WQ0006018_Residual Annual Report 2019_20200302

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0006018
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0006018
Applicant\Permittee * SYNAGRO
Facility Name * Town of Morehead City
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for Morehead City
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
MOREHEAD CITY NC 2019 Annual Report
10.65MB
FINAL.pdf
upload only 1 RJF document. NLltiple docurrents rust be corrbined into one RJF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/27/2020

435 W iams Court, Suite 100
Baltimore, tiID 21220
wwwsvnagro.com
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0006018
Dear NCDEQ:
SYNAGRIO"
5ynagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the Town of Morehead City, NC.
If you have any questions or need additional information, please do not hesitate to contact
Daniel Williams at [phone] or Melinda Boyd at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Daniel Williams, Town of Morehead City
Melinda Boyd, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

TOWN OF MOREHEAD CITY, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ000601.8
2019 ANNUAL REPORT

Town of Morehead City, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Page
3. Annual Land Application Field Summary Forms
4, TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00006018 County Carteret Year 2019
Facility Name (as shown on permit) Town of Morehead City W WTP NPDES No. NCO026611
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 7
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 76.51
Total number of acres utilized for land application during the year: 48.2
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
T All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CF'R Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CPR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit,
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information including the possibility of flues and imprisonment for
knowing violations." 7)
Daniel Williams Utilities Director
Pen ' cc am . an pe or p t) u nDate
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 02T .1102 (26) D'ENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
MOREHEAD CITY, NC
MOREHEAD CITY, NC CAKE
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
May 2019
575.00 Y
76.51
D
YEARLY TOTAL
575.00 Y
76.51
D
DRY METRIC
TONS
69.40
69.40
1/30/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006018
Facility Name: MOREHEAD CITY, NC
NPDES## : NCO026611
or WQ## (residual only)
WWTP Name: MOREHEAD CITY
Residuals Analysis Data
Product Type
CAx
Date Sampled (grab) or 04/16/19
Date Composited
Percent Solids
15. 80
PARAMETERS (mg/kg dry weight)
Arsenic
<5
Cadmium
<1
Mercury
0.104
Chromium
2.81
Copper
119
Lead
<3
Molybdenum
<2.5
Nickel
<2.5
Selenium
<5
Zinc
149
Total Phosphorus
4580
TKN
69000
Ammonia -Nitrogen
6770
Nitrate and Nitrite
59. 9
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X \ I Date o?— -14> -.2 0,2(i
(SIGNATURE OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Saturday - February 1 2020 at 14:08:16 for: 2252 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006018
Facility Name: MOREHEAD CITY, NC
NPDES# : NCO026611
or WQ# (residual only)
WWTP Name: MOREHEAD CITY
Residuals Analysis Data
Product Type CAK
Date Sampled (grab) or 04/16/19
Date Composited
Percent Solids ? 5.80
PARAMETERS (mg/kg dry weight)
Aluminum
1910
Calcium
4830
Magnesium
977
pH
7.40
Potassium
807
Sodium
977
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for [snowing violations."
x Date
(SIGNATU
ER)
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Saturday - February 1, 2020 at 14:08:59 for: 2252 01

(2)
Waynt.PA
NALYT[CAL
4/30/2019
Synagro Central LLCI Morehead City
Clint Williams
One Commerce Square
Suite 204
Washington, NC, 27889
Ref: Analytical Testing
Report Number: 19-108-0205
Project Description: Moreahead WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Clint Williams:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/18/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam, 11' 61,E
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
hefa��.
Page 1 of 6

s
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-108-0205
Client Project Description: Mareahead WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65951
Moreahead WWTP
Solids
04/16/2019
09:15
04/18/2019
65951
Moreahead WWTP
Solids
04/16/2019
09:15
04/18/2019
65951
Moreahead WWTP
Solids
04/16/2019
09:15
04/18/2019
65951
Moreahead WWT
Solids
04/16/2019
09:15
04/18/2019
65951
Moreahead WWTP
Solids
04/16/2019
09:15
04/18/2019
65951
Moreahead WWTP
Solids
04/16/2019
09:15
04/18/2019
65951
Moreahead WWTP
Solids
04/16/2019
09:15
04/18/2019
65951
Moreahead WWTP
Solids
04/16/2019
09:15
04/18/2019
WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354
SM-4500--1\11-13C
WfN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WrN
SM-4500-NH3C-TKN
WTN
5M-2540G
WTN
Page 2of6

Report Number: 19-108-0205
Account Number: 46472
Send To: Synagro Central LLC/ Morehead City
Clint Williams
One Commerce Square
Suite 204
Washington , NC 27889
Lab Number: 65951
Sample Id : Moreahead WWTP
Waypoint,(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypointanalytical.com
Project: Moreahead WWTP
REPORT OFANALYSIS Date Sampled: 4/16/2019 09:15:00
Date Received: 04/18/2019 00:00
Date Reported: 04/30/2019
Total Solids "
15.80
158000
100.0
ADM
04/18/2019 15:48
SM-254OG
Moisture *
84.20
100.0
ADM
0411812019 15:48
SM-254OG
Total Kjeldahl Nitrogen
6.90
69000
250
JPJ
04/24/2019 09:30
SM-4500-NH3C-TKN
Phosphorus
0.46
4580
50.0
BKN
04/23/2019 19:30
601 DID
Potassium
0.08
807
50.0
KKM
04128/201917:13
601OD
Sulfur
0.18
1760
50.0
BKN
04/23/201919:30
6010D
Calcium
0.48
4830
250
BKN
04123/201919:30
6010D
Magnesium
0.10
977
50.0
BKN
04/231201919:30
6010D
Sodium
0.10
977
250
BKN
04/231201919:30
6010D
Iron
2040
50.0
BKN
04/231201919:30
6010D
Aluminum
1910
50.0
BKN
04/23/201919:30
6010D
Manganese
59.8
5.00
KKM
04/24/201919:56
6010D
Copper
119
2.50
BKN
04/231201919:30
6010D
Zinc
149
12.5
BKN
04/23/201919:30
6010D
Ammonia Nitrogen
0.68
6770
100
JPJ
04/24/2019 11:15
SM-4500-NH3C
Organic N
6.22
62230
250
04/24/2019 09:30
CALCULATION
Nitrate+Nitrite-N
59.9
4.73
ZBD
04124/201914:24
4500NO3F-2011
All values are on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding Time
?W;L
Air Vewr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made Pau ric McGroary
to the work. the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization Agronomist
Page 3 of 6

Report Number: 19-108-0205
Account Number: 46472
Send To: Synagro Central LLC/ Morehead City
Clint Williams
One Commerce Square
Suite 204
Washington , NC 27889
Lab Number: 65951
Sample Id : Moreahead WWTP
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Moreahead WWTP
REPORT OF ANALYSIS Date Sampled: 4/16/2019 09.15:00
Date Received: 04/1812019 00:00
Date Reported: 04130/2019
Cadmium
<1.00
1.00
BKN
04/23/201919:30
6010D
Chromium
2.81
2.50
BKN
04/23/201919:30
6010D
Nickel
<2.50
2.50
BKN
041231201919:30
6010D
Lead
<3.00
3.00
BKN
04/231201919:30
6010D
Arsenic
<5.00
5.00
BKN
04123/201919:30
601OD
Mercury
0.104
0.0140
TJS
O4/2312019 13:01
SW-7471 B
Selenium
<5.00
5.00
BKN
0412312019 19:30
601OD
pH'
7.4
JSL
04/24/2019 06:53
9045D
Molybdenum
<2.50
2.50
BKN
04/231201919:30
601OD
Comments:
A€I values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and 7etfers are for the exciusive and confidential use of our clients, and may net be reproduced in whole or part, nor may any reference be made
to the work, the resuits, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pwir- X C 0414r,
Pauric McGroary
Agronomist
Page 4 of 6

Waypoint,Q)
ANALYTICAL
7621 Whitepme Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46472
Customer Name: Synagro Central LLC/ Morehead City
Report Number: 19-108-0205
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping containericooler?
0 Yes
0 No
• Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
9 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 19 No
Signature: lBrandi Watson Date & Time: 411812019 14:10:24
Page 5of6

u
D
D
D
D
n
SAMPLING LOG # OD804/7<
A & L I:7621 V�
Richmo
CUSTOMER: SYNAGRO
PROJECT MANAGER: _1 `p `� �•`�I ' Y ��+r10
Phone: ��°) �J 1ST
4
A & L CUSTOMER
SAMPLING
SAMPLE
LAB # I.D.
LOCATION
TYPE
/Sy�AMPLE
' 1 p
CUSTODY
O&
lli
19-108-0205
1111
ANALYSIS
Illlllilllllilii111111111111111illligill �111111ilHill
o441&2019
-CORD
Svnaaso Central LLCI Morehead Cilv
14:03:16
Moreahead WWTP
ling procedures
_ _ .. _ __. _. , it these samples.
•�
+ J
SAMPLER
# OF SAMPLING
METHOD
METHOD
CONTAINERS DATE TIME
PRESERVED
SHIPPED
t
Relinquished by Sampler: Date Time Recieved by: REMARKS:
Relinquished by: Date Time Recieved by:
Relinquished by:
Date Time Recieved by:
SPECIAL INSTRUCTIONS:
-T4-�— (� /,c
U4�j '7:) I For L monitoring purposes. PO#:
(STATE)
SAMPLE ANALYSIS REQUEST
I.D. SL1 SL2 NH -N ND .N Organit Cd Cr Ni Pb A5 H Se CaCO3 Vola#ile
N P equiv. Solids Mo CI NO2N
1,00 � too � pow � pow � 1000 � Pw � loot � 1-*w � por � 10off � P0 � 1,00 toor 1.40
Lab# E 65951-1 Moreahead 1Nwl-P
Cust: 46472 Synaqro Central LLC/ Moreheac
SL1: Total Solids (Moisture), 1 Col: 04/16/2019 09:15 Rec: 04/18/2019 00:00
SL2: Basic Test SL1 plus Sulfi 19-108-0205 Preservation: < = 6 degrees C =se, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample date Report Range Ratio
2252-01-CAK-NC MOREHEAD CITY, NC CAKE 4/16/2019 11112019-1213112019 1.3288
Na mg/I = (Na mg/kg x % Solids) + 100 = (977 x 15.8000) + 100 = 154,366
Ca mgll = (Ca mg/kg x % Solids) + 100 = (4830 x 15.8000) M 100 = 763.14
Mg mg/l = (mg mg/kg x % Solids) + 100 = (977 x 15.8000) + 100 = 154.366
Na meq = Na mg/l + Moiec.Wgt.Na = 154.366 + 23 = 6.71157
Ca meq = Ca mg/l + Molec,Wgt.Ca = 763.14 + 20 = 38.157
Mg meq = Mg mg/l + Molec.Wgt.Mg = 154.366 + 12 = 12.8638
SAR = Na meq ;. SgrRooQ0.5 x (Ca meq + Mg meq)] = 6,71157 + SgrRoot[0.5(38.157+12.8638)] = 1.32882
Printed: 211 /2020
Page 1 14:09

SECTION 3

FACILITY NAME: MOREHEAD CITY, NC
OWNER: COLIN WHETHERINGTON
SITE #: NC CR 00001 FIELD# : CR 00001 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: ONSLOW
PERMIT #1: WQ0006018 ANNUAL DRY TONS APPLIED: 13.31
OPERATOR: ROBERT M RIGGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.90 ACRES PERMITTED: 6.90
Page : I
Lime Applied ***
Date
Lbs/Ae
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
till-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
5/22/19
100.00 (CY)
14.493
15.80
1.929
MOCC
DRY
0-<l/2"
SURIN
1.0
0.30
69,000. p
6,770.00 p
59,90 p
25499
SOYBEANS
May-19
100.00 (CY)
14.493
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds Ac: 14.49
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
TOTALS:
Annual lbs/acre 98
0.019 0.004 0.011 0.459 0.012 <.001 0.010 0.010 0.019 0.575 17.67
Cumulative lbs/acre 0.413 0.247 3.456 80.423 3.606 0.351 0.580 2.760 0.335 67.813
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
155
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
MOCC = MOREHEAD CITY, NC CAKE
/" -0 -1
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR = Not Reported or Not Required % = percent p = ppm or M&g ** Volatilization Rate: Surface 0.5, lnjection/Incorporation 1.0
Application Method: SUR - Surface, IN7 - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: MOREHEAD CITY, NC
OWNER: COLIN WHETHERINGTON
SITE 4: NC CR 00001 FIELD# : CR 00001 0002
RESIDUAL SOURCE(S): See list at bottom of report
LANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: ONSLOW
PERMIT 9: WQ0006018 ANNUAL DRY TONS APPLIED: 26.62
OPERATOR: ROBERT M. RIGGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.70 ACRES PERMITTED: 20.70
Page: 1
Lime Applied
Date
Lbs�Ac
allons (0) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
nation
zation
TKN
Nitrogen
and
(pp-)
Crop
MONTH
'Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/22/19
200.00 (CY)
9.662
15.80
1.286
MOCC
DRY
0-<1/2"
SURIN
1.0
0.30
69,000. p
6,770.00 p
59.90 p
25499
SOYBEANS
May-19
1 200.00 (CY)
9.662
I
1
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 9.66
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
TOTALS:
Annual lbs/acre 66
0.013 0.003 0.007 0.306 0.008 <.001 0.006 0.006 0.013 0.383 11.78
77777,
Cumulative lbs/acre 0.415 0.294 4.718 91.586 4.052 0.396 0.671 3.203 0.358 72,935
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
155
F➢ Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
"'
1339.0
267.9
15.0
375.0
89.0
2500.0
MOCC = MOREHEAD CITY, NC CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR —Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITYNAME: MOREHEAD CITY, NC
OWNER: YOUNG/WETHERINGTON
SITE #: NC CR 00007 FIELD# : CR 00007 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: AUTRYVILLE
PERMIT #: W00006018 ANNUAL DRY TONS APPLIED: 36.60
OPERATOR: ROBERT M. RIGGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20,60 ACRES PERMITTED: 20.60
Page: 1
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
TKN
Nitrogen
and
(PP-)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/21/19
125.00 (CY)
6.068
15,80
0.807
MOCC
DRY
0-<1/2"
SURIN
1.0
0.30
69,000. p
6,770.00 p
59.90 p
25499
SOYBEANS
5/22/19
150.00 (CY)
7.282
15.80
0.969
MOCC
DRY
0-Q/211
SURIN
1.0
0.30
69,000. p
6,770.00 p
59.90 p
25499
SOYBEANS
May-19
1 275.00 (CY)
13.350
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 13.35
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
TOTALS:
Annual lbs/acre 1
0.018 0.004 0.010 0.423 0.011 <.001 0.009 0.009 0.018 0.529 16.27
Cumulative lbs/acre 0.356 0.135 3.692 51.459 1.103 0.130 0.339 1.740 0.281 50.512
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
. . ....... ..
.... ...... .
. . .......
1I9
FD Cumulative Pollutant Loading Rate Limit (Ibslacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
MOCC = MOREHEAD CITY, NC CAKE
x d-r
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Mabcd: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

SECTION 4

Summing
Awfyticaf f.afioratorJe
May 07, 2019
Melinda Boyd
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Morehead City WWTP
Dear Melinda Boyd:
Summit Environmental Technologies, Inc.
3310 Win St.
Cu whoga Falls. Ohio 44223
TEL: [phone] FAX: [phone]
Website: http:/19)yw.seltelc.com
Order No.: 19041250
Summit Environmental Technologies, Inc. received 1 sample(s) on 4/ 18/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
11�
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA,.Colorado, Connecticut PI I-0108, Delaware, Florida NELAC E87688, Georgia E87688, Tdaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York I1777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VA?
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA0003I7, South Carolina 92 IMI, Texas T104704466-11-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 31

��,� SunrmitL'nvrronrraentalTechnologies, Inc. Case Narrative
S3310 Win St.
ENVIROMPAENTAL IrEC&iMMOGI=S, We Cuyahoga Falls, Ohio44223 WO#: 19041250
Arrafyh'�al +aborafvne • TEL: [phone] FAX.- [phone]
Website: http://ivinv.settek.com Date: 5/7/2019
CLIENT: Synagro
Project: Morehead City WWTP
WorkOrder Narrative:
19041250: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-.dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
19041250-OOIA 444096: Prep Comments for MtlPrep TCLP(3010A), Sample 19041250-OOIA: TCLP
was filtered after digestion.
Analytical Sequence Sample Notes:
19041250-00IA TCLP-svoc-CPEST(8081B): CCV exhibits high recovery for Methoxychlor.
Associated samples are N.D.
Original
Page 2of31

ill
Summit Environmental Technologies, In Qualifiers and Acronyms
summ3310 Wins t
R4V1110WMENTAL Ir-C1iiot0.0iFS,INC Cuyahoga Falls, Ohio4421 WO#; 19041250
Ani?iyticaf t aborgtoroes TEL: [phone] FAX: [phone]b
Website: http:11ii,viu.settek.co Date; 5n/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution,
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
rn Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The results presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high ( }.
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-h- The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV -I+ The ICV recovery failed low (-) or high (+),
s The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Luuit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvi
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
lCV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 31

SUMMITanSaniitEnrironnientalTechnologies, Inc. `'Vorkorcler
3310 Win St.
Ehl4 tIONFAENTAL rC71.h1[]1.ti7 �ifr,,'kr: CuyabogaFalls, Ohio44223 Sample Summary
Acnlyllcaf tdbofalarjomE TEL: [phone] FAX.- [phone] W014: 19041250
Websile; 07-May-19
CLIENT: Synagro
Project: Morehead City WWTP
Lab SampleID Client Sample ID Tag No Date Collected
19041250-001 MC19 4/16/2019 9:15:00 AM
Date Received Matrix
4/18/2019 9:55:00 AM Solid
Page 4 of 31

'
summ
Summit Environmental Technologies, Inc.
331 O Win St.
DATES REPORT
t+IiiC3fdiiiErdTA� rEc a�❑ rslGr_=s, utst Cuyahoga Falls, Ohio 44223
An: 4thcal Laboralonee TEL: [phone] FAX [phone]
WO#: 19041250
Website: htW:1Avivw.settekcom
07-Mav-19
Client:
Synagro
Project:
Morehead City WW3P
Sample ID
Client Sample 1D Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
190.41250-001A MC19 4/16/2019 9:15:00 AM Solid Ignitability of Solids (SW-846: 1030)
4/26/2019 3:30:00 PM
pH (SW9045D)
5/V2019 2:53:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
4/22/2019 4:40:00 PM
Reactive Sulfide (9034)17.3.4.2
4/24/20I9 4:I0:00 PM
TCLP Herbicides Analysis (SW1311/84/18/2019 424:30 PM
4/24/2019 10:50:00 A
4/30/2019 1:50:00 AM
solid
TCLP Mercury Analysis (SW1311/7414/18/2019 4:24:30 PM
4/22/2019 12:50:00 PM
4/22/2019 6:30:00 PM
TCLP Metals Analysis (SW13I1/60104/1812019 4:24:30 PM
4/22/2019 8:15:00 AM
4/23/2019 3:35:32 PM
TCLP Metals Analysis (SW1311/60104/1812019 4:24;30 PM
4/22/2019 8:15:00 AM
4/22/2019 9:12:04 PM
TCLP Pesticides Analysis (SW1311/8[4/1812019 4:24:30 PM
4/19/2019 5:00:00 PM
4/24/2019 1:13:00 AM
TCLP Semi-Volatiles Analysis 4/18/2019 4:24:30 PM
4/22/2019 4:00:00 PM
4/23I2019 8:46:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
4/18/2019 4:25:10 PM
4/19/2019 7:37:00 PM
Original
Page 5 of 31

U'-
SunanrtEnvironmental Technologies,Inc.
33Technologies,
es, St.
Analytical Report
ENVIROAMENTAL TEm3 NQLL)GlrI3, °:'
Cuyahoga rails, Ohio 44223
TEL: [phone] FAX. [phone]
(base report)
W09: 1"41250
Wehsite; httu://tivii
u.seftek.con:
Date Reported: 5/7/2019
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
4/16/2019
9:15:00 AM
Lab ID: 19041250-OOIA
Project: Morehead City WWTP
Client Sample ID MCI
Analyses Result
RL
Qual Units
Dr
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND
0.00500
mglL
1
4/22120196:30:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
1.25
mglL
1
4/22/2019 9:12:04 PM
TCLP Barium(Ba)
ND
12.5
mglL
1
4/22/2019 9:12:04 PM
TCLP Cadmium(Cd)
ND
0.250
mglL
1
4/22/2019 9:12:04 PM
TCLP Chromium(Cr)
ND
0.500
mglL
1
4/23/2019 3:35:32 PM
TCLP Lead(Pb)
ND
1.25
mglL
1
4/22/2019 9:12:04 PM
TCLP Selenium(Se)
ND
0.125
mglL
1
4/22/2019 9:12:04 PM
TCLP Silver(Ag)
ND
1.25
mglL
1
4122/2019 9:12:04 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichlorcbenzene
ND
0.0800
mg1L
2
4/23/2019 8:46:00 PM
2,4,5-Trichlorophenol
ND
0.200
mglL
2
4/23/2019 8:46:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg1L
2
4/23/2019 8:46:00 PM
2,4-Dinitrotoluene
ND
0.0400
mgiL
2
4/23/2019 8:46:00 PM
Cresols, Total
ND
4.00
mg1L
2
4/23/2019 8:46:00 PM
Hexachloro-1,3-butadiene
ND
0.0160
mglL
2
4/23/2019 8A6:00 PM
Hexachlorobenzene
ND
0.0400
mglL
2
4/23/2019 8:46:00 PM
Hexachloroethane
ND
0.0800
mglL
2
4/23/2019 8:46:00 PM
Nitrobenzene
ND
0.0800
mglL
2
4/23/2019 8:46:00 PM
Pentachlorophenol
ND
0.200
mglL
2
4/23/2019 8:46:00 PM
Pyridine
ND
0.200
mglL
2
4/23/2019 8:46:00 PM
Surr: 2-Fluorophenol
72.3
10 - 109
%Rec
2
4/23/2019 8:46:00 PM
Surr: Phenol-d6
94.1
10 - 109
%Rec
2
4/23/2019 8:46:00 PM
SUM Nitrobenzene-d5
86.8
19 - 120
%Rec
2
4/2312019 8:46:00 PM
Surr: 2,4,6-Tribromophenol
84.1
10 - 120
%Rec
2
4/23/2019 8:46:00 PM
Surr. 2-Fluerobiphenyl
100
22 - 117
%Rec
2
4/23/2019 8:46:00 PM
Surr: p Terphenyl-d14
118
34 - 130
%Rec
2
4/23/2019 8:46:00 PM
Qualifiers: E
Value above quantitation range
M
Manual Integration used to determine area response
N
Tentatively identified compounds
O
RSD is greater (bat) RSDlimit
PL
Permit Limit
RL
Reporting Detection Limit
H Itolding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 6 of 31

Summit Em,irornnental Technologies, Inc. Analytical Report
summmir 3310 Wiz St.
€f+Vlrr0NPA5N-rAI.Tr-C3OJOL{1 TRi ;N(., Cuyahoga Falls, Ohio44223 (base report)
Ansfyrffpal Laboral arlttv TEL: [phone] Fil Y: [phone] WO#: 19041250
II'ebsite: htto:11ivirw.settelr.com Date Reported: 51712019
CLIENT:
Synagro
Matrix:
SOLID
Lab ID:
19041250-OOIA
Project:
Morehead City WWTP
Client Sample ID MC19
Tag Number:
Collection Date: 4/16/2019 9:15:00 AM
Analyses
Result
RL,
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC
Analyst: MES
TCLP PESTICIDES ANALYSIS
(SW1311/8081)
Chlordane, total
ND
0.0260
mg1L
10
4/24/2019 1:13:00 AM
Toxaphene
ND
0.0500
mglL
10
4124/2019 1:13:00 AM
Endrin
ND
0.00500
mglL
10
4/24/2019 1:13:00 AM
gamma-BHC
ND
0.00500
mglL
10
4/24/2019 1:13:00 AM
Heptachlor
ND
0.00500
d mglL
10
4/24/2019 1:13:00 AM
Heptachlor epoxide
ND
0.00500
mglL
10
4/24/2019 1:13:00 AM
Methoxychlor
ND
0.00500
dQC} mglL
10
4124/2019 1:13:00 AM
Surr: TCMX
33.2
10 - 119
%Rec
10
4124/2019 1:13:00 AM
Surr: DCB
69.6
10 - 119
%Rec
10
4124/2019 1:13:00 AM
TCLP HERBICIDES-S(8151)
TCLP HERBICIDES ANALYSIS (SW131118151)-SOLID
2,4-D
2,4,5-TP
Surr: DCAA
SW8151A SW8151A Analyst: MES
ND R.0100 mg1L 1 4/30/2019 1:50:00 AM
ND 0.00500 mg1L 1 4/30/2019 1:50:00 AM
73.4 20 - 140 %Rec 1 4/30/2019 1:50:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.500
mglL
100
4/19/2019 7:37:00 PM
1,2-Dichloroothane
ND
0.500
mglL
100
4/19/2019 7:37:00 PM
MEK
ND
10.0
mglL
100
4/19/2019 7:37:00 PM
Benzene
ND
0.500
mglL
100
4/19/2019 7:37:00 PM
Carbon tetrachloride
ND
0.500
mglL
100
4119/2019 7:37:00 PM
Chlorobenzene
ND
5.00
mglL
100
4/19/2019 7:37:00 PM
Chloroform
ND
0.500
mglL
100
4/19/2019 7:37:00 PM
Tetrachloroothene
ND
0.500
mg1L
100
4/19/2019 7:37:00 PM
Trichloroothene
ND
0.500
mglL
100
4/1912019 7:37:00 PM
Vinyl chloride
ND
0.200
mglL
100
4/19/2019 7:37:00 PM
Surr: 4-Bromofluorobenzone
87.5
70 - 130
%Rec
100
4/19/2019 7:37:00 PM
Surr: Dibromofluoromethane
100
70 - 130
%Rec
100
4/19/2019 7737:00 PM
Surr: Toluene-d8
98.1
70 - 130
%Rec
100
4/19/2019 7:37:00 PM
Qualifiers: E
Value above yuantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to detcnnine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column continuation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Original
RL
Reporting Detection Limit
U
Samples with CalcVal < MDL
Page 7 of 31

T- Summitlnvirowntenlal Technologies, Inc. Analytical Report
PT SUMMI3316 T-Nn St.
irPkullT4fkfA ASTA.L ri'_011N0I i7331 5, 'N.- Cuyahoga Falls, Ohio 44223 (base report)
p:,rui(vrlcal tabcrafarl@5 IEL: [phone] F.4 .- [phone] W04: 19041.250
Websile: ham:11 vnnv.settelr.com Date Reported: 5/7/2019
Matrix: SOLID Collection Date: 4/16/2019 9:15:00 AM
Lab ID: 19041250-OOIA
Project: Morehead City WWTP
Client Sample ID MC19
Analyses Result RL Qua] Units DF Date Analyzed
RCI-SOLID-W1IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND 0.485
mg/Kg 1
4122/2019 4:40:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABiLITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1
4/26/2019 3:30:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH 7.4
s.u.@22.4C 1
6/2/2019 2:53:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND 25.0
mg/Kg 1
412412C19 4:10:00 PM
Qualifiers: E
Value above quantitation range
M
Manual Integration used to determine area response
N
Tentatively identified compounds
O
RSD is grcater than RSDlimit
PL
Permit Limit
RL
Reporting Detection Limit
IT Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CalcVaI < MDL
Page 8 of 31

UM'Eff SurnmitEnt>ironntenial Technologies, Inc. Accreditation Program
3310 Win M. Anal tes Report
E141UMN1AENTALTCCtlil1(bti7GWS,NC Cuyahoga Falls, Ohio44223 � Y
Ana;ytical Laboraxor *s TEL: [phone] FAX; [phone] WO##; 19041250
Website: h1(b:11www.xe1tek.com 07-May-19
Client: Synagro State: NW
Project: Morehead City WWTP Program Name: NC_WW_SCM
Sample H3 Matrix
Test Name
Analyte
Status
19041250-OOIA Solid
lgnitabilityofSolids (SW-846:1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (901417.3.3.2)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)17.3.4.2
Sulfide; Reactive
U
Solid
TCLP Herbicides Analysis (SW131118151)-solid
2,4,5-TP
A
Solid
TCLP Herbicides Analysis (SW131118151)-solid
2,4-D
A
Solid
TCLP Mercury Analysis (SW 1311/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW 1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis (SW 1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW 13l 1/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW 1311 /6010)
Chromium
A
Solid
TCLP Metals Analysis (SW 1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW131116010)
Selenium
A
Solid
TCLP Metals Analysis (SW131V6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW131118081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW131 1/809 1)
Eadrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/809t)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW131 V809 t)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SW1311/8091)
Toxaphene
A
Solid
TCLP Setni-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzerie
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/9270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/9270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW 131119270)
flexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW 131119270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270.)
Hexachlorocthane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311 /8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
NG WW SCM A Accredited NC WW SCM U Unavailable
Original #1
Page 9 of 31

E�lU'T SumnritEnvirwurrental Technologies, Inc. Accreditation Program
r=3n0!3 S3310 Win St. Analytes Report
EFll+RIOWAENTAL TLC1iNi3t.0 1 S,1KC Cuyahoga Falls, Ohio 44223 Y
Arr,Vy0cal Laboralorlas TEL: [phone] FAY..- [phone] W04: 19041250
Website: hitp:/hvutw.settek.coni 07-May-19
CIrent: Synagro ,State: NW
Project: Morehead City WWTP Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19041250-001. A Solid
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbontetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCvI U Unavailable
Original #1
Page 10 of 31

IT -Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
? r:.`i-wlRORMEtdiAL TECHNOLOGIES, !Nr' Cuyahoga Falls, Ohio 44223
WO#: 19041250
A.naayticaf TEL: [phone] FAX.- [phone]
Website: htto://wwiv.seliek.com 07-May-19
Client: Synagro
Project: Morehead City WWTP BatchlD: 36953
Sample ID MB-36953
SampType: MBLK
TestCode: telp-vac-mstr Units: mg1L
Prep Date: 4118/2019
RunNo: 97314
client ID: PBS
Batch ID: 36953
TestNo: SW0260 SW1311M
Analysis Date: 412012019
SegNo: 2066295
\nalyte
Result
PQL SPK value SPK Ref Val
%RI=C LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
9.1 Dichloroethene
ND
0.0500
lt2-Dichloroethane
ND
0.0500
MEK
ND
1.00
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloreethene
ND
0.0600
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
474
Surr: Dibromofluoromethane
505
Surr: Toluene-d8
491
500.0 94.7 70 130
500.0 101 70 130
500.0 98.2 70 130
Qualifiers: B Analyze detected in the associated Method Blank E Value above quantitation range H I-Tolding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 11 of 31

'lt Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summ3310 Win St.
EP WRONMENThLW17 Cuyahoga Falls, Ohio 44223
WO#: 19041250
Anifynlcaf Labcrralones TEL: [phone] FAX.- [phone]
Website: http://www.settekcom 07-May-19
Client: Synagro
Project: Morehead City WWTP HatchID: 36953
Sample ID LCS-97317
SampType: LCS
TestCode: tclp-voc-mstr Units: mg1L
Prep Date:
RunNo: 97317
:Nent ID: LCSS
Batch ID: 36953
TestNo: SW8260 SW1311M
Analysis Date: 411912019
SegNo: 2092105
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLtmit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.0205
0.00500
0.0200
0
102
79.4
131
1,2-Dichloroethane
0.0190
0.00500
0.0200
0
95.2
73.6
137
MEK
ND
0.100
0.100
0
99.0
55.1
163
Benzene
0.0194
0.00500
0.0200
0
96.9
73.1
132
Carbon tetrachloride
0.0189
0.00500
0.0200
0
94.4
63.7
139
Chlorobenzene
ND
0.0500
0.0200
0
101
72.3
139
Chloroform
0.0190
0.00500
0,0200
0
95.1
79.3
129
Tetrachloroethene
0.0206
0,00500
0.0200
0
103
56.2
187
Trichloroethene
0.0189
0,00500
0.0200
0
94.6
64.1
138
Vinyl chloride
0.0215
0.00200
0.0200
0
107
22.1
147
Surr:4-Bromoflucrobenzene
52.7
50.00
105
80.4
126
Surr: Dibromofluoromethane
47.7
50.00
95.4
70.3
125
Surr: Toluene-d8
50.0
50.00
100
82
117
Sample ID 19041087-00laMS
SampType: MS
TestCode: telp-voc-mstr Units: mglL
Prep Date:
RunNo: 97317
Client ID: Batch=
Batch ID: 36953
TestNo: SW8260 SW1311M
Analysis Date: 4/19/2019
SegNo: 2092106
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
2.34 0.500
2.00 0 117
39.9
160
1,2-Di(hloroethane
1.98 0.500
2.00 0 99.0
42.5
157
MEK
ND 10.0
10.0 0.707 85.5
16.6
227
Benzene
2.17 0.500
2,00 0 108
38.1
155
Qualifiers: B
Analyte detected in the associated Method Blank
S
Value above quantitation range
H
Holding times for preparation or anal}
7
Analyte detected below quantitation limits
M
Manual Integration used to determine area
response
MC
Value is below Minimum Compound
Original
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 12 of 31

.M, Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3210 Win St.
Et;VNIONMEWAL tt:C4N0L0GJr---S, Cuyahoga Falls, Ohio 44223
WQ#: 19041250
.my(+cal' Labor�lanos TEL: [phone] FAX: [phone] Ar
YYebsite: httn://ivwiv.settek.com 07-Mav-19
Client: Synagro
Project: Morehead City W WTP BatchID: 36953
iample ID 19041087-001aMS
SampType: MS
TestCode: telp-voc-mstr Units: mg1L
Prep Date:
RunNo: 97317
lient ID: BatchQC
Batch ID: 36953
TestNo: SW8260 SW1311M
Analysis Date: 411912019
SegNo: 2092106
\nalyte
Result
PQL SPK value SPK Ref Val
%RE Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
2.14
0.500
2.00
0
107
40.8
162
Chlorobenzene
ND
5.00
2.00
0
104
35.7
168
Chloroform
2.12
0.500
2.00
0
106
18.3
199
Tetra chloroethene
2.26
0.500
2.00
0
113
10
261
TrichIoroethene
1.89
0.500
2.00
0
94.6
23.8
175
Vinyl chloride
2.46
0.200
2.00
0
123
10
165
Surr:4-Bromofluorobenzene
5190
5000
104
84.6
130
Surr: Dibromofluoromethane
4840
5000
96.8
71.4
127
Surr: Toluene-d8
5120
5000
102
74.6
127
Sample ID 19041087-001aMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mglL
Prep Date:
RunNo: 97317
client ID: BatchQC
Batch ID: 36953
TestNo: SW8260 SW1311M
Analysis Date: 411912019
SegNo: 2092107
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichlorcethene
2.19
0.500
2,00
0
110
39.9
160
2.34
6.49
25
1,2-Dichlorcethane
1.97
0.500
2.00
0
98.6
42.5
157
1.98
0.405
25
MEK
10.1
10.0
10.0
0.707
93.9
16.6
227
9.26
8.64
25
Benzene
2.09
0.500
2.00
0
105
38.1
155
2.17
3.66
25
Carbon tetrachloride
2.15
0.500
2.00
0
107
40.8
162
2.14
0.467
25
Chlorobenzene
ND
5.00
2.00
0
102
35.7
168
0
0
25
Chloroform
2.00
0.500
2.00
0
99.9
18.3
199
2.12
5.88
25
Tetrachloroethene
2.12
0.500
2.00
0
106
10
261
2.26
6.20
25
Qualifiers: S Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
l Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 13 of 31

'
summn3310
Summit Environmental Technologies, Inc.
Win St.
QC SUMMARY REPORT
EP;OPMt,lldENTAL TEC4N€ LOGIr-S, INC
1 �,fytleal i a>7oraIdrta
Cuyahoga Falls, Ohio 44223
TEL: [phone] FOX [phone]
WQ#: 19041250
Website: http://Www.settek eom
07-May-l9
Client:
Synagro
Project:
Morehead City WWTP
BatchID: 36953
Sample ID 19041087-00laMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mg1L
Prep Date:
RunNo: 97317
aient ID: Batch4C
Batch ID: 36953
TestNo: SW8260 SW1311M
Analysis Date: 4/1912019
SegNo: 2092107
knalyte
Result
POL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Trichioroethene
1.91 0.500
2.00
0 95.4
23.8
175
1.89 0.789 25
Vinyl chloride
2.41 0.200
2.00
0 121
10
165
2.46 1.85 25
Surr:4-Bromofluorobenzene
5070
5000
101
84.6
130
0 25
Surr: Dibromofluoromethane
4820
5000
96.3
71.4
127
0 25
Surr: Toluene-d8
4980
5000
99.6
74.6
127
0 25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDhmit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 14 of 31

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMINt 3310 Win St.
ENVIt10W.IEtd7AL TECHNaL.QGI_-,, Cuyahoga Falls, Ohio 44223
WO#: 19041250
Anaiyrlra1iabarafonos TEL: [phone] FAX- [phone]
Y1'ebsite: httn:/hv)viv.settekcom 07-May-19
Client: Synagro
Project: Morehead City WWTP SatchlD: 36994
Sample ID MB-36994
SampType: MBLK
TestCode: HG—TCLP(74 Units: PPM
Prep Date: 412212019
RunNo: 97344
Client ID: PBS
Batch ID: 36994
TestNo: SW7470A SW7470A
Analysis Date: 412212019
SegNo: 2069607
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-36994
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 412212019
RunNo: 97344
Client tD: LCSS
Batch ID: 36994
TestNo: SW7470A SW7470A
Analysis Date: 4/22/2019
SegNo: 2069608
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00434 0.00200 0.00400 0 108 80 120
Sample ID 19041086-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 412212019
RunNo: 97344
CIient ID: BatchQC
Batch ID: 36994
TestNo: SW7470A SW7470A
Analysis Date: 4/22/2019
SegNo: 2069612
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00446 0.00200 0.00400 0 112 75 125
Sample ID 19041086-001AMSD
SampType: MSD
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 4/22/2019
RunNo: 97344
Client ID: BatchQC
Batch ID: 36994
TestNa:
SW7470A SW7470A
Analysis Date: 412212019
SegNo: 2069613
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00453 0.00200 0.00400 0 113 75 125 0.00446 1.56 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range 1-1 Holding times for preparation or ana)
I Analyte detected below quantitation limits M Manual integration used to determine area response MC Value is below Minimum Compound
Original
ND Not Detected Q RSD is greater than RSDlimit P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 31

Su
m,
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EWII*OJAI NTAL TECHNOLOG;ES, INC
Ar?a(VOcP i_aboralCnas
Cuyahoga Falls. Ohio 44223
TEL: [phone] FAX: [phone]
WOE: 19041250
Website: htm:/hvwtv.settek.com
07-May-19
Client:
Synagro
Project:
Morehead City WWTP
BatchID: 36994
Sample ID 19041086-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 412212019
RunNo: 97344
Client ID: Batch=
Batch ID: 36994
TestNo: SW7470A SW7470A
Analysis Date: 412212019
SegNo: 2069613
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank
l Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
I Value above quantitation range H Holding times for preparation or anal)
M Manual integration used to determine area response MC Value is below' inimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 16 of 31

mi Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
EKV111014MENTAL TECHHOLOG; -5, - Cuyahoga Falls. Ohio 44223 WO#: 19041250
�rfafy[JcaFLar�rsY��l�� TEL: [phone] FAX: [phone]
Website: htin:lfivww.settek.cow 07-May-19
Client: Synagro
Project: Morehead City WWTP
BatchID: 37005A
Sample ID 19041088-001AMS
SampType: M5
TestCode:
TCLP-SVOC- Units: mg1L
Prep Date: 4/22/2019
RunNo: 97433
�;Iient ID: BatchQC
Batch ID: 37005A
TestNo:
SW8270
Analysis Date: 412412019
SegNo: 2092386
4nalyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.523
0.0800
0.8000
0
65.4
15.2
124
2,4,5-Trichiorophenol
0.601
0.200
0.8000
0
75.2
30.6
152
2,4,6-Trichiorophenol
0.656
0.200
0.8000
0
82.0
27.6
150
2,4-Dinitrotoluene
0.635
0.0400
0.8000
0
79.4
58
141
o-Cresol
0.644
0.200
0.8000
0
80.4
26.9
132
Cresols, Total
ND
4.00
1.600
0
77.3
27.6
132
Hexachloro-1,3-butadiene
0.543
0.0160
0.8000
0
67.9
-5.3
156
Hexachlorobenzene
0.626
0.0400
0.8000
0
78.2
54.3
142
Hexachloroethane
0.498
0.0800
0.8000
0
62.2
1.92
131
Nitrobenzene
0.654
0.0800
0.8000
0
81.8
21
135
PentachlorophenoI
0.463
0.200
0.8000
0
57.9
47.4
134
Pyridine
ND
0.200
0.8000
0
0
-10.3
64.2
Surr:2-Fluorophenol
0.623
1.000
62.3
9.77
146
Sum Phenol-d6
0.815
1.000
81.5
20.7
130
Surr: Nitrobenzene-d5
0.753
1.000
75.3
13.9
156
Surr:2,4,6-Ttibromophenol
0.693
1.000
69.3
27.3
183
Surr.2-Fluorobiphenyl
0.815
1.000
81.5
21.4
163
Sum p-Terpheryl-r114
1.02
1.000
102
54.8
154
m
QC+
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound Original
ND Not Detected O RSD is greater than RSDlirnit P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 17 of 31

M' • summit Environmental Technologies, Inc.
SU3310 Win St.
QC SUMMARY REPORT
EhVOONME rrA.L TECH' N01-Grir-S, INC
Cuyahoga Falls, Ohio 44223
wo#:
19041250
Asraiyflcai i abnfasorie5 TEL: [phone] FAX.- [phone]
Website: http://wivw.settekcom
07 May-1v
Client: Synagro
Project: Morehead City WWTP
BatchID: 37005A
Sample ID 19041088-001AMSD SampType: MSD
TestCode: TCLPSVOC_ Units:
m9111-
Prep Date:
4/2212019 RunNo: 97433
Client ID: Batch= Batch ID: 37005A
TestNo: SW8270
Analysis date:
4/24/2019 SegNe: 2092387
AnaIyte Result
PQL SPK value SPK Ref Val
%REC
LowLimit Highl-imit
RPD Ref Val %RPD RPDLimit Qua]
1,4-Dichlorobenzene 0.486
0.0800 0.8000
0
60.7
15.2
124
0.5228 7.38
30
2,4,5-Trichloraphenol 0.528
0.200 0.8000
0
66.0
30.6
152
0.6012 13.0
30 m
2,4,6-Trichlorophenol 0.580
0.200 0.8000
0
72.6
27.6
150
0.6560 12.2
30
2,4-Dinitrotoluene 0.579
0.0400 0.8000
0
72.4
58
141
0.6352 9.22
30
o-Cresol 0.617
0,200 0.8000
0
77.1
26.9
132
0.6436 4.25
30 QC+
Cresols, Total ND
4.00 1,600
0
72.2
27.6
132
0 0
30
Hexachlorc-1,3-butadiene 0.500
0.0160 0,8000
0
62.6
-5.3
156
0.5432 8.20
30
Hexachlorobenzene 0.551
0.0400 0.8000
0
68.9
54.3
142
0.6260 12.7
30
Hexachloroethane 0.448
0.0800 0.8000
0
56.0
1.92
131
0.4976 10.5
30
Nitrobenzene 0.569
0.0800 0.8000
0
71.1
21
135
0.6544 14.0
30
Pentachlorophenol 0,428
0.200 0.8000
0
53.5
47.4
134
0.4632 7.90
30
Pyridine ND
0.200 0.8000
0
0
-10.3
64.2
0 0
30
Sum 2-Fluorophenol 0.564
1.000
56.4
9.77
146
0
Surr: Phenol-d6 0.706
1,000
70.6
20.7
130
0
Surr: Nitrobenzene-d5 0.691
1.000
69.1
13.9
156
0
Surr:2,4,6-Tribromophenof 0.599
1.000
59.9
27.3
183
0
Surr:2-Fluorobiphenyl 0.742
1.000
74.2
21.4
153
0
Surr: p-Terphertyl-d14 0.895
1.000
89.5
54.8
154
0
Qualifiers: B Analyte detected in the associated Method Blank
B Value above quantitation
range
H
Holding times for preparation or anal;
J Analyte detected below quantitation Iimits
M Manuai Integration
used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
0 RSD is greater than
RSDlimit
P
Second column confirmation exceeds
PL Perinit Limit
R RPD outside accepted
recovery limits
RL
Reporting Detection Limit
Page 18 of 31

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIV 3310 Win St.
Eh;1�IFtaJdh1cN74L�EMHOL[Gi�_s. Cuyahoga Falls, Ohio 44223
WO#: 19041250
Anaij t cal LaHcrazorvs TEL: [phone] FAX.- [phone]
Website: http://ivwlv.settek.cam 07May-19
Client: Synagro
Project: Morehead City WWTP
BatchID: 37005A
Sample ID MB-37005
SampType: MBLK
TestCode: TCLP-SVOC_ Units: mg1L
Prep Date: 412212019
RunNo: 97396
client ID: PBS
Satch ID: 37005AA
TestNo: SW8270
Analysis date: 412312019
SegNo: 2073464
�ralyte
Result
POL SPK value SPK Ref Val
%REC LowLimit Highl-irnit RPD Ref Val
%RPD RPDLimit Qual
14-Dichiorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichlorophenol
ND
0.100
2,4-Dinitrotoluene
ND
0.0200
c-Cresol
ND
0.100
Cresols, Total
ND
2.00
Hexachlore-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0.100
Pyridine
ND
0.100
Surr: 2-Fluorophenal
0.549
Surr: Phenol-d6
0.645
Surr: Nitrobenzene-d5
0,540
Surr: 24,6-Tribromophencl
0.881
Surr: 2-Fluorobiphenyl
0.547
Surr: p-Terphenyl-d14
0,821
1.000
54.9
10
109
1.000
64.5
10
109
1.000
54.0
19
120
1.000
88.1
10
120
1.000
54.7
22
117
1.000
82.1
34
116
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana13
J Analyte detected below quantitation limits M Manual Integration used to detennine area response MC Value is below Minimum Compound
Original
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 31

lir
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summ3310 Win St.
EtiVJft0NMEt4TALT,ECHU0LGG1f-S, -- Cuyahoga Falls, Ohio44223
WO#: 14041250
A-"Wyrlca#iaberralivies TEL: [phone] FAX..- [phone]
Website: hup.-Ilwivw.seuckCom 07 May-19
Client: Synagro
Project: Morehead City WWTP BatchID: 37005A
Sample ID LCS-37005
SampType: LCS
TestCode: TCLP-SVOC_ Units: mglL
Prep Date: 412212019
RunNo: 97396
Client ID: LOSS
Batch ID: 37005A
TestNe: SW0270
Analysis Date: 4/2312019
SegNo: 2073466
Analyte
Result
PQL SPK value SPK Ref Val
%RFC LowLimit Highl-imit RPD Ref Val
°/%RPD RPDLimit Qual
1,4-❑ichlorobenzene
0.438
0.0400
0.8000
0
54.8
19.1
126
2,4,5-Trichlorophenel
0.632
0.100
0,8000
0
79.1
11.7
151
2,4,6-Trichlorophenel
0.614
0.100
0.8000
0
76.8
12.4
150
2,4-❑initrotoluene
0.648
0.0200
0.8000
0
81.0
20.6
140
0-Cresol
0.502
0.100
0,3000
0
62.7
13.8
137
Cresols, Total
ND
2.00
1.600
0
64.9
10
129
Hexachloro-1,3-butadiene
0.458
0.00800
0.8000
0
57.2
14.7
137
Hexachlorobenzene
0.598
0.0200
0.8000
0
74.7
12
139
Hexachloroethane
0.440
0.0400
0.8000
0
55.0
14.8
132
Nitrobenzene
0.472
U400
0.8000
0
59.0
15.6
138
Pentachlorophenol
0,682
0.100
0.8000
0
85.2
10
156
Pyridine
ND
0.100
0.8000
0
9.83
1
130
Surr. 2-Fluorophenol
0.539
1.000
53.9
1 D
147
Surr: Phenol-d6
0.631
1.000
63.1
10
140
Surr: Nitrobenzene-d5
0.558
1.000
55.8
10
169
Surr: 2,4,6-Tribromophenol
0.837
1.000
83.7
10
185
Surr: 2--Fluoroblphenyl
0.580
1.000
58.0
10
169
Surr: p-Terphenyl-d14
0.799
1.000
79.9
10
179
m
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 20 of 31

SUMM1vt
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
E�iV[r?O1J1dEtdTALTEC9iKCL.��Gr=_;,"--
Anafyrlca✓' Labor dories
Cuyahoga Falls, Ohio44773
TEL: [phone] FAX: [phone]
WO#= 19041250
Website: htm:/hvww-settek.com
07-May-I9
Client:
Synagro
Project:
Morehead City WWTP
BatchID: 37045
2,4-D ND 0.0100 0 0
2,4,5-TP ND 0.00500 0 0
Surr: DCAA 361 500.0 72.2 20 140
2,4-D
0.515 0.0100
0.500
0 103
43.8
130
2,4,5-TP
0.576 0.00500
0,500
0 115
51.5
133
Surr: DCAA
488
500.0
97.6
34.2
150
2,4-D
0.448 0.0100
0.500 0 89.6 37
130
2,4,5-TP
0.496 0.00500
0.500 0 99.2 38
130
Surr: DCAA
473
500.0 94.6 20
140
Qualifiers:
B
Analyte detected in the associated Method Blank
E
VaIue above quantitation range
H
HoIding times for preparation or anal;
J
AnaIyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 21 of 31

Summit Environmenial Technologies, Inc. QC SUMMARY "PORT
SUMMINt 3310 Win St.
EN4rlrtONNIENTAL TECHNbL. -�1�S, INC. Cuyahoga Fails, Ohio 44223
WO#: 19041250
Anatyticaf Labcrataraee TEL: [phone] FAX: [phone]
Website: httn://wivw.settelccom 07-MaV-19
Client: Synagro
Project: Morehead City WWTA BatchlD: 37045
Sample ID 19041120-005amsd
SampType: MSD
TestCode: tclpSVOC-H Units: mg1L
Prep Date: 4124/2019
RunNo: 97649
Client ID: BatchQC
Batch ID: 37045
TestNo: SW8151A SW8151A
Analysis Date: 412912019
SegNo: 2091033
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.537 0.0100 0.500 0 107 37 130 0.448 18.0 30
2,4,5-TP 0.603 0.00500 0.500 0 121 38 130 0.496 19.5 30
Surr: DCAA 357 500.0 71.3 20 140 0
Qualifiers: B Analyte detected in the associated Method Blank B Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 22 of 31

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIMt 3310 Win St.
tr,;VIltOtdtoe:r,rAL TECH aOWGI=S,:PJr: Cuyahoga Falls, Ohio44223
WO#: 19041250
ArifP(vucal Labcrmordo-f TEL: [phone] FAX: [phone]
Website: http://ivwiv.settek.com 07-May-19
Client: Synagro
Project: Morehead City WWTP BatchlD: R97449
Sample ID 19041237-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 97449
Client ID: SatchQC
Batch ID: R97449
TestNo: SW9014
Analysis Date: 4/22/2019
SegNo: 2073899
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RP❑ RPDLimit Qual
Cyanide, Reactive 9.00 0.495 10.00 0.09317 89.1 81.6 122
Sample ID 19041237-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 97449
Client ID: BatchQC
Batch ID: R97449
TestNo: SW9014
Analysis Date: 4/2212019
SegNo: 2073900
Analyte
Result
PQL SPK value SPK Ref Val
%RI=C Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.12 0.485 10.00 0.09317 90.3 81.6 122 9.003 1.29 5
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H HoIding times for preparation or anal;
1 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
m
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 23 of 31

SUMMI't
Summit Environmental Technologies, Inc.
3310 Win St.
PORT
QC SUMMARY Tl �T REPORT
1[ l 7 V 1.1L►lc`]1\ i R P. l
ERVIROWFtiENTAL TECN¢dOWGIPS, ONG Cuyahoga Falls, Ohio 44223
Arral rt1C,21 Lab TEL: [phone] FAX.- [phone]
WO#: 19041250
Website: http://wivw.sette.k.com
07-may-19
Client:
Synagro
Project:
Morehead City WWTP
BatchID: R97449
Sample ID Blank
SampType: MBLK
TestCode: Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 97449
Client ID: PBW
Batch ID: R97449
TestNo: SW9014
Analysis Date: 412212019
SegNo: 2073884
Analyte
Result
PQL SPK value SPK Ref Val
%RFC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive ND 0.485
Sample ID LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mglL
Prep Date:
RunNc: 97449
Client ID: LCSW
Batch ID: R97449
TestNo: SW9014
Analysis Date: 4/2212019
SegNo: 2073885
Analyte
Result
PQL SPK value SPK Ref Val
%RFC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.68 0.495 10.00 0 96.8 85 115
Sample ID RLCheck
SampType: RLC
TestCode: Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 97449
Client ID: BatchQC
Batch ID: R97449
TestNo: SW9014
Analysis Date: 412212019
SegNo: 2073887
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
ND 0.490 0.5000 0 93.1 50 150
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
] Analyte detected below quantitation limits M Manual Integration used to detennirie area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 24 of 31

M�� Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
Et4Vlit0ldMa WALTEGHN01.aai=9,'r.,7 Cuyahoga Falls, Rhto44223
Anaiyrilca1 Laboratone= TEL: [phone] FAX.- [phone] WO#: 191}41250
Website: hQ,11www.settekcom 07-May-19
Client: Synagro
Project: Morehead City WWTP BatchID: R97455
Sample ID 19041237-001AMSD
SampType: MSD
TestCode:
Sulfide,React Units: mg1Kg
Prep Date:
RunNo: 97455
Client ID: Batch=
Batch ID: R97455
TestNo:
SW9034
Analysis Date: 4124/2019
SegNo: 2074127
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4140 25.0 4800 0 86.2 80 120 4220 1.91 30
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal;
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected d RSD is greater than RSDlimconfirmation it P Second column conrmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 25 of 31

IT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
et-VlftOtJMr:NTAL TEC4NOtn, rl5!3, mt(` Cuyahoga Falls, Ohio 4422.3
WO#: 19041250
Anatyifcal laboraremw TEL: [phone] FAX.- [phone]
Website: httn://www.settekcom 07-May-I9
Client: Synagro
Project: Morehead City WWTP BatchlD: R97455
Sample I❑ MB-R97455
SampType: MBLK
TestCode: Sulfide,React Units: mg1L
Prep Date:
RunNo: 97455
Client ID: PBW
Batch ID: R97455
TestNo: SW9034
Analysis Date: 4/24/2019
SegNo: 2074114
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Va]
%RPD RPDLimit Qua[
Sulfide, Reactive ND 25.0
Sample ID LCS-R97455
SampType: LCS
TestCode: Sulfide,React Units: mg]L
Prep Date:
RunNo: 97455
Client ID: LCSW
Batch ID: R97455
TestNo: SW9034
Analysis Date: 4124/2019
SegNo: 2074115
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4670 25.0 4800 0 97.3 85 115
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 26 of 31

SUMMIT
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
Eh V1rk0S,lrs FNTAL TECHNOLOCI=S, WrF Cuyahoga Falls, Ohio 44223
WO#: 19041250
A naiytleal Laborarono� TEL: [phone] FAX.- [phone]
Website: htm://wrvw.swek.com 07-May-19
Client: Synagro
Project: Morehead City WWTP SatchlD: R97577
Sample ID LCS-R97577
SampType: LCS
TestCode: lgnitability_S Units:
Prep Date:
RunNo: 97577
Client ID: LCSS
Batch ID: R97577
TestNo: SW1030
Analysis Date: 4/26/2019
SegNc: 2078506
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 7.e6 7.240 0 106 70 130
Sample ID 19041250-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNc: 97577
Client ID: MC19
Batch ID: R97577
TestNo: SW1030
Analysis Date: 4126/2019
SegNa: 2078508
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability non-flammable 0 0 20
Sample ID 19041252-001ADUP
SampType: DUP
TestCode: Ignitabi[ity_S Units:
Prep Date:
RunNo: 97577
Client ID: BatchQC
Batch ID: R97577
TestNo: SW1030
Anaiysis Date: 412612019
SegNo: 2078510
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19041399-006ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 97577
Client ID: BatchQC
Batch ID: R97577
TestNo: SW1030
Analysis Date: 412612019
SegNo: 2070512
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 6.90 7.750 11.6 20
Qualifiers: D Analyte detected in the associated Method Blank E Value above quantitation range ld Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 27 of 31

. summill Summit Environmental Technologies, lrrc. QC SUMMARY REPORT
3310 Win St.
EXelilONP 5t,JTALTeC2?1,Tol.r r7=S, INC Cuyahoga Falls, Ohio 44223
WO#: 19041250
A aiplcarf Labc:raton,,s TEL: [phone] FAX: [phone]
Website: htty://rviv)v.settek.com 07-Mav-19
Client: Synagro
Project: Morehead City WWTP BatchlD: R97577
Sample ID 19041399-006ADUP
SampType: DUP
TestCode: lgnitability_S Units:
Prep Date:
RunNc: 97577
lient ID: BatchQC
Batch ID: R97577
TestNo: SW1030
Analysis Date: 412612019
SegNo: 2078512
�nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 19041399-000ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 97577
,Gent ID: BatchQC
Batch ID: R97577
TestNo: SW1030
Analysis Date: 412612019
SegNO: 2078513
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 3.62 7.750 72.6 20 R
Qualifiers: S Analyte detected in the associated Method Blanlc E Value above quantitation range H Holding times for preparation or anal}
3 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds �ilglrial
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 28 of 31

UM
'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
E k'll' +W?.1EP1TAL fi ltni�]LC�G1 ,'fit=^ Cuyahoga Falls, Ohio 44223
WO#: 19041250
Arrjfyr.' VP L'2;7Crralorias TEL: [phone] FAX: [phone]
We&site: htt ://ivww.settek.com 07-Merv-19
Client: Synagro
Project: Morehead City NVWTP SatchlD: R97808
Sample ID LCS-R97808
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@,21.2C
Prep Date:
RunNo: 97808
Client ID: LCSW
Batch ID: R97808
TestNo: SW9045D
Analysis Date: 51212019
SegNo: 2087733
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH TO 7.0 0 100 90 110
Sample ID 19050025-001ADUP
SampType: PUP
TestCode: pH_011(9045 Units: s.u.@22.00
Prep Date:
RunNo: 97808
Client ID: BatchQC
Batch ID: R97808
TestNo: SW9045D
Analysis Date: 5/2/2019
SegNo: 2087735
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 6.4 0 0 6.4 0.3 10
Sample ID CHECK 7
SampType: LCS
TestCode: PH_O[L(9045 Units: s.u.@21.00
Prep Date:
RunNo: 97808
Client ID: LCSW
Batch ID: R97808
TestNo: SW9045D
Analysis Date: 51212019
SegNo: 2087765
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0
7.0 0 100 90 110
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for pfeparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDhmit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 29 of 31

Summit Environmental TechnoloInc. In
MODOU Analvsis Reauest/Chain of Custody
Heim uislied In: C►atc -- I sl.od UL SJLA117;U
Rom! ved by:
jDTCOMVIJANCU YEs NO
CIERTMCATION REOUIRLD Y U"'
Rumi-ro s rAn (r)w ONL YUS,
Ir v, picase Print PWS, STU. MI
_,,,
'FFMe NI I'a he approyw
Received in Lab by: [lairlimeRequested BY: Woag�- Ilk w: jw DW (—R, to W.,
Oq Thc chfil rMnims It,c P;IA �Qgz w tho bhoratory 434
Page 30 of 31

Summit Environmental Technologies, Lsc.
SUMMIT3310 ff"in St.
FERVIItoNMENTAL MGHN010411139, INC CuyahoguFalls, Ohio44223 Sample Log -In Check List
d,R,tlyvoal tabIralones TFL: [phone] FAX: [phone]
Website: blip://ttriiii.serrek.cons
Client Name: SYN-NC-27028 Work Order Number: 19041250 RcptNo: 1
Logged by: Jesseca E. Westfall
Completed By: Jesseca E. Westfall
Reviewed By: Jonnifor Woolf
Chain of Custody
1. Is Chain of Custody complete?
2_ How was the sample delivered?
Loq In
3. Coolers are present?
4/1812019 9:55:00 AM
4/18/2019 1:05:15 PM
411912019 1,10:64 PM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Sea[ Date:
5, Was an attempt made to cool the samples?
6, Were all samples received at a temperature of >0° C to 6.0°C
7_ Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
g. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. fs the headspace in the VOA vials less than 114 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14 Are matrices corfectiy identified on Chain of Custody?
15, Is it clear what analyses were requested?
16. Were ali holding times able to be met?
(If no. notify customer for authorization.)
Special Han_dAng ff applicable
17. Was client notified of all discrepancies with this order?
Yes ❑�
UPS
Yes ❑d
Yes 0
Yes ❑
Signed By:
Yes ❑�/
Yes �/❑
Yes ❑�
Yes
Yes
Yes ❑
Yes ❑
Yes ❑
Yes (✓I
Yes
Yes ❑�
Yes
No ❑ Not Present ❑
No ❑ NA ❑
No ❑
No ❑ Not Present
No ❑ NA ❑
No ❑ NA ❑
No ❑
No ❑
No ❑
No W NA ❑
No ❑ No VOA Vials❑
No e❑
No ❑
No ❑
No ❑
No ❑
No ❑ NA ❑�
Person Notified: Date 1
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Yes ❑
Cooler No Temp °C Condition I Seal Intact I Seal No Seal Date Signed By
J 4.9 Good, Not Presentl
Page 31 of 31

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period
Town of Morehead City WQ Permit Number: WQ0006018
Town of Morehead City WWTP NPDES Number: NCO026611
From 01/01/19 To 12/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt..2/B (Alk Treatment) Alt. 31C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) 'indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If—lirahlP to alternative nerfnrmerl (Gins A nr Chas Rl rmmnlete the fallnwinn mnnitnrinu data!
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 611,
MPN
12300
26237
50300
CFU/g
0
Annually
Grab
9222D
Coliform
power per gram
of total solids
MPN
I000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying— Stable) (Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation) X
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 I06 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met," (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been trade under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information use etermine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are siq�,ena/les Xr f e certification including fine and imprisonment."
Daniel Williams Publi es Director G Todd Larson, O erations Di ector
Prepay a e and Ile pe or i !Land:A��ppljer d 1 f tic 1 print)
Signature of Preparcr* Date Signature of La Applier (if app ' able) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 IO2 (26)

Cameron Testing Services, Inc. Laboratory Report
NC DENR #654
NC PHHS #37799
US EPA4NCO1918
190644
Yes
J. Zubeck 04/04119
190644 MCI
Sludge Gr Fec. Coliform-S 17900
CFulg
5990 04/05/19 SB 9222D - NIF
MC2
24700
CFu19
6170
MC3
37500
CFurg
6250
MC4
20400
Mig
5710
MC5
40900
uulg
5850
MC6
12300
CFur9
6170
MC7
50300
CFur9
6290
Geomean 26237
190644 MC1
Sludge Gr TS (°/a) 16.7%
0.01 04/05/19 SB 2540 G7 -TS
MC2
16.2%
0.01
MC3
16.0%
0.01
MC4
19.6%
0.01
MC5
17.1 %
0.01
MC6
162%
0.01
MC7
15.9%
0.01
Report '
Review _-_..I"q
Project Manageraati,
219 S. Steele Str. 919-208-4240
Sanford NC 27330 [e-mail]

Pro e t
2ZY,&
Samp�
Name:
t
.
Col�eci „
Signature:
Sap�p'Ie>Inforination
,,,E , Number. of bottles �.. preservafirre ....,,
:,
Client Sample
�,
j z
� 0 �
Pry
ID
j 00 IUI
T ; m '
0
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Rush work will require prior approval. Additional charges will apply

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project; Morehead City, NC
IlField Soil II Dime Requirement II Tons/Acre II Date Applied II
(state -count -site -field) j off (tons/acre) [ Anolled
NC-CR-01-02 1 5.3 1.0 0.0 nla
NC-CR-07-2 1 5.0 1.0 0.0 n/a
Lime to be applied beofore next haul

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.govlagronomil
Report No. FY19-SL019500
Client: Bobby Riggs
Advisor: Shane (Stephen) Sykes
Predictive
483 Weatherington Landing Rd
Nutrien Ag Solutions
Stella, NC 28582
372 Hwy 58 South PO
Soil Report
Mehlich-3 Extraction
sox 658
Sampled County: Onslow
Trenton, NC 28585
a tIlth' k
Links to Helpful Information
Client ID: 467267
Advisor ID: 403805
Sampled: 12/12/2018 Received: 12/13/2018 Completed: 01/23/2019 Farm: RJ 0
Sample ID: 1
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tonslacre) N P2O5
K2O Mg S Mn
Zn
Cu B
Information
Lime History:
1-Soybean
0.8 0 0
90 0 0 0
0
0 0
Note: 3
2 -
0.0
Test Results [units - WN in glcm3; CEC and Na in meg1100
cm3; NO3-N in mgldm3l:
Soil Class: Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1 Ca% Mg% S-1
Mn-1 Mn-All Mn-Al2 Zn-1
Zn-Al
Cu-1 Na ESP SS-1 NO3-N
0.81 1.28
3.7 58 1.5 5.4
125 25 43 12 51
52 41 130
130
93 0.2 6
Sample 1D: 2
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tonslacre) N P2O5
K2O Mg S Mn
Zn
Cu B
Information
Lime History:
1-Soybean
1.0 0 0
90 0 0 0
0
0 0
Note: 3
2 -
0.0
Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3j;
Soil Class: Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1 Ca% Mg% S-1
Mn-1 Mn-All Mn-Al2 Zn-I
Zn-Al
Cu-1 Na ESP SS-1 NO3-N
1.19 1.28
4.0 53 1.9 5.3
119 26 39 11 55
42 35 92
92
128 0.2 5
N
orth Carolina
folytt,_' Tani t F12-1,A Cmmmw ion
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY19-SLO19500
Bobby Riggs
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib11000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
copper index
ESP
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
Mn-All
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-o
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib11000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr..gov/agronomilobpart4.htm s�ind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
Zn-AI
zinc availability indexM%,
The first seven values [soil class, HWN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-I
zinc index
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-[, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-I, S-1, SS-1, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov1a ronomi1uyrst.htm

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomc
Report No.
FY20-SL001712
:r.
Client:
Bobby Riggs
Advisor:
I Predictive
Landing Weatherin ton 483 Rd
9 g
'V Mehlich-3
Extraction
Stella, NC 28582
�1r oil Report
S
Sampled County: Carteret
w�
Links to Helpful Information
Client ID: 467267
Advisor ID:
Sampled: Received: 08/02/2019 completed: 08/12/2019
Farm:
Sample ID: 01-3A
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1-Soybean 0.4
0 0
100
0 0 0
0
0 0
Note: 3
2 -Corn, grain 0.0
120 - 160 0
100
0 0 0
0
0 0
Note: 3
Test Results [units - W/V in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldrrl3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
1.14 1.31 4.5 73 1.2 5.7 194 20
56 14
45
62
47 54 282
282
265 0.1
2
Sample ID: 07-02
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1-Soybean 1.0
0 0
80
25 0 0
0
0 0
Note: 3
2--Corn, grain 0.0
120- 160 0
80
$ 0 0
0
0 0
Note: 3 Note:
Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldM3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-Al
Cu-I Na ESP
SS-1 NO3-N
0.66 1.36 3.6 57 1.6 5.0 385 28
47 6
38
88
63 70 261
261
498 0.1
3
North Caroling
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.govlagronomil
Report No. FY20--SL001712
Bobby Riggs
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MC is recommended and lime is needed, use dolomitric lime.
Cu-1
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-1
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to Note: Secondary Nutrients and Micronutdents In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
0RG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib11000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncaar.c7ovlayronomiloboart4.htmlllsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P20s
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-Al
Zn-I
zinc availability index
zinc index
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncacir.vovlapronomiluyrst.htm