Loading...
HomeMy WebLinkAboutWQ0031725_Residual Annual Report 2019_202003020 O O O 3 (2 - m CD cu < O CD m m oZ m m m Q- Q � m 3 — v' Q 3 to m 7 O_ Q O CD to J O M X v -< O (D a) n CD m a) 7 CD L• � 7F a1 Z .n•. z CD CL m cAu 0 *' o a n a� � o' O o cfl O Cl) v N UUl N 0 N O ID 3 S N z - O C M 3 -' X a' O n D M v C Q (D � 7 C — 6' Q � •J � (D K a D o 7 O v = _ O v Q 3 - 3. v �u to O :3O_ O 0 O Q O• 7 al 7• 0 O 3 d O 7 Submitted Form Project Contact Information Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues. .......................................................................................................................................................................................................................................................................................................................................................................... Name * Corey Carpentier Email Address* Corey_carpentier@baxter.com Project Information ......................................................................................... Submittal Type* r New Permit Application r Renewal r Annual Report r Other Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted? r Yes r Nor N/A Permit Number* WQ0031725 ApplicantTermittee * Baxter Healthcare Corporation Facility Name * Baxter Healthcare Phone Number* 8287566636 r Modification (Major or Minor) r Additional Information r Residual Annual Report r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Annual report is attached. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) 2019 Annual Sludge Report WQ0031725.pdf 1.74MB Upload only 1 R7F document. NL@iple documents must be combined into one R7F file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required, be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been received. The paper copy shall include the following: o Application Form o All relevant attachments {talcs, soils report, specs, etc.] o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) Mailine address: Division of Water Resources ! Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W - = Raleigh, NC 27699-1617 S12 N.5alisburySt. For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560. * rJ By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/26/2020 Medical Products Baxter February 21, 2020 Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC27699-1617 RE: 2019 Annual Land Application Report Permit No. WQ0031725 Baxter Healthcare Corporation McDowell County Please find the enclosed annual land application report for calendar year 2019. No non- compliance or other irregular events occurred in 2019. If you have any questions or require additional information, please contact me at 828-756-6636. Sincerely, Corey Carpentier Sr. Environmental Engineer Attachment: 2019 Land Application Report (3 copies with enclosures) Cc: EHS File Copy 2019 Baxter Healthcare Corporation 2019 Annual Report Land Application Program Permit No. WQ0031725 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0031725 County: Facility Name (as shown on permit): Land Application Operator: McDowell Year: _ 2019 Baxther Healthcare Corporation Phone: 336-957-7871 Land application of residuals as allowed by the permit occurred during the past calendar year? 21 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Southern Soil Builders, Inc. Total number of application fields in the permit:1 10 Total number of fields utilized for land application during the year: 9 Total amount of dry tons applied during the year for all application sites: 160.39 Total number of acres utilizes for land application during the year:1 67.07 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes LJ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T , I I 1 I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were cornplied with or, in the case of a deviation, prior authorization was received frorn the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and rernediations. 1 1) Vegetative cover was maintained and proper crop management was perfnr;,1cd on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." x[ U + C701� ScorT �-71� . t�t_RgEtrc � YE � 02-1132JZo Permittee Name and Title (type or print) Signature a ermittee Date of - r3 -- Zo 0.," Date Si of Land Applier a dean Date (if different from Permittee) (if different fmm Permittee and Preparer) *D..,,............. .7,. C....,A... nn r'rn n. en, n. . .,r.... ....... ...- ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0031725 Laboratory: 1) Facility Name: Baxter Healthcare -Corporation 2) Residual Source WQ # or WQ0031725 3) NPDES #: 4) WWTP Name: Baxter Healthcare Corporation 5) Residual Analvsis Data Waypoint Conc. Sample or Composite Date Parameter Limit (mg/kg) (mg/kg Percent Solids (%) NA 149 Arsenic 75 8.81 Cadmium 85 1 Copper 4,300 105 Chromium NA 119 Lead 840 8.91 Mercury 57 0.0365 Molybdenum 75 5.82 Nickel 420 32.4 Selenium 100 5 Zinc 7,500 102 Total Phosphorus NA 14300 TKN NA 83200 Ammonia -Nitrogen NA 5300 Nitrate and Nitrite NA 4.67 a For surface disposal facilities the ceiling concenrrnt,nn limit, lictail in thic f.,r.,, .,,,t -r,. W. Le ;-A ..:A...J _ _:. r "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties_"mi>g4alse information, including the possibility of fines and imprisonment for knowing violations." Signaturf Preparer * Date ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ003I725 Facility Name: Baxter Healthcare Corporation Residual Source WQ0031725 NPDES # or WQ#: WWTP Name: Baxter Healthcare Corporation Residual Analysis Data Laboratory: 1) Waypoint 2) 3) 4) 5) Parameter (mg/kg) Sample or .. Date --- -Elm- a ®- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penal ' s for su i .ng false information, including the possibility of fines and imprisonment for knowing violations." - 2 -- /3 -za Signature of Pr arer * Date *PrPnnrPr is riafinaA in AA I -PR Part 1,01 Ofr1 -d 1 r A N[r A r 17 1 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxtller Healthcare Corporation Total Dry Tons Applied (Annual): 12.19 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcC2 Acres Used: 5.5 Acres Permitted: 5.5 Site #: DP Field #: 1A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 1 2 3 4 5 6 7 8 9 10 11 12 Com- posite Date 2/4/19 % Solids 14.9 Arsenic 8.81 Cadmium I Copper 105 Chromium 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 horus Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total 1 DT/Ac. � App. Event 2.22 2 3 4 5 6 7 8 gf 10 11 12 � m y Arsenic 0.039 Cadmium 0.004 Copper 0.465 �hrorrliurn 0.527 Lead 0.039 Mercury 0.002 Mnlvh_ 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00fl 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.039 0.004 0.465 0.000 0.527 0.000 0.000 1 0.039 0.002 denum 10.026 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Nickel 0.144 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.144 Selenium 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Zinc 0.452 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.452 Total Phos- 63.378 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 63.378 horus , I "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". '"' ,f Signature of Land Appher Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxther Healthcare Corporation Total Dry Tons Applied (Annual): 3.44 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcC2 Acres Used: 1.6 Acres Permitted: 1.6 Site #: DP Field #: Ili Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Ll J _2j 3j 4 J L5 6 7 8 g 10 LIJ 12 Com- posite Date 2M/19 % Solids 14,9 Arsenic 8.81 Cadmium I Copper 105 �hromium 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 Annual Heavy Total t DT/Ac.r App. Event 2.15 Arsenic 0.038 Cadmium 0.004 Copper 0.451 �hromium 0.511 Lead 0.038 Mercury 0.002 Molyb- 0.025 denum Nickel 0.139 Selenium 0.021 Zinc 0.438 Total Phos- Metal Field Loadings (Calculated in Ibs/acre): 0 sv 0.000 0.000 0.000 0.000 0.00.0 0.000 0.000 0.000 0.000 0.000 0.000 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.451 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.511 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.00o 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.139 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 0.000 1 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.438 61.461 10.000 10.000 10.000 1 0.000 1 0.000 1 0.000 1 0.000 10.000 1 0.000 10.000 10.000 161.461 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxtlier Healthcare Corporation Total Dry Tons Applied (Annual): 6.60 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcC2 Acres Used: 3 Acres Permitted: 3 Site #: DP Field #: 1C Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or t 2 3 4 5 6 7 L8J g �p �� 12 Com- posite Date 214119 % Solids 14.9 Arsenic 8.81 Cadmium 1 Copper 105 �hromium 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 Annual H Total DT/Ac. App. Event 2.20 Arsenic 0.039 Cadmiujnj 0.004 0.462 0.524 0.039 0.002 0.026 0.143 0.022 0.449 .nromti Lead Mercui Molvb N ickel Selenium Zinc Total Phos- dings (Calculated in lbs/acre): 0 N 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.000 1 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0 00 0.000 0.000 0.000 0.000 0.000 0.039 0.004 0.462 0.524 0.039 0.0 00 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0 00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.143 0.000 0.022 0.000 0.449 62.9201 0.000 f 0.000 10.000 1 0.000 10.000 1 0.000 1 0.000 1 0.000 1 0.000 1 0.000 1 0.000 1 62.920 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1..., 7 ���1 • �aav Sig ature of Land/ Applier Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Residual Anall Sample or 1 Corn- posite Date 2/4/19 % Solids 14.9 Arsenic 8.81 Cadmium I Copper 105 'hromium 119 Lead 8.91 Mercury 0.365 denum 5.82 Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 Baxther Healthcare Corporation Total Dry Tons Applied (Annual): WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: 9.6 Acres Permitted: 9.6 Site #: DP Field #: sis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent Annual Heavy M Total t _ DT/Ac./ App. Event 2.07 Arsenic 0.036 Cadmium 0.004 Copper 0.435 -hro[�Zrp 0.493 Lead 0.037 Mercury 0.002 MnJ"h ated in lbs/acre): 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00( 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00( o.000 o.000 0.000 0.000 0.000 0.000 0.000 O.00( 0.0 00 0.000 0.000 0.000 0.000 0. 000 0.000 0.00( 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.000 o.00C 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00C 0.024 0.000 1 0.000 1 0.000 1 0.000 1 0.000 1 0.000 1 o.000 o.0oo Nickel 0.134 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Selenium 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Zinc 0.422 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Total Phos- 59.202 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 horus "I certify, under penalty of law that this do-e t 19.87 rcL.s ISO] Loj 11 12 y 0 y 0.000 0.000 0.000 0.000 0.036 0.000 0.000 0.004 o.000 0.000 0.000 0.000 0.000 0.000 o.000 o.000 0.435 0.0 00 0.000 0.493 0.000 0. 000 0.037 0.000 0.000 0.002�_ 0.000 0.000 0.024 0.000 0.000 0.134 0.000 0.000 0.000 0.021 0.000 1 0.000 0.000 0.422 0.000 0.000 0.000 59.202 n was piepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". �-y-coif 0 Signature of Land Applier Date ANNUAL, METALS FIELD LOADING SOMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxther Healthcare Corporation Total Dry Tons Applied (Annual): 20.30 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 5.887 Acres Permitted: 5.887 Site #: DP Field #: 3-Corn Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ., - - Com- posite Date 2/4/ 19 % Solids 14.9 Arsenic 8.81 Cadmium I Copper 105 Chromium 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 Annual Heavy Total _J DT/A c./ App. Event 3.45 Arsenic 0.061 Cadmium 0.007 Copper 0.724 :hromium 0.821 Lead 0.061 Mercury 0.003 Molyb- 0.040 denum Nickel 0.223 Selenium 7034 Zinc 0.704 Total Phos- Meta lculated in lbs/acre): 0.000 0.000 0.000 0.00o o.000 0.00o 0.006 c 0.000 O.Oao o.000 0.00o 0.000 0.000 0.000 c 0.000 0.000 0.000 0.000 0.000 0.000 0.000 c 0.000 0.000 0.000 0.000 0.000 0.000 0.000 c 0.000 0.000 0.000 0.000 0.000 0.000 0.000 C 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0 0.000 0.000-1 0.000 0.000 0.000 0.000 0.600 6 0.000 0.000 1 0.000 1 0.000 0.000 0.000 0.000 0 98.641 1 0.000 1 0.000 1 0.000 1 0.0001 0.000 1 0.000 1 0.000 1 0 000 LOJ Jilli2 0 su W 0.000 0.000 0.000 0.061 .000 0.000 0.000 0.000 0.007 .000 .000 0.000 0.600 0.000 0.724 0.000 0.000 0.000 0.821 '000 0.000 0.000 0.000 0.061 000 0.000 0.000 0.000 0.003 000 0.000 0.000 0.000 0.040 000 0.000 0.000 0.000 0.223 000 0.000 0.000 0.000 0.034 000 0.000 0.000 0.000 0.704 000 0.000 0.000 0.000 98.641 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land A �Iier- Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxther Healthcare Corporation Total Dry Tons Applied (Annualy 25.39 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator; Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 6.983 Acres Permitted: 6.983 Site #: DP Field #: 3-Grass ........ n..R. j - uaaa kaicavy lurtais anu i orat rnospnorus use mg/kg, % Solids use Raw Percent #); Sample or L21 3 4 5 71 7 1 8j 9 J10 11 J 12 Com- posite Date 21019 % Solids 14.9 Arsenic 8.81 Cadmium 1 Copper 105 Chromium 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 horus Total - ---o- ♦- 3j 4 �-.�...» ..... 5 .varnuup _2j 6 7 8 9 10 11 12 DT/Ac./ , App. 0 Event 3.64 Arsenic j 0.064 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.064 Tadmiuml 0,007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.764 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.764 Chromium 0.865 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.865 Lead 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 a.o0o 0.003 Molyb 0.042 denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Nickel 0.236 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.236- Selenium 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 Zinc 0.742 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.742 Total Phos- 103.990 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 103.99( horus "I certify, under penalty of law, that this document was prepared under my direction with a system designed to assure that qualified personnel or supervision properly gathered and evaluated in accordance I am aware that there are significant penalties the for submitting false information, including the information submitted. possibility of fines and imprisonment for knowing violations". a�y a Sigi ure of Lai d Ay pplier Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxther Healthcare Corporation Total Dry Tons Applied (Annual): 24.05 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 8.7 Acres Permitted: 8.7 Site #: DP _ Field #; 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #); Sample or L 1-1 L2J L4j 5 6 7 8 9 10 11 12 Com- posite Date 21V 19 % Solids 14.9 Arsenic 8.81 Cadmium l Copper 105 Chronflurni 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 ` 2 3, 4 5 S_ 7� 8 9, 10� 111 2 DT/Ac./ App.° Event 2.76 Arsenic 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 1 0.580 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.580 Chromium 0.658 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.658 Lead 0.049 0.000 0.000 i 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 MolybMercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 denuni 0.032 0.000 0.00o 0.000 0.000 enum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Nickel 0.179 0.000 ---f-0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.179 Selenium 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Zinc 0.564 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.564 Total Phos- 79.050 0.000 0.000 0.000 0.000 h orus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 79 .OSU "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for rryknowing violations". Signature of Land Applier Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxther Healthcare Corporation Total Dry Tons Applied (Annual): 28.21 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FCC2 Acres Used: 15.9 Acres Permitted: 15.9 Site #: DP Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 1 2 L3J L 4 5 L§J 7 LOJ 9 10 11 12 Com- posite Date V4/19 % Solids 14.9 Arsenic 8.81 Cadmium 1 Copper 105 �hrcniium 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 Annual Heavy Total 1 DT/Ac.l App. Event 1.77 Arsenic 0.031 Cadmium 0.004 Copper 0.373 Chromium 0.422 Lead 0.032 Mercury 0.001 Molyb- 0.021 denum Nickel 0.115 Selenium 0.018 Zinc 0.362 Total Phos- Metal Field Load in Ibs/acre 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.00 0.000 0.000 1 0.000 0.000 0.000 0.000 0.00, 0.000 0.000 0.000 0.00 00.000 0.000 0.001 0.000 0.000 o.000 0.000 0.000 0.000 0.001 50.7361 0.000 1 0.000 f 0.000 1 0.000 1 0.000 1 0.000 1 0.001 3 T } } 0.000 0.000 0.000 0.000 0.000 0.000 a w y 0.000 0.000 0.031 6.000 o.000 0.000 0.004 0.000 0.000 7000 0.373 0.000 2200 0.000 0.422 0.000 0.000 0.000 0.032 1 0.000 0.000 6A00 0. 000 0.001 1 0.000 0.000 0.000 0.000 0.021 I 0.000 0.000 0.000 0.000 0,115 1 0.000 0.000 0.000 0.000 0.018 i 0.000 0.000 0.000 0.000 0.362 0.000 0.000 0.000 0.000 50.736 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxther Healthcare Corporation Total Dry Tons Applied (Annual): 10.63 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcC2 Acres Used: 5.5 Acres Permitted: 5.5 Site #: DP Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 2j 1 31 1 a 5 J I 6 1 g F. Com- posite Date % Solids Arsenic Cadmium Copper Chromiuml Lead - 214/19 14.9 8.81 I 105 119 8.91 9 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 horus Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total 1j W 2 3 4 5 6 7 g g DTfAc./ App. Event 1.93 Arsenic 0.034 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0. Cadmium 0,004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0. Copper 0.406 0.000 0.000 0.000 0.000 4.000 0.000 0.000 0.+ Chromium 0.460 0.000 0.000 0.000 0.004 0.000 0.000 0.000 1 Lead 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.1 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.1 Molyb denum 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.1 Nickel 0.125 0.400 0.000 0.000 0.000 0.000 0.000 0.000 0.( Selenium 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.( Zinc 0.394 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.( Total Phos- 55.255 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.( phorus 300 200 )00 )00 10 j11� 0.000 0.000 0.000 0.000 f2 y 0 as W 0.000 0.000 0.034 0.000 0.000 0.004 0.000 0.000 0.406 0.000 0.000 0.460 )00 )00 )00 100 0.000 0.000 0.000 0.000 0.034 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.022 0.000 0.000 0.125 100 100 100 0.000 0.000 0.000 0.019 0.000 0.000 0.000 0.394 0.000 0.000 0.000 55.255 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for [snowing violations". Signature of Land A plies Date ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxther Healthcare Corporation Total Dry Tons Applied (Annual): 9.71 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FCC2 Acres Used: 4,4 Acres Permitted: 4.4 Site #: DP Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #}: Sample or ?. 2 3 4 5 6 7 8 9 10 11 12 Com- posite Date 214119 % Solids 14.9 Arsenic 8.81 Cadmium 1 Copper 105 Chromium' 119 Lead 8.91 Mercury 0.365 Molyb- 5.82 denum Nickel 32.4 Selenium 5 Zinc 102 Total Phos- 14300 Annual Heavy Total 1 DT/Ac.l App. Event 2.21 Arsenic 0.039 Cadmium OA04 Copper 0.463 Chromium 0,525 Lead 0.039 Mercury 0.002 Molyb- 0 026 denum Nickel 0.143 Selenium 0,022 Zinc 0.450 Total Phos- etal Field Loadings (Calculated in lbs/acre): 2 3 1 1.71 j 5 1 1 6 7 0.000 0.000 o.000 - a.oao 6.066 o.000 a. 0.000 0.000 0.000 0.000 0.0 00 0.000 0. 0.000 0.000 0.000 -00 0.000 0.000 0.000 0. 0.000 To o.oao 0.000 0.000 0.000 0. 0.000 0.000 0.000 0.000 0.000 0.000 0. 0.000 0.000 0.000 0.000 0.000 0.000 0. 0.000 0.000 0.000 0.000 0.000 0.000 0. 0.000 0.000 0.000 0.000 0.000 0,000 0.� 0.000 0.000 1 0.000 0.000 0.000 0.000 0,1 0.000 0.000 0.000 0.oao TO-0 0-1 0.000 0.1 63.120 f 0.000 1 0.00o 1 0.000 j 0.000 I 0,000 1 0.000 1 o.l 9 10 11 12 0 w c� y 000 0.000 0.000 0,000 0.000 0.039 300 0.000 0.000 0.000 0.000 0.004 )00 0,000 0.000 0,000 0,000 0.463 )00 0.000 0.000 500 0.000 0.525 )00 0.000 o.oao 0.000 0.000 0.039 )00 0.000 0.000 0.000 0.000 0.002 )00 0.000 0.000 0,000 0.000 0.026 )00 0.000 0.000 0.000 0.000 0.143 )00 0.000 0.000 0.000 0.000 0.022 100 0.000 0.000 0.000 0.000 0.450 00 0.000 0,000 0.000 0.000 63.120 "I certify, under penaity of law, that this document was prepared under my direction or supervision Nn, accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations ) Signat ire of Land Applier a 6 Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: 1A Acres Utilized: 5.5 Land Owner: Douglas Poplin Annual Dry Tons Applied: 12.1857 Site #: DP Acres Permitted: 5.5 Operator: Douglas Poplin Predominant Soil Series: FcC2 Cation Exchange Capacity (non 503): Crop I Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: Volume applied (enter one) Solids/ O Liquid Cu. Yds Gallons -19 97.11 kLS:l 97.11 ual I bs/acre Volume Residual Sources Joif Applied per (NPDFS #, WQ#, Cond Solids Acre Fen., Animal (Dry' (Dry TonslAc} Waste, etc) Wet' Moist 14.9 2.216 WQ0031725 dry 0.000 0.000 0.000 o.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 r Years Cumulative lbs/ac •ent Cumulative Ibs/ac fitted C. P. L. R.**** iit PAN Limit I st/2nd C Residuals Applic As Cd Cu 0.039 0.004 0.465 0.16 0.051 2.794 0.199 0.055 3.259 36 34 1338 Precip. > Past 24 Hrs, o a ^ t Q• inches ,t tions totals on FORM FSF Cr I Pb I Hg 0.527 0.039 0.002 1.857 0.0242 0.009 2.384 0.064 0.011 NA 267 I5 Nitrate PAN A Iced pp Name of Crop Type and ]bs/acre}NitriteA Receiving Residual U50. JTKN lication PP mg/kg Ci Crop 2 Crop I Crop 2 3 4.67 115.320 NA Fescue ipp ( attach FORM FSF su Mo Ni Se 0.026 0.144 0.022 0.124 0.643 0.106 0.150 0.787 0.128 NA 374 89 0.000 0.000 0.000 0.000 o.000 0.000 0.000 0.000 0.000 0.000 0.000 p to this form): Zn I P 1115.320 0.452 63.378 4.507 4.959 2498 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lime Applied Date lbs/ac 0 158 srtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false rmation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation ?� l+w **Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ003I725 Field #: IB Land Owner: Douglas Poplin Annual Dry Tons Applied: 3.4383 Acres Utilized: 1.6 Operator: Douglas Poplin Predominant Soil Series: FcC2 Site #: DP Acres Permitted: 1.6 Crop 1 Name: Fescue Crop I Max. PAN: 158 Cation Exchange Crop 2 Name: Capacity (non 503): Crop 2 Max. PAN: Volume applied Volume Soil Residual Sources Precip. 0 3 z D 15 (enter one Solids/ o /o Cond. K Applied per (Npp£S # WQ#, Past 24 c'o z » TICN o y Nitrate PAN Applied Name of Crop Type Liquid Solids Acre (Dry, s �' (Dry, Animal Firs. o w R = � °� N' * o0 o �, and ( lbs/acre) Receiving Residual Cu. Yds GaIlOr1S a Waste, etc Wet' * o (Dry Tons/Ac) � � * N' * • » " Nitrite Application - 14 27.4 Moist } ruches � mglkg mg/kg mg/kg Crop I Cro 2 Cro 7 tit t ,®ram ■�� t t t t �����■��� t t t; t t t t �� t t t t ���■���.�� t t t t t t t _- �� �� t t t t �����.■��.... t t;; t t t t �� .LS:l 27 ual Ibs/acre Years Cumulative Ibs/ac ent Cumulative lbs/ac fitted C. P. L. R.**** it PAN Limit 1st/2nd C ' r F supp ( attach FORM FSF supp to this form): As Cr36 Cr Pb H Mo Ni Se Zn p 0.038 0.00 0.511 0.038 0.002 0.025 0.139 0.021 0.438 6L461 0.158 0.04 1.734 0.227 0.009 0.118 0.603 0.103 4.193 0.196 0.05 2.245 0265 0.011 0.143 0.742 0.124 4.631 36 341338 NA 267 IS 1 NA 1 374 89 2498 111.8491 0.000 1 LimeApplied Date Ibs/ac 11-19 1 000 rtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false 'mation, including the possibility of fines and imprisonment for knowing violations." ,„� *Application Method: S - Surface, IN - Injection, INC - Incorporation D Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date " Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Heahbcare WQ Permit #• W 0031725 ' Q Field # I Acres Utilized: 3 Land Owner: Douglas Poplin Annual Dry Tons Applied: 6.6004 Site #• Df Operator: Douglas Poplin Predominant Soil Series: FcC2 Acres Permitted: 3 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: Volume applied PP Volume Soil Residual Sources Precip. y c � z Y Nitrate o (enter one) Solid4: ob Applied per (NPDES #, WQ# Cond. Past 24 w TKN _ PAN Applied Name of Crop Type Liquid Solids Acre (Dry, - Fert., Animal Hrs. o N' �, in - o3 o c, 0 and ( lbs/acre) Receivin; Residual Cu. Yds Gallons Waste, etti s Wet' = N Nitrite Application (Dry Tan51Ac; Moist,, inches mg/kg mg/kg mg/kg Crop I Crop 2 Crop I Crop 2 -19 52.6 14.9 2.200 WQ003172; dry D S 0.5 0.3 83200 5300 4.67 I14.516 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF 0.000 1 0.000 %LS 52.6 0 As Cd Cu Cr Pb H Mo 1 supp Ni I Se to this form): TJ4.51b uallbs/acre 0.039 0.004 0.462 0.x:24 0.039 0.002 0.026 0.1430.022 Zn 0.449 P 1 0.0o0 Lime Applied r Years Cumulative !bs/ac 0.739 0.063 3.328 2.11 0.278 0.011 0.142 0.744H0.122 5.608 62.920 Date Ibs/ac 'ent Cumulative Ibs/ac 0.778 7 0.067 3.790 2.634 0.317 0.013 0.168 0.887 0.144 6.057 11-19 1000 Witted C. P. L. R.**** 36 34 NA 267 IS NA 374 89 2498 iit PAN Limit I st/2nd Crop 158 mtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lifted personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false rmation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection:/Incorporation - 1.0 Signature of Land Applier'�" Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 **"*C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" 1N A BLANK OR BOX WHEN NOT APPLICABLE Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: 1D Acres Utilized: 9.6 Land Owner: Douglas Poplin Annual Dry Tons Applied: 19.8766 Site #: Dp Acres Permitted: 9.6 Operator: Douglas Poplin Predominant Soil Series: Cation Exchange Capacity g P Y (non 503): Crop 1 Name: Fescue Crop I Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: volume applied Volume Residual Sources Soil Precip. D � � � Nitrate one) Solids! I� p App ed er (NPDES #, WQ#, Cond. Past 24 F v Nz i KNo0 3/o J-,��(enter Liquid Solids Acre Animal (Dry, lirs. = �' o ^, = " - 0Fert., and Yds Gallons (Dry TonslAc) Waste, etc ) Wet, p- ,N�, # * �, Nitrite -2019 158.4 14.9 2.070 WQ0031725 MoiSt) dry inches 0 _ mglkg mglkg mglkg S 0.5 0.3 83200 5300 4.67 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 +--7 "ALS: Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 158.41 01 As Cd I Cu I Cr I Pb I Ha I Mo Ni I Se 1 Zn P Waal !bs/acre 0.036 0.004 0.435 0.493 0.037 0.002 0.024 0.134 0.021 0.422 59.202 or Years Cumulative Ibs/ac 0.156 0.047 2.606 1.716 0.247 0.007 O.nS 0.58 0.087 3.972 rrent Cumulative Ibs/ac 0.192 0.051 3.041 2.209 0.284 0.009 0.139 0.714 0.108 4.394 miffed C. P. L. R.**** 36 34 1338 NA 1 267 15 NA -nit PAN Limit lst/2nd Crop 374 89 1 2498 PAN Applied ( Ibs/acre) Crop 1 107.767 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.000 0.000 107.767 Crop 2 NA 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 Name of Crop Type Receiving Residual Application Crop I Crop 2 Fescue 0.000 Lime Applied Date Ibs/ac 0 158 :ertify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that diked personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false )rmation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation aua6_ "Volatilization Rate: Surface - 0.5, Injection/Incorporation - I.0 Signature of Land Applier Date x** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ""C.P,L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLI Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 CABLE. Field Land Owner: Dou Douglas Poplin g P #: 3-Corn Acres Utilized: 5.887 Annual Dry Tons Applied: 20.3033 Site #: DP Operator: Douglas Poplin Predominant Soil Series: FcB2 Acres Permitted: 5.887 Crop1 Name: Cation Exchange Capacity (non 503 )� Corn Crop 1 Max. PAN: 214 Crop 2 Name: Crop 2 Max. PAN: i Volume applied (enter one Solids/ ) Volume Soil Residual Sources Precip. > Cond. o S Nitrate i o o /o Liquid Solids Applied per Acre (NPDES #, WQ#, Past 24 (Dry, n � y ? z CD ;, TKN " o PAN Applied and Name of Crop Type Receiving 1 Fert., Animal Hrs. 5 a, (1bs/acre) Residual Cu. Yds Gallons (Dry Tons/Ac) Wet, a Waste, etc) o" * g m' Nitrite Application 2019 161.8 14.9 3.449 Moist) inches WQ0031725 dry 0 o mg/kg mgAg mglkg Crop i Crop _ Crop 1 Crop 2 0.000 Inc I 0.3 83200 5300 4.67 197.788 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.000 0.000 0.0oo 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 'kLS:1 161.81 p+ ival lbs/acre r Years Cumulative lbs/ac •ent Cumulative Ibs/ac nitted C. P. L. R.**** in PAN Limit Ist/2nd Crop Residuals App As I Cd Cu 0.061 0.007 0.724 0.395 0.126 1.512 0.456 0.133 2.236 36 34 1338 [ions totals on FORM FSF supp ( attach FORM FSF Cr I Pb I Ha I Mo I Ni I Se 0.821 0.061 0.003 (?.0400.223 0.034 4.609 0.596 0.02 0.271 1.421 0.568 105.430 0.657 0.023 0.311 NA 267 15 0.000 0.000 1p to this form): Zn P 197.788 "000 Lime Applied 0.704 98.64] Date lbs/ac 13.144 0 13.848 2498 :rtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false rmation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation D"W • a` 51kO **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: 3-Grass Land Owner: Douglas Poplin Annual Dry Tons Applied: 25.3942 Acres Utilized: 6.983 Operator: Douglas Poplin Site #: DP Acres Permitted: 6.983 Predominant Soil Series: Crop 1 Name: Fescue Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 194 Crop 2 Name: Crop 2 Max. PAN: Volume applied � � (enter one) Solids/ o o /o Volume Applied per Soil Residual Sources Cond. Precip. � (NPDES #, WQ#, Past 24 �_ n o _� z D Nitrate y fD PAN Name of crop Type } - Liquid Solids Acre Fert., Animal (Dry' Hrs. o m w �' TKN o ? * N ; " Jr, o and Applied (lbs/acre) Receiving Residual Cu. Yds Gallons (Dry TonslAc) Waste, etc Wet, n o ) R t ^ Nitrite „ y ' Application 2019 130.52 14.9 2.345 Moist mcties WQ0031725 d fy 0 o2 mg/kg mg/kg mg/kg Cr0 1 Cr0 P p _ Crop I Crop 2 2019 71.85 14.9 1.291 S WQ0031725 dr0 0.5 0.3 83200 5300 4.67 122.078 NA Fescue 0.000 y S 0.5 0.3 83200 5300 4.67 67.203 NA Fescue 0.000 0,000 0.000 0.000 0.000 0,000 o.000 0.000 0.000 a.000 o.000 o.00a 0.000 o.oao o.000 0.000 0.000 0.000 0,000 0.000 O.00o 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF 0.000 0.000 4LS: 262.37 0 As Cd Cu Cr Pb supp to this form): ual s/acre 0.064 H 0.007 0,764 0.865 0.065 0.003 Mo Ni 0.042 189.281 0.000 Lime ADD lied r Years rs Cumulative ]bs/ac 0.387 0.131 6.904 4.576 0.592 0.236 0,036 0.742 103 990 Date I lbs/ac -ent Cumulative lbs..ac 0.451 0.02 0.138 7 668 5 441 0 6 0.281 L42 0.581 13 168 0 57 0.02J 0.323 1.656 0.617 13.910 � fitted C. P. L. R. * * * * tit PAN Limit st/2nd 36 34 1338 NA 267 15 NA 374 89 2498 lCrop -rtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submittingfalse -mation, including the possibility of fines and imprisonment for knowing violations." Jc f *Application Method: S - Surface, IN - Injection, INC - Incorporation 07�`1-Zoac **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date "** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate AININ UAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031715 Field Land Owner: Dou Douglas Poplin g P #: 4 _ _ Acres Utilized: 8,7 Annual Dry Tons Applied: 24.0427 Site # DP Operator: Douglas Poplin Predominant Soil Series: FcB2 Acres Permitted: 8.7 Cation Exchange Capacity (non 503): Crop I Name: Fescue Crop I Max. PAN: 194 Crop 2 Name: Crop 2 Max. PAN: Volume applied Volume Residual Sources Soil Preci p' < K a .. o enter one Solids/ o ( ) /o Applied per (NPDES #, WQ#, Cond Past 24 O - Z Nitrate �' 2 c PAN Applied Name of Crop Type Liquid Solids Acre Fert„ Animal (Dry, Hrs. a TKN �" ° °' rra o and t �, a (lbs/acrc) Receiving Residual Cu. Yds Gallons (Dry TortslAc} Waste, etc) Wet a * '� ' iv Nitrite application >.019 535 14.9 0.772 Moist) inches WQ0031725 dry 0 o' m /k g 9 mglkg mg/kg Crop 1 Crop 2 Crop ] C2 rop >019 1381 34.9 1.992 s WQ0031725 d'0 y 0.5 0.3 83200 5300 4.67 40.164 NA Fescue 0.000 S 0.5 0.3 83200 5300 4.67 103.676 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 070 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF 0.000 0.000 BLS 191.E o As Cd Cu supp ( attach FORM FSF supp to this form): uallbs/acre 0.049 Cr Pb Ha 0.006 0.580 0.658 0.049 MO Ni Se Zn P 143.840 00 .00 Lime Applied r Years Cumulative 165/ac 0.295 0.002 0.094 4.999 0.032 0.179 0.028 0.564 79.050 Date lbs/ac -ent Cumulative lbs/ac 0.344 3.425 0.42 0.015 0.100 5 579 4 083 0 469 0.206 1.156 0.151 9.532 11-19 1000 0.238 l.335 0.179 l0.096 pitted C. P. L. R.**** 36 34 1338 NA 267 0.017 15 NA 374 89 2498 it PAN Limit Ist/2nd Crop ,rtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false -mation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: 5 Acres Utilized: 15.9 Land Owner: Douglas Poplin Annual Dry Tons Applied: 28.2113 Site #: DP Acres Permitted: 15.9 Operator: Douglas Poplin Predominant Soil Series: FcC2 Cation Exchange Capacity (non 503): Crop 1 Name Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: Volume applied pp Volume Residual Sources Soil Precip. D < o K �. z y Nitrate Name of Crop "Type (enter one) Solids/ % Applied per Pp p (NPDES #, WQ#, Cond. Past 24 C X ? n, - z 0 a+ TKN 3 o 3 and PAN Applied Receiving Residual 0 Li Liquid 9 Solids Acre Fert., Animal (Dry, Hrs. - �' o a - �' �' tlO ° Nitrite ( Ibs/acre) Application Cu. Yds Gallons {Dry TonslAc) Waste, etc) Wet, Moist) inches Q q O r g mglkg mglkg mglkg Crop 1 Crop 2 Crop 1 Crop 2 !019 83.8 14.9 0.661 WQ0031725 dry 0 S 0.5 03 83200 5300 4.67 34.423 NA Fescue !019 14102 14.9 1.113 W00031725 dry 0 S 0.5 03 83200 5300 4.67 57.928 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ALSI 224.821 01 As Cd Cu Cr Pb Ho Mo Ni Se Zn P 92.351 0.000 Lime Applied wallbs/acre 0.031 0.257 0.288 36 0.004 0.079 0.083 34 0.373 4.216 4.589 1338 0.422 2.8 3.222 NA 0.032 0.373 0.405 267 1 0.001 0.014 0.015 15 1 0.021 0.174 0.195 NA 1 0.115 0.982 1.097 374 1 0.018 0.117 0.135 89 0.362 8.137 8.499 2498 50.736 Date lbs/ac ►r Years Cumulative lbs/ac 11-19 2000 rent Cumulative lbs/ac n itted C. P. L. R.* * * * nit PAN Limit Istl2nd Crop 158 entry, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false ,rmation, including the possibility of fines and imprisonment for knowing violations." �n *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: ti Land Owner: Douglas Poplin Acres Utilized: 5.5 Annual Dry Tons Applied: 10.6260 Site #: DP Operator: Douglas Poplin Acres Permitted: S.5 Predominant Soil Series: FcC2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: Volume applied Volume a o z a Nitrate Soil Residual Sources PJrs. enter one Solids/ o o ) /o Applied per Cond. Name of CropType (NPDES #, WQ#, Pa^ a m d fD TKN PAN Applied YP Liquid Solids Acre o (Dry. - �' �, - a, o and (1bs/acre) Receiving Residual Fen., Animal Ho , N � 0 Cu. Yds Gallons (Dry Tons/Ac} Nitrite Waste, etc Wet, n o• w �' Application ) ° 019 84.68 14.9 1.932 moiS[) in mglkg mglkg mg/kg Cro I Cro W 0031725 Crop 1 Crop 2 Q dry 0.000 s 0.5 0.3 83200 53004.67 100.559 NA Fescue 0.000 o.000 o_ooa 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0.000 0.000 0.,000 000 0.000 0.000 o.000 0.000 0.000 0.000 0.000 0.000 0.00o 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp { attach FORM FSF iLS: 84.681 01 As supp to this form): Cd Cu Cr Pb Ha I Mo Ni I Se I Zn ual lbs/acre 0.034 P 100.559 O.o00 Lime Applied 0.004 0.406 0,460 0.034 0 001 0.022 0.125 0.019 0.394 Years Cumulative lbs/ac 0.349 55.255 Date lbs/ac 0.106 5.816 4.046 0.532 0.016 0.231 1.135 0.134 ent Cumulative Ibs/ac 0.383 11,233 0.1 10 6.222 4.506 0.566 0.017 0.253 1.260 0.153 11.627 0 fitted C. P. L. R. * * * * 36 34 1338 NA 267 I S NA 374 89 2498 it PAN Limit I st/2nd Crop 158 •rtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ified personnel properly gathered and evaluated the information submitted. I am aware that there are significant for •mation, including the possibility of fines penalties submitting false and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 9' **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: 7 Acres Utilized: 4.4 Land Owner: Douglas Poplin Annual Dry Tons Applied: 9.7124 Site #: DP Acres Permitted: 4.4 Operator: Douglas Poplin Predominant Soil Series: Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: Volume applied pp Volume Residual Sources Soil Precip. > 0 3 z D Nitrate Name of CropType YP y enter one Solids/ ( ) o /o Applied per (Ni PDES #, WQ#, Cond. Past 24 K m v m ? y TKN o R and PAN Applied pp ReceivingResidual Liquid Solids Acre Fert., Animal (Dry, Hrs. 3 oN" = „ S° - °O o Nitrite ( Ibs/acre) Application Cu. Yds Gallons (Dry TonslAc) Waste, etc) Wet Moist) mches x �' mglkg mg/kg mglkg Crop 1 TCrop 2 Crop 1 Crop 2 ?019 T 77.4 4 _- -__- -_ NOT, rfl 1 111 _- -__- ___- -__- -__- -_ _- -_-- -_-- Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): -T- 'ALS.1 nuallbs/acre 77.401 As 0.039 Cd 0.004 Cu 0.463 Cr 0.525 Pb 0.039 Hg 0.002 I Mo 0.026 Ni 0.143 Se 0.022 Zn 0.450 I P 114.892 1 0.000 63.120 Lime Applied Date Ibs/ac )r Years Cumulative lbs/ac 0.289 0.084 4.611 3.104 0.413 0.015 0.19 1.085 0.131 8.677 0 -rent Cumulative Ibs/ac 0.328 0.088 5.074 3.629 0.452 0.017 0.216 1.228 0.153 9.127 mitted C. P. L. R. * * * * 36 34 1 1338 1 NA 267 15 NA 374 89 2498 nit PAN Limit lst/2nd Crop I 158 :ertify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that tlified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false )rmation, including the possibility of tines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation -.700 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate Report Number: 19-037-0200 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 A'm'h Waypoint ANALYTICAL Project : Baxter 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.way pointanalytical.com Lab Number: 64662 REPORT OF ANALYSIS Date Sampled: 2/4/2019 14•.00-.00 Sample Id :Baxter Date Received: 02/06/2019 00:00 __ Date Reported: 02/18/2019 Total Solids 14.90 149000 100.0 CJR 02/11/2019 16:17 Moisture' 85.10 100.0 CJR 02/11/201916.17 Total Kjeldahl Nitrogen 8.32 83200 250 CLP Phosphorus 02/14/2019 14= 1.43 14300 50.0 CCR 02/1412019 05:02 Potassium 0.69 6880 50.0 KKM 02/1412019 05:02 Sulfur 1.03 10300 50.0 CCR 02/14/2019 05:02 Calcium 0.94 9360 250 CCR 02/1412o19 05:02 Magnesium 0.44 4440 50.0 CCR 02/14/2019 05:02 Sodium 0.36 3610 250 CCR 02/14/2019 05:02 Iron 7670 50.0 CCR 02/14)2019 05:02 Aluminum Manganese 1450 50.0 KKM 02/14a019 20,32 Copper 102 5.00 KKM 02/14/2019 05-02 Zinc 105 2.50 CCR 02/1412019 05.02 Ammonia Nitrogen 102 12.5 CCR 02/14/2019 05:02 Organic N 0.53 5300 100 ZBD 02/12/2079 13:00 Nitrate+Nitrite N 7.79 77900 250 02/12/2019 13:00 <4.67 4.67 ZBD 02/12/2019 14:30 All values are on a dry weight basis except as noted by asterisk Detection lima on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time , SM-2540G SM-254OG SM-4500-NH3C-TKN 601 OD 601 OD 601 OD 601 OD 6010D 601 OD 601 OD 601 OD 6010D 601 OD 6010D SM-4500-NH3C CALCULATION 45001\103P-2011 OF Gor Pawir Mrrrnarl/ Report Number: 19-037-0200 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River. NC 28669 Waypoint-(D ANALYTICAL Project : Baxter 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www-waypointanalytica l.corn Lab Number: 64662 REPORT OF ANALYSIS Date Sampled: 2,412019 14:00'00 Sample !d :Baxter Date Received: 02/06/2019 00:00 n..e 0------ A. An 1, n in - Chromium -- %.Irl uU14IZu19 05:02 6010D Nickel 119 2.50 CCR 02/14/2019 05:02 6010D Lead 32.4 2.50 CCR 02/14/2019 05 02 601 OD Arsenic 8.91 3-00 CCR 02/14.2019 05:02 6010D Mercury 8.81 5-00 CCR 02114,"2019 05:02 6010D Selenium<5.00 0.0365 0.0155 TJS 02/11 /2019 13.27 SW -7471 B pH • 5.00 CCR 02/14/2019 05.02 6010D Molybdenum 7.3 SAJ 021l2J2019 06:49 9045D Comments: 5.82 250 CCR 02114I2019 05.02 6010D All values are on a dry weight basis except as noted by asterisk Detection limit on all N series is on a wet basis B - Analyte detected in blank H - Beyond Holding Time 1"C Gem P�L4 r PR ri.- Urr:rnor.. 'G► Rate TKN NH030 NO3 80 350.3 4.67 PAN Surface 26024.67 mg/kg 52.04934 Ibsld ton 0 lbs total PAN #DIV10! Ibs PAN/acre PAN Injection 28674.67 mg/kg 57.34934 Ibs/d ton 0 Ibs total PAN #DIV/01 Ibs PANlacre ry Tons/1000 gal. 0.62133 '� :t year PAN Ibs./acre arFace Ibs• Surface0 #DIV/OR t year PAN Ibs./acre ecte�d lbs 0 J injected --� #DIV/OR NO2 % Solids ARREed on 0 0.149 MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg mg/kg x .002=lbs/dry ton MR(TKN-NH3) + 1(NH3)+NO3+NO2 =mg/kg mg/kg x .002 =Ibs/dry ton 1000 X 8 34 X %solids X s rave "=dry tons/1000gal." 2000 SAR Sodium Absorption Ratio Na: Sodium (Mg/L) Equivalent weight: 23 Ca: Calcium (Mg/L) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 Milli Equivalent = Mg/L / Equivalent weight Na M /L Ca M /L M M /L 537.89 1394.64 661.56 Na (ME] Qp—(ME�. Mg -(ME) 23.38652 69.732 55.13 SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent))0.5 power SAR = 2.959821 (From Mg/L entered above) SAR= 0.417061 ](From ME entered below) Na ME Ca ME Mg OSN 0.29 1 0.328 0.639 The amour amount of c Permitting A�L Project 1 tix t ��I�I III INIIId����,�lll���[I1II�1[��Illfllllll�i�o '.�° � Saaur t2 to 11 Submitted By Southern Soil Builders, Inc 958 Hoots Road Roaring River, NC 28669 Charge To Southern Soil Builders, Inc 958 Hoots Road Roaring River. NC 28669 Sample Information FOUY Copy To Southern Soil Builders. Inc. 958 Hoots Road Roaring River, NC 28669 Sampie i3 La'.,m,ber CNkc!.-or. Inljr' 9!,Gr. Cenlainer wa-ma:ion ?!ease Check Des -red Tests !Lay1JUsc Orly; YAe mate ',me Number 1 7 5C3 Nitro en ;of 80!tfes YA= Vol��e SLt 5-2 9 .w IESalids, + petals Series CC= i4wL—s `z Camoosi!e 7 -pa nn i P 'lactc —" 1.41 ;"� V Gmn }last C-ab• ai i ! — Gaass i oz i I r Grab Ij t Glass oZ I Test Packs a Details 1,.: �.:i:_ I'4"� 4�I � ♦ 1'.. �r'.'' �: "" \!. ._ems �. 1j , D3 Metals: A,-W_ti'C. CaC^^ ,.+7 w;t-gm�urn-!vie.-�;,y. V �ly':Yen�,T '. eao \,"Chl�. ;•r'-le^,i,l�'. (Copse- & Zv,c -c..ded ')SLZ2 CE: Car„•�r.: -;"- �;e�x'..' LIP:-.. Cabo;'a;3 Ecu:vatPn'. c• ":!alneuraUza;:orr VaP�e'For _r..•e 'rc:3:a�y 4'uo�e; Account 46381 Otae,s Analytical Results x +� S Southern Soil Builders 958 Hoots Roadf Roaring River, NC 28669 Receive Date: 05/21/2019 Reported: 05/23/2019 For: Baxter Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 190521-41-01 Fecal Coliforms B-1 113475 MPN/g SM92210E-2006 05/21+2019 WC 190521-41-01 Percent Solids B-1 14.11 % SM25408-2o11 05/22)2019 WC 190521-41-02 Fecal Coliforms B-2 97561 MPN/g SM92210E-2008 05121l2019 WC 190521.41-02 Percent Solids 8-2 16.4 % SM25408-2011 05/22f2019 WC 190521-41-03 Fecal Coliforms B-3 114286 MPN/g SM92210E-2008 05/2112019 WC 190521-41-03 Percent Solids B-3 14 % SM254OB-2011 05/22/2019 WC 190521-41-04 Fecal Coliforms 8-4 114286 MPN/g SM02210E•2006 05/21/2019 WC 190521-41-04 Percent Solids B-4 14.0 % SM254OB-2011 05/22;'2019 WC 190521-41-05 Fecal Coliforms B-5 110345 MPN/g SM92210E-2008 05-121;2019 WC 190521-41-05 Percent Solids B-5 14.5 % SM25408-2011 05/22/2019 WC 190521-41-06 Fecal Coliforms B-6 111889 MPN/g SM92210E-2006 05/21/2019 WC 190521-41-06 Percent Solids B-6 14.3 % SM25409.2011 05/22/2019 WC 190521-41-07 Fecal Coliforms B-7 113475 MPN/g SM92210E-2006 05/21/2019 WC 190521-41-07 Percent Solids B-7 14.1 % SM25408-2011 05/22/2019 WC Respectfully submitted, ,.c )i' -" (A,J) )1 !,, , Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 190521-41-01 TeMD on Arrival: 5A Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Collforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 190521-41-02 Temp on Arrival: 5.4 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 190521-41-03 Tem on Arrival: 5.4 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 190521-41-04 Temp on Arrival: 5.4 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 190521-41.05 Tem on Arrival: 5.4 Parameter Schedule: Percent Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 4 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 190521-41-06 Temp on Arrival: 5.4 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Collforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 190521-41-07 Temp on Arrival: 5.4 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 Analytical Results 4r, STATE aVIUr ANALYTICAL Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 04/11/2019 Reported: 05/2412019 For: Baxter Comments: Sample Number parameter Sample ID Result Unit Method Analyzed Analyst 190411-20-01 30 Day Benchscale Baxter 12.9 °'o EPA625•R•9210 Analyzed An WC Respectfully submitted, ,9n wo, J'Y1-,- , Dena Myers NC Cert #440, NCDW Cert #37765, EPA #NC00909 PO Box 228 • Statesville, NC 28687. 704/872/4697 Page 1 of 3 Condition of Receipt Sample Number 190411-20-01 Temp on Arrival: Parameter Schedule: Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 3 14•1 Lab -ID s A j?C-9S')--+ itioned by. 4`11-�w IC V) PX4'M nmqueeed rw .Wyws Relinquished by: ct Time /?� a�pm oat, � 1 jj 1 Received by: �� Timezz-6 am, otfp Date y/� Imo/ Relinquished by: Time :1� am, pm Date /__/ Received by: 24@ow-It-Sam21ing Al Time begin am, pm Date _! I Time end am, pm Date._// 9 t2' Time begin+ am. pm Date ___/___/ Time end am, pm Date Time am, pm Date Lab Comments: STATESVUJXANALMCAL 122 Court Sum • P.O. Bad 228 Sutccsvilk, NC 2SU7 (70C1872A697 Chain of Custody Record Sampled by: Z f Transported by: Holding limes met: Compliance work IVon-ompliance work: Samples TransPwW On lee: Initials: rn N O 00 M o a f` Ih DD lD 00 N U Z a: w m 00 N N x O m O a - Analytical Results.► t Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 05/21/2019 Reported: 06/10/2019 For: Baxter Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 190521-40-01 TCLP Baxter See Attached 05/23/2019 PACE Respectfully submitted, r Dena Myers NC Cert #440, NCDW Cert #37755 EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 38 Pace Analytical Services, LLC aceAnalytical a 980010nreyAve 5u,b 10c �MeWs,cmi Hui Iersvd NG 26978 17041875-9"02 ANALYTICAL RESULTS Project Baxter Pace Project No 92430419 Sample- i9052i-40 Lab to: 924304190D1 Collected 0512t119 12 15 Received: 05123/19 12:41 Matrix- Solid Results reported on a 'dry weight' basis and are adjusted for percenf moisture, sample size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 6081 TCLP Pesticides RVE Analytical Method EPA8081 B Preparation Method: EPA 3510C Leachale Mothod+Date' EPA 1311. 05/30/19 15:30 Initial pH: 5.74; Final pH: 5 gamma-BHC (Lindane) ND ug1L D.50 1 05131119 13:4a 06101119 15,50 56.89.9 Chlordane (Techn cal) NO uglL 3.0 1 05f3i119 13-48 06101/19 1550 57.74-9 Endrin NO ug. L 050 1 05131/19 13:48 06101/19 15 50 72-20-8 Heplachlor ND ug+, 050 1 0513109 13:48 06/01/19 15.50 76-44.8 Heplachlor epoxide ND ug/L 050 1 05/31/19 13,48 06101/19 15.50 1024-57.3 Methoxychlor ND ug-1 1000 1 05131li913:48 0610111915'50 72.43.5 Toxaphene ND u91- 3.0 1 05131/1913:48 0610111915:50 8001.35.2 Surrogates Oecachlorobiphenyt (S) 68 % 101.138 1 05/31/19 13:48 06/01/19 15'60 2051.24 3 Tetrachloro-m-xylens (S! 78 `h 10010 1 05/31119 13:48 06101/19 15,5D 877.09.8 8082 GCS PCB Ana ylcal Method: EPA 8082A Preparation Method: EPA 3546 PCB-1016 (Aroclor 1016) NO ugfkg 242 1 05/28/19 11:0S 05131/19 19:49 12674.11.2 PCB-1221 (Aroclor 1221) NO ug%k9 242 05/2811917:05 M31/1919:49 11104-28.2 PCB-1232 (Aroclor 1232) ND ugfkg 242 1 05128/19 17:05 05/31/19 19:49 11141-16-5 P4CB-1242 (Aroclor 1242) ND ugfkg 242 1 05128/19 17:05 05/31119 19:49 53469.21.9 PCB-1248 (Aroclor 1248: NO ugfkg 242 1 05/28/19 17:05 0513V19 1949.-12672.29-6 PCB-1254 (Aroclor 1254; ND uglkg 242 1 05/28119 17.05 05131J19 19A9 11097-69.1 PCB-1260(Amclor 126 .'l NO ugfkg 242 1 05/28119 T7:05 05131/1919A9 11096-82-5 Surrogaior Oecachlorobiphenyl (S) 57 % 10-139 1 05/28/19 17:05 05131/19 19 49 2051.24.3 $082 TCLP PCBs RVE Anayyicca Method, EPA 8082A Preparation Method EPA3510C Leachale Method Cate EPA 1311 05Q0;19 1530 nihal pH! 5.74; Final pH 5 PCB-1016 (Aroclor 1016} NO ugil- 1000 1 05131/19 13:48 06101/19 2345 12674.11.2 PCB-1221 (Aroclor 1221: ND ug/L 1000 1 05131119 13:48 06101/19 23,55 11104-28.2 PCB. 1232 (Aroclor 1232) ND uglL 1000 1 OSI31/191348 06101 f192355 71141-16.5 PCB-1242 (Aroclor 1242) NO ugiL 1000 1 05131A9 13.48 OW1119 23-55 53469-21.9 PCB-1248 (Aroclor 1248) ND ugiL 1000 1 05031019 13:48 06f01119 2355 12672.29-6 PCB-1254 (Aroclor 1254) ND ug-1 1000 1 05131f19 13749 05/01/19 23:55 11097.69-1 PCB-1260 (Aroclor 1260) ND ug1L 1000 1 05131l19 13:48 06JO1119 23.55 11096.82.5 Surrogates Decachlorobiphanyl (S) 71 % 10-132 1 05/31119 13:48 06/01119 23'.55 2051-24-3 6010 MET iCP. TCLP Analytical Method; EPA 6010D Preparation Method. EPA 301 OA Leachale MelhodlDale, EPA 1311: 05130/19 20:46 Initial pH-7.24; Final pH 4.5 Arsenic Barium ND mgll 0.050 1 05131r1915:50 0610111914:56 7440.38-2 Cadmium NO mgfL 0.25 1 05131/1915:50 06101/1914,56 7440.39.3 Chromium NO mg1L 0.0050 1 05/31/19 45:50 06/01/19 14,56 7440.43.9 NO mglL 0.050 1 05131/1915.50 0610111914.56 7440.47.3 Lead Selenium NO mg1L D.025 1 05131119 15:50 06101119 14 56 7439.92-1 Silver NO mg1L 0A0 1 05/31/19 15:50 06/01/19 14 56 7782-49.2 NO mg1L O.D25 1 05131119 15:50 06101fl9 14 56 7440-22.4 REPORT OF LABORATORY ANALYSIS Date: 05M712019 04:58 PM Ti -s repll shall not tie reprdd-ed, exeept r fun wilhoN the writlen consent of Pace Analytical Services. LLC Page 4 0! 35 PO Box 228 a Statesville, NC 28687 o 704/872/4697 Page 7 of 38 Z ,,PaceAnalytical eww.pacnlrbecar.+ ANALYTICAL. RESULTS Pace Analytical Strolcea, LLC 9600 Kmcey Ave. Suite 100 Hunteravile. NC 2BD78 (704)875.9092 Project: Baxter Pace Project No.: 92430419 Sample; 190521-40 Lab ID: 92430419001 Collected: 05121M912:15 Received: 05t2311912=41 Matra, Solid Results reported on a 'dry weight' basis and are adjusted for perdenI moisture, sampfe size and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed GAS Np Qual 7470 Mercury, TCLP Analylical Method: EPA 7470A Preparation Method: EPA 7470A Leachale MelhedfDale- EPA 1311. 05/30119 20:46 Initial pH: 7 24; Final pH: 4 S Mercury NO mg/L 0.00020 1 05/31/19 18:46 OW03/19 11 ❑9 7438.97-6 6270E MSSV TCLP Sap Funnel Analytical Method: EPA 8270E Preparation Method EPA 3510C i,4-Dichlorobenzene NO ugfL 50.0 1 06/04/19 11:34 06/04/19 20 13 106.40.7 2,4-Dintuotoluene NO uglL 50.0 1 06104/1911:34 0610411920.13 121-142 Hexachloro-1,3-butadiene NO ug/L 50 0 1 06/04719 11:34 06404119 20A3 87.6E-3 Hexachlorobenzene NO ug1L 50.0 1 06f04119 11:34 06104119 20:13 11844.1 Hexachloroefhane NO ug/L 50.0 1 06/04/19 11,34 08104t19 20 13 67-72-1 2-Melhylphenol(o•Cresol) NO ugll- 50.0 1 06/04119 11.34 06104P19 20.13 95-48.7 364-Methylphenol(mHpCresol) 1050 ugfL 100 2 061OV1911.34 06/05t 19 09.26 15831.10.4 Nitrobenzene NO ugfL 50-0 1 06/04119 11.34 06/04/19 20.13 98.95.3 Pentachlorophenol NO ug/L 100 1 061041191$,34 0610411920:13 87.86-5 Pyridine NO ug/L 50.0 1 06/04119 11 34 06/04f192013 110.66-1 2,4,5-Trichlorophenol NO ug/L 50.0 1 06104119 11 34 06/04/19 20;13 95-954 2,4,6-Trichloraphenol NO ug/L 50.0 1 06J04119 11:34 06ID4119 20:13 88.05.2 L2 Surrogales Nitrobanzen"fi (S) 82 % 12-102 1 06104119 1134 06/04/19 2013 4165.60.0 2-Fluorobiphenyl (S) 73 % 13.107 1 06104119 11:34 06J04119 20:13 321.60.8 Terphenyl-d14 (S) 78 % 21-132 1 06/0411911;34 06/04/19 20,13 1718.51.0 Phenol-d6 (S) 27 % 10.110 1 06/04/19 1134 06/04119 20 13 13127-88.3 2-Fluorophenol (S) 40 % 10.110 1 06/04/19 1134 06104119 20 13 367.42.4 2,4,6-Tribfomophenot(S) 99 % 27-108 1 06104119 11:34 06104119 20:13 1184" 8260D MSV TCLP Analytical Method. EPA8260D Benzene NO ugfL 100 20 06106/1904A2 71-43.2 2-Butanone (MEK) 1220 ugrL 20C 20 06/06119 04:42 78.93.3 Carbon tetrachloride NO ug11. 100 2:. 06106/19 04:42 56.23.5 Chlorobenzene NO ugfL 100 20 06106/19 04:42 108-90-7 Chloroform NO ugfL 100 20 06/06/19 04.42 67.66-3 1.4-Od-Jorobenzene NO ug1L 100 20 0610611904,42 106-46.7 1,2-Dichloroelhene NO ug1L 100 20 46f06119 04:42 107-06.2 1,1-Dichloroelhene NO ugrL 100 20 06t0611904A2 75.354 Tetrachloroethene NO ug-IL 100 20 06/06/19 04:42 127-18-4 Trichloroethene NO ug1L 100 20 06/06/19 04:42 79.01.6 Vinyl chloride NO ug-1L 100 20 O6/06119 04:42 75-01.4 Surrogates 1,2-Dichloroalhaned4 (S) 97 % 70.130 20 06106/19 04:42 17060.07.0 Toluene-d8 (S) 100 % 67.135 20 06106/19 04:42 2037.26-5 4-Brarno0uorobenzene(S) 100 % 70.130 20 06/06119 04:42 460-00.4 Percent Moisture Analytical Method, ASTM 02974.87 Percent Moisture 86 2 % 0 10 1 05/23/19 17:44 REPORT OF LABORATORY ANALYSIS T. ns repolf shau not be rep" cruced. except ` (u: Dale 06/07/2019 04'58 PM without the written consent of Pact Analylical Servicea. LLC Page 5 o(35 PO Box 228 a Statesville, INC 28687 a 704/872/4697 Page 8 Of 38 ,1 -I�aceAnalKical9 wwxpeelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave Smile 100 HWnersvine. NC 28078 (7041875.9092 PF*Cl Baxter Pace Protect No 92430419 Sample, 19/521.40 Lab ID: 92430419001 Collected 051209 12.15 Received- 0523f19 12:41 Matrix, Solid Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Lien t OF Prepared Analyzed CAS No. Qual 1010 Flashpolnt,Closed Cup Analytical Method EPA 1010A Flashpoint >200 deg F 7D 0 1 W03119 11:41 9045 pH Sell Analytical Method. EPA 9045D pH at 25 Degrees C 6.9 Sid. Units 14 1 05/26119 17;48 H3 9095 Paint Filter Liquid Test Analytical Method EPA 90958 Free Liquids Pass 1 G 1 05/28/19 13:11 733C S Reactive Cyanide Ana ytical Method EPA9014 Preparation Method SW-846 7 3 3 2 Cyanide, Reactive NO mglkg 7 2 1 05129+19 15.33 05/30/19 22:08 734S Reactive Sulfide Analyl c81 Method. SM 4500S2F.00 Prepwatr9n Method: SW-846 7.3A.2 Sulfide,Reactive NO mg/kg 722 1 05129r'1915:33 0512911915:52 H1,H2 REPORT OF LABORATORY ANALYSIS This repod shall not be rewoouced. except in W . Date. 0510712019 04'58 PM wilh4ut the written consent of PaceAnalyticai Servires. L_1: Page 6 of 35 PO Box 228 a Statesville, NC 28687 a 704/872/4697 Page 9 of 38 190521-40 SAMPLE RESULTS - 01 C.11-1e4 4a106— 05'21119 12.15 L1102721S P'e;Jl,r-.11iufl by W-11lod 1.311 Result Qualifier Prep Batch Analyte dote 1 tinm TCLP(waclion 5130720192:42'17PM KG1288678 I Auld1 5130/2019 2'4217 PM %VW288678 141int pN 687 5;3UR0192!17'17 PM W078867f. Final OF 476 U3012019 2A217 PM 49G1788678 C tl,;r -MC-d A,-Icl by MIC'11Tnd 8151A G' ReSull Ouali6er ROL Lino Dilution Anatysls Balch AAalyle ngff mgtl IN -. mile 11,1112 2.4.5dPIS+vex1 ND 0.00200 1 1 MVV201917A3 V+G129019 2.4 D ND 0.00200 10 1 05103720t91743 VtG1240019 (S)2.4tok,,. ophe'vaft'4a AcW 55.4 14.0-758 0r,Jig6191743 WGi250011 Page 30 of 35 ACCOUNT: PROJECT: 54}3: oATEMM£" PAGE- PA[cAnmyka! NO911e15va1e.NC 9243041IJ kIW72< 06.041191038 5cf 10 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 33 of 38 NCDABCS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ 7 Client: Doug Poplin Predictive 594 Austin Little Mtn Rd Ronda, NC 28670 Soil Report Mehlich-3 Extraction Sampled County : Wilkes Links to Helpful Information Client ID: 160157 Sampled: 10114/2019 Received; 10/23/2019 Completed: 11/01/2019 Farm - Sample ID: DP1a Recommendations: Lime Crop (tonslacre) N Lime History: 1 -Fescue/OGfassfTim, M 00 120-200 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]: HM% W1V CEC BS% Ac pH P-1 K4 Ca% Mg', 0.60 0.91 15.4 91 1.4 6.3 442 260 59 23 SamplelD: dplb Recommendations: Lime Crop (tonslacre) N Lime History: 1 Fescue/OGrass/Tim, M 0.0 120-200 2 - 0.0 Test Results [units - WN in g1cm13; CEC and Na in meq/100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg° 0.51 0.93 12.5 89 1.4 6.1 238 204 55 25 Sample ID: dplc Recommendations: Lime Crop (tonslacre) N Lime History: 1 - FescuelOGrass/Tim, M 0.3 120-200 2 - 0.0 Test Results [units - WIV in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dnr3]: HM% WN CEC BS% Ac pH P-I K4 Ca% Mg% 0.51 0.87 11.7 85 1.8 5.9 220 106 56 24 Report No. FY20-SL011364 Advisor; Zach Key Southern Soil Builders, Inc. 958 Hoots Rd Roaring River, NC 28669 Advisor ID: 231531 P205 K20 Mg S Mn Zn Cu B 0 0 0 0 0 0 0 0 Soil Class: Mineral o S-1 Mn-f Mn All Mn-AI2 Zn-I Zn-AI Cu-I Na 49 142 97 461 461 1057 0.1 Nutrients (Ib/acre) P205 K20 Mg S Mn Zn Cu B 0 0 0 0 0 0 0 0 Soil Class: Mineral /, S-1 Mn-I Mn-All Mn Al2 Zn-I Zn-AI Cu-I Na 78 113 83 662 662 694 0.1 Nutrients (lb/acre) P205 K20 Mg S Mn Zn Cu B 0 0 0 0 0 0 0 0 Information Note: 12 ESP SS-1 NO3-N 1 More Information Note: 12 ESP SS-1 NO3-N 1 More Information Note 12 Soil Class: Mineral S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS4 NO3-N 45 167 117 809 809 1183 0.1 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded E;* through a grant from the North Carolina Tobacco Trust Fund Commission. l� Jr.Thank you for using agronomic services to manage nutrients and safeguard environmental quality. f` Steve Troxler. Commissioner of Aqriculture CDA CS Agronomic Division Phone: (919) 733-2655 Website: *ww.ncagr.gov/agronami/ Doug Poplin F Report No. FY20-SL011364 Sample ID: dpld Recommendations: Lime Page 2 of 4 Crop (tonslacre) Lime Nutrients (lb/acre) N P205 K20 Mg History: 1-FesCuelOGrass/Tim, M 0.0 120-200 0 0 S Mn Information 2- 0.0 0 0 0 =CuMore Note. 12 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3j: HM% WN CEC BS% Ac PH P-1 K-I Ca% Mg% S-1 Soil Class: Mineral 0.41 0.95 13.3 89 1.5 6.2 291 Mn-I Mn-Ali Mn-AI2 Zn4 Zn-AI Cu-I Na ESP SS-1 NO3-N 196 Sample ID: dp2 Recommendations: Lime 53 29 66 166 114 747 747 690 0.1 1 Crop (tons/acre) N Pz05 Kz0 Nutrients (Ib/acre) More Lime History: 1 - Corn, silage 9 0.0 180-220 0 20 Mg S Mn Zn Cu B Information 2_ 0.0 0 0 0 0 0 0 Note: 3 Test Results [units - WN in 9/crn3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): HM% WN CEC BS% Ac pH P-1 K4 Ca% Mg% 3-1 Soil Class: Mineral 0.46 0.90 8.8 84 1.4 6.0 185 Mn-1 Mn-Ail Mn-Al2 Zn4 Zn-AI Cu-1 Na ESP SS-1 NO3-N 100 Sample 10: dp3c Recommendations: Lime 53 26 82 122 90 504 504 785 0.1 1 Crop (tonslacre) N P205 K20 Nutrients (lb/acre) More Lime History: 1 -Corn, silage 0.0 180-220 0 60 Mg S Mn Zn Cu B Information 1.00 tonslacre; 8/2019 2 - o.a 0 D 0 0 0 0 Note: 3 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3j; HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Soil Class: Mineral 0.32 0,92 8.0 77 1.9 5.5 225 Mn-I Mn-Ali Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 69 Sample ID: dp3 9 Recommendations: Lime 46 26 114 114 85 575 575 405 0.1 1 Crop (tonslacre) N P205 K20 Nutrients (lb/acre) Lime History: 1 - Fescue/OGrass/Tim, M 0.0 120-200 0 8D MMore g S Mn B Information 1.00 tonslacre; 612019 2 ' 0.0 =ZnCU 0 0 0 0 Note: 12 Test Results (units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3j: HM% WN CEC BS% Ac pH P-1 K-1 Soil Class: Mineral 0.41 0,89 9.3 80 1.8 5.7 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 147 31 47 32 70 75 62 428 428 538 0.2 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.neagr.gov/agronomi! ReportNo. FY20-SL01 1364 Doug Poplin Sample ID: dp4 Lime History: Recommendations: Lime Crop (tonslacre) N P205 1-Fescue/OGrass/Tim, M 0.5 120-200 0 2 - 0.0 Nutrients (ib/acre) Page 3 of 4 More B Information 0 Note. i2 KzO 0 Mg S Mn Zn 0 0 0 0 Cu 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH Pd K4 Ca% Mg% S-1 1.25 0.97 11.0 81 2.1 5.8 138 164 44 29 99 Sample ID: dp5 Recommendations: Lime Crop (tonslacre) N P205 Lime History: 1 -Fescue/OGrass/Tim, M 1.0 120-200 0 - 2 O.Q Mn-I 11 Q Mn-Ali Mn Al2 Zn-I Zn-AI 83 718 718 Nutrients (Iblacre) Cu-I Na 350 0.1 ESP SS-1 NO3-N i 8 0 More Information Note:12 K20 0 M S g Mn Zn 0 0 0 0 Cu 0 Test Results [units - WN in 9/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]; HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S4 0.92 0.97 10.9 80 2.2 5.5 113 205 44 26 109 Sample ID: dp6 Recommendations: Lime Crop (tonslacre) N P205 Lime History: 1 -Fescue/OGrassfTim, M 0.0 120-200 0 - 2 0.0 Mn4 101 Soil Class: M neral Mn-All Mn-AI2 Zn4 Zn-AI 78 580 580 Nutr.ents {Iblacre) Cu-I Na 599 02 ESP SS-1 NO3-N 2 B 0 More More Note; 12 K20 0 Mg S Mn Zn 0 0 0 0 Cu Q Test Results [units -WN in g1cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3): HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 0.51 0.93 12.7 88 1.6 5.9 117 184 54 27 61 Sample ID: dp7 Recommendations: Lime Crop (tonslacre) N P205 Lime History: 1 - Fescue/OGrassfTim, M 0.0 120-200 0 1.00 tonslacre; 6/2019 2 - 0.0 Mn-I 85 Soil Class: Mineral Mn-All Mn-AI2 Zn4 Zn-AI 68 771 771 Cu-1 Na 626 0.1 ESP SS-1 NO3-N i Nutrients (Ib/acres More 0 Information 0 Note: 12 K20 40 M S g Mn 0 0 0 0 0 0 0 ITest Results [units -WN in 9lcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-1 K4 Ca% Mq% S-1 0.32 0.92 9.7 88 1.2 6.1 143 54 58 27 47 Mn-I 93 Soil Class: Mineral Mn-Ali Mn-AI2 Zn4 Zn-AI 71 575 575 Cu-I Na 680 01 ESP SS-1 NO3-N 1 NCDABCS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil Report No. FY20-SL011364 Doug Poplin Page 4 of 4 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either , B ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate%, CEC is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu4 Fertilizer Recommendations for Feld crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50, if they are not, follow the fertilizer recommendations given If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to Note.• Secondary Nutrients and Micronutrients In genera], homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/aqronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ibl1 JO sq ft , If you cannot find the exact fertilizer grade recommended on the report, visit www.nca r ov/a ronom art4ht ind information that may help you choose a comparable alternate. For more information, read A Homeowner's Gu;de to Ferwize Test Results The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinet available)] indicate levels of plant nutrients or other fertility measurement. Visit www nca r ov/a ronomdu rst.htm ESP HM% K4 K20 Mg% MIN Mn Mn-Ali Mn-Al2 Mn4 M-O N Na NOs-N ORG pH P-1 P20s S-1 ss-1 WN Zn-AI Zn-I exchangeable acidity boron % CEC occupied by basic cations % CEC occupied by calcium cation exchange capacity copper index exchangeable sodium percent percent humic matter potassium index potash % CEC occupied by magnesium mineral sod class manganese Mn-availability index for crop 1 Mn-availability index for crop 2 manganese index minerat-organic sod class nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sutfur index soluble salt index weight per volume zinc availability index zinc index ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Baxter Healthcare Corporation WQ Permit Number: WQ0031725 WWTP Name. Baxter Healthcare Corporation NPDES Number: NCO006564 Monitoring Period: From I/I/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .11061- Please indiente IPVPI at-htPVPr1 q.,.t Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑ A1t.1) (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Glass B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com >ostin ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitor ing data: Parameter Allowable Level Pathogen Density Num er o Frequency Sample natic y in Sludge Excee- of Analysis Type Tech- Minimu Geo. Mean Maximu Units 2x IOtothe 6th owes MPN 97561 110371 p 114286 0 7 grab nintie sm922 per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliforrn) weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ It. 2 (40-day bench) L..I Alt. 3 (30-day bench) 0 Alt. 4 (Spec. O, uptake; Alt. 5 (14-Day Aerobic) [I Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - EJnstable) Alt. 9 (Injection) [j Alt. 10 (Incorporation)_ _ [ j No vector attraction reduction alternatives were nerformed 1 la;K•1IFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T 1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." afe , Xv.1\V, L Dennis Key Southern Soil Builders, Inc. Preparer ne and itle (type -or print) Land Applier Name and Title (if applicable)(type or print; Sigr ture o reparer* Date Signature of Land Applies• (if applicable) Date *Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)