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HomeMy WebLinkAboutWQ0006017_Residual Annual Report 2019_20200302Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application r Annual Report what is the submittal r Residual Annual Report type?* r Additional Information r Other Annual Report 2019 Year* Date Paper Copy 3/2/2020 Received:* Project Number* WQ0006017 Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues. .......................................................................................................................................................................................................................................................................................................................................................................... Name * Lysa Finnerty Email Address* Ifinnerty@synagro.com Project Information Submittal Type* r New Permit Application r Renewal r Annual Report r Other Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted? r Yes r Nor N/A Permit Number* WQ0006017 Applicant\Permittee * SYNAGRO Facility Name * Town of Beaufort Phone Number* 4434899026 r Modification (Major or Minor) r Additional Information r Residual Annual Report r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. 2019 Annual Report for Beaufort Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) BEAUFORT NC 2019 Annual Report FINAL.pdf 10.5MB Upload only 1 R7F document. NL@iple documents must be combined into one R7F file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required, be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been received. The paper copy shall include the following: o Application Form o All relevant attachments {talcs, soils report, specs, etc.] o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) Mailine address: Division of Water Resources ! Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W - = Raleigh, NC 27699-1617 S12 N.5alisburySt. For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560. * rJ By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/27/2020 435 Williams Court, Suite 100 Baltimore, A4D 21220 -,\vw synagro. com FEBRUARY 27, 2020 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2019 Annual Report for Permit No. WQ0006017 Dear NCDEQ: Synagro is submitting one copy and one electronic copy of the above referenced report on behalf of the Town of Beaufort, NC. If you have any questions or need additional information, please do not hesitate to contact Donovan Willis at (252) 728-7166 or Melinda Boyd at 336-909-8627. Sincerely, Derrick Shivar Environmental Compliance Manager Enclosures cc: Donovan Willis - Town of Beaufort Melinda Boyd, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD TOWN OF BEAUFORT, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0006017 2019 ANNUAL REPORT Town of Beaufort, NC Residuals Land Application Program 2019 Annual Report TABLE OF CONTENTS Certification Form and Annual Operations Summary 2, Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Page 3. Annual Land Application Field Summary Form 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analysis SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM Permit Number W00006017 County Carteret Year2019 Facility Name (as shown on permit) Beaufort WWTP NPDES No. NCO021831 Land Application Operator SynaQro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year X YES NO. If NO, skip Part A, and PartB and proceed to Part C, Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary *Total number of application fields in permit. 2 *Total number of fields utilized for land application during the year. 1 *Total amount of dry tons applied during the year for all application sites. 86.33 *Total number of acres utilized for land application during the year. 23.40 Part B — Annual Compliance Statement Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 I05(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .I I I i were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality, 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. i t . Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12, No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Donovan Willis. Public Utilities Director Permiteee Name and Title (type or print)/ Signature of Preparer* Date (if different from Permittee) r Si f e i ee ate Signre of Land App er Date (if different from Permitter, and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2019 ANNUAL OPERATIONS SUMMARY a LAND APPLICATION IN NC BEAUFORT, NC BEAUFORT, NC AEROBICALLY DIGESTED CAKE MONTHNEAR May 2019 YEARLY TOTAL AMOUNT UNIT DRY TONS 625.00 Y 86.33 625.00 Y 86.33 DRY METRIC UNIT TONS D 78.30 D 78.30 1/30/2020 SECTION 2 0 m z "n O U) n cri N 0 0 z C ;[l m 0 'R -u m m 0 w D L Q. 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(D C-) O C �V, o a rn cn E CD MCDv {a a " CD =r C� CD Q C 0roa cn OL (D CD ro !: ; (D � o �r ° ° o O o �:3 � o > (ncLn: O 0-0 v ar 7 � QL) ((DD C ps p ^ o (a (D � Z)3m a' �h � � CD J O zF ❑l v � � CD (D ro -a (D ro 0 m 0 m D �0 n � o 3 v3 Q O O � w ro N n 0 CDo (D Er (o 07D (D c m � N (D 3 0 N (D m c m Q O Q• (D 3 N' (D Q. O 7 N --n 0 z z c 30 x y v c a /r w y a 3 r z a to c 3 0 3 Waypointo ANALYTICAL 4/30/2019 Synagro Central/Beaufort Marshall Puryear 284 Boger Road Suite 204 Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-108-0206 Project Description: Beaufort WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www,wayp o f nta n a l yti ca l.co m Dear Marshall Puryear: Waypoint Analytical Virginia, Inc. received sample(s) on 4/18/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pawn is' 6-r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Vlrginia 460014 Page 1 of 6 Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www,waypointanalytical.com Sample Summary Table Report Number: 19-108-0206 Client Project Description: Beaufort WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 65952 Beaufort WWTP Solids 04/16/2019 09:00 04/18/2019 65952 Beaufort WWTP Solids 04/16/2D19 09:00 04/18/2019 SM-4500-NH3C WTN 65952 Beaufort WWTP Solids 04/16/2019 09:00 04/18/2019 9045D WTN 65952 Beaufort WWTP Solids 04/16/2019 09:00 04/18/2019 450ONO3F-2011 WTN 65952 Beaufort WWTP Solids 04/16/2019 09:00 04/18/2019 6010D WTN 65952 Beaufort WWTP Solids 04/16/2019 09:00 04/18/2019 SW-74713 WTN 65952 Beaufort WWTP solids 04/16/2019 09:00 04/18/2019 SM-4500-NH3C-TKN WTN 65952 Beaufort WWTP Solids 04/16/2019 09:00 04/18/2019 SM-254OG WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2of6 W s co Cl) O z 0 a cm CD D m CD 0 3 0 CD (n Fn' D Z5 m m Z O N P E O 0 p�j C O S m 0 S m m o � w 0 En c' o m m _ � � Q �. Z (u (n v (n a z LaZ o (n rn Ln 0 0 0 0 0 0 0 cs co 3 w rn CD w C71 {Jt U7 �I w Ul CA o 0 rn o o Q oo co °' a s A a o �' CD a o0 0 0 N CD Q a N 0 0 0 a (7 O CDU1 O CD v Cl o (1i O a o 0 0 a a O O Q Q O 6 N c m qo X m W W W m W X m C- > D D � z Z�Z Z Z Z z Z Z E Z C-EE;: Q 0 0 o a a CD o a 0 0 0 a 0 0 o Q 4� .P 4�1, 4� A A .A 4�- 4� 4N -P� A .A 4�, 4�, A N N N N N N N N N N N N N N N N 0 0 0 0 0 0 o a 0 0 a Q 0 0 a a 0 8 1 s( a, -W o m co a 0 (a 0 c0 co co m co co 0 co co m P cn cfl to o m 0 0 (n o m co cfl cn N t y w W o CnW W w W W W 1 W C 1 4P 4�, cn 0 Ul m CTi 1 cn Cal m m 0 w U7 0 m m (n .A C� o D (fir, CA Cf Z C7 Crr al (D CD O7 0 n CD CA a (D O7 a0 � C7 Q o 0 o a O — Q o o i N h o c o � — �. � z -TiZ D D D D D C7 D D D D D CD a d O w Z 0 X Z b 0 L co CI�w I! v v o (D ((DD rt CD CD CD O M, N (CD (D a a a w j rn 0 m N 0 CD 1 0 ffl (fl CD 0 0 0 0 0 cn (D m a 0 U) N K co o pq.�m (D m C. a (a o (D C� G (D Z 0 Q D � a pr N OD 4 n ."4 c o Z a 3 R aCD - CD rn � 1 w a C.T1 co O N a O� L�� V a+ N Q "F V CD mw a o n) S fu X O z Do pQ n D N n � W G1 V o O a CD a m C a+ Q v m Sm o CD CL bN 5 � n t y � CDa m Q rr m � O m 2 � o o � CD � o O o w O O cn S O_ O � CD N b � o (gyp 4 o� o � � m o (D Z3 0 6] o w n� o n CD m 0 oS (D (D N can :� (D m 0 7 a a tT :3 0 c A A O A 4, N A. 1 IV CJi CT f n al CD CDO (D — C-0 O (DO i O O N Cn � Cn W N N C71 O O O Cn C31 O O O m O O O O O co [_ z r z M z z z z z 31V N N fV N N N N N W 4P W W W W W W W N N N N N N N N N O O O O O O O O O CO co (D co CD (D CD CD CO CD � O W CD CD CD CD CO W Ch W O W W W W W U1 W (31 N Ol Ch Ch m 0 m CD m C m W W W m O O O O O O O O o cn O O o 0 0 0 0 0 0 1 0 0 0 0 C� m r w s 3 CD a. Q W m W CO y Ch O N �C C "D m O C) r 0 W a o v M N rt CD 4 (D CD0 (D 0. Q O- O CD .A N N NO O O 1 co Cfl O O p O o C> o 0 6 O m m Q 0 0 co w C N O ti O [L2 _ O (D -0 0 C (D C) CL v CD O � N W rt a D � 0 CD 0 o c z rr C z a 3 s s CD (D O) (D 4h- j w O Ul Cb Q N O W V N OF rr O -0 V (D A 0 Di 4 Q 1� ;a � a n w X 0 7 � z w Q. D M. 6 N � V Waypoint,,. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www,waypointanalytical.com Cooler Receipt Form Customer Number: 46435 Customer Name: Synagro Central/Beaufort Report Number: 19-108-0206 Shipping Method 0 Fed Ex 0 US Postal 0 Lab • UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received F 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? • Yes 0 No COC agrees with sample [abel(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Water - Sample containers properly preserved 0 Yes 0 No r♦ NIA Water - VOA vials free of headspace 0 Yes 0 No NIA Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No NIA High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes No Comments: Signature: Brandi Watson Date & Time: 104118/2019 14:1t54 Page 5 of 6 9 jo 9 abed p� UM —Ia N Q U - crj z y. a —_ m cn C z cn D z A kD Q L — 0 ww�.. W 62cr z o Q ' i1 V Ch.0 Ln M Q g z m o. 0 Lei 0 r7 N CL o a. 01 W 0 CD cl cc b n C 13 n z S T N � m p = 0 C (n Q n � 0m G a 0 r'. F�O Eno 0 ci iF N iF o z N� CD N n 0O a (0 Cb CD m m m rD n n m CD C Q a. m D m pp Ro r � � rO M b� 0 zC) Cl' D mr, m 0 0 D� Q m m _ A rn m> m m mm m m m� m= �O Cd M 4 m 3: m 00 C D O m z m c z Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2226-01-AEDCAK-NC BEAUFORT, NC AEROBICALLY DIGESTED 4/16/2019 11112019-1213112019 0.5268 CAKE Na mgll = (Na mg/kg x % Solids) + 100 = (354 x 16.4000) + 100 = 58.056 Ca mg1l = (Ca mg/kg x % Solids) + 100 = (4710 x 16.4000) + 100 = 772.44 Mg mgll = (mg mg/kg x % Solids) + 100 = (534 x 16.4000) + 100 = 87.576 Na meq = Na mgll + Moloc.Wgt.Na = 58.056 + 23 = 2.52417 Ca meq = Ca mgll + Molec.Wgt.Ca = 772.44 + 20 = 38.622 Mg meq = Mg mgll + Molec.VVgt.Mg = 87.576 + 12 = 7.298 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.52417 + SgrRoot[0.5(38.622+7.298)] = 0.526785 Printed: 2/1/2020 Page 1 14:09 SECTION 3 CO O T7 d " C] C cr CA CD p O R 4 � fy n rn V cr b t�J w a � � � v R O � A W � J 41 w R w � o N a ro rn oa o VNi ` h7 w {[ , , 4 1 o � CD 4 O O P' O O N F a" 0 n n R 00 o 4� o, 0 Cl rn d d � R � N N O C R �r a o cn cn U U 6, T O O O O ro ro a It, q C, a, p o w ro ro z� z CD CD oa � a U is W W � � n O O o ✓y' � Y5 SECTION 4 summilu Srrnamit Environmental Technologies, Inc: 3310 Win St. FNVIRONMENIAL IECfltJOLOG1-�S, INC Cuyahoga Falls, Ohio 44223 Afraly iml Ctibnjreh36a3 TEL: (330) 253-8211 FAK- (330) 253-4489 Website: http://www.settek.conr April 25, 2017 Will Varner Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 999.7150 FAX: (336) 998-8450 RE: Beaufort Dear Will Varner: Order No.: 17040288 Summit Environmental Technologies, Inc. received 1 sample(s) on 416/2017 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Massachusetts M-OP11923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH00923201 1- 1, Vennont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 9957C Page 1 of 36 Suraalrait Enviaronnrental Technologies, Inc. MSUMMIT 3310 Win St. VMVIRONMENTAL ]ECONOLOGlE5, INC- Cuyahoga falls, Ohio 44223 ArrralVtiosl Labarstorivs TEL; (330) 253-8211 FAX: (330) 253-4489 Website: hap.-IM v.settek.coan CLIENT: Synagro Project: Beaufort WorkOrder Narrative: Case Narrative WO,#: 17040288 Date: 4/25/201.7 17040288: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the acereditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certif cates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies; Inc. and that -of the customer. It cannot -be reproduced in any -form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. WorkOrder Comments: Sample Receipt Temperature = 12.4C Original Page 2 of 36 Sunitnit E'nvii•onirtental Technologies, In %lualA�Ae1Cs and Acronyms SUMMINt 3310 Win 5 i� fKVIA.OM ENTAL IECBNOLC?CirS, irlr Cuyahoga Falls, Ohio 442� CVO#: 17040288 Arralytiea4 LaborWoFivs TEL: (330) 253-8211 FIX.- (330) 253-445 Website: http://w)v.settek.co Date: 4/25/2017 ti These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected, .I The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. Y The result exceeds the Regulatory Limit or Maximum Contamination Limit. rn Manual integration was used to determine the area response. N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confirmed when GUMS Analysis was performed. B/MS+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-l+ The CCV recovery failed low (-) or high (f). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits, QM-/ +- The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV -I+ The ICV recovery failed Iow (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitatim Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 36 rMSUMMIT Sur�rmitErrvira�nrel�tal Technologies, Irae. WOrl�Order 3310 Win St. MVIROMN1ENTAL ll± 4NOLOMESS, 1NQ Cuyahoga Falls, Ohio 44223 Sample Summary Arrafyfical t_abora odes TEL (330) 253-8211 FAX.- (330) 253-4489 WO##: 17040288 Website: h1tv:11www.setteh.com 25-Apr-17 CLIENT: Synagro Project: Beaufort Lab SampleID Client Sample iD Tag No Date Collected Date Received Matrix 17040299-001 Beaufort 3/29/2017 3:15:00 PM 416/2017 9:55:00 AM Sludge Page 4 of 36 .S'2lt777711t l'P7V lf'6f1I71L'i7ta1 T8C1111010gICS, Inc. Analytical Report SUMMIT 3310 Win St. (base report) Cuyahoga Fa113, Ohio 44223 fidlriRt33hJh1t=MTlEt_ ><gCi�d�OLOGt_5, 'Mc 7irralyficsf LalharatorJe5 TEL: (330) 253-8211 FAX.., (330) 253-4489 WO#: 17040288 Websile: htW.-11www.settek.Con7 Date Repotted: 4/25/2017 CLIENT: Syxaagro Matrix: SLUDGE Lab ID: 17040288-OOIA Project: Beaufort Client Sample ID Beaufort Tag Number: Collection Date: 3/29/2017 3:15:00 PM Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP MERCURY ANALYSIS (SW131117470) TCLP Mercury ND 0,00200 mg1L SW7470A SW7470A Analyst: ALJ 1 4/10/2017 4:39:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW601OC SW3010A Analyst: VVK TCLP METALS ANALYSIS (SW131116010) TGLP Arsenic(As) ND 0.500 mg/L 1 4/11/2017 10:32:31 AM TCLP Barium(Ba) ND 5.00 mg/L 1 4/11/2017 10:32i31 AM TCLP Cadmium(Cd) ND 0.100 mg/L 1 4/11/2017 10:32:31 AM TCLP Chromium(Cr) ND 0.200 mg/L 1 4/11/2017 10:32:31 AM TCLP Lead(Pb) ND 0.500 mg1L 1 4/11/2017 10:32:31 AM TCLP Selenium(Se) ND 0.500 mg/L 1 4/11/2017 10:32:31 AM TCLP Silver(Ag) ND 0.500 mg1L 1 4/11/2017 10:32:31 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270C SW351OC Analyst: CxA TCLP SEMI-VOLATILES ANALYSIS (SW131118270) 1,4-Dichlorobenzene ND 0.0300 mg/L 2 4/11/2017 12:40:00 PM 2,4,5-Trichlorophenol ND 0.200 mg/L 2 4/11/2017 12:40:00 PM 2,4,6-Trichlorophenol ND 0.200 mg/L 2 4/11/2017 12:40:00 PM 2,4-Dinitrotoluene ND 0.100 mg/L 2 4/11/2017 12:40:00 PM Cresols, Total ND 4.00 mg/L 2 4/11/2017 12:40:00 PM Hexachlore-1,3-butadiene ND 0.100 mg/L 2 4/11/2017 12:40:00 PM Hexachlorobenzene ND 0.100 mg/L 2 4/11/2017 12:40i00 PM Hexachloroethane ND 0,0800 mg/L 2 4/11/2017 12:40:00 PM Nitrobenzene ND 0.0800 mg/L 2 4/11/2017 12:40:00 PM Pentachlorophenol ND 0,200 mg/L 2 4/11/2017 12:40:00 PM Pyridine ND 0.200 mg/L 2 4/11/2017 12:40:00 PM Surr: 2-Fluorophenol 41.2 10 - 109 %Rec 2 4/11/2017 12:40:00 PM Surr: Phenol-d6 42.5 10 - 109 %Rec 2 4/11/2017 12:40:00 PM Surr: Nitrobenzene-d5 45.1 19 - 120 %Rec 2 4111/2017 12AM00 PM Surr: 2,4,6-Tribromophenol 47.3 10 - 120 %Rec 2 4/11/2017 12:40:00 PM Surr: 2-Fluorobiphenyl 45.1 22 - 117 %Rec 2 4/11/2017 12:40:00 PM Surr: p-Terphenyl-d14 53.7 34- 116 %Rec 2 4/11/2017 12:40:00 PM Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minnnum Compound Limit. N Tentatively identiticd compounds ND Not Detected at the Deporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 5 of 36 IT Sewziaait Environmental Technologies, Inc. Analytical Report SUMM3310 Yf'irr St. rpP VIROMPilEN'rAL IPClitJOLC�e1ca, ;il5. Cuyahoga Falls, Ohio 44223 {base report) Atragvt,ral Labaretones TEL: (330) 253-8211 FIX: (330) 253--4489 WO#: t704O288 fi/ebsite: htlz2:/hvtviv.settek.com Date Reported: 4/25/2017 CLIENT: Synagro Matrix: SLUDGE Lab ID: 17040288-001A Project: Beaufort Client Sample ID Beaufort Tag Number: Collection Date: 3/29/2017 3:15:00 PM Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081A SW3510C Analyst: JBN TCLP PESTICIDES ANALYSIS (SW131118081) Chlordane, total ND C.0100 mglL 1 4/11/2017 4:19:00 PM Toxaphene ND 0.0200 mg/L 1 4/11/2017 4:19:00 PM Endrin ND 0.00100 mglL 1 4/11/2017 4:19:00 PM gamma-BHC ND 0.00100 mg/L 1 4/11/2017 4:19:00 PM Heptachlor ND 0.00100 mg/L 1 4/11/2017 4:19:00 PM Heptachlor epoxide ND C.00100 m mg/L 1 4/11/2017 4:19:00 PM Methoxychlor ND 0.00100 mg1L 1 4/11/2017 4:19:00 PM Surr: TCMX 50.5 10 - 119 %Rec 1 4/11/2017 4:19:00 PM Surr: DCB 79.6 10 - 119 %Rec 1 4/11/2017 4:19:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SVOC SW-846: 8151 HERBICIDES-TCLP 2,4-D 2,4,5-TP ND 11.3 mg/L ND 11.3 mg/L SW8151A SW8151A Analyst: JBN 1 4/19/2017 1:59:00 PM 1 4/19/2017 1:59:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B Analyst: MES TCLP VOLATILES ANALYSIS (SW131118260) 1,1-Dichloroethene ND 0A00 mg/L 1 4/11/2017 8:32:00 PM 1,2-Dichloroethane ND 0.100 mg/L 1 4/11/2017 8:32:00 PM MEK ND 2.00 mglL 1 4/11/2017 8:32:00 PM Benzene ND 0.100 mg/L 1 4/11/2017 8:32:00 PM Carbon tetrachloride ND 0.100 mg/L 1 4/11/2017 8:32:00 PM Chlorobenzene ND 0.100 mg/L 1 4/11/2017 8:32:00 PM Chloroform ND 0.100 mg/L 1 4/11/2017 8:32:00 PM Tetrachloroethene ND 0.100 mglL 1 4/11/2017 8:32:00 PM Trichloroethene ND 0A00 mglL 1 4/11/2017 8:32:00 PM Vinyl chloride ND 0.200 mg/L 1 4/11/2017 8:32:00 PM Surr: 4-Bromofluorobenzene 98.1 70 - 130 %Roc 1 4/11/2017 8:32:00 PM Surr: ❑ibromofluoromethane 104 70 - 130 %Rec 1 4/11/2017 8:32:00 PM Surr: Toluene-d8 101 70 - 130 %Rec 1 4/11/2017 8:32:00 PM * Qualifiers: Value exceeds Maximum Contaminant Level. E Value above quantization range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 6 of 36 SUMMIT 3urrrrszitEnvironn�ental Technologies, Inc. 3310 Win St. Analytical Report rNVIRONMEWAL 1ECJ4N0L[tG:E5, INQ Cuyahoga falls, Ohio 44223 Arrafytiri3l LabufaTor)es TEL: (330) 253-8211 FAX. (330) 253-4489 (base report) WO#: 17040288 Website: htt :11wwiv.sWek.com Date Reported: 4/25/2017 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 3/29/2017 3:15:00 PM Lab ID: 17040288-OOIA Project: Beaufort Client Sample ID Beaufort Analyses Result RL Qual Units DF Date. Analyzed RCI SW9014 Analyst: MS REACTIVE CYANIDE (901417.3.3.2)-SOLID - Cyanide, Reactive ND 0,500 mg/Kg 1 4/10/2017 2:06:00 PM IGNITAMLITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: RMT Ignitability Non-flammable: 1 4/11/2017 7:46:00 AM RCI SW9045D Analyst: DHC PH (SW9043D) pH 5.6 s.u.@19.9C 1 4/17/2017 9:57:00 AM RCI SW9034 Analyst: MS REACTIVE SULFIDE (9034) Sulfide, Reactive ND 25.0 mg/Kg 1 4/10/2017 2:06:00 PM Qualifiers: Value exceeds Maximum Contaminant Level[. E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit, N Tentatively identified compounds ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 7 of 36 $umrreitEnvi�ronmental Technologies, Inc. QC SUMMARY REPORT 3310 Win St. SUMMIT ENVIRON1A€NTAL cECH OLOG4E-S, lk-'- Cuyahoga Falls, Ohio 44223 WO#: 17040288 , slalyLrcal >: aboralarles TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http:llwww.settelc.com 25-Apr-17 Client: Synagro Project: Beaufort BatchXD: 26346 Sample ID MB-26346 SampType: MBLK TestCode: Mtl-TCLP-7(6 Units: mg1L Prep Date: 4110/2017 RunNo: 67853 ;lient ID: PBW Batch ID: 26346 TestNo: SW6010C SW3010A Analysis Date: 4110/2017 SegNo: 1119853 analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) ND 0.500 TCLP Barium(Ba) ND 5.00 TCLP Cadmium(Cd) ND 0.100 TCLP Chromium(Cr) ND 0.200 TCLP Lead(Pb) ND 0.500 TCLP Selenium(Se) ND 0.500 TCLP Sllver(Ag) ND 0.500 Sample ID LCS-26346 SampType: LCS TestCode: Mtl-TCLP-7(6 Units: mglL Prep Date: 4/1012017 RunNo: 67853 ;lient ID: LCSW Batch ID: 26346 TestNo: SW6010C SW3010A Analysis Date: 411012017 SegNo: 1119854 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl.imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) 2.05 0.500 2.000 0 103 80 120 TCLP Barium(Ba) ND 5.00 2.000 0 100 80 120 TCLP Cadmium(Cd) 2.05 0.100 2.000 0 103 s0 120 TCLP Chromium(Cr) 2.03 0.200 2.000 0 102 80 120 TCLP Lead(Pb) 2.05 0.500 2.000 0 103 80 120 TCLP Selenium(Se) 2.05 0.500 2.000 0 103 80 120 TCLP Silver(Ag) 1.01 0.500 1,000 0 101 80 12C Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding tunes for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 8 of 36 E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Summit Environmental Technologies, Inc. SUM3310 Win St. MI QC SUMMARY REPORT ENVIRONMf NTAL ifCiF NOLOWES, AC Cuyahoga Falls, Ohio 44223 W4#: 17040288 Anayyt,' ? TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hQ:Ilwww.setteic.com 25-Apr-I Client: Synagro Project: Beaufort BatchID: 26358 Sample ID MB-26358 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prop Date: 411012017 RunNo: 67889 Client ID: PBW Batch ID: 26358 TestNo: SW7470A SW7470A Analysis Date: 4/1012017 SegNo: 1119901 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury ND 0.00200 Sample ID LCS-26358 SampType: LCS TestCode: HG_TCLP(74 Units: PPM Prep Date: 411012017 RunNo: 67889 CIient ID: LCSW Batch ID: 26358 TestNo: SW7470A SW7470A Analysis Date: 411012017 SegNo: 1119902 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00382 0.00200 0.00400 0 95.5 80 120 Sample ID 17040237-001AMS SampType: MS TestCode: HG_TCI.P(74 Units: PPM Prep Date: 4/10/2017 RunNo: 67889 Client ID: BatchQC Batch ID: 26358 TestNo: SW7470A SW7470A Analysis Date: 4110/2017 SegNo: 1119904 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00396 0.00200 0.00400 0 99.0 75 125 Sample ID 17040237-001AMSD SampType: MSD TestCode: HG TCLP(74 Units: PPM Prop Date: 411012017 RunNo: 67889 Client ID: BatchQC Batch ID: 26358 TestNo: SW7470A SW7470A Analysis Date: 4/1012017 SegNo: 1119905 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00386 0.00200 0.00400 0 96.5 75 125 0.00396 2.56 20 Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDIimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 9 of 36 'Nt Summit Enviponmental Technologies, Inc. SUMM3310 Win St. QC SUMMARY REPORT VZVI ONMENTAL TfC0k 0WGfEZ, ;N---- Cuyahoga Falls, Ohio 44223 WO#: 170402$$ ArwfyUcaf Loborasorte,-, TEL: (330) 253-82 1 TAX: (330) 253-4489 Website: http://wwiv.settek.corn 25Apr-17 Client: Synagro Project: Beaufort BatchlD: 26358 Sample ID 17040237-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 4110/2017 RunNo: 67889 Client ID: Batch= Batch ID: 26358 TestNo: SW7470A SW7470A Analysis Date: 4110/2017 SegNo: 1119905 Analyte Result PQL SPK vaiue SPK Ref Val Qualifiers: * Value exceeds Maximum Contaminant Level. H bolding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual S Analyte detected in the associated Method Blank Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine 0 RSD is gzeater than RSDlimit R RPD outside accepted recovery limits Original Page 10 of 36 Summit Environmental Technologies, Inc. QC SUMMARY REPORT summiot 3310 Win St. E-PIWIRONPAUNTAL fECHNOL004E-ST 7'N- C Cuyahoga Falls, Ohio 44223 WO#: 17040288 ff 1tnalyLrco1 Laborsfana5 TEL: (330) 253-8211 F.4X.- (330) 253-4489 DT/ebsite: htt :Ilvww.settek.com 25-Apr-17 Client: Synagro Project: Beaufort BatchID: 26372 Sample ID MB-26372 SampType: MBLK TestCode: SVOC-BNA_T Units: mg1L Prep Date: 4/10/2017 RunNo: 67966 Client ID: PBW Batch ID: 26372 TestNo: SW8270C SW3510C Analysis Date: 4111/2017 SegNo: 1121265 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzene ND 0.0400 2,4,5-Trichlorophenol ND 0.100 2,4,6-Trichlorophenol ND 0.100 2,4-Dinitrotcluene ND 0.0200 o-Cresol ND 0.100 mlp-Crescl(s) ND 0.100 Cresols, Total ND 2.00 Hexachloro-1,3-butadiene ND 0.00800 Hexachlorobenzene ND 0.0200 Hexachloroethane ND 0.0400 Nitrobenzene ND O.O400 Pentachlorophenol ND 0A00 Pyridine ND 0.100 Surr: 2-Fluorophenol 0.677 Surr: Phenol-d6 0.674 Surr: Nitrobenzene-d5 0.757 Surr: 2,4,6-Tribromophenol 0.954 Surr: 2-Fluorobiphenyl 0.716 Surr: p-Terphenyl-d14 0.965 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column conf=ation exceeds 1.000 67.7 10 109 1.000 67.4 10 109 I.000 75.7 19 120 1.000 95.4 10 120 1.000 71.6 22 117 1.000 96.5 34 116 B Analyte detected in the associated Method Blank .l Analyte detected below quantization limits ND Not Detected at the Reporting Limit PL Permit Limit L Value above quantitation range M Manual Integration used to deterniine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 11 of 36 M111L Summit Environmental Technologies, Inc. QC SUMMARY REPORT SUM3310 Win St. ENVIRONMENTAL TFCONOLOCIES. fig•= Cuyahoga Falls, Ohio 44223 WO#: 17040288 TEL: (330) 253-8211 FAX.- (330) 2S3-4489 Website: htt :Ilwww.settek.com 25Apr 17 Client: Synagro Project: Beaufort BatchID: 26372 Sample ID LCS-26372 SampType: LCS TestCode: SVOC-BNA_T Units: mglL Prep Date: 411012017 RunNo: 67966 Client ID: LCSW Batch ID: 26372 TestNo: SW8270C SW3510C Analysis Date: 4/1112017 SegNo: 1121266 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,4-DicNorobenzene 0.187 0.0400 0.4000 0 46.7 19-1 126 2,4,5-Trichlorophenol 0.248 0.100 0.4000 0 62.0 11.7 151 2,4,6-Trichlorophenol 0.230 0.100 0.4000 0 57.5 12.4 150 2,4-Dinitrotoiuene 0.281 0.0200 0.4000 0 70.4 20.6 140 o-Cresol 0.212 0.100 0.4000 0 53.0 13.8 137 mlp-Cresol(s) 0.208 0.100 0.4000 0 52.0 10 134 Cresols, Total ND 2.00 0.8000 0 52.5 10 129 Hexachloro-1,3-butadiene 0.188 0.00800 0.4000 0 46.9 14.7 137 Hexachlorobenzene 0,229 0.0200 0.4000 0 57.3 12 139 Hexachloroethane 0.210 0.0400 0.4000 0 52A 14.8 132 Nitrobenzene 0.216 0.0400 0.4000 0 53.9 15.6 133 Pentachlorophenol 0.246 0.100 0.4000 0 61.6 10 156 Pyridine ND 0.100 0.4000 0 11.2 10 126 Surr: 2-Fluorophenol 0.511 1.000 51.1 10 147 Surr: Phenol-d6 0.533 1.000 53.8 10 140 Surr: Nitrobenzene-d5 0.542 1.000 54.2 10 169 Surr: 2,4,6-Tribrcmophenol 0.713 1.000 71.3 10 185 Surr: 2-Ftuorobiphenyi 0.513 1.000 51.3 10 169 Surr: p-Terphenyl-d14 0.668 1.000 66.8 10 179 Qualifiers: �: Value exceeds Maximum Contaminant Level. B Analyte detected hi the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 36 111 Summit Environmental Technologies, Inc. QC SUMMARY REPORT SUMM3310 Win St, fNVIRQNMENTdtiL i1rCONOLOGIES. NC Cuyahoga Falls, Ohio 44223 WO#: 17040288 Ana?yQcaf Lsborsa cries TEL: (330) 233-8211 FAY, (330) 233-4489 Website: htloJhvww.settek,.com 25-Apr-17 Client: Syz}agro Project: Beaufort BatchID: 26372 Sample ID 17040174-001AMS SampType: MS TestCode: SVOC-BNA-T Units: mglL Prep Date: 4110/2017 RunNo: 67966 Client ID: Batch= Batch ID: 26372 TestNo: SW8270C SW3510C Analysis Date: 4/1112017 SegNo: 1121268 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzene 0.228 0.0800 0.4000 0 57.0 29 112 2,4,5-Trichlorophenol 0.294 0.200 0.4000 0 73.6 53 123 2,4,6-Trichlcrophenol 0.263 0.200 0.4000 0 65.7 50 125 2,4-Dinitrotoiuene 0.281 0.0400 0.4000 0 70.2 57 128 o-Cresol 0.246 0.200 0.4000 0 61.6 30 117 mlp-Cresol(s) 0.252 0.200 0.4000 0 63.0 29 110 Cresols, Total ND 4.00 0.8000 0 62.3 20 125 Hexachloro-1,3-butadiene 0.241 0.0160 0.4000 0 60.2 22 124 Hexachlorobenzene 0.255 0.0400 0.4000 0 63.8 53 125 Hexachloroethane 0.263 0.0800 0.4000 0 65.8 21 115 Nitrobenzene 0.264 0.0800 0.4000 0 66.1 45 121 Pentachlorophenoi 0.295 0.200 0.4000 0 73.8 35 138 Pyridine ND 0.200 0.4000 0 22.1 10 126 Surr: 2-Fluorophenol 0.669 1.000 66.9 10 147 Surr: Phenol-d6 0.712 1.000 71.2 10 140 Surr: Nitrobenzene-d5 0.694 1.000 69.4 10 169 Surr, 2,4,6-Tribromophenol 0.914 1.000 91.4 10 185 Surr: 2-Fluorobiphenyl 0.656 1.000 65.6 10 169 Surr: p-Terphenyl-d14 0.859 1.000 86.9 10 179 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine Original MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 13 of 36 Summit Environmental Technologies, Inc. QC SUMMARY REPORT Insummint 3310 Win St. �C ENVIRONMENTAL eECa-! MLOGIES, ;-N Cuyahoga Falls, Ohio 44223 WO#: 17040288 Ar�tt.lyilcgl Labb��larief TEL: (330) 253-8211 FAX: (330) 253-4489 Website: hQ2:11www.sette1c.coM 25 Apr-17 Client: Synagro Project: Beaufort BatchED: 26372 Sample ID 17040174-001AMSD Client ID: BatchQC Analyte SampType: MSD Batch ID: 26372 Result TestCode: TestNo: PQL SVOC-BNA_T Units: mg1L SW8270C SW3510C SPK value SPK Ref Val %REC Prep Date: 4/1012017 Analysis Date: 411112017 Lowl-imit HighLimit RPD Ref Val RunNo: 67966 SegNo: 1121269 %RPD RPDLimit Qual 1,4-Dichlorobenzene 0.261 0.0800 0.4000 0 65.2 29 112 02280 13.4 30 2,4,5-Trichlorophenol 0.335 0.200 0.4000 0 83.8 53 123 0,2944 13.0 30 2,4,6-Trichlorophenol 0.300 0.200 0.4000 0 75.1 50 125 0,2628 13.4 30 2,4-Dinitrotoluene 0,337 0.0400 0.4000 0 84.3 57 128 0.2808 18.3 30 a -Cresol 0.278 0.200 0.4000 0 69.4 30 117 0.2464 11.9 30 mip-Cresol(s) 0.275 0.200 0.4000 0 68.8 29 110 0.2520 8.80 30 Cresols, Total ND 4.00 0.8000 0 69.1 20 125 0 0 30 Hexachloro-1,3-butadiene 0.254 0.0160 0.4000 0 63.6 22 124 0.2408 5.49 30 Hexachlorobenzene 0.278 0.0400 0.4000 0 69.5 53 125 0.2552 8.55 30 Hexachloroethane 0.290 0.0800 0.4000 0 72.5 21 115 0.2632 9.69 30 Nitrobenzene 0.290 0.0800 0.4000 0 72.6 45 121 0.2644 9.37 30 Pentachlorophenol 0.334 0.200 0.4000 0 83.4 35 138 0.2952 12.2 30 Pyridine ND 0.200 0.4000 0 17.1 10 126 0 0 30 Surr: 2-Fluorophenol 0.656 1.000 65.6 10 147 0 Surr: Phenol-d6 0.700 1.000 70.0 10 140 0 Surr: Nitrobenzene-d5 0.707 1.000 70.7 10 169 0 Surr: 2,4.6-Tribromophenol 0.928 1.000 92.8 10 185 0 Surr: 2-Fluorobiphenyl 0.658 1.000 65.8 10 169 0 Surr: p-Terphenyl-d14 0.866 1.000 86.6 10 179 0 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BIank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original MC Value is below Minim urn Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 14 of 36 .Summit Environmental Technologies, Inc. QC SUMMARY REPORT SUMM17- 3310 Win Sl, ENVIRONI'11Et+1TAL TEC14t4 )LGG]Es, _ Cuyahoga Falls, Ohio 44223 WO#: 17040288 91 1lrpalyrffcaf LobnrslDna� TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http:11Ww.settelc.cow 25-Apr-17 Client: Synagro Project: Beaufort Sample ID mb-26373 SampType: mblk TestCode: tclp-svoc-cpe Units: mglL Client ID: PBW Batch ID: 26373 TestNo: SW8081A SW3510C BatchID: 26373 Prep Date: 411012017 Analysis Date: 4/1112017 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val Chlordane, totai ND 0.0100 Toxaphene ND 0.0200 Endrin ND 0.00100 gamma-BHC ND 0.00100 Heptachlor ND 0.00100 Heptachlor epoxide ND 0.00100 Methoxychlor ND 0.00100 Surr: TCMX 13.0 20.00 64.8 10 119 Surr. DCB 14.7 20.00 73.4 10 119 Sample ID Ics-26373 SampType: Ics TestCode: tclp-svoc-cpe Units: mg1L Prep Date: 411012017 Client 1D: LCSW Batch ID: 26373 TestNo: SW8081A SW3510C Analysis Date: 411112017 Analyte Result PQL SPK value SPK Ref Val %REC Lowt-imit HighLimit RPD Ref Val Endrin 0.0101 0.00100 0.0100 0 101 20 157 gamma-BHC 0.00790 0.00100 0.0100 0 79.0 22 137 Heptachlor 0.00913 0.00100 0.0100 0 91.3 24 121 Heptachlor epoxide 0.00905 0.00100 0.0100 0 90.5 27 152 Methoxychlor 0.0101 0.00100 0.0100 0 101 10 199 Surr. TCMX 20.9 20.00 104 10 119 Surr: DCB 22.9 20.00 115 10 119 Qualifiers: Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 15 of 36 RunNo: 67913 SegNo: 1121427 %RPD RPDLimit Qual m m RunNo: 67913 SegNo: 1121428 %RPD RPDLimit Qual E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDIimit R RPD outside accepted recovery limits Original Ilu Summit Environmental Technologies, Inc. QC SUMMARY REPORT SUMM3310 Win St. EKVIROM61tw.NTA6 '-eCI4�4OL-'?^'_ , •-.N.,= Cuyahoga Falls, Ohio 44223 WO#: 17040288 AtselyUcaf Laborafurl TEL: (330) 253-8211 FAX: (330) 253-4489 Website: hit :1Avww.3ettekcom 25-Apr-17 CIient: Synagro Project: Beaufort BatchID: 26373 Sample ID 17040174-001ams SampType: ms TestCode: tclp-svoc-cpe Units: mglL Prep Date: 4/10/2017 RunNo: 67913 client ID: BatchQC Batch 1D: 26373 TestNo: SW8081A SW3510C Analysis Date: 4/11/2017 SegNc: 1121429 knalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Endrin 0.00975 0.00100 0.0100 0 97.5 20 157 gamma-BHC 0.00817 0.00100 0.0100 0 81.7 22 137 Heptachlor 0.00890 0.00100 0.0100 0 89.0 24 121 Heptachlor epoxide 0.00915 0.00100 0.0100 0 91.5 27 152 Methoxychlor 0.0105 0.00100 0.0100 0 105 10 199 Surr: TCMX 19.3 20.00 96.7 10 119 Surr: DCB 21.8 20.00 109 10 119 Sample ID 17040174-001amsd SampType: msd TestCode: tclp-svoc-cpe Units: mglL Prep Date: 4/1012017 RunNo: 67913 Client ID: BatchQC Batch ID: 26373 TestNo: SW8081A SW3510C Analysis Date: 4/11/2017 SegNo: 1121430 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Endrin 0.00959 0.00100 0.0100 0 95.9 20 157 0.00975 1.62 30 gamma-BHC 0.00792 0.00100 0.0100 0 79.2 22 137 0,00817 3.18 30 Heptachlor 0.00888 0.00100 0.0100 0 88.8 24 121 0.00890 0.150 3C Heptachlor epoxide 0.00911 0.00100 0.0100 0 91.1 27 152 0.00215 0.533 30 Methoxychlor 0.0104 0.00100 0.0100 0 104 10 199 0.0105 0.954 30 Surr: TCMX 17.0 20.00 85.1 10 119 0 Surr: DCB 19.6 20.00 97.8 10 119 0 Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine Original MC Value is below Minimum Compound Limit. NID Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 16 of 36 Summit Environmental Technologies, Inc. QC SUMMARY 17 ZT REPORT PORT SUMMI-21 3310 Win St. l .. V L i_[\ i itG 1 cFgri+NP,gt�{T�}I r,Cq�t�7L�k •.._ Cuyahoga Falls, Ohio44223 WO#: 17040288 ffl st.r9 IyrUcaf L.0aralunar TEL: (330) 253-8211 FAX: (330) 253-4489 Website: httu:/fivww.settefc.com 25-Apr-17 Client: Synagro Project: Beaufort BatchID: 26476 ,ample ID mb-26476 SampType: mblk TestCode: tclp-svoc-her Units: mg1L Prep Date: 4/12/2017 RunNo: 68367 client ID: PBW Batch ID: 26476 TestNo: SW8151A SW8151A Analysis Date: 4/19/2017 SegNo: 1129030 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 2,4-D ND 1.00 0 0 2,4,5-TP ND 0.500 0 0 Surr: DCAA 442 500.0 88.4 20 140 Sample ID Ics-26476 Client ID: LCSW Analyte 2,4-D 2,4,5-TP Sum DCAA SampType: Ics Batch ID: 26476 Result ND ND 449 TestCode: telp-svoc-her Units: mg1L TestNo: SW8151A SW8151A PQL SPK value SPK Ref Val 1.00 0.500 0 0.500 0.500 0 500.0 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds Prep Date: 4/1212017 Analysis Date: 4/1912017 %REC LowLimit HighLimit RPD Ref Val 88.5 62.6 125 84.9 52.5 128 89.8 20 140 B. Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 17 of 36 RunNo: 68367 SegNc: 1129031 %RPD RPDLimit Qua] E Value above quantitation range M ManuaI Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original SUMMIT-- Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT ENVIR0 N MENTAL TECHNOLOGIES. '., W Cuyahoga Falls, Ohio 44223 WO#: 17040288 A-rWy Uca.f taborolaries TEL: (330) 253-8211 FAUX: (330) 253-4489 Website: htt2:llwww.settek.com 25-Apr-17 Client: Synagro Project: Beaufort BatclxID: R67896 Sample ID 17040184-001ADUP SampType: DUP TestCode: Ignitability_5 Units: Prep Date: RunNo: 67896 '.lient ID: BatchQC Batch ID: R67896 TestNo: SW1030 Analysis Date: 4/11/2017 SegNo: 1120094 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability Jon -flammable. 0 0 20 Sample ID 17040184-001ATRIP SampType: DUP TestCode: lgnitability_S Units: Prep Date: RunNo: 67896 Client ID: Batch= Batch ID: R67896 TestNo: SW1030 Analysis Date: 4/11/2017 SegNo: 1120095 Analyte Result PQL SPK value SPK Ref Val %REC LcwLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability Jon -flammable. 0 0 20 Sample ID 17040288-001ADUP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 67896 ;fient ID: Beaufort Batch ID: R67896 TestNo: SW1030 Analysis Date: 4111/2017 SegNo: 1120097 knalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability Jon -flammable. C 0 20 Sample ID 17040288-001ATRIP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNc: 67896 Client [D: Beaufort Batch ID: R67896 TestNo: SW1030 Analysis Date: 4/1112017 SegNo: 1120098 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability Jon -flammable. 0 0 20 Qualifiers: * Value exceeds Maximum Contaminant Level. H HoIding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank Analyte detected below quantitation limits ND Not Detected at the Reporting Lunn PL Permit Limit Page 18 of 36 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDt mit R RPD outside accepted recovery limits Original SUMMINt Summit Environmental Technologies, Inc. 3316 Win St. QC SUMMARY REPORT ENVIRONMENTAL TECt# 40LOGIES, AnalyUcal L borstorie5 Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 F19X.- (330) 253-4489 Website: htW:/hvww.settek.com WO#: 17040288 25 Apr 17 Client: Synagro Project: Beaufort BatchXD: R67896 Sample ID 17040288-001ATRIP SampType: DUP TestCode: Ignitability_S Units: Prep Date: RunNo: 67896 Client ID: Beaufort Batch ID: R67896 TestNo: SW1030 Analysis Date: 4111/2017 SegNo: 1120098 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua] Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 19 of 36 summimp- Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT VMIRONFAENTAL Tf2CONOLCiNIE . . - Cuyahoga Falls, Ohio 44223 WO#: 17040288 k gatyrilcol Laborerorjes TFL: (330) 253-8211 FAX.- (330) 253-4489 Website: htty7l1www.settek.com 25-Apr-17 Client: Synagro Project: Beaufort BatchID: R67931 Sample ID MB-R67931 SampType: MBLK TestCode: Cyanide,Rea Units: mglL Prep Date: RunNo: 67931 Client ID: PBW Batch ID: R67931 TestNo: SW9014 Analysis Date: 411012017 SegNo: 1120700 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive ND 0.500 Sample ID LCS-R67931 SampType: LCS TestCode: Cyanide,Rea Units: mg1L Prep Date: RunNo: 67931 Client ID: LCSW Batch ID: R67931 TestNo: SW9014 Analysis Date: 4/10/2017 SegNe: 1120701 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 1,04 0.500 1,000 0 104 85 115 Sample ID 17040325-005AMS SampType: MS TestCode: Cyanide,Rea Units: mg1L Prep Date: RunNo: 67931 Client ID: BatchQC Batch ID: R67931 TestNo: SW9014 Analysis Date: 4110/2017 SegNo: 1120703 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 1.03 0.500 1.000 0 103 81.3 118 Sample ID 17040325-005AMSD SampType: MSS TestCode: Cyanide,Rea Units: mglL Prep Date: RunNc: 67931 Client ID: BatchQC Batch ID: R67931 TestNo: SW9014 Analysis Date: 4/1012017 SegNo: 1120704 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref VaI %RPD RPDLimit Qual Cyanide, Reactive 1.03 0.500 1.000 0 103 81.3 118 1.027 0 5 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds S Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 20 of 36 E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Summit EnvitronmentalTechnolagies,Inc. QC SUMMARY REPORT 'l— summ 3310 Win St. ENVIRONMENTAL 7EC4N0LC;EE, -n,,, Cuyahoga Falls, Ohio44223 WQ##: 17040258 ArWy1J=sf L xbDratoriew TEL: (330) 253-8211 FAX: (330) 253-4489 Website: h9.:11www.settek.com 23 Apr I7 CIient: Synagro Project: Beaufort BatchID: R67931 Sample ID 17040325-005AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/L Client ID: Batch= Batch ID: R67931 TestNo: SW9014 Analyte Result PQL SPK value SPK Ref Val Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds Prep Date: RunNo: 67931 Analysis Date: 4/10/2017 SegNo: 1120704 %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual B Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 21 of 36 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery Emits Original Summit Environmental Technologies, Inc. SUM3310 Win St. MIT QC SUMMARY REPORT 91� EWRONMENT"4L F C!#NOLOGrES, NC Cuyahoga Falls, Ohio 44223 WO#: 17040288 ,��yG'c�1 La �retcsrde TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hity://www.settek.com 25-Apr-17 Client: Synagro Project: Beaufort Batch]][): R67936 Sample ID MB-R67936 SampType: MBLK TestCode: Sulfide,React Units: mglL Prep Date: RunNo: 67936 Client ID: PBW Batch ID: R67936 TestNo: SW9034 Analysis Date: 4110/2017 SegNo: 1120846 Analyte Result PQL SPK value SPK Ref Val %REC Lowt-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive ND 25.0 Sample ID LCS-R67936 SampType: LCS TestCode: Sulfide,React Units: mglL Prep Date: RunNo: 67936 Client ID: LCSW Batch ID: R67936 TestNo: SW9034 Analysis Date: 4/1012017 SegNo: 1120847 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide. Reactive 1390 25.0 1400 0 99.3 85 115 Sample ID 17040325-005AMS SampType: MS TestCode: Sulfide,React Units: mg1L Prep Date: RunNo: 67936 CIient 1D: BatchQC Batch ID: R67936 TestNo: SW9034 Analysis Date: 4/10/2017 SegNo: 1120848 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 1400 25.0 1400 0 100 75 125 Sample ID 17040325-005AMSD SampType: MS❑ TestCode: Sulfide,React Units: mglL Prep Date: RunNo: 67936 Client [D: Batch= Batch ID: R67936 TestNo: SW9034 Analysis Date: 411012017 SegNo: 1120849 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Vai %RPD RPDLimit Qual Sulfide, Reactive 1360 25.0 1400 0 97.1 75 125 1400 2.90 30 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation Limits ND Not Detected at the Reporting Limit PL Permit Limit Page 22 of 36 E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Summit Environmental Technologies, Inc. QC SUMMARY RFPORT summil— 3310 Win St. EPWIRQNM NTAL 7FCW40L0G'E8. �R-2 Cuyahoga Falls, Ohio 44223 WQ#: 17040288 1 galytico4 Laboralone- TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hltn //www.settek.com 25 Apr-17 Client: Synagro Project: Beaufort BatchID: R67936 Sample ID 17040325-005AMSD SampType: MSD TestCode: Sulfide,React Units: mg/L. Prep Date: RunNo: 67936 Client ID: Batch= Batch ID: R67936 TestNo: SW9034 Analysis mate: 4/1012017 SegNo: 1120849 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BIank E Value above quantitation range H Holding tunes for preparation or analysis exceeded 7 Analyte detected below quantization limits M Manual Integration used to determine Original MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 23 of 36 Summit Environmental Technologies, Inc. SUMM111 3310 Win St. QC SUMMARY REPORT EPIVIRON14ENTAL EC9 NOLOGAES, ;CAM Cuyahoga Falls, Ohio 44223 WO#: 17040288 AnafyUcal Laboradartee,; TEL: (330) 253-8211 F,4X.- (330) 253-4489 Website: hgpJ/www.setteic.com 25 Apr-17 Client: Synagro Project: Beaufort BatchID: R67975 Sample ID lcs 20ppb L04041 SampType: LCS TestCode: voc-mstr_np Units: mg1L Prep Date: RunNo: 67975 Client ID: LCSW Batch ID: R67975 TestNo: SW8260B Analysis Date: 4/11/2017 SegNo: 1121402 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloreethene 0.0215 0.00500 0.0200 0 108 71 138 Benzene 0.0182 0.00500 0.0200 0 91.1 75 137 Chlorobenzene 0.0200 0,00500 0.0200 0 100 77 132 Trichloroethene 0.0238 0.00500 0.0200 0 118 64 119 Surr:4-Bromofluorobenzene 49.3 50.00 98.7 70 130 Surr: Dibromofluoromethane 53.0 50.00 106 70 130 Surr: Toluene-d8 51.0 50.00 102 70 130 Sample ID LCSD 20PPB L0404 SampType: LCSD TestCode: voc-mstr np Units: mglL Prep Date: RunNo: 67975 Client ID: LCSS02 Batch ID: R67975 TestNo: SW8260B Analysis Date: 411112017 SegNo: 1121403 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroothene 0.0203 0.00500 0.0200 0 101 71 138 0.0215 5.88 30 Benzene 0.0176 0.00500 0.0200 0 87.6 75 137 0.0182 3.81 30 Chlorobenzene 0.0193 0.00500 0.0200 0 96.5 50 150 0.0200 3.66 30 Trichloroethene 0,0223 0.00500 0.0200 0 112 64 119 0.0238 5.66 30 Surr: 4- Bromof luoro benzene 49.7 50.00 99.4 70 130 0 0 Surr: Dibromofluorom ethane 53.0 50.00 106 70 130 0 0 Surr: Toluene-d8 50.6 50.00 101 70 130 0 0 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual 1mcgration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 24 of 36 Summit Environmental Technologies, Inc. 331O Win St. QC SUMMARY REPORT frsumm-OT- r=%rI8Q,NId1;NTAL A".00y i=s1 LH&ararraneF. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489 Website: http://www.settelc.corn WOO: 17040288 25 Apr-17 Client: Synagro Project: Beaufort BatchED: R67975 Sample I❑ MBLK SampType: MBLK TestCode: roc-mstr_np Units: mglL Prep Date: RunNo: 67975 Client ID: PBW Batch ID: R67975 TestNo: SW8260B Analysis Date: 4/1112017 SegNo: 1121405 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,1-Dichloroethene ND 0.00500 1,2-Dichloroethane ND 0.00500 MEK ND 0.0250 Benzene ND 0.00500 Carbon tetrachloride ND 0.00500 Chlorobenzene ND 0.00500 Chloroform ND 0.00500 Tetrachioroethene ND 0.00500 Trichloroethene ND 0.00500 Vinyl chloride ND 0,00200 Sum 4-Bromofluorobenzene 48.4 50.00 96.7 70 130 Sum Dibromofluoromethane 50.3 50.00 101 70 130 Surr: Toluene-d8 50.0 50.00 100 70 130 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 25 of 36 Original MIT Summ it Environmental Technologies, Inc. QC SUMMARY REPORT 91SUM3310 Win St. ENVIRONFAENTP.1- T EEC-4NOLOGIES, '. - Cuyahoga Falls, Ohio 44223 WO#: 17040288 11tWyUcel -_ atone TEL: (330) 253-8211 FAX- (330) 253-4489 Website: htto://www.settek.com 25-Apr-17 Client: Synagro Project: Beaufort BatchID: R67975 Sample ID 17040234-001ams SampType: MS TestCode: tclp-voc-mstr Units: mg1L Prep Date: RunNo: 67975 client ID: BatchQC Batch 1D: R67975 TestNo: SW8260B Analysis Date: 411112017 SegNo: 1121420 gnalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 0.194 0.0100 0.200 0 96.8 39.9 160 1,2-Dichloroethane 0.181 0.0100 0.200 0 90.3 42.5 157 MEK 0.968 0.0500 1.00 0,0314 93.7 16.6 227 Benzene 0.201 0.0100 0200 0.0202 90.6 38.1 155 Carbon tetrachloride 0.200 0.0100 0.200 0 100 40.8 162 Chlorobenzene 0.191 0.0100 0.200 0 95.3 35.7 168 Chloroform 0.197 0.0100 0200 0 98.3 18.3 199 Tetrachloroethene 0.207 0.0100 0.200 0.0155 96.0 10 261 Trichloroethene 0.202 0.0100 0.200 0 101 23.8 175 Vinyl chloride 0.192 0.0100 0.200 0 95.9 10 165 Surr: 4-Bromofluorobenzene 504 500.0 101 84.6 130 Surr: ❑ibromofluoromethane 492 500.0 98.4 71.4 127 Surr: Toluene-d8 489 500.0 97.7 74.6 127 Sample ID [cs 20pph L04041 SampType: LCS TestCode: teip-vac-mstr Units: mglL Prep Date: RunNo: 67975 :;Iient ID: LCSW Batch ID: R67975 TestNo: SW8260B Analysis Date: 4/11/2017 SegNo: 1121422 anaiyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroeth 1,2-Dichloroeth MEK Benzene Qualifiers: ene 0.0215 0.0100 ane 0.0224 0.0100 0.0929 0.0500 0.0182 0.0100 * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds 0.0200 0 108 79.4 0.0200 0 112 73.6 0.100 0 92.9 55.1 0.0200 0 91.1 73.1 B Analyte detected in the associated Method Blank T Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 26 of 36 131 137 163 132 E Value above quantitation range M Manual Integration used to determine 0 RSD is gzeater than RSDlimit R RPD outside accepted recovery limits Original 'NI- Summit Environmental Technologies, Inc. QC SUMMARY REPORT SUMM3310 Win St. ENVIRONNIFNTAI 1EC� t40L0G1E5, ;Nr: Cuyahoga Falls, Ohio 44223 WO#: 17040288 Ana]VUcaf Lsbs rsfari05 TEL: (330) 253-8211 FAX: (330) 253-4489 Website: htW:Ilwww.settek-.com 25-Apr-17 Client: Synagro Project: Beaufort BatchlD: R67975 Sample ID les 20ppb L04041 SampType: LCS TestCode: tclp-vac-mstr Units: mglL Prep Date: RunNo: 67975 Client ID: LCSW Batch ID: R67975 TestNo: SW8260B Analysis Date: 4/1112017 SegNo: 1121422 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Carbon tetrachloride 0,0238 0.0100 0.0200 0 119 63.7 139 Chlorobenzene 0.0200 0.0100 0.0200 0 100 72.3 139 Chloroform 0,0210 0.0100 0.0200 0 105 79.3 129 Tetrachloroethene 0.0223 0.0100 0.0200 0 111 56.2 187 Trichloroethene 0.0236 0.0100 0.0200 0 118 64.1 138 Vinyl chloride 0,0190 0.0100 0.0200 0 95.2 22.1 147 Surr:4-Bromofluorobenzene 49.3 50.00 98.7 80.4 126 Surr: Dibromofluorom ethane 53.0 50.00 106 70.3 125 Surr: Toluene-d8 51.0 50.00 102 82 117 Sample ID LCSD 20PPB L0404 SampType: LCSD TestCode: tclp-voc-mstr Units: mg1L Prep Date: RunNo: 67975 Client ID: LCSS02 Batch ID: R67975 TestNo: SW8260B Analysis Date: 411112017 SegNo: 1121423 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Hight-imit -RPD Ref Val %RPD RPDLimit Qua[ 1,1-Dichloroethene 0.0203 0.0100 0.0200 0 101 79.4 131 0.0215 5.88 25 1,2-Dichloroethane 0.0214 0.0100 0.0200 0 107 73.6 137 0.0224 4.25 25 MEK 0.0951 0.0500 0.100 0 95.1 55.1 163 0.0929 2.35 25 Benzene 0.0175 0.0100 0.0200 0 87.6 73.1 132 0.0182 3.81 25 Carbon tetrachloride 0.0225 0.0100 0,0200 0 113 63.7 139 0.0238 5.61 25 Chlorobenzene 0.0193 0.0100 0.0200 0 96.5 72.3 139 0.0200 3.66 25 Chloroform 0.0206 0.0100 0.0200 0 103 79.3 129 0.0210 1.59 25 Tetrachloroethene 0.0217 0,0100 0.0200 0 108 56.2 187 0.0223 2.78 25 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H HoIding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit P Second column conf=ation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 27 of 36 SUMMIT 'Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT ffJ ENVIRONFAENTAL T6C"NOLOGIF- . _ Cuyahoga Falls, Ohio 44223 WO#: 17040288 ,9Pyb1cal TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://www.sertelc.coni 25-Apr-17 Client: Synagro Project: Beaufort BatchID: R67975 Sample I❑ LCSD 20PPB L0404 SampType: LCSA TestCode: telp-vac-mstr Units: mglL Prep Date: RunNo: 67975 Client ID: LCSS02 Batch ID: R67975 TestNo: SW8260B Analysis Date: 411112017 SegNo: 1121423 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Trichlorcethene 0.0223 0.0100 0.0200 0 112 64.1 138 0.0236 5.66 25 Vinyl chloride 0.0174 0.0100 0.0200 0 87.1 22.1 147 0.0190 8.94 25 Surr:4-Bromotlucrobenzene 49.7 50.00 99.4 80.4 126 0 25 Surr: Dibromof] uoromethane 53.0 50.00 106 70.3 125 0 25 Surr. Toluene-d8 50.6 50.00 101 82 117 0 25 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 28 of 36 imt Summit Environmental Technologies, Inc. QC SUMMARY REPORT summ3310 Grin St. V4VIRONFA04TAL TECHNOLOGIES, .INC Cuyahoga Falls, Ohio 44223 WO#: 17040288 fn Rrmlyb1cal Labarsdarae5 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htt :11www.settek.com 25-Apr-17 Client: Project: Synagro Beaufort BatehID: R68172 Sample ID 17040872-001ADUP SampType: DUP TestCode: pH_011{9045 Units: s.u.@21.1C Prep Date: RunNc: 68172 client ID: BatchQC Batch ID: R68172 TestNc: SW9045D Analysis Date: 4/1712017 SegNo: 1125289 knalyte Result PQL SPK value SPK Ref Val %RFC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual pH 5.7 Qualifiers- * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is beiow Minimum Compound Limit. P Second column confirmation exceeds 0 0 B Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 29 of 36 5.7 0.5 10 E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Originai MMIT Summit Environmental Technologies, Inc. 3312 Win Sf. QC SUMMARY REPORT 91SU rc?tVIR0NMENTAL TECONOLOGIES, 'k. AnafyUcaf L:sbarigiones Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hf(L:Ilwww.settek.com WO#_ 17040288 25 Apr-17 CIient: Synagro Project: Beaufort BatchID: R68172 Sample ID LCS-R68172 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@20.5C Prep Date: RunNo: 68172 ;Gent ID: LCSW Batch ID: R68172 TestNo: SW9045D Analysis Date: 411712017 SegNo: 1124949 analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighUrnit RPD Ref Val %RPD RPDLimit Qual pH 7.0 7.0 0 101 98.6 101.4 Sample lD 17040279-001CDUP SampType: DUP TestCode: pH_NPW(450 Units: s.u.@19.2C Prep Date: RunNo: 68172 lient ID: BatchQC Batch ID: R68172 TestNo: SW9045D Analysis Date: 411712017 SegNo: 1124951 knalyte Result PQL SPK value SPK Ref Vai %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ pH 6A Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank 1 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 30 of 36 6.4 0 5 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original 1]C-QACOC33S RN 0 FAcbveDme:)2fE a5 SUMMITAnalysis Request I Chain of Custody 33*0VSoroo1.for Swmmit Gnviro:urental Technologies, Ina. use only 3�td 1iVIn SArgxre CL-vaheoo Felts. Ohio A4223 age 1 of 2 Dc-7 Rev. 16 Summit Fnvitonmental Technologies, Inc. Cooler Receipt: Form Uff,ctivu ❑sloaMM1& initials of person inspeng�oafer and sampfes:�� �4 W 47 client;-- —ISl- A Air N :1 Order Number: hate ReceivedTime Received: . � i)ate coolers) opened and samples inspected: Number of Coolers/Uoxes: I NIA Shippe(l"EC7 UPS DIAL Airhnme US Postal Walk-in Pickup Other; Packaging: Peanuts Bubble Wr Paper Foam None Other: -tape an Coo$L-M)ox, (D N .NIA Custody Seats intact Y N N/ C-Q-C in plastic N NIA Ice, Blue ice present I absent melted) NIA 1 Sample Temperature IR Gun #1802g459 CF i1 0 'C - `C WA Radiolagicall'esting Instrument serial1635127 Y N NIA_ (see page 2 for scan results) "Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be notified immediately. C-O-C fisted out properly ) N NIA CD Samples in separate bags N MA Sample containers intact` N N1A By `If no, list broken sampfels): Sample labels) complete (ID, date, etc.) Y N NIA Lobel(s) agree with C-O-C Y N NIA Correct containers used Y N NIA Sufficient sample received Y N NIA Samples received within holding time Y N Bubbles absent from 40 mL vials" Y N f �riQi " Samples with bubbles <5mm are accoptebte. Indicate bubble size it }Omm. Was client writacteci about samples Y N Will client send now samples Y N Client contact: Logged in by; Page 1 of 2 4- 0 N N t� IL Page 32 of 36 North Carolina Wastewater/Groundwater Laboratory Certification Certified Parameters Listing Lab Name: Summit Environmental Techno[ogies, Inc: Certificate Number: 631 Address: 3310 Win Street Effective Date: 1/1/2017 Cuyahoga Falls, OH 44223- Expiration Date: 12/31/2017 Date of Last Amendment: 3114/2017 The above named laboraim, having duly met the requirements of 15A NCAC 21-1.0800, is hereby certified for the measurement of the parameters listed below. __. CERTIFIED PARAMETERS _ _..... INORGANIC PHOSPHATE, ORTHO BOD EPA 300.0, Rev. 2.1, 1993 (Aqueous) SM 5210 B-2001 (Aqueous) SW-846 9056 A (Aqueous) CHLORIDE SW-845 9056 A (Non -Aqueous) SW-846 9056 A (Aqueous) PHOSPHORUS, TOTAL SW-846 9058 A (Non -Aqueous) EPA 200.7, Rev. 4.4 (1994) (Aqueous) coo SW-845 6010 D (Aqueous) SM 5220 C-1997 (Aqueous) SW-845 6010 D (Non -Aqueous) FLUORIDE RESIDUE, DISSOLVED 180 C EPA 300.0, Rev. 2.1, 1993 (Aqueous) SM 2540 C-1997 (Aqueous) SW-846 9056 A (Aqueous) RESIDUE, SUSPENDED SW-340 90H A (Non -Aqueous) SM 2540 D-1997 (Aqueous) iGNiTABILITY SILICA SW-8461030 (Non -Aqueous) EPA 200.7, Rev: 4A, 1994 (Aqueous) 1NCRGANIC PHENOLS SW-846 0010 D (Aqueous) EPA 420.1, Rev. 1978 (Aqueous) SW-846 6010 D (Non -Aqueous) NITROGEN, NITRATE SULFATE EPA 300.0, Rev. 2.1, 1993 (Aqueous) EPA 300.0, Rev, 2.1, 1993 (Aqueous) SW-846 9056 A (Aqueous) SW-846 9056 A (Aqueous) SW-846 905e A (Non -Aqueous) SW-846 9056 A (Non Aqueous) NITROGEN, NITRITE SULFIDE EPA 300.0, Rev. 2.1, 1993 (Aqueous) SW-846 9034 (Aqueous) SW-846 9056 A (Aqueous) SW-846 9034 (Non -Aqueous) SW-846 9056A (Non -Aqueous) METAL NITROGEN, NO3 + NO2 TCLP METALS EPA 300-0, Rev, 2.1, 1993 (Aqueous) SW-8461311 (Aqueous) SW-846 9056 A (Aqueous) ALUMINUM SW-846 9056 A (Non -Aqueous) EPA 200.7, Rev, 4.4, 1994 (Aqueous) NITROGEN, TOTAL KJELDAHL SW-846 6010 D (Aqueous) SM 4500 Norg B-1997 (SM 4500 NH3 C-1997) (Aqueous) SW-846 6010 D (Non -Aqueous) OIL 6 GREASE EPA 200.8, Rev, 5.4, 1994 (Aqueous) EPA 1664 Rev. B (Aqueous) SW-846 6020 B (Aqueous) SW-846 9071 B (Non -Aqueous) SW-846 6020 B (Nan -Aqueous) pH ANTIMONY SW-846 9045 D (Nan -Aqueous) EPA200.7, Rev. 4.4, 1994 (Aqueous) i lr,s CWfIlf2fiEMMCLiM MjW2MOe of an acceptable qual''ty assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penalties and/or decertification for infractions as set forth in t 5A NCAC 2H.0807. w O r Q) a7 M CL 0 M O M Cr) 0) 0.- North Carolina WastewaterlGroundwater Laboratory Certification Certified Parameters Listing Lab dame: Summit Environmental Technologies, Inc. Address: 3310 Win Street Cuyahoga Palls, OH 44223- The above named laboratory, having duty met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below. .......__. - — _..._.� CERTIFIED PARAMETERS SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) EPA 200.6. Rev. 5.4. 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) ARSENIC EPA200.7, Rev. 4.4, 1994 (Aqueous) SW-845 6010 D (Aqueous) SW-840 6010 D (Non -Aqueous) EPA 200.8, Rev. 5.4, 1994 {Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non Aqueous) BARIUM EPA 200,7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) EPA 200.8, Rev, 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non Aqueous) BERYLLIUM EPA 200.8, Rev_ 5.4, 1994 (Aqueous) SW 846 6020 B (Aqueous) S1N-846 6020 B (Non Aqueous) BORON EPA2C0.8, Rev. 5.4, 1994 (Aqueous) SW-846 6C20 B (Aqueous) SW-846 6020 B (Nan Aqueous) CADMIUM EPA20C.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Nan -Aqueous) EPA200-0, Rev. 5,4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) CALCIUM EPA 200.7, Rev. 4A, 1994 (Aqueous) SW-846 Solo D (Aqueous) SW-845 6010 D (Non -Aqueous) CHROMIUM TOTAL EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 60111 D (Non -Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aque(1us) SW-846 6020 B (Non -Aqueous) COBALT EPA 200.7. Rev. 4.4, 1994 (Aqueous) 5W-846 6010 D (Aqueous) SW-846 601 a b (Nan -Aqueous) EPA 200.8, Rev, 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) COPPER EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) EPA 200.8, Rev_ 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 8 (Non -Aqueous) IRON EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Nan -Aqueous) LEAD EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) Certificate Nurntw: 631 Effective Date: 111/2017 Expiration Date: 12f3112017 Date of Last Amendment: 3/141201 T This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to duct pena{ties andfor decertification for infractions as set forth in 15A NCAC 2H.0897. Nr 4— O N N M 0.- Q0 ce) 4— O d- c'7 0) (15 d North Carolina WastewaterlGmundwater Laboratory Cert"rfication Certified Parameters Listing Lab Name: Summit Environmental Technologies, Inc. Certificate Number: 631 Address: 3310 Win Street Effective Date: 111/2017 Cuyahoga Falls, OH 44223- Expiration Date: 12f31l2017 Date of Last Amendment: 3/14/2017 The above named laboratory, having duly met the requirements of t 5A NCAC 211,0800, is hereby certifed for the measurement of the parameters ilsted below. r...... .. ._.__...,.. .......___ __. ...... . CERTIFIED PARAMETERS MAGNESIUM EPA 200.7. Rev, 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) MANGANESE EPA 200.7, Rev, 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous EPA 200.9, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) MERCURY EPA245.1, Rev.3.0, 1994 (Aqueous) SW-846 747C A (Aqueous) SW-846 7471 B (Non -Aqueous) EPA 1631 E (Aqueous) MOLYBDENUM EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 601C D (Aqueous) SW-845 601C D (Nan -Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) NICKEL SW-846 601C D (Non -Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6C20 B (Non -Aqueous) POTASSIUM EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) SELENIUM SW-846 6010 D (Non -Aqueous) EPA 24C.8, Rev. SA, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-8466020 B (Non -Aqueous) SILVER EPA 200.7. Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 8 (Non -Aqueous) SODIUM EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Nan -Aqueous) STRONTIUM EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) EPA 200.8. Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) THALLIUM EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) EPA 200.8, Rev. 5.4, 1004 (Aqueous) SW-846 6020 S (Aqueous) SW-846 6020 S (Non -Aqueous) TIN EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Non -Aqueous) VANADIUM EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) SW-846 6020 B (Non -Aqueous) T imce-Acab[xt requires r 4ffmo= a[ an mccictable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples, labaratories are subject to dvi[ penalties andlar decertification for infractions as set forth in 15A NCAC 2HA807. IT H O M W O) (>3 0.. North Carolina Wastewater/Groundwater Laboratory Certification Certified Parameters Listing Lab Name: Summit Environmental Technologies, Inc. Address: 3310 Win Street Cuyahoga Falls, OH 44223- Certificate Number: 631 Effective Date: 1/1/2017 Expiration Date: 12131/2017 Bate of Last Amendment: V1412017 The above named laboratory, having duly met the requirements of 15A NCAC 2H.C8OO, is hereby ceffk for the measuremeni of the parameters listed below, CERTIFIED PARAMETERS ZINC TOTAL ORGANIC HALIDES SW-846 6010 D (Nan -Aqueous) SW-846 9020 B (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) TPH DIESEL RANGE, ORGANICS SW-846 6020 B (Aqueous) SW-846 8015 C (Aqueous) SW-846 6020 B (Non -Aqueous) SW-846 9015 C (Non Aqueous) ORGANIC TPH GASOLINE RANGE, ORGANICS TCLP ORGANICS SW-846 8015 C (Aqueous) SW-846 1311 (Aqueous) SW-846 8015 C (Nan -Aqueous) ADSORBABLE ORGANIC HALIDES VOLATILE PETROLEUM HYDROCARBONS EPA 1650, Rev. C, 1997 (Aqueous) MADEP, May 2004, Rev. 1.1 (Aqueous) BASE NEUTRAL/ACID, ORGANICS EPA 625 (Aqueous) SW-846 8270 D (Aqueous) SW-846 8270 D (Non -Aqueous) CHLORINATED ACID HERBICIDES SW-846 8151 A (Aqueous) SW-846 8151 A (Non -Aqueous) CHLORINATED PHENOLICS EPA 1653, Rev. A, 1997 (Aqueous) EXTRACTABLE PETROLEUM HYDROCARBONS MADEP, May 2004, Rev_ 1.1 (Aqueous) NONHALOGENATED VOLATILE, ORGANICS SW-8M 8015 C (Aqueous) PESTICIDES, ORGANOCHLORINE EPA 608 (Aqueous) SW-846 8081 B (Aqueous) SW-846 8081 B (Non Aqueous) POLYCHLORINATED BIPHENYLS (PCBs) EPA608 (Aqueous) SW-846 8082 A (Aqueous) SW-846 8082 A (Nan -Aqueous) PURGEABLE, ORGANICS EPA 624 (Aqueous) SW-846 a260 B (Aqueous) 5W-846 8260 B (Non -Aqueous) This certification requires maintance of an aoceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penalties and/or decertification for infractions asset forth In 15A NCAC 2H.0807. O (D 0) SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Beaufort WWTP Name: Town of Beaufort WWTP WQ Permit Number: WQ0006017 NPDES Number: NCO021831 Monitoring Period: From 01/01/2019 To 12/31/2019 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt, 1/A (time/temp) Alt. 2/B (Aik Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If ., n1: hln to altnv.00ti.. —fnr,, A lf9acc A nr Cl... Rl nnm W. tha fnnnwina m h.rina dnfn- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 611 MPN MPN/g Coliform power per gram of total solids 4640 8220 39200 CFU/g 0 Annually Grab SM9222D CFU 1000 MPN per gram of MPNIg total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33115A NCAC 02T.1107) -Please indicate optionlalternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Aft. 6 OptionlAlt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Ir&ction) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Donavan Willis, Director of Public Works Todd Larson, OperaAoQWirhptor Preparer Name and Title (type or print) Land e a e) (type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report NC DENR #654 NO PHHS #37799 US EPA#NG01918 190643 Yes J. zubeck 0 04104/19 190643 B1 9ludse Of Pec, Collform-5 3920o GFurs 6640 04/04/19 SB 9222D - MF B2 <6140 cruie 6140 B3 11800 CFu/9 5880 B4 5680 ePuio 5680 B5 4640 mig 4610 B6 <5780 uuig 5780 B7 5850 Mfg 5860 Geomean 8220 190643 B1 siudgq or TS (%} 15.3% 0.01 04/04/19 SB 2540 0 -TS B2 16.3% 0.01 83 17.0% 0.01 B4 17.6% 0.01 B5 21.7% 0.01 B6 17.3% 0.01 B7 17.1 % 0.01 Report RBYIeW Project Manager Date 919-208-4240 219 S. Steele Str. chris{3a aamerontesting.co►n Sanford NC 27330 219 S. Steele Str. g ihain of Cult y Cameron Testing Services Inc.. ga9� l of Rnniard_ NC 27330 .....n,,.�.+,R� .+-. 4Q9A Alf, ❑E-tNC C orrt # 17799 LIS EPA NC01918 SECTION 6 Agricultural Lime Application Log Year: 2©19 Beaufort, NC Field 11 Soil Lime Requirement 11 Tons/Acre Date Applied (state -county -site -field) pH (tons/acre) L Applied NC-CR-7T3A 5.71 OAJ 0 nla *Lime will be spread when conditions improve SECTION 7 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil Report No. FY20-SL001712 Client: Bobby Riggs Advisor: Predictive 483 Weatherington Landing Rd ,.! Stella, NC 28582 Soil Report Mehlich-3 Extraction Sampled County: Carteret Links to Helpful Information Client ID: 467267 Advisor 1D: Sampled: Received: 08/0212019 Completed: 08/12/2019 Farm: Sample ID: 01-3A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu 13 Information Lime History: 1-Soybean 0.4 0 0 100 0 0 0 0 0 0 Note: 3 2 -Corn, grain 0.0 120 - 160 0 100 0 0 0 0 0 0 Nate: 3 Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-Al Cu-1 Na ESP SS-1 NO3-N 1.14 1.31 4.5 73 1.2 5.7 194 20 56 14 45 62 47 54 282 282 265 0.1 2 Sample ID: 07-02 Recommendations: Lime Nutrients (Iblacre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 1.0 0 0 80 25 0 0 0 0 0 Note: 3 2 -Corn, grain 0.0 120 - 160 0 80 $ 0 0 0 0 0 Note: 3 Note: Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.66 1.36 3.6 57 1.6 5.0 385 28 47 6 38 88 63 70 261 261 498 0.1 3 —k,N:orth Carolinal Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxier, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.neagr.gov/agronomi/ Report No. FY20-SLOOl712 Bobby Riggs Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. -I copper index ES ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K2O potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. if they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source, 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-O mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients, In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronorri/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawnslgardens, are listed in units of Ib11000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncaar.govlagronomiloboart4.htm sfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P2O5 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-Al Zn-I zinc availability index zinc index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-1, Zn-Al, Cud, S-1, SS-1, Na, ESP, SS -I, NO3-N (not routine])' available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.govlagronomiluyrst.htm