HomeMy WebLinkAboutWQ0008778_Residual Annual Report 2019_20200302Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0008778
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer Kendall.Williams@ncdenr.gov
Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
Ifinnerty@synagro.com
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0008778
Applicant\Permittee * SYNAGRO
Facility Name * Town of Farmville
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for Town of Farmville
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
FARMVILLE NC 2019 Annual Report FINAL.pdf 11.03MB
upload only 1 R7F document. NL@iple documents must be combined into one R7F file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/27/2020
435 Williams Court, Suite 100
Baltimore, .nfff7 21220
Nvwwsynagro.com
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0008778
Dear NCDEQ:
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the Town of Farmville, NC.
I€ you have any questions or need additional information, please do not hesitate to contact
James Shoulders at (252) 753-3913 or Melinda Boyd at (336) 909-8627.
SinceteIy,
Detrick Shivar
Environmental Compliance Manager
Enclosures
cc: James Shoulders
Melinda Boyd, Synagro
YOUR PARTNER FORA CLEANER,GREENERVI/ORLD
TOWN OF FARMVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No, WQ0008778
2019 ANNUAL REPORT
Town of Farmville, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
5. Soil pH & Lime Application Records
7. Soil Analyses
SECTION 1
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00008778 County Pitt Year 2019
Facility Name (as shown on permit) F—armville WWTP NPDES No. NCO029572
Land Application Operator Synagro Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, slip Part A, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 7
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 23.58
Total number of acres utilized for land application during the year: 39.1
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
I . Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105 (a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I 1 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C -- Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." /1 i A . . rl
David P. I-lodgkins, Town Manager Jair ('l `[ II 7-oy,3
Per itte Name an itle (type or print) Signatu er e
11 702A> C�
Signature o€Prep r* Date Signatu if Land ApplidV Date
(if different from Permittee) (if different from erm'ttee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
FARMVILLE, NC
FARMVILLE, NC AEROBICALLY DIGESTED LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
April 2019 353,400.00 G 23.58 D 21.39
YEARLY TOTAL 353,400M G 23.58 D 21.39
1/30/2020
SECTION 2
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0008778
Facility Name: FARMVILLE, NC
NPDES# : NCO029572
or WQ# (residual only)
WWTP Name: FARMVILLE
Residuals Analysis Data
Product Type AEDLIQ
Date Sampled (grab) or 03/06/19
Date Composited
Percent Solids 1.60
PARAMETERS (mglkg dry weight)
Arsenic
5.22
Cadmium
1.24
Mercury
0.653
Chromium
35.1
Copper
366
Lead
24
Molybdenum
5.86
Nickel
22.2
Selenium
<5
Zinc
822
Total Phosphorus
22800
TKN
69400
Ammonia -Nitrogen
16300
Nitrate and Nitrite
616
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF PREP
Date >> U2..
DENR FORM RSSF (512003) Printed: Wednesday - February 5 2020 at 18:48:44 for: 2015 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0008778
Facility Name: FARMVILLE, NC
NPDES# : NCO029572
or WQ# (residual only)
WWTP Name: FARMVILLE
Residuals Analysis Data
Product Type AEDLIQ
Date Sampled (grab) or 03/06/19
Date Composited
Percent Solids 1.60
PARAMETERS (mglkg dry weight)
Aluminum
11000
Calcium
10600
Magnesium
2920
pH
6.50
Potassium
3990
Sodium
1810
Laboratory
Waypoint Analytical Virginia Inc.
1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submittinglalse information, including the possibility of fines and imprisonment for knowing violations."
X J4 �� I'
(SIGNATURE OF PREP
NR - Data Not Reported or Data Not Required
Date 911 ?ato
DENR FORM RSSF-13 (712002) Printed: Wednesday - February 5, 2020 at 18:49:06 for: 2015 01
Waypointo
ANALYTICAL
3/15/2019
Synagro Central/Farmville
Marshall Puryear
284 Boger Road
Suite 204
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-067-0202
Project Description: Farmville WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax 804-271-6446
www.waypointanalytical.com
Dear Marshall Puryear:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam,. W (,—/-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona A70629 New Jersey VAO11 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Page '1 of 6
AdIIIIIIIIIIIII
VV
Waypoint.. 42V
4':W-tn'--�. ��
Report Number: 19-067-0202
Client Project Description: Farmville WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
6SI92
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
65192
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
SM-4500-NH3C
WTN
65192
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
9045D
WTN
65192
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
4500NO3F-2011
WTN
65192
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
6010D
WTN
65192
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
SW-7471B
WTN
65192
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
SM-4500-NH3C-TKN
WTN
65192
Farmville WWTP
Solids
03/06/2019 10:00
03/08/2019
SM-2540G
WiN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
Report Number: 19-067-0202
Account Number: 46454
Send To: Synagro Central/Farmville
Marshall Puryear
284 Boger Road
Suite 204
Mocksville , NC 27028
Lab Number: 65192
Sample Id : Farmville WWTP
Waypo0t.a,
(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: Farmville WWTP
REPORT OF ANALYSIS
Date Sampled: 31612019 10:00:00
Date Received: 03/08/2019 00:00
Date Reported: 03/15/2019
Total Solids "
1.60
16000
100.0
CJR
03/13/2019 16:34
Moisture *
98.40
100.0
CJR
03/13/2019 16:34
Total Kjeldahl Nitrogen
6.94
69400
250
CLP
03/14/2019 09:30
Phosphorus
2.28
22800
50.0
KKM
03/141201918:24
Potassium
0.40
3990
50.0
KKM
03114/201918:24
Sulfur
0.78
7780
50.0
KKM
03/141201918:24
Calcium
1.06
10600
250
KKM
03/141201918:24
Magnesium
0.29
2920
50.0
KKM
03/141201918:24
Sodium
0.18
1810
250
KKM
03/14/201918:24
Iron
36100
50.0
KKM
03/14/201918:24
Aluminum
11000
50.0
KKM
03/14/201918:24
Manganese
438
5.00
KKM
03114/201918:24
Copper
366
2.50
KKM
03114/201918:24
Zinc
822
12.5
KKM
03/14/201918:24
Ammonia Nitrogen
1.63
16300
100
ZBD
03/14/2019 12:30
Organic N
5.31
53100
250
03/14/2019 09:30
Nitrate}Nitrite-N
616
4.74
ZBD
03/151201915:26
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding
Time
pwic-
ourrepoils and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made
to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
SM-2540G
S M-2540 G
SM-4500-NH3C-TKN
601 OD
601 OD
6010D
6010D
6010D
6010D
6010D
6010D
6010D
601 OD
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
PC 10i�
Pauric McGroary
Agronomist
Page 3 of 6
Report Number: 19-067-0202
Account Number: 46454
Send To: Synagro Central/Farmville
Marshall Puryear
284 Boger Road
Suite 204
Mocksville , NC 27028
s
ya
Wa of nt
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: Farmville WWTP
REPORT OF ANALYSIS Date Sampled: 3/6/2019 10:00:00
Lab Number: 65192 Date Received: 03/08/2019 00:00
Sample Id : Farmville WWTP Date Reported: 03/15/2019
Cadmium
1.24
1.00
KKM
03114/201918:24
6010D
Chromium
35.1
2.50
KKM
03114/201918:24
6010D
Nickel
22.2
2.50
KKM
03114/201918:24
601OD
Lead
24.0
3.00
KKM
03/14/201918:24
601OD
Arsenic
5.22
5.00
KKM
03/14/201918:24
6010D
Mercury
0.653
0.0155
TJS
03/13/2019 15:55
SW-7471 B
Selenium
<5.00
5.00
KKM
0311412019 18:24
6010D
pH *
6.5
JSL
03/1512019 09:21
9045D
Molybdenum
5.86
2.50
KKM
03/14/201918:24
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series
is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding Time
Our reports and fetters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 4 of 6
s
Waye nt.,.
PANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46454
Customer Name: Synagro CentrallFarmVille
Report Number: 19-067-0202
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
0 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
10 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 -- compliance criteria met
0 Yes
0 No
0 NIA
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Brandi Watson Date & Time: 1:03/08/2019 12:42:47
Page 5 of 6
m
0
0
rn
SAMPLING LOG #
A �
AL
UN Off' CUSTODY
R�
IlII11I�IIllllllllllllllllll[11IIIIIIIIIII
IllllIIIIIIIII�III��I�
l l
�4� -0202 ORD & ANALYSES
CUSTOMER:-
SYNA ��
®
Svnaaro CenlrallFarmvifle
03-08-2019 RECORD$�,
Farmvflle UVWTP 11 U-51
PROJECT MANAGER:
f sampling procedures
were used aurfng me cuuection of these samples.
Phone: }
} -1 �
SAMPLER
A & L
CUSTOMER
SAMPLING
SAMPLE
# OF SAMPLING METHOD METHOD
LAB #
SAMPLE I.D.
LOCATION
TYPE
CONTAINERS DATE TIME PRESERVED SHIPPED
j
Relinquished by Sampler:
4;12A LAA
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS:
For � L
monitoring purposes.
Date Time Recieved by:
D to Time Red y:
3��, c
Lute Time Recieved by:
PO#:
REMARKS:
SAMPLE ANALYSIS REQUEST
I.D. SLR I SL2 NHS N NO3-N Organic Cd Cr Ni Pb As Hg Se pH CSC03 Volatile Mo CI NO -N
equiv. Solids z
SLI., Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SO 9: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2015-01-AEDLI4-NC FARMVILLE, NC AEROBICALLY DIGESTED 3/6/2019 3/112019-613012019 0.5062
LIQUID
Na mgll = (Na mglkg x % Solids) + 100 = (1810 x 1.6000) � 100 = 28.96
Ca mgll = (Ca mg/kg x % Solids) + 100 = (10600 x 1.6000) + 100 = 169.6
Mg mg1I = (mg mg/kg x % Solids) 100 = (2920 x 1.6000) _ 100 = 46.72
Na meq = Na mg1I :. Molec.Wgt.Na = 28.96 + 23 = 1.25913
Ca meq = Ca mgll + Molec.Wgt.Ca = 169.6 + 20 = 8.48
Mg meq = Mg mgll � Molec.Wgt.Mg = 46.72 + 12 = 3.89333
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.25913 + SgrRoot[0.5(8.48+3.89333)] = 0.506224
Printed: 2/5/2020
Page 1 18:51
SECTION 3
FACILITY NAME: FARMVILLE, NC
OWNER: HAROLD FLANAGAN
SITE 4: NC P1 00001 FIELD# : PI 00001 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION .FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT 4: W00008778 ANNUAL DRY TONS APPLIED: 7.86
OPERATOR: HAROLD FLANAGAN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40
Page: 1
Lime Applied ***
Date
LbslAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(PP-)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/17/19
117,800.00 (G)
18406.2501
1.60
1.228
FARAEDL
MOIST
0-<1/2"
SUA
0.5
0.30
69,400.p
16,300.00 p
616.00 p
24696
CORN
Apr-19
117,800.00 (G)
18,406.250
I
1
1
1
Total Gallons/Ac: 18,406.25
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 61
0.013 0.003 0.086 0.899 0.059 0.002 0.014 0A55 0.012 2.019 56.00
Cumulative lbs/acre 0.273 0.162 4,783 56.419 2.737 0.060 0.609 3.721 0.240 44.748
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
148
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
FARAEDL=FARMVILLE, NC AEROBICALLY DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
FACILITYNANIE: FARMVIILE, NC
OWNER: FIAROLD FLANAGAN
SITE #: NC PI 00001 FIELD# : PI 00001 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: WQ0008778 ANNUAL DRY TONS APPLIED: 15.72
OPERATOR: HAROLD FLANAGAN' CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 32.70 ACRES PERMITTED: 32.70
Page: I
Lime Applied ***
Date
LbstAc
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
2ation
nation
TKN
Nitrogen
and
(PP-)
Crop
MONTH
Total
Per Aare
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/17/19
68,200.00 (G)
2085.627
1,60
0,139
FARAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
69,400.p
16,300.00 p
616.00 p
24696
BERMUDAGRASS
4/18/19
167,400,00 (G)
5I19.266
1.60
0.342
FARAEDL
DRY
0-<1/2"
SUR
0.5
0,30
69,400. p
16,300.00 p
616.00 p
24696
BERMUDAGRASS
Apr-19
235,600.00 (G)
7,204.893
Total Gallons/Ac: 7,204.89
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 24
0.045 0.001 0.034 0.352 0.023 <.001 0.006 0.021 0.005 0.790 21.92
Cumulative lbs/acre 0.015 0.006 0.155 1.363 0.090 0.002 0.020 0.085 0.018 2.429
Permit PAN Limit (lbs/acre) IA Crop/2nd Crop
230
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15 0
375.0
89.0
2500.0
FARAEDL = FARMVILLE, NC AEROBICALLY DIGESTED LIQUID
X 9\ 0 n�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or w&kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SUR1N - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
SECTION 4
SUMMIT
,
Anafytical Laborgloroals
March 20, 2019
Melinda Boyd
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Farmville W WTP
Dear Melinda Boyd:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.• (330) 253-4489
Mebsite: htt ://wiviv.settek.coni
Order No.: 19030281
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/6/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
A
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho 01-100923, Illinois
200061, Indiana C -OHA 3, Kansas F-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New .lersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
011009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 31
UMMIT SunanaitEnvir.onnaental Technologies, Inc. Case Narrative
S3310 Win St.
01040P,IrJEWrAL TZC1VNM()C4i)FS, INC Cuyahoga Falls, Ohio 44223 WO#: 1.9030281
rr J 1T;r{`yllcal Laboratoirior TEL: (330) 253-8211 FAX., (330) 253-4489
Website: hitn:/hviviv.settek.coiaa date: 3/20/2019
CLIENT: Synagr•o
Project: Parmville WWTP
WorkOrder Narrative:
19030281: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Notes:
CCV 40ng 18589 SVOC-MSTR S(8270): CCV exhibited high recovery for Pentachlorophenol;
Sample is ND
Original
Page 2of31
' SF 5`u'7a'nrt EnvirorzrnentalTechnoilogies, In Qualifiers and Acronyms
ffl SUMM3310 Win S
EN,',IROWrIy WrA Cuyahoga Falls, Ohio442� WO#: 19030281
Mv,-,i Mittel Laboratorlas TEL: (330) 253-8211 FAX.- (330) 253-446
Website: httv:11Www.settekxo Date: 3/20/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
11.1 The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The 1CB or CCB contained reportable amounts of analyte.
QC -I#- The CCV recovery failed low (-) or high (+),
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCSILCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+),
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
.Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvI
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Deporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3of31
SUMM111
SunamitEnvironnaentalTechnolagies, Inc. Workorder
3310 Win St.
ENVIRONNIrNTA.L TECH O1 CtMr3, WC, Cuyahoga Falls, Ohio 44223 Sample Summary
ArrMyNcal Laboralarfoe TEL: (330) 253-8211 Ff1X.• (330) 253-4489 WOO: 19030281
Website: http://�vw.setlelc.com 20-Mar-19
CLIENT: Synagro
Project: Farmville WWTP
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
1.9030281-001 Farmville WWTP 3/4/2019 12:15:00 PM 3/6/2019 10:20:00 AM Sludge
Page 4 of 31
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Sannnait Environnsental Technologies, Lac. Analytical Report
su3310 N�in St.
l"I`WIrIONffi1l='NTA.L YEC!hNOLtjQdrR; INC Cuyahoga Fails, Ohio 44223 (base report)
An atyilcal LaborafewoG 7TL: (330) 253-8211 FAX: (330) 253-4489 WD#: 19030281
Ffiebsite: http://lviviv.seltel(.coni Date Reported: 3/20/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/4/2019 12:15:00 PM
Lab ID: 19030281-OOIA
Project: Farrnville WWTP
Client Sample ID Fartnviile WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND 0.00200 mg1L
SW7470A SW7470A Analyst: DNS
1 3/7/2019 4:37:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW301OA Analyst: KMO
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
3/11/2019 12:02:56 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
3/110019 12:02:56 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
3/11/2019 12:02:56 PM
TCLP Chromium(Cr)
N❑
0.200
mg/L
1
3/11/2019 12:02:56 PM
TCLP Lead(Pb)
ND
0,500
mg/L
1
3/11/2019 12:02:66 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
3/11/2019 12:02;56 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
3/11/2019 12:02:56 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC
Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichlorobenzene
ND
0.0800
mglL
2
3/13/2019 7:05:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
3/13/2019 7:05:00 PM
2,4,6-Trichlorophenol
ND
0.200
mglL
2
3/13/2019 7:05:00 PM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2
3/13/2019 7:05:00 PM
Cresols, Total
ND
4.00
mg1L
2
3/13/2019 7:05:00 PM
Hexachloro-1,3-butadiene
ND
0.0160
mg/L
2
3/13/2019 7:05:00 PM
Hexachlorobenzene
ND
0.0400
mg/L
2
3/13/2019 7:05:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
3/13/2019 7:05:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
3/13/2019 7:05:00 PM
Pentachlorophenol
ND
0.200
QC+ mg/L
2
3/13/2019 7:05:00 PM
Pyridine
ND
0.200
mg/L
2
3/13/2019 7:05:00 PM
Surr: 2-Fluorophenol
63.1
10 - 109
%Rec
2
3/13/2019 7:05:00 PM
Surr: Phenol-d6
64.6
10 - 109
%Rec
2
3/13/2019 7:05:00 PM
Surr: Nitrobenzene-d5
78.8
19 - 120
%Rec
2
3/13/2019 7:05:00 PM
Surr: 2,4,6-Tribromophenol
742
10 - 120
%Rec
2
3/13/2019 7:05:00 PM
Surr: 2-Fluorobiphenyl
75.6
22 - 117
%Rec
2
3/13/2019 7:05:00 PM
Surr: p-Terphenyl-dU
96.3
34 - 116
%Rec
2
3/13/2019 7:05:00 PM
Qualifiers: E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine
area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
0 RSD is greater than RSDlimit
P Second column
confirmation
exceeds
PL Permit Limit
R R-PI) outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal
< MDL
Page 6 of 31
summly
ENVIfaONNIENTAL IrEGHW01_QGf r,. Wf
frAmWyUca1 Laboratarlc:=
SmavaaitEnvirorvneritul Technologies, bac.
3310 GYin St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 253-4489
[Vehsite: hllp:/hv7vw.settekcOin
AnalyticalReport
(base report)
WO#: 19030281
Date Reported: 3/20/201.9
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/4/2019 12:15:00 PM
Lab ID: 19030281-OOIA
Project: Farmville WWTP
Client Sample ID Fartuviilc WWTP
Analyses Result
RL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total
ND
0.250
mg/L
10 3/15/2019 11:00:00 PM
Toxaphene
ND
0.500
mg/L
10 3/15/2019 11:00:00 PM
Endrin
ND
0.0250
mg/L
10 3/15/2019 11:00:00 PM
gamma-BHC
ND
0.0250
mg/L
10 3/15/2019 11:00:00 PM
Heptachlor
ND
0,0250
mg/L
10 3/15/2019 11:00:00 PM
Heptachlor epoxide
ND
0,0250
mgJL
10 3/15/2019 11:00:00 PM
Methoxychlor
ND
0.0250
mgJL
10 3/16/2019 11:00:00 PM
Surr: TCMX
66.2
10 - 119
%Rec
10 3/15/2019 11:00:00 PM
Surr: DCB
88.2
10 - 119
%Rec
10 3/15/2019 11:00:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
2,4,5-TP
ND 1.00 mg/It-
ND 0.500 mg1L
SW8151A SW8151A Analyst: SFG
1 3/12/2019 10:53:00 PM
1 3/12/2019 10:53:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260 SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.125
mgJL 25 3/7/2019 12:48:00 PM
1,2-Dichloroethane
ND
0.125
mg/L 25 3/7/2019 12:48:00 PM
MEK
ND
0.625
mgJL 25 3/7/2019 12:48:00 PM
Benzene
ND
0.125
mg/L 25 3/7/2019 12:48:00 PM
Carbon tetrachloride
ND
0.125
mglL 25 3/7/2019 12:48:00 PM
Chlorobenzene
ND
0,125
mgJL 25 3/7/2019 12:48:00 PM
Chloroform
ND
0.125
mg/L 25 3/7/2019 12:48:00 PM
Tetrachloroethene
ND
0.125
mg1L 25 3/7/2019 12:48:00 PM
Trichloroethene
ND
0.125
mg/L 25 3/7/2019 12:48:00 PM
Vinyl chloride
N❑
0,0500
mg/L 25 3/7/2019 12:48:00 PM
Surr: 4-Bromofluorobenzene
92.0
70 - 130
%Roc 25 3/7/2019 12'A8:00 PM
Surr: Dibromofluoromethane
90.7
70 - 130
%Rec 25 3M2019 12:48:00 PM
Surr: Toluene-d8
104
70 - 130
%Rec 25 3/7/2019 12AR00 PM
Qualifiers: L Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine
area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery Inuits Original
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 7 of 31
- -
S3310
� � � �-
Summit Environmental Technologies, Ir��•.
Win fit.
Analytical Report
EfWIRONNIENTAL YE-C4iNMCf{;��5, INC
Clojahoga Falls, Ohio 44223
(base report)
Anaiy0cal Laboratories
TEL: (330) 253-821.1 FAX: (330) 253-4489
WO#: 19030281
Website: hU,2:11iyiviv.settelr..com
Date Reported: 3/20/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/4/2019 12:15:00 PM
Lab ID:
19030281-OOIA
Project:
Farmville WWTP
Client Sample ID Fanmville WWTP
Analyses
Result RL Qual Units
DF Date Analyzed
RCI-SOLID-WI IGNITABILITY1030
SW9014 Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND 0.485
mg/Kg 1 3/14/2019 4:00:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW1030 Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1 3/12/2019 12:30:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9045D Analyst: VVK
PH (SW9045D)
pH 6.1
s.u.@20.5C 1 3/7/2019 4:01:53 PM
RCI-SOLID-WI IGNITABILITY1030
SW9034 Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND 25.0
mg/Kg 1 3/14/2019 4:00:00 PM
Qualifiers: r Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to deterinine area response
MC Value is below Minimurn Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal < MDL
Page 8 of 31
strmnnit Environmental Technologies, Inc. Accreditation Program
summist 3310 win St. Anal tes Report
ENIV11IONIAENTAL TEC�i�ICl�ilt;lt=S, INC Cuyahoga Falls, Ohio 44223 Y p
An riytiCal Labaratar'les TEL: (330) 253--3211 Fff: (330) 253-4489 WO#: 19030281
Website: htW:11www.sette1c com 20-Mat,-19
Client: Synagro State: NW
Project: Farinville WWTP Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19030281-001A Sludge
Ignitability of Solids (SW-846, 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
SVOC SW-846: 9151 I-lerbicides-TCLP
2,4,5-TP
A
Sludge
SVOC SW-846: 8151 Herbicides-TCLP
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW13 11/808 1)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SWI311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
I,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols,Total
A
Sludge
TCLP Sena-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SWI311/8270)
Hexachiorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexacbloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentael-lorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/827.0)
Pyridine
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original 41
Page 9 of 31
- � �, � Summit Environmental Technologies, Inc. Accreditation Program
3310 Win St. Analtes Report
ENIVIRLMNI W-rAL 7 Ca��t l_.t� �.r• , INC Cuyahoga Falls, Ohio 44223 Y p
A nMyflcal Laborato6ae- TEL: (330) 253-8211 FAX- (330) 253-4489 WO#: 19030281
Website: h0p.-Ilwww.settek eom 20-Mar-19
Client: Synagro State: NW
Project: Farmville WWTP Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19030291-001A Sludge
TCLP Volatiles Analysis
II-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Diebloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetfachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroetbene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original # 1
Page 10 of 31
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Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Insummiar 3310 Win St.
E€ VIinONh1ENTAL IFECHN01 Ck JE;-3j .?' Cuyahoga Falls, Ohio 44223
WO#: 19030281
AnalyOcal Laboralori€s TEL: (330) 253-8211 FAY: (330) 253-4489
Websiie: htlp:llwww.settek-.com 20-Mar-19
Client: Synagro
Project: 1 armville WWTP BatchID: R95445
Sample ID LCS-R95445
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u. ,20.2C
Prep Date:
RunNo: 95445
Client ID: LCSW
Batch ID: R95445
TestNo: SW9045D
Analysis Date: 3/7/2019
SegNo: 1987930
Analyte
Result
PQL SPK value SPK Ref Val %RBC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
7.0 0 101 90
$ Value above quantitation range
M Manual Integration used to determine area response
Q RSD is greater than RSDlimit
R RPD outside accepted recovery limits
110
H HoIding times for preparation or anal
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 22 of 31
I. UMMI]y Summit Environmental Technologies, Inc. QC SUMMARY REPORT
MS 3310 Win St.
Cuyahoga Falls, Ohio 44223
WO#: 19030281
A4 Wyr)cjal TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httl2://www.settek.com 20-Afar-19
Client: Synagro
Project: Farmville WWTP
BatchID: R95445
Sample ID 19030088-005ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.2C
Prep Date:
RunNo: 95445
;lient ID: BatchQC
Batch ID: R95445
TestNo: SW9045D
Analysis Date: 3/7/2019
SegNo: 1988115
\nalyte
Result
PQL SPK vaiue SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.8
7.7 0.5 5
)ample ID CHECK 7
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@20.6C
Prep Date:
RunNo: 95445
;lient ID: LCSW
Batch ID: R95445
TestNo: SW9045D
Analysis Date: 3/7/2019
SegNo: 1988116
\nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
Qualifiers: S Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
7.0 0 101 98.6 101.4
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery Iimits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 23 of 31
fflsummly
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIiLONMENTAL E C#ili4]4 jai h'
Cuyahoga Falls, Ohio 44223
W09: 19030281
Anjry rical Labrrafar os TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: hRp://www.settek.con7,
20-Mar-19
Client:
Synagro
Project:
Farraville WWTP
BatchID: R95604
Sample ID LCS-R95604
SampType: LCS
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: LCSS
Batch ID: R95604
TestNo: SW1030
Analysis Date: 311212019
SegNo: 1994382
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 7.84 7240 0 108 70 130
Sample ID 19030190-001ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: BatchQC
Batch ID: R95604
TestNo:
SW1030
Analysis Date: 3/12/2019
SegNo: 1994384
Anaiyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Vai
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19030281-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: Farmville WWTP
Batch ID: R95604
TestNo: SW1030
Analysis Date: 3/12/2019
SegNo: 1994386
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19030364-001ADUP
SampType: DUP
TestCode:
lgnitability_S Units:
Prep Date:
RunNo: 95604
Client ID: Batch=
Batch ID: R95604
TestNo:
SW1030
Analysis Date: 3/12/2019
SegNo: 1994388
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
F Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding tunes for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 24 of 31
MM
,� SummitEnvironmental Technologies, Inc. QC SUMMARY REPORT
MSU3310 Win St.
IENVIITOINNIE t-ITAL Cuyahoga Falls, Ohio 44223 WO#: 19030281
.arparyrlcaf Laboraione TEL: (330) 253-8211 FAX: (330) 253-4489
Website: htt :11www.settek.com 20-Mar-19
Client: Synagro
Project: Fannville WWTP BatchID: R95604
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 25 of 31
ummint
Summit ,Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EENWItZONMENTALric—CHNGLDGtiE5F3FP,: Cuyahoga Falls, Ohio44223
A;rlaPrC f La.baralarles TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 19030281
YYebsite: hgpWwww.settek.com
20-Mar--19
CIient:
Synagro
Project:
Parraville WWTP
BatchED: R95757
Cyanide, Reactive ND 0.490
Cyanide, Reactive 9.54 0.485 10.00 0 95.4 85 110
Cyanide, Reactive ND 0.435 0.5000 0 95.3 50 150
Cyanide, Reactive 9.61 0.495 10.00 0,2400 93.7 81.6 122
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
0 RSD is greater than RSDiimit P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 26 of 31
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffl SUMMIRt 3310 Win St.
ENVI eOhlrTEIN7AL 17ECHNOLC 5= ' ? Cuyahoga Falls, Ohio 44223
A..rF8i'ydCz1 Labaralerms TEL: (330) 253-8211 FAX..- (330) 253-4489 WO#: 19030281
Website: hitp://www.settek.CGM 20-Mar-19
Client: Synagro
Project: Farmville WWTP
BatchID: R95757
Sample ID 19030656-001AMS
SampType: MS
TestCode:
Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 95757
Client ID: Batch=
Batch ID: R95757
TestNo:
SW9014
Analysis Date: 3114/2019
SegNo: 2000212
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Quai
Sample lD 19030656-001AMSD
SampType: MSD
TestCode:
Cyanide,Rea Units: mg/Kg
Prep Date:
RurtiNo: 95757
Client ID: Batch=
Batch ID: R95757
TestNo:
SW9014
Analysis Date: 3/1412019
SegNo: 2000213
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qcal
Cyanide, Reactive
9.57 0.490 10.00 0.2400 93.3 81.6 122 9.608 0.354 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDIimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 27 of 31
mmiso Summit Environmental Technologies, Inc. QC SUMMARY M�y �i OR 1
3310 Win St.
E1�91FlliC?NhtEfdTALtl=+Cw�io[[�it_, '!r Cuyahoga Falls, Ohio44223
WO#: 190302$1
ATWx YtJCa) Lab&Y.1l6t'i0•: TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httn://www.settek.com 20-Mar-19
Client: Synagro
Project: Farmville WWTP BatchID: R95759
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4710 25.0 4800 0 98.1 85 115
Sulfide, Reactive 4320 25.0 4800 0 90.0 80 120 W
Sulfide, Reactive 4530 25.0 4800 0 94.4 80 120 4320 4.75 30 W
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range 1-1 Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
R RPD outside accepted recovery limits R - Reporting Detection Limit
Page 28 of 31
ffl
summly
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY 1�`��LVJARY REPORT
�C
Ei4"litCtifiJklEi1TAL�cC%EliC1[ G�If, 'i� <^_
Cuyahoga Falls, Ohio 44223
WO#: 19030281
Ana?yUc2l LaL-cYalarieg TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htt,2://www.settek.com
20-Mar-19
Client:
Synagro
Project:
Fannville WWTP
BatchID: R95759
Sample ID 19030656-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mglKg
Prep Date:
RunNo: 95759
Client ID: Batch=
Batch ID: R95759
TestNo: SW9034
Analysis Date: 3114/2019
SegNo: 2000586
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quamitation limits
ND Not Detected
PL Permit Limit
E Value above quamitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
Rl, Reporting Detection Limit
Original
Page 29 of 31
OUIJIMMI: "Vironmental Technologies, Inc,'
3310 Win St=t Analysis west of Custody
Summit Environukantal Technologies, Inc.. useuse
'Cuyahoga Falls, Ohio 44223 Tel: 330.253.8211 Fax-- 330.253.4499 For
Company Name (Please Print) I Prniper A—. SLrf Nu
Ttci — �
Client
1pled by t Check... 7
i:
Q
itt. tot I (.X,. 1�
ChmkAnbj
Z4S+Wu;CmMMIELF —1
�p�Rd of Sample Origin -J1
(),L FOR COMPLIANCYj-!NOkCLlo'jRc&TIONkEo[);J(U�D YES No
TFptREPju ri,QSTATE q DW ()Nr_y, YtS NOe&o
It J,!:� I'leAst PTLI,idc PW�. STUMP
Rush Requesw By: Must be appmVed
— — —D-ft by lab mmW�>� IUN� My
Page 30 of 31
SUMMIT Summit Environmental Technologies, Inc.
3310 Win St_
i4WllttlN�dlhlT11L1fECi1C1Ql,tif;;-n� ,. Cuyahoga Falls, 0hio44223 Sample Log -in Check List
AnaiyNcai Laborasories TEL: (330) 253-8211 FAX: (330) 253-4489
Websile: httn://www.settek.can
Client Name:
Logged by:
SYN-NC-27028
Christopher Livengood
Completed By: Jesseca E. Westfall
Reviewed By: Jennifer Woolf
Chain of Custody_
1. Is Chain of Custody complete?
Z. How was the sample delivered?
Log In
3. Coolers are present?
Work Order Number: 19030281
3/6/2019 10:20:00 AM
3/6/2019 4:01:02 PM
3/7/2019 1:33:03 PM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5, Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0' C to 6.0'C
7, Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
g. Are samples (except VOA and ONG) properly preserved?
1(). Was preservative added to bottles?
1 1 . Is the headspace in the VOA v'rais less than 1 /4 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14, Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable}
Yes❑
UPS
Yes ❑�
Yes R/1
Yes ❑
Signed By:
Yes 0
Yes 0
Yes 0
Yes 0
Yes
Yes ❑
Yes ❑
Yes ❑
Yes IV]
Yes d❑
Yes❑
Yes ❑�
RcptNo: 1
No ❑ Not Present ❑
No ❑ NA ❑
No ❑
No ❑ Not Present 0
No ❑ NA ❑
No ❑ NA ❑
No ❑
No L_]
No ❑
No IVA
No ❑
No W
No ❑
No ❑
No ❑
No ❑
NA ❑
No VOA Vials d❑
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA �/❑
Person Notified: --- _...._......_._.._ Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C Condition Seal Intact Seal_N__o_
11 5.3 Good Not Present
Seal Date
Page 31 of 31
SECTION 5
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
Town of Farmville
WQ Permit Number: WQ0008778
WWTP Name: Town of Farmville WWTP, Digester Basin NPDES Number: NCO029572
Monitoring Period: From 01/01/19 To 12/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 31C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B.
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
<22800
<28300
<78700
CFU/g
0
Annually
Grab
SM9221E
CFU
1000 MPN per gram of
MPN/g
total solids (dreight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliformn
Vector Attraction Reduction (40 CFR 503.3.3/15A NCAC 02T.1107) _ Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt, 6
Option/Mt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives
were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
David Hodgkins, Town Manager 71R GA S
Prep arer rye d Tit] type print) Land Applier Name and Title (if applicable) (type or print)
7v/,`J 41,110W `�/ ,� :) .14 - -1-V
Signature of Preparer* 6 Date Signature of Land Applier (if applicable.) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Cameron Testing Services, Inc. Laboratory Report
Synagro
Farmvilie WWTP
Sample Information
A r-
a M. Boyd 03/04/19 ;
Analyses and Results
NC DENR #654
NO PHHS 037790
US EPA#NC01918
190386
Yes
M. Sims 03/04/19
190385 -1
sludge Gr Fec. Coliform-S <24700
CFUIg
24700 03/04/19 SB 9222D - MF
-2
<78700
CFUrg
78700
-3
<23400
CFU/g
23400
_4
<25400
CFU,g
25400
-5
<23800
cFUrg
23800
-6
<22800
CFU/g
22800
-7
<23300
CFU/g
23300
Geomean <28300
190385 -1
sludge Gr TS (%) 4.05%
%
0.01 03/07/19 SB 2540 G -TS
-2
1.27%
%
0.01
-3
4.28%
%s
o.o1
-4
3.94%
%
o.o1
-5
4.21 %
%
0.01
-6
4.39%
%
ao1
-7
4.30%
%
aw
Report
Review
Project Manager i7afe
219 S. Steele Str.
Sanford NC 27330 919-208-4240
chris@camerontesting. corn
1
219 S_ Steele Str.
Sanford, NC 27330
Cameron Testing Services, Inc. Clain of Custody
Phone: 919-208-424D
NC WW/GW Celt. 9654 NC PHHS Cert # 37799 US EPA
NC0191 a Page
of
Company: _I
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CTS lab use
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Contact:
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(Phone:
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Address (City, l--- ` -
Fax:
Ice (YIN}
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-
Permit iN
Project V)L�� W �h��t�
I
Rush (YIN) Due:
Collected: Name: VjAn��
Signature:
Sample Information
Number of bnttlec
ta.r n^u►..�.�
.
' m E
Salrrple ��
`�
ru _:�
Ln C13m
Preservatives: (U)npreserved, H(cy,
CTS Lab
F- C�
W r
o O O
H2(S)04, H(N)03, (NaFhiosulfate, Na(0)H, ID
r—'
`o >
Other (X), Indicate
Cv a
I
�1
�
I I
-
I
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—
II
.Relinquished.
/ -Received:
Dateffime
Rush work will require prior approval. Additional charges will apply
Project:
Client:
Sampled
By M. Boyd
Elate 07/02/19
Type Grab
191220-08
Final Results
Farmville
Synagro
Received
By F. Steen
Date 07/02/19
Matrix Sludae
30D Report Sheet
30 Day Benchtop Test
(EPA 6251R-921013, Appendix D)
Due I Ref. Methods
Date 08/08/19 1 Requested Analysis
Start (< 2%) 1.76%
67.3%
07/05/19
2.77%
76.2%
7111/19
1.77%
66.9%
7118/19
1.73%
67.1 %
7/25119
END 1.52%
65.0%
08/06/19
FVSR (VK)
Project Mgr
Notes: Sample started at TS s 2%.
FVSR (VK)
55;3%:.
FVSR (VK)
2.0%,
FVSR (VK)
1.2%..:.
FVSR (VK)
9 8%
Pass, < 15%
Page 1
CTS Proj.
Regulatory
Std. Meth. 19t' ed.
2540 G - TS
2540 G - VS
tl)g -�9
Date:
2nford, Steele Cameron Testing Services, Inc.
Sanford, NC 27330 Chain of Custody
Phone: 919-208-4240 NC WW/GW Cert. #694 NC PHHS Cert # 37799 US EPA NCO1918 Page of
Company: Synagro Entail: m CTS lab use only
Contact: -
l
I f ti }(/f
hone:
336-909-8627
Address (city, 1284 Boger Rd.
G,
Fax:
State, Zip)
IMocksville, NC 27028
1(Notes:
Project -
i
Collected. Name: 'i, k
[[ 1
g Si n ature: ;✓ /
Sample information
Number of bottles
Sample ID
N
(V a -0'
I` 1= cc
.X
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}
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c�
0 4
.'
Q
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v
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io ✓ .
Relli}�� iAinuished: Received--
Jam` z't"
Sample Temp — ---- -
(C) - - Lab tq
Ice (YIN)
Permit (YIN)
Rush (YIN] Due:
Requested Analysis
Preservatives: (U)npreserved, H(c)I, CTS Lab
H2(S)04, H(N)03, (Na)Thiosuifate, Na(D)H, ID
Other (X), Indicate
�03 .
Rush work will require prior approval. Additional charges will apply
SECTION 6
Agricultural Lime Application Log
2019
Farmvllle, NC
SECTION 7
NCDA&CS Agronomic Division Phone: (919) 733-2655
Website: www.ncagr.gov/agronomi/
Report No.
FY20-SL008271
�, + ti'�fi 4i
Predictive
Client:
Josio Baker
Morgan Fertilizer Co
Advisor:
PO Box649
Farmville, NC27828
Soil Re ort
-{ p
Mehlich-3
Extraction
Sampled County: Pitt
Links to Helpful Information
Client ID:
Advisor ID:
Sampled: 1010212019 Received: 1010812019 completed: 10/15/2019
Farm: Stump Jerry Flanagan
Sample ID: 1
Recommendations:
Lime
Nutrients (Iblacre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M
0.5
180-220 0
20
0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
2.44 1.08 13.4 86 1.9 5.8
382 108
62 19
59
83
67
1323
1323
589 0.1
1
Sample ID: 2
Recommendations:
Lime
Nutrients (Iblacre)
More
Crop
(tonslacre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M
0.6
180-220 0
150
0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100
cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS -I NO3-N
2.08 1.11 11.3 83 1.9 5.7
323 33
65 17
33
55
50
1353
1353
513 0.1
1
Sample ID: 3
Recommendations;
Lime
Nutrients (Iblacre)
More
Crop
(tonslacre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M
0.8
180-220 0
170
0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS -I NO3-N
2.01 1.14 7.5 76 1.8 5.5
75 27
55 19
31
36
39
218
218
160 0.1
1
North. Carolina
I
x
11,1,]Cil JILIN-F1r=titsr�.r�w..r
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxier. Commissioner of A.miculture
NCDA&CS Agronomic Division Phone: (919) 733-2655
Website: www.neagr.gov/agronomi/
Report No.
FY20-SL008271
Josie Balser
Page 2 of 3
Sample ID: 4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda haylpast., M
1.8
180-220 0
170
0
0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units -WIV in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
2.29 1.01 7.7
64 2.8 4.9
88 27
45 17
34
30
35
444
444
223 0.1
1
Sample ID: 5
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda haylpast., M
1.9
180-220 0
110
0
0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WIV in glcm3; CEC and Na in meg1100
cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-AI1
Mn-AI2
Zn-I
Zn-Al
Cu-1 Na ESP
SS-1 NO3-N
2.22 0.99 10.8
70 3.2 5.1
130 50
54 14
41
63
55
826
826
173 0.1
1
Sample ID: 6
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda haylpast., M
0.5
180-220 0
180
0
0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
2.52 1.04 12.8
86 1.8 5.8
146 25
61 24
44
43
43
507
507
282 0.1
1
Sample ID: 7
Recommendations:
Lime
Nutrients (Iblacre)
More
Crop
(tonslacre)
N P205
K20
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M
0.0
180-220 0
40
0
0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mgldrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-I K-I
Ca% Mg%
S-I
Mn-I
Mn-All
Mn-AI2
Zn-1
Zn-A1
Cu-1 Na ESP
SS-1 NO3-N
2.29 1.07 15.5
89 1.7 6.1
481 87
68 18
58
69
57
1588
1588
456 0.1
1
NCDA&CS Agronomic division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil
Report No. FY20-SL008271
Josie Baker
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
B
boron
ton/acre or lb11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-1
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
Mn-All
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient Levels. If $, pH$, $pH, C or Z
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib11000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htrr nd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Ferfilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
Zn-AI
zinc availability index
The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pHj describe the soil and its degree of acidity. The
Zn-I
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www. ncagr.govlac7ronomiluyrst.htm