Loading...
HomeMy WebLinkAboutWQ0037637_Residual Annual Report 2019_20200228 (2)Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application r Annual Report what is the submittal r Residual Annual Report type?* r Additional Information r Other Annual Report 2019 Year* Date Paper Copy 2/28/2020 Received:* Project Number* WQ0037637 Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues. .......................................................................................................................................................................................................................................................................................................................................................................... Name * Robert T. Branch Email Address* bbranch@branchrs.com Project Information Submittal Type* r New Permit Application r Renewal r Annual Report r Other Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted? r Yes r Nor N/A Permit Number* WQ0037637 Applicant\Permittee * Craven Ag Services Facility Name * Craven Ag Services Phone Number* 336.510-0340 r Modification (Major or Minor) r Additional Information r Residual Annual Report r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. This is a revised 2019 Annual report for Craven Ag that reflects a changed updated ARSS for the Town of Maysville. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) 2019 Craven Ag AR Final REV.pdf 2.9MB Upload only 1 R7F document. Maniple documents must be combined into one R7F file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required, be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been received. The paper copy shall include the following: o Application Form o All relevant attachments {talcs, soils report, specs, etc.] o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) Mailine address: Division of Water Resources ! Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W - = Raleigh, NC 27699-1617 S12 N.5alisburySt. For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560. * rJ By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 3/16/2020 2019 ANNUAL REPORT CRAVEN AG SERVICES, INC. LAND APPLICATION PROGRAM PERMIT #WQ0037637 Prepared For: Craven Ag Services, Inc. 2115 NC Highway 55 New Bern, North Carolina 28562 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill, SC 29732 February 2020 BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732 PHONE (336) 312-9007 February 26, 2020 North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2019 LAND APPLICATION ANNUAL REPORT Craven Ag Services, Inc. Permit No. WQ0037637 Branch Residuals & Soils Project No. 2019-132 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of the Craven Ag Services, Inc. This data includes: 1) Certification Forms, 2) Annual Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data 10) 2019 Application Summary Table, and 11) 2019 Application Condition Summaries. A total of 141,500 gallons (5.38 dry tons) of Class B lime -stabilized biosolids were incorporated to 27.3 acres in 2019. This material was divided as follows: 0 84,000 gallons (4.90 dry tons) from Maysville WWTP, • 57,500 gallons (0.48 dry tons) from Bridgeton WWTP. and • 0 gallons (0 dry tons) from Pruitt Health Sealevel WWTP. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sincerely, Robert T. Branch, L.S.S. Land Application/Residuals Operator #15676 RTB Enclosures cc: Town of Maysville Town of Bridgeton Craven Ag Services, Inc. Pruitt Health Sealevel, NC TABLE OF CONTENTS SECTION NO. TITLE I Certification Forms II Annual Residual Sampling Summary Forms III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary Forms V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Forms VIII Pathogen and Vector Attraction Reduction Documentation IX Soil Analysis Reports X 2019 Application Summary Table XI 2019 Application Condition Summaries CERTIFICATION FORMS AIv1N UAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0037637 County: Craven Facility Name (as sh)tivn on permit): Year: 2019 Craven Ag r Services, Inc Land Application Operator: Craven Ag Services, Inc. Phone: (252 633-5334 1-nd application of residuals as allowed by the permit occurred during the past calendar year? _'1 Yes j: J No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A- RPdrhiale A.,.,l:...a:_- Total number of application fields in the ermit: 23 Total number of fields utilized for land application during the year: 3 Total amount of dry tons applied during the year for all application sites: 5.38 Total number of acres utilizes for land application during the year 27.3 Part B Annual Compiance Statement Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. Yes LJ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. o) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Mr. John W. Dunham, Owner 'tmittee Name and Title (type or print) \ \J:t a- v J.Wignaet±urte of Permittee Date See Attached Signature of Preparer* Date (ignature of Land Applier Date (if different from Permittee) (if different from Pernttee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL LAND APPLICATION CERTIFICATION FORM TOWN OF MAYSVILLE Art B - Annual Comniance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes Ll No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the pernut. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Pen -nit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). w I) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the pemut were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Date (if different from Permittee) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. I 102 (26) ANNUAL LAND APPLICATION CERTIFICATION FORM TOWN OF BRIDGETON . art B - Annual Com iance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes :J No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Preparer* Date (if different from Perm ittee) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) ANNUAL RESIDUAL SAMPLING SUMMARY FORMS ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0037637 Facility Name: Craven Ag Services, Inc Residual Source WQ # or NPDES #: NCO021482 WWTP Name: Town of Maysville WWTP Residual Analysis Data Laboratory: 1) 2) 3) 4) 5) Environmental Chemists, Inc. Parameter (mg/kg) Conc. Limit m Sam le or Composite Date 11 /6/2019 Percent Solids (%) NA 1.40 Arsenic 75 <13.8 Cadmium 85 <13.8 Copper 4,300 403.00 Chromium NA <13.8 Lead 840 18.20 Mercury 57 <1.00 Molybdenum 75 <13.8 Nickel 420 14.50 Selenium 100 <13.8 Zinc 7,500 871.00 Total Phosphorus NA 19,400 TKN NA 28,300 Ammonia -Nitrogen NA r_1,640 Nitrate and Nitrite NA 126 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submittfj>�g false information, including the possibility of fines and imprisonment for knowing violations." of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SA, ) ING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0037637 Laboratory: 1) Facility Name: Craven Ag Services, Inc 2) Residual Source WQ # or NCO074837 3) NPDES #: 4) WWTP Name: Town of Bridgeton WWTP 5) Residual Analysis Data Environment One, Inc. Parameter (mg/kg) Ceiling Conc. Limit Sample or Composite Date 1/2/2019 Percent Solids (%) NA 0.20 Arsenic 75 <2.50 Cadmium 85 Copper 4,300 335.00 Chromium NA 17.00 Lead 840 31.00 Mercury 57 0.25 Molybdenum 75 <5.00 Nickel 420 10.00 Selenium 100 <5.00 Zinc 7,500 1754.00 Total Phosphorus NA 17,650 TKN NA 45,750 Ammonia -Nitrogen NA 76 Nitrate and Nitrite • percent solids were not collected on Gymd NA smnple until 2/I4/17 21 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penaly s for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date np:mp Pr)pdA L7CCc /aoMnnc� ANNUAL METALS FIELD LOADING SUMMARY FORMS ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: -I.rmit #: ,rator: . _..res Used: 2.60 n/a Se 6.6 Acres Permitted: 5.6 Site #: 3 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): N119-47778 BEI.440A Craven Ag Services Total Dry Tons Applied (Annual): WQ0037637 Cation Exchange Capacity (non 503 only): Allen Roach Owner: Allen & Gloria Roach Predominant Soil Series • ` 11 . 1 ncavy ARM rtela Loadings luaiculated in the/nerpl- � f 11 OEM- MEMM -1 cerury, under penalty of law, that this document was prepared under my direction or supervision in ,ordance with a system designed to assure that qualified personnel properly gathered and evaluated the irmation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" i ature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) A1N1N UAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Craven Ag Services Total Dry Tons Applied (.Annual): .-Rermit #: WQ0037637 Cation Exchange Capacity (non 503 only): erator: Allen Roach Owner: Allen & Gloria Roach Predominant Soil Series ..ores Used: 14.6 Acres Permitted: 14.6 Site #• 3 To n/a 35.06 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): BEI-440AO-W000956 N419-4777R Sample or Com- posite Date 1/2/19 2/22/19 11/6/19 % Solids 0.20 74.10 1.40 Arsenic 2.50 0.00 13.80 Cadmium 1.90 0.00 13.80 Chromium 17.00 0.00 0.00 Copper 335.00 0.89 403.00 Lead 31.00 0.02 18.20 Mercury 0.25 0.00 1.00 Molyb- denum 5.00 0.00 13.80 Nickel 10.00 0.03 14.50 Selenium 5.00 0.00 13.80 Zinc 1754.00 1.56 871.00 Total phos- ;orus 17,650 60 19,400 c 1111-1 ucavy tvietai yield Loatiln¢5 f('stlrulatpd in the/onrnl. 1 1 1 ' • r�e t 1 ,NMI -�' L iy, unber penalty o haw, that this document was prepared under my direction or supervision in ^ordance with a system designed to assure that qualified personnel properly gathered and evaluated the .ormation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" 4'gnature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) TUNA UAL lvtE I AL, 1"IELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility ame. -X",krmit #: :rator: titres Used: Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): BEI-"OA Craven Ag Services Total Dry Tons Applied (Annual): 0.18 WQ0037637 Cation Exchange Capacity (non 503 only): n/a Allen Roach Owner: Allen & Gloria Roach Predominant Soil S T 6.1 Acres Permitted: 6.1 Site #: . .1 J4M1 1-l- tr�.CLi1, meta LOaa - 1 1 • , 1 11 -_------ 1 11 Total • • ^ • «, ME uuuer penalty oI taw, that this document was prepared under my direction or supervision in cordance with a system designed to assure that qualified personnel properly gathered and evaluated the rormation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" ignature �ofLand Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. r1r,l.,L 0u1vI1v1AKY itUKiVI PLF rAKE A COPY OF THIS BLANK FORM TO BE COMPLET }ND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BG HEN NOT APPLICABLE. Facility Name: Craven Ag Services WQ Permit #: WQ0037637 Field #: 3 Acres Utilized: Owner: Allen & Gloria Roaclt Annual Dry Tons Applied: 2.60 Site #: I Acres Permitted: Operator: Allen Roach Predominat Soil Series Se Cation Exchange Capacity (non 503): Crop I Name: Millet Crop I Max PAN: 100.00 Crnn 2 Nnmp- RM/A , hR--. -- 6.60 5.60 NA C7 � �' o Jul-19 Specify Totals Per Acre 61364 Solids ° As Decimal 1.40 Volume Applied per Acre DT/Ae 0.37 Residual Sources {NPDES tl, WQtf, Feri., Animal Waste, etc.) Maysville W WTP Site Cord. (Dry Wet Moist) Precip. Past 24 yrs, Inches D a n. o W a _ � 'o' a INC o „ N 1.00 m . W W = 0.30 TKN nt • k • 28,300 z D 2 3 °o o a �' m • k • 1,640 Nitrate and Nitrite m • k • 126 PAN Applied PP (lbs/acre) J Gal'o Must Select Crop 1 or Crop 2 C1,.Yd. Report Totals in Gal. 42,000 Crop I 7.25 Crop 2 Crop 1 X Crop 2 Jul-19 18,000 2,727 0.20 0.02 Bridgeton WWTP INC 1.00 0.30 45,750 76 21 0.63 X TOTALS: 9,091 Annuallbs/acre Current Cumulative lbs/acre As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 0.01 0.01 0.00 0.31 0.01 0.00 0.01 0.01 0.01 0.73 15.22 7.88 0.00 0.01 0.01 NA 0.57 0.02 0.00 NA 0.03 0.02 2.77 0.00 0.00 0.02 0.25 0.00 0.00 0.01 0.02 0.01 20 3G 34 NA 1,338 267 IS NA 374 89 2,498 too 00 t{,.� a� ...... wf . _J - _ J___ Lime A lied Date lbs/ac Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I rprtifv nnrinr nanolfn, of ln.., kh -- - - --- 11. -1 -- ......... ...J uu oa.a,vaa UA auPca V mum ui accuruance wim a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation [/ U **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading,�,t�,� pp"HF�tuR F(1RC\A FCG I1.7J-)nnr-% PLY Facility Name: Owner: Operator: . 'v_' 11 a_,�11.iJt1 Ll1.1•1t1VLY rLV I,u ,0UIVINIAKY 11UIUV1 MAKE A COPY OF THIS BLANK FORM TO BE COMPLE" �ND SUBMITTED FOR EACH APPLICATION FIELD. } ll PLACE A "N/A" IN A BLANK OR BG_ EN NOT APPLICABLE. Craven Ag Services WQ Permit #: WQ0037637 Field #: 3 Acres Utilized: 14.60 Allen & Gloria Roach Annual Dry Tons Applied: 35.06 Site #• 2 Acres Permitted: 14.60 Allen Roach Crop I Name: Corn (Grain) Predominat Soil Series Crop l Max PAN: 138.00 To Croa 2 Name Cation Exchange Capacity (non 503): NA Rye(Grain) rrnn7Mov PAN Snnn od w f9 o SpeciN Totals Per Acre ^„ Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Site Cond. (Dry' Wet, Moist) Preci p. Past 24 1-Irs. Inches a 3:., �� �' o w ° o =• * �, ; rb TKN jug/kg D z g o 3 `� w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Must Select Crop I or Crop 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Mar-19 18,500 1,267 0.20 0.01 Bridgeton WWTP INC 1.00 0.30 45,750 76 21 0.29 X Nov-19 44 3 74.10 2.22 Craven Wood Energy INC 1.00 0.30 1 0 0 0.00 X Nov-19 42,000 2,877 1.40 0.17 Maysville WWTP INC 1.00 0.30 28,300 1,640 126 3.28 X TOTALS: 4,147 : As Cd Cr Cu I Pb Hg Mo Ni Se Zn P PAN 1 PAN Lime Applied Annuallbs/acre Current Cumulative lbs/acre 0.00 0.00 0.00 0.15 0.01 0.00 0.00 0.01 0.00 0.34 7.16 0.29 3.28 0.00 0.00 NA 0.15 0.01 0.00 NA 0.01 0.00 0.34 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 • • • 36 34 NA 1,338 267 15 NA 374 89 2,498 138.00 50 Date Nov-19 Ibs/ac 128 Prior Years Cumulative Ibs/acre Permitted C. P. L. R,**** Permit PAN Limit Ist/2nd Crop __11 ____ 1._.__..� ,...»,,, ,.,,,„- },1 a. jjakc uNg. 1;1 111y u11 CLAIM, Vt w1jervlsiun m aeeoruanee wttn a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / ] *Application Method: S - Surface, IN - Injection, INC -Incorporation �.Z 9 **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading R `Y7%R F(IRKA FCF (4,)i-,nna1 PLE Facility Name: Owner: Operator: AININUAL LA1v1J AYYL1l,AI IVIN VIEL l) NUMMARY NORM YIAKE A COPY OF THIS BLANK FORM TO BE COMPLET "ND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BO,_ . I EN NOT APPLICABLE. Craven Ag Services WQ Permit #: WQ0037637 Field M 3 Acres Utilized: 6.10 Allen & Gloria Roach Annual Dry Tons Applied: 0.18 Site #: 3 Acres Permitted: 6.10 Allen Roach Predominat Sail Series To Cation Capacity Exchange Ca g p ty (non 503): NA Crop 1 Name: Wheal (Grain) Crap 1 Max PAN: 111.00 Crop 2 Name: #N/A Cron 2 Max. PAN #N/A CJ o m o S Peci FV Totals Per Acre OQ Solids As Decimal Volume Applied per Acre DTAc Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.) Se1C Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs. Inches K d n, _. 0 ? o 7 o - a + h j ;a 0 � w o' =1 TKN mg/kg Z a 9 o 9 m•k• Nitrate and Nitrite m•k• PAN Applied PF (Ibs/acre) Must Select Crop 1 or Crop 2 Gal. Cu.Yd. Report Totals in Gat. Crop I Crop 2 Crop I Crop 2 Oct-19 21,000 3,443 0.20 0.03 Bridgeton WWTP INC 1.00 0.30 45,750 76 21 0.79 X TOTALS: 3,443 As Cd Cr I Cu Pb Re I Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.00 0.60 0.00 0.02 0.00 0.00 0.00 0.00 0.00 0.10 1.01 0.79 1 0.00 Date lbs/ac Current Cumulative lbs/acre 0.00 0.00 NA 0.02 0.00 0.00 NA 0.00 1 0.00 0.10 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 36 34 NA 1,338 267 15 NA 374 89 2,498 111.001 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop --I CCCLIIy, UlluCr penally UI 111W, Inal tnls uocumenE was preparea unaer my arreclion or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading R� •`F1fNR Fr1RhA F'CF 117Mnnm RESIDUAL ANALYSIS LAB SHEETS Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Town of Bridgeton Bridgeton WWTP Havelock, North Carolina Carven Ag Services Wastewater Treatment Plant BEI-440A 1/2/2019 1 /28/2019 Annual 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids* 0.20 Nitrogen (TKN)* 4.575 45,750.000 Phosphorus * 1.765 17,650.000 Potassium 0.528 5,283.000 Sulfur 0.000 0.000 Calcium 4.752 47,517.000 Magnesium 0.308 3,084.000 Sodium 3.130 31,302.000 Iron --- Aluminum --- 3,391.000 Manganese --- Copper --- 335.000 1,500 Zinc --- 1,754.000 2,800 Ammonia Nitrogen* 0.008 76.140 Nitrate N / Nitrite N* --- 21.200 Cadmium --- 1.900 39 Chromium --- 17.000 1,200 Nickel --- 10.000 420 Lead --- 31.000 300 Arsenic --- 2.500 41 Mercury --- 0.250 17 Selenium --- 5.000 100 pH 6.900 Calcium Carbonate Eq. (est) 0.000 Organic Nitrogen 4.567 45,673.860 Molybdenum --- 5.000 75 Chloride --- Boron Available P2O5 Specific Gravity 8.340 Wastewater Treatment Plant Bridgeton WWTP Havelock, North Carolina Carven Ag Services Annual 2019 Date Reported: 1/28/2019 Report No: BEI-440A Note All Units in Pounds Per Dry Ton Macro Nutrients Physical Characteristics PAN Surf. 27.523 PAN Inj. 27.599 P 35.300 K 10.566 Lime (estimated) 0.000 Secondary Nutrients Calcium 95.034 Magnesium 6.168 Sodium 62.604 SAR 1.677 Chloride 0.000 Iron 0.000 Alumium 6.782 Manganese 0.000 Boron 0.000 Sulfur 0.000 % Solids 0.20 pH 6.900 Min Rate 0.300 Metals Arsenic 0.005 Cadmium 0.004 Chromium 0.034 Copper 0.670 Lead 0.062 Mercury 0.001 Molybdenum 0.010 Nickel 0.020 Seleniun 0.010 Zinc 3.508 EMAMMEW Flo dMC@TP@T@%d Ds3nIsidg 4fa �s� 's'37715 {{astawatar ID, 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 TOWN OF BRIDGETON HYDRO SERVICES & CONSULTING MR. KEVIN MULLINEAUX P.O. BOX 317 HAVELOCK ,NC 28532 PH (not to be used for reporting) Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Sodium Adsorption Ratio (calc) Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 6.9 01/02/19 HAI 4 4500HB-11 3991 01/15/19 LFJ EPA200.7 <2.5 01/22/19 MTM 3113B-04 47517 01/15/19 LFJ EPA200.7 1.9 01/17/19 MTM 3113B-04 335 01/15/19 LFJ EPA200.7 17 01/15/19 LFJ EPA200.7 31 01/18/19 MTM 3113B-04 3084 01/15/19 LFJ EPA2110.7 0.25 01/18/19 MTM EPA7471B 10 01/15/19 LFJ EPA200.7 5283 01/15/19 LFJ EPA200.7 <5.0 01/15/19 MTM 3113B-04 31302 01/15/19 LFJ EPA200.7 1754 01/15/19 LFJ EPA200.7 37.6 0.20 01/03/19 J1NIS 2540G-11 c 45750 01/16/19 CLO 351.2 R2-93 c 76.14 01/11/19 DTL 350.1 R2-93 c 17650 01/16/19 DTL 365.4-74 c 21.20 01/11/19 CLO 353.2 R2-93 <5.0 01/15/19 LFJ EPA200.7 PHONE (252) 756-6208 F.r, ;~52) 756-0633 ID#: 440 A DATE COLLECTED: 01/02/19 DATE REPORTED : 01/28/19 REVIEWED BY: Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Town of Maysville Maysville WWTP Maysville, North Carolina Carven Ag Services Wastewater Treatment Plant 19-47778 11/6/2019 12/4/2019 Annual 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids* 1.40 Nitrogen (TKN)* 2.830 28,300.000 Phosphorus * 1.940 19,400.000 Potassium 0.377 3,770.000 Sulfur 0.000 0.000 Calcium 3.890 38,900.000 Magnesium 0.291 2,910.000 Sodium 0.757 7,570.000 Iron --- Aluminum --- 5,110.000 Manganese --- Copper --- 403.000 1,500 Zinc --- 871.000 2,800 Ammonia Nitrogen* 0.164 1,640.000 Nitrate N / Nitrite N* --- 126.000 Cadmium --- 13.800 39 Chromium --- 1,200 Nickel --- 14.500 420 Lead --- 18.200 300 Arsenic --- 13.800 41 Mercury --- 1.000 17 Selenium --- 13.800 100 H 6.740 Calcium Carbonate Eq. (est) 0.000 Organic Nitrogen 2.666 Molybdenum --- 13.800 75 Chloride --- Boron Available P2O5 Specific Gravity 8.340 Wastewater Treatment Plant Maysville WWTP Maysville, North Carolina Carven Ag Services Annual 2019 Date Reported: 12/4/2019 Report No: M19-47778 Note All Units in Pounds Per Dry Ton Macro Nutrients Physical Characteristics PAN Surf. 17.888 PAN Inj. 19.528 P 38.800 K 7.540 Lime (estimated) 0.000 Secondary Nutrients Calcium 77.800 Magnesium 5.820 Sodium 15.140 SAR 1.178 Chloride 0.000 Iron 0.000 Alumium 10.220 Manganese 0.000 Boron 0.000 Sulfur 0.000 % Solids 1.40 pH 6.740 Min Rate 0.300 Metals Arsenic 0.028 Cadmium 0.028 Chromium 0.000 Copper 0.806 Lead 0.036 Mercury 0.002 Molybdenum 0.028 Nickel 0.029 Seleniun 0.028 Zinc 1.742 envirochem srn ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill 6 ay, Wilrnington, NC 28405 a 910392.0223 Lab • 910.392.4424 Fax 710 Bowsertok�n Road, Nianteo, NC 27954 • 252.473.5702 Lab/Fax 2i5-A Wilminoton t lighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infou em ironmentalcheniists.com Town of Maysville Post Office Box 265 Maysville NC 28555 Attentions Date of Report: Dec 04, 2019 Customer PO #: Customer ID: 17020023 Report #: 2019-18771 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-47778 Site: Sludge 11/6/2019 2:30 PM Solid/Sludge boomer Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 8081B/3510 <0.02 mg/L 11/20/2019 Endrin (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 11/20/2019 Heptachlor (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 11/20/2019 Heptachlor epoxide (TCLP) SW 846 Method 608113/3510 <0.0005 mg/L 11/20/2019 Lindane (TCLP) SW 846 Method 80816/3510 <0.0005 mg/L 11/20/2019 Methoxychlor (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 11/20/2019 Toxaphene (TCLP) SW 846 Method 8081B/3510 <0.05 mg/L 11/20/2019 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 11/19/2019 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/19/2019 2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 11/20/2019 2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 11/20/2019 1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Benzene (TCLP) SW845 Method 8260/5030 <0.01 mg/L 11/19/2019 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Rannrt@ 7n1q_1A771 Environmental Chemists, Inc, env-wochem 6602 Windmill Vviw, Wilmington, NC 28405 • 910.392.0223 Lab • 910.391.4424 Fax 710 Bowsertown Road, 1%,tanteo, NC 27954 6 252.473.5702 Lab/Fax sr.t '_55-A Wilmington Highway, Jacksorwille, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info'a em irinu»entalchenlists.com Town of Maysville Date of Report: Dec 04, 2019 Post Office Box 265 Customer PO #: Maysville NC 28555 Customer ID: 17020023 Attention: Report #: 2019-18771 Project ID: Sludge Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 11/19/2019 Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 RCI Cyanide EPA 335 4 Reporting limit elevated due to matrix interference. <0.05 mg/kg 11 /15/2019 Sulfide SM 4500 S D 0.22 mg/kg 11/08/2019 Ignitability SW 846 method 1010 >195 °F 11/15/2019 pH SW 846 Method 9045D 6.74 units 11/13/2019 Sludge Residuals Aluminum EPA 200.7 5110 mg/kg 11/18/2019 Arsenic EPA 200 7 <13.8 mg/kg 11/18/2019 Cadmium EPA 200 7 <13.8 mg/kg 11/18/2019 Calcium EPA 200 7 38900 mg/kg 11/18/2019 Chromium EPA 2007 <13.8mg/kg 11/18/2019 Copper EPA 200 7 403 mg/kg 11/18/2019 Lead EPA 200 7 18.2 mg/kg 11/18/2019 Magnesium EPA 200 7 2910 mg/kg 11/18/2019 Molybdenum EPA 200 7 <13.8 mg/kg 11/18/2019 Nickel EPA 200 7 14.5 mg/kg 11118/2019 Potassium EPA200.7 3770 mg/kg 11/19/2019 Selenium EPA 2007 <13.8mg/kg 11/18/2019 Sodium EPA 200 7 7570 mg/kg 11/18/2019 Zinc EPA 200 7 871 mg/kg 11/18/2019 Total Kjeldahl Nitrogen (TKN) EPA 351 2 28300 mg/kg 11/18/2019 Nitrate+Nitrite-Nitrogen EPA 353 2 126 mg/kg 11/18/2019 Total Solids (%) SM 2540 8 1.40 % 11 /11 /2019 Report # 2019-18771 Environmental Chemists, Inc. envirochem 6602 Windmill 4VaY Wilmin;tun, iti'C 28105 910.392.0223 Lab • 910.392-1421 Fax 710 Bowsertown Road, Nlanteo, NC 27954 • 252.473.5702 Lab/Far Sr.+ 25-9-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS u11i-);u em,ironnlentalchemisti.con1 Town of Maysville Date of Report: Dec 04, 2019 Post Office Box 265 Customer PO #: Maysville NC 28555 Customer ID: 17020023 Attention: Report #: 2019-18771 Project ID: Sludge Ammonia Nitrogen SM 4500 NH3 C 1640 mg/kg 11/18/2019 Total Phosphorus SM 4500 P F 19400 mg/kg 11/13/2019 Mercury Sw8467471B <1.00mg/kg 11/11/2019 TCLP Metals Arsenic EPA 2007 <1.0mg/L 11/21/2019 Barium EPA 2007 <1.0mg/L 11/21/2019 Cadmium EPA 200.7 <1.0 mg/L 11/21/2019 Chromium EPA 200 7 <1.0 mg/L 11/21/2019 Lead EPA 200 7 <1.0 mg/L 11/21/2019 Selenium EPA 200 7 <1.0 mg/L 11/21/2019 Silver EPA 200 7 <1.0 mg/L 11/21/2019 Mercury EPA 2451 <0.0002mg/L 11/21/2019 Comment: Sludge residuals reported on a dry weight basis. Reviewed by: Report # 2019-18771 _ , _ 6602 Windmill Way ton ENVIRONMENTAL CHEMISTS, INC OFFICE: 0-392-02 3iIFAX9910392.44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Town of Maysville WWTP PROJECT NAME: Annual Sludge REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By:_ 00'"a/ SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae_ Other: Sample Identification Collection m E a `o a U S o` 0 a _ o �d, " E W m g g= PRESERVATION ANALYSIS REQUESTED D Time Tem i Z = p _ o = 0 Z o w o Slud e u l� /Y3ZOO C P `�� X Full TCLP/Nutrients/Metals/RCI G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received:Accepted: Rejected: Resample Re sted: Delivered By: Received By: Date: /1 Time: f—� Comments: TUR ROUND: NCDA&C? nomic Division Phone: (919) 733-2666 Website: www.nc. Craven Ag Services, Inc. lov/agronomi/ Report No. d-WO05304 Sampled: 02/22/2019 ( Received: 02/26/2019 1 Completed: 03/04/2019 Page 2 of 3 Sample Information Nutrient Measurements are given in units of ID: LFMEAS parts per million (ppm), unless utherwise Nitrooen lN) specifed. Other Results Code: CSO P K Ca Mg S Fe Mn Zn TotalN:881 17800 29500 143000 11200 3980 4850 1090 1050 Cu B Mo C Al Na CI Description: Ash, Inorganic: 603 - 110 165200 10400 5680 - Mixed orOther NH4-N-----------------_ Grower Not Pro Comments: Not Pro( NO3-N SEC pH BD CCE ALE C:N DM 'S (10 S/cm) (mS/cm) (Unitless) (lb/ d ( Y ) (�o) 1470 14.73 12.18 (tons) (Unitless) a (/o) �(� 42.0 289 74.0 : 1 74.1 Estimate of Nutrients Available for First Year (lb/ton) ApplicationMethod: i N Other Results (lb/ton) P205 K20 Ca Mg S Fe Mn Zn 1.31 60.4 52.4 211 Cu B Mo AI Na Cl Soil Incorporated 16.7 5.90 7.19 1.62 1.56 1.31 60.4 52.4 0.89 0.16 I 15.4 8.42 _ 211 16.7 5.90 7.19 1.62 1.56 13i 0.89 0.16 15.4 0.02 I G G - ilk Heavy Me Is are given in units of parts per million (ppm). Heavy Metals Estimate of Availability (lb/ton) As Cd Cr Ni Pb Se - 1.12 Application Method: As Cd Cr Ni Pb Se - 14.7 8.46 - Broadcast _ T _ 0.02 0.01 - Soil Incorporated - T - 0.02 0.01 - Agronomist's Comments: Insufficient information is available regarding the first year availability of nutrients in this material. The nutrient availability reported here is therefore the TOTAL nutrients in the material. Samples submitted prior to 2016 reported an estimated value rather than total nutrient levels. Please contact me if you have any questions. TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORTS A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES: TOWN OF BRIDGETON AND TOWN OF MAYSVILLE Orlando, FL The results set forth herein are provided by SGS North America Inc. Technical Report for Environment 1, Inc e-Hardcopy 2.0 Automated Report Town of Bridgeton Hydro Services & Consulting; Havelock, NC 440C SGS Job Number: FA70914 Sampling Date: 12/12/19 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentIinc.com �ATTN: Deedee Woolard Total number of pages in report: 13 pC eflin* rice, M.S. Test results contained within this data package meet the requirements General Manager of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063). NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV. OK, OR, UT, INA. M This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 - tel: 407-425-6700 • fax: 407-425-0707 SCiS is the :ol: aut.ioriq for authorizing c.!it, ur m„Uiti.: uun, 10 111i, d _unt il: Pir.t:t ;!allatit idea; abotit Sfl&t% Lfiau;horized modification of this report is strictly Pruhritte l can serve you betwr a!: Re%standard term; at: IMF,: N': ': en term, -ant! -.on hoot) FFIS [, S Cu.s:onierCarc a;, "0111 1 of 1 FA7091 Table of Contents Sections: Section1: Sample Summar�.................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 4 Section3: Sample Results........................................................................................................ 5 3.1: FA70914-1: SLUDGE SAMPLE.................................................................................. 6 Section4: Misc. Forms............................................................................................................ 11 4.1: Chain of Custody........................................................................................................... 12 SGS2 of 13 FA70914 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA70914 Town of Bridgeton Hydro Services & Consulting; Havelock, NC Project No: 440C Sample Collected Matrix Client Kumber Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA70914-1 12/12/19 09:37 KM 12/14/19 SO Sludge SLUDGE SAMPLE Soil samples reported on a dry weight basis unless otherniise indicated on result page. SGS_ 3 of 13 FA70914 Summary of Hits Page 1 of 1 Job Number: FA70914 Account: Environment 1, Inc Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Collected: 12/12/19 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA70914-1 SLUDGE SAMPLE 1,2-Dichloroethane 0.0106 0.010 0.0031 mg/I SW846 8260B SGS4 of 1 FA70914 Orlando, FL :., Sample Results Report of Analysis Section 3 �I SOS5of13 FA70914 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA70914-1 Date Sampled: 12/12/19 Matrix: SO - Sludge Date Received: 12/14/19 Method: SW846 8260B SW846 1311 Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 5E19799.D 10 12/23/19 16:01 SO 12/16/19 14:00 OP78166 V5E899 Run #2 Purge Volume Run #1 5.0 ml Run #2 VOA TCLP List CAS No. Compound Result HW# MCL RL 71-43-2 Benzene ND D018 0.50 0.010 78-93-3 2-Butanone (MEK) ND D035 200 0.050 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 108-90-7 Chlorobenzene ND D021 100 0.010 67-66-3 Chloroform ND D022 6.0 0.010 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 107-06-2 1,2-Dichloroetliane 0.0106 D028 0.50 0.010 75-35-4 1, 1 -Dichloroethylene ND D029 0.70 0.010 127-18-4 Tetrachloroethylene ND D039 0.70 0.010 79-01-6 Trichloroethylene ND D040 0.50 0.010 75-01-4 Vinyl Chloride ND D043 0.20 0.010 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101% 83-118% 17060-07-0 1,2-Dichloroethane-D4 109% 79-125% 2037-26-5 Toluene-D8 105% 85-112% 460-00-4 4-Bromofluorobenzene 111% 83-118% TCLP Leachate method SW846 1311 MDL Units Q 0.0031 mg/l 0.020 mg/l 0,0036 ing/l 0.0020 mg/1 0.0030 mg/l 0.0026 mg/1 0.0031 mg/l 0.0032 mg/I 0.0022 mg/1 0.0035 mg/l 0.0041 mg/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound SG6of13 FA70914 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA70914-1 Date Sampled: 12/12/19 Matrix: SO - Sludge Date Received: 12/14/19 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X068591.1) 1 12/19/19 20:27 MV 12/19/19 07:47 OP78217 SX2818 Run #2 Initial Volume Final Volume :un #1 100 ml 1.0 ml :un #2 ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Methylphenol ND D023 200 0.050 0.0056 mg/1 3&4-Methylphenol ND D024 200 0.050 0.0098 mg/1 87-86-5 Pentachlorophenol ND D037 100 0.25 0.050 mg/1 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.050 0.0074 mg/1 88-06-2 2,4,6-Trichlorophenol ND D042 2.0 0.050 0.0075 mg/1 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.050 0.0050 mg/1 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.050 0.0081 mg/l 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/1 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 0.0050 mg/I 67-72-1 Hexachloroethane ND D034 3.0 0.050 0.016 mg/I 98-95-3 Nitrobenzene ND D036 2.0 0.050 0.0093 mg/I 110-86-1 Pyridine ND D038 5.0 0.10 0,020 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluoroplienol 36% 14-67% 4165-62-2 Phenol-d5 26% 10-50% 118-79-6 2,4,6-Tribromophenol 82% 33-118% 4165-60-0 Nitrobenzene-d5 78% 42-108% 321-60-8 2-Fluorobiphenyl 80% 40-106% 1718-51-0 Terphenyl-dl4 84% 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound &_A,%S_ 7 of 13 FA74914 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA70914-1 Date Sampled: 12/12/19 Matrix: SO - Sludge Date Received: 12/14/19 Method: SW846 8151A SW846 3510C Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC065678.1) 1 12/23/19 18:37 RS 12/21/19 11:10 OP78260 GCC1573 Run #2 Initial Volume Final Volume Run #1 10.0 ml 5.0 ml Run #2 Herbicide TCLP List CAS No. Compound Result HW# MCL RL 94-75-7 2,4-D a ND D016 10 0.050 93-72-1 2,4,5-TP (Silvex) a ND D017 1.0 0.0050 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 60% 39-135% (a) Associated BS outside of control limits high, sample was ND. TCLP Leachate method SW846 1311 MDL Units Q 0.017 mg/l 0.0013 mg/I ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Ots8of13 FA70414 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA70914-1 Date Sampled: 12/12/19 Matrix: SO - Sludge Date Received: 12/14/19 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 KK96255.D 1 12/23/19 14:09 WH 12/21/19 12:45 OP78259 GKK3070 Run #2 Initial Volume Final Volume .un #1 100 ml 5.0 ml .un #2 Pesticide TCLP List CAS No. Compotind Result HW# MCL RL TCLP Leachate method SW846 1311 MDL Units Q 58-89-9 gamma-BHC (Lindane) a ND D013 0.40 0.00010 0.000022 mg/1 12789-03-6 Chlordane b ND D020 0.030 0.0010 0,00038 mg/l 72-20-8 Endrin b ND D012 0.020 0.00020 0.000021 mg/l 76-44-8 Heptachlor b ND D031 0.0080 0.00010 0.000026 mg/l 1024-57-3 Heptachlor epoxide a ND D031 0.0080 0.00010 0.000020 mg/l 72-43-5 Methoxychlor ND D014 10 0.00020 0.000050 mg/l 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09 8 Tetrachloro-m-xylene 125% 42-127% 2051-24-3 Decachlorobiphenyl 115% 27-127% (a) Associated BS outside of control limits high, sample was ND. Associated CCV outside of control limits high. sample was ND. (b) Associated CCV outside of control limits high, sample was ND. (c) Associated BS outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9of13 SGS FA7091: SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA70914-1 Date Sampled: 12/12/19 Matrix: SO - Sludge Date Received: 12/14/19 Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Page 1 of 1 Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/l 1 12/18/19 12/20/19 LM SW846 6010D 2 SW846 3010A 3 Barium < 2.0 D005 100 2.0 mg/1 1 12/18/19 12/20/19 LM SW846 6010D 2 SW846 3010A 3 Cadmium < 0.050 D006 1.0 0.050 mg/l 1 12/18/19 12/20/19 LM SW846 6010D 2 SW846 3010A 3 Chromium < 0.10 D007 5.0 0.10 mg/l 1 12/18/19 12/20/19 LM SW846 6010D 2 SW946 3010A 3 Lead < 0.050 D008 5.0 0.050 mg/l 1 12/18/19 12/20/19 LM SW846 6010D'- SW846 3010A 3 Mercury < 0.0050 D009 0.20 0.0050 mg/l 1 12/19/19 12/19/19 1c SW846 7470A 1 SW846 7470A 4 Selenium < 0.10 D010 1.0 0.10 mg/l 1 12/18/19 12/20/19 LM SW846 6010D 2 SW846 3010A 3 Silver <0.10 D011 5.0 0.10 mg/i 1 12/18/19 12/20/19 LM SW846 6010D 2 SW846 3010A 3 (1) Instrument QC Batch: MA16416 (2) Instrument QC Batch: MA16420 (3) Prep QC Batch: MP36569 (4) Prep QC Batch: MP36576 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) SGS10 of 13 FA70914 Orlando, FL Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 C SAS_ 11 of 13 FA70914 Environment I, Inc. P.O. Box 7085,114 Oakmont Dr. Greenville, NC 27858 environmentl inc.com DiSI1VFECTION Phone (252) 756-6208 • Fax (252) 756-0633 ry CHLORINE CLIENT: 440 C Week:1 �•UV TOWN OF BRIDGETON NONE HYDRO SERVICES & CONSULTING MR. KEVIN MULLINEAUX P.O. BOX 317 HAVELOCK NC 23532' o CHAIN OF CUSTODY RECORD E G (252) 723-0101 w � °i} COLLECTION ES SA�VPIELOCATION DATE I TIME Sludge Sample �j .2— -?.' 37 3 WWI FORM eS PLEASE READ Irl-siruetlons for 1 giORNE NE1rWIZEDATC0.- tL;i Km+ pH CHECK PB) CDNTAPERTYPE Pr- CHEMY,ALPREGEFiVX DN A•NGNE D•NACH B•HNO, E•HCL C•H1,SO, F- ZINC ACEfATFJNAOH 0 • "JATh°.ASt1LFATE a QASSIFICATION WASTEVlATER �PCES) ORI=WWATER ' D1Vfl�'I! SOLD WASTE 5ECT 01 GRAIN OF CUSTODY (SEAL) MIARJTAINED DURIN IENTlDELIVERY Y N SAMPLES COLLECTED by- ft. � � �, SAIAKES P,ECSVED V LABITT f CATErA+t COMMEM: DATEFM r 2 zs�) U. C • 12/3 7-30' 1 0 D FInh1E 01 1 Iffy/9 ?b� Sampler must place a "C" for composite samp10 or a "G" for on he reverse silo. Gab sample in the blocks above ter each parameter rvGue5lad N U 3760,65 1C I A70914: Chain of Custody Page I of 2 sUa 92 of 1, FA7o91, SGS Sample Receipt Summary Job Number: FA70914 Client: ENVIRONMENT 1, INC. Project: TOWN OF BRIDGETON Date / Time Received: 12/14/2019 9.00.00 AM Delivery Method: FED EX Airbill ids: Therm ID: IR 1; Therm CF: -0.8. # of Coolers: 1 Cooler Temps (Raw Measured) °C: Cooler 1: (2.3); Cooler Temps (Corrected) °C: Cooler 1: (1.5); Cooler Information Y or N Sam0e Information Y or bL NIA 1. Custody Seals Present 2 Cl 1. Sample labels present on bottles ❑ 2. Custody Seals Intact ❑ 2 Samples preserved property �r ❑ 3 Temp criteria achieved ❑ 3. Sufficient volumelcontainers recvd for analysis: ;� ❑ 4. Cooler temp verification IR Guri 4. Condition of sample Intact 5 Cooler media Ice a 5. Sample recvd within HT Q ❑ 6. Dates/Tmes/IDs on COG match Sample Label Trip Blank Information Y or N N/A 7. VOCs have headspace ❑ ❑ CYl 1. Trip Blank present / cooler ❑ Ri ❑ e. Bottles received for unspecified tests ❑• 2 Trip Blank listed on COG ❑ ❑ 9. Compositing instructions clear ❑ ❑ E 10 Voa Soil Kits/Jars received past 48hrs? 1 17 9 W or S NIA 11. °k Solids Jar received? ❑ ❑ 3. Type Of TB Received ❑ ❑ Q 12. Residual Chlorine Present? ❑ ❑ Misc. Information Number of Encores. 25-Gram 5-Gram Number of 5035 Field Kits, Number of Lab Filtered Metals Test Strip Lot #s: pH 0.3 230315 pH 10-12 219813A Other: (Specify) _ Residual Chlorine Test Strip Lot # Comments s%1001 Technician: TRINITYb1 Date 12/14/2019 9.00 00 A Rev. Date 05,74117 Reviewer Date FA70914: Chain of Custody Page 2 of 2 SGS 13of1 FA7091 r7 . -, 0"441 ANALYTICAL & CONSULTING CHEMISTS Town of Maysville Post Office Box 265 Maysville Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910..',92.4424 Fax 710 Bowsertown [goad, Nlanteo, NC 27954 • 252.473.5702 Lab/Fax 23-9-A Wilmington Highway, Jacksonville, NC 2S5-10 • 910.347.5843 Lab/Fax hillo!a em ironnlentalchenlists.com Date of Report: Dec 04, 2019 Customer PO #: NC 28555 Customer ID: 17020023 Report #: 2019-18771 Project ID: Sludge Lab ID Sample ID: 19-47778 Site: Sludge Test Chlordane (TCLP) Endrin (TCLP) Heptachlor (TCLP) Heptachlor epoxide (TCLP) Lindane (TCLP) Methoxychlor (TCLP) Toxaphene (TCLP) 1,4-Dichlorobenzene (TCLP) 2,4,5-Trichlorophenol (TCLP) 2,4,6-Trichlorophenol (TCLP) 2,4-Dinitrotoluene (TCLP) Cresol (TCLP) Hexachloro-1,3-butadiene (TCLP) Hexachlorobenzene (TCLP) Hexachloroethane (TCLP) m + p-Cresol (TCLP) Nitrobenzene (TCLP) o-Cresol (TCLP) Pentachlorophenol (TCLP) Pyridine (TCLP) 2,4,5-TP (TCLP) 2,4-D (TCLP) 1,1-Dichloroethylene (TCLP) 1,2-Dichloroethane (TCLP) Benzene (TCLP) Carbon Tetrachloride (TCLP) Collect Date/Time Matrix 11/6/2019 2:30 PM Solid/Sludge Method SW 846 Method 8081 B/3510 SW 846 Method 8081 B/3510 SW 846 Method 8081B/3510 SW 846 Method 8081 B13510 SW 846 Method B0818/3510 SW 846 Method 8081 B/3510 SW 846 Method 8081B/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW 846 method 8270/3510 SW846 Method 8151A SW846 Method 8151A SW846 Method 8260/5030 SW846 Method 8260/5030 SW846 Method 8260/5030 SW846 Method 8260/5030 Results Sampled by boomer Date Analyzed <0.02 mg/L 11/20/2019 <0.0005 mg/L 11/20/2019 <0.0005 mg/L 11/20/2019 <0.0005 mg/L 11/20/2019 <0.0005 mg/L 11/20/2019 <0.0005 mg/L 11/20/2019 <0.05 mg/L 11/20/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.250 mg/L 11/19/2019 <0.050 mg/L 11/19/2019 <0.003 mg/L 11/20/2019 <0.003 mg/L 11/20/2019 <0.01 mg/L 11/19/2019 <0.01 mg/L 11/19/2019 <0.01 mg/L 11/19/2019 <0.01 mg/L 11/19/2019 Reoort #:. 2019.18771 Environmental Chemists, Inc. envirochem 6602 Windmill WaY, Wilminl;ton, NC 25405 • 910.392.0223 Lab • 910.392.442.4 Fax 710 Bowserto%,vn Road, Manteo, NC 27954 • 2-2.=473.5702 Lab/Fax si+ 255-A Wilmington Highway, Jacksonville, `1C 285-40 • 910.3.47.58 43 1_ab/Fax ANALYTICAL & CONSULTING CHEMISTS inlo it em ironmentalchemists.com Town of Maysville Date of Report: Dec 04, 2019 Post Office Box 265 Customer PO #: Maysville NC 28555 Customer ID: 17020023 Attention: Report #: 2019-18771 Project ID: Sludge Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Chloroform (TCLP) SW846 Method 8260/5030 <0 01 mg/L 11/19/2019 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 11/19/2019 Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 11/19/2019 RCI Cyanide EPA 3354 Reporting limit elevated due to matrix interference. <0.05mg/kg 11/15/2019 Sulfide SM 4500 S D 0.22 mg/kg 11 /08/2019 Ignitability SW846 method 1010 >195 OF 11/15/2019 pH SW 846 Method 9045D 6.74 units 11/13/2019 Sludge Residuals Aluminum EPA 2007 5110mg/kg 11/18/2019 Arsenic EPA 200 7 <13.8 mg/kg 11/18/2019 Cadmium EPA 2007 <13.8mg/kg 11/18/2019 Calcium EPA 200 7 38900 mg/kg 11/18/2019 Chromium EPA 200 7 <13.8 mg/kg 11/18/2019 Copper EPA 200 7 403 mg/kg 11/18/2019 Lead EPA 200 7 18.2 mg/kg 11/18/2019 Magnesium EPA 200 7 2910 mg/kg 11/18/2019 Molybdenum EPA 2007 <13.8mg/kg 11/18/2019 Nickel EPA 200 7 14.5 mg/kg 11/18/2019 Potassium EPA 2007 3770mg/kg 11/19/2019 Selenium EPA 200 7 <13.8 mg/kg 11/18/2019 Sodium EPA 200 7 7570 mg/kg 11/18/2019 Zinc EPA 200 7 871 mg/kg 11/18/2019 Total Kjeldahl Nitrogen (TKN) EPA 351.2 28300 mg/kg 11/18/2019 Nitrate+Nitrite-Nitrogen EPA353.2 126 mg/kg 11/18/2019 Total Solids (%) SM 2540 B 1.40 % 11/11/2019 Report # : 2019-18771 Environmental Chemists, Inc. L�nvirocheM 6602 Windmill Wav, Wilmington, INK 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Botesertuwt1 Road, i\lanteo, NC 279-94 • 252.473.5702 Lab/Fax 255-A Wilmington Ftighwat', Jacksonville, NC 28540 • 910.347.5843 I_ab/Fax ANALYTICAL & CONSULTING CHEMISTS infouemiroil mentalchemists.com Town of Maysville Date of Report: Dec 04, 2019 Post Office Box 265 Customer PO #: Maysville NC 28555 Customer ID: 17020023 Attention: Report #: 2019-18771 Project ID: Sludge Ammonia Nitrogen SM4500 NH3 C 1640 mg/kg 11/18/2019 Total Phosphorus SM 4500 P F 19400 mg/kg 11 /13/2019 Mercury SW8467471B <1.00mg/kg 11/11/2019 TCLP Metals Arsenic EPA 200 7 <1.0 mg/L 11/21/2019 Barium EPA 2007 <1.0 mg/L 11/21/2019 Cadmium EPA 2007 <1.0 mg/L 11/21/2019 Chromium EPA 200 7 < 1.0 mg/L 11/21/2019 Lead EPA 200 7 <1.0 mg/L 11/21/2019 Selenium EPA 200 7 <1.0 mg/L 11/21/2019 Silver EPA 200 7 <1.0 mg/L 11/21/2019 Mercury EPA 245.1 <0.0002 mg/L 11/21/2019 Comment: Sludge residuals reported on a dry weight basis. Reviewed by: a Q \J�j Report #:: 2019-18771 Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com Client: Town of Maysville WWTP PROJECT NAME: Annual Sludge REPORT NO: / - /V-Jov ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: email: Sampled B a+MC/ SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other: Sample Identification p Collection E m a o E c U 9 `� C 0 o 0. ` o' U M m g Z PRESERVATION ANALYSIS REQUESTED D,atja Time Tem z z 0 = 0 x zo z _o w O Sludge a lP C P `{� X Full TCLP/Nutrients/Metals/RCI G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: 5 C Accepted: Delivered By: R Comments: Time: S'� PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The Towns of Bridgeton and Maysville meet pathogen reduction and vector attraction reduction requirements through lime stabilization. Craven Ag Services, Inc. performed the lime stabilizations. This applications were incorporated that same day. The forms for these facilities are marked appropriately. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Craven Ag Services, Inc. WQ Permit Number: WQ0037637 'V 'WTP Name: Town of Maysville WWTP NPDES Number: NCO021482 .onitoringPeriod: From 1/1/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerfnrmPd- Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) LJ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathocengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic f l Beta Ray t...J Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density ❑ I Alt. (2) Process to Significantly Reduce Pathogens �1 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ,?l Air Drying Cl Coniposting ❑ Aerobic Digestion [J Anaerobic Digestion v If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Densit r " } um er o 1 Excee- Frequency ofAnalysis Sample Type n a jca Tech - ninm- Minimuni Geo. Mean Maximum Units Fecal Coliform 2 x 10 to die 6th power per gram of total solids ivl N CFU 1000 mpu per gram of total solid (dry weight) monella bacteria (in lieu of fecal coliform) t. 3 MPN per 4 grams total solid (dry I wei ht) vector Attraction Reduction (15A N At 02T .1107) - Please Indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ jAlt. 4 (Spec. O, uptake) U Alt. 5 (14-Day Aerobic) D Alt. 6 (Alk. Stabilization El Alt 7 (Drying -Stable) ❑ 1 Alt. 8 (Drying -Unstable) 0 Alt. 9 (Injection) (..) Alt. 10 (Incorporation) 1J No vector attraction reduction alternatives were erformed i_l CERTIFICATION STATEMENT (please check the appropriate statement) 1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the .I vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) e under my airection ana su ce with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. John W. Dunham Mr. John W. Dunham Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 0 ,1p - ) 4-�o -jZ) Lg t9 a of Preparer* Date ' n ture of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1 2/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Craven Ag Services, Inc. WQ Permit Number: WQ0037637 WIYVTP Name: Town of Bridgeton WWTP NPDES Number: NCO074837 Monitoring Period: From 1/l/2019 To 12/31/2019 thogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ? � A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs 1J If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo lnilic Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: TA—It(l) Fecal Density ❑ I Alt. (2) Process to Significantly Reduce Pathogens E3 If applicable to alternative per (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization F1 Air Drying ❑ L Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density Number o Frequency Sample Analytical in Sludge Excee- of Anal Tech- g Minimu Geo. Mean Maximu Units ysis Type Fecal Coliform ilmonella bacteria (in lieu of fecal 2 x 10 to the MPl` 6th power per gram of total solids CFU ivvu mpn per gram of total solid (dry b1PN per 4 grams total solid (dry vector Attraction Reduction (ISA NCAC WT .111171 - PIPasP inrl;ratP altPrnatCvP r%avrnvM A. Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ElAlt. 4 (Spec. O, uptake) El Alt. 5 (14-Day Aerobic) [IAlt. 6 (Alk. StabilizationEl Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) Cl Alt. 9 (Injection) J Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ cJ- x it iL m 11V14 a 1 A 1 r ivi it i (please cnecK the appropriate statement) ;J " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the 1:1 vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. John W. Dunham Preparer Name and Title (type or print) —,i a ure of Preparer* Date Mr. John W. Dunham Land Applier Name and Title (if applicable)(type or print) S ature of Land Applier (if applicable) Date reparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DFNR FORM PVRF 02T (12/2006) PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The Towns of Bridgeton and Maysville meet pathogen reduction and vector attraction reduction requirements through lime stabilization. Craven Ag Services, Inc. performed the lime stabilizations. These applications were incorporated that same day. Documentation of these activities are found in the following section. -CRAVEN A_G_SERVICES INC. Alkaline Stabilization Of Solids Analysis Bench Sheet Facility Name: S 'c P.O. # Batch Size ( gallons) Lbs. or Gallons Used: O c ! c - —Material used for Stabilization:r✓lae�✓�l :. ��, Initial ph 2 Hour pH 24 Hour pH DATE pH Temp C Corr Fa + Corr. pH Time pH Temp C Corr Fa + Corr H ,Time p pH Temp C Corr Fa + lCorr pH jTime Intial - �- ' 30 L ' 70 I 0.30 'G I,L a G ,�►, p 4?, 03 :1,'0 IE3 CRAVEN AG SERVICES INC, 'Alkatine, stabifizationOf • • AAM ..�,M� ,. "fir M��� m W�v ms �.. .. 1-m-........ m. m_ CRAVEN AG SERVICES INC. A aline Stabilization Of Solids Analysis Bench Sheet Facility Name • — - -- Batch —Size—(,- — ' - - -- -- lbs. or Gallons Used: �{ �U — Material used for Stabilization: &Idfy,7- e Initial ph 2 Hour H - p I 24 Hour pH DATE pH Temp C Icorr Fa + jCorr. pH p pH Temp C ICorr Fa + jCorr pH Time pH Temp C ICorr Fa + Corr pH Time Intial ,%_'gyp . �/ h �<<Ii"'Pavi -- - - - - - -- - 4 r -- --_ A G CRAVEN AG SERVICES INC. Alkaline Stabilization Of Solids Analysis Bench Sheet - Facility Name • .� P.O. # Batch Sae ( gallons) Lbs. or Gallons Used: a, yao /,4 Material used for Stabilization: Initial ph 2 Hour pH 24 Hour pH DATE pH JTempC �CorrFa+ Corr. H p Time IpH Temp C Corr Fa + Corr pH Time pH Temp C Corr Fa + Corr pH Time Intia I 81 a . I .66 l�.�y D . r z 1349 a; �ZµA T . oG 9 /D:as ZAQ a .� o , 2 .a / p !ro /3 e: 4 .00 2 G 3pi9 ,,n m m — . 3 �. . o 'l • 39 : e-,- ..rU 3 4• .� .09 lo.� va� t 'S'3 . • Q �,hil i240 S. 0 1 Dad . s, fS .3 / Wti RIM ILI d d 1C111- 9 d o 5 S Tj d i d l M N m oo N (y gj m CD ti r m r b T � 1 t CRAVEN AtAG SERVICES INC. Alkaline Stabilization Of Solids Analysis Bench Sheet Name: i Batch Size (gallons) : YZl atrm Initial ph Lbs. or Gallons Used: A, YwA �- 2 Hour pH -DATE ' pH Temp C 1(;orrFa+ Corr. pH Time LH Temp C t !J-Ys/f 4,77 1e.1 - .!b j /a ct.W tl�! le �( 7.sY i �. �• ., '. � '1 tTj� 12•y3 1�• t -Y•� P.O. # Material used for Stabilization: *61.4 24 Hour pH P` k IpH pat, Corr Fa + Corr pH Time �TempC1CorrFa+jCorrpH Time intia I —Y 13.,L p'y — lost /00 Q l f'j�r t3•; /t- _ . y1. � !e to I?pl3 — •?-� t . ! pf. j° 11.0 / a.s — • 39 ry ! 1) �4•t , -!8' i- 13Ye /z.64 /7- ?/t t� PJl Z.4s /I. ,z•s -34 , 34 34 l -� 1 _ LG � raf �.ay l� tia0 �p � /��� npQ -7. l d �197 /2.7C /7• s- .7-� r .3 �� 4.71-144 -t 8 .; 3 t7 f ty.e /z. �y 1x,7 /7• t j.f� --7•l "•11 ,�7 ,3£s' tc ,o /a 'f is.�o t?.bz �z• SOIL ANALYSIS REPORTS The Town of Bridgeton and Maysville met pathogen reduction and vector attraction reduction requirements through lime stabilization. The soil pH will continue to be raised through the continued application of lime stabilized biosolids to these application fields. In addition, application of mixed ash was applied to Field 3-2. WaYP• Ao�nt.� NALYTICAL Client : Craven Ag Services, Inc. Mr. Billy Durham 2115 Hwy 85 W Newbern NC 28562 Lab Number: 33733 Test Method Results Soil pH 11 7.6 Buffer pH Phos horus(P) M3 412 ppm Potassium K) 1V13 42 ppm Calcium c a I M3 1523 ppm Ma nesium (M) N13 44 ppm Sulfur (S) M3 13 ppr, Boron (8) M3 0.4 ppm Co er Cu) M3 2 9 ppm Iron (Fe 1%13 199 ppm Manganese (Mn) M3 8 ppm Zinc (Zn) M3 9.4 ppm Sodium Na N13 32 ppm Soluble Salts Organic Matter LOI 1 .4 % ENR 72 Nitrate Nitrogen 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213,2440 "Every acre... Every years wwW.Waypointanalytical.com Grower: Report No: Craven Ag Services Inc. Field Id : Cust No: Date Printed: Date Received PO: Page: Sample Id: R3-1 SOIL FERTILITY GUIDELINES Crop : Rye_ Yield Goal : 60 bu/acre Rec Units: (Ibs) LIME (tons) N pz 05 K vO Mg.,. S B SOIL ANALYSIS 18-311-0804 24170 11/12/2018 11/07/2018 1 of 6 Exchange Capacity 8.2 meq/100g % sat meq K 1.3 0.1 Ca 92.9 7.6 Mg 4.5 0.4 H 0.0 0.0 Na 1.7 0.1 Ratio: LB/ACRE u M11 cn - Fe 0 0 86 0 89 18 13 05 0 4 0 tCr p : M(tlet Pasture Yield Goal : 3 tons/acre Rec Units: LB/ACRE 0 0 90 0 80 18 10 0.5 0 4 0 Comments Rye For small grains apply 20-40 lbs N/acre in the fall and the remainder as a top dressing before jointing. For high yields of small grains or for small grains on wet soils, a split application of spring N may be benefic al. When small grain is grazed, increase the N fertilization rate by 60 lbs N/Acre. Apply 1/2 in the fall and the rest in mid or late winter. On small grains apply recommended P and K before or at planting. Millet Pasture • When millet or sorghum sudans are harvested for silage or hay apply 40 lbs N/Acre at seeding and 60 lbs. N/Acre after establishment. Then apply 60 lbs. N/Acre after each harvest except the last. • When millets or sorghum sudans are used for grazing apply 40 to 60 lbs N/Acre at seeding and 60 lbs N/Acre per month during the growing season. M3 - Mehiich 3 BPH - Lime Index LOI - Loss On Ignition 1.1 - `Nater off Analysis prepared by Waypoint Analytical Tennessee. Inc. 9-270( ort No: 104365 punt No: 4365 Waypoint ANALYTICAL isor: Harvey Fertilizer Co - Kinston Branch Client: Alan Roach Robbie Whitfield 1321 Hwy. 258 N. Kinston NC 28504 2850 Daisy Lane, Wilson, NC Main 252-206-1721 ° Fax 2S2-206-997 www.waypointanalytical.com Farm: D. Kylmen Submitted By: Harvey Fertilizer Co - Kinston Branch Date Received: 09/27/2019 Date of Report: 09/30/2019 No Field ID Sample ID Soll Class HM% WN pH Ac P-1 K-1 S-1 Mn4 Zn-1 Zn-Al Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO: N 142 DK 02A MIN 2.5 1.3 6.0 2.1 121 87 10 50 155 155 95 6.3 66 48 11 0.8 0 op Recommendations: Soybeans Rec Uom lb/acre Lime (Vacre) 0.0 N 0 P205 0 K20 0 S 20 Mn 0 Mn-AI 40 Zn 0 Cu 0 B 0 Mg 0 Last Crop 143 DK 02B MIN 2.6 1.3 5.9 2.3 116 67 15 44 160 160 105 6.2 63 47 10 0.6 0 op Recommendations: Soybeans Rec Uom lb/acre Lime (Vacre) 0.3 N 0 P205 0 K20 20 S 20 Mn 0 Mn-AI 38 Zn 0 Cu 0 B 0 Mg 0 Last Crop 144 3 iZ DK 02C >f--ORT' MIN 3.0 1.2 5.7 2.1 140 51 15 38 128 128 75 6.9 69 55 9 0.6 0 op Recommendations: Soybeans Aw 3' 7- Rec Uom lb/acre Lime (t(acre) 0.7 N 0 P205 0 K20 40 S 20 Mn 0 Mn-AI 37 Zn 0 Cu 0 B 0 Mg 0 Last Crop 145 DK 02D MIN 2.2 1.4 6.1 1.9 107 39 6 50 128 128 80 7.3 74 61 10 0.6 0 op Recommendations: Soybeans Rec Uom lb/acre Lime (t/acre) 0.0 N 0 P205 0 K20 60 S 20 Mn 0 Mn-AI 38 Zn 0 Cu 0 B 0 Mg 0 Last Crop 146 DK 03A MIN 3.0 1.2 5.6 1.7 120 46 21 50 200 200 80 6.8 75 60 11 0.6 0 op Recommendations: Soybeans Rec Uom lb/acre Lime (Vacre) 0.7 N 0 P205 0 K20 40 S 20 Mn 0 Mn-Al 46 Zn 0 Cu 0 B 0 Mg 0 Last Crop 147 DK 036 M-0 3.8 1.1 5.7 2.2 101 57 2 44 183 228 95 7.9 73 58 11 0.6 0 -op Recommendations: Soybeans Rec Uom lb/acre Lime (t/acre) 0.0 N 0 P205 0 K20 30 S 20 Mn 0 Mn-AI 41 Zn 0 Cu 0 B 0 Mg 0 Last Crop 1148 DK 03C MIN 2.5 1.4 5.9 1.4 123 87 8 50 123 123 110 7.0 80 64 9 0.7 0 -op Recommendations: Soybeans Rec Uom lb/acre Lime (Vacre) 0.0 N 0 P205 0 K20 0 S 20 Mn 0 Mn-Al 42 Zn 0 Cu 0 B .0 Mg 0 Last Crop !150 DK 03D M-0 4.2 0.9 5.4 2.7 81 47 21 56 188 234 80 8.5 68 51 9 4.9 0.4 op Recommendations: Soybeans Rec Uom lb/acre Lime (Nacre) 0.0 N 0 P205 0 K20 40 S 20 Mn 0 Mn-Al 53 Zn 0 Cu 0 B 0 Mg 0 Last Crop t result units = CEC and Na in meq/100cm3; NO3 N in rng/dm3; WN in g/cm3 th Carolina Division of Water duality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by. Waypoinl Analytical Carolina, Inc. • T 1 t ort No: 19-270-0521 :count No: 04365 Waypoi nt,u 2850 Daisy Lane, WilsNNMain 252-206-1721 a Fax 2 ANALYTICAL www.waypointanalytical.com 9visor: Harvey Fertilizer Co - Kinston Branch Robbie Whitfield 1321 Hwy. 258 N. Kinston NC 28504 mil. A#- Ol.,rd rn Client: Alan Roach Farm: D. Kylmen Submitted By: Harvey Fertilizer Co - Kinston Date Received: 09/27/2019 Date of Report: 09/30/2019 �- •-� • •a•� •� .idrurav Im son crass HM% W/V pH Ac P-1 K-1 S-1 Mn4 Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO: N 12142 DK 02A MIN 2.5 1.3 6.0 2.1 121 87 10 50 155 155 95 6.3 66 48 11 0.8 0 .'rop Recommendations: I- Soybeans Rec Uom lb/acre Lime (Uacre) 0.0 N 0 P205 0 K20 0 S 20 Mn 0 Mn-AI 40 Zn 0 Cu 0 B 0 Mg 0 Last Crop 12143 DK 02B MIN 2.6 1.3 5.9 ' 2.3 116 67 15 44 160 160 105 6.2 63 47 10 0.6 0 ^rop Recommendations: I- Soybeans Rec Uom lb/acre Lime acre 0.3 N 0 P205 0 K20 20 S 20 Mn 0 Mn-Al 38 Zn 0 Cu 0 B 0 Mg 0 Last Crop 12144 DK 02C MIN 3.0 1.2 X.7 11 2.1 140 51 15 38 128 128 75 6.9 69 55 9 0.6 0 Crop Recommendations: 1- Soybeans Rec Uom lb/acre Lime ( acre) 7 N 0 P205 0 K20 40 S 20 Mn 0 Mn-At 37 Zn 0 Cu 0 B 0 Mg 0 Last Crop 12145 DK 02D MIN 2.2 1.4 6.1 1.9 107 39 6 50 128 128 80 7.3 74 61 10 0.6 0 Crop Recommendations: 1- Soybeans Rec Uom lb/acre Lime (Uacre) 0.0 N 0 P205 0 K20 60 S 20 Mn 0 Mn-AI 38 Zn 0 Cu 0 B 0 Mg 0 Last Crop 12146 DK 03A - MIN 3.0 1.2 5.6 1.7 120 46 21 50 200 200 80 6.8 75 60 11 0.6 0 Crop Recommendations: 1- Soybeans Rec Uom lb/acre Lime acre) t.7l N 0 P205 0 K20 40 S 20 Mn 0 Mil -Al 46 Zn 0 Cu 0 B 0 Mg 0 Last Crop 12147 DK 03B M-0 3.8 1.1 5.7 2.2 101 57 2 44 183 228 95 7.9 73 58 11 0.6 0 Crop Recommendations: 1- Soybeans Rec Uom lb/acre Lime (Uacre) 0.0 N 0 P205 0 K20 30 S 20 Mn 0 Mn-At 41 Zn 0 Cu 0 B 0 Mg 0 Last Crop 12148 DK 03C MIN 2.5 1.4 5.9 1.4 123 87 8 50 123 123 110 7.0 80 64 9 0.7 0 Crop Recommendations: 1- Soybeans Rec Uom lb/acre Lime (Uacre) 0.0 N 0 P205 0 K20 0 S 20 Mn 0 Mn-Al 42 Zn 0 Cu 0 B 0 Mg 0 Last Crop 12150 DK 03D M-0 4.2 0.9 5.4 2.7 81 47 21 56 188 234 • 80 8.5 68 51 9 4.9 0.4 Crop Recommendations: 1- Soybeans Rec Uom Iblacre Lime (Uacre) 0.0 N 0 P205 0 K20 40 S 20 Mn 0 Mn-AI 53 Zn 0 Cu 0 B 0 Mg 0 Last Crop 3st result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/v in g/cm3 orth Carolina Division of Water Quality Certification 0257, Analysis and fertility recommendations shown on this report are performed In accordance within NCDA guldelinus, Analysis proparod by: W aypoini Analytical Carolina, Inc 2019 APPLICATION SUMMARY TABLE CRAVEN AG SERVICES, INC LAND APPLICATION PROGRAM PERMIT NO. WQ0037637 2019 APPLICATION SUMMARY ........................ ...................... ............... . ...................... ...... .. ............ : : ............. .............. .........Site:... ...... .......................... ........ . . ....... ............... . .... . -, -, -'. -, -'. -, -, -, -'. -'.. ... . . ....... ................ . ....... ......... .................. ... .......... j 41 ..... ............. - - ........................... ...... . . . . . .................. ............. ........................................... ....... .. . .............................................. .......... ..................... .............................................. .... . ...... ................................... ............... ..... * ... ........ .... .. . . . S6.4�v� ... ..... ...... ............. ...... ....... ...... ........... . .... Allen Roach 3 -_ 1 6.6 Jul-19 42,000 0.37 2.45 Millet Maysville 7.88 Jul-19 18,000 0.02 0.15 Millet Bridgeton 2 14.6 1 Mar- 19 18,500 0.01 0.15 Corn (Grain) Bridgeton 3.57 Nov-19 42,000 0.17 2.45 Rye Maysville 3 1 6.1 Oct- 19 21,000 0.03 0.18 Wheat (Grain) Bridgeton 0.79 Number of Fields Applied to: 3 2730 Town of Maysville Town of Bridgeton Pruite Health Sea Level C&P Enterprises .......... .... ................. ....... :::Gallons:;:...... ................ ..... ............:::...::Metric................ .. * .......... ..... .. .. ... ........................... . .... ........... .... ............................ .............................. ......... . ...... ............ ............ ... .... ...... .............................. 84,000 4.90 4.46 15 57,500 0.48 0.44 5 0 0.00 1 0.00 0.73 0 0.00 1 0.00 1 Permit Limit 21.73 Branch Residuals Soils, LLC Confidential 2/19/2020 Page 1 2019 APPLICATION CONDITION SUMMARIES Town of Bridgeton Havelock, North Carolina Carven Ag Services WQ0037637 Annual 2019 Bridgeton WWTP Farmer: Allen Roach Acres: 6.6 Site/Tract: 3 Application Method: Incorporated Field: 1 Percent Solids: 0.20 Residual Report No.: BEI-440A Crop: Millett Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 7/3/19 1 18,000.0 Dry Hot 0.00 Total Gallons 18,000.0 Town of Bridgeton Havelock, North Carolina Carven Ag Services WQ0037637 Annual 2019 Bridgeton WWTP Farmer: Allen Roach Acres: 14.6 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 0.20 Residual Report No.: BEI-440A Crop: Corn (Grain) Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 3/13/19 2 18,500.0 Dry Warm 0.00 Total Gallons 18,500.0 Town of Bridgeton Havelock, North Carolina Carven Ag Services WQ0037637 Annual 2019 Bridgeton WWTP Farmer: Allen Roach Acres: 6.1 Site/Tract: 3 Application Method: Incorporated Field: 3 Percent Solids: 0.20 Residual Report No.: BEI-440A Crop: wheat (Grain) Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 10/24/19 3 21,000.0 Dry Warm 0.00 Total Gallons 21,000.0 Town of Maysville Maysville, North Carolina Carven Ag Services WQ0037637 Annual 2019 Maysville WWTP Farmer: Allen Roach Acres: 6.6 Site/Tract: 3 Application Method: Incorporated Field: 1 Percent Solids: 1.40 Residual Report No.: 19-47778 Crop: Soybeans Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 7/1/19 1 42,000.0 Dry Hot 0.00 Total Gallons 42,000.0 Town of Maysville Maysville, North Carolina Carven Ag Services WQ0037637 Annual 2019 Maysville WWTP Farmer: Allen Roach Acres: 14.6 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 1.40 Residual Report No.: 19-47778 Crop: Rye Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 11/14/19 2 42,000.0 Dry Cool 0.00 Total Gallons 42,000.0