WQ0001026_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:*
Project Number* WQ0001026
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0001026
Applicant\Permittee * City of Washington
Facility Name * City of Washington
Phone Number*
336-751-1441
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Washington Annual Report- WQ0001026.pdf 11.5MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/24/2020

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001026 County
Facility Name (as shown on permit):
Land Application Operator:
Beaufort County, NC Year:
City of Washington
EMA Resources Inc.
2019
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
54
Total number of fields utilized for land application during the year:
10
Total amount of dry tons applied during the year for all application sites:
323.79
Total number of acres utilizes for land application during the year:
177.5
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
I) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at Ieast 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached,
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .l 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T . i 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Adam Waters - Public Works Director
Permittee Namp and Title (type or print)
1 N5
lf�� � /;Zg- ZLZ& !S 20Zo
Signature of Permittee Date
Z�Ke•• v6/2020
Signature of Preparer* LJ ; Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and I5A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - H
WQ Permit Number:
WQ0001026
Facility Name: City of Washington
Residual Source WQ # or
NPDES #:
NCO020648
WWTP Name: Washington W WTP
Residual Analysis Data
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg�g)
Cone.
Limit
ma
Sam le or Composite Date
311$119
411119
e
Average
91I91] 9
l 0131119
Percent Solids (%)
NA
3.32
3.26
3.3
3.27
3.75
Arsenic
75
12.6
12.7
12.7
12.7
11.3
Cadmium
85
1.49
1.5
1.5
1.5
1.34
Copper
4,300
292
260
276.0
261
124
Chromium
NA
24.2
19.1
21.7
20
26.5
Lead
840
30.7
25.5
28.1
24.3
17.8
Mercury
57
3.77
2.7
L 17
0.884
Molybdenum
75
5.66
5.7
5.42
3.51
Nickel
420
15.2
14.(]
13.8
13.6
Selenium
100
14.8
d30000
14.8
17.7
13.2
Zinc
7,500
726
689.0
688
370
Total Phosphorus
NA
32500
3l250
33300
15400
TKN
NA
53600
58450
86400
37600
Ammonia -Nitrogen
NA
8730
$480
8605.0
14800
9300
Nitrate and Nitrite
NA
434
209
321.5
235
128
'For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penAlties for submitting k se information, including the possibility of fines. and imprisonment for knowing violations."
Signature Af Pre a er * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are Part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0001026 Laboratory: 1) Waypoint Analytical
Facility Name: City of Washington 2)
Residual Source NCO020648 3)
NPDES # or WQ#: 4)
WWTP Name: Washington WWTP 5)
Residual Analysis Data
Parameter
{mg�g}
Sarn 1e or Com osite Date
3118119
411119
Spring
P `a8
g
4119119
1t7131114
Aluminum
32800
30000
31400
31200
34300
Calcium
26700
23400
25050
26100
13500
Magnesium
2700
2510
2605
2440
2140
PH
7.2
6.5
6.85
7
7.1
Potassium
2640
2590
2615
2330
2260
Sodium
2870
2800
2835
3550
2730
PAN
18260
20895
19577.5
29115
13268
SAR
0.81
0.84
1.02
1.11
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are
significant penalties fpr submitting false information, including the possibility of fines and imprisonment for knowing violations."
5ivnature of
*Preparer is deli6ed in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
I �j f, L,
Date
DENR FORM RSSF - B (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
16.5 Acres Permitted: 16.5 Site #: BF210 Field #:
7.13
CrB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phoms
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.43
Arsenic
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.238
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.238
Chromiuni
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Lead
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
denum
Nickel
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Selenium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Zinc
0.595
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.595
Total
Phos-
27.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
27.000
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 7.13 Site #:
Predominant Soil Series: CrB
Crop 1 Name: Soybeans Crop 1 Max. PAN:
151
Crop 2 Name:
Acres Utilized: 16.5
BF210 Acres Permitted: 16.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
cc
0
� �
*
?.
* �'
o'
p
7�
- ~
�. �
a•
o
TKN
mg/kg
Z >
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/15
52000
3.29
0.432
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
16.930
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
52000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
16.930
0.000
Lime Applied
Annuallbs/acre
0.011
0.001
0.238
0.019
0.024
0.002
0.005
0.012
0.013
0.595 27.000
2.311
2.906
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.018
0.007
0.818
0.195
0.089
0.005
0.036
0.106
0.018
11/11
2000
Current Cumulative lbs/ac
0.029
0.008
1.056
0.214
0.113
0.007
0.041
0.118
0.031
Permitted C. P. L. R.****
36
1 34
1339
267
1 15
374
89
Permit PAN Limit 1 st/2nd Crop
1
1 151
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
16 Acres Permitted: 16 Site #: BF210 Field #:
25.70
Ra
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.61
Arsenic
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
Cadmium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.838
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.838
Chromiuni
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
Lead
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
denum
Nickel
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Selenium
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Zinc
2.210
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.210
Total
Phos-
106.960
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
106.960
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
Land Owner: Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 25.70 Site #:
Predominant Soil Series: Ra
Crop 1 Max. PAN:
106
Crop 2 Name:
Acres Utilized: 16
BF210 Acres Permitted: 16
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 -t
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/5
110500
3.27
0.942
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
54.837
NA
Wheat
10/6
78000
3.27
0.665
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
38.708
NA
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
tss5oo
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
93.545
o.000
Lime Applied
Annuallbs/acre
0.041
0.005
0.838
0.064
0.078
0.004
0.017
0.044
0.057
2.210 106.9601
5.307
7.517
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.037
0.015
2.099
0.382
0.292
0.011
0.045
0.217
0.037
11/11
2000
Current Cumulative lbs/ac
0.078
0.020
2.937
0.446
0.370
0.015
0.062
0.261
0.094
Permitted C. P. L. R.****1
3
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 106
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
15.5 Acres Permitted: 15.5 Site #: BF210 Field #:
41.01
Le
6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phoms
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.65
Arsenic
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.461
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.461
Chromiuni
0.115
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.115
Lead
0.149
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.149
Mercury
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Molyb-
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
denum
Nickel
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Selenium
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Zinc
3.646
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.646
Total
Phos-
165.375
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
165.375
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 41.01 Site #:
Predominant Soil Series: Le
Crop 1 Name: Soybeans Crop 1 Max. PAN:
146
Crop 2 Name:
Acres Utilized: 15.5
BF210 Acres Permitted: 15.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
cc
0
� �
*
?.
* �'
o'
7�
- ~
�. �
a•
o
TKN
mg/kg
Z >
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/17
240500
3.29
2.129
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
83.352
NA
Beans
3/18
58500
3.29
0.518
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
20.275
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
299000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
103.6261
0.000
Lime Applied
Annuallbs/acre
0.067
0.008
1.461
0.115
0.149
0.014
0.030
0.074
0.078
3.646 165.375
11.33
14.976
2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.084
0.03
4.982
0.651
0.51
0.02
0.094
0.334
0.083
11/11
2000
Current Cumulative lbs/ac
0.151
0.038
6.443
0.766
0.659
0.034
0.124
0.408
0.161
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
Permit PAN Limit 1 st/2nd Crop
I
F-146
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
13.5 Acres Permitted: 13.5 Site #: BF210 Field #:
35.67
Le
7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.64
Arsenic
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.458
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.458
Chromiuni
0.114
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.114
Lead
0.148
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.148
Mercury
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Molyb-
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
denum
Nickel
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Selenium
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Zinc
3.641
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.641
Total
Phos-
165.125
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
165.125
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 35.67 Site #:
Predominant Soil Series: Le
Crop 1 Name: Soybeans Crop 1 Max. PAN:
146
Crop 2 Name:
Acres Utilized: 13.5
BF210 Acres Permitted: 13.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
cc
0
� �
*
?.
* �'
o'
7�
- ~
�. �
a•
o
TKN
mg/kg
Z >
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/18
143000
3.29
1.453
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
56.903
NA
Beans
3/19
117000
3.29
1.189
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
46.557
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
260000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
103.4591
0.000
Lime Applied
Annuallbs/acre
0.067
0.008
1.458
0.114
0.148
0.014
0.030
0.074
0.078
3.641 165.1251
8.845
12.486
2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.069
0.026
3.893
0.516
0.416
0.015
0.076
0.272
0.068
11/11
2000
Current Cumulative lbs/ac
0.136
0.034
5.351
0.630
0.564
0.029
0.106
0.346
0.146
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
Permit PAN Limit 1 st/2nd Crop
I
F-146
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
17.5 Acres Permitted: 17.5 Site #: BF210 Field #:
48.16
Le
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.75
Arsenic
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.519
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.519
Chromiuni
0.119
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.119
Lead
0.155
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.155
Mercury
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Molyb-
0.031
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.031
denum
Nickel
0.077
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.077
Selenium
0.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Zinc
3.792
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.792
Total
Phos-
172.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
172.000
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 48.16 Site #:
Predominant Soil Series: Le
Crop 1 Name: Soybeans Crop 1 Max. PAN:
146
Crop 2 Name:
Acres Utilized: 17.5
BF210 Acres Permitted: 17.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
cc
0
� �
*
?.
* �'
o'
7�
- ~
�. �
a•
o
TKN
mg/kg
Z >
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/19
45500
3.29
0.357
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
13.967
NA
Beans
3/20
169000
3.29
1.325
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
51.877
NA
Beans
5/14
84500
3.29
0.662
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
25.939
NA
Beans
5/15
52000
3.29
0.408
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
15.962
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
1 0.000
TOTALS:
01
351000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
107.7461
0.000
Lime Applied
Annuallbs/acre
0.070
0.008
1.519
0.119
0.155
0.015
0.031
0.077
0.081
3.792 172.0001
6.535
10.327
2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.055
0.021
2.863
0.392
0.326
0.01
0.059
0.215
0.054
11/11
2000
Current Cumulative lbs/ac
0.125
0.029
4.382
0.511
0.481
0.025
0.090
0.292
0.135
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
Permit PAN Limit 1 st/2nd Crop
I
F-146
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
27.5 Acres Permitted: 27.5 Site #: BF210 Field #:
35.45
GoA
12
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.29
Arsenic
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.673
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.673
Chromiuni
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
Lead
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
denum
Nickel
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Selenium
0.046
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Zinc
1.774
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.774
Total
Phos-
85.847
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
85.847
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
Land Owner: Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 35.45 Site #:
Predominant Soil Series: GoA
Crop 1 Max. PAN:
136
Crop 2 Name:
12 Acres Utilized: 27.5
BF210 Acres Permitted: 27.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 -t
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/2
143000
3.27
0.709
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
41.289
NA
Wheat
10/5
117000
3.27
0.580
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
33.782
NA
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
0
26000o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
75.071
o.000
Lime Applied
Annuallbs/acre
0.033
0.004
0.673
0.052
0.063
0.003
0.014
0.036
0.046
1.774 85.847
5.091
6.865
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.035
0.013
2.166
0.312
0.233
0.01
0.041
0.161
0.035
Current Cumulative lbs/ac
0.068
0.017
2.839
0.364
0.296
0.013
0.055
0.197
0.081
Permitted C. P. L. R.****1
3
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 136
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
26.5 Acres Permitted: 26.5 Site #: BF210 Field #:
35.46
CrA
13
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phoms
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.34
Arsenic
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.698
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.698
Chromiuni
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
Lead
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
denum
Nickel
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Selenium
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Zinc
1.841
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.841
Total
Phos-
89.111
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
89.111
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
Land Owner: Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 35.46 Site #:
Predominant Soil Series: CrA
Crop 1 Max. PAN:
112
Crop 2 Name:
13 Acres Utilized: 26.5
BF210 Acres Permitted: 26.5
Cation Exchange Capacity (non 503): 0
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 -t
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/4
221000
3.27
1.137
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
66.218
NA
Wheat
10/6
39000
3.27
0.201
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
11.686
NA
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
0
26000o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
77.904
o.000
Lime Applied
Annuallbs/acre
0.034
0.004
0.698
0.054
0.065
0.003
0.015
0.037
0.047
1.841 89.111
0
1.841
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
o
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.034
0.004
0.698
0.054
0.065
0.003
0.015
0.037
0.047
Permitted C. P. L. R.****1
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
112
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Washington Total Dry Tons Applied (Annual): 12.41
Permit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator: Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series: GoA
Acres Used: 6 Acres Permitted: 6 Site #: BF210 Field #: 14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
2.07
Arsenic
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
1.079
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.079
Chromiuni
0.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Lead
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.101
Mercury
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
denum
Nickel
0.057
0.000
0.000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.057
Selenium
0.073
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.073
Zinc
2.846
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.846
Total
Phos-
137.729
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
137.729
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
Land Owner: Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 12.41 Site #:
Predominant Soil Series: GoA
Crop 1 Max. PAN:
136 Crop 2 Name:
14
BF210
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503): 0
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 -t
� �
*
o
* �'
o'
p
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/3
91000
3.27
2.068
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
120.426
NA
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
0
9t000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
1120.4261
o.000
Lime Applied
Annuallbs/acre
0.053
0.006
1.079
0.083
0.101
0.005
0.022
0.057
0.073
2.846 137.7291
7.213
10.059
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.047
0.016
3.22
0.387
0.284
0.013
0.055
0.182
0.047
Current Cumulative lbs/ac
0.100
0.022
4.299
0.470
0.385
0.018
0.077
0.239
0.120
Permitted C. P. L. R.****1
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 136
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
13 Acres Permitted: 13 Site #: BF210 Field #:
21.27
Ly
15
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phoms
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.64
Arsenic
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Cadmium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.854
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.854
Chromiuni
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Lead
0.080
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.080
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
denum
Nickel
0.045
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
Selenium
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Zinc
2.251
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.251
Total
Phos-
108.958
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
108.958
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington
Land Owner: Hunter Roost Farms
Operator: Hunter Roost Farms
Crop 1 Name: Wheat
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 21.27 Site #:
Predominant Soil Series: Ly
Crop 1 Max. PAN:
106 Crop 2 Name:
15 Acres Utilized: 13
BF210 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
13
0
o
Volume applied
(enter one) Solids/
Liquid
q
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>o
� �
*
* �'
o'
p
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/3
156000
3.27
1.636
Washington
D
<.5"
S
0.5
0.3
86400
14800
235
95.282
NA
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
t56000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
95.282
0.000
Lime Applied
Annuallbs/acre
0.042
0.005
0.854
0.065
0.080
0.004
0.018
0.045
0.058
2.251 108.958
0
2.251
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.042
0.005
0.854
0.065
0.080
0.004
0.018
0.045
0.058
Permitted C. P. L. R.****1
3
1 34
1 1338
1
1 267
15
374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 106
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
25.5 Acres Permitted: 25.5 Site #: BF210 Field #:
61.53
CrA
16
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phoms
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.41
Arsenic
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.061
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
1.332
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.332
Chromiuni
0.104
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.104
Lead
0.136
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.136
Mercury
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Molyb-
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
denum
Nickel
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Selenium
0.071
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.071
Zinc
3.325
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.325
Total
Phos-
150.813
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
150.813
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/6/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 61.53 Site #:
Predominant Soil Series: CrA
Crop 1 Name: Soybeans Crop 1 Max. PAN:
154
Crop 2 Name:
16 Acres Utilized: 25.5
BF210 Acres Permitted: 25.5
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
cc
0
� �
*
?.
* �'
o'
7�
- ~
�. �
a•
o
TKN
mg/kg
Z >
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/14
97500
3.29
0.525
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
20.540
NA
Beans
3/15
195000
3.29
1.049
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
41.079
NA
Beans
3/16
156000
3.29
0.839
Washington
D
<.5"
S
0.5
0.3
58450
8605
322
32.864
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
448500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
94.483
0.000
Lime Applied
Annuallbs/acre
0.061
0.007
1.332
0.104
0.136
0.013
0.027
0.067
0.071
3.325 150.8131
8.133
11.458
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.054
0.019
3.483
0.489
0.366
0.016
0.064
0.25
0.054
Current Cumulative lbs/ac
0.115
0.026
4.815
0.593
0.502
0.029
0.091
0.317
0.125
Permitted C. P. L. R.****
36
1 34
1339
267
1 15
374
89
Permit PAN Limit 1 st/2nd Crop
154
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
3/28/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-078-0223
Client Project Description: Analytical Testing
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 3/19/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
XZ-10��
Jimmy R. Ferguson
Assistant Technical Director
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015 VA NELAP #460181 Texas #T104704180-11-6 Arkansas #88-0650
Mississippi California #2904 NC #415 Oklahoma #9311 Virginia #00106
Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST #41
III
Page 1 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Analytical Testing
Lab Report Number: 19-078-0223
Date: 3/27/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L427663
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L427603
MS/MSD Recovery failed, DT confirmed matrix interference
Analyte: Iron
QC Batch No: L427663
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L427603
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: L427663
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Molybdenum
QC Batch No: L427603
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L427603
MS/MSD Recovery failed, DT confirmed matrix interference
Analyte: Selenium
QC Batch No: L427603
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 2 of 8

Wa OI �� ' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Y ANALYTICAL www.wa ointanal tical.com
Yp Y
46245
EMA Resources Inc
Brent Collins Project Analytical Testing Report Date : 03/28/2019
755 Yadkinville Rd Information : Received : 03/19/2019
Mocksville , NC 27028
Report Number : 19-078-0223 REPORT OFANAL YSIS Jimmy R. Ferguson
Assistant Technical Director
Lab No : 93303
Matrix: Solids
Sample ID : Washington
Sampled:
3/18/2019
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
96.68
%
0.010
1
03/22/19 15:03
CJR
SW-DRYWT
Ammonia Nitrogen
0.873
% - dry
0.060
0.301
1
03/25/19 11:00
ZBD
4500NH3C-2011
Nitrate+Nitrite-N
434
mg/Kg -
dry
150
150
1
03/22/19 16:13
ZBD
4500NO3F-2011
pH
7.2
S.U.
1
03/25/19 11:20
JSL
9045D
Total Solids
3.32
%
0.010
0.010
1
03/22/19 15:03
CJR
2540G-2011
Total Volatile Solids
61.9
%
0.010
0.010
1
03/22/19 15:03
CJR
2540G-2011
Total Kjeldahl Nitrogen
5.36
% - dry
0.030
0.753
1
03/26/19 11:00
CLP
4500NH3C-2011
Phosphorus
32500
mg/Kg -
dry
77.4
151
1
03/22/19 19:05
KKM
6010D
Aluminum
32800
mg/Kg -
dry
61.1
151
1
03/22/19 19:05
KKM
6010D
Arsenic
<12.6
mg/Kg -
dry
12.6
15.1
1
03/22/19 19:05
KKM
6010D
Cadmium
<1.49
mg/Kg -
dry
1.49
3.01
1
03/22/19 19:05
KKM
6010D
Calcium
26700
mg/Kg -
dry
506
753
1
03/22/19 19:05
KKM
6010D
Chromium
24.2
mg/Kg -
dry
5.72
7.53
1
03/27/19 16:21
KKM
6010D
Copper
292
mg/Kg -
dry
4.37
7.53
1
03/22/19 19:05
KKM
6010D
Iron
19000
mg/Kg -
dry
128
151
1
03/22/19 19:05
KKM
6010D
Lead
30.7
mg/Kg -
dry
4.49
9.04
1
03/25/19 19:23
KKM
6010D
Magnesium
2700
mg/Kg -
dry
66.9
151
1
03/22/19 19:05
KKM
6010D
Manganese
554
mg/Kg -
dry
5.51
15.1
1
03/22/19 19:05
KKM
6010D
Mercury
3.77
mg/Kg -
dry
0.106
0.479
1
03/25/19 09:53
TJS
7471A
Molybdenum
5.663
mg/Kg -
dry
3.92
7.53
1
03/22/19 19:05
KKM
6010D
Nickel
15.2
mg/Kg -
dry
4.97
7.53
1
03/22/19 19:05
KKM
6010D
Potassium
2640
mg/Kg -
dry
89.8
151
1
03/22/19 19:05
KKM
6010D
Selenium
<14.8
mg/Kg -
dry
14.8
15.1
1
03/22/19 19:05
KKM
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 5 of 8

Waypoint,
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-078-0223
Lab No : 93303
Sample ID : Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Analytical Testing
Information :
REPORT OFANALYSIS
Report Date : 03/28/2019
Received : 03/19/2019
Jimmy R. Ferguson
Assistant Technical Director
Matrix: Solids
Sampled: 3/18/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Sodium
2870
mg/Kg - dry
233
753
1
03/22/19 19:05
KKM
6010D
Zinc
726
mg/Kg - dry
32.5
37.7
1
03/22/19 19:05
KKM
6010D
Sulfur
10100
mg/Kg - dry
147
151
1
03/22/19 19:05
KKM
6010D
Organic N
4.49
% - dry
0.060
0.301
1
03/25/19 11:00
CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 6 of 8

(2)W•
ayPoi nt 2790 Whitten Road, Memphis, 21.2440
Main 901.213.2400 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-078-0223
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
5
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: Rory Phillips Date & Time: 03/19/2019 09:24:57
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSH -Additional charges apply
Detection
Method of Shipment
Fed Ex UPS �USPS
Matrix Key
WW -Wastewater GW -Groundwater
Special Limit(s)
Date Results Needed
Courier Client Drop Off
DW - Drinking Water S - Soil /Solid O -Oil
P - Product M - Misc
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID #
336-399-3646
brent.collIns@emaresources, corn
A Cool < Na25203 (Micro Only)
Z
�
<= 6C
B Cool 6C
• LL
N
U
a; CD
_
_
C H2SO4 pH<2
Wa O'
Y-ANALYTICAL
A x
_
o 0 r M
Q
D None Required
4
v m
o S E O
Cn
_
111
E HNO3NzOH pH>10
F HNO3 pH<2
2790 Whitten Road
Unless noted, all containers
y
° E
7_5u Q
Z
(i5
+-�
f ,
> V
G HCL pH<2
H H3PO4 pH<2
Memphis, TN 38133
[phone]
per Table II of 40 CFR Part
p
M
r
0
a Y
~ Z
~
Q
I Cool <= 6C NAZS203
136.
Date Time Sample Identification
@
Z
Required
Analysis / Preservative
Comments/Notes
'
3�/y
C
tj
�/ ✓
Metals:Al,As,Ca,Cd,Cr,Cu,Fe,Pb
`.�
18 Po
��
� ��
C
�/ ✓
✓
✓ ✓
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,2n
J%4 or, osif>n
n
�
IIIIIIIIIIIIIIIII E11I IIIIII IIIIIIII11IIII
111IIIIA � 9 019
EMA Resources Inc
Soil Samolina
09 18:50
For Laboratory Use Only
Ice Custody Lab Comments
Sampled by (Name -Print)
41 wti��•kv
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Seals
Y.%N �
Relinqui a y' I N U
�
-Date Time Receive by: (SIGNATU ) Date Time
311Y 11:20c—
y/N
Blank/ ooler Temp
Relinq J ed by: (SIGN TURE)
Date Time Received byNATURE) Date Time
: G
3I1 y a: SOPA,
Relinquished by: (SIGNATURE)
Date Time nb(SI
UREA Dat Time
O U-n

Waypoint
ANALYTICAL
4/9/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-092-0234
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/2/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
. L +� i vxu
CL
Page 1 of 7

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 19-092-0234
Date: 4/9/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L429984
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L429984
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L429984
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L429984
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: L429984
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Manganese
QC Batch No: L429984
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L429984
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 2 of 7

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Solids Total Mercury Analysis - CVAA Method 7471A
Analyte: Mercury
QC Batch No: L429623
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 3 of 7

Wa OI �� ' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Y ANALYTICAL www.wa ointanal tical.com
Yp Y
46245
EMA Resources Inc
Brent Collins Project Washington, NC Report Date : 04/09/2019
755 Yadkinville Rd Information : Received : 04/02/2019
Mocksville , NC 27028
Report Number : 19-092-0234 REPORT OFANAL YSIS Danyale Love
Project Manager
Lab No : 97337
Matrix: Solids
Sample ID : Washington
Sampled:
4/1/2019
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
96.7
%
0.010
1
04/08/19 15:07
ADM
SW-DRYWT
Ammonia Nitrogen
0.848
% - dry
0.060
0.303
1
04/06/19 13:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
209
mg/Kg -
dry
146
146
1
04/03/19 13:37
ZBD
4500NO3F-2011
pH
6.5
S.U.
1
04/04/19 06:50
JSL
9045D
Total Solids
3.26
%
0.010
0.010
1
04/08/19 15:07
ADM
2540G-2011
Total Volatile Solids
61.6
%
0.010
0.010
1
04/08/19 15:07
ADM
2540G-2011
Total Kjeldahl Nitrogen
6.33
% - dry
0.030
0.757
1
04/08/19 13:30
CLP
4500NH3C-2011
Phosphorus
30000
mg/Kg -
dry
77.9
152
1
04/05/19 20:02
BKN
6010D
Aluminum
30000
mg/Kg -
dry
61.5
152
1
04/05/19 20:02
BKN
6010D
Arsenic
<12.7
mg/Kg -
dry
12.7
15.2
1
04/05/19 20:02
BKN
6010D
Cadmium
<1.50
mg/Kg -
dry
1.50
3.03
1
04/05/19 20:02
BKN
6010D
Calcium
23400
mg/Kg -
dry
509
758
1
04/05/19 20:02
BKN
6010D
Chromium
19.1
mg/Kg -
dry
5.76
7.58
1
04/05/19 20:02
BKN
6010D
Copper
260
mg/Kg -
dry
4.39
7.58
1
04/05/19 20:02
BKN
6010D
Iron
17200
mg/Kg -
dry
128
152
1
04/05/19 20:02
BKN
6010D
Lead
25.5
mg/Kg -
dry
4.52
9.09
1
04/05/19 20:02
BKN
6010D
Magnesium
2510
mg/Kg -
dry
67.3
152
1
04/05/19 20:02
BKN
6010D
Manganese
503
mg/Kg -
dry
5.55
15.2
1
04/05/19 20:02
BKN
6010D
Mercury
1.61
mg/Kg -
dry
0.105
0.479
1
04/04/19 13:53
TJS
7471A
Molybdenum
5.673
mg/Kg -
dry
3.94
7.58
1
04/05/19 20:02
BKN
6010D
Nickel
12.7
mg/Kg -
dry
5.00
7.58
1
04/05/19 20:02
BKN
6010D
Potassium
2590
mg/Kg -
dry
90.3
152
1
04/05/19 20:02
BKN
6010D
Selenium
<14.8
mg/Kg -
dry
14.8
15.2
1
04/05/19 20:02
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 4 of 7

Waypoint,
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-092-0234
Lab No : 97337
Sample ID : Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Washington, NC
Information :
REPORT OFANALYSIS
Report Date : 04/09/2019
Received : 04/02/2019
Q0"
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/1/2019 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Sodium
2800
mg/Kg - dry
234
758
1
04/05/19 20:02
BKN
6010D
Zinc
652
mg/Kg - dry
32.7
37.9
1
04/05/19 20:02
BKN
6010D
Sulfur
9300
mg/Kg - dry
148
152
1
04/05/19 20:02
BKN
6010D
Organic N
5.48
% - dry
0.060
0.303
1
04/06/19 13:00
ACA
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 5 of 7

(2)W•
ayPoi nt 2790 Whitten Road, Memphis, 21.2440
Main 901.213.2400 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-092-0234
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
5
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: Rory Phillips Date & Time: 04/02/2019 09:47:24
Page 6 of 7

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSH - Additional charges apply
Method of Shipment
Matrix Key
Special Detection Limit(s)
Fed Ex UPS �USPS
WW -Wastewater GW -Groundwater
/Nsr
Date Results Needed
EJ Courier Client Drop Off
DW - Drinking Water S - Soil /Solid O -Oil
�g9��y+5-�on
P-Product M-Mist
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID q
336-399-3646
[e-mail]
t6
z
U)
A Cool < iDC Na2S203 (Micro Only)
k2
::
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C
U
70
8 Cool <= 6C
Waypoint_
`a
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><
C1.
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pH<2c
D NoonnO4e Required
D N
ANALYTICAL
0
B
E
cfl
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21
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(�
W
is N30H pH>10
2790 Whitten Road
Memphis, TN 38133
Unless noted, all containers
y
°.�'
w
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to
75
Q
Z
T
\
U
F HNO3 pH<2
G HCL pH<2(901)
o
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/�
213-2400
per Table II of 40 CFR Part
CDZ
! ,
H H3PO4 pH<2
136.
Z
10
LJ
I Cool <= 6C NA2S203
Date
Time
Simple Identification
Required
Analysis / Preservative
Comments/Notes
°ate,
C
x
X
Metals:Al,As,Ca.Cd,Cr,Cu,Fe,Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
4
r+ SO/7oI C 5 IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII 46245
-02-0419
EMA Resources Inc 09 Washington. NC
Please_
For Laboratory Use Only
Sampled by (Name - Print)
>zo., k,}Gk,_
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
CS als
Lab Comments
l-/ N
�
YC"1
Reli u' a URE)
Date Time
Received by: (SIGNATURE)
Date Time
—
4111r9 ):�oP
yalllg 13opM
Tem
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Y )
Date rime
Receive b SIGNATURE
Y� ( )L/h/19
Date Time
3:ooPRelinquished
n11l',-1e,
by: (SIGNATURE)
Date Time
Rec ed : (SIG LIRE`

Waypointo
ANALYTICAL
10/1/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-263-0047
Client Project Description: Washington
Washington, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 9/20/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 6

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington
Lab Report Number: 19-263-0047
Date: 10/1 /2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 95106 (Washington WWTP)
Analyte: Aluminum
QC Batch No: 1-455238/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: 1-455238/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: 1-455238/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: 1-455238/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Phosphorus
QC Batch No: 1-455238/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 2 of 6

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Washington Report Date : 10/01/2019
755 Yadkinville Rd Information : Washington, NC Received : 09/20/2019
Mocksville , NC 27028
Report Number : 19-263-0047 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 95106
Matrix: Solids
Sample ID: Washington WWTP
Sampled:
9/19/2019
7:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
96.7
%
0.010
1
09/20/19 16:59
ADM
SW-DRYWT
Ammonia Nitrogen
14800
mg/Kg -
dry
758
1
10/01/19 09:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
235
mg/Kg -
dry
146
146
1
10/01/19 14:36
ZBD
4500NO3F-2011
Organic N
71500
mg/Kg -
dry
7580
1
10/01/19 09:00
CALCULATION
pH
7.0
S.U.
1
09/30/19 06:58
JSL
9045D
Total Solids
3.27
%
0.010
0.010
1
09/20/19 16:59
ADM
2540G-2011
Total Volatile Solids
57.8
%
0.010
0.010
1
09/20/19 16:59
ADM
2540G-2011
Total Kjeldahl Nitrogen
86400
mg/Kg -
dry
7580
5
10/01/19 16:06
CLP 4500NORGD-2011
Phosphorus
33300
mg/Kg -
dry
77.9
152
1
09/23/19 21:40
BKN
6010D
Aluminum
31200
mg/Kg -
dry
61.5
152
1
09/23/19 21:40
BKN
6010D
Arsenic
<12.7
mg/Kg -
dry
12.7
15.2
1
09/23/19 21:40
BKN
6010D
Cadmium
<1.50
mg/Kg -
dry
1.50
3.03
1
09/23/19 21:40
BKN
6010D
Calcium
26100
mg/Kg -
dry
509
758
1
09/23/19 21:40
BKN
6010D
Chromium
20.0
mg/Kg -
dry
5.76
7.58
1
09/23/19 21:40
BKN
6010D
Copper
261
mg/Kg -
dry
4.39
7.58
1
09/23/19 21:40
BKN
6010D
Iron
19700
mg/Kg -
dry
128
152
1
09/23/19 21:40
BKN
6010D
Lead
24.3
mg/Kg -
dry
4.52
9.09
1
09/23/19 21:40
BKN
6010D
Magnesium
2440
mg/Kg -
dry
67.3
152
1
09/23/19 21:40
BKN
6010D
Manganese
545
mg/Kg -
dry
5.55
15.2
1
09/23/19 21:40
BKN
6010D
Mercury
1.17
mg/Kg -
dry
0.101
0.458
1
09/23/19 14:09
TJS
7471A
Molybdenum
5.423
mg/Kg -
dry
3.94
7.58
1
09/23/19 21:40
BKN
6010D
Nickel
13.8
mg/Kg -
dry
5.00
7.58
1
09/23/19 21:40
BKN
6010D
Potassium
2330
mg/Kg -
dry
90.3
152
1
09/23/19 21:40
BKN
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 6

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-263-0047
Lab No : 95106
Sample ID: Washington WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington
Information : Washington, NC
REPORT OFANALYSIS
Report Date : 10/01/2019
Received : 09/20/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/19/2019 7:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
17.7
mg/Kg - dry
14.8
15.2
1
09/23/19 21:40
BKN
6010D
Sodium
3550
mg/Kg - dry
234
758
1
09/23/19 21:40
BKN
6010D
Zinc
688
mg/Kg - dry
32.7
37.9
1
09/23/19 21:40
BKN
6010D
Sulfur
11200
mg/Kg - dry
148
152
1
09/23/19 21:40
BKN
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
09/23/19 21:40
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 4 of 6

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-263-0047
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#70
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lKristinaA. McAdams Date & Time: 09/20/2019 10:38:27
Page 5 of 6

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location(ciity/State)
RUSH -Add ItIona I Charges appiy
Special Detection Llmltis)
rNe dof Shipment
fed
Matrix Key
I
ppp
�
Date Res uIts Needed
Ex ®ups OuSPS
El Courier Client Orop Off
WW -Wastewater GW-Groundwater
DW - Urinking Water S- Soil /Solid O - Oil
�0l
�f � o�
P- Product M -Misc
r
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Faciiity ID rt
336-399-3646
[e-mail]
(L1
Z
(n
A cool < JOE Na2S203 (Mitre only)
�Waypaint
a Cool5C
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ANALYTICAL
a
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O None Required
E NaCk
27" Whitten Road
"
�
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F E
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Memphis, TN 38133
Unless noted, all containers
a
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[phone]
per Tabie II of 40 CFR Part
R
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K N3PO4 prft2
135.
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m
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1 Cool <= 6C NA25203
Date
Time
Sample Identification
Required
A alysis / P eservatiye
Comments/Notes
..1D
G� �I
Metals:Al,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,Mg,Mo,hlg,Ni,Se,Na,P,S,K,Zn
lti �l`t111�11111111illilt i tiwtlilill .6 � 7
EINA RC5011 (L`S hnc
Washington
For Laboratory use Only
Sampled by )Name - Print)
p {�
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Sears
Lab Comments
lin Re
Da e Time
Received by: (SIGNATURE]
Date lime
y
�N
aian Co I.ertemp
Relinquished by: (SIGNATURE)
at Time
Received by: (SIGNATURE)
Date Time
Relinquished by: (SIGNATURE)
Date Time
:SIGNATURE]
�)hy-.
-Date Time
.r) i "

Waypointo
ANALYTICAL
11/12/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-305-0044
Client Project Description: Washington
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 11/1/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 6

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington
Lab Report Number: 19-305-0044
Date: 11 /12/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 88457 (Washington)
Analyte: Aluminum
QC Batch No: 1-462827/1-462465
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: 1-462827/1-462465
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Iron
QC Batch No: 1-462827/1-462465
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: 1-463094/1-462465
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: 1-462827/1-462465
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: 1-462827/1-462465
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 6

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Washington Report Date : 11/12/2019
755 Yadkinville Rd Information : Received : 11/01/2019
Mocksville , NC 27028
Report Number : 19-305-0044 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 88457
Matrix: Solids
Sample ID : Washington
Sampled:
10/31/2019
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.3
%
0.010
1
11/04/19 17:45
ADM
SW-DRYWT
Ammonia Nitrogen
9300
mg/Kg -
dry
676
1
11/12/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<128
mg/Kg -
dry
128
128
1
11/06/19 14:24
ZBD
4500NO3F-2011
Organic N
28270
mg/Kg -
dry
37.84
1886
1
11/12/19 15:00
CALCULATION
pH
7.1
S.U.
1
11/11/19 06:22
JSL
9045D
Total Solids
3.75
%
0.010
0.010
1
11/04/19 17:45
ADM
2540G-2011
Total Volatile Solids
45.6
%
0.010
0.010
1
11/04/19 17:45
ADM
2540G-2011
Total Kjeldahl Nitrogen
37600
mg/Kg -
dry
1890
1
11/12/19 15:38
CLP 4500NORGD-2011
Phosphorus
15400
mg/Kg -
dry
69.5
135
1
11/06/19 01:54
KKM
6010D
Aluminum
34300
mg/Kg -
dry
54.9
135
1
11/06/19 01:54
KKM
6010D
Arsenic
<11.3
mg/Kg -
dry
11.3
13.5
1
11/06/19 01:54
KKM
6010D
Cadmium
<1.34
mg/Kg -
dry
1.34
2.70
1
11/06/19 01:54
KKM
6010D
Calcium
13500
mg/Kg -
dry
454
676
1
11/06/19 01:54
KKM
6010D
Chromium
26.5
mg/Kg -
dry
5.14
6.76
1
11/06/19 01:54
KKM
6010D
Copper
124
mg/Kg -
dry
3.92
6.76
1
11/06/19 01:54
KKM
6010D
Iron
17000
mg/Kg -
dry
115
135
1
11/06/19 01:54
KKM
6010D
Lead
17.8
mg/Kg -
dry
4.03
8.11
1
11/06/19 18:51
BKN
6010D
Magnesium
2140
mg/Kg -
dry
60.0
135
1
11/06/19 01:54
KKM
6010D
Manganese
411
mg/Kg -
dry
4.95
13.5
1
11/06/19 01:54
KKM
6010D
Mercury
0.884
mg/Kg -
dry
0.0900
0.408
1
11/06/19 14:57
TJS
7471A
Molybdenum
<3.51
mg/Kg -
dry
3.51
6.76
1
11/06/19 01:54
KKM
6010D
Nickel
13.6
mg/Kg -
dry
4.46
6.76
1
11/06/19 01:54
KKM
6010D
Potassium
2260
mg/Kg -
dry
80.5
135
1
11/06/19 18:51
BKN
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 6

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-305-0044
Lab No : 88457
Sample ID : Washington
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington
Information :
REPORT OFANALYSIS
Report Date : 11/12/2019
Received : 11/01/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 10/31/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<13.2
mg/Kg -
dry
13.2
13.5
1
11/06/19 01:54
KKM
6010D
Sodium
2730
mg/Kg -
dry
209
676
1
11/06/19 01:54
KKM
6010D
Zinc
370
mg/Kg -
dry
29.2
33.8
1
11/06/19 01:54
KKM
6010D
Sulfur
4950
mg/Kg -
dry
132
135
1
11/06/19 01:54
KKM
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
11/06/19 01:54
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
L Limit Exceeded
Page 4 of 6

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-305-0044
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
-7
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ISovanchampa Yos Date & Time: 11/01/2019 09:49:56
Page 5 of 6

Client Name/Address
Client Project Manager/Contact
Billing information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NG 27028
Project Description
Project/Site Location (City/State)
RUSH - Additional charges apply
Met od of Shipment
Matrix Key
Special Detection Urnit(s)
Fed Ex �u5P5
WW - wastewater GW -Groundwater
Date Results Needed
�uPS
rier Client Drop Off
DW -Drinking Water S - Soil /Solid 0-Oil
P- Product M • Mis[
Other
Project Number
Project Manager Phone n
Project Manager Email
Purchase Carder Number
Site/Facility M p
336-399-3646
brent col lins@emaresources. coin
Z
(/)
A Cool r 10C Na2S203 (Micro Only)
°i
-�
U
-
B Cool <= 6C
Waypoint.
'd
-
C]
ra
C pHc2
ANALYTICAL
yv
=
0
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6
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21
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None
p None Required
E NaOH pH>10
'790 Whitten Road
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UJ
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1■
F HNO3 pH-2
Memphis, IN 38133
Unless noted, all containers
p
o
Z
G HCL pHc2
[901) 213-2400
per Table II of 40 CFR Part
V
E
x
m
Q]
�_
O
C)
H H3Pp4 pH<2
I Cool t= 6C NA25203
13&
3
r
g
Z
I--
Date
Tine
Sample Identification
Required
Analysis / Preservative
Comments/Notes
✓
V-
tf
tI
V
Meta Is:AI,As,Ca, Cd,Cr, Cu, Fe, Pb
17-
M n,Mg, Mo, Hg, Ni, Se, Na, P,S, K,Zn
I U
111��Illlll�lllllllIIIIIINIIl11IIIIIIIIIII Illlll�I Illf 46 ,*-0°
T 1-01-201�
9
09:49:35
Washington
Ll
IF
For Laboratory Use Only
Sampled by (Name - Print)
�p � �[
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Lab Comments
Sea
(.s/� i rr
y/
Relinqui : { NA T E)
pate Time
Receive by: {SIGNATURE}
Date Time
y
.(
�a]3 ] �, cc
Blank/C ter mp
Rehn hed by [Sl A
Date Time
Received by: {SIGNATURE)
Date Time
/ V/3 s I y
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Relinquished by: SIGNATURE)
Date Time
Receive by: `S GN UREj
Date Time
o
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Page 6 of 6

aceAnalytical a ANALYTICAL REPORT
National Center for Testing &Innovation March 26, 2019
EMA Resources
Sample Delivery Group: L1079944
Samples Received: 03/19/2019
Project Number:
Description: Washington
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: z � /��
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
Is performed per guidance provided in laboratory standard operating procedures:060302, 060303,and 060304.
F +

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
WASHINGTON L1079944-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FC
Wet Chemistry by Method D93/1010A
10
F
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
RC
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1079944
03/26/1916:25 2 of 21

ONE LAB. NATIONWIDE. *
WASHINGTON L1079944-01 Waste
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
M
SAMPLE SUMMARY
Collected by
Brent Collins
Batch
WG1252668
WG1253413
WG1253125
WG1254957
WG1252575
WG1254956
WG1254006
WG1254729
WG1253188
WG1254854
WG1254114
WG1254111
Dilution Preparation
date/time
1 03/20/191148
1 03/21/1914:51
1 03/21/1910:44
1 03/26/1914:32
1 03/21/1910:55
1 03/25/1914:43
1 03/22/1913:12
1 03/25/19 00:01
1 03/21/1917:02
1 03/25/19 07:03
1 03/22/1916:51
1 03/23/19 06:15
Collected date/time Received date/time
03/18/19 08:30 03/19/19 08:30
Cp
Analysis
date/time
03/20/191148
03/21/1914:51
03/22/191100
03/26/1914:32
03/21/191121
03/25/1914:43
03/22/19 2121
03/25/1919:09
03/21/1917:02
03/25/1918:23
03/23/1912:03
03/24/1915:22
Analyst
RT
CGD
SDL
MJA
JZW
BAM
TCT
CCE
JHH
KLM
LEL
LEA
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG:
EMA Resources L1079944
DATE/TIME: PAGE:
03/26/19 16:25 3 of 21

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
7
GI
Cassandra Foster
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 4 of 21

WASHINGTON
Collected date/time: 03/18/19 08:30
Preparation by Method 1311
SAMPLE RESULTS - 01
L1079944
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
3/21/2019 2:5113 PM
WG1253413
TCLP ZHE Extraction -
3/20/20191148:34 AM
WG1252668
Fluid 1
3/21/2019 2:5113 PM
WG1253413
Initial pH 7
3/21/2019 2:5113 PM
WG1253413
Final pH 5
3/21/2019 2:5113 PM
WG1253413
Wet Chemistry by Method 9012 B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Cyanide ND 0.250 1 03/22/20191100 WG1253125
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide 66.8 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 03/26/201914:32 WG1254957
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.20 T8 1 03/21/20191121 WG1252575
Sample Narrative:
L1079944-01 WG1252575: 7.2 at19.5C
Wet Chemistry by Method D93/1010A
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Result
Qualifier
Dilution
Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1
03/25/201914:43
WG1254956
Mercury by Method 7470A
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Mercury ND
0.0100
0.20
1 03/22/2019 2121
WG1254006
Metals (ICP) by Method 6010D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Arsenic ND
0.100
5
1 03/25/201919:09
WG1254729
Barium ND
0.100
100
1 03/25/201919:09
WG1254729
Cadmium ND
0.100
1
1 03/25/201919:09
WG1254729
Chromium ND
0.100
5
1 03/25/201919:09
WG1254729
Lead ND
0.100
5
1 03/25/201919:09
WG1254729
Selenium ND
0.100
1
1 03/25/201919:09
WG1254729
Silver ND
0.100
5
1 03/25/201919:09
WG1254729
Volatile Organic Compounds (GC/MS) by Method
8260D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Benzene ND
0.0500
0.50
1 03/21/201917:02
WG1253188
Carbon tetrachloride ND
0.0500
0.50
1 03/21/201917:02
WG1253188
Chlorobenzene ND
0.0500
100
1 03/21/201917:02
WG1253188
Chloroform ND
0.250
6
1 03/21/201917:02
WG1253188
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1079944
03/26/19 16:25 5 of 21

WASHINGTON
SAMPLE RESULTS
- 01
Collected date/time: 03/18/19 08:30
L1079944
Volatile Organic Compounds
(GC/MS) by Method 8260D
Result
Qualifier RDL Limit Dilution
Analysis
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
03/21/201917:02
1,1-Dichloroethene
ND
0.0500 0.70 1
03/21/201917:02
2-Butanone (MEK)
ND
0.500 200 1
03/21/201917:02
Tetrachloroethene
ND
0.0500 0.70 1
03/21/201917:02
Trichloroethene
ND
0.0500 0.50 1
03/21/201917:02
Vinyl chloride
ND
0.0500 0.20 1
03/21/201917:02
(S) Toluene-dH
91.1
80.0-120
031211201917.02
(S) a, a,o-Trifluorotoluene
88.7
80.0-120
031211201917:02
(S)4-Bromofluorobenzene
93.8
77.0-126
031211201917:02
(S) 1,2-Dichloroethane-d4
121
70.0-130
031211201917:02
Chlorinated Acid Herbicides (GC)
by Method 8151A
Batch
WG1253188
WG1253188
WG1253188
WG1253188
WG1253188
WG1253188
WG1253188
WG1253188
WG1253188
WG1253188
ONE LAB. NATIONWIDE. *
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I _
mg/I
mg/I
date/time
2,4,5-TP (Silvex)
ND
0.00200
1
1 03/25/201918:23
WG1254854
2,4-D
ND
0.00200
10
1 03/25/201918:23
WG1254854
(S)2,4-DichlorophenylAcetic Acid
59.4
14.0-158
031251201918.23
WG1254854
Pesticides (GC) by Method
8081B
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 03/23/201912:03
WG1254114
Endrin
ND
0.00500
0.02
1 03/23/201912:03
WG1254114
Heptachlor
ND
0.00500
0.0080
1 03/23/201912:03
WG1254114
Lindane
ND
0.00500
0.40
1 03/23/201912:03
WG1254114
Methoxychlor
ND
0.00500
10
1 03/23/201912:03
WG1254114
Toxaphene
ND
0.0100
0.50
1 03/23/201912:03
WG1254114
(S) Decochlorobiphenyl
78.2
10.0-128
031231201912.03
WG1254114
(S) Tetrochloro-m-xylene
E7.4
10.0-127
031231201912.03
WG1254114
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) 2,4, 6-Tribromophenol
(S) p-Terphenyl-d14
ACCOUNT:
EMA Resources
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 03/24/201915:22
WG1254111
ND
0.100
0.13
1 03/24/201915:22
WG1254111
ND
0.100
0.13
1 03/24/201915:22
WG1254111
ND
0.100
0.50
1 03/24/201915:22
WG1254111
ND
0.100
3
1 03/24/201915:22
WG1254111
ND
0.100
2
1 03/24/201915:22
WG1254111
ND
0.100
5
1 03/24/201915:22
WG1254111
ND
0.100
400
1 03/24/201915:22
WG1254111
ND
0.100
200
1 03/24/201915:22
WG1254111
ND
0.100
100
1 03/24/201915:22
WG1254111
ND
0.100
400
1 03/24/201915:22
WG1254111
ND
0.100
2
1 03/24/201915:22
WG1254111
44.8
10.0-120
031241201915.22
WG1254111
25.1
10.0-120
031241201915.22
WG1254111
67.0
10.0-127
031241201915.22
WG1254111
70.9
10.0-130
031241201915.22
WG1254111
64.0
10.0-155
031241201915.22
WG1254111
78.4
10.0-128
031241201915.22
WG1254111
PROJECT:
SDG:
DATE/TIME: PAGE:
L1079944
03/26/19 16:25 6 of 21

WG1253125
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3394178-1 03/22/191046
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
L1080438-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1079944-01
(OS) L1030433-01 03/22/1911:04 • (DUP) R3394173-5 03/22/191105
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide ND 0.000 1 0.000 20
L1080625-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1030625-02 03/22/1911:16 • (DUP) R3394173-6 03/22/191107
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.000 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3394178-2 03/22/19 10:47
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.44 97.5
Rec. Limits LCS Qualifier
50.0-150
L1079918-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1079913-01 03/22/19 10:54 • (MS) R3394173-3 03/22/19 10:55 • (MSD) R3394173-4 03/22/19 10:56
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.28 1.27 76.6 76.3 1 75.0-125 0.416 20
L1080659-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1030659-02 03/22/19 11:10 • (MS) R3394173-7 03/22/19 1111 • (MSD) R3394173-8 03/22/19 1112
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.37 1.18 82.4 71.0 1 75.0-125 J6 14.9 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 7 of 21

WG1254957
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3395262-1 03/26/191432
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1081233-03 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1079944-01
(OS) L1031233-03 03/26/19 14:32 • (DUP) R3395262-3 03/26/19 14:32
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide 54.6 54.6 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3395262-2 03/26/19 1432
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Reactive Sulfide 100 72.9 72.9 70.0-130
ONE LAB. NATIONWIDE. *
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 3 of 21

WG1252575 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1079944-01
L1079918-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1079913-01 03/21/191121 • (DUP) R3393737-2 03/21/191121
Original Result DUP Result Dilution DUP RPD
Analyte su su
Corrosivity by pH >13 7.42 1 2.40
Sample Narrative:
OS: 760 at19.5C
DUP:7.42 at19.4C
Laboratory Control Sample (LCS)
(LCS) R3393737-1 03/21/19 1121
Spike Amount LCS Result
Analyte su su
Corrosivity by pH 10.0 9.98
Sample Narrative:
LCS: 9.98 at19.6C
DUP Qualifier DUP RPD
Limits
J3 1
LCS Rec. Rec. Limits LCS Qualifier
99.8 99.0-101
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 9 of 21

WG1254956 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1079944-01
L1079944-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1079944-01 03/25/19 14:43 • (DUP) R3394331-2 03/25/1914:43
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000
Laboratory Control Sample (LCS)
DUP Qualifier DUP RPD
Limits
i
10
(LCS) R3394881-1 03/25/191443
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 83.3 102 96.0-104
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 10 of 21

WG1254006
Mercury by Method 7470A
Method Blank (MB)
(MB) R3394372-1 03/22/19 20:54
MB Result
Analyte mg/I
Mercury U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00330 0.0100
QUALITY CONTROL SUMMARY
L1079944-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3394372-2 03/22/19 20:57 • (LCSD) R3394372-3 03/22/19 20:59
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0297 0.0289 99.0 96.2 80.0-120 2.86 20
L1080699-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1030699-02 03/22/19 21:02 • (MS) R3394372-4 03/22/19 21:04 • (MSD) R3394372-5 03/22/19 2111
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0316
0.0296 105 98.8 1 75.0-125 6.48 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
SAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 11 of 21

WG1254729
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1079944-01
(MB) R3395011-1 03/25/19 18:50
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0330
0.100
Barium U
0.0330
0.100
Cadmium U
0.0330
0.100
Chromium U
0.0330
0.100
Lead U
0.0330
0.100
Selenium 0.0352
J 0.0330
0.100
Silver U
0.0330
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3395011-2 03/25/19 18:53 • (LCSD) R3395011-3 03/25/19 18:56
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
10.3
10.2
103
102
80.0-120
Barium
10.0
10.3
10.2
103
102
80.0-120
Cadmium
10.0
10.3
10.3
103
103
80.0-120
Chromium
10.0
9.98
10.0
99.8
100
80.0-120
Lead
10.0
10.3
10.3
103
103
80.0-120
Selenium
10.0
10.6
10.5
106
105
80.0-120
Silver
2.00
1.95
1.95
97.7
97.6
80.0-120
L1079918-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1079913-01 03/25/19 13:53 • (MS) R3395011-5 03/25/19 19:04 • (MSD) R3395011-6 03/25/19 19:06
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
10.2
10.2
102
102
Barium
10.0
ND
10.3
10.3
103
103
Cadmium
10.0
ND
10.3
10.2
103
102
Chromium
10.0
ND
10.1
10.0
101
100
Lead
10.0
ND
10.4
10.3
104
103
Selenium
10.0
0.157
10.6
10.5
104
103
Silver
2.00
ND
1.96
1.96
97.8
97.9
ACCOUNT: PROJECT:
EMA Resources
LCS Qualifier LCSD Qualifier RPD
RPD Limits
0.478
20
0.458
20
0.525
20
0.234
20
0.442
20
0.930
20
0.0736
20
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
0.361
20
1 75.0-125
0.544
20
1 75.0-125
0.300
20
1 75.0-125
0.0767
20
1 75.0-125
0.349
20
1 75.0-125
1.02
20
1 75.0-125
0.103
20
SDG:
DATE/TIME:
PAGE:
L1079944
03/26/1916:25
12 of21

WG1253188 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1079944-01
Method Blank (MB)
(MB) R3393313-3 03/21/19 1132
MB Result
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-d8
85.0
(S) a, a, a- Trifluorotoluene 88.9
(S) 4-Bromofluorobenzene 93.4
(S) 1,2-Dichloroethane-d4 120
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
0.0833
0.250
0.0167
0.0500
0.0167
0.0500
0.167
0.500
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
80.0-120
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3393818-1 03/21/19 09:02 • (LCSD) R3393818-2 03/21/19 09:22
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.0250
0.0267
0.0266
107
107
70.0-123
0.171
20
Carbon tetrachloride
0.0250
0.0244
0.0247
97.5
98.6
68.0-126
1.14
20
Chlorobenzene
0.0250
0.0208
0.0204
83.0
81.7
80.0-121
1.64
20
Chloroform
0.0250
0.0240
0.0244
96.1
97.8
73.0-120
1.77
20
1,2-Dichloroethane
0.0250
0.0259
0.0255
104
102
70.0-128
1.43
20
1,1-Dichloroethene
0.0250
0.0213
0.0219
85.2
87.5
71.0-124
2.63
20
2-Butanone (MEK)
0.125
0.191
0.187
153
149
44.0-160
2.32
20
Tetrachloroethene
0.0250
0.0188
0.0184
75.3
73.8
72.0-132
1.97
20
Trichloroethene
0.0250
0.0227
0.0227
90.7
90.9
78.0-124
0.234
20
Vinyl chloride
0.0250
0.0275
0.0283
110
113
67.0-131
2.90
20
(S) Toluene-d8
95.0
91.9
80.0-120
(S) a, a, a- Trifluorotoluene
85.7
84.9
80.0-120
(S) 4-Bromofluorobenzene
90.6
92.2
77.0-126
(S) 1,2-Dichloroethane-d4
115
122
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 13 of 21

WG1253188 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1079944-01
L1078760-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1073760-01 03/21/19 14:21 • (MS) R3393313-4 03/21/19 19:43 • (MSD) R3393313-5 03/21/19 20:03
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier
RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
1.25
ND
0.851
1.34
68.1
107
1 17.0-158
J3
44.5
27
Carbon tetrachloride
1.25
ND
0.524
1.23
41.9
98.2
1 23.0-159
J3
80.3
28
Chlorobenzene
1.25
ND
0.702
1.02
56.2
81.2
1 33.0-152
J3
36.5
27
Chloroform
1.25
ND
0.910
1.20
72.8
95.7
1 29.0-154
27.1
28
1,2-Dichloroethane
1.25
ND
1.15
1.32
92.0
105
1 29.0-151
13.5
27
1,1-Dichloroethene
1.25
ND
0.512
1.14
41.0
91.5
1 11.0-160
J3
76.3
29
2-Butanone (MEK)
6.25
ND
9.21
9.67
147
155
1 10.0-160
4.89
32
Tetrachloroethene
1.25
ND
0.421
0.892
33.7
71.4
1 10.0-160
J3
71.7
27
Trichloroethene
1.25
ND
0.589
1.08
47.1
86.5
1 10.0-160
J3
58.9
25
Vinyl chloride
1.25
ND
0.667
1.54
53.3
123
1 10.0-160
J3
79.3
27
(S) Toluene-d8
98.5
95.2
80.0-120
(S) a, a, a- Trifluorotoluene
94.8
91.0
80.0-120
(S) 4-Bromofluorobenzene
90.5
83.8
77.0-126
(S) 1,2-Dichloroethane-d4
118
119
70.0-130
L1078833-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1073333-01 03/21/19 15:21 • (MS) R3393313-6 03/21/19 20:23
Spike Amount
Original Result
MS Result
MS Rec. Dilution
Rec. Limits MS Qualifier
Analyte mg/I
mg/I
mg/I
Benzene 1.25
ND
1.34
107 1
17.0-158
Carbon tetrachloride 1.25
ND
1.25
100 1
23.0-159
Chlorobenzene 1.25
ND
0.977
78.2 1
33.0-152
Chloroform 1.25
ND
1.28
102 1
29.0-154
1,2-Dichloroethane 1.25
ND
1.31
105 1
29.0-151
1,1-Dichloroethene 1.25
ND
1.27
102 1
11.0-160
2-Butanone (MEK) 6.25
ND
10.2
163 1
10.0-160 J5
Tetrachloroethene 1.25
ND
0.840
67.2 1
10.0-160
Trichloroethene 1.25
ND
1.06
84.5 1
10.0-160
Vinyl chloride 1.25
ND
1.67
134 1
10.0-160
(S) Toluene-d8
94.1
80.0-120
(S) a, a, a- Trifluorotoluene
88.6
80.0-120
(S) 4-Bromofluorobenzene
89.7
77.0-126
(S) 1,2-Dichloroethane-d4
122
70.0-130
ACCOUNT:
PROJECT:
SDG: DATE/TIME: PAGE:
EMA Resources
L1079944 03/26/19 16:25 14 of 21

WG1254854
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1079944-01
(MB) R3395113-1 03/25/191653
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 56.6
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3395113-2 03/25/19 1713
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
2,4-D 0.0500
0.0390
78.0
50.0-120
2,4,5-TP (Silvex) 0.0500
0.0421
84.2
50.0-125
(S) Z4-Dichlorophenyl Acetic
74.2
14. 0-158
Acid
L1079918-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1079913-01 03/25/19 17:27 • (MS) R3395113-3 03/25/19 17:41 • (MSD) R3395113-4 03/25/19 17:55
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0395
0.0387
79.0
77.4
1 50.0-120
2.05
20
2,4,5-TP (Silvex)
0.0500
ND
0.0425
0.0419
85.0
83.8
1 50.0-125
1.42
20
(S) Z4-Dichlorophenyl Acetic
73.0
75.6
14.0-158
Acid
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 15 of 21

WG1254114 QUALITY CONTROL SUMMARY
Pesticides (GC) by Method 8081B L1079944-01
Method Blank (MB)
(MB) R3394554-1 03/23/19 09:59
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
92.6
10.0-128
(S) Tetrochloro-m-xylene
90.9
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3394554-2 03/23/19 10:24
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00904
90.4
55.0-129
Endrin
0.0100
0.00967
96.7
57.0-134
Heptachlor
0.0100
0.00913
91.3
27.0-132
Methoxychlor
0.0100
0.00899
89.9
54.0-155
(S) Decachlorobiphenyl
84.1
10.0-128
(S) Tetrochloro-m-xylene
91.1
10.0-127
L1079891-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1079391-01 03/23/19 1101 • (MS) R3394554-3 03/23/19 1114 • (MSD) R3394554-4 03/23/19 1126
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00993
0.00918
99.3
91.8
1 14.0-141
Endrin
0.0100
ND
0.0102
0.00954
102
95.4
1 10.0-160
Heptachlor
0.0100
ND
0.00975
0.00901
97.5
90.1
1 16.0-136
Methoxychlor
0.0100
ND
0.00979
0.00894
97.9
89.4
1 10.0-160
(S) Decachlorobiphenyl
89.2
80.4
10.0-128
(S) Tetrochloro-m-xylene
97.5
89.0
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
7.85 40
6.69 39
7.89 40
9.08 34
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1079944 03/26/19 16:25 16 of 21

WG1254111 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1079944-01
Method Blank (MB)
(MB) R3394641-2 03/24/191100
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
72.6
10.0-127
(S) 2-Fluorobiphenyl
72.5
10.0-130
(S) p-Terphenyl-d14
82.4
10.0-128
(S) Phenol-d5
29.7
10.0-120
(S) 2-Fluorophenol
49.2
10.0-120
(S) Z4, 6-Tribromophenol
73.0
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3394641-1 03/24/19 10:36
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.0500
0.0383
76.6
18.0-120
2,4-Dinitrotoluene 0.0500
0.0445
89.0
49.0-124
Hexachlorobenzene 0.0500
0.0450
90.0
44.0-120
Hexachloro-1,3-butadiene 0.0500
0.0381
76.2
19.0-120
Hexachloroethane 0.0500
0.0381
76.2
15.0-120
Nitrobenzene 0.0500
0.0354
70.8
27.0-120
Pyridine 0.0500
0.0163
32.6
10.0-120
2-Methylphenol 0.0500
0.0351
70.2
28.0-120
3&4-Methyl Phenol 0.0500
0.0378
75.6
31.0-120
Pentachlorophenol 0.0500
0.0438
87.6
23.0-120
2,4,5-Trichlorophenol 0.0500
0.0453
90.6
44.0-120
2,4,6-Trichlorophenol 0.0500
0.0463
92.6
42.0-120
(S) Nitrobenzene-d5
73.3
10.0-127
(S) 2-Fluorobiphenyl
78.1
10.0-130
(S) p-Terphenyl-d14
83.3
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1079944 03/26/19 16:25 17 of 21

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Abbreviations and Definitions
u
Fc
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
FS
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fn
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard Anal es added to eve blank, sample, Laboratory Control Sample/Duplicate and
9 ( 9 )- Yt n1 P n1
F
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
F
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
e
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
AI
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
Rc
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1079944 03/26/19 16:25 19 of 21

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
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ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1079944 03/2 6/19 16:2 5 20 of 21

Billing Information:
Analysis
/
Container
/ Preservative
Chain of Custody Page _ of_
EMA Resources
Mr. Brent Collins i Pres
Ch kI'MVEWeAnal
755 Yadkinville Roadi�
lcal
755 Yadkinville Road
-
Mocksville, NC 27028
-' Cents rnr 7 tlnp 8lnrwvetron
Mocksville, NC 27028
12065 Lebanon Rd
Report to.
Email To: [e-mail]
Mr. Brent Collins
vone-6157ssaass2[An
Far 615-758-5859I Phone; 59
Pro ect
City/State ,�/
`L
Description: ��,ns�n
Collected:
1�
q
L a V I
DI 70'
Phone: [phone]
Client Project #
Lab Project #
Fax: [phone]
0
Collected by (print):
Site/Facility ID #
P.D. #
Acctnum: EMARES
&lti.,.s
u7
W
,
7emplate:T11413
Collected by (signature}:
Rush? (Lab MUST Be Notified} Quote #
I
�
O
U
Prelogin: P6$9634
i'J��� ,/�'(,�(�/.7-
Same Day _ Five Day
Next Day _ 5 Day (Rad Only) Date Results Needed
TSR: --1 Cassandra Foster
Immediately /
—Two Day 10 Day (Rad Only) No.
4�-
1702
PB: f f R
Packed on Ice N y_✓
Three Day of
a
Shipped Via: FedEX Ground
Sample 10
Comp/Grab
Matrix •
Depth
Date
Time
ntrs
rsen,a,Ls
r.,
_ m.-
DC
F--
ss
3
311k119
8';,X6-,
2
x
x
—o I
sl,�, -►
I
* Matrix:Remarks:
Sample Pccei heck'liat
SS - Soil AIR - Air F - Filter
pH Temp
COC Seal Pseser.t/Intact: NP Y N
COC Signed/Accurate: "f WN
GW- Groundwater B- Bioassay
Bottles arrive inta^-t: 24
WW - Waste Water
Flow Other
_N
Correct bottles used: _ZY _N
DW - Drinking at r
OT - Other s
Samples `r urned via: e{ �!�
Y FedEx Tracking# 7 �l t7.J 14�
Sufficient volume sent: ,Y _N
If Applicable
_UPS _Courier _
f
VOA Zero Headspace: _Y N
///
Preservatlen Correct/Checked: Y —N
Relinquished by : (Signature)
Date:
Time:
Received by: (Signature)
Trip Blank Received: Yes No
>h
TBR
Relinquished by : (Signature)
Pate:
Time:
Received by: (Signature)
Temp: T Bottles Received:
2.
If preservation required by Login: Date/Time
r(}z(i.6e
Relinquished by (Signature)
Date:
Time,
Received for la y: (Si atu e)
Date: Time: -7
3/ iG (� 1 C JU
Hold:
Conditi
NCF /�

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (I5A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
ClassA:71
Alt. A (timeltemp) ❑ I Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicahle to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density 211
Alt. (2) Process to S ignificantly Reduce Patho ens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"':
Lime Stabilization ❑
Air Drying ❑
Composting ❑
JAerobic Digestion ❑
Anaerobic ❑i estion
If applicable to alternative rformed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
37444.9
67252
248428
MPNIg
0
Quarterly
G
SM92210E
CFtJ
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
cvliform)
3 MPN per 4 grams
total solid (dry
Weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt-1 (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) 0
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ w "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are
significant penalties for false certification including fine and imprisonment."
Hope Woolard - Water Resources Superintendent
Preparer Name and Title (type or print)
I ok& Q ']b L
1f5-I >
Signatu of parer* Date
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
1/6/2020
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
4ENR FORM PVRF 02T (1212006)

Date
Location ##
1
I
Summary Sheet
Fecal Coliforms
PathogenReduction
MPN/g
248427.7
37444.9
112244.9
42606.5
88709.7
41269.8
38202.2
Log
5.3952
4.5734
5.0502
4.6295
4.9480
4.6156
4.5821
67252
Geometric Means/g
Total Dry Solids
Signature

AE DATE / TIME
Sampled By
Received By 0&-))14-dS 3-14-1G 0 24 hr. Check,3-1/
Analyzed By - / q - l c° 1,3, 48hr. Check 316--i-I a 11,5� &T)
Calculated By r/1072 hr. Check 3
Checked By S i
Temp 3sT.-5- OC
4-41-f OC
Sample Location Slit dge# I
Sample Type: Grab x Composite
Preservation:. NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Pre-mmntive Test
ON 1TWO
Fecal Coliform Test
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
Fecal Coliform Test
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
L—
I
Revised 5-23-16
MPN/g= lox ::rq = ;Iqa--�-
6,

Sampled By
Received By
3-14-1 C el
Analyzed By
toix
Calculated By
3 -i6 W-5
Checked By
Temp OC
A E DATE / TIME OC
Sample Location Sludge# 1 _14" t llc_a t,,�2
24 hr. Cheek3 Sample Type: Grab x Composite
48 hr. Check JND Preservation: —NONE
72 hr. Check JRP
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumntive Test pUi-)
Fecal Coliform Test
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
a Pat,
I A) 0
Revised 5-23-16
MPN/g = 10 x 0 "wIPG �a1 fti
O'CO/ n c. C031g
C>D000c-) I (#-q,) �q- -4 , -3k-s1 te,

DATE / TIME
Sampled By
Received By 6-4 ic 3-1:4-1
Analyzed By
Calculated By 02L
Checked By PW,,—
Temp OC
4-q, -t 0 C
I
Sample Location sill dge# 211-
24 hr. Checks 15-/� 11 17—��o Sample Type: Grab x Composite
48 hr. Check:3 -&, - /1 , 1.2 C5 &P Preservation: NONE
72 hr. Check.3 --/ -I-lq
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
I US
MMMWM==M=wM===wwwM
Mi
mmmmmil
Fecal Coliform Test
111111
riTITITITITI I Z=Mna�
NM
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
I j
Revised 5-23-16
MPN/,g = 10 x �14 ' 4- q 0

"iN A E DATE / TIME
Sampled By All,
Received By
Analyzed By
Calculated By
Checked By
24 hr. Check]
48 hr. Check
72 hr. Check 1,20
Temp OC
4q.-t OC
Sample Location Sludge #
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumntive Test
Fecal Coliform Test
lyqc
Kip —qg-l�
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes 10 mL
Double Strength (DS) Control
Single Strength (SS) Control
H EC Broth Control
Revised 5-23-16
MPN/g = 10 x 33 1
- 11,1/5-
rot

A DATE / TIME
�
Sampled By 17,444--
Received By k'-v 5 —14
Analyzed By
Calculated By
Checked By
24 hr. Che&31511. '113'y'
48 hr. Check -16 - 11
72 hr. Check Ae
Temp OC
4-q, -1- 0 C
Sample Location Slufte # A
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(WN)(Aqueous)
Pri-qiimnfivi- Ti-qf
-11010
-
24 hours
win=
IMEJ
SIMON,
Fi-en] C'nlifnrm Teqt
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
1 EC Broth Control
Revised 5-23-16
MPN/g = 10 x
o-c®> x 3,qq C, CO3 q
33D

nOVA E DATE / TIME
, "W�
Sampled By 05-44C, Sam
Received B Lsy Analyzed By 0�66 24 hr. Check-3-/,,57-/ Sam
J-P; 10V 48hr.Cheek:3 ,-i 1123(
Calculated By 72 hr. Check
Checked By
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Prequmntive Test
Pres
Temp OC
q-q.-f OC
ple Location Sludge # f
pie Type: Grab x Composite
ervation: NONE
L I
mmmm
MMMOOM
MMMMON
Ow '9, Ky- /I
Fecal Coliform Test
OF M I
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength (DS) Control
Sin gle Strength (SS) Control Al -
EC Broth Control A,
MPN/g = 10 x
114-
Revised 5-23-16

APNE DATE / TIME
-
Sampled By ✓
Received B
"y Analyzed By
Calculated By
Checked By
Temp OC
4-11—r OC
Sample Location Sludge
24 hr. Check3
11i:i I Sample Type: Grab x Composite
48 hr. Check 12 fHP Preservation: — NONE
72 hr. Check 3 12 A)
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MEPN)(Aqueous)
Presumptive Test
I111
hou:r:sAMIM===IM=OM
Fecal Coliform Test
WIS. I*=
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
N-0-ort)- -L
Single Strength (SS) Control
EC Broth Control
U
Revised 5-23-16
MPN/g = 10 x
0 "Oo

A E
Sampled By
'� J
Received By
Analyzed By
Calculated By
Checked By
DATE / TIME
Temp °C
4• °C
Sample Location Sludge 7
24 hr. Check3`%7-/g J j � Z'�7 Sample Type: Grab x Composite
48 hr. Check? /��i �a%��r 114D Preservation: NONE
72 hr. Check
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
Ii1
1 1111 ,� 11111 �4
1 11IIIII
I II1111 _
_Y_�,
Fecal Coliform Test
—
� 1•
_ 1 1 1 -■�-
1 1 1 1 .—;
I J 1 1 1 1 1 1 1 1 b
; 1 1 1 1 1 1 1
� 1 1 1 1 1 1 1 1 i�
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
7
Single Strength (SS) Control
y
EC Broth Control
I.p
V
Revised 5-23-16
MPN/g = 10 x 6-9 — 49
%v,

CITY OF WASHINGTON
SLUDGE
Name
Date/Time
Sampled By
-'
Received By`
||nneon\8/aharBath
—
Time inOven
ADa|yZedBy
--12
'
Time out of Oven
Ca\cu|,ated By
Time Weighed
/
Checked By

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Time
Sampled By r ;� '�`� afPn-- 3-i� -1 g G 8 g
Received By
Analyzed By 14-19 1019
Calculated By-/-i%g j 33
Checked By �1 -
Time on Water Bath / c
Time in Oven r 34
Time out of Oven I�tg
Time Weighed 115,50
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Wei ht
% Dry Solids
Revised 5-23-16, 3-13-19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Time
Sampled By
;!2,3 G—
Received By S-{-
Analyzed By J,," IJA,�'& _3 - 14-19 �e
Calculated By � lovz
Checked By
Time on Water Bath /� 3 3
Time in Oven i q 5-/
Time out of Oven /52154
Time Weighed '� 30 (-3 1
Sample #
Eva p Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dr v Weiciht
% Dry Solids
Sir I Ice±a
or
q�,3 6
Revised 5-23-16, 3-13-19 JDW

0 Name Date/Time
Sampled By
Received By `
Analyzed By
Calculated By --
Checked By
CITY OF A|NGTSLUDGE
O
Time onVVaterBath
Time in Oven
Time out OfOven
Time Weighed 4\
�
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weiaht
06 r Solids

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Time
Sampled By ' Y 3-1�l-I `�, o ado
Received Bye,,,
Analyzed By
Calculated By ?
Checked By 6gtiL,-�f3 p i�l d5
Time on Water Bath i l-)-,�l
Time in Oven e�
Time out of Oven
Time Weighed
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Wei ht
% D Solids
Revised 5-23-16, 3-13-19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
0 Named Date/Time
Sampled By`,Ur i'='°-!✓'►4-11
Received By.�
Analyzed By 71,wzL 3
Calculated By % eg�
Checked By t -Tt"-
Time on Water Bath 134�
Time in Oven 1031
Time out of Oven i tG1
Time Weighed C)
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids
/ 2 7:T 3gk-
933,Z
-�g133.5
11,561,6
1 ,51, q�
I5
Revised 5-23-16, 3-13-19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Time
Sampled By (14 ,- � 4 - / ? ,
V
Received By
Analyzed By fwC Z
Calculated By
Checked By
Time on Water Bath R53
Time in Oven !031
Time out of Oven
Time Weighed
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
DrV Wei q t
% Dry Solids
4i3 0 �6 z;y
904�'
,3
/y
Revised 5-23-16, 3-13-19 JDW

Contact: Brent Collins Report Date: 4/24/2019
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 3/18/2019
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test
Meritech Work Order # 03181954 Sample: Washington Composite 3/18/19
Total Solids Volatile Solids % Volatile Solids
Week 1 1.13 0.700 0.620
Week 2 1.20 0.750 0.626
Weep 3 1.26 0.750 0.591
Week 4 0.830 0.530 0.641
Week 5 0.870 0.560 0.640
Pass or Fail
Van Kleek Reduction (%): -9.12 Pass
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016 Chain of Custody Record (COC)
NPDES#:
Client: EMA Resources Inc. Phane:-336-751-1441
Address:-755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email: brent-collies, a e iarps©v,cesin, ..QM
Project:
P.O.#:
Turn Around Time*
Attention:_ Brent Collins
Wow would you like your report sent? *RUSH work needs prior approval.
Std(10da s) 3 S Da 5 2a_d8Mrs
Circle all that appl Email referred) , Fax, Mail
_J�
��.
ERITECH' NC.
IVIJl I�
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: info@meritech[abs.com
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print):
Lab Use Only
Start
End
Camp ?
Grab?
#of
Cont.
T
i est(s) Required
On Ice?
Yes / No
pH OK?
C1 OK?
Date
Time
Date
Time
W � s� 0.,
3/t1 sr�19
�G'• 30,,�..
C
3 4 Z a,7 .
11 C /'1
n/ i.�n2"rs"7Y7n ,G'I'F i �ti}�'
3!l �Il g
6 •+Yjow
C
r
S
Temperature Upon
Receipt:
•U
Method of
Shipment:
*** Dechlorination (10.5 pm) of Ammonia, Cy snide, Phenol and TKN samples must be done in the field priorto preservation. ***
Comments:
Compositor #
Q UPS
Jug #
Li Fed Ex
Are these results for regulatory purposes? Yes No
Report results in: mg/L [ mg/kg ug/L
Hand Delivery
R finq dy _ Date: Time:
//..3oow. 3/ip/i9
Received by: Dat Time:
�3f8/�P //,
Other
Relinquis y: Dale: Time:
1511 f 1: a! .�,
Received by: Date: Time:
"
Relinquished by:,.
Date: Time:
Receive b Lab: � D Time: 1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number:
WWTP Name: Washington WWTP NPDES Number:
Monitoring Period: From 1/1/2019 To 12/31/2019
WQOOO 1026
NCO020648
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timelternp) g7
Alt B (Alk Treatment)❑
I Alt. C (Prior Testing)
Alt.D (No Prior Test) ElProcess
to Further Reduce Pathogengs
M
lfapplicabletoalternative performed (Class A only) indicate "Process to Further Reduce Pathogens";
Compost ❑
Heat Drying ❑
Ileat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class 13:
Alt, (1) Fecal Density_ 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ JAeroblc
Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative perfarmed Class A or Class 13 complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
tY
Number o
Excee-
ences
Frequency
of Analysis
Sample
'Type
Analytical
Tech-nique
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
5202.3
5877
6451.6
MPNIg
0
Quarterly
G
SM9221 CE
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
wei ht)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternativeperformed:
Alt.] (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt, 3 (30-day bench) ❑Alt.
4 (Spec. 0, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. S (Drying - Unstable) ❑
Alt. 9 (Injection) []
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."'
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Hope Woolard - Water Resources Superintendent
Pre arer Name and Title (type or rint)
SignaturJ of Pre er*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
s L ) 1/612020
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Date: 4/25/2019
Location
1
2
3
4
5
6
7
Summary Sheet
Fecal Coliforms
7 t •, . e Reduction
MPN/g
5202.3
5882.4
6451.6
5980.1
6060.6
5882.4
5750.8
Log
3.7162
3.7696
3.8097
3.7767
3.7825
3.7696
3.7597
5877
Geometric Means/g
Total Dry Solids
D�-,
Signature

/N M
Sampled By��`-�'�
Received By
Analyzed By h
Calculated By
Checked By G
DATE�/I E
Li 1 (u Ct..') 24 hr. Check 2 / —C
HI 1�t 48 hr. Check,�/3"/q
72 hr. Check iJ
�t13
Temp -3H, 7 5 °C
--357; cOC
Sample Location Sludae # 1 ` qaC -
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
Fecal Coliform Test
mL Sample 0.001
0.0001
0.00001 0.000001
0.0000001
0.00000001
MPN
24 hours
-
—
—
.<
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
/V
Revised 5-23-16
MPN/g = 10 x (� _
C,Cc) I X .�.T� T� ✓ 0 ,CC) P L+a

NAMF
Sampled By
Received By
Analyzed By
Calculated By
Checked By
DATE / �'I_ME
`t�ti�li �c�f�g
LI) 1, l (I OgC5
Cl 1 4-1 -),
24 hr. Check
48 hr. Check 3 / 0 tj
72 hr. Check p
Temp` I S °C
aS, C°C
Sample Location S1uCl
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
PrPcmm�fivn Tack
$I of elm
1
0.00000001
NO
Feral ("nlifnrm Tno1-
mL Sample 0.001 0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours -+-
—I
I
I
I
Ia
>.
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength (DS) Control j1 fy
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
MPN/g = 10 x-
0,CC) f x 21 a a.cc�3S

N MI
Sampled By
Received By
Analyzed By
Calculated By cam,
Checked By
DATE / TIME
' u 111 0*sue.
Lq11117
24 hr. Check a %i.J
48 hr. Check 3 / JYVJ
72 hr. Check i -t I pj,,J
Temp '�9, 7 5 °C
aSa C
Sample Location Sludge # wo.}ems hcAfh `�`I,7'C.
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM 'TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
PrPcmmntivn TPef
0.00000001
Eon
MMMMMM
MMMMMMMMMM
11
Mmm"0111,
IFPPQI Cnlifnrm TPc4
0.0000001
1 0.00000001
MMMU
M-MMMM!
'I", -H
-- ,
--1- -1----
11
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
/
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
MPN/g = 10 x ) , _ 9
t .oC I x .3 O ay oa 3GCo S �a.4 m NAp

N
Sampled By
Received By
Analyzed By
Calculated By
Checked By
24 hr. Check /'0 ,)
48 hr. Check S / 11r-I JNJ
72 hr. Check
i
Temp '�H,?5°C
�S (1-°C
Sample Location Sludge # 3�C-
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
PrPcmmnfi— TPc1
mL Sample 0.001
0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours —
_
_
_I
I
F
I
I
I
1
1
2
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
/
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
MPN/g = 10 x _
C ,00 1
`f.5�.�o

N M
r
Sampled By
Received By
Analyzed By L
Calculated By it�
Checked By
DATE / TIME
�t l li �m9 ,io
ii 1, `I DC3
24 hr. Check
y l 1 ��l G
48 hr. Check//3/4 J&J
72 hr. Check t 141, JOLJ
qlol1353
Temp 2` ,75'C
C:�ro C
Sample Location Sludge
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM 'TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presmmntive Test
1 I I I 1 1 I
_III 1 I I 1 1 .
� 4' -
F+'eeal C'nlifnrm Test
mL Sample
1 0.001
0.0001
0.00001
0.000001
0.000001
0.00000001
MPN
24 hours
—
I —
I —
I
I
I
I
I
I
I
I<
! 7
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes 10 mL
Double Strength (DS) Control 1V&
Single Strength (SS) Control IV
EC Broth Control
Revised 5-23-16
MPN/g = 10 x P , $ _ V
Ca3�t

NA
Sampled By
Received By
Analyzed By
Calculated By -
Checked By
DATE / TIME
Clks
1z(��cb 24hr. Check
�/ L-
'd ! l 1 �1 /v /O 48 hr. Check
3 /
72 hr. Checker
Temp 5 °C
�S i�!rOC
Sample Location SIudLi e C--.
Sample Type: Grab x Composite
Preservation: NONE
FECAL. COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
P---fivn ,Y'naf
����
� �'
j■ � � � �
� � � � �
? �. � � � � �
� � � � � � �
� � � �"� � � �
�
e©ae�seevoesev�eseive����������
III
IMMI
;ems®�eeeveoves©®©$���■�������
_ ___a
VA-1 f'nlif— 'r—+
mL Sample
1 0.001
0.0001
0.00001 0.000001 0.0000001
0.00000001
MPN
24 hours
—
I
I.—
_
—I
I_I
I
I
I<
P
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Contrnl
Quality Control Tubes
10 mL
Double Strength (DS) Control
11 f j
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
MPN/g = 10 x
o,00Z19

Sampled By
Deceived By
Analyzed By
Calculated By t
Checked By po-��,
DATE / TIME
=/S /13/
24 hr. Check / 5y�,,1,J
48 hr. Check/WV/1
72 hr. Check
Tempi !S°C
aS �°c
Sample Location SludLye -
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
IT, 1�1�1
II11
1 II1II;
1 IIt111
�1 III1111
�iese�®©sM
NM�����
Ti'Pnal !'nlifnrm Tom+
II ,��1
1II
F III1'MEN�
t IIIII
�III1t1, _
� _ 1 IIILIII� _
IE
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Cnntrnl
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
MPN/g = 10 x P s
o,ocl x 3.0� co3C

Sampled By
Received By
Analyzed By
Calculated By
Checked By
24 hr. Check
48 hr. CheckVOI J YJ
72 hr. Check z, JDI,J
TempS°C
C
Sample Location Sludge # — We.� � l��Eh q`d,�'C.
Sample 'Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
-
-----------
—`
I l 1 I 1 1
11 1 I I I 1. ■
1 1 1 1 I I I I_
_.
Wmw-
P... I f M;f- Tom+
mL Sample
0.001 0.0001
0.00001
0.000001
0.0000001
0.00000001
MPN
24 hours
I—
—
_
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control 'Tubes
10 mL
Double Strength (DS) Control
j1 f
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
MPN/g = 10 x / , g =
�j 5 , g rim _IA/c�r .
b,o0/ K
3135 0,003i 3

Name
Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Date/Time
Time on Water Bath I ol'�
Time in Oven t 115
Time out of Oven 141+2>
Time Weighed 11'
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids
ltuz ,
(" V
d 1 ]
cl IS 3,5
6L� C i .
l c� S W, 7
"1 35 ,
ej
0
i
^'g }�
[ V - �
­gp
e @
b,q"
7 ,5-79 � , 3
p
d"Y �� �c @C3
—7 Q n
3 a 5C,
Revised 5-23-16, 3-13-19 JDW

Name
Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Date/TMm,
Time on Water Bath 1C)PO
Time in Oven 1114`3
Time out of Oven way
Time Weighed 1-34'i
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids
Revised 5-23-16, 3-13-19 JDW

CITY OF WASHINGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Tirr %,,,
Sampled By I 41 11 t� C)Time on Water Bath
Received By�, J �j jr� Cc� �� Time in Oven
Analyzed By aL� il� 4 ill Time out of Oven
Calculated By-s5=19, / 3 3 Time Weighed '-'
Checked By
#
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids
GSample
�' -7 ,�
�V `-� R ®c
5 C) ...i11 t)
a Q
Scp f c)r
fl J �C ✓1 d i
J F l s3
Revised 5-23-16, 3-13-19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Sampled By
Received By
Analyzed By
Calculated By
Checked By � .j
Name Date/Time
eto5 C),S-
1-1�—
Time on Water Bath 11 15-%
Time in Oven I
Time out of Oven I I
Time Weighed t 5;Lf
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids
<
"1
119
q0-7 �5��
�F �
���3:�
'9�7;k,15Y
1517
310 t'1'
Revised 5-23-16, 3-13-19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Tim
Sampled By v / 44 1. tc 0�
Received By
Analyzed By
Calculated By
Checked By e-c Z 5-/!2
Time on Water Bath t
Time in Oven 139,13
Time out of Oven 11
Time Weighed
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids
Revised 5-23-16, 3-13-19 JDW

Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
� t~ �-il►�►`� IiS�
r
Time on Water Bath /aO
Time in Oven i 3
Time out of Oven
Time Weighed i
Sample #
Evap Dish #
Wet Weight +
Dish Weig�hjt
Wet Weight
Dry Weight +
Dish( Weight
Dry Weight
% Dry Solids
;--
]�j
''D)is+h Weight
Dish ^'Weight
Revised 5-23-16, 3-13-19 JDW

N me Date/Ti
SampledB
Received By -I,,
Analyzed By D9 ko
Calculated By
Checked By cc)
SLUDGE
CITY OF A|NGTON
Time onWater Bath
Time in Oven
Time out of Oven
Time Weighed
Sample #
Evap Dish #
Wet Weight +
Dish Weight
—Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington
WWTP Name: Washington WWTP
Monitoring Period: From 1/1/2019 To
WQ Permit Number: WQ0001026
NPDES Number: NCO020648
12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If a plicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal 2ensity Ell
Alt. (2) Process to Significantly Reduce Pathogens ❑
If a plicable to alternative performed (CIass B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ jAerobic
Digestion ❑
Anaerobic Digestion ❑
1fapplicableto alternative erfarmed Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number oFrequency
Excee-
of Analysis
Sample
]
Type
Analytical
Tech-ni que
inimu
Geo. Mean
aximu
Unitsences
Fecal Coliform
2 x 10 to the
6th power
gramper of
total solids
MPN
3614.5
9087
48920.9
MPNIg
0
Quarterly
G
SM92210E
CPU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of Fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ©
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑Alt.
4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were Performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 115A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
reouirements.)
"This determination has been made under my directiop and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including tine and imprisonment."
Hope Woolard - Water Resources Superintendent Brent Collins; Director of Technical Services
Prep4rer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
V
1.� Lam"- 1/6/2020
Signs of arer* Date Signature of Land Applier {if applicable} Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212006)

Date: 9/23/2019
Location
1
2
3
4
5
6
7
Summary Sheet
Fecal Coliforms
Pathogen Reduction
MPN/g
3614.5
4864.9
3636.4
16352.2
48920.9
10309.3
9698.3
Log
3.5580
3.6871
3.5607
4.2136
4.6895
4.0132
3.9867
9087
Geometric Means/g
Total Dry Solids
Signature

N /4ME DATE / TIME
Sampled By OC">
Received
By Analyzed By MR)
Calculated By Do
Checked By
Temp '; S. 0 'C
0 C
Sample Location Sludee
24 hr. Check q- 2a I Ci t'�,S(69'3 Sample Type: Grab x Composite
48 hr. Check Lj-,,) q Preservation: (Ckllkca
72 hr. Checkcj -a 0L-1 I F3
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Pirpciamnfivp Tprt
11
0.0000001
NOW
Fecal Coliform Test
0.0001 0.00001 1 0.000001 0.0000001 0.00000001
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Control Tubes 1 10 mL
Double Strength (DS) Control A),- a c, 1-/ V-Q
Single Strength (SS) Control Ct CL"l I re
EC Broth Control A Alfa '(I CCJ Y' vleJ
Revised 5-23-16
MPN/g = 10 x 19
D-00IX

Sampled By
Received By
Analyzed By
Calculated By
Checked By
/ N ME
Temp 5. C:i °C
0
Sample Location SI L7e #
24 hr. Check q-.� C , l �� Sample 'Type: Grab x Composite
48 hr. Checkqcj j, 8' Preservation: C-
72 hr. Check6t-j_`
FECAL COLIFORM 'TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
' rtive Test
Fecal Coliform Test
�f
MPN Fecal Colifform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility C ontrni
Quality Control 'Tubes
10 mL
Double Strength (DS) Control
a V-Q.
Single Strength (SS) Control
Il%('C-CL,iI Erb.
EC Broth Control
e CL-y
Revised 5-23-16 ✓

NAME
Sampled By
Received By
Analyzed By
Calculated By
Checked By
DATE / TIME
%:23-15i, 1005
07 -, Z3 - 1 1-f 16),,? 5-
1-3507
Temp 15, G OC
IiN 0 C
Sample Location Sludee 9
24 hr. Check q-.� -I L-1 Sample Type: Grab x Composite
48 hr. CheckL 5--j 01 I- Preservation: T410TITE C-C, A
72 hr. Check(—al;-1 Q ),>/4 F127
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Pyo,enmnfivp TpQf
ME M,
0 - .00000001
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
A)e a 1-/ V-Q
Single Strength (SS) Control
�
ALeq-CLY, 1/,Q
EC Broth Control
�� CL
Revised 5-23-16
MPN/g = 10 x / 9 — = /9 — � � � y, �
0 - Oo/ Y, 3 -�O 0, VC3�

NAME
Sampled By
Received By
Analyzed By
Calculated By I
Checked By
mL Sample 0.001
24 hours —
48 hours k --+-
DATE / TIME
Temp 3 5, OC
Sample Location Sludee 9
24 hr. Check C -92 j, k"?S(o Sample Type: Grab x Composite
48 hr. Check ol Preservation: -NOTILf- C-Cc-"i CC! h) 14 " C,
72 hr. Check9 -I Q �o F-3j
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
IUM 0.000001
I 1x1lli1i1jl
0-000III 001
II I I it II 191' 1 ,iI qi�
IV% 01
MPN Fecal Coliform/g, = . 10 x MPN index f 100 ml
largest volume X % dry solids tested
Control Tubes
10 mL
fQuality
S t Double Strength (DS) Control
V-q
Single Strength (SS) Control
1ALe
ControlEC Eroth
a CL-1
Revised 5-23-16
MPN/g = 10 x /9 = I %9
"Y' 95) 36 36., 0111"

Sampled By
N /4ME
Received By
Analyzed By
Calculated By
Checked By
DATE / TIME
0,55
Temp 5, ')C
I OC
Sample Location Sludge #64 ---
24 hr. Check ctl- 9�tj Ci, 13S(DSample Type: Grab x Composite
48 hr. 5-Check(I',,,2 � ]Preservation: NOtIff CC-1cl <-QA I-C� �-A 'C, -10i 1 4�01 f 0�
72 hr. Check (ikq�,- I Cj
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumnfive Te..qt
41 =
Vi-enf d-nfifhrm Tpet
-
In
r I loll
MPN Fecal Coliform/g = 10 x MPN index f 100 ml
largest volume X % dry solids tested
Sterility Cnntrn]
Quality Control Tubes
10 mL
Double Strength (DS) Control
)UP CI a!-/ V-Q
Single Strength (SS) Control
V-ejc?- CLV- ' I"Q
EC Broth Control
Ve C. aL Le,
Revised5-23-16
MPN/g = 10 x �, 2
-�-
"All

Sampled By
N 'ME
C
17
Received By
Analyzed By
Calculated By
Checked By
DATE / TIME
223 -1 10 Iq
ID110hS 1357
Temp 3 5, G OC
Sample Location Slud eg. GD- C
24 hr. Check Cj, 1361t--V�5 Sample Type: Grab x Composite
48 hr. CheckC'I',,2 �5*-� 130 Preservation: —NftNE Cl:x'i <6 Ic-
72hr. Check0i-�(,-icl, 12.nlf-P,2
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
PrAciYmMiwo T.e+
-100 O I TIr V '
Fecal Coliform Test
1111=11 WIN
MPN Fecal Coliform/a = 10 x MPN index / 100 real
largest volume X % dry solids tested
S I terflitv Confrni
Quality Control Tubes
10 mL
Double Strength (DS) Control
VO a -t-1 V-q
Single Strength (SS) Control
(.I- CL�/- J/,Q
C Broth Control
[±ECL
Revised 5-23-16
MPN/g= IOx
�9
01 VrI35

Sampled By
N��ME
�
-
Received By
n /,Lw"
Analyzed By
Calculated By
Checked By
DATE / TIME
1313
jbjjojj"[ 135-7
Temp 3 5, G OC
'Ei- OC
Sample Location S1udL;e4,Uo_)
24 hr. Check Cj, r 0J 5 Sample Type: Grab x Composite
48 hr. Checkq,,) �5-_j q f,301 Preservation: NfWE C_001<-Cj 'tz-4'C
72hr. CheckOt-.q4,,j, J'� 4Z��
I
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(WN)(Aqueous)
Press' mntive Test
Ww�
MWO
I
Fecal Coliform Test
1111V
-ST 01'1111-,Oi
F 0-066600f ��U!
MPN Fecal Coliform/g, = 10 x MPN index / 100 nil
largest volume X % dry solids tested
,qfPri1i*v Cnnfrnl
Quality Control Tubes
10 mL
Double Strength (DS) Control
c� r, j-/ V-Q.
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
MPN/g = 10 x --' 0
C �OO/ x
C
= 1 3Q �. 3 ,�twf�

NAME
Sampled By
Received By
Analyzed By
Calculated By
Checked By tN
DATE / TIME
31
24hr. Check (t1-._2�-,Cj, /If T1?7
48 hr. CheckCj', t(;ijjL30/jR-D
72hr. Cbeck6'i-At,-IC
j
Temp 3 5, 0 IC
O
Sample Location Sludge # 7)_ C
Sample Type: Grab x Composite
Preservation: Ni)f,W Ci:,(-;Je-C-1
FECAL COLIFORM TEST
Standard Methods 9221 C E-2JIB (MPN)(Aqueous)
Presumptive Test
. . . . . . . . . . .
0.000001 1,1! fill
V ... I C-1;f- 'r-+
MW
0001 .00
M
0.006 001
wx
MPN Fecal Coliform/g = —.. 10 x MPN index / 100 ml
largest volume X % dry solids tested
0 'fPrili+- C-1-1
Quality Control Tubes
10 mL
Double. Strength (DS) Control
Cal V-e
Single Strength (SS) Control
EC Broth Control
L—e �� CLi
Revised 5-23-16
MPN/g = 10 x
0, 00
3

Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF !;
SLUDGE
Standard Methods 2540 1 A• -r
Time on water bath
Time in oven
Time out of oven
Time weighed
_T
Sample #
V--
Evaporating Dish #
,���_
r '
Sample #
-�
Evaporating Dish
11
Wet Weight + Dish Weight
_
Wet Weight + Dish Weight
%. 3 1 5 CK a 123
Dish Weight
/.`JC
� � �
Dish Weight
� C, E � k
Wet Weight
Wet Weight
' -
1st Dry Weight + Dish Weight
1st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Dish Weight (end -1st)
L , i'
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd -1st)
Dry Weight (2nd Dry Weight + Dish
Weight -Dish Weight)
,� �-.� .'� � �
Dry Weight (2nd Dry Weight + Dish
Weight -Dish Weight)
® 4,
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
r 9' j
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
9 -,
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF WASHINGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
1st
2nd
Time on water bath ki
Time in oven
s 013
Time out of oven 1
/ /
Time weighed
i
Sample #
61a
Evaporating Dish #
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
Wet Weight + Dish Weight
/ 3 6
Dish Weight
Dish Weight
9 0 7 g C& • O
Wet Weight
Wet Weight
14 2 & 4fC ,
1st Dry Weight + Dish Weight
- a S 0 5
1st Dry Weight + Dish Weight
19 a, 54, D I
2nd Dry Weight + Dish Weight
9, S'
2nd Dry Weight + Dish Weight
' (p 0 .
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd -1st)
®
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd -1st)
C7
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
j` `�-��_��
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
/
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
3 C
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASHINGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Nam,eDate/Time
Sampled By /'4 t 1 d3 / air �R
Received By Time on water b&
Analyzed By Time in over
Calculated By C -ate- 6-/Time out of over
Checked By /(-) f /m/ "q�; _;- Time weighec
1st
2nd
q4(
II
g L
Ea
it l
Sample #
1 3
Evaporating Dish #
12�
Sample # I
Evaporating Dish #
Wet Weight + Dish Weight
/ a 34
Wet Weight + Dish Weight
Dish Weight
ca--1,4
Dish Weight
Wet Weight
LQ S-( ,S
Wet Weight
1st Dry Weight + Dish Weight
& `r` ,3- 4, 4
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
_
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd -1st)
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd -1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
O Qj
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF WASHINGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Time on water bath
Time in oven
Time out of oven
Time weighed
1st
07-10
2nd
�a
a2
2,12
/3 12,
ioa4
Sample #
1 4/
Evaporating Dish #
/ O
Sample #
I
Evaporating Dish
Wet Weight + Dish Weight
/ 3 0 7- CP 3
Wet Weight + Dish Weight
Dish Weight
p a5
Dish Weight
Wet Weight
4y 01 l O 2r, 113,
Wet Weight
1st Dry Weight + Dish Weight
1st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd -1st)
- -
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd -1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
Q
a 3
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
_Tow 'o- q-f 9
4, -;f-7
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASINGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name, Date/Time
Sampled By a_3n.i % a3 % / o 1-A
Received By Time on water bath
Analyzed By „, t' -j Ala Time in oven
Calculated By %c c T 4 2' S Time out of oven
Checked By /9M, lC 0 Z Time weighed
Sample #
1 17S
Evaporating Dish #
3 3
Sample #
I
Evaporating Dish #
Wet Weight + Dish Weight
© -;r , (,
Wet Weight + Dish Weight
Dish Weight
0 7 (0
Dish Weight
Wet Weight
Wet Weight
1st Dry Weight + Dish Weight
1st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd -1st)
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
'Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9126/19 JDW

Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name ® Date/Time
( 7-;?4)
1st 2nd
I L2f ` aY/7 Time on water bath
Time in oven
> I - - 5' Time out of oven 9
/_ Time weighed / 3 5
Sample #
Evaporating Dish #
5S
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
j p
Wet Weight + Dish Weight
Dish Weight
g 3 $ 3
Dish Weight
Wet Weight
p o -7, -7
Wet Weight
1st Dry Weight + Dish Weight
1st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
g j 3
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd -1st)
—
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd -1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
C�?�
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
,j
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

Sampled By
Received By
Analyzed By
Calculated By
Checked By
CITY OF WASHINGTON
SLUDGE
St 9=Vr Ski
Time on water bath l 1
Time in oven
Time out of oven
Time weig
1 st 12,nd
Sample #
Evaporating Dish 0
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
1 Cl I I
Wet Weight + Dish Weight
Dish Weight
a_2O
Dish Weight
Wet Weight
­bo�� - , S� —
Wet Weight
1st Dry Weight + Dish Weight
0 a
1st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
C) a
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight +
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd -1st)
b 0
Dish Weight (2nd -1st)
Dry Weight (2nd Dry Weight + Dish
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight) -_
� ,--+
Weight - Dish Weight)
% Dry Solids ((Dry Weight/ Wet
% Dry Solids ((Dry Weight/ Wet
Weight) x 100)
(,,-, q-
Weight) x 100)
*Note -Differences should agree within 4% or 0.5 Mg, which ever is less
Revised 9/26/19 JDW

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Washington WQ Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timeltemp) ❑
I Alt B (Alk Treatment) [3
1 Alt_ C (Prior Testing) ❑
A1t.D (No Prior Test) [3Process
to Further Reduce Pathogengs ❑
If applicable to alternative erformed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ T13ermophilic El
Beta Ray❑
Gamma RayEl
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density ®
Alt. (2) Process to Si ficantly Recluse Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly- Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ JAerobic
Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the followin
monitoring
data:
Parameter
Allowable Level
in Sludge
8
Pathogen Density
Number o
Ex`ee-
Frequency
of Anal sis
Y
Sample
Type
Analytical
Tech-ni ue
a
inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 1t] tothe
6th power
per gram of
total solids
MPN
3550.3
3940
4500
MPNIg
0
Quarterly
G
SM92210E
CF[J
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternativeperformed:
Alt. I (VS reduction) ©
Alt. 2 (40-day bench)
JAIt. 3 (30-day bench) ❑
lAlt. 4 (Spec. Dz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization
JAIt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
JNo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Hope Woolard - Water Resources Superintendent Brent Collins; Director of Technical Services
Prep er Name and Title (type print) Land Applier Name and Title (if applicable)(type or print)
1 1/6/2020
Signaturi of parer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Date: 10/1 /2019
Location
El
Summary Sheet
Fecal Coliforms
MPN/g
3688.5
4192.9
4500
3550.3
3742.2
4235.3
7 3765.7
Log
3.5668
3.6225
3.6532
3.5503
3.5731
3.6269
3.5758
3940
Geometric Means/g
Total Dry Solids
Signature

A E DATE / TIME
Sampled By poj�z C1
Received By kdt/,) 10s io-l-o t q,24
Analyzed By nn J Idl4ki- !D-H�(/6,,aj
Calculated By /dQ l %G���l� /7.
Checked By
24 hr. Check 1p:-u-jrj
48 hr. Check
72 hr. Check
Temp Z3,,S, C,il
OC
4A5 OC
Sample Location _ Sludge# I
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORA4 TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Prg-evimnfivp Tpef
m"mm=.111 ENE00100
Fecal Coliform Test
MMMMMENIMINE MENIME
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength_(DS) Control V-e
Single Strength (SS) Control qa--L "'f-
EC Broth Control )"Q-
Revised 5-23-16
EMMEN NMI
MPN/g = 10 x / 9 — = if — �6 S 9 6 , )�
01 00/ x �, 99 - 00�98 —-, "Ilk

E
Sampled By
Received By
Analyzed By J 1'-L&(-�
Calculated By
Checked By
24 hr. Check 1p:Q-?(I, 174F(
1
48 hr. Check L)-,-,Aj fC*?Ab
72 hr. Check to Fjt3-�,3tk)
Temp 5")-JD 'C
Sample Location — Sludge 9 / du PY; j+A,5 Oc
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumntive Test
11111111111111111
= UITVjQI=I
pn�jj 1 M, ��I 11,11 g��111111111,j
NEW01, I EMMMMMMMI
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
WIRTUATMI 960MITM,
Fecal Coliform Test
0.00001 0.000001 0.0000001
MPN/g = 10 x
Quality Control Tubes
10 mL
Double Strength (DS) Control
>�
Single Strength (SS) Control
L
EC Broth Control
521L
Revised 5-23-16
I I I I 11, 11 �Nmg
Emm 011 1 1- - I

A
Sampled By
Received By
Analyzed By j
Calculated By
Checked By
DATE / TIME
Ac AM
/0 0-1q, /-7'5-'7
24 hr. Check 10Q-jcj,
48 hr. Check
72 hr. Check 10-q—jq,10j 3&,-)
Temp Oc
Sample Location SludLye # -�
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORAI TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumntive Test
TIM 171,
1 11 fill
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength (DS) Control 11-p SCLI . Ve
Single Strength (SS) Control Ale �ia--t;
EC Broth Control A )" j ;'C' .
Revised 5-23-16
Fecal Coliform Test
MPN/g = 10 x x

A
Sampled By POAZ re,-r�-
Received By
Analyzed By
Calculated By
Checked By
DATE / TIME
/c,6 fJ
A
24 hr. Check /0�-jcj, 0/�-9'
48 hr. Check -ICI
72 hr. Check 1p-4-)q 1, jv3,-t snij
Temp Oc
0 C
Sample Location Sludge #3
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORA4 TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
_� �
�
Q
I IIII
_
�
_ '
Q�0
OQQ�QQQlQQ�QOOOQ�Q
�
QQ
Q
� _�
mffi�, - 1 11,111
WN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength (DS) Control �LLP-SCL/ - V-?-
Sin gle Strength (SS) Control S&IJ,
EC Broth Control A 1" n—'i . qI-AC,
Revised 5-23-16
Fecal Coliform Test
MPN/g = 10 x /9 0100/ Co1�� oc�f�

Sampled By
Received By
Analyzed By J�
Calculated By
Checked By
DATE / TIME
io-j-IcT ilo4
/C I 19fiq oq
/0--In--/,, /5-cl
24 hr. Check j0:,2-j(j
48 hr. Check
72 hr. Cheek .10-4-)q 1, j o3 Z&J
Temp D'rD,0 OC
4A,5 Oc
Sample Location Sludge 9 2�
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MP1)(Aqueous)
PresUMDtive Test
---------------
t I Ii f I
Ron=
ER24 Iffl,
Um
IMI
WN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Fecal Coliform Test
TIITI I
Quality Control Tubes
Double Strength (AS) Control
10 mL
SCL"V-e
Single Strength (SS) Control
Lf. V-e—
EC Broth Control
qaj,
Revised5-23-16
MPN/g = 10 x
R/14

Sampled By
Received By
Analyzed By J j /Li F-P
Calculated By -7) g-,-,OL
Checked By
DATE / TIME
24 hr. Check
48 hr. Check
72 hr. Check 10-±A /VS , ni")
Temp OC
4A.5 Oc
Sample Location Sludge # E
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORA4 TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
T 1,
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Control Tubes
10 mL
FQuality
Double Strength (IDS) Control
Single Strength (SS) Control
EC Broth Control
Revised 5-23-16
Fecal-Coliform- Test
MPN/g = 10 x /1 9
0,0/ x 9/
I
0 - 00/�S/
own

A E
Sampled By
Received By
Analyzed By
Calculated By FOQr
Checked By
24 hr. Check 1j):g-jq, 94q
1
48 hr. Check j&-,--jCj 1, jot�2
72 hr. Check 1p-q—IT Ic"; C,,1,-P3L-)
Temp OC
4AOc
Sample Location Sludge
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
PresUMDtive Test
on
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
W-371"TIUKA07,71 M11, I
Quality Control Tubes
Double Strength (AS) Control
10 mL
. L-e
. . ... . ...... ... ......
Single Strength (SS) Control
.. .. .. .. ...
,-P—
EC Broth Control
Revised 5-23-16
Fecal-Coliform Test
MPN/g = 10 x 2 3,--
cc)/x

Sampled By
Received By
Analyzed By J) 1
Calculated By 4
Checked By
DATE / TIME
9-i-le! , c) nq
24 hr. Check
48 hr. Check
72 hr. Check 10-4-)�
Temp 9 6-, 0 OC
4A,5 Oc
Sample Location Sludge # 7
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORA4 TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Preumntive. Te..Qt
0.0000001
PRIM
ZII,�o 'I I I �
ITIVITI., �.=M
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterility Control
Quality Control Tubes 10 mL
Double Strength (DS) Control I4,
V LL
Single Strength (SS) Control ,,-
EC Broth Control A
Revised 5-23-16
Fecal Coliform Test
MPN/g = 10 x
0100/1;� 0 C) ytz

CITY OF WHSHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Time
Sampled By
Received By
Analyzed By
Calculated By
Checked By
Time on water bath
Time in oven
Time out of oven
Time weighed
1st
2nd
eart_,3z�
�
Cl
11
Sample #
SL-
Evaporating Dish #
q
Sample #
�SU#-
Evaporating Dish #
Wet Weight + Dish Weight
t ` 1_13il
Wet Weight + Dish Weight
13k S?S .11
Dish Weight
(.,-,j
Dish Weight
D-1 � e
Wet Weight
'
Wet Weight
�.
1 st Dry Weight + Dish Weight
,
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weighty
-
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd - 1st)
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd - 1st)
,
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
_
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
_ a
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
,, /'
LA ,�'�
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
"Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WHSHINGTON
SLUDGE
Standard Methods 2540 G-2011(Aqueous)
Name Date/Time
Sampled By
Received By
Analyzed By
Calculated By
Checked By
Time on water bath
Time in oven
Time out of oven
Time weighed
1st
2nd
aQD'
c>ci a
t 1
Sample #
d= NCt A `
Evaporating Dish #
a
`
Sample #
S . �
Evaporating Dish #
Y� 1
Wet Weight + Dish Weight
Wet Weight + Dish Weight
1 ` f
Dish Weight
'D u� •
Dish Weight
ci l 00 • �,
Wet Weight
Wet Weight
14
1 st Dry Weight + Dish Weight
5.,u 1
1 st Dry Weight + Dish Weight
, 3
2nd Dry Weight + Dish Weight
�. •' 7--Q,'a149
2nd Dry Weight + Dish Weight
o
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
e1
F
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1 st)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
LA
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*(dote -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9126/19 JDW

CITY OF VVHSHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
me
NAL
Date/Time
✓✓JJ /�
Sampled By
/
Received By
r, UC�i'r'`14�
Time on water bath
Analyzed By
" , . ,
u',
u t Time in oven
Calculated By
Time out of oven
Checked By
ea&� mkk:.
/ i
L 3 Time weighed
Sample #
Sems# S
Evaporating Dish #
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
l JCS ,
Wet Weight + Dish Weight
Dish Weight
Dish Weight
Wet Weight
C) d 9,9,5
Wet Weight
1st Dry Weight + Dish Weight
?
1st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight,
m
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Q
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wets
Weight) x 100)�
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9126/19 JDW

CITY OF VVHSI-IINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
rl-4-- /T;.,-, -
Sampled By
Received By
Analyzed By
Calculated By
Checked By
Time on water bath
Time in oven
Time out of oven
Time weighed
Sample #
���'
Evaporating Dish #
:� er
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
l9qaXAC,
Wet Weight + Dish Weight
Dish Weight.
Dish Weight
Wet Weight
'jl
Wet Weight
1 st Dry Weight + Dish Weight
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
—] (
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd - 1st)
a
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd -1st)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
�� r.,
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
"Dote -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WHSNINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Time
Sampled By
Received By
Analyzed By
Calculated By
Checked By
Time on water bath
Time in oven
Time out of oven
Time weighed
1 st
2nd
'33 G i
�Ci a -
Sample #
Evaporating Dish #
1�
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
.cs
Wet Weight + Dish Weight
Dish Weight
r .
Dish Weight
Wet Weight_.
Wet Weight
1 st Dry Weight + Dish Weight
S _b
1 st Dry Weight + Dish Weight
2nd Dry Weight+ Dish Weight
�c"�+`� ° 1
2nd Dry Weight+ Dish Weight
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd - 1st)
')
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
_
3k a
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
� Y,
, /
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*Mote -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9126119 JDW

CITY OF WtASHINGTON
SLUDGE
Standard Methods 25.40 G-201 1 (Aqueous)
Name Date/Time
Sampled By�(���'
Received By Time on water bath
Analyzed By 3"1�= Time in oven
Calculated By 1vC6 Time out of oven
Checked By / k a ` Time weighed
Sample #
Evaporating Dish #
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
vCa"01�1,9
Wet Weight + Dish Weight
Dish Weight
Dish Weight
Wet Weight
��j?�� ,
Wet Weight
1 st Dry Weight + Dish Weight
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
C6 1P`12, 1 -1.
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd - 1st)
Difference in 1st & 2nd Dry Weight+
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
Dry Weight (2nd Dry Weight+ Dish
Weight - Dish Weight)
% Dry Solids ((Dry weight/ Wet
Weight) x 100)
__ . Y
r F�ll�.�) ®
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
"Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF "..,)'HINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Name Date/Time
010,3 jDLj
Sampled By
Received By rL' g c Time on water bath
Analyzed By 1,� �, �� Time in oven
Calculated By r 1 L Time out of oven
Checked By /oP Time weighed
Sample #
SL;7
Evaporating Dish #
y
Sample #
Evaporating Dish #
t L4-1 _?
Wet Weight + Dish Weight
9
Wet Weight + Dish Weight
.—i �'A '23, o
Dish Weight
Dish Weight
Wet Weight
5r1;;1 t+-4,9
Wet Weight
1 st Dry Weight + Dish Weight
147 S
1 st Dry Weight + Dish Weight
2nd Dry Weight+ Dish Weight
jLf-75Z-1.9
2nd Dry Weight+ Dish Weight
Difference in 1st & 2nd Dry Weight +
CD
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight + Dish
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
�, u
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
9,
""� y
Weight) x 100)
*Dote -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY19-SL033302
CU)-Toeg
Predictive
Client:
Harvey Williamson
Advisor:
Brent Collins
�C'
Hunters Roost Farm Septic Service
EMA Resources Inc
Soi I Report
Mehlich-3 Extraction
5365 US Hwy 17 N
755 Yadkinville Rd
b
Washington, NC 27889
Mocksville, NC 27028
Fob a7-
Links to Helpful Information
Sampled: Not Provided
Sampled County : Beaufort
Received: 06/04/2019
Farm: BF210
Completed: 06/13/2019
Client ID: 282102
Advisor ID: 405413
Sample ID: 00001
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn Zn
Cu B
Information
Lime History:
1-Soybean
1.0 0 0
80 0 0
0 0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dnfl:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH
P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.76 1.24
4.3 58 1.8 5.3
229 31 41 14
43 52 41
93 93
89 0.1 2
North Carolina
x
AL
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SL011357
Client:
Harvey/Scott Williamson
Advisor:
Brent Collins
vo-
Predictive
1774 Wharton Station Rd
EMA Resources Inc
Washington, NC 27889
755 Yadkinville Rd
.'..,$'
Soil Report Mehlich-3 Extraction
Mocksville, NC27028
Sampled County : Beaufort
Links to Helpful Information
Client ID: 407660
Advisor
ID: 405413
Sampled:
Received: 10/23/2019 Completed: 11/01/2019 Farm: BF210
Sample ID: 12
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG) 0.0 80-100 0
0
0 0 0
0
0
0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.86 1.08
8.6 93 0.6 6.5 124 178 59 24
35
62
40 150
150
139
0.1 1
Sample ID: 14
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG) 0.0 80-100 0
0
0 0 0
0
0
0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.56 1.03
10.4 88 1.2 6.0 214 156 59 21
39
91
64 405
405
281
0.1 1
Sample ID: 15
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG) 0.0 80-100 0
0
0 0 0
0
0
0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V
CEC BS% Ac pH P-1 K-I Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.86 1.07
7.7 87 1.0 6.0 150 108 60 21
34
72
53 271
271
287
0.1 1
North Carolina
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY20-SL011357
Harvey/Scott Williamson
Page 2 of 3
Sample ID: 13
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Small Grain (SG) 0.0
80-100 0
0
0
0
0
0
0 0
Note: 3
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.51 1.06 9.6
90 1.0 6.2 208 110
65 19
39
109
73
391
391
391 0.1
1
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Small Grain (SG) 0.4
80-100 60
60
0
0
10
6
2 0
Note: 3
2- 0.0
0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.97 1.16 6.8
83 1.2 5.7 32 39
49 32
60
12
17
23
23
20 0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY19-SL030863
CU)-ToegPredictive
Client:
Harvey Williamson
Advisor:
Brent Collins
�C'
Hunters Roost Farm Septic Service
EMA Resources Inc
Soi I Report
Mehlich-3 Extraction
5365 US Hwy 17 N
755 Yadkinville Rd
b
Washington, NC 27889
Mocksville, NC 27028
Fob a7- Links to Helpful Information
Sampled: Not Provided
Sampled County : Beaufort
Received: 04/26/2019
Farm: BF210
Completed: 05/08/2019
Client ID: 282102
Advisor ID: 405413
Sample ID: 00006
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.4 0 0
20 0 0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dn73]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
2.44 1.02 8.8 80 1.7 5.8
161 68 58 18
38 43 36
110
110
116 0.1 1
Sample ID: 00007
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.6 0 0
20 0 0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
2.29 1.08 6.2 74 1.6 5.6
226 67 54 15
40 41 35
115
115
100 0.1 2
Sample ID: 00008
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
1.4 0 0
40 0 0
0
0
0 0
Note: 3
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dnfl:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
2.60 1.01 6.9 64 2.5 5.2
181 49 44 16
48 33 30
129
129
90 0.1 1
North Carolina
x
AL
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY19-SL030863
Harvey Williamson
Page 2 of 3
Sample ID: 00016
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5 K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1-Soybean 0.0
0 0 40
0 0
0 0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg% S-1 Mn-I
Mn-All Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS -I NO3-N
0.92 1.01 7.2 90 0.7 6.4 108 48
67 19 30 51
35
110 110
112 0.1 1

Nutrien Ag Solutions, Inc.
■
NC (271)
J :_lumen
INVOICE
X 6Z8
PO BO 628
Pa BOX
VANCEBORO, NC 28586
Ag Solutions
252-244-1490
Invoice #:
40817802
Invoice Date:
11/11/19
Due Date:
01/10/20
Delivery Date:
11/11/19
CITY OF WASHINC3TON (1624435)
Order #:
156936992ND
P O BOX
pO#:
Hunters Roast
102 EAST STREET
Sales Rep:
SPAIN, Randy
WASHINGTON, NC 27889
Ship Via: Customer Vehicle County: CRAVEN
Gross Unit
Gross ExVd
Product # Product Description
Quantity
Price
Sales Tax Price
1000184035 - LIME HYDRATED 50LB
.6000 TN
S60.0000
336.00
1200.0000 LB
1000189836 - TONNAGE TAX
1.0000 EA
0.3000
0.30
Safety Data Sheets are available upon request for applicable products. Contact your local branch for details. For a medical emergency
Involving this product, call 1-866-944-8565. For help with any spill, leak, fire or exposure, call Chemtrec at 1-800-424-9300.
*** Invoice Notes ***
per Harvey Williamson
Payment in full is due and payable on the 101h of the month following the slalentenI dale; for invoice ainouMs not paid by the 251h of the month following the statement dale, customer shall
also be liable Far a late fee equal to four perePill i4%1 of the unpaid amount far purchases in North Carolina and Mississippi and rive percent 15%y in ocher states; (iIi) for invoice amuunts not
paid by the 25th of the month following the slalemem date, yua shall also be liable for interest accrued an the unpaid balance al the highest rate allowable by law. In the event of any conflict
between the terms of the invoice and the C:usivaner Profile, the terms a Lit invoice shall contral.
Additional Ipayment Terms: DUE IOTH OF SECOND MONTH Invoice Sub Total:
336.30
Sales Tax:
0.00
Invoice Total:
336.30
Less Prepay Used:
0.00
Less Prepay Discount:
0.00
Gross Invoice Total:
336.30
Amount Due:
336,30
Remit To.
Nutrien Ag Solutions, Inc.
1 of 1 PO 80X 628
VANCE60RO, NC 285136

Nutrien Ag Solutions, Inc.
•
VANCEBORO NC (271)
`.�� M ■
rtrien
INVOICrz
PO BOX 628
•rJ
VANCEBORO, NC 28586
Ag Solutions-
252-244-1490
Invoice #:
40817979
Invoice Mate:
11/11/19
VANCEBORO (Dry Only)
Due date:
01/10/20
Delivery Date:
11/11/19
CITY OF WASHINGTON (1624435)
Order It:
15693804
P O BOX 1988
PO#:
Hunters Roost
102 EAST 2ND STREET
Sales Rep:
SPAIN, Randy
WASHINGTON, NC 27889
Ship Via: Company Vehicle County: BEAUFORT
Gross unit
GrossExt`d
Product # Product Description
Quantity
Price
Sales Tax Price
1000180759 - DOLOMITE BULK
53.9500 TN
48.0000
2,589.60
107900.0000 LB
1000189836 - TONNAGE TAX
1.0000 EA
26.9750
26.98
1000000078 - APPLICATION CHARGES /TON
53.9500 TN
14.0000
755.30
Safety Data Sheets are available upon request for applicable products. Contact your focal branch for details. For a medical emergency
involving this product, call 1-866.944-8565. For help with any spill, leak, fire or exposure, call Chemtrec at 1-800-424-9300.
*** Invoice Notes***
per Harvey Williamson
wt tickets 13324 13325 13326
SSG
1500 lb p/a
AS t ' ov,
Payment in Full N due and payable on the 10th of the month following the statement dale; for invoice amounts not paid by the 25111 of the month following the statement date, customershall
also be liable for a late fee equal to four percent (4 J) of the unpaid amount for purchases in North C'nrnlinn and hi i ssi ssi pp and five percent [5 % ) is other states; (iii) for invoice amounts not
ltald by the 15th of lbe month following the statement date, you shall also Fie liable for interest Accrued an the unpaid balance at the highest rate allowable by law. In the event of any conflict
between the terms of the invoice and the Customer Prufde, the terms of the invoice shall control.
Additional Information ' Payment Terms: DUE LOTH OF 5ECON❑ MONTH Invoice Sub Total:
3,371.88
Sales Tax:
MO
Invoice Total;
3,371.88
Less Prepay Used:
0.00
Less Prepay Discount:
0.00
Gross Invoice Total:
3,371.88
Amount Due:
3,371.88
Remit To:
Nutrien Aq Solutions, Inc.
1 of i PO BOX 628
VANCEBORO, NC 28586

I& a
iklutrien
Ag Solutions-
P.O. Box 628
Vanceboro, NC 28586
bill Tn
Harvey Williamson
Date 511012019
IShip 7o
Harvey Williamson
Quantity
Description
Price Each
Amount
57.92 tons
Bulk Lime
,$50.09
$2,896.00
57.92 tons
lime tax
$0.55
$31.86
57.92 tons
Spread fee
$12.00
$695.04
►��1'�►"lE'17
Total ,$3,622.90
Sututions

Nutrien Ag Solutions, Inc.
NC [2]1}
J ien
INVOICE
PO BOX 628
PO BOX 628
.lutr
VANCESORO, NC 28586
Ag Solutions
252-244-1490
Invoice #:
40817757
Invoice Date: 11/11119
Due Date:
01/10/20
Delivery Date: 10/02/19
CITY OF WASHINGTON (1624435)
Order #:
15506378
P O Box 1988
PO#:
Hunters Roost
102 EAST 2ND STREET
Sales Rep:
SPAIN, Randy
WASHINGTON, NC 27889
Ship Via: Company Vehicle Coun : BEAUFORT
Gross Unit
Gross Ext`d
Product # Product DescripUon
Quantity
Price
Sales Tax Price
1000184035 - LIME HYDRATED 50LB
1,1250 TN
560.0000
630.00
2250,0000 LB
1000189836 - TONNAGE TAX
1.0000 EA
0,5625
0.56
Safety Data Sheets are available upon request for applicable products, Contact your local branch far details. Far a medical emergency
involving this product, call I-866-944.8565, For help with any spill, leak, fire or exposure, call Chemtrec at 1-800-424-9300.
* * * Invoice Notes
delivered to sewer plant per Harvey Williamson
Payment in full is due and pnyable on the loth of the month following the slllemeni date; for invoice amenats not paid by the 25th of the month following the siatement dale, ru0nmer shall
also he liable for t late fee equal to four percent (d%) of the unpaid amount fur purchases in North Carolina aad NIississippi And rive percent (S I ) in otlicrsIales: (iii) for invoica amonots nor
paid by she 25th of the month fallowing the statement date, you shall also be Whir fur interest accrued on the unpaid bnlance at the highest rate allowable by Imr. In the event of any ruaflict
between the terms of the invoice itnd the Customer Pro rile, the terms of the invoice shall control.
Additional Information Payment Terms: DUE 10TH OF SECOND MONTH Invoice Sub Total:
630.56
Sales Tax:
0.00
Invoice Total:
630.56
Less Prepay Used:
0.00
Less Prepay Discount:
0.00
Gross Invoice Total:
630.56
Amount Due:
630.56
Remit To:
Nutrien Ag Solutions, Inc.
1 of 1 PO BOX 628
VANCEBORO, NC 219586

Nutrien Ag Solutions, Inc.
■
VANCEBORO NC (271)
a; al��l 1�r
INVOICE
PO sox 628
■
VANCEBQRO, NC 28586
Ag Solutions
252-244-1490
Invoice #:
40817781
Invoice Date:
11/11/19
Due Date:
01/10/20
Delivery Date:
10/03/19
CITY OF WA5HINGTON {1624435}
Order #:
15512142pQ#:
P O B
Hunters Roost
102 EAST 2N p STREET
Sales Rep:.
SPAIN, Randy
WASHINGTON, NC 27889
Ship Via; Company Vehicle Coun : BEAUFORT
Gross Unit
Gross W'd
Product # Product Description
Quantity
Price
Sales Tax Price
1000184035 - LIME HYDRATED 50LB
1.1250 TN
560.0000
630.00
2250.0000 LB
1000189836 - TONNAGE TAX
1.0000 EA
0.5625
0.56
Safety Data Sheets are available upon request for applicable products. Contact your local branch for details. For a medical emergency
involving this product, call 1-866-944-8565. For help with any spill, leak, fire or exposure, call Chemtrec at 1-800-424-9300.
*** Invoice Notes ***
delivered to sewer plant per Harvey Williamson
Va} mint in full is tiue anti payable on the IOth of the month following the s fiicvrneu I dale; for invoice amounts not paid by thr 25th of the month folloiving the ssatemenl date, customer shalt
also he liable for late fee equal to four percent (1 / ) of the unpaid amount for Purchases in North Carolina and Mississippi nod file percent (5 % ) in other states; (iii) for invoice amounts not
paid by the 25th of the month following [he slalentent date, you Antl also be liable far itrleresI acertied nn the unpaid ha Fence at the highest rate allowable by law. is the event or any conilirr
henveen site terms of the invoice and the Caatomer Promr, Ote terms of IN lnvolce shall control.
Additional Infvnmation Payment Terms: DUE 10TH OF 5ECDN❑ MONTH Invoice Sub Total:
630.56
w� Sales Tax:
0.00
Invoice Total:
630.56
Less Prepay Used:
0.00
Less Prepay Discount;
0.00
Gross Invoice Total:
630.56
Amount Due:
630.56
Remit To:
Nutrien Ag Solutlens, Inc.
1 of 1 PO BOX 628
VANCESORO, NC 28586