WQ0021577_Residual Annual Report 2019_20200320

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/20/2020
Received:*
Project Number* WQ0021577
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Christopher M. Williams
Email Address*
chris. [e-mail]
Project Information
.........................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0021577
Phone Number*
252-533-6237
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
ApplicantTermittee * WestRock Kraft Paper, LLC/KapStone Kraft Paper Corporation
Facility Name * WestRock Kraft Paper, LLC
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Annual Distribution of Residuals Report.pdf 1.38MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 3/19/2020

WestRock
March 4, 2020
NCDENR-DWR
Water Quality Permit Section
Non -Discharge Permitting Unit
Attn: Information Processing Unit
6th Floor
Division of Water Resources
512 N. Salisbury Street
Raleigh, NC 27699
To Whom It May Concern:
100 Gaston Road office: 252.533.6000
Roanoke Rapids, NC 27870 www.westrock.com
WO0021577 requires submission of an annual Distribution of Residuals Solids report. Enclosed you will
find our Annual Report for CY2019. Please be aware that the Roanoke Rapids Mill was purchased from
KapStone Kraft Paper Corporation by WestRock Kraft Paper, LLC in November 2019. Permit renewals
and application for name change have been made for all permits held by KapStone Kraft Paper
Corporation Roanoke Rapids Mill.
There were no distribution of residuals events in 2019. All residuals were disposed of in the Roanoke
Rapids Mill Landfill in compliance with WO0000436 for CY2019.
Please feel free to contact me at 252-533-6237 with any questions or concerns.
Sincerely,
G
Christopher M. Williams
Environmental Engineer

Annual Distribution of Residuals Report CY2019
WQ0021577
KapStone Kraft Paper Corporation
Roanoke Rapids, NC
Table of Contents
Annual Land Application Certification Form
1
Form DMSDF — Primary Clarifier Residuals Annual Certification 2019
2
Form RSSF — Primary Clarifier Residuals Sampling Summary
3
Form RSSF (B) — Primary Clarifier Residuals Sampling Summary (B)
4
Sample Analysis — Primary Clarifier Residuals
5
TCLP Sample Analysis— Primary Clarifier Residuals
10
Form PVRF 02T— Primary Clarifier Residuals Annual Pathogen Reduction Form
15
Form DMSDF — Flyash Residuals Annual Certification 2019
16
Form RSSF — Flyash Residuals Sampling Summary
17
Form RSSF (B) — Flyash Residuals Sampling Summary (B)
18
Sample Analysis — Flyash Residuals
19
TCLP Sample Analysis — Flyash Residuals
24
Form PVRF 02T— Flyash Residuals Annual Pathogen Reduction Form
29

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0021577 County: Halifax Year: 2019
Facility Name (as shown on permit): KapStone Kraft Paper Corporation
Land Application Operator: Chris Williams Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number of application fields in thepermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. ❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Benjamin P. White, General Manager
Permittee Name and Title (type or print)
01/Z - 3 -y- zo
SignalUre
of Permittee
Date
mi nature of Preparer* Date Signature of Land A6plier
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Date
DENR FORM ACF (12/2006)

Form DMSDF
Primary Clarifier Residuals
Annual Certification
2019

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0021577 FACILITY NAME: KapStone Kraft Paper Corporation
PHONE: [phone] COUNTY: Halifax OPERATOR: Chris Williams
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
© Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ —► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
Primary Clarifier (NC0000752)
0
No Distribution in 2019
0
February
Primary Clarifier (NC0000752)
0
March
Primary Clarifier (NC0000752)
0
April
Primary Clarifier (NC0000752)
0
May
Primary Clarifier (NC0000752)
0
June
Primary Clarifier (NC0000752)
0
July
Primary Clarifier (NC0000752)
0
August
Primary Clarifier (NC0000752)
0
September
Primary Clarifier (NC0000752)
0
October
Primary Clarifier (NC0000752)
0
November
Primary Clarifier (NC0000752)
0
December
Primary Clarifier (NC0000752)
0
Total from FORM DMSDF (sup)
Totals:
Annual (dry tons):
0
0
0
0
Amendments used: I I Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
113h 21,.x,
4&2-d /� W c"
Signature f Permittee Date Signature of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
3-��-
Date
N
DENR FORM DMSDF (12/2006)

Form RSSF
Primary Clarifier Residuals Sampling
Summary

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0021577
Facility Name: KapStone Kraft Paper Corporation
Residual Source WQ # or
NPDES #:
NC0000752
WWTP Name: KapStone Kraft Paper Corporation
Residual Analysis Data
Laboratory: 1)
2)
3)
4)
Meritech, Inc. Reidsville, NC
5) Primary Clarifier Residuals
Parameter
Co
Limit
or • p• Date
Nitrate and Nitrite___]��
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
("� 3 - v- w
Signature of Preparer * Date
`' *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

Form RSSF (B)
Primary Clarifier Residuals Sampling
Summary (B)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0021577
Facility Name: KapStone Kraft Paper Corporation
Residual Source
NPDES # or WQ#:
NC0000752
WWTP Name: KapStone Kraft Paper Corporation
Residual Analysis Data
Laboratory: 1) Meritech, Inc. Reidsville
2)
3)
4)
5) Primary Clarifier Residuals
CompositeSample or Date
Barium, Total
Nitrogen, Total
TotalParameter
.::1
-----------
Calcium, Total
Magnesium,..
11
----__-----
Potassium, Total
Sodium, Total
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
11/V 61jc,)?�
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
3 - y 20
Date
DENR FORM RSSF - B (12/2006)

Sample Analysis
Primary Clarifier Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 071119113
Parameters moults
Sample: Primary Clarifier Residuals Grab
Analysis Date Analt
• % Total Solids
48.4 %
7/12/19
JM
Ammonia, Nitrogen
<20.7 mg/kg
7/16/19
LH
s TKN
349 mg/kg
8/2/19
NW
Nitrate/Nitrite Nitrogen
<20.7 mg/kg
7/14/19
LH
+ Nitrogen, total
349 mg/kg
8/5/19
NW
+ Aluminum, total
6,880 mg/kg
7/17/19
ED
Arsenic, total
2.27 mg/kg
7/17/19
ED
Barium, total
382 mg/kg
7/17/19
ED
Cadmium, total
4.30 mg/kg
7/17/19
ED
Calcium, total
146,700 mg/kg
7/17/19
ED
• Chromium, total
33.9 mg/kg
7/17/19
ED
Copper, total
100 mg/kg
7/17/19
ED
Lead, total
7.91 mg/kg
7/17/19
ED
Magnesium, total
8100 mg/kg
7/17/19
ED
Mercury, total
0.052 mg/kg
7/16/19
MR
Molybdenum, total
<0.516 mg/kg
7/17/19
ED
Nickel, total
30.2 mg/kg
7/17/19
ED
' Phosphorous, total
2230 mg/kg
7/17/19
ED
Potassium, Luca!
i230 mg/kg
7/ 17/19
Lu
+ Selenium, total
2.38 mg/kg
7/17/19
ED
+ Sodium, total
4480 mg/kg
7/17/19
ED
Zinc, total
533 mg/kg
7/17/19
ED
SAR
2.15 -
7/23/19
ED
+ pH
8.0 S.U.
7/12/19
JM
CCE*
34.9 %
7/29/19
LH
* Results not for regulatory purposes
Report Date:
8/5/2019
NPDES#:
WQ0021577
WQ0000436
Project:
Monthly
Date Sample Rcvd:
7/11/2019
7/11/19
Reporting Limit Method
0-100 %
SM2540B
20.7 mg/kg
EPA 350.1
20 mg/kg
EPA 351.1
20.7 mg/kg
EPA 353.2
20 mg/kg
EPA 353.2
5.00 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
0.500 mg/kg
EPA 200.7
0.200 mg/kg
EPA 200.7
10.0 mg/kg
EPA 200.7
0.100 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
0.50 mg/kg
EPA 200.7
10.0 mg/kg
EPA 200.7
0.02 mg/kg
EPA 245.1
0.516 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
2.00 mg/kg
EPA 200.7
20.0 rng/l.g
EPA 2� 0.7
0.50 mg/kg
EPA 200.7
20.0 mg/kg
EPA 200.7
1.0 mg/kg
EPA 200.7
1.0 -14.0 S.U.
SM 4500 H B
1 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data. '-I) fflia &&t"
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-I0-3013 Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ0021577
Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC. Email:_ Neal. [e-mail]
27870 Project:_ Monthly
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your report sent? •R rk needs prior approval.
td (10 3 - 5 Da s 24 - 48 Hrs
Circle all that apply. Em ' preferred), Fa , Ma'
da s
M E R I TE C H INC.
J
ENVIRONMENTAL LABORATORIES
' 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www. meritec —,,++-��
a s. com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print); �/
Lab Use
Start
End
Grab?
# of Cont.
a st
(s) Required
�1 Ice?
Eyes / No
pH OK?
Cl OK?
Date
Time
Date
Time
Primary Clarifier Residuals
/J
�,��
�r1A3
%TOTAL SOLIDS, Ph,
Metals: Al, Ar, Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,
Na,Ni, Se, Zn, Ptot, NH3, TKN, NO2, NO3
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperature Upon
7 ll Receipt:
Method of
Shipment:
"' Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to reservation. ""
Comments:
Compositor #
JJUg #
UPS
Fed Ex
Are these results for regulatory purposes? Ye"
Report results in: mg/L [J mg/kg
FJ ug/L FJ
Hand Delivery.
Relinquished bte: Time: 0 .Zq
/ . /;L.�
Received by: T ,p�
�U
Imo,
Other
Relinquish ate: Time:
Received by: D te: Time:
Relinquished by: Date: Time:
Received by Lab:
_,
7Dit —q. Time:
0

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 1
Contact: Neal Davis Report Date: 7/23/2019
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC-27870 Date Sample Rcvd: 7/11/2019
Meritech Work Order # 07111982 Sample: PCR-15-7-19 Grab 7/11/19
Parameters Results Analysis Date Anal st Reporting Limit Method
% Total Solids 46.3 % 7/12/19 JM 0-100 % SM 2540B
Fecal Coliform 196 col/ g dry 7/11/19 CD 153 col/ g dry SM 9222 D
Meritech Work Order # 07111983 Sample: PCR-16-7-19 Grab 7/11/19
Parameters Results Analysis Date Analyst Reporting Limit Method
% Total Solids
Fecal Coliform
46.1 %
197 col/ g dry
7/12/19
7/11/19
JM
CD
0-100 %
158 col/ g dry
SM 2540B
SM 9222 D
Meritech Work Order #
07111984 Sample: PCR-17-7-19 Grab
7/11/19
Parameters
Results
Analysis Date Anal st
Reporting Limit
Method
% Total Solids
46.6 %
7/12/19
JM
0-100 %
SM 2540B
Fecal Coliform
<195 col/ g dry
7/11/19
CD
195 col/ g dry
SM 9222 D
Meritech Work Order # 07111985 Sample: PCR-18-7-19 Grab
7/11/19
Parameters Results Analysis Date Anal s Reporting Limit Method
% Total Solids
47.0 %
7/12/19
JM
0-100 %
SM 2540B
Fecal Coliform
387 col/ g dry
7/11/19
CD
158 col/ g dry
SM 9222 D
Meritech Work Order # 07111986 Sample: PCR-19-7-19 Grab
7/11/19
Parameters Results Analysis Date Analyst Reporting Limit Method
% Total Solids
47.7 %
7/12/19
JM
0-100 %
SM 2540B
Fecal Coliform
384 col/ g dry
7/11/19
CD
158 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Neal Davis Report Date: 7/23/2019
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 7/11/2019
Meritech Work Order # 07111987 Sample: PCR-21-7-19 Grab gV11/19
Parameters Results Analysis Date Analt Reporting Limit Method
% Total Solids 47.8 % 7/12/19 JM 0-100 % SM 2540B
Fecal Coliform 190 col/ g dry 7/11/19 CD 158 col/ g dry SM 9222 D
Meritech Work Order # 07111988 Sample: PCR-21-7-19 Grab 7/11/19
Parameters Results Analysis Date Analyst Reporting Limi Method
% Total Solids
47.0 %
7/12/19
JM
0-100 %
SM 2540B
Fecal Coliform
387 col/ g dry
7/11/19
CD
158 col/ g dry
SM 9222 D
I hereby certify that 1 have reviewed and approve these data. $6 I T &Ru�_
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

S9-ml6 Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
M E R ITE C H INC.
1
Address:_ 100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email:_ Neal.Davis Kapstonepaper.cor
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Neal Davis Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
www.meritechlabs.com
Circle that Pi I(preferred), Fax, of Std lOda s) 3-5 Da 6 24-49Hrs
all apply:
k
Sampling Dates & Times
Person Taking Sample (Sign/P in ):
` ' /
�v
Lab Use Only
Sample Location and/or ID #
Start
End
Comp?
# of
fesf(s)
Required
On Ice?
/ No
pH OK?
Date
Time
Date
Time
Grab?
Cont.
e
Cl OK?
PRIMARY CLARIFIER
PCR-15-7-19
7 // /�
�.(�.7I
ICLASS
A FECAL COLIFORM ANALYSIS
PCR-16-7-19
CLASS A FECAL COLIFORM ANALYSIS
PCR-17-7-19
'J ��
CLASS A FECAL COLIFORM ANALYSIS
PCR-18-7-19
726
CLASS A FECAL COLIFORM ANALYSIS
PCR-19-7-19
J •��
CLASS A FECAL COLIFORM ANALYSIS `�
PCR-20-7-19
7,130
CLASS A FECAL COLIFORM ANALYSIS
PCR-21-7-19
7'3-5-'
CLASS A FECAL COLIFORM ANALYSIS
Temperature Upon
Receipt: L� I
� )i
Method of
'** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to reservation. ***
Comments: �° �,,�� �� did S�.U.EJ -r li�•���!//J��tc �iL'CY�� ? 9 /9 Aee&- ' ayw v
Compositor #
Shipment:
Jug #
UPS
❑ Fed Ex
Are these results foi regulatory purposes? Yes No FJ
Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Hand Delivery
Relinquished by: Date: Time:
/ O
Received by: J y Da Time:
C/ — �%1E
❑ Other
Relinquished by: C .� pl e: Time .
(Date:
Received by: Date: Time.
Relinquished by: Time:
Received by Lab: 1 - I - 7 MI Time:
0

TCLP Sample Analysis
Primary Clarifier Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd
Page 1
8/23/2019
WQ0021577
WQ0000436
8/8/2019
Meritech Work Order # 080819149 Sample: Primary Clarifier Residuals Grab 8/8/2019
1311- TCLP Metals
Parameter
Results
Analysis Date
Analyst
Det. Limit
Reg. Limit
Method
Arsenic
<0.010 mg/L
8/19/2019
ED
0.100
5.0
EPA 200.7
Barium
0.642 mg/L
8/19/2019
ED
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
8/19/2019
ED
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
8/19/2019
ED
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
8/19/2019
ED
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
8/13/2019
MR
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
8/19/2019
ED
0.100
1.0
EPA 200.7
Silver
<0.050 mg/L
8/19/2019
ED
0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date Analyst
Reporting Limit
Method
Volatiles 8260
Attached
8/14/2019 VV
-
8260
Semi Vol. 8270
Attached
8/20/2019 PM
-
8270
Other Tests
Parameter
Results
Analysis Date Analyst
Reporting Limit
Method
Cyanide, total
<0.500 mg/kg
8/16/2019 LH
0.500 mg/kg
EPA 335.4
Sulfide
<10 mg/kg
8/14/2019 LH
10 mg/kg
SW 846 9038
lgnitability
Will Not Ignite
8/19/2019 NW
-
EPA 1030
Corrositivity (pH)
9.0 S.U.
8/12/2019 1M
1.0 - 14.0 S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Contact: Neal Davis Report Date: 8/23/2019
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 8/8/2019
Meritech Work Order # 080819149 Sample: Primary Clarifier Residuals Grab 8/8/2019
1311 - TCLP Pesticides & Herbicides
Pesticide - SW;Q46 8081A
Parameter
Results Analysis Date Analyst Det. Limit Reg. Limit Dilution Factor
Endrin
Attached - - - -
Chlordane
Attached - - - -
Toxaphene
Attached - - - -
Methoxychlor
Attached - - - -
Heptachlor
Attached - - - -
Lindane
Attached - - - -
Herbicides - SW-846 8151A
Parameter
2,4-D
2,4,5-TP (Silvex)
Results Analysis Date Analyst Det. Limit Reg. Limit Dilution Factor
Attached
Attached
/hereby certify that I have reviewed and approve these data.
�Laoratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
_ Environmental Laboratories
Laboratory Certificate #165
Client: Kapstone Kraft Paper Corp
Project: TCLP
Client Sample ID: Primary Clarifier Residuals
Sample Collection: 08/08/19
Meritech Sample ID: 080819149
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 08/14/19
Extraction:
08/12/19
Analyst: VWV
Report Date:
08/20/19
Parameter
Result
Units
Det. Limit
Rea. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
< 0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 08/20/19
Extraction:
08/ 12/ 19
Analyst: PM
Report Date:
08/20/19
Parameter
Result
Units
net. Limit
Reg. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data. tle,. ,, W, 1/t,
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]
12

RESEARCh & ANALYTICAL
== q LAboFtATORIES, INC.
Analytical/Process Consultations
Toxicity Characteristic Leachate Procedure (TCLP) Analysis for Meritech, Inc., collected 08 August 2019)
08081947 08081.9141 080819149 080819150
EPA HW Quantitation Results Results Results Results Characteristic
Number Contaminant Limit(mg/L) (my/L) (mg/L) (mg/L) (mg1L) Level(mp/L) EPA Method Analyst
I. TCLP PESTICIDESMERBICIDES
D-020
Chlordane
0.003
BQL
BQL
BQL
BQL
0.030
8081
MG
D-016
2,4-D
1.000
BQL
BQL
BQL
BQL
10.0
8151
MG
D-012
Endrin
0.002
BQL
BQL
BQL
BQL
0.020
8081
MG
D-031
Heptachlor
0.0008
BQL
BQL
BQL
BQL
0.008
8081
MG
D-013
Lindane
0.040
BQL
BQL
BQL
BQL
0.400
8081
MG
D-014
Methoxychlor
1.000
BQL
BQL
BQL
BQI,
10.0
8081
MG
D-015
Toxaphene
0.05
BQL
BQL
BQL
BQL
0.500
8081
MG
D-017
2,4,5-TP(Silvex)
0.100
BQL
BQL
BQL
BQL
1.00
8151
MG
Sample Number
70551-01
70552-01
70552-02
70552-03
Sample Date
08/08/19
08/08/19
08/08/1.9
08/08/19
Sample Time (hrs)
1000
0855
0830
0840
Sample Matrix
Sludge
Sludge
Sludge
Sludge
Date Analyzed
08/15-08/19/19
08/1.5-08/20/19
08/15-08/20/19
08/15-08/20/19
rf%&g —milligrams per kilogram — parts per million (ppm) BQL — Below Quantitation Limits

s�mu
Chain of Custody Record (COC)
NPDES#:_
WQ 0021577 & WQ 0000436
M E R ITE C H INC.
Client: Kapstone Kraft Paper Corp Phone:_
Fax:
252-533-6295
252-533-6264
Address: 100 Gaston Road
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email:_
Neal. Davis@ Kapstoneaamr.cor
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Neal Davis
Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
www.meritechiabs.com
Circle all that apply Email(peferred), Fax, Ma'
SOd Std a 3 5 Da s) -s 124-48 I-Irs
Sampling Dates &Times Person Taking Sample (Sign/Print):
Lab Use Only
Sample Location
and/or ID # Start End
Comp? #f On Ice? pH OK?
.Zest(s) Required Yes / No Cl OK?
Date Time Date
Time Grab? Conot.
e
CLAIFIER RESIDUALS (� �. 3
TCLP analysis shall include the. fol.116wing parameters (the rdkdlatory level in milligrams per liter
PRIMARY
in
parentheses): � 0 L;d •
Arsenic (5.0) 1,4-Dichlorobenzene ( .5)
Nitrobenzene (2.0)
Barium (100.0) 1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5) 1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0) 2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5) Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Heptachlor (and its hydroxide)
Toxaphene (0.5)
0.008
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
Method of
"' Dechlorination <0.5 m of Ammonia
Comments:
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
Shipment:
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
UPS
Fed Ex
Are these results for regulatory purposes?
Cresol (200.0)
Methoxychlor (10.0)
Hand Delivery
Relinquished by: k1- fJ C Date:
T
2,4-D (10.0)
Methyl ethyl ketone (200.0)
❑ Other
Relinquished by: Date:
������. n �L
���.�....,.
- •••••-• 670
Relinquished by:
Tlme:
Received by Lab: n
Time: a
c4 ^ I 1

Form PVRF 02T
Primary Clarifier Residuals
Annual Pathogen Reduction Form

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: KapStone Kraft Paper Corporation
WWTP Name: KapStone Kraft Paper Corporation
Monitoring Period: From 1/1/2019 To
WQ Permit Number: WQ0021577
NPDES Number: NC0000752
12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) p
A1t.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A
only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑
Heat Treatment ❑
Thermophihc ❑
Beta Ray ❑ Gamma Ray ❑
Pasteurization ❑
Class B: Alt. (1) Fecal Density ❑
T Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ I
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
190
260.9
387
col/g dry
0
Annual
Fecal
9222D
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
1Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed❑
CERTIFICATION STATEMENT (please check the appropriate statement)
D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Christopher M. Williams, Env. Engineer No Distribution in 2019
Preparer Name and Title (type or print) Land Applier Name and �Titlle (if applicable)(type or print)
3
C� /"l c,��ii— -3-1-0 1114
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006) 15

Form DMSDF
Flyash Residuals
Annual Certification
2019

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0021577 FACILITY NAME: KapStone Kraft Paper Corporation
PHONE: [phone] COUNTY: Halifax OPERATOR: Chris Williams
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ --* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
Flyash (NC0000752)
0
No Distribution in 2019
0
February
Flyash (NC0000752)
0
March
Flyash (NC0000752)
0
April
Flyash (NC0000752)
0
May
Flyash (NC0000752)
0
June
Flyash (NC0000752)
0
July
Flyash (NC0000752)
0
August
Flyash (NC0000752)
0
September
Flyash (NC0000752)
0
October
Flyash (NC0000752)
0
November
Flyash (NC0000752)
0
December
Flyash (NC0000752)
0
Total from FORM DMSDF (sup)
Totals:
Annual (dry tons):
0
0
0
0
Amendments used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No P- If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
—7-y7-0
Date
rn
DENR FORM DMSDF (12/2006)

Form RSSF
Flyash Residuals Sampling
Summary

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0021577
Facility Name: KapStone Kraft Paper Corporation
Residual Source WQ # or
NPDES #:
NC0000752
WWTP Name: KapStone Kraft Paper Corporation
Residual Analysis Data
Laboratory: I)
2)
3)
4)
Meritech, Inc. Reidsville, NC
5) Flyash
Limit
Sampleor • •• Date
TotalParameter
..
t t
_--_-------
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
i'y -6,JL,�
Signature of Preparer *
Date
v *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

Form RSSF (B)
Flyash Residuals Sampling
Summary (B)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0021577
Facility Name: KapStone Kraft Paper Corporation
Residual Source
NPDES # or WQ#:
1►CKI:I:I:lyl•Y►a
WWTP Name: KapStone Kraft Paper Corporation
Residual Analysis Data
Laboratory: 1)
2)
3)
4)
Meritech, Inc. Reidsville, NC
5) Flyash
Parameter
Sampleor . •• Date
Barium, total
Nitrogen, Total
Total
• : 1
Magnesium,-----------
•
1 1
-----------
Potassium, Total_
Sodium,
1
-----------
------------
------------
------------
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
o *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF - B (12/2006)

Sample Analysis
Flyash Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
8/5/2019
Contact: Neal Davis
NPDES#:
WQ0021577
Client: Kapstone Paper
& Packaging
WQ0000436
100 Gaston Rd.
Project:
Monthly
Roanoke Rapids, NC 27870
Date Sample Rcvd:
7/11/2019
Meritech Work Order #
071119112 Sample: Flyash Grab
7/11/19
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
54.8 %
7/12/19
JM
0-100 %
SM2540B
Ammonia, Nitrogen
<18.2 mg/kg
7/16/19
LH
18.2 mg/kg
EPA 350.1
TKN
737 mg/kg
8/2/19
NW
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
<18.2 mg/kg
7/17/19
LH
18.2 mg/kg
EPA 353.2
Nitrogen, total
737 mg/kg
8/5/19
NW
20 mg/kg
EPA 353.2
,Aluminum, total
15,500 mg/kg
7/17/19
ED
5.00 mg/kg
EPA 200.7
-Arsenic, total
14.4 mg/kg
7/17/19
ED
1.00 mg/kg
EPA 200.7
Barium, total
453 mg/kg
7/17/19
ED
0.500 mg/kg
EPA 200.7
Cadmium, total
0.633 mg/kg
7/17/19
ED
0.200 mg/kg
EPA 200.7
Calcium, total
9,820 mg/kg
7/17/19
ED
10.0 mg/kg
EPA 200.7
• Chromium, total
27.6 mg/kg
7/17/19
ED
0.100 mg/kg
EPA 200.7
• Copper, total
68.2 mg/kg
7/17/19
ED
1.00 mg/kg
EPA 200.7
Lead, total
21.4 mg/kg
7/17/19
ED
0.50 mg/kg
EPA 200.7
Magnesium, total
2040 mg/kg
7/17/19
ED
10.0 mg/kg
EPA 200.7
Mercury, total
0.091 mg/kg
7/16/19
MR
0.02 mg/kg
EPA 245.1
Molybdenum, total
1.35 mg/kg
7/17/19
ED
0.500 mg/kg
EPA 200.7
Nickel, total
37.2 mg/kg
7/17/19
ED
1.00 mg/kg
EPA 200.7
• Phosphorous, total
1200 mg/kg
7/17/19
ED
2.00 mg/kg
EPA 200.7
'PGtaSsiLim, total
5.110 n',g/ng
7/1// 17
LtJ
20.0 1'ilgj itg
,:rti 200./
Selenium, total
<0.912 mg/kg
7/17/19
ED
0.912 mg/kg
EPA 200.7
• Sodium, total
2810 mg/kg
7/17/19
ED
20.0 mg/kg
EPA 200.7
Zinc, total
57.3 mg/kg
7/17/19
ED
1.0 mg/kg
EPA 200.7
SAR
4.99 -
7/17/19
ED
-
-
. pH
9.0 S.U.
7/12/19
JM
1.0 - 14.0 S.U.
SM 4500 H B
CCE*
<1 %
7/29/19
LH
1 %
AOAC 955.01
* Results not for regulatory purposes
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-20-2013 Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ0021577
Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC. Email:— Neal. Davis@Kapstonepaper.c
27870 Project:_ Monthly
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your report sent? / *RUSH work needs prior approval.
m� ' v Sa(50 3-5 Da s 24-48Hrs
Circle all that apply: ail .referred), Fax, ail d
M E R I T E C H INC.
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW. meritec — 1.1 S . com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sam (Sig P t):
Lab Use
Start
End
Comp?
Grab?
# of Cont.
Test(s)
Required
On Ice?
ne / No
pH OK?
Cl OK?
Date
Time
Date
Time
Flyash
%TOTAL SOLIDS, Ph, O
Metals: Al, Ar, Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,
Na,Ni, Se, Zn, Ptot, NH3, TKN, NO2, NO3
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperature Upon
1 Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor #
Jug #
UPS
Fed Ex
Are these results for regulatory purposes? Ye N-3
Report results in: mg/L mg/kg
FJ ug/L FJ
Hand Delivery
Relinquished by: D te: Time:
ZZ
Received by: te: Ti e:
Other
Relinqulsh by: Time:
Received by: bateF. Time:
Relinquished by: ate: Time:
Received by Lab: jr �atf� /
Time: p
tJ
CD

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Neal Davis Report Date: 7/23/2019
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 7/11/2019
Meritech Work Order # 07111975 Sample: Flyash 0 7-19 Grab 7/11/19
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
54.1 %
7/12/19
JM
0-100 %
SM 2540B
Fecal Coliform
<168 col/ g dry
7/11/19
CD
168 col/ g dry
SM 9222 D
Meritech Work Order #
07111976
Sample: Flyash P 7-19 Grab
7/11/19
Parameters
Results
Analysis Date Analyst Reporting Limit
Method
% Total Solids
52.1 %
7/12/19
JM
0-100 %
SM 2540B
Fecal Coliform
<174 col/ g dry
7/11/19
CD
174 col/ g dry
SM 9222 D
Meritech Work Order #
07111977
Sample: Flyash Q 7-19 Grab
7/11/19
Parameters
Results
Analysis Date Analyst
Reporting Limit
M!pthgd
% Total Solids
54.3 %
7/12/19 JM
0-100 %
Sl+i[f540B
Fecal Coliform
<167 col/
g dry 7/11/19 CD
167 col/ g dry
SM 9222 D
Meritech Work Order #
07111978
Sample: Flyash R 7-19 Grab
7/11/19
Parameters
Results
Angllysis Date Analyst
Reporting Limit
Method
% Total Solids
53.6 %
7/12/19 JM
0-100 %
SM 2540B
Fecal Coliform
<170 col/
g dry 7/11/19 CD
170 col/ g dry
SM 9222 D
Meritech Work Order #
07111979
Sample: Flyash S 7-19 Grab
7/11/19
Parameters
Results
Analysis Date Analyst
Reporting Limit
Method
% Total Solids
52.4 %
7/12/19
JM
0-100 %
SM 2540B
Fecal Coliform
<173 col/ g dry
7/11/19
CD
173 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
21

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Page 2
Report Date: 7/23/2019
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 7/11/2019
Meritech Work Order #
07111980 Sample: Flyash T 7-19 Grab
7/11/19
Parameters
Results Analysis Date Analyst
Reporting
Method
% Total Solids
53.7 % 7/12/19 JM
0-100 %
SM 2540B
Fecal Coliform
<169 col/ g dry 7/11/19 CD
169 col/ g dry
SM 9222 D
Meritech Work Order #
07111981 Sample: Flyash U 7-19 Grab
7/11/19
Parametgrs
Results Analysis Date Anal st
Reporting Limit
Method
% Total Solids
54.4 % 7/12/19 JM
0-100 %
SM 2540B
Fecal Coliform
<167 col/ g dry 7/11/19 CD
167 col/ g dry
SM 9222 D
1 hereby certify that 1 have reviewed and approve these data. -00ja. [h me
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

S3m16 Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
E R IT E C H INC.
M 1
Address:_ 100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email:_ Neal.Davis Kapstonepaper.cor
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Turn Around Time*
Email: [e-mail]
Attention:_ Neal Davis *RUSH work needs prior approval.
How would you like your report sent?
www.meritechlabs.com
rs
s S) 3-5 DaVs 2d-48 k
Circle all that apply: Em ' (preferred), Fax, ai
Sampling Dates & Times
Person Taking Sample (Sign/ i *
Lab Use Only
Sample Location and/or ID #
Start
End
Comp?
#of
Required
Ice?
es, / No
pH OK?
Cl OK?
Date
Time
Date
Ti a
Grab?
front.'test(s)
FLYASH 0 7-19
1 IL
5
X
CLASS A FECAL COLIFORM ANALYSISillv 4�
FLYASH P 7-19
1
71;50
X
CLASS A FECAL COLIFORM ANALYSIS
FLYASH Q 7-19
; $S
X
CLASS A FECAL COLIFORM ANALYSIS
FLYASH R 7-19
�',�O
X
CLASS A FECAL COLIFORM ANALYSIS
FLYASH S 7-19
S
X
CLASS A FECAL COLIFORM ANALYSIS
FLYASH T 7-19
i
X
CLASS A FECAL COLIFORM ANALYSIS 0
FLYASH U 7-19
1 ��
X
CLASS A FECAL COLIFORM ANALYSIS
Temperature Upon
Receipt:
it t I
Method of
*** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor #
Shipment:
Jug #
UPS
Fed Ex
FA
Are these results for regulatory purposes? Yes No
Report results in: mg/L mg/kg I ug/L
RHand Delivery
Relinquished by Date: i Tim c
) /f �
Received by:
/
❑ Other
Relinquished t e•
Received by: Date: Time:
Relinquished by: Dat : Time:
Received by Lab: 7 $tg:/1 Time: L�
J f1 l/l )
N
w

TCLP Sample Analysis
Flyash Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
s
Page 1
Contact: Neal Davis
Report Date:
8/23/2019
Client: Kapstone Paper & Packaging
NPDES#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids, NC 27870
Date Sample Rcvd:
8/8/2019
Meritech Work Order It 080819150 Sample: Flyash Grab
8/8/2019
1311- TCLP Metals
Parameter
Results
Analysis Date
Analyst
Det. Limit
Reg. Limit
Method
Arsenic
<0.010 mg/L
8/19/2019
ED
0.100
5.0
EPA 200.7
Barium
0.819 mg/L
8/19/2019
ED
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
8/19/2019
ED
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
8/19/2019
ED
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
8/19/2019
ED
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
8/13/2019
MR
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
8/19/2019
ED
0.100
1.0
EPA 200.7
Silver
<0.050 mg/L
8/19/2019
ED
0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date
Analyst
Reporting Limit
Method
Volatiles 8260
Attached
8/14/2019
VV
-
8260
Semi Vol, 8270
Attached
8/20/2019
PM
-
8270
Other Tests
Parameter
Results
Analysis Date
Analyst
Reporting Limit
Method
Cyanide, total
<0.500 mg/kg
8/16/2019 LH 0.500 mg/kg EPA 335.4
Sulfide
<10 mg/kg
8/14/2019 LH 10 mg/kg SW 846 9038
Ignitability
Will Not Ignite
8/19/2019 NW - EPA 1030
Corrositivity (pH)
7.9 S.U.
8/12/2019 JM 1.0 -14.0 S.U. SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
A
Page 2
Contact: Neal Davis Report Date: 8/23/2019
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 8/8/2019
Meritech Work Order # 080819150 Sample: Flyash Grab 8/8/2019
1311- TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Analyst Det. Limit Reg. Limit Dilution Factor
Endrin Attached - - - -
Chlordane Attached - - - -
Toxaphene Attached - - - -
Methoxychlor Attached - - - -
Heptachlor Attached - - - -
Lindane Attached - - - -
Herbicides - SW-846 8151A
Parameter Results Analysis Date Analyst Det. Limit Reg. Limit Dilution Factor
2,4-D Attached - - -
2,4,5-TP (Silvex) Attached - - -
I hereby certify that 1 have reviewed and approve these data. yrM aajoo= ft)
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
Environmental Laboratories
- Laboratory Certificate #165
Client: Kapstone Kraft Paper Corp
Project: TCLP
Client Sample ID: Flyash
Sample Collection: 08/08/19
Meritech Sample ID: 080819150
1311 - TCLP Oraanics
Volatiles: SW-846 8260
Analysis: 08/14/19
Extraction:
08/12/19
Analyst: VWV
Report Date:
08/20/19
Parameter
Result
Units
Det. Limit
Ree. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
I,1-Dichloroethene
<0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 08/20/19
Extraction:
08/12/19
Analyst: PM
Report Date:
08/20/19
Parameter
Result'.'
-'-nits
Det_Limit
Ree. Limit
Dilution !:actor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed
these data.
r
and
approve
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]
26

R ESEARCh & ANA[yTICA1
LAhORATORIES� INC.
Analytical/Process Consultations
Toxicity Characteristic Leachate Procedure (TCLP) Analysis for Meritech, Inc., collected 08 August 2019)
,,��f11111►I►I�I
1% NO #34 Z!
`....ECT�Q'�g16���•
�E0 Att •��
08081947 080819148 080819149 0808191
EPA RW Quantitation Results Results Results esults Characteristic
Number Contaminant Limit(ms/L) (my/L) (ml?/L) (my —IL) m /L Level(mL/L) EPA Method Analyst
I. TCLP PESTICIDESMERBICIDES
D-020
Chlordane
0.003
BQL
BQL
BQL
BQL
0.030
8081
MG
D-016
2,4-D
1.000
BQL
BQI,
BQL
BQL
10.0
8151
MG
D-012
Endrin
0.002
BQL
BQL
BQL
BQL
0.020
8081
MG
D-031
Heptachlor
0.0008
BQL
BQL
BQL
BQL
0.008
8081
MG
D-013
Lindane
0.040
BQL
BQL
BQL
BQL
0.400
8081
MG
D-014
Methoxychlor
1.000
BQL
BQL
BQL
BQL
10.0
8081
MG
D-015
Toxaphene
0.05
BQL
BQL
BQL
BQL
0.500
8081
MG
D-017
2,4,5-TP(Silvex)
0.100
BQL
BQL
BQL
BQL
1.00
8151
MG
Sample Number
70551-01
70552-01
70552-02
70552-03
Sample Date
08/08/19
08/08/19
08/08/19
08/08/19
Sample Time (Itrs)
1000
0855
0830
0840
Sample Matrix
Sludge
Sludge
Sludge
Sludge
Date Analyzed
08/15-08/19/19
08/15-08/20/19
08/15-08/20/19
08/15-08/20/19
mgUrg = milligrams per kilogram= parts per million (ppm) BQL a Below QuanGlation Limits
v

5-9-3016 Chain of Custody Record (COC)
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
4L 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
Client: Kapstone Kraft Paper Corp
Address: 100 Gaston Road
Roanoke Rapids, NC 27870
NPDES#:_ WQ 0021577 & WQ 0000436
Phone:_ 252-533-6295
Fax: [phone]
Email: Neal. Davis6D Kanstonevaoer.cor
Project: `
P.O.#: If
Attention:_ Neal Davis Turn Around Time*
How would you like your report sent?? "RUSH work needs prior approval.
Circle all that apply: ma' referred) , Fax, : �Z Std 110 days) 1 3 -5 Da s 24-48 Hr
Sampling Dates &Times Person Taking Sample (Sign/Print):rlG J ' i�b Use Only
Sample Location and/or ID # ' 4"
Start E e TCLP analysis shall include the followi g parameters (theiregulatory level in milligrams per liter
Date I Ti'/m,�e Date in parenthe
�s(� ses):
FLYASH ��yi/ Arsenic (5 0)
Method of
Shipment:
UPS
Fed Ex
Hand Deliver
Other
www.meritechlabs.com
Comments:
Are these resuVs for regulatorypurposes?
Relinquished by Date:
40
Relinquish Date:
Relinquished y: Date:
Barium (100.0)
Benzene (0.5)
Cadmium (1.0)
Carbon tetrachloride (0.5)
Chlordane (0.03)
Chlorobenzene (100.0)
Chloroform (6.0)
Chromium (5.0)
m-Cresol (200.0)
o-Cresol (200.0)
p-Cresol (200.0)
Cresol (200.0)
2,4-D (10.0)
Time,/ 00
Time: /-irs -
Time:
1,4-Dichlorobenzene (7.5)
1,2-Dichloroethane (0.5)
1,1-Dichloroethylene (0.7)
2,4-Dinitrotoluene (0.13)
Endrin (0.02)
Hexachlorobenzene (0.13)
Heptachlor (and its hydroxide)
Hexachloro-1,3-butadiene (0.5)
Hexachloroethane (3.0)
Lead (5.0)
Lindane (0.4)
Mercury (0.2)
Methoxychlor (10.0)
Methyl ethyl ketone (200.0)
Received by:
Received by:
Received byJ.ab:
Nitrobenzene (2.0)
Pentachlorophenol(100.0)
Pyridine (5.0)
Selenium (1.0)
Silver (5.0)
Tetrachloroethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,6-Trichlorophenol (2.0)
2,4,5-TP (Silvex) (1.0)
Vinyl chloride (0.2)
J
_6 Time: 1H I
N
00

Form PVRF 02T
Flyash Residuals
Annual Pathogen Reduction Form

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: KapStone Kraft Paper Corporation
WWTP Name: KapStone Kraft Paper Corporation
Monitoring Period: From 1/l/2019 To
WQ Permit Number:
NPDES Number:
12/31 /2019
WQ0021577
NC0000752
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ I
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) p
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A
only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density L31
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ 1
Air Drying ❑
1 Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
y
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
<167
169.7
<174
col/g dry
0
Annual
Fecal
9222D
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed RI
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Christopher M. Williams, Env. Engineer
Preparer Name and Title (type or print)
&�e1/4 `tl 3 y-w
No Distributions in 2019
Land Applier Name and Title (if applicable)(type or print)
N f �-
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006) 29