HomeMy WebLinkAboutWQ0037637_Residual Annual Report 2019_20200228 (2)Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/28/2020
Received:*
Project Number* WQ0037637
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer Kendall.Williams@ncdenr.gov
Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Robert T. Branch
Email Address*
bbranch@branchrs.com
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0037637
Applicant\Permittee * Craven Ag Services
Facility Name * Craven Ag Services
Phone Number*
336.510-0340
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
This is a revised 2019 Annual report for Craven Ag that reflects a changed updated ARSS for the Town of Maysville.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Craven Ag AR Final REV.pdf 2.9MB
Upload only 1 R7F document. Maniple documents must be combined into one R7F file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 3/16/2020
2019 ANNUAL REPORT
CRAVEN AG SERVICES, INC.
LAND APPLICATION PROGRAM
PERMIT #WQ0037637
Prepared For:
Craven Ag Services, Inc.
2115 NC Highway 55
New Bern, North Carolina 28562
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
February 2020
BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE (336) 312-9007
February 26, 2020
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2019 LAND APPLICATION ANNUAL REPORT
Craven Ag Services, Inc.
Permit No. WQ0037637
Branch Residuals & Soils Project No. 2019-132
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Craven Ag Services, Inc. This data includes: 1) Certification Forms, 2) Annual Residual
Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field
Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen & Vector Attraction
Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data 10) 2019 Application
Summary Table, and 11) 2019 Application Condition Summaries.
A total of 141,500 gallons (5.38 dry tons) of Class B lime -stabilized biosolids were incorporated to 27.3 acres in
2019. This material was divided as follows:
0 84,000 gallons (4.90 dry tons) from Maysville WWTP,
• 57,500 gallons (0.48 dry tons) from Bridgeton WWTP. and
• 0 gallons (0 dry tons) from Pruitt Health Sealevel WWTP.
If any further information is required regarding this land application program, please do not hesitate to contact
me at (336) 312-9007.
Sincerely,
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures
cc: Town of Maysville Town of Bridgeton
Craven Ag Services, Inc. Pruitt Health Sealevel, NC
TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Forms
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2019 Application Summary Table
XI 2019 Application Condition Summaries
CERTIFICATION FORMS
AIv1N UAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0037637 County: Craven
Facility Name (as sh)tivn on permit): Year: 2019
Craven Ag
r Services, Inc
Land Application Operator: Craven Ag Services, Inc. Phone: (252 633-5334
1-nd application of residuals as allowed by the permit occurred during the past calendar year?
_'1 Yes j: J No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A- RPdrhiale A.,.,l:...a:_-
Total number of application fields in the ermit: 23
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 5.38
Total number of acres utilizes for land application during the year 27.3
Part B Annual Compiance Statement
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. Yes LJ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
o) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Mr. John W. Dunham, Owner
'tmittee Name and Title (type or print)
\ \J:t
a- v
J.Wignaet±urte of Permittee Date
See Attached
Signature of Preparer* Date (ignature of Land Applier Date
(if different from Permittee) (if different from Pernttee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)
ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF MAYSVILLE
Art B - Annual Comniance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes Ll No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the pernut.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Pen -nit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
w I) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the pemut were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
of
Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. I 102 (26)
ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BRIDGETON
. art B - Annual Com iance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes :J No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
of Preparer*
Date
(if different from Perm ittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
ANNUAL RESIDUAL SAMPLING SUMMARY FORMS
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0037637
Facility Name: Craven Ag Services, Inc
Residual Source WQ # or
NPDES #:
NCO021482
WWTP Name: Town of Maysville WWTP
Residual Analysis Data
Laboratory:
1)
2)
3)
4)
5)
Environmental Chemists, Inc.
Parameter
(mg/kg)
Conc.
Limit
m
Sam le or Composite Date
11 /6/2019
Percent Solids (%)
NA
1.40
Arsenic
75
<13.8
Cadmium
85
<13.8
Copper
4,300
403.00
Chromium
NA
<13.8
Lead
840
18.20
Mercury
57
<1.00
Molybdenum
75
<13.8
Nickel
420
14.50
Selenium
100
<13.8
Zinc
7,500
871.00
Total Phosphorus
NA
19,400
TKN
NA
28,300
Ammonia -Nitrogen
NA
r_1,640
Nitrate and Nitrite
NA
126
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submittfj>�g false information, including the possibility of fines and imprisonment for knowing violations."
of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)
ANNUAL RESIDUAL SA, ) ING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037637 Laboratory: 1)
Facility Name: Craven Ag Services, Inc 2)
Residual Source WQ # or NCO074837 3)
NPDES #: 4)
WWTP Name: Town of Bridgeton WWTP 5)
Residual Analysis Data
Environment One, Inc.
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
1/2/2019
Percent Solids (%)
NA
0.20
Arsenic
75
<2.50
Cadmium
85
Copper
4,300
335.00
Chromium
NA
17.00
Lead
840
31.00
Mercury
57
0.25
Molybdenum
75
<5.00
Nickel
420
10.00
Selenium
100
<5.00
Zinc
7,500
1754.00
Total Phosphorus
NA
17,650
TKN
NA
45,750
Ammonia -Nitrogen
NA
76
Nitrate and Nitrite
• percent solids were not collected on Gymd
NA
smnple until 2/I4/17
21
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penaly s for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
np:mp Pr)pdA L7CCc /aoMnnc�
ANNUAL METALS FIELD LOADING SUMMARY FORMS
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
-I.rmit #:
,rator:
. _..res Used:
2.60
n/a
Se
6.6 Acres Permitted: 5.6 Site #: 3 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
N119-47778 BEI.440A
Craven Ag Services Total Dry Tons Applied (Annual):
WQ0037637 Cation Exchange Capacity (non 503 only):
Allen Roach Owner: Allen & Gloria Roach Predominant Soil Series
•
` 11
. 1
ncavy ARM rtela Loadings luaiculated in the/nerpl-
�
f
11
OEM-
MEMM
-1 cerury, under penalty of law, that this document was prepared under my direction or supervision in
,ordance with a system designed to assure that qualified personnel properly gathered and evaluated the
irmation submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
i ature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
A1N1N UAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Craven Ag Services Total Dry Tons Applied (.Annual):
.-Rermit #: WQ0037637 Cation Exchange Capacity (non 503 only):
erator: Allen Roach Owner: Allen & Gloria Roach Predominant Soil Series
..ores Used: 14.6 Acres Permitted: 14.6 Site #• 3
To
n/a
35.06
Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
BEI-440AO-W000956 N419-4777R
Sample
or Com-
posite
Date
1/2/19
2/22/19
11/6/19
% Solids
0.20
74.10
1.40
Arsenic
2.50
0.00
13.80
Cadmium
1.90
0.00
13.80
Chromium
17.00
0.00
0.00
Copper
335.00
0.89
403.00
Lead
31.00
0.02
18.20
Mercury
0.25
0.00
1.00
Molyb-
denum
5.00
0.00
13.80
Nickel
10.00
0.03
14.50
Selenium
5.00
0.00
13.80
Zinc
1754.00
1.56
871.00
Total
phos-
;orus
17,650
60
19,400
c 1111-1 ucavy tvietai yield Loatiln¢5 f('stlrulatpd in the/onrnl.
1 1
1
' •
r�e
t
1
,NMI
-�' L iy, unber penalty o haw, that this document was prepared under my direction or supervision in
^ordance with a system designed to assure that qualified personnel properly gathered and evaluated the
.ormation submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
4'gnature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
TUNA UAL lvtE I AL, 1"IELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility ame.
-X",krmit #:
:rator:
titres Used:
Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
BEI-"OA
Craven Ag Services Total Dry Tons Applied (Annual): 0.18
WQ0037637 Cation Exchange Capacity (non 503 only): n/a
Allen Roach Owner: Allen & Gloria Roach Predominant Soil S T
6.1 Acres Permitted:
6.1
Site #:
.
.1
J4M1 1-l- tr�.CLi1, meta LOaa
-
1 1
• ,
1 11
-_------
1 11
Total
• •
^ • «, ME uuuer penalty oI taw, that this document was prepared under my direction or supervision in
cordance with a system designed to assure that qualified personnel properly gathered and evaluated the
rormation submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
ignature �ofLand Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As — Arsenic
Cd
— Cadmium
Cr — Chromium
Cu
— Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients (lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.
r1r,l.,L 0u1vI1v1AKY itUKiVI
PLF rAKE A COPY OF THIS BLANK FORM TO BE COMPLET }ND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BG HEN NOT APPLICABLE.
Facility Name: Craven Ag Services WQ Permit #: WQ0037637 Field #: 3 Acres Utilized:
Owner: Allen & Gloria Roaclt Annual Dry Tons Applied: 2.60 Site #: I Acres Permitted:
Operator: Allen Roach Predominat Soil Series
Se Cation Exchange Capacity (non 503):
Crop I Name: Millet Crop I Max PAN: 100.00 Crnn 2 Nnmp- RM/A , hR--. --
6.60
5.60
NA
C7
�
�' o
Jul-19
Specify
Totals
Per Acre
61364
Solids
° As
Decimal
1.40
Volume
Applied per
Acre
DT/Ae
0.37
Residual Sources
{NPDES tl, WQtf,
Feri., Animal Waste,
etc.)
Maysville W WTP
Site
Cord.
(Dry
Wet
Moist)
Precip.
Past 24
yrs,
Inches
D
a n.
o W
a _
� 'o'
a
INC
o
„ N
1.00
m
. W
W
=
0.30
TKN
nt • k •
28,300
z D
2 3
°o o
a
�'
m • k •
1,640
Nitrate
and
Nitrite
m • k •
126
PAN Applied
PP
(lbs/acre)
J
Gal'o
Must Select
Crop 1 or Crop 2
C1,.Yd.
Report
Totals
in Gal.
42,000
Crop I
7.25
Crop 2
Crop 1
X
Crop 2
Jul-19
18,000
2,727
0.20
0.02
Bridgeton WWTP
INC
1.00
0.30
45,750
76
21
0.63
X
TOTALS: 9,091
Annuallbs/acre
Current Cumulative lbs/acre
As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2
0.01 0.01 0.00 0.31 0.01 0.00 0.01 0.01 0.01 0.73 15.22 7.88 0.00
0.01 0.01 NA 0.57 0.02 0.00 NA 0.03 0.02 2.77
0.00 0.00 0.02 0.25 0.00 0.00 0.01 0.02 0.01 20
3G 34 NA 1,338 267 IS NA 374 89 2,498
too 00
t{,.� a� ...... wf . _J - _ J___
Lime A lied
Date lbs/ac
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
"I rprtifv nnrinr nanolfn, of ln.., kh
-- - - --- 11. -1 -- ......... ...J uu oa.a,vaa UA auPca V mum ui accuruance wim a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
[/ U **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading,�,t�,�
pp"HF�tuR F(1RC\A FCG I1.7J-)nnr-%
PLY
Facility Name:
Owner:
Operator:
. 'v_' 11 a_,�11.iJt1 Ll1.1•1t1VLY rLV I,u ,0UIVINIAKY 11UIUV1
MAKE A COPY OF THIS BLANK FORM TO BE COMPLE" �ND SUBMITTED FOR EACH APPLICATION FIELD. }
ll PLACE A "N/A" IN A BLANK OR BG_ EN NOT APPLICABLE.
Craven Ag Services WQ Permit #: WQ0037637 Field #: 3 Acres Utilized: 14.60
Allen & Gloria Roach Annual Dry Tons Applied: 35.06 Site #• 2 Acres Permitted: 14.60
Allen Roach
Crop I Name: Corn (Grain)
Predominat Soil Series
Crop l Max PAN: 138.00
To
Croa 2 Name
Cation Exchange Capacity (non 503): NA
Rye(Grain) rrnn7Mov PAN Snnn
od
w
f9
o
SpeciN
Totals
Per Acre
^„ Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(Dry'
Wet,
Moist)
Preci p.
Past 24
1-Irs.
Inches
a
3:.,
�� �'
o w
°
o
=•
*
�,
; rb
TKN
jug/kg
D
z g
o 3
`�
w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Must Select
Crop I or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Mar-19
18,500
1,267
0.20
0.01
Bridgeton WWTP
INC
1.00
0.30
45,750
76
21
0.29
X
Nov-19
44
3
74.10
2.22
Craven Wood Energy
INC
1.00
0.30
1
0
0
0.00
X
Nov-19
42,000
2,877
1.40
0.17
Maysville WWTP
INC
1.00
0.30
28,300
1,640
126
3.28
X
TOTALS:
4,147 :
As
Cd
Cr
Cu I
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN
Lime Applied
Annuallbs/acre
Current Cumulative lbs/acre
0.00 0.00 0.00 0.15 0.01 0.00 0.00 0.01 0.00 0.34 7.16 0.29 3.28
0.00 0.00 NA 0.15 0.01 0.00 NA 0.01 0.00 0.34
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 • • •
36 34 NA 1,338 267 15 NA 374 89 2,498
138.00 50
Date
Nov-19
Ibs/ac
128
Prior Years Cumulative Ibs/acre
Permitted C. P. L. R,****
Permit PAN Limit Ist/2nd Crop
__11 ____ 1._.__..� ,...»,,, ,.,,,„- },1 a. jjakc uNg. 1;1 111y u11 CLAIM, Vt w1jervlsiun m aeeoruanee wttn a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/ ] *Application Method: S - Surface, IN - Injection, INC -Incorporation
�.Z 9 **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading R
`Y7%R F(IRKA FCF (4,)i-,nna1
PLE
Facility Name:
Owner:
Operator:
AININUAL LA1v1J AYYL1l,AI IVIN VIEL l) NUMMARY NORM
YIAKE A COPY OF THIS BLANK FORM TO BE COMPLET "ND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BO,_ . I EN NOT APPLICABLE.
Craven Ag Services WQ Permit #: WQ0037637 Field M 3 Acres Utilized: 6.10
Allen & Gloria Roach Annual Dry Tons Applied: 0.18 Site #: 3 Acres Permitted: 6.10
Allen Roach Predominat Sail Series To Cation Capacity Exchange Ca g p ty (non 503): NA
Crop 1 Name: Wheal (Grain) Crap 1 Max PAN: 111.00 Crop 2 Name: #N/A Cron 2 Max. PAN #N/A
CJ
o m
o
S Peci FV
Totals
Per Acre
OQ Solids
As
Decimal
Volume
Applied per
Acre
DTAc
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Se1C
Cond.
(Dry'
Wet,
Moist)
Precip.
Past 24
Hrs.
Inches
K d
n, _.
0
? o
7
o
-
a
+ h
j
;a 0
� w
o'
=1
TKN
mg/kg
Z a
9
o 9
m•k•
Nitrate
and
Nitrite
m•k•
PAN Applied
PF
(Ibs/acre)
Must Select
Crop 1 or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gat.
Crop I
Crop 2
Crop I
Crop 2
Oct-19
21,000
3,443
0.20
0.03
Bridgeton WWTP
INC
1.00
0.30
45,750
76
21
0.79
X
TOTALS:
3,443
As
Cd
Cr I
Cu
Pb
Re I
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.00
0.60
0.00
0.02
0.00
0.00
0.00
0.00
0.00
0.10
1.01
0.79 1
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.00 0.00 NA 0.02 0.00 0.00 NA 0.00 1 0.00 0.10
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
36 34 NA 1,338 267 15 NA 374 89 2,498
111.001
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
--I CCCLIIy, UlluCr penally UI 111W, Inal tnls uocumenE was preparea unaer my arreclion or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading R� •`F1fNR Fr1RhA F'CF 117Mnnm
RESIDUAL ANALYSIS LAB SHEETS
Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Bridgeton
Bridgeton WWTP
Havelock, North Carolina
Carven Ag Services
Wastewater Treatment Plant
BEI-440A
1/2/2019
1 /28/2019
Annual 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
0.20
Nitrogen (TKN)*
4.575
45,750.000
Phosphorus *
1.765
17,650.000
Potassium
0.528
5,283.000
Sulfur
0.000
0.000
Calcium
4.752
47,517.000
Magnesium
0.308
3,084.000
Sodium
3.130
31,302.000
Iron
---
Aluminum
---
3,391.000
Manganese
---
Copper
---
335.000
1,500
Zinc
---
1,754.000
2,800
Ammonia Nitrogen*
0.008
76.140
Nitrate N / Nitrite N*
---
21.200
Cadmium
---
1.900
39
Chromium
---
17.000
1,200
Nickel
---
10.000
420
Lead
---
31.000
300
Arsenic
---
2.500
41
Mercury
---
0.250
17
Selenium
---
5.000
100
pH
6.900
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.567
45,673.860
Molybdenum
---
5.000
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340
Wastewater Treatment Plant
Bridgeton WWTP
Havelock, North Carolina
Carven Ag Services
Annual 2019
Date Reported: 1/28/2019 Report No: BEI-440A
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
27.523
PAN Inj.
27.599
P
35.300
K
10.566
Lime (estimated)
0.000
Secondary Nutrients
Calcium
95.034
Magnesium
6.168
Sodium
62.604
SAR
1.677
Chloride
0.000
Iron
0.000
Alumium
6.782
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
0.20
pH
6.900
Min Rate
0.300
Metals
Arsenic
0.005
Cadmium
0.004
Chromium
0.034
Copper
0.670
Lead
0.062
Mercury
0.001
Molybdenum
0.010
Nickel
0.020
Seleniun
0.010
Zinc
3.508
EMAMMEW Flo dMC@TP@T@%d
Ds3nIsidg 4fa �s� 's'37715
{{astawatar ID, 10
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
TOWN OF BRIDGETON
HYDRO SERVICES & CONSULTING
MR. KEVIN MULLINEAUX
P.O. BOX 317
HAVELOCK ,NC 28532
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio (calc)
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.9
01/02/19
HAI 4 4500HB-11
3991
01/15/19
LFJ
EPA200.7
<2.5
01/22/19
MTM
3113B-04
47517
01/15/19
LFJ
EPA200.7
1.9
01/17/19
MTM
3113B-04
335
01/15/19
LFJ
EPA200.7
17
01/15/19
LFJ
EPA200.7
31
01/18/19
MTM
3113B-04
3084
01/15/19
LFJ
EPA2110.7
0.25
01/18/19
MTM
EPA7471B
10
01/15/19
LFJ
EPA200.7
5283
01/15/19
LFJ
EPA200.7
<5.0
01/15/19
MTM
3113B-04
31302
01/15/19
LFJ
EPA200.7
1754
01/15/19
LFJ
EPA200.7
37.6
0.20
01/03/19
J1NIS
2540G-11
c 45750
01/16/19
CLO
351.2 R2-93
c 76.14
01/11/19
DTL
350.1 R2-93
c 17650
01/16/19
DTL
365.4-74
c 21.20
01/11/19
CLO
353.2 R2-93
<5.0
01/15/19
LFJ
EPA200.7
PHONE (252) 756-6208
F.r, ;~52) 756-0633
ID#: 440 A
DATE COLLECTED: 01/02/19
DATE REPORTED : 01/28/19
REVIEWED BY:
Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Maysville
Maysville WWTP
Maysville, North Carolina
Carven Ag Services
Wastewater Treatment Plant
19-47778
11/6/2019
12/4/2019
Annual 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
1.40
Nitrogen (TKN)*
2.830
28,300.000
Phosphorus *
1.940
19,400.000
Potassium
0.377
3,770.000
Sulfur
0.000
0.000
Calcium
3.890
38,900.000
Magnesium
0.291
2,910.000
Sodium
0.757
7,570.000
Iron
---
Aluminum
---
5,110.000
Manganese
---
Copper
---
403.000
1,500
Zinc
---
871.000
2,800
Ammonia Nitrogen*
0.164
1,640.000
Nitrate N / Nitrite N*
---
126.000
Cadmium
---
13.800
39
Chromium
---
1,200
Nickel
---
14.500
420
Lead
---
18.200
300
Arsenic
---
13.800
41
Mercury
---
1.000
17
Selenium
---
13.800
100
H
6.740
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
2.666
Molybdenum
---
13.800
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340
Wastewater Treatment Plant
Maysville WWTP
Maysville, North Carolina
Carven Ag Services
Annual 2019
Date Reported: 12/4/2019 Report No: M19-47778
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
17.888
PAN Inj.
19.528
P
38.800
K
7.540
Lime (estimated)
0.000
Secondary Nutrients
Calcium
77.800
Magnesium
5.820
Sodium
15.140
SAR
1.178
Chloride
0.000
Iron
0.000
Alumium
10.220
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.40
pH
6.740
Min Rate
0.300
Metals
Arsenic
0.028
Cadmium
0.028
Chromium
0.000
Copper
0.806
Lead
0.036
Mercury
0.002
Molybdenum
0.028
Nickel
0.029
Seleniun
0.028
Zinc
1.742
envirochem
srn
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill 6 ay, Wilrnington, NC 28405 a 910392.0223 Lab • 910.392.4424 Fax
710 Bowsertok�n Road, Nianteo, NC 27954 • 252.473.5702 Lab/Fax
2i5-A Wilminoton t lighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infou em ironmentalcheniists.com
Town of Maysville
Post Office Box 265
Maysville NC 28555
Attentions
Date of Report: Dec 04, 2019
Customer PO #:
Customer ID: 17020023
Report #: 2019-18771
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-47778 Site: Sludge
11/6/2019
2:30 PM Solid/Sludge boomer
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW 846 Method 8081B/3510
<0.02 mg/L
11/20/2019
Endrin (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
11/20/2019
Heptachlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
11/20/2019
Heptachlor epoxide (TCLP)
SW 846 Method 608113/3510
<0.0005 mg/L
11/20/2019
Lindane (TCLP)
SW 846 Method 80816/3510
<0.0005 mg/L
11/20/2019
Methoxychlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
11/20/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
11/20/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
11/19/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
11/19/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.003 mg/L
11/20/2019
2,4-D (TCLP)
SW846 Method 8151A
<0.003 mg/L
11/20/2019
1,1-Dichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
1,2-Dichloroethane (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Benzene (TCLP)
SW845 Method 8260/5030
<0.01 mg/L
11/19/2019
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Rannrt@ 7n1q_1A771
Environmental Chemists, Inc,
env-wochem 6602 Windmill Vviw, Wilmington, NC 28405 • 910.392.0223 Lab • 910.391.4424 Fax
710 Bowsertown Road, 1%,tanteo, NC 27954 6 252.473.5702 Lab/Fax
sr.t '_55-A Wilmington Highway, Jacksorwille, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info'a em irinu»entalchenlists.com
Town of Maysville
Date of Report: Dec 04, 2019
Post Office Box 265
Customer PO #:
Maysville NC
28555
Customer ID: 17020023
Attention:
Report #: 2019-18771
Project ID: Sludge
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
11/19/2019
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
RCI
Cyanide EPA 335 4
Reporting limit elevated due to matrix interference.
<0.05 mg/kg 11 /15/2019
Sulfide
SM 4500 S D
0.22 mg/kg
11/08/2019
Ignitability
SW 846 method 1010
>195 °F
11/15/2019
pH
SW 846 Method 9045D
6.74 units
11/13/2019
Sludge Residuals
Aluminum
EPA 200.7
5110 mg/kg
11/18/2019
Arsenic
EPA 200 7
<13.8 mg/kg
11/18/2019
Cadmium
EPA 200 7
<13.8 mg/kg
11/18/2019
Calcium
EPA 200 7
38900 mg/kg
11/18/2019
Chromium
EPA 2007
<13.8mg/kg
11/18/2019
Copper
EPA 200 7
403 mg/kg
11/18/2019
Lead
EPA 200 7
18.2 mg/kg
11/18/2019
Magnesium
EPA 200 7
2910 mg/kg
11/18/2019
Molybdenum
EPA 200 7
<13.8 mg/kg
11/18/2019
Nickel
EPA 200 7
14.5 mg/kg
11118/2019
Potassium
EPA200.7
3770 mg/kg
11/19/2019
Selenium
EPA 2007
<13.8mg/kg
11/18/2019
Sodium
EPA 200 7
7570 mg/kg
11/18/2019
Zinc
EPA 200 7
871 mg/kg
11/18/2019
Total Kjeldahl Nitrogen (TKN)
EPA 351 2
28300 mg/kg
11/18/2019
Nitrate+Nitrite-Nitrogen
EPA 353 2
126 mg/kg
11/18/2019
Total Solids (%)
SM 2540 8
1.40 %
11 /11 /2019
Report # 2019-18771
Environmental Chemists, Inc.
envirochem 6602 Windmill 4VaY Wilmin;tun, iti'C 28105 910.392.0223 Lab • 910.392-1421 Fax
710 Bowsertown Road, Nlanteo, NC 27954 • 252.473.5702 Lab/Far
Sr.+
25-9-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS u11i-);u em,ironnlentalchemisti.con1
Town of Maysville Date of Report: Dec 04, 2019
Post Office Box 265 Customer PO #:
Maysville NC 28555 Customer ID: 17020023
Attention: Report #: 2019-18771
Project ID: Sludge
Ammonia Nitrogen SM 4500 NH3 C 1640 mg/kg 11/18/2019
Total Phosphorus SM 4500 P F 19400 mg/kg 11/13/2019
Mercury Sw8467471B <1.00mg/kg 11/11/2019
TCLP Metals
Arsenic
EPA 2007
<1.0mg/L
11/21/2019
Barium
EPA 2007
<1.0mg/L
11/21/2019
Cadmium
EPA 200.7
<1.0 mg/L
11/21/2019
Chromium
EPA 200 7
<1.0 mg/L
11/21/2019
Lead
EPA 200 7
<1.0 mg/L
11/21/2019
Selenium
EPA 200 7
<1.0 mg/L
11/21/2019
Silver
EPA 200 7
<1.0 mg/L
11/21/2019
Mercury
EPA 2451
<0.0002mg/L
11/21/2019
Comment:
Sludge residuals reported on a dry weight basis.
Reviewed by:
Report # 2019-18771 _ , _
6602 Windmill Way
ton
ENVIRONMENTAL CHEMISTS, INC OFFICE: 0-392-02 3iIFAX9910392.44245
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: Town of Maysville WWTP
PROJECT NAME: Annual Sludge
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled By:_ 00'"a/ SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae_ Other:
Sample Identification
Collection
m
E
a
`o a
U
S
o`
0 a
_
o �d,
" E
W
m g
g=
PRESERVATION
ANALYSIS REQUESTED
D
Time
Tem
i
Z
=
p
_
o
=
0
Z
o
w
o
Slud e
u l�
/Y3ZOO
C
P
`��
X
Full TCLP/Nutrients/Metals/RCI
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Temperature when Received:Accepted: Rejected: Resample Re sted:
Delivered By: Received By: Date: /1 Time: f—�
Comments: TUR ROUND:
NCDA&C? nomic Division Phone: (919) 733-2666 Website: www.nc.
Craven Ag Services, Inc.
lov/agronomi/
Report No. d-WO05304
Sampled: 02/22/2019 ( Received: 02/26/2019 1 Completed: 03/04/2019
Page 2 of 3
Sample Information
Nutrient Measurements are given in units of
ID: LFMEAS
parts per million (ppm), unless utherwise
Nitrooen lN)
specifed.
Other Results
Code: CSO
P K Ca Mg S Fe Mn Zn
TotalN:881 17800 29500 143000 11200 3980 4850 1090 1050
Cu
B Mo
C Al Na CI
Description: Ash,
Inorganic:
603
-
110 165200
10400 5680 -
Mixed orOther
NH4-N-----------------_
Grower
Not Pro Comments:
Not Pro(
NO3-N SEC pH BD CCE
ALE
C:N
DM
'S
(10 S/cm) (mS/cm) (Unitless) (lb/ d
( Y ) (�o)
1470 14.73 12.18
(tons)
(Unitless)
a
(/o)
�(�
42.0
289
74.0 : 1
74.1
Estimate of Nutrients Available for First Year (lb/ton)
ApplicationMethod:
i N
Other Results (lb/ton)
P205 K20 Ca Mg S Fe Mn Zn
1.31 60.4 52.4 211
Cu
B Mo
AI Na Cl
Soil Incorporated
16.7 5.90 7.19 1.62 1.56
1.31 60.4 52.4
0.89
0.16 I
15.4 8.42
_ 211 16.7 5.90 7.19 1.62 1.56
13i
0.89
0.16
15.4 0.02
I G G - ilk
Heavy Me Is are given in units of parts per million (ppm).
Heavy
Metals
Estimate of Availability
(lb/ton)
As Cd Cr Ni Pb Se
- 1.12
Application Method:
As
Cd Cr
Ni Pb Se
- 14.7 8.46 -
Broadcast
_
T _
0.02 0.01 -
Soil Incorporated
-
T -
0.02 0.01 -
Agronomist's Comments: Insufficient information is available regarding the first year availability of nutrients in this material. The nutrient availability reported here is
therefore the TOTAL nutrients in the material. Samples submitted prior to 2016 reported an estimated value rather than total nutrient levels. Please contact me if you have
any questions.
TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS
A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES:
TOWN OF BRIDGETON
AND
TOWN OF MAYSVILLE
Orlando, FL
The results set forth herein are provided by SGS North America Inc.
Technical Report for
Environment 1, Inc
e-Hardcopy 2.0
Automated Report
Town of Bridgeton Hydro Services & Consulting; Havelock, NC
440C
SGS Job Number: FA70914
Sampling Date: 12/12/19
Report to:
Environment 1, Inc
PO Box 7085
Greenville, NC 27835
dwoolard@environmentIinc.com
�ATTN: Deedee Woolard
Total number of pages in report: 13
pC
eflin*
rice, M.S.
Test results contained within this data package meet the requirements General Manager
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Jean Dent -Smith 407-425-6700
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063). NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV. OK, OR, UT, INA. M
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 - tel: 407-425-6700 • fax: 407-425-0707
SCiS is the :ol: aut.ioriq for authorizing c.!it, ur m„Uiti.: uun, 10 111i, d _unt il: Pir.t:t ;!allatit idea; abotit Sfl&t%
Lfiau;horized modification of this report is strictly Pruhritte l can serve you betwr a!:
Re%standard term; at: IMF,: N': ': en term, -ant! -.on hoot) FFIS [, S Cu.s:onierCarc a;, "0111
1 of 1
FA7091
Table of Contents Sections:
Section1: Sample Summar�....................................................................................................
3
Section2: Summary of Hits....................................................................................................
4
Section3: Sample Results........................................................................................................
5
3.1: FA70914-1: SLUDGE SAMPLE..................................................................................
6
Section4: Misc. Forms............................................................................................................
11
4.1: Chain of Custody...........................................................................................................
12
SGS2 of 13
FA70914
SGS North America Inc.
Sample Summary
Environment 1, Inc
Job No: FA70914
Town of Bridgeton Hydro Services & Consulting; Havelock, NC
Project No: 440C
Sample
Collected
Matrix
Client
Kumber
Date Time By
Received Code Type
Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA70914-1 12/12/19 09:37 KM 12/14/19 SO Sludge SLUDGE SAMPLE
Soil samples reported on a dry weight basis unless otherniise indicated on result page.
SGS_ 3 of 13
FA70914
Summary of Hits Page 1 of 1
Job Number: FA70914
Account: Environment 1, Inc
Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC
Collected: 12/12/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA70914-1 SLUDGE SAMPLE
1,2-Dichloroethane 0.0106 0.010 0.0031 mg/I SW846 8260B
SGS4 of 1
FA70914
Orlando, FL :.,
Sample Results
Report of Analysis
Section 3
�I
SOS5of13
FA70914
SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FA70914-1 Date Sampled: 12/12/19
Matrix: SO - Sludge Date Received: 12/14/19
Method: SW846 8260B SW846 1311 Percent Solids: n/a
Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 5E19799.D 10 12/23/19 16:01 SO 12/16/19 14:00 OP78166 V5E899
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA TCLP List
CAS No.
Compound
Result
HW#
MCL
RL
71-43-2
Benzene
ND
D018
0.50
0.010
78-93-3
2-Butanone (MEK)
ND
D035
200
0.050
56-23-5
Carbon Tetrachloride
ND
D019
0.50
0.010
108-90-7
Chlorobenzene
ND
D021
100
0.010
67-66-3
Chloroform
ND
D022
6.0
0.010
106-46-7
1,4-Dichlorobenzene
ND
D027
7.5
0.010
107-06-2
1,2-Dichloroetliane
0.0106
D028
0.50
0.010
75-35-4
1, 1 -Dichloroethylene
ND
D029
0.70
0.010
127-18-4
Tetrachloroethylene
ND
D039
0.70
0.010
79-01-6
Trichloroethylene
ND
D040
0.50
0.010
75-01-4
Vinyl Chloride
ND
D043
0.20
0.010
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
83-118%
17060-07-0
1,2-Dichloroethane-D4
109%
79-125%
2037-26-5
Toluene-D8
105%
85-112%
460-00-4
4-Bromofluorobenzene
111%
83-118%
TCLP Leachate method SW846 1311
MDL
Units Q
0.0031
mg/l
0.020
mg/l
0,0036
ing/l
0.0020
mg/1
0.0030
mg/l
0.0026
mg/1
0.0031
mg/l
0.0032
mg/I
0.0022
mg/1
0.0035
mg/l
0.0041
mg/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SG6of13
FA70914
SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FA70914-1 Date Sampled: 12/12/19
Matrix: SO - Sludge Date Received: 12/14/19
Method: SW846 8270D SW846 3510C Percent Solids: n/a
Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X068591.1) 1 12/19/19 20:27 MV 12/19/19 07:47 OP78217 SX2818
Run #2
Initial Volume Final Volume
:un #1 100 ml 1.0 ml
:un #2
ABN TCLP List
TCLP Leachate method SW846 1311
CAS No.
Compound
Result
HW#
MCL RL
MDL
Units Q
95-48-7
2-Methylphenol
ND
D023
200
0.050
0.0056
mg/1
3&4-Methylphenol
ND
D024
200
0.050
0.0098
mg/1
87-86-5
Pentachlorophenol
ND
D037
100
0.25
0.050
mg/1
95-95-4
2,4,5-Trichlorophenol
ND
D041
400
0.050
0.0074
mg/1
88-06-2
2,4,6-Trichlorophenol
ND
D042
2.0
0.050
0.0075
mg/1
106-46-7
1,4-Dichlorobenzene
ND
D027
7.5
0.050
0.0050
mg/1
121-14-2
2,4-Dinitrotoluene
ND
D030
0.13 0.050
0.0081
mg/l
118-74-1
Hexachlorobenzene
ND
D032
0.13 0.050
0.0069
mg/1
87-68-3
Hexachlorobutadiene
ND
D033
0.50 0.050
0.0050
mg/I
67-72-1
Hexachloroethane
ND
D034
3.0
0.050
0.016
mg/I
98-95-3
Nitrobenzene
ND
D036
2.0
0.050
0.0093
mg/I
110-86-1
Pyridine
ND
D038
5.0
0.10
0,020
mg/1
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluoroplienol
36%
14-67%
4165-62-2
Phenol-d5
26%
10-50%
118-79-6
2,4,6-Tribromophenol
82%
33-118%
4165-60-0
Nitrobenzene-d5
78%
42-108%
321-60-8
2-Fluorobiphenyl
80%
40-106%
1718-51-0
Terphenyl-dl4
84%
39-121%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
&_A,%S_ 7 of 13
FA74914
SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FA70914-1 Date Sampled: 12/12/19
Matrix: SO - Sludge Date Received: 12/14/19
Method: SW846 8151A SW846 3510C Percent Solids: n/a
Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CC065678.1) 1 12/23/19 18:37 RS 12/21/19 11:10 OP78260 GCC1573
Run #2
Initial Volume Final Volume
Run #1 10.0 ml 5.0 ml
Run #2
Herbicide TCLP List
CAS No.
Compound
Result
HW#
MCL RL
94-75-7
2,4-D a
ND
D016
10 0.050
93-72-1
2,4,5-TP (Silvex) a
ND
D017
1.0 0.0050
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
19719-28-9
2,4-DCAA
60%
39-135%
(a) Associated BS outside of control limits high, sample
was ND.
TCLP Leachate method SW846 1311
MDL Units Q
0.017 mg/l
0.0013 mg/I
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
Ots8of13
FA70414
SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FA70914-1 Date Sampled: 12/12/19
Matrix: SO - Sludge Date Received: 12/14/19
Method: SW846 8081B SW846 3510C Percent Solids: n/a
Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 KK96255.D 1 12/23/19 14:09 WH 12/21/19 12:45 OP78259 GKK3070
Run #2
Initial Volume Final Volume
.un #1 100 ml 5.0 ml
.un #2
Pesticide TCLP List
CAS No. Compotind
Result HW# MCL RL
TCLP Leachate method SW846 1311
MDL Units Q
58-89-9
gamma-BHC (Lindane) a
ND
D013
0.40 0.00010
0.000022
mg/1
12789-03-6
Chlordane b
ND
D020
0.030 0.0010
0,00038
mg/l
72-20-8
Endrin b
ND
D012
0.020 0.00020
0.000021
mg/l
76-44-8
Heptachlor b
ND
D031
0.0080 0.00010
0.000026
mg/l
1024-57-3
Heptachlor epoxide a
ND
D031
0.0080 0.00010
0.000020
mg/l
72-43-5
Methoxychlor
ND
D014
10 0.00020
0.000050
mg/l
8001-35-2
Toxaphene
ND
D015
0.50 0.0050
0.0021
mg/l
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
877-09 8 Tetrachloro-m-xylene 125% 42-127%
2051-24-3 Decachlorobiphenyl 115% 27-127%
(a) Associated BS outside of control limits high, sample was ND. Associated CCV outside of control limits high.
sample was ND.
(b) Associated CCV outside of control limits high, sample was ND.
(c) Associated BS outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9of13
SGS
FA7091:
SGS North America Inc.
Report of Analysis
Client Sample ID: SLUDGE SAMPLE
Lab Sample ID: FA70914-1 Date Sampled: 12/12/19
Matrix: SO - Sludge Date Received: 12/14/19
Percent Solids: n/a
Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC
Page 1 of 1
Metals Analysis, TCLP Leachate SW846 1311
Analyte
Result
HW#
MCL
RL
Units
DF
Prep
Analyzed
By
Method
Prep Method
Arsenic
< 0.10
D004
5.0
0.10
mg/l
1
12/18/19
12/20/19
LM
SW846 6010D 2
SW846 3010A 3
Barium
< 2.0
D005
100
2.0
mg/1
1
12/18/19
12/20/19
LM
SW846 6010D 2
SW846 3010A 3
Cadmium
< 0.050
D006
1.0
0.050
mg/l
1
12/18/19
12/20/19
LM
SW846 6010D 2
SW846 3010A 3
Chromium
< 0.10
D007
5.0
0.10
mg/l
1
12/18/19
12/20/19
LM
SW846 6010D 2
SW946 3010A 3
Lead
< 0.050
D008
5.0
0.050
mg/l
1
12/18/19
12/20/19
LM
SW846 6010D'-
SW846 3010A 3
Mercury
< 0.0050
D009
0.20
0.0050
mg/l
1
12/19/19
12/19/19
1c
SW846 7470A 1
SW846 7470A 4
Selenium
< 0.10
D010
1.0
0.10
mg/l
1
12/18/19
12/20/19
LM
SW846 6010D 2
SW846 3010A 3
Silver
<0.10
D011
5.0
0.10
mg/i
1
12/18/19
12/20/19
LM
SW846 6010D 2
SW846 3010A 3
(1) Instrument QC Batch: MA16416
(2) Instrument QC Batch: MA16420
(3) Prep QC Batch: MP36569
(4) Prep QC Batch: MP36576
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 7/1/11)
SGS10 of 13
FA70914
Orlando, FL
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Section 4
C
SAS_ 11 of 13
FA70914
Environment I, Inc.
P.O. Box 7085,114 Oakmont Dr.
Greenville, NC 27858
environmentl inc.com
DiSI1VFECTION
Phone (252) 756-6208 • Fax (252) 756-0633
ry CHLORINE
CLIENT: 440 C Week:1
�•UV
TOWN OF BRIDGETON
NONE
HYDRO SERVICES & CONSULTING
MR. KEVIN MULLINEAUX
P.O. BOX 317
HAVELOCK NC 23532'
o
CHAIN OF CUSTODY RECORD E
G
(252) 723-0101
w
�
°i}
COLLECTION
ES
SA�VPIELOCATION
DATE I
TIME
Sludge Sample
�j .2—
-?.' 37
3
WWI
FORM eS PLEASE READ Irl-siruetlons for
1
giORNE NE1rWIZEDATC0.- tL;i Km+
pH CHECK PB)
CDNTAPERTYPE Pr-
CHEMY,ALPREGEFiVX DN
A•NGNE D•NACH
B•HNO, E•HCL
C•H1,SO, F- ZINC ACEfATFJNAOH
0 • "JATh°.ASt1LFATE
a
QASSIFICATION
WASTEVlATER �PCES)
ORI=WWATER '
D1Vfl�'I!
SOLD WASTE 5ECT 01
GRAIN OF CUSTODY (SEAL) MIARJTAINED
DURIN IENTlDELIVERY
Y N
SAMPLES COLLECTED by-
ft.
� � �,
SAIAKES P,ECSVED V LABITT
f CATErA+t COMMEM:
DATEFM
r 2 zs�) U. C •
12/3 7-30' 1 0
D FInh1E 01
1 Iffy/9 ?b�
Sampler must place a "C" for composite samp10 or a "G" for
on he reverse silo. Gab sample in the blocks above ter each parameter rvGue5lad N U 3760,65
1C
I A70914: Chain of Custody
Page I of 2
sUa
92 of 1,
FA7o91,
SGS Sample Receipt Summary
Job Number: FA70914 Client: ENVIRONMENT 1, INC. Project: TOWN OF BRIDGETON
Date / Time Received: 12/14/2019 9.00.00 AM Delivery Method: FED EX Airbill ids:
Therm ID: IR 1; Therm CF: -0.8. # of Coolers: 1
Cooler Temps (Raw Measured) °C: Cooler 1: (2.3);
Cooler Temps (Corrected) °C: Cooler 1: (1.5);
Cooler Information
Y or
N
Sam0e Information
Y or
bL
NIA
1. Custody Seals Present
2
Cl
1. Sample labels present on bottles
❑
2. Custody Seals Intact
❑
2 Samples preserved property
�r
❑
3 Temp criteria achieved
❑
3. Sufficient volumelcontainers recvd for analysis:
;�
❑
4. Cooler temp verification
IR Guri
4. Condition of sample
Intact
5 Cooler media
Ice a
5. Sample recvd within HT
Q
❑
6. Dates/Tmes/IDs on COG match Sample Label
Trip Blank Information
Y or
N
N/A
7. VOCs have headspace
❑
❑
CYl
1. Trip Blank present / cooler
❑
Ri
❑
e. Bottles received for unspecified tests
❑•
2 Trip Blank listed on COG
❑
❑
9. Compositing instructions clear
❑
❑
E
10 Voa Soil Kits/Jars received past 48hrs?
1
17
9
W or S
NIA
11. °k Solids Jar received?
❑
❑
3. Type Of TB Received
❑
❑
Q
12. Residual Chlorine Present?
❑
❑
Misc. Information
Number of Encores. 25-Gram
5-Gram
Number of 5035 Field Kits, Number of Lab Filtered Metals
Test Strip Lot #s:
pH 0.3
230315
pH 10-12 219813A Other: (Specify)
_
Residual Chlorine Test Strip Lot #
Comments
s%1001 Technician: TRINITYb1 Date 12/14/2019 9.00 00 A
Rev. Date 05,74117
Reviewer Date
FA70914: Chain of Custody
Page 2 of 2
SGS
13of1
FA7091
r7 . -, 0"441
ANALYTICAL & CONSULTING CHEMISTS
Town of Maysville
Post Office Box 265
Maysville
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910..',92.4424 Fax
710 Bowsertown [goad, Nlanteo, NC 27954 • 252.473.5702 Lab/Fax
23-9-A Wilmington Highway, Jacksonville, NC 2S5-10 • 910.347.5843 Lab/Fax
hillo!a em ironnlentalchenlists.com
Date of Report: Dec 04, 2019
Customer PO #:
NC 28555 Customer ID: 17020023
Report #: 2019-18771
Project ID: Sludge
Lab ID Sample ID:
19-47778 Site: Sludge
Test
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
Collect Date/Time Matrix
11/6/2019 2:30 PM Solid/Sludge
Method
SW 846 Method 8081 B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081 B13510
SW 846 Method B0818/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
Results
Sampled by
boomer
Date Analyzed
<0.02 mg/L
11/20/2019
<0.0005 mg/L
11/20/2019
<0.0005 mg/L
11/20/2019
<0.0005 mg/L
11/20/2019
<0.0005 mg/L
11/20/2019
<0.0005 mg/L
11/20/2019
<0.05 mg/L
11/20/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.250 mg/L
11/19/2019
<0.050 mg/L
11/19/2019
<0.003 mg/L
11/20/2019
<0.003 mg/L
11/20/2019
<0.01 mg/L
11/19/2019
<0.01 mg/L
11/19/2019
<0.01 mg/L
11/19/2019
<0.01 mg/L
11/19/2019
Reoort #:. 2019.18771
Environmental Chemists, Inc.
envirochem 6602 Windmill WaY, Wilminl;ton, NC 25405 • 910.392.0223 Lab • 910.392.442.4 Fax
710 Bowserto%,vn Road, Manteo, NC 27954 • 2-2.=473.5702 Lab/Fax
si+ 255-A Wilmington Highway, Jacksonville, `1C 285-40 • 910.3.47.58 43 1_ab/Fax
ANALYTICAL & CONSULTING CHEMISTS inlo it em ironmentalchemists.com
Town of Maysville
Date of Report: Dec 04, 2019
Post Office Box 265
Customer PO #:
Maysville NC
28555
Customer ID: 17020023
Attention:
Report #: 2019-18771
Project ID: Sludge
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0 01 mg/L
11/19/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
11/19/2019
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
11/19/2019
RCI
Cyanide EPA 3354
Reporting limit elevated due to matrix interference.
<0.05mg/kg
11/15/2019
Sulfide
SM 4500 S D
0.22 mg/kg
11 /08/2019
Ignitability
SW846 method 1010
>195 OF
11/15/2019
pH
SW 846 Method 9045D
6.74 units
11/13/2019
Sludge Residuals
Aluminum
EPA 2007
5110mg/kg
11/18/2019
Arsenic
EPA 200 7
<13.8 mg/kg
11/18/2019
Cadmium
EPA 2007
<13.8mg/kg
11/18/2019
Calcium
EPA 200 7
38900 mg/kg
11/18/2019
Chromium
EPA 200 7
<13.8 mg/kg
11/18/2019
Copper
EPA 200 7
403 mg/kg
11/18/2019
Lead
EPA 200 7
18.2 mg/kg
11/18/2019
Magnesium
EPA 200 7
2910 mg/kg
11/18/2019
Molybdenum
EPA 2007
<13.8mg/kg
11/18/2019
Nickel
EPA 200 7
14.5 mg/kg
11/18/2019
Potassium
EPA 2007
3770mg/kg
11/19/2019
Selenium
EPA 200 7
<13.8 mg/kg
11/18/2019
Sodium
EPA 200 7
7570 mg/kg
11/18/2019
Zinc
EPA 200 7
871 mg/kg
11/18/2019
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
28300 mg/kg
11/18/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
126 mg/kg
11/18/2019
Total Solids (%)
SM 2540 B
1.40 %
11/11/2019
Report # : 2019-18771
Environmental Chemists, Inc.
L�nvirocheM 6602 Windmill Wav, Wilmington, INK 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Botesertuwt1 Road, i\lanteo, NC 279-94 • 252.473.5702 Lab/Fax
255-A Wilmington Ftighwat', Jacksonville, NC 28540 • 910.347.5843 I_ab/Fax
ANALYTICAL & CONSULTING CHEMISTS infouemiroil mentalchemists.com
Town of Maysville Date of Report: Dec 04, 2019
Post Office Box 265 Customer PO #:
Maysville NC 28555 Customer ID: 17020023
Attention: Report #: 2019-18771
Project ID: Sludge
Ammonia Nitrogen SM4500 NH3 C 1640 mg/kg 11/18/2019
Total Phosphorus SM 4500 P F 19400 mg/kg 11 /13/2019
Mercury SW8467471B <1.00mg/kg 11/11/2019
TCLP Metals
Arsenic
EPA 200 7
<1.0 mg/L
11/21/2019
Barium
EPA 2007
<1.0 mg/L
11/21/2019
Cadmium
EPA 2007
<1.0 mg/L
11/21/2019
Chromium
EPA 200 7
< 1.0 mg/L
11/21/2019
Lead
EPA 200 7
<1.0 mg/L
11/21/2019
Selenium
EPA 200 7
<1.0 mg/L
11/21/2019
Silver
EPA 200 7
<1.0 mg/L
11/21/2019
Mercury
EPA 245.1
<0.0002 mg/L
11/21/2019
Comment:
Sludge residuals reported on a dry weight basis.
Reviewed by:
a Q \J�j
Report #:: 2019-18771
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX 910-392-4424
info@environmentalchemists.com
Client: Town of Maysville WWTP
PROJECT NAME: Annual Sludge
REPORT NO: / - /V-Jov
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
email:
Sampled B a+MC/ SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other:
Sample Identification
p
Collection
E
m
a o
E c
U
9 `�
C 0
o 0.
`
o'
U
M
m g
Z
PRESERVATION
ANALYSIS REQUESTED
D,atja
Time
Tem
z
z
0
=
0
x
zo
z
_o
w
O
Sludge
a lP
C
P
`{�
X
Full TCLP/Nutrients/Metals/RCI
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Temperature when Received: 5 C Accepted:
Delivered By: R
Comments:
Time: S'�
PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS
PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Towns of Bridgeton and Maysville meet pathogen reduction and vector attraction reduction
requirements through lime stabilization. Craven Ag Services, Inc. performed the lime
stabilizations. This applications were incorporated that same day.
The forms for these facilities are marked appropriately.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Craven Ag Services, Inc. WQ Permit Number: WQ0037637
'V 'WTP Name: Town of Maysville WWTP NPDES Number: NCO021482
.onitoringPeriod: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerfnrmPd-
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) LJ
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathocengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic f l
Beta Ray t...J
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens �1
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ,?l
Air Drying Cl
Coniposting ❑
Aerobic Digestion [J
Anaerobic Digestion v
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Densit r
" }
um er o
1 Excee-
Frequency
ofAnalysis
Sample
Type
n a jca
Tech -
ninm-
Minimuni
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to die
6th power
per gram of
total solids
ivl N
CFU
1000 mpu per gram
of total solid (dry
weight)
monella bacteria
(in lieu of fecal
coliform)
t.
3 MPN per 4 grams
total solid (dry
I wei ht)
vector Attraction Reduction (15A N At 02T .1107) - Please Indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ jAlt.
4 (Spec. O, uptake) U
Alt. 5 (14-Day Aerobic) D
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying -Stable) ❑ 1
Alt. 8 (Drying -Unstable) 0
Alt. 9 (Injection) (..)
Alt. 10 (Incorporation) 1J
No vector attraction reduction alternatives were erformed i_l
CERTIFICATION STATEMENT (please check the appropriate statement)
1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
.I vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
e under my airection ana su
ce with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. John W. Dunham
Mr. John W. Dunham
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
0 ,1p - ) 4-�o -jZ)
Lg t9
a of Preparer* Date ' n ture of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1 2/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Craven Ag Services, Inc. WQ Permit Number: WQ0037637
WIYVTP Name: Town of Bridgeton WWTP NPDES Number: NCO074837
Monitoring Period: From 1/l/2019 To 12/31/2019
thogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ? �
A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs 1J
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo lnilic
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: TA—It(l) Fecal Density ❑ I Alt. (2) Process to Significantly Reduce Pathogens E3
If applicable to alternative per (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization F1 Air Drying ❑ L Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter Allowable Level Pathogen Density Number o Frequency Sample Analytical
in Sludge Excee- of Anal Tech-
g Minimu Geo. Mean Maximu Units ysis Type
Fecal Coliform
ilmonella bacteria
(in lieu of fecal
2 x 10 to the MPl`
6th power
per gram of
total solids CFU
ivvu mpn per gram
of total solid (dry
b1PN per 4 grams
total solid (dry
vector Attraction Reduction (ISA NCAC WT .111171 - PIPasP inrl;ratP altPrnatCvP r%avrnvM A.
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ElAlt.
4 (Spec. O, uptake) El
Alt. 5 (14-Day Aerobic) [IAlt.
6 (Alk. StabilizationEl
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) Cl
Alt. 9 (Injection) J
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
cJ- x it iL m 11V14 a 1 A 1 r ivi it i (please cnecK the appropriate statement)
;J " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
1:1 vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. John W. Dunham
Preparer Name and Title (type or print)
—,i a ure of Preparer* Date
Mr. John W. Dunham
Land Applier Name and Title (if applicable)(type or print)
S ature of Land Applier (if applicable) Date
reparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DFNR FORM PVRF 02T (12/2006)
PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Towns of Bridgeton and Maysville meet pathogen reduction and vector attraction reduction
requirements through lime stabilization. Craven Ag Services, Inc. performed the lime
stabilizations. These applications were incorporated that same day.
Documentation of these activities are found in the following section.
-CRAVEN A_G_SERVICES INC.
Alkaline Stabilization Of Solids Analysis Bench Sheet
Facility Name: S 'c P.O. #
Batch Size ( gallons) Lbs. or Gallons Used: O c ! c - —Material used for Stabilization:r✓lae�✓�l :. ��,
Initial ph 2 Hour pH 24 Hour pH
DATE pH Temp C Corr Fa + Corr. pH Time pH Temp C Corr Fa + Corr H ,Time p pH Temp C Corr Fa + lCorr pH jTime Intial
-
�-
' 30
L
' 70
I
0.30
'G
I,L
a G
,�►, p
4?, 03
:1,'0
IE3
CRAVEN AG SERVICES INC,
'Alkatine, stabifizationOf • •
AAM
..�,M�
,.
"fir
M���
m
W�v
ms
�..
..
1-m-........
m.
m_
CRAVEN AG SERVICES INC.
A aline Stabilization Of Solids Analysis Bench Sheet
Facility Name •
— - --
Batch —Size—(,-
— ' - - -- --
lbs. or Gallons Used: �{ �U — Material used for Stabilization: &Idfy,7- e
Initial ph 2 Hour H -
p I 24 Hour pH
DATE pH Temp C Icorr Fa + jCorr. pH p pH Temp C ICorr Fa + jCorr pH Time pH Temp C ICorr Fa + Corr pH Time Intial
,%_'gyp . �/ h �<<Ii"'Pavi
-- - - - - - -- - 4 r
-- --_
A
G
CRAVEN AG SERVICES INC.
Alkaline Stabilization Of Solids Analysis Bench Sheet
-
Facility Name • .� P.O. #
Batch Sae ( gallons) Lbs. or Gallons Used: a, yao /,4 Material used for Stabilization:
Initial ph 2 Hour pH 24 Hour pH
DATE
pH
JTempC
�CorrFa+
Corr. H
p
Time
IpH
Temp C
Corr Fa +
Corr pH
Time
pH
Temp C
Corr Fa +
Corr pH
Time
Intia I
81
a . I
.66
l�.�y
D
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1349
a;
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T
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9
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CRAVEN AtAG SERVICES INC.
Alkaline Stabilization Of Solids Analysis Bench Sheet
Name: i
Batch Size (gallons) : YZl atrm
Initial ph
Lbs. or Gallons Used: A, YwA
�- 2 Hour pH
-DATE '
pH
Temp C
1(;orrFa+
Corr. pH
Time
LH
Temp C
t
!J-Ys/f
4,77
1e.1
- .!b
j
/a
ct.W
tl�!
le
�(
7.sY
i �. �•
., '. �
'1
tTj�
12•y3
1�•
t -Y•�
P.O. #
Material used for Stabilization: *61.4
24 Hour pH
P` k
IpH
pat,
Corr Fa +
Corr pH
Time
�TempC1CorrFa+jCorrpH
Time
intia I
—Y
13.,L
p'y
—
lost
/00
Q
l f'j�r
t3•;
/t-
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�
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I?pl3
— •?-�
t . !
pf. j°
11.0
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— • 39
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13Ye
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-34
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SOIL ANALYSIS REPORTS
The Town of Bridgeton and Maysville met pathogen reduction and vector attraction reduction
requirements through lime stabilization. The soil pH will continue to be raised through the
continued application of lime stabilized biosolids to these application fields. In addition, application
of mixed ash was applied to Field 3-2.
WaYP•
Ao�nt.�
NALYTICAL
Client :
Craven Ag Services, Inc.
Mr. Billy Durham
2115 Hwy 85 W
Newbern NC 28562
Lab Number:
33733
Test
Method
Results
Soil pH
11
7.6
Buffer pH
Phos horus(P)
M3
412 ppm
Potassium K)
1V13
42 ppm
Calcium c a I
M3
1523 ppm
Ma nesium (M)
N13
44 ppm
Sulfur (S)
M3
13 ppr,
Boron (8)
M3
0.4 ppm
Co er Cu)
M3
2 9 ppm
Iron (Fe
1%13
199 ppm
Manganese (Mn)
M3
8 ppm
Zinc (Zn)
M3
9.4 ppm
Sodium Na
N13
32 ppm
Soluble Salts
Organic Matter
LOI
1 .4 % ENR 72
Nitrate Nitrogen
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 a Fax 901.213,2440
"Every acre... Every years wwW.Waypointanalytical.com
Grower: Report No:
Craven Ag Services Inc.
Field Id :
Cust No:
Date Printed:
Date Received
PO:
Page:
Sample Id: R3-1
SOIL FERTILITY GUIDELINES
Crop : Rye_ Yield Goal : 60 bu/acre Rec Units:
(Ibs) LIME (tons) N pz 05 K vO Mg.,. S B
SOIL ANALYSIS
18-311-0804
24170
11/12/2018
11/07/2018
1 of 6
Exchange Capacity
8.2 meq/100g
% sat meq
K 1.3 0.1
Ca 92.9 7.6
Mg 4.5 0.4
H 0.0 0.0
Na 1.7 0.1
Ratio:
LB/ACRE
u M11 cn - Fe
0 0 86 0 89 18 13 05 0 4 0
tCr
p : M(tlet Pasture Yield Goal : 3 tons/acre Rec Units: LB/ACRE
0 0 90 0 80 18 10 0.5 0 4 0
Comments
Rye
For small grains apply 20-40 lbs N/acre in the fall and the remainder as a top dressing before jointing.
For high yields of small grains or for small grains on wet soils, a split application of spring N may be benefic al.
When small grain is grazed, increase the N fertilization rate by 60 lbs N/Acre. Apply 1/2 in the fall and the rest in mid or
late winter.
On small grains apply recommended P and K before or at planting.
Millet Pasture
• When millet or sorghum sudans are harvested for silage or hay apply 40 lbs N/Acre at seeding and 60 lbs. N/Acre after
establishment. Then apply 60 lbs. N/Acre after each harvest except the last.
• When millets or sorghum sudans are used for grazing apply 40 to 60 lbs N/Acre at seeding and 60 lbs N/Acre per
month during the growing season.
M3 - Mehiich 3 BPH - Lime Index LOI - Loss On Ignition 1.1 - `Nater off
Analysis prepared by Waypoint Analytical Tennessee. Inc.
9-270(
ort No: 104365
punt No: 4365 Waypoint
ANALYTICAL
isor: Harvey Fertilizer Co - Kinston Branch Client: Alan Roach
Robbie Whitfield
1321 Hwy. 258 N.
Kinston NC 28504
2850 Daisy Lane, Wilson, NC
Main 252-206-1721 ° Fax 2S2-206-997
www.waypointanalytical.com
Farm: D. Kylmen
Submitted By: Harvey Fertilizer Co - Kinston Branch
Date Received: 09/27/2019
Date of Report: 09/30/2019
No Field ID
Sample ID
Soll Class HM%
WN pH
Ac
P-1
K-1
S-1
Mn4
Zn-1
Zn-Al
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO: N
142
DK 02A
MIN 2.5
1.3 6.0
2.1
121
87
10
50
155
155
95
6.3
66
48
11
0.8 0
op Recommendations:
Soybeans
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
0
P205
0
K20
0
S
20
Mn
0
Mn-AI
40
Zn
0
Cu
0
B
0
Mg
0
Last Crop
143
DK 02B
MIN 2.6
1.3 5.9
2.3
116
67
15
44
160
160
105
6.2
63
47
10
0.6 0
op Recommendations:
Soybeans
Rec Uom
lb/acre
Lime (Vacre)
0.3
N
0
P205
0
K20
20
S
20
Mn
0
Mn-AI
38
Zn
0
Cu
0
B
0
Mg
0
Last Crop
144 3 iZ
DK 02C >f--ORT'
MIN 3.0
1.2 5.7
2.1
140
51
15
38
128
128
75
6.9
69
55
9
0.6 0
op Recommendations:
Soybeans
Aw 3' 7-
Rec Uom
lb/acre
Lime (t(acre)
0.7
N
0
P205
0
K20
40
S
20
Mn
0
Mn-AI
37
Zn
0
Cu
0
B
0
Mg
0
Last Crop
145
DK 02D
MIN 2.2
1.4 6.1
1.9
107
39
6
50
128
128
80
7.3
74
61
10
0.6 0
op Recommendations:
Soybeans
Rec Uom
lb/acre
Lime (t/acre)
0.0
N
0
P205
0
K20
60
S
20
Mn
0
Mn-AI
38
Zn
0
Cu
0
B
0
Mg
0
Last Crop
146
DK 03A
MIN 3.0
1.2 5.6
1.7
120
46
21
50
200
200
80
6.8
75
60
11
0.6 0
op Recommendations:
Soybeans
Rec Uom
lb/acre
Lime (Vacre)
0.7
N
0
P205
0
K20
40
S
20
Mn
0
Mn-Al
46
Zn
0
Cu
0
B
0
Mg
0
Last Crop
147
DK 036
M-0 3.8
1.1 5.7
2.2
101
57
2
44
183
228
95
7.9
73
58
11
0.6 0
-op Recommendations:
Soybeans
Rec Uom
lb/acre
Lime (t/acre)
0.0
N
0
P205
0
K20
30
S
20
Mn
0
Mn-AI
41
Zn
0
Cu
0
B
0
Mg
0
Last Crop
1148
DK 03C
MIN 2.5
1.4 5.9
1.4
123
87
8
50
123
123
110
7.0
80
64
9
0.7 0
-op Recommendations:
Soybeans
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
0
P205
0
K20
0
S
20
Mn
0
Mn-Al
42
Zn
0
Cu
0
B
.0
Mg
0
Last Crop
!150
DK 03D
M-0 4.2
0.9 5.4
2.7
81
47
21
56
188
234
80
8.5
68
51
9
4.9 0.4
op Recommendations:
Soybeans
Rec Uom
lb/acre
Lime (Nacre)
0.0
N
0
P205
0
K20
40
S
20
Mn
0
Mn-Al
53
Zn
0
Cu
0
B
0
Mg
0
Last Crop
t result units = CEC and Na in meq/100cm3; NO3 N in rng/dm3; WN in g/cm3
th Carolina Division of Water duality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by. Waypoinl Analytical Carolina, Inc.
• T 1
t ort No: 19-270-0521
:count No: 04365 Waypoi nt,u 2850 Daisy Lane, WilsNNMain 252-206-1721 a Fax 2
ANALYTICAL www.waypointanalytical.com
9visor: Harvey Fertilizer Co - Kinston Branch
Robbie Whitfield
1321 Hwy. 258 N.
Kinston NC 28504
mil. A#- Ol.,rd rn
Client: Alan Roach
Farm: D. Kylmen
Submitted By: Harvey Fertilizer Co - Kinston
Date Received: 09/27/2019
Date of Report: 09/30/2019
�- •-� • •a•� •�
.idrurav Im
son crass HM% W/V pH
Ac
P-1
K-1
S-1
Mn4
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO: N
12142
DK 02A
MIN 2.5
1.3 6.0
2.1
121
87
10
50
155
155
95
6.3
66
48
11
0.8 0
.'rop Recommendations:
I- Soybeans
Rec Uom
lb/acre
Lime (Uacre)
0.0
N
0
P205
0
K20
0
S
20
Mn
0
Mn-AI
40
Zn
0
Cu
0
B
0
Mg
0
Last Crop
12143
DK 02B
MIN 2.6
1.3 5.9 '
2.3
116
67
15
44
160
160
105
6.2
63
47
10
0.6 0
^rop Recommendations:
I- Soybeans
Rec Uom
lb/acre
Lime acre
0.3
N
0
P205
0
K20
20
S
20
Mn
0
Mn-Al
38
Zn
0
Cu
0
B
0
Mg
0
Last Crop
12144
DK 02C
MIN 3.0
1.2 X.7 11
2.1
140
51
15
38
128
128
75
6.9
69
55
9
0.6 0
Crop Recommendations:
1- Soybeans
Rec Uom
lb/acre
Lime ( acre)
7
N
0
P205
0
K20
40
S
20
Mn
0
Mn-At
37
Zn
0
Cu
0
B
0
Mg
0
Last Crop
12145
DK 02D
MIN 2.2
1.4 6.1
1.9
107
39
6
50
128
128
80
7.3
74
61
10
0.6 0
Crop Recommendations:
1- Soybeans
Rec Uom
lb/acre
Lime (Uacre)
0.0
N
0
P205
0
K20
60
S
20
Mn
0
Mn-AI
38
Zn
0
Cu
0
B
0
Mg
0
Last Crop
12146
DK 03A -
MIN 3.0
1.2 5.6
1.7
120
46
21
50
200
200
80
6.8
75
60
11
0.6 0
Crop Recommendations:
1- Soybeans
Rec Uom
lb/acre
Lime acre)
t.7l
N
0
P205
0
K20
40
S
20
Mn
0
Mil -Al
46
Zn
0
Cu
0
B
0
Mg
0
Last Crop
12147
DK 03B
M-0 3.8
1.1 5.7
2.2
101
57
2
44
183
228
95
7.9
73
58
11
0.6 0
Crop Recommendations:
1- Soybeans
Rec Uom
lb/acre
Lime (Uacre)
0.0
N
0
P205
0
K20
30
S
20
Mn
0
Mn-At
41
Zn
0
Cu
0
B
0
Mg
0
Last Crop
12148
DK 03C
MIN 2.5
1.4 5.9
1.4
123
87
8
50
123
123
110
7.0
80
64
9
0.7 0
Crop Recommendations:
1- Soybeans
Rec Uom
lb/acre
Lime (Uacre)
0.0
N
0
P205
0
K20
0
S
20
Mn
0
Mn-Al
42
Zn
0
Cu
0
B
0
Mg
0
Last Crop
12150
DK 03D
M-0 4.2
0.9 5.4
2.7
81
47
21
56
188
234 •
80
8.5
68
51
9
4.9 0.4
Crop Recommendations:
1- Soybeans
Rec Uom
Iblacre
Lime (Uacre)
0.0
N
0
P205
0
K20
40
S
20
Mn
0
Mn-AI
53
Zn
0
Cu
0
B
0
Mg
0
Last Crop
3st result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/v in g/cm3
orth Carolina Division of Water Quality Certification 0257, Analysis and fertility recommendations shown on this report are performed In accordance within NCDA guldelinus, Analysis proparod by: W aypoini Analytical Carolina, Inc
2019 APPLICATION SUMMARY TABLE
CRAVEN AG SERVICES, INC
LAND APPLICATION PROGRAM
PERMIT NO. WQ0037637
2019 APPLICATION SUMMARY
........................
......................
............... .
......................
...... ..
............
: :
.............
..............
.........Site:...
......
..........................
........
. . .......
...............
. ....
.
-, -, -'. -, -'. -, -, -, -'. -'..
... .
. .......
................
.
....... .........
..................
... ..........
j 41 .....
.............
- -
...........................
...... . . . .
. ..................
.............
...........................................
.......
..
.
..............................................
.......... .....................
..............................................
....
. ......
...................................
...............
.....
* ... ........
....
.. . . . S6.4�v� ...
..... ......
.............
......
....... ......
........... .
....
Allen Roach
3
-_
1
6.6
Jul-19
42,000
0.37
2.45
Millet
Maysville
7.88
Jul-19
18,000
0.02
0.15
Millet
Bridgeton
2
14.6
1
Mar- 19
18,500
0.01
0.15
Corn (Grain)
Bridgeton
3.57
Nov-19
42,000
0.17
2.45
Rye
Maysville
3
1 6.1
Oct- 19
21,000
0.03
0.18
Wheat (Grain)
Bridgeton
0.79
Number of Fields Applied to:
3 2730
Town of Maysville
Town of Bridgeton
Pruite Health Sea Level
C&P Enterprises
.......... ....
.................
.......
:::Gallons:;:......
................
.....
............:::...::Metric................
.. * ..........
..... .. ..
...
...........................
.
....
...........
....
............................
..............................
.........
. ...... ............
............ ... .... ......
..............................
84,000
4.90
4.46
15
57,500
0.48
0.44
5
0
0.00
1 0.00
0.73
0
0.00
1 0.00
1
Permit Limit 21.73
Branch Residuals Soils, LLC Confidential 2/19/2020 Page 1
2019 APPLICATION CONDITION SUMMARIES
Town of Bridgeton
Havelock, North Carolina
Carven Ag Services
WQ0037637
Annual 2019
Bridgeton WWTP
Farmer: Allen Roach
Acres: 6.6
Site/Tract: 3
Application Method: Incorporated
Field: 1
Percent Solids: 0.20
Residual Report No.: BEI-440A
Crop: Millett
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/3/19
1
18,000.0
Dry
Hot
0.00
Total Gallons
18,000.0
Town of Bridgeton
Havelock, North Carolina
Carven Ag Services
WQ0037637
Annual 2019
Bridgeton WWTP
Farmer: Allen Roach
Acres: 14.6
Site/Tract: 3
Application Method: Incorporated
Field: 2
Percent Solids: 0.20
Residual Report No.: BEI-440A
Crop: Corn (Grain)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/13/19
2
18,500.0
Dry
Warm
0.00
Total Gallons
18,500.0
Town of Bridgeton
Havelock, North Carolina
Carven Ag Services
WQ0037637
Annual 2019
Bridgeton WWTP
Farmer: Allen Roach
Acres: 6.1
Site/Tract: 3
Application Method: Incorporated
Field: 3
Percent Solids: 0.20
Residual Report No.: BEI-440A
Crop: wheat (Grain)
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/24/19
3
21,000.0
Dry
Warm
0.00
Total Gallons
21,000.0
Town of Maysville
Maysville, North Carolina
Carven Ag Services
WQ0037637
Annual 2019
Maysville WWTP
Farmer: Allen Roach
Acres: 6.6
Site/Tract: 3
Application Method: Incorporated
Field: 1
Percent Solids: 1.40
Residual Report No.: 19-47778
Crop: Soybeans
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/1/19
1
42,000.0
Dry
Hot
0.00
Total Gallons
42,000.0
Town of Maysville
Maysville, North Carolina
Carven Ag Services
WQ0037637
Annual 2019
Maysville WWTP
Farmer: Allen Roach
Acres: 14.6
Site/Tract: 3
Application Method: Incorporated
Field: 2
Percent Solids: 1.40
Residual Report No.: 19-47778
Crop: Rye
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/14/19
2
42,000.0
Dry
Cool
0.00
Total Gallons
42,000.0