WQ0039552_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:*
Project Number* WQ0039552
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0039552
Applicant\Permittee * Town of Mocksville
Facility Name * Town of Mocksville - WTP
Phone Number*
336-751-1441
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Mocksville WTP Annual Report -
2.8MB
WQ0039552. pdf
upload only 1 RJF docurrent. Miltiple docurrents rust be corrbined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/24/2020

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039552 FACILITY NAME: Town of Mocksville - Water Treatment Plant
PHONE: COUNTY: Davie OPERATOR: Town of Mocksville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
© Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ 10 If No skip parts A, B, C and certify form below
Part A*: Part B*:
Sources s Volume (dry tons)
Month O (include NPDES # if Amendment! Recipient Information
applicable) Residual In Product Out Name s
Bulking Agent Volume (dry tons) Intended use(s)
a
March
October
November
December
Total from FORM DMSDF (sup) 0 299.14 299.14 299.14
Totals: I Annual (dry tons): b 1 299.14 299.14 299.I4
Amendments used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) p
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No --► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. 1 am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for kno,&� violations."
Signature of Permittee Date Si t of Preparer** ate
fferent from Permittee)
**Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .I 102 (26)
DENR FORM DMSDF (1212006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0039552 FACILITY NAME: Town of Mocksville - Water Treatment Plant
PHONE: COUNTY: Davie OPERATOR: Town of Mocksville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
V Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume ( dry
tons)
Intended use(s)
June
Town of Mocksville WTP
18
18
Town of Mocksville
18
soil amendment
July
Town of Mocksville WTP
153.4
153.4
Town of Mocksville
153.4
soil amendment
July
Town of Mocksville WTP
19.38
19.38
Roger Spillman
19.38
soil amendment
August
Town of Mocksville WTP
84.48
84.48
Roger Spillman
84.48
soil amendment
August
Town of Mocksville WTP
23.88
23.88
Town of Mocksville
23.88
soil amendment
Totals:
Annual (dry tons):
0
299.14
299.14 299.14
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF -13
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Anah+sis Data
WQ0039552
Town of Mocksville - WTP
NCO230010
Mocksville WTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Cone.
Limit
m /k a
Sarrt le or Composite Date
719119
9/11119
# I
9/11/19
#2
9/11/19
93
Percent Solids (%)
NA
7.38
29
30
29.6
Arsenic
75
5.66
8.45
8.03
8.24
Cadmium
85
0.669
0.201
0.174
0.167
Copper
4,300
14.3
34
32
32.9
Chromium
NA
11.7
68.3
64
66.2
Lead
840
5.77
27.7
26.2
26.7
Mercury
57
0.0551
0.0524
0.0793
0.0794
Molybdenum
75
1.76
1.26
1.12
1.23
Nickel
420
5.64
29.9
28.1
29
Selenium
100
6.62
1.69
1.63
1.66
Zinc
7,500
36.4
92.4
89
90.5
Total Phosphorus
NA
551
1540
1450
1490
TKN
NA
2640
634
2390
905
Ammonia -Nitrogen
NA
I570
634
987
639
Nitrate and Nitrite
NA
61.1
17.2
15.7
1 14.7
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for su g false information, including the possibility of fines and imprisonment for knowing violations."
Sign of Preparer 17 to
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
RPsidunl Analvsk Data
WQ0039552
Town ofMocksville - WTP
NCO230010
Mocksville WTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
Sample or Composite Date
• •
a
a
--------
1--------
Calcium
®
' 1
®®--------
1:
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalti ors bmittiug false information, including the possibility of fines and imprisonment for knowing violations."
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12-12006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville-WTP Total Dry Tons Applied (Annual):
WQ0039552 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
21.8 Acres Permitted: 21.8 Site #: DV08 Field #:
103.86
CeB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
4.76
Arsenic
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.136
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.136
Chromiuni
0.111
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.111
Lead
0.055
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
denum
Nickel
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
Selenium
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Zinc
0.347
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.347
Total
Phos-
5.250
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.250
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Mocksville-WTP
Roger Spillman
Operator: Roger Spillman
WQ Permit #: WQ0039552 Field #:
Annual Dry Tons Applied: 103.86 Site #:
Predominant Soil Series: CeB2
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
209
Crop 2 Name:
Acres Utilized: 21.8
DV08 Acres Permitted: 21.8
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
(Dry,
Moist)
Precip.
Past 24
Hrs.
inches
>
c�c
m
* o
t�tj
c
?.
* �'
o
TKN
mg/kg
Z a
o
ac o
Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/31/19
63000
7.38
0.889
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
1.695
NA
Fescue
8/1/19
81000
7.38
1.143
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
2.180
NA
Fescue
8/2/19
54000
7.38
0.762
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
1.453
NA
Fescue
8/5/19
94500
7.38
1.334
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
2.543
NA
Fescue
8/6/19
1
45000
7.38
0.635
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
1.211
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
01
337500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
9.082
1 0.000
Lime Applied
Annuallbs/acre
0.054
0.006
0.136
0.111
0.055
0.001
0.017
0.054
0.063
0.347
5.250
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.054
0.006
0.136
0.111
0.055
0.001
0.017
0.054
0.063
0.347
Permitted C. P. L. R.****
36
34
1338
1
1 267
1 15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
I *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville-WTP Total Dry Tons Applied (Annual): 77.55
Permit #: WQ0039552 Cation Exchange Capacity (non 503 only):
Operator: Town of Mocksville Owner: Town of Mocksville Predominant Soil Series: CeB2
Acres Used: 4.7 Acres Permitted: 4.7 Site #: MK05 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
16.50
Arsenic
0.187
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.187
Cadmium
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Copper
0.472
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.472
Chromiuni
0.386
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.386
Lead
0.190
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.190
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
denum
Nickel
0.186
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.186
Selenium
0.218
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.218
Zinc
1.201
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.201
Total
Phos-
18.183
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
18.183
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Mocksville-WTP
Town of Mocksville
Operator: Town of Mocksville
WQ Permit #: WQ0039552 Field #:
Annual Dry Tons Applied: 77.55 Site #:
Predominant Soil Series: CeB2
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
209
Crop 2 Name:
Acres Utilized: 4.7
MK05 Acres Permitted: 4.7
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
50
o
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
(Dry,
Moist)
Precip.
Past 24
Hrs.
inches
>
c�c
m
* o
t�tj
c
?.
* �'
`q
o
TKN
mg/kg
Z a
o
ac o
Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/8/19
49500
7.38
3.241
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
6.178
NA
Fescue
7/9/19
40500
7.38
2.652
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
5.055
NA
Fescue
7/11/19
18000
7.38
1.179
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
2.247
NA
I Fescue
7/12/19
40500
7.38
2.652
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
5.055
NA
Fescue
7/15/19
1
9000
7.38
0.589
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
1.123
NA
Fescue
7/29/19
72000
7.38
4.714
Mocksville WTP
Dry
<.5"
S
0.5
1 0.1
2640
1570
1 61.1
8.987
NA
Fescue
7/31/19
22500
7.38
1.473
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
2.808
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4-0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
01
252000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
31.453
0.000
Lime Applied
Annuallbs/acre
0.187
0.022
0.472
0.386
0.190
0.002
0.058
0.186
0.218
1.201
18.183
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.187
0.022
0.472
0.386
0.190
0.002
0.058
0.186
0.218
1.201
Permitted C. P. L. R.****
36
1 34
1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
209 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
I *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville-WTP Total Dry Tons Applied (Annual):
WQ0039552 Cation Exchange Capacity (non 503 only):
Town of Mocksville Owner: Town of Mocksville Predominant Soil Series:
4 Acres Permitted: 4 Site #: MK05 Field #:
117.73
CfB2
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
7/9/19
2
Cake
Average
3
4
5
6
7
8
9
10 J
11
12
% Solids
1 7.38
29.53
Arsenic
5.66
8.24
Cadmium
0.669
0.18
Copper
14.3
32.97
Chromium
11.7
66.17
Lead
5.77
26.87
Mercury
0.0551
0.07
Molyb-
denum
1.76
1.2
Nickel
5.64
29
Selenium
6.62
1.66
Zinc
36.4
90.63
Total
Phos-
horns
551
1493.3
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
App.
Event
4.50
24.93
Arsenic
1 0.051
0.411
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.462
Cadmium
0.006
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
0.129
1.644
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.773
Chromium0.105
3.300
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.405
Lead
0.052
1.340
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.392
Mercury
0.000
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.016
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.076
denum
Nickel
0.051
1.446
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.497
Selenium
0.060
0.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.142
Zinc
0.328
4.519
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.847
Total
Phos-
4.960
74.463
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
79.424
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Mocksville-WTP
Town of Mocksville
Operator: Town of Mocksville
WQ Permit #: WQ0039552 Field #:
Annual Dry Tons Applied: 117.73 Site #:
Predominant Soil Series: CfB2
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
209
Crop 2 Name:
Acres Utilized: 4
MK05 Acres Permitted: 4
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
50
o
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
(Dry,
Moist)
Precip.
Past 24
Hrs.
inches
�
m
* o
c
?.
* �'
o
TKN
mg/kg
Z a
o
ac o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/17/19
36000
7.38
2.770
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
5.280
NA
Fescue
6/28/19
22500
7.38
1.731
Mocksville WTP
Dry
<.5"
S
0.5
0.1
2640
1570
61.1
3.300
NA
Fescue
7/22/19
125
29.53
7.772
Mocksville WTP
Dry
<.5"
S
0.5
0.1
1309.67
753.33
15.87
6.966
NA
Fescue
7/23/19
120
29.53
7.461
Mocksville WTP
Dry
<.5"
S
0.5
0.1
1309.67
753.33
15.87
6.687
NA
Fescue
7/24/19
1 60
29.53
3.730
Mocksville WTP
Dry
<.5"
S
0.5
0.1
1309.67
753.33
15.87
3.344
NA
Fescue
8/22/19
96
29.53
5.969
Mocksville WTP
Dry
<.5"
S
0.5
0.1
1 1309.67
753.33
1 15.87
5.350
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
401
58500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
30.926
0.000
Lime Applied
Annuallbs/acre
0.462
0.015
1.773
3.405
1.392
0.004
0.076
1.497
0.142
4.847
79.424
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.462
0.015
1.773
3.405
1.392
0.004
0.076
1.497
0.142
4.847
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
209 50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
I *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
7/19/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-191-0043
Client Project Description: Mocksville WTP
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 7/10/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 6

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville WTP
Lab Report Number: 19-191-0043
Date: 7/19/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 91921
Analyte: Arsenic
QC Batch No: L445687
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Iron
QC Batch No: L445687
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L445687
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 90815
Analyte: Mercury
QC Batch No: L444676
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 6

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Mocksville WTP Report Date : 07/19/2019
755 Yadkinville Rd Information : Received : 07/10/2019
Mocksville , NC 27028
Report Number : 19-191-0043 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 90666
Matrix: Solids
Sample ID : Mocksville WTP
Sampled:
7/9/2019
11:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
92.6
%
0.01
1
07/10/19 14:35
CJR
SW-DRYWT
Ammonia Nitrogen
1570
mg/Kg -
dry
338
1
07/19/19 11:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<61.1
mg/Kg -
dry
61.1
61.1
1
07/17/19 12:18
ZBD
4500NO3F-2011
Organic N
1070
mg/Kg -
dry
13.5
676
1
07/15/19 15:26
ACA
CALCULATION
pH
6.3
S.U.
1
07/18/19 07:21
JSL
9045D
Total Solids
7.38
%
0.010
0.010
1
07/10/19 14:35
CJR
2540G-2011
Total Volatile Solids
17.6
%
0.010
0.010
1
07/10/19 14:35
CJR
2540G-2011
Total Kjeldahl Nitrogen
2640
mg/Kg -
dry
676
1
07/15/19 15:26
CLP 4500NORGD-2011
Phosphorus
551
mg/Kg -
dry
34.7
67.6
1
07/17/19 22:14
BKN
6010D
Aluminum
15900
mg/Kg -
dry
27.4
67.6
1
07/17/19 22:14
JTR
6010D
Arsenic
<5.66
mg/Kg -
dry
5.66
6.76
1
07/17/19 22:14
BKN
6010D
Cadmium
<0.669
mg/Kg -
dry
0.669
1.35
1
07/17/19 22:14
BKN
6010D
Calcium
720
mg/Kg -
dry
227
338
1
07/17/19 22:14
BKN
6010D
Chromium
11.7
mg/Kg -
dry
2.57
3.38
1
07/17/19 22:14
BKN
6010D
Copper
14.3
mg/Kg -
dry
1.96
3.38
1
07/17/19 22:14
BKN
6010D
Iron
6850
mg/Kg -
dry
57.3
67.6
1
07/17/19 22:14
BKN
6010D
Lead
5.77
mg/Kg -
dry
2.01
4.05
1
07/17/19 22:14
BKN
6010D
Magnesium
708
mg/Kg -
dry
30.0
67.6
1
07/17/19 22:14
BKN
6010D
Manganese
211
mg/Kg -
dry
2.47
6.76
1
07/17/19 22:14
BKN
6010D
Mercury
0.05513
mg/Kg -
dry
0.0458
0.208
1
07/11/19 12:51
TJS
7471A
Molybdenum
<1.76
mg/Kg -
dry
1.76
3.38
1
07/17/19 22:14
BKN
6010D
Nickel
5.64
mg/Kg -
dry
2.23
3.38
1
07/17/19 22:14
BKN
6010D
Potassium
653
mg/Kg -
dry
40.3
67.6
1
07/17/19 22:14
BKN
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 6

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-191-0043
Lab No : 90666
Sample ID : Mocksville WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Mocksville WTP
Information :
REPORT OFANALYSIS
Report Date : 07/19/2019
Received : 07/10/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 7/9/2019 11:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<6.62
mg/Kg -
dry
6.62
6.76
1
07/17/19 22:14
BKN
6010D
Sodium
1503
mg/Kg -
dry
104
338
1
07/17/19 22:14
BKN
6010D
Zinc
36.4
mg/Kg -
dry
14.6
16.9
1
07/17/19 22:14
BKN
6010D
Sulfur
384
mg/Kg -
dry
66.1
67.6
1
07/17/19 22:14
BKN
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
07/17/19 22:14
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 4 of 6

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-191-0043
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T39
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
® No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ISovanchampa Yos Date & Time: 07/10/2019 09:26:29
Page 5 of 6

Client Name/Address
Client Project Manager/:
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksvllle. NC 27028
Project Description
Prole-A/Site Location Ki
Project Number
project Manager Phone i
336-399-3
Waypoin# (ly-
aNAz.YTKAL
179U LL'hav,p kuatl
-MvMPW' TIN M1.31
Unless noted, all rontam
[phone]
per Table li of d0 CFR Pa
13fi.
date
Time
Sample Identification
711
a:aS
/1
6110114 C.rtG Y-
'19
e:ns
Tug Yr��
7/9
ooks - it c- W TP
111111IIII!IlIII111III1I��III1111I
Hill 11I1111111IIIoEMA 25
201
Resuuroes lac
08-35-54
Grant Creek
I IIII IIII1� 111�111N1111 III
II1111�11111�1111 ICI fl o_
EMA Resources Inc 0024
Town Creek
Ice Custody Lab Comments
Seats
Y N
Y11--16
8lank/C ier emp

Waypointo
ANALYTICAL
9/26/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-255-0022
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 9/12/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015 VA NELAP #460181 Texas #T104704180 Arkansas #88-0650
Mississippi California #2904 NC #415 Oklahoma #9311 SC #84002
Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST #80215 PA DEP #68-03195
Page 1 of 10

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 19-255-0022
Date: 9/25/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L454349
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L454349
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L454188
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 92686 (Mockville WTP #3)
Analyte: Mercury
QC Batch No: 1-454094/1-453956
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 10

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Mocksville, NC Report Date : 09/26/2019
755 Yadkinville Rd Information : Received : 09/12/2019
Mocksville , NC 27028
Report Number : 19-255-0022 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92684
Matrix: Solids
Sample ID: Mockville WTP #1
Sampled:
9/11/2019
11:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
71.0
%
0.010
1
09/16/19 16:59
ADM
SW-DRYWT
Ammonia Nitrogen
634
mg/Kg -
dry
86.2
1
09/23/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<17.2
mg/Kg -
dry
17.2
17.2
1
09/23/19 14:13
ZBD
4500NO3F-2011
Organic N
<172
mg/Kg -
dry
172
1
09/23/19 15:00
CALCULATION
pH
6.2
S.U.
1
09/23/19 07:03
JSL
9045D
Total Solids
29.0
%
0.010
0.010
1
09/16/19 16:59
ADM
2540G-2011
Total Kjeldahl Nitrogen
634
mg/Kg -
dry
172
1
09/24/19 14:35
CLP 4500NORGD-2011
Phosphorus
1540
mg/Kg -
dry
8.86
17.2
1
09/13/19 21:53
JTR
6010D
Aluminum
91000
mg/Kg -
dry
70.0
172
10
09/17/19 14:05
BKN
6010D
Arsenic
8.45
mg/Kg -
dry
1.44
1.72
1
09/13/19 21:53
JTR
6010D
Cadmium
0.2013
mg/Kg -
dry
0.171
0.345
1
09/13/19 21:53
JTR
6010D
Calcium
1260
mg/Kg -
dry
57.9
86.2
1
09/13/19 21:53
JTR
6010D
Chromium
68.3
mg/Kg -
dry
0.655
0.862
1
09/13/19 21:53
JTR
6010D
Copper
34.0
mg/Kg -
dry
0.500
0.862
1
09/13/19 21:53
JTR
6010D
Iron
42400
mg/Kg -
dry
146
172
10
09/17/19 14:05
BKN
6010D
Lead
27.7
mg/Kg -
dry
0.513
1.03
1
09/13/19 21:53
JTR
6010D
Magnesium
4140
mg/Kg -
dry
7.66
17.2
1
09/13/19 21:53
JTR
6010D
Manganese
693
mg/Kg -
dry
0.631
1.72
1
09/13/19 21:53
JTR
6010D
Mercury
0.05243
mg/Kg -
dry
0.0118
0.0534
1
09/16/19 12:14
TJS
7471A
Molybdenum
1.26
mg/Kg -
dry
0.448
0.862
1
09/13/19 21:53
JTR
6010D
Nickel
29.9
mg/Kg -
dry
0.568
0.862
1
09/13/19 21:53
JTR
6010D
Potassium
2830
mg/Kg -
dry
10.3
17.2
1
09/13/19 21:53
JTR
6010D
Selenium
<1.69
mg/Kg -
dry
1.69
1.72
1
09/13/19 21:53
JTR
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 10

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-255-0022
Lab No : 92684
Sample ID: Mockville WTP #1
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Mocksville, NC
Information :
REPORT OFANALYSIS
Report Date : 09/26/2019
Received : 09/12/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 11:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Sodium
90.0
mg/Kg - dry
26.6
86.2
1
09/13/19 21:53
JTR
6010D
Zinc
92.4
mg/Kg - dry
3.72
4.31
1
09/13/19 21:53
JTR
6010D
Sulfur
1310
mg/Kg - dry
16.9
17.2
1
09/13/19 21:53
JTR
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
09/13/19 21:53
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 4 of 10

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-255-0022
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
t45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ICarleen Qualls Date & Time: 09/12/2019 08:31:49
Page 9 of 10

Client Name/Address
Client Project Manager/Contact
Billing IRformatlOtt
For laboratory Use Only
EMA Resources Inc
great Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Desrription
Project/Site Location (City/State)
17RUSH— Additional charges apply
Special Detection Limit($)
Mel of Shipment
Fed Ex
Matrix Key
u
��
�U oGKs y� ��,
Date Results
UPS DUSPS
HClientDropOff
WW —Wastewater GW — Groundwater
/�
o
Needed
ElCourier
DW — Drinking Water S —Svll /Solid 0— oil
r�
P - Product M - Misc
�J L—
(/_
Other
Project Number
Project Manager Phone p
Project Manager Email
Purchase Order Number
Site/Facility ID it
336-399-3646
[e-mail]
td Z uj
A Coal [ TOC Na25203 (Micro only}
r
0 U -0
8 sc
Waypoint
ANALYTICAL
Y(3
Y
r >`
E E 0
Cn
4H�
C 142S H2So4 p2
O None Required
2790 Whitten Road
-�'
E
` O
Cr N Q
W
E NaOH pFlalO
F "NO3 pH<2
Memphis, TN W33
Unless noted, all containers � V
c [4 Z m �
� > f �
v
C HCL PW2
[phone]
per Table II of 40 CFR Part a x
a u] }_ Q
0- 0
H H3PC4 pHc2
136.
Identification z
1—
Required Analysis
I Cool c- 6C NAZS203
Date
Time
Sample
JYPreservative
Camments/Notes
/jLMOD
Hi Noa<'sZ'Jr�q -0
Metals:Al,A.�;,Ca,Cd,_Qr,C�r,Fe,Pb
itIq
/1 r
In V0C/Csi/C[CC �cl Tip
I
(,
✓
Mn,M
,Mo.Hg,Ni,Se,Na,P,S,K,Zn
I�
1
µ" /LGCx IC �/lf1CL- rr'
U
I I{Il{1 III { I� I {{I{Illy { III I II 11{lit I II I II I1111I111 lilt 46246 92
EMAResources Inc 08:30.35
Mocksville, NC
For
Laboratory Use Only
Sa d by IName — Print]
�,C�Sludge
Client Remarks/Cornments
Samples - Report Dry Weight
r�
CSaiy
Wm
bComentsO
Ly')/ N
y/ke
l
D to Time
Received hy: [SIGNAT`UREj
Ti
bate me
i
Blank/ ler T
Relinquished by: [SIGNATURE]
Date rime
Received by: (SIGNATURE[
Date Time
Relinquished by: (SIGNATUAEj
Date Time
Re v [SIGNATURE] f7
Date Ti
"[

Waypointo
ANALYTICAL
9/26/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-255-0022
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 9/12/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015 VA NELAP #460181 Texas #T104704180 Arkansas #88-0650
Mississippi California #2904 NC #415 Oklahoma #9311 SC #84002
Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST #80215 PA DEP #68-03195
Page 1 of 10

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 19-255-0022
Date: 9/25/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L454349
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L454349
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L454188
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 92686 (Mockville WTP #3)
Analyte: Mercury
QC Batch No: 1-454094/1-453956
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 10

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Mocksville, NC Report Date : 09/26/2019
755 Yadkinville Rd Information : Received : 09/12/2019
Mocksville , NC 27028
Report Number : 19-255-0022 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92685
Matrix: Solids
Sample ID: Mockville WTP #2
Sampled:
9/11/2019
11:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
70.0
%
0.010
1
09/16/19 16:59
ADM
SW-DRYWT
Ammonia Nitrogen
987
mg/Kg -
dry
83.3
1
09/23/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<15.7
mg/Kg -
dry
15.7
15.7
1
09/23/19 14:15
ZBD
4500NO3F-2011
Organic N
1400
mg/Kg -
dry
185
1
09/23/19 15:00
CALCULATION
pH
6.1
S.U.
1
09/23/19 07:03
JSL
9045D
Total Solids
30.0
%
0.010
0.010
1
09/16/19 16:59
ADM
2540G-2011
Total Kjeldahl Nitrogen
2390
mg/Kg -
dry
185
1
09/25/19 17:37
CLP 4500NORGD-2011
Phosphorus
1450
mg/Kg -
dry
8.57
16.7
1
09/13/19 21:58
JTR
6010D
Aluminum
84700
mg/Kg -
dry
67.7
167
10
09/17/19 14:10
BKN
6010D
Arsenic
8.03
mg/Kg -
dry
1.40
1.67
1
09/13/19 21:58
JTR
6010D
Cadmium
0.1743
mg/Kg -
dry
0.165
0.333
1
09/13/19 21:58
JTR
6010D
Calcium
1170
mg/Kg -
dry
56.0
83.3
1
09/13/19 21:58
JTR
6010D
Chromium
64.0
mg/Kg -
dry
0.633
0.833
1
09/13/19 21:58
JTR
6010D
Copper
32.0
mg/Kg -
dry
0.483
0.833
1
09/13/19 21:58
JTR
6010D
Iron
38000
mg/Kg -
dry
141
167
10
09/17/19 14:10
BKN
6010D
Lead
26.2
mg/Kg -
dry
0.496
1.00
1
09/13/19 21:58
JTR
6010D
Magnesium
3800
mg/Kg -
dry
7.40
16.7
1
09/13/19 21:58
JTR
6010D
Manganese
577
mg/Kg -
dry
0.610
1.67
1
09/13/19 21:58
JTR
6010D
Mercury
0.0793
mg/Kg -
dry
0.0116
0.0527
1
09/16/19 12:16
TJS
7471A
Molybdenum
1.12
mg/Kg -
dry
0.433
0.833
1
09/13/19 21:58
JTR
6010D
Nickel
28.1
mg/Kg -
dry
0.550
0.833
1
09/13/19 21:58
JTR
6010D
Potassium
2560
mg/Kg -
dry
9.93
16.7
1
09/13/19 21:58
JTR
6010D
Selenium
<1.63
mg/Kg -
dry
1.63
1.67
1
09/13/19 21:58
JTR
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 10

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-255-0022
Lab No : 92685
Sample ID: Mockville WTP #2
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Mocksville, NC
Information :
REPORT OFANALYSIS
Report Date : 09/26/2019
Received : 09/12/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 11:15
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Sodium
86.3
mg/Kg - dry
25.7
83.3
1
09/13/19 21:58
JTR
6010D
Zinc
89.0
mg/Kg - dry
3.60
4.17
1
09/13/19 21:58
JTR
6010D
Sulfur
1120
mg/Kg - dry
16.3
16.7
1
09/13/19 21:58
JTR
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
09/13/19 21:58
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 6 of 10

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-255-0022
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
t45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ICarleen Qualls Date & Time: 09/12/2019 08:31:49
Page 9 of 10

Client Name/Address
Client Project Manager/Contact
Billing IRformatlOtt
For laboratory Use Only
EMA Resources Inc
great Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Desrription
Project/Site Location (City/State)
17RUSH— Additional charges apply
Special Detection Limit($)
Mel of Shipment
Fed Ex
Matrix Key
u
��
�U oGKs y� ��,
Date Results
UPS DUSPS
HClientDropOff
WW —Wastewater GW — Groundwater
/�
o
Needed
ElCourier
DW — Drinking Water S —Svll /Solid 0— oil
r�
P - Product M - Misc
�J L—
(/_
Other
Project Number
Project Manager Phone p
Project Manager Email
Purchase Order Number
Site/Facility ID it
336-399-3646
[e-mail]
td Z uj
A Coal [ TOC Na25203 (Micro only}
r
0 U -0
8 sc
Waypoint
ANALYTICAL
Y(3
Y
r >`
E E 0
Cn
4H�
C 142S H2So4 p2
O None Required
2790 Whitten Road
-�'
E
` O
Cr N Q
W
E NaOH pFlalO
F "NO3 pH<2
Memphis, TN W33
Unless noted, all containers � V
c [4 Z m �
� > f �
v
C HCL PW2
[phone]
per Table II of 40 CFR Part a x
a u] }_ Q
0- 0
H H3PC4 pHc2
136.
Identification z
1—
Required Analysis
I Cool c- 6C NAZS203
Date
Time
Sample
JYPreservative
Camments/Notes
/jLMOD
Hi Noa<'sZ'Jr�q -0
Metals:Al,A.�;,Ca,Cd,_Qr,C�r,Fe,Pb
itIq
/1 r
In V0C/Csi/C[CC �cl Tip
I
(,
✓
Mn,M
,Mo.Hg,Ni,Se,Na,P,S,K,Zn
I�
1
µ" /LGCx IC �/lf1CL- rr'
U
I I{Il{1 III { I� I {{I{Illy { III I II 11{lit I II I II I1111I111 lilt 46246 92
EMAResources Inc 08:30.35
Mocksville, NC
For
Laboratory Use Only
Sa d by IName — Print]
�,C�Sludge
Client Remarks/Cornments
Samples - Report Dry Weight
r�
CSaiy
Wm
bComentsO
Ly')/ N
y/ke
l
D to Time
Received hy: [SIGNAT`UREj
Ti
bate me
i
Blank/ ler T
Relinquished by: [SIGNATURE]
Date rime
Received by: (SIGNATURE[
Date Time
Relinquished by: (SIGNATUAEj
Date Time
Re v [SIGNATURE] f7
Date Ti
"[

Waypointo
ANALYTICAL
9/26/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-255-0022
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 9/12/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015 VA NELAP #460181 Texas #T104704180 Arkansas #88-0650
Mississippi California #2904 NC #415 Oklahoma #9311 SC #84002
Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST #80215 PA DEP #68-03195
Page 1 of 10

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 19-255-0022
Date: 9/25/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L454349
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L454349
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L454188
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 92686 (Mockville WTP #3)
Analyte: Mercury
QC Batch No: 1-454094/1-453956
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 10

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Mocksville, NC Report Date : 09/26/2019
755 Yadkinville Rd Information : Received : 09/12/2019
Mocksville , NC 27028
Report Number : 19-255-0022 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92686
Matrix: Solids
Sample ID: Mockville WTP #3
Sampled:
9/11/2019
11:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
70.4
%
0.010
1
09/16/19 16:59
ADM
SW-DRYWT
Ammonia Nitrogen
639
mg/Kg -
dry
84.5
1
09/23/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<14.7
mg/Kg -
dry
14.7
14.7
1
09/23/19 14:16
ZBD
4500NO3F-2011
Organic N
267
mg/Kg -
dry
169
1
09/23/19 15:00
CALCULATION
pH
6.0
S.U.
1
09/23/19 07:03
JSL
9045D
Total Solids
29.6
%
0.010
0.010
1
09/16/19 16:59
ADM
2540G-2011
Total Kjeldahl Nitrogen
905
mg/Kg -
dry
169
1
09/24/19 14:39
CLP 4500NORGD-2011
Phosphorus
1490
mg/Kg -
dry
8.68
16.9
1
09/13/19 22:03
JTR
6010D
Aluminum
87200
mg/Kg -
dry
68.6
169
10
09/17/19 14:15
BKN
6010D
Arsenic
8.24
mg/Kg -
dry
1.42
1.69
1
09/13/19 22:03
JTR
6010D
Cadmium
<0.167
mg/Kg -
dry
0.167
0.338
1
09/13/19 22:03
JTR
6010D
Calcium
1210
mg/Kg -
dry
56.8
84.5
1
09/13/19 22:03
JTR
6010D
Chromium
66.2
mg/Kg -
dry
0.641
0.844
1
09/13/19 22:03
JTR
6010D
Copper
32.9
mg/Kg -
dry
0.490
0.845
1
09/13/19 22:03
JTR
6010D
Iron
39200
mg/Kg -
dry
143
169
10
09/17/19 14:15
BKN
6010D
Lead
26.7
mg/Kg -
dry
0.503
1.01
1
09/13/19 22:03
JTR
6010D
Magnesium
3950
mg/Kg -
dry
7.50
16.9
1
09/13/19 22:03
JTR
6010D
Manganese
588
mg/Kg -
dry
0.618
1.69
1
09/13/19 22:03
JTR
6010D
Mercury
0.0794
mg/Kg -
dry
0.0117
0.0530
1
09/16/19 12:17
TJS
7471A
Molybdenum
1.23
mg/Kg -
dry
0.439
0.844
1
09/13/19 22:03
JTR
6010D
Nickel
29.0
mg/Kg -
dry
0.557
0.844
1
09/13/19 22:03
JTR
6010D
Potassium
2720
mg/Kg -
dry
10.1
16.9
1
09/13/19 22:03
JTR
6010D
Selenium
<1.66
mg/Kg -
dry
1.66
1.69
1
09/13/19 22:03
JTR
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 7 of 10

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-255-0022
Lab No : 92686
Sample ID: Mockville WTP #3
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Mocksville, NC
Information :
REPORT OFANALYSIS
Report Date : 09/26/2019
Received : 09/12/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 11:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Sodium
81.13
mg/Kg - dry
26.1
84.5
1
09/13/19 22:03
JTR
6010D
Zinc
90.5
mg/Kg - dry
3.65
4.22
1
09/13/19 22:03
JTR
6010D
Sulfur
1260
mg/Kg - dry
16.5
16.9
1
09/13/19 22:03
JTR
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
09/13/19 22:03
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 8 of 10

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-255-0022
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
t45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ICarleen Qualls Date & Time: 09/12/2019 08:31:49
Page 9 of 10

Client Name/Address
Client Project Manager/Contact
Billing IRformatlOtt
For laboratory Use Only
EMA Resources Inc
great Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Desrription
Project/Site Location (City/State)
17RUSH— Additional charges apply
Special Detection Limit($)
Mel of Shipment
Fed Ex
Matrix Key
u
��
�U oGKs y� ��,
Date Results
UPS DUSPS
HClientDropOff
WW —Wastewater GW — Groundwater
/�
o
Needed
ElCourier
DW — Drinking Water S —Svll /Solid 0— oil
r�
P - Product M - Misc
�J L—
(/_
Other
Project Number
Project Manager Phone p
Project Manager Email
Purchase Order Number
Site/Facility ID it
336-399-3646
[e-mail]
td Z uj
A Coal [ TOC Na25203 (Micro only}
r
0 U -0
8 sc
Waypoint
ANALYTICAL
Y(3
Y
r >`
E E 0
Cn
4H�
C 142S H2So4 p2
O None Required
2790 Whitten Road
-�'
E
` O
Cr N Q
W
E NaOH pFlalO
F "NO3 pH<2
Memphis, TN W33
Unless noted, all containers � V
c [4 Z m �
� > f �
v
C HCL PW2
[phone]
per Table II of 40 CFR Part a x
a u] }_ Q
0- 0
H H3PC4 pHc2
136.
Identification z
1—
Required Analysis
I Cool c- 6C NAZS203
Date
Time
Sample
JYPreservative
Camments/Notes
/jLMOD
Hi Noa<'sZ'Jr�q -0
Metals:Al,A.�;,Ca,Cd,_Qr,C�r,Fe,Pb
itIq
/1 r
In V0C/Csi/C[CC �cl Tip
I
(,
✓
Mn,M
,Mo.Hg,Ni,Se,Na,P,S,K,Zn
I�
1
µ" /LGCx IC �/lf1CL- rr'
U
I I{Il{1 III { I� I {{I{Illy { III I II 11{lit I II I II I1111I111 lilt 46246 92
EMAResources Inc 08:30.35
Mocksville, NC
For
Laboratory Use Only
Sa d by IName — Print]
�,C�Sludge
Client Remarks/Cornments
Samples - Report Dry Weight
r�
CSaiy
Wm
bComentsO
Ly')/ N
y/ke
l
D to Time
Received hy: [SIGNAT`UREj
Ti
bate me
i
Blank/ ler T
Relinquished by: [SIGNATURE]
Date rime
Received by: (SIGNATURE[
Date Time
Relinquished by: (SIGNATUAEj
Date Time
Re v [SIGNATURE] f7
Date Ti
"[

aceAnalytical
National Center for Testing & Innovation
>r
ANALYTICAL REPORT
July 18, 2019
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
L1117219
07/10/2019
Town of Mocksville
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
Is performed per guidance provided in laboratory standard operating procedures:060302, 060303,and 060304.
In.
4
AP- IMMEMW "Op
M
FC
FS
Fn
Fr
FC
HGI
[Al]
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 1 of 23

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
MOCKSVILLE WTP L1117219-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
9
10
11
12
13
15
17
18
19
21
22
23
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1117219 07/13/19 20:27
PAGE:
2 of 23

MOCKSVILLE WTP L1117219-01 Waste
SAMPLE
SUMMARY
Collected by
Roy Whitaker
Collected date/time
07/09/19 07:30
ONE LAB. NATIONWIDE.
Received date/time
07/10/19 08:45
FP
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
F
Preparation by Method 1311
WG1309661
1 07/11/191101
07/11/191101
RT
Mt. Juliet, TN
Preparation by Method 1311
WG1309763
1 07/11/1912:53
07/11/1912:53
RT
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1311886
1 07/16/1913:05
07/16/19 2114
JER
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1312588
1 07/17/1917:18
07/17/1917:18
BAM
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1310691
1 07/15/1912:40
07/15/1914:57
AJC
Mt. Juliet, TN
Fn
Wet Chemistry by Method D93/1010A
WG1312546
1 07/17/191135
07/17/191135
EDA
Mt. Juliet, TN
Mercury by Method 7470A
WG1310359
1 07/12/1910:46
07/14/19 2124
TCT
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1311007
1 07/15/1914:59
07/16/19 04:48
CCE
Mt. Juliet, TN
Fr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1310508
1 07/13/1917:13
07/13/1917:13
BMB
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1311320
1 07/15/19 08:53
07/16/19 05:25
LEL
Mt. Juliet, TN
FC
Pesticides (GC) by Method 8081B
WG1311227
1 07/17/19 00:24
07/17/1910:34
LEL
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1311226
1 07/15/1917:18
07/17/1912:59
AO
Mt. Juliet, TN
GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1117219
07/13/19
20:27
3 of 23

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 4 of 23

MOCKSVILLE WTP
Collected date/time: 07/09/19 07:30
Preparation by Method 1311
SAMPLE RESULTS - 01
L1117219
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
7/11/201912:53:22 PM
WG1309763
TCLP ZHE Extraction -
7/11/2019110127 AM
WG1309661
Fluid 1
7/11/201912:53:22 PM
WG1309763
Initial pH 6.54
7/11/201912:53:22 PM
WG1309763
Final pH 4.94
7/11/201912:53:22 PM
WG1309763
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
07/16/2019 2114
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Batch
WG1311886
Dilution Analysis Batch
date / time
1 07/17/201917:18 WG1312588
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 6.75 T8 1 07/15/201914:57 WG1310691
Sample Narrative:
L1117219-01 WG1310691: 6.75 at 25.1C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis
Analyte Deg. F date / time
Ignitability DNI at170 1 07/17/20191135
Mercury by Method 7470A
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
0.271
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Batch
WG1312546
Dilution Analysis Batch
date / time
1 07/14/2019 2124 WG1310359
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 07/16/2019 04:48
WG1311007
1 07/16/2019 04:48
WG1311007
1 07/16/2019 04:48
WG1311007
1 07/16/2019 04:48
WG1311007
1 07/16/2019 04:48
WG1311007
1 07/16/2019 04:48
WG1311007
1 07/16/2019 04:48
WG1311007
Dilution Analysis
Batch
date / time
1 07/13/201917:13
WG1310508
1 07/13/201917:13
WG1310508
1 07/13/201917:13
WG1310508
1 07/13/201917:13
WG1310508
SDG:
DATE/TIME: PAGE:
L1117219
07/13/19 20:27 5 of 23

MOCKSVILLE WTP SAMPLE RESULTS
Collected date/time: 07/09/19 07:30 L1117219
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
07/13/201917:13
WG1310508
1,1-Dichloroethene
ND
0.0500 0.70 1
07/13/201917:13
WG1310508
2-Butanone (MEK)
ND
0.500 200 1
07/13/201917:13
WG1310508
Tetrachloroethene
ND
0.0500 0.70 1
07/13/201917:13
WG1310508
Trichloroethene
ND
0.0500 0.50 1
07/13/201917:13
WG1310508
Vinyl chloride
ND
0.0500 0.20 1
07/13/201917:13
WG1310508
(S) Toluene-dH
107
80.0-120
071131201917.13
WG1310508
(S) 4-Bromofluorobenzene
104
77.0-126
071131201917.13
WG1310508
(S) 1,2-Dichloroethane-d4
106
70.0-130
071131201917.13
WG1310508
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) Z4-Dichlorophenyl Acetic Acid 63.8
Pesticides (GC) by Method 8081B
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 07/16/2019 05:25
WG1311320
0.00200
10
1 07/16/2019 05:25
WG1311320
14.0-158
0711612019 05.25
WG1311320
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 07/17/201910:34
WG1311227
Endrin
ND
0.00500
0.02
1 07/17/201910:34
WG1311227
Heptachlor
ND
0.00500
0.0080
1 07/17/201910:34
WG1311227
Lindane
ND
0.00500
0.40
1 07/17/201910:34
WG1311227
Methoxychlor
ND
0.00500
10
1 07/17/201910:34
WG1311227
Toxaphene
ND
0.0100
0.50
1 07/17/201910:34
WG1311227
(S) Decochlorobiphenyl
89.6
10.0-128
071171201910.34
WG1311227
(S) Tetrochloro-m-xylene
56.3
10.0-127
071171201910.34
WG1311227
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4, 6-Tribromophenol
(S) p-Terphenyl-d14
ACCOUNT:
EMA Resources
ONE LAB. NATIONWIDE.
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 07/17/201912:59
WG1311226
ND
0.100
0.13
1 07/17/201912:59
WG1311226
ND
0.100
0.13
1 07/17/201912:59
WG1311226
ND
0.100
0.50
1 07/17/201912:59
WG1311226
ND
0.100
3
1 07/17/201912:59
WG1311226
ND
0.100
2
1 07/17/201912:59
WG1311226
ND
J4 0.100
5
1 07/17/201912:59
WG1311226
ND
0.100
400
1 07/17/201912:59
WG1311226
ND
0.100
200
1 07/17/201912:59
WG1311226
ND
0.100
100
1 07/17/201912:59
WG1311226
ND
0.100
400
1 07/17/201912:59
WG1311226
ND
0.100
2
1 07/17/201912:59
WG1311226
24.9
10.0-120
071171201912.59
WG1311226
15.3
10.0-120
071171201912.59
WG1311226
43.4
10.0-127
071171201912.59
WG1311226
36.1
10.0-130
071171201912.59
WG1311226
55.0
10.0-155
071171201912.59
WG1311226
62.5
10.0-128
071171201912.59
WG1311226
PROJECT:
SDG:
DATE/TIME: PAGE:
L1117219
07/13/19 20:27 6 of 23

WG1311886 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1117219-01
Method Blank (MB)
(MB) R3431249-1 07/16/19 20:43
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1116587-10 Original Sample (OS) • Duplicate (DUP)
(OS) L1116537-10 07/16/19 20:55 • (DUP) R3431249-3 07/16/19 20:56
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg
Reactive Cyanide 0.122 0.165 1 30.1 J P1 20
L1117182-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1117132-01 07/16/19 2112 • (DUP) R3431249-3 07/16/19 2131
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide 0.364 0.498 1 31.2 P1 20
Laboratory Control Sample (LCS)
(LCS) R3431249-2 07/16/19 20:49
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.54 102
Rec. Limits LCS Qualifier
50.0-150
L1116587-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
F—P
ITC]
FS-1
[Cn]
Fr
�GI
1711
Fc
(OS) L1116537-13 07/16/19 2101 • (MS) R3431249-4 07/16/19 2102 • (MSD) R3431249-5 07/16/19 2103
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 3.11 U 1.46 1.66 47.1 53.5 1 75.0-125 J6 J6 12.7 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 7 of 23

WG1311886 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1117219-01
L1117641-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1117641-01 07/16/19 2115 • (MS) R3431249-6 07/16/19 2116 • (MSD) R3431249-7 07/16/19 2117
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 0.592 0.350 29.5 15.1 1 75.0-125 J6
ONE LAB. NATIONWIDE. *
MSD Qualifier RPD RPD Limits
J3 J6 51.2 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 3 of 23

WG1312588
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3431639-1 07/17/191713
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1115683-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1117219-01
(OS) L1115633-02 07/17/191713 • (DUP) R3431639-3 07/17/191713
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide 90.4 89.5 1 0.978 20
L1116137-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1116137-02 07/17/19 1713 • (DUP) R3431639-4 07/17/191713
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3431639-2 07/17/19 1718
Spike Amount LCS Result
Analyte mg/kg mg/kg
Reactive Sulfide 100 96.9
LCS Rec. Rec. Limits LCS Qualifier
96.9 70.0-130
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 9 of 23

WG1310691
Wet Chemistry by Method 9045D
L1118135-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1113135-04 07/15/19 14:57 • (DUP) R3430729-3 07/15/19 14:57
Original Result DUP Result Dilution DUP RPD
Analyte su su
Corrosivity by pH 9.29 9.31 1 0.215
Sample Narrative:
OS: 9.29 at23.6C
DUP:9.31 at23.7C
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1117219-01
DUP Qualifier DUP RPD
Limits
(LCS) R3430729-1 07/15/19 14:57
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.96 99.6 99.0-101
Sample Narrative:
LCS: 9.96 at 22AC
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 10 of 23

WG1312546
Wet Chemistry by Method D93/1010A
L1117219-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1117219-01 07/17/191135 • (DUP) R3431453-2 07/17/191135
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000
L1118726-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1117219-01
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1113726-01 07/17/19 1135 • (DUP) R3431453-3 07/17/19 1135
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability 90.7 88.7 1 2.23 10
Laboratory Control Sample (LCS)
(LCS) R3431458-1 07/17/19 1135
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 81.7 99.6 96.0-104
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 11 of 23

WG1310359 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1117219-01
Method Blank (MB)
(MB) R3430466-1 07/14/19 2050
MB Result MB Qualifier
MB MDL MB RDL
Analyte mg/I
mg/I mg/I
Mercury U
0.00330 0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3430466-2 07/14/19 20:53 • (LCSD) R3430466-3 07/14/19 20:55
Spike Amount LCS Result
LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I
mg/I
Mercury 0.0300 0.0267
0.0285 89.1 95.0 80.0-120 6.42 20
L1116770-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1116770-01 07/14/19 20:57 • (MS) R3430466-4 07/14/19 2100 • (MSD) R3430466-5 07/14/19 2102
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0273
0.0269 91.1 89.7 1 75.0-125 1.61 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
SAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 12 of 23

WG1311007
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3430339-1 07/16/19 0440
QUALITY CONTROL SUMMARY
L1117219-01
ONE LAB. NATIONWIDE. *
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Arsenic U 0.0333 0.100
Barium U 0.0333 0.100
Cadmium U 0.0333 0.100
Chromium U 0.0333 0.100
Lead U 0.0333 0.100
Selenium U 0.0333 0.100
Silver U 0.0333 0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3430339-2 07/16/19 04:42 • (LCSD) R3430339-3 07/16/19 04:45
Spike Amount LCS Result LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte mg/I mg/I mg/I
Arsenic 10.0 9.98 10.1 99.8
101
80.0-120
1.15
20
Barium 10.0 10.5 10.6 105
106
80.0-120
1.16
20
Cadmium 10.0 10.3 10.4 103
104
80.0-120
1.16
20
Chromium 10.0 9.81 9.97 98.1
99.7
80.0-120
1.57
20
Lead 10.0 9.93 10.0 99.3
100
80.0-120
0.917
20
Selenium 10.0 10.2 10.2 102
102
80.0-120
0.348
20
Silver 2.00 1.86 1.88 93.1
94.2
80.0-120
1.21
20
L1117219-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate
(MSD)
(OS) L1117219-01 07/16/19 04:43 • (MS) R3430339-5 07/16/19 04:53 • (MSD) R3430339-6 07/16/19 04:56
Spike Amount Original Result MS Result MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier
MSD Qualifier
RPD
RPD Limits
Analyte mg/I mg/I mg/I mg/I
Arsenic 10.0 ND 10.0 10.2
100
102
1 75.0-125
1.60
20
Barium 10.0 0.271 10.8 10.9
105
107
1 75.0-125
1.13
20
Cadmium 10.0 ND 10.4 10.5
104
105
1 75.0-125
1.16
20
Chromium 10.0 ND 9.92 9.96
99.2
99.6
1 75.0-125
0.430
20
Lead 10.0 ND 10.1 10.1
101
101
1 75.0-125
0.828
20
Selenium 10.0 ND 10.3 10.4
103
104
1 75.0-125
1.46
20
Silver 2.00 ND 1.88 1.90
94.1
94.8
1 75.0-125
0.704
20
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 13 of 23

WG1311007 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1117219-01
L1117903-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1117903-01 07/16/19 04:59 • (MS) R3430339-7 07/16/19 05:02 • (MSD) R3430339-3 07/16/19 05:04
Spike Amount
Original Result
MS Result
MSD Result MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
U
9.83
9.99 98.3
99.9
1 75.0-125
1.62
20
Barium
10.0
U
10.7
10.8 106
107
1 75.0-125
1.32
20
Cadmium
10.0
U
10.2
10.4 102
104
1 75.0-125
1.16
20
Chromium
10.0
U
9.87
9.94 98.7
99.4
1 75.0-125
0.658
20
Lead
10.0
U
9.89
9.99 98.9
99.9
1 75.0-125
1.02
20
Selenium
10.0
U
9.90
10.1 99.0
101
1 75.0-125
1.77
20
Silver
2.00
U
1.85
1.87 92.6
93.3
1 75.0-125
0.698
20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1117219
07/13/19 20:27
14 of 23

WG1310508 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1117219-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3430375-3 07/13/19 12:43
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-d8
107
80.0-120
(S) 4-Bromofluorobenzene
104
77.0-126
(S) 1,2-Dichloroethane-d4
106
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3430375-1 07/13/1910:00 • (LCSD) R3430375-2 07/13/1910:21
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.0250
0.0257
0.0257
103
103
70.0-123
Carbon tetrachloride
0.0250
0.0307
0.0307
123
123
68.0-126
Chlorobenzene
0.0250
0.0261
0.0255
104
102
80.0-121
Chloroform
0.0250
0.0261
0.0260
105
104
73.0-120
1,2-Dichloroethane
0.0250
0.0261
0.0257
104
103
70.0-128
1,1-Dichloroethene
0.0250
0.0293
0.0287
117
115
71.0-124
2-Butanone (MEK)
0.125
0.173
0.171
138
137
44.0-160
Tetrachloroethene
0.0250
0.0270
0.0269
108
108
72.0-132
Trichloroethene
0.0250
0.0254
0.0250
102
100
78.0-124
Vinyl chloride
0.0250
0.0287
0.0285
115
114
67.0-131
(S) Toluene-d8
108
105
80.0-120
(S) 4-Bromofluorobenzene
107
104
77.0-126
(S) 1,2-Dichloroethane-d4
107
108
70.0-130
LCS Qualifier
LCSD Qualifier RPD
0.0299
0.143
2.01
0.626
1.52
2.22
0.849
0.182
1.67
0.734
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 15 of 23

WG1310508 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1117219-01
L1117085-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1117035-01 07/13/19 17:35 • (MS) R3430375-4 07/13/19 17:57 • (MSD) R3430375-5 07/13/19 18:13
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Benzene 1.25
2.77
6.40
6.44
72.8
73.4
4
17.0-158
0.488
27
Carbon tetrachloride 1.25
ND
4.22
3.88
84.5
77.6
4
23.0-159
8.41
28
Chlorobenzene 1.25
ND
4.22
4.10
84.5
81.9
4
33.0-152
3.11
27
Chloroform 1.25
ND
4.03
3.88
80.6
77.5
4
29.0-154
3.85
28
1,2-Dichloroethane 1.25
ND
4.15
4.32
83.0
86.4
4
29.0-151
4.01
27
1,1-Dichloroethene 1.25
ND
3.46
3.20
69.3
63.9
4
11.0-160
8.02
29
2-Butanone (MEK) 6.25
ND
23.2
24.1
92.8
96.4
4
10.0-160
3.82
32
Tetrachloroethene 1.25
ND
3.73
3.43
74.6
68.6
4
10.0-160
8.38
27
Trichloroethene 1.25
ND
3.58
3.40
71.7
68.0
4
10.0-160
5.31
25
Vinyl chloride 1.25
ND
2.95
2.72
58.9
54.5
4
10.0-160
7.88
27
(S) Toluene-d8
107
107
80.0-120
(S) 4-Bromofluorobenzene
101
106
77.0-126
(S) 1,2-Dichloroethane-d4
108
110
70.0-130
Sample Narrative:
OS: Non -target compounds too high to run at
a lower dilution.
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1117219
07/13/19 20:27
16 of 23

WG1311320
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3430905-1 07/16/19 0404
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) Z4-Dichlorophenyl Acetic 61.8
Acid
QUALITY CONTROL SUMMARY
L1117219-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3430905-2 07/16/19 04:13
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
2,4,5-TP (Silvex) 0.0500 0.0465 93.0 50.0-125
2,4-D 0.0500 0.0439 87.8 50.0-120
(S) Z4-Dichlorophenyl Acetic 83.2 14. 0-158
Acid
L1116697-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1116697-01 07/16/19 04:31 • (MS) R3430905-3 07/16/19 04:45 • (MSD) R3430905-4 07/16/19 04:53
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
2,4,5-TP (Silvex)
0.0500
ND
0.0514
0.0448
103
89.6
1 50.0-125
13.7
20
2,4-D
0.0500
ND
0.0491
0.0419
98.2
83.8
1 50.0-120
15.8
20
(S) Z4-Dichlorophenyl Acetic
100
74.6
14.0-158
Acid
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 17 of 23

WG1311227
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1117219-01
(MB) R3431409-2 07/17/19 09:44
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
92.7
10.0-128
(S) Tetrochloro-m-xylene
63.9
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3431409-1 07/17/19 09:32
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00856
85.6
55.0-129
Endrin
0.0100
0.00923
92.3
57.0-134
Heptachlor
0.0100
0.00889
88.9
27.0-132
Methoxychlor
0.0100
0.00917
91.7
54.0-155
(S) Decachlorobiphenyl
92.9
10.0-128
(S) Tetrochloro-m-xylene
76.0
10.0-127
L1117150-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1117150-01 07/17/19 09:57 • (MS) R3431409-3 07/17/19 10:09 • (MSD) R3431409-4 07/17/19 10:22
Spike Amount
Original Result
MS Result
MSD Result MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Gamma BHC 0.0100
ND
0.00934
0.00953 93.4
95.3
1 14.0-141
2.01
40
Endrin 0.0100
ND
0.0105
0.0113 105
113
1 10.0-160
7.34
39
Heptachlor 0.0100
ND
0.0101
0.0104 101
104
1 16.0-136
2.93
40
Methoxychlor 0.0100
ND
0.0107
0.0107 107
107
1 10.0-160
0.000
34
(S) Decachlorobiphenyl
96.5
101
10.0-128
(S) Tetrochloro-m-xylene
71.6
79.7
10.0-127
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1117219
07/13/19 20:27
13 of 23

WG1311226 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1117219-01
Method Blank (MB)
(MB) R3431459-2 07/17/19 0143
MB Result
Analyte
mg/I
1,4-Dichlorobenzene
U
2,4-Dinitrotoluene
U
Hexachlorobenzene
U
Hexachloro-1,3-butadiene
U
Hexachloroethane
U
Nitrobenzene
U
Pyridine
U
2-Methylphenol
U
3&4-Methyl Phenol
U
Pentachlorophenol
U
2,4,5-Trichlorophenol
U
2,4,6-Trichlorophenol
U
(S) Nitrobenzene-d5
44.8
(S) 2-Fluorobiphenyl
43.1
(S) p-Terphenyl-d14
55.3
(S) Phenol-d5
170
(S) 2-Fluorophenol
30.5
(S) Z4, 6-Tribromophenol 50.0
MB Qualifier
Laboratory Control Sample (LCS)
MB MDL
mg/I
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
10.0-127
10.0-130
10.0-128
10.0-120
10.0-120
10.0-155
(LCS) R3431459-1 07/17/19 0127
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
1,4-Dichlorobenzene
0.500
0.199
39.8
18.0-120
2,4-Dinitrotoluene
0.500
0.333
66.6
49.0-124
Hexachlorobenzene
0.500
0.293
58.6
44.0-120
Hexachloro-1,3-butadiene
0.500
0.156
31.2
19.0-120
Hexachloroethane
0.500
0.167
33.4
15.0-120
Nitrobenzene
0.500
0.242
48.4
27.0-120
Pyridine
0.500
0.0164
3.28
10.0-120 J4
2-Methylphenol
0.500
0.220
44.0
28.0-120
3&4-Methyl Phenol
0.500
0.237
47.4
31.0-120
Pentachlorophenol
0.500
0.324
64.8
23.0-120
2,4,5-Trichlorophenol
0.500
0.303
60.6
44.0-120
2,4,6-Trichlorophenol
0.500
0.310
62.0
42.0-120
(S) Nitrobenzene-d5
58.4
10.0-127
(S) 2-Fluorobiphenyl
48.7
10.0-130
(S) p-Terphenyl-d14
60.3
10.0-128
ACCOUNT:
PROJECT:
EMA Resources
SDG: DATE/TIME: PAGE:
L1117219 07/13/19 20:27 19 of 23

WG1311226 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1117219-01
Laboratory Control Sample (LCS)
(LCS) R3431459-1 07/17/19 0127
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 19.4 10.0-120
(S) 2-Fluorophenol 30.2 10.0-120
(S) 2,4, 6-Tribromophenol 58.0 10. 0-155
L1115673-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1115673-03 07/17/19 02:54 • (MS) R3431459-3 07/17/19 0316 • (MSD) R3431459-4 07/17/19 03:33
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.191
0.200
38.2
40.0
2,4-Dinitrotoluene
0.500
ND
0.338
0.346
67.6
69.2
Hexachlorobenzene
0.500
ND
0.269
0.291
53.8
58.2
HexachIoro-1,3-butadiene
0.500
ND
0.144
0.149
28.8
29.8
Hexachloroethane
0.500
ND
0.160
0.172
32.0
34.4
Nitrobenzene
0.500
ND
0.431
0.432
86.2
86.4
Pyridine
0.500
ND
0.0654
ND
13.1
0.000
2-Methylphenol
0.500
ND
0.0509
0.0586
10.2
11.7
3&4-Methyl Phenol
0.500
ND
ND
0.0359
0.000
7.18
Pentachlorophenol
0.500
ND
0.310
0.326
62.0
65.2
2,4,5-Trichlorophenol
0.500
ND
0.273
0.293
54.6
58.6
2,4,6-Trichlorophenol
0.500
ND
0.269
0.294
53.8
58.8
(S) Nitrobenzene-d5
59.2
63.1
(S) 2-Fluorobiphenyl
46.3
49.8
(S) p-Terphenyl-d14
62.5
64.7
(S) Phenol-d5
0.000
0.000
(S) 2-Fluorophenol
25.5
4.06
(S)2,4,6-Tribromophenol
47.4
49.8
Sample Narrative:
OS: Low surrogate recovery due to matrix interference
Dilution Rec. Limits
MS Qualifier MSD Qualifier
RPD
1 17.0-120
4.60
1 39.0-125
2.34
1 35.0-122
7.86
1 12.0-120
3.41
1 10.0-120
7.23
1 12.0-120
0.232
1 10.0-120
J3 J6
200
1 10.0-120
14.1
1 10.0-120
J6 J3 J6
200
1 10.0-128
5.03
1 33.0-120
7.07
1 26.0-120
8.88
10.0-127
10.0-130
10.0-128
10.0-120
J2 J2
10.0-120
J2
10.0-155
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1117219 07/13/19 20:27 20 of 23

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
and Definitions
u
FcAbbreviations
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
FS
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
Fn
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Fr
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate, used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
Fc
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
SAI
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
R
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J2
Surrogate recovery limits have been exceeded, values are outside lower control limits.
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1117219 07/13/19 20:27 21 of 23

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1117219 07/13/19 20:27 22 of 23

Billing Information: I
Analysis
/
Container
/ Preservative
Chain of Custody Page Cf AL
EMA Resources
755 Yadkinville Road
Mr. Brent Collins Pres
755 Yadkinville Road ' chk1!
Mocksville, NC 27028
aCeAnaIr ical ®
- Hatfmm! CersLer 7nrT 11np 8 Enrnrs�7�
Mocksville, NC 27028
12065 Leb1anon Rd
Phone: [phone]Phone:2
Report t0:
Mr. Brent Collins
Email To: brent. col lins@em aresou rcesinc.com
Fax: 6180s59 esRSg
Project
Description:
`v
O
City/State
Collected: �j%d S, -&(
V `-``
y
L #
H1 2!3
Phone:[phone]
Client Project #
Lab Project ii,"<
Fax, 336-751-1442
0Prelogin:
Z
U
e
d
o
S
L
�
Ll
LJ
Colle (prin
o�
Site/Facility ID P
P.O. #
Acctnum: EMARES
Template:711413
P689631
TSR: 702 - Cassandra Foster
` E
PB• l
Collected (Sig at e):
mmediately (Z�--
Packed on Ice N _ Y Y/
Rush? {Lab MUST Be Notified) Quote #
Same Day _ Five Day
Next Day _ 5 Day (Rad only) Date Results Needed
_ Two Day to Day {Rad Only} No.
T Three Day Qf
Shipped Via: FedEX Ground
Sample ID
Comp/Grab
Matrix"
Depth
Date
Time
ntrs
Remarks Sam plea (lab only)
�OCY6`CC
Ss
?
2
V
A
J�
CJ
I
i
I
i
-t I
Matrix:Remarks: R w c` ist
SS - Soil AIR - Air IF- Filter pH Temp COC seal Present /Intact: _oP _Y N
GW- Groundwater B- Bioassa CCC Signed/Accurate: �Y _N
Y Bottles arrive intact: _Y _N
WW - Wastewater Flow Other Correct bottles used: r Y _N
DW Drinking Water Samples retu ed Via: Sufficient volume sent: . Y _N
/!_
Oi Other U S edEx Courier _ hacking # Il�pplicable
i 7 r, Q t� t� VOA zero Heads ace! Y
_N
Relinquish by ign u } Date: Time. Receive (Signature) Trip Blank Received; Ye No Preservation Correct/Checked:— N
7 11 9 M HCL Meol-i W SCREEN: <0.5 mMr
TBR
Relin ish b ignature]
Date:
Time,
Received by: (Signature)
Temp: �C Battles Received:
If preservation required by Login; Date/Time
Relinquls y : (Signature)
Date:
Time:
Received for lab by: (Signature)
Dat Time:
Hold:
Conditio `,,
NCI / pK