WQ0014885_Residual Annual Report 2019_20200302

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0014885
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0014885
Applicant\Permittee * SYNAGRO
Facility Name * Harnett WTP Class A Residuals
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for Harnett WTP Class A Residuals
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
HARNETT WTP NC 2019 Annual Report FINAL.pdf 13.61 MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/27/2020

435 Williams Court, Suite 100
Baltimore, NID 21220
wwwsyinagro.coin
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0014885
Dear NCDEQ:
Enclosed are one copy and one electronic copy of the above referenced report on behalf of
Harnett WTP Class A Residuals under Permit No. WQ0014885.
If you have any questions or comments, please contact Steve Ward at [phone] or Melinda
Boyd at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Steve Ward, Harnett County
Melinda Boyd, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

HARNETT COUNTY WTP, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0014885
2019 ANNUAL REPORT

Harnett County WTP, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WQ0014885 County Harnett Year 2019
Facility Name (as shown on permit) Harnett County Utilities Regional WTP PW S 1D No. 00-076-84
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part Band proceed to Part C. Also, if residuals were generated but not Iand applied,
please attach an explanation on how the residuals were handled.
Part A -- Residuals Application SummM:
Total number of application fields in the permit: NIA
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 515.91
Total number of acres utilized for land application during the year: 106.3
Part B — Annual Comt}liance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
Iimit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4, Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC. 02T . 1105(a) or the Pollutant Loading
Rates in I5A NCAC 02T . 1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1 I 11 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were. complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations,
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit,
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and b,07f, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the po i ity of fines and imprisonment for
knowing violations."
Steve Ward Director of Public Utiliti
ape or Signatin Per ittee Date
/-av �(OLe
gature of Pre er* Date Sig e Date
(if different fr m Permittee) (if different fro P e and arer}
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
HARNETT CO. UTILITIES, NC
HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
DRY METRIC
MONTHNEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
January 2019
1,010,600.00
G
81.33
D
73.78
February 2019
942,400.00
G
75.85
D
68.80
March 2019
892,800.00
G
71.85
D
65.18
April 2019
1, 016, 800.00
G
106.85
D
96.92
May 2019
861,800.00
G
90.56
D
82.13
June 2019
601,400.00
G
12.14
D
11.02
July 2019
489,800.00
G
9.89
D
8.97
August 2019
607,600.00
G
12.26
D
11.12
September 2019
471,200.00
G
9.52
D
8.62
October 2019
973,400.00
G
19.65
D
17.82
November 2019
520,800.00
G
10.50
D
9.53
December 2019
768,800,00
G
15.51
D
14.08
YEARLY TOTAL.
9,157,400.00
G
515.91
D
467.97
2/6/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014885
Facility Name: HARNETT CO. UTILITIES, NC
NPDES# : NCO007684
or WQ# (residual only)
WWTP Name: COH REGIONAL WTP
Residuals Analysis Data
Product Type WPL WPL WPL
Date Sampled (grab) or 02/12/19 04/26/19 09/10/19
Date Composited
Percent Solids 1.93 2.52 0.24
PARAMETERS (mglkg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
Laboratory
Waypoint Analytical Virginia Inc.
SHEALY ENVIRONMENTAL SERVICES INC.
WPL
10/03/19
0.484
6.45
6.8
17.6
32
<1
<1
<1.99
<4.2
0.0559
0.062
0.0685
<3.8
27.9
30.7
11.9
19
320
190
219
210
7.42
15.2
10.8
<15
4.05
<2.5
16.2
74
10
12.8
8.35
<35
<5
<5
<9.94
<27
45.5
54.1
37.8
43
1570
1640
2360
2100
40000
12400
165000
26000
<100
4800
<100
<110
<4.84
<4.9
3480
170
"I certify, under penalty of law, that this document was prepared u
designed to assure that qualified personnel properly gathered anc
significant p r
mir e inf inc[udin
r
X
GNATURE OF PREPARE
my direction or supervision in accordance with a system
uated the information submitted. I am aware that there are
ibility of fines and imprisonment for knowing violations."
Date � / r 02_0
DENR FORM RSSF (512003) Printed: Saturday - February 1 2020 at 15:54:47 for: 2037 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0014885
Facility Name: HARNETT CO. UTILITIES, NC
NPDES# : NCO007684
or WQ# (residual only)
WWTP Name: CON REGIONAL WTP
Residuals Analysis Data
Product Type WPL WPL WPL
Date Sampled (grab) or 02/12/19 04/26/19 09/10/19
Date Composited
Percent Solids 1.93 2.52 0.24
PARAMETERS (mgfkg dry weight)
Laboratory
Waypoint Analytical Virginia Inc.
SHEALY ENVIRONMENTAL SERVICES INC.
WPL
10/03/19
0.484
Aluminum
134000
101000
150000
20 00 00
Calcium
552
734
2290
2200
Magnesium
888
1260
922
<2100
pH
5.30
5.80
5.30
5.30
Potassium
429
621
660
2900
Sodium
308
317
954
3600
"I certify, under penalty of law, that this document was prepared under myection or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluafd the information submitted. I am aware that there are
significant pe 4"i— f r s mittWalals�inf�m n, including the possi pity of fines and imprisonment for knowing violations."
X
TURE OF PREPARER)
NR - Data Not Reported or Doa Not Required
Date r� �( F 0-12-0
DENR FORM RSSF-B (7/2002) Printed: Saturday- February 1, 2020 at 15:56:07 for: 2037 01

WayPAaint. a
NALYTICAL
2/22/2019
Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-045-0203
Project Description: HWTP 19 #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypointanalyNcal.com
Dear Mary Brewer;
Waypoint Analytical Virginia, Inc. received sample(s) on 2/14/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam• W 611117�
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZO629 Pennsylvania 68-03109 Virginia 460014
South Carolina 93007
New Jersey VA011
Florida E871087
North Carolina 257
Page 1 of 6

Waypoint(l)
ANALYTICAL
Report Number: 19-045-0203
Client Project Description: HWTP 19 #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
64802
HWTP 19 #1
Solids
02/12/2019 11:20
(12/14/2019
64802
HWTP 19 41
Solids
02/12/2019 11:20
02/14/2019
SM-4500-NH3C
WTN
64802
HWTP 19 #1
Solids
02/12/2019 11:20
02/14/2019
9045D
WTN
64802
HWTP 19 #1
Solids
02/12/2019 11:20
02/14/2019
4500NO3F-2011
WTN
64802
HWTP 19 #1
Solids
02/12/2019 11:20
02/14/2019
6010D
WTN
64802
HWTP 19 #1
Solids
02/12/2019 11:20
02/14/2019
SW-7471B
WTN
64802
HWTP 19 #1
Solids
02/12/2019 11:20
02/14/2019
SM-4500-NH3C-TKN
WTN
64802
HWTP 19 #1
Solids
02/12/2019 11:20
02/14/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certifcation: #1354
Page 2 of 6

Report Number: 19-045-0203
Account Number: 46460
Send To: Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville , NC 27028
Lab Number: 64802
Sample Id : HWTP 19 #1
Waypoint(2)
ANALYTICAL
Project: HWTP 19 #1
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Date Sampled: 2/12/2019 11:20:00
Date Received: 02/14/2019 00:00
Date Reported: 02/22/2019
Total Solids *
1.93
19300
100.0
CJR
02/18/2019 13:58
SM-254OG
Moisture *
98.10
100.0
CJR
02/18/2019 13:58
SM-254OG
Total Kjeldahl Nitrogen
4.00
40000
250
CLP
02/20/2019 09:30
SM-4500-NH3C-TKN
Phosphorus
0.16
1570
50.0
KKM
02/19/2019 21:37
6010D
Potassium
0.04
429
50.0
KKM
02/19/2019 21:37
6010D
Sulfur
1.50
15000
50.0
KKM
02119/2019 21:37
6010D
Calcium
0.06
552
250
KKM
02/1912019 21:37
6010D
Magnesium
0.09
888
50.0
KKM
02119/2019 21:37
6010D
Sodium
0.03
308
250
JTR
02/201201919:34
6010D
Iron
29300
50.0
KKM
02/19/2019 21:37
6010D
Aluminum
134000
500
JTR
02/22/2019 05:35
6010D
Manganese
553
5.00
KKM
02/19/2019 21:37
6010D
Copper
320
2.50
KKM
02/19/2019 21:37
6010D
Zinc
45.5
12.5
KKM
02/19/2019 21:37
6010D
Ammonia Nitrogen
<0.01
<100
100
ZBD
02/20/2019 09:00
SM-4500-NI3C
Organic N
4.00
40000
250
02/20/2019 09:00
CALCULATION
Nitrate+Nitrite-N
<4.84
4.84
ZBD
02/18/201914:00
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time pwiG P 6ewr
Our reports and fetters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results. or the company in any advertising, news release. cr other public announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number: 19-045-0203
Account Number: 46460
Send To: Synagro Central LLCI Harnett
Mary Brewer
County
284 Boger Road
Mocksville , NC 27028
Lab Number: 64802
Sample Id : HWTP 19 #1
Waypoint(2)
ANALYTICAL
Project: HWTP 19 #1
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Date Sampled: 2/12/2019 11:20:00
Date Received: 02/14/2019 00:00
Date Reported: 0212212019
Cadmium
<1.00
1.00
KKM
02/19/2019 21:37
6010D
Chromium
27.9
2.50
KKM
02/19/2019 21:37
6010D
Nickel
10.0
2.50
KKM
02/19/2019 21:37
6010D
Lead
7.42
3.00
KKM
0211912019 21:37
6010D
Arsenic
6.45
5.00
KKM
0211912019 21:37
601 OD
Mercury
0.0559
0.0146
TJs
02/19/2019 13:48
SW-7471 B
Selenium
<5.00
5.00
KKM
0211912019 21:37
601 OD
pH*
5.3
JSL
02/20/2019 08:05
9045D
Molybdenum
4.05
2.50
KKM
0211912019 21:37
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Anaiyte detected in blank H - Beyond Holding Time
Our reports and letters are for the erciusrve and conPdentiai use of our clients, and may not be reproduced in whole or part. nor may any reference be made
to the work. the results, or t!?e compony in any advertising, news release, or other public announcements without obtaining our prior written authorization.
rGwftG #1 V6~1
Pauric McGroary
Agronomist
Page 4 of 6

Waypoint.Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46460
Customer Name: Synagro Central LLC/ Harnett
Report Number: 19-045-0203
Shipping Method
Fed Ex 0 US Postal (D Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping containerlcooler uncompromised?
0 Yes
0 No
Number of coolers received
�1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
Yes
No
COC properly completed
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
(—j No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
• NIA
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
No
Comments:
Signature: !Morgan Tichacek I Date & Time: 02/14/2019 13:12:11
Page 5 of 6

SAMPLING LOG #
CUSTOMER: SYNAGRO
IIII#I#I###ll#III#i1#[IIII#III#Illl#Illlllll##I ;9�
Svm cf- Central LLC! Hamett o
HWTP 19 *1 13:11:10
PROJECT MANAGER:
Phone: (�t� ;1Vjc�~
.ASS, IBC. CHAUN OF CUSTO®v
RECORD & ANALYSES
RECORD
1 attest that the proper field sampling procedures
were used during the collection of these samples.
SAMPLER
A & L CUSTOMER
SAMPLING
SAMPLE
# OF
SAMPLING
METHOD
METHOD
LAB 4 SAMPLE I.D.
LOCATION
TYPE
CONTAINERS
DATE TIME
PRESERVED
SHIPPED
Relinquisher! by Sampler:
Date Tme
Recieved by:
REMARKS:
Relinquished by:
bate Time
Recieved by,
Relinquished by:
Date Time
Recieved by:
SPECIAL INSTRUCTIONS:
For `-
fCT.lT�
1
monitoring purposes,
Pot :
S:AMPL E
AW,-L;�SIS REQUEST
).D.
j
e-,.
SLI SL!
NH.,-N1IVC3
l
NIl]rgNnl
3
!
Cd Cr
Nt
Pb As
1
Hg
Se
PIS
C�t'O
equiv.
Volatile
Solids
Mo.
CI
NO2-N
SLI: Totai Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL 2: Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 2112/2019 111/2019-3/3112019 0.2610
WTP LIQUID
Na mgll = (Na mg/kg x % Solids) + 100 = (308 x 1.9300) + 100 = 5.9444
Ca mg/1 = (Ca mg/kg x % Solids) + 100 = (552 x 1.9300) + 100 = 10.6536
Mg mgll = (mg mglkg x % Solids) + 100 = (888 x 1.9300) + 100 = 17.1384
Na meq = Na mg/l + Molec. Wgt.Na = 5.9444 + 23 = 0.258452
Ca meq = Ca mgll Molec.Wgt.Ca = 10.6536 + 20 = 0.53268
Mg meq = Mg mgll + Molec.Wgt.Mg = 17.1384 + 12 = 1.4282
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.258452.+ SgrRoot[0.5(0.53268+1.4282)] = 0.261018
Printed: 2/1/2020
Page 1 15:57

WayPAoint.. 6
NALYTICAL
5/9/2019
Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-121-1028
Project Descriptlon: Harnett WTP 2 of 4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www,waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/1/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
? r. to 6��
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 8

(2)
Waypoint.
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL_
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-121-1028
Client Project
Description: Harnett WTP
2 of 4
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
66128
Harnett WTP 2 of 4
Solids
04/26/2019 14:15
05/01/2019
66128
Harnett WTP 2 of 4
Solids
04/26/2019 14:15
05/01/2019
SM-4500--NH3C
WTN
66128
Harnett WTP 2 of 4
Solids
04/26/2019 14:15
05/01/2019
9045D
Writ/
66128
Harnett WTP 2 of 4
Solids
04/26/2019 14:15
05/01/2019
45DDNO3F-2011
WTN
66128
Harnett WTP 2 of 4
Solids
04/26/2019 14:15
05/01/2019
6010D
WTN
66128
Harnett WTP 2 of
Solids
04/z6/2019 14:15
05/01/2019
SW-74716
WTN
66128
Harnett WTP 2 of 4
Solids
04/26/2019 14:15
05/01/2019
SM-4500-NH3C-TI<N
WTN
66128
Harnett WTP 2 of 4
Solids
04/26/2019 14:15
D5/01/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number: 19-121-1028
Account Number: 46460
Send To: Synagro Central LLCI Harnett
Mary Brewer
County
284 Boger Road
Mocksville , NC 27028
Lab Number: 66128
Sample Id : Harnett WTP 2 of 4
r
Waypoin(2t.M
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Harnett WTP 2 of 4
REPORT OFANALYSIS Date Sampled: 4/26/2019 14:15:00
Date Received: 05/01/2019 00:00
Date Reported: 05/09/2019
Total Solids *
2.52
25200
100.0
ADM
05/02/2019 15:52
SM-2540G
Moisture *
97.50
100.0
ADM
05/02/2019 15:52
SM-2540G
Total Keldahl Nitrogen
1.24
12400
250
JPJ
05/08/2019 14:30
SM-4500-NH3C-TKN
Phosphorus
0.16
1640
50.0
BKN
051061201918:46
6010D
Potassium
0.06
621
50,0
BKN
051061201918:46
6010D
Sulfur
0.94
9430
50.0
BKN
0510612019 18:46
6010D
Calcium
0.07
734
250
BKN
05106/201918:46
6010D
Magnesium
0,13
1260
50.0
BKN
05106/201918:46
6010D
Sodium
0.03
317
250
BKN
051061201918:46
6010D
Iron
27600
50.0
BKN
05/061201918A6
6010D
Aluminum
101000
500
BKN
05/07/201911:36
6010D
Manganese
768
5.00
BKN
05106/201918:46
6010D
Copper
190
2.50
BKN
051061201918:46
6010D
Zinc
54.1
12.5
BKN
05/06/201918:46
6010D
Ammonia Nitrogen
0.48
4800
100
JPJ
05/08/2019 10:30
SM-4500-NH3C
Organic N
0.76
7600
250
05/08/2019 10:30
CALCULATION
Nitrate+Nitrite-N
<4.90
4.90
ZBD
05/071201913:28
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. .� //
B-Analyte detected in blank H - Beyond Holding Time ?W, r- P 6ew
OLlr reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part. nor may any reference be made Pauric McGroary
to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number. 19-121-1028
Account Number: 46460
Send To: Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville , NC 27028
Lab Number: 66128
Sample Id : Harnett WTP 2 of 4
Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Harnett WTP 2 of 4
REPORT OF ANALYSIS date Sampled: 4/26/2019 14:15:00
Date Received: 05/01/2019 00:00
Date Reported: 05/09/2019
Cadmium
<1.00
1.00
BKN
05/06/201918:46
6010D
Chromium
30.7
2.50
BKN
05/061201918:46
601OD
Nickel
12.8
2.50
BKN
05/061201918:46
601OD
Lead
15.2
3.00
BKN
05/06/201918:46
601OD
Arsenic
6.80
5,00
BKN
05/06/201918:46
601OD
Mercury
0,0620
0.0158
TJS
05/06/201912:22
SW-7471B
Selenium
<5.00
5.00
BKN
05106/201918:46
6010D
pH *
5.8
JSL
05/07/2019 07:08
9045D
Molybdenum
<2.50
2.50
BKN
05/06/201918:46
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on aV N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients; and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pofic- X 60wr
Pauric McGroary
Agronomist
Page 4 of 6

(2)iWaypont
7621 ain 80 -7 Road, Richmond, 27 -6446
Main 804-743-94p1 1Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46460
Customer Name: Synagro Central LLC/ Harnett
Report Number: 19-121-1028
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
• Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments: F___ - -
0 Yes 40 No
Signature: lBrandi Watson 1 Date & Time: 5/01/2019 14:40.30
Page 5 of 6

SAMPLING LOG #762
EiElf—EIE� A A "
CUSTOMER: SYNAGR® 804 04
�
PROJECT MANAGER: fvv �i nck— 7Dc,\jd
Phone: L'�;" ) C1 of TL C
A & L CUSTOMER SAMPLING
LAB # SAMPLE I.D. LOCATION
Relinquished by Sampler:
SAMPLE
TYPE
�L
Date
4/-3r,
Relinquished by: D
Relinquished by: p
SPECIAL fNSTRUCTIONS:
For `"
monitoring purposes.
SAMPLE
1111I11111I1111111!!!1!1l1�IIlllllll ll!!!ll1111111111111111[111t10
102
Svnaoro Central LLC/ Harnett019
z$
Harnett WfP 2 of 4
14:39:14
# OF
CONTAINERS
,ON OF CUSTODY
:)RD & ANALYSES
RECORD
- - bat11pury proceaures
were used during the collection of these samples.
SAMPLER T
SAMPLING METHOD METHOD
DATE TIME PRESERVED SHIPPED
Time Recieved by: REMARKS:
A. '' + C;
Time Re ieved by:
I
Time Recieved by:
PO#:
ANALYSIS REQUEST
I.D. SLI SL2 NHS N NO3 N gr �ni�tdC Ali Pb As Hg g� w CaCO3 VolatileP equiv. SolidsM°CIN0N
� � � � 1ow
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2. Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 4/26/2019 411/2019-513112019 0.2599
WTP LIQUID
Na mgll = (Na mg/kg x % Solids) + 100 = (317 x 2.5200) + 100 = 7.9884
Ca mg/1 = (Ca mg/kg x % Solids) + 100 = (734 x 2.5200) + 100 = 18.4968
Mg mg/1 = (mg mglkg x % Solids) + 100 = (1260 x 2.5200) + 100 = 31.752
Na meq = Na mgll = Molec.Wgt.Na = 7.9884 = 23 = 0.347322
Ca meq = Ca mgll = Molec.Wgt.Ca = 18.4968 = 20 = 0.92484
Mg meq = Mg mg/1 -:. Molec.Wgt.Mg = 31.752 : 12 = 2.646
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.347322 + SgrRoot[0.5(0.92484+2.646)] = 0.259933
Printed: 2/1/2020
Page 1 15:57

Waypoint
ANALYTICAL
9/1812019
Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-255-0004
Project Description: HWTP3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www,waypo inta n alyti ca I. co m
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/12/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pia(w0-r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

(2)
Waypoint,
7621 Whitepine Read, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary fable
Report Number, 19-255-0004
Client Project Description: HWTP3
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
68175
HWTP3
Solids
09/10/2019
15:15
09/12/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
W1N
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-254OG
WTN
Page 2 of 6

Report Number: 19-255-0004
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68175
Sample ld : HWTP3
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
0.24
99.80
16.50
0.24
0,07
1.53
0.23
0,09
0.10
<0.01
16.50
Waypoi * (D
t.
ANALYTICAL
Project: HWTP3
REPORT OF ANALYSIS
165000
2360
660
15300
2290
922
954
18400
150000
1890
219
37.8
<100
165000
3480
250
99.4
99.4
99.4
497
99.4
497
99.4
99.4
9.94
4.97
24.9
100
250
5.00
ADM
ADM
J PJ
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
JPJ
ZBD
7621 Whiitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.way p of nta n a lytical.corn
Date Sampled: 9/10/2019 15:15:00
Date Received: 09/12/2019 00:00
Date Reported: 09/18/2019
09/16/2019 16:43
09/16/2019 16:43
09/17/2019 14:00
09/1712019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 15:00
09/17/2019 14:00
09/17/2019 14:48
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confrdentiaf use of our clients, and may not be reproduced in whole or pan, nor may any reference be made
to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization
SM-2540G
S M-254OG
S M-4500-N H3 C-TKN
6010D
6010D
6010D
601 OD
601 OD
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
pofi4 If ow
Pauric McGroary
Agronomist
Page 3 of 6

Report Number: 19-255-0004
Account Number: 46622
Send To: Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68175
Sample ld : HWTP3
Waypoint,0 (D
ANALYTICAL
Project: HWTP3
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 9/10/2019 15:15:00
Date Received: 09/12/2019 00:00
Date Reported: 09/18/2019
Cadmium
<1.99
1.99
BKN
09117/201915:00
6010D
Chromium
17.9
4.97
BKN
09117/201915:00
6010D
Nickel
8.35
4.97
BKN
09117/201915!00
6010D
Lead
10.8
5.96
BKN
09/17/201915:00
601OD
Arsenic
17.6
9.94
BKN
09/17/201915:00
601OD
Mercury
0.0685
0.0163
TJS
09/17/2019 13:37
SW-7471 B
Selenium
<9.94
9.94
BKN
09/171201915:00
6010D
pH *
5.3
JSL
09/16/2019 06:52
9045D
Molybdenum
16.2
4.97
BKN
09/171201915:00
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series
is on a wet basis.
B-Analyte detected in blank
H - Beyond holding timeG]�AKj
Our reports and letters are for the exclusive and confidential use of our clients; and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work; the results, or the company in any advertising. news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 4 of 6

(D
WayPAo rat
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 G Fax [phone]
www.waypointanalytica Isom
Cooler Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLCI Technical
Report Number: 19-255-0004
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
J '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
C) No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
• NIA
Water - VOA vials free of headspace
0 Yes
0 No
• NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
• NIA
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Brandi Watson I Date & Time: I0921212019 10:35:51
Page 5 of 6

SAMPLING LOG #
CUSTOMER: SYNA RO QD
PROJECT MANAGER: le-vt'
Phone: (SUS) Novi -VL X
A & L CUSTOMER
LAB ## SAMPLE I.D.
SAMPLING
LOCATION
HuTP3
Tow AM
Relinquished by Sampler:
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS:
(OKII For
SAMPLE
ID
96S
SAMPLE
TYPE
jIL
Date
IM
Date
a
Date
monitoring purposes.
SL1 SL2 I NH4-N 1 NOS N uramu Cd Cr Ni
09- 12-2019 MAIN OF CUSTODY
s, a4�a can,tai LLCI recfinicai 10:3133 ECORD & ANALYSIS
S
HWTP3 RECORD
! attest that the proper field sampling procedures
were used during the collection of these samples,
SAMPLER
# OF SAMPLING METHOD METHOD
CONTAINERS [SATE. TIME PRESERVED SHIPPED
Time
s '15• Time
�` �!1• ,�, : � � � C.s a Crs�'
Recieved by: REMARKS:
Recieved
Reci
ANALYSIS REQUEST
Plb FAs I HS l Se
PO#:
M
20an wonown
Solids I MO I CI I NO2 N
®_E2
SL1: Total Solids (Moisture), Total I<jeldahl Nitrogen, Phosphorus, and Potassium' «
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
i
ivy
Page 6 of 6 ,�

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL., NC COH REGIONAL 9/10/2019 f 1 - f 1 0.2078
WTP LIQUID
Na mg/l = (Na mg/kg x % Solids) + 100 = (954 x 0.2400) + 100 = 2.2896
Ca mgll = (Ca mg/kg x % Solids) _ 100 = (2290 x 0.2400) + 100 = 5.496
Mg mgll = (mg mg/kg x % Solids) + 100 = (922 x 0.2400) + 100 = 2.2128
Na meq = Na mgll + Molec.Wgt.Na - 2.2896 + 23 = 0.0995478
Ca meq = Ca mgli + Molec.Wgt.Ca = 5.496 + 20 = 0.2748
Mg meq = Mg mgll + Molec.Wgt.Mg = 2.2128 + 12 = 0.1844
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.0995478 + SgrRoot[0.5(0.2748+0.1844)] = 0.207752
Printed: 2/7/2020
Page 1 09:57

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Nate Roth
Project Name: Harnett Co.
Lot Number:UJ04028
Date Completed:10/17/2019
10/17/2019 4:04 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
_ ACC7Fp
/ AMM
DOD ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Coiumbfa, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 6639
Case Narrative
Synagro
Lot Number: UJ04028
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: UJ04028-001. Due to low % solids, the initial amount of these samples were 3 times the
standard procedure amount. The LOQ has been adjusted accordingly.
Nitrite/Nitrate
A laboratory control sample was analyzed instead of an opening continuning calibration verification
standard during nitrite/nitrate analysis. target analyte reoveries are within acceptance criteria. Results are
reported. Affected samples: UJ04028-001
Shealy Environmental Services, lnc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 7

Client: Synagro Laboratory ID: UJ04028-001
Description: Harnett WTP Matrix: Solid
Date Sampled:1010312019 0900 % Solids: 0.484 10/0612019 1439
Date Received:1010412019
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Hatch
2
(% Solids) SM 2540G
1
10/05/2019 1439 KFE
31092
1 350.1
(Ammonia - N ) 350.1
1
10/08/2019 1727 DFR
31315
1
(Nitrate - N) 9056A
1
10/11/2019 1436 GMH
31973
1
(Nitrite - N) 9056A
1
10/11/2019 1436 GMH
3196B
1
(Phosphorus) 365.1
1
10/07/2019 1603 DMA
10/07/2019 1135 31146
1
(Soil pH meas) 9045D
1
10/07/2019 2204 HET
31236
1 351.4
(TKN) 351.2
1
10/10/2019 1029 DMA
10/09/2019 1730 31510
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
knits
Run
% Solids
SM 254OG
0.484
%
2
Ammonia - N (gas diffusion)
350.1
ND
210
110
mglkg
1
Nitrate - N (soluble)
9056A
170
100
5.1
mglkg
1
Nitrite - N (soluble)
9056A
37 J
41
4.0
mglkg
1
Phosphorus
7723-14-0 365.1
2100
1000
210
mglkg
1
Soil pH measured in water @ I ° C
9045D
5.3
su
1
TKN
351.2
26000
5200
5200
mglkg
1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 10/08/2019 1254 KSH2 10/07/2019 1550 31131
CAS Analytical
Parameter Number Method Result Q LOQ DL knits Run
Mercury 7439-97-6 7471E ND 16 3.8 mglkg 1
1CP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/10/2019 0544 LLL 10/09/2019 0857 31269
2 3050B 6010D 1 10/11/2019 0547 LLL 10/09/2019 0857 31269
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Aluminum
7429-90-5
6010D
200000
1300
500
mglkg
1
Arsenic
7440-38-2
6010D
32
J
50
17
mglkg
1
Cadmium
7440-43-9
6010D
ND
17
4.2
mg/kg
1
Calcium
7440-70-2
6010D
2200
J
17000
2100
mglkg
1
Chromium
7440-47-3
6010D
19
J
34
8.4
mglkg
1
Copper
7440-50-8
601OD
210
34
15
mglkg
1
Iron
7439-89-6
601OD
11000
B
340
150
mglkg
2
Lead
7439-92-1
6010D
ND
34
15
mglkg
1
Magnesium
7439-95-4
6010D
ND
17000
2100
mglkg
1
Manganese
7439-96-5
6010D
3500
50
20
mglkg
1
Molybdenum
7439-98-7
6010D
74
J
130
34
mglkg
1
LOQ = Limit of Quantitatfon B = Detected in the method blank E = Quantitation of compound exceeded the calihralior range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result � LOU and? DL
H = OLt of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
108 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyfab.com
Page 3 of 7

Client:Synagro Laboratory ID:UJ04028-001
Description: Harnett WTP Matrix: Solid
Date Sampled:10103/2019 0900 % Solids: 0.484 10105/2019 1439
Date Received:10104/2019
1CP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601 OD 1 10/10/2019 0544 LLL 10/09/2019 0857 31269
2 3050B 601 OD 1 10/11/2019 0547 LLL 10/09/2019 0857 31269
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Nickel
7440-02-0
601 OD
ND
130
35
mg/kg
1
Potassium
7440-09-7
601 OD
2900
J
17000
2100
mglkg
1
Selenium
7782-49-2
601 OD
ND
67
27
mg/kg
1
Sodium
7440-23-5
601 OD
3600
J
17000
2100
mglkg
1
Zinc
7440-66-6
6010D
43
J
170
42
mg/kg
1
LOQ = Limit of QLantitation B = Detected In the method blank E = Quantitation of compound exceeded the caflbratlon range DL - Detection Limit
ND — Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W W Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
sk'mlw envinxilmcntal servvicr;, the Page 1 ur I
TaowiwuxN Lmbcr. MHO Effi;Oiw DPW 3-'1r2011
Sample Receipt Cbecklist (SRQ
CliMr [,; SYl4At ltC) Cooler ln5occted byldalc; LKH ,` 14-04-2019 Lot if UJ04028
Means of receipt: 0 SESI ❑ Client 071PS
[] FedFx Q Other_
""0
1- Were custody seals present oat #lie ctolcr?
rl Yes
No
1� A 2. 1f custody coals weir prmcnt, were thq ingot cad unbroken?
p1=1 Strip ID: NA ... _...._ ._ Chlorino Strip ID, NA _ � _ _ '1765ted by: WA.
Origirurl hemp= rtl�,r` uponreeaopt i Derived (Corrected) temperature upon receipt %Solid Snap -Cup ID: I�~1GIG
5,11 15.9 ' : NA 1 NA w'e, ,'� A 7 A �,(, NA 1NA 4�ti
Method-. LJTcmn raturw Blunk OAgairtsd B-)WO5 IR GLul ID. S [It Oun Clorrectian Factor: 4 ''C.
�#entered uf=cuolant: Z Wet ice D Ice Packs El D� Ice El Alone
Ycs
No
®NA
3. 1f tonipemture of any carrle�r exceeded 6.VC, was project Manager Notified?
1'1V1 was Notificd by: phone.+ crnail I face-to-face {circle one).
Yes
❑ No
�1.�1.k
4. Is The enmrnereial courier's. packing Slut attached to this forM? .......... .........
Yes
j0 Yes
El No
5- WcTc proper cuslody prnwrlije I`reliriTiisheei4�ceived) A�1ltrwtcl?
00 Yea
® Yes
Nn
Q Not
6- Were sample 1Ds 1lffwd on the COC ?
7_ Were sample; I17fi lisled ,on all-oimple. cnrilairierx?
Yes
® No
S. Was aollectlon date & time limed on the COO?
®Yes
W
® No
® No
`7- WKs collocli(m clritn & tirrlr lisic-d (in all -,mrrtplc: c unlarinl:"?
10. Did rill container lahz1 infor Inadon (ID, date, time) agree Nr,dtli the c0c.'
® yes
® No
I l ,'Alerts tests Lu bc: N601711W lislLd a_sra thu COC'?
0 Yet;
I--1 No
11 Lard -.%.11 samples arrive in ilia proper c ontahwra tbt eaGll LeNI attdh)r-111 a4old i,oadkjon
(unbroken, lids i;rl, vw'fl
Yes
Y
® Na
❑No
l 3 'Was mdoqualq. s�rnpk' voltnne available?
114. Were alI satnples mei~retl with -in 1.j the holding lime or48 hours, whiab wier corrtes flw?
Yes
V1 No
15, Were any sa rn les eont9i.rtcrs missin `excess (eir,ele ogre) samples Nbt listed on COC'?.—
El Ycs
Q No
® NA
16, For VOA. and RSK-175 sam[Av L were bubbles 6rnm in diarntA::r)
in airy of the VOA vialq?
Ycs
0 No
VJ NA
17, Were ;:all I]I1.Umctals!nutrient samples received at a pH of < 2?
0 Yes
❑ No
® NA
18. Were all gymicle sae pics rcc4ivcd at al, pH f 12 alad sulfide samples received al a nH > �1'?
Y-e
El No
1Z NA
19, Won, nl l upplitatblij MyrTI NAti yanidc; pher oY625 (< Umg3L) sdtnp es tr-ee Rsld❑
c ual
chlcar•€rae�......................................
❑ Ycs
® No
� NA
20. W=4�licnl rcntarks rcqucsts (i.e. requested dilutions, s��JS}f��15t3 de _t�5�#int�c etc---)
correctly teansodbed from the COC into the winrnvnt section in LIN] S?
® Yves
Net
al . Wz-5 the quotp, number 11sted on the oorxtainer lath]'? if vcs, Quote A
Somple lP'reservaiiion ()r u,31 be completed For any sample(s) mple(s) jrtcorreo4y presmW or wkh laeadspacc.)
Saamplra(s) NA sArere. rec-dwd incorrwily presertrd and vocre aijusted a=rdhi gly
in simple re06i,•ing with NA - rnL of circle one.142SChl-, HNO-3,1.10, NaGH wing SR i'A ,
itne of preservation NA if r�trrc than one ppmscrvative is needed, please note in the cernments bolovv,
Sarrnplc�5) _N- ...._.. ___wore recciv- with bubblc5 --6 rant in dianiaci•.
Surnp n(s) NA were tereived with 7RC = 0.5 Ing'L (if tl 19 is no) and were
adjusW acotdingly in satnp[c recedving xvidi sod`nun tltirrsulrate with Shicaly ID, NA
Slid baizode labels applic4 by, DMN
'<LML411nk;Tll�
Shealy Environmental Services, inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2037-01-WPL-NC HARNETT CO. UTIL„ NC COH REGIONAL 10/3/2019 6/112019-12131/2019 0.9122
WTP LIQUID
Na mgll = (Na mg/kg x % Solids) + 100 = (3600 x 0.4840) + 100 = 17,424
Ca mg/l = (Ca mg/kg x % Solids) + 100 = (2200 x 0.4840) 100 = 10.648
Mg mgll = (mg mglkg x % Solids) + 100 = (2100 x 0.4840) + 100 = 10,164
Na meq = Na mgll + Molec.Wgt.Na = 17.424 + 23 = 0.757565
Ca meq = Ca mgll + Moiec.Wgt.Ca = 10.648 + 20 = 0,5324
Mg meq = Mg mgll + Molec.Wgt.Mg = 10,164 + 12 = 0,847
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.757565 + SgrRoot[0.5(0.5324+0.847)] = 0.9122
Printed: 2/1/2020
Page 1 15:58

SECTION 3

FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: HARNETT COUNTY
SITE #: NC HA 0OX43 FIELD# : HA 0OX43 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 476.25
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page
Lime Applied ***
Date
Lbs1Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vo1a-
Nliner-
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
nation
tili-
ali-
Ammonia
Nitrate
PAN
Total
( Per Acre
DATE or
MONTH
Solids
Per
Residua]
Dry, Wet,
Past 24
Method
zation
nation
TKN
Nitrogen
and
(pp-)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
117119
291,400.00 (G)
7414.758
1.93
0.597
HCUCOH
SUR
0.5
0.20
40,000.p
100.00 p
4,84 p
8055
BERMUDAGRASS
1/8/19
254,200.00 (G)
6469-193
1.93
0.521
HCUCOH
SUR
0.5
0.20
40,000. p
100.00 p
4.84 p
8055
I BERMUDAGRASS
1/22/19
229,400.00 (G)
5837.150
L93
0.470
HCUCOH
SUR
0.5
0.20
40,_000.p
100.00 p
4.84 p
8055
BERMUDAGRASS
1/23/19
235,600.00 (G)
5994.911
193
0.482
HCUCOH
SUR
0.5
0.20
40,000. p
100.00 p
4,84 p
8055
BERMUDAGRASS
Jan-19
L010,600.00 (G)
25,715.012
2/4/19
241,800.00 (G)
6152.672
193
0.495
HCUCOH
MOIST
0-<112"
SUR
0.5
0.20
4000. p
100.00 p
4.84 p
8055
I BERMUDAGRASS
2/5/19
204,600.00 (G)
5206107
193
0.419
HCUCOH
MOIST
0-<1/2"
SUR
0.5
0.20
40,000. p
100.00 p
4.84 p
8055
I BERMUDAGRASS
2/26/19
260,400.00 (G)
6625,954
1.93
0.533
HCUCOH
MOIST
0-<1/2"
SUR
0.5
0.20
40,000. p
100.00 p
4.84 p
8055
I BERMUDAGRASS
2/27/19
235,600.00 (G)
5994.911
1.93
0.482
HCUCOH
MOIST
0-<1/2"
SUR
0.5
0.20
40,000. p
100.00 p
4.84 p
8055
BERM-UDAGRASS
Feb-19
942,400.00 (G)
23,979.644
3/7/19
235,600.00 (G)
5994.911
1.93
0.482
HCUCOH
SUR
0.5
0,20
40,000. p
100.00 p
4.84 p
8051
BERMUDAGRASS
3/8/19
204,600.00 (G)
5206107
1.93
0.419
HCUCOH
SUR
0.5
0,20
40,000. p
100.00 p
4.84 p
8055
BERMUDAGRASS
3/20/19
223,200.00 (G)
5679.389
1,93
0A57
HCUCOH
SUR
0.5
0.20
40,000. p
100.00 p
4.84 p
8055
BERMUDAGRASS
3/21/19
229,400.00 (G)
5837.150
1.93
0.470
HCUCOH
SUR
0.5
0.20
40,000. p
100.00 p
4.84 p
8055
BERMUDAGRASS
Mar-19
892,800.00 (G)
22,717.557
4/3/19
235,600.00 (G)
5994.911
2.52
0.630
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
4/4/19
272,800.00 (G)
6941.476
2.52
0.729
HCUCOH
SUR
0.5
0,20
12,400. p
4,800.00 p
4.90 p
3925
f BERMUDAGRASS
4/18119
A0,200.00 (G)
3312.977
2_52
0.348
HCUCOH
SUR
0.5
0.20
12,400.p
4,800.00 p
4.90 p
3925
I BERMUDAGRASS
4/22/19
254,200.00 (G)
6468.193
2,52
0.680
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
I[ BERMUDAGRASS
4/23/19
124,000.00 (G)
3155.216
2.52
0.332
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
Apr-19
1,016,800.00 (G)
25,872.773
5/6/19
204,600.00 (G)
5206.107
2.52
0.547
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
5/7/19
130,200.00 (0)
3312.977
2.52
0.348
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
5/8/19
161,200.00 (G)
4101.781
2.52
0.431
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
5/28/19
142,600.00 (G)
3628.499
2.52
0.381
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
5I29119
86,800.00 (G)
2208.651
2.52
0.232
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
5/30/19
74,400.00 (G)
1893.130
2,52
0.199
HCUCOH
SUR
0.5
0.20
12,400, p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
5/31/I9
62,000.00 (G)
1577.608
2.52
0.166
HCUCOH
SUR
0.5
0.20
12,400. p
4,800.00 p
4.90 p
3925
BERMUDAGRASS
May-19
861,800.00 (G)
21,928.753
6/3/19
1I7,800.00 (G)
2997.455
0.48
0.061
HCUCOH
SUR
0.5
0.20
26,000.p
110.00 p
170.00 p
5403
BERMUDAGRASS
6/12/19
241,800.00 (G)
6152.672
0.48
0.124
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
BERMUDAGRASS
6/13/19
241,800.00 (G)
6152.672
OAS
0,124
HCUCOH
SUR
0.5
0.20
26,000.p
110.00 p
170.00 p
5403
BERMUDAGRASS
Jun-19
601,400.00 (G)
15,302.799
7/25/19
260,400.00 (G)
6625.954
0.48
0.134
HCUCOH
SUR
0.5
0.20
26,000.p
110.00 p
170.00 p
5403
BERMUDAGRASS
7/26/19
1 229,400.00 (G)
5837.150I
0.48
l 0.118
I HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
I 5403
l BERMUDAGRASS

FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: HARNETT COUNTY
SITE #: NC HA 0OX49 FIELD# : HA 0OX43 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : LAKELAND
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 476.25
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page
Lane Applied ***
Date
Lb,/A.
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Matbod
zation
zation
TKN
Nitrogen
and
[ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
Jul-19
489,800.00 (G)
12,463.104
8112/19
179,800.00 (G)
4575.064
0.48
0.092
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
8/13/19
49,600.00 (G)
1262.087
0.48
0.025
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
8/23/19
173,600.00 (G)
4417.303
0,48
0.089
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
8/26/19
37,200.00 (G)
946.565
0.48
0.019
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
8/27/19
167,400.00 (G)
4259,542
0.48
0.086
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
BERMUDAGRASS
Aug-19
607,600.00 (G)
15,460,561
12/6/19
99,200.00 (G)
2524.173
0.48
0.051
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
12/7/19
111,600,00 (G)
2839.695
0.48
0.057
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
12/8/19
86,800.00 (G)
2208.651
0.48
0.045
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
12/9/19
86,800.00 (G)
2208.651
0.48
0.045
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
12/10/19
142,600.00 (G)
3628.499
0.48
0.073
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
12/26/19
86,800.00 (G)
2208.651
0.48
0.045
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
BERMUDAGRASS
12/27/19
155,000.00 (G)
3944.020
0.48
0.080
HCUCOH
SUR
0.5
0,20
26,000. p
110.00 p
170.00 p
5403
BERMUDAGRASS
Dec-19
768,800.00 (G)
19,562.340

FACILITYNAME: HARNETT CO. UTILITIES, NC
OWNER: HARNETT COUNTY
SITE #: NC HA OOX43 FIELD# : HA 0OX43 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LAKELAND
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 476.25
OPERATOR: HARNETT COUNTY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 39.30 ACRES PERMITTED: 39.30
Page : 3
Lime Applied ***
Date
LbsAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
1'K1V
Nitrogen
and
(PP-)
Crop
!!
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1 UCai uarlons/Ac: 18S,UUL.54
Total Wet Tons/Ac:
As
Cd
Cr
Cu
Pb
H9
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
147
0.225
0.032
0.692
6.171
0.277
0.011
0.260
0.334
0.177
1.183
40.10
Cumulative lbs/acre
I.982
0.392
6.326
48.448
1.959
0.086
2.132
2.896
1.124
18.359
Permit PAN Limit Obs/acre) Ist Crop/2nd Crop
I47
FD Cumulative Pollutant Loading Rate Limit abs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
HCUC014WPL = HARNETT CO. UTII.., NC COH REGIONAL WTP LIQUID
AlkK�� � -�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, lnjectionlincorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: HARNETT CO. UTILITIES, NC PREDOMINANT SOIL SERIES: AYCOCK
OWNER: JW POPE PERMIT 4: WQ0014885 ANNUAL DRY TONS APPLIED: 3.88
SITE 4: NC HA 0OX47 FIELD# : HA 0OX47 0002 OPERATOR: JW POPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 11.00 ACRES PERMITTED: 11.00
Page
Lime Applied
***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
ova
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tili-
zation
Miner=
ali-
nation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
drop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/18/19
86,800.00 (G)
7890.909
0.48
0159
HCUCOH
SUR
0.5
0.20
26,OOO.p
110.00 p
170.00 p
5403
BERMUDAGRASS
9/19/19
105,400.00 (G)
9581,818
0.48
0.193
HCUCOH
SUR
0.5
0.20
26;000. p
110.00 p
170.00 p
5403
BERIVI[_1DAGRASS
Sep-191
192,200.00 (G)
17,472.777
Total Gallons/Ac: 17,472.73
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS
As Cd Cr Cu Pb Hg Mo Ni Se I Zn I F I PAN
Annual Ibs/acre
4
0.023
0.003
0.013
0.148
0.011
0.003
0.052
0.025
0.0I9
0.030
1.48
Cumulative Ibs/acre
0,023
0.003
0.013
0.148
0.011
0.003
0.052
0.025
0.0I9
0.030
Permit PAN Limit (lbslacre) 1 st Crop/2nd Crop
220
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
99.0
2500.0
HCUCOHWPL = HARNETT CO. UIIL, NC COH REGIONAL WTP LIQUID
(SIGNATURE OF LAND APPL[kR) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: HARNETT CO. UTILITIES, NC PREDOMINANT SOIL SERIES: AYCOCK
OWNER: JW POPE PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 3.50
SITE #: NC HA 00X47 FIELD# : HA 00X47 0003 OPERATOR: JW POPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: I 1.00 ACRES PERMITTED: 11.00
Page
Lime Applied
***
Date
Lb,/A-
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
ova
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
nation
Miner -
ali-
2ation
TKN
Ammonia
Nitrogen
Nitrate PAN
and (ppm)
Crop
j
MONTH
Total
1
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/17/19
130,200.00 (G)
I1836.364
0.48
0.239
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p 5403
BERMUDAGRASS
9/18/19
43,400.00 (G)
3945.455
0.48
0.080
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p 5403
BERMUDAGRASS
Sep-19
1 173,600.00 (G)
15,781.819
Total Gallons/Ac:
Total Wet Tons/Ac:
15,781.82
A VLGl l.UV1V lUV C14+. U.UV
As
Cd
Cr
Cu
Pb
Hg
IV
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
3
0.020
0.003
0.012
0.134
0.010
0.002
0.047
0.022
0.017
0.027
1.34
Cumulative lbs/acre
0.020
0.003
0.012
0.134
0.010
0.002
0.047
0.022
0.017
0.027
Permit PAN Limit (lbs/acre) 1 st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
HCUCOHWPL = HARNETT CO. UM., NC COH REGIONAL WTP LIQUID
R&k:
C,
X ;—r/ — ,-9C)
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR =Not Reported or Not Required % = percent p — pp- or mg/ke ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FOLD SUMMARY FORM
FACILITYNAME: HARNETT CO. UTILITIES, NC PREDOMINANT SOIL SERIES: AYCOCK
OWNER: iW POPE PERMIT #: WQ0014885 ANN-UAL DRY TONS APPLIED: 2.13
SITE #: NC HA 0OX47 FIELD# : HA 0OX47 0004 OPERATOR: iW POPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 5.00 ACRES PERMITTED: 5.00
Page: I
Lune Applied ***
Date Lbs�Ac
DATE or
Gallons (G) or Cubic Yards (CY)
of%
Wet Tons (VTT} (specify}
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(PP-)
Crop
Total
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
9/161I9
74,400.00 (G)
14880.000
0,48
0.300
HCUCOH
SUR
0.5
0.20
26,OOO.p
110.00 p
170.00 p
5403
BERMUDAGRASS
9/17/19
31,000.00 (G)
6200.000
0.48
0.125
HCUCOH
SUR
0.5
4.20
26,000.p
110.00 p
170.00 p
5403
SERMUDAGRASS
Sep-19
1 105,400.00. (G)
21,080,000
Total Gallons/Ac: 21,080.00
Total Wet Tons/Ac:
. 4..,,.... u.,,.z...
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS
Annual lbslacre
5
0.027
0.004
0.016
0.179
0.013
0.003
0.063
0,030
0.023
0.037
1.79
Cumulative lbslacre
0.027
0.004
0.0I6
0.179
0.013
0.003
0.063
0.030
0.023
0.037
Permit PAN Limit (lbslacre) Ist Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
1 36.6
34,8
1339.0
267.9
15.0
375.0
89.0
2500.0
HCUCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted I am aware that there are significant penalties for submitting false information,. including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Raquired % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: HARNETT CO. UTILITIES, NC
OWNER: BOBBY BRANCH
SITE #: NC LE 00OX2 FIELD# : LE 00OX2 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CAB
PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 30.16
OPERATOR: BOBBY BRANCH CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 40.00 ACRES PERMITTED: 40.00
Page
Luce Applied ***
Date
Lb/A.
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond,
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
I
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
111
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
10/9/19
179,800.00 (G)
4495.000
0.48
0.091
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
BERMUDAGRASS
10/10/19
248,000.00 (G)
6200.000
0.48
0.125
HCUCOH
SUR
0.5
0.20
267000. p
110.00 p
170,00 p
5403
BERMUDAGRASS
10/1i/19
229,400.00 (G)
5735.000
0.48
0.116
HCUCOH
SUR
0.5
0.20
26;000.p
110.00 p
170.00 p
5403
BERMUDAGRASS
10/15/19
204,600,00 (G)
5115.000
0.48
0.103
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
10/18/I9
111,600.00 (G)
2790.000
0A8
0,056
HCUCOH
SUR
0.5
0.20
26,000, p
110.00 p
170.00 p
5403
BERMUDAGRASS
Oct-19
973,400.00 (G)
24,335.000
11/14/19
148,800.00 (G)
3720.000
0.48
0.075
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
11/18/19
198,400.00 (G)
4960.000
0.48
0.100
I-]CUCOH
SUR
0.5
0,20
26,000. p
110.00 p
170.00 p
5403
I BERMUDAGRASS
11/19/19
173,600.00 (G)
4340.000
0.48
0.088
HCUCOH
SUR
0.5
0.20
26,000. p
110.00 p
170.00 p
5403
BERMUDAGRASS
Nov-19
520,800.00 (0)
13,020.000

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME : HARNETT CO. UTILITIES , NC PREDOMINANT SOIL SERIES: CAB
OWNER: BOBBY BRANCH PERMIT #: WQ0014885 ANNUAL DRY TONS APPLIED: 30.16
SITE #: NC LE OOOX2 FIELD# : LE 000X2 0001 OPERATOR: BOBBY BRANCH CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 40.00 ACRES PERMITTED: 40.00
Page: 2
Luce Applied ***
Date
Lbs�Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Condd
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAID]
Total Per Acre
DATE or
MONTH
Solids
Per
rre
Residual
Dry, Wet,
Past 24
Method
nation
zation
`1'KN
Nitrogen
and
(PP-)
Crop
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1 Mat ua13ons/Pxe:
Total Wet Tons/Ac:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
8
0.048
0.006
0.029
0317
0.023
0.006
0.112
0,053
0.041
0.065
3.I7
Cumulative lbs/acre
0.04E
0.006
0.029
0.317
0.023
0.006
0.112
0.053
0,041
0.065
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
166
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
2679
15.0
375.0
89.0
2500.0
HCUCOHWPL = HARNETT CO. UTIL., NC COH REGIONAL WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"l certify, under penalty of law, that this document was prepared under my direction or Supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injectionacorporation LO
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

SECTION 4

summiat
S
AnsPyc cal LAbornxorles
March 20, 2019
Melinda Boyd
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Harnett WTP
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] rAX.• [phone]
Website: httn://wmiv.settek.com
Dear Melinda Boyd: Order No,: 19030418
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/8/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St,
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108,17elaware, Florida NELAC E87688, Georgia E87688, Idaho 01-100923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey Oi-1006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Olio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon 0112O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas TI04704466-11-5, Utah
OH009232011.1, Virginia VELAP9456, WashingtonC991
Page 1 of 35

U I T
Sunrnrit Eni ironme"tal Technologies, Inc.
3310 Yin St.
3310 Win
Case Narrative
ENVIMMMENTAL if C?i�7C3i.t7�33:FS,INC
Cuyahoga Falls, Ohio44223
WO#: 19030418
Analytical Laboratorotw
TEL: [phone] FAX: [phone]
Wehsite; httn:1Amvw.settekcom
Date: 3/20/2019
CLIENT:
Synagro
Project:
Harnett WTP
WorkOrder Narrative:
19030418: This report- in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt. Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
tithes and at different sampling conditions. Summit Environmental Technologies, Inc, is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
19030418-00IA 436012: Prep Comments for MtlPrep_TCLP(301OA), Sample 19030418-OOIA: TCLP
was filtered after digestion.
Prep Sample QC Comments:
TCLP Blank 3-12-19 436027: Prep Comments for MtlPrep_TCLP(3010A), Sample TCLP Blank 3-12-
19: TCLP was filtered after digestion.
Original
Page 2 of 35

IT
Summit Environmental Technologies, In Qualifiers and Acronyms
SUMM3310 Win t
EPa ROMMENTAL t cltr�n[csri=S, ghlC Cuyahoga FaHs, Ohio 442; ' oii: 19030418
Anafy0asl tnbcraf000,—s TEL: [phone] FAX'. (330) 253-446
Website: httv:/1}viviv.settek.co Date: 3/20/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
3 The reported value is greater than the Method Detection Limit but less than the Reporting Limit,
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit,
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response,
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
BIMB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-1+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery Iimits.
QV-/+ The ICV recovery failed Iow (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level oPQuantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
Cl2QL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 35

Sannnzit Envia onnaentgl Technologies,
Workorder
summil-
O, INC.
3310 Win St.
St.
CfryahogaFglls, Ohio 44223
Sample Summary
14rrt#fyfloaf Eiatrrafoneg
TEL: [phone] FAX; [phone]
WO#: 19030418
Website: htta://iyinyaeltek.cpm
20-mar-19
CLIENT:
Synagro
Project:
Harnett WTI'
Lab Samplelll Client Sample ID Tag No Date Collected
Date Received Matrix
19030418-001
Haniett WTP
3/5/2019 10:00:00 AM
3/8/2019 10;05:00 AM Sludge
Page 4 of 35

SUMMIT
Summit Environmental Technologies, Inc,
3310 Win St.
DATES REPORT
54VI9?OtdM�n]TAL ra �ara[]Lt�et=S.wc
Cuyahoga Falls, Ohio44223
WO#:
19030418
AwtyNcal Labarafoni?5
TEL: [phone] FAX.- [phone]
Wehsite: http.lAvww.settek.com
20-Mar-19
Client:
Synagro
Project:
Harnett WTP
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
19030418-001A Harnett WTP 3/5/2019 lU0:00 AM Sludge lgnitability of Solids (SW-846: 1030)
3/12/2019 12:30:00 PM
pH (SW9045D)
3/19/2019 3:31:12 PM
Reactive Cyanide (901417.3.3.2)-Solid
3/14/2019 4:00:00 PM
Reactive Sulfide (9034)/7.3.4.2
3/14/2019 4:00:00 PM
SVOC SW-846: 8151 Herbicides-TCL3/11/2019 6:00:00 PM
3/14/2019 6:00:00 PM
3/19/2019 4:39:00 PM
TCLP Mercury Analysis (SW1311174i3111/2019 6:00:00 PM
3/15/2019 1:00:00 PM
3/15/2019 4:48:00 PM
TCLP Metals Analysis (SW 1311/60I0 3/11/2019 6:00:00 PM
3/13/2019 8:45:00 AM
3/18/2019 3:06:06 PM
TCLP Metals Analysis (SW13l l/6010 3/11/2019 6:00:00 PM
3/13/2019 8:45:00 AM
3/15/2019 6:05:21 PM
TCLP Pesticides Analysis (SW 1311/8(3/11/2019 6:00:CC PM
3/11/2019 5:20:00 PM
3/15/2019 11:53:00 PM
TCLP Semi-Volatiles Analysis 3/11/2019 6:00:00 PM
3/13/2019 3:30:00 PM
3/19/2019 10:08:00 PM
(SW1311/9270)
TCLP Volatiles Analysis
3/12/2019 6:19:00 PM
Original
Page 5 of 35

Ammit Environmental Technologies, Inc.
3310WinSt.
Analytical ReportSUMMIT-
ENVIRONMENTAL �.5, INC
Anaty lleal LaboralarMa=_
Cuyahoga Falls, Ohio44223
TEL: [phone] Fi1K- [phone]
(base report)
WO#: 19030418
Website: httn:11mini,.settek.com
Date Reported: 3/20/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/5/2019 10:00:00 AM
Lab 1D:
19030418-OOIA
Project:
Harnett WTP
Client Sample ID Harnett WTP
Analyses Result
RL Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -LIQUID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND
0.00500
mg1L
1
3/16/2019 4:48:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -LIQUID
SW601OD
SW301OA
Analyst: KMO
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
NO
1.25
mg1L
1
3115/2019 6:05:21 PM
TCLP Barium(Ba)
NO
12.5
mg1L
1
3/15/2019 6:05:21 PM
TCLP Cadmium(Cd)
NO
0.250
mg1L
1
3/15/2019 6:05:21 PM
TCLP Chromium(Cr)
NO
0.500
mg1L
1
3115/2019 6:05:21 PM
TCLP Lead(Pb)
ND
1.25
mg/L
1
3115/2019 6:05:21 PM
TCLP Selenium(Se)
ND
0.125
mg/L
1
3/18/2019 3:W06 PM
TCLP Silver(Ag)
ND
1.25
mg1L
1
3115/2019 6:05:21 PM
TCLP METALS, VOC, BNA, PEST, HERB -LIQUID
SW8270
SW351OC
Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichlorobenzene
ND
0.0800
mg1L
2
3118/2019 10:08:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
3/18/2019 10:08:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
3118/2019 10:08:00 PM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2
3118/2019 10:08:00 PM
Cresols, Total
ND
4.00
mg1L
2
3118/2019 10:08:00 PM
Hexachlora-1,3-butadiene
ND
0.0160
mg/L
2
3118/2019 10:08:00 PM
Hexachlorobenzene
ND
0.0400
mg/L
2
3118/2019 10:08:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
3118/2019 10:08:00 PM
Nitrobenzene
ND
0.0800
mg1L
2
3118/2019 10:08:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
3/18/2019 10:08:01) PM
Pyridine
ND
0.200
mg/L
2
3118/2019 10:08:00 PM
Surr. 2-Fluorophenol
38.1
10 - 109
%Rec
2
3/18/2019 10:08:00 PM
Surr: Phenol-d6
43.6
10 - 109
%Rec
2
3/18/2019 10:08:00 PM
Surr: Nitrobenzene-d5
47.3
19 - 120
%Rec
2
3/18/2019 10:08;00 PM
Surr: 2,4,6-Tftromophenol
41.6
10 - 120
%Rec
2
3/18/2019 10:08:00 PM
Surr: 2-Fluorobiphenyl
39.4
22 - 117
%Rec
2
3/18/2019 10:08:0D PM
Surr: p-Terphenyl-d14
66.3
34- 116
%Rec
2
3/18/2019 10:08:0D PM
Qualifiers: E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Original
RL
Reporting Detection Limit
U
Samples with CatcVal < MDL
Page 6 of 35

SUMM3310
111
summit Environmental Technologies, Inc.
Win St.
Analytical Report
EhV1R0t4?Ar=Wfir.AL )TG7iN0LGG$r-S, FWC
l�n.rlytfcaf boraforde�
Cuyahoga Falls, Ohio 44223
TEL: {330) 253-8211 FAX.- [phone]
{base report}
W09: 19030418
Website: but :lAviviv.settek.com
Date Reported: 3/20/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/5/2019 10:00:00 AM
Lab ID:
19030418-OOIA
Project:
Harnett WTP
Client Sample ID Harnett WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -LIQUID
SW8081
SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW1311I8081)
Chlordane, total
ND
0.250
mglL
10
3/15/2019 11:53:00 PM
Toxaphene
ND
0.500
mglL
10
3/15/2019 11:53:00 PM
Endrin
ND
0.0250
mglL
10
3/15/2019 11:53:00 PM
gamma-BHC
ND
0.0250
mglL
10
3/15/2019 11:53:00 PM
Heptachlor
ND
0.0250
d mglL
10
3/15/2019 11:53:00 PM
Heptachlor epoxide
ND
0.0250
mglL
10
3/15/2019 11:53:00 PM
Methoxychlor
ND
0.0250
d mglL
10
3/15/2019 11:53:00 PM
Surr: TCMX
59.4
10 - 119
%Rec
10
3/15/2019 11:53:01) PM
Surr: DCB
88.0
10- 119
%Rec
10
3/1512019 11:53:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -LIQUID
SW8151A
SW8151A
Analyst: MES
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
ND
1.00
mglL
1
3/19/2019 4:39:00 PM
2,4,5-TP
ND
0.500
mglL
1
3/19/2019 4:39:00 PM
Surr. 2,4-Dichlorophenylacetic aci
65.7
20 - 140
%Rec
1
3/19/2019 4:39:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -LIQUID
SW8260
Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.500
mglL
100
3/12/2019 6:19:00 PM
1,2-Dichloroethane
ND
0.500
mglL
100
3/12/2019 6:19:00 PM
MEK
ND
2.50
mglL
100
3/12/2019 6:19:00 PM
Benzene
ND
0.500
mglL
100
3/12/2019 6:19:00 PM
Carbon tetrachloride
ND
0.500
mg1L
100
3/12/2019 6:19:00 PM
Chlorobenzene
ND
0.500
mglL
100
3/12/2019 6A 9:00 PM
Chloroform
ND
0.500
mglL
100
3/12/2019 6:19:00 PM
Tetrachloroethene
ND
0.500
mg/1-
100
3/12/2019 6:19:00 PM
Trichloroethene
ND
0.500
mglL
100
3/12/2019 6:19:00 PM
Vinyl chloride
ND
0.200
mg1L
100
3/12/2019 6:19:00 PM
Surr: 4-Bromofluorobenzene
96.2
70 - 130
%Rec
100
3/12/2019 6:19:00 PM
Surr: Dibromofluoromethane
104
70 - 130
%Rec
100
3/12/2019 6:19:00 PM
Surr: Toluene-d8
107
70 - 130
%Rec
100
3/12/2019 6:19:00 PM
Qualifiers: E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine
area response
MC Value is below Minimum
Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column
confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal < MDI.
Page 7 of 35

U
Seunmit Environmental Technologies, hw,
3310 Win St,
Analytical Report
ffISMMIT-
E=F OTONMENTAL TECHNc3lOMF r, f,ffr
Cuyahoga Falls, Ohio 44223
(base report)
Itnoytical Labaraturdoy
TEL: [phone] FAX: [phone]
W0#: 19030418
Website: htty://ii wu,.settek.com
Date Reported: 3/20/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/5/2019 10:00:00 AM
Lab ID:
19030418-001A
.Project:
Harnett WTP
Client Sample ID Harnett WTP
Analyses
Result RL Qual Units
DF Date Analyzed
RC[-SOLID-W1 [GNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND
0.481 mg/Kg 1
3114/2019 4:00:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1
3/12/2019 12:30:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9045D
Analyst: V1/K
PH (SW9045D)
pH 5.2
s.u.@20.3C 1
311912D19 3:31:12 PM
RCI-SOLID-WI IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg 1
3114/2019 4:00:00 PM
Qualifiers: D
Value above quantitation range
M
Manual Integration used to determine area response
N
Tentatively identified compounds
O
RSD is greater than RSDlnmit
PL
Permit Limit
RL
Reporting Detection Urn it
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
i1 Samples with CalcVaI < MDL
Page 8 of 35

r:zr.0OU
Summit Eintronmenta7Technologies, Inc.
Accreditation
Program
S UMM 'i 3310 Win St.
Analytes Report
€NVIrtOMMENTAL r€C!i%si31.C1c;i
$,'WO Cuyahoga Falls, Ohio 44223
Analytlaat Laboraloriee
TEL: [phone] .FAX' [phone]
NVO#:
19030418
Website: httb:/Ann u+.settek.co" n
20 Mar-79
Client: Synagro
State: NW
Project: Harnett WTP
Program Name: NC WWSCM
Sample ID Matrix
Test Name
Analyte
Status
19030418-OOIA Sludge
lgnitabilityofSolids (SW-846:1030)
Ignitahility
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (901417.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
SVOC SW-846: 8151 Herbicides-TCLP
2,4,5-TP
A
Sludge
SVOC SW-846: 8151 Herbicides-TCLP
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW131116010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW131116010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SWI311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW131118081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
I-leptaehlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphepe
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW 131118270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW131119270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW131118270)
2,4-Dinitrotaluene
A
Sludge
TCLP Semi-Volatilos Analysis (SW 1311/8270)
Cresols, Total
A
Sludge
TCLP Setni-Volatiles Analysis (SW1311/9270)
Hexachlorobenzene
A
Sludge
TCLP Setni-Volatiles Analysis (SW 1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloraethane
A
Sludge
TCLP Semi-Volatiles Analysis (SWI311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachloroplrenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
ley
NC WW SCM A Accredited
NC WW SCM U Unavailable
Original #1
Page 9 of 35

SUMM111
_ Strnzrait Er�vironntental Technologies, Inc. Accreditation Program
3310 Win St. Anal tes Report
ERVIRONMENTAL TECFBhif9C.CfGI S, INC Cuyahoga Falls, 017io 44223 y P
AnafyOcal Libarator{pLc TEL: [phone] FAX.- [phone] WO#: 19030418
Website; h[lp:1Avww.settek.corn
20-Mar-19
Client: Synagro State: NW
Project: Harnett WTP Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
I9030418-OOIA Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
'TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original 41
Page 10 of 35

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENV1f10l IMEWALTECNNc)I. MS, INC
Cuyahoga Falls, Ohio 44223
�VO#�: 19030418
Ar:2P}rtJcal L_4b0rad0,rJes
TEL: [phone] FAX.. [phone]
Website: http://vvvvw.settek.com
20-Mar-19
CIient:
Synagro
Project:
Harnett WTP
BatchID: 36332
Sample iD MB-36332
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg1L
Prep Date: 3/1112019
RunNo: 95664
lient ID: PBS
Batch ID: 36332
TestNo: SW8081 SW3510C
Analysis Date: 3/12/2019
SegNo: 1996798
analyte
Result
PQL SPK value SPK Ref Val
%REC LowUmit HighLimit RPD Ref Val
%RP❑ RPDLimit Qual
Chlordane, total
ND
0.0250
Toxaphene
ND
0.0500
Endrin
ND
0.00250
gamma-BHC
ND
0.00250
Heptachlor
ND
0.00250
Heptachlor epoxide
ND
0.00250 d
Methoxychior
ND
0.00250 d
Surr: TCMX
12.1
20.00 60.3 10 119 m
Surr: DCB
15.4
20.00 77.1 10 119
Sample ID LCS-36332
SampType: LCS
TestCode: TCLPSVOC- Units: mglL
Prep Date: 3MI12019
RunNc: 96664
client ID: LCSS
Batch ID: 36332
TestNo: SW8081 SW3510C
Analysis Date: 3/1212019
SegNo: 1996799
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref VaI
%RPD RPDLimit Quai
Endrin
0.0130
0.00250
0.0250
0
62.0
20
157
gamma-BHC
0.0112
0.00250
0.0250
0
44.7
22
137
Heptachlor
0.0105
0.00250
0.0250
0
42.2
24
121
Heptachlor epoxide
0.0117
0.00250
0.0250
0
46.9
27
152
Methoxychlor
0.0131
0.00250
0.0250
0
52.4
10
199
Surr: TCMX
12.8
20.00
64.0
10
119
Surr: DCB
16.7
20.00
83.5
10
119
Qualifiers; B Analyte detected in the associated Method Blank E Value above quantitation range H HoIding times for preparation or anal}
3 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 11 of 35

U ' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
1
3310 Win St.
EAdul34ONMENTAL Tf CflhiC7E f?Gt�S, INC Cuyahoga Falls, Ohio 44223 WO#: 19030418
A4galyglt:alLaborworw TEL. [phone] FAY..- [phone]
Website: hap:/hvivw.settek.com 20-Mat'-19
Client: Synagro
Project: Harnett WTP BatehlD: 36332
Sample ID 19030122-001AMS
SampType: MS
TestCode: TCLP-SVOC- Units: mg1L
Prep Date: 311112019
RunNo: 95664
Client ID: BatchQC
Batch ID: 36332
TestNo: SW8081 SW351CC
Analysis Date: 311212019
SegNo: 1996800
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
Endrin
ND
0.0250
0.0250
0
71.1
20
167
gamma-31-1C
ND
0.0250
0.0250
0
60.3
22
137 m
Heptachlor
ND
0.0250
0.0250
0
59.6
24
121
Heptachlor epoxide
ND
0.0250
0.0250
0
67.8
27
152
Methoxychlor
ND
0.0250
0.0250
0
77.8
10
199
Surr: TCMX
18.9
20.00
94.4
10
119
Surr: DCB
21.7
20.00
109
10
119
Sample ID 19030122-001AMSD
SampType: MSS
TestCode: TCLPSVOC- Units: mglL
Prep Date: 3111/2019
RunNo: 95664
Client ID: SatchQC
Batch ID: 36332
TestNo: SW8081 SW3510C
Analysis Date: 3/1212019
SegNo: 1996801
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Endrin
ND
0.0250
0.0250
0
56.7
20
157
0
0
30
gamma-BHC
ND
0.0250
0.0250
0
53.1
22
137
0
0
30
Heptachlor
ND
0.0250
0.0250
0
50.2
24
121
0
0
30
Heptachlor epoxide
ND
0.0250
0.0250
0
56.6
27
152
0
0
30
Methoxychlar
ND
0.0250
0.0250
0
59.1
10
199
0
0
30
Surr. TCMX
16.5
20.00
82.3
10
119
0
Surr: DCB
17.5
20.00
87.7
10
119
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation ranee H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Original
D Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds
ND
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 12 of 35

ITr
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
EKV111014fAFMTAL TE-CHNOLGGIF.5, INC Cuyahoga Falls, Ohio 44223
WO#: 19030418
d!tqfyClr-z:'r i zr5cr.r,3idr'leg TEL: [phone] FrIX:- [phone]
Wehsite: httn://iviviv.settek.com 20-Mar-19
Client: Synagro
Project: Harnett WTP BatchTD: 36356
Sample ID MB-36356
SampType: MBLK
TestCode: MTL-TCLP-7( Units: mglL
Prep Date: 311312019
RunNo: 95756
Client ID: PBS
Batch ID: 36356
TestNo: SW6010D SW3010A
Analysis Date: 311512019
SegNo: 2000340
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5A0
TCLP Cadmium(Ccl)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-36356
SampType: LCS
TestCode: MTL-TCLP-7( Units: mglL
Prep Date: 311312019
RunNo: 95756
Client ID: LCSS
Batch ID: 36356
TestNo: SW6010D SW3010A
Analysis Date: 3115/2019
SegNo: 2000349
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.12
0.500
2.000
0
106
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
107
80
120
TCLP Cadmium(Cd)
1.94
0.100
2.000
0
97.0
80
120
TCLP Chromium(Cr)
2.19
0.200
2.000
0
110
80
120
TCLP Lead(Pb)
2.20
0.500
2.000
0
110
80
120
TCLP Selenium(Se)
2.15
0.0500
2.000
0
'108
80
120
TCLP Silver(Ag)
2.32
0.500
2.000
0
116
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
l Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 13 of 35

ill Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summ3310 Win St.
E%tirII101,1MENTAL'TEC4NOLOGIC-8, 11RC Cuyahoga Falls, Ohio 44223
WO#: 1903041$
Apt ;l,n:'c J i �h�rraldt� t TEL: [phone] FAX: [phone]
Website: httn:/wiviv.settekcom 20-1V1ar--19
Client: Synagro
Project: Harnett WTP BatchED: 36374
3ampie I❑ LCS-36374
SampType: LCS
TestCcde:
TCLP-SVOC_ Units: mg1L
Prep Date: 3/1312019
RunNo: 95730
client ID: LCSS
Batch ID: 36374
TestNo:
SWO270 SW3510C
Analysis Date: 3/14/2019
SegNo: 2008532
4nalyte
Result
PQL
SPK value SPK Ref Val
°/oREC Lowtimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.352
0.0400
MOM
0
44.0
19.1
126
2,4,5-Trichlorophenol
0.545
0.100
0.8000
0
68.2
11.7
151
2,4,6-Trichlorophenol
0.588
0,100
0.8000
0
73.5
12.4
150
2.4-Dinitrotoluene
0.654
0.0200
0.8000
0
81.8
20.6
140
Cresols, Total
ND
2.00
1.600
0
58.1
10
129
Hexachloro-1,3-butadiene
0.267
0.00800
0.8000
0
33.3
14.7
137
Hexachlorobenzene
0.607
0.0200
0.8000
0
75.9
12
139
Hexachloroethane
0.262
0.0400
0.8000
0
32.8
14.8
132
Nitrobenzene
0.533
0.0400
0.8000
0
66.6
15.6
138
Pentachlorophonol
0.666
0.100
0.8000
0
83.3
10
156
Pyridine
0,215
0.100
0.8000
0
26.8
1
130
Surr: 2-Fiuorophenol
0.434
1.000
43.4
10
147
Surr: Phenol-d6
0.460
1.000
46.0
10
140
Surr. Nitrobenzene-d5
0.582
1.000
58.2
10
169
Surr: 2,4,6--Tribromophenol
0.699
1.000
69.9
10
185
Surr: 2--Fluorobiphenyl
0.575
1.000
57.5
10
169
Surr: p-Terphenyl-d14
0.975
1.000
97.5
10
179
Sample ID 19030451-003AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg1L
Prep Date: 3/13/2019
RunNo: 95730
Client ID: BatchQC
Batch ID: 36374
TestNo: SW8270 SW3510C
Analysis Date: 311412019
SegNo: 2008533
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowtimit HighLimit RPD Ref Val
%RPD RPDLimit QuaI
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal;
3 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Original
ND Not Detected 0 RSD is greater than LRSDIimit P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery Iimits RL Reporting Detection Limit
Page 14 of 35

summier
SummaEnv(ronmenlal Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
Etkw1fs0NMEWAL TECHN0[-0GiF$, INC
Cuyahoga Falls, Ohio 44223
WO#: I9030418
elnalyffwl Laboratorjeis
TEL: [phone] FA' [phone]
X.
Website; hQ,-11ivivw.settek,com
20 Mar-19
Client:
Synaa o
Project:
Harnett WTP
BatchID: 36374
Sample ID 19030451-003AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mglL
Prep Date: 311312019
RunNo: 95730
client ID: BatchQC
Batch ID: 36374
TestNo: SW8270 SW3510C
Analysis Date: 311412019
SegNo: 2008533
4nalyte
Result
PQL SPK value SPK Ref Val
%PEC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.398
0.0800
0.8000
0
49.7
15.2
124
2,4,5-Trichlorophenol
0.500
0.200
0.8000
0
62.4
30.6
152
2,4,6-Trichlorophenol
0.597
0,200
a.8000
0
74.6
27.6
150
24-Dinitrotoluene
0.608
0.0400
0.8000
0
76.0
58
141
Cresols, Total
ND
4.00
1.600
0
65.5
27.6
132
Hexachloro-1,3-butadiene
0.325
0.0160
0.8000
0
40.6
-5.3
166
Hexachlorobenzene
0.582
0.0400
0.8000
0
72.8
54.3
142
Hexachloroethane
0.310
0.0800
0.8000
0
38.7
1.92
131
Nitrobenzene
0.716
0.0800
0.8000
0
89.5
21
135
PentachlorophenoI
0.595
0.200
0.8000
0
74.4
47.4
134
Pyridine
0.242
0.200
0.8000
0
30.2
-10.3
64.2
Surr.2-Fluorophenol
0.495
1.000
49.5
9.77
146
Surr: Phenol-d6
0.518
1.000
51.8
20.7
130
Surr: Nitrobenzene-d5
0.633
1.000
63.3
13.9
156
Surr.2,4,6-Tribramophenol
0.643
1.000
64.3
27.3
183
Sum 2-FIuorobiphenyI
0.616
1.000
61.6
21 A
153
Surr: p-Terphenyl-d14
0.903
1.000
90.3
54.8
154
Sample ID 19030451-003AMSD
SampType: MSD
TestCode: TCLPSVOC^ Units: mglL
Prep Date: 3113/2019
RunNo: 95730
Client ID: BatchQC
Batch ID: 36374
TestNo: SW8270 SW3510C
Analysis Date: 3/1412019
SegNe: 2008547
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal;
7 Analyte detected below quantitation limits M Manual Integration used to detennine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds OI15Trial
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 35

Summit Environmental Technologies, Inc.
SUMM1 3310Win St.
EP�ti+It?ON61EWrAL rfCliNO! ^ - Cuyahoga Falls, Ohio 44223
Anaf lticaf Laboraxoner TEL: [phone] FAX- [phone]
Website: httn:llwivw.settek.com
QC SUMMARY REPORT
WO#: 19030418
20 Mar-X 9
Client: Synagro
Project: Harnett WTP Bateh[D: 36374
Sample ID 19030451-003AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg1L
Prep Date: 311312019
RunNo: 95730
DIient ID: Batch=
Batch ID: 36374
TestNo: SW8270 SW3510C
Analysis Date: 311412019
SegNo: 2008547
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.362
0.0800
0.8000
0
45.2
15.2
124
0.3976
9.37
30
2,4,5-Trichlorophenol
0.528
0.200
0.8000
0
66.1
30.6
152
0.4996
5.60
30
2,4,6-Trichlorophenol
0.617
0.200
0,8000
0
77.2
27.6
150
0.5968
3.36
30
2,4-Dinitrotoluene
0.616
0,0400
0.8000
0
77.0
58
141
0.6080
1.24
30
Cresols, Total
ND
4.00
1.600
0
65.4
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.278
0.0160
0.8000
0
34.8
-5.3
155
0,3248
15.5
30
Hexachlorobenzene
0,596
0A400
0.8000
0
74.5
54.3
142
0.5820
2.38
30
Hexachloroethane
0.280
0.0800
0.8000
0
35.0
1.92
131
0.3096
10.2
30
Nitrobenzene
0.686
0.0800
0.8000
0
85.7
21
135
0.7160
4.34
30
Pentachlorophenol
0.589
0.200
0.8000
0
73.6
47.4
134
0.5948
0.946
30
Pyridine
0.306
0.200
0.8000
0
38.3
-10.3
64.2
0.2416
23.5
30
Surr:2-FluorophenoI
0,453
1.000
45.3
9.77
146
0
Surr: Phenol-d6
0.501
1.000
50.1
20.7
130
0
Surr. Nitrobenzene-d5
0.568
1.000
56.8
13.9
156
0
Surr: 2,4.6-Tribromophenol
0,698
1.000
69.8
27.3
183
0
Surr:2-Flucrobiphenyl
0.562
1.000
56.2
21.4
153
0
Surr: p-Terphenyl-d14
0.943
1.000
94.3
54.8
154
0
Sample ID MB-36374
SampType: MBLK
TestCode: TCLP-SVOC_ Units: mglL
Prep Date: 311312019
RunNo: 95730
Client ID: PBS
Batch ID: 36374
TestNo: SW8270 SW3510C
Analysis Date: 311412019
SegNo: 2008567
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range IT Holding times for preparation or anal
1 Analyte detected below quantitation Iimits M Manual Integration used to determine area response MC Val ue is below Minimum Compound
ND Not Detected O RSD is greater than RSDIiit P Second column confirmation exceeds Original
m
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 16 of 35

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
f°iV ROMMENTAL TEC3iNOLOCICS, WC
Cuyahoga Falls, Ohio 44223
W04: 19030418
An&0yt€calf Laboraterlas TEL: [phone] FAX.- [phone]
Website: httb://ivtvw.settelccom
20-Mar-19
Client:
Synagro
Project:
Harnett WTP
DatchID: 36374
Sample ID MB-36374
SampType: MBLK
TestCode: TCLP-SVQC_ Units: mglL.
Prep Date: 3/13/2019
RunNo: 95730
Client ID: PBS
Batch ID: 36374
TestNo: SW8270 SW3510C
Analysis Date: 311412019
SegN0: 2008567
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl.imit RPD Ref VaI
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichlorophenol
ND
0.100
2,4-Dinitroteluene
ND
0.0200
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenoi
ND
0.100
Pyridine
ND
0.100
Surr: 2-Fluorophenol
0.342
1.000
34.2
10
109
Surr: Phenol-d6
0.368
1.000
36.8
10
109
Surr. Nitrobenzene-d5
0.446
1.000
44.6
19
120
Surr: 2,4,6-Tribromophenal
0.491
1.000
49.1
10
120
Surr: 2-Fiuorobiphenyl
0.431
1.000
43.1
22
117
Surr: p-Terphenyl-d14
0.721
1.000
72.1
34
116
Qualifiers: B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal)
J Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery
limits
RL
Reporting Detection Limit
Page 17 of 35

U'M' Summit Environmental Technologies, Inc. 3310 YYin St. QC SUMMARY REPORT
r:KVII?OIJMEWAL 1 PcHNot [3c,'- r Cuyahoga Falls, Ohio 44223 WO#: 19030418
,ilrrad?`f.lc P taborgiones TEL: [phone] FAX.- [phone]
Website: httn:11www.se1tek.com 20-Mar-19
Client: Synagro
Project; Harnett WTP BatchID: 36399
Sample ID MB-36399
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/1512019
RunNo: 95790
Client ID: PBS
Batch ID: 36399
TestNo: SW7470A SW7470A
Analysis Date: 3/1512019
SegND: 2001219
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-36399
SampType: LCS
TestCode: HG TCLP(74 Units: PPM
Prep Date: 3/1512019
RunNo: 95790
Client ID: LCSS
Batch fD: 36399
TestNo: SW7470A SW7470A
Analysis Date: 311512019
SegNo: 2001220
Arialyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00406 0.00200 0.00400 0 102 80 120
Sample ID 19030559-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 311512019
RunNo: 95790
Client ID: BatchQC
Batch ID: 36399
TestNo: SW7470A SW7470A
Ana€ysis Date: 311512019
SegNo: 2001472
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury 0.00419 0.00200 0.00400 0.000100 102 75 125
Sample 1D 19030559-OOIAMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 311512019
RunNo: 95790
Client ID: BatchQC
Batch ID: 36399
TestNo: SW7470A SW7470A
Analysis Date: 311512019
SegNo: 2001473
Analyte
Result
PQL SPK value SPK Ref Val
°/cREC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00415 0.00200 0.00400 0.000100 101 75 125 0.00419 0.959 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal;
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits AL Reporting Detection Limit
Page 18 of 35

' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
suftiml3310 Win St.
ENVJQWJPJcFMAL TECHN007,G195.INC Cuyahoga Falls, Ohio44223
s3?r�fi�i'lC�i L��:traFarids TEL: [phone] FAX: [phone]
WO#: 19030418
Website: httn://www.settek.com 20-Mar-19
Client: Synagro
Project: Harnett WTP 1BatchlD: 36399
Sample ID 19030559-001AMSD
SampType: MSD
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 3115/2019
RunNo: 95790
Client ID: Batch=
Batch ID: 36399
TestNo:
SW7470A SW7470A
Analysis Date: 3115/2019
SegNe: 2001473
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Quaf
Qualifiers: B Analyte detected in the associated Method Blank F Value above quantitation range H Molding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 35

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summlir 3310 Win St.
EP.VirtON1dEWTAL t€chmolOC31=5, IPxC Cuyahoga Falls, Ohio 44223
ArwfyrOcaf L&bcraaartes TEL: [phone] FAX- [phone] WO#: I903041$
Websire: http://wivw.settek.com 20 Mar-19
Client: Synagro
Project: Hamett WTP BatchED: 36408
Sample ID mb-36408
SampType: MBLK
TestCode: tclp-SVOC-H Units: rnglL
Prep Date: 311412019
RunNo: 95900
Client ID: PBS
Batch ID: 36408
TestNo: SW8151A SW8151A
Analysis Date: 3/1912019
SegNo: 2006992
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowUmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 d
2,4,5-TP ND 0.500 d
Surr: 2,4-Dichlorophenylacetic acid 379 500.0 75.9 20 140
Sample ID ICS-36408
SampType: LCS
TestCode: tclp-SVOC-H Units: mglL
Prep Date: 311412019
RunNo: 95900
Client ID: LCSS
Batch ID: 36408
TestNo: SW8151A SW8151A
Analysis Date: 3/19/2019
SegNo: 2006993
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref VaI
%RPD RPDLimit QuaI
2,4-D
ND
1.00 0.500
0 70.0
37
105
2,4,5-TP
ND
0.500 0.500
0 63.5
38
106
Surr: 2,4-Dichlorophenylacetic acid
402
500.0
80.3
20
140
Sample ID 19030418-001ams
SampType: MS
TestCode:
tclp-SVOC-H Units: mglL
Prep Date: 311412019
RunNo: 95900
Client ID: Harnett WTP
Batch ID: 36408
TestNo:
SW8151A SW8151A
Analysis Date: 311912019
SegNo: 2006994
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit QuaI
2,4-D ND 1.00
0.500 0 69.2 37
105
2,4,5-TP ND 0.500
0.500 0 63.2 38
106
Surr. 2,4-Dichlorophenylacetic acid 417
500.0 83.5 20
140
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal}
.l Analyte detected below quantitation limits
ND Not Detected
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
MC
P
Value is below Minimum Compound
Second column confirmation exceeds Original
PL Permit Limit
R RFD outside accepted recovery limits
AL
Reporting Detection Limit
Page 20 of 35

SUMMIT
Summit Environmental Technologies, Ina 3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TE CHN€7LoGli55, INC
Cuyahoga Falls, Ohio 44223
W04: 19030418
Anaf r0caf Laboratories TEL: [phone] FAX.- [phone]
Website: httmllhN iv.settek.com
20-Mar-19
Client:
Synagro
Project:
Harnett WTP
SatchID: 36408
iampie ID 19030418-001amsd
SampType: MSD
TestCode: tclp-SVOC-H Units: mglL.
Prep Date: 311412019
RunNo: 95900
;lient ID: HarnettWTP
Batch ID: 36408
TestNo: SW8151A SW8151A
Analysis Date: 3/19/2019
SegNo: 2006995
#nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDUrnit Qual
2,4-D ND I.00 0.500 0 76.1 37 105 0 0 30
2,4,5-TP ND 0.500 0.500 0 71.2 38 106 0 0 30
Surr: 2,4-Dichlorophenylacetic acid 472 500.0 94.5 20 140 0 30
Qualifiers: B Analyte detected in the associated Method Stank E Value above quantitation range H Holding times for preparation or anal}
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 21 of 35

, ' Summit Environmental Technologies, Inc. { �C S V � i ltl'�1 OR 1
3310 Win St. `t
ENVI130)4MENTAL IECHNOLL GTI, .S, NC' Cuyahoga Falls: Ohio 44223 WO#: 19030418
AnjNUc, ? Lnboratoroes TEL: [phone]?11 FAX.- [phone]
Website: http://wwtiv.settek.com 20-Mar-19
Client: Synagro
Project: Harnett WT'P BatchED: R95604
Sample ID LCS-R95604
SampType: LCS
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: LCSS
Batch ID: R95604
TestNo: SW1030
Analysis Date: 311212019
SegNo: 1994382
AnaIyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 7.84 7.240 0 108 70 130
Sample ID 19030190-001ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: Batch=
Batch ID: R95604
TestNo:
SW1030
Analysis Date: 311212019
SegNo: 1994384
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19030281-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 95604
Cfent iD: BatchQC
Batch ID: R95604
TestNo: SW1030
Analysis Date: 311212019
SegNo: 1994386
AnaIyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19030364-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: BatchQC
Batch ID: R95604
TestNo: SW1030
Analysis Date: 3/1212099
SegNo: 1994388
AnaIyte
Result
PQL SPK value SPK Ref Val
%REC LowUmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: B AnaIyte detected in the associated Method Blank E VaIue above quantitation range H Holding times for preparation or anal;
J AnaIyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 22 of 35

'
SUMMN3310
Summit Environmental Technologies, Inc.
Win St.
QC SUMMARY REPORT
Et�YlYt4lJMENTAL'Cl7Nt7t+G15,7Nr.
(L rbcra caag
Cuyahoga Falls, Ohio44223
TEL: [phone] FAX- [phone]
WO#t: 19U3041$
Website: http:IA",)v.,3ettek.com
20-Mar-19
Client:
Synagro
Project:
Harnett WTP
BatchiD: R95604
IgnitabiIity non-flammable 0 0 20
IgnitabiIity non-flammable 0 0 20
IgnitabiIity non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
I Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 23 of 35

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summilu 3310 Win St.
EkVIttONMENTAL McHNOLc q�u:S, iNCL Cuyahoga Falls, Ohio 44223
Anafy0caf Labarialdnes TEL: [phone] FAX.- [phone] W0�#: I90304I8
Website: ham://x,ivu,.settek.com 20 Mar-19
Client: Synagro
Project: Harnett W"1P BatchID: R95638
Sample 1D LCS-95638
SampType: LCS
TestCode: voc-mstr_np Units: mglL
Prep Date:
RunNo: 95638
client 1D: LCSW
Batch ID: R95638
TestNo: SW8260
Analysis Date: 311212019
SegNo: 1995888
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RP❑ RPDLimit Qual
1,1-Dichloroethene
0.0207
0.00500
0.0200
0
104
70
138
1,2-Dichloroethane
0.0224
0,00500
0.0200
0
112
70
130
MEK
0.0965
0.0250
0A00
0
96.5
70
130
Benzene
0.0199
0.00500
0.0200
0
99.5
10
199
Carbon tetrachloride
0.0215
0.00500
0.0200
0
107
21.3
240
ChIorobenzene
0.0209
0.00500
0.0200
0
105
70
132
Chloroform
0.0200
0.00500
0.0200
0
100
70
130
Tetrachloroethene
0.0210
0.00500
0.0200
0
105
10
130
Trichloroethene
0.0202
0.00500
0.0200
0
101
70
130
Vinyl chloride
0.0166
0.00200
0.0200
0
83.2
70
130
Sum 4-Bromofluorobenzene
50.1
50.00
100
70
130
Sum ❑ibromofluoromethane
57.6
50.00
115
70
130
Surr: Toluene-d8
52.9
50.00
106
70
130
Sample ID MB-95638
SampType: MBLK
TestCode: voc-mstr np Units: mglL
Prep Date:
RunNo: 95638
,lient ID: PBW
Batch ID: R95638
TestNo: SW8260
Analysis Date: 3/12/2019
SegNo: 1995890
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or aria]!
T Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Lnnit R RPD outside accepted recovery- limits RL Reporting Detection Limit
Page 24 of 35

Summit Environmental Technologies, Inc, QC SUMMARY "PORT
vsummi3310 Win St. 1
EPWRIONIAENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 W04: 19030418
Arrailytfcal LabnrstarRes TEL: [phone] FAX: [phone]
Website: httn://�vwiv.settekcom 20-Mar-19
Client: Synagro
Project: Harnett WTP BatchID: R95638
iample ID MB-95638
SampType: MBLK
TestCode: voc-mstr_np Units: mg1L
Prep Date:
RunNo: 95638
;lienf ID: PBW
Batch ID: R95638
TestNo: SW8260
Analysis Date: 3/12/2019
SegNo: 1995890
lnalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
47.5
Surr: Dibromoflucromethane
51.8
Surr: Toluene-d8
51.2
50.00 95.0 70 130
50.00 104 70 130
50.00 103 70 130
iample ID 19030589-009aMS
SampType: MS
TestOode: voc-mstr_np Units: mg1L
Prep Date:
RunNo: 95638
,lient ID: BatchQC
Batch ID: R95638
TestNo: SW0260
Analysis Date: WiV2019
SegNo: 1995911
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit QuaI
1,1-Dichloroethene
0.862
0.250
1.00 0 86.2
63.8
148
1,2-Dichloroethane
1.05
0.250
1.00 0 105
70
130
MEK
4.14
1.25
5.00 0 82.8
10
130
Benzene
1.74
0.250
1.00 0.805 93.6
70
130
Carbon tetrachloride
0.862
0.250
1.00 0 86.2
70
130
Chlorobenzene
0.996
0.250
1.00 0 99.6
70
130
Chloroform
0.915
0.250
1.00 0 91.5
70
130
Tetrachloroethene
1.06
0.250
1.00 0 106
70
130
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quamitation range
H
Holding times for preparation or anal`
I
Analyte detected below quantitation limits
M
Manual Integration used to determine area
response
MC
Value is below Minimum Compound
Original
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 25 of 35

SUMMIT
Summit Environmental Technologies, Inc. 3310 Pi'in Si. QC SUMMARY REPORT
EkMll??N kIENTAL TEC4N0 Wru-5, INC. Cuyahoga Fails, Ohio 44223
WQ#: 19030418
Arf3iy0c.t1 L3bcrrarot'!8s TEL: [phone] FAX. [phone]
We6site: hM.Ilwww.settek.com 20-Mar-19
Client: Synab o
Project: Harriett WTP BatchZll: R95638
Sample ID 19030589-009aMS
SampType: MS
TestCode: voc-mstr_np Units: mg1L
Prep Date:
RunNo: 95638
Client ID: BatchQC
Batch ID: R95638
TestNo: SW8260
Analysis Date: 311212019
SegNo: 1995911
Analyte
Result
PQL SPK value SPK Ref Val
%RFC Lowl-imit HighUmit RPD Ref Val
%RPD RPDLimit Qual
Trichloroethene
0.936 0.250
1,00
0 93.6
70
130
Vinyl chloride
0.690 0.100
1,00
0 69.0
53.9
141
Surr:4-Bromofluorobenzene
2470
2500
98.8
70
130
Surr: Dibromofluoromethane
2680
2500
107
70
130
Surr: Toluene-d8
2650
2500
106
70
130
Sample ID 19030589-009aMS❑
SampType: MSD
TestCode:
voc-mstr_np Units: mg1L
Prep Date:
RunNo: 95638
Client ID: BatchQC
Batch ID: R96638
TestNo:
SW8260
Analysis Date: 3/1212019
SegNo: 1995912
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RP❑ RPDLimit Qual
1,1-Dichloroethene
0.810
0.250
1.00
0
81.0
63.8
148
0.862
6.22
30
1,2-Dichloroethane
1.03
0.250
1.00
0
103
70
130
1.05
2.69
25
MFK
4.29
1.25
5.00
0
85.8
10
130
4.14
3.48
25
Benzene
1.72
0.2,90
1.00
0.805
91.3
70
130
1.74
1.36
30
Carbon tetrachloride
0.787
0.250
1.00
0
78.7
70
130
0.862
9.15
25
Chlorobenzene
0.987
0.250
1.00
0
98.7
70
130
0.996
0.858
30
Chloroform
0.901
0.250
1.00
0
90.1
70
130
0.915
1.54
25
Tetra chloroethene
0.996
0.250
1.00
0
99.6
70
130
1.06
5.99
26
Trichloroethene
0.922
0.250
1.00
0
92.2
70
130
11.936
1.51
30
Vinyl chloride
0.654
0.100
1.00
0
65.4
53.9
141
0.690
5.51
25
Surr:4-Bromofluorobenzene
2410
2500
96.5
70
130
0
25
Surr: Dibromofuoromethane
2690
2500
108
70
130
0
25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H HoIding times for preparation or anal;
1 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 26 of 35

SUMMI
Summit Environmental Technologies, 331 p WinSSt, QC SUMMARY REPORT
t.
EkulitQt,ErtEtsTAL TECHNE)LOGI€S, INC Cuyahoga Falls, Ohio 44223
WO#: 19030418
ArraPyrJcai c.alsoratarlas TEL: [phone]I FAX.- [phone]
YYebsite: htt ://www.settekcom 20-Mar-19
Client: Synagro
Project: Harnett WTP BatchID: R95638
Sample ID 19030589-009aMSD
SampType: MSD
TestCode: voc-mstr_np Units: mg1L
Prep Date:
RunNo: 95638
client ID: Batch=
Batch ID. R96638
TestNo: SW8260
Analysis Date: 3/12/2019
SegNo: 1995912
%nalyte
Result
PQL SPK value SPK Ref Val
%REC LowUmit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sum Toluene--d8
2650
2500
105 70 130
0 25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 27 of 35

SUMM111
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
ER Vii'tOtJ1AENTALTECHNOLQG7ES, 1KC
Cuyahoga Falls, Ohio 44223
Artaipi al Labafalones TEL: [phone] FAX: [phone]
WO#: 19030418
IWebsite. ham_:/Cwiviv;settek.com
20-Mar-19
Client:
Synagro
Project:
Harnett WTP
BatehiD. R95757
Cyanide, Reactive ND 0.490
Cyanide, Reactive 9.54 0.485 10.00 0 95.4 85 110
Cyanide, Reactive ND 0.485 0.5000 0 95.3 50 150
Cyanide, Reactive
9.61 0.495
10.00 0.2400 93.7 81.6
122
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal}
7
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
O RSD is greater than RSDliinit
P
Second column confirmation exceeds Original
PL
Pen -nit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 28 of 35

SUMMI330 Summit Environmental Technol10 Win St. es, Inc. QC SUMMARY REPORT
Et4'Jlt#Cit,EllE3JTRL FEi~4iN4[�sPS, :Nfi Cuyahoga Falls, Ohio 44223
ArraiyVcat Latsoraiones TEL: [phone] FAX: [phone] WO#: 19030418
Website: httpa/wwtii+.settekcom 20-Mar-19
Client: Synagro
Project: Hamett WTP Batch ID: R95757
Sample ID 19030656-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 95757
Client ID: BatchQC
Batch ID: R95757
TestNo: SW9014
Analysis Date: 311412019
SegNo: 2000212
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Re# Val
%RPD RPDLimit Qua]
Sample ID 19030656-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mglKg
Prep Date:
RunNc: 95757
Client ID: SatchQC
Batch ID: R95757
TestNo: SW9014
Analysis Date: 311412019
SegNo: 2000213
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.57 0.490 10.00 0,2400 93.3 81.6 122 9.608 0.354 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H HoIding times for preparation or anal}
3 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than R-Mlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 29 of 35

Summit Environmental Technologies, Inc, ummill 3310 Win St. QC SUMMARY
REPORT
04uIO014MEt4TAL r1=C%iNOJ..I� l�r'$, INC: Cuyahoga Falls, Ohio 44223
A.M'W rtdcaf Labaralaws TEL: [phone] FAX.- [phone] WO#: 19030418
Website: http:lAvivTv.settek.com 20-Mar-19
Client: Synagro
Project: Harnett WTP Batehll): R95759
Sample ID MB-R95759
SampType: MBLK
TestCode: Sulfide,React Units: mglKg
Prep Date:
RunNe: 95759
Client ID: PBS
Batch ID: R95759
TestNo: SW9034
Analysis Date: 311412019
SegNo: 2000573
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R95759
SampType: LCS
TestCode: Sulfide,React Units: mglKg
Prep Date:
RunNo: 95759
Client ID: LCSS
Batch ID: R95759
TestNo: SW9034
Analysis Date: 3/1412019
SegNo: 2000574
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4710 25.0 4800 0 98.1 85 115
Sample ID 19030656-001AMS
SampType: MS
TestCode: Sulfide,React Units: mglKg
Prep Date:
RunNo: 95759
Client ID: SatchQC
Batch ID: R95759
TestNo: SW9034
Analysis Date: 311412019
SegNo: 2000585
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4320 25.0 4800 0 90.0 80 120 W
Sample ID 19030656-001AMSD
SampType: MSD
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 95759
Client ID: BatchQC
Batch ID: R95759
TestNo:
SW9034
Analysis Date: 311412019
SegNo: 2000586
Anafyte
Result
PQL
SPK value SPK Ref Val
%RFC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 4530 25.0 4800 0 94.4 80 120 4320 4.75 30 W
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
I Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSA is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Litnit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 30 of 35

summi
st 3310 WinSfSummit Environmental Technologies, St. QC SUMMARY REPORT
.
EFSVlf2OtJldl=t4TALTECHNOWr# ]rS, INC Cuyahoga Falls, Ohio 44223
AnafyNcal iabaratarias TEL: [phone] FAX., [phone] WO#: 1903Q418
Website: hQ://www.settek.com 20 Mar-19
Client: Synagro
Project: Harnett WTP P,atehlD: R95759
Sample ID 19030656-001AMSD
SampType: MS❑
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 95759
:;lient 1D: BatchQC
Batch ID: R95759
TestNo: SW9034
Analysis Date: 311412019
SegNo: 2000586
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal;
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 31 of 35

su ''� Win
Summit Environmental QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TEC!iR10LCk�t�$, INC Cuyahoga Falls, Ohio 44223
larr$ffr[,' ant iai3or8tcrte� TEL: [phone]I1 FAX.- [phone]
WO#: 19030418
Wehsite: http:/hvtiviv.settek com 20-Mar-19
Client: Synagro
Project: Harnett WTP BatchID: R95888
Sample ID CHECK 7
SampType: LCS
TestCode:
pH_S(9045D) Units: s.u.@20.7C
Prep Date:
RunNo: 95888
Client ID: LCSS
Batch ID: R95888
TestNo:
SW9045D
Analysis Date: 3119/2019
SegNe: 2006953
Analyte
Result
PQL
SPK value SPK Ref Val %REC
Lowl-imit HighLlmit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.6 90 110
Sample ID CHECK 7
SampType: LCS
TestCode:
pH_S(9045D) Units: s.u. 21.1C
Prep Date:
RunNo: 95888
Client ID: LCSS
Batch ID: R95888
TestNo:
SW9045D
Analysis Date: 311912019
SegNa: 2006961
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit QuaI
pH 7.0 7.0 0 99.4 90 110
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 32 of 35

summly
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
EPWIP01VIdEWAL TECHNOi R =7-3, Cuyahoga Falls, Ohio 44223
Ani� ly?fcrP Laborayconas TEL: [phone] FAX: [phone] WO#: 19030418
Website: http://wwiv.settek.coni 20-Mar-19
Client: Synagro
Project: Harnett WTP BatchID: R95888
Sample ID LCS-R95888
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@19.9C
Prep Date:
RunNo: 95888
Client ID: LCSW
Batch ID: R95888
TestNo: SW9045D
Analysis Date: 3/1912019
SegNo: 2005784
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLlmit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID 19030814-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: S.u. ,20.1C
Prep Date:
RunNo: 95888
Client ID: BatchgC
Batch ID: R95888
TestNo: SW9045D
Analysis Date: 3/19/2019
SegNo: 2005787
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 6.8
6.7 0.4 5
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H HoIding times for preparation or anal}
3 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
fi
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 33 of 35

SA! lVIMIT
EiMf1TJR� TUCHNOI.OGJ18. INC.
3310 Win $~
C+ryouapa I'nM CWO 44223
eoa-vr.az�a
DC-QACOC339 R,, D
ur.-Daw-Im Is
Analysis Request / Chain of Custody
for Summit Environmental Technologies, Inc. use only
Page 34 of 35

J' y Sarnmait Environmental Technologies, Inc.
sum3310 Win St.
ENURC7tdl ENtTALttCal 1pLttCit,,tF1r, Cuyahoga Falls, Ohio44223 Sample Log -in Check List
AmOy+fical Laboratones TEL: [phone] FAX.- [phone]
Web3ne: ht ://tvtvtv.sett k.cont
Client Name: SYN-NC-27028 Work Order Number: 19030418 RcptNo: 1
Logged by: Christopher Livengood 3/8/2019 10:05;00 AM
Completed By: Christopher Liven good 3/8/2019 11:38:42 AM
Reviewed By; Jennifer Woolf - 2 3/12/2019 12:01:03 PM
Chain of Cus#ody
1. Is Chain of Custody complete?' Yes ❑ No ❑ Not Present ❑
2, How was the sample delivered? UPS
Loa In
3. Coolers are present? Yes ❑ No ❑ NA ❑
4. Shipping containerlcooler in good condition? Yes 0 No ❑
Custody seals intact on shipping containerlcooler? Yes ❑ No ❑ Not Present FV1
No. Seal Date: Signed By:
5, Was an attempt made to cool the samples? Yes 0 No ❑ NA ❑
6, Were all samples received at a temperature of >0° C to 6.0°C Yes 0❑ No ❑
7, Sample(s) in proper container(s)?
Yes
0
No ❑
8. Sufficient sample volume for indicated test(s)?
Yes
No ❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
No ❑
1 p• Was preservative added to bottles?
Yes
❑
No ❑�
11. Is the headspace in the VOA vials less than 114 inch or 6 mm?
Yes
❑
No ❑
12. Were any sample containers received broken?
Yes
❑
No
13. Does paperwork match bottle labels?
Yes
❑
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑
No ❑
15. Is it clear what analyses were requested?
Yes
No ❑
16. Were all holding times able to be met?
Yes
0
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
NA C_I
NA ❑
No VOA Vials M
17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA
Person Notified: Date
By Whom: Via: ❑ eMail Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Page 35 of 35