WQ0014868_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:*
Project Number* WQ0014868
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0014868
Applicant\Permittee * Smithfield Fresh Meats Corp
Facility Name * Smithfield Fresh Meats Corp
Phone Number*
336-751-1441
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Smithfield Fresh Meats Annual Report -
7.34MB
WQ0014868. pdf
upload only 1 RJF docurrent. Miltiple docurrents rust be corrbined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/24/2020

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014868 County: Bladen Year:
Facility Name (as shown on permit):
Land Application Operator:
Smithfield Fresh Meats Corp.
EMA Resources Inc_
2019
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
© Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application. fields in the ennit:
37
Total number of fields utilized for land application during the year:
10
Total amount of dry tons applied during the year for all application sites:
355.02
Total number of acres utilizes for land application during the year:
162.7
Part B - Annual Com iance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. © Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T A 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T . l I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations." >
Donovan Owens - General Manager 1.0/� A
Pe y ee Name and Title a or print) Signature of Permittee Date
Z!:f-e 1f5/2020
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T
Signature of Land Applier Date
(if different from Permittee and Preparer)
1102 (26) DENR FORM ACF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0014868
Facility Name: Smithfield Fresh Meats Corp.
Residual Source WQ # or NCO078344
NPDES#:
WWTP Name: Tarheel Plant WWTP
Dao:.l..ol Anolvaia Poto
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
to a
Sam le or Composite Date
North
6/3/19
South
6/3/19
North
6/19/19
South
6/19/19
Average
Percent Solids (%)
NA
3.35
2.23
3.52
3.89
3.25
Arsenic
75
12.7
19
12
10.7
13.6
Cadmium
85
1.5
2.25
1.41
1.27
1.61
Copper
4,300
294
1140
446
213
523.25
Chromium
NA
9.39
60
25.9
16.2
27.87
Lead
840
4.52
6.77
4.69
3.82
4.95
Mercury
57
0.102
0.143
0.096
0.0856
0.11
Molybdenum
75
3.94
12.1
8.4
6.05
7.623
Nickel
420
11.2
32
23.7
17.5
21.1
Selenium
100
14.8
22.3
14.0
12.6
15.93
Zinc
7,500
542
1960
1030
477
1002.3
Total Phosphorus
NA
4030
6590
6260
3150
5007.5
TKN
NA
71200
67700
40000
74100
63250
Ammonia -Nitrogen
NA
15000
21700
6510
5970
12295
Nitrate and Nitrite
NA
14$
220
143
128
159.75
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penal for submittialse information, including the possibility of fines and imprisonment for knowing violations."
Signature of
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
�- �U
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0014868
Facility Name: Smithfield Fresh Meats Corp.
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
NCO078344
Tarheel Plant W WTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Sate le or C mposite Date
North
6/3/19
South
6/3/19
North
6/19/19
South
6/19/19
Average
Aluminum
1480
5910
4430
2030
3462.5
Calcium
3730
12200
45100
34600
23907.5
M2knesium
903
3140
1830
1050
1 1730.75
H
7.2
7.5
11.8
12.1
9.65
Potassium
4300
5860
3030
2740
3982.5
Sodium
17200
30200
9430
8870
16425
PAN
18888
20270
10096
16739
16498.3
SAR
11.96
9.39
2.22
2.52
6.52
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are
signific�t penalties for sto�mitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
21.6 Acres Permitted: 21.6 Site #: SF03 Field #:
47.56
LaB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.20
Arsenic
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.093
Chromiuni
0.123
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.123
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
denum
Nickel
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.414
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.414
Total
Phos-
22.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
22.053
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 1 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 47.56 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 147
LaB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.6
21.6
0
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/27
45500
3.25
0.285
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
9.420
NA
Bermuda
6/28
273000
3.25
1.713
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
56.519
NA
Bermuda
6/29
32500
3.25
0.204
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
6.728
NA
Bermuda
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
35t000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
72.668
0.000
Lime Applied
Annuallbs/acre
0.060
0.007
2.093
0.123
0.022
0.000
0.034
0.093
0.070
4.414 22.053
163.314
167.728
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.183
0.084
38.475
2.17
0.596
0.021
1.184
3.486
0.257
Current Cumulative lbs/ac
0.243
0.091
40.568
2.293
0.618
0.021
1.218
3.579
0.327
Permitted C. P. L. R.****1
1 9
1 250
1000
1
250
Permit PAN Limit 1 st/2nd Crop
1
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
13.3 Acres Permitted:
13.3 Site #: SF03 Field #:
29.07
8.6
Cc
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.19
Arsenic
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.078
Chromiuni
0.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
denum
Nickel
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.382
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.382
Total
Phos-
21.893
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.893
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 2 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 29.07 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 168
Ce
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
13.3
13.3
8.6
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/17
188500
3.25
1.921
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
63.379
NA
Bermuda
6/18
26000
3.25
0.265
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
8.742
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
0
214500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
72.121
0.000
Lime Applied
Annuallbs/acre
0.059 0.007 2.078 0.122 0.022 0.000 0.033 0.092 0.070 4.382 21.893
0.19 0.072 43.316 1.85 0.688 0.021 1.11 3.905 0.243 164.855
0.249 0.079 45.394 1.972 0.710 0.021 1.143 3.997 0.313 169.237
1 9 1 250 1000 1 250 500
1 168
Date
lbs/ac
Prior Years Cumulative lbs/ac
10/2
2000
Current Cumulative lbs/ac
Permitted C. P. L. R.****1
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
21.3 Acres Permitted: 21.3 Site #: SF03 Field #:
46.69
5.7
Cc
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.19
Arsenic
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.084
Chromiuni
0.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
denum
Nickel
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.394
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.394
Total
Phos-
21.953
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.953
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 3 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 46.69 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 168
Ce
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.3
21.3
5.7
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/7
71500
3.25
0.455
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
15.011
NA
Bermuda
6/8
117000
3.25
0.744
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
24.564
NA
Bermuda
6/18
156000
3.25
0.993
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
32.752
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
344500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
72.326
0.000
Lime Applied
Annuallbs/acre
0.060
0.007
2.084
0.122
0.022
0.000
0.033
0.093
0.070
4.394 21.953
134.707
139.101
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.158
0.081
35.853
1.405
0.528
0.017
0.89
3.007
0.199
10/2
2000
Current Cumulative lbs/ac
0.218
0.088
37.937
1.527
0.550
0.017
0.923
3.100
0.269
Permitted C. P. L. R.****
9
250
1000
250
Permit PAN Limit 1 st/2nd Crop
1 168
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
Acres Permitted:
Site #: SF03 Field #:
16.74
LaB
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.09
Arsenic
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
1.989
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.989
Chromiuni
0.117
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.117
Lead
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.032
denum
Nickel
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.088
Selenium
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Zinc
4.193
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.193
Total
Phos-
20.951
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
20.951
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 5 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 16.74 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 147
LaB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
8
8
0
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/18
39000
3.25
0.661
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
21.800
NA
Bermuda
6/19
84500
3.25
1.431
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
47.234
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
o
t235oo
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
69.034
0.000
Lime Applied
Annuallbs/acre
0.057
0.007
1.989
0.117
0.021
0.000
0.032
0.088
0.067
4.193 20.951
99.002
103.195
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.115
0.062
25.359
1.185
0.326
0.013
0.655
2.099
0.156
Current Cumulative lbs/ac
0.172
0.069
27.348
1.302
0.347
0.013
0.687
2.187
0.223
Permitted C. P. L. R.****1
1 9
1 250
1000
1
250
Permit PAN Limit 1 st/2nd Crop
1
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
16.5 Acres Permitted:
16.5 Site #: SF03 Field #:
36.12
4.9
LaB
6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.19
Arsenic
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.081
Chromiuni
0.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
denum
Nickel
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.388
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.388
Total
Phos-
21.923
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.923
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 6 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 36.12 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 147
LaB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
16.5
16.5
4.9
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/6
130000
3.25
1.068
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
35.233
NA
Bermuda
6/7
136500
3.25
1.121
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
36.994
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
0
266soo
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
72.227
0.000
Lime Applied
Annuallbs/acre
0.060 0.007 2.081 0.122 0.022 0.000 0.033 0.092 0.070 4.388 21.923
0.138 0.068 23.269 1.204 0.427 0.015 0.874 2.609 0.186 119.414
0.198 0.075 25.350 1.326 0.449 0.015 0.907 2.701 0.256 123.802
1 9 1 250 1000 1 250 500
1 1 147
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****1
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
47.57
13.5
Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: AaA
Acres Used: 21.8 Acres Permitted: 21.8 Site #: SF07 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.18
Arsenic
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.074
Chromiuni
0.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
denum
Nickel
0.092
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.374
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.374
Total
Phos-
21.853
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.853
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz G;-
Signature of Land Applier
1/5/2020
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 1 Acres Utilized:
JW Burney Annual Dry Tons Applied: 47.57 Site #: SF07 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 207
AaA
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.8
21.8
13.5
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/19
91000
3.25
0.566
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
18.667
NA
Bermuda
6/20
130000
3.25
0.808
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
26.667
NA
Bermuda
6/21
130000
3.25
0.808
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
26.667
NA
lBermuda
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
35t000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
72.001
0.000
Lime Applied
Annuallbs/acre
0.059
0.007
2.074
0.122
0.022
0.000
0.033
0.092
0.070
4.374 21.853
298.242
302.616
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.165
0.233
99.128
1.277
1.297
0.02
1.097
2.511
0.264
Current Cumulative lbs/ac
0.224
0.240
101.202
1.399
1.319
0.020
1.130
2.603
0.334
Permitted C. P. L. R.****1
1 9
1 250
1000
1
250
Permit PAN Limit 1 st/2nd Crop
1
207
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
42.29
Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: WmB
Acres Used: 19.3 Acres Permitted: 19.3 Site #: SF07 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.19
Arsenic
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.083
Chromiuni
0.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
denum
Nickel
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.392
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.392
Total
Phos-
21.943
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.943
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 6 Acres Utilized:
JW Burney Annual Dry Tons Applied: 42.29 Site #: SF07 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 210
WniB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
19.3
19.3
0
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/22
123500
3.25
0.867
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
28.615
NA
Bermuda
6/23
32500
3.25
0.228
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
7.530
NA
Bermuda
6/24
149500
3.25
1.050
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
34.639
NA
Bermuda
6/25
6500
3.25
0.046
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
1.506
NA
Bermuda
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
3t2000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
72.291T
0.000
Lime Applied
Annuallbs/acre
0.060
0.007
2.083
0.122
0.022
0.000
0.033
0.092
0.070
4.392 21.943
379.147
383.539
1 500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.261
0.251
110.304
6.398
1.831
0.029
1.677
14.998
0.356
10/2
2000
Current Cumulative lbs/ac
0.321
0.258
112.387
6.520
1.853
0.029
1.710
15.090
0.426
Permitted C. P. L. R.****1
1 9
1 250
1
1 1000
1
1
1 250
1
Permit PAN Limit 1 st/2nd Crop
1
1 210
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
26.43
12.7
Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: AaA
Acres Used: 12.1 Acres Permitted: 12.1 Site #: SF07 Field #: 8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.18
Arsenic
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.076
Chromiuni
0.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
denum
Nickel
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.092
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.378
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.378
Total
Phos-
21.873
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.873
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 8 Acres Utilized:
JW Burney Annual Dry Tons Applied: 26.43 Site #: SF07 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 207
AaA
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
12.1
12.1
12.7
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/27
162500
3.25
1.820
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
60.056
NA
Bermuda
6/28
32500
3.25
0.364
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
12.011
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
o
t95000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
72.067
0.000
Lime Applied
Annuallbs/acre
0.059
0.007
2.076
0.122
0.022
0.000
0.033
0.092
0.070
4.378 21.873
131.867
136.245
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.156
0.069
31.774
4.36
0.713
0.018
0.994
2.841
0.231
10/2
2000
Current Cumulative lbs/ac
0.215
0.076
33.850
4.482
0.735
0.018
1.027
2.933
0.301
Permitted C. P. L. R.****1
1 9
1 250
1000
1
250
Permit PAN Limit 1 st/2nd Crop
1
207
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
46.69
4.7
Operator: Richard Dunham Owner: JW Burney Predominant Soil Series: WmB
Acres Used: 21.3 Acres Permitted: 21.3 Site #: SF07 Field #: 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.19
Arsenic
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.084
Chromiuni
0.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
denum
Nickel
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
4.394
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.394
Total
Phos-
21.953
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.953
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/5/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 9 Acres Utilized:
JW Burney Annual Dry Tons Applied: 46.69 Site #: SF07 Acres Permitted:
Richard Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 210
WniB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.3
21.3
4.7
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/20
58500
3.25
0.372
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
12.282
NA
Bermuda
6/21
6500
3.25
0.041
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
1.365
NA
Bermuda
6/25
110500
3.25
0.703
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
23.199
NA
Bermuda
6/26
169000
3.25
1.075
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
35.481
NA
Bermuda
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
344500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
72326T
0.000
Lime Applied
Annuallbs/acre
0.060
0.007
2.084
0.122
0.022
0.000
0.033
0.093
0.070
4.394 21.953
147.707
152.101
1 500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.175
0.101
32.239
3.907
0.757
0.018
1.038
3.214
0.22
10/2
2000
Current Cumulative lbs/ac
0.235
0.108
34.323
4.029
0.779
0.018
1.071
3.307
0.290
Permitted C. P. L. R.****1
1 9
1 250
1
1 1000
1
1
1 250
1
Permit PAN Limit 1 st/2nd Crop
1
1 210
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
15.86
Operator: Steve Dunham Owner: JW Burney Predominant Soil Series: LaB
Acres Used: 7.5 Acres Permitted: 7.5 Site #: SF07 Field #: 14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.11
Arsenic
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
2.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.010
Chromiuni
0.118
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
Lead
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.032
denum
Nickel
0.089
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Selenium
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Zinc
4.238
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.238
Total
Phos-
21.172
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.172
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz G;-
Signature of Land Applier
1/5/2020
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 14 Acres Utilized:
JW Burney Annual Dry Tons Applied: 15.86 Site #: SF07 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 147
LaB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
7.5
7.5
0
o
Volume applied
(enter one) Solids/
Liquid
q
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
p
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/27
117000
3.25
2.114
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
63250
12295
159.75
69.761
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
o
n7000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
69.761
0.000
Lime Applied
Annuallbs/acre
0.058
0.007
2.010
0.118
0.021
0.000
0.032
0.089
0.067
4.238 21.172
146.236
150.474
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.159
0.075
39.493
2.521
0.663
0.019
1.037
3.167
0.234
Current Cumulative lbs/ac
0.217
0.082
41.503
2.639
0.684
0.019
1.069
3.256
0.301
Permitted C. P. L. R.****1
1 9
1 250
1000
1
250
Permit PAN Limit 1 st/2nd Crop
1
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/5/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
6/ 13/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-155-0242
Client Project Description: Smithfield
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 6/4/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield
Lab Report Number: 19-155-0242
Date: 6/13/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L440367
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L440224
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L440367
MS/MSD Recovery failed, DT confirmed matrix interference
Analyte: Potassium
QC Batch No: L440367
MS/MSD Recovery failed, PDS confirmed matrix interference
Analyte: Phosphorus
QC Batch No: L440224
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Analyte: Mercury
QC Batch No: L440259
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 8

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Smithfield Report Date : 06/13/2019
755 Yadkinville Rd Information : Received : 06/04/2019
Mocksville , NC 27028
Report Number : 19-155-0242 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 89111
Matrix: Solids
Sample ID : North Basin
Sampled:
6/3/2019
7:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
96.7
%
0.010
1
06/04/19 15:25
ADM
SW-DRYWT
Ammonia Nitrogen
15000
mg/Kg -
dry
758
1
06/12/19 11:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<148
mg/Kg -
dry
148
148
1
06/13/19 12:18
ZBD
4500NO3F-2011
Organic N
56400
mg/Kg -
dry
30.3
1520
1
06/05/19 14:55
CALCULATION
pH
7.2
S.U.
1
06/11/19 05:53
JSL
9045D
Total Solids
3.35
%
0.010
0.010
1
06/04/19 15:25
ADM
2540G-2011
Total Volatile Solids
81.6
%
0.010
0.010
1
06/04/19 15:25
ADM
2540G-2011
Total Kjeldahl Nitrogen
71200
mg/Kg -
dry
1520
1
06/05/19 14:55
CLP 4500NORGD-2011
Phosphorus
4030
mg/Kg -
dry
77.9
152
1
06/11/19 17:10
JTR
6010D
Aluminum
1480
mg/Kg -
dry
61.5
152
1
06/13/19 12:52
KKM
6010D
Arsenic
<12.7
mg/Kg -
dry
12.7
15.2
1
06/11/19 17:10
JTR
6010D
Cadmium
<1.50
mg/Kg -
dry
1.50
3.03
1
06/11/19 17:10
JTR
6010D
Calcium
3730
mg/Kg -
dry
509
758
1
06/11/19 17:10
JTR
6010D
Chromium
9.39
mg/Kg -
dry
5.76
7.58
1
06/11/19 17:10
JTR
6010D
Copper
294
mg/Kg -
dry
4.39
7.58
1
06/11/19 17:10
JTR
6010D
Iron
2550
mg/Kg -
dry
128
152
1
06/11/19 17:10
JTR
6010D
Lead
<4.52
mg/Kg -
dry
4.52
9.09
1
06/11/19 17:10
JTR
6010D
Magnesium
903
mg/Kg -
dry
67.3
152
1
06/11/19 17:10
JTR
6010D
Manganese
62.4
mg/Kg -
dry
5.55
15.2
1
06/11/19 17:10
JTR
6010D
Mercury
<0.102
mg/Kg -
dry
0.102
0.461
1
06/11/19 12:06
TJS
7471A
Molybdenum
<3.94
mg/Kg -
dry
3.94
7.58
1
06/11/19 17:10
JTR
6010D
Nickel
11.2
mg/Kg -
dry
5.00
7.58
1
06/11/19 17:10
JTR
6010D
Potassium
4300
mg/Kg -
dry
90.3
152
1
06/11/19 17:10
JTR
6010D
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 3 of 8

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-155-0242
Lab No : 89111
Sample ID : North Basin
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield
Information :
REPORT OFANALYSIS
Report Date : 06/13/2019
Received : 06/04/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 6/3/2019 7:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<14.8
mg/Kg -
dry
14.8
15.2
1
06/11/19 17:10
JTR
6010D
Sodium
17200
mg/Kg -
dry
234
758
1
06/12/19 17:51
KKM
6010D
Zinc
542
mg/Kg -
dry
32.7
37.9
1
06/11/19 17:10
JTR
6010D
Sulfur
4270
mg/Kg -
dry
148
152
1
06/11/19 17:10
JTR
6010D
Sodium Absorption Ratio
11.9
Ratio
2.22
5.00
1
06/11/19 17:10
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-155-0242
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lKristinaA. McAdams Date & Time: 06/04/2019 08:53:36
Page 7 of 8

ro
(4
m
00
0
rh
00
Client Name/Address
EMA Resources inc
755 yadkinville Rd
Mocksville, NC 27028
Project Description
Project Number
Waypoint "ll
ANALYTICAL
2790 Whilten [load
Memphis, TN 38133
[phone]
Date Time
(0/3 7.-30 NOr}i,
Q�
Client Project Mana
Brent Collins
Project/Site Location
Billing Information
Account #46245
For Laboratory Use Only
RUSH - Additional charges apply Method of Shipment
Special Detection Lim 171 Fed Ex ❑UPS MUSPS
Date Resuits Needed Courier Client Drop Off
Other
Project Manager Phone #
Project Manager Email
Purchase Order Number
336-399-3646
Brent-collins@emaresources-com
v
C
z
ca
U)
ro
°
0
C7
CD
E
a
CL
0
WLU
Unless noted, all containers
per Table 11 of 40 CFR Part
E
u
a
( 1
v
136,
Identification
o
m
Required
Analysis I Preservative
i>cick— 1.3Q
Matrix Key
WW -Wastewater GW-Groundwater
DW - Drinking Water 5 -Soil /Solid 0 -- Oil
P - Product M - Misc
Site/Facility ID #
A Cool < 10C Na2$2O3 [Micro Only]
a Cool <- 6C
C H25D4pW2
D None Required
E N30H P"110
f HNO3 pW2
G HCL pHQ
H H3PO4 pH<2
I Cool — GC NA2$203
Metals:Al,As, Ca, Gd,Cr,Cu,Fe, Pb
Mn, Mg, Mo,Hg,Ni,Se,Na,RS,K,Zn
Iti1u1111{1{1Nltill{�4�1�{Ili{I��111111{�1{1l{11 {1111{I1{
a � 019
FMA Resources Inc
Smithfield
For Laboratory Use Only Sampled by (Name - Print[ Client Remarks/Comments
Ice Custody Lab Ccmmerits boy . � ,f Sludge Samples - Report Dry Weight
r► Seals
LY N �Relinq lay• E Date Time Receiv by: (SIGNATURE) Date Time
y ,j GIB I. 613 lz-
Blan /CoolerTe p Rel ed by: {SIGNATUREI Date Time Received by: (SIGNATURE) Date Time
��
e Relinquished by: (SIGNATURE) Date Time Receive by: (SIGNATURE) Date Time

Waypointo
ANALYTICAL
6/ 13/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-155-0242
Client Project Description: Smithfield
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 6/4/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield
Lab Report Number: 19-155-0242
Date: 6/13/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L440367
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L440224
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L440367
MS/MSD Recovery failed, DT confirmed matrix interference
Analyte: Potassium
QC Batch No: L440367
MS/MSD Recovery failed, PDS confirmed matrix interference
Analyte: Phosphorus
QC Batch No: L440224
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Analyte: Mercury
QC Batch No: L440259
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 8

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Smithfield Report Date : 06/13/2019
755 Yadkinville Rd Information : Received : 06/04/2019
Mocksville , NC 27028
Report Number : 19-155-0242 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 89112
Matrix: Solids
Sample ID : South Basin
Sampled:
6/3/2019
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
97.8
%
0.010
1
06/04/19 15:25
ADM
SW-DRYWT
Ammonia Nitrogen
21700
mg/Kg -
dry
1140
1
06/12/19 11:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<220
mg/Kg -
dry
220
220
1
06/13/19 12:20
ZBD
4500NO3F-2011
Organic N
45900
mg/Kg -
dry
59.1
2950
1
06/05/19 15:47
CALCULATION
pH
7.5
S.U.
1
06/11/19 05:53
JSL
9045D
Total Solids
2.23
%
0.010
0.010
1
06/04/19 15:25
ADM
2540G-2011
Total Volatile Solids
75.9
%
0.010
0.010
1
06/04/19 15:25
ADM
2540G-2011
Total Kjeldahl Nitrogen
67700
mg/Kg -
dry
2950
1
06/05/19 15:47
CLP 4500NORGD-2011
Phosphorus
6590
mg/Kg -
dry
117
227
1
06/11/19 17:15
JTR
6010D
Aluminum
5910
mg/Kg -
dry
92.3
227
1
06/12/19 17:56
KKM
6010D
Arsenic
<19.0
mg/Kg -
dry
19.0
22.7
1
06/11/19 17:15
JTR
6010D
Cadmium
<2.25
mg/Kg -
dry
2.25
4.55
1
06/11/19 17:15
JTR
6010D
Calcium
12200
mg/Kg -
dry
764
1140
1
06/11/19 17:15
JTR
6010D
Chromium
60.0
mg/Kg -
dry
8.64
11.4
1
06/11/19 17:15
JTR
6010D
Copper
1140
mg/Kg -
dry
6.59
11.4
1
06/11/19 17:15
JTR
6010D
Iron
9230
mg/Kg -
dry
193
227
1
06/11/19 17:15
JTR
6010D
Lead
<6.77
mg/Kg -
dry
6.77
13.6
1
06/11/19 17:15
JTR
6010D
Magnesium
3140
mg/Kg -
dry
101
227
1
06/11/19 17:15
JTR
6010D
Manganese
192
mg/Kg -
dry
8.32
22.7
1
06/11/19 17:15
JTR
6010D
Mercury
<0.143
mg/Kg -
dry
0.143
0.645
1
06/11/19 12:10
TJS
7471A
Molybdenum
12.1
mg/Kg -
dry
5.91
11.4
1
06/11/19 17:15
JTR
6010D
Nickel
32.0
mg/Kg -
dry
7.50
11.4
1
06/11/19 17:15
JTR
6010D
Potassium
5860
mg/Kg -
dry
135
227
1
06/11/19 17:15
JTR
6010D
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 5 of 8

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-155-0242
Lab No : 89112
Sample ID : South Basin
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield
Information :
REPORT OFANALYSIS
Report Date : 06/13/2019
Received : 06/04/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 6/3/2019 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<22.3
mg/Kg -
dry
22.3
22.7
1
06/11/19 17:15
JTR
6010D
Sodium
30200
mg/Kg -
dry
351
1140
1
06/12/19 17:56
KKM
6010D
Zinc
1960
mg/Kg -
dry
49.1
56.8
1
06/11/19 17:15
JTR
6010D
Sulfur
12000
mg/Kg -
dry
222
227
1
06/11/19 17:15
JTR
6010D
Sodium Absorption Ratio
9.35
Ratio
2.22
5.00
1
06/11/19 17:15
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 8

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-155-0242
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lKristinaA. McAdams Date & Time: 06/04/2019 08:53:36
Page 7 of 8

ro
(4
m
00
0
rh
00
Client Name/Address
EMA Resources inc
755 yadkinville Rd
Mocksville, NC 27028
Project Description
Project Number
Waypoint "ll
ANALYTICAL
2790 Whilten [load
Memphis, TN 38133
[phone]
Date Time
(0/3 7.-30 NOr}i,
Q�
Client Project Mana
Brent Collins
Project/Site Location
Billing Information
Account #46245
For Laboratory Use Only
RUSH - Additional charges apply Method of Shipment
Special Detection Lim 171 Fed Ex ❑UPS MUSPS
Date Resuits Needed Courier Client Drop Off
Other
Project Manager Phone #
Project Manager Email
Purchase Order Number
336-399-3646
Brent-collins@emaresources-com
v
C
z
ca
U)
ro
°
0
C7
CD
E
a
CL
0
WLU
Unless noted, all containers
per Table 11 of 40 CFR Part
E
u
a
( 1
v
136,
Identification
o
m
Required
Analysis I Preservative
i>cick— 1.3Q
Matrix Key
WW -Wastewater GW-Groundwater
DW - Drinking Water 5 -Soil /Solid 0 -- Oil
P - Product M - Misc
Site/Facility ID #
A Cool < 10C Na2$2O3 [Micro Only]
a Cool <- 6C
C H25D4pW2
D None Required
E N30H P"110
f HNO3 pW2
G HCL pHQ
H H3PO4 pH<2
I Cool — GC NA2$203
Metals:Al,As, Ca, Gd,Cr,Cu,Fe, Pb
Mn, Mg, Mo,Hg,Ni,Se,Na,RS,K,Zn
Iti1u1111{1{1Nltill{�4�1�{Ili{I��111111{�1{1l{11 {1111{I1{
a � 019
FMA Resources Inc
Smithfield
For Laboratory Use Only Sampled by (Name - Print[ Client Remarks/Comments
Ice Custody Lab Ccmmerits boy . � ,f Sludge Samples - Report Dry Weight
r► Seals
LY N �Relinq lay• E Date Time Receiv by: (SIGNATURE) Date Time
y ,j GIB I. 613 lz-
Blan /CoolerTe p Rel ed by: {SIGNATUREI Date Time Received by: (SIGNATURE) Date Time
��
e Relinquished by: (SIGNATURE) Date Time Receive by: (SIGNATURE) Date Time

Waypointo
ANALYTICAL
7/ 1 /2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-171-0232
Client Project Description: Smithfield Tar Heel
Tar Heel, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 6/20/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield Tar Heel
Lab Report Number: 19-171-0232
Date: 7/1/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L442989
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L442989
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 92674 (North Lagoon)
Analyte: Mercury
QC Batch No: L441966/L441742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 8

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Smithfield Tar Heel Report Date : 07/01/2019
755 Yadkinville Rd Information : Tar Heel, NC Received : 06/20/2019
Mocksville , NC 27028
Report Number : 19-171-0232 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92674
Matrix: Solids
Sample ID : North Lagoon
Sampled:
6/19/2019
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
96.5
%
0.010
1
06/21/19 15:00
CJR
SW-DRYWT
Ammonia Nitrogen
6510
mg/Kg -
dry
714
1
07/01/19 09:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<143
mg/Kg -
dry
143
143
1
07/01/19 15:15
ZBD
4500NO3F-2011
Organic N
33400
mg/Kg -
dry
40.0
2010
1
06/26/19 15:01
CALCULATION
pH
11.8
S.U.
1
06/27/19 08:40
JSL
9045D
Total Solids
3.52
%
0.010
0.010
1
06/21/19 15:00
CJR
2540G-2011
Total Volatile Solids
73.8
%
0.010
0.010
1
06/21/19 15:00
CJR
2540G-2011
Total Kjeldahl Nitrogen
40000
mg/Kg -
dry
2010
1
06/26/19 15:01
CLP 4500NORGD-2011
Phosphorus
6260
mg/Kg -
dry
73.4
143
1
06/27/19 01:00
BKN
6010D
Aluminum
4430
mg/Kg -
dry
58.0
143
1
06/27/19 01:00
BKN
6010D
Arsenic
<12.0
mg/Kg -
dry
12.0
14.3
1
06/27/19 01:00
BKN
6010D
Cadmium
<1.41
mg/Kg -
dry
1.41
2.86
1
06/27/19 01:00
BKN
6010D
Calcium
45100
mg/Kg -
dry
480
714
1
06/27/19 01:00
BKN
6010D
Chromium
25.9
mg/Kg -
dry
5.43
7.14
1
06/27/19 01:00
BKN
6010D
Copper
446
mg/Kg -
dry
4.14
7.14
1
06/27/19 01:00
BKN
6010D
Iron
5090
mg/Kg -
dry
121
143
1
06/27/19 01:00
BKN
6010D
Lead
4.693
mg/Kg -
dry
4.26
8.57
1
06/27/19 01:00
BKN
6010D
Magnesium
1830
mg/Kg -
dry
63.4
143
1
06/27/19 01:00
BKN
6010D
Manganese
153
mg/Kg -
dry
5.23
14.3
1
06/27/19 01:00
KKM
6010D
Mercury
<0.0960
mg/Kg -
dry
0.0960
0.434
1
06/21/19 13:40
TJS
7471A
Molybdenum
8.40
mg/Kg -
dry
3.71
7.14
1
06/27/19 01:00
BKN
6010D
Nickel
23.7
mg/Kg -
dry
4.71
7.14
1
06/27/19 01:00
BKN
6010D
Potassium
3030
mg/Kg -
dry
85.1
143
1
06/27/19 01:00
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 8

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-171-0232
Lab No : 92674
Sample ID : North Lagoon
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield Tar Heel
Information : Tar Heel, NC
REPORT OFANALYSIS
Report Date : 07/01/2019
Received : 06/20/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 6/19/2019 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<14.0
mg/Kg -
dry
14.0
14.3
1
06/27/19 01:00
BKN
6010D
Sodium
9430
mg/Kg -
dry
221
714
1
06/27/19 01:00
BKN
6010D
Zinc
1030
mg/Kg -
dry
30.9
35.7
1
06/27/19 01:00
BKN
6010D
Sulfur
7370
mg/Kg -
dry
140
143
1
06/27/19 17:22
KKM
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
06/27/19 01:00
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 4 of 8

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-171-0232
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#70
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lKristinaA. McAdams Date & Time: 06/20/2019 09:56:21
Page 7 of 8

ro
00
0
rh
00
Client Name/Address
EMA Resources Inc
755 Yadkinville Rd
Mocksville. NC 27028
Project Description
Project Number
Waypoint
ANALYTICAL
2790 Whitten Road
Memphis, IN 38133
1901)213.2400
Date I Time
Client Project Manager/Contact
Brent Collins
Location (City/State)
7ft�Q �L AI
Project Manager Phone 0
336-399-3646
Billing Information
Account#46245
For Laboratory Use Only
�Met d of Shipment
Foed Ex SUPS �USPS
Courier Client Drop Off
Other
Project Manager Email Purchase Order Number
brent.coll'[e-mail]
o Cri z rn
RUSH - Additional charges
Special Detecticr Umit(sl
Date Results Needed
C
C
0
U
c
°
S
E
u
CO
to
E
Q
U}
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Unless noted, all containers
°
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Z
T
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C
per Table I I of 40 CFR Pa rt
135.
ro
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Z
O
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L r-ir�,00rt�
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Matrix Key
WW -Wastewater GW-Groundwater
DW- Drinking Water 5-Soil/Solid O - Oil
P • Product M • Misc
Site/Facllity ID 0
A Cool c IOC Na2S203 (Micro Only)
B Cool c= GC
C H2MM pHc2
b None Required
E NaOH pHa10
F HNO3 pHc2
G HCL pHc2
H H3PC4 pHc2
I Cool c 6C NA25203
Metals:Al,As, Ca,Cd,Cr,Cu, Fe, Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
I III IIIIICI III IIII III11111111111111111III 1111II106 7a 0192
EMA Resources Inr, 09:55.44
Smdhfreld Tar Heel
For
Laboratory Use Only
Sampled by (Name - Print)
�� �r
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
IN
CSeals
Lab Comments
oy
�j
Relin u
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Dat Time I ceived by: [SIGNATURE] bate Time
v
ReImcl she y: (SIGNATURE)
.:To
to Time Received by: (SIGNATURE) Date Time
/Blartt'.,191iemp
Relinquished by: (SIGNATURE)
Date Time ^Rereive by: (SIGNATURE) Date Time
�� S

Waypointo
ANALYTICAL
7/ 1 /2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-171-0232
Client Project Description: Smithfield Tar Heel
Tar Heel, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 6/20/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield Tar Heel
Lab Report Number: 19-171-0232
Date: 7/1/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L442989
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L442989
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L442712
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 92674 (North Lagoon)
Analyte: Mercury
QC Batch No: L441966/L441742
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 8

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Smithfield Tar Heel Report Date : 07/01/2019
755 Yadkinville Rd Information : Tar Heel, NC Received : 06/20/2019
Mocksville , NC 27028
Report Number : 19-171-0232 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92675
Matrix: Solids
Sample ID : South Lagoon
Sampled:
6/19/2019
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
96.1
%
0.010
1
06/21/19 15:00
CJR
SW-DRYWT
Ammonia Nitrogen
5970
mg/Kg -
dry
641
1
07/01/19 09:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<128
mg/Kg -
dry
128
128
1
07/01/19 15:17
ZBD
4500NO3F-2011
Organic N
68200
mg/Kg -
dry
41.5
2070
1
06/26/19 15:02
CALCULATION
pH
12.1
S.U.
1
06/27/19 08:40
JSL
9045D
Total Solids
3.89
%
0.010
0.010
1
06/21/19 15:00
CJR
2540G-2011
Total Volatile Solids
68.6
%
0.010
0.010
1
06/21/19 15:00
CJR
2540G-2011
Total Kjeldahl Nitrogen
74100
mg/Kg -
dry
2070
1
06/26/19 15:02
CLP 4500NORGD-2011
Phosphorus
3150
mg/Kg -
dry
65.9
128
1
06/27/19 01:15
BKN
6010D
Aluminum
2030
mg/Kg -
dry
52.1
128
1
06/27/19 01:15
BKN
6010D
Arsenic
<10.7
mg/Kg -
dry
10.7
12.8
1
06/27/19 01:15
BKN
6010D
Cadmium
<1.27
mg/Kg -
dry
1.27
2.56
1
06/27/19 01:15
BKN
6010D
Calcium
34600
mg/Kg -
dry
431
641
1
06/27/19 01:15
BKN
6010D
Chromium
16.2
mg/Kg -
dry
4.87
6.41
1
06/27/19 01:15
BKN
6010D
Copper
213
mg/Kg -
dry
3.72
6.41
1
06/27/19 01:15
BKN
6010D
Iron
2360
mg/Kg -
dry
109
128
1
06/27/19 01:15
BKN
6010D
Lead
<3.82
mg/Kg -
dry
3.82
7.69
1
06/27/19 01:15
BKN
6010D
Magnesium
1050
mg/Kg -
dry
56.9
128
1
06/27/19 01:15
BKN
6010D
Manganese
71.8
mg/Kg -
dry
4.69
12.8
1
06/27/19 01:15
KKM
6010D
Mercury
<0.0856
mg/Kg -
dry
0.0856
0.387
1
06/27/19 10:31
TJS
7471A
Molybdenum
6.053
mg/Kg -
dry
3.33
6.41
1
06/27/19 01:15
BKN
6010D
Nickel
17.5
mg/Kg -
dry
4.23
6.41
1
06/27/19 01:15
BKN
6010D
Potassium
2740
mg/Kg -
dry
76.4
128
1
06/27/19 01:15
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-171-0232
Lab No : 92675
Sample ID : South Lagoon
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield Tar Heel
Information : Tar Heel, NC
REPORT OFANALYSIS
Report Date : 07/01/2019
Received : 06/20/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 6/19/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<12.6
mg/Kg -
dry
12.6
12.8
1
06/27/19 01:15
BKN
6010D
Sodium
8870
mg/Kg -
dry
198
641
1
06/27/19 01:15
BKN
6010D
Zinc
477
mg/Kg -
dry
27.7
32.1
1
06/27/19 01:15
BKN
6010D
Sulfur
4050
mg/Kg -
dry
125
128
1
06/27/19 17:27
KKM
6010D
Sodium Absorption Ratio
2.53
Ratio
2.22
5.00
1
06/27/19 01:15
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-171-0232
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#70
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lKristinaA. McAdams Date & Time: 06/20/2019 09:56:21
Page 7 of 8

ro
00
0
rh
00
Client Name/Address
EMA Resources Inc
755 Yadkinville Rd
Mocksville. NC 27028
Project Description
Project Number
Waypoint
ANALYTICAL
2790 Whitten Road
Memphis, IN 38133
1901)213.2400
Date I Time
Client Project Manager/Contact
Brent Collins
Location (City/State)
7ft�Q �L AI
Project Manager Phone 0
336-399-3646
Billing Information
Account#46245
For Laboratory Use Only
�Met d of Shipment
Foed Ex SUPS �USPS
Courier Client Drop Off
Other
Project Manager Email Purchase Order Number
brent.coll'[e-mail]
o Cri z rn
RUSH - Additional charges
Special Detecticr Umit(sl
Date Results Needed
C
C
0
U
c
°
S
E
u
CO
to
E
Q
U}
l
L1
Unless noted, all containers
°
,=
s
x
Z
T
1
C
per Table I I of 40 CFR Pa rt
135.
ro
to
W
Z
O
�—
Q
rr �
LJ
IdentifiC&Cr
PAquired
Analysis / Preservative
L r-ir�,00rt�
I
�
CT
Matrix Key
WW -Wastewater GW-Groundwater
DW- Drinking Water 5-Soil/Solid O - Oil
P • Product M • Misc
Site/Facllity ID 0
A Cool c IOC Na2S203 (Micro Only)
B Cool c= GC
C H2MM pHc2
b None Required
E NaOH pHa10
F HNO3 pHc2
G HCL pHc2
H H3PC4 pHc2
I Cool c 6C NA25203
Metals:Al,As, Ca,Cd,Cr,Cu, Fe, Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
I III IIIIICI III IIII III11111111111111111III 1111II106 7a 0192
EMA Resources Inr, 09:55.44
Smdhfreld Tar Heel
For
Laboratory Use Only
Sampled by (Name - Print)
�� �r
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
IN
CSeals
Lab Comments
oy
�j
Relin u
tt
Dat Time I ceived by: [SIGNATURE] bate Time
v
ReImcl she y: (SIGNATURE)
.:To
to Time Received by: (SIGNATURE) Date Time
/Blartt'.,191iemp
Relinquished by: (SIGNATURE)
Date Time ^Rereive by: (SIGNATURE) Date Time
�� S

aceAnalytical
National Center for Testing & Innovation
>r
ANALYTICAL REPORT
June 17, 2019
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
L110 5179
06/04/2019
Smithfield Tar Heel
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
Is performed per guidance provided in laboratory standard operating procedures:060302, 060303,and 060304.
In.
4
AP- IMMEMW "Op
M
FC
FS
Fn
Fr
FC
HGI
[Al]
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 1 of 21

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
SMITHFIELD TARHEEL ANAEROBIC LAGOON L1105179-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FC
Wet Chemistry by Method D93/1010A
10
F
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
RC
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1105179
06/17/19 14:49 2 of 21

SMITHFIELD TARHEEL ANAEROBIC LAGOON
SAMPLE
L1105179-01
SUMMARY
Collected by
Waste Roy Whittaker
Collected date/time
06/03/1907:45
ONE LAB. NATIONWIDE.
Received date/time
06/04/1908:45
FP
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
F
Preparation by Method 1311
WG1293463
1 06/09/1918:09
06/09/1918:09
CGD
Mt. Juliet, TN
Preparation by Method 1311
WG1293751
1 06/10/1913:23
06/10/1913:23
CGD
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1292307
1 06/07/1910:08
06/07/1916:39
SDL
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1294836
1 06/17/1912:40
06/17/1912:40
TCC
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1293870
1 06/11/1912:18
06/11/1917:50
ANP
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG1293403
1 06/11/1916:42
06/11/1916:42
TCC
Mt. Juliet, TN
Mercury by Method 7470A
WG1293919
1 06/10/19 2142
06/11/191102
ABL
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1293959
1 06/11/19 06:29
06/11/19 08:55
CCE
Mt. Juliet, TN
Fr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1294094
1 06/11/1914:23
06/11/1914:23
BMB
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1293974
1 06/11/1910:58
06/11/19 2136
LEL
Mt. Juliet, TN
FC
Pesticides (GC) by Method 8081B
WG1294075
1 06/12/19 2128
06/13/19 09:37
LEL
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1293362
1 06/11/19 08:25
06/12/19 23:46
AO
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1105179
06/17/19
14:49
3 of 21

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 4 of 21

SMITHFIELD TARHEEL ANAEROBIC LAGOON
Collected date/time: 06/03/19 07:45
Preparation by Method 1311
■
SAMPLE RESULTS - 01
L1105179
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
6/9/2019 6:09:38 PM
WG1293463
TCLP ZHE Extraction -
6/10/2019123:16 PM
WG1293751
Fluid 1
6/9/2019 6:09:38 PM
WG1293463
Initial pH 7.39
6/9/2019 6:09:38 PM
WG1293463
Final pH 4.89
6/9/2019 6:09:38 PM
WG1293463
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
06/07/201916:39 WG1292307
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide 48.6 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 06/17/201912:40 WG1294836
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.51 T8 1 06/11/201917:50 WG1293870
Sample Narrative:
L1105179-01 WG1293870: 7.51 at21.6C
Wet Chemistry by Method D93/1010A
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Result
Qualifier
Dilution
Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1
06/11/201916:42
WG1293403
Mercury by Method 7470A
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Mercury ND
0.0100
0.20
1 06/11/20191102
WG1293919
Metals (ICP) by Method 6010D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Arsenic ND
0.100
5
1 06/11/2019 0855
WG1293959
Barium ND
0.100
100
1 06/11/2019 0855
WG1293959
Cadmium ND
0.100
1
1 06/11/2019 08:55
WG1293959
Chromium ND
0.100
5
1 06/11/2019 0855
WG1293959
Lead ND
0.100
5
1 06/11/2019 0855
WG1293959
Selenium ND
0.100
1
1 06/11/2019 0855
WG1293959
Silver ND
0.100
5
1 06/11/2019 0855
WG1293959
Volatile Organic Compounds (GC/MS) by Method
8260D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Benzene ND
0.0500
0.50
1 06/11/201914:23
WG1294094
Carbon tetrachloride ND
0.0500
0.50
1 06/11/201914:23
WG1294094
Chlorobenzene ND
0.0500
100
1 06/11/201914:23
WG1294094
Chloroform ND
0.250
6
1 06/11/201914:23
WG1294094
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1105179
06/17/19 14:49 5 of 21

SMITHFIELD TARHEEL ANAEROBIC LAGOON SAMPLE RESULTS - 01
ONE LAB. NATIONWIDE. *
Collected date/time: 06/03/19 07:45 L1105179
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1 06/11/201914:23
WG1294094
1,1-Dichloroethene
ND
0.0500
0.70
1 06/11/201914:23
WG1294094
2-Butanone (MEK)
ND
0.500
200
1 06/11/201914:23
WG1294094
Tetrachloroethene
ND
0.0500
0.70
1 06/11/201914:23
WG1294094
Trichloroethene
ND
J4 0.0500
0.50
1 06/11/201914:23
WG1294094
Vinyl chloride
ND
0.0500
0.20
1 06/11/201914:23
WG1294094
(S) Toluene-dH
105
80.0-120
0611112019 14.23
WG1294094
(S) 4-Bromofluorobenzene
100
77.0-126
0611112019 14.23
WG1294094
(S) 1,2-Dichloroethane-d4
96.3
70.0-130
061111201914.23
WG1294094
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) Z4-Dichlorophenyl Acetic Acid 72.2
Pesticides (GC) by Method 8081B
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 06/11/2019 2136
WG1293974
0.00200
10
1 06/11/2019 2136
WG1293974
14.0-158
0611112019 21.36
WG1293974
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 06/13/2019 09:37
WG1294075
Endrin
ND
0.00500
0.02
1 06/13/2019 09:37
WG1294075
Heptachlor
ND
0.00500
0.0080
1 06/13/2019 09:37
WG1294075
Lindane
ND
0.00500
0.40
1 06/13/2019 09:37
WG1294075
Methoxychlor
ND
0.00500
10
1 06/13/2019 09:37
WG1294075
Toxaphene
ND
0.0100
0.50
1 06/13/2019 09:37
WG1294075
(S) Decochlorobiphenyl
79.2
10.0-128
0611312019 09.37
WG1294075
(S) Tetrochloro-m-xylene
87.7
10.0-127
0611312019 09.37
WG1294075
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4, 6-Tribromophenol
(S) p-Terphenyl-d14
ACCOUNT:
EMA Resources
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 06/12/2019 23:46
WG1293362
ND
0.100
0.13
1 06/12/2019 23:46
WG1293362
ND
0.100
0.13
1 06/12/2019 23:46
WG1293362
ND
0.100
0.50
1 06/12/2019 23:46
WG1293362
ND
0.100
3
1 06/12/2019 23:46
WG1293362
ND
0.100
2
1 06/12/2019 23:46
WG1293362
ND
J4 0.100
5
1 06/12/2019 23:46
WG1293362
ND
0.100
400
1 06/12/2019 23:46
WG1293362
ND
0.100
200
1 06/12/2019 23:46
WG1293362
ND
J4 0.100
100
1 06/12/2019 23:46
WG1293362
ND
0.100
400
1 06/12/2019 23:46
WG1293362
ND
0.100
2
1 06/12/2019 23:46
WG1293362
17.4
10.0-120
061121201923.46
WG1293362
11.4
10.0-120
061121201923.46
WG1293362
13.0
10.0-127
061121201923.46
WG1293362
13.8
10.0-130
061121201923.46
WG1293362
23.7
10.0-155
061121201923.46
WG1293362
36.5
10.0-128
061121201923.46
WG1293362
PROJECT:
SDG:
DATE/TIME: PAGE:
L1105179
06/17/19 14:49 6 of 21
Fp
Fc
FS
Fn
FA
Fc
�GI
SAI
Rc

WG1292307
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3419020-1 06/07/191613
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
L1104404-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1105179-01
(OS) L1104404-01 06/07/1916:23 • (DUP) R3419020-3 06/07/1916:29
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide ND 0.0666 1 0.000 20
L1105657-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1105657-02 06/07/1916:40 • (DUP) R3419020-3 06/07/1916:41
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.102 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3419020-2 06/07/19 16:14
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.54 101
Rec. Limits LCS Qualifier
50.0-150
L1104405-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1104405-01 06/07/19 16:30 • (MS) R3419020-4 06/07/19 16:31 • (MSD) R3419020-5 06/07/19 16:32
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.59 1.66 90.4 94.6 1 75.0-125 4.26 20
L1105157-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1105157-02 06/07/19 16:34 • (MS) R3419020-6 06/07/19 16:35 • (MSD) R3419020-7 06/07/19 16:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.33 1.45 79.8 86.7 1 75.0-125 8.31 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 7 of 21

WG1294836
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3421663-1 06/17/1912:40
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1105179-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1105179-01
(OS) L1105179-01 06/17/1912:40 • (DUP) R3421663-3 06/17/1912:40
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Sulfide 48.6 54.6 1 11.8 20
Laboratory Control Sample (LCS)
(LCS) R3421663-2 06/17/19 12:40
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Reactive Sulfide 100 85.0 85.0 70.0-130
ONE LAB. NATIONWIDE. *
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 3 of 21

WG1293870 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1105179-01
L1106842-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1106342-02 06/11/1917:50 • (DUP) R3420090-2 06/11/1917:50
Original Result DUP Result Dilution DUP RPD
Analyte su su
Corrosivity by pH 7.36 7.51 1 2.02
Sample Narrative:
OS: 7.36 at21.1C
DUP:7.51 at22C
L1106842-05 Original Sample (OS) • Duplicate (DUP)
(OS) L1106342-05 06/11/1917:50 • (DUP) R3420090-3 06/11/1917:50
Original Result DUP Result Dilution DUP RPD
Analyte su su
Corrosivity by pH 8.90 8.87 1 0.338
Sample Narrative:
OS: 8.9 at21.8C
DUP: 8.87 at 20.8C
Laboratory Control Sample (LCS)
(LCS) R3420090-1 06/11/19 17:50
Spike Amount LCS Result LCS Rec. Rec. Limits
Analyte su su
Corrosivity by pH 10.0 9.95 99.5 99.0-101
Sample Narrative:
LCS: 9.95 at19.8C
DUP Qualifier DUP RPD
Limits
J3 1
DUP Qualifier DUP RPD
Limits
1
LCS Qualifier
ONE LAB. NATIONWIDE. *
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 9 of 21

WG1293403 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1105179-01
L1105508-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1105503-01 06/11/1916:42 • (DUP) R3420071-2 06/11/19 16:42
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability 80.4 82.4 1 2.46
L1105513-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1105513-01 06/11/1916:42 • (DUP) R3420071-3 06/11/1916:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability 79.4 80.4 1 1.25 10
L1106682-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1106632-02 06/11/1916:42 • (DUP) R3420071-4 06/11/19 16:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability 105 104 1 0.953 10
Laboratory Control Sample (LCS)
(LCS) R3420071-1 06/11/19 16:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 82.4 101 96.0-104
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 10 of 21

WG1293919 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1105179-01
Method Blank (MB)
(MB) R3419936-1 06/11/191003
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
Mercury U 0.00330
0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3419936-2 06/11/1910:11 • (LCSD) R3419936-3 06/11/191013
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0298 0.0316
99.2 105 80.0-120 5.90 20
L1104192-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1104192-01 06/11/19 1015 • (MS) R3419936-4 06/11/19 10:13 • (MSD) R3419936-5 06/11/19 10:23
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0305
0.0319 102 106 1 75.0-125 4.47 20
L1105116-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1105116-06 06/11/19 10:30 • (MS) R3419936-6 06/11/19 10:33 • (MSD) R3419936-7 06/11/19 10:35
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0322
0.0295 107 98.2 1 75.0-125 8.93 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
SAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 11 of 21

WG1293959
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1105179-01
(MB) R3419334-1 06/11/19 08:47
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0330
0.100
Barium U
0.0330
0.100
Cadmium U
0.0330
0.100
Chromium U
0.0330
0.100
Lead U
0.0330
0.100
Selenium U
0.0330
0.100
Silver U
0.0330
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3419884-2 06/11/19 08:50 • (LCSD) R3419884-3 06/11/19 08:52
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.96
10.0
99.6
100
80.0-120
Barium
10.0
10.4
10.4
104
104
80.0-120
Cadmium
10.0
10.1
10.2
101
102
80.0-120
Chromium
10.0
9.91
9.98
99.1
99.8
80.0-120
Lead
10.0
10.0
10.0
100
100
80.0-120
Selenium
10.0
10.5
10.5
105
105
80.0-120
Silver
2.00
1.91
1.91
95.4
95.4
80.0-120
L1105179-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1105179-01 06/11/19 08:55 • (MS) R3419334-5 06/11/19 09:01 • (MSD) R3419334-6 06/11/19 09:04
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
10.1
9.96
101
99.6
Barium
10.0
ND
10.4
10.3
104
103
Cadmium
10.0
ND
10.2
10.1
102
101
Chromium
10.0
ND
10.0
9.88
100
98.8
Lead
10.0
ND
10.1
10.0
101
100
Selenium
10.0
ND
10.5
10.5
105
105
Silver
2.00
ND
1.93
1.90
96.3
95.0
ACCOUNT:
EMA Resources
PROJECT:
LCS Qualifier LCSD Qualifier RPD
RPD Limits
0.423
20
0.0969
20
0.440
20
0.690
20
0.00949
20
0.101
20
0.00241
20
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
1.11
20
1 75.0-125
0.999
20
1 75.0-125
0.904
20
1 75.0-125
1.25
20
1 75.0-125
0.670
20
1 75.0-125
0.820
20
1 75.0-125
1.34
20
SDG:
DATE/TIME:
PAGE:
L1105179
06/17/19 14:49
12 of 21

WG1294094 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1105179-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3420023-3 06/11/191224
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-d8
108
80.0-120
(S) 4-Bromofluorobenzene
101
77.0-126
(S) 1,2-Dichloroethane-d4
94.6
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3420023-1 06/11/19 09:22 • (LCSD) R3420023-2 06/11/19 09:42
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.0250
0.0252
0.0278
101
ill
70.0-123
Carbon tetrachloride
0.0250
0.0269
0.0293
107
117
68.0-126
Chlorobenzene
0.0250
0.0270
0.0294
108
118
80.0-121
Chloroform
0.0250
0.0251
0.0275
100
110
73.0-120
1,2-Dichloroethane
0.0250
0.0249
0.0275
99.6
110
70.0-128
1,1-Dichloroethene
0.0250
0.0250
0.0275
99.9
110
71.0-124
2-Butanone (MEK)
0.125
0.143
0.158
114
127
44.0-160
Tetrachloroethene
0.0250
0.0283
0.0307
113
123
72.0-132
Trichloroethene
0.0250
0.0281
0.0317
112
127
78.0-124
Vinyl chloride
0.0250
0.0269
0.0299
108
120
67.0-131
(S) Toluene-d8
103
100
80.0-120
(S) 4-Bromofluorobenzene
99.6
101
77.0-126
(S) 1,2-Dichloroethane-d4
105
108
70.0-130
LCS Qualifier
LCSD Qualifier RPD
9.83
8.73
8.42
9.45
9.79
9.63
10.2
8.20
J4 12.1
10.6
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 13 of 21

WG1294094 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1105179-01
L1104926-02 Original Sample (OS) • Matrix Spike (MS)
(OS) L1104926-02 06/11/19 14:03 • (MS) R3420023-4 06/11/19 1443
Spike Amount
Original Result
MS Result
MS Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
1.25
ND
1.14
91.1
1 17.0-158
Carbon tetrachloride
1.25
ND
1.13
90.4
1 23.0-159
Chlorobenzene
1.25
ND
1.28
102
1 33.0-152
Chloroform
1.25
ND
1.18
94.1
1 29.0-154
1,2-Dichloroethane
1.25
ND
1.23
98.3
1 29.0-151
1,1-Dichloroethene
1.25
ND
1.03
82.5
1 11.0-160
2-Butanone (MEK)
6.25
ND
7.19
115
1 10.0-160
Tetrachloroethene
1.25
ND
1.21
96.5
1 10.0-160
Trichloroethene
1.25
ND
1.25
100
1 10.0-160
Vinyl chloride
1.25
ND
1.07
85.8
1 10.0-160
(S) Toluene-d8
101
80.0-120
(S) 4-Bromofluorobenzene
100
77.0-126
(S) 1,2-Dichloroethane-d4
105
70.0-130
MS Qualifier
L1105179-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1105179-01 06/11/19 14:23 • (MS) R3420023-6 06/11/19 15:03 • (MSD) R3420023-7 06/11/19 15:22
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
1.25
ND
1.18
1.29
94.5
103
Carbon tetrachloride
1.25
ND
1.21
1.33
96.4
106
Chlorobenzene
1.25
ND
1.28
1.40
102
112
Chloroform
1.25
ND
1.21
1.31
96.6
104
1,2-Dichloroethane
1.25
ND
1.20
1.32
95.7
105
1,1-Dichloroethene
1.25
ND
1.11
1.18
89.1
94.1
2-Butanone (MEK)
6.25
ND
6.72
7.50
108
120
Tetrachloroethene
1.25
ND
1.27
1.38
102
110
Trichloroethene
1.25
ND
1.30
1.41
104
113
Vinyl chloride
1.25
ND
1.15
1.22
92.1
97.9
(S) Toluene-d8
102
102
(S) 4-Bromofluorobenzene
99.3
100
(S) 1,2-Dichloroethane-d4
105
98.9
ACCOUNT:
EMA Resources
PROJECT:
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
8.48
27
1 23.0-159
9.54
28
1 33.0-152
9.11
27
1 29.0-154
7.71
28
1 29.0-151
9.68
27
1 11.0-160
5.46
29
1 10.0-160
11.0
32
1 10.0-160
8.13
27
1 10.0-160
8.44
25
1 10.0-160
6.17
27
80.0-120
77.0-126
70.0-130
SDG:
DATE/TIME:
PAGE:
L1105179
06/17/19 14:49
14 of 21

WG1293974
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1105179-01
(MB) R3420112-1 06/11/191745
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 77.4
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3420112-2 06/11/19 17:59
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
2,4-D 0.0500
0.0478
95.6
50.0-120
2,4,5-TP (Silvex) 0.0500
0.0474
94.8
50.0-125
(S) Z4-Dichlorophenyl Acetic
89.8
14. 0-158
Acid
L1104192-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1104192-01 06/11/19 20:55 • (MS) R3420112-3 06/11/19 2109 • (MSD) R3420112-4 06/11/19 2122
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0402
0.0482
80.4
96.4
2,4,5-TP (Silvex)
0.0500
ND
0.0430
0.0504
86.0
101
(S) Z4-Dichlorophenyl Acetic
828
994
Acid
Dilution Rec. Limits
1 50.0-120
1 50.0-125
14.0-158
MS Qualifier MSD Qualifier RPD
18.1
15.8
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 15 of 21

WG1294075
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1105179-01
(MB) R3420719-2 06/13/19 08:33
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
72.3
10.0-128
(S) Tetrochloro-m-xylene
84.5
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3420719-1 06/13/19 0824
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00906
90.6
55.0-129
Endrin
0.0100
0.00927
92.7
57.0-134
Heptachlor
0.0100
0.00991
99.1
27.0-132
Methoxychlor
0.0100
0.0139
139
54.0-155
(S) Decachlorobiphenyl
73.9
10.0-128
(S) Tetrochloro-m-xylene
81.6
10.0-127
L1104192-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1104192-01 06/13/19 08:53 • (MS) R3420719-3 06/13/19 09:03 • (MSD) R3420719-4 06/13/19 09:23
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00921
0.00928
92.1
92.8
1 14.0-141
Endrin
0.0100
ND
0.00942
0.00951
94.2
95.1
1 10.0-160
Heptachlor
0.0100
ND
0.0104
0.0107
104
107
1 16.0-136
Methoxychlor
0.0100
ND
0.0141
0.0145
141
145
1 10.0-160
(S) Decachlorobiphenyl
75.2
81.0
10.0-128
(S) Tetrochloro-m-xylene
89.0
879
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
0.757 40
0.951 39
2.84 40
2.80 34
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 16 of 21

WG1293362 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1105179-01
Method Blank (MB)
(MB) R3420534-2 06/12/19 2043
MB Result
Analyte
mg/I
1,4-Dichlorobenzene
U
2,4-Dinitrotoluene
U
Hexachlorobenzene
U
Hexachloro-1,3-butadiene
U
Hexachloroethane
U
Nitrobenzene
U
Pyridine
U
2-Methylphenol
U
3&4-Methyl Phenol
U
Pentachlorophenol
U
2,4,5-Trichlorophenol
U
2,4,6-Trichlorophenol
U
(S) Nitrobenzene-d5
31.3
(S) 2-Fluorobiphenyl
35.2
(S) p-Terphenyl-d14
70.5
(S) Phenol-d5
11.0
(S) 2-Fluorophenol
19.2
(S) Z4, 6-Tribromophenol 50.5
MB Qualifier
Laboratory Control Sample (LCS)
MB MDL
mg/I
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
10.0-127
10.0-130
10.0-128
10.0-120
10.0-120
10.0-155
(LCS) R3420534-1 06/12/19 2023
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
1,4-Dichlorobenzene
0.500
0.337
67.4
18.0-120
2,4-Dinitrotoluene
0.500
0.594
119
49.0-124
Hexachlorobenzene
0.500
0.531
106
44.0-120
Hexachloro-1,3-butadiene
0.500
0.319
63.8
19.0-120
Hexachloroethane
0.500
0.318
63.6
15.0-120
Nitrobenzene
0.500
0.337
67.4
27.0-120
Pyridine
0.500
0.0297
5.94
10.0-120 J4
2-Methylphenol
0.500
0.384
76.8
28.0-120
3&4-Methyl Phenol
0.500
0.389
77.8
31.0-120
Pentachlorophenol
0.500
0.630
126
23.0-120 J4
2,4,5-Trichlorophenol
0.500
0.561
112
44.0-120
2,4,6-Trichlorophenol
0.500
0.566
113
42.0-120
(S) Nitrobenzene-d5
57.7
10.0-127
(S) 2-Fluorobiphenyl
89.9
10.0-130
(S) p-Terphenyl-d14
105
10.0-128
ACCOUNT:
PROJECT:
EMA Resources
SDG: DATE/TIME: PAGE:
L1105179 06/17/19 14:49 17 of 21

1
WG1293362 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1105179-01
Laboratory Control Sample (LCS)
(LCS) R3420534-1 06/12/19 2023
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 33.4 10.0-120
(S) 2-Fluorophenol 470 10.0-120
(S) 2,4, 6-Tribromophenol ill 10. 0-155
L1104192-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1104192-01 06/13/19 00:06 • (MS) R3420534-3 06/13/19 00:26 • (MSD) R3420534-4 06/13/19 00:47
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.110
0.0718
22.0
14.4
2,4-Dinitrotoluene
0.500
ND
0.393
0.395
78.6
79.0
Hexachlorobenzene
0.500
ND
0.351
0.341
70.2
68.2
HexachIoro-1,3-butadiene
0.500
ND
0.0833
0.0507
16.7
10.1
Hexachloroethane
0.500
ND
0.0807
0.0505
16.1
10.1
Nitrobenzene
0.500
ND
0.202
0.162
40.4
32.4
Pyridine
0.500
ND
0.128
0.0997
25.6
19.9
2-Methylphenol
0.500
ND
0.224
0.186
44.8
37.2
3&4-Methyl Phenol
0.500
ND
0.236
0.193
47.2
38.6
Pentachlorophenol
0.500
ND
0.404
0.366
80.8
73.2
2,4,5-Trichlorophenol
0.500
ND
0.359
0.330
71.8
66.0
2,4,6-Trichlorophenol
0.500
ND
0.344
0.316
68.8
63.2
(S) Nitrobenzene-d5
41.0
33.3
(S) 2-Fluorobiphenyl
49.3
46.4
(S) p-Terphenyl-d14
72.0
71.1
(S) Phenol-d5
17.1
13.4
(S) 2-Fluorophenol
26.0
18.2
(S)2,4,6-Tribromophenol
71.0
72.0
Dilution Rec. Limits
MS Qualifier MSD Qualifier
RPD
1 17.0-120
J3 J6
42.0
1 39.0-125
0.508
1 35.0-122
2.89
1 12.0-120
J3 J6
48.7
1 10.0-120
J3
46.0
1 12.0-120
22.0
1 10.0-120
24.9
1 10.0-120
18.5
1 10.0-120
20.0
1 10.0-128
9.87
1 33.0-120
8.42
1 26.0-120
8.48
10.0-127
10.0-130
10.0-128
10.0-120
10.0-120
10.0-155
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1105179 06/17/19 14:49 13 of 21

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Abbreviations and Definitions
u
Fc
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
FS
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fn
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard Anal es added to eve blank, sample, Laboratory Control Sample/Duplicate and
9 ( 9 )- Yt n1 P n1
F
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
F
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
e
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
AI
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
Rc
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1105179 06/17/19 14:49 19 of 21

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
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ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1105179 06/17/19 14:49 20 of 21

/ Pre=Prat
.e
Chain of Custody Page of
EMA Resources
Billing Information:
Mr. Brent Collins Pres
Anatysis
/
Container
755 Yadkinville Road
Mocksville, NC 27028
755 Yadkinville Road Chk
Mocksville, NC 27028
aceAnalytrcal'
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Phoney 615-758.5858 [ i-jr'4•
Phone: [phone]
fan fii5 758 5859 1 �
Report to:
Mr. Brent Collins
Finah To: [e-mail]
Project
Description: S�(x'./1�/.�
lez_x
City/State
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Collected � �
Phone: [phone]
Client Project rr
Lab Project 9L
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Fax: [phone]
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Acctnum: EMARES
Template:T11413
Prelogin: P689639
TSR: 702 -Cassandra Foster
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PB: ` L
Golfe ed by (print):
LfJ '/
Site/Facility ID N
PC y
Coll2 ed (sig re
Immed atel Y
Packed on Ice N _ y _
Rush? (Lab MUST Be Notified) Quote #
Same Day Five Day
�
_ Next Day _5 Day (Rad only) Date Results Needed r
_Two Day — 10 Day )Rad Only)
_ Three Day of .
Sample ID
Comp/Grab
Matrix'
Depth
Date
Time
ntrs
shipped via: Ill Ground
4 (lab only)
1AGl
SS
5
2
X
X
4
7
I
i
' Matrix: - -- --�--- -
Remarks:
AIR -Air F- Filter pH Temp
GW-Gi Groundwater
GW -Groundwater B Bioassay
WW - Waste Water
Flow Other
DW -Drinking Water Samples retur d via: [�`
OT -Other UPS t#Ex —Courier _ Tracking q 7/j� 3 4/it�
-
COC Seal Present/Tntact a p _Y N
COC signed/Accurate:
Bottles arrive intact:
Correct bottles used: N
Sufficient volume sent: N
FiS�g
1 l _`t" " l�j
Relinq 5' natur Date Time: Received by: {Signatl�re� Trip Blank Received: Yes o Pi
G 3 1 tOD4iA H[ ECH
!! TBR
Re Inquis d by : (Signature) Date, Time Received b (Signature) Bottles Received:
Y� ( g ) °C
Temp:
Relinquished by; (Signature) Date: Time: 1 Receiv r lab by: (Signature) D e: Time:
ff I Gt
v0A Zero Headspace: Y N
Preservation. Correct/Checked: _Y _N
W SCREM <0,5 MPAr
if preservation required by Login: Date/Time
HOI& Conditic
NCF / OK

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number:
WWTP Name: Tarheel WWTP NPDES Number:
W Q0014868
NCO078344
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ I
All B (Alk Treattent)❑ Alt. C (Prior Testing)❑
Alt.D (No Prior Test) Lp
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens".
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gatnma RaX ❑
Pasteurization El
Class B:
jAlt. (1) Fecal Densit Ell
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
Tiapplicable to alternative performed Class A or Class B complete the followin
monitorin
data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
ence
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
inimu�
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
1365
4370
10438
MPN/G
0
Quarterly
G
SM92210E-
2006
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Prep r Name and Title e or print) Land Applier Name and Title (if applicable)(type or print)
1 /5/2020
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 06/03/2019
Reported: 06/05/2019
For: Smithfield TarHeel North Basin
Comments: Geometric Mean: 4370 MPN/g
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190603-08-01
Fecal Coliforms
N-1
4832
MPN/g
SM92210E-2006
06/03/2019
MD
190603-08-01
Percent Solids
N-1
4.76
%
SM2540B-2011
06/03/2019
MD
190603-08-02
Fecal Coliforms
N-2
6302
MPN/g
SM92210E-2006
06/03/2019
MD
190603-08-02
Percent Solids
N-2
4.76
%
SM2540B-2011
06/03/2019
MD
190603-08-03
Fecal Coliforms
N-3
1365
MPN/g
SM92210E-2006
06/03/2019
MD
190603-08-03
Percent Solids
N-3
5.13
%
SM2540B-2011
06/03/2019
MD
190603-08-04
Fecal Coliforms
N-4
2500
MPN/g
SM92210E-2006
06/03/2019
MD
190603-08-04
Percent Solids
N-4
5.2
%
SM2540B-2011
06/03/2019
MD
190603-08-05
Fecal Coliforms
N-5
6329
MPN/g
SM92210E-2006
06/03/2019
MD
190603-08-05
Percent Solids
N-5
4.74
%
SM2540B-2011
06/03/2019
MD
190603-08-06
Fecal Coliforms
N-6
4432
MPN/g
SM92210E-2006
06/03/2019
MD
190603-08-06
Percent Solids
N-6
5.19
%
SM2540B-2011
06/03/2019
MD
190603-08-07
Fecal Coliforms
N-7
10438
MPN/g
SM92210E-2006
06/03/2019
MD
190603-08-07
Percent Solids
N-7
4.79
%
SM2540B-2011
06/03/2019
MD
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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STATF.SVILI,E ANALYTICAL
Address:
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122 Court Street Y.O. Box 228
Statesville, INC 2868787
(7114)872-4697
Contact Person: Phone #
FAX#
Chain of
Custody Record
PO # Sr/fFtGr7 R f���[ Requisitioned by: (Time Date)
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Relinquished by:
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Composite Sampling #1:
Time begin am, pm Date ____/—(
Time end am, pm Date _/ /_
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date _/�(
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Time l a , pm ate � /� Sampled by: 0
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Time am, pm Date _/ /� Holding times met:
Time am, pm Date _/ /_
Compliance work:
Non-compliance work:
Lab Comments: Samples Transported On Ice:
Initials:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number: WQ0014868
WWTP Name: Tarheel WWTP NPDES Number: NCO078344
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (AIk Treatment) [3
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑ I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Rav ❑
Gamma Ray ❑ I
Pasteurization ❑
Class B:
Alt. (1) Fecal DensitypI
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Cop2osting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
S
Pathogen Density
Number o
Excee-
Frequency
of Analysis
y
Sample
T e
Type
Analytical
Tech-ni ue
q
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per of
total solids
MPN
1751
4433
7538
MPN/g
0
Quarterly
G
SM9221CF-
2006
CFL
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per a grains
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ 1
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T 1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC
Prep Name and Titl type or print)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
L-�,- ;� d 2! �— e Z"o 24- 115/2020
Date Signature of Land Annlier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 06/03/2019
Reported: 06/05/2019
For: Smithfield TarHeel South Basin
Comments: Geometric Mean: 4433 MPN/g
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190603-07-01
Fecal Coliforms
S-1
7317
MPN/g
SM92210E-2006
06/03/2019
MD
190603-07-01
Percent Solids
S-1
4.1
%
SM2540B-2011
06/03/2019
MD
190603-07-02
Fecal Coliforms
S-2
5299
MPN/g
SM92210E-2006
06/03/2019
MD
190603-07-02
Percent Solids
S-2
4.34
%
SM2540B-2011
06/03/2019
MD
190603-07-03
Fecal Coliforms
S-3
5582
MPN/g
SM92210E-2006
06/03/2019
MD
190603-07-03
Percent Solids
S-3
4.12
%
SM2540B-2011
06/03/2019
MD
190603-07-04
Fecal Coliforms
S-4
1751
MPN/g
SM92210E-2006
06/03/2019
MD
190603-07-04
Percent Solids
S-4
4.57
%
SM2540B-2011
06/03/2019
MD
190603-07-05
Fecal Coliforms
S-5
7538
MPN/g
SM92210E-2006
06/03/2019
MD
190603-07-05
Percent Solids
S-5
3.98
%
SM2540B-2011
06/03/2019
MD
190603-07-06
Fecal Coliforms
S-6
3125
MPN/g
SM92210E-2006
06/03/2019
MD
190603-07-06
Percent Solids
S-6
4.16
%
SM2540B-2011
06/03/2019
MD
190603-07-07
Fecal Coliforms
S-7
3768
MPN/g
SM92210E-2006
06/03/2019
MD
190603-07-07
Percent Solids
S-7
3.45
%
SM2540B-2011
06/03/2019
MD
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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122 CourtStreet • P.O. Box 228
Statesville, NC 28687
Address: !��
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Contact Person: o Y i 1 �����
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Phone #
FAX#
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PO # -
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Requisitioned by:
(rme Date)
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Relinquished by:
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Composite Sampling #1:
Time begin am, pm Date _/__J_
Time end am, pm Date �_/_
Composite Sampling #2:
Time begin am, pm Date _//_
Time end am, pm Date _/ /
TimelR a,
Tim/2 9.1
Time
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am46 Date/ /_Z_� Sampled by: lot
am, 9Date i0 /L� Transported by:
am, pm Date /_/_ Holding times met:
am, pm Date //
Compliance work:
Non-compliance work:
Samples Transported On Ice:
Initials:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number:
WWTP Name: Tarheel WWTP NPDES Number:
Monitoring Period: From 1/1/2019 To 12/31/2019
WQ0014868
NCO078344
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
AIt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to further Reduce Pathogens" -
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma RaX ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density R1
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
Ifapplicableto alternative performed (Class A or Class B) complete the followin
monitorin data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number oFrequency
Excee-
s
of Anal sis
Y
Sample
Type
Analytical
Tech-ni ue
q
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
4283
5244
5990
MPNIG
0
Quarterly
G
SM92210E-
2006
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑r
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alit. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Prep ame and Titl e or print) Land Applier Name and Title
(if applicable)(type or print)
1/5/2020
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 06/20/2019
Reported: 06/21 /2019
For: Smithfield Tar Heel North Lagoon
Comments: Geometric Mean 5244 MPN/g
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190620-14-01
Fecal Coliforms
1
5555
MPN/g
SM92210E-2006
06/20/2019
WC
190620-14-01
Percent Solids
1
4.14
%
SM2540B-2011
06/20/2019
WC
190620-14-02
Fecal Coliforms
2
4283
MPN/g
SM92210E-2006
06/20/2019
WC
190620-14-02
Percent Solids
2
5.37
%
SM2540B-2011
06/20/2019
WC
190620-14-03
Fecal Coliforms
3
5679
MPN/g
SM92210E-2006
06/20/2019
WC
190620-14-03
Percent Solids
3
4.05
%
SM2540B-2011
06/20/2019
WC
190620-14-04
Fecal Coliforms
4
5882
MPN/g
SM92210E-2006
06/20/2019
WC
190620-14-04
Percent Solids
4
3.91
%
SM2540B-2011
06/20/2019
WC
190620-14-05
Fecal Coliforms
5
4822
MPN/g
SM92210E-2006
06/20/2019
WC
190620-14-05
Percent Solids
5
4.77
%
SM2540B-2011
06/20/2019
WC
190620-14-06
Fecal Coliforms
6
5990
MPN/g
SM92210E-2006
06/20/2019
WC
190620-14-06
Percent Solids
6
3.84
%
SM2540B-2011
06/20/2019
WC
190620-14-07
Fecal Coliforms
7
4752
MPN/g
SM92210E-2006
06/20/2019
WC
190620-14-07
Percent Solids
7
4.84
%
SM2540B-2011
06/20/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190620-14-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-14-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-14-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-14-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-14-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-14-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-14-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Client: /� �!% �3.
STATESVILLE ANALYTICAL
122 Court Street P.O. Box 228
Statesville, NC 28687
Address L O�
X11401 cy e5c CC ` ^ .17 O
[phone]
Contact Person: � Phone
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# _ 7s FAX*
Chain of
Custody Record
PO # s„�G�[.�J .?" Requisitioned by: (Time Date)
d
Customer A/fp�(,Z[t
Sample IDb
Lab to r
Time Sampled
(Grab Only)
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a
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peters requested for analysis
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Relinquished by:
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Composite Sampling #1:
Time begin am, pm Date _(,/
Time end am, pm Date /_/_
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date _I_I^
--- Time � !O(, ri pm Date /6Jaa1 ' Sampled by:
Timey5p am, pm Date !,/ � I Transported by: G
Time am, pm Date _/ / Holding times met:
Time am, pm Date,_)/— Compliance work:
Non-compliance work:
Lab Comments: Samples Transported On Ice:
Initials:
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number: WQ0014868
WWTP Name: Tarheel WWTP NPDES Number: NCO078344
Monitoring Period: From 1/l/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1
Alt B (Alk Treatment)❑
Alt_ C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens" -
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Densit p1
Alt. (2) Process to Significantly Reduce Pathogens ❑
if applicable to alternative performed (Class B only) indicate "Process to Mgoficantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B) complete the followin
monitorin
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er o
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech-ni ue
q
MinimumGeo.
Mean
MaximumUnits
Fecal Colifornt
2 x 10 to the
6th power
per gram of
total solids
MPN
431
461
504
MPN/G
0
Quarterly
G
SM92210E-
2006
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 gams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Prep ame and Titi e or print) Land Applier Name and Title (if applicable)(type or print)
29. 1 /5/2020
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 06/20/2019
Reported: 06/21 /2019
For: Smithfield Tar Heel South Lagoon
Comments:
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190620-15-01
Fecal Coliforms
s1
<431
MPN/g
SM92210E-2006
06/20/2019
WC
190620-15-01
Percent Solids
s1
4.64
%
SM2540B-2011
06/20/2019
WC
190620-15-02
Fecal Coliforms
s2
<438
MPN/g
SM92210E-2006
06/20/2019
WC
190620-15-02
Percent Solids
s2
4.57
%
SM2540B-2011
06/20/2019
WC
190620-15-03
Fecal Coliforms
s3
<431
MPN/g
SM92210E-2006
06/20/2019
WC
190620-15-03
Percent Solids
s3
4.64
%
SM2540B-2011
06/20/2019
WC
190620-15-04
Fecal Coliforms
s4
<459
MPN/g
SM92210E-2006
06/20/2019
WC
190620-15-04
Percent Solids
s4
4.36
%
SM2540B-2011
06/20/2019
WC
190620-15-05
Fecal Coliforms
s5
<500
MPN/g
SM92210E-2006
06/20/2019
WC
190620-15-05
Percent Solids
s5
4.00
%
SM2540B-2011
06/20/2019
WC
190620-15-06
Fecal Coliforms
s6
<504
MPN/g
SM92210E-2006
06/20/2019
WC
190620-15-06
Percent Solids
s6
3.97
%
SM2540B-2011
06/20/2019
WC
190620-15-07
Fecal Coliforms
s7
<468
MPN/g
SM92210E-2006
06/20/2019
WC
190620-15-07
Percent Solids
s7
4.27
%
SM2540B-2011
06/20/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190620-15-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-15-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-15-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-15-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-15-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-15-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190620-15-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Client:
�SQ„ ,fir
�
STATESVILLE ANALYTICAL
122 Court sP.O. Box 229
, NC 28687
Statesville,
[phone]
Address: �� r r✓��` o
�Y
✓zGf—— d2T
Contact Person:
o
Phone #
FAX#
Chain of
PO # SAv r>��6
f A2 _4—
! /1
Requisitioned by:
(Time
Date)
Custody Record
Customer . �
Sample IDM
Lab-1 D tl
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
m
d
Matrix
pe,ameters requested for analysis
Sea
w
ww
s'-
l Oi
*t
z
5'
s�
S'3
J'
PH
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date
Time end am, pm Date _/ /
Composite Sampling #2:
Time begin am, pm Date _/ /
Time end am, pm Date ,/_._/_
Time 'F! 641
Time
Time
Time
Lab Comments:
pm Date ( L/-L% Sampled by:
am, pm Date 6l Transported by:'
am, pm Date _IJ Holding times met:
am, pm Date /u!_
Compliance work:
Non-compliance Non-compliance work:
Samples Transported On Ice:
Initials:
n
tb
tb
eV
U
Z
N
N
00
tV
eV
X
O
Do
0
n

Land App ANL Volatile Solids In
Jan 2019
84,700
75,750
89.43
Feb 2019
65,600
61,650
93.98
Mar 2019
79,900
74,010
92.63
Apr 2019
69,867
66,400
95.04
May 2019P783,860
0
51,750
93.58
Jun 20190
48,600
91.78
Jul 20190
39,300
89.93
Aug 20190
45,050
87.82
Sep 20193
64,803
94.54
Oct 20190
85,450
93.64
Nov 20190
67,100
94.31
Dec 20190
47,200
95.16
Minimum00
39,300
Maximum50
85,450
Total
0
727,063
Average
65,3221
60,589
92.65

Volatile Solids Out
Volatile Solids IN average
% Reduction
6/3/19 North Basin
81.6
92.65
64.82
6/3/19 South Basin
75.9
92.65
75.02
6/19/19 North Basin
73.8
92.65
77.65
6/19/19 South Basin
68.60
92.65
82.67

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY20-SL001692
Client: Brent Collins Advisor:
vo- Predictive EMA Resources Inc
755 Yadkinville Rd
Mehlich-3 Extraction Mocksville, NC 27028
�1+= Soil Report
Links to Helpful Information Sampled County: Bladen
Client ID: 405413 Advisor ID:
Sampled: Received: 08/02/2019 Completed: 08/12/2019 Farm: NC-SF-03 (Steve Dunham)
Agronomist's Comments:
This report provides Test Results and Recommendations for each sample submitted for testing. Look for Lime Recommendations and N-P-K Fertilizer Recommendations.
The lime recommendation is always listed next to the first crop and will be based on the higher target pH if the pH targets for crop 1 and crop 2 differ. Application at the
indicated rate will raise soil pH to the optimal level for the plant you specified and should be sufficient for 2 to 3 years, depending on soil type. Common target pH values
are as follows: 5.0 for azalea, camellia, rhododendron and mt. laurel; 5.5 for centipedegrass; 6.0 for other lawn grasses, shrubbery, and; flowering plants; and 6.5 for
vegetable gardens. N-P-K Recommendations are based on the nitrogen (N) needs of the plants being grown and the soil test results for phosphorus (P-1) and potassium
(K-I); a 50 to 70 index for either is optimum. If the exact fertilizer cannot be found, find the closest match and adjust the rate accordingly. Refer to "Understanding the Soil
Report" last page of this report) for additional explanation and links to helpful information.
Sample ID: 00001
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 0 180 0 0 pH$ 0 0 0
Note: 12 Note:
2- 0.0
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP
SS -I NO3-N
0.46 1.36 7.6 95 0.4 6.8 346 22 85 9 36 75 50 1012 1012 255 0.1 1
Sample ID: 00002
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Bermuda hay/past., M 0.0 180-220 0 120 0 0 0 0 0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP
SS -I NO3-N
1.74 1.40 8.6 84 1.4 5.9 567 46 72 9 60 147 105 1821 1821 716 0.1 1
North Carolina
Tobww Trust Fw►d C47mmisslan
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY20-SL001692
Brent Collins
Page 2 of 3
Sample ID: 00003
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M
0.8
180-220 0
180
0
0
0
0 0
Note: 12
2-
0.0
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.36 1.38 3.9
66 1.3 5.1
535 24
54 10
43
117
87
1723
1723
567 0.1
3
Sample ID: 00005
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M
0.0
180-220 0
80
0
0
0
0
0 0
Note: 12
2-
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.60 1.35 6.3
85 1.0 6.0
449 65
66 13
47
93
73
1429
1429
639 0.1
2
Sample ID: 00006
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M
0.0
180-220 0
170
0
0
pH$
0
0 0
Note: 12 Note: $
2-
0.0
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.27 1.32 8.2
100 0.0 7.1
350 28
87 10
34
90
54
1608
1608
553 0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY20-SL001694
CU)-ToegPredictive Client: Brent Collins Advisor:
�C,
EMA Resources Inc
Mehlich-3 Extraction 755 Yadkinville Rd
Soil Report
b Mocksville, NC 27028
Links to Helpful Information Sampled: Not Provided
Sampled County: Bladen
Received: 08/02/2019
Farm: NC-SF-07 (JW Bernie) Completed: 08/12/2019 Client ID: 405413 Advisor ID:
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop
production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is
designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for
Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by
DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where
they become toxic to crops rown on a field.
Sample ID: 00001
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0 20 0 0 0 0 0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/do]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.32 1.08 14.7 93 1.0 6.5 231 68 62 29 54 240 154 1470 1470 923 0.1 1
Sample ID: 00006
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.9 120-200 0 20 0 0 0 Z 0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.56 1.11 9.4 81 1.8 5.4 446 68 67 10 55 139 100 2157 2157 756 0.1 1
North Carolina
x
AL
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SL001694
Brent Collins
Page 2 of 3
Sample ID: 00008
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.1
120-200 0
0
0
0
0
Z
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.36 1.12 8.8
78 2.0 5.2 787 134
59 11
69
134
97
3068
3068
1340 0.1 1
Sample ID: 00009
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.5
120-200 0
20
0
0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.32 1.14 6.7
81 1.2 5.6 441 63
64 13
46
106
81
1359
1359
497 0.1 1
Sample ID: 00014
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 0
120
0
0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/do]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.46 1.34 6.8
92 0.6 6.4 158 13
73 18
42
51
42
683
683
262 0.1 1

-,r,A6lJ -I}lds
Nutrien Ag Solutions, Inc.
a
LUMBERTON NC (280)
trien
INVOICE
PO BOX 807
A Solutions'
9
LUMBERTON, NC 28359
910-739-6993
Invoice #: 40590047
Invoice Date: 10J02�19
Due Date: Cash On Delivery
Delivery Date: 10/02/19
EMA RESOURCES (1419521)
Order #: 15506932
755 YADKINVILLE ROAD
PO#;
MOCKSVILLE, NC 27028
Sales Rep: Britt Jr, Bobby
Shin Via:
1000180759 - DOLOMITE BULK 202.3900 TN 50.0000 10,119.50
404780.0000 LB
1000189836 - TONNAGE TAX 1.0000 EA 101.1950 101.20
1000000077 - APPLICATION CHARGES /AC 202.3900 AC 8.0000 1,619.12
Safety Data Sheets are avaIIable upon request for appiicable products. Contact your IocaI branch for details. For a medical emergency
involving this product, tali 1-866-944-8565. For help with any spill, leak, fire or exposure, tall Chemtrec at 1-800-424-9300.
*** Invoice Notes ***
REL# 38599-1--8
John Deere Financing
Pay meal in fuIt is due and payable nn the 101h of the month fall awing the sta Iement date; for invoice amounts not paid by the 25th of the man th following the gtatemenI date, customer shall
also be liable for a late fee equal to four percent (4%) of the unpaid amount far purchases in !North CArolino and hfessissitlpi and lire percent (5%) in at her states; (6ij for inruite amonatS Mat
paid by the 21th of the month (oilnwing the statementdate, you shall also be liable for interest accrued an the unpaid balance at the highest rate allowable by law. I the event of any conflict
brtaeen thr trans of the invoice and the Customer Profile, the terms of the invoice shall can tral.
FRAUD ALERT — Our hank Informadon has NOT changed. Please immediately call [phone] and speak to a member of our Credit Department If you are asked to change bank
information. Again, DO NOT CHANGE OUR BANK REMITTANCE INFORMATION.
Payment Terms: IMMEDIATE Invoice Sub Total:
11,839.62
Sales Tax;
0.00
Invoice Total:
11,839.82
Less prepay Used:
0.00
Less Prepay Discount:
0.00
Gross Invoice Total,
11,839.82
Arnount Due:
11,839.82
Nutrien Ag Solutions, Inc.
1 of 1 PO BOX 807
LLJMBERTON, NC 28359

Nutrien Apf,olutions, Inc.
l •
+ IN trier
LUMBERTON NC (280)
INVOICE
PO sax 8117
A Solutions-
9
LUMBERTON, NC 28359
910-739-6993
Invoice At:
40590047
Invoice Date:
10/02119
Due Date:
Cash On Delivery
Delivery Date: IG/02J19
EMA RESOURCES (1419521)
Order #:
15506932PO#;
755 YADKINVILLE ROAD
Sales Rep:
Britt Jr, Bobby
MOCKSVILLE, NC 27028
Ship Via: Com n Vehicle County: DAVIE
--
�.:. .. ,.
Gross Unit
GrosS.t'".
.
Product # Product Description
Quantity
Price
Sales Tax
1000180759 - DOLOMITE BULK
202.3900
TN
50.0000
10,119.50
404780.0000
LB
1000189836 - TONNAGE TAX
1,0000
EA
101.1950
101.20
1000000077 - APPLICATION CHARGES /AC
202.3900
AC
8.0000
1,619.12
Safety Data Sheets are available upon request for applicable products. Contact your local branch for details. For a medical emergency
involving this product, call 1-866-944-8565. For help with any spill, leak, fire or exposure, call Chemtrec at 1-800-424-9300.
*** Invoice Notes ***
a- b,_4koM 1 T Orr
REL# 38599-1--8
]ohn Deere Financing
Paynicnt in full is Sue and payable on the IOth of the month following the statement date; for invoice amounts not Raid by the 25th of the month following the statement date, customer shall
also be liable for a late fee equal to four percent (4'%) of the unpaid amount fur purchases in North Carolina and Mississippi and five percent (51/4) in other states; (iii) for invoice amounts not
paid by the 2511t of the month following the statement date, you shall also be liable for interest accrued on the unpaid balance at the highest rate allowable by law. In the event of any conflict
bet«een the terms of the invoice and the Customer Profile, the terms of the invoice shall control.
FRAUD ALERT — Our bank information nas NOT changed. Please immediately call [phone] and Speak to a member of our Credit Department if you are asked to change bank
Informatirn. Again, DO NOT CHANGE OUR BANK REMn7ANCE INFORMATION.
Additional Infdrrnati6n' Payment Terms: IMMEDIATE Invoice Sub Total:
11,839.82
Sales Tax:
0.00
Invoice Total:
11,839.82
Less Prepay Used:
- 0.00
Less Prepay Discount:
0.00
Gross Invoice Total:
11,839.82
Amount Due:
11,639.82
Remit To:
Nutrien Ag Solutions, Inc.
1 of 1 PO BOX 807
LUMBERTON, NC 28359