HomeMy WebLinkAboutWQ0004609_Residual Annual Report 2019_20200302Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0004609
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer Kendall.Williams@ncdenr.gov
Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
Ifinnerty@synagro.com
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0004609
Applicant\Permittee * SYNAGRO
Facility Name * Wayne Farms, LLC-Dobson
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for Wayne Farms, LLC-Dodson
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
WAYNE FARMS NC 2019 Annual Report FINAL.pdf 15.3MB
Upload only 1 RDF document. NL@iple documents must be combined into one RDF file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/27/2020
435 Wilhgms Court, Suite 100
Baltimore, 11ID 21220
www synagro. corn
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0004609
Dear NCDEQ:
SYNAGR00341
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the Wayne Farms, L.L.C.-Dobson, NC.
If you have any questions or need additional information, please do not hesitate to contact Paul
Nordin at (336) 356-8151 or Alex Fox at (336) 703-8681.
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Paul Nordin, Wayne Farms, L.L.C.-Dobson
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD
WAYNE FARMS, L.L.C. , NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0004609
2019 ANNUAL REPORT
Wayne Farms, L.L.C. - Dobson, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form & Annual Operations Summary
2. Annual Residual Sampling Summary Forms and SAR Calculation
Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Control of Possible Nuisance Conditions
6. Soil pH & Lime Application Records
7. Soil Analyses
SECTION 1
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00004609 County Surry Year 2019
Facility Name (as shown on permit) Wayne Farms NPDES No. NCO006548
Land Application Operator Synagro Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A— Residuals Application Summary:
Total number of application fields in the permit: 32
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 131.32
Total number of acres utilized for land application during the year: 110.30
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results.are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
it. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13, All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Cory Earlv, Complex Manaaer
Pern ee Name an Title (type or print) Signature of Permittee Date
(/_� 02 20 ZO O
Signat ofp-repareri Date Signatur of plie Date
(if different from Permittee) (if different from P ittee and Prep er)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
WAYNE FARMS, L.L.C., NC
WAYNE FARMS LLC, NC FOOD PROCESSING LIQUID
DRY METRIC
MONTHIYEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
April 2019
638,600.00 G
62.05
D
56.27
May 2019
409,200.00 G
39,75
D
36.06
December 2019
303,800.00 G
29.52
D
26.79
YEARLY TOTAL
1,351,600.00 G
131.32
D
119.12
1 /30/2020
SECTION 2
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0004609
Facility Name: WAYNE FARMS, L.L.C., NC
NPDES# : NCO006548
or WQ# (residual only)
WWTP Name: WAYNE FARMS L.L.C.
Residuals Analysis Data
Product Type
FPLIQ
Date Sampled (grab) or 04/03/19
Date Composited
Percent Solids
2.33
PARAMETERS (mg/kg dry weight)
Arsenic
<5
Cadmium
<1
Mercury
<0 . 0155
Chromium
43.7
Copper
431
Lead
7.26
Molybdenum
5.79
Nickel
27.8
Selenium
<5
Zinc
953
Total Phosphorus
10600
TKN
63900
Ammonia -Nitrogen
8700
Nitrate and Nitrite
<4 . 85
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date Ot/Za/zaz-o
(SIGNATURE Of PREP
DENR FORM RSSF (5/2003) _ Printed: Friday- February 7, 2020 at 18:18:12 for: 2061 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number WQ0004609
Facility Name WAYNE FARMS, L.L.C., NC
NPDES# NC0006548
or WQ# (residual only)
WWTP Name WAYNE FARMS L.L.C.
Residual Analysis Data
Product Type
FPLIQ
Date Sampled
04/03/19
Date Composited
Percent Soilds
2.33
PARAMETERS (mglkg dry weight)'
Aluminium
12300
Calcium
73900
Magnesium
18000
pH
11.10
Potasium
2690
Sodium
4130
PAN
20915
SAR
0.5378
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting fal information, in luding the possibility of fines and imprisonment for knowing violations."
x Date 0Z- 20 2Dz 0
(SIGNATURE OF REPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/7/2020 6:19:50 PM
Waypoint,o
ANALYTICAL
4/15/2019
Synagro Central LLCI Wayne Farm
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-095-0204
Project Description: Wayne Farms
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P.,<< 'A. 6&�
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6
(2)
Waypoe
�� 7621 Whitepine Road, Richmond, VA 23237
w Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-095-0204
Client Project Description: Wayne Farms
Lab No Client Sample ID Matrix (Date Collected Date Received Method Lab ID
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
65765
Wayne
Farms
Solids
04/03/2019
14:00
04/05/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
SM-4500-NFi3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-2540G
WTN
Page 2 of 6
Report Number: 19-095-0204
Account Number: 46499
Send To: Synagro Central LLCI Wayne Farm
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 65765
Sample Id : Wayne Farms
(D
Waypoint
ANALYTICAL
Project: Wayne Farms
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 904-271-6446
www.waypointanalytical.com
Date Sampled: 4/3/2019 14:00:00
Date Received: 04/05/2019 00:00
Date Reported: 0411512019
Total Solids
2.33
23300
100.0
CJR
04/1012019 14:21
Moisture *
97.70
100.0
CJR
04/10/2019 14:21
Total Kjeldahl Nitrogen
6.39
63900
250
CLP
04/11/2019 13:30
Phosphorus
1.06
10600
50.0
BKN
04/10/2019 23:47
Potassium
0.27
2690
50.0
BKN
04/10/2019 23:47
Sulfur
1.12
11200
50.0
BKN
04/11/201919:31
Calcium
7.39
73900
250
BKN
04/10/2019 23:47
Magnesium
1.80
18000
50.0
BKN
04/1012019 23:47
Sodium
0.41
4130
250
BKN
04/10/2019 23:47
Iron
12300
50.0
KKM
04/1012019 23:47
Aluminum
12300
50.0
BKN
04/10/2019 23:47
Manganese
519
5.00
BKN
04110/2019 23:47
Copper
431
2.50
BKN
04/10/2019 23A7
Zinc
953
12.5
BKN
04/10/2019 23:47
Ammonia Nitrogen
0.87
8700
100
JPJ
04/12/2019 12:00
Organic N
5.52
55200
250
04/11/2019 13:30
Nitrate+Nitrite-N
<4.85
4.85
ZBD
04/081201915:53
SM-254OG
S M-2540 G
SM-4500-NH3C-TKN
601 OD
6010D
6010D
6010D
6010D
6010D
6010D
6010D
601 OD
601 OD
601 OD
SM-4500-NH3C
CALCULATION
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time
porie.
of
6ewr
Our reports and letters are for the exclusive and confidential use of our clients; and may not be reproduced in whole or part, nor may any reference be made
to the work. the results; or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page 3 of 6
Report Number: 19-095-0204
Account Number: 46499
Send To: Synagro Central LLC/ Wayne Farm
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 65765
Sample Id : Wayne Farms
•
vp
Wa of nt
ANALYTICAL
Project: Wayne Farms
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 4/3/2019 14:00:00
Date Received: 0410512019 00:00
Date Reported: 04/15/2019
Cadmium
<1.00
1.00
BKN
04/10/2019 23:47
6010D
Chromium
43.7
2.50
BKN
04110/2019 23:47
6010D
Nickel
27.8
2.50
BKN
04/10/2019 23:47
6010D
Lead
7.26
3.00
BKN
04/10/2019 23:47
6010D
Arsenic
<5.00
5.00
BKN
04/1012019 23:47
6010D
Mercury
<0.0155
0.0155
TJS
04/101201914:37
SW-7471B
Selenium
<5.00
5,00
BKN
04110/2019 23:47
601OD
pH *
11.1
JSL
04/11/2019 07:09
9045D
Molybdenum
5.79
2.50
BKN
04/10/2019 23:47
601 OD
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding Time
/
Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made Pauric MCGroary
to the work; the resets, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization Agronomist
Page 4 of 6
(2)
Ways®' ■ ■t 7621 1 ain 80 -7 Read, Richmond, 27 -6446
Main St34-743-94U1 °Fax 804-2i1-6446
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46499
Customer Name: Synagro Central LLCI Wayne Farm
Report Number: 19-095-0204
Shipping Method
0 Fed Ex 0 US Postal C) Lab
• UPS 0 Client 0 Courier
0 Other:
Thermometer [D:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping contain erlcooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
(-) No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 - compliance criteria met
0 Yes
0 No
0 NIA
High concentration container (48 hr) j Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments: 7_-
0 Yes 0 No
Signature: Brandi Watson Date & Time: 104/05/2019 13:19:55
Page 5 of 6
SAMPLING LOG # if ZJ A & L
7621
Ri hn
CUSTOMER: SYNAGR® ® 804/7
PROJECT MANAGER: r-k S Jti'-* -
Phone: �331a -763 Eya 1
A & L CUSTOMER SAMPLING SAMPLE
LAB # SAMPLE I.D. ,LOCATION TYPE
Relinquished by Sampier:
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIOINS:
1� For
uv. > -
monitoring purposes.
Date Time
4 1-z'.cc)
s ime
Time
Il!l11111I1111111Illllllllllll>1111111IIIlll1l11>�1111111I1111!l146499
Svnaaro Central LLC/ Wavrte Farm 9 ®� ������fl�
wameFarms 13:19:25 RECORD
f arrest urcac utc N, u� -._._ _ampling procedures
were used during the collection of these samples.
SAMPLER
# OP SAMPLING METHOD METHOD
CONTAINERS �DATE TIME PRESERVED SHIPPED
j
1 A '7 . ! ,, 1 1,
Recieved by:
rR7i-
:1ecieved
by:
P O#:
REMARKS:
SAMPLE ANALYSIS REQUEST
I.C. SLI SL2 NH,-N NOa N grganic Cd Cr Ni Pb As H CaCO Volatile
-;�TN 9 Se PH epuiv3 Solids Mo Cl NO2 N
w�7
P �PO � ;00 'P�o A000poJ'/'/ boo
SL1: Total Solids (Moisture), Total }fleldahl [Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Suffur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zfnc
rU
0
co
m
m
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2061-01-FPLIQ-NC WAYNE FARMS LLC, NC FOOD PROCESSING 4/3/2019 41112019-12/3112019 0.5378
LIQUID
Na mgll = (Na mg/kg x % Solids) _ 100 = (4130 x 2,3300) + 100 = 96.229
Ca mgll = (Ca mg/kg x % Solids) = 100 = (73900 x 2.3300) . 100 = 1721.87
Mg mg/l = (mg mglkg x % Solids) + 100 = (18000 x 2.3300) _ 100 = 419A
Na meq = Na mgll + Molec.Wgt.Na = 96.229 _ 23 w 4.18387
Ca meq = Ca mgll + Molec.Wgt.Ca = 1721.87 + 20 = 86.0935
Mg meq = Mg mgll _ Molec.Wgt.Mg = 419.4 -�- 12 = 34.95
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.18387 SgrRoot[0.5(86.0935+34.95)] = 0.537802
Printed: 2/5/2020
Page 1 10:37
SECTION 3
FACILITY NAME: WAYNE FARMS, L.L.C., NC
OWNER: JOANN DUNBAR
SITE #: NC SU 00013 FIELD : SU 00013 0010
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT #: WQ0004609 ANNUAL DRY TONS APPLIED: 46.39
OPERATOR: WALTER JOHNSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 42.90 ACRES PERMITTED: 42.90
Page
Lune Applied •*
Date
LbsAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons. (WT) (specify)
%
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
4/30/19
68,200.00 (G)
1589-7441
2.33
0.154
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900.p
8,700.00 p
4.85 p
209I5
SOYBEANS
Apr-19
68,200.00 (G)
1,589.744
5/1/19
130,200.00 (G)
3034.965
2.33
0.295
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900.p
8,700.00 p
4.85 p
20915 1
SOYBEANS
5/2/19
86,800.00 (G)
2023.310
2.33
0.197
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
I SOYBEANS
5/3/19
124,000.00 (G)
2890.443
2.33
0.291
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
I SOYBEANS
5/8/19
12,400.00 (G)
289.044
2.33
0.028
WFFPL
MOIST
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
I SOYBEANS
5/9119
55,800.00 (G).
1300.699
2.33
0.126
WFFPL
MOIST
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700,00 p
4.85 p
20915
SOYBEANS
May-19
409,200.00 (G)
9,538A61
i orat Uationsi,Ac:
Total Wet Tons/Ac:
ii,i2u.lr
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
45
0.011
0.002
0.095
0.932
0.016
<001
0.013
0.060
0.011
2.061
22.92
Cumulative lbs/acre
0.030
0.015
0277
2.246
0.054
0.003
0.064
0.I69
0.043
5.879
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
152
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
26T9
15.0
375.0
89.0
2500.0
WFFPL = WAYNE FARMS LLC, NC FOOD PROCESSING LIQUID
I Qu, � )_LZ 11tv
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonmentfor knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p =ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, E U - Injection SUR1N -incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Wayne Farms, L.L.C., NC Total Dry Tons Applied (Annual):
WQ0004609 Cation Exchange Capacity (non 503 only):
Walter Johnson Owner: Walter Johnson Predominant Soil Series:
42.9 Acres Permitted:
42.9
Site #: NC SU 00013 Field #:
46.39
Fairview
SILT 00013 0010
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1
4/3/19
2
3
4
5
6
7
8
9
10
11
12
% Solids
2.33
Arsenic
5
Cadmium
I
Copper
431
Chromium
43.7
Lead
7.26
Mercury
0.0155
Molyb-
denum
5.79
Nickel
27.8
Selenium
5
Zinc
953
Total
Phos-
horus
10600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 11
L2J
3 J
L4J
L5J
6
L7J
L8J
L9j
Loi
11 J
] 2
DTIAc.I
App.
Event
1.08
Arsenic
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.002
0.000
0.000 1
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.002
Copper
0932
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.932
Chromium
0.094
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.094
Lead
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
denum
Nickel
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.060
Selenium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Zinc
2.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.060
Total
Phos-
22.917
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
22.917
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonme for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)
FACILITY NAME : WAYNE FARMS, L.L.C., NC
OWNER: JAMES WALTER JOHNSON
SITE #: NC SU 00013 FIELD# : SU 00013 0012
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUM31ARY FORM
PREDOMINANT SOIL SERIES: WOOLWINE/FAIRVIEW/WESTFIELD
PERMIT#: WQ0004609 ANNUAL DRY TONS APPLIED: 43.98
OPERATOR: DONALD JOE & JUDY MOORS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 32.90 ACRES PERMITTED: 32.90
Page
Lime Applied ***
Date
Lb,/A,
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
MONTH
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/3119
31,000.00 (G)
942.249
2.33
0,092
WFFPL
DRY
0-<112"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
CORN
4/4/19
105,400.00 (G)
3203.647
2.33
0.311
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4,85 p
20915
CORN
4/24/19
130,200.00 (G)
3957.447
2.33
0.385
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
CORN
4/25/19
136,400.00 (G)
4145.897
2.33
0.403
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
CORN
4/30/19
49,600.00 (G)
1507.599
2.33
0.146
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
CORN
Apr-19
452,600.00 (G)
13,756.839
Total Gallons/Ac:
Total Wet Tons/Ac:
13,756.84
a v-i,. iu.r au. U.VV
-
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
56
0.013
0.003
0.117
1.152
0.0I9
<.00I
0.015
0.074
0.013
2.548 28.34
Cumulative lbs/acre
0.013
0.003
0.117
1.152
0.019
<.001
0.015
0.074
0.013
2.548
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
157
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
WFFPL = WAYNE FARMS LLC, NC FOOD PROCESSING LIQUID
x
(SIGNATURE OF LAND APPLIER) DATE
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % =percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN -incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Wayne Farms, L.L.C., NC Total Dry Tons Applied (Annual): 4398
Permit #: WQ0004609 Cation Exchange Capacity (non 503 only):
Operator: Donald & Judy Moore Owner: Donald & Judy Moore Predominant Soil Series: RoolwinelFairviev
Acres Used: 32.9 Acres Permitted: 329 Site #: NC STU 00013 Field #: SU 00013 0012
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 11
413119
L2J
3 J
L4J
L5J6
7
8]
L9J
LOJ
11 J
12
% Solids
2.33
Arsenic
5
Cadmium
1
Copper
431
Chromium
43.7
Lead
7.26
Mercury
0.0155
Molyb-
denum
5.79
Nickel
27.8
Selenium
5
Zinc
953
Total
Phos-
horus
10600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
App.
Event
1.34
Arsenic
0.013
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
1.152
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
1.152
Chromium
0.117
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.117
Lead
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
denum
Nickel
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Selenium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.01.3
Zinc
2.548
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.548
Total
Phos-
28.344
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
28.344
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonmi t for knowing violations".
Z�
Signature of Land Applier Date
DENR FORM MFL.SF (12/2006)
FACILITY NAME: WAYNE FARMS, L.L.C., NC
OWNER: JAMES WALTER JOHNSON
SITE #: NC SU 00013 FIELD# : SU 00013 0013
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WOOLWINE/FAIRViEWMFSTFIELD
PERMIT #: WQ0004609 ANNUAL DRY TONS APPLIED: 1 L45
OPERATOR: DONALD JOE & JUDY MOORE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40
Page: I
Lime Applied ***
Date LWAc
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TI{N
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/2/19
74,400.00 (G)
11625.000
2.33
1.1301
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
FESCUE HAY
413/19
43,400.00 (G)
6781.250
2.33
0.659
WFFPL
DRY
0-<1/2"
SUR
0.5
0.30
63,900.13
8,700.00 p
4,85 p
20915
FESCUE HAY
Apr-19
I17,800.00 (G)
18,406.250
1
Total Gallons/Ac: 18,406.25
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0 00
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbslacre
75
0.018
0.004
0.156
1.542
0.026
<.001
0-021
0.099
0.018
3.409
37.91
Cumulative lbs/acre
0.018
0.0.04
0.156
1.542
0.026
<.001
0.021
0.099
0.018
3.409
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
178
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
WFFPL — WAYNE FARMS LLC, NC FOOD PROCESSING LIQUID
LX 71-Z 71J
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg&g ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
e Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SUMAIARY FORM*
Attach this form to the corresponding Field Loading Summary Form to he submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Wayne Farms, L.L.C., NC Total Dry Tons Applied (Annual): 11.45
WQ0004609 Cation Exchange Capacity (non 503 only):
Donald & Judy Moore Owner: Donald & Judy Moore
Predominant Soil Series: Noolwine/Fairvlev
6.4 Acres Permitted: 6.4 Site H. NC SU 00013 Field #:
SU 00013 0013
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
4/3/19
L2 jL_j3
A
L5 j6
7
8
9 j10
f 1
12
% Solids
2.33
Arsenic
5
Cadmium
I
Copper
431
Chromiu
43.7
Lead
7.26
Mercury
0.0155
Molyb-
denum
5.79
Nickel
27.8
Selenium
5
Zinc
953
Total
Phos-
horus
10600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5]
L6J
7
8
9
10
11
12
DT/Ac./
o
App
rt
Event
1.79
14
Arsenic 1
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.018
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
1.542
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.542
Chromium
0.156
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.156
Lead
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
denum
Nickel
0.099
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.099
Selenium
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Zinc
3.410
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.410
Total
Phos-
37.927
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
37.927
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonnpelpt for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)
FACILITY NAME: WAYNE FARMS, L.L.C., NC
OWNER: TIMOTHY DAVIS
SITE #: NC SU 00020 FIELD# : SU 00.020 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT #: WQ0004609 ANNUAL DRY TONS APPLIED: 25.30
OPERATOR: DAVIS FAMILY PROPERTIES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.50 ACRES PERMITTED; 20.50
Page
Lime Applied ***
Date
Lbs1Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond_
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tili-
zation
Minex
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
12/20/19
24,800.00 (G)
1209.756
2.33
0.118
WFFPL
MOIST
0- 1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
FESCUE HAY
12/21/19
49,600.00 (Cr)
2419.512
2.33
0235
WFFPL
MOIST
0 <1/2"
SUR
0.5
0,30
63,900. p
8,700,00 p
4.85 p
20915
FESCUE HAY
12/26/19
86,800.00 (G)
4234.146
2.33
0.411
WFFPL
DRY
110-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
FESCUE HAY
12/27/19
74,400.00 (0)
3629.268
2.33
0.353
WFFPL
DRY
"0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
FESCUE HAY
12/28/19
24,800.00 (G)
1209.756
2.33
0.118
WFFPL
DRY
"0-<1/2"
SUR
0.5
0.3.0
63,900. p
8,700.00 p
4.85 p
20915
FESCUE HAY
Dec-19
260,400.00 (G)
12,702,438
t Oral kimlonslillc: 12, I VL.44
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo.
Ni
Se
Zn
P
PAN
Annuallbs/acre
52
0.012
0.002
0.108
1.064
0.018
<.00I
0,014
0.069
0.012
2.352
26.16
Cumulative lbs/acre
0.012
0.002
0.108
1.064
0.018
<.001
0.014
0.069
0.012
2.352
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
194
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
2679
15.0
375.0
89.0
2500.0
WFFPL = WAYNE FARMS LLC, NC FOOD PROCESSING LIQUID
XL '�__ z//7->
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection./Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURiN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Wayne Farms, L.L.C., NC Total Dry Tons Applied (Annual): 25.30
WQ0004609 Cation Exchange Capacity (non 503 only):
Davis Family Properties Owner: Davis Family Properties Predominant Soil Series:
20.5 Acres Permitted: 20.5 Site #: NC SU 00020 Field #:
Fairview
SU 00020 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % SoIids use Raw Percent #):
Sample or
Com-
posite
Date
1 11
4/3119
2
3
4
5
6
7
8
9
10
11
12
% Solids
2.33
Arsenic
5
Cadmium
1
Copper
431
Chrolmiun
43.7
Lead
7.26
Mercury
0.0155
Molyb-
denum
5.79
Nickel
27.8
Selenium
5
Zinc
953
Total
Phos-
horus
10600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 11
L2]3
L4-1
5
6-1
7
8-1
91
00111
I
12
DT/Ac./
App.
Event
1.24
Arsenic
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
1.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.065
Chromium
0.108
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.108
Lead
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0M00
Molyb-
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
denum
Nickel
0.069
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Selenium
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
.Zinc
2.354
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 2.354
Total
Phos-
26.182
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
26.182
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonyment for knowing violations".
atr, �)�_ Z/z r z
Signature of Land Applier Date
DE;NR FORM MFLSF (12/2006)
FACILITY NAME: WAYNE FARMS, L.L.C., NC
OWNER: 13EN WATSON
SITE #: NC SU 00022 FIELD# : SU 00022 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: WQ0004609 ANNUAL DRY TONS APPLIED: 4.22
OPERATOR: BEN WATSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.60 ACRES PERMITTED: 7.60
Page
Lime Applied ***
Date
Lbs Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
"�O
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip,
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crap
Total
Per Acre.
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
12/27/19
18,600.00 (G)
2447.368
2.33
0.238
WFFPL
DRY
"0-<1/2"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
20915
FESCUE PASTURE
12/28/19
24,800.00 (G)
3263.158
2.33
0.317
WFFPL
DRY
"0-<112"
SUR
0.5
0.30
63,900. p
8,700.00 p
4.85 p
21111
FESCUE PASTURE
Dec-19
1 43,400.00 (0)
5,710.526
1
1 otal UallonsIAc: 5,71U.53
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
23
0.006
0.001
0.048
0.478
0.008
<.001
0.006
0.031
0.006
1.058 11.76
Cumulativelbs/acre
0.006
0.001
0.048
0.478
0.008
<.001
0.006
0.031
0.006
1-058
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
151
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
WFFPL = WAYNE FARMS LLC, NC FOOD PROCESSING LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported orNot Required % = percent p — ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit 4;
Operator:
Acres Used:
Wayne Farms, L.L.C., NC Total Dry Tons Applied (Annual):
WQ0004609 Cation Exchange Capacity (non 503 only):
Ben Watson Owner: Ben Watson Predominant Soil Series:
4.22
Clifford
7.6 Acres Permitted: T6 Site #: NC SU 00022 Field #: SU 00022 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
4/3119
L2]3
4
5
B
7
8
9
10
11
12
% Solids
2.33
Arsenic
5
Cadmium
1
Copper
431
Chromium
43.7
Lead
7.26
Mercury
0.0155
Molyb-
denumn
5.79
Nickel
1 27.8
Selenium
5
Zinc
953
Total
Phos-
horus
10600
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
I 1 I
L2]3
4
5
6
7
8
9
10
11
12
DT/Ac./
0
App.
Event
0.56
Arsenic
0.006
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.006
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
0.478
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.478
Chromium
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
Lead
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.008
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
denurn
Nickel
0.031
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.031
Selenium 1
0.006
0.000
0.000
0.000
1 0.000
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
0.006
Zinc
1.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.058
Total
Phos-
11.766
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.766
horus
"T certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
f am aware that there are significant penalties for submitting false information, including the possibility of fines and
impriso ent for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (1212006)
SECTION 4
rrsummint
ENVIIIONPAT NTAL TECiiN0I..[. rlrS, INC
AnityNcal Labaratorlos
August 21, 2019
Nate Roth
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Wayne Farms
Dear Nate Roth:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX- (330) 253-4489
Website: hQ://www.settek.com
Order No.: 19071834
Summit Environmental Technologies, Inc. received 1 sample(s) on 7/26/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, Califomia 07256CA, Colorado, Connecticut PH-O IOS, Delaware, Florida NELAC E87688, Georgia E87688, Idaho 01100923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hainpshirc 2996, New jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
01-1009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 36
Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
EN:VHION?Ar�NTAL TEC3ih1O1_OmFS, INC Cuyahoga Falls, Ohio 44223
Arta(y(leal taborararl&s TEL: (330) 253-8211 FIX.- (330) 253-4489
Website: hQ://www.settek.conz
CLIENT: Synagro
Project: Wayne Fauns
WorkOrder Narrative:
Case Narrative
WO#: 19071834
Date: 8/21/2019
19071934: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditationslcertifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19071834-OOIA TCLP-SVOC_8270E: Surrogate recovery was outside of the laboratory established
acceptance criteria for: p-Terphenyl-dl4. All other surrogates exhibited recoveries within the
acceptance criteria.
Original
Page 2 of 36
Saanunit Environmental Technologies, In Quali%ens and Acronyms
SUMMINt 331O Win 5
i N��If�C7N��I�NTAL Tr ClGNOi.[ G3�$, �Att' Cuyahoga Falls, Ohio 442� WO#: 19071834
Anafyflcal faboyarorlas TEL: (330) 253-8211 FAY.- (330) 253-445
Date: 8/21I2019
Wehside; lattb://ivww.seitek,co
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
BIMB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+),
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low () or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
,S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCI,
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 36
U MM I Ot Summit Environmental Technologies, Inc. Workorder
3310 Win St.
ENti{IfIOtJMENTAL ttCHNOLOM17 k, INC, Cuyahoga Falls, Ohio 44223 Sample Summary
Analytical Laboretot"las TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 19071834
Wehsite: httn:1Avww.settek.com 21-Aug-19
CLIENT: Synagro
Project: Wayne Farms
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
19071834-001 Wayne Farms 7/25/2019 9:00:00 AM 7/26/2019 9:50:00 AM Sludge
Page 4 of 36
MMIT
Summit Environmental Technologies, Inc. DATES REPORT
SU3310 Win St.
EMkOITIONMENTALTCi1NOLC:1--i�!;,Nr' Cuyahoga Falls, Ohio44223
WO#: 19071834
,��alyflaal i��rarrries TEL: (330) 253-8211 FAX.- (330) 253-44$9
Website: hLW:11www.settekcom 21-Aug-19
Client:
Project:
Synagro
Wayne Farms
Sample ID
Client Sample ID
Collection Date Matrix 'Pest Name Leaebate Date
Prep Date
Analysis Date
19071834-OOIA
Wayne Farms
7/25/2019 9:00:00 AM Sludge Flashpoint Determination (1010)
7/31/2019 12.01:41 PM
pH (SW9045D)
7/29/2019 3.21:02 PM
Reactive Cyanide (90I4/7.3.3.2)-Solid
7/31/2019 12:26:00 PM
Reactive Sulfide (9034)17.3.4.2
7/31/2019 12:26:00 PM
TCLP Herbicides Analysis (SW1311/8
8/7/2019 12:15:00 PM
8/13/20I9 5:34:00 PM
solid
TCLP Mercury Analysis (SW1311/7478/1/2019 5:00:00 PM
8/2/2019 2:40:00 PM
8/2/2019 5:29:00 PM
TCLP Metals Analysis (5W1311/6010 8/l/2019 5:00:00 PM
8/5/2019 9:30:00 AM
8/5/2019 6:03:12 PM
TCLP Pesticides Analysis (SWI311/8(8/l/2019 5:00:00 PM
8/6/2019 11:10:00 AM
8/6/2019 4:13:00 PM
TCLP Semi-Volatiles Analysis 8/l/2019 5:00:00 PM
8/5/2019 1:00:00 PM
8/6/2019 6:13:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
8/5/2019 2:00.00 PM
TCLP Volatiles Analysis
8/1/2019 5:00:00 PM
8/5/2019 2:00:00 PM
Original
Page 5 of 36
summilr
summit Environmental Technologies, Lac.
3310 t Pin St.
Analytical Report
EPf4iIRONNIENTALIrECHNOLOCIr-S,'W-7
Cu),ahogaFalls, Ohio 44223
(base report)
4rratytfcaf Laborratmes
TEL: (330) 253-8211 FAX: (330) 253-4489
WO#: 19071834
R'ehsite: 1Wp:11www.sette1r.00M
Date Reported: 8/21/2019
CLIENT:
Tag Number:
Synagro
Matrix:
SLUDGE
Collection Date:
7/25/2019 9:00:00 AM
Lab ID:
19071834-OOIA
Project:
Wayne Farms
Client Sample
ID Wayne Farms
Analyses
Result
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
TCLP Barlum(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Seienium(Se)
ND
TCLP Silver(Ag)
ND
FLASHPOINT DETERMINATION (1010)
Flashpoint (140°F) ND
SW7470A
SW7470A Analyst: DNS
0.00500
mg/L 1
8/2/2019 5:29:00 PM
SW6010D
SW301OA Analyst: EAM
0.500
mg/L 1
8/5/2019 6:03:12 PM
5.00
mg/L 1
8/5/2019 6:03:12 PM
0.100
mglL 1
8/5/2019 6:03:12 PM
0.200
mg/L 1
8/5/2019 6:03:12 PM
0.500
mg/L 1
8/5/2019 6:03:12 PM
0.0500
mg/L 1
8/5/2019 6:03:12 PM
0,500
mg/L 1
8/5/2019 6:03:12 PM
SW1010 Analyst: TAH
° F 1 7/31/2019 12: 01:41 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichlorobenzene
ND
0.200
mg/L
2 8/6/2019 6:13:00 PM
2,4,5-Trichlorophenol
ND
0.600
mg/L
2 8/6/2019 6:13:00 PM
2,4,6-Trichlorophenol
ND
0.500
mg/L
2 8/6/2019 6:13i00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2 8/6/2019 6:13:00 PM
Cresols, Total
ND
10.0
mglL
2 8/6/2019 6:13:00 PM
Hexachloro-1,3-butadiene
ND
0.0400
mg/L
2 8/6/2019 6:13:00 PM
Hexachl o ro benzene
ND
0.100
mg/L
2 8/6/2019 6:13:00 PM
Hexachloroethane
ND
0.200
mg/L
2 8/6/2019 6:13:00 PM
Nitrobenzene
ND
0.200
mg/L
2 8/6/2019 6:13:00 PM
Pentachlorophenol
ND
0.500
mg/L
2 8/6/2019 6:13:00 PM
Pyridine
ND
0.500
mg/L
2 8/6/2019 6:13:00 PM
Surr: 2-Fluorophenol
20.7
10 - 109
%Rec
2 8/6/2019 6il3:00 PM
Surr: Pherol-d6
26,9
10 - 109
%Rec
2 8/6/2019 6:13:00 PM
Surr: Nitrobenzene-d5
24.2
19 - 120
%Rec
2 8/6/2019 6:13:00 PM
Qualifiers: B Analyte detected in the associated
Method Blank
E Value above quantitation
range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound
Limit,
N Tentatively identified compounds
ND Not Detected
P Second column
confirmation exceeds
PL Permit Limit
R RPD outside accepted
recovery limits Original
RL Reporting Detection Limit
U Samples with CaleVal < MDL
Page 6 of 36
Setraimit Envi7•onraaental Technologies, Inc. Analytical Report
SUMMIT 3310 Tlrirr St.
ENVIRONNItNTAL frcb uol i1.�1t-S, 'I' " Cuyahoga Falls, Ohio 44223 (base report)
ArrR$yf;c,?1 Laboralarfor TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 19071834
Website: hQ://wmv.setteJc.con: Date Reported: 8/21/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 7/25/2019 9:00:00 AM
Lab ID: 19071834-001A
Project: Wayne Farms
Client Sample ID Wayne Farms
Analyses Result
RL
Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW3510C
Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
Surr: 2,4,6-Tribromophenol 27.0
10 - 120
%Rec
2
8/6/2019 6:13:00 PM
Surr: 2-Fluorobiphenyl 24.7
22 - 117
%Rec
2
8/6/2019 6:13:00 PM
Surr: p-Terphenyl-d 14 25.9
34 - 116
S
%Rec
2
8/6/2019 6:13:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C
Analyst: MES
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total ND
0.0250
mglL
10
8/6/2019 4:13:00 PM
Toxaphene ND
0.0500
mg/L
10
8/6/2019 4:13:00 PM
Endrin ND
0.00500
mg/L
10
8/6/2019 4:13:00 PM
gamma-BHC ND
0.00500
mg/L
10
8/6/2019 4:13:00 PM
Heptachlor ND
0.00500
mg/L
10
8/6/2019 4:13:00 PM
Heptachlor epoxide ND
0,00500
d
mg/L
10
8/6/2019 4:13:00 PM
Methoxychlor ND
0.00500
d
mg/L
10
8/6/2019 4:13:00 PM
Surr: TCMX 47.1
10 - 119
%Rec
10
8/6/2019 4:13:00 PM
Surr: DCB 50.1
10 - 119
%Rec
10
8/6/2019 4:13:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW131118151)-SOLID
2,4-D
2, 4, 5-TP
Surr: DCAA
SW8151A SW8151A Analyst: MES
ND 0.0100 d mg/L 1 8/13/2019 5:34:00 PM
ND 0,00500 mglL 1 8/13/2019 5:34:00 PM
99.9 20 - 140 %Rec 1 8/13/2019 5:34:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260 Analyst: CTB
TCLP VOLATILES
ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L 50 81512019 2:00:00 PM
1,2-Dichloroethane
ND
0.250
mglL 50 8/5/2019 2:00:00 PM
MEK
ND
5.00
mglL 50 8/5/2019 2:00:00 PM
Benzene
ND
0.250
mg/L 50 8/5/2019 2:0&00 PM
Carbon tetrachloride ND
0.250
mg/L 50 8/5/2019 2:00:00 PM
Chlorobenzene
ND
2.50
mg/L 50 8/5/2019 2:00:00 PM
Chloroform
ND
0.250
mglL 50 8/5/2019 2:00:00 PM
Tetrachloroethene
ND
0.250
mg1L 50 8/5/2019 2:00:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND
Not Detected
P Second column confirmation exceeds
PI,
Permit Limit
R RPD outside accepted recovery limits Original
RL
Reporting Detection Limit
t] Samples with CalcVal < MDL
Page 7 of 36
summill
Summit Environmental Technologies,hie.
3310 Chin St.
Analytical Report
1=1�tWRON1�9ENTAL tr-CH164 M t1€;t�S, ,N"
Cuyahoga Falls, Ohio 44223
(base report)
Ai7alyftal Labarataries
Tl L: (330) 253-8211 FAX: (330) 253-4489
WO#: 19071834
Website: http:/hviv)v.settelf.cona
Date Reported: 8/21/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
7/25/2019 9:00:00 AM
Lab ID:
19071834-001A
Project:
Wayne Farms
Client Sample ID Wayne Farms
Analyses
Result RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
Analyst: CTB
TCLP VOLATILES ANALYSIS
Trichloroethene
ND
0.250
mglL
50
8/5/2019 2:00:00 PM
Vinyl chloride
ND
0.100
mg1L
50
8/5/2019 2:00:00 PM
Surr: 4-Bromofluorobenzere
93.9
70 - 130
%Rec
50
8/5/2019 2:00:00 PM
Surr: Di brom ofluorom ethane
97.3
70 - 130
%Rec
50
8/5/2019 2:00:00 PM
Surr: TolueneA8
97.0
70 - 130
%Rec
50
8/5/2019 2:00:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive
ND
0.490
mg/Kg
1
7/31/2019 12:26:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9045D
Analyst: VVK
PH (SW9045D)
pH
6.7
s.u.@20.00
1
7/29/2019 3:21:02 PM
RC[ -SOLID -WI IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive
ND
25.0
mg/Kg
1
7/31/2019 12:26:00 PM
Qualifiers: B
Analytc detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Original
RL
Reporting Detection Limit
U
Samples with CaleVal < MDL
Page 8 of 36
Summit Environmental Technologies, Inc. Accreditation Program
summist 3310 Win St. Anal te5 Report
�H�rI1tL�1W�11 h1TALT CIiIJt]I C�{ilF$, INC Cuyahoga Falls, Ohio 44223 y p
Arr fyNcal Laboratories TEL: (330) 253-8211 FAX., (330) 253-4489 WO#: 19071834
Website: http:11www.settek.co)n 21-Aug-19
Client: Synagro State: NW
Project: Wayne Farms Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
19071834-001A Sludge
Flaslipoint Determination (1010)
Flashpoint (140°F)
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
SIudge
Reactive Sulfide (9034)/7.3,4,2
Sulfide, Reactive
11
Sludge
TCLP Herbicides Analysis (SW 131119151)-solid
2,4,54P
A
Sludge
TCLP Herbicides Analysis (SW 131119151)-solid
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW131118081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychior
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
SIudge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
SIudge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
SIudge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Setni-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
'TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Sena-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
Key -
-
NC WW SCM A Accredited
NC WW SCM U Unavailable
Version #2
Page 9 of 36
Summit Environmental Technologies, Inc. Accreditation Program
SUMM111 331.0 Win St. Anal tes Report
ENVIRONPAtiNTAL TECI I6tiOQ C)faiFS,�fNC Cuyahoga Falls, Ohio 44223 � p
Analytical Laboratories TEL: (330) 253-8211 FAX., (330) 253--4489 WO#: 19071834
Website: http:/hvww.settek.co2;7 21-Aug-19
Client: Synagro
Project: Wayne Farms
State: NW
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19071834-OOIA Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chlorofonn
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC_W W_SCM
A
Key
Accredited NC WW SCM U Unavailable
Version 42
Page 10 of 36
MIT
'Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUM3310 Win St.
1 1;4'Eit41d�1t 41i� L 3�GiNC)1_Lb Sly, ;F�? Cuyahoga Falls, Ohio 44223
ArZarl Val Labaratr nos TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 19071834
Wehsite: http://www.settek.com 21 Aug-19
Client: Synagro
Project: Wayne Farms BatchID: 38679
Sample ID MB-38679
SampType: MBLK
TestCode: TCLP-voc-M Units: %Rec
Prep Date: 8/112019
RunNo: 101545
client ID: PBS
Batch ID: 38679
TestNo: SW8260 SW1311M
Analysis Date: 8/212019
SegNo: 2253693
�nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr.4-Bromofluorobenzene
509
500.0
102
70
130
Surr: Dibromofluoromethane
500
500.0
100
70
130
Surr: Toluene-d8
498
500.0
99.6
70
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to detern-tine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 11 of 36
H Holding times for preparation or anah
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
ff1summi Summit Environmental Technologies, Inc. QC SUMMARY REPORT
n3310 Win St.
ENVI lZOA M 5 NTAL 1rr—cmH(3 w;; iE5„ Cuyahoga Falls, Ohio 44223
An$lyrtlal Labot'laones TEL: (330) 253-82JI FAX, (330) 253-4489 WO#: 19471834
Website: hLp://www.settelc.com 21Aug 19
Client: Synagro
Project: Wayne Fauns BatchID: 38692
Sample ID MB-38692
SampType: MBLK
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 8/2/2019
RunNo: 101551
Client ID: PBS
Batch ID: 38692
TestNo:
SW7470A SW7470A
Analysis Date: 8/2/2019
SegNo: 2253785
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
rCLP Mercury
ND 0.00200
Sample ID LCS-38692
SampType: LCS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 812/2019
RunNo: 101551
Client ID: LCSS
Batch ID: 38692
TestNo:
SW7470A SW7470A
Analysis Date: 8/2/2019
SegNo: 2253786
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
rCLP Mercury
0.00403 0.00200 0.00400
0 101 80 120
Sample ID MB2-38692
SampType: MBLK
TestCode:
HG,-TCLP(74 Units: PPM.
Prep Date: 8/212019
RunNo: 101551
Client 1D: PBS
Batch ID: 38692
TestNo:
SW7470A SW7470A
Analysis Date: 8/2/2019
SegNo: 2253787
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID 19071918-002AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 8/212019
RunNo: 101551
Client ID: Batch=
Batch ID: 38692
TestNo: SW7470A SW7470A
Analysis Date: 8/212019
SegNe: 2254325
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ret Val
%RPD RPDLimit Qual
fCLP Mercury
0.00253 0.00200 0.00400 0 64.5 75 125
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
S
Original
Page 12 of 36
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
mnsummill
>'brl;tcuMFaT�Lci�or t EIS, Cuyahoga Falls, Ohio 44223
413atytical Laboratoroes TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 19t171834
Website: http:llwww.settek-.com 2I Aug-19
CIient: Synagro
Project: Wayne Farms
BatchID: 38692
Sample 1D 19071918-002AMS
SampType: MS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 8/2/2019
RunNo: 101551
Client ID: Batch=
Batch ID: 38692
TestNo:
SW7470A SW7470A
Analysis Date: 812/2019
SegNo: 2254325
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 19071918-002AMSD
SampType: MSD
TestCode:
HG TCLP(74 Units: PPM
Prep Date: 81212019
RunNo: 101551
Client 1D: BatchQC
Batch ID: 38692
TestNo:
SW7470A SW7470A
Analysis Date: 812/2019
SegNo: 2254328
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00214 0.00200 0.00400 0 53.5 75 125 0.00258 18.6 20 S
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column conformation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 13 of 36
prSUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVITtWIMENTk! tlt�c�[ cs ��. , InC
Cuyahoga Falls, Ohio 44223
Vi70#: 19071834
A.nilytlt<a11�boratarlec
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: htto:11www.settek.com
21 Aug-19
CIient:
Synagro
Project:
Wayne Farms
BatchID: 38702
Sample ID MB-38702
SampType: MBLK
TestCode: Mti-TCLP-7(6 Units: mglL
Prep Date: 8/512019
RunNo: 101580
-Iient ID: PBS
Batch ID: 38702
TestNo: SW6010D SW3010A
Analysis Date: 815/2019
SegNo: 2257435
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLlmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
C.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-38702
SampType: LCS
TestCode:
Mtl-TCLP-7(6 Units: mg1L
Prep Date: 815/2019
RunNo: 101580
Client ID: LCSS
Batch ID: 38702
TestNo:
SW6010D SW3010A
Analysis Date: 815/2019
SegNo: 2257436
A,nalyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Quai
TCLP Arsenic(As)
1.89
0.500
2.000
0
94.7
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
101
80
120
TCLP Cadmium(Cd)
1.77
0.100
2.000
0
88.5
80
120
TCLP Chromium(Cr)
2.01
0.200
2.000
0
100
80
120
TCLP Lead(Pb)
2.02
0.500
2.000
0
101
80
120
TCLP Selenium(Se)
1.89
0.0500
2.000
0
94.3
80
120
TCLP Silver(Ag)
2.08
0.500
2.000
0
104
80
120
Qualifiers
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 14 of 36
H Idolding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
MMI
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUA3310 Win St.
ENVITZO N MENTAL %—z-C9iEVt7wdGIrS, w Cuyahoga Falls, Ohio 44223
WO#: 14071834
Anatytival LaLtcraivrloLe TEL: (330) 253-8211 FAX. (330) 253-4489
Website: ht(L:Ilwww.settek.com 21-Aug-19
Client: Synagro
Project: Wayne Farms BatebID: 38702
Sample ID 19072115-004AMS
SampType: MS
TestCode:
Mtl-TCLP-7(6 Units: mg1L
Prep Date: 8/512019
RunNo: 101580
Client ID: BatchQC
Batch ID: 38702
TestNo:
SW6010D SW3010A
Analysis Date: 8/512019
SegNo: 2257448
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Vai
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.32
0.50C
2.000
0
116
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.2739
102
70
130
TCLP Cadmium(Cd)
2.03
0.100
2.000
0
102
70
130
TCLP Chromium(Cr)
2.10
0.200
2.000
0.0009437
105
70
130
TCLP Lead(Pb)
2.16
0.500
2.000
0
108
70
130
TCLP Selenium(Se)
2.43
0.0500
2.000
0
122
70
130
TCLP Silver(Ag)
2.32
0.500
2.000
0
116
70
130
Sample ID 19072115-004AMSD
SampType: MSD
TestCode:
Mtl-TCLP-7(6 Units: mg1L
Prep Date: 8/5/2019
RunNo: 101580
Client ID: BatchQC
Batch ID: 38702
TestNo:
SW6010D SW3010A
Analysis Date: 8/512019
SegNo: 2257449
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.28
0.500
2.000
0
114
70
130
2.315
1.47
20
TCLP Barium(Ba)
ND
5.00
2.000
0.2739
99.2
70
130
0
0
20
TCLP Cadmium(Cd)
1.98
0.100
2.000
0
99.0
70
130
2.032
2.63
20
TCLP Chromium(Cr)
2.04
0.200
2.000
0.0009437
102
70
130
2.096
2.53
20
TCLP Lead(Pb)
2.13
0.500
2.000
0
106
70
130
2.159
1.51
20
TCLP Selenium (Se)
2.40
0.0500
2.000
0
120
70
130
2.430
1.36
20
TCLP SiIver(Ag)
2.26
0.500
2.000
0
113
70
130
2.317
2.45
20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted rece
Original
Page 15 of 36
MSUMMIT
SummitEnvit'onmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
?cE4ttlR010diEWAL T—rGH 0E.()GIrt5, INC
Cuyahoga Falls, Ohio 44223
WO#: 19071834
Arfa lyfdel taboratonas
TEL: (330) 253-821.1 FAX- (330) 253-4489
Website: htto:llwww.settek.com
21-Aug-19
Client:
Synagro
Project:
Wayne Farms
BatchID: 38719
Sample ID mb-38719
SampType: MBLK
TestCode:
svoc-bna tcl Units: mg1L
Prep Date: 81512019
RunNo: 101650
Client ID: PBS
Batch ID: 38719
TestNo:
SW8270 SW3510C
Analysis Date: 816/2019
SegNo: 2258308
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit QuaI
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichlorophenol
ND
0.100
2,4-Dinitrotoluene
ND
0.0200
o-Cresol
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0.100
Pyridine
ND
0.100
Surr: 2-FIuorophenol
0.395
Surr: Phenol-d6
0.430
Surr: Nitrobenzene-d5
0.400
Surr: 2,4,6-Tribromophenol
0.456
Surr: 2-Pluorobiphenyl
0.362
Surr: p-Terphenyl-d14
0.518
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
1.000
39.5
10
109
1.000
43.0
10
109
1.000
40.0
19
120
1.000
45.6
10
120
1.000
36.2
22
117
1.000
51.8
34
116
E Value above quantitation range
M Manual hltegration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or mall
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 16 of 36
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
fflsummly 3310 Win St.
EP4VITCf]AM.ENTAL�CliNOLL-+GirS, 1FtC Cuyahoga Falls, Ohio 44223
A:naiy0=1 Laboralones TEL: (330) 253-8211 FAX..- (330) 253-4489 WO#: 19071834
Website: htto:llwww.settek.com 21-Aug-19
Client: Synagro
Project: Wayne Farms
BatchID: 38719
Sample ID Ics-38719
SampType: LCS
TestCode: svoc-bna tcl Units: mg1L
Prep Date: 815/2019
RunNo: 101650
Client ID: LCSS
Batch ID: 38719
TestNo: SW8270 SW3510C
Analysis Date: 8/6/2019
SegNo: 2258309
Analyte
Result
PQL SPK value SPK Ref Val
%RLC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.423
0.0400
0.8000
0
52.9
36.4
130
2,4,5-Trichlorophenol
0.523
0.100
0.8000
0
65.3
31.7
132
2,4,6-Trichlorophenol
0.500
0.100
0.8000
0
62.5
31.1
133
2,4-Dinitrotoluene
0.532
0.0200
0.8000
0
66.5
43.3
130
o--Cresol
0.532
0.100
0.8000
0
66.5
32.9
130
Cresols, Total
ND
2.00
1.600
0
66.7
31.7
130
Hexachloro-1,3-butadiene
0.421
0,00800
0.8000
0
52.6
31.4
130
Hexachlorobenzene
0.435
0.0200
0.8000
0
54.4
43.1
130
Hexachloroethane
0.423
0.0400
0.8000
0
52.9
36.5
130
Nitrobenzene
0.541
0.0400
0.8000
0
67.7
39.5
130
Pentachlorophenol
0.528
0.100
0.8000
0
66.0
34
130
Pyridine
0.349
0.100
0.8000
0
43.6
10
130
Sum 2-Fluorophenol
0.556
1.000
55.6
17.1
130
Surr: Phenol-d6
0.640
1.000
64.0
10
130
Sum Nitrobenzene-d5
0.616
1.000
61.6
32.6
130
Surr:2,4,6-Tribromophenol
0.632
1.000
63.2
4.43
130
Surr:2-Fluorobiphenyl
0.544
1.000
54.4
41.8
130
Surr: p-Terphenyl-d14
0.572
1.000
57.2
36.4
130
Qualifiers
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anah
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted recc
Original
Page 17 of 36
M111
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffl SUM3310 Win St.
ENIVInON?-IENTAL TECHt Ot.aGlr S, KC. Cuyahoga Falls, Ohio 44223
ArPMyOCal Lab6ratbr`aes TEL: (330) 253-82.11 FAX: (330) 253-4489 WO#: 19071534
Wehsite: htto:llwww.setteic.corn 21Aug-l9
CIient: Synagro
Project: Wayne Farms
BatchID: 38719
Sample 1D 19072156-001ams
SampType: MS
TestCode: svoc-bna_tcl Units: mg/L
Prep Date: 8/5/2019
RunNo: 101650
Client ID: BatchQC
Batch ID: 38719
TestNo: SW8270 SW3510C
Analysis Date: 8/612019
SegNo: 2261123
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.546
0.0800
0.8000
0
68.2
33.8
126
2,4,5-Trichlorophenol
0.643
0.200
0.8000
0
80.4
28.7
144
2,4,6-Trichlorophenol
0.598
0.200
0.8000
0
74.7
12.8
153
2,4-Dinitrotoluene
0.658
0.0400
0.8000
0
82.2
20.4
155
o-Cresol
0.681
0.200
0.8000
0
85.2
10
148
Cresols, Total
ND
4.00
1.600
0
86.4
10
148
Hexachloro-1,3-butadiene
0.528
0.0160
0.8000
0
66.1
29
126
Hexachlorobenzene
0.500
0.0400
0.8000
0
62.4
33.7
134
Hexachloroethane
0.560
0.0800
0.8000
0
70.0
32.8
132
Nitrobenzene
0.696
0.0800
0.8000
0
87.0
20
158
Pentachlorophenol
0.693
0.200
0.8000
0
86.7
10
176
Pyridine
0,430
0,200
0.8000
0
53.7
10
130
Surr. 2-Fluorophenol
0.741
1.000
74.1
3,39
130
Surr: Phenol-d6
0.816
1.000
81.6
5
130
Surr: Nitrobenzene-d5
0.791
1.000
79.1
14.5
154
Surr: 2,4, 6-Tribromophenol
0.752
1.000
75.2
19.5
130
Sum 2-Fluorobiphenyl
0,665
1.000
66.5
34.4
130
Surr: p-Terphenyl-d14
0.751
1.000
75.1
8.86
156
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quamitation limits
ND Not Detected
R RPD outside accepted recovery Iimits
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 18 of 36
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
frSummint 3310 Win St.
Et,'Vl LONPoE!wTAL-rCttNCLD--I q ;a,,. Cuyahoga Falls. Ohio 44223
Anaiy0ca11_abcratjorJeLe TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 19071834
Website: http.-Ilwww.settek.com 21-Aug-19
Client: Synagxo
Project: Wayne Fanns
SatchID: 38719
Sample ID 19072156-001amsd
SampType: MSD
TestCode: svoc-bna_tcl Units: mg/L
Prep Date: 8/5/2019
RunNo: 101650
Client ID: BatchQC
Batch ID: 38719
TestNo: SW8270 SW3510C
Analysis Date: 31612019
SegNo: 2261124
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.547
0.0800
0.8000
0
68A
33.8
126
0.5460
0.220
30
2,4,5-Trichlorophenol
0.686
0.200
0.8000
0
35.7
28.7
144
0.6432
6,38
30
2,4,6-Trichlorophenol
0.643
0.200
0.8000
0
80.4
12.8
153
0.5976
7.29
30
2,4-Dinitrotoluene
0.648
0.0400
0.8000
0
81.0
20.4
155
0.6580
1.59
30
o-Cresol
0.684
0.200
0.8000
0
85.6
10
148
0.6812
0.469
30
Cresols, Total
N❑
4.00
1.600
0
86.2
10
148
0
0
30
Hexachloro-1,3-butadiene
0.559
0.0160
0.8000
0
69.8
29
126
0.5284
5.59
30
Hexachlorobenzene
0.536
0.0400
0.8000
0
67.0
33.7
134
0.4996
7.10
30
Hexachloroethane
0,532
0,0800
0.8000
0
66.5
32.8
132
0.5600
5.20
30
Nitrobenzene
0.712
0.0800
0.8000
0
89.0
20
158
0.6956
2.27
30
Pentachlorophenol
0.765
0.200
0.8000
0
95.7
10
176
0.6932
9.87
30
Pyridine
0.542
0.200
0.8000
0
67.8
10
130
0.4296
23.2
30
Surr:2-Fluorophenol
0.740
1.000
74.0
3.39
130
0
Surr: Phenol-d6
0.830
1.000
83.0
10
130
0
Surr: Nitrobenzene-d5
0.776
1.000
77.6
14.5
154
0
Surr: 2,4,6-Tribromophenol
0.745
1X00
74.5
19.5
130
0
Surr:2-Fluorobiphenyl
0.690
1.000
69.0
34.4
130
0
Surr: p-Terphenyl-d14
0.756
1.000
75.6
8.86
156
0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal~
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 19 of 36
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
33I0 YPin St.
, iNf Cuyahoga Falls, Ohio 44223ffISUMMIMIL
An$Vhml boralnnot TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 1907t$34
C.a
Website: htW://www..vettek.com 21-Aug-I9
Client: Synagro
Project: Wayne Farms
BatchID: 38740
Sample ID 19080252-001ams
SampType: MS
TestCode: TCLP-SVOC- Units: mglL
Prep Date: 8/6/2019
RunNo: 101668
Client ID: SatchQC
Batch ID: 38740
TestNo: SW8081 SW3510C
Analysis Date: 8/6/2019
SegNo: 2260684
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00544
0.00500
0.0100
0
54.4
10
224
gamma-BHC
ND
0.00500
0.0100
0
45.1
10
192
Heptachlor
ND
0.00500
0.0100
0
0
10
197 S
Heptachlor epoxide
ND
0.00500
0.0100
0
42.8
10
208
Methoxychlor
ND
0.005e0
0.0100
0
32.1
10
251
Sum TCMX
7.01
20.00
35.1
10
157
Sum DCB
9.22
20.00
46.1
10
194
Sample ID 19080252-001amsd
SampType: MSD
TestCode: TCLP-SVOC- Units: mglL
Prep Date: 816/2019
RunNo: 101668
Client ID: Batch=
Batch [D: 38740
TestNo: SW8081 SW3510C
Analysis Date: 816/2019
SegNo: 2260686
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00741
0.00500
0.0100
0
74.1
10
224
0.00544
30.6
30 R
gamma-BHC
0.00618
0.00500
0.0100
0
61.8
10
192
0.00451
31.2
30 R
Heptachlor
ND
0.00500
0.0100
0
0
10
197
0
0
30 S
Heptachlor epoxide
0.00630
0.00500
0.0100
0
63.0
10
208
0.00428
38.0
30 R
Methoxychlor
ND
0.00500
0.0100
0
49.7
10
251
0
0
30 R
Surr. TCMX
9.48
20.00
47.4
10
157
0
Sum DCB
12.5
20.00
62.5
10
194
0
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H HoIding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 20 of 36
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMINIL 3310 Win St.
EN'0,10Nl1 ENTA.L C1h@�CFLES ',�_ ,. INC! Cuyahoga Falls, Ohio 44223
A-uaiy dca1 Laboratories TEL: (330) 253-8211 F.4X.- (330) 253-4489 WO#: 19071834
Website: httn://www.settek.corn 21 Aug-19
Client: Synagro
Project: Wayne Farms BatchID: 38740
Sample ID mb-38740
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg1L
Prep Date: 81612019
RunNo: 101668
Client ID: PBS
Batch ID: 38740
TestNo: SW8081 SW3510C
Analysis Date: 8/612019
SegNo: 2260868
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
d
gamma-BHC
ND
0.000500
d
Heptachlor
ND
0.000500
d
Heptachlor epoxide
ND
0.000500
d
Methoxychlor
ND
0.000500
d
Surr: TCMX
10.3
20.00 51.7 10 119
Surr: DCB
10.5
20.00 52.3 10 119
Sample ID lcs-38740
SampType: LCS
TestCode: TCLP-SVOC- Units: mg1L
Prep Date: 8/6/2019
RunNo: 101668
Client ID: LCSS
Batch ID: 38740
TestNo; SW8081 SW3510C
Analysis Date: 8/612019
SegNo: 2260869
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0,00395
0.000500
0.0100
0
39.5
20
216
gamma-BHC
0.00268
0.000500
0.0100
0
26.8
20
197
Heptachlor
0.00243
0.000500
0.0100
0
24.3
20
200
Heptachlor epoxide
0.00348
0.000500
0.0100
0
34.8
20
200
Methoxychlor
0.00330
0.000500
0.0100
0
33.0
20
227
Surr: TCMX
5.46
20.00
27.3
20
143
Surr: DCB
5.57
20.00
27.9
20
151
Qualifiers:
B Analyte detected in the associated Method Blank
J Analyte defected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 21 of 36
ffISUMM
IT
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EWP1014M ENTAL 171:h NOL[tGizfi, ;�tr_'
Cuyahoga Falls, Ohio 44223
.dnuiyClc2l l`abaraloYdes TEL:(330) 253-821I FAX:(330) 253-4489
WD#: 19071834
Website: htW:Ilwww,settek.com
21-Aug-19
Client:
Synagro
Project:
Wayne Farms
BatchID: 38780
Sample 1D MB-38780
SampType: MBLK
TestCode: tclp-svoc-her Units: mglL
Prep Date: 817/2019
RunNo: 101987
Client ID: PBS
Batch ID: 38780
TestNo: SW8151A SW8151A
Analysis Date: 8113/2019
SegNo: 2274709
Aralyte
Result
PQL SPK value SPK Ref Val
%REC LowUmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 0.0100 0 0
2,4,5-TP ND 0.00500 0 0
Surr: DCAA 409 500.0 81.8
20 140
Sample ID LCS-38780
SampType: LCS
TestCode: tclp-svoc-her Units: mg/1-
Prep Date: 817/2019
RunNo: 101987
Client ID: LCSS
Batch ID: 38780
TestNo: SW8151A SW8151A
Analysis Date: 8/1312019
SegNo: 2274710
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.419 0.0100
0.500
0 83.9
43.8
130
2,4,5-TP
0.355 0.00600
0.500
0 71.0
51.5
111
Surr: DCAA
472
500.0
94.3
34.2
150
Sample ID LCSD-38780
SampType: LCSD
TestCode: telp-svoc-her Units: mg1L
Prep Date: 8/7/2019
RunNo: 101987
Client ID: LCSS02
Batch ID: 38780
TestNo: SW8151A SW8151A
Analysis Date: 8/13/2019
SegNo: 2274711
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.477 0.0100
0.500
0 95.5
43.8
130 0.419
12.9 30
2,4,5-TP
0.344 0.00500
0.500
0 68.8
51.5
130 0.355
3.11 30
Surr: DCAA
463
500.0
92.6
34.2
150
0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted rece
Original
Page 22 of 36
'�` Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMs 3310 Win St.
EN'Vl i OtJMEMTAL 3EiCtiIr1r r-OGi-_�M1 Cuyahoga Falls, Ohio 44223
- A-Raiy6va l Labomfnrleg TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 19071834
Website: ht0:11wWw.setteLcom 21 Aug-19
Client: Synagro
Project: Wayne Farms
BatchID: R101322
Sample ID CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@a 21.2
Prep Date:
RunNo: 101322
Client ID: LCSS
Batch ID: R101322
TestNo: SW9045D
Analysis Date: 7/2912019
SegNo: 2241818
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
Qualifiers:
7.0
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
7.0 0 100 90
E VaIue above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 23 of 36
110
H Holding times For preparation or anal!
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
int Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffJ Summ3310 Win St.
ENVInONMENTAL TEECHN4-OCIIIESr INC. Cuyahoga Falls, Ohio 44223
WO#: 19071834
A!'+iTfy+t}ca)' Laboralnoes TEL: (330) 253-8211 F14X.- (330) 253-4489
Website: http://www.settek_com 21 Aug-19
Client: Synagro
Project: Wayne Farms BatchID: R101322
Sample ID LCS-R101322
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@20.6C
Prep Date:
RunNo: 101322
Client ID: LCSW
Batch ID: R101322
TestNo: SW9045D
Analysis Date: 7/29/2019
SegNc: 2241117
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0 0 99.9 90 110
Sample ID CHECK 7
SampType: LCS
TestCode: pH_011(9045 Units: s.u.@20.6C
Prep Date:
RunNo: 101322
Client ID: LCSW
Batch ID: R101322
TestNo: SW9045D
Analysis Date: 712912019
SegNo: 2241138
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
pH
7.0
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
7.0 0 100 90
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 24 of 36
110
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted rece
Original
SUMM111
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ES+ VITtO;Nh1E'NTIIL TFCH Oc LIGIt=_3, JW!
Cuyahoga Falls, Ohio 44223
WO#: 19071834
Anctytical Laboratnrlag
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http://Www.settek.com
21 Aug-19
Client:
Synagro
Project:
Wayne Farms
SatchID: R101322
Sample ID 19071527-001ADUP
SampType: DUP
TestCode:
pH_NPW{450 Units: s.u.@,20.6C
Prep Date:
RunNc: 101322
client ID: BatchQC
Batch ID: R101322
TestNo:
SW9045D
Analysis Date: 712912019
SegNo: 2241137
4nalyte
Result
PQL
SPK value SPK Ref Val %REC
Lowl-imit Highl imit RPD Ref Val
%RPD RPDLimit Qual
PH
Qualifiers:
11.9
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
11.9 0.5
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
5 H
Original
Page 25 of 36
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffISUMMIT 3310 Win St.
clN'blt?0t,lMENTALtr--CHNCLC9C.3rS,. �S,^ Cuyahoga Falls, Ohio44223
�lnsty0ca1 Labaralones TEL: (330) 253-8211 FLY- (330) 253-4489 WO#: 19071$34
Website: htW:Ilwww.settek.com 21 Aug-19
Client: Synagro
Project: Wayne Farms
BatchID: R101417
Sample ID LCS-R101417
SampType: LCS
TestCode: FlashPt_S(10 Units: OF
Prep Date:
RunNo: 101417
Client ID: LCSS
Batch ID: R101417
TestNo: SW1010
Analysis Date: 7/31/2019
SegNo: 2246281
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLtmit Qual
Flash point (140°F)
136
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
135.4 0 100 98 102
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal!
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted recc
Original
Page 26 of 36
fflsu
mmly
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
E2,y4MONPAENTALTECH gDUIei-CZ, NC Cuyahoga Falls, Ohio44223
Ar7Wytica) Labor'atores TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 19071834
Website: http://www.settek.com
21-.Aug-19
Client:
Synagro
Project:
Wayne Farms
BatchlD: R101441
Cyanide, Reactive ND 0.495
Cyanide, Reactive 9.25 0.490 10.00 0 92.5 85 110
Cyanide, Reactive 9.43 0.490 10.00 0 94.3 81.6 122
Cyanide, Reactive
9.41 C.490
10.00 0 94.1 81.6
122
9.427 0.208 5
Qualifiers: B
Analyte detected in the associated Method Blaak
E Value above quantitation range
H
Holding times for preparation or anal,
7
ND
Analyte detected below quantitation limits
Not Detected
M Manual Integration used to determine area response
P Second column confirmation exceeds
MC
PL
Value is below Minimum Compound
Permit Limit Original
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted rece
Page 27 of 36
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffl SUMMIEr 3310 Win St.
ERVItIONPdYEI.JTALT—rCH iC LQGI�E',%, NC. Cuyahoga Falls, Ohio44223
Anafyt�cal Latsoratorje55 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 19071834
Website: httt):Ilwww.settek.com 2I Aug-19
Client: Synagro
Project: Wayne Farms BatchID: R101441
Sample ID
19071654-001AMSD SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 101441
'-lient ID:
Batch= Batch ID: R101441
TestNo: SW9014
Analysis Date: 7/31/2019
SegNo: 2247614
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 28 of 36
ffISUMMIT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St,
ENti'lnOj4HlENTAL 1rCHNC3F,DG1E-7-1�, 'Nr Cuyahoga Falls, Ohio 44223
Aus(y+iraf Laboraloroes TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 19D71$34
Website: htto:llwww.settek.com .21 Aug-19
Client: Synagro
Project: Wayne Farms BatchlD: R101444
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4780 25.0 4800 0 99.6 85 115
Sulfide, Reactive 4670 25.0 4800 0 97.3 80 120
Sample ID
19071654-001AMSD SampType: MSD
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 101444
Client ID:
BatchQC Batch ID: R101444
TestNo:
SW9034
Analysis Date: 7/3112019
SegNo: 2247640
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4640
Qualifiers: B Analyte detectedni the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
25.0 4800 0 96.7 80
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 29 of 36
120 4670 0.644 30
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
ff
ISummitSumit
SUMM
Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVlR0NP, EMTAL TECH 0L0 Gir:;, INC
Cuyahoga Falls, Ohio 44223
A ljOyt1 1 LaborattWor TEL: (330) 253-821I FAX- (330) 253-4489
WO#: 19071834
Website: hhQ://1,vww.settekx2m
21-Auk 19
Client:
Synagro
Project:
Wayne Farms
EatchID: R101444
Sample ID 19071654-001AMSD
SampType: MSD
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 101444
client ID: BatchQC
Batch ID: R101444
TestNo:
SW9034
Analysis Date: 7/31/2019
SegNo: 2247640
gnalyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 30 of 36
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
fn
MSummitSumit
SUMIL
Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
Ef'SVInONMEWAL cC}BN0LGGi�_ , lIi?"
Cuyahoga Falls, Ohio 44223
WO#: 19071834
Ar+alyrt�=I Laboralorie5
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httt?://www.settek.com
21-Aug-19
Client:
Synagro
Project:
Wayne Farms
BatchID: R101627A
Sample ID LCS-101627
SampType: LCS
TestCode: VOC-MSTR_ Units: mg1L
Prep Date:
RunNo: 101627
Client ID: LCSW
Batch ID: R101627A
TestNo: SW8260
Analysis Date: 81512019
SegNo: 2284872
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0196
0.00500
0.0200
0
98.0
70
138
1,2-Dichloroethane
0.0194
0.00500
0.0200
0
96.9
70
130
MEK
0.0951
0.0250
0.100
0
95.1
70
130
Benzene
0.0190
0.00500
0.0200
0
95.1
70
132
Carbon tetrachloride
0.0187
0.00500
0.0200
0
93.3
70
130
Chlorobenzene
0.0197
0.00500
0.0200
0
98.4
10
255
Chloroform
0.0185
0.00500
0.0200
0
92.5
47.7
141
Tetrachloroethene
0.0193
0.00500
0.0200
0
96.7
10
130
Trichloroethene
0.0197
0.00500
0,0200
0
98.5
70
130
Vinyl chloride
0.0175
0.00200
0.0200
0
87.6
70
130
Surr: 4-Bromofluorobenzene
50.6
50.00
101
70
130
Surr: Dibromofluoromethane
49.7
50.00
99.4
70
130
Surr: Toluene-d8
50.0
50.00
99.9
70
130
Sample ID MBLK-101627
SampType: MBLK
TestCode: VOC-MSTR Units: mglL
Prep Date:
RunNo: 101627
Client ID: P13W
Batch ID: R101627A
TestNo: SW8260
Analysis Date: 8/5/2019
SegNo: 2284873
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Qualifiers: B
Analyte detected in the associated Method Blank
7
Analyte detected below quantitation limits
ND
Not Detected
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted recc
Original
Page 31 of 36
ffISUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
1 git'1liCltdlflFAiTAL trCtu1�4t3G+�.�,; :C
Cuyahoga Falls, Ohio 44223
WO#: 19071834
Ailaf,y6=1 � abcrafoneg TEL: (330) 253-8211 FAX.-(330) 253-4489
Website: httn:Ilwww.settek.ccom
21-Aug-19
Client:
Synagro
Project:
Wayne Farms
BatchlD: R101627A
Sample 1D MBLK-101627
SampType: MBLK
TestCode: VOC-MSTR Units: mglL
Prep Date:
RunNo: 101627
Slient ID: PBW
Batch ID: R101627A
TestNo: SW8260
Analysis Date: 815/2019
SegNo: 2284873
4nalyte
Result
PQL SPK value SPK Ref Val
%REG Lowl-Jmit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
TrichIoroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Sum 4-Bromofluorobenzene
47.4
Surr: Dibromofluoromethane
48.0
Sum Toluene-d8
49.2
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
50.00 94.8 70 130
50.00 96.1 70 130
50.00 98.3 70 130
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 32 of 36
H Holding times for preparation or anal
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
IEF `summit Environmental Technologies, .Inc. QC SUMMARY REPORT
frSUMM3310 Win St.
E�'tirlfiril��1�x3TAL9�i€�C[6iRS: 'h ^ Cuyahoga Falls, Ohio 44223
:4rra1JrC1raP Lataoralaraes TEL: (330) 253-8211 FAX., (330) 253-4489
WO#: 19071834
Website: http://Www.settek.com 21 Aug-19
Client: Synagro
Project: Wayne Farms SatchID: R101627A
Sample ID 19072156-00laMS
SampType: MS
TestCode:
telp-voc-mstr Units: mg1L
Prep Date:
RunNo: 101627
Client ID: BatchQC
Batch ID: R101627A
TestNo:
SW8260
Analysis Date: 8/512019
SegNo' 2272450
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroothene
0A84
0.0500
0.200
0
92.0
39.9
160
1,2-Dichloroethane
0.197
0.0500
0.200
0
98.4
42.5
157
MEK
ND
1.00
1.00
0
95.4
16.6
227
Benzene
0.182
0.0500
0.200
0
90.9
38.1
155
Carbon tetrachloride
0,153
0.0500
0.200
0
76.5
40.8
162
Chlorobenzene
ND
0.500
0.200
0
94.8
35.7
168
Chloroform
0.180
0.0500
0.200
0
90.2
18.3
199
Tetrachloroethene
0.162
0.0500
0.200
0
80.8
10
261
Trichloroethene
0.175
0.0500
0.200
0
87.6
23.8
175
Vinyl chloride
0.157
0.0200
0.200
0
78.6
10
165
Surr:4-Bromoflucmbenzene
512
500.0
102
84.6
130
Sum Dibromofluoromethane
494
500.0
98.8
71.4
127
Surr: Toluene-d8
508
500.0
102
74.6
127
Sample ID 19072156-00laMSD
SampType: MS❑
TestCode: tclp-voc-mstr Units: mg1L
Prep Date:
RunNo: 101627
Client ID: Batch=
Batch ID: R101627A
TestNo: SW8260
Analysis Date: 8/512019
SegNo: 2272451
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.182 0.0500
0.200 0 91.0
39.9
160
0.184 1.04
25
1,2-Dichloroethane
0.208 0.0500
0.200 0 104
42.5
157
0.197 5.54
25
MEK
ND 1.00
1.00 0 97.2
16.6
227
0 0
25
Benzene
0.187 0.0500
0,200 0 93.6
38.1
155
0.182 2.93
25
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quamitafron range
H
Holding times for preparation or anal,
J
.Analyte detected below quantitation limits
M Manual Integration used to determine area
response
MC
Value is below Minimum Compound
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted rece
Page 33 of 36
fn
I
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EN VIiZG1NMENTALT—rCaN0LC)G1!;S, iK!7
Cuyahoga Falls, Ohio 44223
WO#: 19071834
.4n&1ytica1' Lataoralcst°Ies� TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http:11www.settek.com
.2I Aug-19
Client:
Synagro
Project:
Wayne Farms
BatchID: R101627A
Sample ID 19072156-00laMSD
SampType: MSD
TestCode: tclp-roc-mstr Units: mglL
Prep Date:
RunNo: 101627
; lient ID: BatchQC
Batch ID: R101627A
TestNo: SW8260
Analysis Date: 815/2019
SegNo: 2272451
41alyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.148
0.0500
0,200
0
73.8
40.8
162
0.153
3,53
25
Chlorobenzene
ND
0.500
0.200
0
97.8
35.7
168
0
0
25
Chloroform
0.192
0.0500
0.200
0
96.1
18.3
199
0.180
6.28
25
Tetrachlorcethene
0.164
0.0500
0.200
0
82.0
10
261
0.162
1.54
25
Trichloroethene
0.180
0.0500
0.200
0
90.2
23.8
175
0.175
2.81
25
Vinyl chloride
0.150
0.0200
0.200
0
74.8
10
165
0.157
4.95
25
Surr:4-Bromofluorobenzene
486
500.0
97.1
84.6
130
0
25
Surr: Dibromofluoromethane
506
500.0
101
71.4
127
0
25
Surr: Toluene-d8
509
500.0
102
74.6
127
0
25
Qualifiers:
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation Iimits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 34 of 36
W
0
W
Summit Environmental Technologies, Inc.
33 10 '%Nin SLI eZL
Cuyahoga Falls. Ohio 44223 Tel_ 330.253.821 1 Fax: 330:25 3_448.
Analysis Request/Chaim of Custody
9 For Sumuiil l nviIoamental Tecfinologic
page -of- SA M�t
AnalytiParameters and Methods
�%C S, l't�i her! u;W M� -1
Rdin u6hedIn Date Twit Receiticd 1}ram I���x NoieslCunuuerrls:
State of Sample Origin,
r `x
Check if FOR C;OMPUANCE
iieecived in;lmb by.
Dalc Time Rush lieyu trd BY: `'1 f
C Dateby kvM� m toatgrr 126392
Whae and -id 1,, v� pages ,hLKIIJ aCCompam S,iw�,lr, U) ttW luhnrtu�r.' 'thy ."rnl rrt,itt� Ihr rtt:k pstRr_
Pang 1 of I
�%C S, l't�i her! u;W M� -1
Rdin u6hedIn Date Twit Receiticd 1}ram I���x NoieslCunuuerrls:
State of Sample Origin,
r `x
Check if FOR C;OMPUANCE
iieecived in;lmb by.
Dalc Time Rush lieyu trd BY: `'1 f
C Dateby kvM� m toatgrr 126392
Whae and -id 1,, v� pages ,hLKIIJ aCCompam S,iw�,lr, U) ttW luhnrtu�r.' 'thy ."rnl rrt,itt� Ihr rtt:k pstRr_
Pang 1 of I
Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONNI1 NTAL 4EC:HNC1I OrdFS, 1NC Cuyahoga Falls, Ohio 44223
Ana.tyfrcal LaherralorJes TEL: (330) 253-8211 FAX.- (330) 253-4489
ff7ebsite: htty:1Ay)yw.settek.com
Client Name: SYN-NC-27028
Logged by: John A.Semenik
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
Chain of Custod
1, Is Chain of Custody complete?
2. How was the sample delivered?
L_op !n
3, Coolers are present?
Work Order Number: 19071834
7/26/2019 9:50:00 AM
7/26/2019 11:18:05 PM
7/29/2019 2:54:58 PM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0° C to 6.0°C
7, Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
Sample Log -In Check List
Yes ❑d No ❑
FedEx
Yes ❑d No ❑
Yes �/❑ No ❑
Yes ❑ No ❑
Signed By:
Yes �/❑ No ❑
Yes d❑ N o ❑
Yes 0
Yes 0
Yes 0
Yes ❑
No ❑
No ❑
No ❑
No �/❑
RcptNo: 1
Not Present ❑
NA ❑
Not Present ❑�
NA ❑
NA ❑
NA ❑
11.
Is the headspace in the VOA vials less than 114 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials❑
12.
Were any sample containers received broken?
Yes
❑
No
J❑
13.
Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14.
Are matrices correctly identified on Chain of Custody?
Yes
❑
No
❑
15.
Is it clear what analyses were requested?
Yes
V
No
❑
16.
Were all holding times able to be met?
Yes
d❑
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17,
Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date IF
-
By Whom: Via:
❑ eMail
❑ Phone
❑
Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C Condition Seal Intact Sea[ No Seal Cate Signed By
4.5 1 Goodl Not Present
Page 36 of 36
SECTION 5
Wayne Farms Land Application Program
Permit #WQ0004609
Calendar Year 2019
Animal processing wastewater residuals were land applied in
two events in the year 2019. The biosolids were sampled at the
time of the land application events for nutrient and metal data.
The biosolids land applied in 2019 had sufficient lime added to
raise the pH of the uniform mixture to a pH of 10 for thirty
minutes prior to being surface land applied. This was
performed to control possible nuisance conditions (see Section
II, Item 7 in permit #WC.Q0004609).
CLASS 33IPSRP PIE LOG FEEET
'Using a pR Meter wit Two Point Staudardizaiion and Automatic Temperature Compensation (ATC) Probe
Analysis Method: SW-846 Method 9045D, Soil And Waste pFlf
].b ONTENEAR.: :1 s a 19 FAc=YMGcAT10N:
SAYDLING LOCATION
y
IG
O
N
"l
°,=
]Czaitaai
m
pH ? 12.0 S.U.
nit al p Ysu
7enp°Cq
1a.13 - 434
Adjusted
YpnitiIaslu
{�
g
r
yg�.{
cq W
Eiour P:K im S. T.
AdyustsP�
NC
p:a*lsaa
►:1-03 -.31 t v4q
II•$
2- Our PH ->11.5 S.U.
A]Fdr pulsu dsusted
'Templ°C BI
pkLi*lsp
'� "�f y F•'S
I°act , 11.J2 _ . 3 %
11:3a �2•I
Il:j
3k3
lls7 �a.�
►l.z2 say
i�°sa
1,2
if xo
y-2A41
L-7
.- y...........,. i,�� . •.,�.«.....�.... .., v..i�....�vu l a��vl ��A:) — u.va px-i 1 aus S �- ,, i mnperiLl re measlTre177.enz — ��-(-;); _L Cquimlem phi=1V1aas=cL p.-1. -r/-'file Uk.
Coll mantsts;
-23-
SECTION 6
Agricultural Lime Application Log
Year. 2019
Project: Wayne farms
Field
Soil 11
Lime Requiirement
Tons/Acre
Date Applied
(state -county -site -field)
pH 11
(from soil analysis)
Applied(CCE Eq.)
SU-13-10
7.3
O.OTIAc.
SU-13-12
6.6
O.OTIAc.
SU-20-1
5.7
0.0 VAC
SU-22-1
6.4
O.OTIAc.
SU-22-2
6.9
O.OTIAc.
SU-13-13
7.4
O.OTIAc.
SECTION 7
Page 1 of 1
Report No: 20-022-9619
Account No: 46431
Advisor: Synagro Central LLC
Marshal Puryear
284 Boger Rd
Mocksville NC 27028
Waypoint(D
ANALYTICAL
Client: Ben Watson
Wayne Farms
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypofntanalytical.com
Farm: 56-22
Date Received: 01/22/2020
Date of Report: 0211312020
Lab No Field 1D Sample ID
Soil Class HM% W/V pH
Ac
P4
K-1
S-1
Mn-1
Zn-1
Zn-Al
Cu-1
CEC
BS%
Ca% Mg% ESP Na SS-1 NO3 N
04066 56-22-1
MIN 2.0
6.4
0.7
138
165
27
113
233
233
100
8.3
92
60 21 0.8 0.1
Crop Recommendations:
1- Pasture
Rec Uom
Iblacre
Lime (f/acre)
0.0
N
50
P2 05
0
K2 0
D
S
16
Mn
2
Mn-Al
79
Zn
a
Cu
0
B
a
Mg
0
Last Crop
04067 56-22-2
MIN 1.8
6.9
0.2
52
45
44
106
4533
4533
180
14.8
99
57 40 0.3 0
Crop Recommendations:
1- Pasture
Rec Uom
Iblacre
Lime (flacre)
0.0
N
50
P2O5
30
K2O
99
S
7
Mn
2
Mn-AI
67
Zn
0
Cu
0
B
0.5
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meg1104cm3; ND3 N in mgldm3; W/V in glcm3
North Carolina Division of Water (Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypcint Analytical Virginia, Inc.
NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.goviagronomil Report No. FY20-SL004630
Client: Walter Johnson Advisor: Alex Fox
Predictive 193 Breezy Ridge Way Synagro
i
MOUNT AIRY, NC 27030 284 Boger Rd
Mehlich-3 Extraction Mocksville, NC 27028
Soil I Report
o rt
Sampled County : Surry
=7.9 +"
Links to Helpful Information
Client ID: 413860 Advisor ID: 501947
Sampled: 09/09/2019 Received: 09/12/2019 Completed: 09119/2019 Farm: NC-SU-13
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or 7" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be
detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with
zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids
and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce
potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for
copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field.
Sample ID: 10
Recommendations: Lime Nutrients (Iblacre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Soybean 0.0 0 0 40 0 0 pH$ 0 0 0
Note: 3 Note:
2 - 0.0
Test Results [units - WIV in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3l: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N
0.32 0.98 12.3 100 0.0 7.3 119 49 73 25 52 159 85 984 984 371 0.1 1
Sample ID: 12
Recommendations: Lime Nutrients (Iblacre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Corn, grain 0.0 120 -160 110 80 0 0 pH$ 0 0 0
Note: 3 Note:
2 - 0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg1dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.51 1.07 7.4 90 0.7 6.6 12 31 58 30 41 69 49 412 412 77 0.1 1
Noah Carolina
er.,l fir: Iq:;I;%Nt ,I,
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Amriculture
NCDA&CS Agronomic Division Phone. (919) 733-2655
Website: www.ncagr.govlagronomil
Report No. FY20-SL004630
Walter Johnson
Page 2 of 3
Sample ID: 13
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 -Corn, grain 0.0
120 - 160 70
70
0
0
pH$ Z
0 0
Note: 3 Note:
2 - 0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3j:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-Ali
Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 1.05 12.8 100 0.0 7.4 27 32
61 38 208
112
63
2780 2780
125 0.1 1
NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/
Report No. FY20-SL004630
Walter Johnson
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to S inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
Iblacre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-1
M-0
manganese index
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs,htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.nca r. goKlagronomilobpart4.ht ind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.nca r. gavlagronomiluvrst.htm
Page 1 of 1
Report Number: 19-354-0536
Account Number:46431
Send To: Synagro Central LLC
Marshal Puryear
284 Boger Rd
Mocksville NC 27028
Waypoint(D
ANALYTICAL
'Every acre... Every year. °TM
Farm: 56-20
SOIL ANALYSIS REPORT
Date Received: 1212012019 Date Of Analysis: 1212312019 Date Of Report: 12/23/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Grower: Tim Davis
Submitted By Alex Fox
Analytical Method(s): Mehlich 3 SM>' Buffer pH Loss On Ignition Water pH
NC = North Carolina Fertilitv Index Value
Sample ID
OM
WIV
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Field ID
Lab
Number
%
Sol[
IbslA
M3
K
M g
Ca
Na
Soil
Suffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pp m Rate
ppm Rate
ppm Rate
p H
Index
meg1100g
meg1104g
1
08495
3.5
114
61 H
92 H
118 H
382 L
14 VL
5.7
6.84
0.9
4.1
MIN
-1
M
NC = 51
NC = 47
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
mslcm Rate
1
5.8
24.0
46.6
1.5
22.0
17 M
8.3 VH
9 L
136 VH
1.2 M
0.2 VL
-1
1
1
1 NC=35 1
NC=207.5 1
NC=56 1
1 NC=60.0
values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. _ Cation Exchange Capacity.
Date Received: 12/20/2019
Date Of Report: 12/23/2019
Explanation of symbols: % (percent), ppm (parts per million), Ibs1A This report applies to sample(s) tested. Samples are retained a
(pounds per acre),mslcm(milli-mhos per centimeter),meg11Dog maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs1A, Sol ubte Salts mslcm x 640 = ppm. analysis prepared by: WaypointMalyt cal Virginia, Inc.
SOIL FERTILITY RECOMMENDATIONS
by: Faw, . PF 6ewr
Pauric McGroary
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Field
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
ID
Tans
Tons1A
Ib1A
Ib1A
Ib1A
Ib1A
IbIA
Ib1A
IblA
WA
Ib1A
IblA
1
Fescue Hay
4
0.8
200
0
102
0
9
0
4
0
0
1.0
-1
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.