WQ0031314_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:*
Project Number* WQ0031314
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * William C. Brewer
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0031314
Applicant\Permittee * City of Winston-Salem
Facility Name * Swann WTP
Phone Number*
3363977727
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
As requested, uploading a digital copy of the City of Winston-Salem's annual report.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 City of Winston-Salem Permit WQ0031314
7.75MB
Residuals Annual Report 021820.pdf
upload only 1 RJF docurrent. NLltiple docurrents must be corrbined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 4/8/2020

Winston-Salem / Forsyth County
I tilitioes
Water • Wastewater • Solid Waste
P.W. Swann Water Treatment Plant, 2800 River Ridge Road, Pfafftown, NC 27040
D: 336-727-8000, F: 336-946-2574, wsfcutiRies. org
Date: February 14, 2020
To: North Carolina Division of Environmental Quality
Aquifer Protection -Land Application Section
1636 Mail Service Center
Raleigh, NC 27699-1636
Subject: 2019 Residuals land Application Annual Report
Permit No. WQ0031314
Swann Water Treatment Plant
Neilson Water Treatment Plant
Thomas Water Treatment Plant
Dear Sir or Madam,
Enclosed are three copies of the Residuals Land Application Annual Report and supporting
documentation for the City of Winston-Salem's Swann, Thomas and Neilson Water Treatment Plants for
permit WQ0031314.
Swann Water Treatment Plant
The Swann Water Treatment Plant operated in compliance with all parameters of its permit during the
2019 calendar year. The Swann WTP operates one equalization basin and two residuals lagoons that
produces a Class A Residual, which is 503 exempt. Residuals generated by filter washes flow through an
equalization basin, whereas solids removed from the plant's sedimentation basins flows by gravity
directly to the residuals lagoon in service. The lagoons are operated such that one lagoon accepts residuals
while the other lagoon is cleaned or in reserve. During the 2019 calendar year, the Swann WTP
contracted with Synagro Central, LLC to transport and apply 336.66 dry tons of residuals from lagoon #1
to nearby farmland owned by various farmers in Forsyth County. Accompanying our report are detailed
maps and soil reports for the residual application sites.
Section f
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form.
+ DEQ Form DMSDF (Supp) - Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form (Supplemental Information)
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
City Council: Mayor Allen Jolnes; Vlv#an H. Burke, Mayor Pro Tempore, Northeast Ward; Denise D. Adams, North Ward; Dan Besse, Southwest Ward; Robert C, Clark,
West Ward; John C. Larson, South Ward; Jeff Macintosh, Northwest Ward; Annette Scippio, East Ward; James Taylor, Jr., Southeast Ward; City Manager: Lee D. Garrity
County Commissioners: David R. Piyler, Chair; Don Martin, Vice Chair; Fleming EI-Amin; Ted Kaplan; Richard V. Linville; Tonya McDaniel; Gloria D. Whisenhunt; County
Call 311 or 336-727-8000 Manager: Dudley Watts, Jr.
Winston-Salem/Forsyth County Utility Commission: Randall S. Tuttle, Chair; L. Wesley Curtis, fr., Vice Chair; Harold E. Day, Tom Gr;ffin; Yvonne H. Hines; Duane Long;
[e-mail] Hugh WJernigan; Chris Parker; James Ruffin; Donald R. Stewart; Allan Younger

Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and chain of custody's)
• Copies of our SAR/PAN calculations
Section 4
+ Maps of the residuals disposal sites
Section 5
+ Field soil sampling results
Thomas Water Treatment Plant
The Thomas Water Treatment Plant operated in compliance with all parameters of its permit during the
2019 calendar year. During the 2019 calendar year the Thomas WTP did not haul any residuals, therefore
there are no reports to file.
Neilson Water Treatment Plant
The Neilson Plant operated in compliance with all parameters of its permit during the 2019 calendar year.
The Neilson Water Treatment Plant operates three residuals lagoons and produces a Class A Residual,
which is 503 exempt. Solids from the sedimentation basins flow directly to the residual lagoon in service.
The lagoons are in a rotation so one lagoon is in service, one lagoon is drying and one is empty and ready
to be placed into service. During the 2019 calendar year, the Neilson Plant had two hauling events to land
apply residuals from lagoons 42 and #3. EMA Resources, Inc. removed and applied 2,334.69 dry tons of
residuals on land owned by Roger Spillman and Greg Dooley. This hauling event represents residuals
generated over a 34-month period for an average annual production rate of 824 dry tons per year
([2,334.69 DT's _ 34 months] X 12 Months). Lagoon #2 was in service from January 2016 until April
2017 and lagoon #3 was in service from April 2017 until October 2018. Due to a change in personnel no
residuals were hauled during the 2015 and 2017 calendar years. This combined with excessively wet
weather resulted in the lagoon rotation getting out of our normal one lagoon a year cycle. Accompanying
our report are detailed maps and soil reports for these residual application sites.
Section I
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
+ DEQ Form DMSDF (Supp) - Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form (Supplemental Information)
+ DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form
Section 2
+ DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and chain of custody's)
• Copies of our SAR/PAN calculations
Section 4
+ Maps of the residuals disposal sites
Section 5
Field soil sampling results

If you have any questions or require additional information regarding our 2019 Annual Report, please call
Bill Brewer, Water Treatment Superintendent, at [phone].
Sincerely,
Courtney L. Driver
Permittee:
Courtney L. Driver
Director of Utilities
Utilities Administration
P.O. Box 2511
Winston-Salem, NC 27102
William C. Brewer
Preparer of Annual Report:
William C. Brewer
Water Treatment Superintendent
Swam Water Treatment plant
2800 River Ridge Road
Pfafftown, NC 27040
Enclosures (3) copies of Annual Report
3

Winston-Salem/Forsyth County Utilities
WQ0031314
2019 Residuals Land Application Report
P.W. Swann Water Treatment Plant
TABLE OF CONTENTS
Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form DMSDF(Supp) - Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form (Supplemental Information)
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF - Annual Metals field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and chain of custody's)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
0 Field soil sampling results

Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface
Disposal Certification and Summary Form
• DEQ Form DMSDF(Supp) -Class A Annual Distribution and
Marketing/Surface Disposal Certification and Summary Form (Supplemental
Information)
• DEQ Form RSSF -Annual Residual Sampling Summary Form
• DEQ Form RSSF B -Annual Residual Sampling Summary Form

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
W Q PERMIT #: WQ00031314 FACILITY NAME: Winston Salem - Swann WTP
PHONE: [phone] COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE (please check one): Cl Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
., r,, XT_ n —.. Tf NT..1r;n "ar#c A R_ C and rertifv form below
Was the facility in
Month
January
February
March
April
May
June
July
August
Seutember
n during the past calendar 1
Part A*:
Sources(s) ('include NPDES ## if Amendment -
applicable) Bulking Agen
Volume (dry tons
Residual In I Product Out
October
November Swann WTP 336.66 336.66
December
Total from FORM DMSDF (sup)
Totals: Annual (dry tons): 01 336.66 336.66
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Nanre(s)
Part B*:
ant Information
Volume (dry tons) � Intended use(s)
Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ® No 0 If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitt' ;sjnformation, including the possibility of fines and imprisonment for knowing violations."
Signature ofPern e Date Signature ofPreparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
WINSTON-SALEM, NC
WINSTON-SALEM, NC PW SWANN WTP LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
November 2019 2,360,600,00 G 336.66 D 305.33
YEARLY TOTAL 2,360,600.00 G 336.66 D 305.33
1/22/2020

ANNUAL. RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: VVQ0031314
Laboratory
Waypoint Analytical Virginia Inc.
Facility Name: WINSTON-SALEM, NC
NPDES# : NCO079821
or WQ# (residual only)
WWTP Name: PW SWANN WTP
Residuals Analysis Data
WPL
Product Type
WPL
WPL
WPL
Date Sampled (grab) or 09/17/19
11/25/19
11/25/19
11/25/19
Date Composited
Percent Solids 3.42
2.19
1.78
1.84
PARAMETERS (mglkg dry weight)
Arsenic 8.73
<22.7
<27.8
<27.8
Cadmium <1
<4.55
<5.56
<5.56
Mercury 0.0332
<0.686
<0.611
<0.85
Chromium 48.9
27.5
36.7
34.2
Copper 49.3
54.5
70.6
65.6
Lead 12.6
19.1
25.4
25.4
Molybdenum <2.5
<11.4
<13.9
<13.9
Nickel 22.9
18
23.8
22.3
Selenium <5
<22.7
<27.8
<27.6
Zinc 442
260
503
387
Total Phosphorus 2870
3610
4920
4440
TKN 20900
26700
25700
34400
Ammonia -Nitrogen 6180
627C
11400
10800
Nitrate and Nitrite <4 . 9
<225
<262
<273
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X L,
(SIGNATURE OF PREPARER)
DENR FORM RSSF (5/2003)
Date
Printed: Tuesday - January 2$ 2020 at 14:36:16 for: 2065 04

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number W00031314 Laboratory
Facility Name WINSTON-SALEM, NO Waypoint Analytical Virginia Inc.
NPDES# NCO079821
or WQ# (residual.only)
WWTP Name
Residual Analysis Data
Product Type
Date Sampled
Date Composited
Percent Scilds
PW SWANN WTP
PARAMETERS (mglkg dry weight)'
Aluminium
Calcium
Magnesium
pH
Potasium
Sodium
PAN
SAR
WPL
WPL
WPL
WPL
09/17/19
11 /25/19
11 /25119
11/25/19
3.42
1.84
2.19
1.78
120000
160000
127000
160000
5290
3670
2840
4520
1670
2110
18C0
2400
6.70
6.30
6.30
6.30
1120
2110
1730
2120
302
<1390
<1140
<1390
8983
15113
11532
11682
0.1709
0.6116
0.607
0.5525
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, includir� the possibility of fines and imprisonment for knowing violations."
X 1�. Date V
(SIGNATURE OF PREPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 1/28/2020 1:45:11 PM

Section Z
o DEQ Form MFLSF - Annual Metals Field Loading Summary Form
e DEQ Form FSF - Annual Land Application Field Summary Form

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Winston-Salem, NC Total Dry Tons Applied (Annual): 38.63
Permit #: WQ0031314 Cation Exchange Capacity (non 503 only):
Operator: Tony Apperson Owner: Tony Apperson Predominant Soil Series: Tomlin
Acres Used: 19 Acres Permitted: 19 Site #: NC FO 00OX9 Field #: FO 00OX9 0001.
Residual Analysis Data (Heavy Metals and Total Phosphorus use
1 2 3 4 5 6 7
Sample or
Com-
posite
Date 9/17/19
Solids 3.42
Arsenic 8.73
Cadmium 1
Copper
49.3
,hromiui
48.9
Lead
12.6
Mercury
0.0332
Molyb-
denum
2.5
Nickel
22.9
Selenium
5
zinc
442
Total
Phos-
2870
Annual Heavy Metal F
Total 2
DT/Ac./
App.
Event 2.03
Arsenic 0.035 0.000
I Cadmium 1 0.004 OA00
Lead
Nickel
Selenium
Zinc
Total
Phos-
0.200 0.000
0.199 0.000
0.051 0.000
a.000 0.000
0.010 0.000
0.093 0.000
0.020 0.000
1.797 i 0.000
11.669 1 0.000
% Solids use Raw Percent #):
1
'Loadings
1 1
1 111
i 111 1 111 1 111 1 ill 1 111 1 111 1 I11 1 111 1 III 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
i 11'
1 Ili
1 ill
1 111
1 III
1 III
1 111
1 111
1 111
111
1 111
1 11
1 III
1 111
1 1 I
1 Ill
1 Ili
1 III
1 III
1 Ill
1111
l 111
1 ••
I I11
1 111
1 111
l 111
till
I III
i 111
1 114
1 111
I III
1 1
I lil
1 111
I III
i 111
1 I11
1 111
1 I11
1 Ili
1 I11
1 ill
1 111
1 111
1 Ill
1 lil
l 111
i III
1 111
1 Ili
1 I11
1 Ill
1 111
I I 1
1 111
1 III
1 Ill
1 ill
1 111
i 111
1 Ill
I lil
1 111
1 ill
1 i'
1111
1I11
I111
1111
1lll
i111
1lli
1111
llll
11 1
lill
1 III
1 lil
1 111
I Ili
l ill
Ili
1 lil
1 Ili
1 111
l 111
Iill
1III
1lll
IIII
1111
1I11
1lli
it 1
iI11
1III
•.'
110i li5
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in actor ante
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Laud Applier Date
nFNR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Page: 1
Lune Applied ***
FACILITY NAME: WINSTON-SALEM, NC
PREDOMINANT SOIL SERIES: TON LIN
Date Lbs/Ac
OWNER: TONY APPERSON
PERMIT #:
WQ0031314
ANNUAL
DRY TONS APPLIED:
38,63
SITE #: NC FO 000X9 FIELD# : FO 00OX9 0001 OPERATOR: TONY APPERSON
CATION
EXCHANGE CAPACITY
(NON-503):
RESIDUAL SOURC) (S): See list at bottom of report
ACRES UTILIZED: 19.00
ACRES PERMITTED:
19.00
allons (G) or Cubic Yards (CY)
Dry Site
inches Appli- Vola-
Miner -
or Wet Tons (WT) (specify)
Tons Cond.
Precip. cation tili-
ali-
Ammonia
Nitrate
PAN
%
DATE or
Per Residual Dry, Wet, Past 24 Method zation
zation
TKN Nitrogen
and
(pprn)
Crop
MONTH Total Per Acre Solids
Acre Source Moist Hours * Rate**
Rate
Nitrite
11/5/19
138,600.00 (G)
7294.737
3.42
1.040
WSPWSW
NUR
0.5
0.44
20,904.p
6,180.00 p
4.90 p
$983
FESCUE
11/6119
132,300.00 (G)
6963.158
3,42
0.993
WSPWSW
SUR
0.5
0.40
20,900.p
6,180.00 p
4.90 p
8983
FESCUE
Nov-19
270,900.00 (G)
14,257.895
Total Crallous/Ac: 14,257.89
As
Cd Cr Cu
Pb
Hg Mo
Ni
Se
Zn
P PAN
TOTALS
37
Annuallbs/acre
0.036
0.004
0.199
0.200
0,051
<.001
0.010
0.093
0.020
1.798
11.67
Cumulative lbs/acre
0,036
0,004
0.199
0.200
0.051
<.001
0.010
0.093
0.020
1.798
194
Permit PAN Limit (lbs/acre) Ist Cropl2nd Crop
I.
FD Cumulative Pollutant Loading Rate Limit (lbslacre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0
WSPWSWPL = WINSTON-SALEM, NC PW SWANN WTP LIQUID
cj�
X � I
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted I am aware that there are significant penalties for submitting false infonnatioa-, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston-Salem, NC
WQ0031314
Keith Matthews Owner
20 Acres Permitted:
Total Dry Tons Applied (Annual): 82.66
Cation Exchange Capacity (non 503 only):
Keith Matthews Predominant Soil Series: Dan River
20 Site #: NC YK OOX39 Field #: YK OOX39 0001.
Residual
Analysis Data (Heavy
Metals and Total Phosphorus
use mg/kg, "/o Noticts use -caw
rercent +f):
Sample or
1 2
3 4 5 6
7 8 9 10
11 12
Com-
posite
Date
9/17/19
Solids
3.42
Arsenic
8.73
Cadmium
l
Copper
49.3
Chromium
48.9
Lead
12.6
Mercury
0.0332
Molyb-
2.5
denum
Nickel
SeleniumZinc
E442
Total
Phos-
2870
horus
Annual
Heavy Metal Field Loadings
(Calculated in lbslaere):
Total
1 2 3
4 5 fi 7 8 9 10 11 12 N
DT/Ac./
0
App.
Event
4.13
0. 772 0.000 0.000
0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.072
Arsenic
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
0.408
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.Ooo
0.000
0.000
0.408
Chromi
0.404
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.404
0.104
0.000
0 021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.104
0.000
0.021
Lead
Mercury
MoIyb-
denum
Nickel
0.189
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.189
Selenium
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
OA0
0.000
0.000
0.041
3.654
0.00a
O.000
O.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.654
Zinc
Total
Phos-
23.729
0.000
0.000
0.000
0.000
0.000 o.00a o.000
o.aao o.oao o.oao a.000 23.729
horus
,._.
r i-, f{,.,f
fhio dtlln
'In t
nc nr=red i=er my
direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (1212006)

FACILITY NAME: WINSTON-SALEM,NC
OWNER: KEITH MATTHEWS
SITE #: NC YK OOX39 FIELD# : YK OOX39 0001
R F.4TnT T A T ..0 nT TR C .F. f Rl - .S eP 1 kt. at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: DAN RIVER
PERMIT #: WQ0031314 ANNUAL DRY TONS APPLIED: 82.66
OPERATOR: KEITH MATTHEWS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.00 ACRES PERMITTED: 20.00
Page: 1
Lune Applied ***
Date
I Lbs Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
nation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total I
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
11/5119
37,800.00 (G)
1890.000
3.42
0.270
WSPWSW
SUR
0.5
0.40
20,900. p
6,180.00 p
4.90 p
8983
WHEAT
11/6/19
182,700.00 (G)
9135.000
3.42
1.303
WSPWSW
SUR
0.5
0.40
20,900. p
6,180.00 p
4.90 p
8983
WHEAT
11/7/19
239,400.00 (G)
11970.000
3.42
1.707
WSPWSW
SUR
0.5
0.40
20,900. p
6,180,00 p
4.90 p
8983
WHEAT
11/11/19
88,200.00 (G)
4410.000
3.42
0,629
WSPWSW
SUR
0.5
0,40
20,900,p
6,180.00 p
4.90 p
8983
WHEAT
11/18/19
31,500.00 (G)
1575.000
3.42
0.225
WSPWSW
SUR
0.5
0.40
20,900. p
6,180.00 p
4,90 p
8983
WHEAT
Nov-19
579,600.00 (G)
28,980.000
Total Gallons/Ac: 28,980.00
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
TOTALS:
74
Annuallbs/acre 0.072 0.008 0.404 0.408 0.104 <001 0.021 0.199 0.041 3.654 23,72
Cumulative lbs/acre 0.072 0.008 0.404 0.408 0.104 <.001 0.021 0.189 0,041 3.654
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop 107
FD Cumulative Pollutant loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 26T9 15.0 375.0 99.0 2500.0
WSPWSWPL = WINSTON-SALEM, NC PW SWANN WTP LIQUID
J
xI x 6
1 aJ
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that claalified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mgAcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 - Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston-Salem, NC Total Dry Tons Applied (Annual):
WQ0031314 Cation Exchange Capacity (non 503 only):
Keith Matthews Owner: Keith Matthews Predominant Soil Series:
12 Acres Permitted:
43.13
Ronda
12 Site #: NC YK 0OX39 Field #: YK 00X39 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or 1 2 3 4 5 7 8 9 10 11 12
Com-
posite
Date 9/17/19
% Solids 3.42
Arsenic 8.73
Cadmium 1
Copper 49.3
Chronuw 48.9
Lead 12.6
Mercury 0.0332
Molyb- 2.5
denum
Nickel 22.9
Selenium 5
Zinc 442
Total
Phos- 2870
horus
A-,.., i F;,.Td 11.nartinvc (C.nivnlated in lbs/acre):
6
6
7
8
9
10
11
12
Total
3
4
H
DT/Ac./
App.
Event
3.59
Arsenic
0.063
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.354
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.354
Chromi
0.351
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
a.000
0.000
0.351
Lead
0.091
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.091
Mercury
(500
0.000
0.000
6.000
0.000
0.000
0.000
0.000
0.000
0.O00
0.000
0.000
0.000
Molyb-
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
denw-a
Nickel
0.165
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.165
Selenium
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.000
0.000
0.036
Zinc
3.176
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.176
Total
Phos-
20.624
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.O00
0.000
20.624
horus
d
"I certify, under penalty of law, that this document was prepared under my direction or supervision rn accor ance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of flues and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: WINSTON-SALEM, NC PREDOMINANT SOIL SERIES: RONDA
OWNER: iCEITH MATTHEWS PERMIT #: WQ0031314 ANNUAL DRY TONS APPLIED: 43.13
SITE #: NC YK OOX39 FI1=LD# : YK OOX39 0002 OPERATOR: KEITH MATTHEWS CATION EXCHANGE CAPACITY (NON 503):
R RCTr1T TAT. cnT TR (`.T-N)- CPe lict nt hnttnm of renort ACRES UTILIZED: 12.00 ACRES PERMITTED: 12.00
page: 1
Lune Applied I"
Date LbsAc
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tilt-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
4
MONTH
Total 1
I
Per Acre
Solids
AcLe
Source
Moist
Hours
*
Rate**
Rate
Nitrite
11/5/19
56,700.00 (0)
4725.000
3.42
0.674
WSPWSW
SUR
0.5
0,40
20,900.p
6,180.00 p
4.90 p
$983
CORN
11/6/19
75,600.00 (G)
6300.000
3.42
0.898
WSPWSW
SUR
0.5
0.40
20,900.p
6,180.00 p
4,90 p
8983
CORN
11/7/19
75,600.00 (G)
6300.000
3.42
0.898
WSPWSW
SUR
0.5
0.40
20,900.p
6,120.00 p
4.90 p
8983
CORN
11/11/19
56,700.00 (G)
4725.000
3.42
0.674
WSPWSW
SUR
0.5
0.40
20,900.p
6,180.00 p
4.90 p
8983
CORN
11/22/19
37,800,00 (G)
3150.000
3.42
0.449
1 WSPWSW
STIR
1 0.5
0.40
20,900. p
6,180,00 p
4.90 p
8983
CORN
Nov-19
302,400.00 (G)
25,200.000
Total Gallons/Ac: 25,200.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
65
Annuallbs/acre
0.063
0.007
0.351
0.354
0.091
<.001
0.018
0.165
0.036
3.177
20.63
Cumulative lbslacre
0,063
0.007
0.351
0.354
0.091
<r001
0.018
0,165
0.036
3.177
Permit PAN Limit (lbslacre) 1st Crop/2nd Crop
90
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
WSPWSWPL = WINSTON-SALEM, NC PW SWANN WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA � Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation L0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Winston-Salem, NC Total Dry Toms Applied (Annual): 172.24
Permit #: WQ0031314 Cation Exchange Capacity (non 503 only):
Operator: Keith Matthews Owner: Keith Matthews Predominant Soil Series: Ronda
e vc-c Ilzd d • 40 Acres Permitted: 40 Site #: NC YK 0OX39 Field #: YK 0OX39 0003
1 u._
Residual
Analysis Data
(Heavy
Metals and Total Fhospnorus
use mglxg,
ro aonus uNe
parr Vx•-ULIL
rrf•
Sample or
1 2
3
4 5 6
7 8
9 10
11
12
Com-
posite
Date
9/17/19
% Solids
3.42
Arsenic
8.73
Cadmium
1
Copper
49.3
Chromiurn
48.9
Lead
12.6
Mercury
0.0332
Molyb-
2.5
denum
Nickel
22.9
Selenium
5
Zinc
442
Total
Phos-
2870
horus
Annual
Heavy
Metal Field
Loadings
(Calculated
in Ibslacre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
y
DT/Ac./
0
App.
Event
4.31
0.07S
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.075
0.009
Arsenic
Cadmium
Copper
0.425
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.425
Chromium
0.421
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.Oo0
0.000
0.421
Lead
0.109
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000-1
0.000
0.000
0.000
0.109
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0,022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.00o
0.000
0.022
denum
Nickel
0.197
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o.000
00
0.197
Selenium
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
00
too
043
Zinc
3.8 77
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
00
3.807
3.807
Total
Phos- 24.716 0.000 0.000 0.000 0.000 0.000
0.000 0.000
0.000 0.000 0.000 0.000 24.716
c horus c_ ___ a.._ -__ iZ ^r r„�, that thic r1nrrem ,nt wa.c nranared
under my
direction or supervision in accordance
1 l R .,, uwn. t•-"' --.1 -- --- ,
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: WINSTON-SALEM, NC
PREDOMINANT SOE_ SERIES: RONDA
ANNUAL DRY TONS APPLIED:
172.24
OWNER:
ISEITH MATTHIrWS
PERMIT #: WQ0031314
CATION EXCHANGE CAPACITY
SITE #:
NC YK OOX39 FIELD# : YK 00X39 0003
OPERATOR: KEITH MATTHEWS
ACRES UTILIZED: 40.00
ACRES PERMITTED:
ACCRES P
40.00
RESIDUAL SOURCE(S): See list at bottom of report
allons (G) or Cubic Yards (CY)
Dry Site Inches Appli-
Vola-
Miner -
or Wet Tons (WT) (specify) ova
Tons Cond. Precip. cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per Residual Dry, Wet, Past 24 Method
nation
nation
TKN Nitrogen
and
(ppm)
Crop
MONTH
Total I Per Acre Solids
Acre Source Moist Hours *
Rate"
Rate
Nitrite
11/11/19
143,000.00 (G) 3575.000 - 3.42
0.510 WSPWSW SUR
0.5
0.40
20,900, p 6,180.00 p
4,90 p
8983
CORN
11/18/19
56,700.00 (G) 1417.500 3.42
0.202 WSPWSW SUR
0.5
0.40
20,900.p 6,180.00 p
4.90 p
8983
CORN
11/20/19
352,900.00 (G) 8820.000 3,42
1.258 WSPWSW SUR
0.5
0.40
20,900. p 6,180.00 p
4.90 p
8983
CORN
11/21/19
371,700.00 (G) 9292.500 3,42
1.325 WSPWSW SUR
0.5
0.40
20,900.p 6,180.00 p
490 p
8983
CORN
11/22/19
283,500,00 (G) 7087.500 3,42
1.011 WSPWSW SUR
0.5
0.40
20,900. p 6,180.00 p
4.90 p
8983
CORN
Nov-19
1,207,700.00 (G) 30,192.500
Total Gallons/Ac: 30,192.50
Page : 1
Lime Applied ***
Date Lbs1Ac
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
77
Annuallbs/acre
0.075
0.009
0.421
0.425
0.109
<.001
0.022
0.197
0.043
3.806
24.72
Cumulative lbslacre
0.075
0.009
0.421
0.425
0.109
<.001
0.022
0.197
0.043
3.806
F777
Permit PAN Limit (lbslacre) Ist Cropl2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
WSPWSWPL = WINSTON-SALEM, NC PW SWANN WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, InjectionllncorpOration LO
Application Method: SUR - Surface, INI -Injection, SUR1N -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

Section 3
® Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and
chain of custody's)
® Copies of our SAR/PAN calculations

Waypointo
ANALYTICAL
9/27/2019
Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-262-0017
Project Description: Winston WTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyticat.com
Clear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/19/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pw;• 0 & I.
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

Waypoint(b
ANALYTICAL
Report Number: 19-262-0017
Client Project Description: Winston WTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SM-4500-NI3C
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
9045D
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
4500NO3F-2011
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
6010D
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SW-7471B
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SM-4500-NH3C-TKN
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
Page 2 of 6

Report Number: 19-262-0017
Account Number: 46622
Send To: Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68269
Sample Id : Winston WTP
b
Waypoint
ANALYTICAL
Project; Winston WTP
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypo into nalytical.corn
Date Sampled: 9/17/2019 14:00:00
Date Received,. 09/1912019 00:00
Date Reported: 09/27/2019
Total Solids "
3.42
ADM
09/20/2019 16:38
SM-2540G
Moisture *
96.60
ADM
09120/2019 16:38
SM-2540G
Total Kjeldahl Nitrogen
2,09
20900
250
JPJ
09/26/2019 13:00
SM-4500-NH3C-TKN
Phosphorus
029
2870
50.0
BKN
09/24/2019 21:47
6010D
Potassium
0.11
1120
50.0
BKN
09/24/2019 21:47
6010D
Sulfur
0.41
4110
50.0
BKN
09/24/2019 21A7
6010D
Calcium
0.53
5290
250
BKN
09/24/2019 21:47
6010D
Magnesium
0.17
1670
50.0
BKN
09/24/2019 21:47
6010D
Sodium
0.03
302
250
BKN
09/24/2019 21:47
6010D
Iron
24200
50.0
BKN
09/24/2019 21:47
6010D
Aluminum
120000
500
BKN
09/251201913:37
6010D
Manganese
1120
5.00
BKN
09/24/2019 21:47
6010D
Copper
49.3
2.50
BKN
09/24/2019 21:47
60100
Zinc
442
12.5
BKN
09/24/2019 21:47
6010D
Ammonia Nitrogen
0.62
6180
100
JPJ
0912612019 13:00
SM-4500-NH3C
Organic N
1.47
14720
250
09/26/2019 13:00
CALCULATION
Nitrate+Nitrite-N
<4.90
4.90
ZBD
09/24/201915:33
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time ?Of�G C �f�OKy
Our reports and letters are for the exclusive and confrdentiai use of our ciients, and may not be reproduced in whoie or part. nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 3 of 6

Report Number. 19-262-0017
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NO 27028
Lab Number: 68269
Sample Id : Winston WTP
0 a
Waypoint
r a
►��
..
Project: Winston WTP
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.vvaypointanalytical.com
Date Sampled: 9/17/2019 14:00:00
Date Received: 09/1912019 00:00
Date Reported: 09/2712019
Cadmium
<1.00
1.00
BKN
09/24/2019 21:47
6010D
Chromium
48.9
2,50
BKN
09/24/2019 21:47
6010D
Nickel
22.9
2.50
BKN
09/24/2019 21:47
6010D
Lead
12.6
3.00
BKN
09/24/2019 21:47
6010D
Arsenic
8.73
5.00
BKN
09/24/2019 21:47
601 OD
Mercury
0.0332
0.0155
TJS
09/24/2019 13:43
SW-7471 B
Selenium
<5.00
5.00
BKN
09/24/2019 21:47
601OD
pH*
6.7
JSL
09/24/2019 06:50
9045D
Molybdenum
<2.50
2.50
BKN
09/24/2019 21:47
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and fetters are for the exclusive and confidential use of our clients, and may not he reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, nevus release, or other public announcements without obtaining our prior written authorization.
Pxf�G fa V0"I
Pauric McGroary
Agronomist
Page 4 of 6

Waypoint
o
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
ANALYTICAL www.waypointanalocal.com
Cooler Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLCI Technical
Report Number: 19-262-0017
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other
Thermometer ID:
Shipping container/cooler uncompromised?
4D Yes
0 No
Number of coolers received
F - �
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
40 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
4D Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
® Yes
0 No
Cooler/Samples arrived at the laboratory on ice,
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® NIA
Water - VOA vials free of headspace
0 Yes
0 No
® NIA
Trip Blanks received with VOAs
0 Yes
0 No
® NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® NIA
F High concentration container (48 hr)
F High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments;
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
0 Yes 0 No
Signature;[Brand i Watson Date &Time: 09/19/2019 13:42:2$
Page 5 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2065-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 9/1712019 9/112019-1213112019 0.1709
LIQUID
Na mgll = (Na mglkg x % Solids) + 100 = (302 x 3.4200) + 100 = 10.3284
Ca mgll = (Ga mglkg x % Solids) + 100 = (5290 x 3.4200) + 100 = 180,918
Mg mgll = (mg mglkg x % Solids) + 100 = (1670 x 3,4200) 100 = 57.114
Na meq = Na mg/l + Molec.Wgt.Na = 10.3284 + 23 = 0.449061
Ca meq = Ca mgll + Molec.Wgt.Ca = 180.918 + 20 = 9.0459
Mg meq = Mg mgll + Molec.Wgt.Mg = 67.114 -� 12 = 4.7595
SAR = Na meq SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.449061 SgrRoot[0.5(9.0459+4.7595)] = 0.170921
Printed: 1 /22/2020
17:02
Page 1

Waypointo
ANALYTICAL
121512019
Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-330-0005
Project Description: Winston 2nd
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
i'"�. V 6'—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
n-,-- 1 -F C

Sample Summary Table
Report Number: 1.9-330-0005
Client Project Description: Winston 2nd
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
9045D
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
4500NO3F-2011
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
6010D
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
SW-74716
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C-TKN
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Paaa 2 of 6

7621 Whitepine Road, Richmond, VA 23237
Waypoi tMain 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46622
Synagro Central LLC/ Technical
Mary Brewer Project Winston 2nd Report Date : 12/05/2019
284 Boger Road Information : Received : 11/26/2019
Mocksville , NC 27028 me G4wr
?or;.
Pauric McGroary
Report Number :19-330-0005 REPORTOFANAL Y5XS Agronomist
Lab No : 69699 Matrix: Solids
Sample ID : Winston 2nd sampled: 11/25/2019 13.45
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Moisture 98.2 % 0.010 1 12/02/1918:43 ADM SM-2540G
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Ammonia Nitrogen
10800
mg/Kg - dry
5560
1
12/05/19 08:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<273
mg/Kg - dry
273
1
12/05/19 12:05
7BD
4500NO3F-2011
Organic N
23600
mg/Kg - dry
13900
1
12/04/19 09:00
CALCULATION
pH
6.3
s.u,
1
12/03/19 07:06
JSL
9045D
Total Solids
1.84
%
0.010
1
12/02/19 18:43
ADM
SM-2540G
Total Kjeldahl Nitrogen
34400
mg/Kg - dry
13900
1
12/04/19 09:00
JPJ
;M-4500-NH3C-TKi`
Phosphorus
4440
mg/Kg - dry
278
1
12/03/19 19:27
BKN
6010D
Aluminum
16000D
mg/Kg - dry
278
1
12/03/19 19:27
KKM
6010D
Arsenic
<27.8
mg/Kg - dry
27.8
1
12/03/19 19:27
BKN
6010D
Calcium
3670
mg/Kg - dry
1390
1
12/03/19 19:27
KKM
6010D
Cadmium
<5.56
mg/Kg _ dry
5.56
1
12/03/19 19:27
BKN
6010D
Chromium
34.2
mg/Kg - dry
13.9
1
12/03/19 19:27
BKN
6010D
Copper
65.6
mg/Kg - dry
13.9
1
12/03/19 19:27
BKN
6010D
Iron
35800
mg/Kg - dry
278
1
12/03/19 19:27
KKM
6010D
Lead
25.4
mg/Kg - dry
16.7
1
12/03/19 19:27
BKN
6010D
Magnesium
2110
mg/Kg - dry
278
1
12/03/19 19:27
KKM
6010D
Manganese
1130
mgIK9 - dry
27.8
1
12/03/19 19:27
BKN
6010D
Qualifiers/ DF
Dilution Factor
L
Limit
Exceeded
Definitions MQL
Method Quantitation Limit

WavD061
,•
ANALYTICAL
46622
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Report Number : 19-330-0005
Lab No : 69698
Sample ID : Winston 2nd
Test
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytical.corn
Project Winston 2nd
Information :
REPORT" OFANAL YSIS
Results Units MQL
Report Date ; 12/05/2019
Received : 11/26/2001199'
pug;` #1` 6'�°"O
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11/ 25 / 2019 13.45
DF [late 1 Time By Analytical
Analyzed Method
Mercury
<0.850
mg/Kg - dry
0.850
1
12/04/19 15:23
KKM
SW-7471B
Molybdenum
<13.9
mg/Kg - dry
13.9
1
12/03/19 19:27
BKN
6010D
Nickel
22.3
mg/Kg - dry
13.9
1
12/03/19 19:27
BKN
6010D
Potassium
2110
mg/Kg - dry
278
1
12/03/19 19:27
KKM
6010D
Selenium
<27.8
mg/Kg - dry
27.8
1
12/03/19 19:27
BKN
6010D
Sodium
<1390
mg/Kg - dry
1390
1
12/03/19 19:27
BKN
6010D
Zinc
387
mg/Kg - dry
69.4
1
12/03/19 19:27
BKN
6010D
Sulfur
6110
mg/Kg - dry
278
1
12/03/19 19:27
BKN
6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Pacsp 4 of 6

waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax W4-271-6446
www.waypo9nta nalyticai.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LL,CI Technical
Report Number: 19-330-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
UPS 0 Client 0 Courier Thermometer ID: - -
Shipping container/cooler uncompromised? @ Yes 0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
16 Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun,
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
® NIA
Trip Blanks received with VOAs
0 Yes
0 No
® NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
[_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Brandi Watson Date &Time: 11/26/2019 13:37:11
n--- F _F 9

SAMPLING LOG #
�+ ffilllllllflflllllllllllllllllllllllllllllllflllllllllllliliflll46622 Q°9� I EC RECORD & ANALV� 2
RECORD
CUSTOMER: w�������COP Svnaero Central LLC7 Tachn�cal 13:36:37
t_ Winstan end
PROJECT MANAGER:oper field sampling procedures
collection of these samples.
Phone:..( ) - 749 3 - s'G9W
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OI' SAMPLING METHOD METHOD
LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
Relinquished by Sampler:
Relinquished by:
SPECIAL INSTRUCTIONS:
��&6 For.
/1/z:
1z
Date
monitoring purposes.
Time
I • -tS"
i Tme
Time
Recieved by:
Recieved bv:
REMARKS:
................
Recieved b -
SAMPLE ANALYSIS REQUEST
I D SLI SL2 NH4 N NOS N Organic Cd Cr NI Pb As Fig Se pH
�� 900 PO boo Pow '�o 100
L.f P3r
SLIT: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL i plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
nmw
MMM MGM
r fr
C,
Page 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 11/25/2019 ! I - ! ! 0.6116
LIQUID
Na mg/I = (Na mglkg x % Solids) 100 = (1390 x 1.8400) + 100 = 25.576
Ca mg/I = (Ca mglkg x % Solids) + 100 = (3670 x 1.8400) + 100 = 67.528
Mg mg11 = (mg mg/kg x % Solids) + 100 = (2110 x 1.8400) + 100 = 38.824
Na meq = Na mgll + Moloc.Wgt.Na = 25.576 + 23 = 1 A 12
Ca meq = Ca mgll + Molec.Wgt.Ca = 67.528 + 20 = 3.3764
Mg meq = Mg mg/I + Molec.Wgt.Mg = 38.824 12 = 3.23533
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.112 + SgrRoot[0.5(3.3764+3.23533)] = 0.611592
Printed: 1/28/2020
13:25
Page 1

Waypointo
ANALYTICAL
121512019
Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-330-0006
Project Description: Winston 3rd
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypointanaiytica (.corn
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CI=R 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 16 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Q�re W 0—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Para 1 of e

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number:
19-330-0006
Client Project Description:
Winston 3rd
Lab No Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C
WTN
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
9045D
WTN
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
4500NO3F-2011
WTN
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
6010D
WTN
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SW-7471B
WTN
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C-TKN
WTN
69699 Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Parry 7 of 6

7621 Whitepine Road, Richmond, VA 23237
WaypointMain 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalocal.com
46622
Synagro Central LLC/ Technical
Mary Brewer Project Winston 3rd Report Date ; 12/05/2019
284 Boger Road Information : Received : 11/26/2019
Mocksville , NC 27028 me 607-�-
Report Number :19-330-0006
REPORT OFAIVALYSIS
Pauric McGroary
Agronomist
Lab No : 69699 Matrix: Solids
Sample ID : Winston 3rd Sampled: 11/25/2019 13:45
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Moisture
97.8
%
0.010
1
12102/1918:43
ADM
SM-254OG
Test
Results
Units
MQL
DF
Date 1 Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
6270
mg/Kg - dry
4550
1
12/05/19 08:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<225
mg/Kg - dry
225
1
12/05/19 12:06
ZBD
4500NO3F-2011
Organic N
20500
mg/Kg - dry
11400
1
12/04/19 09:00
CALCULATION
pH
6.3
SM.
1
12/03/19 07:06
JSL
9045D
Total Solids
2.19
°gyp
0.010
1
12/02/19 18:43
ADM
SM-2540G
Total Kjeldahl Nitrogen
26700
mg/Kg - dry
11400
1
12/04/19 09:00
JPJ
;M-4500-NH3C-TKP
Phosphorus
3610
mg/Kg - dry
227
1
12/03/19 19:43
BKN
6010D
Aluminum
127000
mg/Kg - dry
227
1
12/03/19 19:43
KKM
6010D
Arsenic
<22.7
mglKg - dry
22.7
1
12/03/19 19:43
BKN
6010D
Calcium
2-840
mg/Kg - dry
1140
1
12/03/19 19:43
KKM
6010D
Cadmium
<4.55
mg/Kg - dry
4,55
1
12/03/19 19:43
BKN
6010D
Chromium
27,5
mg/Kg - dry
11.4
1
12/03/19 19:43
BKN
6010D
Copper
54.5
mg/Kg - dry
11.4
1
12/03/19 19:43
BKN
6010D
Iron
29100
mg/Kg - dry
227
1
12/03/19 19:43
KKM
6010D
Lead
19.1
mg/Kg - dry
13.6
1
12/03/19 19:43
BKN
6010D
Magnesium
1800
mg/Kg - dry
227
1
12/03/19 19:43
KKM
6010D
Manganese
836
mg/Kg - dry
22,7
1
12/03/19 19:43
BKN
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Pacaa 3 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalVtical.com
Mary Brewer Project Winston 3rd
284 Boger Road Information
Mocksville , NC 27028
Report Number : 19-330-0006 REPORTOFANALYSIS
Lab No : 69699
Sample ID: Winston 3rd
Report Date ; 12/05/2019
Received : 11/26/2019
paiG m` owr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11/ 25 / 2019 13:45
Test
Results
Units
MOL
DF
Date I Time
Analyzed
By
Analytical
Method
Mercury
<0.686
mg/Kg - dry
0.686
1
12/04/19 15:24
KKM
SW-7471B
Molybdenum
<11.4
mg/Kg - dry
11.4
1
12/03/19 19:43
BKN
60100
Nickel
18.0
mg/Kg - dry
11.4
1
12/03/19 19:43
BKN
6010D
Potassium
1730
mg/Kg - dry
227
1
12/03/19 19:43
KKM
6010D
Selenium
<22.7
mg/Kg - dry
22.7
1
12/03/19 19:43
BKN
6010D
Sodium
<1140
mg/Kg - dry
1140
1
12/03/19 19:43
BKN
6010D
Zinc
260
mg/Kg - dry
56.8
1
12/03/19 19:43
BKN
6010D
Sulfur
5000
mg/Kg - dry
227
1
12/03/19 19:43
BKN
6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
n-„ - n --F C

.19. 0
ANALYTICAL
Waypoinr.,.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLCI Technical
Report Number: 19-330-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping contain erlcooler uncompromised?
9 Yes
0 No
Number of coolers/boxes received
F1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
JD Not Present
Chain of Custody (COC) present?
4D Yes
0 No
COC agrees with sample label(s)?
40 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
40 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
4D Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
10 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
i® Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
® NIA
Trip Blanks received with VOAs
0 Yes
0 No
® NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® NIA
High concentration container (48 hr) F Low
High concentration pre -weighed (methanol -14 d) F_ Low
concentration EnCore samplers (48 hr)
cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No
Signature: Brandi Watson Date & Time: 11 6 2019 13:38:17

SAMPLING LOG #
A & L Er
- "" ••, nr d1,RS. INC.
7621 W'
CI ADN OF CUS'T®®y
CUSTOMER: SYNAGRO
m
Richma
1[I1lflf�llf�l�lIIl11�11f1��illfl��flll
C ANALY5�5
RECORD
y
80¢/74�
o C�ntrai I����fflfl�lflllfil�f�
is.zs2-oot�
PROJECT MANAGER: tk
`-le
LLC/ Technical
vvinsl°h wrp
4662Z
°g T9_2d78 npling procedures
17 of these samples.
Phone:
SAMPLER
A & L CUSTOMER
LAB SAMPLE I,.D..;
SAMPLING
LOCATION
SAMPLE
TYPE
# OP SAMPLING
METHOD METHOD
n
CONTAINERS DATE TIME
PRESERVED SHIPPED
--Hu,o, i— uy cj&wpler:
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS;
For
monitoring purposes.
Date Time
Date I Time
1 li flI
Re laved by:
Recieved by:
Rec' y;
POTr:
REMARKS:
SAMPLE ANALYSIS REQUEST
I.D. SLR SL2 NH -N NO -N Organic jI CaCO Volatile
4 3 N Cd I Cr NiTPb As Hg Se pH equiv. Solids
Mo CI iV02 N
SLV: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Page 6 of 6

Sl�,iv, Pi_iXiG LOG
a
CUS_FOMER: �r�r��sr
n `a f
GR llllllllllllllllllllllllllllllll Ill lIIIIIIIIIIII
19-330 0006
IIII 46622
U9E(CGFRI I,
Svnaero Central LLC' Technical
13-37:50
• 1'RG..i'C f ��9��P�J�aG
1h IWinston 3rd
itE--i: _ -f (�'1"- I.�,�•
_.,., �_.
_`
ru�;i` that the ra cr jrord samplrf'7gproceCoras
°e used dtTr�14. C ollwction of these .3afT7ples.
SAMPLEn._..--
:'': _
=.6 -
CUSTMER SAMPL€NG SAMPLE
SAMPLE I.C. uOCPJ101v -rfPE
: OF
SA
.tllll, LJi�ll3 iETHOi� METI .OD
CONTAINERS
DATE TIIUC PRESERVED SHIPPED
ram!
Redaved by: REMARKS:
Daie
Time
Rr.h squished by:1
j
R �1i11a e oved by:
1 1
t
jCi
REflillo,ui-:hed by:
f
Dale
-�'
Tirr4
----...
_ Fieci l y
3HEUAL JNSTRUCTJONS: —
purposes.
SAiviPLE ANALYSIS REQUEST
,
SLn SL2 NH _M Nru3_N 0: �nic Cu Cf i Ni A� �� s,r � CaCC Uc€at€ie
€g PH � 3 Mn C-I i NO,-N I
J� egUly. j Solids
> i
t
•� i'j 1Jf� i � it � .—__- + `— _ I .... —_ __� _......_.__. _
r
71
SLJ: ToY�I Solids (Moisturr.), To[,l K;151dEhl'\11€roge;r�,
, F,hosphoru,s, and Patassiulii�L?: 33sic Test SI_i p€l;kSluarl,%laeiurn, Afumirunl , %langarlose, Clipper arlet Zirl�
Wage 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 11/2512019 1 ! - ! I O.6070
LIQUID
Na mgll = (Na Mg/kg x % Solids) + 100 = (1140 x 2.1900) - 100 = 24.966
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (2840 x 2.1900) + 100 = 62.196
Mg mgll = (mg mglkg x % Solids) 100 = (1800 x 2.1900) + 100 = 39.42
Na meq = Na mg1l + Mo[ec.Wgt.Na = 24.966 + 23 = 1.08548
Ca meq = Ca mg1l + Molec.Wgt.Ca = 62.196 20 = 3.1098
Mg meq = Mg mgll + Molec.Wgt.Mg = 39.42 + 12 = 3.285
SAR = Na meq + SgrRoof[0.5 x (Ca meq + Mg meq)] = 1.08549 : SgrRoot[0.5(3.1098+3.285)1 = 0.607047
Printed: 1 /2812020
13:32
Page 1

e
lag
Walkipoint
ANALYTICAL
12f612019
Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-330-0007
Project Description: Winston 4th
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pw:4 ,, cam
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

0
Waypoint,
ANALYTICAL
7621 White pine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sampie Summary Table
Report Number: 19-330-0007
Client Project Description: Winston 4th
Lab No client Sample ID Matrix Date Collected Date Received Method Lab ID
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
9045D
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
4500NO3F-2011
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
6010D
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
SW-7471B
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C-TKN
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Dana '7 of 9

liar .10 Wa7621 Whitepino Road, Richmond, VA 23237 lipointMain 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46622
Synagro Central LLC/ Technical
Mary Brewer Project Winston 4th Report Date : 12/D5/2019
284 Boger Road Information : Received : 11/26/2019
Mocl<sville , NC 27028
paw. g owr
Report Number: 19-330-0007 REPORTOFAtVALY5I5 Pauric McGroary
Agronomist
Lab No : 69700 Matrix: Solids
Sample ID : Winston 4th Sampled: 11/25/2019 13:45
Test
Results
Units
MQL
DF
Date ITime
By
Analytical
Analyzed
Method
Moisture
98.2
°/a
0.010
1
12/02/1918:43
ADM
SM-254OG
Test
Results
Units
MQL
DF
Date ITime
By
Analytical
Analyzed
Method
Ammonia Nitrogen
11400
mg/Kg - dry
5560
1
12/05/19 08:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<262
mg/Kg - dry
262
1
12/05/19 12:06
ZBD
4500NO3F-2011
Organic N
14300
mg/Kg - dry
13900
1
12/04/19 09:00
CALCULATION
pH
6.3
s.u.
1
12/03/19 01:06
JSL
9045D
Total Solids
1.78
%
0.010
1
12/02/19 18:43
ADM
SM-2540G
Total Kjeldahl Nitrogen
25700
mg/Kg - dry
13900
1
12/04/19 09:00
JPJ iM-4500-NH3C-TKP
Phosphorus
4920
mg/Kg - dry
278
1
12/03/19 19:48
BKN
6010D
Aluminum
160000
mg/Kg - dry
278
1
12/03/19 19:48
KKM
6010D
Arsenic
<27.8
mg/Kg - dry
27.8
1
12/03/19 19:48
BKN
6010D
Calcium
4520
mg/Kg - dry
1390
1
12/03/19 19:48
KKM
6010D
Cadmium
<5.56
mg/Kg - dry
5.56
1
12/03/19 19:48
BKN
6010D
Chromium
36.7
mg/Kg - dry
13.9
1
12/03/19 19:48
BKN
6010D
Copper
70.6
mg/Kg - dry
13.9
1
12/03/19 19:48
BKN
6010D
Iron
36100
mg/Kg - dry
278
1
12/03/19 19:48
KKM
6010D
Lead
25.4
mg/Kg - dry
16.7
1
12/03/19 19:48
BKN
6010D
Magnesium
2400
mg/Kg - dry
278
1
12/03/19 19:48
KKM
6010D
Manganese
1360
rng/K9 - dry
27.8
1
12/03/19 19:48
BKN
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quandtation Limit
Paqe 3 of 6

a
wavD061
,.
ANALYTICAL
46622
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Report Number :19-330-0007
Lab No : 69700
Sample ID ; Winston 4th
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
www.waypointa nalytical. corn
Project Winston 4th
Information :
REPORT OFANAL. YSIS
Report Date : 12/05/2019
Received : 11/26/2019
pwz' XF 60wr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11 / 25 / 2019 13:45
Test
Results
Units
MQL
DF
Date 1 Time
Analyzed
By
Analytical
Method
Mercury,
<0,811
mg/Kg - dry
0.811
1
12/04/19 15:25
KKM
SW-7471B
Molybdenum
<13.9
mg/Kg - dry
13.9
1
12/03/19 19:48
BKN
6010D
Nickel
23.8
mg/Kg - dry
13.9
1
12/03/19 19:48
BKN
6010D
Potassium
2120
mg/Kg - dry
278
1
12/03/19 19:48
KKM
6010D
Selenium
<27.8
mg/Kg - dry
27.8
1
12/03/19 19:48
BKN
6010D
Sodium
<1390
mg/Kg - dry
1390
1
12/03/19 19:48
BKN
6010D
Zinc
503
rng/Kg - dry
69.4
1
12/03/19 19:48
BKN
6010D
Sulfur
5720
mg/Kg - dry
278
1
12/03/19 19:48
BKN
6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Aarra 4 of 6

Waypoint(o
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9441 P Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLCI Technical
Report Number.- 19-330-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
I- 11
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
is Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
® NIA
Trip Blanks received with VOAs
0 Yes
0 No
® NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® NIA
F_ High concentration container (48 hr) 7 Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments: F—
Signature: p19 Brandi Watson Date &Time: 111261213:40:02

SAMPLING LOG 1#
CUSTOMER: SYNAGRO
PROJEC T MANAGER:
A & L EASTERN AGRIG1.11 h o Rrs
76PI tn"-:' '
CHARM OF CUSTORIV
RECORD
1�&0 ��ip1p�4A11;VSOS
lCV ��®FhY�
svnaure C;CCIVat LLC1 iachnica13:38'56l -oper field sampling procedures
wins,on AV, IEctlon of these samples.
Phone:j3j 70
A & L CUSTOMER SAMPLING SAMPLE
LAB k- SAMPLE I.D. LOCATION TYPE
SA
J'
# OF SAMPLING METHOD METHOD
CONTAINERS DATE TIME PRESERVED SHIPPED
0
Relinquished by Sampler:
hk
D to /f
Time
Recieved by: REMARKS:
Relinquished by,
Date
16)
Time
Recieved by:
�2
Relinquished by:
P &Cfal.
Time
Recieved by:
SPECIAL INSTRUCTIONS:
L&-)67
For monitoring purposes. PO#k: _
SAMPLE
ANALYSIS REQUEST
I.D.SLi
SL2
NHS N
NO N
Organic anlc
Cd
Cr
Ni
Pb
As
H 9
Se
P H
CaG03
equiv.
volatile
Solids
Mo
CI
NOZ»IV
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Page 6 of 6

Sodium Absorption Ratio Calculation (SAID)
Product Code Product Name Sample Date Report Range Ratio
2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 11/25/2019 1 1 - 1 1 0.5525
LIQUID
Na mg1l = (Na mglkg x % Solids) _ 100 = (1390 x 1.7800) + 100 = 24.742
Ca mg1l = (Ca mglkg x % Solids) + 100 = (4520 x 1.7800) W 100 = 80.456
Mg mg/1 = (mg mglkg x % Solids) + 100 = (2400 x 1,7800) + 100 = 42.72
Na meq m Na mg1l = Molec.Wgt.Na = 24.742 + 23 = 1.07574
Ca meq = Ca mg11 � Molec.Wgt.Ca = 80.456 = 20 = 4.0228
Mg meq = Mg mg1l _ Molec,Wgt.Mg = 42.72 -. 12 = 3.56
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.07574 � SgrRoot[0.5(4.0228+3.56)] = 0.552468
Printed: 1 /28/2020
Page 1 13:37

'10
/0000
T /�
- --- ---- --

I %
I-t
- ------ - ------------
s
... ... ... . ..... .... . .....

Section 4
® Maps of the residuals disposal sites

111412019
Paschat W. "Pat" Swann Water Treatment Plant to 3690 Woos iey Rd, Pfafftown, NC 27040 - Google Maps
Paschal W. "Pat" Swann Water Treatment Plant to 3690 Woosley Rd, Pfafftown, NC Drive 1.6 miles, 4 min
Y te 1' 1aps, 27040
Imagery ©2019 Google, Imagery 002019 Landsat / Copernicus, Maxar Technologies, U.S. Geological Survey, USDA Farm Service Agency, Map data ©2019 1000 ft
Paschal W. "Pat" Swann Water Treatment Plant
2200 River Ridge Rd, Pfafftown, NC 2704-0 V �
t
https:Ilwww.googie.comlmapsldirlPaschal+W.+^Pat'+Swann+Water+Treatment+Plant,+2800+River+Ridge+Rd,+Pfafftown,+NC+27040136.1569745,-80.4333771(c_b36.1528681,-80.4344533,2462m/am=t.._ 112

111412019 Paschal W. "Pat" Swann Water Treatment Plant to 5818 Jordans Gale Dr, East Bend, NC 27018 - Google Maps
t.^ Y _ e. � �I_} Paschal W, "Pat" Swann Water Treatment Plant to 5818 Drive 3.7 miles, 7 min
Jordans Gate Dr, East Bend, NC 27018
Imagery Q2019 Googie, Imagery @2019 Landsat / Copernicus, Maxar Technologies, U.S. Geological Survey, USDA Farm Service Agency,2000 ft
Map data ©2019
Paschal W. "Pat" Swann Water Treatment Plant
2800 River Ridge Rd, Pfafftown, NC 27040
1. Head northeast
ReMiici z:l Its:=file ti :�Ci rn
197 ft
2. Turn left
f;c'sLI;Jod rrlad
<, 3. Turn left onto River Ridge Rd
<, 4. Turn left onto Beroth Rd
r 5. Turn right onto Yadkinville Rd
6, Turn right onto Old U.S. 421/Yadkinville Rd
� Continue to follow Old U.S. 421
r> 7. Turn right onto Taylor Rd
0.2 mi
281 ft
1.7 mi
0.7 mi
0.1 mi
0.3 mi
h ttps:!lwww.google.coinlmaps/dir/Pasch aI+W.+'pat"+Swann+Water+Treatment+Plant,+2800+River+Ridge+Rd,+Pfafftown,+NC+27040/36,1408812,-5... 1 /2

111412019 Paschal W. ,Pal, Swann Water Treatment Plant to 1244 Vernon Rd, East Bend, NC 27018 - Google Maps
Paschal W, "Pat" Swann Water Treatment Plant to 1244 Drive 4.2 miles, 9 min
�'`� Maps Vernon Rd, East Bend, NC 27018
Imagery 02019 Google, Imagery ©2019 Landsat / Copernicus, Maxar Technologies, U.S. Geological Survey, USDA Farm Service 2UUU tt
Agency, Map data ©2019
yk-ys1 --a-
11 ttps:llvvvw,google.Gotnlm a psldi r/Paschal+W,+Ta t„+Swa nn+Water+Treatment+Plan t,+2800+River+Ridge+ Rd. +Pfafftown,+NC+27040136,1331766,-8... 111

Section 5
® Field soil sampling results

Agricultural Lime Application Log
Year: 2019
Project: Winston
Field
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied(CCE Eq.)
[��teApplied(state-county-site-field)
FO-X9-1
5.4
1.OT/Ac.
YK-X39-1
5.6
1.OT/Ac.
1.0
11/30/19
YK-X39-2
5.5
1.0 T/AC
1.0
11/30/19
YK-X39-3
5.5
1.OT/Ac.
1.0
11/30/19
-i- Me will ae appiiecl when conditions improve.

Page 1 of 1
Report Number: 19-317-0569(a Account Number: 46434 Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
Send To: Synagro Central LLCIAsheboro ANALYTICAL www.waypointanalytical.com
Mary Brewer "Every acre ... Everyyear."TM Grower: Tony Apperson
284 Boger Road
Mocksville NC 27028
Farm: FC-x9
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 11/13/2019 Date Of Analysis: 11/14/2019 Date Of Report: 11/14/2019 NC = North Carolina Fertility Index Value
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample [D
Lab
%
Soil
M3
K
Mg
Ca
Na
Soil
Buffer
H
Field [D
Number
Rate
Class
Ibs1A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meg1100g
megl100g
1
09944
5.7
149
31 M
64 VL
448 VH
1301 M
12 VL
7.0
0.0
10.5
H
I MIN
NC=26
NC=33
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
K
Mg
Ca
Na
H
NO,N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
%
IN,
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
mslcm Rate
1
1.6
35.6
62.0
0.5
0.0
15 L
23.9 VH
85 VH
87 VH
1.5 M
0.6 M
NC=31
NC=597.5
NC=531
NC=75.0
Values on this report represent the plant availaNe nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Date Received: 11/13/2019
Date Of Report: 11/14/2019
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), mslcm (milti-mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: waypeintAnalytical Virginia, Inc.
Salts ms/cm x 640 = ppm.
SOIL FERTILITY RECOMMENDATIONS
by: gwp , Iff 6a7---
Pauric McGroary
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P20,
K
z O
Mg
S
Zn
Mn
Fe
Cu
B
Field lD
Tons
TonslA
Ib1A
Ib1A
Ib1A
IblA
IblA
Ib1A
IblA
IblA
IblA
Ib1A
1
Fescue Hay
4
0.0
200
50
157 j
0
9
0
D
0
0
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whale or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.

Page 1 of 1
Report Number: 19-326-0588
Account Number:46431 7621 Whitepine Road, Richmond, VA 23237 aypoint,Main 804-743-9401 ° Fax [phone]
Send To: Synagro Central LLC ANALYTICAL www.waypointanalytical.com
Marshal Puryear "Every acre ... Everyyear,'T. Grower. Tony Apperson
284 Boger Rd
Mocksville NC 27028
SOIL ANALYSIS REPORT
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 11/22/2019 Date Of Analysis: 11/2512019 Date Of Report: 11/25/2019
NC = North Carolina Fertility Index Value
Sample I❑
Lab
oM
WN
ENR
Phosphorus
Potassium
alcium
Sodium
pH
Acidity
C.E.0
%
Soil
Ibs1A
M3
K
n;78
Ca
Na
Soil
Buffer
H
Field ID
Number
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pm Rate
ppm Rate
PH
Index
megllDDg
meg11009
FO-X9
16365
3.8
119
13 VL
65 L
137
L
27 L
6.4
6.80
1.3
4.6
MIN
M
NC=11
NC=33
Sample ID Percent Base Saturation
Nitrate Sulfur ,Zinc Manganese
Iron Copper Boron Soluble Salts
Field ID K Mg Ca Na H
NO, N S Zn Mn
Fe Cu B SS
% % % %
ppm Rate ppm Rate ppm Rate ppm Rate
ppm Rate ppm Rate ppm Rate mslcm Rate
FO-X9 3.6 24.8 41.1 2.6 28.3 37 VH 4.1 H 161 VH
88 VH 0.9 M 0.2 VL
NC=77 NC=102.5 1 NC=1006
NC=45.0
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
Explanation of symbols: % (percent), ppm (parts per mi€lion), IbslA
(pounds per acre), mslcm (milli -mhos per centimeter), meg1100g
This report applies to sample{s) tested. Samples are reta€red a
maximum of thirty days testing,
H (High), VH (Very High). ENR - Estimated Nitrogen Release,
(millii-equivalent per 10D grams). Conversions: ppm x 2 = Ibs1A, Soluble
after
by
idur�c m
C.E.C. - Cation Exchange Capacity.
Salts mslcm x 640 = ppm.
Analysis prepares by: Waypoint Analyi cal Virginia, Inc.
Pauric McGroary

Page 1 of 1
Report No: 19-317-9569
Account No: 46434
Advisor: Synagro Central LLCI Asheboro
Mary Brewer
284 Boger Road
Mocksville NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypointanalytical.com
Farm:FO-x9
Date Received: 11/13/2019
Date of Report: 02f1312020
ab No Field 1D Sample ID
Soil Class HM% WN pH
Ac
P-1
K-1
S-1
Mn-1
Zn-I
Zn-Al
Cu-1
CEC
BS% Ca% Mg% ESP Na SS-1 NO3 N
)9944 1
MIN 7.0
0.0
26
33
31
531
598
59B
75
10.5
100 62 36 0.5 0.1
:rop Recommendations:
Rec Uom Lime (t/acre)
N
P205
K20
S
Mn
Mn-Al
Zn
Cu
B
Mg Last Crop
I- Fescue Hay
Iblacre 0.0
150
76
72
20
0
320
0
0
0
0
Comment:
Test result units = CEC and Na in meg1100cm3: NO3 N in mgldm3; WA/in glcm3
North Carolina Division of Water Quality Certification 4257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

jj44 {I ly l} lj 4i} j4i4 1 j{ 19.317-0569 • ORM Account #
Waypoint
1ll IIII���I�� 11-13-2019
4G434
Svnaaro Central t -C7 Asheboro
11 27 39
ANALYTICAL Tonv AaaersonOD,x9
Grower/Project Information Customer
Information
Submitted By
Charge To
Farm ID
J�tJ
Field ID
Credit Card #
CSV
Exp. Date:
/
phone #
E-mail address
Crop Info For Recommendations
Sample ID
p
Lab Number
( Lab Use
Only)
S1 M
S21VI -Specify Additional
Tests
53M
Soluble
Salts
Texture
NO3-N
Additional
Tests
Intended
Crop
Yield
Goal
Alternative
Crop
Yield
Goal
Previous Crop
S
Gu
Fe
Mn
Na
S
Zn
Mehlich
III
Test Packages
Special
Instructions or Additional
Tests
S1M - Organic matter, Phosphorus, Potassium, Calcium, Magnesium, pH, Buffer pH
Cation Exchange Capacity, and % Base Saturation.
S2M - Test S1 M plus any two of the following: Sodium, Sulfur, Boron, Zinc,
Manganese, Iron, Copper. Each additional test (above two) cost $2.00.
S3M - Test S1 M plus Sodium, Sulfur, Boron, Zinc, Manganese, Copper, and Iron.

Page 1 of 2
Report Number: 19-317-0540
Account Number: 46434
Send To: Synagro Central LLCI Asheboro
Mary Brewer
284 Boger Road
Mocksville NO 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Keith Matthews
Farm: YK-X39
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss Cn Ignition Water pH
Date Received: 1111 W2019 Date Of Analysis: 11/14/2019 Date Of Report: 11/14/2019 NO = North Carolina Fertility index Value
OM
W!V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
IAcidity
C.E.0
Sample ID
Lab
%
Soil
M3
K
Mg
Ca
Na
Soil
Buffer
H
Field [D
Number
Rate
Class
lhs1A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meg1100g
meglloog
1
09803
2.6
96
149 VH
73 M
102 H
442 M
8 VL
5.6
6.83
1.0
4.3
M
NO = 124
NO = 37
MIN
2
09804
3.9
122
185 VH
1' 8 VH
100 H
429 L
8 VL
5.5
6.81
1.2
4.6
M
NC=154
NC=60
MIN
3
09805
2.9
101
209 VH
140 VH
108 H
454 L
9 VL
5.5
5.81
1.2
4.8
M
MIN
NC = 174
NC = 72
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
K
Mg
Ca
Na
H
NO, N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
mslcm Rate
1
4.4
19.8
51.4
0.8
23.3
11 L
10.8 VH
34 H
277 VH
1.5 M
0.3 VL
NC=23
NC=270.0
NC=213
NC=75.0
2
6.7
18.5
47.7
0.8
26.7
9 VL
9.6 VH
28 H
249 VH
1.5 M
0.3 VL
NC=19
NC=240.0
NC=175
NC=75.0
3
7.5
18.8
47.3
0.8
25.0
12 L
11.6 VH
20 M
211 VH
1.2 M
0.3 VL
NC=25
NC=290.0
NC=125
NC=60.0
values on this report represent the plant available nutrients in the Explanation of symbols; / (percent), ppm (parts per million), IbslA This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), mslcm (milli -mhos per centimeter), meg1100g maximum of thirty days after testing. by:
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs1A, Soluble Analysis prepared by: WaypointAnaiytical Virginia, Inc. i
C.E.C. - Cation Exchange Capacity. Salts mslcm x 640 = ppm.
PaUrlG McGroary

Page 2 of 2
Report Number: 19-317-0540
Account Number:46434
N 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
Send To: Synagro Central LLC/Asheboro ANALYTICAL www.waypointanalytical.com
Mary Brewer "Every acre... Every year"rM Grower: Keith Matthews
284 Boger Road
Mocksville NC 27028
Farm: YK-X39
Date Received: 11/13/2019
Date Of Report. 11/14/2019 SOIL FERTILITY RECOMMENDATIONS
Sample 10
Yield Goal
Lime
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Field ID
Intended Crop
bu
Tons/A
N
PzOs
K2C
Mg
S
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
1
Soybeans
60
0.8
15
0
97
0
11
2LSoybeans
60
0.8
15
0
54
0
13
rornnT-
150
0.8
183
0
40
0
23
Comments:
Zinc
Zn
Ib/A
Manganese
Mn
Ib/A
Iron
Fe
Ib/A
Copper
Cu
WA
Boron
B
Ib/A
0
0
0
0
1.0
0
0
0
0
1.0
0
4
0
0
1.4
Sample(s) : 2 Crop: Soybeans
Boren recommendations are on a broadcast basis.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." y�
Our reports and letters are far the exclusive and confidential use of cur c€ients„ and may not be reproduced in whole or part, nor may any reference be made to the pwi. Ke 60wr
werk,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 1 of 1
Report No: 19-317-954D
Account No: 46434
Advisor: Synagro Central LLCI Asheboro
Mary Brewer
284 Boger Road
Mocksville NC 27028
f
Client: Keith Matthews
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanaiytical.com
Farm: YK-X39
Date Received: 11/13/2010
Date of Report: 02/13/2020
Lab No Fleld lD
Sample 1D
Soil Class HM% WIV pH
Ac
P-1
K-1
S-1
Mn-1
Zn-1
Zn-Al
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
109803
1
MI N
5.6
1.0
124
37
23
213
270„
270
75
4.3
76
51
20
0.8 0 I
Crop Recommendations:
1- Soybeans
Rec Uom
Iblacre
Lime (t/acre)
0.5
N
0
P205
0
K20
64
S
20
Mn
0
Mn-Al
144
Zn
0
Cu
0
B
0
Mg
0
Last Crop
09804
2
MIN
5.5
1.2
154
60
19
175
240
240
75
4.5
74
48
19
0.8 0
Crop Recommendations:
1- Soybeans
Rec Uom
lb/acre
Lime (Uacre)
0.5
N
0
P205
0
K20
30
S
20
Mn
0
Mn-Al
123
Zn
0
Cu
0
S
0
Mg
0
Last Crop
09805
3
MIN
5.5
1.2
174
72
25
125
290
290
60
4.8
74
47
19
0.8 0
Crop Recommendations:
1-Corn
Rec Uom
lb/acre
Lime (Yacre)
0.5
N
160
P205
0
K20
10
S
20
Mn
0
Mn-Al
100
Zn
0
Cu
0
B
1A
Mg
0
Last Crop
Comment:
Test result units = C5C and Na in meg1100cm3: NO3 N in mgldm3: WN in glcm3
North Carolina Division of Water Quality Certification 9257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

. FORM
111 flflllfII fEIII IIifllffllllIl f ffIlllI�Illif11IfIlfIllfflll 4434 0190 637
Keith MatihewsNK_X39
I
istomer Information
Submitted By
A1�
Account #
Charge To
Farm 1D
Field ID
— -
Credit Card #
CSV
Exp. Date: 1
Phone #
E-mail address
�1J�„ 9
Crop Info For Recommendations
LZ Number
S2M - Specify Additional
Intended
Yield
Alternative
Yield
Sample ID
p
(Lab Use
S1M Tests S3M
Soluble
Texture NO -N Additional
s
Only)
B Cu Fe Mn Na S Zn
Salts
Tests
Crop
Goal
Crop
Goal
Previous Crop
M - Organic matter, Phosphorus, Potassium, Calcium, Magnesium, pH, Buffer pH QPmac i instrucrions or
Cation Exchange Capacity, and % Base Saturation.
M -"rest S1 M plus any two of the following: Sodium, Sulfur, Boron, Zinc,
Manganese, Iron, Copper. Each additional test (above two) cost $2.00.
M - Test SIM plus Sodium, Sulfur, Boron, Zinc, Manganese, Copper, and Iron.

Winston-Salem/Forsyth County Utilities
WQ0031314
2019 Residuals Land Application Report
R.W. Neilson Water Treatment Plant
TABLE OF CONTENTS
Section 1
• DEQ Form DMSDF.- Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Farm
• DEQ Form DMSDF(Supp) - Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form (Supplemental Information)
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and chain of custody's)
• Copies of our SAR/PAIN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
0 Field soil sampling results

Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface
Disposal Certification and Summary Form
• DEQ Form DMSDF(Supp) -Class A Annual Distribution and
Marketing/Surface Disposal Certification and Summary Form (Supplemental
Information)
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: W00031314 FACILITY NAME: Winston Salem - Neilson Water Treatment Plant
PHONE: COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes El No If No slop parts A, R, C and certify form below
Part A": P $*
Month Sources(s) (include NPDES # if
applicable)
A
December
from
Volume (dry tons)
Amendment/ rResidualIn Product Out
Bulking Agent I
2334.69
2334.69
aent(s) used:
a
Recipient Information
Name(s) Volume (dry tons) Intended use(s)
2334.69
2334.69
* If more space is required, attach additional information sheets (FORM D (supp) . Total Number of Form DMSDF (Supp) 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit El Yes
(including but not limited to items I-3 below) issued by the Division of Water Quality: ❑ No : if No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting fal xn o mation, including the possibility of fines and imprisonment for knowing violations."
Signature
0 '.2334
Annual (dry tons): 0 ±BuIkin-9
34.oy
iment(s) used: A
MSDF }
Date Signatu fPreparer**
(if different from Permittee)
**Preparer is defined in. 40 CFR Part 503.9(r) and 15A NCAC 2`I' .1102 (26)
1-8S--q,aav
D ate
DENR FORM DMSDF (12I2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ ]PERMIT #: WQ0031314 FACILITY NAME: Winston Salem - Neilson Water Treatment Plant
PHONE: COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE (please cheep one): El Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
Ud Tlictrihntinn And Mnrlretinu (comnlete Parts A. and B)
Part A*:
Part B *. .
Month
Sources(s) (include NPDES # if
a
applicable)
PP )
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In,
Product Out
Narne(s)
Volume (dry
tons)
Intended uses)
May
Neilson WTP - NCO086011
709.83
709.83
Roger Spillman
709.83
soil amendment
September
Neilson WTP - NCO0860 i 1
1624.86
1624.86
Greg Dooley
1624.86
soil amendment
Totals:
Annual (dry tons):
0
2334.69
2334.69 . 2334,69
Amendment(s) used: Bulking Agent(s) used:
Tf mnrP snare k reoiiired. attach additional information sheets (FORM DMSDF (sum))): Total Number of Form DMSDF (Supp) I
DENR FORM DMSDF (Sapp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WQ0031314 Laboratory:
Winston Salem/Forsyth County Utilities Commission
NCO086011
WWTP Name: Neilson Water Treatment Plant
2)
3)
4)
5)
Waypoint Analytical
Residual Analvsis Bata
Cone.
Sample or Composite Date
Parameter Limit
4/25/19
4/25/19
4/25/19
4/25/19
Spring 9/11/19 9/11/19 9/11/19
9/11/19
Pall
(mg/kg) m nc a
#1
#2
#3
#4
Average #1 #2
#3
#4
Average
Percent Solids (%) NA
21.6
23.8
29.6
28.3
26 23.4 23.2
28.4
20.8
23.95
Arsenic 75
6.67
7.46
7.26
7.81
7 8.25 6.51
5.39
6.54
6.67
Cadmium 85
0.229
0.371
0.378
0.382
0 0.212 0.344
0.359
0.353
0.32
Copper 4,300
34.6
50.7
37.8
37.8
40 45.3 46.6
40.8
44.9
44.4
Chromium NA
35
60.6
44.3
43.5
46 44 49.1
43
45.1
46.05
Lead 840
23.1
37.2
28.7
29.1
30 24.9 28
25.3
27.1
26.33
Mercury 57
0.0912
0.0859
0.0912
0.0746
0 0.0739 0.078
0.0856
0.0846
0.08
Molybdenum 75
0.787
1.27
1.05
0.985
1 1.5 0.771
0.602
0.625
0.87
Nickel 420
16.2
26.9
19.7
19.5
21 22 22.1
19.4
22.5
21.5
Selenium 100
2.27
2.3
1.66
1.73
2 2.09 2.11
1.73
2.36
2.073
Zinc 7,500
96.3
144
106
108
114 123 130
115
137
126.25
Total Pbosphorus NA
2990
2590
2070
2210
2465 2300 2470
2510
2500
2445
TKN NA
5320
5540
4360
4450
4918 3970 1590
1170
1150
1970
onia-Nitrogen NA
Lrrate
284
445
358
392
370 1290 741
683
480
798.5
and Nitrite NA
75.9
54
47.3
32
52 21.4 21.6
17.6
21.1
20.43
'For surface disposal facilities the ceiling concentration limits listed in this form are
not applicable. Reference the individual permit
for metals limits.
"I certify, under penalty of law, that this document was prepared
under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant
penalties for submitting false inf creation,
including the possibility
of fines and imprisonment for knowing violations."
Signature reparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and
15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0031314
Facility Name: Winston Salem/Forsyth County Utilities Commission
Residual Source
NPDES # or WQ#:
WWTP Name:
'D ;11,,.,1 A- 1-0;0 "l +i
NCO086011
Neilson Water Treatment Plant
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
2\LrJIIIJµui �\aaaaa
Parameter
(mg/kg)
Sample or Composite Date
4/25/19
#1
4/25/19
#2
4/25/19
43
4/25/19
44
Spring
Average
9/11/19
#1
9/11/19
#2
9/11/19
#3
9/11/19
#4
Fall
Average
Aluminum
117000
140000
116000
118000
122750
104000
109000
102000
112000
106750
Calcium
861
869
652
809
797.8
974
1030
838
1080
980.5
Magnesium
1500
2330
2040
1880
1937.5
2260
2450
2140
2440
2322.5
PH
7.1
6.6
6.4
5.9
6.50
6.1
5.9
5.6
6.2
5.95
Potassium
1440
2310
1950
1780
1870
1920
2130
1880
2150
2020
Sodium
357
362
261
273
313.25
1 79.5
102
60.9
101
85.85
PAN
722
786
627
634
692
934
477
408
328
536.83
SAR
0.79
0.7
0.61
0.64
0.15
0.19
0.13
0.18
Eld
I
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature "reparer *
'"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
1-1,3-- a.0 &0
Date
DENR FORM RSSF - B (12/2006)

Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF -Annual Land Application Field Summary Form

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Residual
Sample or
Com-
posite
Date
% Solids
Arsenic
Lead
Nickel
Selenium
Zinc
Total
Phos-
Winston Salem - Neilson Water Treatment Plant Total Dry Tons Applied (Annual): 607.55
WQ0031314 Cation Exchange Capacity (non 503 only): 0
Roger Spillman Owner: Roger Spillman Predominant Soil Series: MrC2
18 Acres Permitted: 18 Site #: DV8 Field #: 5
;is Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
�019 019
Spring Fall
Average Average
25.8 24
7.3 6.7
0.3 0.3
40.2 44.4
45.9 46.1
29.5 26.3
0.1 0.1
1 0.9
20.6 21 J
2 2.1
113.6 126.3
2465 1 2445
.,1 u- , A4a+ri1 Pii,.IA T.narlinac (C'alenlafPtl in the/noel-
Total
2
3
4
5
6
7
S
9
10
1 i
12
y
DT/Ac./
App,
14
Event
11.09
22.66
Arsenic
0.162
0.304
0.000
0.000
1 0.000
0.000 1
0.000.
0.000
0.000
0.000
0.000:
0.000
0,466
Cadmium
0.007
` 0.014
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
0.020
Copper
0.892
2.012
0.000'
`0.000
0.000
0.000
0.000
0.000`
0.000
0.000
0.000
0.000.
2.904
Chromium
1.018
2.089
0.000
0.000 `
0.000
0A00
0.000
0.000
0.000
0.000
0.000 .
' 0.000
3.108:.
Lead
0.654
1.192
. 0.000 '
' 0.000
0,000
0.000
0.000
0.000
> 0.000
0.000
0.000.
0.000
1.846.`
Mercury
'0.002
0.005:
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.022,
0.041'
0.000
0.004
0.000
0.000
0.000.
0 000
0.000
0.000
0.000
0.000
0.063
denum
Nickel
0.457
0.97.4
0.000
0.000
0.000
0.000.
0.000
0.000`
> 0.000
0.000
0,000
0.000
1.431 `
Selenium
0.044
0.095
' 0.000
0.000.
0.000`.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0..140
Zinc
2.520
' S.724`
0.000
0.000
0.000
0.000
0.000
0.000
:0.000
0.000
0.000:
0.000
8.244
Total
Phos-
54.688
110,807
0.000.
0.000
0.000.
0.000
0.000
0.000
.0.000
0.000
0.000
0.000
165.496
horus
"1 certify, unner penalty of law, inai finis uUcunient Was prepat VU uuuGx ruy UAIIa.,,Vu v,
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
dY 4; - 1/13/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
F'e ld # 5 Acres Utilized: 18
Facility Name: � Salem - Neilson Water Treatm( WQ Permit # W00031314 1
Land Owner: Roger Spillman Annual Dry Tons Applied 607.55 Site #: DV8
Acres Permitted: 18
Operator: Roger Spillman Predominant Soil Series: MrC2 Cation Exchange Capacity (non 503):
Crop 1 Name: CirriPx Crop 1 Max. PAN: 186 Crop Z Name: Rye Grass Crop 2 Max. PAN: 50
o
Ga
5/23/19
5/24/19
5/28119
9/25/19
9126119
Volume applied Volume
(enter one) Solids/ % Applied per
Liquid I Solids Acre
Cu. Yds I Gallons
486
117
316
712
1306
WTons/Ac)25A25.825.8
24
7 995
24
14.665
0.000
OMO
0.000
0.000
0.000
0.000
0 O00
Residual Sources
(NF'DES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
�et'
Precip•
Past 24
Hrs.
inches
oa* D
o
C
v
*
0
4�
I- -
w.
o
TIN
mglkg
Z
o
ac o
rn
mglkg
Nitrate
and
Nitrite
mglkg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Czop 1 Crop 2
Neilson WTP
Moist)
Dry
<.5"
S
0.5
0.1
4917.5
369.8
52.3 I
8.119
NA:':
Sudex
Neilson WEDry
<.5"
S
0.5
0.1
4917.5
369.$
52.3
1.955
NA :
Sudex
NeilsonWTP
Dry
<_5"
4917.5
369.8
52.3
5.279
= NA:?
Sudex
Neilson WTP
Dry
C5"
S
0.5
0.1
1970
798.5
20.4
Na
8 583
Rye
Neilson WTP
Dry
<5"
S
0.5
0.1
1970
798.5
20.4
Na
% I5.744
RYe
0.000
0.000
0.000
0.000
..0.000
0.000
0:000 ;
: 0.000
0.0DD
O.Dao
0.000'
>' 0.00V
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS: 2937 (0) AS Cd Cu Cr Pb H Mo Ni Se Zn P 15.353 24.328 Lizne A lied
Annual lbslacre gO.466 0.020 2.904 3.108' "1.846 O.D07: 0.063' ''1.431 0.140 8.244 165.496 DatelbslacPrior Years Cumulative lbs/ac 0 0 0 D 0 0 0 0 0
Current Cumulative lbslac 66 0.020 2.904 3.108 ` 1.846 O.007 0.063 1.431 0.1Permitted C. P. L. R.**** 34 1338 267 15 374 89 2498
186, :;:SD.
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/13/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land ApplieT Date aerobically digested -0.3, raw sludge -0.4
* * **C.P.L.R.: Cumulative Pollutant LoadinIZ Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary norm to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Winston Salem -Neilson Water Treatment Plant Total Dry Tons Applied (Annual):
WQ0031314 Cation Exchange Capacity (non 503 only):
721.28
0
Roger Spillman Owner: Roger Spillman Predominant Soil Series: MrB2
20 Acres Permitted: 20 Site #: DV8 Field #: 6
Residual
Analysis Data
(Heavy
Metals and Total Phosphorus
use mg/kg, % Solids use
Raw Percent 14):
Sample or
1 2
3
4 5 6
7 8 9 10
11 12
a19 019
Corn-
Spring Fall
posite
Average Average
Date
% Solids 1
25.9
24
Arsenic
73
6.7
Cadmium
0.3
0.3
Copper
40.2
44.4
Ch-romium
45.9
46.1
Lead
29.5
26.3
Mercury
0.1
0.1
Molyb-
1
0.9
denum
Nickel
20.6
21.5
Selenium
2
2.1
Zinc
113.6
126.3
Total
Phos-
2465
2445
horus
Annual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
y
DT/Ac./
°
m
App.
Event
10.52
25.55
Arsenic
0.154
.0.342
0.000
0.000
0.000.
` 0.000
0.000
0,000
1.0.000
0.0.00
0.000
0.000
0.496
Cadmium
0.006
0.015''
0.000
6.000
0.000
0.000
0.000'
' 0.000
0.000
0.000
0.000 •
0.000
0.022
Copper
0.845
2.269 `'
0.000
0.000
0.000
` 0.000
0.000
0.000
0.000
0.000.
0.000
.0.000.
3.114
Chromium
0.965
2.356:
0.000
0.000
0,000.
0.000
0.000
0.000
0.000
0.000
0.000`
0.000
3.321
Lead
0.620.
1.344'
: 0.000
0.000
0.000
0.000 `
0.000
0.000
0.000
: 0.000
0.000.
0.000
1.964.
Mercury
0.002 :
0.005
0.000
0.000
0.000
: 0.000
0.000 `
.0.000..
0,000.1
0.000
0.000
' 0.000
0.00.7
Molyb-
.021
0 046 .:
O.Ooo..
0.000
0.00.0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067'
denum
:.. , :
.
0.433
1.099.
0.000
0.000
0.000 `
0.000
0.000
0.000 `
' 0.000
0.000
0.000'
0.000
1.532
S
tZine
`0.042`
0.107
0.000:
0.000
0.000..
OA00
0.000
0.000 :
0.000
' 0.000
0.000.
0.000 `
0.149.
2:389
.6.453..
` 0.000:
0.000
0.000
`0.000 .
0.000
0.000..
' 0.000
.0.000
0.000 `
0.000
8.843
Total
Phos-
51.844
.124.930
0.000,
0.000
0.000.
0,000.
0.000.
0.000_
'.0.000
0.000...
0.000.
0.00.0
176.774
horns
I
J
"I t'f under
enalty of law that this document vas prepared under my direction
or supervision in accordance with
cer y, p f
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
4; _ 1/13/2020
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
d # b Acres Utilized: 20
Facility Name: i Salem - Neilson Water Treatmi WQ Permit # WQ0031314 F iel
Land Owner: Roger Spillman Annual Dry '.Cons Applied. 72128 Site #: DV8 Acres Permitted: 20
Operator: Roger Spillman Predominant Soil Series: MrB2 Cation Exchange Capacity (non 503):
221 Crop 50
Crop 1 Name: Sudex Crop 1 Max. PAN: p 2 Name: Rye Grass Crop 2 Max. PAN:
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
�e'
Moisf
applied
(enter one) Solids)
Liquid
Cu.Yds Gallons
%
Solids
Volume
Applied per
Acre
(DsyTonslAc)
jVolume
734
25.8
7.974
Neilson WTP
Neilson WTP
Neilson WTP
Neilson WTP
Dry
Dry
Dry
Dry
195
25.8
2.118'
39
25.8
0.424
1580
24
15.969 "
9/25119
948
24
9.5811.
Neilson WTP
Dry
0.000
0.000
0.000
0.000
0.000 '
0.000
Residuals Application:
Cd I Cu
I CT
0.000
As
TOTALS:1
3T961
7 0
Precip.
a
o
�
Nitrate
PAN Applied
Name of Crop Type
Past 24
-0
m
v
�
TAT
� �
o
an d
(lbs/acre)
Receiving Residual
Hrs
P.
Nitrite
Application
3,
mglkg
mg/kg
mglkg
Crop 1 Crop 2
Crop 1 Crop 2
inches
�
S
0.5
0.1
4917.5
369.8
52.3
11,036NA.''
Sudex
<.5
S
0.5
0.1
4917.5
369.$
52.3
2.932 -NA
Sudex
<.5"
S
0.5
0.1
4917.5
369.8
52.3
0.586 ` ' : NA.:'
Sudex
<,5"
S
0.5
0.1
1970
798.5
20A
Na 17,143
Rye
<.5"
S
0.5
0.1
1970
798.5
20.4
Na 10.286:
Rye
0.000:: 0.000
0.000
0.000:
0.000 ''
!; 0.000
0,000 ;
` 0.000'
0.000
0.000 '
0.000
0.000
0.000 '
totals on FORM
FSF
supp ( attach
FORM
FSF supp
to this form):
Pb
H
Mo
Ni
Se
I Zn P
14.554:
27.429
LimeApplied
D t
lbslac
Annual lbs/acre 0.496 0.022 1 3,114 1 3.321 1 1.964 ° 0.007 0,067 1 1.532 0.149 8.843 176.774 a e
Prior Years Cumulative ibs/ac 0 0 0 0 0 %0.007
0 0 0 0
Current Cumulative lbs/ac 0.496 0.022 3.114 3,321 1.9640.067 1,532 0.149 8.843
Permitted C. P. L. R.**** 36 34 1338 267 374 89 2498
Permit PAN Limit 1 st/2nd Crop 221 50:
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/13/2020 **Volatilization Rate: Surface - 0.5, Injectionllncorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant LoadinjZ Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Residual
Winston Salem - Neilson WTP Total Dry Tons Applied (Annual): 1005.86
W00031314 Cation Exchange Capacity (non 503 only): 0
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
27 Acres Permitted: 27 Site #: DV8 Field #:
;is Data (Heavy Metals and Total Phosphorus use mg/kg, %_Solids use Raw Percent
Com-
posite
Date
019
Spring
Average
019
Fall
Average
% Solids
25.8
24
Arsenic
7.3
6.7
Cadmium
0.3
0.3
Copper
40.2
44.4
Mromium
45.9
46.1
Lead
29.5
26.3
Mercury
0.1
0.1
Molyb-
denum
1
0.9
Nickel
20.6
21.5
Selenium
2
2.1
Zinc
113.6
126.3
Total
Phos-
2465
2445
AX-4..3 'P.-IA i .,.,r�{nrr� (f nimilnl-nr'i in IhQh CrPi•
MrB2
9
3
4
5
6
7
8
9
10 J
11j
12 Ja
Total
2
DT/Ac./
a
App.
14
Event
11.11
26.15
Arsenic
0.162
0,350
0.000
` 0.000
0.000.`
0.000 :
0,000
0.000
0.000`1
0.000
` 0.000:
' 0.000
0.513
Cadmium
' 0.007 :
0.016
'. 0,000
0.000
0.000 '
0.000 `
' 0.000
0.000
0.000
0.000.
0.000.
0.000
0.022 "
Copper
0.893
2.322
0.000
0.000
6.000
0.000
0.000
0.000
0.000
0.000
0.000 `
. 0.000
3,215
Chromiu
` 1.019
2.411
0.000-
0.000
0.000.
0.000
0.000
0.000
0.000 ::
0,000.
.0.000.
0.000.
; ` 3.430 .
Lead
0.655
1.375
0.000
0.400 :
0.000 `
0.0041
0.000
0.000
0.000.
0.000:
• 0,000
.' 0.000
2.031
Mercury
0.002
`0.005
0.000
0.000
6.000:
'0.000
0.000
0.000
0.000:
0.000:
0.000
0,000`
0.007'
Molyb-
0.02.2
Q 047..
0.000 :
0.000
0.000
0.000
0.000
0.000
0.000
0,0001
0.000...
0.000
0.0.69
denum
Nickel
0.458
1.124
0.000
0,000
0.000
0.000
0.000.
0.000
0.000.1
0.000
0.000
0.000:
`1.582
Selenium
:`0.044
0.110 `
0.000
0.000
0.000.:
0.000
`0.000.
0.000
0.000
0.000
0.000
0.000
0.154:
Zinc
2.523.
6.605'
0.000 `
0.000
0.000
0.000
0.000
0..000
0.000
0.000 '
0.000
0,000
9.128
Total
Phos-
54.748
127,869
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
182.616
horns
'.
"i certily, antler penalty of law, Trial in is uucunnenn ryas PI upaI VU uuuci AAAY U11 V . 1-- --..y..........0 --- «--- --»--__ .. _
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/13/2020
Date
DENR FORM MFLSF (12/2006)

]Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Winston Salem - Neilson WTP WQ Permit #: WQ0031314 Field #: 9 Acres Utilized: 27
Roger Spillman Annual Dry Tons Applied:1005.86 Site #: DV8 Acres Permitted: 27
Roger Spillman Predominant Soil Series: MrB2 Cation Exchange Capacity (non 503):
221 Crop 2 Name: Rye Grass Crop 2 Max. PAN: 50
Crop 1 Name:
Sudex
Crop 1 Max.
PAN.
Volume applied
pP
Volume
Residual Sources
Soil
Cond.
Precip.
Y
<
o
��,
rate
PAN Applied
Name of
Receiving
Crop Type
Residual
o
(enter one) Solids)
a Applied per
/o pp P
DES #, W #,
(NP Q
(Dry,
Past 24
E. n-
F, �
TKNand
trite
lbslacre
( )
Application
PP
N
QLiquid
Solids Acre
Fert., Animal
Wet
s
p o
* N
Umg/kg
Cu. Yds Gallons
{Dry TonslAcj
Waste, etc)
Moist)inches
o'
mglkglkg5/22119
815
25.$ 6.567
Neilson WTP
Dry
<.5
S
0.5
0.149172.3
9.488 NA:
Sudex
5/23/19
564
25.8 4.539
Neilson WTP
Dry
<.5"
S
0.5
0.1
4917.5
369.9 52.3
6.291 NA
Sudex
9/19119
590
24 4.417
Neilson WTP
Dry
<.5"
S
0.5
0.1
1970
798.5 20.4
Na 4.742
Rye
9120/19
552
24 4.132
Neilson WTP
Dry
<.5"
S
0.5
0.1
1970
798.5 20.4
Na.... 4.436
Rye
4/23119
1955
24 14.635 -
Neilson WTP
Dry
<.5"
S
0.5
0.1
1970
798.5 20.4
Na 15.712
Rye
9/24/19
396
24 2.964
Neilson WTP
Dry
<.5"
S
0.5
0.1
1970
798.5 20.4
Na " 3:183
Rye
0.000 0.000
0.000.
0.000 0.000
0.000
0.000 0.000
0.000
0.000 : 0.000
0.000
0.000 0.000:
0.000
0.000 0.000
0.000
Residuals Applications
totals
on FORM
FSF
supp ( attach
FORM
FSF supp
to this form):
TOTALS:
4873 0
As
Cd Cu
Cr
Pb
H
Mo
Ni
Se
Zn P
15.369 28.073
Lime
A lied
Annuallbs/acre 0.513 0.022 3.215 3.430 2.031 0.007 0.069 1.582 0.154 9.128 182:616 Date I lbs
Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0
Current Cumulative lbs/ac 0.513 0.022 3.215 3.430 2.031 0.007 0.069 1.582 0.154 9.128
Permitted C. P. L. R.:'*** 36 34 1338 267 1 15 F 374 89 2498
Permit PAN Limit 1st12nd Crop 221 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
/j *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/13/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land Applier aerobically digested -0.3, raw sludge -0.4
""C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and
chain of custody's)
• Copies of our SAR/PAN calculations

Waypdint,a
ANALYTICAL.
5/7/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-116-0282
Client Project Description: Neilson WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointana[Ocal.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/26/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama 940750 Louisiana P04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA HTN00012
Texas NT104704180 Arkansas #88-0650
Oklahoma #9311 SC 484002
Kentucky UST #80215 PA DEP 468-03195
Page 1 of 13

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Neilson WTP
Lab Report Number: 19-116-0282
Date: 5/7/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalybcal.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L434240
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L434067
MS/MSD Recovery failed, DT confirmed matrix interference
Analyte: Iron
QC Batch No: L434240
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L434240
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: L434067
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was not within the method limits. Matrix interference is suspected.
Analyte: Manganese
QC Batch No: L434067
The matrix spike (MS) andlor the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was not within the method limits. Matrix interference is suspected.
Analyte: Molybdenum
QC Batch No: L434067
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L434067
Page 2 of 13

W poin
0
ay t
n
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypo€ntanalytical.com
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was not within the method limits. Matrix interference is suspected.
Analyte: Selenium
QC Batch No: L434067
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 3 of 13

ILG
Waypoinic-
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :19-116-0282
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax 901,213.2440
www.waypointanalyticaLcom
Project Neilson WTP
Information :
REPORT OFANAL YSIS
Report Date : 05/07/2019
Received, �: 04/26/2019
Qor, ''6 t�Q-Q.
Danyale Love
Project Manager
Lab No : 92234 Matrix: Solids
Sample ID : Neilson WTP *I Sampled: 4/25/2019 8.30
Test Results Units MDL MQL DF Date I Time By Analytical
Analyzed Method
% Moisture
78.4
°7a
0.010
1
04/26/19 16:25
ADM
SW-DRYWi
Ammonia Nitrogen
284
mg/Kg - dry
116
1
05/06/19 15:00
JP3
4500NH3C-2011
Nitrate+Nitrite-N
75.9
mg/Kg - dry
21.5
21.5
1
05/03/19 12:45
ZBD
4500NO3F-2011
Organic N
5050
mg/Kg - dry
323
1
05/06/19 15:00
CALCULATION
pH
7.1
s.u.
1
05/06/19 07:11
1SL
9045D
Total Solids
21.6
%
0.010
0.010
1
04/26/19 16:25
ADM
2540G-2011
Total Volatile Solids
25.1
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Kjeldahl Nitrogen
5320
mg/Kg - dry
323
1
05/07/19 14:22
CLP
4500NORGD-2011
Phosphorus
2990
mg/Kg - dry
11.9
23.1
1
05/01/19 22:34
BKN
6010D
Aluminum
117000
mg/Kg - dry
94.0
231
10
05/02/19 13:57
BKN
6010D
Arsenic
6.67
mg/Kg - dry
1.94
2.31
1
05/01/19 22:34
BKN
6010D
Cadmium
<0.229
mg/Kg - dry
0.229
0.463
1
05/01/19 22:34
BKN
6010D
Calcium
861
mg/Kg - dry
77.8
116
1
05/01/19 22:34
BKN
60101)
Chromium
35.0
mg/Kg - dry
0.879
1.16
1
05/01/19 22:34
BKN
6010D
Copper
34.6
mg/Kg - dry
0.671
1.16
1
05/01/19 22:34
BKN
6010D
Iron
3280D
mg/Kg - dry
19.6
23A
1
05/01/19 22:34
BKN
6010D
Lead
23.1
mg/Kg - dry
0.689
1.39
1
05/01/19 22:34
BKN
60101)
Magnesium
1500
mg/Kg - dry
10.3
23.1
1
05/01/19 22:34
BKN
6010D
Manganese
359
mg/Kg - dry
0.847
2.31
1
05/01/19 22:34
BKN
6010D
Mercury
0.0912
mg/Kg - dry
0,0150
0.0681
1
05/02/19 11:25
KKM
7471A
Molybdenum
0.7871
mg/Kg - dry
0.601
1.16
1
05/01/19 22:34
BKN
60101)
Nickel
16.2
mg/Kg - dry
0.763
1.16
1
05/01/19 22:34
BKN
6010D
Potassium
1440
mg/Kg - dry
13.8
23A
1
05/01/19 22:34
BKN
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 4 of 13

e
W pol
ay
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number: 19-116-0282-
Lab No : 92234
Sample ID : Neilson WTP #1
Test
Selenium
Sodium
Zinc
Sulfur
Sodium Absorption Ratio
2790 Whitten Road, Memphis, TN 38133
Main 9U1.213.2400 0 Fax 901.213,2440
www.waypointanalytical.com
Project Neilson WTP
Information :
REPORT OFANAL PSIS
Results Units MDR
Report Date : 05/07/2019
Received : 04/26/2019
10C 6&'Z� w-a
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/25/2019 8.30
MQL DF Date f Time By Analytical
Analyzed Method
<2.27 mg/Kg - dry 2.27 2.31 1 05/01/19 22:34 BKN 6010D
<357 mg/Kg - dry 357 1160 10 05/02/19 13:57 BKN 6010D
96.3 mg/Kg - dry 5.00 5.79 1 05/01/19 22:34 BKN 6010D
2780 mg/Kg - dry 22.6 23.1 1 05/01/19 22:34 BKN 6010D
<5.00 Ratio 5.00 1 05/01/19 22:34 CALCULATION
Dilution Factor
Qualifiers/ B Analyte detected in blank pF DF Method factortation Limit
Definitions I Estimated value
Page 5 of 13

2790 Whitten Road, Memphis, TN 38133
Waypoint
Main 901.213.2400 1 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Neilson WTP Report Date: 05/07/2019
755 Yadkinvi[le Rd Information : Received : 04/26/2019
Mocksville , NC 27028
Report Number: 19-116-0282 REPOR T OF A IVA L YSIS Danyale Love
Project Manager
Lab No : 92235 Matrix: Solids
Sample ID : Neilson WTP #2 Sampled: 4/25/2019 8:30
Test Results Units MDL MQL DF Date I Time By Analytical
Analyzed Method
Moisture
78.7
%
0.010
1
04/2611916:25
ADM
SW-DRYWT
Ammonia Nitrogen
445
mg/Kg - dry
117
1
05/06/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
54.0
mg/Kg - dry
22.9
22.9
1
05/03/19 12:45
ZBD
450ONO3F-2011
Organic N
5120
mg/Kg - dry
245
1
05/06/19 15:00
CALCULATION -
pH
6.6
S.U.
1
05/06/19 07:11
JSL
9045D
Total Solids
23.8
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Volatile Solids
24.9
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Kjeldahl Nitrogen
5540
mg/Kg - dry
245
1
05/07/19 14:23
CLP
4500NORGD-2011
Phosphorus
2590
mg/Kg - dry
12.1
23.5
1
05/01/19 22:39
BKN
6010D
Aluminum
140000
mg/Kg - dry
95.3
235
10
05/02/19 14:02
BKN
6010D
Arsenic
7.46
mg/Kg - dry
1.97
2.35
1
05/01/19 22:39
BKN
6010D
Cadmium
0.3713
mg/Kg - dry
0.232
0.469
1
05/01/19 22:39
BKN
6010D
Calcium
869
mg/Kg - dry
78.9
117
1
05/01/19 22:39
BKN
6010D
Chromium
60.6
mg/Kg - dry
0.892
1.17
1
05/01/19 22:39
BKN
6010D
Copper
50.7
mg/Kg - dry
0.681
1.17
1
05/01/19 22:39
BKN
6010D
Iron
60600
mg/Kg - dry
199
235
10
05/02/19 14:02
BKN
6010D
Lead
37.2
mg/Kg - dry
0.699
1.41
1
05/01/19 22:39
BKN
6010D
Magnesium
2330
mg/Kg - dry
10.4
23.5
1
05/01/19 22:39
BKN
6010D
Manganese
402
mg/Kg - dry
0.859
2.35
1
05/01/19 22:39
BKN
60101)
Mercury
0.0859
mg/Kg - dry
0.0160
0.0723
1
05/02/19 11:27
KKM
7471A
Molybdenum
1.27
mg/Kg - dry
0.610
1.17
1
05/01/19 22:39
BKN
6010D
Nickel
26.9
mg/Kg - dry
0.774
1.17
1
05/01/19 22:39
BKN
6010D
Potassium
2310
mg/Kg - dry
14.0
23.5
1
05/01/19 22:39
BKN
6010D
Qualifiers/ B
Anaiyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 6of13

-d-O
Waypoeinc.
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :19-116-0282
Lab No : 92235
Sample ID : Neilson WTP #2
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.21.3.2400 0 Fax [phone]
www.waypointanalytical.com
Project Neilson WTP
Information :
REPORT OFANAL VS.I'S
Results Units MDL
Report Date ; 05/07/2019
Received : 04/26/2019
Danyale Love
Project Manager
Matrlx; Solids
Sampled: 4/25/2019 8:30
MQL DF Date 1 Time By Analytical
Analyzed Method
Selenium <2.30 mg/Kg - dry 2.30 2.35 1 05/01/19 22:39 BKN 6010D
Sodium <362 mg/Kg - dry 362 1170 10 05/02/19 14:02 BKN 6010D
Zinc 144 mg/Kg - dry 5.07 5.87 1 05/01/19 22:39 BKN 6010D
Sulfur 3030 mg/Kg - dry 23.0 23.5 1 05/01/19 22:39 BKN 6010D
Sodium Absorption Ratio <5.00 Ratio 5.00 1 05/01/19 22:39 CALCULATION
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions 3 Estimated value MQL Method Quantitation Limit
Page 7 of 13

.d.- a 2740 Whitten Road, Memphis, TN 38133
Wayposim-Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
FMA Resources Inc
Brent Collins Project Neilson WTP Report Date : 05/07/2019
755 Yadkinville Rd Information : Received : 04/26/2019
Mocksville , NC 27028 0 ' n _ n
Report Number :19-116-0282
REPORT OFANALYSIS
Danyale Love
Project Manager
Lab No : 92236 Matrix: Solids
Sample ID : Neilson WTP #3 Sampled: 4/25/2019 8.30
Test
Results Units MbL MQL DF Date 1 Time By Analytical
Analyzed Method
% Moisture
70.4
%
0.010
1
04/26/19 16:25
ADM
SW-DRYWT
Ammonia Nitrogen
356
mg/Kg - dry
84.5
1
05/06/19 15:00
3P3
4500NH3C-2011
Nitrate+ N itrite-N
47.3
mg/Kg - dry
15.7
15.7
1
05/03/19 12:46
ZBD
4500NO3F-2011
Organic N
3990
mg/Kg - dry
281
1
05/06/19 15:00
CALCULATION
pH
6.4
S.U.
1
05/06/19 07:11
3SL
9045D
'total Solids
29.6
%
0.010
0.010
1
04/26/19 16:25
ADM
2540G-2011
Total Volatile Solids
22.5
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Kjeldahl Nitrogen
4360
mg/Kg - dry
281
1
05/07/19 14:24
CLP 4500NORGD-2011
Phosphorus
2070
mg/Kg - dry
8.68
16.9
1
05/01/19 22:44
BKN
6010D
Aluminum
116000
mg/Kg - dry
68.6
169
10
05/02/19 14:07
BKN
6010D
Arsenic
7.26
mg/Kg - dry
1.42
1.69
1
05/01/19 22:44
BKN
60100
Cadmium
0.378
mg/Kg - dry
0.167
0.338
1
05/01/19 22:44
BKN
6010D
Calcium
652
mg/Kg - dry
56.8
84.5
1
0S/01/19 22:44
BKN
6010D
Chromium
44.3
mg/Kg ` dry
0.641
0.844
1
05/01/19 22:44
BKN
6010D
Copper
37.8
mg/Kg - dry
0.490
0.845
1
05/01/19 22:44
BKN
6010D
Iron
49300
mg/Kg - dry
143
169
10
05/02/19 14:07
BKN
6010D
Lead
28.7
mg/Kg - dry
0.503
1.01
1
05/01/19 22:44
BKN
6010D
Magnesium
2040
mg/Kg - dry
7.50
16.9
1
05/01/19 22:44
BKN
6010D
Manganese
588
mg/Kg - dry
0.618
1.69
1
05/01/19 22:44
BKN
6010D
Mercury
0.0912
mg/Kg - dry
0.0114
0.0514
1
05/02/19 11:28
KKM
7471A
Molybdenum
1.05
mg/Kg - dry
0.439
0.844
1
05/01/19 22:44
BKN
60101)
Nickel
19.7
mg/Kg - dry
0.557
0.844
1
05/01/19 22A4
BKN
6010D
Potassium
1950
mg/Kg - dry
10.1
16.9
1
05/01/19 22:44
BKN
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution
Factor
Definitions 3
Estimated value
MQL
Method
Quantitation Limit
Page 8 of 13

e
K
W poini -
ay
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksvilie , NC 2702B
Report Number:19-116-0282
Lab No : 92236
Sample ID : Neilson WTP #3
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 a Fax [phone]
www.waypointanalytical.com
Project Neilson WTP
Information
REPORT OPANAL YSIS
Results Units MDL
Report Date ; 05/07/2019
Received ; 04/26/2019
Danyale Love
Project Manager
Matrix; Solids
Sampled: 4/25/201.9 8:30
MQL DF Date I Time By Analytical
Analyzed Method
<1.66
mg/Kg - dry
1.66
1.69
1
05/01/19 22:44
BKN
6010D
Selenium
<261
mg/Kg - dry
261
B45
10
05/02/19 14:07
BKN
6010D
Sodium
106
mg/Kg - dry
3.65
4.22
1
05/01/19 22:44
BKN
6010D
Zinc
2470
mg/Kg - dry
16.5
16.9
1
05/01/19 22:44
BKN
6010D
Sulfur
Ratio
5.00
1
05/01/19 22:44
CALCULATION
Sodium Absorption Ratio
<5.00
Qualil•iers/ B Analyte detected in blank DF Dilution Factor
Definitions i Estimated value MQL Method Quantitation Limit
page 9 of 13

2790 Whitten Road, Memphis, TN 38133
Waypoint.
Main 901.213.2400 ° Pax 901.213.2440
ANALYTICAL www,waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Neilson WTP Report Date : 05/07/2019
755 Yadkinville Rd Information : Received : 04/26/2019
Mocksville , NC 27028
Report Number : 19-116-0282 REPORTOFANALKSIS Danyale Love
Project Manager
Lab No : 92237
Matrix: Solids
Sample ID: Neilson WTiP #4
Sampled:
4/25/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date/Time
By
Analytical
Analyzed
Method
% Moisture
71.7
%
0,010
1
04/26/19 16:25
ADM
SW-DRYWT
Ammonia Nitrogen
392
mg/Kg - dry
88.3
1
05/06/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
32.0
mg/Kg - dry
17.7
17.7
1
05/03/19 12:47
2BD
4500NO3F-2011
Organic N
4060
mg/Kg - dry
248
1
05/06/19 15:00
CALCULATION
pH
5.9
s.u,
1
05/06/19 07:11
J5L
9045D
Total Solids
28,3
11/0
0,010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Volatile Solids
23.3
%
0.010
0,010
1
04/26/19 16:25
ADM
2540G-2011
Total Kjeldahl Nitrogen
4450
mg/Kg - dry
248
1
05/07/19 14:25
CLP 4500NORGD-2011
Phosphorus
2210
mg/Kg - dry
9.08
17.7
1
05/01/19 22:50
BKN
6010D
Aluminum
118000
mg/Kg - dry
71.7
177
10
05/02/19 14:12
BKN
6010D
Arsenic
7.81
mg/Kg - dry
1.48
1.77
1
05/01/19 22:50
BKN
6010D
Cadmium
0,382
mg/Kg - dry
0,175
0,353
1
05/01/19 22:50
BKN
6010D
Calcium
809
mg/Kg - dry
59,4
88.3
1
05/01/19 22:50
BKN
6010D
Chromium
43.5
mg/Kg - dry
0,671
0,883
1
05/01/19 22:50
BKN
6010D
Copper
37.8
mg/Kg - dry
0,512
0.883
1
05/01/19 22:50
BKN
6010D
Iron
47700
mg/Kg - dry
150
177
10
05/02/19 14:12
BKN
6010D
Lead
29.1
mg/Kg - dry
0,526
1.06
1
05/01/19 22:50
BKN
6010D
Magnesium
1880
mg/Kg - dry
7.84
17,7
1
05/01/19 22:50
BKN
6010D
Manganese
537
mg/Kg - dry
0.646
1,77
1
05/01/19 22:50
BKN
6010D
Mercury
0.0746
mg/Kg - dry
0,0123
0,0555
1
05/02/19 11:29
KKM
7471A
Molybdenum
0.985
mg/Kg - dry
0.459
0.883
1
05/01/19 22:50
BKN
6010D
Nickel
19.5
mg/Kg - dry
0,583
0,883
1
05/01/19 22:50
BKN
6010D
Potassium
1780
mg/Kg - dry
1015
17,7
1
05/01/19 22:50
BKN
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 10 of 13

Waypoint-
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksviile , NC 27028
Report Number :19-116-0282
Lab No : 92237
Sample ID : Neilson WTP #4
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213,2440
www.waypointanalytical.com
Project Neilson WTP
Information :
REPORT OFANALYSIS
Results Units MDL
Report Date : 05/07/2019
Received : 04/Z6/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/25/2019 8:30
MOL DF Date I Time By Analytical
Analyzed Method
Selenium <1.73 mg/Kg - dry 1.73 1.77 1 05/01/19 22:50 BKN 6010D
Sodium <273 mg/Kg - dry 273 883 10 05/02/19 14:12 BKN 6010D
Zinc 3.08 mg/Kg - dry 3.82 4.42 1 05/01/19 22:50 BKN 6010D
Sulfur 2590 mg/Kg - dry 17.3 17.7 1 05/01/19 22:50 BKN 6010D
Sodium Absorption Ratio <5.00 Ratio 5.00 1 05/01/19 22:50 CALCULATION
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions
Page 11 of 13

Waypoint2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-116-0282
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 40 Courier
0 Other:
Thermometer ID;
1#45
Shipping container/cooler uncompromised?
4D Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
is Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
40 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
40 Yes
0 No
Sufficient sample volume for indicated test(s)?
4D Yes
0 No
All samples received within holding time?
9 Yes
0 No
Cooler temperature in compliance?
19 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
® NIA
Soil VOA method 5035 -- compliance criteria met
0 Yes
0 No
0 NIA
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments:
Signature: ory Phillips Date & Time: 4/26/2019 13:35:27
Page 12of13

a
w
CtientName/Address
Client Project Manager/Contact
Wiling Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
MI
19-11 "282
Project Description
Project/Site Location (City/State)
RUSH —Additional charges apply
�262019
DateSpecial
Date Results Needed
Results Needed
EIu1A Resources Inc
I —Oil
13:32:42
Pu.
Neilson WTP
Project Number
Pro]eCt Manager Phone #
Pra]ect Manager Email
336-399-3646
[e-mail]
to
z
in
A COOP a 10C NaM203 (?'/Hero Only)
e Coal <= GC
aypoint
O
C
C H2504PH42
ANALYTICAL,°.
ro
a
o
a
E
E
M
oEl
0
[%)
P None Required
E N20H pHa10
2790 Whiticn Road
Unless noted, all containers
m
u
u7
M
Q
U
F HNO3;;W2
G HCL pHe2
Memphis, TN 38133
V
a`
(9til) 213-2900
per Table Il of 40 CFR Part
m
N
�
ce"
Z
r
H Coo6C NAZs203
136.
�
z
io
i
v
Date
Time
Sample Identification
Required
Analysis / Preservative
Comments/Notes
��s
B'31°"
N ea,..
wnp 44 1
I
C
Meta1s:A1,As,Ca,Cd,Cr,CU,Fe,Pb
Z
C
'}C
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
For Laboratory Use Only
Sampl by
x oY
(Na a —Print)
-� �'�
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Lab Comments
CN
R s
d TU EJ
Date
Time
Received
by: (SIGNATURE)
Date rime
Y[H l
Blank% polerTe
Rel nci (shed by: (5IGNATURE) Date Time
Received
: (51 NATURE)
Date Time
Relinquished by: (SIGNATURE)
Date
Time
Rece
: (SIG LIRE)
oat Time
0

W u 0 a
a.rpoint,
ANALYTICAL
9/24/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-255-0023
Client Project Description: Winston- Salem, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 9/12/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis 1.n question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015 VA NELAP #460181 Texas #T104704180 Arkansas #88-0650
Mississippi California #2904 NC #415 Oklahoma #9311 SC #84002
Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST 490215 PA DEP #69-03195
�.cc..5
Page 1 of 13

Waypoint,e
ANALYTICAL
Client: EMA Resources lnc
Project: Winston- Salem, NO
Lab Report Number: 19-255-0023
Date: 9/24/2019
2790 Whitten Road, Memphis, TN 38133
main 901.713.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 92694 (Neilson WTP #1)
Analyte: Aluminum
QC Batch No: 1-454349/1-453670
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: 1-454349/1-453670
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: 1-454188/1-453670
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92696 (Neilson WTP #3)
Analyte: Aluminum
QC Batch No: L454323IL453733
The matrix spike and/or the matrix spike duplicate was outside qualify control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L4543231L453733
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: 1-454323/1-453733
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: 1-45410111-453733
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L4541011L453733
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Page 2 of 13

Waypoeint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Analyte: Sulfur
QC Batch No: L454101/L453733
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 92697 (Neilson WTP #4)
Analyte: Aluminum
QC Batch No: 1-454323/1-453811
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Iron
QC Batch No: L454323/1-453811
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Potassium
QC Batch No: L454323/1-453811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: 1-454137/1-453811
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Analyte: Mercury
QC Batch No: L454339/L454229
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 13

e
Waypoint,
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-255-0023
Lab No : 92694
Sample ID : Neilson WTP #1
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.213,2400 0 Fax [phone]
www.waypointanalytical.com
Project Winston- Salem, NC
Information :
REPORT OFANALYSIS
Report Date : 09/24/2019
Received : 09/12/2019
0C"'6&:� 0�-a
Danyale Love
Project Manager
Matrix; Solids
Sampled: 9/11/2019 9:00
Results Units MDL MQL DF Date I Time By Analytical
Analyzed Method
% Moisture
Ammonia Nitrogen
Nitrate+ Nitrite-N
Organic N
pH
Total Solids
Total Kjeldahl Nitrogen
Phosphorus
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Potassium
Selenium
76.6
1290
<21.4
2680
6=1
23.4
3970
2300
104000
8.25
<0.212
974
44.0
45.3
45300
24.9
2260
551
0.0739
1.50
22.0
1920
<2,09
%
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
SM.
%
mg/Kg - dry
mg1Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg-dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
m91Kg - dry
21.4
0.010
11.0
86.8
1.79
0.212
71.8
0.811
0.620
181
0.636
9.49
0.782
0.0150
0.555
0.705
12.7
2.09
0.010
107
21.4
214
0.010
214
21.4
214
2.14
0.427
107
1.07
1.07
214
1.28
21.4
2.14
0.0679
1.07
1.07
21.4
2.14
1
1
1
1
1
1
1
1
10
1
1
1
1
1
10
1
1
1
1
1
1
1
1
09/16/19 16:43
09/23/19 15:00
09/23/19 14:16
09/23/19 15:00
09/23/19 07:03
09/16/19 16:43
09/24/19 14:40
09/13/19 22:08
09/17/19 14:20
09/13/19 22:08
09/13/19 22:08
09/13/19 22:08
09/13/19 22:08
09/13/19 22:08
09/17/1914:20
09/13/19 22:08
09/13/19 22:08
09/13/19 22:08
09/17/19 14:07
09/13/19 22:08
09/13/19 22:08
09/13/19 22:08
09/13/19 22:08
ADM SW-DRYWT
IPJ 4500NH3C-2011
ZBD 4500NO3F-2011
CALCULATION -
JSL 9045D
ADM 2540G-2011
CLP 4500NORGD-2011
JTR 6010D
BKN 6010D
JTR 6010D
3TR 6010D
JTR 6010D
JTR 6010D
JTR 6010D
BKN 6010D
JTR 6010D
3TR 6010D
)TR 6010D
TJS 7471A
JTR 6010D
JTR 6010D
JTR 6010D
JTR 6010D
Dilution Factor
Limit Exceeded
J
MQL
Estimated value
Method Quantitation Limit
Qualifiers/ DF
Definitions L
Page 4 of 13

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number: 19-255-0023
Lab No : 92694
Sample ID : Neilson WTP #1
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213,2440
www.waypointanalytical.com
Project Winston- Salem, NC
Information :
REPORT OFANALYSIS
Report Date : 09/24/2019
Received : 09/12/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 9:00
Test
Results
Units
MDL
MQL
DF
Date I Time
Analyzed
By
Analytical
Method
Sodium
79.51
mg/Kg - dry
33.0
107
1
09/13/19 22:08
JTR
6010D
Zinc
123
mg/Kg - dry
4.62
5.34
1
09/13/19 22:08
JTR
6010D
Sulfur
2220
mg/Kg - dry
20.9
21.4
1
09/13/19 22:08
JTR
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
09/13/19 22:08
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
Estimated value
MQL Method Quantitation Limit
Page S of 13

2790 Whitten Road, Memphis, TN 38133
Waypoint, Main 901.213.7400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr, Brent Collins Project Winston- Salem, NC Report Date : 09/
755 Yadkinville Rd Information : Received: D9/12/2019
/2019
Mocksville , NC 27028�
Report Number :19-255-0023
Lab No: 92695
Sample ID: Neilson WTP #2
Test
REPORT OPANAL PSIS
Danyale Love
Project Manager
Matrix; Solids
Sampled: 9/11/2019 9:15
Results units MDL MQL DF Date ITime By Analytical
Analyzed Method
% Moisture
Ammonia Nitrogen
Nitrate+Nitrite-N
76.8
741
<21,6
%
mg/Kg - dry
mg/Kg - dry
21.6
0.010
108
21.6
1 09/16/19 16:59
1 09/23/19 15:00
1 09/23/19 14:17
ADM
JPJ
ZBD
SW-DRYWT
4500NH3C-2011
4500NO3F-2011
Organic N
pH
Total Solids
Total Kjeldahl Nitrogen
Phosphorus
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nickel
Potassium
Selenium
845
5.9
23.2
1590
2470
109000
6.51
0.3443
1030
49.1
46.6
50000
28.0
2450
582
0.0780
0.7711
22.1
2130
<111
mg/Kg - dry
S.U.
%
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
0.010
11A
43.5
1.81
0,213
72.4
0,818
0,625
91.4
0.642
9.57
0.788
0.0140
0,560
0,711
64.2
2.11
216
0.010
216
21.6
108
2.16
0.431
108
1.08
1.08
108
1.29
21.6
2.16
0.0634
1.08
1.08
108
2.16
1 09/23/19 15:00
1 09/23/19 07:03
1 09/16/19 16:59
1 09/24/19 14:41
1 09/13/19 18:55
5 09/16/19 19:02
1 09/13/19 18:55
1 09/13/19 18:55
1 09/13/19 18:55
1 09/13/19 18:55
1 09/13/19 18:55
5 09/16/19 19:02
1 09/13/19 18:55
1 09/13/19 18:55
1 09/13/19 18:55
1 09/17/19 14:18
1 09/13/19 18:55
1 09/13/19 18:55
5 09/16/19 19:02
1 09/13/19 18:55
CALCULATION -
JSL 90450
ADM 2540G-2011
CLP 4500NORGD-2011
JTR 6010D
BKN 6010D
JTR 6010D
JTR 6010D
JTR 6010D
JTR 6010D
JTR 6010❑
BKN 6010D
JTR 6010D
JTR 6010D
JTR 6010D
TJS 7471A
JTR 6010D
JTR 6010D
BKN 6010D
JTR 6010D
Dilution Factor
Limit Exceeded
J
MQL
Estimated value
Method Quantitation Limit
Qualifiers/ DF
Definitions L
Page 6 of 13

edd
ANALYTICAL
Waypoint,
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901,213.2440
www.waypointanaiytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Winston- Salem, NC Report Date : 09/24/2019
755 Yadlunville Rd information : Received : 09/12/2019
Mocksville , NC 27028
Report Number :19-255-0023 REPDRrOFANALYSIS Danyale Love
Project Manager
Lab No ; 92695 Matrix; Solids
Sample ID: Neilson WTP #2 Sampled: 9/11/2019 9:15
Test
Results
Units
MDL
MQL
DF Date 1 Time
Analyzed
By
Analytical
]Method
Sodium
1023
mg/Kg - dry
33.3
108
1 09/13/19 18:55
JTR
6010D
Zinc
130
mg/Kg - dry
4.66
5.39
1 09/13/19 18:55
JTR
6010D
Sulfur
2420
mg/Kg - dry
21.1
21.6
1 09/13/19 18:55
JTR
6010D
Sodium Absorption Ratio
¢5,00
Ratio
5.00
1 09/13/19 18:55
CALCULA'HON
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 7 of 13

0
2790 Whitten Road, Memphis, TN 38133
Wayp 0'1* t - Main 901.213.7400 0' Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Report Date : 09/24/2019
Mr. Brent Collins Project Winston- Salem, NC
Information : Received: 09/12/2019
755 Yadkinville Rd
Mocksville. NC27028
Report Number :l9-255-0023
Lab No : 92696
Sample ID: Neilson WTP #3
Test
REPORT OFANAL YSIS
Results Units MDL
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 9:30
MQL DF Date I Time By Analytical
Analyzed Method
71.6
%
0.010
1 09/16/19 16:59
ADM
SW-DRYWT
% Moisture
mg/Kg - dry
88.0
1 09/23/19 15:00
JPJ
4500NH3C-2011
Ammonia Nitrogen
683
mg/Kg - dry
17.6
17.6
1 09/23/19 14:18
ZBD
4500NO3F-2011
Nitrate+Nitrite-N
<17.6
489
mg/Kg - dry
176
1 09/23/19 15:00
CALCULATION -
Organic N
1 09/23/19 07:03
JSL
90450
pH H
5.6
S.U.
28.4
%
0.010
0.010
1 09/16/19 16:59
ADM
254OG-2011
Total Solids
1170
mg/Kg " dry
176
1 09/24/19 14:42
CLP 4500NORGD-2011
Total Kjeldahl Nitrogen
2510
mg/Kg - dry
9.05
17.6
1 09/13/19 19:01
JTR
6010D
Phosphorus
102000
mg/Kg - dry
35.6
88.0
5 09/16/19 19:07
BKN
6010D
Aluminum
5.39
mg/Kg - dry
1.48
1.76
1 09/13/19 19:01
JTR
6010D
Arsenic
0.359
mg/Kg - dry
0.174
0.352
1 09/13/19 19:01
JTR
6010D
Cadmium
838
mg/Kg - dry
59.2
88.0
1 09/13/19 19:01
JTR
6010D
Calcium
43.0
mg/Kg - dry
0,669
0.880
1 09/13/19 19:01
JTR
6010D
Chromium
40,8
mg/Kg - dry
0.511
0.880
1 09/13/19 19:01
JTR
6010D
Copper
44000
mg/Kg - dry
74.6
88.0
5 09/16/19 19:07
BKN
6010D
Iron
25.3
mg/Kg - dry
0.524
1.06
1 09/13/19 19:01
JTR
6010D
Lead
2140
mg/Kg - dry
7.82
17.6
1 09/13/19 19:01
JTR
6010D
Magnesium
521
mg/Kg - dry
0.644
1.76
1 09/13/19 19:01
JTR
6010D
Manganese
0.0856
mg/Kg - dry
0.0119
0.0539
1 09/17/19 14:22
TJ5
7471A
Mercury
0.6021
mg/Kg - dry
0.457
0.880
1 09/13/19 19:01
JTR
6010D
Molybdenum
19.4
mg/Kg - dry
0.580
0.880
1 09/13/19 19:01
JTR
6010D
Nickel
1880
mg/Kg - dry
52.5
88.0
5 09/16/€9 19:07
BKN
6010D
Potassium
<1.73
mg/Kg - dry
1.73
1.76
1 09/13/19 19:01
JTR
60101)
Selenium
J
Estimated value
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation
Limit
Definitions L
Limit Exceeded
Page 8 of 13

.90
waypoeint,
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :19-255-0023
Lab No : 92696
Sample ID: Neilson WTP #3
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Winston- Salem, NC
Information :
REPORT OFANAL YSIS
Report Date : 09/24/2019
Received : 09/12/2019
Q(�''6&� 0-�
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 9:30
Test
Results
Units
MDL
MQL
DF Date I Time
Analyzed
By
Analytical
Method
Sodium
60.93
mg/Kg - dry
27.2
89.0
1 09/13/19 19:01
JTR
6010D
Zinc
115
mg/Kg - dry
3.80
4.40
1 09/13/19 19:01
JTR
6010D
Sulfur
2450
mg/Kg - dry
17.2
17.6
1 09/13/19 19:01
JTR
6010D
Sodium Absorption Ratio
<5,00
Ratio
5.00
1 09/13/19 19:01
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
I Estimated value
MQL Method Quantitation Limit
Page 9 of 13

2790 Whitten Road, Memphis, TN 38133
waypoint.Main 901.213.2400 ° Fdx 901.213.2440
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Winston- Salem, NC Report Date : 09/24/2019
755 Yadkinville Rd Information : Received: 09/12/2019
Macksviile , NC 27028�-
Danyale Love
Report Number :19-255-0023 REPORrOFANAL rSIS Project Manager
Lab No: 92697 Matrix: Solids
Sample ID : Neilson WTP #4 Sampled: 9/11/2019 9:45
Test Results Units MDL MQL DF Date I Time By Analytical
Analyzed Method
% Moisture
79.2
%
0.010
1
09/26/19 16:59
ADM
SW-DRYWT
Ammonia Nitrogen
48D
mg/Kg - dry
120
1
09/23/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<21.1
mg/Kg - dry
21.1
21.1
1
09/23/19 14:18
ZBD
4500NO3F-2011
Organic N
673
mg/Kg - dry
240
1
09/23/19 15:00
CALCULATION -
pH
6.2
S.U.
1
09/23/19 07:03
JSL
9045D
Total Solids
20.8
%
0.010
0.010
1
09/16/19 16:59
ADM
254OG-2011
Total Kjeldahl Nitrogen
1150
mg/Kg - dry
240
1
09/24/19 14:43
CLP
4500NORGD-2011
Phosphorus
2500
mg/Kg - dry
12.4
24.0
1
09/13/19 17:35
JTR
6010D
Aluminum
112000
mg/Kg - dry
97.6
240
10
09/16/19 18:13
BKN
6010D
Arsenic
6.54
mg/Kg - dry
2.01
2.40
1
09/13/19 17:35
JTR
6010D
Cadmium
0.3533
mg/Kg - dry
0.238
0.481
1
09/13/ 19 17:35
JTR
6010D
Calcium
1080
mg/Kg - dry
80.8
120
1
09/13/19 17:35
JTR
6010D
Chromium
48.1
mg/Kg - dry
0.913
1.20
1
09/13/19 17:35
JTR
6010D
Copper
44.9
mg/Kg - dry
0.697
1.20
1
09/13/19 17:35
JTR
6010D
Iron
4860D
mg/Kg - dry
204
240
10
09/16/19 18:13
BKN
6010D
Lead
27.1
mg/Kg - dry
0.716
1.44
1
09/13/19 17:35
-JTR
6010D
Magnesium
244D
mg/Kg - dry
10.7
24.0
1
09/13/19 17:35
JTR
6010D
Manganese
625
mg/Kg - dry
0.879
2.40
1
09/13/19 17:35
JTR
6010D
Mercury
0.0846
mg/Kg - dry
0.0151
0,0688
1
09/17/19 14:23
TJS
7471A
Molybdenum
<0.625
mg/Kg - dry
0.625
1.20
1
09/13/19 17:35
JTR
6010D
Nickel
22.5
mg/Kg - dry
0.793
1.20
1
09/13/19 17:35
JTR
6010D
Potassium
2150
mg/Kg - dry
143
240
10
09/16/19 18:13
BKN
6010D
Selenium
<2.36
mg/Kg - dry
2.36
2.40
1
09/13/19 17:35
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 10 of 13

14-0
Waypoinic,
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :19-255-0023
Lab No : 92697
Sample ID : Neilson WTP #4
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Project Winston- Salem, NC
Information :
REPORT OFANALYSIS
Report Date ; 09/24/2019
Received : 09/12/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 9.45
Test
Results
Units
MDL
MQL
DF
Date 1 Time
Analyzed
By
Analytical
Method
Sodium
1017
mg/Kg - dry
37.1
120
1
09/13/19 17:35
JTR
6010D
Zinc
137
mg/Kg - dry
5.19
6.01
1
09/13/19 17:35
JTR
60101)
Sulfur
2450
mg/Kg - dry
23.5
24.0
1
09/13/19 17:35
JTR
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
09/13/19 17:35
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 11 of 13

aftto
Poll I
Way *
ANALYTICAL
Customer Number: 46245
Customer Name: EMA Resources !nc
Report Number: 19-255-0023
Fed Ex 0 US Postal
0 UPS 0 Client
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Shipping Method
0 Lab 0 Other:
i) Courier Thermometer IQ:
Shipping container/cooler uncompromised? 0 Yes
Number of coolers received
0 No
Custody seals intact on shipping container/cooler? 0 Yes 0 No
Custody seals intact on sample bottles? 0 Yes 0 No
45
Not Required
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
® Yes
0 No
Samples in proper containers?
® Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
® Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
® Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved
0 Yes
0 No ®NIA
Water -VOA vials free of headspace
0 Yes
0 No � NIA
Trip Blanks received with VOAs
0 Yes
0 Na 0 NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No NIA
High concentration container (48 hr)
[_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Arleen Qualls Date &Time: 9/12/2019 08:36:46
Page 12 of 13

Client Name/Address
client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location {City/State)
RUSH — Additional charges apply
Met of Shipment
Matrix Key
f
C.e a -A
Special Detection Limit(s}
Date ResultNeeded
Fed Fae HsUPS �U5P5
Courier Client Drop Off
WW —Wastewater GW—tiraundwaEer
OW— Drinking water S —Soil /Solld o—oil
jVp.'I
i�
( j + ►J
�
Other
P - Product M - Mi=
Project Number
Project Manager Phone p
Project Manager Email
Purchase Order Number
Site/Facility ID p
336-399_3646
[e-mail]
z
fi
'ice
A Coal < 10C NaMO3 IMlvo Only)
y
rs�
;:
O
V
a Coco < 6c
aypoi ■ Y _
ANALYTICALo
c
e
c}i
m
°
-
d
E
a
C
rn
d
(/}
c HtSO4 pH42
0 None Required
E NaOH
279l1 Whitten Road
'�
�°.�
o
Vl
Q
pH>30
F HNO3 pH<2
Memphis, TN 38133
Unless noted, all containers
c
a
`o
Lb
1,
✓
G HCL pH<2
(yul) 219 2400
per Table II of 40 CFR Part
a
p
dJ
LO
(�
H 14004 pHc2
135.
E
a
z
q
�
Z
1�
V
1 Cool — SC NA2S203
Date
Time
Sample Identification
R
uired nalysis / servative
Comments/Notes
Ef,
c o
E,f/�'J- r
[�
Meials:Al,As,Ca,Cd,Cr,Gu,Fe,Pb
G�Sa --(-00
j
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
:.
A%z1= O J Lxll
1
scr-
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C,
IlilEt�If1���141��1�11��lllfd�lll��llal���l����111� �� 093
EMA Resources Inc 08.35A8
Winston- Salem. NC
for Laboratory Use only
Sampled by (Name — Print)
` r—rk J)
/
Client Remarks/Comments
Sludge Samples - Report Dry Weight
lee
Custody
SealY
Lab Comments
N
Relln she b ( I A RE)
Ole Time
Received by: (SIGNATURE)
pate Time
f "7 •
xi
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Rellnqulshed by: (SIGNATURE}
at Time
Received by: (SIGNATURE)
Pate Time
S�BRIa-fn�k/%%
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Rel[nquished by: (SIGNATURE)
Date Time
Aere
b .: {SlGNA7U
Date Time

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.� uz- - F f

Section 4
• Maps of the residuals disposal sites

OWNER: Gregory Dooley
692 Godbey Road
Mocksville, NC 27028
Phone: (M) 336-671-7197
OPERATOR: Same
Site 1!D
DV� 1
DV-11
Meld
01
02
Crop
Fescue Ha
Fescue Pasture
TOTALS-
Total
Acres
12.9
14.8
27.7
Net
Aeres
9.7
10.4
20.1
Predominant
Soil Series
Clifford
Fairview
Dapping
CfB2
FeC2

OWNER: Roger Spillman
P.O. Box 738
Cooieemee, NC 27014
Phone: (M) 336-918-8000
(0) 336-284-2551
OPERATOR: Same
Total
Net
Predominant
Mapping
Site ITS
Field
Crop
Acres
Acres
Soil Series
Unit
Bem uda
24.6
18.0
Cecil
CeB2
NC-DV-08
04
05
06
07
Pasture
Row Crop_20.3
Row Cro
Orchard Grass
21.7
68.7
18,0
20.0
44.5
Mecklenburg
Mecklenbur
Mecklenburg
MrC2
MrC2
MrC2
ITC-DV-08
NC-DV-08
NC-DV-08
Ha
Orchard Grass
29.8
18,2
Mecklenburg
MrC2
NC-DV-08
08
Ha
TOTALS=
165.1
118.7

xmap4i) B
u
�64IT =
3'A�"
�v�
ti tiF E
<
p?
V::
Aulurnn Cara N M6 .
' rme:�_Q�
s
ct
'Y
[ re ek
RED PA K_TRL
E�nger Spillman
f�
,'s
`'
�"�..
i
� CRE!?�-fIYRTLE LNf
4 --
.✓ %' �
I , _
AY 4
>' 1.✓� O X ! Y~MaNRa i q DUG I =
E CHINASERRY CC -?z y
To c'iJr1 i [Egg c�: �2 F -
g.
IL
jj 4'j !b
I3 ti
f s q,
�RcO° Roger 5p111me
LznS$rG� 60t ``
t I}AISY LN
RP
CLQf3FE1.`CER f�i x n
ofo-
NA Gy 4S7ER Lpnp 4, 4�
CAaLE LN w
U .r Qom,
,vt
} VICINITY MAP
ROGER SPILLMAN
SITE: NC DV-08
FIELDS: 04,05,06,07 & 08
BIC
Scale 1:25,000
,ft
�, 0 $DO '16(l0 Z40{7 3200 4000
ft Data Zoom 13-0
YN
raw se.�+rn

I =&
AdIMff=giz= Stream
4v�= lm= gain
�-Resources, Inc.
V71IApplicationArea OnSiteWell
OnSiteHouse ram-+ MiteWell
SurfaceWater OffSiteHouse(SllifAA) C) SoilDescrlption
x T x _ Fence OffSiteHouse Unsuitable
PropertyLine Outbuilding
Phone 336.751* 1441— Fax 336e751®1442
755 Yad cinville Road — Mocksville, NC 27028

Rukj L l � .. ..-..... Ttr
SITE: NC-DV-08
FIELDS. 07 & 08

ROGER SPILLMAN
SITE: NC-DV-08
'FIELDS: 05 & 06

RbGER SPILLMAN
SITE: NC-DV-GS Fm
FIELDS: 04

Gabriel Sparks
From: Roy Whitaker <[e-mail]>
Sent: Monday, January 27, 2020 2:24 PM
To: Gabriel Sparks
Cc: [e-mail]
Subject: [EXTERNAL] FW: Site Maps
Attachments: Roger Spillman.pdf, Spillman Field 9.pdf
CAUTION: This email originated from outside of the organization. Do not click links or open attachments
unless you recognize the sender and know the content is safe.
Gabe:
You will find attached the maps for 2019 operations.
Two of the fields were used during both operations. Field# 9 was applied in the second lagoon event.
Field#9 is located on the same Spillman Farm, just on the other side of the railroad tracks.
If you have any questions, you can reach me on the mobile number listed below.
Roy
Roy L. Whitaker
Director Business Development/Operations
EMA Resources, Inc.
755 Yadkinville Road
Mocksville, NC 27028
Office: 336-751-1441
Mobile: [phone]
From: Roy Whitaker <[e-mail]>
Sent: Friday, February 15, 2019 9:22 AM
To:'Gabriel Sparks' <[e-mail]>; Bill Brewer ([e-mail]) <[e-mail]>
Subject: Site Maps
Roy L. Whitaker
Director Business Development/Operations
EMA Resources, Inc.
755 Yadkinville Road
Mocksville, NC 27028
Office: 336-751-1441
Mobile: [phone]

Gabriel Sparks
From: Roy Whitaker <[e-mail]>
Sent: Monday, January 27, 2020 2:24 PM
To: Gabriel Sparks
Cc: [e-mail]
Subject: [EXTERNAL] FW: Site Maps
Attachments: Roger Spillman.pdf; Spillman Field 9.pdf
CAUTION: This email originated from outside of the organization. Do not click links or open attachments
unless you recognize the sender and know the content is safe,
Gabe:
You will find attached the maps for 2019 operations.
Two of the fields were used during both operations. Field# 9 was applied in the second lagoon event.
Field#9 is located on the same Spillman Farm, just on the other side of the railroad tracks.
If you have any questions, you can reach me on the mobile number listed below.
Roy
Roy L. Whitaker
Director Business Development/Operations
EMA Resources, Inc.
755 Yadkinville Road
Mocksville, NC 27028
Office: 336-751-1441
Mobile: [phone]
From: Roy Whitaker <[e-mail]>
Sent: Friday, February 15, 2019 9:22 AM
To: 'Gabriel Sparks' <[e-mail]>; Bill Brewer ([e-mail]) <[e-mail]>
Subject: Site Maps
Roy L. Whitaker
Director Business Development/Operations
EMA Resources, Inc.
755 Yadkinville Road
Mocksville, NC 27028
Office: 336-751-1441
Mobile: [phone]
t

Section 5
Field soil sampling results

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.govlagronomi/
u�TURF
og �G4LC Saco Predictive Client: Roger Spillman
PO Box 378
y Cooleemee, NC 27014
y Soil Report Mehlich-3 Extraction
o,
Sampled County: Davie
Links to Helpful Information S N 4- P amI d
p e o rovided
Received: 05/15/2019
Farm: NC-DV-08
Completed: 05/24/2019
Sample ID: 00004
Recommendations:
Lime
Crop
(tons/acre) N
Lime History:
1 -Bermuda hay/past., M
0.0 180-220
2 -
0.0
Test Results [units - WN in g/cn�; CEC and Na in meg1100 cm3; NO3-H in mgldrrr ]:
HM% WN CEC
BS% Ac pH
P-1 K-1 Ca% Mg')
0.51 1.00 6.2
81 1.2 6.0
15 52 48 29
Sample ID: 00005
Recommendations:
Lime
Crop
(tonslacre) N
Lime History:
1 -Sudan/Sorghum silage
0.0 180-220
2 -
0.0
Test Results [units - W1V in glcrnr ; CEC and Na in megll00 crnr ; NO3-N in mg/drrr ]:
HM% WN CEC
BS% Ac pH
P-1 K-1 Ca% MgO/
0.22 1.03 14.6
91 1.3 6.4
33 36 57 33
Sample ID: 00006
Recommendations:
Lime
Crop
(tonslacre) N
Lime History:
1 -Sudan/Sorghum silage
0.0 180-220
2 -
0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100
crrP; NO3-N in mgldrrr]:
HM% WN CEC
BS% Ac pH
P-1 K-1 Ca% Mg%
0.18 1.01 16.7
94 1 A 6.4
50 33 56 36
.,North Carolina
Tobacco Tntsl Fund Commission
Client ID: 411288
Nutrients I
P205 K20 Mg S
110 110 0 0
P205
70
P205
40
No. FY19-SL032178
Advisor: Brent Collins
EMA Resources Inc
756 Yadkinville Rd
Mocksville, NC 27028
Advisor ID: 405413
Mn Zn Cu B
0 0 0 0
Soil Class: Mineral
S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-
36 312 204 175 175 35
Nutrients (Ib/acre)
K20 Mg S Mn Zn
130 0 0 0 0
Soil Class. Mineral
Na
0.1
Cu B
0 0
S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na
48 1075 656 431 431 180 0.1
Nutrients (lb/acre)
K20 Mg S Mn Zn Cu
130 0 0 0 0 0
More
Information
Note: 12
ESP SS -I NO3-N
2
More
Information
Note: 12
ESP SS-1 NO3-N
1
More
B Information
0 Note: 12
Soil Class: Mineral
S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS -I NO3-N
32 659 406 431 431 125 0.1 1
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.neagr.gov/agronomi/
Report No. FY19-SL032178
Roger Spillman
Page 2 of 3
Sample ID: 00007
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0
120-200 100
40
0
0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in g/cr&-, CEC and Na in meg1100 cm3; NO3-N
in mg/d0j:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na ESP SS -I NO3-N
022 0.97 15.2 95 0.8 6.6 17 48
64 30
37
558
343
384
384
182 0.1
1
Sample ID: 00008
Recommendations: Lime
Nutrients (lblacre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 120
90
0
0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - WN in glcrrr3; CEC and Na in meg1100 cm3; NO3-N
in mg/do):
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.32 1.04 7.7 89 0.9 6.3 10 26
61 26
35
1396
850
116
115
104 0.1
1

NCDA&CS Agronomic Division Phone: [phone]
G�Gull'uR£ Website: www.ncagr,govlagronomil
A vo Predictive
Client. Brent Collins
Soil
g Report
Resources Inc
�7 � A )�1.]()]"t Mehiich-3 extraction 755 Yadkinville Rd
b,'`c Link Mocksville, NC 27028
1019DLB�' s to Hel fuI infiormation
Sampled: Not Provided
Farm: NC-DV-08 Roger Spillman
Received: 05/24/2019
Completed: 07/03/2019
commendations:
Sa:History;
D: 00009J2-
Lime
p
LimFescue/OGrass/T im,
(tons/acre) N
M P2O5
0.0 120-200 30
0.0
Test Results [units -Wtv in glcrrr3; CEC and Na in megl1oo crn3; NO3-N
HM% WN CEC BS% Ac pH
in mgldm3]:
P-1
0.18 1.01 11.7 91 1.0
K-1 Ca% Mg%
6.4
46 26 57 34
North Carolina
I
Tobacco Trust Fund Commission
Sampled County: Davie
Client ID: 405413
K2O Mg
90 0
Advisor:
Advisor ID:
(Ib/acre)
S Mn Zn Cu
0 0 0 0
Soil Class: Mineral
S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn Al Cu-I Na
28 1813 1099 198 198 118 0.1
Report No. PYIS-SLO34293
More
13 information
0 MO—tgL 12
ESP SS-1 NO3-N
1
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve TrOXIer, Commisclnnor of n,.r. .,rs..