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Cashiers Lake
Jackson County
Cashiers, North Carolina
Headwater Project # A20-111.01
Prepared for:
Cashiers Canoe Club Development, LLC, and
Lake Association, Inc.
PO Box 300849
Austin, Texas 78703
March 5, 2020

Pre -Dredging Assessment
Cashiers Lake
Jackson County
Cashiers, North Carolina
Headwater Project # A20-111.01
March 5, 2020
Prepared for
Cashiers Canoe Club Development, LLC, and
Lake Association, Inc.
PO Box 300849
Austin, Texas 78703
Prepared by
Headwater Geology, PLLC
43 College Place, Suite 212
Asheville, North Carolina 28801
SEAL:
2186
Adam M. Tripp, PG
Mike H. Falknor

Cashiers Lake —Pre -Dredging Assessment
TABLE OF CONTENTS
Tableof Contents............................................................................................................ 1
1 Introduction............................................................................................................... 3
1.1 Background and Purpose................................................................................................... 3
2 Work Plan Summary................................................................................................. 6
2.1 Initial Contaminants of Concern and Historical Environmental Review ..............................
6
2.1.1 Consolidated Metco Facility...................................................................................
7
2.1.1.1 Soil and Groundwater Assessment Report..........................................................
7
2.1.1.2 Comprehensive Site Assessment........................................................................
7
2.1.1.3 Plant Closure and Soil Remediation....................................................................8
2.1.1.4 Sample Analysis Summary ..................................................................................
8
2.1.2 Plastics Industry Information..................................................................................9
2.1.3 Cashiers Lake Sediment Sampling........................................................................
9
2.1.4 DEQ Comment — Requested Analyses................................................................
10
2.1.4.1 VOCs by EPA Method 8260..............................................................................10
2.1.4.2 SVOCs by EPA Method 8270............................................................................11
2.1.4.3 Chlorinated Pesticides by EPA Method 8081....................................................11
2.1.4.4 Poly -Chlorinated Bisphenols (PCBs) by EPA Method 8082 ..............................
11
2.1.4.5 Herbicides by EPA Method 8151.......................................................................11
2.1.4.6 Organophosphorus Pesticides by EPA Method 8141........................................
12
2.1.4.7 Cyanide by Standard Method 4500...................................................................12
2.1.4.8 Sulfide by Standard Method 4500.....................................................................
12
2.1.4.9 RCRA Metals by EPA Method 6010C and 7471...............................................
12
2.2 Identification of Constituents of Concern..........................................................................
13
2.3 Sediment Sample Grid Evaluation...................................................................................
13
3 Sediment Sampling Methodology...........................................................................
15
3.1 Sediment Observations....................................................................................................
15
3.2 Sample Analysis..............................................................................................................
15
4 Summary of Results................................................................................................
16
4.1 Tier 2 Risk Evaluation......................................................................................................
16
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Cashiers Lake —Pre -Dredging Assessment
5 Conclusions and Recommendations...................................................................... 18
6 References............................................................................................................. 19
FIGURES
Figure 1 Site Location Map
Figure 2 Site Layout Map
Figure 3 Sample Location Map
TABLES
Table 1 Sediment Analytical Results Summary
Table 2 Site -Specific Leaching Potential Results
APPENDICES
Appendix A Laboratory Analytical Report
Appendix B Tier 2 Risk Evaluation Data Sheet
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Cashiers Lake —Pre -Dredging Assessment
1 Introduction
Headwater Geology PLLC. (Headwater), on behalf of Cashiers Canoe Club Development, LLC
and Lake Association, Inc. (Client), prepared this Pre -Dredging Assessment Report detailing the
environmental review of an approximate 6.5-acre portion of accumulated sediment within
Cashiers Lake. The subject area is located to the south of Frank Allen Road in Cashiers, Jackson
County, North Carolina (the Site). The lake location, and proposed dredging area, is shown on
the attached Figure 1, Figure 2, and Figure 3.
Prior to completing on -Site activities, Headwater submitted a Pre -Dredging Assessment Plan
dated November 26, 2019 to the North Carolina Department of Environmental Quality (DEQ).
Based on verbal comments provided by the DEQ, Headwater revised the Work Plan, as detailed
in the Pre -Dredging Assessment Plan —Revision 1 (Work Plan), dated December 18, 2019. The
Work Plan was approved by the DEQ in an email sent on January 17, 2020.
This report contains a project background and purpose, a summary of the Work Plan methodology
and scope, and a summary of the sediment assessment methodology, results, and conclusions.
1.1 Background and Purpose
Cashiers lake was constructed in the early-1920's. In order to address significant sediment
accumulation in the area where the Chattooga River discharges to Cashiers Lake, the Client is
proposing to dredge accumulated sediment from this area. Headwater is not aware of previous
sediment removal from the Site.
An Individual Permit application for dredging of Cashiers Lake was submitted to the United States
Army Corps of Engineers (USACE) and the North Carolina Department of Environmental Quality
(DEQ) Division of Water Resources (DWR) on April 24, 2018.
The USACE issued a Corps Comment and Request for Additional Information notice on June 28,
2018, requesting chemical analysis of sediment. Headwater submitted a Pre -Dredge
Environmental Review, dated December 14, 2018 for the Site to address this request for
additional information (Headwater 2018). See Section 2.1.3 for details of that assessment.
Subsequently, a public hearing, regarding the Site dredging plan was held on September 5, 2019.
Based on comments received during the hearing and public comment period (July 29, 2019 to
October 7, 2019); the DEQ issued a second Request for Additional Information, dated October
28, 2019.
DEQ's October 2019 letter included the following comment:
1) "...it was brought to the Division's attention during the hearing a plastics manufacturing
facility previously existed in Cashiers and that it may have had discharges upstream of
Cashiers Lake. It was also noted that sampling data provided to the Division indicated high
levels of Chromium. Please provide a proposed sediment sampling plan that includes all
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Cashiers Lake —Pre -Dredging Assessment
constituents listed in 40 CFR EPA Appendix II to Part 258-List of Hazardous Inorganic and
Organic Constituents to ensure compliance with the May 2019 NCDEQ Preliminary Soil
Remediation Goals PSRGs. The sampling plan must include a detailed description of the
proposed locations and methodology for the proposed sampling. The Division
recommends following the guidance detailed in Part III of the EPA/USACE Evaluation of
Dredged Material Proposed For Discharge in Waters of the U.S. - Testing Manual (Inland
Testing Manual)."
Note that the plastics manufacturing facility was identified as the former Consolidated Metco
facility.
Public comments were submitted to the DEQ as oral comments during the public meeting and as
written comments during the public comment period. Headwater reviewed multiple written
comments as well as DEQ staff notes regarding oral comments. Multiple comments referenced
the plastics manufacturing facility located upstream of the Site. Some of these comments were
referenced in a letter sent from Mr. Scott Jones, Esq. with Barbour, Searson, Jones, and Cash,
Attorneys to the DEQ-DWR, dated October 7, 2019. Public comments documented in this letter
include references to potential historical releases from the plastics manufacturing facility that may
have resulted in the presence of contaminants in the lake sediment.
The Barbour, Searson, Jones, and Cash letter contained additional information relevant to this
assessment, including:
• In the early-1970s, the Cashiers Plastics plant began manufacturing injection molded
plastic goods.
• One of the most common Priority Toxic Pollutants generated from the Plastics Molding
and Forming manufacturing process is bis (2-ethylhexyl) phthalate (aka di(2-ethylhexyl)
phthalate and DEHP).
• Other common EPA Priority Toxic Pollutants generated as a result of the Plastics Molding
and Forming, manufacturing process are: phenol, zinc, di-n-butyl phthalate, and dimethyl
phthalate.
Note that bis(2-ethylhexyl)phthalate, di(2-ethylhexyl)phthalate and DEHP are synonyms for the
same compound.
In order to address the Request for Additional Information dated October 7, 2019, Headwater
prepared the Work Plan dated December 18, 2019. The Work Plan was approved by the DEQ in
an email sent on January 17, 2020.
The Work Plan included a summary of documented releases, assessment, and remediation at
the former plastics manufacturing facility (former Consolidated Metco facility). Based on review of
that data and previous Site assessment information, Headwater evaluated potential contaminants
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Cashiers Lake —Pre -Dredging Assessment
of concern and developed a methodology for additional assessment. A summary of the Work Plan
is included in Section 2.0
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Cashiers Lake —Pre -Dredging Assessment
2 Work Plan Summary
The Work Plan addressed the requests detailed in the October 28, 2019 DEQ Request for
Additional Information (Item 1) and was prepared in general accordance with the Evaluation of
Dredged Material Proposed for Discharge to Waters of the U.S — Testing Manual (Inland Testing
Manual) prepared by the United States Environmental Protection Agency (EPA) and dated
February 1998 (EPA 1998) as well as the Dam Removal Analysis Guidelines for Sediment,
prepared by the Advisory Committee on Water Information Subcommittee on Sedimentation,
Published by the US. Department of the Interior Bureau of Reclamation Technical Service Center
(TSC), dated December 2017 (TSC 2017)
The Work Plan included an evaluation of potential sources of contamination proximate to the Site
in order to identify constituents of concern (COCs) that might be present in Cashiers Lake
sediment. Sediment sampling was then defined to target those COCs.
This approach is supported by the Inland Testing Manual. Specifically, "Subpart G of the 404(b)(1)
guidelines requires the use of available information to make a preliminary determination
concerning the need for testing of the material proposed for dredging." Further, "knowledge of the
proposed dredging site proximity to other sources of contamination as well as that gained from
previous testing, may be utilized to conclude that there is no reason to believe that contaminants
are present" (EPA 1998)
A summary of existing environmental data and information regarding contaminants of concern is
included in the following sub -sections.
2.1 Initial Contaminants of Concern and Historical Environmental Review
Prior to completing additional assessment activities, Headwater performed a search of incidents
listed in the DEQ-Division of Waste Management Site Locator Tool on November 25 and 26,
2019. An incident associated with the Consolidated Metco facility was identified in a location
adjacent to the Chatooga River, upstream of Cashiers Lake. The location of the Consolidated
Metco facility is shown on the attached Figure 2 and appears to the plastics manufacturing facility
referenced in DEQ and public comments. Additional minor incidents, primarily associated with
underground storage tank (UST) releases, were identified within the watershed, but were not
located adjacent to surface water bodies that would transport contaminants to Cashiers Lake in
appreciable amounts.
Headwater has reviewed existing environmental data for the former Consolidated Metco facility,
located upstream of the Site, general contaminant information associated with the plastics
industry, as well as sediment sampling previously performed in Cashiers Lake by Headwater in
order to perform a preliminary review of COCs and prior to completing on -Site activities. That
review is discussed in the following subsections.
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Cashiers Lake —Pre -Dredging Assessment
2.1.1 Consolidated Metco Facility
According to available DEQ documents, the Consolidated Metco was formerly located at 95
Plastic Plant Road, Cashiers, North Carolina, approximately 0.25-miles northwest of the Site. The
facility was constructed in 1970 and produced molded plastics parts for the trucking and other
industries. Process at the facility included the storage of raw materials (plastic pellets), injection
molding of plastic resins, sanding and finishing, and painting and coating, and assembly of plastic
parts (Besinger & Garrison [B&G] 2008)
According to documents available via the DEQ-DWM, Laserfiche website, soil samples were
initially collected from the facility in association with due diligence related to a potential property
transaction in January 15, 2007 (B&G 2007a). The results of that assessment identified volatile
and semi -volatile compounds (primarily petroleum -related constituents) in soil and recommend
further soil and groundwater review. As a result of this initial assessment, a release was attributed
to the operations of the facility. The then Department of Environment and Natural Resource
(DENR) issued a Notice of Violation (NOV) on March 7, 2007. That NOV references the facility
as Incident Number 88035 and requested further assessment and remediation of the Consolidate
Metco Plant.
2.1.1.1 Soil and Groundwater Assessment Report
In response to the March 7, 2007 NOV, Consolidate Metco engaged Besinger & Garrison (B&G)
to complete additional soil and groundwater review. B&G issued an August 21, 2007 Soil and
Groundwater Report. During this assessment approximately 50 soil and sediment samples and
10 groundwater samples were collected and analyzed (B&G 2007b).
The conclusions of the Soil and Groundwater Report did not identify impacts to groundwater
outside of the building footprint. Multiple compounds were detected in soil, but most were below
applicable standards. B&G recommended that more extensive groundwater monitoring be
completed within the building footprint and downgradient of the facility as -well -as the collection of
additional soil samples to further delineate identified impacts. Tables and figures from the B&G
August 2007 report are included in Appendix A. Figure 2 of B&G's report shows three outfalls
discharging to the Chattooga River (referenced as Cashiers Creek on the figure). Outfall 001
appears to be associated with stormwater drainage from the access road to the facility, and Outfall
002 and 003 appear to be associated with stormwater drainage from the facility footprint (B&G
2007b).
2.1.1.2 Comprehensive Site Assessment
B&G later issued a Comprehensive Site Assessment (CSA) report in January of 2008. This
assessment included the collection of approximately 38 soil and sediment samples and 15
additional groundwater samples. The results of the CSA identified impacted soil; including
locations beneath a "hydraulic press room", within a "drum storage area", beneath a "storm drain
adjacent to the drum storage area", and downgradient of stormwater "outfall 003". Figures and
tables from the 2008 CSA are included in Appendix B.
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Cashiers Lake —Pre -Dredging Assessment
Additionally, assessment during the completion of the CSA, confirmed several locations of
impacted groundwater and soil. A recovery well was installed to remove petroleum product from
groundwater. The results of the CSA also identified the conveyance of impacted stormwater
downgradient of the facility via a stormwater outflow (Outfall 003). Soil assessment at this outflow
discharge identified oil and grease constituents in excess of the regulatory allowable limits. In
response, soil excavation and off -site disposal was engaged in the vicinity of the outflow
discharge, as -well -as in vicinity to the associated storm drain inlet, and a drum storage area. A
total of approximately 65 tons of impacted soil were removed for off -site disposal.
The CSA results indicated that plant demolition was planned for 2008, at which time further
remediation was recommended (B&G 2008a).
2.1.1.3 Plant Closure and Soil Remediation
Plant demolition occurred between February and April of 2008. After plant demolition was
completed, B&G engaged a series of soil excavation and disposal events between June 2008
and November 2008. The total amount of soil removed from the facility totaled approximately
2,275 tons (B&G 2008b).
Additionally, groundwater remediation pits and a free product recovery well were utilized to
address previously inaccessible areas and to recover free -phase product. After four events, the
pits and well were abandoned as infiltration of impacted groundwater was no longer observed.
Various additional assessment and reporting documents were provided by B&G to the DENR
through March 2009. In a Report of Additional Assessment Activities, dated March 2, 2009, B&G
requested that a No Further Action status be applied for on behalf of the Responsible Party,
Consolidated Metco.
On March 11, 2009 the DENR issued a Notice of No Further Action (NFA) regarding the
Consolidated Metco facility, Incident Number 88035. No additional facility -specific documentation
was available after this date.
2.1.1.4 Sample Analysis Summary
Soil, sediment, and groundwater evaluation at the Consolidated Metco facility consisted primarily
of analysis of Volatile Organic Compounds (VOCs) by EPA Method 8260 and Semi -Volatile
Organic Compounds (SVOCs) by EPA Method 8270. Additionally, analysis included Metals by
EPA Method 6010 and 7471, and Polychlorinated Biphenyls (PCBs) by Method. Additional
"screening level analysis" such as Oil and Grease by Method 9071, Diesel Range Organics (DRO)
by Method CA-LUFT and Gasoline Range Organics (GRO) by Method CA-LUFT was also
performed on some soil and sediment samples.
PCBs were not detected in soil. Multiple VOCs, SVOCs, were detected in soil at concentrations
exceeding the DEQ-Solid Waste Section, Underground Storage Tank (UST) Section Soil -to -
Groundwater Maximum Soil Contaminant Concentration Levels (MSCCs). Several samples
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Cashiers Lake —Pre -Dredging Assessment
contained Oil and Grease, DRO, and GRO exceeding screening levels. However, a screening
level for Oil and Grease is no longer used by the UST Section or other DEQ divisions. DRO and
GRO are considered to be screening level analysis, where an exceedance indicates that the
sample should also be analyzed for risk -based constituents which include VOCs, SVOCs, and
other petroleum fraction analyses, depending on what the source of the release was.
2.1.2 Plastics Industry Information
According to Table 4-1 of the Inland Testing Manual, the plastics industry is associated with
sediment impacts from acenaphthene and lead (EPA 1998). Acenaphthene is included in the
Method 8270 SVOC analysis and lead is included in the 6010 RCRA metals analysis.
Additional compounds that may be present include bis(2-ethylhexyl)phthalate, di-n-butyl
phthalate, and dimethyl phthalate, and phenol (EPA 1984). These compounds are all included in
the Method 8270 SVOC analysis
Other than low concentrations of lead (below applicable standards), these compounds were not
detected in the Cashiers Lake sediment samples collected in 2018 (see Section 2.1.3.)
2.1.3 Cashiers Lake Sediment Sampling
Headwater previously submitted a Pre -Dredge Environmental Review, dated December 14, 2018
for the Site (Headwater 2018). Sample locations from this assessment are shown on Figure 2.
As documented in this report, Headwater collected six sediment samples from two depths at three
separate locations (SB-1 [0-2], SB-1 [2-4], SB-2 [0-2] SB-2 [2-4], SB-3 [0-2], and SB-3 [2-4]) from
within the proposed dredging area of Cashiers Lake and from two depths at each of two
"background" locations (BG-1 [0-2], BG-1 [2-4], BG-2 [0-2], and BG-2 [2-4]). Each sample was
collected at an area considered to be representative of Site conditions at that location. Sample
collection was performed on November 28, 2018.
At each location, sediment samples were collected from a 0-to-2 feet below grade surface (ft-bgs)
and a 2-to-4 ft-bgs depth interval. Additionally, four background samples were collected for
analysis of Resource Conservation Recovery Act (RCRA) metals from outside the proposed
dredging footprint at the same depths as the lake dredge samples. Samples were collected
utilizing a stainless -steel hand auger. The hand auger was decontaminated with an Alconox
solution and rinsed with de -ionized water before and between advancement at each sampling
point.
Sediment samples were analyzed for
• Volatile Organic Compounds (VOCs)
• Semi -Volatile Organic Compounds (SVOCs) and
• RCRA metals
Sediment samples collected from the background locations were analyzed for RCRA metals only.
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Cashiers Lake —Pre -Dredging Assessment
No constituents were identified above the Preliminary Soil Remediation Goals (PSRG) with the
exception of total chromium in all 10 samples (including background samples). Headwater
requested the laboratory speciate total chromium to allow for a more thorough comparison to
regulatory standards. The results of the chromium speciation analysis indicated that trivalent
chromium concentrations were below applicable regulatory standards. Hexavalent chromium was
not detected above laboratory reporting limits in any sample analyzed (Headwater 2018).
Only two VOCs, toluene and p-isopropyltoluene were detected above the laboratory reporting
limits. Toluene was detected at a concentration of 0.0371 milligrams per kilogram (mg/kg) in only
one sample, which is below the most conservative PSRG, the Protection of Groundwater PSRG
of 8.3 mg/kg. P-isopropyltoluene was detected at a concentration of 0.155 mg/kg, also below the
Protection of Groundwater PSRG of 1.24 mg/kg.
2.1.4 DEQ Comment — Requested Analyses
Based on an October 28, 2019 Request for Additional Information, the DEQ had requested that
pre -dredge assessment activities include analysis for all constituents listed in 40 CFR EPA
Appendix II Part 258 - List of Hazardous Inorganic and Organic Constituents (Appendix 11). These
analyses would include:
• VOCs by EPA Method 8260
• SVOCs by EPA Method 8270
• Chlorinated Pesticides by EPA Method 8081
• Poly -Chlorinated Bisphenols (PCBs) by EPA Method 8082
• Herbicides by EPA Method 8151
• Organophosphorus Pesticides by EPA Method 8141
• Cyanide by Standard Method 4500
• Sulfide by Standard Method 4500
• RCRA Metals by EPA Method 6010C and 7471
A description of the constituents included in each of these analyses and their potential presence
in dredge sediment is included in the following sub -sections.
2.1.4.1 VOCs by EPA Method 8260
VOCs area class of chemicals that have a high vapor pressure at room temperature and easily
convert from a solid or liquid to a vapor. There are approximately 62 compounds that are reported
via the 8260 Method. VOCs are commonly used in chemical processes, as solvents and
degreasers, as additives to gasoline and other petroleum products and for a variety of additional
uses. They are both anthropogenically manufactured and naturally occurring. Common VOCs
include benzene, trichlorethylene, xylene, tetrachlorethlyene, toluene, etc. Health effects from
VOCs vary but typically include long-term effects such as cancer.
VOCs, specifically petroleum constituents were detected at the Metco facility. Two VOCs (toluene,
and p-isopropyltoluene) were detected in Site sediment during Headwater's 2018 sediment
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Cashiers Lake —Pre -Dredging Assessment
assessment. The concentration of these constituents was below applicable standards (Headwater
2018).
2.1.4.2 SVOCs by EPA Method 8270
SVOCs area sub -group of VOCs that have a higher boiling point and molecular weight than typical
VOCs. There are approximately 144 compounds that are reported via the 8270 Method. SVOCs
are commonly used in pesticides, ingredients in cleaning agents and personal care products,
additives to vinyl flooring, furniture, clothing, etc. SVOCs are also present in petroleum products
and coal/coal tar. They are both anthropogenically manufactured and naturally occurring.
Common SVOCs include acenaphthene, benzoic acid, bis(2-ethylhexyl)phthalate, 1,2-
dichlorobenzene, etc. Health effects from SVOCs vary but typically include long-term effects such
as cancer.
SVOCs, specifically petroleum constituents and bis(2-ethylhexyl)phthalate, a common plasticizer
were detected at the Metco facility.
2.1.4.3 Chlorinated Pesticides by EPA Method 8081
Chlorinated pesticides are a class of pesticides that have mostly been phased out for use in the
United States, predominantly during the 1970's. There are approximately 24 compounds that are
reported via the 8081 Method. Chlorinated pesticides were used abundantly between the 1940s
and 1970s. They were phased out of use due to their toxicity and persistence in the environment.
Common chlorinated pesticides include DDT, Aldrin, Dieldrin, Endrin, etc.
Chlorinated pesticides have not been sampled for at the Metco facility nor at the Site. However,
a source, such as a large agricultural facility, has not been identified in the vicinity of Cashiers
Lake or its tributaries. As such, the potential presence and concentration of these compounds in
lake sediments is expected to be consistent with the surrounding area.
2.1.4.4 Poly -Chlorinated Bisphenols (PCBs) by EPA Method 8082
PCBs are a group of chemicals manufactured for uses in scenarios where resistance to great
pressure or heat is required. PCBs were used as dielectric fluid in transformers as well as other
uses. There are approximately 8 compounds that are reported via the 8082 Method. PCBs were
used abundantly between the 1940s and 1970s and were phased out of use due to their toxicity
and persistence in the environment. Common PCBs include Aroclor 1254, Aroclor 1262, etc.
PCBs were not detected at the Metco facility. As such, the potential presence and concentration
of these compounds in lake sediments is expected to be consistent with the surrounding area.
2.1.4.5 Herbicides by EPA Method 8151
Herbicides are a group of chemicals used to control weeds or other unwanted plants. There are
approximately 19 compounds that are reported via the 8151 Method, many of which are still in
use. Some of these compounds have been phased out of use due to their toxicity. Common PCBs
include herbicides detected by Method 8151 include MCPA, 2,4-D, Dicamba, etc.
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Cashiers Lake —Pre -Dredging Assessment
Herbicides have not been sampled for at the Metco facility or the Site. However, a source such
as a large agricultural facility, has not been identified in the vicinity of Cashiers Lake or its
tributaries. As such, the potential presence and concentration of these compounds in lake
sediments is expected to be consistent with the surrounding area.
2.1.4.6 Organophosphorus Pesticides by EPA Method 8141
Organophosphorus pesticides are a different class of pesticides than chlorinated pesticides, most
of which are still in use today. There are approximately 26 compounds that are reported via the
8141 Method. Common organophosphorus pesticides include Chlorpyrifos, Azinphos-methyl,
Coumaphos, etc.
Organophosphorus pesticides have not been sampled for at the Metco facility nor at the Site.
However, a source such as a large agricultural facility, has not been identified in the vicinity of
Cashiers Lake or its tributaries. As such, the potential presence and concentration of these
compounds in lake sediments is expected to be consistent with the surrounding area.
2.1.4.7 Cyanide by Standard Method 4500
Cyanide is a naturally occurring and man-made chemical compound that contains a carbon -
nitrogen bond. Cyanides are produced by bacteria and fungi found in many plants. Cyanide is
used in the mining industry, as pest control, and for some other uses
Cyanide has not been sampled for at the Metco facility nor at the Site. However, a source such
as a large mining facility, has not been identified in the vicinity of Cashiers Lake or its tributaries.
As such, the potential presence and concentration of this compound in lake sediments is expected
to be consistent with the surrounding area.
2.1.4.8 Sulfide by Standard Method 4500
Sulfide is a naturally occuring anion of sulfer. Many important ores are sulfides. However,
dissolved sulfides are corrosive. Hydrogen sulfide is a toxic gas, produced by the decay of organic
matter.
Sulfide has not been sampled for at the Metco facility nor at the Site. Although hydrogen sulfide
may be produced during the decay of organic matter in sediment at the Site, it is expected to off -
gas and not to accumulate in significant quantities.
2.1.4.9 RCRA Metals by EPA Method 6010C and 7471
RCRA metals are a group of metals defined in the RCRA legislation passed in 1976. There are 8
metals that are reported via the 6010 and 7471 Methods. RCRA metals are naturally occurring in
minerals and soil but are also concentrated through anthropogenic processes. Common RCRA
metals include arsenic, barium, lead, and mercury.
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Cashiers Lake —Pre -Dredging Assessment
RCRA metals have been sampled for both at the Metco facility and the Site. Although certain
metals have been detected at both the Site and the Metco facility, metals have not been detected
above applicable standards at either location.
2.2 Identification of Constituents of Concern
Headwater has reviewed the historical assessment data from the Metco facility, the Site, literature
related to plastics manufacturing, as well as comments provided by DEQ and the public in order
to identify COCs for further analysis at the Site. Only compounds that are suspected to be present
in Site sediment at concentrations above background levels are recommended for inclusion and
further analysis. Specifically, Headwater recommended that sediment at the Site be analyzed for
the following:
• VOCs by EPA Method 8260
• SVOCs by EPA Method 8270
This sampling procedure recommendation was approved by the DEQ on January 17, 2020, and
executed by Headwater between February 11 and 12, 2020, and is further detailed in the
following sections.
2.3 Sediment Sample Grid Evaluation
Headwater understands that the Consolidated Metco facility operated upstream of the Site
between 1970 and 2007. This off -Site facility is associated with historical petroleum release and
is the primary identified source of potential contaminants to Site sediment. As Cashiers Lake was
constructed in the 1920s, the Metco facility operated for approximately one third of the period
during which expected sedimentation has occurred at the Site. Further, as the Metco facility
operated during a more recent timeframe, sediment that has deposited during its operation is
expected to be closer to the surface and closer to the main channel flowing through deposited
sediment. The primary COC identified at the Metco facility is petroleum. Petroleum constituents
are generally soluble in water. Further, when diesel or fuel oil is spilled to surface water, it spreads
quickly to a thin film less than 0.0005 inches thick so that a relatively small release could impact
a large body of water. Based on these factors, contamination in sediment at the Site, if present,
was expected to be relatively homogenous and more concentrated in the areas adjacent to the
main channel(s) flowing through the deposited sediment.
Headwater utilized the Visual Sample Plan (Version 7.12, released April 25, 2019), geostatistical
software, provided by Pacific Northwest Laboratory, US Department of Energy to evaluate the
number of samples needed to locate a "hot spot" of certain size with 95% probability. The size of
the potential dredge area is 288,000-square-feet and Headwater proposed a square grid sample
cell of 15 feet per side. Headwater assumed a "hot spot" shape and size of ellipses with semi -
major axis of 75 feet. Based on these parameters, a total of 18 samples spaced at a maximum
spacing of approximately 112 feet would be required to achieve 95% probability of "hot spot"
detection (Pacific Northwest Laboratory, 2019). In order to further increase confidence of "hot spot
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Cashiers Lake —Pre -Dredging Assessment
detection, each of the samples would be collected as composite samples composed of three (3)
aliquots collected in a triangular shape, approximately 10 to 15 feet apart. Note that the sample
collected for VOC analysis should not be composited but collected discreetly from one of the
aliquot locations in order to avoid volatilization of contaminants and present more accurate
findings. Because three sediment sample locations (total of six samples) were collected and
analyzed for Site COCs during the 2018 assessment, Headwater proposed to collect only 15
additional samples to achieve appropriate sample quantities in order to meet the proposed 95%
confidence probability. Approximate historical sample locations in conjunction with recent sample
locations are shown on Figure 3.
Headwater Geology 14

Cashiers Lake —Pre -Dredging Assessment
3 Sediment Sampling Methodology
Between February 11 and 12, 2020, Headwater collected 15 sediment samples (S-1 to S-15) at
the Site in the locations prescribed in the Work Plan (See Figure 3 for locations). Each sample
was composed of three aliquots collected in a triangular shape at approximately 10 to 15 feet
apart. Sample aliquots were collected using a piston core sampler and were collected from
sediment surface to a depth of approximately 2 to 3 feet below sediment surface, a depth
consistent with the expected dredging depth. Sample preference was for fine-grained, organic
sediment which is more likely to sorb contaminants (TSC 2017).
3.1 Sediment Observations
Sediment cores would often contain layered sediment composed of finer grained silts and clays
and courser grained sand, which is indicative of sediment deposition from a bifurcating stream.
Organic material such as roots, leaves, and other woody debris was often observed. If abundant
sample volume was present, most of the sand size sediment would be discarded in order to
include a larger proportion of finer grained sediment in the sample. Some litter, such as soda
bottles and plastic planter pots, was observed in the sample area. However, this material was not
observed in the sample aliquots. Headwater's environmental technicians also observed sediment
samples for the presence of staining, odor, or debris that may indicate the presence of
contamination. No such observations were made during sampling.
3.2 Sample Analysis
Once collected, the sample aliquot cores were placed in a stainless -steel bowl. A sample for VOC
analysis was collected from one of the sample aliquots. The sample aliquots were then mixed in
the bowl by hand. Nitrile-gloves were used by technicians, but other plastic products were avoided
so as not to introduce potential plasticizer (e.g. bis(2-ethylhexyl)phthalate) cross contamination.
One duplicate sample (DUP-1) was collected concurrently with sample S-8 in order to measure
laboratory reproducibility.
After mixing the aliquots into a composite sample, the sediment samples were then transferred to
laboratory supplied sample containers and placed in a cooler on ice. The sample cooler was
delivered to Pace Analytical Services, LLC, a North Carolina -certified laboratory under chain -of -
custody protocol. Sediment samples were analyzed for Site COCs, specifically:
• VOCs by EPA Method 8260
• SVOCs by EPA Method 8270
Headwater Geology 15

Cashiers Lake —Pre -Dredging Assessment
4 Summary of Results
Laboratory analysis of sediment samples did not identify compounds above laboratory reporting
limits with the exception of two constituents (1-Methylnapthalene and 2-Methylnapthalene) at
sample location S-12, and Acetone at sample location S-6 and S-8. Sample results were
compared to the North Carolina Department of Environmental Quality Preliminary Soil
Remediation Goals (PSRGs), dated December 2019. A summary of results is included in Table 1.
Acetone is a common laboratory contaminant and is therefore not considered to be present in
Site sediment. Additionally, the reported concentrations of Acetone at sample locations S-6 and
S-8 are below the associated PSRGs.
1-Methylnapthalene and 2-Methylnapthalene, both SVOCs, were identified above the laboratory
reporting limit at sample location S-12. Additionally, the concentration of 1-Methylnapthalene
(0.17 milligrams per kilogram [mg/kg]) was identified slightly above the Protection of Groundwater
PSRG of 0.11 mg/kg but below the Residential PSRG of 18 mg/kg. 1-Methyl naphthalene and
2-methyl naphthalene are polycyclic aromatic hydrocarbons (PAHs) and are typically used to
make other chemicals such as dyes and resins. 2-Methyl naphthalene is also used to make vitamin
K. These chemicals are present in cigarette smoke, wood smoke, tar, asphalt, and petroleum
products (ATSDR 2005).
The Protection of Groundwater PSRG is determined by the DEQ using conservative assumptions
about the potential for a chemical to leach from soil at a concentration that would exceed the
North Carolina Administrative Code (NCAC) Title 15A, Chapter 2, Subchapter 2L Groundwater
Classifications and Standards (21L Standard) or Interim Allowable Concentration (IMAC). In order
to determine a Site -specific leaching potential for this chemical, Headwater requested the
laboratory complete Synthetic Precipitation Leaching Procedure (SPLP) by EPA method 1312 for
analysis of 1-Methylnapthalene in material collected from sample location S-12. SPLP analysis is
used to assess the mobility of organic and inorganic constituents in liquids and solids.
The results of the SPLP analysis indicate that concentrations of 1-Methyl napthalene in the
leachate from S-12 are not present at a concentration above the laboratory method detection limit
of 2 pg/L. SPLP analysis results are summarized on Table 2. The IMAC for 1-Methylnapthalene
is 1 pg/L. As such, Headwater performed a Tier 2 Risk Evaluation to further evaluate leaching
potential.
4.1 Tier 2 Risk Evaluation
Headwater performed a Tier 1 Risk Screening and Tier 2 Risk Evaluation in accordance with the
guidelines outlined in DEQ's Technical Guidance for Risk -Based Remediation document dated
March 2017 (DEQ 2017), and the North Carolina Department of Environmental Quality Risk
Calculator User Guide dated May 2019 (DEQ 2019).
Headwater Geology 16

Cashiers Lake —Pre -Dredging Assessment
Sediment sample analytical results did not exceed the Residential or Industrial/Commercial
PSRGs. Therefore, no unacceptable risk associated with direct contact with sediment was
identified.
The Tier 2 Risk Evaluation was performed to evaluate the source soil to groundwater contaminant
migration pathway. As such, the most elevated concentration of detected compounds
(1-Methylnapthalene and 2-Methyl napthalene detected in sample S-12) in sediment was used in
in the most recent DEQ Risk Calculator (Version Date: December 2019).
The default distance of 0 feet from the source soil to the point of exposure was used which
considers vertical leaching to groundwater below source soil. The leaching calculation assumes
an unlimited source mass to evaluate chronic exposure. The following assumptions were used in
the calculation:
• length of affected soil of 112 feet (the approximate distance between sample points).
hydraulic conductivity of 2x10-5 cm/d, which is consistent with fine to medium sand
hydraulic gradient of 0.05
• Aquifer thickness of 20 feet
The calculated groundwater concentration for 1-Methyl napthalene and 2-Methylnapthalene is
0.082 and 0.14 pg/L, respectively. These values are below the IMAC (1 pg/L) and 2L Standard
(30 pg/L) for 1-Methylnapthalene and 2-Methylnapthalene, respectively. The Tier 2 Risk
Evaluation data sheet is included in Appendix B.
Headwater Geology 17

Cashiers Lake —Pre -Dredging Assessment
5 Conclusions and Recommendations
Based on the result of this assessment, COCs were not detected in sediment at concentrations
above the Residential or Industrial/Commercial PSRGs. Therefore, no unacceptable risk
associated with direct contact with sediment was identified.
One compound (1-Methyinapthalene) in sample S-12 was detected at a concentration above the
Protection of Groundwater PSRG. However, the results of a Site -specific leaching evaluation and
Tier 2 Contaminant Migration Risk Evaluation indicate that an unacceptable risk of this compound
leaching to groundwater at concentrations in excess of the IMAC was not identified.
These results indicate that dredge material is acceptable for unrestricted use and can be used as
beneficial fill in accordance with applicable permitting and regulatory standards. No further
assessment of proposed dredge material is recommended.
Headwater Geology 18

Cashiers Lake —Pre -Dredging Assessment
6 References
Agency for Toxic Substances and Disease Registry (ATSDR). Public Health Statement —
Naphthalene, 1-Methylnaphthalene, and 2-Methylnaphthalene. August
Headwater 2018. Pre -Dredge Environmental Review. December 14
Headwater 2019. Pre -Dredge Assessment Plan —Revision 1. December 18
B&G 2007a. Initial Soil Sampling Report —Consolidated Metco, Inc. Cashiers Plant. February
2007
B&G 2007b. Soil and Groundwater Sampling Report —Consolidated Metco, Inc. Cashiers Plant.
August 2007
B&G 2008a. Comprehensive Site Assessment Report —Consolidated Metco, Inc. Cashiers
Plant. January 2008
B&G 2008b. Soil and Groundwater Remediation Report, Consolidated Metco, Inc. Cashiers
Plant. December 2008.
DEQ 2017. Technical Guidance for Risk -Based Remediation. March 2017.
DEQ 2019. North Carolina Department of Environmental Quality Risk Calculator User Guide.
May.
DEQ-Division of Waste Management Site Locator Tool. Incident #88035. Accessed between
November 25 and 26, 2019.
Pacific Northwest Laboratory. Visual Sample Plan Software, Version 7.12. April 25, 2019
TSC - Bureau of Reclamation 2017. Dam Removal Analysis Guidelines for Sediment. Advisory
Committee on Water Information Subcommittee on Sedimentation. December 2017
USEPA 1984. Development Document for Effluent Limitations Guidelines for Plastics Molding
and Forming. December 1984
USEPA 1998. Evaluation of Dredged Material Proposed for Discharge to Waters of the U.S —
Testing Manual (Inland Testing Manual). February 1998
Headwater Geology 19

FIGURES

8
01.r� $ a
as '. � � . 1 • l
1 • •��•�
%r 3 t �i� 0 Project area
CcooI�
14
l l0 1 • ��
1113 � � i i d Al
lC
y ° ' - - y� •� 11 �� � • � L
4 0 °�as�a��'w .� I ''�• . y�• a $��; r •� "y � , �1, C /
a` ° ►� i i 1 12
s S o r� •,a M+ N
Pt
a
a � � � 433 Gglf
J
R
11
11 `
. 4.
jl e rah4-h -
Legend IIU) -
1
Proposed dredging area 'ry . Feet
1,000 2,000 4,000
SOURCE FIGURE 1
Headwater USGS SITE LOCATION MAP
./ ENV I RON MENTAL I N c. 7.5-minute Topographic Quadrangles Cashiers Canoe Club
Cashiers, North Carolina (1997) Cashiers, Jackson County
Date: 11/25/2019 Contour Interval = 40 feet North Carolina
Headwater Project # A20-111
1 inch = 2,000 feet
Prepared by: NJC //

r
Cashiers Lake
Legend
Proposed dredging area
Former Metco plant location
Surface waters
Note: This is not a survey. All locations are approximate.
Feet
0 200 400 800
Headwater
SOURCE
NC One Map
FIGURE 2
SITE LAYOUT MAP
E N V I R O N M E N T A L I N C.
Orthoimagery (2015)
ArcGIS Online
Waterbodies and Rivers of Jackson
Cashiers Canoe Club
I Cashiers, Jackson County
North Carolina
Date:
3/3/2020
County, NC
Headwater Project # A120-111
Prepared by:
NJC
" 1 inch = 400 feet

03
c
3
N
N
N
0
d SB-3
R •
Frar�pJ\er
S-1
X
3
S-2
BG-1 • s
•
S-7
S-4
S-5
S-8
♦S-9
S-10
S-11
S-12
SB-2
• S-14
♦ S-13
S-15
~S+ N
0
U
Legend
Proposed dredging area
Surface waters
2020 dredge sampling location
• Headwater 2018 sampling location
Note: This is not a survey. All locations are approximate.
Headwater
ENVIRONMENTAL INC.
Date: 3/3/2020
Prepared by: NJC
Cashiers Lake
SOURCE
NC One Map
Orthoimagery (2015) and NC Routes
ArcGIS Online
Waterbodies and Rivers of Jackson
County, NC
/ N 1 inch = 200 feet
BG-2
R
I?,-oe
Gar
Feet I I
0 100 200 400
FIGURE 3
DREDGE SAMPLE LOCATION
MAP
Cashiers Canoe Club
Cashiers, Jackson County
North Carolina
Headwater Project # A20-111

TABLES

Table 1
Sediment Analytical Results Summary
Cashiers Canoe Club
Well ID
Sample Collection
Date
Volatile Organic
Compounds (mg/Kg)
Semi Volatile Organic Compounds
(mg/Kg)
Acetone
1-Methylnaphthalene
2-Methylnaphthalene
S-1
2/11/2020
<0.230
<0.037
<0.037
S-2
2/11/2020
<0.187
<0.032
<0.032
S-3
2/11/2020
<0.522
<0.050
<0.050
S-4
2/11/2020
<0.309
<0.20
<0.20
S-5
2/11/2020
<0.233
<0.17
<0.17
S-6
2/11/2020
0.406
<0.063
<0.063
S-7
2/11/2020
<0.202
<0.020
<0.020
S-8
2/12/2020
0.538
<0.029
<0.029
DUP-1 (S-8)
2/12/2020
<0.300
<0.024
<0.024
S-9
2/12/2020
<0.127
<0.019
<0.019
5-10
2/12/2020
<0.315
<0.034
<0.034
5-11
2/12/2020
<0.304
<0.037
<0.037
5-12
2/12/2020
<0.342
0.17
0.28
5-13
2/12/2020
<0.280
<0.037
<0.037
5-14
2/12/2020
<0.354
<0.030
<0.030
5-15
2/12/2020
<0.229
<0.034
<0.034
Soil -to -Water Soil Remediation Goal
25
0.11
3.1
Residential Soil Remediation Goal
12,000
18
48
Industrial/Commercial Soil Remediation Goal
140,000
73
600
Notes:
Hits only
This table only includes compounds that were detected above the laboratory reporting limit or limit of
quantitation. For a completelist of analyzed constituents, see the laboratory analytical report.
mg/Kg
milligrams per kilogram
<0.230
Indicates the constituent was not detected at a concentration above the laboratory reporting limit or
limit of quantitation.
0.406
Detected concentrations are shown in bold.
8.6
Grey shading indicates an exceedance of the Soil -to -Water Soil Remediation Goal.
Page 1 of 1

Table 2
Site -Specific Leaching Potential Results
Cashiers Canoe Club
Sample ID:
S-12
Date Collected:
2/12/2020
Units:
µg/L
SPLP - SVOCs by EPA 8270
2L Standard
Result
1-Methylnaphthalene
1
< 2.0
Notes:
SPLP Synthetic precipitation leaching procedure
SVOC Semi -volatile organic compounds
EPA U.S. Environmental Protection Agency
21-standard North Carolina Administrative Code (NCAC) Title 15A, Chapter 2, Subchapter 2L- Groundwater
Classifications and Standards, and Interim Allowable Concentrations (IMAC) DENR (Last Amended April 1, 2013)
µg/L micrograms per liter
< 2.0 Indicates constituent concentration was not detected above the method detection limit (DL).

APPENDICES

APPENDIX A
LABORATORY ANALYTICAL REPORT

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
March 04, 2020
Mr. Mike Falknor
Headwater Environmental, Inc.
43 College Place, Suite 212
Asheville, NC 28801
RE: Project: A19-158-02
Pace Project No.: 92464978
Dear Mr. Falknor:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Revised Report. SPLP 8270 added to S-12.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Mr. Adam Tripp, Headwater Environmental, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 114

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Project: A19-158-02
Pace Project No.: 92464978
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 114

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
A19-158-02
92464978
Analytes
Lab lD
Sample ID
Method
Analysts
Reported
Laboratory
92464978001
S-1
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978002
S-2
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978003
S-3
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978004
S-4
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978005
S-5
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978006
S-6
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978007
S-7
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978008
S-8
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978009
S-9
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978010
S-10
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978011
S-11
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978012
S-12
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978013
S-13
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978014
S-14
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978015
S-15
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92464978016
DUP-1
EPA 8260D
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 114

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-1 Lab ID: 92464978001 Collected: 02/11/20 14:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
230
1
02/17/20 09:45
02/17/20 19:35
67-64-1
Benzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
71-43-2
Bromobenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
108-86-1
Bromochloromethane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
74-97-5
Bromodichloromethane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
75-27-4
Bromoform
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
75-25-2
Bromomethane
ND
ug/kg
23.0
1
02/17/20 09:45
02/17/20 19:35
74-83-9
2-Butanone (MEK)
ND
ug/kg
230
1
02/17/20 09:45
02/17/20 19:35
78-93-3
n-Butylbenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
104-51-8
sec-Butylbenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
135-98-8
tert-Butyl benzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
98-06-6
Carbon tetrachloride
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
56-23-5
Chlorobenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
108-90-7
Chloroethane
ND
ug/kg
23.0
1
02/17/20 09:45
02/17/20 19:35
75-00-3
Chloroform
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
67-66-3
Chloromethane
ND
ug/kg
23.0
1
02/17/20 09:45
02/17/20 19:35
74-87-3
2-Chlorotoluene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
95-49-8
4-Chlorotoluene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
96-12-8
Dibromochloromethane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
106-93-4
Dibromomethane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
106-46-7
Dichlorodifluoromethane
ND
ug/kg
23.0
1
02/17/20 09:45
02/17/20 19:35
75-71-8
1,1-Dichloroethane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
75-34-3
1,2-Dichloroethane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
107-06-2
1,1-Dichloroethene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
156-60-5
1,2-Dichloropropane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
78-87-5
1,3-Dichloropropane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
142-28-9
2,2-Dichloropropane
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
594-20-7
1,1-Dichloropropene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
10061-02-6
Diisopropyl ether
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
108-20-3
Ethylbenzene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
87-68-3
2-Hexanone
ND
ug/kg
115
1
02/17/20 09:45
02/17/20 19:35
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
98-82-8
p-Isopropyltoluene
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
99-87-6
Methylene Chloride
ND
ug/kg
46.0
1
02/17/20 09:45
02/17/20 19:35
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
115
1
02/17/20 09:45
02/17/20 19:35
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
1634-04-4
REPORT OF LABORATORY ANALYSIS
Qual
L1.v1
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-1 Lab ID: 92464978001 Collected: 02/11/20 14:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
91-20-3
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
103-65-1
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
100-42-5
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
630-20-6
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
79-34-5
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
127-18-4
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
108-88-3
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
87-61-6
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
120-82-1
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
71-55-6
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
79-00-5
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
79-01-6
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
75-69-4
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
96-18-4
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
95-63-6
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
108-67-8
ND
ug/kg
115
1
02/17/20 09:45
02/17/20 19:35
108-05-4 L1,v1
ND
ug/kg
23.0
1
02/17/20 09:45
02/17/20 19:35
75-01-4
ND
ug/kg
23.0
1
02/17/20 09:45
02/17/20 19:35
1330-20-7
ND
ug/kg
23.0
1
02/17/20 09:45
02/17/20 19:35
179601-23-1
ND
ug/kg
11.5
1
02/17/20 09:45
02/17/20 19:35
95-47-6
100
%
70-130
1
02/17/20 09:45
02/17/20 19:35
2037-26-5
100
%
70-130
1
02/17/20 09:45
02/17/20 19:35
460-00-4
101
%
70-132
1
02/17/20 09:45
02/17/20 19:35
17060-07-0
Analytical Method: ASTM D2974-87
55.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:45
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-2 Lab ID: 92464978002 Collected: 02/11/20 14:30 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
187
1
02/19/20 09:35
02/19/20 12:49
67-64-1
Benzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
71-43-2
Bromobenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
108-86-1
Bromochloromethane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
74-97-5
Bromodichloromethane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
75-27-4
Bromoform
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
75-25-2
Bromomethane
ND
ug/kg
18.7
1
02/19/20 09:35
02/19/20 12:49
74-83-9
2-Butanone (MEK)
ND
ug/kg
187
1
02/19/20 09:35
02/19/20 12:49
78-93-3
n-Butylbenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
104-51-8
sec-Butylbenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
135-98-8
tert-Butyl benzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
98-06-6
Carbon tetrachloride
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
56-23-5
Chlorobenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
108-90-7
Chloroethane
ND
ug/kg
18.7
1
02/19/20 09:35
02/19/20 12:49
75-00-3
Chloroform
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
67-66-3
Chloromethane
ND
ug/kg
18.7
1
02/19/20 09:35
02/19/20 12:49
74-87-3
2-Chlorotoluene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
95-49-8
4-Chlorotoluene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
96-12-8
Dibromochloromethane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
106-93-4
Dibromomethane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
106-46-7
Dichlorodifluoromethane
ND
ug/kg
18.7
1
02/19/20 09:35
02/19/20 12:49
75-71-8
1,1-Dichloroethane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
75-34-3
1,2-Dichloroethane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
107-06-2
1,1-Dichloroethene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
156-60-5
1,2-Dichloropropane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
78-87-5
1,3-Dichloropropane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
142-28-9
2,2-Dichloropropane
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
594-20-7
1,1-Dichloropropene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
10061-02-6
Diisopropyl ether
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
108-20-3
Ethylbenzene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
87-68-3
2-Hexanone
ND
ug/kg
93.6
1
02/19/20 09:35
02/19/20 12:49
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
98-82-8
p-Isopropyltoluene
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
99-87-6
Methylene Chloride
ND
ug/kg
37.4
1
02/19/20 09:35
02/19/20 12:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
93.6
1
02/19/20 09:35
02/19/20 12:49
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-2 Lab ID: 92464978002 Collected: 02/11/20 14:30 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
91-20-3
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
103-65-1
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
100-42-5
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
630-20-6
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
79-34-5
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
127-18-4
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
108-88-3
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
87-61-6
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
120-82-1
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
71-55-6
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
79-00-5
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
79-01-6
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
75-69-4
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
96-18-4
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
95-63-6
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
108-67-8
ND
ug/kg
93.6
1
02/19/20 09:35
02/19/20 12:49
108-05-4
ND
ug/kg
18.7
1
02/19/20 09:35
02/19/20 12:49
75-01-4
ND
ug/kg
18.7
1
02/19/20 09:35
02/19/20 12:49
1330-20-7
ND
ug/kg
18.7
1
02/19/20 09:35
02/19/20 12:49
179601-23-1
ND
ug/kg
9.4
1
02/19/20 09:35
02/19/20 12:49
95-47-6
103
%
70-130
1
02/19/20 09:35
02/19/20 12:49
2037-26-5
96
%
70-130
1
02/19/20 09:35
02/19/20 12:49
460-00-4
99
%
70-132
1
02/19/20 09:35
02/19/20 12:49
17060-07-0
Analytical Method: ASTM D2974-87
47.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:45
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-3 Lab ID: 92464978003 Collected: 02/11/20 15:15 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
522
1
02/19/20 09:35
02/19/20 13:14
67-64-1
Benzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
71-43-2
Bromobenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
108-86-1
Bromochloromethane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
74-97-5
Bromodichloromethane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
75-27-4
Bromoform
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
75-25-2
Bromomethane
ND
ug/kg
52.2
1
02/19/20 09:35
02/19/20 13:14
74-83-9
2-Butanone (MEK)
ND
ug/kg
522
1
02/19/20 09:35
02/19/20 13:14
78-93-3
n-Butylbenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
104-51-8
sec-Butylbenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
135-98-8
tert-Butyl benzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
98-06-6
Carbon tetrachloride
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
56-23-5
Chlorobenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
108-90-7
Chloroethane
ND
ug/kg
52.2
1
02/19/20 09:35
02/19/20 13:14
75-00-3
Chloroform
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
67-66-3
Chloromethane
ND
ug/kg
52.2
1
02/19/20 09:35
02/19/20 13:14
74-87-3
2-Chlorotoluene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
95-49-8
4-Chlorotoluene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
96-12-8
Dibromochloromethane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
106-93-4
Dibromomethane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
106-46-7
Dichlorodifluoromethane
ND
ug/kg
52.2
1
02/19/20 09:35
02/19/20 13:14
75-71-8
1,1-Dichloroethane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
75-34-3
1,2-Dichloroethane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
107-06-2
1,1-Dichloroethene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
156-60-5
1,2-Dichloropropane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
78-87-5
1,3-Dichloropropane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
142-28-9
2,2-Dichloropropane
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
594-20-7
1,1-Dichloropropene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
10061-02-6
Diisopropyl ether
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
108-20-3
Ethylbenzene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
87-68-3
2-Hexanone
ND
ug/kg
261
1
02/19/20 09:35
02/19/20 13:14
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
98-82-8
p-Isopropyltoluene
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
99-87-6
Methylene Chloride
ND
ug/kg
104
1
02/19/20 09:35
02/19/20 13:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
261
1
02/19/20 09:35
02/19/20 13:14
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-3 Lab ID: 92464978003 Collected: 02/11/20 15:15 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
91-20-3
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
103-65-1
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
100-42-5
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
630-20-6
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
79-34-5
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
127-18-4
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
108-88-3
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
87-61-6
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
120-82-1
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
71-55-6
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
79-00-5
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
79-01-6
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
75-69-4
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
96-18-4
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
95-63-6
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
108-67-8
ND
ug/kg
261
1
02/19/20 09:35
02/19/20 13:14
108-05-4
ND
ug/kg
52.2
1
02/19/20 09:35
02/19/20 13:14
75-01-4
ND
ug/kg
52.2
1
02/19/20 09:35
02/19/20 13:14
1330-20-7
ND
ug/kg
52.2
1
02/19/20 09:35
02/19/20 13:14
179601-23-1
ND
ug/kg
26.1
1
02/19/20 09:35
02/19/20 13:14
95-47-6
104
%
70-130
1
02/19/20 09:35
02/19/20 13:14
2037-26-5
97
%
70-130
1
02/19/20 09:35
02/19/20 13:14
460-00-4
96
%
70-132
1
02/19/20 09:35
02/19/20 13:14
17060-07-0
Analytical Method: ASTM D2974-87
69.7 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:45
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-4 Lab ID: 92464978004 Collected: 02/11/20 15:45 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
309
1
02/19/20 09:35
02/19/20 13:38
67-64-1
Benzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
71-43-2
Bromobenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
108-86-1
Bromochloromethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
74-97-5
Bromodichloromethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
75-27-4
Bromoform
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
75-25-2
Bromomethane
ND
ug/kg
30.9
1
02/19/20 09:35
02/19/20 13:38
74-83-9
2-Butanone (MEK)
ND
ug/kg
309
1
02/19/20 09:35
02/19/20 13:38
78-93-3
n-Butylbenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
104-51-8
sec-Butylbenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
135-98-8
tert-Butyl benzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
98-06-6
Carbon tetrachloride
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
56-23-5
Chlorobenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
108-90-7
Chloroethane
ND
ug/kg
30.9
1
02/19/20 09:35
02/19/20 13:38
75-00-3
Chloroform
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
67-66-3
Chloromethane
ND
ug/kg
30.9
1
02/19/20 09:35
02/19/20 13:38
74-87-3
2-Chlorotoluene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
95-49-8
4-Chlorotoluene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
96-12-8
Dibromochloromethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
106-93-4
Dibromomethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
106-46-7
Dichlorodifluoromethane
ND
ug/kg
30.9
1
02/19/20 09:35
02/19/20 13:38
75-71-8
1,1-Dichloroethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
75-34-3
1,2-Dichloroethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
107-06-2
1,1-Dichloroethene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
156-60-5
1,2-Dichloropropane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
78-87-5
1,3-Dichloropropane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
142-28-9
2,2-Dichloropropane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
594-20-7
1,1-Dichloropropene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
10061-02-6
Diisopropyl ether
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
108-20-3
Ethylbenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
87-68-3
2-Hexanone
ND
ug/kg
154
1
02/19/20 09:35
02/19/20 13:38
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
98-82-8
p-Isopropyltoluene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
99-87-6
Methylene Chloride
ND
ug/kg
61.8
1
02/19/20 09:35
02/19/20 13:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
154
1
02/19/20 09:35
02/19/20 13:38
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 114

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Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-4
Lab ID: 92464978004
Collected: 02/11/20 15:45
Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
826013/5035A Volatile Organics
Analytical Method:
EPA 8260D
Preparation Method:
EPA 5035A
Naphthalene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
91-20-3
n-Propylbenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
103-65-1
Styrene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
79-34-5
Tetrachloroethene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
127-18-4
Toluene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
79-00-5
Trichloroethene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
79-01-6
Trichlorofluoromethane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
108-67-8
Vinyl acetate
ND
ug/kg
154
1
02/19/20 09:35
02/19/20 13:38
108-05-4
Vinyl chloride
ND
ug/kg
30.9
1
02/19/20 09:35
02/19/20 13:38
75-01-4
Xylene (Total)
ND
ug/kg
30.9
1
02/19/20 09:35
02/19/20 13:38
1330-20-7
m&p-Xylene
ND
ug/kg
30.9
1
02/19/20 09:35
02/19/20 13:38
179601-23-1
o-Xylene
ND
ug/kg
15.4
1
02/19/20 09:35
02/19/20 13:38
95-47-6
Surrogates
Toluene-d8 (S)
104
%
70-130
1
02/19/20 09:35
02/19/20 13:38
2037-26-5 1g
4-Bromofluorobenzene (S)
76
%
70-130
1
02/19/20 09:35
02/19/20 13:38
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-132
1
02/19/20 09:35
02/19/20 13:38
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
62.6
%
0.10
1
02/14/20 13:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-5 Lab ID: 92464978005 Collected: 02/11/20 16:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
233
1
02/19/20 09:35
02/19/20 14:03
67-64-1
Benzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
71-43-2
Bromobenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
108-86-1
Bromochloromethane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
74-97-5
Bromodichloromethane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
75-27-4
Bromoform
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
75-25-2
Bromomethane
ND
ug/kg
23.3
1
02/19/20 09:35
02/19/20 14:03
74-83-9
2-Butanone (MEK)
ND
ug/kg
233
1
02/19/20 09:35
02/19/20 14:03
78-93-3
n-Butylbenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
104-51-8
sec-Butylbenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
135-98-8
tert-Butyl benzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
98-06-6
Carbon tetrachloride
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
56-23-5
Chlorobenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
108-90-7
Chloroethane
ND
ug/kg
23.3
1
02/19/20 09:35
02/19/20 14:03
75-00-3
Chloroform
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
67-66-3
Chloromethane
ND
ug/kg
23.3
1
02/19/20 09:35
02/19/20 14:03
74-87-3
2-Chlorotoluene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
95-49-8
4-Chlorotoluene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
96-12-8
Dibromochloromethane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
106-93-4
Dibromomethane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
106-46-7
Dichlorodifluoromethane
ND
ug/kg
23.3
1
02/19/20 09:35
02/19/20 14:03
75-71-8
1,1-Dichloroethane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
75-34-3
1,2-Dichloroethane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
107-06-2
1,1-Dichloroethene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
156-60-5
1,2-Dichloropropane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
78-87-5
1,3-Dichloropropane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
142-28-9
2,2-Dichloropropane
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
594-20-7
1,1-Dichloropropene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
10061-02-6
Diisopropyl ether
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
108-20-3
Ethylbenzene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
87-68-3
2-Hexanone
ND
ug/kg
117
1
02/19/20 09:35
02/19/20 14:03
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
98-82-8
p-Isopropyltoluene
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
99-87-6
Methylene Chloride
ND
ug/kg
46.7
1
02/19/20 09:35
02/19/20 14:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
117
1
02/19/20 09:35
02/19/20 14:03
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-5 Lab ID: 92464978005 Collected: 02/11/20 16:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
91-20-3
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
103-65-1
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
100-42-5
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
630-20-6
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
79-34-5
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
127-18-4
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
108-88-3
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
87-61-6
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
120-82-1
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
71-55-6
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
79-00-5
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
79-01-6
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
75-69-4
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
96-18-4
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
95-63-6
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
108-67-8
ND
ug/kg
117
1
02/19/20 09:35
02/19/20 14:03
108-05-4
ND
ug/kg
23.3
1
02/19/20 09:35
02/19/20 14:03
75-01-4
ND
ug/kg
23.3
1
02/19/20 09:35
02/19/20 14:03
1330-20-7
ND
ug/kg
23.3
1
02/19/20 09:35
02/19/20 14:03
179601-23-1
ND
ug/kg
11.7
1
02/19/20 09:35
02/19/20 14:03
95-47-6
101
%
70-130
1
02/19/20 09:35
02/19/20 14:03
2037-26-5
85
%
70-130
1
02/19/20 09:35
02/19/20 14:03
460-00-4
103
%
70-132
1
02/19/20 09:35
02/19/20 14:03
17060-07-0
Analytical Method: ASTM D2974-87
54.8 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:46
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-6 Lab ID: 92464978006 Collected: 02/11/20 16:30 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
406
ug/kg
387
1
02/19/20 09:35
02/19/20 14:28
67-64-1
Benzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
71-43-2
Bromobenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
108-86-1
Bromochloromethane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
74-97-5
Bromodichloromethane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
75-27-4
Bromoform
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
75-25-2
Bromomethane
ND
ug/kg
38.7
1
02/19/20 09:35
02/19/20 14:28
74-83-9
2-Butanone (MEK)
ND
ug/kg
387
1
02/19/20 09:35
02/19/20 14:28
78-93-3
n-Butylbenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
104-51-8
sec-Butylbenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
135-98-8
tert-Butyl benzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
98-06-6
Carbon tetrachloride
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
56-23-5
Chlorobenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
108-90-7
Chloroethane
ND
ug/kg
38.7
1
02/19/20 09:35
02/19/20 14:28
75-00-3
Chloroform
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
67-66-3
Chloromethane
ND
ug/kg
38.7
1
02/19/20 09:35
02/19/20 14:28
74-87-3
2-Chlorotoluene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
95-49-8
4-Chlorotoluene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
96-12-8
Dibromochloromethane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
106-93-4
Dibromomethane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
106-46-7
Dichlorodifluoromethane
ND
ug/kg
38.7
1
02/19/20 09:35
02/19/20 14:28
75-71-8
1,1-Dichloroethane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
75-34-3
1,2-Dichloroethane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
107-06-2
1,1-Dichloroethene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
156-60-5
1,2-Dichloropropane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
78-87-5
1,3-Dichloropropane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
142-28-9
2,2-Dichloropropane
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
594-20-7
1,1-Dichloropropene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
10061-02-6
Diisopropyl ether
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
108-20-3
Ethylbenzene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
87-68-3
2-Hexanone
ND
ug/kg
194
1
02/19/20 09:35
02/19/20 14:28
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
98-82-8
p-Isopropyltoluene
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
99-87-6
Methylene Chloride
ND
ug/kg
77.4
1
02/19/20 09:35
02/19/20 14:28
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
194
1
02/19/20 09:35
02/19/20 14:28
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-6 Lab ID: 92464978006 Collected: 02/11/20 16:30 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
91-20-3
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
103-65-1
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
100-42-5
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
630-20-6
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
79-34-5
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
127-18-4
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
108-88-3
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
87-61-6
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
120-82-1
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
71-55-6
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
79-00-5
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
79-01-6
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
75-69-4
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
96-18-4
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
95-63-6
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
108-67-8
ND
ug/kg
194
1
02/19/20 09:35
02/19/20 14:28
108-05-4
ND
ug/kg
38.7
1
02/19/20 09:35
02/19/20 14:28
75-01-4
ND
ug/kg
38.7
1
02/19/20 09:35
02/19/20 14:28
1330-20-7
ND
ug/kg
38.7
1
02/19/20 09:35
02/19/20 14:28
179601-23-1
ND
ug/kg
19.4
1
02/19/20 09:35
02/19/20 14:28
95-47-6
96
%
70-130
1
02/19/20 09:35
02/19/20 14:28
2037-26-5 10
69
%
70-130
1
02/19/20 09:35
02/19/20 14:28
460-00-4 S1
128
%
70-132
1
02/19/20 09:35
02/19/20 14:28
17060-07-0
Analytical Method: ASTM D2974-87
65.7 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:46
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-7 Lab ID: 92464978007 Collected: 02/11/20 17:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
202
1
02/19/20 09:35
02/19/20 14:53
67-64-1
Benzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
71-43-2
Bromobenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
108-86-1
Bromochloromethane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
74-97-5
Bromodichloromethane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
75-27-4
Bromoform
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
75-25-2
Bromomethane
ND
ug/kg
20.2
1
02/19/20 09:35
02/19/20 14:53
74-83-9
2-Butanone (MEK)
ND
ug/kg
202
1
02/19/20 09:35
02/19/20 14:53
78-93-3
n-Butylbenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
104-51-8
sec-Butylbenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
135-98-8
tert-Butyl benzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
98-06-6
Carbon tetrachloride
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
56-23-5
Chlorobenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
108-90-7
Chloroethane
ND
ug/kg
20.2
1
02/19/20 09:35
02/19/20 14:53
75-00-3
Chloroform
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
67-66-3
Chloromethane
ND
ug/kg
20.2
1
02/19/20 09:35
02/19/20 14:53
74-87-3
2-Chlorotoluene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
95-49-8
4-Chlorotoluene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
96-12-8
Dibromochloromethane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
106-93-4
Dibromomethane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
106-46-7
Dichlorodifluoromethane
ND
ug/kg
20.2
1
02/19/20 09:35
02/19/20 14:53
75-71-8
1,1-Dichloroethane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
75-34-3
1,2-Dichloroethane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
107-06-2
1,1-Dichloroethene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
156-60-5
1,2-Dichloropropane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
78-87-5
1,3-Dichloropropane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
142-28-9
2,2-Dichloropropane
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
594-20-7
1,1-Dichloropropene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
10061-02-6
Diisopropyl ether
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
108-20-3
Ethylbenzene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
87-68-3
2-Hexanone
ND
ug/kg
101
1
02/19/20 09:35
02/19/20 14:53
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
98-82-8
p-Isopropyltoluene
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
99-87-6
Methylene Chloride
ND
ug/kg
40.3
1
02/19/20 09:35
02/19/20 14:53
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
101
1
02/19/20 09:35
02/19/20 14:53
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-7 Lab ID: 92464978007 Collected: 02/11/20 17:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
91-20-3
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
103-65-1
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
100-42-5
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
630-20-6
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
79-34-5
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
127-18-4
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
108-88-3
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
87-61-6
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
120-82-1
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
71-55-6
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
79-00-5
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
79-01-6
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
75-69-4
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
96-18-4
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
95-63-6
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
108-67-8
ND
ug/kg
101
1
02/19/20 09:35
02/19/20 14:53
108-05-4
ND
ug/kg
20.2
1
02/19/20 09:35
02/19/20 14:53
75-01-4
ND
ug/kg
20.2
1
02/19/20 09:35
02/19/20 14:53
1330-20-7
ND
ug/kg
20.2
1
02/19/20 09:35
02/19/20 14:53
179601-23-1
ND
ug/kg
10.1
1
02/19/20 09:35
02/19/20 14:53
95-47-6
101
%
70-130
1
02/19/20 09:35
02/19/20 14:53
2037-26-5
93
%
70-130
1
02/19/20 09:35
02/19/20 14:53
460-00-4
101
%
70-132
1
02/19/20 09:35
02/19/20 14:53
17060-07-0
Analytical Method: ASTM D2974-87
49.5 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:46
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-8 Lab ID: 92464978008 Collected: 02/12/20 11:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
538
ug/kg
437
1
02/19/20 09:35
02/19/20 15:18
67-64-1
Benzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
71-43-2
Bromobenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
108-86-1
Bromochloromethane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
74-97-5
Bromodichloromethane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
75-27-4
Bromoform
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
75-25-2
Bromomethane
ND
ug/kg
43.7
1
02/19/20 09:35
02/19/20 15:18
74-83-9
2-Butanone (MEK)
ND
ug/kg
437
1
02/19/20 09:35
02/19/20 15:18
78-93-3
n-Butylbenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
104-51-8
sec-Butylbenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
135-98-8
tert-Butyl benzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
98-06-6
Carbon tetrachloride
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
56-23-5
Chlorobenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
108-90-7
Chloroethane
ND
ug/kg
43.7
1
02/19/20 09:35
02/19/20 15:18
75-00-3
Chloroform
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
67-66-3
Chloromethane
ND
ug/kg
43.7
1
02/19/20 09:35
02/19/20 15:18
74-87-3
2-Chlorotoluene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
95-49-8
4-Chlorotoluene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
96-12-8
Dibromochloromethane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
106-93-4
Dibromomethane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
106-46-7
Dichlorodifluoromethane
ND
ug/kg
43.7
1
02/19/20 09:35
02/19/20 15:18
75-71-8
1,1-Dichloroethane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
75-34-3
1,2-Dichloroethane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
107-06-2
1,1-Dichloroethene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
156-60-5
1,2-Dichloropropane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
78-87-5
1,3-Dichloropropane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
142-28-9
2,2-Dichloropropane
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
594-20-7
1,1-Dichloropropene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
10061-02-6
Diisopropyl ether
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
108-20-3
Ethylbenzene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
87-68-3
2-Hexanone
ND
ug/kg
218
1
02/19/20 09:35
02/19/20 15:18
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
98-82-8
p-Isopropyltoluene
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
99-87-6
Methylene Chloride
ND
ug/kg
87.4
1
02/19/20 09:35
02/19/20 15:18
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
218
1
02/19/20 09:35
02/19/20 15:18
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 114

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-8 Lab ID: 92464978008 Collected: 02/12/20 11:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
91-20-3
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
103-65-1
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
100-42-5
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
630-20-6
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
79-34-5
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
127-18-4
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
108-88-3
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
87-61-6
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
120-82-1
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
71-55-6
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
79-00-5
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
79-01-6
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
75-69-4
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
96-18-4
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
95-63-6
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
108-67-8
ND
ug/kg
218
1
02/19/20 09:35
02/19/20 15:18
108-05-4
ND
ug/kg
43.7
1
02/19/20 09:35
02/19/20 15:18
75-01-4
ND
ug/kg
43.7
1
02/19/20 09:35
02/19/20 15:18
1330-20-7
ND
ug/kg
43.7
1
02/19/20 09:35
02/19/20 15:18
179601-23-1
ND
ug/kg
21.8
1
02/19/20 09:35
02/19/20 15:18
95-47-6
95
%
70-130
1
02/19/20 09:35
02/19/20 15:18
2037-26-5 10
66
%
70-130
1
02/19/20 09:35
02/19/20 15:18
460-00-4 S1
109
%
70-132
1
02/19/20 09:35
02/19/20 15:18
17060-07-0
Analytical Method: ASTM D2974-87
66.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:46
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-9 Lab ID: 92464978009 Collected: 02/12/20 11:30 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
127
1
02/19/20 09:35
02/19/20 15:42
67-64-1
Benzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
71-43-2
Bromobenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
108-86-1
Bromochloromethane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
74-97-5
Bromodichloromethane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
75-27-4
Bromoform
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
75-25-2
Bromomethane
ND
ug/kg
12.7
1
02/19/20 09:35
02/19/20 15:42
74-83-9
2-Butanone (MEK)
ND
ug/kg
127
1
02/19/20 09:35
02/19/20 15:42
78-93-3
n-Butylbenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
104-51-8
sec-Butylbenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
135-98-8
tert-Butyl benzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
98-06-6
Carbon tetrachloride
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
56-23-5
Chlorobenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
108-90-7
Chloroethane
ND
ug/kg
12.7
1
02/19/20 09:35
02/19/20 15:42
75-00-3
Chloroform
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
67-66-3
Chloromethane
ND
ug/kg
12.7
1
02/19/20 09:35
02/19/20 15:42
74-87-3
2-Chlorotoluene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
95-49-8
4-Chlorotoluene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
96-12-8
Dibromochloromethane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
106-93-4
Dibromomethane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.7
1
02/19/20 09:35
02/19/20 15:42
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
10061-02-6
Diisopropyl ether
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
108-20-3
Ethylbenzene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
87-68-3
2-Hexanone
ND
ug/kg
63.3
1
02/19/20 09:35
02/19/20 15:42
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
99-87-6
Methylene Chloride
ND
ug/kg
25.3
1
02/19/20 09:35
02/19/20 15:42
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
63.3
1
02/19/20 09:35
02/19/20 15:42
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-9 Lab ID: 92464978009 Collected: 02/12/20 11:30 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
91-20-3
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
103-65-1
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
100-42-5
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
630-20-6
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
79-34-5
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
127-18-4
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
108-88-3
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
87-61-6
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
120-82-1
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
71-55-6
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
79-00-5
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
79-01-6
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
75-69-4
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
96-18-4
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
95-63-6
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
108-67-8
ND
ug/kg
63.3
1
02/19/20 09:35
02/19/20 15:42
108-05-4
ND
ug/kg
12.7
1
02/19/20 09:35
02/19/20 15:42
75-01-4
ND
ug/kg
12.7
1
02/19/20 09:35
02/19/20 15:42
1330-20-7
ND
ug/kg
12.7
1
02/19/20 09:35
02/19/20 15:42
179601-23-1
ND
ug/kg
6.3
1
02/19/20 09:35
02/19/20 15:42
95-47-6
103
%
70-130
1
02/19/20 09:35
02/19/20 15:42
2037-26-5
97
%
70-130
1
02/19/20 09:35
02/19/20 15:42
460-00-4
99
%
70-132
1
02/19/20 09:35
02/19/20 15:42
17060-07-0
Analytical Method: ASTM D2974-87
23.4 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:46
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-10 Lab ID: 92464978010 Collected: 02/12/20 12:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
315
1
02/19/20 09:35
02/19/20 16:07
67-64-1
Benzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
71-43-2
Bromobenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
108-86-1
Bromochloromethane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
74-97-5
Bromodichloromethane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
75-27-4
Bromoform
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
75-25-2
Bromomethane
ND
ug/kg
31.5
1
02/19/20 09:35
02/19/20 16:07
74-83-9
2-Butanone (MEK)
ND
ug/kg
315
1
02/19/20 09:35
02/19/20 16:07
78-93-3
n-Butylbenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
104-51-8
sec-Butylbenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
135-98-8
tert-Butyl benzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
98-06-6
Carbon tetrachloride
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
56-23-5
Chlorobenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
108-90-7
Chloroethane
ND
ug/kg
31.5
1
02/19/20 09:35
02/19/20 16:07
75-00-3
Chloroform
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
67-66-3
Chloromethane
ND
ug/kg
31.5
1
02/19/20 09:35
02/19/20 16:07
74-87-3
2-Chlorotoluene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
95-49-8
4-Chlorotoluene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
96-12-8
Dibromochloromethane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
106-93-4
Dibromomethane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
106-46-7
Dichlorodifluoromethane
ND
ug/kg
31.5
1
02/19/20 09:35
02/19/20 16:07
75-71-8
1,1-Dichloroethane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
75-34-3
1,2-Dichloroethane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
107-06-2
1,1-Dichloroethene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
156-60-5
1,2-Dichloropropane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
78-87-5
1,3-Dichloropropane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
142-28-9
2,2-Dichloropropane
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
594-20-7
1,1-Dichloropropene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
10061-02-6
Diisopropyl ether
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
108-20-3
Ethylbenzene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
87-68-3
2-Hexanone
ND
ug/kg
157
1
02/19/20 09:35
02/19/20 16:07
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
98-82-8
p-Isopropyltoluene
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
99-87-6
Methylene Chloride
ND
ug/kg
63.0
1
02/19/20 09:35
02/19/20 16:07
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
157
1
02/19/20 09:35
02/19/20 16:07
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-10 Lab ID: 92464978010 Collected: 02/12/20 12:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
91-20-3
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
103-65-1
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
100-42-5
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
630-20-6
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
79-34-5
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
127-18-4
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
108-88-3
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
87-61-6
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
120-82-1
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
71-55-6
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
79-00-5
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
79-01-6
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
75-69-4
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
96-18-4
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
95-63-6
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
108-67-8
ND
ug/kg
157
1
02/19/20 09:35
02/19/20 16:07
108-05-4
ND
ug/kg
31.5
1
02/19/20 09:35
02/19/20 16:07
75-01-4
ND
ug/kg
31.5
1
02/19/20 09:35
02/19/20 16:07
1330-20-7
ND
ug/kg
31.5
1
02/19/20 09:35
02/19/20 16:07
179601-23-1
ND
ug/kg
15.7
1
02/19/20 09:35
02/19/20 16:07
95-47-6
102
%
70-130
1
02/19/20 09:35
02/19/20 16:07
2037-26-5
91
%
70-130
1
02/19/20 09:35
02/19/20 16:07
460-00-4
105
%
70-132
1
02/19/20 09:35
02/19/20 16:07
17060-07-0
Analytical Method: ASTM D2974-87
61.4 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:46
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-11 Lab ID: 92464978011 Collected: 02/12/20 12:20 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
304
1
02/19/20 09:35
02/19/20 16:32
67-64-1
Benzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
71-43-2
Bromobenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
108-86-1
Bromochloromethane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
74-97-5
Bromodichloromethane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
75-27-4
Bromoform
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
75-25-2
Bromomethane
ND
ug/kg
30.4
1
02/19/20 09:35
02/19/20 16:32
74-83-9
2-Butanone (MEK)
ND
ug/kg
304
1
02/19/20 09:35
02/19/20 16:32
78-93-3
n-Butylbenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
104-51-8
sec-Butylbenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
135-98-8
tert-Butyl benzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
98-06-6
Carbon tetrachloride
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
56-23-5
Chlorobenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
108-90-7
Chloroethane
ND
ug/kg
30.4
1
02/19/20 09:35
02/19/20 16:32
75-00-3
Chloroform
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
67-66-3
Chloromethane
ND
ug/kg
30.4
1
02/19/20 09:35
02/19/20 16:32
74-87-3
2-Chlorotoluene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
95-49-8
4-Chlorotoluene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
96-12-8
Dibromochloromethane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
106-93-4
Dibromomethane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
106-46-7
Dichlorodifluoromethane
ND
ug/kg
30.4
1
02/19/20 09:35
02/19/20 16:32
75-71-8
1,1-Dichloroethane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
75-34-3
1,2-Dichloroethane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
107-06-2
1,1-Dichloroethene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
156-60-5
1,2-Dichloropropane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
78-87-5
1,3-Dichloropropane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
142-28-9
2,2-Dichloropropane
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
594-20-7
1,1-Dichloropropene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
10061-02-6
Diisopropyl ether
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
108-20-3
Ethylbenzene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
87-68-3
2-Hexanone
ND
ug/kg
152
1
02/19/20 09:35
02/19/20 16:32
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
98-82-8
p-Isopropyltoluene
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
99-87-6
Methylene Chloride
ND
ug/kg
60.7
1
02/19/20 09:35
02/19/20 16:32
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
152
1
02/19/20 09:35
02/19/20 16:32
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-11 Lab ID: 92464978011 Collected: 02/12/20 12:20 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
91-20-3
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
103-65-1
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
100-42-5
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
630-20-6
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
79-34-5
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
127-18-4
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
108-88-3
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
87-61-6
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
120-82-1
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
71-55-6
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
79-00-5
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
79-01-6
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
75-69-4
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
96-18-4
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
95-63-6
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
108-67-8
ND
ug/kg
152
1
02/19/20 09:35
02/19/20 16:32
108-05-4
ND
ug/kg
30.4
1
02/19/20 09:35
02/19/20 16:32
75-01-4
ND
ug/kg
30.4
1
02/19/20 09:35
02/19/20 16:32
1330-20-7
ND
ug/kg
30.4
1
02/19/20 09:35
02/19/20 16:32
179601-23-1
ND
ug/kg
15.2
1
02/19/20 09:35
02/19/20 16:32
95-47-6
103
%
70-130
1
02/19/20 09:35
02/19/20 16:32
2037-26-5
98
%
70-130
1
02/19/20 09:35
02/19/20 16:32
460-00-4
101
%
70-132
1
02/19/20 09:35
02/19/20 16:32
17060-07-0
Analytical Method: ASTM D2974-87
61.5 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:46
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-12 Lab ID: 92464978012 Collected: 02/12/20 12:40 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
342
1
02/19/20 09:35
02/19/20 16:57
67-64-1
Benzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
71-43-2
Bromobenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
108-86-1
Bromochloromethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
74-97-5
Bromodichloromethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
75-27-4
Bromoform
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
75-25-2
Bromomethane
ND
ug/kg
34.2
1
02/19/20 09:35
02/19/20 16:57
74-83-9
2-Butanone (MEK)
ND
ug/kg
342
1
02/19/20 09:35
02/19/20 16:57
78-93-3
n-Butylbenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
104-51-8
sec-Butylbenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
135-98-8
tert-Butyl benzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
98-06-6
Carbon tetrachloride
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
56-23-5
Chlorobenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
108-90-7
Chloroethane
ND
ug/kg
34.2
1
02/19/20 09:35
02/19/20 16:57
75-00-3
Chloroform
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
67-66-3
Chloromethane
ND
ug/kg
34.2
1
02/19/20 09:35
02/19/20 16:57
74-87-3
2-Chlorotoluene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
95-49-8
4-Chlorotoluene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
96-12-8
Dibromochloromethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
106-93-4
Dibromomethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
106-46-7
Dichlorodifluoromethane
ND
ug/kg
34.2
1
02/19/20 09:35
02/19/20 16:57
75-71-8
1,1-Dichloroethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
75-34-3
1,2-Dichloroethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
107-06-2
1,1-Dichloroethene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
156-60-5
1,2-Dichloropropane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
78-87-5
1,3-Dichloropropane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
142-28-9
2,2-Dichloropropane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
594-20-7
1,1-Dichloropropene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
10061-02-6
Diisopropyl ether
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
108-20-3
Ethylbenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
87-68-3
2-Hexanone
ND
ug/kg
171
1
02/19/20 09:35
02/19/20 16:57
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
98-82-8
p-Isopropyltoluene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
99-87-6
Methylene Chloride
ND
ug/kg
68.4
1
02/19/20 09:35
02/19/20 16:57
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
171
1
02/19/20 09:35
02/19/20 16:57
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-12
Lab ID: 92464978012
Collected: 02/12/20 12:40
Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
826013/5035A Volatile Organics
Analytical Method:
EPA 8260D
Preparation Method:
EPA 5035A
Naphthalene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
91-20-3
n-Propylbenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
103-65-1
Styrene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
79-34-5
Tetrachloroethene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
127-18-4
Toluene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
79-00-5
Trichloroethene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
79-01-6
Trichlorofluoromethane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
108-67-8
Vinyl acetate
ND
ug/kg
171
1
02/19/20 09:35
02/19/20 16:57
108-05-4
Vinyl chloride
ND
ug/kg
34.2
1
02/19/20 09:35
02/19/20 16:57
75-01-4
Xylene (Total)
ND
ug/kg
34.2
1
02/19/20 09:35
02/19/20 16:57
1330-20-7
m&p-Xylene
ND
ug/kg
34.2
1
02/19/20 09:35
02/19/20 16:57
179601-23-1
o-Xylene
ND
ug/kg
17.1
1
02/19/20 09:35
02/19/20 16:57
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
02/19/20 09:35
02/19/20 16:57
2037-26-5 1g
4-Bromofluorobenzene (S)
77
%
70-130
1
02/19/20 09:35
02/19/20 16:57
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-132
1
02/19/20 09:35
02/19/20 16:57
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
55.8
%
0.10
1
02/14/20 13:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-13 Lab ID: 92464978013 Collected: 02/12/20 13:20 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
280
1
02/19/20 09:35
02/19/20 17:21
67-64-1
Benzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
71-43-2
Bromobenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
108-86-1
Bromochloromethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
74-97-5
Bromodichloromethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
75-27-4
Bromoform
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
75-25-2
Bromomethane
ND
ug/kg
28.0
1
02/19/20 09:35
02/19/20 17:21
74-83-9
2-Butanone (MEK)
ND
ug/kg
280
1
02/19/20 09:35
02/19/20 17:21
78-93-3
n-Butylbenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
104-51-8
sec-Butylbenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
135-98-8
tert-Butyl benzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
98-06-6
Carbon tetrachloride
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
56-23-5
Chlorobenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
108-90-7
Chloroethane
ND
ug/kg
28.0
1
02/19/20 09:35
02/19/20 17:21
75-00-3
Chloroform
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
67-66-3
Chloromethane
ND
ug/kg
28.0
1
02/19/20 09:35
02/19/20 17:21
74-87-3
2-Chlorotoluene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
95-49-8
4-Chlorotoluene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
96-12-8
Dibromochloromethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
106-93-4
Dibromomethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
106-46-7
Dichlorodifluoromethane
ND
ug/kg
28.0
1
02/19/20 09:35
02/19/20 17:21
75-71-8
1,1-Dichloroethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
75-34-3
1,2-Dichloroethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
107-06-2
1,1-Dichloroethene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
156-60-5
1,2-Dichloropropane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
78-87-5
1,3-Dichloropropane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
142-28-9
2,2-Dichloropropane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
594-20-7
1,1-Dichloropropene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
10061-02-6
Diisopropyl ether
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
108-20-3
Ethylbenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
87-68-3
2-Hexanone
ND
ug/kg
140
1
02/19/20 09:35
02/19/20 17:21
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
98-82-8
p-Isopropyltoluene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
99-87-6
Methylene Chloride
ND
ug/kg
55.9
1
02/19/20 09:35
02/19/20 17:21
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
140
1
02/19/20 09:35
02/19/20 17:21
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-13
Lab ID: 92464978013
Collected: 02/12/20 13:20
Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
826013/5035A Volatile Organics
Analytical Method:
EPA 8260D
Preparation Method:
EPA 5035A
Naphthalene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
91-20-3
n-Propylbenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
103-65-1
Styrene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
79-34-5
Tetrachloroethene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
127-18-4
Toluene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
79-00-5
Trichloroethene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
79-01-6
Trichlorofluoromethane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
108-67-8
Vinyl acetate
ND
ug/kg
140
1
02/19/20 09:35
02/19/20 17:21
108-05-4
Vinyl chloride
ND
ug/kg
28.0
1
02/19/20 09:35
02/19/20 17:21
75-01-4
Xylene (Total)
ND
ug/kg
28.0
1
02/19/20 09:35
02/19/20 17:21
1330-20-7
m&p-Xylene
ND
ug/kg
28.0
1
02/19/20 09:35
02/19/20 17:21
179601-23-1
o-Xylene
ND
ug/kg
14.0
1
02/19/20 09:35
02/19/20 17:21
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
02/19/20 09:35
02/19/20 17:21
2037-26-5 1g
4-Bromofluorobenzene (S)
71
%
70-130
1
02/19/20 09:35
02/19/20 17:21
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-132
1
02/19/20 09:35
02/19/20 17:21
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
46.6
%
0.10
1
02/14/20 13:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-14 Lab ID: 92464978014 Collected: 02/12/20 13:40 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
354
1
02/19/20 09:35
02/19/20 17:46
67-64-1
Benzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
71-43-2
Bromobenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
108-86-1
Bromochloromethane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
74-97-5
Bromodichloromethane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
75-27-4
Bromoform
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
75-25-2
Bromomethane
ND
ug/kg
35.4
1
02/19/20 09:35
02/19/20 17:46
74-83-9
2-Butanone (MEK)
ND
ug/kg
354
1
02/19/20 09:35
02/19/20 17:46
78-93-3
n-Butylbenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
104-51-8
sec-Butylbenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
135-98-8
tert-Butyl benzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
98-06-6
Carbon tetrachloride
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
56-23-5
Chlorobenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
108-90-7
Chloroethane
ND
ug/kg
35.4
1
02/19/20 09:35
02/19/20 17:46
75-00-3
Chloroform
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
67-66-3
Chloromethane
ND
ug/kg
35.4
1
02/19/20 09:35
02/19/20 17:46
74-87-3
2-Chlorotoluene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
95-49-8
4-Chlorotoluene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
96-12-8
Dibromochloromethane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
106-93-4
Dibromomethane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
106-46-7
Dichlorodifluoromethane
ND
ug/kg
35.4
1
02/19/20 09:35
02/19/20 17:46
75-71-8
1,1-Dichloroethane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
75-34-3
1,2-Dichloroethane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
107-06-2
1,1-Dichloroethene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
156-60-5
1,2-Dichloropropane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
78-87-5
1,3-Dichloropropane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
142-28-9
2,2-Dichloropropane
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
594-20-7
1,1-Dichloropropene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
10061-02-6
Diisopropyl ether
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
108-20-3
Ethylbenzene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
87-68-3
2-Hexanone
ND
ug/kg
177
1
02/19/20 09:35
02/19/20 17:46
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
98-82-8
p-Isopropyltoluene
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
99-87-6
Methylene Chloride
ND
ug/kg
70.9
1
02/19/20 09:35
02/19/20 17:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
177
1
02/19/20 09:35
02/19/20 17:46
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-14 Lab ID: 92464978014 Collected: 02/12/20 13:40 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
91-20-3
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
103-65-1
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
100-42-5
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
630-20-6
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
79-34-5
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
127-18-4
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
108-88-3
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
87-61-6
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
120-82-1
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
71-55-6
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
79-00-5
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
79-01-6
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
75-69-4
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
96-18-4
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
95-63-6
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
108-67-8
ND
ug/kg
177
1
02/19/20 09:35
02/19/20 17:46
108-05-4
ND
ug/kg
35.4
1
02/19/20 09:35
02/19/20 17:46
75-01-4
ND
ug/kg
35.4
1
02/19/20 09:35
02/19/20 17:46
1330-20-7
ND
ug/kg
35.4
1
02/19/20 09:35
02/19/20 17:46
179601-23-1
ND
ug/kg
17.7
1
02/19/20 09:35
02/19/20 17:46
95-47-6
101
%
70-130
1
02/19/20 09:35
02/19/20 17:46
2037-26-5
93
%
70-130
1
02/19/20 09:35
02/19/20 17:46
460-00-4
102
%
70-132
1
02/19/20 09:35
02/19/20 17:46
17060-07-0
Analytical Method: ASTM D2974-87
63.9 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:47
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-15 Lab ID: 92464978015 Collected: 02/12/20 14:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
229
1
02/20/20 09:37
02/20/20 12:29
67-64-1
Benzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
71-43-2
Bromobenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
108-86-1
Bromochloromethane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
74-97-5
Bromodichloromethane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
75-27-4
Bromoform
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
75-25-2
Bromomethane
ND
ug/kg
22.9
1
02/20/20 09:37
02/20/20 12:29
74-83-9
2-Butanone (MEK)
ND
ug/kg
229
1
02/20/20 09:37
02/20/20 12:29
78-93-3
n-Butylbenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
104-51-8
sec-Butylbenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
135-98-8
tert-Butyl benzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
98-06-6
Carbon tetrachloride
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
56-23-5
Chlorobenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
108-90-7
Chloroethane
ND
ug/kg
22.9
1
02/20/20 09:37
02/20/20 12:29
75-00-3
Chloroform
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
67-66-3
Chloromethane
ND
ug/kg
22.9
1
02/20/20 09:37
02/20/20 12:29
74-87-3
2-Chlorotoluene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
95-49-8
4-Chlorotoluene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
96-12-8
Dibromochloromethane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
106-93-4
Dibromomethane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
106-46-7
Dichlorodifluoromethane
ND
ug/kg
22.9
1
02/20/20 09:37
02/20/20 12:29
75-71-8
1,1-Dichloroethane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
75-34-3
1,2-Dichloroethane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
107-06-2
1,1-Dichloroethene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
156-60-5
1,2-Dichloropropane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
78-87-5
1,3-Dichloropropane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
142-28-9
2,2-Dichloropropane
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
594-20-7
1,1-Dichloropropene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
10061-02-6
Diisopropyl ether
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
108-20-3
Ethylbenzene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
87-68-3
2-Hexanone
ND
ug/kg
114
1
02/20/20 09:37
02/20/20 12:29
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
98-82-8
p-Isopropyltoluene
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
99-87-6
Methylene Chloride
ND
ug/kg
45.7
1
02/20/20 09:37
02/20/20 12:29
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
114
1
02/20/20 09:37
02/20/20 12:29
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: S-15 Lab ID: 92464978015 Collected: 02/12/20 14:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
91-20-3
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
103-65-1
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
100-42-5
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
630-20-6
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
79-34-5
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
127-18-4
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
108-88-3
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
87-61-6
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
120-82-1
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
71-55-6
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
79-00-5
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
79-01-6
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
75-69-4
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
96-18-4
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
95-63-6
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
108-67-8
ND
ug/kg
114
1
02/20/20 09:37
02/20/20 12:29
108-05-4
ND
ug/kg
22.9
1
02/20/20 09:37
02/20/20 12:29
75-01-4
ND
ug/kg
22.9
1
02/20/20 09:37
02/20/20 12:29
1330-20-7
ND
ug/kg
22.9
1
02/20/20 09:37
02/20/20 12:29
179601-23-1
ND
ug/kg
11.4
1
02/20/20 09:37
02/20/20 12:29
95-47-6
102
%
70-130
1
02/20/20 09:37
02/20/20 12:29
2037-26-5
98
%
70-130
1
02/20/20 09:37
02/20/20 12:29
460-00-4
95
%
70-132
1
02/20/20 09:37
02/20/20 12:29
17060-07-0
Analytical Method: ASTM D2974-87
55.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:47
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 114

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ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: DUP-1 Lab ID: 92464978016 Collected: 02/12/20 11:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
ug/kg
300
1
02/20/20 09:37
02/20/20 13:02
67-64-1
Benzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
71-43-2
Bromobenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
108-86-1
Bromochloromethane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
74-97-5
Bromodichloromethane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
75-27-4
Bromoform
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
75-25-2
Bromomethane
ND
ug/kg
30.0
1
02/20/20 09:37
02/20/20 13:02
74-83-9
2-Butanone (MEK)
ND
ug/kg
300
1
02/20/20 09:37
02/20/20 13:02
78-93-3
n-Butylbenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
104-51-8
sec-Butylbenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
135-98-8
tert-Butyl benzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
98-06-6
Carbon tetrachloride
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
56-23-5
Chlorobenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
108-90-7
Chloroethane
ND
ug/kg
30.0
1
02/20/20 09:37
02/20/20 13:02
75-00-3
Chloroform
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
67-66-3
Chloromethane
ND
ug/kg
30.0
1
02/20/20 09:37
02/20/20 13:02
74-87-3
2-Chlorotoluene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
95-49-8
4-Chlorotoluene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
96-12-8
Dibromochloromethane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
106-93-4
Dibromomethane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
106-46-7
Dichlorodifluoromethane
ND
ug/kg
30.0
1
02/20/20 09:37
02/20/20 13:02
75-71-8
1,1-Dichloroethane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
75-34-3
1,2-Dichloroethane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
107-06-2
1,1-Dichloroethene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
156-60-5
1,2-Dichloropropane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
78-87-5
1,3-Dichloropropane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
142-28-9
2,2-Dichloropropane
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
594-20-7
1,1-Dichloropropene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
10061-02-6
Diisopropyl ether
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
108-20-3
Ethylbenzene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
87-68-3
2-Hexanone
ND
ug/kg
150
1
02/20/20 09:37
02/20/20 13:02
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
98-82-8
p-Isopropyltoluene
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
99-87-6
Methylene Chloride
ND
ug/kg
59.9
1
02/20/20 09:37
02/20/20 13:02
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
150
1
02/20/20 09:37
02/20/20 13:02
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
1634-04-4
REPORT OF LABORATORY ANALYSIS
I:
v2
Qual
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Al9-158-02
Pace Project No.: 92464978
Sample: DUP-1 Lab ID: 92464978016 Collected: 02/12/20 11:00 Received: 02/13/20 08:11 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
91-20-3
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
103-65-1
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
100-42-5
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
630-20-6
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
79-34-5
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
127-18-4
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
108-88-3
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
87-61-6
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
120-82-1
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
71-55-6
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
79-00-5
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
79-01-6
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
75-69-4
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
96-18-4
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
95-63-6
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
108-67-8
ND
ug/kg
150
1
02/20/20 09:37
02/20/20 13:02
108-05-4
ND
ug/kg
30.0
1
02/20/20 09:37
02/20/20 13:02
75-01-4
ND
ug/kg
30.0
1
02/20/20 09:37
02/20/20 13:02
1330-20-7
ND
ug/kg
30.0
1
02/20/20 09:37
02/20/20 13:02
179601-23-1
ND
ug/kg
15.0
1
02/20/20 09:37
02/20/20 13:02
95-47-6
95
%
70-130
1
02/20/20 09:37
02/20/20 13:02
2037-26-5 10
63
%
70-130
1
02/20/20 09:37
02/20/20 13:02
460-00-4 S1
101
%
70-132
1
02/20/20 09:37
02/20/20 13:02
17060-07-0
Analytical Method: ASTM D2974-87
55.4 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/14/20 13:47
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 114

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QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
QC Batch: 525447 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92464978001
METHOD BLANK: 2808433
Associated Lab Samples: 92464978001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
02/17/20 15:02
1,1,1-Trichloroethane
ug/kg
ND
5.0
02/17/20 15:02
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
02/17/20 15:02
1,1,2-Trichloroethane
ug/kg
ND
5.0
02/17/20 15:02
1,1-Dichloroethane
ug/kg
ND
5.0
02/17/20 15:02
1,1-Dichloroethene
ug/kg
ND
5.0
02/17/20 15:02
1,1-Dichloropropene
ug/kg
ND
5.0
02/17/20 15:02
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
02/17/20 15:02
1,2,3-Trichloropropane
ug/kg
ND
5.0
02/17/20 15:02
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
02/17/20 15:02
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
02/17/20 15:02
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
02/17/20 15:02
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
02/17/20 15:02
1,2-Dichlorobenzene
ug/kg
ND
5.0
02/17/20 15:02
1,2-Dichloroethane
ug/kg
ND
5.0
02/17/20 15:02
1,2-Dichloropropane
ug/kg
ND
5.0
02/17/20 15:02
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
02/17/20 15:02
1,3-Dichlorobenzene
ug/kg
ND
5.0
02/17/20 15:02
1,3-Dichloropropane
ug/kg
ND
5.0
02/17/20 15:02
1,4-Dichlorobenzene
ug/kg
ND
5.0
02/17/20 15:02
2,2-Dichloropropane
ug/kg
ND
5.0
02/17/20 15:02
2-Butanone (MEK)
ug/kg
ND
100
02/17/20 15:02
2-Chlorotoluene
ug/kg
ND
5.0
02/17/20 15:02
2-Hexanone
ug/kg
ND
50.0
02/17/20 15:02
4-Chlorotoluene
ug/kg
ND
5.0
02/17/20 15:02
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
02/17/20 15:02
Acetone
ug/kg
ND
100
02/17/20 15:02
Benzene
ug/kg
ND
5.0
02/17/20 15:02
Bromobenzene
ug/kg
ND
5.0
02/17/20 15:02
Bromochloromethane
ug/kg
ND
5.0
02/17/20 15:02
Bromodichloromethane
ug/kg
ND
5.0
02/17/20 15:02
Bromoform
ug/kg
ND
5.0
02/17/20 15:02
Bromomethane
ug/kg
ND
10.0
02/17/20 15:02 v1
Carbon tetrachloride
ug/kg
ND
5.0
02/17/20 15:02
Chlorobenzene
ug/kg
ND
5.0
02/17/20 15:02
Chloroethane
ug/kg
ND
10.0
02/17/20 15:02
Chloroform
ug/kg
ND
5.0
02/17/20 15:02
Chloromethane
ug/kg
ND
10.0
02/17/20 15:02
cis-1,2-Dichloroethene
ug/kg
ND
5.0
02/17/20 15:02
cis-1,3-Dichloropropene
ug/kg
ND
5.0
02/17/20 15:02
Dibromochloromethane
ug/kg
ND
5.0
02/17/20 15:02
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 114

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QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
METHOD BLANK: 2808433
Matrix:
Solid
Associated Lab Samples: 92464978001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Dibromomethane
ug/kg
ND
5.0
02/17/20 15:02
Dichlorodifluoromethane
ug/kg
ND
10.0
02/17/20 15:02
Diisopropyl ether
ug/kg
ND
5.0
02/17/20 15:02
Ethylbenzene
ug/kg
ND
5.0
02/17/20 15:02
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
02/17/20 15:02
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
02/17/20 15:02
m&p-Xylene
ug/kg
ND
10.0
02/17/20 15:02
Methyl-tert-butyl ether
ug/kg
ND
5.0
02/17/20 15:02
Methylene Chloride
ug/kg
ND
20.0
02/17/20 15:02
n-Butylbenzene
ug/kg
ND
5.0
02/17/20 15:02
n-Propylbenzene
ug/kg
ND
5.0
02/17/20 15:02
Naphthalene
ug/kg
ND
5.0
02/17/20 15:02
o-Xylene
ug/kg
ND
5.0
02/17/20 15:02
p-Isopropyltoluene
ug/kg
ND
5.0
02/17/20 15:02
sec-Butylbenzene
ug/kg
ND
5.0
02/17/20 15:02
Styrene
ug/kg
ND
5.0
02/17/20 15:02
tert-Butyl benzene
ug/kg
ND
5.0
02/17/20 15:02
Tetrachloroethene
ug/kg
ND
5.0
02/17/20 15:02
Toluene
ug/kg
ND
5.0
02/17/20 15:02
trans-1,2-Dichloroethene
ug/kg
ND
5.0
02/17/20 15:02
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
02/17/20 15:02
Trichloroethene
ug/kg
ND
5.0
02/17/20 15:02
Trichlorofluoromethane
ug/kg
ND
5.0
02/17/20 15:02
Vinyl acetate
ug/kg
ND
50.0
02/17/20 15:02
v1
Vinyl chloride
ug/kg
ND
10.0
02/17/20 15:02
Xylene (Total)
ug/kg
ND
10.0
02/17/20 15:02
1,2-Dichloroethane-d4 (S)
%
98
70-132
02/17/20 15:02
4-Bromofluorobenzene (S)
%
100
70-130
02/17/20 15:02
Toluene-d8 (S)
%
102
70-130
02/17/20 15:02
LABORATORY CONTROL SAMPLE & LCSD:
2808434
2808435
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
51.7
55.9
103 112
70-130
8 30
1,1,1-Trichloroethane
ug/kg
50
52.4
57.6
105 115
70-130
9 30
1,1,2,2-Tetrachloroethane
ug/kg
50
48.3
53.0
97 106
55-130
9 30
1,1,2-Trichloroethane
ug/kg
50
53.8
56.1
108 112
70-130
4 30
1,1-Dichloroethane
ug/kg
50
50.1
53.7
100 107
68-130
7 30
1,1-Dichloroethene
ug/kg
50
54.4
59.8
109 120
70-130
9 30
1,1-Dichloropropene
ug/kg
50
57.3
62.1
115 124
70-130
8 30
1,2,3-Trichlorobenzene
ug/kg
50
52.5
55.7
105 111
70-130
6 30
1,2,3-Trichloropropane
ug/kg
50
48.0
49.4
96 99
70-130
3 30
1,2,4-Trichlorobenzene
ug/kg
50
55.2
57.6
110 115
70-130
4 30
1,2,4-Trimethylbenzene
ug/kg
50
50.2
51.0
100 102
69-130
2 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
LABORATORY CONTROL SAMPLE & LCSD:
2808434
2808435
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
1,2-Dibromo-3-chloropropane
ug/kg
50
49.2
54.6
98
109
57-141
10
30
1,2-Dibromoethane (EDB)
ug/kg
50
50.9
55.4
102
111
70-130
8
30
1,2-Dichlorobenzene
ug/kg
50
51.4
52.7
103
105
70-130
2
30
1,2-Dichloroethane
ug/kg
50
49.6
54.4
99
109
70-130
9
30
1,2-Dichloropropane
ug/kg
50
51.8
56.5
104
113
70-130
9
30
1,3,5-Trimethylbenzene
ug/kg
50
49.5
51.5
99
103
70-130
4
30
1,3-Dichlorobenzene
ug/kg
50
51.7
53.1
103
106
70-130
3
30
1,3-Dichloropropane
ug/kg
50
50.5
54.2
101
108
70-130
7
30
1,4-Dichlorobenzene
ug/kg
50
51.6
53.0
103
106
70-130
3
30
2,2-Dichloropropane
ug/kg
50
52.3
57.4
105
115
70-130
9
30
2-Butanone (MEK)
ug/kg
100
104
120
104
120
60-130
15
30
2-Chlorotoluene
ug/kg
50
49.5
51.4
99
103
70-130
4
30
2-Hexanone
ug/kg
100
97.9
105
98
105
70-132
7
30
4-Chlorotoluene
ug/kg
50
50.7
52.6
101
105
70-130
4
30
4-Methyl-2-pentanone (MIBK)
ug/kg
100
98.8
107
99
107
69-130
8
30
Acetone
ug/kg
100
90.3J
104
90
104
49-148
30
Benzene
ug/kg
50
53.9
58.1
108
116
70-130
8
30
Bromobenzene
ug/kg
50
49.8
53.5
100
107
70-130
7
30
Bromochloromethane
ug/kg
50
50.7
55.0
101
110
70-130
8
30
Bromodichloromethane
ug/kg
50
49.8
53.0
100
106
70-130
6
30
Bromoform
ug/kg
50
45.4
49.9
91
100
68-136
9
30
Bromomethane
ug/kg
50
69.8
78.3
140
157
60-140
11
30 L1,v1
Carbon tetrachloride
ug/kg
50
51.9
56.7
104
113
70-130
9
30
Chlorobenzene
ug/kg
50
50.1
53.0
100
106
70-130
6
30
Chloroethane
ug/kg
50
53.0
58.0
106
116
51-147
9
30
Chloroform
ug/kg
50
49.8
55.0
100
110
70-130
10
30
Chloromethane
ug/kg
50
40.6
44.6
81
89
48-130
9
30
cis-1,2-Dichloroethene
ug/kg
50
48.4
53.0
97
106
70-130
9
30
cis-1,3-Dichloropropene
ug/kg
50
52.5
55.9
105
112
70-130
6
30
Dibromochloromethane
ug/kg
50
51.5
55.2
103
110
70-130
7
30
Dibromomethane
ug/kg
50
50.4
54.3
101
109
70-130
7
30
Dichlorodifluoromethane
ug/kg
50
47.6
49.8
95
100
49-130
5
30
Diisopropyl ether
ug/kg
50
53.2
59.2
106
118
66-130
11
30
Ethylbenzene
ug/kg
50
50.0
53.5
100
107
70-130
7
30
Hexachloro-1,3-butadiene
ug/kg
50
56.1
57.9
112
116
70-130
3
30
Isopropylbenzene(Cumene)
ug/kg
50
49.8
53.2
100
106
70-130
6
30
m&p-Xylene
ug/kg
100
99.7
106
100
106
70-130
6
30
Methyl-tert-butyl ether
ug/kg
50
57.6
60.5
115
121
70-130
5
30
Methylene Chloride
ug/kg
50
46.0
51.2
92
102
50-137
11
30
n-Butylbenzene
ug/kg
50
50.6
52.7
101
105
70-130
4
30
n-Propylbenzene
ug/kg
50
49.5
51.9
99
104
70-130
5
30
Naphthalene
ug/kg
50
48.3
51.5
97
103
70-131
6
30
o-Xylene
ug/kg
50
49.1
51.8
98
104
70-130
5
30
p-Isopropyltoluene
ug/kg
50
49.8
52.3
100
105
70-130
5
30
sec-Butylbenzene
ug/kg
50
49.8
51.4
100
103
70-130
3
30
Styrene
ug/kg
50
49.2
52.7
98
105
70-130
7
30
tert-Butyl benzene
ug/kg
50
43.4
46.1
87
92
69-130
6
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 114

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
LABORATORY CONTROL SAMPLE & LCSD:
2808434
2808435
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Tetrachloroethene
ug/kg
50
52.1
56.1
104
112
56-130
7
30
Toluene
ug/kg
50
49.5
53.7
99
107
70-130
8
30
trans-1,2-Dichloroethene
ug/kg
50
50.9
56.3
102
113
70-130
10
30
trans- 1,3-Dichloropropene
ug/kg
50
50.4
55.1
101
110
70-130
9
30
Trichloroethene
ug/kg
50
54.2
58.9
108
118
70-141
8
30
Trichlorofluoromethane
ug/kg
50
49.3
54.3
99
109
67-130
10
30
Vinyl acetate
ug/kg
100
135
141
135
141
10-136
4
30 L1,v1
Vinyl chloride
ug/kg
50
53.9
58.8
108
118
67-130
9
30
Xylene(Total)
ug/kg
150
149
158
99
105
70-130
6
30
1,2-Dichloroethane-d4 (S)
%
97
95
70-132
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8(S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC.
Page 39 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
QC Batch: 525693 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92464978002, 92464978003, 92464978004, 92464978005, 92464978006, 92464978007, 92464978008,
92464978009,92464978010,92464978011,92464978012,92464978013,92464978014
METHOD BLANK: 2809932 Matrix: Solid
Associated Lab Samples: 92464978002, 92464978003, 92464978004, 92464978005, 92464978006, 92464978007, 92464978008,
92464978009,92464978010,92464978011,92464978012,92464978013,92464978014
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
02/19/20 11:59
1,1,1-Trichloroethane
ug/kg
ND
5.0
02/19/20 11:59
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
02/19/20 11:59
1,1,2-Trichloroethane
ug/kg
ND
5.0
02/19/20 11:59
1,1-Dichloroethane
ug/kg
ND
5.0
02/19/20 11:59
1,1-Dichloroethene
ug/kg
ND
5.0
02/19/20 11:59
1,1-Dichloropropene
ug/kg
ND
5.0
02/19/20 11:59
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
02/19/20 11:59
1,2,3-Trichloropropane
ug/kg
ND
5.0
02/19/20 11:59
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
02/19/20 11:59
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
02/19/20 11:59
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
02/19/20 11:59
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
02/19/20 11:59
1,2-Dichlorobenzene
ug/kg
ND
5.0
02/19/20 11:59
1,2-Dichloroethane
ug/kg
ND
5.0
02/19/20 11:59
1,2-Dichloropropane
ug/kg
ND
5.0
02/19/20 11:59
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
02/19/20 11:59
1,3-Dichlorobenzene
ug/kg
ND
5.0
02/19/20 11:59
1,3-Dichloropropane
ug/kg
ND
5.0
02/19/20 11:59
1,4-Dichlorobenzene
ug/kg
ND
5.0
02/19/20 11:59
2,2-Dichloropropane
ug/kg
ND
5.0
02/19/20 11:59
2-Butanone (MEK)
ug/kg
ND
100
02/19/20 11:59
2-Chlorotoluene
ug/kg
ND
5.0
02/19/20 11:59
2-Hexanone
ug/kg
ND
50.0
02/19/20 11:59
4-Chlorotoluene
ug/kg
ND
5.0
02/19/20 11:59
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
02/19/20 11:59
Acetone
ug/kg
ND
100
02/19/20 11:59
Benzene
ug/kg
ND
5.0
02/19/20 11:59
Bromobenzene
ug/kg
ND
5.0
02/19/20 11:59
Bromochloromethane
ug/kg
ND
5.0
02/19/20 11:59
Bromodichloromethane
ug/kg
ND
5.0
02/19/20 11:59
Bromoform
ug/kg
ND
5.0
02/19/20 11:59
Bromomethane
ug/kg
ND
10.0
02/19/20 11:59 IH
Carbon tetrachloride
ug/kg
ND
5.0
02/19/20 11:59
Chlorobenzene
ug/kg
ND
5.0
02/19/20 11:59
Chloroethane
ug/kg
ND
10.0
02/19/20 11:59
Chloroform
ug/kg
ND
5.0
02/19/20 11:59
Chloromethane
ug/kg
ND
10.0
02/19/20 11:59
cis-1,2-Dichloroethene
ug/kg
ND
5.0
02/19/20 11:59
cis-1,3-Dichloropropene
ug/kg
ND
5.0
02/19/20 11:59
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 114

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
METHOD BLANK: 2809932 Matrix: Solid
Associated Lab Samples: 92464978002, 92464978003, 92464978004, 92464978005, 92464978006, 92464978007, 92464978008,
92464978009,92464978010,92464978011,92464978012,92464978013,92464978014
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Dibromochloromethane
ug/kg
ND
5.0
02/19/20 11:59
Dibromomethane
ug/kg
ND
5.0
02/19/20 11:59
Dichlorodifluoromethane
ug/kg
ND
10.0
02/19/20 11:59
Diisopropyl ether
ug/kg
ND
5.0
02/19/20 11:59
Ethylbenzene
ug/kg
ND
5.0
02/19/20 11:59
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
02/19/20 11:59
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
02/19/20 11:59
m&p-Xylene
ug/kg
ND
10.0
02/19/20 11:59
Methyl-tert-butyl ether
ug/kg
ND
5.0
02/19/20 11:59
Methylene Chloride
ug/kg
ND
20.0
02/19/20 11:59 v2
n-Butylbenzene
ug/kg
ND
5.0
02/19/20 11:59
n-Propylbenzene
ug/kg
ND
5.0
02/19/20 11:59
Naphthalene
ug/kg
ND
5.0
02/19/20 11:59
o-Xylene
ug/kg
ND
5.0
02/19/20 11:59
p-Isopropyltoluene
ug/kg
ND
5.0
02/19/20 11:59
sec-Butylbenzene
ug/kg
ND
5.0
02/19/20 11:59
Styrene
ug/kg
ND
5.0
02/19/20 11:59
tert-Butyl benzene
ug/kg
ND
5.0
02/19/20 11:59
Tetrachloroethene
ug/kg
ND
5.0
02/19/20 11:59
Toluene
ug/kg
ND
5.0
02/19/20 11:59
trans-1,2-Dichloroethene
ug/kg
ND
5.0
02/19/20 11:59
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
02/19/20 11:59
Trichloroethene
ug/kg
ND
5.0
02/19/20 11:59
Trichlorofluoromethane
ug/kg
ND
5.0
02/19/20 11:59
Vinyl acetate
ug/kg
ND
50.0
02/19/20 11:59
Vinyl chloride
ug/kg
ND
10.0
02/19/20 11:59
Xylene (Total)
ug/kg
ND
10.0
02/19/20 11:59
1,2-Dichloroethane-d4 (S)
%
101
70-132
02/19/20 11:59
4-Bromofluorobenzene (S)
%
98
70-130
02/19/20 11:59
Toluene-d8 (S)
%
105
70-130
02/19/20 11:59
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2809933
Units
Spike
Conc.
2809934
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
45.1
50.6
90
101
70-130
11
30
1,1,1-Trichloroethane
ug/kg
50
49.5
50.4
99
101
70-130
2
30
1,1,2,2-Tetrachloroethane
ug/kg
50
48.1
47.2
96
94
55-130
2
30
1,1,2-Trichloroethane
ug/kg
50
48.5
48.3
97
97
70-130
0
30
1,1-Dichloroethane
ug/kg
50
49.5
49.9
99
100
68-130
1
30
1,1-Dichloroethene
ug/kg
50
52.7
55.6
105
111
70-130
5
30
1,1-Dichloropropene
ug/kg
50
52.9
56.0
106
112
70-130
6
30
1,2,3-Trichlorobenzene
ug/kg
50
50.5
50.3
101
101
70-130
1
30
1,2,3-Trichloropropane
ug/kg
50
46.8
45.7
94
91
70-130
2
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
LABORATORY CONTROL SAMPLE & LCSD:
2809933
2809934
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/kg
50
50.2
52.4
100
105
70-130
4
30
1,2,4-Trimethylbenzene
ug/kg
50
42.6
48.4
85
97
69-130
13
30
1,2-Dibromo-3-chloropropane
ug/kg
50
48.3
46.9
97
94
57-141
3
30
1,2-Dibromoethane (EDB)
ug/kg
50
48.4
49.1
97
98
70-130
2
30
1,2-Dichlorobenzene
ug/kg
50
44.1
47.8
88
96
70-130
8
30
1,2-Dichloroethane
ug/kg
50
50.1
47.3
100
95
70-130
6
30
1,2-Dichloropropane
ug/kg
50
47.3
48.5
95
97
70-130
3
30
1,3,5-Trimethylbenzene
ug/kg
50
42.5
47.6
85
95
70-130
11
30
1,3-Dichlorobenzene
ug/kg
50
44.3
48.7
89
97
70-130
9
30
1,3-Dichloropropane
ug/kg
50
49.0
50.6
98
101
70-130
3
30
1,4-Dichlorobenzene
ug/kg
50
45.9
48.1
92
96
70-130
5
30
2,2-Dichloropropane
ug/kg
50
51.5
51.8
103
104
70-130
1
30
2-Butanone (MEK)
ug/kg
100
104
103
104
103
60-130
1
30
2-Chlorotoluene
ug/kg
50
43.4
48.5
87
97
70-130
11
30
2-Hexanone
ug/kg
100
98.9
99.8
99
100
70-132
1
30
4-Chlorotoluene
ug/kg
50
45.5
49.3
91
99
70-130
8
30
4-Methyl-2-pentanone (MIBK)
ug/kg
100
92.4
94.9
92
95
69-130
3
30
Acetone
ug/kg
100
108
93.3J
108
93
49-148
30
Benzene
ug/kg
50
47.0
50.9
94
102
70-130
8
30
Bromobenzene
ug/kg
50
44.1
48.1
88
96
70-130
9
30
Bromochloromethane
ug/kg
50
50.0
49.3
100
99
70-130
1
30
Bromodichloromethane
ug/kg
50
45.7
44.6
91
89
70-130
2
30
Bromoform
ug/kg
50
42.9
44.3
86
89
68-136
3
30
Bromomethane
ug/kg
50
62.4
65.5
125
131
60-140
5
30 IH
Carbon tetrachloride
ug/kg
50
48.1
48.8
96
98
70-130
1
30
Chlorobenzene
ug/kg
50
46.0
50.0
92
100
70-130
8
30
Chloroethane
ug/kg
50
44.5
49.0
89
98
51-147
10
30
Chloroform
ug/kg
50
48.7
48.4
97
97
70-130
1
30
Chloromethane
ug/kg
50
38.5
40.8
77
82
48-130
6
30
cis-1,2-Dichloroethene
ug/kg
50
49.2
48.4
98
97
70-130
2
30
cis-1,3-Dichloropropene
ug/kg
50
47.6
48.0
95
96
70-130
1
30
Dibromochloromethane
ug/kg
50
49.3
49.0
99
98
70-130
1
30
Dibromomethane
ug/kg
50
49.8
45.5
100
91
70-130
9
30
Dichlorodifluoromethane
ug/kg
50
37.9
41.7
76
83
49-130
9
30
Diisopropyl ether
ug/kg
50
48.1
53.1
96
106
66-130
10
30
Ethylbenzene
ug/kg
50
44.6
49.3
89
99
70-130
10
30
Hexachloro-1,3-butadiene
ug/kg
50
45.5
48.5
91
97
70-130
6
30
Isopropylbenzene (Cumene)
ug/kg
50
45.6
49.7
91
99
70-130
9
30
m&p-Xylene
ug/kg
100
88.2
98.6
88
99
70-130
11
30
Methyl-tert-butyl ether
ug/kg
50
50.6
54.1
101
108
70-130
7
30
Methylene Chloride
ug/kg
50
37.8
39.7
76
79
50-137
5
30 v3
n-Butylbenzene
ug/kg
50
44.7
50.3
89
101
70-130
12
30
n-Propylbenzene
ug/kg
50
43.6
48.9
87
98
70-130
12
30
Naphthalene
ug/kg
50
47.4
46.8
95
94
70-131
1
30
o-Xylene
ug/kg
50
44.0
48.8
88
98
70-130
10
30
p-Isopropyltoluene
ug/kg
50
43.2
48.4
86
97
70-130
11
30
sec-Butylbenzene
ug/kg
50
43.1
47.7
86
95
70-130
10
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
LABORATORY CONTROL SAMPLE & LCSD:
2809933
2809934
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Styrene
ug/kg
50
45.0
49.2
90
98
70-130
9
30
tert-Butyl benzene
ug/kg
50
37.4
42.5
75
85
69-130
13
30
Tetrachloroethene
ug/kg
50
45.3
51.5
91
103
56-130
13
30
Toluene
ug/kg
50
41.7
45.7
83
91
70-130
9
30
trans-1,2-Dichloroethene
ug/kg
50
52.5
51.4
105
103
70-130
2
30
trans- 1,3-Dichloropropene
ug/kg
50
47.6
46.4
95
93
70-130
3
30
Trichloroethene
ug/kg
50
48.1
51.2
96
102
70-141
6
30
Trichlorofluoromethane
ug/kg
50
44.2
46.8
88
94
67-130
6
30
Vinyl acetate
ug/kg
100
126
130
126
130
10-136
4
30
Vinyl chloride
ug/kg
50
45.5
51.7
91
103
67-130
13
30
Xylene (Total)
ug/kg
150
132
147
88
98
70-130
11
30
1,2-Dichloroethane-d4 (S)
%
114
97
70-132
4-Bromofluorobenzene (S)
%
102
99
70-130
Toluene-d8(S)
%
101
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC.
Page 43 of 114

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
QC Batch: 526104 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92464978015, 92464978016
METHOD BLANK: 2811720
Associated Lab Samples: 92464978015, 92464978016
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
02/20/20 11:15
1,1,1-Trichloroethane
ug/kg
ND
5.0
02/20/20 11:15
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
02/20/20 11:15
1,1,2-Trichloroethane
ug/kg
ND
5.0
02/20/20 11:15
1,1-Dichloroethane
ug/kg
ND
5.0
02/20/20 11:15
1,1-Dichloroethene
ug/kg
ND
5.0
02/20/20 11:15
1,1-Dichloropropene
ug/kg
ND
5.0
02/20/20 11:15
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
02/20/20 11:15
1,2,3-Trichloropropane
ug/kg
ND
5.0
02/20/20 11:15
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
02/20/20 11:15
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
02/20/20 11:15
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
02/20/20 11:15
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
02/20/20 11:15
1,2-Dichlorobenzene
ug/kg
ND
5.0
02/20/20 11:15
1,2-Dichloroethane
ug/kg
ND
5.0
02/20/20 11:15
1,2-Dichloropropane
ug/kg
ND
5.0
02/20/20 11:15
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
02/20/20 11:15
1,3-Dichlorobenzene
ug/kg
ND
5.0
02/20/20 11:15
1,3-Dichloropropane
ug/kg
ND
5.0
02/20/20 11:15
1,4-Dichlorobenzene
ug/kg
ND
5.0
02/20/20 11:15
2,2-Dichloropropane
ug/kg
ND
5.0
02/20/20 11:15
2-Butanone (MEK)
ug/kg
ND
100
02/20/20 11:15
2-Chlorotoluene
ug/kg
ND
5.0
02/20/20 11:15
2-Hexanone
ug/kg
ND
50.0
02/20/20 11:15
4-Chlorotoluene
ug/kg
ND
5.0
02/20/20 11:15
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
02/20/20 11:15
Acetone
ug/kg
ND
100
02/20/20 11:15
Benzene
ug/kg
ND
5.0
02/20/20 11:15
Bromobenzene
ug/kg
ND
5.0
02/20/20 11:15
Bromochloromethane
ug/kg
ND
5.0
02/20/20 11:15
Bromodichloromethane
ug/kg
ND
5.0
02/20/20 11:15
Bromoform
ug/kg
ND
5.0
02/20/20 11:15
Bromomethane
ug/kg
ND
10.0
02/20/20 11:15 IH
Carbon tetrachloride
ug/kg
ND
5.0
02/20/20 11:15
Chlorobenzene
ug/kg
ND
5.0
02/20/20 11:15
Chloroethane
ug/kg
ND
10.0
02/20/20 11:15
Chloroform
ug/kg
ND
5.0
02/20/20 11:15
Chloromethane
ug/kg
ND
10.0
02/20/20 11:15
cis-1,2-Dichloroethene
ug/kg
ND
5.0
02/20/20 11:15
cis-1,3-Dichloropropene
ug/kg
ND
5.0
02/20/20 11:15
Dibromochloromethane
ug/kg
ND
5.0
02/20/20 11:15
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
METHOD BLANK: 2811720
Matrix:
Solid
Associated Lab Samples: 92464978015, 92464978016
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Dibromomethane
ug/kg
ND
5.0
02/20/20 11:15
Dichlorodifluoromethane
ug/kg
ND
10.0
02/20/20 11:15
Diisopropyl ether
ug/kg
ND
5.0
02/20/20 11:15
Ethylbenzene
ug/kg
ND
5.0
02/20/20 11:15
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
02/20/20 11:15
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
02/20/20 11:15
m&p-Xylene
ug/kg
ND
10.0
02/20/20 11:15
Methyl-tert-butyl ether
ug/kg
ND
5.0
02/20/20 11:15
Methylene Chloride
ug/kg
ND
20.0
02/20/20 11:15
v2
n-Butylbenzene
ug/kg
ND
5.0
02/20/20 11:15
n-Propylbenzene
ug/kg
ND
5.0
02/20/20 11:15
Naphthalene
ug/kg
ND
5.0
02/20/20 11:15
o-Xylene
ug/kg
ND
5.0
02/20/20 11:15
p-Isopropyltoluene
ug/kg
ND
5.0
02/20/20 11:15
sec-Butylbenzene
ug/kg
ND
5.0
02/20/20 11:15
Styrene
ug/kg
ND
5.0
02/20/20 11:15
tert-Butyl benzene
ug/kg
ND
5.0
02/20/20 11:15
Tetrachloroethene
ug/kg
ND
5.0
02/20/20 11:15
Toluene
ug/kg
ND
5.0
02/20/20 11:15
trans-1,2-Dichloroethene
ug/kg
ND
5.0
02/20/20 11:15
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
02/20/20 11:15
Trichloroethene
ug/kg
ND
5.0
02/20/20 11:15
Trichlorofluoromethane
ug/kg
ND
5.0
02/20/20 11:15
Vinyl acetate
ug/kg
ND
50.0
02/20/20 11:15
Vinyl chloride
ug/kg
ND
10.0
02/20/20 11:15
Xylene (Total)
ug/kg
ND
10.0
02/20/20 11:15
1,2-Dichloroethane-d4 (S)
%
99
70-132
02/20/20 11:15
4-Bromofluorobenzene (S)
%
100
70-130
02/20/20 11:15
Toluene-d8 (S)
%
102
70-130
02/20/20 11:15
LABORATORY CONTROL SAMPLE & LCSD:
2811721
2811722
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
49.4
48.3
99 97
70-130
2 30
1,1,1-Trichloroethane
ug/kg
50
47.9
50.0
96 100
70-130
4 30
1,1,2,2-Tetrachloroethane
ug/kg
50
44.7
44.0
89 88
55-130
2 30
1,1,2-Trichloroethane
ug/kg
50
45.8
46.8
92 94
70-130
2 30
1,1-Dichloroethane
ug/kg
50
46.1
48.6
92 97
68-130
5 30
1,1-Dichloroethene
ug/kg
50
50.7
53.1
101 106
70-130
5 30
1,1-Dichloropropene
ug/kg
50
53.0
54.6
106 109
70-130
3 30
1,2,3-Trichlorobenzene
ug/kg
50
46.9
48.1
94 96
70-130
3 30
1,2,3-Trichloropropane
ug/kg
50
41.6
41.6
83 83
70-130
0 30
1,2,4-Trichlorobenzene
ug/kg
50
48.6
48.8
97 98
70-130
0 30
1,2,4-Trimethylbenzene
ug/kg
50
44.5
46.7
89 93
69-130
5 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 114

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
LABORATORY CONTROL SAMPLE & LCSD:
2811721
2811722
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
1,2-Dibromo-3-chloropropane
ug/kg
50
43.2
45.7
86
91
57-141
6
30
1,2-Dibromoethane (EDB)
ug/kg
50
47.3
46.4
95
93
70-130
2
30
1,2-Dichlorobenzene
ug/kg
50
45.5
47.4
91
95
70-130
4
30
1,2-Dichloroethane
ug/kg
50
43.8
44.8
88
90
70-130
2
30
1,2-Dichloropropane
ug/kg
50
46.1
47.0
92
94
70-130
2
30
1,3,5-Trimethylbenzene
ug/kg
50
45.0
46.6
90
93
70-130
3
30
1,3-Dichlorobenzene
ug/kg
50
45.8
47.1
92
94
70-130
3
30
1,3-Dichloropropane
ug/kg
50
47.1
47.3
94
95
70-130
0
30
1,4-Dichlorobenzene
ug/kg
50
46.5
47.7
93
95
70-130
2
30
2,2-Dichloropropane
ug/kg
50
49.3
49.4
99
99
70-130
0
30
2-Butanone (MEK)
ug/kg
100
88AJ
91.7J
88
92
60-130
30
2-Chlorotoluene
ug/kg
50
44.9
47.6
90
95
70-130
6
30
2-Hexanone
ug/kg
100
86.2
85.3
86
85
70-132
1
30
4-Chlorotoluene
ug/kg
50
46.7
47.6
93
95
70-130
2
30
4-Methyl-2-pentanone (MIBK)
ug/kg
100
83.1
83.0
83
83
69-130
0
30
Acetone
ug/kg
100
83AJ
85.7J
83
86
49-148
30
Benzene
ug/kg
50
49.7
49.9
99
100
70-130
0
30
Bromobenzene
ug/kg
50
45.8
48.4
92
97
70-130
5
30
Bromochloromethane
ug/kg
50
46.8
48.1
94
96
70-130
3
30
Bromodichloromethane
ug/kg
50
43.4
43.4
87
87
70-130
0
30
Bromoform
ug/kg
50
42.2
42.8
84
86
68-136
1
30
Bromomethane
ug/kg
50
62.8
64.4
126
129
60-140
3
30 IH
Carbon tetrachloride
ug/kg
50
48.1
48.5
96
97
70-130
1
30
Chlorobenzene
ug/kg
50
47.0
46.7
94
93
70-130
1
30
Chloroethane
ug/kg
50
45.1
47.5
90
95
51-147
5
30
Chloroform
ug/kg
50
45.9
48.2
92
96
70-130
5
30
Chloromethane
ug/kg
50
37.3
38.2
75
76
48-130
2
30
cis-1,2-Dichloroethene
ug/kg
50
44.4
46.7
89
93
70-130
5
30
cis-1,3-Dichloropropene
ug/kg
50
46.5
47.0
93
94
70-130
1
30
Dibromochloromethane
ug/kg
50
47.9
47.7
96
95
70-130
1
30
Dibromomethane
ug/kg
50
45.3
45.9
91
92
70-130
1
30
Dichlorodifluoromethane
ug/kg
50
39.9
40.4
80
81
49-130
1
30
Diisopropyl ether
ug/kg
50
47.9
50.9
96
102
66-130
6
30
Ethylbenzene
ug/kg
50
46.8
46.5
94
93
70-130
1
30
Hexachloro-1,3-butadiene
ug/kg
50
48.3
49.4
97
99
70-130
2
30
Isopropylbenzene (Cumene)
ug/kg
50
47.3
47.5
95
95
70-130
0
30
m&p-Xylene
ug/kg
100
92.1
91.4
92
91
70-130
1
30
Methyl-tert-butyl ether
ug/kg
50
48.2
50.5
96
101
70-130
5
30
Methylene Chloride
ug/kg
50
35.9
38.3
72
77
50-137
6
30 v3
n-Butylbenzene
ug/kg
50
47.6
47.7
95
95
70-130
0
30
n-Propylbenzene
ug/kg
50
45.7
47.2
91
94
70-130
3
30
Naphthalene
ug/kg
50
44.1
45.4
88
91
70-131
3
30
o-Xylene
ug/kg
50
45.3
45.8
91
92
70-130
1
30
p-Isopropyltoluene
ug/kg
50
45.2
47.7
90
95
70-130
5
30
sec-Butylbenzene
ug/kg
50
45.4
46.3
91
93
70-130
2
30
Styrene
ug/kg
50
46.4
46.8
93
94
70-130
1
30
tert-Butyl benzene
ug/kg
50
39.5
41.5
79
83
69-130
5
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
LABORATORY CONTROL SAMPLE & LCSD:
2811721
2811722
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Tetrachloroethene
ug/kg
50
50.3
48.9
101
98
56-130
3
30
Toluene
ug/kg
50
43.6
43.3
87
87
70-130
1
30
trans-1,2-Dichloroethene
ug/kg
50
47.2
49.6
94
99
70-130
5
30
trans- 1,3-Dichloropropene
ug/kg
50
44.0
45.7
88
91
70-130
4
30
Trichloroethene
ug/kg
50
48.9
50.2
98
100
70-141
2
30
Trichlorofluoromethane
ug/kg
50
45.0
47.1
90
94
67-130
5
30
Vinyl acetate
ug/kg
100
116
114
116
114
10-136
2
30
Vinyl chloride
ug/kg
50
46.7
49.7
93
99
67-130
6
30
Xylene(Total)
ug/kg
150
137
137
92
92
70-130
0
30
1,2-Dichloroethane-d4 (S)
%
95
95
70-132
4-Bromofluorobenzene (S)
%
101
97
70-130
Toluene-d8(S)
%
98
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC.
Page 47 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: A19-158-02
Pace Project No.: 92464978
QC Batch: 525251 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92464978001, 92464978002, 92464978003, 92464978004, 92464978005, 92464978006, 92464978007,
92464978008,92464978009,92464978010,92464978011,92464978012,92464978013,92464978014,
92464978015,92464978016
SAMPLE DUPLICATE: 2807521
92464978001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 55.6 54.7 2
SAMPLE DUPLICATE: 2807522
92465102004 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 20.6 20.6 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC.
Page 48 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: A19-158-02
Pace Project No.: 92464978
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
1g The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
10 The internal standard response was outside the laboratory acceptance limits confirmed by reanalysis. The results
reported are from the most QC compliant analysis.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
S1 Surrogate recovery outside laboratory control limits (confirmed by re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/04/2020 08:49 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 114

leAnalyiical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
A19-158-02
Pace Project No.:
92464978
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92464978001
S-1
EPA 5035A
525447
EPA 8260D
525461
92464978002
S-2
EPA 5035A
525693
EPA 8260D
525897
92464978003
S-3
EPA 5035A
525693
EPA 8260D
525897
92464978004
S-4
EPA 5035A
525693
EPA 8260D
525897
92464978005
S-5
EPA 5035A
525693
EPA 8260D
525897
92464978006
S-6
EPA 5035A
525693
EPA 8260D
525897
92464978007
S-7
EPA 5035A
525693
EPA 8260D
525897
92464978008
S-8
EPA 5035A
525693
EPA 8260D
525897
92464978009
S-9
EPA 5035A
525693
EPA 8260D
525897
92464978010
S-10
EPA 5035A
525693
EPA 8260D
525897
92464978011
S-11
EPA 5035A
525693
EPA 8260D
525897
92464978012
S-12
EPA 5035A
525693
EPA 8260D
525897
92464978013
S-13
EPA 5035A
525693
EPA 8260D
525897
92464978014
S-14
EPA 5035A
525693
EPA 8260D
525897
92464978015
S-15
EPA 5035A
526104
EPA 8260D
526118
92464978016
DUP-1
EPA 5035A
526104
EPA 8260D
526118
92464978001
S-1
ASTM D2974-87
525251
92464978002
S-2
ASTM D2974-87
525251
92464978003
S-3
ASTM D2974-87
525251
92464978004
S-4
ASTM D2974-87
525251
92464978005
S-5
ASTM D2974-87
525251
92464978006
S-6
ASTM D2974-87
525251
92464978007
S-7
ASTM D2974-87
525251
92464978008
S-8
ASTM D2974-87
525251
92464978009
S-9
ASTM D2974-87
525251
92464978010
S-10
ASTM D2974-87
525251
92464978011
S-11
ASTM D2974-87
525251
92464978012
S-12
ASTM D2974-87
525251
92464978013
S-13
ASTM D2974-87
525251
92464978014
S-14
ASTM D2974-87
525251
92464978015
S-15
ASTM D2974-87
525251
92464978016
DUP-1
ASTM D2974-87
525251
Date: 03/04/2020 08:49 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 50 of 114

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)Page 1 of 2
.r aceAnalytical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving sa les:
AshevilleEden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
.--'Sample Condition Client Name: Wa# : 92464978
Upon Receipt Project
Courier: []Fed Ex ❑UPS ❑USPS Client
❑ Commercial ❑Pace ❑Other: 92464978
Custody Seal Present? Ryes No Seals Intact? ❑Yes —C No l �
pate/Initials Person Examining Contents J �— j �z
Packing Material: []bubble Wrap ,Bubble Bags ❑None ❑ Other
Thermome/ Type of Ice: �t ❑Blue
0Gun lD: C'
Cooler Temp (°C): �/ ' �• Z ,� Correction factor: Add/Subtract (°C) `
Cooler Temp Corrected (°C):_.�._�
USDA Regulated Soil (❑ N/A, water sample)
Did samples o,_rigina�t in a quarantine zone within the United States: CA, NY, or SC (check maps)?
nYes ,YTNo
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CDC?
-Includes Date/Time/ID/Analysis
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
Yes
Yes
�o
No
❑No
❑No
[-]No
J2ye's ❑No
]N/A 1.
:]NIA 2.
]N/A 3.
] N/A 4.
❑N/A 5.
❑N/A 6.
❑ N/A
❑N/A 7.
8.
❑ WA 9.
❑Yes ❑No •—e1�/A 10.
Dyes —4D+4o- DN//AA 11.
I—IYes r INo .2N/A
Biological Tissue F en?
❑Yes ❑No N/A
❑None
Temp should be above freezing to 6'C
[]Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
inciudirg Hawaii and Puerto Rico)? Dyes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes No
Person contacted: Date/Time:
Date:i S
Project Manager SCURF Review: ( f
Project Manager SRF Review: Date: C7 1 ,
Page 51 of 114

�. PiceAnalytical
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
ProjE W4## : 92464978
PM: UP Due Date: 02/20/20
CLIENT: 93-Headwater
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adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Caroiina DEHNR Certification Office (Le
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 52 of 114

�r Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
%/' c�CBf!]c�1;fCclr Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quatity Office
`Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Colifcrm, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project#
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Nate: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina 0EHNK Lertmcatian umce p.e.
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Page 53 of 114

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N
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0
aceAnalytical
Report of Analysis
Pace Analytical Services, LLC
2225 Riverside Drive
Asheville, NC 28804
Attention: Lord Patton
Project Name: A19-158-02
Project Number: 92464978
Lot Number:VB14033
Date Completed:02/20/2020
02/20/2020 3:32 PM
Approved and released by:
Project Manager: Cathy S. Dover
pCC/►F0
ANSI National Accreditation Board
qe�
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 56 of 114
Page 1 of 45

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical Services, LLC
Lot Number: VB14033
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier.
SVOA 8270E
Samples VB14033-004 (S-4) and VB14033-005 (S-5) were diluted due to appearance or color (greenish
black). The LOQ has been elevated to reflect the dilution.
There were a few biased high recoveries in the LCS batch 45207, but the associated samples were non -
detect for these analytes.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 57 of 114
Page 2 of 45

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: VB14033
Project Name: A19-158-02
Project Number: 92464978
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
S-1
Solid
02/11/20201400
02/14/2020
002
S-2
Solid
02/11/20201430
02/14/2020
003
S-3
Solid
02/11/20201515
02/14/2020
004
S-4
Solid
02/11/20201545
02/14/2020
005
S-5
Solid
02/11/20201600
02/14/2020
006
S-6
Solid
02/11/20201630
02/14/2020
007
S-7
Solid
02/11/20201700
02/14/2020
008
S-8
Solid
02/12/20201100
02/14/2020
009
S-9
Solid
02/12/20201130
02/14/2020
010
S-10
Solid
02/12/20201200
02/14/2020
011
S-11
Solid
02/12/20201220
02/14/2020
012
S-12
Solid
02/12/20201240
02/14/2020
013
S-13
Solid
02/12/20201320
02/14/2020
014
S-14
Solid
02/12/20201340
02/14/2020
015
S-15
Solid
02/12/20201400
02/14/2020
016
DUP-1
Solid
02/12/20201100
02/14/2020
(16 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 58 of 114
Page 3 of 45

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical Services, LLC
Lot Number: VB14033
Project Name: A19-158-02
Project Number: 92464978
Sample Sample ID Matrix Parameter Method Result Q Units Page
012 S-12 Solid 1-Methylnaphthalene 8270E 0.17 mg/kg 28
012 S-12 Solid 2-Methylnaphthalene 8270E 0.28 mg/kg 28
(2 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 59 of 114
Page 4 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-001
Description: S-1 Matrix: Solid
Date Sampled:02/11/2020 1400 Project Name: A19-158-02 % Solids: 35.1 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1557 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.037
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.037
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.94
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.037
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.037
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.037
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.037
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.037
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.037
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
4.8
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.19
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.19
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.19
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.19
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.19
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.19
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.19
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.19
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.19
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.19
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.19
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.037
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.037
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.19
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.19
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.19
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.19
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.19
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.19
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.19
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.19
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.19
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.19
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.94
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.94
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.37
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.37
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.19
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.37
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.037
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.037
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.19
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.19
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.94
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 60 of 114
Page 5 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-001
Description: S-1 Matrix: Solid
Date Sampled:02/11/2020 1400 Project Name: A19-158-02 % Solids: 35.1 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1557 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.19
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.037
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.19
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.037
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.037
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.19
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.37
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.037
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.37
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.37
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.37
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.19
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.37
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.94
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.19
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.19
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.19
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.94
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.037
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.19
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.037
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.19
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.19
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.19
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.19
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
68
24-137
2-Fluorophenol
95
16-136
Nitrobenzene-d5
60
12-144
Phenol-d5
93
26-148
Terphenyl-d14
89
20-127
2,4,6-Tribromophenol
82
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 61 of 114
Page 6 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-002
Description: S-2 Matrix: Solid
Date Sampled:02/11/2020 1430 Project Name: A19-158-02 % Solids: 40.6 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1622 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.032
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.032
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.81
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.032
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.032
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.032
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.032
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.032
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.032
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
4.2
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.17
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.17
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.17
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.17
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.17
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.17
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.17
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.17
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.17
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.17
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.17
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.032
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.032
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.17
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.17
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.17
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.17
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.17
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.17
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.17
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.17
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.17
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.17
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.81
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.81
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.32
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.32
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.17
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.32
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.032
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.032
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.17
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.17
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.81
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 62 of 114
Page 7 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-002
Description: S-2 Matrix: Solid
Date Sampled:02/11/2020 1430 Project Name: A19-158-02 % Solids: 40.6 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1622 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.17
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.032
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.17
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.032
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.032
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.17
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.32
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.032
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.32
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.32
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.32
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.17
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.32
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.81
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.17
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.17
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.17
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.81
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.032
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.17
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.032
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.17
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.17
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.17
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.17
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
69
24-137
2-Fluorophenol
89
16-136
Nitrobenzene-d5
56
12-144
Phenol-d5
93
26-148
Terphenyl-d14
86
20-127
2,4,6-Tribromophenol
76
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 63 of 114
Page 8 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-003
Description: S-3 Matrix: Solid
Date Sampled:02/11/2020 1515 Project Name: A19-158-02 % Solids: 25.7 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1647 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.050
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.050
mg/Kg
1
Aniline
62-53-3
8270E
ND
1.3
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.050
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.050
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.050
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.050
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.050
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.050
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
6.6
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.26
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.26
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.26
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.26
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.26
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.26
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.26
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.26
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.26
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.26
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.26
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.050
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.050
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.26
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.26
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.26
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.26
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.26
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.26
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.26
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.26
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.26
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.26
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
1.3
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
1.3
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.50
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.50
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.26
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.50
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.050
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.050
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.26
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.26
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
1.3
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 64 of 114
Page 9 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-003
Description: S-3 Matrix: Solid
Date Sampled:02/11/2020 1515 Project Name: A19-158-02 % Solids: 25.7 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1647 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.26
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.050
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.26
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.050
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.050
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.26
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.50
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.050
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.50
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.50
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.50
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.26
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.50
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
1.3
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.26
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.26
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.26
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
1.3
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.050
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.26
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.050
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.26
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.26
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.26
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.26
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
64
24-137
2-Fluorophenol
83
16-136
Nitrobenzene-d5
52
12-144
Phenol-d5
82
26-148
Terphenyl-d14
81
20-127
2,4,6-Tribromophenol
72
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 65 of 114
Page 10 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-004
Description: S-4 Matrix: Solid
Date Sampled:02/11/2020 1545 Project Name: A19-158-02 % Solids: 32.4 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
5 02/18/2020 1712 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.20
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.20
mg/Kg
1
Aniline
62-53-3
8270E
ND
5.1
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.20
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.20
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.20
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.20
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.20
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.20
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
26
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
1.0
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
1.0
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
1.0
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
1.0
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
1.0
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
1.0
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
1.0
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
1.0
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
1.0
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
1.0
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
1.0
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.20
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.20
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
1.0
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
1.0
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
1.0
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
1.0
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
1.0
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
1.0
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
1.0
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
1.0
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
1.0
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
1.0
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
5.1
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
5.1
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
2.0
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
2.0
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
1.0
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
2.0
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.20
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.20
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
1.0
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
1.0
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
5.1
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 66 of 114
Page 11 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-004
Description: S-4 Matrix: Solid
Date Sampled:02/11/2020 1545 Project Name: A19-158-02 % Solids: 32.4 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
5 02/18/2020 1712 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
1.0
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.20
mg/Kg
1
Isophorone
78-59-1
8270E
ND
1.0
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.20
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.20
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
1.0
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
2.0
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.20
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
2.0
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
2.0
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
2.0
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
1.0
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
2.0
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
5.1
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
1.0
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
1.0
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
1.0
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
5.1
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.20
mg/Kg
1
Phenol
108-95-2
8270E
ND
1.0
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.20
mg/Kg
1
Pyridine
110-86-1
8270E
ND
1.0
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
1.0
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
1.0
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
1.0
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
54
24-137
2-Fluorophenol
60
16-136
Nitrobenzene-d5
48
12-144
Phenol-d5
63
26-148
Terphenyl-d14
72
20-127
2,4,6-Tribromophenol
59
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 67 of 114
Page 12 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-005
Description: S-5 Matrix: Solid
Date Sampled:02/11/2020 1600 Project Name: A19-158-02 % Solids: 38.5 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
5 02/18/2020 1737 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.17
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.17
mg/Kg
1
Aniline
62-53-3
8270E
ND
4.2
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.17
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.17
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.17
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.17
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.17
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.17
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
22
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.86
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.86
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.86
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.86
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.86
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.86
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.86
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.86
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.86
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.86
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.86
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.17
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.17
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.86
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.86
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.86
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.86
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.86
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.86
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.86
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.86
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.86
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.86
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
4.2
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
4.2
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
1.7
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
1.7
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.86
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
1.7
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.17
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.17
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.86
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.86
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
4.2
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 68 of 114
Page 13 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-005
Description: S-5 Matrix: Solid
Date Sampled:02/11/2020 1600 Project Name: A19-158-02 % Solids: 38.5 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
5 02/18/2020 1737 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.86
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.17
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.86
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.17
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.17
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.86
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
1.7
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.17
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
1.7
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
1.7
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
1.7
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.86
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
1.7
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
4.2
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.86
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.86
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.86
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
4.2
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.17
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.86
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.17
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.86
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.86
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.86
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.86
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
60
24-137
2-Fluorophenol
78
16-136
Nitrobenzene-d5
53
12-144
Phenol-d5
81
26-148
Terphenyl-d14
79
20-127
2,4,6-Tribromophenol
62
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 69 of 114
Page 14 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-006
Description: S-6 Matrix: Solid
Date Sampled:02/11/2020 1630 Project Name: A19-158-02 % Solids: 20.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1802 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.063
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.063
mg/Kg
1
Aniline
62-53-3
8270E
ND
1.6
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.063
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.063
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.063
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.063
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.063
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.063
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
8.2
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.32
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.32
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.32
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.32
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.32
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.32
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.32
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.32
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.32
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.32
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.32
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.063
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.063
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.32
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.32
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.32
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.32
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.32
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.32
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.32
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.32
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.32
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.32
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
1.6
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
1.6
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.63
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.63
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.32
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.63
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.063
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.063
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.32
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.32
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
1.6
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 114
Page 15 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-006
Description: S-6 Matrix: Solid
Date Sampled:02/11/2020 1630 Project Name: A19-158-02 % Solids: 20.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1802 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.32
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.063
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.32
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.063
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.063
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.32
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.63
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.063
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.63
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.63
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.63
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.32
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.63
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
1.6
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.32
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.32
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.32
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
1.6
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.063
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.32
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.063
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.32
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.32
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.32
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.32
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
66
24-137
2-Fluorophenol
87
16-136
Nitrobenzene-d5
55
12-144
Phenol-d5
84
26-148
Terphenyl-d14
85
20-127
2,4,6-Tribromophenol
77
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 114
Page 16 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-007
Description: S-7 Matrix: Solid
Date Sampled:02/11/2020 1700 Project Name: A19-158-02 % Solids: 65.0 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1827 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.020
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.020
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.50
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.020
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.020
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.020
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.020
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.020
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.020
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
2.6
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.10
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.10
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.10
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.10
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.10
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.10
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.10
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.10
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.10
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.10
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.10
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.020
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.020
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.10
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.10
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.10
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.10
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.10
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.10
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.10
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.10
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.10
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.10
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.50
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.50
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.20
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.20
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.10
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.20
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.020
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.020
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.10
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.10
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.50
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 72 of 114
Page 17 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-007
Description: S-7 Matrix: Solid
Date Sampled:02/11/2020 1700 Project Name: A19-158-02 % Solids: 65.0 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1827 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.10
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.020
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.10
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.020
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.020
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.10
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.20
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.020
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.20
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.20
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.20
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.10
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.20
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.50
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.10
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.10
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.10
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.50
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.020
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.10
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.020
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.10
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.10
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.10
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.10
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
72
24-137
2-Fluorophenol
97
16-136
Nitrobenzene-d5
59
12-144
Phenol-d5
96
26-148
Terphenyl-d14
89
20-127
2,4,6-Tribromophenol
84
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 73 of 114
Page 18 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-008
Description: S-8 Matrix: Solid
Date Sampled:02/12/2020 1100 Project Name: A19-158-02 % Solids: 44.8 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1852 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.029
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.029
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.74
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.029
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.029
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.029
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.029
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.029
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.029
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
3.8
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.15
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.15
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.15
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.15
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.15
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.15
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.15
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.15
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.15
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.15
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.15
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.029
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.029
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.15
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.15
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.15
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.15
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.15
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.15
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.15
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.15
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.15
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.15
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.74
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.74
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.29
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.29
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.15
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.29
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.029
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.029
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.15
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.15
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.74
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 74 of 114
Page 19 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-008
Description: S-8 Matrix: Solid
Date Sampled:02/12/2020 1100 Project Name: A19-158-02 % Solids: 44.8 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1852 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.15
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.029
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.15
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.029
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.029
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.15
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.29
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.029
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.29
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.29
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.29
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.15
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.29
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.74
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.15
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.15
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.15
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.74
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.029
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.15
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.029
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.15
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.15
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.15
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.15
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
70
24-137
2-Fluorophenol
85
16-136
Nitrobenzene-d5
60
12-144
Phenol-d5
88
26-148
Terphenyl-d14
85
20-127
2,4,6-Tribromophenol
78
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 75 of 114
Page 20 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-009
Description: S-9 Matrix: Solid
Date Sampled:02/12/2020 1130 Project Name: A19-158-02 % Solids: 68.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1917 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.019
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.019
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.48
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.019
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.019
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.019
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.019
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.019
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.019
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
2.5
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.097
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.097
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.097
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.097
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.097
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.097
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.097
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.097
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.097
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.097
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.097
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.019
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.019
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.097
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.097
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.097
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.097
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.097
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.097
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.097
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.097
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.097
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.097
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.48
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.48
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.19
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.19
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.097
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.19
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.019
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.019
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.097
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.097
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.48
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 76 of 114
Page 21 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-009
Description: S-9 Matrix: Solid
Date Sampled:02/12/2020 1130 Project Name: A19-158-02 % Solids: 68.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1917 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.097
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.019
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.097
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.019
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.019
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.097
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.19
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.019
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.19
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.19
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.19
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.097
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.19
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.48
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.097
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.097
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.097
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.48
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.019
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.097
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.019
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.097
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.097
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.097
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.097
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
72
24-137
2-Fluorophenol
101
16-136
Nitrobenzene-d5
62
12-144
Phenol-d5
100
26-148
Terphenyl-d14
80
20-127
2,4,6-Tribromophenol
83
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 77 of 114
Page 22 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-010
Description: S-10 Matrix: Solid
Date Sampled:02/12/2020 1200 Project Name: A19-158-02 % Solids: 36.5 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 1942 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.034
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.034
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.88
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.034
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.034
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.034
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.034
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.034
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.034
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
4.5
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.18
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.18
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.18
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.18
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.18
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.18
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.18
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.18
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.18
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.18
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.18
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.034
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.034
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.18
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.18
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.18
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.18
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.18
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.18
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.18
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.18
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.18
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.18
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.88
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.88
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.34
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.34
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.18
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.34
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.034
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.034
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.18
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.18
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.88
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 78 of 114
Page 23 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-010
Description: S-10 Matrix: Solid
Date Sampled:02/12/2020 1200 Project Name: A19-158-02 % Solids: 36.5 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 1942 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.18
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.034
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.18
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.034
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.034
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.18
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.34
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.034
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.34
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.34
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.34
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.18
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.34
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.88
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.18
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.18
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.18
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.88
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.034
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.18
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.034
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.18
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.18
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.18
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.18
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
70
24-137
2-Fluorophenol
98
16-136
Nitrobenzene-d5
58
12-144
Phenol-d5
98
26-148
Terphenyl-d14
82
20-127
2,4,6-Tribromophenol
82
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 79 of 114
Page 24 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-011
Description: S-11 Matrix: Solid
Date Sampled:02/12/2020 1220 Project Name: A19-158-02 % Solids: 35.6 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 2007 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.037
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.037
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.93
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.037
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.037
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.037
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.037
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.037
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.037
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
4.8
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.19
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.19
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.19
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.19
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.19
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.19
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.19
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.19
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.19
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.19
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.19
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.037
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.037
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.19
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.19
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.19
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.19
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.19
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.19
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.19
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.19
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.19
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.19
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.93
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.93
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.37
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.37
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.19
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.37
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.037
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.037
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.19
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.19
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.93
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 80 of 114
Page 25 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-011
Description: S-11 Matrix: Solid
Date Sampled:02/12/2020 1220 Project Name: A19-158-02 % Solids: 35.6 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 2007 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.19
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.037
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.19
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.037
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.037
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.19
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.37
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.037
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.37
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.37
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.37
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.19
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.37
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.93
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.19
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.19
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.19
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.93
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.037
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.19
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.037
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.19
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.19
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.19
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.19
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
70
24-137
2-Fluorophenol
94
16-136
Nitrobenzene-d5
57
12-144
Phenol-d5
94
26-148
Terphenyl-d14
85
20-127
2,4,6-Tribromophenol
84
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 81 of 114
Page 26 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-012
Description: S-12 Matrix: Solid
Date Sampled:02/12/2020 1240 Project Name: A19-158-02 % Solids: 25.9 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 2032 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.048
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.048
mg/Kg
1
Aniline
62-53-3
8270E
ND
1.2
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.048
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.048
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.048
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.048
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.048
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.048
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
6.2
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.25
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.25
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.25
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.25
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.25
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.25
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.25
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.25
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.25
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.25
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.25
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.048
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.048
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.25
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.25
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.25
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.25
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.25
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.25
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.25
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.25
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.25
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.25
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
1.2
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
1.2
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.48
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.48
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.25
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.48
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.048
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.048
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.25
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.25
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
1.2
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 82 of 114
Page 27 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-012
Description: S-12 Matrix: Solid
Date Sampled:02/12/2020 1240 Project Name: A19-158-02 % Solids: 25.9 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 2032 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.25
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.048
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.25
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
0.17
0.048
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
0.28
0.048
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.25
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.48
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.048
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.48
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.48
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.48
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.25
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.48
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
1.2
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.25
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.25
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.25
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
1.2
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.048
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.25
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.048
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.25
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.25
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.25
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.25
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
67
24-137
2-Fluorophenol
91
16-136
Nitrobenzene-d5
60
12-144
Phenol-d5
87
26-148
Terphenyl-d14
81
20-127
2,4,6-Tribromophenol
92
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 83 of 114
Page 28 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-013
Description: S-13 Matrix: Solid
Date Sampled:02/12/2020 1320 Project Name: A19-158-02 % Solids: 33.4 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 2057 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.037
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.037
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.93
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.037
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.037
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.037
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.037
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.037
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.037
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
4.8
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.19
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.19
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.19
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.19
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.19
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.19
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.19
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.19
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.19
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.19
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.19
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.037
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.037
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.19
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.19
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.19
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.19
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.19
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.19
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.19
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.19
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.19
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.19
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.93
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.93
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.37
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.37
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.19
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.37
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.037
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.037
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.19
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.19
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.93
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 84 of 114
Page 29 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-013
Description: S-13 Matrix: Solid
Date Sampled:02/12/2020 1320 Project Name: A19-158-02 % Solids: 33.4 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 2057 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.19
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.037
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.19
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.037
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.037
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.19
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.37
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.037
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.37
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.37
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.37
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.19
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.37
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.93
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.19
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.19
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.19
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.93
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.037
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.19
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.037
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.19
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.19
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.19
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.19
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
64
24-137
2-Fluorophenol
83
16-136
Nitrobenzene-d5
52
12-144
Phenol-d5
87
26-148
Terphenyl-d14
79
20-127
2,4,6-Tribromophenol
72
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 85 of 114
Page 30 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-014
Description: S-14 Matrix: Solid
Date Sampled:02/12/2020 1340 Project Name: A19-158-02 % Solids: 42.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 2122 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.030
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.030
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.77
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.030
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.030
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.030
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.030
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.030
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.030
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
4.0
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.16
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.16
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.16
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.16
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.16
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.16
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.16
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.16
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.16
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.16
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.16
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.030
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.030
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.16
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.16
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.16
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.16
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.16
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.16
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.16
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.16
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.16
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.16
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.77
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.77
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.30
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.30
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.16
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.30
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.030
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.030
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.16
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.16
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.77
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 86 of 114
Page 31 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-014
Description: S-14 Matrix: Solid
Date Sampled:02/12/2020 1340 Project Name: A19-158-02 % Solids: 42.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 2122 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.16
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.030
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.16
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.030
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.030
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.16
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.30
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.030
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.30
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.30
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.30
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.16
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.30
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.77
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.16
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.16
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.16
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.77
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.030
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.16
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.030
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.16
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.16
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.16
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.16
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
64
24-137
2-Fluorophenol
71
16-136
Nitrobenzene-d5
52
12-144
Phenol-d5
70
26-148
Terphenyl-d14
71
20-127
2,4,6-Tribromophenol
71
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 87 of 114
Page 32 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-015
Description: S-15 Matrix: Solid
Date Sampled:02/12/2020 1400 Project Name: A19-158-02 % Solids: 38.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 2147 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.034
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.034
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.85
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.034
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.034
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.034
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.034
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.034
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.034
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
4.4
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.17
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.17
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.17
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.17
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.17
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.17
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.17
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.17
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.17
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.17
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.17
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.034
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.034
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.17
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.17
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.17
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.17
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.17
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.17
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.17
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.17
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.17
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.17
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.85
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.85
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.34
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.34
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.17
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.34
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.034
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.034
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.17
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.17
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.85
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 88 of 114
Page 33 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-015
Description: S-15 Matrix: Solid
Date Sampled:02/12/2020 1400 Project Name: A19-158-02 % Solids: 38.2 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 2147 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.17
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.034
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.17
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.034
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.034
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.17
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.34
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.034
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.34
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.34
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.34
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.17
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.34
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.85
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.17
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.17
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.17
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.85
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.034
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.17
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.034
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.17
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.17
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.17
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.17
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
69
24-137
2-Fluorophenol
79
16-136
Nitrobenzene-d5
55
12-144
Phenol-d5
86
26-148
Terphenyl-d14
79
20-127
2,4,6-Tribromophenol
80
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 89 of 114
Page 34 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-016
Description: DUP-1 Matrix: Solid
Date Sampled:02/12/2020 1100 Project Name: A19-158-02 % Solids: 53.0 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 02/18/2020 2213 SCD
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.024
mg/Kg
1
Acenaphthylene
208-96-8
8270E
ND
0.024
mg/Kg
1
Aniline
62-53-3
8270E
ND
0.60
mg/Kg
1
Anthracene
120-12-7
8270E
ND
0.024
mg/Kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.024
mg/Kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.024
mg/Kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.024
mg/Kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.024
mg/Kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.024
mg/Kg
1
Benzoic acid
65-85-0
8270E
ND
3.1
mg/Kg
1
Benzyl alcohol
100-51-6
8270E
ND
0.12
mg/Kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
0.12
mg/Kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
0.12
mg/Kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
0.12
mg/Kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
0.12
mg/Kg
1
4-Chloroaniline
106-47-8
8270E
ND
0.12
mg/Kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
0.12
mg/Kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
0.12
mg/Kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
0.12
mg/Kg
1
2-Chlorophenol
95-57-8
8270E
ND
0.12
mg/Kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
0.12
mg/Kg
1
Chrysene
218-01-9
8270E
ND
0.024
mg/Kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.024
mg/Kg
1
Dibenzofuran
132-64-9
8270E
ND
0.12
mg/Kg
1
1,2-Dichlorobenzene
95-50-1
8270E
ND
0.12
mg/Kg
1
1,3-Dichlorobenzene
541-73-1
8270E
ND
0.12
mg/Kg
1
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.12
mg/Kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
0.12
mg/Kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
0.12
mg/Kg
1
Diethylphthalate
84-66-2
8270E
ND
0.12
mg/Kg
1
Dimethyl phthalate
131-11-3
8270E
ND
0.12
mg/Kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
0.12
mg/Kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
0.12
mg/Kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
0.60
mg/Kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
0.60
mg/Kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.24
mg/Kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
0.24
mg/Kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
0.12
mg/Kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
0.24
mg/Kg
1
Fluoranthene
206-44-0
8270E
ND
0.024
mg/Kg
1
Fluorene
86-73-7
8270E
ND
0.024
mg/Kg
1
Hexachlorobenzene
118-74-1
8270E
ND
0.12
mg/Kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.12
mg/Kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
0.60
mg/Kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 90 of 114
Page 35 of 45

Semivolatile Organic Compounds by GC/MS
Client: Pace Analytical Services, LLC Laboratory ID:VB14033-016
Description: DUP-1 Matrix: Solid
Date Sampled:02/12/2020 1100 Project Name: A19-158-02 % Solids: 53.0 02/15/2020 2241
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 02/18/2020 2213 SCD
Prep Date Batch
02/17/2020 1743 45207
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
0.12
mg/Kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.024
mg/Kg
1
Isophorone
78-59-1
8270E
ND
0.12
mg/Kg
1
1-Methylnaphthalene
90-12-0
8270E
ND
0.024
mg/Kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.024
mg/Kg
1
2-Methylphenol
95-48-7
8270E
ND
0.12
mg/Kg
1
3+4-Methylphenol
106-44-5
8270E
ND
0.24
mg/Kg
1
Naphthalene
91-20-3
8270E
ND
0.024
mg/Kg
1
2-Nitroaniline
88-74-4
8270E
ND
0.24
mg/Kg
1
3-Nitroaniline
99-09-2
8270E
ND
0.24
mg/Kg
1
4-Nitroaniline
100-01-6
8270E
ND
0.24
mg/Kg
1
Nitrobenzene
98-95-3
8270E
ND
0.12
mg/Kg
1
2-Nitrophenol
88-75-5
8270E
ND
0.24
mg/Kg
1
4-Nitrophenol
100-02-7
8270E
ND
0.60
mg/Kg
1
N-Nitrosodimethylamine
62-75-9
8270E
ND
0.12
mg/Kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
0.12
mg/Kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
0.12
mg/Kg
1
Pentachlorophenol
87-86-5
8270E
ND
0.60
mg/Kg
1
Phenanthrene
85-01-8
8270E
ND
0.024
mg/Kg
1
Phenol
108-95-2
8270E
ND
0.12
mg/Kg
1
Pyrene
129-00-0
8270E
ND
0.024
mg/Kg
1
Pyridine
110-86-1
8270E
ND
0.12
mg/Kg
1
1,2,4-Trichlorobenzene
120-82-1
8270E
ND
0.12
mg/Kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.12
mg/Kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.12
mg/Kg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
72
24-137
2-Fluorophenol
89
16-136
Nitrobenzene-d5
56
12-144
Phenol-d5
93
26-148
Terphenyl-d14
87
20-127
2,4,6-Tribromophenol
88
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 91 of 114
Page 36 of 45

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: VB14033
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 92 of 114
Page 37 of 45

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ45207-001 Matrix: Solid
Batch: 45207 Prep Method: 3546
Analytical Method: 8270E Prep Date: 02/17/2020 1743
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Acenaphthene
ND
1
0.013
mg/kg
02/18/2020 1212
Acenaphthylene
ND
1
0.013
mg/kg
02/18/2020 1212
Aniline
ND
1
0.33
mg/kg
02/18/2020 1212
Anthracene
ND
1
0.013
mg/kg
02/18/2020 1212
Benzo(a)anthracene
ND
1
0.013
mg/kg
02/18/2020 1212
Benzo(a)pyrene
ND
1
0.013
mg/kg
02/18/2020 1212
Benzo(b)fluoranthene
ND
1
0.013
mg/kg
02/18/2020 1212
Benzo(g,h,i)perylene
ND
1
0.013
mg/kg
02/18/2020 1212
Benzo(k)fluoranthene
ND
1
0.013
mg/kg
02/18/2020 1212
Benzoic acid
ND
1
1.7
mg/kg
02/18/2020 1212
Benzyl alcohol
ND
1
0.067
mg/kg
02/18/2020 1212
4-Bromophenyl phenyl ether
ND
1
0.067
mg/kg
02/18/2020 1212
Butyl benzyl phthalate
ND
1
0.067
mg/kg
02/18/2020 1212
bis (2-Chloro-1-methylethyl) ether
ND
1
0.067
mg/kg
02/18/2020 1212
4-Chloro-3-methyl phenol
ND
1
0.067
mg/kg
02/18/2020 1212
4-Chloroaniline
ND
1
0.067
mg/kg
02/18/2020 1212
bis(2-Chloroethoxy)methane
ND
1
0.067
mg/kg
02/18/2020 1212
bis(2-Chloroethyl)ether
ND
1
0.067
mg/kg
02/18/2020 1212
2-Chloronaphthalene
ND
1
0.067
mg/kg
02/18/2020 1212
2-Chlorophenol
ND
1
0.067
mg/kg
02/18/2020 1212
4-Chlorophenyl phenyl ether
ND
1
0.067
mg/kg
02/18/2020 1212
Chrysene
ND
1
0.013
mg/kg
02/18/2020 1212
Dibenzo(a,h)anthracene
ND
1
0.013
mg/kg
02/18/2020 1212
Dibenzofuran
ND
1
0.067
mg/kg
02/18/2020 1212
1,2-Dichlorobenzene
ND
1
0.067
mg/kg
02/18/2020 1212
1,3-Dichlorobenzene
ND
1
0.067
mg/kg
02/18/2020 1212
1,4-Dichlorobenzene
ND
1
0.067
mg/kg
02/18/2020 1212
3,3'-Dichlorobenzidine
ND
1
0.067
mg/kg
02/18/2020 1212
2,4-Dichlorophenol
ND
1
0.067
mg/kg
02/18/2020 1212
Diethylphthalate
ND
1
0.067
mg/kg
02/18/2020 1212
Dimethyl phthalate
ND
1
0.067
mg/kg
02/18/2020 1212
2,4-Dimethylphenol
ND
1
0.067
mg/kg
02/18/2020 1212
Di-n-butyl phthalate
ND
1
0.067
mg/kg
02/18/2020 1212
4,6-Dinitro-2-methyl phenol
ND
1
0.33
mg/kg
02/18/2020 1212
2,4-Dinitrophenol
ND
1
0.33
mg/kg
02/18/2020 1212
2,4-Dinitrotoluene
ND
1
0.13
mg/kg
02/18/2020 1212
2,6-Dinitrotoluene
ND
1
0.13
mg/kg
02/18/2020 1212
Di-n-octylphthalate
ND
1
0.067
mg/kg
02/18/2020 1212
bis(2-Ethylhexyl)phthalate
ND
1
0.13
mg/kg
02/18/2020 1212
Fluoranthene
ND
1
0.013
mg/kg
02/18/2020 1212
Fluorene
ND
1
0.013
mg/kg
02/18/2020 1212
Hexachlorobenzene
ND
1
0.067
mg/kg
02/18/2020 1212
Hexachlorobutadiene
ND
1
0.067
mg/kg
02/18/2020 1212
Hexachlorocyclopentadiene
ND
1
0.33
mg/kg
02/18/2020 1212
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 45
QC Data for Lot Number: VB14033
Page 93 of 114

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: VQ45207-001 Matrix: Solid
Batch: 45207 Prep Method: 3546
Analytical Method: 8270E Prep Date: 02/17/2020 1743
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Hexachloroethane
ND
1
0.067
mg/kg
02/18/20201212
Indeno(1,2,3-c,d)pyrene
ND
1
0.013
mg/kg
02/18/20201212
Isophorone
ND
1
0.067
mg/kg
02/18/20201212
1-Methyl naphthalene
ND
1
0.013
mg/kg
02/18/20201212
2-Methyl naphthalene
ND
1
0.013
mg/kg
02/18/20201212
2-Methylphenol
ND
1
0.067
mg/kg
02/18/20201212
3+4-Methylphenol
ND
1
0.13
mg/kg
02/18/20201212
Naphthalene
ND
1
0.013
mg/kg
02/18/20201212
2-Nitroaniline
ND
1
0.13
mg/kg
02/18/20201212
3-Nitroaniline
ND
1
0.13
mg/kg
02/18/20201212
4-Nitroaniline
ND
1
0.13
mg/kg
02/18/20201212
Nitrobenzene
ND
1
0.067
mg/kg
02/18/20201212
2-Nitrophenol
ND
1
0.13
mg/kg
02/18/20201212
4-Nitrophenol
ND
1
0.33
mg/kg
02/18/20201212
N-Nitrosodimethylamine
ND
1
0.067
mg/kg
02/18/20201212
N-Nitrosodi-n-propylamine
ND
1
0.067
mg/kg
02/18/20201212
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
0.067
mg/kg
02/18/2020 1212
Pentachlorophenol
ND
1
0.33
mg/kg
02/18/20201212
Phenanthrene
ND
1
0.013
mg/kg
02/18/20201212
Phenol
ND
1
0.067
mg/kg
02/18/20201212
Pyrene
ND
1
0.013
mg/kg
02/18/20201212
Pyridine
ND
1
0.067
mg/kg
02/18/20201212
1,2,4-Trichlorobenzene
ND
1
0.067
mg/kg
02/18/20201212
2,4,5-Trichlorophenol
ND
1
0.067
mg/kg
02/18/20201212
2,4,6-Trichlorophenol
ND
1
0.067
mg/kg
02/18/20201212
Acceptance
Surrogate Q % Rec Limit
2-Fluorobiphenyl
68
24-137
2-Fluorophenol
92
16-136
Nitrobenzene-d5
60
12-144
Phenol-d5 89 26-148
Terphenyl-d14 93 20-127
2,4,6-Tribromophenol 65 27-128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 45
QC Data for Lot Number: VB14033
Page 94 of 114

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ45207-002
Matrix:
Solid
Batch: 45207
Prep Method:
3546
Analytical Method: 8270E
Prep Date:
02/17/2020 1743
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
0.67
0.56
1
83
12-111
02/18/2020 1237
Acenaphthylene
0.67
0.55
1
82
44-122
02/18/2020 1237
Aniline
0.67
0.73
1
109
30-130
02/18/2020 1237
Anthracene
0.67
0.51
1
77
16-122
02/18/2020 1237
Benzo(a)anthracene
0.67
0.58
1
87
40-121
02/18/2020 1237
Benzo(a)pyrene
0.67
0.55
1
83
36-114
02/18/2020 1237
Benzo(b)fluoranthene
0.67
0.59
1
88
38-123
02/18/2020 1237
Benzo(g,h,i)perylene
0.67
0.64
1
95
43-120
02/18/2020 1237
Benzo(k)fluoranthene
0.67
0.55
1
82
40-126
02/18/2020 1237
Benzyl alcohol
0.67
0.76
1
115
13-121
02/18/2020 1237
4-Bromophenyl phenyl ether
0.67
0.49
1
74
46-118
02/18/2020 1237
Butyl benzyl phthalate
0.67
1.0
N 1
157
46-128
02/18/2020 1237
bis (2-Chloro-1-methylethyl) ether
0.67
0.77
N 1
116
31-102
02/18/2020 1237
4-Chloro-3-methyl phenol
0.67
0.65
1
97
49-118
02/18/2020 1237
4-Chloroaniline
0.67
0.40
1
60
17-106
02/18/2020 1237
bis(2-Chloroethoxy)methane
0.67
0.49
1
74
39-108
02/18/2020 1237
bis(2-Chloroethyl)ether
0.67
0.64
1
96
32-105
02/18/2020 1237
2-Chloronaphthalene
0.67
0.52
1
78
31-127
02/18/2020 1237
2-Chlorophenol
0.67
0.71
1
106
37-106
02/18/2020 1237
4-Chlorophenyl phenyl ether
0.67
0.49
1
73
47-116
02/18/2020 1237
Chrysene
0.67
0.56
1
84
41-124
02/18/2020 1237
Dibenzo(a,h)anth race ne
0.67
0.63
1
94
38-125
02/18/2020 1237
Dibenzofuran
0.67
0.48
1
72
45-112
02/18/2020 1237
1,2-Dichlorobenzene
0.67
0.58
1
87
39-94
02/18/2020 1237
1,3-Dichlorobenzene
0.67
0.53
1
80
30-130
02/18/2020 1237
1,4-Dichlorobenzene
0.67
0.53
1
80
39-92
02/18/2020 1237
3,3'-Dichlorobenzidine
0.67
0.43
1
64
10-119
02/18/2020 1237
2,4-Dichlorophenol
0.67
0.58
1
87
41-113
02/18/2020 1237
Diethylphthalate
0.67
0.53
1
79
49-123
02/18/2020 1237
Dimethyl phthalate
0.67
0.51
1
77
48-120
02/18/2020 1237
2,4-Dimethylphenol
0.67
0.63
1
95
33-123
02/18/2020 1237
Di-n-butyl phthalate
0.67
0.56
1
84
51-129
02/18/2020 1237
4,6-Dinitro-2-methyl phenol
0.67
0.59
1
89
40-130
02/18/2020 1237
2,4-Dinitrophenol
1.3
1.2
1
86
10-113
02/18/2020 1237
2,4-Dinitrotoluene
0.67
0.55
1
83
48-124
02/18/2020 1237
2,6-Dinitrotoluene
0.67
0.54
1
81
47-125
02/18/2020 1237
Di-n-octylphthalate
0.67
0.57
1
86
49-142
02/18/2020 1237
bis(2-Ethylhexyl)phthalate
0.67
0.57
1
86
45-128
02/18/2020 1237
Fluoranthene
0.67
0.51
1
77
26-133
02/18/2020 1237
Fluorene
0.67
0.56
1
84
19-108
02/18/2020 1237
Hexachlorobenzene
0.67
0.53
1
80
44-122
02/18/2020 1237
Hexachlorobutadiene
0.67
0.45
1
68
33-103
02/18/2020 1237
Hexachlorocyclopentadiene
3.3
2.6
1
77
18-121
02/18/2020 1237
Hexachloroethane
0.67
0.54
1
81
30-96
02/18/2020 1237
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 45
QC Data for Lot Number: VB14033
Page 95 of 114

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ45207-002
Matrix:
Solid
Batch: 45207
Prep Method:
3546
Analytical Method: 8270E
Prep Date:
02/17/2020 1743
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg)
Q
Dil
% Rec
Limit
Analysis Date
Indeno(1,2,3-c,d)pyrene
0.67
0.60
1
90
42-123
02/18/20201237
Isophorone
0.67
0.55
1
82
41-113
02/18/20201237
1-Methyl naphthalene
0.67
0.53
1
80
19-129
02/18/20201237
2-Methyl naphthalene
0.67
0.55
1
83
10-107
02/18/20201237
2-Methylphenol
0.67
0.76
N
1
114
32-107
02/18/20201237
3+4-Methylphenol
0.67
0.81
N
1
122
39-108
02/18/20201237
Naphthalene
0.67
0.50
1
75
10-112
02/18/20201237
2-Nitroaniline
0.67
0.50
1
75
45-123
02/18/20201237
3-Nitroaniline
0.67
0.42
1
64
24-127
02/18/20201237
4-Nitroaniline
0.67
0.69
1
104
48-127
02/18/20201237
Nitrobenzene
0.67
0.50
1
75
33-114
02/18/20201237
2-Nitrophenol
0.67
0.56
1
84
35-108
02/18/20201237
4-Nitrophenol
1.3
0.94
1
71
18-154
02/18/20201237
N-Nitrosodimethylamine
0.67
0.50
1
75
24-107
02/18/20201237
N-Nitrosodi-n-propylamine
0.67
0.71
1
107
32-115
02/18/20201237
N-Nitrosodiphenylamine (Diphenylamine) 0.67
0.54
1
81
53-150
02/18/2020 1237
Pentachlorophenol
1.3
1.1
1
81
27-138
02/18/20201237
Phenanthrene
0.67
0.52
1
77
16-123
02/18/20201237
Phenol
0.67
0.79
N
1
118
36-108
02/18/20201237
Pyrene
0.67
0.61
1
91
34-121
02/18/20201237
Pyridine
0.67
0.68
N
1
102
10-74
02/18/20201237
1,2,4-Trichlorobenzene
0.67
0.46
1
70
30-130
02/18/20201237
2,4,5-Trichlorophenol
0.67
0.53
1
80
46-122
02/18/20201237
2,4,6-Trichlorophenol
0.67
0.56
1
85
38-115
02/18/20201237
Acceptance
Surrogate Q % Rec Limit
2-Fluorobiphenyl
75
24-137
2-Fluorophenol
93
16-136
Nitrobenzene-d5
70
12-144
Phenol-d5 100 26-148
Terphenyl-d14 94 20-127
2,4,6-Tribromophenol 81 27-128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 45
QC Data for Lot Number: VB14033
Page 96 of 114

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 97 of 114
Page 42 of 45

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 45
Page 98 of 114

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 99 of 114
Page 44 of 45

PACE ANALYTICAL SERVICES, LLC
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Sample Receipt Checklist (SRC)
CJi--nt. PUC' A vilytied GOOleC IF, erted b ldatc; ta= ? 42714f20111 O. VD14033
cat `vuclnipL_ ST Clictrt UPS W1 Fedrx Othcr: -
-K L—I_Tti0 1. c CUM-Ddy seals PIMM r oil L[Lv cvulgr?
Yr`-8 Na NA,2, Ifsustod scab;were r-ticn{, wweth intartan> unbrokcr.,!
pi ] 51 Tr NA — Chlorine Strip ID; NA _ 'J ested b NA
Y -. _
ie}nal tcmpwnrure ujwmrc�olptI Defivad(CL)rti-ct=d)ternpej lLrc upou receipt 'Y�wPlid Sapp -Cep if}; L9 t J
2,¢ (2.4 aC NA /NA OC NA /NA T. NA INA GC
Nlctb0d Q l'9lttpeu:rLerLv B1rrLLk mrl inst BpEtle; 1K (iun [D: _6 1R Gun Cr rrertior FPutaw-= 0 °C
Me'-13(3 3 Of cltalant: 0 %Ve[ Jeo. L] lce Pack S 0 D: Tuo ❑ N1oLie
.p� if ;crape -al -UM of airy U93Tpr axceeded 6.0 , was Projcat Managar Notified?
El r la A Phi was NDLJ Gcd : phtmp I Mai [ I If rfacc (circle one)-
® Yet 0 Ttia p NA 4. Js he W--nmel�[al cothrieL parkin slip attachee to thi~ >=arm?
Yes ❑'N 3, ?dare pan_unr cudndy rrvicedr:ras (3+elirrquiahedlrooeived) fbllowcd?
❑ Q� Ye4 No' 69 Were �n �,lc, IUs lismdon the CCCC
ifr ❑ No .'. Were ^,trGtplc IDs 19'soed on a[I �uaplq �camainers?
Yes ❑ No S, Wfls col Iadiai: dab a 01[IC listed ork the COC?
Yes ❑ No 4. WSS colleutidn date & rime listed rn all sampir q,0nta[ue1M?
® Yes ❑ NQ 11). Did all ContiLIrlor Iahel in£onnatioc (ID, date„ tlm.a) ee SviCh the COC?
Yes d Na 11. Were tegfs to be µer_uLTocd JisrMd on the COC?
J 2. laid all samples arri vu in the propw con La ii iers fix eacl= Wns: andfar in good oaitdition
Iunbrplcon, lids on, cee,)?
I des � Ja t,. was adegin."samo[r; volimneavaitabfe7
LJ 'a� Na 14, Were ali dam pies remivod within ;S lie hol4hig [inte o- 4$ hotrs, Jsi�ichever COMC3 fl.,.
Yes 7�Fa 15, Mere an ' 3ampics cDntain4l m�iing+axM%9 Circle oA¢] samples Not listed oil C'OC?
t - r^ r�IGA znd i25 175 ,ampfes uer; bLtbbfes pr�u�Gt>`:peZ-s[Ze' (�r;"Or 6-rttn in dfitci=Cc
❑ yes 11®
Ja NA ii3 auv of the VOA via Is?
❑ Ye No NA 17, We-e all DR&rr etalAutriern aaat JLS nxxiN'e-d at a R of -< 2''
❑ Yes lMcl, ®TNA 118. %%Ier* all oyanidc sTnAIDle.3 Imuived at a pH > 12 and sulfide um ]� d n
CJ Yed L- lol 0
Ls races V-� ELL a
p r��ol?6?5 f� �.. mgfLj sLrmples tree txf t�B.3ilual
El `fys ❑ No DNAW= client re3Tlsriishtegl[MSLs (L& regge;ted dilLlNttn4, 1wlSI[�+pSD designations, eLc...}
raireetly zlnscribed r ant the CQC into the ccminf;nt 9ccation in L1MS7
❑ Yes Na 21. wm `he ue[e riumber listed on tlla cuntaEnEr label If vas. Quote # NA
SAMple Preser3'3tlau (Mast be L41mpleted ibr dry Earnpic(sj incntt oCtly ya nrveii rr a i lh keadspaGt.) ..
Sampler NA _were "rived Fncartiectly Far-;x.rved. aMd were adjvSlod acocwdhigl}
n %ample neceivingwith NA. lnl.of�;irckone.112S 4, HMOl ,HCI,-NaOH LwjugSj�_V NA
Din L` of preservation NA = If MOM thin one pry irw�tive is nocded, p1rax rare in Llle onmmMts below,
Sa:npie(s) -NA WG"e re-iwd with bubbles :}
� 6 ram in diumrt_r.
Sj'jSI dac NA were receivzdwitt TRC> 0-5 iigfL(If 0i� is no) and trwe
IdjaslcdacentrlFnei}'[�; sou lereceiving3vikh2cdiumthiwsulfate(N,o S�O�}witliSaea ill �1A
bacoda laOets appfiod by: BNf(3 Date. OVI V2020
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 45
Page 100 of 114

0
aceAnalytical
Report of Analysis
Pace Analytical Services, LLC
2225 Riverside Drive
Asheville, NC 28804
Attention: Lord Patton
Project Name: A19-158-02
Project Number: 92464978
Lot Number:VB25035
Date Completed:03/03/2020
Revision Date: 03/03/2020
03/03/2020 4:50 PM
Approved and released by:
Project Manager: Cathy S. Dover
pCC/►F0
ANSI National Accreditation Board
qe�
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 101 of 114
Page 1 of 14

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical Services, LLC
Lot Number: VB25035
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier.
This PDF report has been revised per client to report any estimated J flagged results to the
MDL/DL. The results were reprocessed by the reviewer and this sample is non -detect and there
were no detects down to the MDL/DL of 0.0020 mg/L.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 102 of 114
Page 2 of 14

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: VB25035
Project Name: A19-158-02
Project Number: 92464978
Sample Number Sample ID Matrix Date Sampled Date Received
001 S-12 Solid 02/12/20201240 02/14/2020
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 103 of 114
Page 3 of 14

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical Services, LLC
Lot Number: VB25035
Project Name: A19-158-02
Project Number: 92464978
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 14
Page 104 of 114

SPLP Semivolatiles
Client: Pace Analytical Services, LLC Laboratory ID: VB25035-001
Description: S-12 Matrix: Solid
Date Sampled:02/12/2020 1240 Project Name: A19-158-02
Date Received:02/14/2020 Project Number: 92464978
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1312/3520C 8270E 1 03/02/2020 1550 JCG 02/28/2020 1514 46424 02/26/2020 0140
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1-Methylnaphthalene 90-12-0 8270E ND 0.0080 0.0020 mg/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
Nitrobenzene-d5
Terphenyl-d14
92 37-129
88 38-127
106 10-148
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 105 of 114
Page 5 of 14

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: VB25035
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 106 of 114
Page 6 of 14

SPLP Semivolatiles - MB
Sample ID: VQ46424-001 Matrix: Solid
Batch:46424 Prep Method: 1312/3520C
Analytical Method: 8270E Prep Date: 02/28/2020 1514 Leachate Date: 02/26/2020 0140
Parameter Result Q Dil LOQ DL Units Analysis Date
1-Methyl naphthalene ND 1 0.0080 0.0020 mg/L 03/02/20201500
Acceptance
Surrogate Q % Rec Limit
2-Fluorobiphenyl
96
37-129
Nitrobenzene-d5
89
38-127
Terphenyl-d 14
115
10-148
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: VB25035
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 107 of 114
Page 7 of 14

SPLP Semivolatiles - LCS
Sample ID: VQ46424-002
Matrix: Solid
Batch:46424
Prep Method: 1312/3520C
Analytical Method: 8270E
Prep Date: 02/28/2020 1514
Leachate Date: 02/26/2020 0140
Spike
Amount
Result
% Rec
Parameter
(mg/L)
(mg/L) Q
Dil % Rec
Limit Analysis Date
1-Methyl naphthalene
0.40
0.34
1 84
42-126 03/02/20201525
Surrogate
Q % Rec
Acceptance
Limit
2-Fluorobiphenyl
88
37-129
Nitrobenzene-d5
86
38-127
Terphenyl-d 14
101
10-148
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: VB25035
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 108 of 114
Page 8 of 14

SPLP Semivolatiles - MS
Sample ID: VB25035-001 MS Matrix: Solid
Batch:46424 Prep Method: 1312/3520C
Analytical Method: 8270E Prep Date: 02/28/2020 1514 Leachate Date: 02/26/2020 0140
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
1-Methyl naphthalene ND 0.40 0.35 W 1 88 42-126 03/02/20201614
Acceptance
Surrogate Q % Rec Limit
2-Fluorobiphenyl
94
37-129
Nitrobenzene-d5
89
38-127
Terphenyl-d 14
107
10-148
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: VB25035
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 109 of 114
Page 9 of 14

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 110 of 114
Page 10 of 14

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 111 of 114
Page 11 of 14

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 14
Page 112 of 114

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 14
Page 113 of 114

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 14
Page 114 of 114

APPENDIX 6
TIER 2 RISK EVALUATION DATA SHEET

Risk for Individual Pathways
rim
Version Date: December 2019
Basis: November 2019 EPA RSL Table
7
Site ID: Cashier Canoe Club
Exposure Unit ID:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Receptor
Pathway
Risk Carcinogenic
Hazard Index
Risk exceeded`.,
Resident
Soil
NC
NC
NC
NC
Groundwater Use*
NC
NC
Non -Residential Worker
Soil
NC
NC
NC
Groundwater Use*
NC
NC
NC
Construction Worker
Soil
NC
NC
NC
Recreator/Trespasser
Soil
NC
NC
NC
Surface Water*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
NC
NC
NC
Soil Gas to Indoor Air
NC
NC
NC
Indoor Air
NC
NC
NC
Non -Residential Worker
Groundwater to Indoor Air
NC
NC
NC
Soil Gas to Indoor Air
NC
NC
NC
Indoor Air
NC
NC
NC
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target Receptor Concentrations Exceeded?
Groundwater
Source Soil
Exceedence of 21, at Receptor?
NO
Source Groundwater
Exceedence of 21, at Receptor?
NC
Surface Water
Source Soil
Exceedence of 2B at Receptor?
NO
Source Groundwater
Exceedence of 2B at Receptor?
NC
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC
213 Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based
closure.
3. NM = Not Modeled
4. NC = Pathway not complete
North Carolina DEQ Risk Calculator