.145 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.262 Mromium 0.000 0.000 0.000 3.532 0.583 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.115 Lead 0.000 0.000 0.000 0.409 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.444 Mercury 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.475 0.101 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.577 Nickel 0.000 0.000 0.000 1.761 0.125 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.885 Selenium 0.000 0.000 0.000 0.133 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.191 Zinc 0.000 0.000 0.000 15.004 0.208 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 15.212 Total Phos- horus 0.000 0.000 0.000 374.440 6.226 0.000 0.000 0.000 0.000 0.000 0.000 0.000 380.67 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". L � �, 4�a� ') -/,p-.)ea j Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Henry Myers Operator: Same Crop 1 Name: corn WQ Permit #: WQ0001346 Field #: 5 Acres Utilized: 17.6 Annual Dry Tons Applied: 231.3180 Site #: NC-UN18 Acres Permitted: 17.6 Predominant Soil Series: TbB2-Tatum Crop 1 Max. PAN: 123 Crop 2 Name: Cation Exchange Capacity (non 503): N/A Crop 2 Max. PAN: 50 Q Volume applied (enter one) Solids/ Liquid 4 Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NpDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, e ' Moist) Precip. past 24 Hrs. inches a a o c * =$ 4 w =° * TKN mg/kg Z Y o E3 °Q ° w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 April 19 195 74.1 6.914 WWTPC D 0 S 0.5 1 0.3 109300 1,270 4.66 46.307 NA Corn May 19 78 74.1 2.766 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 18.523 NA Corn Sept 19 50 21.9 0.524 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 Na 11.834 Wheat Sept 19 225 27.3 2.939 WTPC D 0 S 0.5 0.4 12,300 769 4.58 Na 29.401 Wheat 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 5481 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 64.829 1 41.236 Lime Applied Annual lbs/acre 0.278 0.028 7.317 3.872 0.333 0.003 0.592 1.556 0.249 12.828 300.848::::::::::::::::::::::::::::::::::.Date .................. ........................... : lbs/ac Prior Years Cumulative lbs/ac 1.254 0.151 18.282 20.757 2.123 0.045 2.211 1.7 0.314 48.776 Current Cumulative lbs/ac 1.532 0.179 25.599 24.629 2.456 0.048 2.803 3.256 0.563 61.604 Permitted C. P. L. R.**** 36 34 1 1338 1 X 267 15 X 374 89 2498 i PAN Limst/ 2nd Crop PermLimit1 123 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report acility Name: City of Monroe Total Dry Tons Applied (Annual): 231.32 'ermit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Henry Myers Owner: Same Predominant Soil Series: TbT2-Tatum Acres Used: 17.6 Acres Permitted: 17.6 Site #: NC-UN31 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 [4//1/19 5 6 [7/1/19 8 7/1/19 9 10 11 12 % Solids 74.1 21.9 27.3 Arsenic 9.75 1 10.9 1 13.3 Cadmium 1.01 1 1.27 Copper 268 304 308 Chromium 133 133 197 Lead 15.4 14.9 3.2 Mercury 0.162 0.199 0.0165 Molyb- denum 17.9 24 37.4 Nickel 1 66.3 58.2 36 Selenium 5 5 25 Zinc 565 704 196 Total I Phos- horus 14100 14200 2210 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total I DT/Ac./50. App. Event 1 2 3 4 9.68 5j 7 0.52 8 2.94 9 10 11 12 y 0 14 Arsenic 0.000 1 0.000 0.000 0.189 1 0.000 0.000 0.011 1 0.078 0.000 0.000 1 0.000 0.000 0.278 Cadmium 0.000 0.000 0.000 0.020 0.000 0.000 0.001 0.007 0.000 0.000 0.000 0.000 0.028 Copper 0.000 0.000 0.000 5.188 0.000 0.000 0.319 1.810 0.000 0.000 0.000 0.000 7.317 'hromium 0.000 0.000 0.000 2.575 0.000 0.000 0.139 1.158 0.000 0.000 0.000 0.000 3.872 Lead 0.000 0.000 0.000 0.298 0.000 0.000 0.016 0.019 0.000 0.000 0.000 0.000 0.333 Mercury 0.000 0.000 0.000 0.003 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.347 0.000 0.000 0.025 0.220 0.000 0.000 0.000 0.000 0.592 Nickel 0.000 0.000 0.000 1.284 0.000 0.000 0.061 0.212 0.000 0.000 0.000 0.000 1 1.556 Selenium 0.000 0.000 0.000 0.097 0.000 0.000 0.005 0.147 0.000 0.000 0.000 0.000 0.249 Zinc 0.000 0.000 0.000 10.938 0.000 0.000 0.738 1 1.152 0.000 0.000 1 0.000 0.000 12.828 Total Phos- horus 0.000 0.000 0.000 272.976 0.000 0.000 14.882 12.990 0.000 0.000 0.000 0.000 300.85 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Henry Myers Operator: Same WQ Permit #: WQ0001346 Field #: 6 Acres Utilized: 7.8 Annual Dry Tons Applied: 65.9194 Site #: NC-UN31 Acres Permitted: 7.8 Predominant Soil Series: ChA-Chewacla Crop 1 Name: Corn Crop 1 Max. PAN: 123 Crop 2 Name: Cation Exchange Capacity (non 503): N/A Corn Crop 2 Max. PAN: 50 0 Ca Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs. inches cD 'C$ o m 2. C o N' w w * N TKN mg/kg z a o � w 0 mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type p yp Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 April19 78 74.1 6.241 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 41.795 NA Corn Sept 19 75 27.3 2.211 WTPC D 0 S 0.5 0.4 12,300 769 4.58 Na 22.114 Wheat 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 153 0 :::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 41.795 22.114 Lime Applied Annuallbs/acre 0.181 0.018 4.707 2.531 0.206 0.002 0.389 0.987 0.173 7.919 185.769:::::::::::::::::::::::::::::::::::: .................. ...............I........... : Date lbs/ac Prior Years Cumulative lbs/ac 1.057 0.13 15.027 16.05 1.945 0.036 1.759 2.674 0.27 51.171 Current Cumulative lbs/ac 1.238 0.148 19.734 18.581 2.151 0.038 2.148 3.661 0.443 59.090 Permitted C. P. L. R.**** 36 34 1 1338 1 X 1 267 1 15 1 X 1 374 1 89 1 2498 i Pe rmit PAN Limit 1 st/2nd Crop 123 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation P'`.�LLb)e) **Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 65.93 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Henry Myers Owner: Same Predominant Soil Series: ChA-Chewacla kcres Used: 7.8 Acres Permitted: 7.8 Site #: NC-UN31 Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 2 3 14 4/1/19 5 _6j 1/19 8 9 10 11 12 % Solids 74.1 [71/ 7.3Arsenic 9.75 3.3 Cadmium 1.01 .27 Copper 268 308 Chromium 133 197 Lead 15.4 3.2 Mercury 0.162 0.0165 Molyb- denum 17.9 37.4 Nickel 66.3 36 Selenium 5 25 Zinc 565 196 Total I Phos- horus 14100 2210 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App• Event 1 2 3] L4J 6.24 5 _6j 7 j81 2.21 9 10 11 12 y Arsenic 0.000 1 0.000 0.000 0.122 1 0.000 0.000 0.059 0.000 0.000 0.000 0.000 0.000 1 0.181 Cadmium 0.000 1 0.000 0.000 0.013 0.000 0.000 0.006 0.000 0.000 0.000 0.000 0.000 0.018 Copper 0.000 0.000 0.000 3.345 0.000 0.000 1.362 0.000 0.000 0.000 0.000 0.000 4.707 "hromium 0.000 0.000 0.000 1.660 0.000 0.000 0.871 0.000 0.000 0.000 0.000 0.000 2.531 Lead 0.000 0.000 0.000 0.192 0.000 0.000 0.014 0.000 0.000 0.000 0.000 0.000 0.206 Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.000 0.000 0.000 0.223 0.000 0.000 0.165 0.000 0.000 0.000 0.000 0.000 0.389 Nickel 0.000 0.000 0.000 0.828 0.000 0.000 0.159 0.000 0.000 0.000 0.000 0.000 0.987 Selenium 0.000 0.000 0.000 0.062 0.000 0.000 0.111 0.000 0.000 0.000 0.000 0.000 0.173 Zinc 0.000 1 0.000 0.000 7.052 1 0.000 0.000 0.867 0.000 0.000 0.000 0.000 0.000 7.919 Total Phos- horus 0.000 0.000 0.000 175.996 0.000 0.000 9.773 0.000 0.000 0.000 0.000 0.000 185.769 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ignature of Land Applier w� Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Danny Baker Operator: Same Crop 1 Name: Fescue (past.) WQ Permit #: WQ0001346 Field #: 2 Acres Utilized: 15.5 Annual Dry Tons Applied: 131.6232 Site #: NC-UN32 Acres Permitted: 15.5 Predominant Soil Series: GoB-Golston Crop 1 Max. PAN: 122 Crop 2 Name: Cation Exchange Capacity (non 503): N/A Fescue Crop 2 Max. PAN: 50 &, ° +� ° >~ Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons oho Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NpDES #, WQ#,Past Fert., Animal Waste, etc) Soil Cond.p D We ' Moist) Preci 24 Hrs. inches 4 'a L? a w * C ° w `- * N °� 4 ;0 w �, ?� TKN mg/kg z a o w c mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of CropT yPe Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 May 19 190 74.1 7.650 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 51.232 NA Fescue May 19 100 15.5 0.842 WTPC D 0 S 0.5 0.4 18,100 903 112 12.535 NA Fescue 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 2901 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 63.768 0.000 Lime Applied Annual lbs/acre 0.199 0.024 4.927 2.456 0.261 0.003 0.347 1.104 0.119 8.795 220.226 :::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.199 0.024 4.927 2.456 0.261 0.003 0.347 1.104 0.119 8.795 Permitted C. P. L. R.**** 1 36 1 34 1 1338 X 1 267 1 15 1 X 374 1 89 2498 Permit PAN Limit 1 st/2nd Cro P 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 1 *Application Method: S - Surface, IN - Injection, INC - Incorporation �q pAl�J **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: Danny Baker Owner: Same Predominant Soil Series: kcres Used: 15.5 Acres Permitted: 15.5 Site #: NC-UN32 Field #: 131.63 N/A BdB2-Badin 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 2 3 4 4/1/19 5 4/1/19 6 7 8j 9 10 11 12 % Solids 74.1 15.5 Arsenic 9.75 29.6 Cadmium 1.01 5 Copper 268 491 Chromium 133 250 Lead 15.4 15 Mercury 0.162 0.0524 Molyb- denum 17.9 43.5 Nickel 66.3 53.5 Selenium 5 25 Zinc 565 89.1 Total I Phos- horus 14100 2670 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ APP• Event 1 2 3j L4 7.65 5 0.84 6 7 81 9 Lj 11 12 c Arsenic 0.000 1 0.000 0.000 0.149 1 0.050 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.199 Cadmium 0.000 0.000 0.000 0.015 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 Copper 0.000 0.000 0.000 4.100 0.827 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.927 �hromium 0.000 0.000 0.000 2.035 0.421 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.456 Lead 0.000 0.000 0.000 0.236 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.261 Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.274 0.073 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.347 Nickel 0.000 0.000 0.000 1.014 0.090 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.104 Selenium 0.000 0.000 0.000 0.077 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.119 Zinc 0.000 0.000 0.000 8.645 0.150 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 8.795 Total Phos- horus 0.000 0.000 0.000 215.730 4.496 0.000 0.000 0.000 0.000 0.000 0.000 0.000 220.226 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". �ggn�ature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Danny Baker Operator: Same Crop 1 Name: Fescue (past.) WQ Permit #: WQ0001346 Field #: 3 Acres Utilized: 10 Annual Dry Tons Applied: 140.9015 Site #: NC-UN32 Acres Permitted: 10 Predominant Soil Series: GoB-Golston Crop 1 Max. PAN: 122 Crop 2 Name: Cation Exchange Capacity (non 503): N/A Fescue Crop 2 Max. PAN: 50 ° ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tans/Ac) Residual Sources (NPDES # WQ#, Fert., Animal Waste, etc) Soil Cond. ( ry, Wet, Moist) Precip. Past 24 Hrs. inches Y b � `� o w o %n N' 4 :' * N � �• TKN mg/kg Z Y c � w mg/kg Nitrate and Nitrite mg/kg PAN Applied (Ibslacre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 19 217 74.1 13.542 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 90.694 NA Fescue May 19 42 15.5 0.548 WTPC D 0 S 0.5 0.4 18,100 903 112 8.161 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): .......... .... . . TOTALS: 2591 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 98.8551 0.000 Lime Applied Annuallbs/acre 0.297 0.033 7.797 3.876 0.434 0.004 0.532 1.854 0.163 15.400 384.811 ::::::::::::::::::::::::::..::: Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.297 1 0.033 7.797 3.876 0.434 0.004 0.532 1.854 0.163 15.400 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit lst/2nd Crop ::.:. :::: :::::...:::::::: ::::::::::::::::::... . • : 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date **X Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 140.90 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Danny Baker Owner: Same Predominant Soil Series: GsB- Goldston Acres Used: 10 Acres Permitted: 10 Site #: NC-UN32 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 __2j 3j 4 4/1/19 5 4/1/19 61 7 81 9 10 Lj 12 % Solids 74.1 1 15.5 Arsenic 9.75 29.6 admium 1.01 5 Copper I 268 491 hromium 133 250 Lead 15.4 15 Mercury 0.162 0.0524 Molyb- denum 17.9 43.5 Nickel 66.3 53.5 Selenium 5 25 Zinc 565 89.1 Total I Phos- horus 14100 2670 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ APP• Event 1 2 3 4 13.54 5 0.55 6 7 8 9 10 11 12 H r+ y Arsenic 0.000 0.000 0.000 0.264 1 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.297 Cadmium 0.000 0.000 0.000 0.027 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033 Copper 0.000 0.000 0.000 7.259 0.538 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.797 "hrornium 0.000 0.000 0.000 3.602 0.274 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.876 Lead 0.000 0.000 0.000 0.417 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.434 Mercury 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- denum 0.000 0.000 0.000 0.485 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.532 Nickel 0.000 0.000 0.000 1.796 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.854 Selenium 0.000 0.000 0.000 0.135 1 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.163 Zinc 0.000 0.000 0.000 15.302 0.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 15.400 Total Phos- horus 0.000 0.000 0.000 381.884 2.926 0.000 0.000 0.000 0.000 0.000 0.000 0.000 384.811 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe Land Owner: Danny Baker Operator: Same Crop 1 Name: Fescue (past.) WQ Permit #: WQ0001346 Field #: 4 Annual Dry Tons Applied: 33.0747 Site #: NC-UN32 Predominant Soil Series: GoB-Golston Crop 1 Max. PAN: 122 Crop 2 Name: Acres Utilized: 3.2 Acres Permitted: 3.2 Cation Exchange Capacity (non 503): N/A Fescue Crop 2 Max. PAN: 50 +� >~ q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. D ( ry' Wet, Moist) Precip. Past 24 �S• inches Y n cy 'd a F. * o ° o w * w 4 7y ?� -+ �, w * N' TKN mg/kg X Y o ao o w• mglkg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 May 19 53 74.1 10.336 WWTPC D 0 S 0.5 0.3 10,300 1,270 4.66 69.222 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ............ .. TOTALS: 531 0 :::...:::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 69.222 0.000 Lime A lied Annual lbs/acre 0.202 0.021 5.540 2.749 0.318 0.003 0.370 1.371 0.103 11.680 291.475 ::::::::: :::::::::: :::::: ".. Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.202 0.021 5.540 2.749 0.318 0.003 0.370 1.371 0.103 11.680 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit 1 st/2nd Crop P 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe 'ermit #: WQ0001346 Operator: Danny Baker Owner: kcres Used: 3.2 Acres Permitted: Total Dry Tons Applied (Annual): 33.08 Cation Exchange Capacity (non 503 only): Same Predominant Soil Series 3.2 Site #: NC-UN32 Field #: N/A GsB - Goldston 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 12131 [4/1/19 5 6 7 8 9 10 11 12 % Solids 74.1 Arsenic 9.75 Cadmium 1.01 Copper 268 Chromium 133 Lead 15.4 Mercury 0.162 Molyb- denum 17.9 Nickel 66.3 Selenium 5 Zinc 565 Total Phos- horus 14100 nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 11 1 21 31 0.34 rn 5 6 7 8 9 10 Ill 12 Arsenic 0.000 0.000 0.000 .202 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.202 Cadmium 0.000 0.000 0.000 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Copper 0.000 0.000 0.000 5.540 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.540 'hromium 0.000 0.000 0.000 2.749 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.749 Lead 0.000 0.000 0.000 0.318 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.318 Mercury 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.000 0.000 0.000 0.370 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.370 Nickel 0.000 0.000 0.000 1.371 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 1.371 Selenium 0.000 0.000 0.000 0.103 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.103 Zinc 0.000 0.000 0.000 11.680 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 11.680 Total Phos- horus 0.000 0.000 0.000 291.475 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 291.475 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ature of Lan Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 5 Land Owner: Theodore Funderburk Annual Dry Tons Applied: 21.5790 Site #: NC-UN33 Acres Permitted: 5.0 Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (past.) Crop 1 Max. PAN: 123 Crop 2 Name: fescue Crop 2 Max. PAN: 50 o = Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons o �u Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, e ' Moist) precip. past 24 Hrs. inches a a o ° 2 � - `-° , * 0 TKN mg/kg z 3 o do o F, mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 July 19 117 21.9 4.316 WWTPC D 0 S 0.5 0.3 35,200 3,560 21.2 97.478 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 1171 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 97.478 r 0.00o Lime Applied Annuallbs/acre 0.094 0.009 2.624 1.148 0.129 0.002 0.207 0.502 0.043 6.077 122.574:::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.094 0.009 2.624 1.148 0.129 0.002 0.207 0.502 0.043 6.077 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit 1 st/ 2nd Crop 123 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance wrtn a system aesignea to assure tnat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1--.1, ---,.�05/ *Application Method: S - Surface, IN - Injection, INC - Incorporation Z2 `IP'��,d **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report "acility Name: City of Monroe 'ermit #: WQ0001346 Operator: Theodore Funderburk Owner: Lcres Used: 5 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Same Predominant Soil Series: 5 Site #: NC-UN33 Field #: 21.58 N/A 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ample or Com- posite Date 1 2 3 1 4 5� 6 7 7/ 1 / 19 8 9 10 11 121 /o Solids 21.9 Arsenic 10.9 :admium 1 Copper 304 Chromium 133 Lead 14.9 Mercury 0.199 Molyb- denum 24 Nickel 58.2 Selenium 5 Zinc 704 Total I Phos- horus 14200 knnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 2 3 4! 51 6 7 4.32 8 9 10 11 ! 12 ° 14 Arsenic 0.000 1 0.000 0.000 0.000 1 0.000 0.000 1 0.094 1 0.000 0.000 1 0.000 0.000 0.000 0.094 admium 0.000 0.000 0.000 0.000 0.000 0.000 0.009 0.000 0.000 0.000 0.000 0.000 0.009 Copper 0.000 0.000 0.000 0.000 0.000 0.000 2.624 0.000 0.000 0.000 0.000 0.000 2.624 hromiurn 0.000 0.000 0.000 0.000 0.000 0.000 1.148 0.000 0.000 0.000 0.000 0.000 1.148 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.129 0.000 0.000 0.000 0.000 0.000 0.129 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.000 0.000 0.000 0.000 0.000 0.000 0.207 0.000 0.000 0.000 0.000 0.000 0.207 Nickel 0.000 0.000 0.000 1 0.000 0.000 0.000 0.502 0.000 0.000 0.000 0.000 0.000 0.502 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.043 0.000 0.000 0.000 0.000 0.000 0.043 Zinc 0.000 0.000 0.000 0.000 0.000 0.000 6.077 1 0.000 0.000 0.000 0.000 0.000 1 6.077 Total Phos- horus 0.000 0.000 0.000 0.000 0.000 0.000 122.574 0.000 0.000 0.000 0.000 0.000 122.574 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. [ am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". /V so9od d a ure of Land Applier Date DENR FORM MFLSF (12/2006) Volatile Solids Reduction 2018 Van Kleek equation In (RAS) - Out (digested sludge) _ In (RAS) - (In * Out) (digested sludge) _ 1st 90 days RAS digested sludge IN- OUT 0.6650 0.5060 0.159 IN- (IN -OUT) 0.665 0.33649 0.32851 2nd 90 days IN - OUT 0.7150 0.0337 0.6813 lReduction IN- (IN -OUT) 1 98.61% 0.715 0.024096 0.690905 3rd 90 days IN - OUT 0.7540 0.5340 0.22 lReduction IN- (IN -OUT) 1 62.61% 0.754 0.402636 0.351364 4th 90 days IN - OUT 0.7490 0.5040 0.245 1 Reduction IN- (IN -OUT) L 65.95% 0.749 0.377496 0.371504 AM P/i PROM PT- A CCU RATE• RELIABLE LABORATORIBS, INC W W W.PARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JAN 19 PO BOX 69 DATE: 01/28/19 MONROE, NC 28111- SAMPLE NUMBER- 1345'71 SAMPLE 1=r>- MONROE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 01/09/19 TIME SAMPLED- 0842 DATE RECEIVED- 01/09/19 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 1020 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 01/09/19 1545 RE 2,221 MPN/g LABORATORY DIRECTOR 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 PA&F;Z PROM PT•ACCU RATE- RELIABLE LABORAT'ORIBS, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20, SC Cert # 99003001 • CITY OF MONROE • MONROE WWTP • 01/09/19 FECAL COLIFORM, GEOMETRIC MEAN • • SM 9221 E 7 W-11:1 I I �'� 134571 Fecal Coliform LGeometric Mean= 1 429 16.36% 2,620.45 2 408 19.61 % 2,082.49 3 334 18.71 % 1,783.39 4 433 17.40% 2,489.00 5 429 17.31 % 2,480.85 6 355 19.36% 1,831.97 7 437 18.06% 2,418.63 Lmi���j ;q CHAIN OF CUSTODY soRAroRrPAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.partabs.com Shippinc: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 t IS essential that ail information be recorded on this Chain o` Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina Department of Enviror—emal and Natural Resources. Ccmpany Name Wining) City of Monroe Comments/ Special Instrtictions Address PO Box 69 503 BIOSOLIDS City. State & Zip code Monroe. NC 28111 REPORTING Point of Contact & i eiephone Steve Holden l 704) 252-4679 shoidenDo iionroenc.on, Sample Taken By: 0f! �Q�fiV IS THIS FOR STATE or EPA REPORTING? YES NO "Sample type: DW __ WW )C GWMW _ HW Soil other Sample Temp at time of sampfing: /J._T *C Sample Temp upon receip��i °C `# Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes — No NIA X Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested # I WWT'P X NONE : y� FECAL COLIFORM # 2 WWTP X NONE . y FECAL COLIFORM # 3 WWTP X NONE FECAL COLIFORM # 4 WV✓TP , - X NONE ,yS FECAL COLIFORM # 5 WWTP X NONE �. y FECAL COLIFORM # 6 WWTP X NONE _ - , FECAL COLIFORM # 7 X NONE -� FECAL COLIFORM uished by: 3elinquished by: Date/Time Received by: Da teTme DateTme C=Corttposite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well Ht.V=Hazardous Waste See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WWTP Name: Monroe WWTP cake WQ Permit Number: NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 1/1/2019 To 3/31/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ElAlternative 6 El If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 0 Alternative 2 ❑ ........................ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion 0 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Num er o Excee- Frequency of Analysis y Sample Type Analytical Tech- nioue Minim Geo. Mean aximuences Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 1,783.39 2,221 2,620.45 MGN/g 0 bimonthly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei ht Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) i] Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Ap lier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WWTP Name: WWTP cake NPDES Number: Monitoring Period: From 1/1/2019 To 3/31/2019 WQ0001346 NCO024333 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑............ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑J Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion 0 Anaerobic Digestion ❑ ......................................................................................................................................... . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type Analytical Tech - maue Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 1,783.39 2,221 2,620.45 MPN/g 0 bimonthly grab sm9221 e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 4y� lit- 3- 14.)0 o?Ya-.; IsJ Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) AM PLL PROM PT -ACCURATE- RELIABLE LABORATORIES, INC W W W.PARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: APR 19 PO BOX 69 DATE: 05/20/19 MONROE, NC 28111- SAMPLE NUMBER- 135418 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 04/01/19 TIME SAMPLED- 0825 DATE RECEIVED- 04/01/19 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 1022 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 04/01/19 1350 RE 3,579 MPN/g LABORATORY DIRECTOR f 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 PbLF;Z PROM PT•ACCU RATE• RELIABLE LABORATORIES' INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE MONROE WWTP • 04/01 /19 FECAL COLIFORM, GEOMETRIC MEAN • SM 9221 E 135418 1 592 16.45% 3,597.72 2 611 16.78% 3,643.89 3 595 16.30% 3,648.48 4 623 17.34% 3,595.35 5 539 16.86% 3,196.09 6 587 16.76% 3,500.14 7 648 16.58% 3,907.98 Fecal Coliform Geometric Mean= • [�?� ;CHAIN OF CUSTODY TORPAR Laboratories, Inc � Phone (704) 588-8333 Fax (704) 588-8335 www.partabs.com Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlo ke, NC 26273 Charlotte, NC 28241-1483 , is essential that ail information be recorded on this Chain of Custody docursent for acceptance by PAR Laboratories, Inc. and the North Carolina Deoariment of Environrnemal and Nowral Resources. Ccnnpany Name Ibifiing) City of NZotuoe Comments/ Special Instructions - Address PO BOX 69 503 BIOSOLIDS City. State & zip code Monroe. NC 28111REPORTING Point of Contact & i efophone-r Steve Holden � 704 ) 282-4679 sholden@monroenc.or" Sample Taken By: IS THIS FOR STATE or EPA REPORTING? YE_S .—,� NO "Sample type: DW WW )C GWMW _ HW Soil other / Sample Temp at time of sampling: 3. �C Sample Temp upon receipt: °C Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes — No N/A X Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested # I wWTP X NONE y, $. Z FECAL COLIFORM # 2 WWTP X NONE g , Z FECAL COLIFORM # 3 wWTP X NONE lq , Z FECAL COLIFORM # 4 WWTP - X NONE : 2 FECAL COLIFORM # 5 WViTP X NONE ell l FECAL COLIFORM # 6 WWTP X NONE ; Z FECAL COLIFORM # 7 )A'',Xf'P X NONE , Q : 2 FECAL COLIFORM ?elfin wished by: Date/Time Receiv b - DateTme �y relinquished by: D efTime Received by: DateTme C=Ccrnposrte G=Grab DW=Drinking Water WW=Wastewaier GWMW=Groundwater Monitoring Well H'.V=Hazardous Waste See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: WWTP cake NPDES Number: NCO024333 Monitoring Period: From 4/l/2019 To 6/30/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)[] Alt. C (Prior Testing)[] AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray 01 Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion 0 Anaerobic Digestion ❑ .............................................................................................................. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number ot Excee- encesY Frequency of Analysis Sample Type a ytica Tech- niaue Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 3,196.09 3,579 3,907.98 MPN/g 0 bimonthl grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) v❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Wt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) * It - Signature of Preparer* Steve Holden, Residual Coordinator Land Apo 'er Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WWTP Name: Monroe WWTP cake WQ Permit Number: NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 4/1/2019 To 6/30/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: Alternative 1 21 Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting El Aerobic Digestion 0 Anaerobic Digestion ❑ __.. .... _ .___... _ _ _ _.. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ot Excee- Frequency of Analysis Y Sample Type Analytical Tech - woue Minimum Geo. Mean aximu Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 3,196.09 3,579 3,907.98 MGN/g 0 bimonthly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date rgnature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) P,&IR PROM PT- A CC U RATE -RE LIABLE LABORATORIES, INC W W W.PARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JUL 19 PO BOX 69 DATE: 07/12/19 MONROE, NC 28111- SAMPLE NUMBER- 136384 SAMP',F TD- MONROE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 07/02/"19 TIME SAMPLED- 0843 DATE RECEIVED- 07/02/19 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 1017 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 07/02/19 1515 RE 3,939 MPN/g LABORATORY DIRECTOR E/ �� �,... ,r ,� _✓ �a-- 0 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 PAR PROMPT- A CCU RATE- REL.IA BL-E LABOE2_A�'ORI)�i5� iNC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20, SC Cert # 99003001 CITY OF MONROE MONROE WWTP A 07/02/19 FECAL COLIFORM, GEOMETRIC MEAN SM 9221 E 7 W-1 I : I I I �.� 136384 1 634 15.89% 3,990.57 2 682 16.07% 4,246.30 3 649 15.96% 4,066.01 4 597 16.10% 3,708.11 5 594 16.20% 3,667.84 6 654 15.98% 4,090.13 7 612 15.94% 3,841.77 Fecal Coliform Geometric Mean= • • L.J R CHAIN OF CUSTODY ATOMPAR Laboratories, Inc � Phone (704) 588-8333 Fax (704) 588-8335 www.parfabs.com Shippinc: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 ., �s essential that ail information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North Carolina Deoartment of Environmental and Natural Resources. Conpzny game (billing) Comments/ Special Instructions City of Monroe Address PO Box 69 City. Stale & zip code Monroe. N-C 28111 Point of Contact & Telephone'-.___ Steve Holden ( 704 ) 252-4679 sliolden@monroenc.oi- Sample Taken By: S'f Lo E— '440 503 BIOSOLIDS REPORTING IS THIS FOR STATE or EPA REPORTING? YES „DX— NO *Sample type: DW WW GWMW HW Soil other Sample Temp at time of sampfing: °C Sample Temp upon receipt j;lap - °C_ `* Preserved: Yes _ No X Te Ion liner/ Zero HeadsQace: Yes _ No NIA—X Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested # 1 WWTP X NONE _ _l g.FECAL COLIFORM # 2 WWTP X NONE _/ FECAL COLIFORM # 3 WWTP X NONE 7 -.2_1 -, FECAL COLIFORM n 4 WWTP, - X NONE �,, FECAL COLIFORM # 5 WWTP X NONE yS FECAL COLIFORM # 6 WWTP X NONE y FECAL COLIFORM # 7 ww rn X NONE 8: V FECAL COLIFORM by: / // Daterrime Received by: aelinquished by: DatefTime/ Received by: Da lime DatefTime C=Ccrttposite G=Crab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well WV=Hazardous Waste See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake Monitoring Period: From 7/l/2019 WQ Permit Number: NPDES Number: To 9/30/2019 WQ0001346 NCO024333 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ TAlt. C (Prior Testing)❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ GatnaLRay ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": . Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er o dencesExcee- Frequency of Analysis Sample Type Analytical Tech- nioue MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 3,667.84 3,939 4,246.30 MPN/g 0 bimonthly Grab SM9221 E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Preparer Name and Title (type or print) Steve Holden, Residual Coordinator Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: From 7/1/2019 To 9/30/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 0 Alternative 2 ❑ .......................... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion 0 Anaerobic Digestion ❑ ............... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number o Excee- Frequency of Analysis Y Sample Type na ytica Tech - maue Minimum Geo. Mean aximu Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 3,667.84 3,939 4,246.30 MGN/g 0 bimonthly grab sm9221 e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ jAlt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ElAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) t] "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preeparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) DENR FORM PVRF 503 (12/2006) PLLF;Z PRO MPT•ACCU RATE• RELIABLE LABORATORIES, INC W W W.PARLABS.COM REPORT OF' ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: OCT 19 PO BOX 69 DATE: 10/11/19 MONROE, NC 28111- SAMPLE NUMBER- 137179 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW DATE SAMPLED- 10/01/19 TIME SAMPLED- iu48 DATE RECEIVED- 10/01/19 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 1236 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 10/01/19 1555 RE 7,531 MPN/g LABORATORY DIRECTOR i 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 PA&F;Z PROMPT- A CCU RATE- REL I^E3L..E I. ABOIZATORI-ES, .INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CITY OF MONROE MONROE WWTP 10/01/19 FECAL COLIFORM, GEOMETRIC MEAN • SM 9221 E 137179 1 1,425 18.86% 7,554.11 2 1,423 18.45% 7,711.89 3 1,372 18.17% 7,553.26 4 1,297 18.73% 6,926.81 5 1,395 17.96% 7,764.82 6 1,402 17.99% 7,790.67 7 1,347 18.08% 7,452.13 Fecal Coliform Geometric Mean= L ORfES, INC. www.partabs.com Shippinc: 2217 Graham Park Drive Charlo<e, NC 28273 CHAIN OF CUSTOD Y PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Mailing: PO Box 411483 Charlotte, NC 28241-1483 t !s essential that all information be recorded on ;his Chain of Custody document :or acceptance by PAR Laboratories. Inc. and the North .-Carolina Daoart-ent O: E—irommental and Natural Resovrces. Conpany Name Ib-,Mngl City of MonroeComments/ Special Instluctions Address PO Box 69 503 BIOSOLIDS City. Stare &zip code Monroe. NC 28111 REPORTING I _ � Point of Contact & Telephone'c.--_.-- _.. _ _ Steve Holden ( 704 ) 282-4679 sholden@monroenc.on, Sample Taken By: 5 ., )S k4C-)1J'C IS THIS FOR STATE or EPA REPORTING? YES X_ NO "Sample type: DW WW )C GWMW _ HW Soil other Sample Temp at time of sampring: afJ°C Sample Temp upon receipu . Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes — No NIA X Client Sample I.D. Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested # t WWTP X NONE jo_ I _ 9 9 FECAL COLU70RM # 2 WWTP X NONE I _ FECAL COLMORM # 3 WWTP X NONE p_ y/ FECAL COLIFORM # 4 WWTT , - X NONE _ y FECAL COLIFORM # 5 WWTP X NONE FECAL COLIFORM # 6 WWTP X NONE 9 FECAL COLIFORM n 7 WWTP X NONE _ 1,2 FECAL COLIFORM Relinquished by: Dated ime Received b : DatelTme o- -i /74 /o-al-M. /,;t ?elinquished by: Daterfi a Received by: Dateffime C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HIN=Hazardous Waste See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake Monitoring Period: WQ Permit Number: WQ0001346 NPDES Number: NCO024333 From 10/1/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) D 1 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)[] Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density 0 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": V Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion 0 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er o dences Excee- Frequency of Analysis Sample Type Analytical Tech - maue MinimumGeo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 6,926.81 7,531 7,790.67 MGN/g 0 bimonthl grab sm9221 e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WWTP Name: Monroe WWTP cake WQ Permit Number: NPDES Number: WQ0001346 NCO024333 Monitoring Period: From 10/1/2019 To 12/31/2019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ G am.ZLRay ❑ Pasteurization ❑ Class B: Alternative 1 0 Alternative 2 ❑ ............................... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion 0 Anaerobic Digestion ❑ .._..._... __ ................ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- Frequency of Analencesysis Sample Type Analytical Tech - MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 6,926.81 7,531 7,790.67 MGN/g 0 bimonthly grab sm9221e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei ht Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable)m ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were perfored ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Yt �/131400 �Irll-- Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) Sodium Calcium %Solids, Na, Na, Ca, Magnesium, Date/ Sample decimal mg/kg mg/I Na, meq/L mg/kg Ca, mg/I Ca, meq/L Mg, mg/kg Mg, mg/I Mg, meq/L SAR WWTP 1-8-19 0.142 731 103.81 4.51 10600 1505.2 75.26 WWTP 4-1-19 0.741 447 331.23 14.40 8470 6276.27 313.81 WWTP 7-1-19 0.219 555 121.55 5.28 10200 2233.8 111.69 WWTP 10-1-19 0.216 1160 250.56 10.89 12200 2635.2 131.76 0 0.00 0 0.00 WTP 1-8-19 0.17 610 0 103.7 0.00 4.51 2070 0 351.9 0.00 17.60 4 WTP 4-1-19 0.155 1250 193.75 8.42 2060 319.3 15.97 WTP 7-1-19 WTP 10-1-19 0.273 368 100.46 4.37 3140 857.22 42.86 0.303 825 249.98 0 10.87 0.00 2300 696.9 0 34.85 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 0 0.00 1620 230.04 18.86 0.66 1560 1155.96 94.75 1.01 1450 317.55 26.03 0.64 2100 453.6 37.18 1.19 0 0.00 #DIV/0! 0 0.00 #DIV/0! 539 91.63 7.51 1.27 524 81.22 6.66 2.50 470 128.31 10.52 0.85 538 163.014 13.36 2.21 y 0 0.00 #DIV/0! 0 0.00 #DIV/01 0 0.00 #DIV/0! 0 0.00 #DIV/0! Exchangeable Sodium Percentage ESP = {(Na)/ (Ca+Mg+K+Na)) x 100 Field {(Na) /(Ca+Mg+K+Na)}x100 ESP NC-AN-19-1 A/ (70.6+15+1.5+.4) X 100 .45 NC-UN-18-1 .4 / (70.5+16.7+3.2+.4) X 100 .44 NC-UN-18-2 .3 / (71.5+16.3+3.2+.3) X 100 .32 NC-UN-18-7 .6/ (62.4+20.0+1.5+.6) X 100 .71 NC-U N-25-1 .8 / (60.8+19.7+1.2+.8) X 100 .97 NC-UN-25-3 .8 / (60.6+19.9+1.1+.8) X 100 .97 NC-UN-26-1 .6 / (63.3+17.9+1.2+.6) X 100 .72 NC-UN-26-2 .6 / (64.8+17.9+1.4+.6) X 100 .71 NC-UN-26-3 .5 / (62.1+17.7+2.6+.5) X 100 .60 NC-UN-26-4 .5 / (61.6+16.4+2.2+.5) X 100 .62 NC-UN-26-6 .8 / (58.5+17.8+1.5+.8) X 100 1.02 NC-UN-29-1 1.1 / (60.3+23.6+1.9+1.1) X 100 1.27 NC-UN-29-2 1.1 / (62.4+23.1+1.6+1.1) X 100 1.34 NC-UN-29-3 .5 / (58+23.8+6.5+.5) X 100 .56 NC-UN-30-1 .5 / (58.1+23.5+7.0+.5) X 100 .56 NC-UN-31-3 .4 / (57.1+17.5+4+.4) X 100 .51 NC-UN-31-4 .4 / (54.7+15.9+3.5+.4) X 100 .54 NC-UN-31-5 .5 / (72.3+20.5+2.3+.5) X 100 .52 NC-UN-31-6 .4 / (73.1+21.5+2.2+.4) X 100 .41 NC-UN-32-2 1.6 / (65.6+15.7+3.4+1.6) X 100 1.85 NC-UN-32-3 .7 / (65.1+18.9+6.1+.7) X 100 .77 NC-UN-32-4 .6 / (59.5+17.4+5.6+.6) X 100 .72 NC-UN-33-1 1.2 / (60.9+22.5+1.4+1.2) X 100 1.40 Page 1 of 1 Report Number: 20-028-0852 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 Waypoint0 ANALYTICAL Every acre... Every year". Farm: AN-19 SOIL ANALYSIS REPORT Date Of Analvsis: 01/29/2020 Date Of Report: 01/29/2020 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Calvin Moris 554 Hasty Road Peachland NC 28133 Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NC = North Carolina Fertility Index Value OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ova Soil M3 K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g meq/100g 19-1 09383 11.1 150 256 VH 86 L 262 M 2061 H 14 VL 6.2 1.8 14.6 VH INC =213 NC=44 1 M-O Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID K Mg Ca Na H NO, N S Zn Mn Fe Cu B SS Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 19-1 1.5 15.0 70.6 0.4 12.3 16 M 32.0 VH 28 H 272 VH 6.7 VH 1.0 M 0.15 VL INC =33 NC=800.0 INC =175 INC =335.0 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Date Received: 01/28/2020 nato Of Rpnnrt: oilm2n20 Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypolntAnalytical Virginia, Inc. Salts ms/cm x 640 = ppm. SOIL FERTILITY RECOMMENDATIONS by: Ppuria r F i14- 4 Pauric McGroary Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop veld Goal Lime N P 2 O s K2 O Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 19-1 Fescue Hay 4 0.0 1 200 0 1 130 0 9 0 3 0 0 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Page 1 of 2 Report Number: 20-028-0851 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 • Waypoint ANALYTICAL Every acre... Every year. " 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Ben Myers 3208 Helms Pond Road Monroe NC 28110 Farm: UN-18 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 01/28/2020 Date Of Analysis: 01/29/2020 Date Of Report: 01/29/2020 NC = North Carolina Fertility Index Value OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number o �° Rate Soil Class lbs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meq/100g meq/100g 18-1 09380 10.0 150 530 VH 166 H 269 H 1889 H 11 VL 6.4 1.2 13.4 VH NC = 442 NC = 85 I M-O 18-2 09381 9.3 150 487 VH 170 H 270 H 11973 H 10 VL 6.4 1.2 13.8 VH NC = 406 NC = 87 M-O 18-7 09382 4.4 126 174 VH 46 VL 195 H 1011 M 12 VL 6.0 6.81 1.2 8.1 MH NC = 145 NC = 24 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K ,fie Mg % Ca ova Na % H o/, NO3N PP m Rate S PP m Rate Zn PP m Rate Mn PP m Rate Fe PP m Rate Cu PP m Rate B PP m Rate SS ms/cm Rate 18-1 3.2 16.7 70.5 0.4 9.0 9 VL 34.1 VH 15 M 328 VH 10.2 VH 1.0 M 0.11 VL NC=19 NC=852.5 NC=94 NC=510.0 18-2 3.2 16.3 71.5 0.3 8.7 12 L 31.6 VH 14 M 315 VH 9.7 VH 1.0 M 0.13 VL NC = 25 NC = 790.0 NC = 88 NC = 485.0 18-7 1.5 20.1 62.4 0.6 14.8 12 L 11.6 VH 9 L 430 VH 1.8 H 1.0 M 0.11 VL 1 NC=25 NC=290.0 NC=56 NC=90.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ppplia or Gewr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 20-028-0851 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 Date Of Report: 01/29/2020 Waypoi nt .0 ANALYTICAL "Every acre... Every year. "� Farm: UN-18 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Ben Myers 3208 Helms Pond Road Monroe NC 28110 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop veld Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 18-1 Fescue Hay 4 0.0 200 0 40 0 11 0 4 0 0 0 18-2 Fescue Hay 4 0.0 200 0 40 0 10 0 4 0 0 0 18-7 Fescue Hay 4 0.8 200 0 160 0 10 0 4 0 0 0 Comments: Sample(s) : 18-2,18-7 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." MM / Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 Report Number: 20-028-0846 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Waypoint,0 ANALYTICAL "Every acre... Every year. "rM 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Wayne McBride 3303 Trinity Church Road Monroe INC 28112 Farm: UN-25 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 01/28/2020 Date Of Analysis: 01/29/2020 Date Of Resort: 01/29/2020 NC = North Carolina Fertility Index Value OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab o �0 Soil M3 K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 25-1 09367 5.1 142 72 H 31 VL 163 H 839 M 12 VL 5.9 6.81 1.2 6.9 H NC=60 NC=16 I MIN 25-3 09369 5.1 142 69 H 29 VL 165 H 836 M 13 VL 5.9 6.81 1.2 6.9 HH NC = 57 NC = 15 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID K Mg Ca Na H NO, N S Zn Mn Fe Cu B SS Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 25-1 1.2 19.7 60.8 0.8 17.4 6 VL 11.9 VH 14 M 279 VH 10.0 VH 0.7 M 0.1 VL NC=12 NC=297.5 INC =88 NC=500.0 25-3 1.1 19.9 60.6 0.8 17.4 10 L 11.4 VH 17 M 284 VH 9.4 VH 0.6 M 0.11 VL 1 1 1 NC=21 NC=285.0 NC=106 NC=470.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pwµ , to Gg-r H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 20-028-0846 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 Date Of Renort: 01/29/2020 Waypoi nt ..0 ANALYTICAL "Every acre... Every year. "- Farm: UN-25 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Wayne McBride 3303 Trinity Church Road Monroe NC 28112 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 KZO Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 25-1 Fescue Hay 4 0.8 200 0 179 0 14 0 4 0 0 0 25-3 Fescue Hay 4 0.8 200 0 180 0 11 0 4 0 0 0 Comments: Sample(s) : 25-3 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 14t�+�« ,r•` �� work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 Report Number: 20-028-0845 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Waypoint.0 ANALYTICAL "Every acre... Every year 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Emerson McBride 7210 Rocky River Rd South Monroe NC 28112 Farm: UN-26 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 01/28/2020 Date Of Analysis: 01/29/2020 Date Of Report: 01/29/2020 NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 o �° Rate Soil Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meq/100g megl100g 26-1 09362 5.0 H 138 130 VH NC = 108 40 VL NC = 20 185 H 1089 M 12 VL 5.9 6.78 1.5 8.6 IMIN 26-2 09363 4.7 M 133 127 VH NC=106 42 VL NC=21 168 H 1011 M 10 VL 6.0 6.81 1.2 7.8 MIN 26-3 09364 4.8 M 134 114 VH NC = 95 85 L NC = 43 178 H 1043 M 9 VL 5.9 6.79 1 A 8.4 MIN 26-4 09365 5.4 H 145 136 VH NC = 113 81 L NC = 41 183 H 1146 M 11 VL 5.8 6.75 1.8 9.3 MIN 26-6 09366 4.7 M [__133 92 H NC = 77 44 VL NC = 23 158 H 866 M 13 VL 5.7 6.77 1.6 7.4 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K % Mg % Ca % Na % H % NO, N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 26-1 1.2 17.9 63.3 0.6 17.4 11 L NC=23 22.5 VH NC=562.5 15 M NC=94 372 VH 12.8 VH NC=640.0 0.9 M 0.1 VL 26-2 1.4 17.9 64.8 0.6 15.4 7 VL NC=15 20.5 VH NC=512.5 14 M NC=88 397 VH 10.4 VH NC=520.0 1.0 M 0.11 VL 26-3 2.6 17.7 62.1 0.5 16.7 10 L NC=21 15.9 VH NC=397.5 9 L NC=56 511 VH 7.2 VH NC=360.0 1.1 M 0.15 VL 26-4 2.2 16.4 61.6 0.5 19.4 8 VL NC=17 17.4 VH NC=435.0 8 L NC=50 451 VH 6.5 VH NC=325.0 1.1 M 0.19 VL 26-6 1.5 17.8 58.5 0.8 21.6 12 L NC = 25 13.2 VH NC = 330.0 18 M NC = 113 310 VH 9.5 VH NC = 475.0 0.8 M 0.13 VL Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Ratingafter each value: VL (Very Low), L (Low), M Medium (pounds per acre), ms/cm milli -mhos per centimeter , me /100 maximum of thirty days after testing. ( rI ) ( ) l ) (P P ) ( P ) q 9 by PAuaic m 11�r H (High), VH (Very High). ENR -Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 =Ibs/A, Soluble analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 20-028-0845 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 Date Of Report: 01/29/2020 • 7621 Whitepine Road, Richmond, VA 23237 Waypoint. Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre... Every year. Grower: Emerson McBride 7210 Rocky River Rd South Monroe NC 28112 Farm: UN-26 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P O z s M 9 S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A IblA Ib/A Ib/A IbIA IbIA Ib/A Ib/A Ib/A Ib/A 26-1 Fescue Hay 4 0.8 200 0 167 0 10 0 4 0 0 0 26-2 Fescue Hay 4 0.8 200 0 165 0 13 0 4 0 0 0 26-3 Fescue Hay 4 0.8 200 0 111 0 11 0 4 0 0 0 26-4 Fescue Hay 4 1.0 200 0 116 0 F 12 0 1 4 0 0 0 26-6 Fescue Hay 4 1.0 200 0 162 0 10 0 3 0 0 0 Comments: Sample(s) : 26-2,26-3,26-4,26-6 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 Report Number: 20-028-0849 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Waypoint0 ANALYTICAL 'Every acre... Every year. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 d Fax 804-271-6446 www.waypointanalytical.com Grower: William Griffin 6705 Austin Grove Church Rd Marshville NC 28103 Farm: UN-29 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH r%-6- 113--h-A. ni iwtonon n.+e nF e., 1-ic• ni /9c19mn natP Of RPnnrt: 01/29/2020 NC = North Carolina Fertilitv Index Value OM WIV ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil M3 K Mg Ca Na Soil Buffer H Field ID - Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g meq/1009 29-1 09372 6.2 150 204 VH 73 L 272 H 1157 M 24 VL 6.1 6.80 1.3 9.6 H NC = 170 NC = 37 MIN 29-2 09373 6.2 150 198 VH 60 L 261 H 1174 M 23 VL 6.2 1.1 9.4 H NC = 165 NC = 31 MIN 29-3 09374 7.3 150 1 307 VH 286 VH 1 320 H 1300 M 12 VL 1 6.3 1.2 11.2 VH NC = 256 NC = 146 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble salts Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 29-1 1.9 23.6 60.3 1.1 13.5 13 L 9.8 VH 33 H 211 VH 13.1 VH 0.5 L 0.12 VL NC=27 NC=245.0 NC=206 NC=655.0 29-2 1.6 23.1 62.4 1.1 11.7 14 L 9.5 VH 34 H 210 VH 13.2 VH 0.5 L 0.11 VL NC=29 NC=237.5 NC=213 NC=660.0 29-3 6.5 23.8 58.0 0.5 10.7 15 L 20.2 VH 24 H 196 VH 11.7 VH 0.6 M 0.16 VL 1 NC=31 NC=505.0 NC=150 NC=585.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pod. me 60wr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble ,analysis prepared by: Waypoint Analytical Virginia, Inc C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 20-028-0849 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 Date Of Report: 01/29/2020 • waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 'Every acre... Every year. Grower: William Griffin 6705 Austin Grove Church Rd Marshville NC 28103 Farm: UN-29 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P 2 O s � Mg S Zn Mn Fe Cu B Field ID Tons TonslA lb/A lb/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 29-1 Fescue Hay 4 0.8 200 0 126 0 10 0 0 0 0 0.5 29-2 Fescue Hay 4 0.0 200 0 1 142 0 10 0 0 0 0 0.5 29-3 Fescue Hay 4 0.0 200 0 0 0 9 0 3 0 0 0 Comments: Sample(s) : 29-3 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." QAte« OF r Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 1 Report Number: 20-028-0848 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 Waypoint0 ANALYTICAL Every acre... Every year. "rM Farm: UN-30 SOIL ANALYSIS REPORT Date OfAnalvsis: 01/29/2020 Date Of Report: 02/03/2020 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Tom Appenzeller 830 Clover Road Marshville NC 28103 Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NC = North Carolina Fertility Index Value OM WIV ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil M3 K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 30-1 09371 8.5 150 263 VH 280 VH 290 H 1196 M 11 VL 6.3 1.1 10.3 VH NC = 219 NC = 143 I MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts Sample ID K Mg Ca Na H NO,N S Zn Mn Fe Cu B SS Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 30-1 7.0 23.5 58.1 0.5 10.7 16 M 18.1 VH 18 M 183 VH 9.4 VH 0.6 M 0.14 VL NC = 33 NC = 452.5 NC = 113 I NC = 470.0 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Date Received: 01/28/2020 Date Of Report: 02/03/2020 Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble ,analysis prepared by. Waypoint Analytical Virginia, Inc. Salts ms/cm x 640 = ppm. SOIL FERTILITY RECOMMENDATIONS by: paµria or 60w4 Pauric McGroary Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop veld Goal Lime N P 2O s K zO Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A IbIA 30-1 Fescue Hay 4 0.0 200 0 0 0 9 0 3 0 0 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Page 1 of 2 Report Number: 20-028-0850 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Waypoint0 ANALYTICAL 'Every acre... Every year "Tm 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Henry Myers 3809 Farmwood Road Monroe NC 28110 Farm: UN-31 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition water pH Date Received: 01/28/2020 Date Of Analvsis: 01/29/2020 Date Of Report: 01/29/2020 NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class lbs/A M3 pprn Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 31-3 09375 9.8 VH 150 139 VH NC=116 151 H NC=77 206 H 1120 M 10 VL 5.7 6.72 2.1 9.8 M-O 31-4 09376 10.5 VH 150 131 VH NC = 109 140 M NC = 72 199 H 11117 M 1 9 VL 1 5.5 1 6.66 1 2.7 10.4 M-O 31-5 09377 6.5 H 150 252 VH NC=210 107 M NC=55 297 H 1749 H 13 VL 6.7 0.5 12.1 MIN t-6 09378 6.9 H 150 309 VH NC = 257 -T- 110 M I NC = 56 333 H 1886 H 11 VL 6.8 0.4 12.9 MIN Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts K % Mg % Ca % Na % H % NOs N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 31-3 4.0 17.5 57.1 0.4 21.4 10 L NC=21 13.9 VH NC=347.5 13 M NC=81 341 VH 5.2 VH NC=260.0 0.8 M 0.13 VL 31-4 3.5 15.9 54.7 0.4 26.0 7 VL NC 15 12.9 VH NC=322.5 14 M NC=88 365 VH 5.3 VH NC=265.0 0.9 M 0.13 VI - 31-5 2.3 20.5 72.3 0.5 4.1 9 VL NC=19 16.8 VH NC=420.0 27 H NC=169 299 VH 6.8 VH NC=340.0 1.0 M 0.13 VL 31-6 2.2 21.5 73.1 0.4 3.1 6 VL NC=12 20.3 VH NC=507.5 26 H NC=163 289 VH 7.7 VH NC=385.0 1.2 M 0.13 VL Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g ma dmum of thirty days after testing. by: Pow;. or 60wr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: waypointAnaiytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 20-028-0850 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 rfafa Of Rannrt. n1/29/2n2n 0 0 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 'Every acre... Every year. ", Grower: Henry Myers 3809 Farmwood Road Monroe NC 28110 Farm: UN-31 SOIL FERTILITY RECOMMENDATIONS . Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P O 2 s Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A IbIA Ib/A Ib/A IbIA Ib/A Ib/A Ib1A Ib/A IbIA 31-3 Fescue Hay T- 4 0.5 200 0 40 0 11 0 4 0 0 0 31-4 Fescue Hay 4 0.5 200 0 63 0 13 0 4 0 0 0 31-5 Corn 125 0.0 153 0 105 0 22 0 3 0 0 0 j 31-6 Corn 125 0.0 153 0 103 0 26 0 3 0 0 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." p Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 Report Number: 20-028-0844 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Waypoint0 ANALYTICAL "Every acre... Every year "rM 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Grower: Danny Baker 2015 Hasty Rd Marshville NC 28103 Farm: UN-32 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 01/28/2020 Date Of Analysis: 01/29/2020 Date Of Report: 01/29/2020 NC = North Carolina Fertility Index Value OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number o �0 Soil Ibs/A M3 K Mg Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 32-2 09359 13.3 150 118 VH 238 VH 340 H 2375 M 68 VL 6.1 6.68 2.5 18.1 VH NC = 98 NC = 122 I M-O 32-3 09360 9.2 150 85 H 272 VH 258 H 1485 M 18 VL 6.4 1.0 11.4 VH M-O NC = 71 NC = 139 32-4 09361 13.8 150 133 VH 243 VH 234 H 1332 M 15 VL 5.9 6.74 1.9 11.2 VH NC = 111 NC = 124 ORG Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID K Mg Ca Na H NO, N S Zn Mn Fe Cu B SS Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 32-2 3.4 15.7 65.6 1.6 13.8 13 L 8.3 VH 55 VH 184 VH 5.7 VH 0.8 M 0.15 VL NC = 27 NC = 207.5 NC = 344 NC = 285.0 32-3 6.1 18.9 65.1 0.7 8.8 12 L 7.3 H 73 VH 157 VH 4.4 VH 0.6 M 0.12 VL NC = 25 NC = 182.5 NC = 456 NC = 220.0 32-4 5.6 17.4 59.5 0.6 17.0 14 L 8.6 VH 60 VH 188 VH 5.4 VH 0.5 L 0.13 VL NC=29 NC=215.0 NC=375 NC=270.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. m� G� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: fir` Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 20-028-0844 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 Date Of Report: 01/29/2020 Waypoint,0 ANALYTICAL "Every acre... Every year. "r,,, Farm: UN-32 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www,waypointanalytical.com Grower: Danny Baker 2015 Hasty Rd Marshville NC 28103 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 32-2 Fescue Hay 4 0.5 200 0 40 0 10 0 0 0 0 0 32-3 Fescue Hay 4 0.0 200 0 0 0 10 0 0 0 0 0 32-4 Fescue Hay 4 0.5 200 0 40 0 10 0 0 0 0 0.5 Comments: Sample(s) : 32-3 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 1 Report Number: 20-028-0847 Account Number:46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Date Received: 01/28/2020 • Waypoi nt ANALYTICAL "Every acre... Every year. "_ Farm: UN-33 SOIL ANALYSIS REPORT Date Of Analysis: 01/29/2020 Date Of Report: 01/29/2020 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Grower: Ted Funderburk 1909 Mt Pleasant Church Rd Monroe NC 28112 Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NC = North Carolina Fertility Index Value OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number o �0 Soil Ibs/A M3 K Mg Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 33-1 09370 3.3 106 31 M 41 VL 197 H 889 M 20 VL 6.1 6.83 1.0 7.3 M NC = 26 1NC = 21 I MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID K Mg Ca Na H NO, N S Zn Mn Fe Cu B SS Field ID % ova % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 33-1 1.4 22.5 60.9 1.2 13.7 10 L 4.0 H 14 M 157 VH 2.9 H 0.4 L 0.11 VL NC=21 NC=100.0 NC=88 NC=145.0 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Date Received: 01/28/2020 Date Of Report: 01/29/2020 Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: �Aylia m� Ge—r (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. Salts ms/cm x 640 = ppm. SOIL FERTILITY RECOMMENDATIONS Pauric McGroary Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 33-1 Fescue Hay 4 0.8 200 50 166 0 11 0 4 0 0 0.5 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.