WQ0032723_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:*
Project Number* WQ0032723
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0032723
Phone Number*
336-751-1441
Applicant\Permittee * City of Reidsville Water Treatment Plant
Facility Name * Reidsville WTP
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Reidsville WTP Annual Report -
2.2MB
WQ0032723. pdf
upload only 1 RJF docurrent. Miltiple docurrents rust be corrbined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/24/2020

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0032723 FACILITY NAME: Reidsville WTP
PHONE: COUNTY: Rockingham OPERATOR: City of Reidsville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑p Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ --* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Names)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
August
September
October
November
December
Total from FORM DMSDF (sup)
0
109.82
109.82
109,82
Totals:
I Annual dry tons):
0
109.82
109.82
109.82
Amendment(s) used:
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)l 0
Facility was compliant during the past calendar year with all conditions of the land application permit 21 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No o If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer* *
(if different from Permittee)
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0032723 FACILITY NAME: City of Reidsville WTP
PHONE: COUNTY: Rockingham OPERATOR: City of Reidsville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
V Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume ( dry
tons)
Intended use(s)
October
City of Reidsville WTP
9.64
9.64
Michael Bray
9.64
Soil Amendment
October
City of Reidsville WTP
6.41
6.41
Lofton Lovelace
6.41
Soil Amendment
November
City of Reidsville WTP
57.16
57.16
Ronnie Marshall
57.16
Soil Amendment
November
City of Reidsville WTP
17.98
17.98
Lofton Lovelace
17.98
Soil Amendment
November
City of Reidsville WTP
18.63
18.63
State of North Carolina
18.63
Soil Amendment
Totals:
Annual (dry tons):
0
109.82
109.82 109.82
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
RPeirival AnAvyic data
WQ0032723
Reidsville WTP
NCO046345
Reidsville WTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
Limit
CompositeConc. Sample or
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
_ _..'W - d 3 "4plb�
Signature of Preparer
* Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Bate
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0032723
Laboratory: 1)
Facility Name:
Reidsville WTP
2)
Residual Source
NCO046345
3)
NPDES # or WQ4:
4)
WWTP Name:
Reidsville WTP
5)
Residual Analysis Data
Waypoint Analytical
Parameter
(mg/kg!
CompositeSample or Date
--------t--
' f f 1
-----------
Magnesium
. t
--_--------
------------
------------
"I Certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C• � 1 -4' A�k 0 -;�� -�-Vj-�b
Signature of Preparer *
*Preparer is defined in 40
Part 503.4(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual):
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
50.09
Operator: Ronnie Marshall Owner: Ronnie Marshall Predominant Soil Series: CgB2
Acres Used: 69 Acres Permitted: 69 Site #: RC001 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.73
Arsenic
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.173
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.173
Chromiuni
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Lead
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
denum
Nickel
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Selenium
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Zinc
0.114
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.114
Total
Phos-
2.193
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.193
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP
Ronnie Marshall
Operator: Ronnie Marshall
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0032723 Field #:
Annual Dry Tons Applied: 50.09 Site #:
Predominant Soil Series: CgB2
Crop 1 Max. PAN:
209 Crop 2 Name:
Acres Utilized: 69
RC001 Acres Permitted: 69
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>o
cc
� �
*
?.
* �'
o'
7� q
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/15
52000
2.37
0.074
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
1.055
NA
Fescue
11/16
162500
2.37
0.233
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
3.298
NA
Fescue
11/17
110500
2.37
0.158
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
2.242
NA
Fescue
11/18
39000
2.37
0.056
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
0.791
NA
Fescue
11/20
52000
2.37
0.074
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
1.055
NA
Fescue
11/21
91000
2.37
0.130
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
1.847
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
10.288
0.000
Lime Applied
Annuallbs/acre
0.025 0.003 0.173 0.047 0.029 0.000 0.008 0.026 0.030 0.114 2.193
o 0 0 0 0 0 0 0 0 0
0.025 0.003 0.173 0.047 0.029 0.000 0.008 0.026 0.030 0.114
36 1 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498
1 209
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****1
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual): 7.07
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
Operator: Ronnie Marshall Owner: Ronnie Marshall Predominant Soil Series: CgB2
Acres Used: 18.9 Acres Permitted: 18.9 Site #: RC001 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
01111m
mammon
Non
no
0
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
0.37
Arsenic
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.089
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Chromium
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Lead
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
denum
Nickel
0.013
0.000
0.000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.013
Selenium
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.015
Zinc
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Total
Phos-
1.129
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.129
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP
Ronnie Marshall
Operator: Ronnie Marshall
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0032723 Field #:
Annual Dry Tons Applied: 7.07 Site #:
Predominant Soil Series: CgB2
Crop 1 Max. PAN:
209 Crop 2 Name:
Acres Utilized: 18.9
RC001 Acres Permitted: 18.9
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>o
cc
� �
*
?.
* �'
o'
7� q
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/21
32500
2.37
0.170
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
2.408
NA
Fescue
11/22
39000
2.37
0.204
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
2.889
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
o
71500
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
5.297
0.000
Lime App lied
Annuallbs/acre
0.013 0.002 0.089 0.024 0.015 0.000 0.004 0.013 0.015 0.059 1.129 1
o 0 0 0 0 0 0 0 0 0
0.013 0.002 0.089 0.024 0.015 0.000 0.004 0.013 0.015 0.059
36 34 1339 267 15 374 89 2498
1 209
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual):
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
9.64
Operator: Auman French Owner: Michael Bray Predominant Soil Series: CgB2
Acres Used: 6.1 Acres Permitted: 6.1 Site #: RC009 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.58
Arsenic
0.055
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.376
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.376
Chromiuni
0.102
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.102
Lead
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
denum
Nickel
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Selenium
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
Zinc
0.247
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.247
Total
Phos-
4.772
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.772
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP
Michael Bray
Operator: Auman French
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0032723 Field #:
Annual Dry Tons Applied: 9.64 Site #:
Predominant Soil Series: CgB2
Crop 1 Max. PAN:
209 Crop 2 Name:
Acres Utilized: 6.1
RC009 Acres Permitted: 6.1
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>o
� �
*
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/28
58500
2.37
0.948
Reidsviile WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
13.428
NA
Fescue
10/29
39000
2.37
0.632
Reidsviile WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
8.952
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
22.380
0.000
Lime Applied
Annuallbs/acre
0.055
0.007
0.376
0.102
0.063
0.000
0.017
0.056
0.064
0.247 4.772
0
0.247
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
o
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.055
0.007
0.376
0.102
0.063
0.000
0.017
0.056
0.064
Permitted C. P. L. R.****1
36
1 34
1 1338
1
267
15
1
1 374
89
Permit PAN Limit 1 st/2nd Crop
1
1 209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Reidsville - WTP Total Dry Tons Applied (Annual):
WQ0032723 Cation Exchange Capacity (non 503 only):
Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series:
11.6 Acres Permitted: 11.6 Site #: RC041 Field #:
3.85
CaD
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
0.33
Arsenic
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.079
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.079
Chromiuni
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Lead
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
denum
Nickel
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.012
Selenium
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Zinc
0.052
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
Total
Phos-
1.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.003
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP WQ Permit #: WQ0032723 Field #: 1 Acres Utilized:
Lofton Lovelace Annual Dry Tons Applied: 3.85 Site #: RC041 Acres Permitted:
Donald Lovelace
Crop 1 Name: Fescue -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 150
CaD
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
11.6
11.6
0
o
Volume applied
(enter one) Solids/
Liquid
q
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 �
� �
*
o
* �'
o'
p
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/29
39000
2.37
0.332
Reidsviile WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
4.708
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
01
39000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
4.708
0.000
Lime Applied
Annuallbs/acre
0.012 0.001 0.079 0.021 0.013 0.000 0.004 0.012 0.014 0.052 1.003
0 0 0 0 0 0 0 0 0 0
0.012 0.001 0.079 0.021 0.013 0.000 0.004 0.012 0.014 0.052
36 34 1338 1 267 1 15 374 89 2498
150
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual):
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
20.56
Operator: Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series: CgB2
Acres Used: 19.4 Acres Permitted: 19.4 Site #: RC041 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.06
Arsenic
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.252
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.252
Chromiuni
0.068
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.068
Lead
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
denum
Nickel
0.038
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
Selenium
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Zinc
0.166
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.166
Total
Phos-
3.201
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.201
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP
Lofton Lovelace
Operator: Donald Lovelace
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0032723 Field #:
Annual Dry Tons Applied: 20.56 Site #:
Predominant Soil Series: CgB2
Crop 1 Max. PAN:
209 Crop 2 Name:
Acres Utilized: 19.4
RC041 Acres Permitted: 19.4
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>o
� �
*
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
10/29
26000
2.37
0.132
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
1.877
NA
Fescue
11/5
130000
2.37
0.662
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
9.383
NA
Fescue
11/6
52000
2.37
0.265
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
3.753
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
2oa000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
15.013
0.000
Lime Applied
Annuallbs/acre
0.037
0.004
0.252
0.068
0.042
0.000
0.011
0.038
0.043
0.166 3.201
0
0.166
2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
o
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.037
0.004
0.252
0.068
0.042
0.000
0.011
0.038
0.043
Permitted C. P. L. R.****1
36
34
1 1339
267
15
374
1 89
Permit PAN Limit 1 st/2nd Crop
1
1 209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Reidsville - WTP Total Dry Tons Applied (Annual): 18.63
Permit #: WQ0032723 Cation Exchange Capacity (non 503 only):
Operator: Auman French Owner: State of N.C. Predominant Soil Series: CgB2
Acres Used: 34 Acres Permitted: 34 Site #: RC126 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
01111110MB
NONE
Non
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
0.55
Arsenic
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.130
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.130
Chromiuni
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Lead
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
denum
Nickel
0.019
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.019
Selenium
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Zinc
0.086
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
Total
Phos-
1.655
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.655
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP
State of N.C.
Operator: Auman French
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0032723 Field #:
Annual Dry Tons Applied: 18.63 Site #:
Predominant Soil Series: CgB2
Crop 1 Max. PAN:
209 Crop 2 Name:
Acres Utilized: 34
RC126 Acres Permitted: 34
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
q
Cu. Yds Gallons
78000
%
Solids
2.37
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>o
� �
*
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
11/6
0.227
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
3.212
NA
Fescue
11/7
110500
2.37
0.321
Reidsville WTP
Dry
<.5"
S
0.5
0.1
7580
15300
206
4.551
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
01
188500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
7.763
0.000
Lime Applied
Annuallbs/acre
0.019 0.002 0.130 0.035 0.022 0.000 0.006 0.019 0.022 0.086 1.655
0 0 0 0 0 0 0 0 0 0
0.019 0.002 0.130 0.035 0.022 0.000 0.006 0.019 0.022 0.086
36 34 1 1338 267 15 1 1 374 89 1 2498
209
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
11/12/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-305-0043
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 11/1/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 19-305-0043
Date: 11 /12/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 88456 (Reidsville WTP)
Analyte: Aluminum
QC Batch No: 1-462710/1-462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: 1-462710/1-462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: 1-462710/1-462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Cadmium
QC Batch No: 1-462710/1-462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Chromium
QC Batch No: 1-462710/1-462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Copper
QC Batch No: 1-462710/1-462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Iron
QC Batch No: 1-462710/1-462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 2 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Analyte: Potassium
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Magnesium
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Molybdenum
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sodium
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Nickel
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Phosphorus
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Lead
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sulfur
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 8

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Analyte: Selenium
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Zinc
QC Batch No: L462710/L462297
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Reidsville, NC Report Date : 11/12/2019
755 Yadkinville Rd Information : Received : 11/01/2019
Mocksville , NC 27028
Report Number : 19-305-0043 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 88456
Matrix: Solids
Sample ID : Reidsville WTP
Sampled:
10/31/2019
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.6
%
0.010
1
11/05/1916:31
ADM
SW-DRYWT
Ammonia Nitrogen
15300
mg/Kg -
dry
1040
1
11/12/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<206
mg/Kg -
dry
206
206
1
11/06/19 14:24
ZBD
4500NO3F-2011
pH
6.9
S.U.
1
11/11/19 06:22
JSL
9045D
Total Solids
2.37
%
0.010
0.010
1
11/05/19 16:31
ADM
2540G-2011
Total Kjeldahl Nitrogen
7580
mg/Kg -
dry
60.0
2990
1
11/12/19 15:37
CLP 4500NORGD-2011
Phosphorus
1510
mg/Kg -
dry
107
208
1
11/05/19 20:28
KKM
6010D
Aluminum
139000
mg/Kg -
dry
84.6
208
1
11/05/19 20:28
KKM
6010D
Arsenic
<17.5
mg/Kg -
dry
17.5
20.8
1
11/05/19 20:28
KKM
6010D
Cadmium
<2.06
mg/Kg -
dry
2.06
4.17
1
11/05/19 20:28
KKM
6010D
Calcium
1880
mg/Kg -
dry
700
1040
1
11/05/19 20:28
KKM
6010D
Chromium
32.3
mg/Kg -
dry
7.92
10.4
1
11/05/19 20:28
KKM
6010D
Copper
119
mg/Kg -
dry
6.04
10.4
1
11/05/19 20:28
KKM
6010D
Iron
31600
mg/Kg -
dry
177
208
1
11/05/19 20:28
KKM
6010D
Lead
19.9
mg/Kg -
dry
6.21
12.5
1
11/05/19 20:28
KKM
6010D
Magnesium
1670
mg/Kg -
dry
92.5
208
1
11/05/19 20:28
KKM
6010D
Manganese
8580
mg/Kg -
dry
7.63
20.8
1
11/05/19 20:28
KKM
6010D
Mercury
<0.139
mg/Kg -
dry
0.139
0.629
1
11/06/19 14:56
TJS
7471A
Molybdenum
<5.42
mg/Kg -
dry
5.42
10.4
1
11/05/19 20:28
KKM
6010D
Nickel
17.7
mg/Kg -
dry
6.88
10.4
1
11/05/19 20:28
KKM
6010D
Potassium
1480
mg/Kg -
dry
124
208
1
11/05/19 20:28
KKM
6010D
Selenium
<20.4
mg/Kg -
dry
20.4
20.8
1
11/05/19 20:28
KKM
6010D
Sodium
6883
mg/Kg -
dry
322
1040
1
11/05/19 20:28
KKM
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-305-0043
Lab No : 88456
Sample ID : Reidsville WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Reidsville, NC
Information :
REPORT OFANALYSIS
Report Date : 11/12/2019
Received : 11/01/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 10/31/2019 8:30
Test
Results
Units
MDL
MQL
DF Date / Time By
Analytical
Analyzed
Method
Zinc
78.3
mg/Kg - dry
45.0
52.1
1 11/05/19 20:28 KKM
6010D
Sulfur
4050
mg/Kg - dry
204
208
1 11/05/19 20:28 KKM
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1 11/05/19 20:28
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 6 of 8

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-305-0043
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
-7
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ISovanchampa Yos Date & Time: 11/01/2019 09:47:11
Page 7 of 8

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aceAnalytical
National Center for Testing & Innovation
AW
ANALYTICAL REPORT
November 20, 2019
EMA Resources
Sample Delivery Group: L1158315
Samples Received: 11/07/2019
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
JJwkC4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 1 of 21

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
REIDSVILLE WTP L1158315-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
9
Wet Chemistry by Method 9045D
10
FC
Wet Chemistry by Method D93/1010A
11
F
Mercury by Method 7470A
12
Metals (ICP) by Method 6010D
13
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
14
Chlorinated Acid Herbicides (GC) by Method 8151A
15
RC
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1153315
11/20/19 09:46 2 of 21

M
SAMPLE SUMMARY
Collected by
REIDSVILLE WTP L1158315-01 Waste Brent Collins
ONE LAB. NATIONWIDE. *
Collected date/time Received date/time
11/06/191130 11/07/19 08:30
Cp
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
Preparation by Method 1311
WG1379675
1 11/13/19 09:44
11/13/19 09:44
BAA
Preparation by Method 1311
WG1380782
1 11/14/19 20:04
11/14/19 20:04
CGD
Wet Chemistry by Method 9012 B
WG1380017
1 11/14/19 08:00
11/14/1914:02
SDL
Wet Chemistry by Method 9034-9030B
WG1379886
1 11/13/19 2100
11/13/19 2100
LDT
Wet Chemistry by Method 9045D
WG1378591
1 11/11/1917:22
11/11/1919:42
ANP
Wet Chemistry by Method D93/1010A
WG1379769
1 11/14/19 00:49
11/14/19 00:49
JD
Mercury by Method 7470A
WG1380253
1 11/14/19 07:22
11/14/191136
ABL
Metals (ICP) by Method 6010D
WG1380258
1 11/14/191112
11/14/1915:20
TRB
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1382386
1 11/19/1915:19
11/19/1915:19
JHH
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1381552
1 11/16/1912:29
11/17/1919:15
RP
Pesticides (GC) by Method 8081B
WG1381559
1 11/16/19 06:12
11/18/1917:38
MT-1
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1381303
1 11/15/1915:55
11/16/1916:43
AO
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1153315 11/20/19 09:46
PAGE:
3 of 21

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 4 of 21

REIDSVILLE WTP
Collected date/time: 11/06/19 11:30
Preparation by Method 1311
SAMPLE RESULTS - 01
L1158315
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
11/13/2019 9:44:58 AM
WG1379675
TCLP ZHE Extraction -
11/14/2019 8:04:45 PM
WG1380782
Fluid 1
11/13/2019 9:44:58 AM
WG1379675
Initial pH 6.83
11/13/2019 9:44:58 AM
WG1379675
Final pH 4.97
11/13/2019 9:44:58 AM
WG1379675
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
11/14/201914:02
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Batch
WG1380017
Dilution Analysis Batch
date / time
1 11/13/2019 2100 WG1379886
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.07 T8 1 11/11/201919:42 WG1378591
Sample Narrative:
L1158315-01 WG1378591: 7.07 at 20AC
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date / time
Ignitability DNI at170 1 11/14/2019 00:49 WG1379769
Mercury by Method 7470A
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
0.279
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
0.277
B 0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Dilution Analysis Batch
date / time
1 11/14/20191136 WG1380253
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 11/14/201915:20
WG1380258
1 11/14/201915:20
WG1380258
1 11/14/201915:20
WG1380258
1 11/14/201915:20
WG1380258
1 11/14/201915:20
WG1380258
1 11/14/201915:20
WG1380258
1 11/14/201915:20
WG1380258
Dilution Analysis
Batch
date / time
1 11/19/201915:19
WG1382386
1 11/19/201915:19
WG1382386
1 11/19/201915:19
WG1382386
1 11/19/201915:19
WG1382386
SDG:
DATE/TIME: PAGE:
L1153315
11/20/19 09:46 5 of 21

REIDSVILLE WTP SAMPLE RESULTS
Collected date/time: 11/06/19 11:30 L1158315
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
11/19/201915:19
WG1382386
1,1-Dichloroethene
ND
0.0500 0.70 1
11/19/201915:19
WG1382386
2-Butanone (MEK)
ND
0.500 200 1
11/19/201915:19
WG1382386
Tetrachloroethene
ND
0.0500 0.70 1
11/19/201915:19
WG1382386
Trichloroethene
ND
0.0500 0.50 1
11/19/201915:19
WG1382386
Vinyl chloride
ND
0.0500 0.20 1
11/19/201915:19
WG1382386
(S) Toluene-dH
97.5
80.0-120
111191201915.19
WG1382386
(S) 4-Bromofluorobenzene
101
77.0-126
111191201915.19
WG1382386
(S) 1,2-Dichloroethane-d4
97.0
70.0-130
111191201915.19
WG1382386
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) Z4-Dichlorophenyl Acetic Acid 50.2
Pesticides (GC) by Method 8081B
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 11/17/20191915
WG1381552
0.00200
10
1 11/17/201919:15
WG1381552
14.0-158
111171201919.15
WG1381552
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 11/18/201917:38
WG1381559
Endrin
ND
0.00500
0.02
1 11/18/201917:38
WG1381559
Heptachlor
ND
0.00500
0.0080
1 11/18/201917:38
WG1381559
Lindane
ND
0.00500
0.40
1 11/18/201917:38
WG1381559
Methoxychlor
ND
0.00500
10
1 11/18/201917:38
WG1381559
Toxaphene
ND
0.0100
0.50
1 11/18/201917:38
WG1381559
(S) Decochlorobiphenyl
88.7
10.0-128
11118120191738
WG1381559
(S) Tetrochloro-m-xylene
74.6
10.0-127
11118120191738
WG1381559
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4, 6-Tribromophenol
(S) p-Terphenyl-d14
ACCOUNT:
EMA Resources
ONE LAB. NATIONWIDE.
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 11/16/201916:43
WG1381303
ND
0.100
0.13
1 11/16/201916:43
WG1381303
ND
0.100
0.13
1 11/16/201916:43
WG1381303
ND
0.100
0.50
1 11/16/201916:43
WG1381303
ND
0.100
3
1 11/16/201916:43
WG1381303
ND
0.100
2
1 11/16/201916:43
WG1381303
ND
0.100
5
1 11/16/201916:43
WG1381303
ND
0.100
400
1 11/16/201916:43
WG1381303
ND
0.100
200
1 11/16/201916:43
WG1381303
ND
0.100
100
1 11/16/201916:43
WG1381303
ND
0.100
400
1 11/16/201916:43
WG1381303
ND
0.100
2
1 11/16/201916:43
WG1381303
27.7
10.0-120
111161201916.43
WG1381303
19.7
10.0-120
111161201916.43
WG1381303
33.3
10.0-127
111161201916.43
WG1381303
45.6
10.0-130
111161201916.43
WG1381303
59.5
10.0-155
111161201916.43
WG1381303
67.3
10.0-128
111161201916.43
WG1381303
PROJECT:
SDG:
DATE/TIME: PAGE:
L1153315
11/20/19 09:46 6 of 21
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc

WG1380017 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1158315-01
Method Blank (MB)
(MB) R3472030-1 11/14/1913:47
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1157700-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1157700-02 11/14/1913:51 • (DUP) R3472030-3 11/14/1913:52
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide 0.380 0.378 1 0.536 20
L1159290-10 Original Sample (OS) • Duplicate (DUP)
(OS) L1159290-10 11/14/19 14:47 • (DUP) R3472030-8 11/14/19 14:43
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg
Reactive Cyanide U 0.000 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3472030-2 11/14/19 13:48
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.45 98.0
Rec. Limits LCS Qualifier
50.0-150
L1158116-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1153116-03 11/14/1913:56 • (MS) R3472030-4 11/14/1913:59 • (MSD) R3472030-5 11/14/19 14:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 U 1.31 1.44 78.6 86.2 1 75.0-125 9.21 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 7 of 21

WG1380017 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1158315-01
L1159290-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1159290-04 11/14/1914:39 • (MS) R3472030-6 11/14/1914:40 • (MSD) R3472030-7 11/14/1914:41
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec.
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.92 U 1.69 1.66 87.6 86.4
Dilution Rec. Limits
75.0-125
MS Qualifier MSD Qualifier RPD
1.41
ONE LAB. NATIONWIDE. *
RPD Limits
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 3 of 21

WG1379886
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3471949-1 11/13/19 2100
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1157700-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1158315-01
(OS) L1157700-02 11/13/19 2100 • (DUP) R3471949-3 11/13/19 2100
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg _ %_
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3471949-2 11/13/19 2100
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Reactive Sulfide 100 87.6 87.6 70.0-130
ONE LAB. NATIONWIDE. *
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 9 of 21

WG1378591 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1158315-01
Laboratory Control Sample (LCS)
(LCS) R3470775-1 11/11/19 19:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.94 99.4 99.0-101
Sample Narrative:
LCS: 9.94 at18.3C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 10 of 21

1
WG1379769 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1158315-01
L1158327-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1153327-01 11/14/191719 • (DUP) R3472147-2 11/14/191719
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability 150 140 1 6.88
L1158351-07 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1153351-07 11/14/191719 • (DUP) R3472147-3 11/14/19 1719
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability 190 172 1 9.92 10
L1158394-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1153394-01 11/14/191719 • (DUP) R3472147-4 11/14/191719
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability 152 157 1 3.23 10
Laboratory Control Sample (LCS)
(LCS) R3472141-1 11/14/19 00:49
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 85.4 104 96.0-104
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 11 of 21

WG1380253
Mercury by Method 7470A
Method Blank (MB)
(MB) R3471926-1 11/14/191116
MB Result
Analyte mg/I
Mercury U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00330 0.0100
QUALITY CONTROL SUMMARY
L1158315-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3471926-2 11/14/191118 • (LCSD) R3471926-3 11/14/191120
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0303 0.0304 101 101 80.0-120 0.264 20
L1158282-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1153232-02 11/14/19 1122 • (MS) R3471926-4 11/14/19 1124 • (MSD) R3471926-5 11/14/19 1130
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0308
0.0281 103 93.7 1 75.0-125 9.25 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
SAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 12 of 21

WG1380258
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1158315-01
(MB) R3472070-1 11/14/1915:01
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0330
0.100
Barium U
0.0330
0.100
Cadmium U
0.0330
0.100
Chromium U
0.0330
0.100
Lead 0.0535
J 0.0330
0.100
Selenium U
0.0330
0.100
Silver U
0.0330
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3472070-2 11/14/1915:04 • (LCSD) R3472070-3 11/14/1915:06
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.62
9.59
96.2
95.9
80.0-120
0.282
20
Barium
10.0
9.74
9.75
97.4
97.5
80.0-120
0.190
20
Cadmium
10.0
9.72
9.77
97.2
97.7
80.0-120
0.508
20
Chromium
10.0
9.73
9.76
97.3
97.6
80.0-120
0.317
20
Lead
10.0
9.73
9.73
97.3
97.3
80.0-120
0.0443
20
Selenium
10.0
9.79
9.74
97.9
97.4
80.0-120
0.573
20
Silver
2.00
1.78
1.78
89.0
89.0
80.0-120
0.0174
20
L1158411-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1153411-01 11/14/1915:09 • (MS) R3472070-5 11/14/1915:15 • (MSD) R3472070-6 11/14/1915:17
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.63
9.59
96.3
95.9
1 75.0-125
0.378
20
Barium
10.0
96.4
107
100
102
39.3
1 75.0-125
V_ 6.10
20
Cadmium
10.0
ND
9.83
9.78
98.3
97.8
1 75.0-125
0.570
20
Chromium
10.0
ND
9.83
9.68
98.3
96.8
1 75.0-125
1.53
20
Lead
10.0
3480
3540
3290
649
0.000
1 75.0-125
E V E V 7.38
20
Selenium
10.0
ND
9.80
9.75
98.0
97.5
1 75.0-125
0.495
20
Silver
2.00
ND
1.82
1.78
91.0
89.1
1 75.0-125
2.09
20
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 13 of 21

WG1382386 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1158315-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3473311-3 11/19/1912:40
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0165
0.0500
Carbon tetrachloride
U
0.0165
0.0500
Chlorobenzene
U
0.0165
0.0500
Chloroform
U
0.0825
0.250
1,2-Dichloroethane
U
0.0165
0.0500
1,1-Dichloroethene
U
0.0165
0.0500
2-Butanone (MEK)
U
0.165
0.500
Tetrachloroethene
U
0.0165
0.0500
Trichloroethene
U
0.0165
0.0500
Vinyl chloride
U
0.0165
0.0500
(S) Toluene-d8
96.1
80.0-120
(S) 4-Bromofluorobenzene
100
77.0-126
(S) 1,2-Dichloroethane-d4
99.8
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3473811-1 11/19/1910:17 • (LCSD) R3473811-2 11/19/19 1137
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.00500
0.00434
0.00401
86.7
80.2
70.0-123
Carbon tetrachloride
0.00500
0.00446
0.00434
89.2
86.9
68.0-126
Chlorobenzene
0.00500
0.00454
0.00410
90.9
82.1
80.0-121
Chloroform
0.00500
0.00443
0.00410
88.7
82.0
73.0-120
1,2-Dichloroethane
0.00500
0.00499
0.00438
99.8
87.6
70.0-128
1,1-Dichloroethene
0.00500
0.00452
0.00438
90.3
87.6
71.0-124
2-Butanone (MEK)
0.0250
0.0231
0.0189
92.2
75.5
44.0-160
Tetrachloroethene
0.00500
0.00425
0.00426
85.0
85.2
72.0-132
Trichloroethene
0.00500
0.00397
0.00396
79.3
79.2
78.0-124
Vinyl chloride
0.00500
0.00419
0.00417
83.8
83.5
67.0-131
(S) Toluene-d8
94.8
94.5
80.0-120
(S) 4-Bromofluorobenzene
99.1
100
77.0-126
(S) 1,2-Dichloroethane-d4
106
104
70.0-130
ACCOUNT:
EMA Resources
PROJECT:
LCS Qualifier LCSD Qualifier RPD
RPD Limits
7.80
20
2.65
20
10.2
20
7.86
20
13.0
20
3.00
20
20.0
20
0.152
20
0.164
20
0.366
20
SDG:
DATE/TIME: PAGE:
L1153315
11/20/19 09:46 14 of 21

WG1381552
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3473063-1 11/17/1916:59
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) Z4-Dichlorophenyl Acetic 51.6
Acid
MB Qualifier MB MDL
mg/I
0.000667
0.000667
Laboratory Control Sample (LCS)
(LCS) R3473068-2 11/17/19 1713
Spike Amount
LCS Result
LCS Rec.
Analyte
mg/I
mg/I
2,4-D
0.0500
0.0304
60.8
2,4,5-TP (Silvex)
0.0500
0.0321
64.2
(S) Z4-Dichlorophenyl Acetic
52.4
Acid
QUALITY CONTROL SUMMARY
L1158315-01
MB RDL
mg/I
0.00200
0.00200
14.0-158
Rec. Limits LCS Qualifier
50.0-120 P
50.0-125 P
14.0-158
L1158212-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153212-01 11/17/19 18:21 • (MS) R3473063-3 11/17/19 13:34 • (MSD) R3473063-4 11/17/19 18:43
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0312
0.0330
62.4
66.0
2,4,5-TP (Silvex)
0.0500
ND
0.0329
0.0340
65.8
68.0
(S) Z4-Dichlorophenyl Acetic
53.2
54.4
Acid
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 50.0-120 P P 5.61 20
1 50.0-125 P P 3.29 20
14.0-158
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 15 of 21

WG1381559
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1158315-01
(MB) R3473199-1 11/13/19 08:53
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
95.4
10.0-128
(S) Tetrochloro-m-xylene
86.3
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3473199-2 11/18/19 09:18
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00845
84.5
55.0-129
Endrin
0.0100
0.00928
92.8
57.0-134
Heptachlor
0.0100
0.00908
90.8
27.0-132
Methoxychlor
0.0100
0.00983
98.3
54.0-155
(S) Decachlorobiphenyl
93.6
10.0-128
(S) Tetrochloro-m-xylene
875
10.0-127
L1157700-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1157700-01 11/13/19 09:43 • (MS) R3473199-3 11/13/19 09:55 • (MSD) R3473199-4 11/13/19 10:07
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00704
0.00703
70.4
70.3
1 14.0-141
Endrin
0.0100
ND
0.00774
0.00774
77.4
77.4
1 10.0-160
Heptachlor
0.0100
ND
0.00607
0.00715
60.7
71.5
1 16.0-136
Methoxychlor
0.0100
ND
0.00984
0.00741
98.4
74.1
1 10.0-160
(S) Decachlorobiphenyl
68.1
67.8
10.0-128
(S) Tetrochloro-m-xylene
4890
4980
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
0.142 40
0.000 39
16.3 40
28.2 34
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 16 of 21

WG1381303 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1158315-01
Method Blank (MB)
(MB) R3472310-2 11/16/1910:09
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
25.8
10.0-127
(S) 2-Fluorobiphenyl
37.0
10.0-130
(S) p-Terphenyl-d14
72.4
10.0-128
(S) Phenol-d5
19.8
10.0-120
(S) 2-Fluorophenol
26.8
10.0-120
(S) Z4, 6-Tribromophenol
57.5
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3472810-1 11/16/19 09:48
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.188
37.6
18.0-120
2,4-Dinitrotoluene 0.500
0.309
61.8
49.0-124
Hexachlorobenzene 0.500
0.317
63.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.210
42.0
19.0-120
Hexachloroethane 0.500
0.183
36.6
15.0-120
Nitrobenzene 0.500
0.183
36.6
27.0-120
Pyridine 0.500
0.199
39.8
10.0-120
2-Methylphenol 0.500
0.206
41.2
28.0-120
3&4-Methyl Phenol 0.500
0.237
47.4
31.0-120
Pentachlorophenol 0.500
0.273
54.6
23.0-120
2,4,5-Trichlorophenol 0.500
0.297
59.4
44.0-120
2,4,6-Trichlorophenol 0.500
0.260
52.0
42.0-120
(S) Nitrobenzene-d5
28.7
10.0-127
(S) 2-Fluorobiphenyl
43.7
10.0-130
(S) p-Terphenyl-d14
62.9
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1158315 11/20/19 09:46 17 of 21

WG1381303 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1158315-01
Laboratory Control Sample (LCS)
(LCS) R3472810-1 11/16/19 09:48
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 22.8 10.0-120
(S) 2-Fluorophenol 30.4 10.0-120
(S) 2,4, 6-Tribromophenol 60.5 10. 0-155
L1157797-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1157797-01 11/16/19 14:03 • (MS) R3472310-3 11/16/19 14:30 • (MSD) R3472310-4 11/16/19 14:52
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.178
0.243
35.6
48.6
2,4-Dinitrotoluene
0.500
ND
0.307
0.355
61.4
71.0
Hexachlorobenzene
0.500
ND
0.309
0.350
61.8
70.0
HexachIoro-1,3-butadiene
0.500
ND
0.215
0.256
43.0
51.2
Hexachloroethane
0.500
ND
0.172
0.232
34.4
46.4
Nitrobenzene
0.500
ND
0.209
0.242
41.8
48.4
Pyridine
0.500
ND
0.0999
0.170
20.0
34.0
2-Methylphenol
0.500
ND
0.191
0.226
38.2
45.2
3&4-Methyl Phenol
0.500
ND
0.224
0.258
44.8
51.6
Pentachlorophenol
0.500
ND
0.292
0.315
58.4
63.0
2,4,5-Trichlorophenol
0.500
ND
0.308
0.354
61.6
70.8
2,4,6-Trichlorophenol
0.500
ND
0.276
0.314
55.2
62.8
(S) Nitrobenzene-d5
31.8
36.6
(S) 2-Fluorobiphenyl
49.1
53.3
(S) p-Terphenyl-d14
61.9
65.9
(S) Phenol-d5
21.3
24.1
(S) 2-Fluorophenol
29.4
33.6
(S)2,4,6-Tribromophenol
65.5
71.0
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 17.0-120
30.9
1 39.0-125
14.5
1 35.0-122
12.4
1 12.0-120
17.4
1 10.0-120
29.7
1 12.0-120
14.6
1 10.0-120
J3 51.9
1 10.0-120
16.8
1 10.0-120
14.1
1 10.0-128
7.58
1 33.0-120
13.9
1 26.0-120
12.9
10.0-127
10.0-130
10.0-128
10.0-120
10.0-120
10.0-155
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 13 of 21

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Fc
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
F
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
Rc
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
E The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J The identification ofthe analyte is acceptable, the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded, values are outside upper control limits.
J3 The associated batch QC was outside the established quality control range for precision.
P RPD between the primary and confirmatory analysis exceeded 40%.
T8 Sample(s) received past/too close to holding time expiration.
v The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1153315 11/20/19 09:46 19 of 21

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1153315 11/20/19 09:46 20 of 21

Billing Information,
Analvsis
i
Coritainpir
/ Pr
ative
Chain of Custody Page _of
EMA Resources
Mr. Brent Collins Pres
755 Yadkinville Road [hk
I
755 Yadkinville Road
Mocksville, NC 27028
1 ;aceAnaij/tlCai1
Mocksville, NC 27028
12065 Lebanon Rd
Report to:
Email To: [e-mail]
Mr. Brent Collins
-iir
phonet 5157oliet, 9-58581
Phone; 615J58�5958
Phone; 800.757.5854
Faa:6L5-758.5859
Project City/State J
j -d5VJiC/AJC
Please Circle:
Description: Sludge Collected:
PT MT CT ET
+
SDG #
Phone: [phone]
Client Project N
Lab Project #
J021
Fax: [phone]
0.
Collected by (print):
Site/Facility ID N
P.O #
Acctnum: EMARES
w
li­,
z
Template:T11413
Collected by (signature):
liuSh. (Lab MUST Be Notified) Quote #
— same Day ____ Five Day
L
J
Prelogin: P733018
_ Next Day _ 5 Day (Rad Only} Date Results Needed
PM: 807-Justin afr
immediately
✓
—Two Day 10 Day (Rad Only) No.
PB.
Packed on Ice N Y
Three Day of
J
,i
�
Shipped ia: Fe EX Standard
Sample ID
Comp/Grab
Matrix`
Depth
Date
Time
-ntrs
U
U
Remarks Sample apabonlyi
!2� dsv�lfC f
55
3h
r�19
ll.-3awy
i 2
X
X
i
I
' Matrix: emarks: Sample Ril h k
SS - Soil AIR - Air F- Filter pH Temp COC Seal present/Intact: _NP Y N
GW - Groundwater B- Bioassay CGC Signed/Accurate: Y N
�N
WW - Wastewater Flow Other Bottles arrive intact: Y
Correct bottles used: Y �N
DW - Drinking W ter Sufficient volume sent: Y N
Samples re rued via: /2/� 7 — —
OT Other d hC Trackingp G3 S � If able
/
UPS FedEx _Courier r VGA Zero Headspace: Y N
ace:
Relinquished by : (Signature) Date: Time: Received by: (Signature) Trip Blank Received: Yes preservation Correct/Checked:' yy, �N
J PAD Screen [0.5 mR/hr: ✓ [ _N
HCL / MeoH
TBR
Relinquishe by : (Signature)
Date Time:
Received by: (Signattfre)
Temp: T Bottles Received:
If preservation required by Login: Date/rime
:t:--3 !�
Relinquished by (Signature)
Date: Time:
Received for lab by: (Signature)
Date: Time:
Hold:
Condition:
NCF 14FKN