WQ0000543_Residual Annual Report 2019_20200302

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0000543
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0000543
Applicant\Permittee * SYNAGRO
Facility Name * City of Sanford
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for City of Sanford
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
SANFORD NC 2019 Annual Report FINAL.pdf 14.59MB
Upload only 1 RDF document. NL@iple documents must be combined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/27/2020

435 Williams Court, Suite 100
Baltimore, NIT) 21220
wwwsynagroxom
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0000543
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Sanford, NC.
If you have any questions or need additional information, please do not hesitate to contact Scott
Siletzky at [phone] or Melinda Boyd at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Melinda Boyd, Synagro
Scott Siletzky, City of Sanford
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF SANFORD
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000543
2019 ANNUAL REPORT

City of Sanford, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Pages
S. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WQ0000543 County Lee Year 2019
Facility Name (as'shown on permit) City of Sanford WWTP .NPDES No. NCO024147
Land Application Operator S na ro Phone#f [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summary;
Total number of application fields in the permit: 43
Total number of fields utilized for land application during the year: 13
Total amount of dry tons applied during the year for all application sites: 427.31
Total number of acres utilized for land application during the year: 231.62
Part —Annual Compliance Statement:
Facility was compliant during calendar year 20I9 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality YES X NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T . 1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T . 1111 were complied with (applicable to 40 CFR Part 503
regulated facilities),
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff' of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C -- Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." _ j , r i
Hal Hewer, Public City Manager, _ _ .
Permittee Name and Title (type or print) Si azure Pe itt Date
)
Signature of Preparer* D e Signat e App1G Date
(if different from Permittee) (if different from ermittee and Preparer)
*Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

!"31Yff N A G R 0
February 10, 2020
REFERENCE: EXPLINATION OF NON -COMPLIANT ANNUAL REPORT OF
PERMIT # WQ0000543 City of Sanford RLAP
On behalf of the City of Sanford, Synagro is submitting an explanation of why the 2019
annual report is marked as "non -compliant:. In this annual report you will find 2 nutrient &
metals analysis results, however due to the dry tons land applied throughout the calendar year
of 2019, 4 are required to be complaint with permit conditions.
The appropriate number of nutrients and metals samples were retrieved throughout the
year, however issues including poor solids representation in samples and shipping/delivery of
material yielded inconsistent sample results. The discovery of the lack of nutrients and metals
was determined after January 1st which has ultimately led to the status of "non -complaint".
Due to wet weather an unsuitable spreading conditions, ample material has been stored and a
sample was taken after January 1st in an effort to preserve compliance. The results of this
sample yielded compliant data and is available upon request.
To avoid future issues, additional training is being conducted to outline the importance of
having the appropriate number of samples in the calendar year. Additionally, a new level of
checks and balances will be developed to ensure samples are taken, delivered and reported in
the correct timeframe.
If you have any further questions, please contact me at [phone] or
mbo d ads na ro.com
Sincerely,
Melinda Boyd
Technical Services Specialist
Synagro
284 Boger Road, Mocksville, IBC 27028 • Phone: [phone] • Fax: [phone]

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
SANFORD,NC
SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
MONTHIYEAR
June 2019
July 2019
August 2019
September 2019
November 2019
December 2019
YEARLY TOTAL
DRY METRIC
AMOUNT
UNIT
DRY TONS
UNIT
TONS
260,400.00
G
19.77
D
17.92
285,200.00
G
21.64
D
19.62
514,600.00
G
72.97
D
66.17
1,370,200.00
G
194.26
D
176.21
737,800.00
G
104.60
D
94.89
99,200.00
G
14.07
D
12.76
3,267,400,00
G
427.31
D
387.57
1 /30/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000543
Facility Name: SANFORD, NC
NPDES## : NCO024147
or WQ# (residual only)
WWTP Name: BUFFALO CREEK WWTP
Residuals Analysis Data
Product Type AEDLIQ AEDL14
Date Sampled (grab) or 02/11/19 09/10/19
Date Composited
Percent Solids 1.82 3.40
PARAMETERS (mgtkg dry weight)
Arsenic
<5
6.26
Cadmium
1.69
2.02
Mercury
0.347
0.496
Chromium
125
110
Copper
413
428
Lead
25.3
27.8
Molybdenum
19.9
16.5
Nickel
57.8
63.1
Selenium
<5
5.06
Zinc
874
928
Total Phosphorus
25200
26000
TKN
128000
55300
Ammonia -Nitrogen
32200
24700
Nitrate and Nitrite
5390
<4. 59
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X '
(SIGNATURE OF PREPORE
DENR FORM RSSF (5/2003)
Date !r) �C�
Printed: Saturda - Febru@rV 1 2020 at 16:05:44 for; 2039 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000543
Facility Name: SANFORD, NC
NPDES# : NCO024147
or WQ# (residual only)
WWTP Name: BUFFALO CREEK WWTP
Residuals Analysis Data
Product Type AEDLIQ AEDLIQ
Date Sampled (grab) or 02/11/19 09/10/19
Date Composited
Percent Solids 1.22 3.40
PARAMETERS (mglkg dry weight)
Aluminum
8030
11800
Calcium
17200
17800
Magnesium
4360
433C
pH
7.70
7.30
Potassium
7050
5080
Sodium
3220
2480
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing Violations."
x
URE OF PREP
NR - Data Not Reported or Data Not Required
Date . 1 ? oQ
DENR FORM RSSF-B (712002) Printed: Saturday- February 1, 2020 at 16:06:46 for: 2039 01

WayPAoi nt,(2)
NALYT[CAL
2/22/2019
Synagro Central LLCI Sanford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 19-045-0201
Project Description: Sanford
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/14/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Page 1 of 6

Waypoint.(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-045-0201
Client Project Description: Sanford
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
SM-4500-NH3C
WTN
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
9045D
WrN
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
4500NO3F-2011
WTN
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
601DD
WTN
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
SW-7471B
WTN
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
SM-45o0-NH3C-TKN
WTN
64800
Sanford 1
Solids
02/11/2019 15:00
02/14/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Momphis, TN, Certification: #1354
Page 2 of 6

Report Number: 19-045-0201
Account Number: 46489
Send To: Synagro Central LLCI Sanford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 64800
Sample Id : Sanford 1
a
Waypoint,(2
ANALYTICAL
Project : Sanford
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa na lytical,com
Date Sampled: 2/11/2019 15:00:00
Date Received: 02/14/2019 00:00
Date Reported: 02/22/2019
Total Solids
1,82
18200
100.0
CJR
02/18/2019 13:58
SM-2540G
Moisture *
98.20
100.0
CJR
02/18/2019 13:58
SM-2540G
Total Kjeldahl Nitrogen
12.80
128000
250
CLP
02/20/2019 09:30
SM-4500-NH3C-TKN
Phosphorus
2.52
25200
50.0
KKM
0211912019 21:32
6010D
Potassium
0,71
7050
50.0
KKM
02/19/2019 21:32
60100
Sulfur
1.19
11900
50.0
KKM
02119/2019 21:32
6010D
Calcium
1.72
17200
250
KKM
02119/2019 21:32
6010D
Magnesium
0.44
4360
50.0
KKM
02119/2019 21:32
6010D
Sodium
0.32
3220
250
JTR
02120/201919:29
6010D
Iron
18500
50.0
KKM
02/1912019 21:32
6010D
Aluminum
8030
50.0
JTR
02/20/201919:29
6010D
Manganese
1540
5.00
KKM
02/1912019 21:32
6010D
Copper
413
2.50
KKM
02/19/2019 21:32
6010D
Zinc
874
12.5
KKM
02/19/2019 21:32
6010D
Ammonia Nitrogen
3,22
32200
100
ZBD
02/20/2019 09:00
SM-4500-NI3C
Organic N
9,58
95800
250
02/20/2019 09:00
CALCULATION
Nitrate-:-Nitrite-N
6390
4.95
ZBD
02/18/201913:59
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time pff;G f"C 6fwr
Our reports and fetters are for the exclusive and confidential use of our ciients, and may not be reproduced in whole or part, aormay any reference be made Pauric McCreary
to the work, the results; or the company in any advertising, news release, or other pudffc announcements without obtaining our prior written authorization_
Agronomist
Page 3 of 6

Report Number: 19-045-0201
Account Number: 46489
Send To: Synagro Central LLC/ Sanford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 64800
Sample Id : Sanford 1
s
Waypoin(2t.
ANALYTICAL
Project : Sanford
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 2/11/2019 15:00:00
Date Received: 02/14/2019 00:00
Date Reported: 02/22/2019
Cadmium
1.69
1.00
KKM
02/1912019 21:32
601 OD
Chromium
125
2.50
KKM
02/1912019 21:32
601 OD
Nickel
57.8
2.50
KKM
02/1912019 21:32
6010D
Lead
25.3
3.00
KKM
02/19/2019 21:32
6010D
Arsenic
<5.00
5.00
KKM
02/19/2019 21:32
601 OD
Mercury
0.347
0.0158
TJS
02/19/2019 13:47
SW-7471 B
Selenium
<5.00
5.00
KKM
0211912019 21:32
6010D
pH*
7.7
JSL
02/20/2019 08:05
9045D
Molybdenum
19.9
2.50
KKM
02/1912019 21:32
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use or our clients, and may not be reproduced in whole or part, nor may any reference be made
fo the work, the results, or the company in any advertising. news release. or other public announcements without obtaining our prior written authorization_
pof 44 60wr
Pauric McGroary
Agronomist
Page 4 of 6

Waypoin(Dt.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46489
Customer Name: Synagro Central LLC/ Sanford
Report Number: 19-045-0201
Shipping Method
Fed Ex (D US Postal 0 Lab
0 UPS C) Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
Yes
No
Number of coolers received
1 '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 NIA
Trip Blanks received with VOAs
0 Yes
i) No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Morgan Tichacek I Date & Time: 2/14/2019 13:04:32
Page 5 of 6

SAMPLING LOG #
1111111111111111111ll
1�11111111111111111111111111
ALLASS, lh C,
q9-44--20181
CHAIN OF CUSTODY
Svnanra Central LLC! Sanford
13:03:27
RECORD & ANALYSIS
CUSTOMER: SYNAGR®
Sanford
446 RECORD
/��
`r'rle�r�
1�fl�cl ��r,��c� W ��t�
-
l attest that the proper held sampling
A PProcedures
PROJECT MANAGER: ! yU'
�
were used during the collection of these samples.
— �
Phone:
SAMPLER
A & L CUSTOMER
SAMPLING SAMPLE
# OF
SAMPLING METHOD METHOD
LAB # SAMPLE I.Q.
LOCATION TYPE
CONTAINERS
DATE TIME PRESERVED SHIPPED
v y SCWJ�rk � 4 L f
A CIrl�r% l05- CKC,i a +tip %\1rc�l LA k "4 '
Relinquished by Sampler: Date Time Recieved by: REMARKS:
2!L3 2:00
Relinquished by: Date Time Recieved by-
kA �---
if/Ii2:
Relinquished by: Date Time tecieved by:
SPECIAL INSTRUCTIONS:
For 1 v L monitoring purposes. pO#,
{STAT Z)
SAMPLE ANALYSIS REQUEST
I.D. SL1 SL2 NH4-N NO3-N Organic Cd Cr Ni Pb As Hg Se pH CaCO3 Volatile Mo ClNO -N
equiv.Solids z
SL1: Total Solids (Moisture), Total Kjeldah) Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc��
`
T)Ug�.h iV C. a z ��
cll � W h,n (0o�r .

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 2/11/2019 2/112019-7/3112019 0.7637
AEROB. DIG, LIQUID
Na mgll = (Na mg/kg x % Solids) � 100 = (3220 x 1.8200) + 100 = 58.604
Ca mg/l = (Ca mg/kg x % Solids) + 100 = (17200 x 1.8200) + 100 = 313.04
Mg mg/1 = (mg mgtkg x % Solids) + 100 = (4360 x 1.8200) + 100 = 79.352
Na meq = Na mgll + Molec.Wgt.Na = 58.604 + 23 = 2.548
Ca meq = Ca mgll _ Molec.Wgt.Ca = 313.04 + 20 = 15.652
Mg meq = Mg mgll + Molec.Wgt.Mg = 79.352 + 12 = 6.61267
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.548 + SgrRoot[0.5(15.652+6.61267)] = 0.763671
Printed: 2/1/2020
Page 1 16:07

(2)
Waypoint.NALYTICAL
9/20/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-255-0005
Project Description: BB3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/12/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
? ', fu 6-7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

Waypoin,(Dt.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-255-0005
Client Project Description: BB3
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
68176
BB3
Solids
09/10/2019
14:30
09/12/2019
68176
BB3
Solids
09/10/201914:30
09/12/2019
SM-45D0-NH3C
WTN
68176
13133
Solids
09/10/201914:30
09/12/2019
9045D
WTN
68176
13133
Solids
09/10/201914:30
09/12/2019
4500NO3F-2011
WTN
68176
B33
Solids
09110/201914:30
09/12/2019
6010D
WTN
681Y6
BB3
Solids
09/10/201914:30
09/12/2019
SW-7471B
WTN
68176
13133
Solids
09/10/2019
14:30
09/12/2019
SM-4500-NH3C TKN
WTN
68176
13133
Solids
09/10/201914:30
09/12/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: 4460181 - Virginia
Page 2 of 6

Report Number: 19-255-0005
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68176
Sample Id : BB3
Waypoint,(2)
ANALYTICAL
Project : BB3
REPORT OF ANALYSIS
76211Nhitepine Road, Richmond, VA 23237
Main 304-743-9401 ° Fax [phone]
www.waypointanalyticai.com
Date Sampled: 9/10/2019 14:30:00
Date Received: 09/12/2019 00:00
Date Reported: 09/20/2019
Total Solids *
3.40
ADM
09/16/2019 16:43
SM-2540G
Moisture *
96.60
ADM
09/16/2019 16:43
SM-254OG
Total Kjeldahl Nitrogen
5.53
55300
250
JPJ
09/1912019 13:00
SM-4500-NH3C-TKN
Phosphorus
2.60
26000
50.0
BKN
09/171201919:47
6010D
Potassium
0.51
5080
50.0
BKN
09117/201919:47
6010D
Sulfur
1.16
11600
50.0
BKN
09/17/201919:47
6010D
Calcium
1.78
17800
250
BKN
09/17/201919:47
6010D
Magnesium
0.43
4330
50.0
BKN
09/17/201919:47
6010D
Sodium
0.25
2480
250
BKN
09/17/201919:47
6010D
Iron
21600
50.0
BKN
091171201919:47
6010D
Aluminum
11800
50.0
BKN
09117/201919:47
6010D
Manganese
1550
5.00
BKN
09117/201919:47
6010D
Copper
428
2.50
BKN
09/17/201919:47
6010D
Zinc
928
12,5
BKN
09117/201919:47
6010D
Ammonia Nitrogen
2.47
24700
100
JPJ
09/19/2019 15:30
SM-4500-NH3C
Organic N
3.06
30600
250
09/19/2019 13:00
CALCULATION
Nitrate+Nitrite-N
<4.59
4.59
ZBD
09/191201915:08
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank
H - Beyond holding
time
pwir-
XC 1QQK1
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising. news release. or other public announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number: 19-255-0005
Account Number: 46622
Send To: Synagro Central LLCI Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68176
Sample Id : BB3
Ar
i
Waypointw
ANALYTICAL
Project : BB3
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.corn
Date Sampled: 9/10/2019 14:30:00
Date Received: 09/12/2019 00:00
Date Reported: 09/20/2019
Cadmium
2.02
1.00
BKN
09117/201919:47
6010D
Chromium
110
2.50
BKN
09117/201919:47
6010D
Nickel
63.1
2.50
BKN
09/171201919:47
6010D
Lead
27.8
3.00
BKN
09117/201919:47
6010D
Arsenic
6.26
5.00
BKN
09/171201919:47
6010D
Mercury
0.496
0.0148
TJS
09/17/2019 13:39
SW-7471 B
Selenium
5.06
5.00
BKN
09117/201919:47
6010D
pH"
7.3
JSL
09118/2019 06:19
9045D
Molybdenum
16.5
2.50
BKN
09/17/201919:47
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising. news release. or other public announcements vdthout obtaining our prior written authorization.
polie. If 11614 /
Pauric McGroary
Agronomist
Page 4 of 6

Waypoint, 7621 (2) Whitepine Road, Richmond, VA 23737
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 19-255-0005
Shipping Method
I* Fed Ex 0 US Postal () Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
0 No
Number of coolers received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
Yes
0 No
0 NIA
Trip Blanks received with VOAs
Yes
0 No
0 NIA
Sail VOA method 5035 — compliance criteria met
0 Yes
0 No
0 NIA
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0 No
Comments:
Signature: !Brandi Watson 1 Date & Time: I09/12/2019 10:37:42
Page 3 of 6

,r: F-- i. CUSTOMER
LAB i{ SAMPLE I.D.
Reel nquishecl by Sampler:
Relinquished by -
Relinquished ay:
SPECIAL ffi3STRUCTIONS'
.��Att
11111�11111111111111111111111111111111 111 09-� �°gs
Svnaflr* Central LLCI T"hnical 10_371-5
BM
SAMPLING SAMPLE r' ,;b
LOCATION TYRE CONTAIhEPS
'4 L
Date
V iit
Bate i
q
©ate r__..'..
r-rloniterirlo p=urpose&
C(DR0 & a x A U117'sC21
RECORD"
, ��(FCS1 Ff7c`Ii f17c' {7�C���'f PiE?�C1` Sc�it7fJ1(I1Cl t`_7fC�C�f�iC1l��
Ivvere used, during the- c-o11ection of th-c-se .3o.,g pies
SAMPLER
SAMPLING
METHOD HOD
METHOD
DAT E
€ iME
PRESERVED
S iPPED
Ott �u:
50
Time Serieve °,,y
fA
Time Rpcleved bv:
S'L v. Tctai Solids (Moisture), Total ; ja€clahl Nitrogen, Phosohcrus. and Potassiu€
S12: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, MLIrtganese. Copper aj�d Zinc b • �
Page 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 9110/2019 81112019-1213112019 0.7950
AEROB. DIG. LIQUID
Na mg11 _ (Na mg/kg x % Solids) + 100 = (2480 x 3.4000) + 100 = 84.32
Ca mg/l = (Ca mg/kg x % Solids) . 100 = (17800 x 3.4000) + 100 = 605,2
Mg mg/l = (mg mg/kg x % Solids) + 100 = (4330 x 3.4000) + 100 m 147.22
Na meq = Na mg/l + Molec.Wgt.Na m 84.32 + 23 = 3.66609
Ca meq = Ca mgll _ Molec.Wgt.Ca = 605,2 + 20 = 30.26
Mg meq = Mg mg/l + Molec.Wgt.Mg m 147.22 + 12 = 12.2683
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.66609 + SgrRoot[0.5(30.26+12.2683)] = 0.795021
Printed: 2/1/2020
Page 1 16:07

SECTION 3

FACILITY NAME: SANFORD, NC
OWNER: HENRY STINSON
SITE #: NC CH 00049 FIELD# : CH 00049 0006
RESIDUAL SOURCE(S): See list at bottom of report
LAAUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 16.70
OPERATOR; HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.34 ACRES PERMITTED: 7.34
Page: 1
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Solids
D �3
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
cation
cation
Method
Villa
tili-
zation
Miner -
ali-
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
p
(pp-)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
11/26/19
55,800.00 (G)
7602.180
3,40
1.078
SBCAEDL
MOIST
"0-<112"
SUR
0.5
0.30
55,300. p
24,700M p
4.59 p
21535
FESCUE
11/27/19
62,0M00 (G)
8446.866
3.40
1.198
SBCAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
Nov-I4
117,800.00 (G)
16,049.046
1 uwj UWJO 5fLic: 10,U4Y.Vn
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual ]bs/acre 98
0.028 0.009 0.501 1,948 0.127 0.002 0.075 0.287 0.023 4.223 118.32
Cumulative lbs/acre
0.159 0.128 2.758 16.029 1.020 0.065 0.720 1.831 0.180 34.389
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
178
PD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.E
34.8
''
1339.E
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg./kg ** Volatilization Rate: Surface 0.5, htjection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD, NC
OWNER: HENRY STINSON
SITE #: NC CH 00049 FIELD# : CH 00049 0007
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : CID
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 50.98
OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 18.86 ACRES PERMITTED: 18.86
Page: I
Lune Applied ***
Date
Lb,/A.
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
[
f Per Acre
l
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1 V21/19
192,200.00 (G)
10190.880
3,40
1.445
SBCAEDL
MOIST
11
0- 1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
11/22/19
167,400.00 ((3)
8875.928
3.40
1.258
SBCAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
55,300, p
24,700.00 p
4.59 p
21535
FESCUE
Nov-19
359,600.00 (G)
19,066.808
Total Gallons/Ac: 19,066.81
Total Wet Tons/AC:
Total Cubic YdslAc: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 116
0.034 0.011 0.595 2314 0150 0.003 0.089 0.341 0.027 5.017 I40.57
Cumulative lbslacre 0.185 0.138 3.216 17.630 1.057 0.066 0.853 2.005 0.196 36.110 Nwi
Permit PAN Limit (lbslacre) Ist Crop/2nd Crop
1 78
i
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15.0go
375.0
89.0
2500.0
;
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
p
X qw`
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted, I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INI - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITYNAME: SANFORD,NC
OWNER: HENRY STINSON
SITE #: NC CH 00049 FIELD# : CH 00049 0009
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID
PERMIT #: W00000543 ANNUAL DRY TONS APPLIED: 13.19
OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.44 ACRES PERMITTED: 9.44
Page: I
Lime Applied I"
Date LbslAc
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
11/26/19
93,000.00 (G)
9851.6951
3.40
L397
SBCAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
p
24,700.00 p
4.59 p
21111
FESCUE
Nov-19
93,000.00 (G)
9,851.695
I
1
[7,300.
1
1
total Canons/ac; y,iS�1.6Y
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.017 0.006 0.307 1,196 0.078 0.001 0.046 0.176 0.014 2.592 72.63 60
Cumulative lbslacre
0.158 0.132 2.579 15.559 0,940 0,066 0.724 1.679 0.172 31.631
Permit FAN Limit (lbslacre) 1st Crap/2nd Crop
178
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X r
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR- Surface, IN7 - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD,NC
OWNER: CYNTHIA/ANGELA STORY/F-ADES
SITE 4: NC CH 00066 FIELD#t : CH 00066 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID
PERMIT 9: WQ0000543 ANNUAL DRY TONS APPLIED: 3.52
OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 21.68 ACRES PERMITTED: 21.68
Page : 1
Lime Applied ***
Date
Lbs1Ac
3allons (0) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli
Vote' -
%
Tons
Cond.
Precip.
cation
Ammonia
Nitrate
PAN
Total
Per Acre
or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
TKN
Nitrogen
and
(ppm}
Crop
Acre
Source
Moist
Hours
*
Nitrite
12/4/19
24,800.00 (G)
1143.9111
3.40
0.1b2
SBCAEDL
DRY
0-<1/2"
SUR
.30
55,M0.p
24,700.00 p
4.59 p
21535
FESCUE
Dec-19
24,800.00 (G)
1,143.911
T7
ro[ai Nations/AC: l,J4S.yl
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.002 <.001 0.036 0.139 0.009 <.001 0.005 0,020 0.002 0.301 8.43 7
Cumulative lbs/acre 0.082 0.024 1.929 6.012 0.339 0.008 0.205 0.853 0.070 9.749
Permit PAN Limit Obs/acre) Ist Crop/2nd Crop
............
17$
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15.0
375A
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X d
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA —Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SANFORD, NC PREDOMINANT SOIL SERIES: CID
OWNER: CYNTHIA/ANGELA STORY/EADES PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 18.46
SITE #: NC CH 00066 FIELD# : CH 00066 0008 OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 6.17 ACRES PERMITTED: 6.17
Page : 1
Lime Applied ***
Date Lbs�Ac
allons (G) or Cubic Yards (CY)
or
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAIN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
#
Rate**
Rate
Nitrite
I 1/27/19
55,800.00 (G)
9043.760
3.40
1.282
SBCAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
55,300, p
24,700.00 p
4.59 p
21535
FESCUE
Nov-19
55,800.00 (G)
9,043.760
12/4/19
1 74,400.00 (G)
12058.3471
3.40
1.710
SBCAEDL
DRY
0-<1/2"
SUR
0.5 1
0.30
55,300. p
24,700,00 p
4.59 p
21535
FESCUE
Dec-19
74,400.00 (G)
12,058.347
1
1
total uattonsiAc:
Total Wet Tons/Ac:
Total Cubic Yds/Ac:
Li,lus.ii
Permit PAN Limit (ibs/acre) 1st Crop/2nd Crop
178
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
9X "2
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR W Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD,NC
OWNER: STINSON, JR HENRY
SITE #: NC CH 00066 FIELD# : CH 00066 0011
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 15.92
OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.13 ACRES PERMITTED: 7.13
Page: 1
Lime Applied ***
Date
Lbs1Ae
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
11/26/19
111,600.00 (G)
B652.1741
3.40
2.219
SBCAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
Nov-19
I11,600.00 (G)
15,652.174
1
Total UallonslAc: 15,052.17
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 96
0.028 0.009 0A88 1.900 0.123 0.002 0.073 0.280 0.022 4.119 115.40
Cumulative ]bs/acre 0.110 0.033 2.121 7.458 0.445 0.009 0.252 1.112 0.091 13.060
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
178
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
?
1339.0
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
x - -J
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A= Not Applicable NR=Not Reported or Not Required %=percent p = pp- or mg/kg ** 'Volatilization Rate : Surface 0.5, hijectien/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection; SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : SANFORD, NC
OWNER: PAUL & LUCY PRICE
SITE #: NC CH 00077 FIELD # : CH 00077 0001
RESIDUAL SOURCE(S): See list at bottom of report
LfNUAL LAND APPLICATION )FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID SILT LOAM
PERMIT 4: WQ0000543 ANNUAL DRY TONS APPLIED: 16.00
OPERATOR: PAUL & LUCY PRICE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.50 ACRES PERMITTED: 16.50
Page: I
Lime ,Applied ***
Date
LbdAc
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
7/2/19
68,200.00 (G)
4133.333
1.82
0.314
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
128,00(p
32,200.00 p
6,390.00 p
51230
FESCUE
7/3/19
111,600.00 (G)
6763.636
1.82
0,513
SBCAEDL
DRY
0-<1/2"
SUR
0.5
030
128,00(p
32,200.00 p
6,390.001)
51230
FESCUE
7/5/19
31,000.00 (G)
1878.788
1.82
0.143
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
128,00(p
32,200.00 p
6,390.00 p
51230
FESCUE
Jul-19
210,800.00 (G)
12,775.757
iomivauons/Ac: iz,rl5.lb
Total Wet Tons/Ac:
Total Cubic Yds1Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Ma Ni Se Zn P PAN
Annual lbs/acre 0,010 0.003 0.242 0.801 0.049 <.001 0.039 0.112 0.010 1.695 48,87 99
Cumulative lbs/acre 0.010 0.003 0.242 0.801 0.049 <.001 0.039 0.112 0.010 1.695
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
t
E
178
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15 0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREED WWTP AEROB. DIG. LIQUID
X ;Z-{,!
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR- Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD, NC
OWNER: PAUL & LUCY PRICE
SITE #: NC CH 00077 FIELD# : CH 00077 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID LIGNUM
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 42.19
OPERATOR: PAUL & LUCY PRICE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 15.60 ACRES PERMITTED: 15.60
Page : 1
Lime Applied sxs
Date
Lbs1Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip,
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/12/19
124,000.00 (G)
794'.7I'
3.40
1.127
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
9/13/19
31,000.00 (G)
1987.171
3.40
0.282
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4,59 p
21135
FESCUE
9/23/19
105,400.00 (G)
6756A10
3.40
0.958
SBCAEDL
DRY
0-<112"
SUR
0.5
0,30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
9/24/19
37,200M (G)
2384.615
3.40
0.338
SBCAEDL
DRY
0-11/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21531
FESCUE
Sep-19
1 297,600.00 (G)
19,076.922
totai uanonslAc: A9,U76.92
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAIN
Annuallbs/acre 0.034 0.011 0.595 2.315 0.150 0.003 0.089 0.341 0.027 5.020 140.65 116
Cumulative lbs/acre 0.034 0.011 0.595 2.315 0A50 0.003 0.089 0,341 0.027 5.020
Permit PAIN Limit (lbs/acre) 1st Crop/2nd Crop
189
i
r
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD, NC
OWNER: PAUL & LUCY PRICE
SITE #: NC CH 00077 FIELD# : CH 00077 0007
RESIDUAL SOURCE(S): See list at bottom of report
[ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID LIGNUM
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 52.74
OPERATOR: PAUL & LUCY PRICE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 23.40 ACRES PERMITTED: 23.40
Page: I
Lime Applied
***
Date
LWAc
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Solids
D�'
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Frecip.
Past 24
Appli-
cation
Method
Voka-
tili-
zation
Miner-
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Aate
Nitrite
9/9/19
117,800.00 (G)
5034.188
3.40
0,714
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
9/10/19
117,800.00 (G)
5034,188
3.40
0.714
S13CAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300.p
24,700.00 p
4.59 p
21535
FESCUE
9/11/19
136,400.00 (G)
5829,060
3.40
0.826
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
Sep-19
1 372,000,00 (G)
15,897.436
Total Gallons/Ac: 15,897.44
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.028 0.009 0.496 1.929 0.125 0.002 0.074 0.284 0.023 4.183 117.20 97
Cumulative lbs/acre
0.028 0.009 0.496 1.929 0125 0.002 0.074 0.284 0.023 4.183
...............
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
189
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
x eju���� a -# q `
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR —Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD, NC
OWNER: PAUL & LUCY PRICE
SITE #: NC CH 00077 FIELD# : CH 00077 0008
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NANFORD BAD1N
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 17.41
OPERATOR: PAUL & LUCY PRICE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 31.70 ACRES PERMITTED: 31.70
Page : 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
q7ation
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Nitrite
6/26H9
80,600.00 (G)
2542.587
1.82
0.193
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
128,00(p
32,200.00 p
6,390.00p
51230
SORGHUM
6I27/19
86,800.00 (G)
2738.170
1.82
0.208
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
128,00(p
32,200.00 p
6,390.00 p
51230
SORGHUM
6I28119
31,000.00 (G)
977.918
1.82
0.074
SBCAEDL
DRY
0-<112"
SUR
0.5
0.30
128,00(p
32,200.00 p
6,390.00 p
51230
SORGHUM
Jun-19
198,400.00 (G)
6,258,675
7/1/19
31,000.00 (G)
977.9181
L82
0.074
SBCAEDL
DRY
0-<I/2"
SUR
0.5
0.30
128,00(p
32,200.00 p
6,390.00 p
51230
SORGHUM
Jul-19
31,000.00 (G)J
977.918
1
Total Gallons/Ac: 7,236.59
Total Wet Tons/Ac:
Total Cubic YdslAc: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 56
0.005 0.002 0.137 0.454 0.028 <.001 0.022 0.063 0.005 0.960 27.68
Cumulative acre 0.005 0.002 0.137 0.454 0.028 <_001 0.022 0.063 0.005 0.960
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
138
3
FD Cumulative Pollutant Loading Rate Limit (lbslacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
x//ba,-/`
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD, NC
OWNER: PAUL & LUCY PRICE
SITE #: NC CH 00077 FIELD# : CH 00077 0011
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID SILT LOAM
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 87.03
OPERATOR: PAUL & LUCY PRICE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 29.10 ACRES PERMITTED: 29.10
Page: 1
Lime Applied ***
Date
Lbs/Ac
3allons (6) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
ova
'Pons
Cond.
Precip,
cation
till-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
TKN
Nitrogen
and
(PP-)
Crop
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
8/20/19
86,800.00 (G)
2982.818
3.40
0.423
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
8/21/I9
148,800.00 (G)
5113.402
3.40
0.725
SBCAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
55,300.p
24,700.00 p
4.59 p
21535
FESCUE
Aug-19
1 235,600.00 (G)
8,096.220
9/3/19
167,400.00 (G)
5752.577
3.40
0.816
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
IFESCUE
9/4/19
136,400.00 (0)
4687.295
3.40
0.665
SBCAEDL
DRY
0-11/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
E
! FESCUE
9/9/I9
74,400.00 (G)
2556.701
3.40
0.362
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
Sep-19
378,200.00 (G)
12,996.563
JFESCUE
lbtal Gallons/Ac: 21,092.78
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.037 0.012 0.658 2.560 0,166 0.003 0.099 0.377 0.030 5.550 155.51 129
Cumulative Ibs/acre 0.037 0.012 0.658 2.560 0.166 0.003 0.099 0.377 0.030 5.550
Permit PAN Limit Obs/acre) Ist Crop/2nd Crop
178
n
a
z
,
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375,0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % - percent p = Pp- or m&8 ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR- Surface, 1NJ - Injection, SURIN - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD, NC
OWNER: PAUL & LUCY PRICE
SITE #: NC CH 00077 FIELD# : CH 00077 0012
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CID SILT LOAM
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 8.00
OPERATOR: PAUL & LUCY PRICE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 14.40 ACRES PERMITTED: 14.40
Page: I
Lime Applied ***
Date
Lbs1Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/28/19
62,000.00 (G)
4305,556
1.82
0.327
SBCAE➢L
DRY
0-<1/2"
SUR
0.5
0.30
128,00(p
32,200,00 p
6,390.00p
51230
FESCUE
Jun-19
62,000.00 (G)4,305.556
7/1/19
43,400.00 (G)
3013.8891
1.82
0.229SBCAEDL
DRY
0<1/2"
SUR
0.30128,00(p
32,200.00 p
6,390.00 p
51230
FESCUE
Jul-19
43,400.00 (G)
3,013.889
Total Gallons/Ac: 7,319.44
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.006 0.002 0.139 0.459 0.028 <.001 0.022 0.064 0.006 0.971 28.00 57
Cumulative lbs/acre 0.006 0.002 0.139 0.459 0.028 <.001 0.022 0.064 0.006 0.971
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
i
«
s
<
178
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15 0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X F/ q -I�--it,
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: SANFORD, NC
OWNER: PAUL & LUCY PRICE
SITE #: NC CH 00077 FIELD# : CH 00077 0016
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD ,SUMMARY FORM
PREDOMINANT SOIL SERIES: CID LIGNUM
PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 85.27
OPERATOR: PAUL & LUCY PRICE CATION EXCHANGE CAPACITY {NON-503):
ACRES UTILIZED: 30.30 ACRES PERMITTED: 30.30
Page: 1
Lime Applied
***
Date
Lbs/A-
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residua]
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/19/19
192,M6.00 (G)
6343,234
3.40
0.899
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
8/20/19
86,800.00 (0)
2864.686
3.40
0,406
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
FESCUE
Aug-19
279,000.00 (G)
9,207.920
9/24/19
86,800.00 (G)
2864.686
3.40
0.406
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
I FESCUE
9125/19
124,000.00 (G)
4092.409
3.40
0.580
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21535
I FESCUE
9/26/19
111,600.00 (G)
3683.168
3.40
0.522
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
55,300. p
24,700.00 p
4.59 p
21135
FESCUE
Sep-19
322,400.00 (G)
10,640.263
Total Gallons/Ac: 19,848.18
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.035 0.011 0,619 2.409 0.156 0.003 0.093 0.355 0.028 5.223 146.33 121
Cumulative lbslacre 0.035 0.011 0.619 2.409 0.156 0.003 0.093 0.355 0.028 5.223 „
Permit PAN Limit (lbs/acre) 1st Crop/211d Crop
" ,
189
r
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15,0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN] - injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

SECTION 4

SUMMIEF
,
AnafyNcAl LAboraaioejog
March 20, 2019
Melinda Boyd
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Sanford WWTP
Summit Environmenial Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL [phone],211 FAX; [phone]
Website: ht 1Avwiy.settek.cont
Dear Melinda Boyd: Order No.: 19030410
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/8/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
Iaboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH06923, Illinois
200061, Indiana C-OH-13, Kansas E-i0347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O000i, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH00923201 I - 1, Virginia VELAP 9456, WashingtonC891
Page 1 of 33

�'T Summit Environmental Technologies, Inc. Case Narrative
S3310 Win St.
ENW([QN1A5NTAL TMIW)l st is. , rNC Cuyahoga Falls, Ohio 44223 WO#; 19030410
A77Mytdcal Laborato"L45 TEL: [phone] FAX: [phone]
Websrte: httv:l/w, msettek.aont Date: 3I2012019
CLIENT: Synagro
Project: Sanford WWTP
WorkOrder Narrative:
19030410: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the acereditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list,
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
19030410-001A 435933: Prep Comments for MtIPrep TCLP(3010A), Sample 19030410-001A: TCLP
was filtered after digestion.
Original
Page 2 of 33

M'T Summit EnrironmenralTechnologies, In Qualilrers and Acronyms
SU3310 Win S
E tVIFtONMENTAL TEiCHN01 �l; FR, lFat. Cuyahoga Falls, Ohio 442a WO#: 19030410
AnaPytical Laborata,rtes TEL: [phone] FAX.- (330) 253-446
Website: hup:11inj, r.settek co. Date: 3/20/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit,
13 The bold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimurn Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectra[ library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The anaiyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
s The spike result was outside of accepted recovery Iimits.
z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MS
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
FL
Permit Limit
MS
Matrix Spike
RegLA
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
1CV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CI'
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 33

Summit Errnironnienta! Technologies, Inc.
summlir 3310 Wiry St.
EftVI ONWENTAL tmiNnLnGiFr,, iNc Cuyahoga Falls, Ohio 44223
Aatffy lcal LaboralariL*s TEL: [phone] FAX. • [phone]
HTebsite; hitp.11unoij,.settek.coni
Workorder
Sample Summary
W04: t9030410
20-Mar-19
CLIENT: Synagro
Project: Sanford. WWTP
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
19030410-001 Sanford WWTP 3/6/2019 3:30:00 PM 3/8/20I9 10:05:00 AM Sludge
Page 4 of 33

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N N N N N N
m m cn Sn c+1 M
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O O O O O
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SUMMIN
Summit Environmental onmentar Technologies, Win StSt. .
3310
Analytical Report
ENVIf1ONIArtNTALTi_CyIPJ7LQglf-'%, �Ne7.
Cuyahoga Falls, Ohio44223
(base report)
Anatytical LAboratorle�
TEL: [phone] FAX, [phone]
Wok 19030410
Websiie: hLW.11 v,v,v. setlek. eom
Date Reported: 3/20/2019
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/6/2019 3:30:00 PM
Lab ID: 19030410-001A
Project: Samford WWTP
Client Sample ID Sanford WWTP
Analyses Result
RL
Qual Units
DP mate Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND
0.00200
mg/L
1 3/13/2019 5:06:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
0.500
mglL
1 3/15/2019 1:58:20 PM
TCLP Barium(Ba)
ND
5.00
mglL
1 3/15/2019 1:58:20 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1 3/15/2019 1:58:20 PM
TCLP Chromium(Cr)
ND
0.200
mglL
1 3/15/2019 1:58:20 PM
TCLP Lead(Pb)
ND
0,500
mglL
1 3/15/2019 1:58:20 PM
TCLP Selenium(Se)
ND
0,0500
mglL
1 3/15/2019 1:58:20 PM
TCLP Siiver(Ag)
ND
0.500
mg/L
1 3./15/2019 1:58:20 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
Analyst: BJH
TCLP SEMI-VOLATiLES ANALYSIS (SW1311/8270)
1,4-Dichlowbenzene
ND
0,0800
mg/L
2 3/12/2019 3:52:00 PM
2,4,5-Trichlarophenol
ND
0.200
mg/L
2 3/12/2019 3:52:00 PM
2,4,6-Trichlorophenol
ND
0.200
mglL
2 3/1212019 3:52:00 PM
2,4-Dinitrotoluene
ND
0.0400
mgll.
2 3/12/2019 3:52:00 PM
Cresols, Total
ND
4.00
mg/L
2 3/12/2019 3:52:00 PM
Hexachloro-1,3-butadiene
ND
0.0160
mglL
2 3/12/2019 3:52:00 PM
Hexachlorobenzene
N❑
0.0400
mglL
2 3/12/2019 3:52:00 PM
Hexachloroethane
ND
0.0800
mglL
2 3/12/2019 3:52:00 PM
Nitrobenzene
ND
0.0800
mglL
2 3/12/2019 3:52:00 PM
Pentachlorophenol
ND
0.200
mglL
2 3/12/2019 3:52:00 PM
Pyridine
ND
0.200
mglL
2 3/12/2019 3:52:00 PM
Surr: 2-Fluorophenol
35.6
10 - 109
%Rec
2 3/12/2019 3:62:00 PM
Surr: PhenoW6
35.8
10 - 109
%Rec
2 3/12/2019 3:52:00 PM
Surr: Nitrobenzene-d5
46.9
19 - 120
%Rec
2 3/12/2019 152:00 PM
Surr: 2,4,6-Tribrom a phenol
46.8
10 - 120
%Rec
2 3/12/2019 3:52:00 PM
Surr: 2-Fluorobiphenyl
45.9
22 - 117
%Rec
2 3/12/2019 3:52:00 PM
Surr: p-Terphenyl-d14
71.8
34 - 116
%Rec
2 3/12/2019 3:52:00 PM
Qualifiers: E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CaleVal
< MDL
Page 6 of 33

*umm;T-
Summit Environmental Technologies, Inc.
3310 Win Sf.
Analytical Report
ff
Arrsfyflcal taboraturM6
Cuyahoga Falls, Ohio 44223
TF7,: [phone] FAX: [phone]
(baserepork)
WO#: 19030410
Website: htw,'11i nV.settek.coin
Date Reported: 3/20/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/6/2019 3:30:00 PM
Lab ID:
19030410-OOIA
Project:
Sanford WWTP
Client Sample ID Sanford WW"IP
Analyses
Result RL Qua[ Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: SFG
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total
ND
0.250
mglL
10
3/12/2019 10:11:OD PM
Toxaphene
ND
0.500
mglL
10
3/12/2019 10:11:00 PM
Endrin
ND
0.0250
mg1L
10
3/12/2019 10:11:00 PM
gamma-BHC
ND
0.0250
mglL
10
3112/2019 10:11:00 PM
Heptachlor
ND
0.0250
d
mglL
10
3/12/2019 10:11:00 PM
Heptachlor epoxide
IUD
0.0250
mglL
10
3/12/2019 10:11:00 PM
Methoxychlor
ND
0.0250
d
mglL
10
3/12/2019 10:11:00 PM
Surf: TCMX
99.5
10 - 119
%Rec
10
3/12/2019 10:11:00 PM
Surf: DC8
114
10 - 119
%Rec
10
3/12/2019 10:11:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8151A
SW8151A Analyst: MES
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
ND
1.00
d
mg1L
1
3/19/2019 5:59:00 PM
2,4,5-TP
ND
0.500
d
mglL
1
3/19/2019 5:59:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311 M Analyst: CTB
TCLP VOLATILES ANALYSIS
M-Ur-Woroethene
ND
0.250
mglL
50
3/11/2019 3:33:00 PM
1,2-DlchloroethFine
ND
0.250
mg1L
50
3/11/2019 3:33:00 PM
MEK
ND
1.25
mglL
5D
3111/2019 3:33:00 PM
Benzene
ND
0.250
mglL
50
3/11/2019 3:33:00 PM
Carbon tetrachloride
ND
0.250
mglL
50
3/11/2019 3:33:00 PM
Chlorobenzene
ND
0.250
mglL
50
3/11/2019 3:33:00 PM
Chloroform
ND
0.250
mglL
50
3/11/2019 3:33:00 PM
Tetrachloroethene
ND
0.250
mg1L
50
3/11/2019 3:33:00 PM
Trichloroethene
ND
0.250
mglL
50
3/11/2019 3:33:00 PM
Vinyl chloride
ND
0.100
mglL
50
3/11/2019 3:33:00 PM
Surr: 4-Bromofluorobenzene
97.1
70 - 130
%Rec
50
3/11/2019 3:33:00 PM
Surr: Dibromofluoromethane
104
70 - 130
%Rec
50
3/11/2019 3:33:00 PM
Surr: Toluene-d8
102
70 - 130
%Rec
50
3/11/2019 3:33:00 PM
Qualifiers: E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit,
N
Tentatively identified compounds
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column continuation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Original
RL
Reporting Detection Limit
U
Samples with CalcVal < MDL
Page 7 of 33

UMM111-
Sr.rmnutEm,iromnental Technologies, Inc.
3310 TYin St.
Analytical Report
ENVlttt WAENTAL rt cakeunl cs o= „iNC
Cuyahoga Falls, Ohio 44223
(base report)
An,7ty0cai LgboralarjaE
TEL: [phone] FAX.- [phone]
WO#: 19030410
Mebsite: hits:/hi,rrii,.seiielr.cone
Date Reported: 3/2012019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
3/6/2019 3:30:00 PM
Lab ID:
19030410-001A
Project:
Sanford WWTP
Client Sample ID Sanford W WTP
Analyses
Result RL Qual Units
DT Date Analyzed
RCI-SOLID-WI IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND
0.490 mg/Kg 1
3/8120196:32:00 PM
RCI-SOLID-W11GNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammabEe
1
3/12/2019 12:30:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH 7.6
S.u.@20.9C 1
3/12/2019 3:21:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg 1
318/2019 6:32:00 PM
Qualifiers; D
Valua above quantitation range
M
Manual Integration used to determine area response
N
Tentatively identified compounds
O
RSD is greater than RSDlimit
PL
Permit Limit
RL
Reporting Detection Limit
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
N➢ Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < M➢L
Page 8 of 33

S Ulm% �� Surmnit Environmental Technologies, W St. Accreditation Program
33l°'v"zs'. Analytes Report
EPIVM0Nt#1CNTAL ttC91A1C7t.[ GIVS, +hii Cuyahoga Falls, Ohio 44223
.huffy 0cal taboralonin; TEL: [phone] PAX: [phone] WO#: 19030410
website: littp:/hvlvtiv.settek.coni 20-Mar-19
Client: Synagro
Project: Sanford WWTP
State: NW
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19030410-001 A Sludge
lgnitability of Solids (SW-846: 1030)
Ignitabihty
A
Sludge
pH (SW9045D)
Hydrogen ton (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4,2
Sulfide, Reactive
U
Sludge
SVOC SW-846: 8151 Herbicides-TCLP
2,4,5-TP
A
Sludge
SVOC SW-846: 9151 Herbicides-TCLP
2,4-D
A
Sludge
TCLP Mercury Analysis (SW131 in470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SWI311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW131116010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/60I0)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8091)
Chlordane, total
A
SIudge
TCLP Pesticides Analysis (SW 1311/9091)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW 13111908 1)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW 13111908 1)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW 1311/9081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Methoxychlor
A
Sludge
TCLP PesticidesAnalysis (SW 1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
IA-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophcnol
A
Sludge
TCLP Semi-Volatiles Analysis (SWI311/8270)
2,4,6-Trichl0r0ph0n0l
A
Sludge
TCLP Semi-Volatiles Analysis (SW131118270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW 131118270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW131118270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW13I1/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW13t1/8270)
Pyridine
A
NC WW SCM A Accredited NG WW SCM U Unavailable
Original #1
Page 9 of 33

SunrnritEnviromnenta! Technologies, Inc.
Accreditation
Program
3310 ruin St.
UM.M' 11
Anal tes Report
Y p
El�4aIRONNIENTAL TECHNOLOGIES,
WC Cuyahoga Farts, Ohio 44223
ArrafyOcal Laboratonle
TEL: [phone] FAX.- [phone]
WO#:
19030410
Website: hilp:1AW}V1y.setteJccom
20 Mar-19
Client: Synagro
State: NW
Project: Sanford WWTP
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19030410-001A Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original #1
Page 10 of 33

UMMISummit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win 5t.
Et V1A0NMf!WALTECHN0LG+ Gi_!,. - Cuyahoga Falls, Ohio 94223 WO#: 19030410
Arralyttcal Labaratarlos TEL: [phone] FAX..- [phone]
Website: httn:/hvww.settek.com 20-Mar-19
Client: Synagro
Project: Sanford WWTP SatchID: 36312
Sample ID MB-36312
SampType: MBLK
TestCode: tclp-voc-mstr Units: mglL
Prep Date: 311012019
RunNo: 95583
Client 1D: PBS
Batch ID: 36312
TestNo: SW8260 SW1311M
Analysis Date: 3/1112019
SegNo: 1993858
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highlimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloreethene
ND
0.0500
1,2-Dichloreethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorcbenzene
471
Surr: Dibromofluoromethane
525
Surr: Toluene-d8
501
500.0 94.1 70 130
500.0 105 70 130
500.0 100 70 130
Sample ID LCS-95583
SampType: LCS
TestCode: telp-voc-mstr Units: mg1L
Prep Date:
RunNo: 95583
Client ID: LCSS
Batch 1D: 36312
TestNo: SW8260 SW1311M
Analysis Date: 3111/2019
SegNo: 1993874
Analyte
Result
PQL SPK value SPK Ref Val
%RI=C LcwLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0209
0.00500
0.0200
0
104
70
131
1,2-Dichloroethane
0,0215
0.00500
0,0200
0
107
70
137
MFK
0.0952
0.0250
0.100
0
95.2
55.1
163
Benzene
0.0200
0.00500
0.0200
0
100
70
132
Qualifiers: B Analyte detected in the associated Method 31ank E Value above quantitation range H Holding times for preparation or anal}
I Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery Iimits RL Reporting Detection Limit
Page 11 of 33

' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMME3310 Win St.
FNVI tONMENTAL T iKii CLOGICS.INC Cuyahoga Falls, Ohio 44223 WO#: 19030410
Arfafytical Laborazonar TEL: [phone] FAX.- [phone]
Website: htm:11WlV-W.5ette%Com 20-Mar-19
Client: Synagro
Project: Sanford WWTP BatchlD: 36312
Sample ID LCS-95583
SampType: LCS
TestCode: tclp-voo-mstr Units: mglL
Prep Date:
RunNo: 95583
,lient ID: LCSS
Batch ID: 36312
TestNo: SW8260 SW1311M
Analysis Date: 3/11/2019
SegNo: 1993874
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDUmit Quaff
Carbon tetrachloride
0.0206
0.00500
0.0200
0
103
63.7
139
Chlorobenzene
0.0208
0.00500
0.0200
0
104
70
139
Chloroform
0.0196
0.00500
0.0200
0
98.1
70
130
Tetrachloroethene
0.0224
0.00500
0.0200
0
112
56.2
187
Trichloroethene
0.0200
0.00500
0.0200
0
99.8
64.1
138
Vinyl chloride
0.0151
0.00200
0.0200
0
75.4
22.1
147
Sum 4-Bromofluorobenzene
50.4
50.00
101
70
130
Surr: Dibromofluoromethane
56.5
50.00
113
70
130
Sum Toluene-d8
52.1
50.00
104
70
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
7 Analyte detected below quautitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 12 of 33

SUMMISummit Environmental Technologies, Inc. QC SUMMARY REPORT
Nt 3310 Win St. ll.. SUMMARY [� i i�Li
ENVIRONIAENTAL 7EC9iEe1L71 ,1-5, lur. Cuyahoga Falls, Ohio 44223
Anaiytical La6crrato(;gG TEL: [phone] R,4X.- [phone] WO#: 19030410
Website: http.lAvwli,.settek.com 20-Mar-19
Client: Synago
Project: Sanford WWTP BatchID: 36331a
Sample ID LCS-36331
SampType: LCS
TestCcde: TCLP-SVOC_ Units: mglL
Prep Date: 311112019
RunNo: 95613
Client ID: LCSS
Batch {D: 36331a
TestNo: SW8270
Analysis Date: 311212019
SegNo: 1996811
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.491
0,0400
0.8000
0
61.4
19.1
126
2,4,5-Trichlorophenol
0.633
0.100
0.8000
D
79.2
11.7
151
2,4,6-Trichlorophenol
0.719
0.10D
0.8000
0
89.9
12A
150
24-Dinitrotoluene
0.741
0.0200
0.8000
0
92.7
20.6
140
o-Cresol
0.623
0,100
0.8000
0
77.9
13.8
137
Cresols, Total
ND
2.00
1.6M
0
77.2
10
129
Hexachlorc-1,3-butadiene
0.376
0.60800
MOW
0
47.2
14.7
137
Hexachlorobenzene
0.672
0.0200
0.8000
0
84.0
12
139
Hexachloroethane
0.386
0.0400
0.8000
0
48.2
14.8
132
Nitrobenzene
0.676
0.0400
0.8000
0
84.6
15.6
138
Pentachlorophenol
0.721
0.100
0.8000
0
90.2
10
156
Pyridine
0.366
0.100
0.8000
0
45.7
1
130
Surr: 2-Fluorophenol
0.609
1.000
60.9
10
147
Surr: Phenol-d6
0.587
1.000
58.7
10
140
Surr: Nitrobenzene-d5
0.763
1.000
76.3
10
169
Surr: 2,4,6-Tribromophencl
0.795
1.000
79.5
10
185
Surr. 2-Fiuorobiphenyl
0.664
1.000
66.4
10
169
Surr: p-Terphenyl-d14
1.02
1.000
102
10
179
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H idol ding times for preparation or anal;
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 13 of 33

91
SUMM111-
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EKwli±C WAENrA1- :ECtte OW45tES. INC
Cuyahoga Falls, Ohio 44223
WO#: 19030410
Ansl ttdcal Labora?oews
TEL: [phone] EIX..- [phone]
Website: httpahv)viv.settek.com
20-Mar-19
Client:
Synagro
Project:
Sanford WWTP
BatehID: 36331a
Sample ID MB-36331
SampType: MBLK
TestCode: TCLP-SVOC_ Units: mglL
Prep Date: 3111/2019
RunNo: 95613
�;Ilent ID: PBS
Batch ID: 36331a
TestNo: SW8270
Analysis Date: 311212019
SegNo: 1998657
Analyte
Result
PQL SPK value SPK Ref Val
%RFC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0,0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichlorophenol
ND
0.100
2,4-Dinitrotoluene
ND
0.0200
c-Cresol
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0.100
Pyridine
ND
0.100
Surr: 2-Pluorophenol
0.496
Surr: Phenol-d6
0.503
Surr: Nitrobenzene-d5
0.621
Surr: 2,4,6-Tribromophenol
0.623
Surr: 2-Fluorobiphenyl
0.567
Surr: p-Terphenyl-d14
0.728
1.000
49.6
10
109
1.000
50.3
10
109
1.000
62.1
19
120
1.D00
62.3
10
120
1.000
56.7
22
117
1.000
72.8
34
116
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected belDNv quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 14 of 33

summill
Summit Environmental Technologies, Inc,
3310 Win St.
QC SUMMARY REPORT
ENVlrt0NMEWALTECHN0L410iES, INC
Cuyahoga Falls, Ohio 44223
WO#: 19030410
�lnslyricat La6aralarias
TELL-[phone] F,4X.- [phone]
Website. hQ.-Ilwrviv.settekcom
20-Mar-19
Client:
Synagro
Project:
Sanford WWTP
SatchlD: 36332
Sample ID MB-36332
SampType: MBLK
TestCode: TCLPSVOC- Units: mglL
Prep Date: 3111/2019
RunNo: 95664
client ID: PBS
Batch ID: 36332
TestNo: SW8081 SW3510C
Analysis Date: 311212019
SegNo: 1996798
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Hight.imit RPD Ref Val
%RPD RPDLimit Qua[
Chlordane, total
ND
0.0250
Toxaphene
ND
0.0500
Endrin
N❑
0.00250
gamma-BHC
ND
0.00250
Heptachlor
ND
0.00250
Heptachlor epoxide
ND
0.00250
Methoxychlor
ND
0.00250
Sum TCMX
12.1
Surr. DCB
15.4
d
d
20.00 60.3 10 119 m
20.00 77.1 10 119
#ample ID LCS-36332
SampType: LCS
TestCode:
TCLPSVOC- Units: mglL
Prep Date: 311112019
RunNo: 95664
lient ID: LCSS
Batch ID: 36332
TestNo:
SW8081 SW3510C
Analysis Date: 311212019
SegNo: 1996799
analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0130
0.00250
0.0250
0
52.0
20
157
gamma-BHC
0.0112
0.00250
0.0250
0
44.7
22
137
Heptachlor
0.0105
0.00250
0.0250
0
42.2
24
121
Heptachlor epoxide
0.0117
0.00250
0.0250
0
46.9
27
152
Methoxychlor
0.0131
0,00250
0.0250
0
52.4
10
199
Surr. TCMX
12.8
20.00
64.0
10
119
Surr: DCB
16.7
20.00
83.5
10
119
Qualifiers: B Analyte detected in the associated Method BIank E Value above quantitation range H Holding times for preparation or anal)
Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 33

M 1 Summit Environmental Technologies, Wrn St. Inc.
33I0 WQC SUMMARY REPORT
EL!t4'lrtOldME14TAL 4YEC8iNOLD;C.IES, 'M1-:` Cuyahoga Falls, Ohio 44223
WO#: I9030410
Ana, yticaf Laboradones TEL: [phone] FAX.- [phone]
Dyebslte: http://www..3ettek.com 20-Mar-19
Client: Synagro
Project: Sanford WWTP BatchlD: 36332
Sample ID 19030122-001AMS
SampType: MS
TestCode: TCLPSVOC- Units: mglL
Prep Date: 3/11/2019
RunNo: 95664
Client ID: BatchQC
Batch ID: 36332
TestNo: SW8081 SW3510C
Analysis Date: 3/1212019
SegNc: 1996800
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
ND
0.0250
0.0250
0
71.1
20
157
gamma-BHC
ND
0.0250
0.0250
0
60.3
22
137 m
Heptachlor
ND
0.0250
0.0250
0
59.6
24
121
Heptachlor epoxide
ND
0.0250
0.0250
0
67.8
27
152
Methoxychlor
ND
0.0250
0.0250
0
77.8
10
199
Surr: TCMX
18.9
20.00
94.4
10
119
Surr: DCB
21.7
20.00
109
10
119
Sample ID 19030122-001AMS❑
SampType: MSD
TestCode: TCLP-SVOC- Units: mglL
Prep Date: 3/11/2019
RunNo: 95664
Client ID: BatchQC
Batch ID: 36332
TestNo: SW8081 SW3510C
Analysis Date: 3/1212019
SegNo: 1996801
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
ND
0.0250
0.0250
0
56.7
20
157
0
0 30
gamma-BHC
ND
0.0250
0.0250
0
53.1
22
137
0
0 30
Heptachlor
ND
0.0250
0.0250
0
50.2
24
121
0
0 30
Heptachlor epoxide
ND
0.0250
0.0250
0
56.6
27
152
0
0 30
Methoxychlor
ND
0.0250
0.0250
0
59.1
10
199
0
0 30
Surr. TCMX
16.5
20.00
82.3
10
119
0
Surr: DCB
17.5
20.00
87.7
10
119
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
Analyte detected below quantitation limits M Manual Integration used to detennine area response MC Value is below Minimum Compound
Original
ND Not Detected 0 RSD is greater than RSDlitnit P Second column confirmation exceeds
PL Pen -nit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 16 of 33

SUMMITSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ERV1110146MEWALTECHUGLOG195 ` Cuyahoga Falls, Ohio 44223 WQ#: 1.903041.0
Anafyfis.21 Lab crDrorias TEL: [phone] FLY. [phone]
Website: http://vvww,,settek.com 20-Mar-19
Client: Synagro
Project: Samford WWTP BatchID: 36354
Sample ID 19030332-003AMS
SampType: MS
TestCode:
MTL-TCLP-7( Units: mglL
Prep Date: 311212019
RunNc: 95756
Client ID: BatchQC
Batch ID: 36354
TestNo:
SW6010D SW3010A
Analysis Date: 311512019
SegNe: 2000351
AnaIyte
Result
PQL
SPK value SPK Ref Val
%RFC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Selenium(Se) 2.54 0.0500 2.000 0.1364 120 70 130
Sample ID 19030332-003AMSD
SampType: MSD
TestCode:
MTL-TCLP-7( Units: mglL
Prep Date: 311212019
RunNo: 95756
Client ID: Batch=
Batch ID: 36354
TestNo:
SW6010D SW3010A
Analysis Date: 3115/2019
SegNo: 2000352
AnaIyte
Result
PQL
SPK value SPK Ref Val
%REG Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
tCLP Selenium(Se) 2.63 0.0500 2.000 0.1364 125 70 130 2.542 3.46 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
7 AnaIyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDIimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 17 of 33

' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMN3310 Win St.
ENVIRONkMAiTTAL TECHN[ILQG19$. INC Cuyahoga Falls, Ohio 44223 WO#: 19030410
ArraiytlCat Laboratari&!s TEL: [phone] FAX: [phone]
Website: httn://lvtivis.setteh.corn 20-Mar-19
Client: Synab o
Project: Sanford WWTP BatchID: 36354
Sample ID 19030332-003AMS
SampType: MS
TestCode: MTL-TCLP-7( Units: mg1L
Prep Date: 3/1212019
RunNo: 95674
Client ID: Batch QC
Batch ID: 36354
TestNo: SW6010D SW3010A
Analysis Date: W1312019
SegNo: 1997983
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.59
0.500
2.000
0
129
70
130
TCLP Barium(Ba)
ND
5.00
2.000
1.034
117
70
130
TCLP Cadmium(Cd)
2.24
0.100
2.000
0.007564
112
70
130
TCLP Chromium(Cr)
2.46
0.200
2.000
0.07596
119
70
130
TCLP Lead(Pb)
2.37
0.500
2.000
0.02152
117
70
130
TCLP Silver(Ag)
2.40
0.500
2,000
0.03658
118
70
130
Sample ID 19030332-003AMSD
SampType: MSD
TestCode: MTL-TCLP-7( Units: mglL
Prep Date: 311212019
RunNc: 95674
Client ID: BatchQC
Batch ID: 36354
TestNo: SW6010D SW3010A
Analysis Date: 311312019
SegNo: 1997984
Analyte
Result
PQL SPK value SPK Ref Vat
%RFC LcwLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
2.45
0.500
2.000
0
123
70
130
2.588
5.27
20
TCLP
Barium(Ba)
ND
5.00
2.000
1.034
106
70
130
0
0
20
TCLP
Cadmium(Cd)
2.12
0.10C
2.000
0.007564
105
70
130
2.240
5.69
20
TCLP
Chromium(Cr)
2.28
0.200
2.000
0.07596
110
70
130
2.457
7.34
20
TCLP
Lead(Pb)
2.22
0,500
2.000
0.02152
110
70
130
2.365
6.18
20
TCLP
Silver(Ag)
2.35
0.500
2.000
0.03658
115
70
130
2.402
2.34
20
Qualifiers: B Analyle detected in the associated Method Blank E Value above quantitation range H Holding tithes for preparation or anal;
I Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater Chan RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 18 of 33

SUA3310
M'
Summit Environmenial Technologies, Inc.
Win St.
QC SUMMARY REPORT
ERVIRONMENTAL TECIiN0L:0GI5S, sivr.
Cuyahoga Falls, Ohio 44223
WO#: 14030410
Anat0caf Labaralonas TEL: [phone] FLY.- [phone]
y
Website; hualhvivw.settek.cam
20-Mar-19
Client:
Synagro
Project:
Sanford WWTP
BatehED: 36365
Sample ID MB-36365
SampType: MBLK
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 311312019
RunNo: 95660
Client ID: PBS
Batch ID: 36365
TestNo:
SW7470A SW7470A
Analysis Date: 311312019
SegNo: 1997113
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-36365
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/13/2019
RunNo: 95680
Ghent ID: LCSS
Batch ID: 36365
TestNo: SW7470A SW7470A
Analysis Date: 3/1312019
SegNo: 1997114
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00414 0.00200 0.00400 0 104 80 120
Sample I❑ M82-36365
SampType: MBLK
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 3/1312019
RunNo: 95680
Client ID: PBS
Batch ID: 36365
TestNo:
SW7470A SW7470A
Analysis Date: 311312019
SegNo: 1997115
Analyte
Result
PQL
SPK value SPK Ref Val
%RFC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample 1D 19030332-003AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 311312019
RunNo: 95680
Client ID: BatchQC
Batch ID: 36365
TestNo: SW7470A SW7470A
Analysis Date: 311312019
SegNo: 1997291
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0,00435 0.00200 0.00400 0.0000500 108 75 125
Qualificrs: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integation used to detennine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Pen -nit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 33

UM'� SummitEnvironntental Technologies, Inc. 3310 Win S[. QC SUMMARY REPORT
EhVIROt4ME74TAL'IrECIINOWCiFS, TN.— Cuyahoga Falls, Ohio 44223 WO#: 19030410
Axvir rld W Lab0r&11;l0eG TEL: [phone] FAX.- [phone]
Website: ha:11wivw.se11ek.corr: 20-Mar-19
Client: Synagro
Project: Sanford WWTP BatchID: 36365
Sample ID 19030332-003AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/13/2019
RunNo: 95680
Client ID: BatchQC
Batch ID: 36365
TestNo: SW7470A SW7470A
Analysis Date: 311312019
SegNo: 1997291
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 19030332-003AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/13/2019
RunNo: 95680
Client ID: SatchQC
Batch ID: 36365
TestNo: SW7470A SW7470A
Analysis Date: 3/1312019
SegNo: 1997292
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00427 0,00200 0.00400 0.0000500 106 75 126 0.00435 20
Qualifiers: B Analyte detected in the associated Method BIank E Value above quantitation range H Holding times for preparation or anal)
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater thanRSDlimit P ,Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 20 of 33

summilt
Summit Environmental Technologies, Inc. 3310 Win St.
��QC SUMMARY REPORT
ENVIRONMtWAL A; CHNOU)C ES, INC
Cuyahoga Falls, Ohio 44223
WO#: 19030410
-
Ana: y[Icaf Laboraaaroe+s
TEL: [phone] FAX: [phone]
Website: htt :111vww.settek.corn
.20 Mar-19
Client:
Synagro
Project:
Sanford WWTP
BatchlD: 36408
2,4-D ND 1.00 d
2,4,5-TP ND 0.500 d
Surr: 2,4-Dichl orophenyl acetic acid 379 500.0 75.9 20 140
2,4-D
ND
1.00 0.500
0 70.0
37
105
2,4,5-TP
ND
0.500 0.500
0 63.5
38
106
Surr: 2,4-Dichlorophenylacetic acid
402
500.0
80.3
20
140
2,4-D ND 1.00
0.500 0 69.2 37
105
2,4,5-TP ND 0.500
0.500 0 63.2 38
106
Surr. 2,4-Dichlorophenylacetic acid 417
500.0 83.5 20
140
Qualifiers: B Analytic detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anah
7 Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
O RSD is greater than RSDlimit
P
Second column continuation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 21 of 33

IT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
ENVIF?C1tJMEWALTECi NOL4GiES, INC Cuyahoga Falls,Ohio 44223 WO#: I903U410
Art�fyrdcai L r fJ.ralO�Jer TEL: [phone] FAY- [phone]
Website: httn://www.settek.com 20112ar-19
Client: Synagro
Project: Sanford WWTP BatchID: 36408
Sample ID 19030418-001amsd
SampType: MSD
TestCode: telp-SVOC-H Units: m91L
Prep Date: 3/14/2019
RunNo: 95900
Client ID: Batch=
Batch ID: 36408
TestNo: SW8151A SW8151A
Analysis Date: 3/19/2019
SegNo: 2006995
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 76.1 37 105 0 0 30
2,4,5-TP ND 0.500 0.500 0 71.2 38 106 0 0 30
Surr: 2,4-Dichlorophenylacetic acid 472 500.0 94.5 20 140 0 30
Qualifiers: B Analyta detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 22 of 33

summill
Summit Environmental Technologies. Inc.
3310 Win St,
QC SUMMARY REPORT
EP4VIrC4ONrilEIJTAL TEC4NOt_fS ,--. , '- _
Cuyahoga Falls, Ohio 44223
WO#: 19030410
ArWlyf'ca1 Laboratarlos
TEL: [phone]?I1 FAX:[phone]
Website: htto://wiyry.seftek.com
20-Mar-19
Client:
Synagro
Project:
Sanford WWTP
BatchID: R95504
Ignitability 7.84 7.240 0 108 70 130
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Sample ID 19030364-001ADUP
SampType: ❑UP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: BatchQC
Batch ID: R95604
TestNo: SWI030
Analysis Date: 3/1212019
SegNo: 1994388
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
ignitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding tunes for preparation or anal]
I fanalyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 23 of 33

Summit Environmental Technologies, Inc. QC SUMMARY
TAT RETORT
S U mm 1 3310 Win St. 7 U 1'�t(i REPORT
1
Eflti�ll?UtdtltIT4LTC3�NpIG1S, 3Nsr. Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
WO#: 19030410
Wehsite: http:/hvinv.settek.conz 20-Mar-19
Client: Synagro
Project: Sanford WWTP BatchID: R95604
Sample ID 19030364-O01ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: BatchQC
Batch ID: R95604
TestNo:
SW1030
Analysis Date: 311212019
SegNo: 1994388
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample lD 19030410-OOIADUP
SampType: DUP
TestCode: Ignitabil4_S Units:
Prep Date:
RunNo: 95604
Client ID: Sanford WWTP
Batch ID: R95604
TestNo: SW1030
Analysis Date: 3/1212019
SegNo: 1994390
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19030418-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 95604
Client ID: BatchQC
Batch ID: R95604
TestNo: SW1030
Analysis Date: 3/12/2019
SegNo: 1994392
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19030420-001ADUP
SampType: DUP
TestCode:
Ignitability S Units:
Prep Date:
RunNo: 95604
Client ID: BatchQC
Hatch ID: R95604
TestNo:
SW1030
Analysis Date: W1212019
SegNo: 1994394
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RS.Dlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 24 of 33

S UM 1 A
Sumrnif Environmental Technologies, Inc.
3310 Win St.
IIOR�'
(�!� SUMMARY REPORT
QC S7 11 R 1 RE
0WIr?ONMENTAL TECHNI)LCPGIFS, INC
Cuyahoga Falls, Ohio 44223
W09: 19030410
An_f±'r[lcal Laboraronefi
TFsL; [phone] FAX-.- [phone]
Website: hM.-11w14,w.se1fekcom
20-Mar-19
Client:
Synagro
Project:
Sanford WWTP
BatclxIIi: R95606
pH 7.0 7.0 0 100 90 110
pH 6.1 0 0 6.1 0 10
pH 7.0 7.0 0 100 90 110
Sample ID CHECK 7
SampType: LCS
TestCode: PH_0IL(9045 Units: s.u.@20.2C
Prep Date:
RunNo: 95606
Client ID: LCSW
Batch ID: R95606
TestNo: SW9045D
Analysis Date: 3/12/2019
SegNo: 1994794
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Highi-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0
7.0 0 100 90
110
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
7 Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND Not Detected
0 RSD is greater than RSDlimit
P
Second column confirmation exceeds Original
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 25 of 33

S u
'lu i
3310 Win SSutnmitEnvironmental Technologies, WInc.
St_ t QC SUMMARY REPORT
ENVI€?ONf EwTAL T€fr?! WQWtk ;;Fg, INC Cuyahoga Falls, Ohio 44223 WO#: 19030410
Anaf tf,lc. ; Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settekcoin 20-Mar-I9
Client: Synagro
Project- Sanford WWTP BatchlD: R95606
Sample ID CHECK 7
SampType: LCS
TestCode: PH_OIL(9045 Units: s.u.@20.2C
Prep Date:
RunNo: 95606
Client ID; LCSW
Batch ID: R95606
TestNo: SW9045D
Analysis Date: 3112/2019
SegNo: 1994794
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID CHECK 7
SampType: LCS
TestCode:
PH_O1L(9045 Units: s.u.@20.1C
Prep Date:
RunNo: 95606
Client ID: LCSW
Batch ID; R95606
TestNo:
SW9045D
Analysis Date: 3/1212019
SegNo: 1994327
Analyte
Result
PQL
SPK value SPK Ref Val %REC
Lcwl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
PH TO 7.0 0 100 90 110
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlitnh P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 26 of 33

UMMISummitnvironmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
t lBblt��t�AlENT4LTCHM{7t37G�S, trtt. Cuyahoga Falls, Ohio 44223
A s«i'iY > l�baret�r£e€ TEL: [phone] FIX.- [phone] WO#: 1903041Q
Website: http://`wisw.settek.co7n 20-Mar-19
Client: Synagro
.Project: Sanford WWTP Batchl[D: R95606
iample ID .19030466-001ADUP
5ampType: DUP
TestCode:
pH_NPW(450 Units: s.u.@20.1C
Prep Date:
RunNo: 95606
'Iient ID: BatchQC
Batch ID: R95606
TestNo:
SW9045D
Analysis Date: 311212019
SegNo- 1994789
knalyte
Result
PQL
SPK value SPK Ref Val %REC
Lowl-imit HighUrnit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0 0.6 5
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Pennit Limit R RPD outside accepted recovery litnits RL Reporting Detection Limit
Page 27 of 33

Summit Environmental Technologies. Inc. QC SUMMARY
TM� t� T Y n T TOR m
SUMMIT- 3310 Win St. \[ 1. J lJ 1V1 f l t( 1\1� r i� 1
El'WH;t3NMEWTAL TPC", )tIG� -S Cuyahoga Falls, Ohio 44223 WO#: 19030410
A1"r yNcal Laboraiarleg TEL: [phone] FXX.- [phone]
Website: http:lAvww.settek.com 20-Mar-19
Client: Synagro
Project: Sanford WWTP BatehID: R95670
Sample ID Blank
SampType: MBLK
TestCade: Cyanide,Rea Units: mglL
Prep Date:
RunNc: 95670
Client ID: PBW
Batch ID: R95670
TestNo: SW9014
Analysis Date: 3/8/2019
SegNo: 1996900
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.495
Sample ID LCS
SampType: LCS
TestCade: Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 95670
Client ID: LCSW
Batch ID: R95670
TestNo: SW9014
Analysis Date: 31812019
SegNo: 1996901
Analyte
Result
PQL. SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.79 0.490 10.00 0 97.9 85 115
Sample ID RLCheck
SampType: RLC
TestCade: Cyanide,Rea Units: mglL
Prep Date:
RunNo: 95670
Client ID: BatchQC
Batch ID: R95670
TestNo: SW9014
Analysis Date: 3/8/2019
SegNo: 1996903
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 0.586 0.495 0.5000 0 117 50 150
Sample ID 19030367-001AMS
SampType: MS
TestCade: Cyanide,Rea Units: mglL
Prep Date:
RunNo: 95670
Client ID: BatchQC
Batch ID: R95670
TestNo: SW9014
Analysis Date: 3/812019
SegNo: 1996905
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-Imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.49 0.490 10.00 0.1046 93.9 81.3 118
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anaI�
7 Analyte detected below quantitation limits M ManuaI Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 28 of 33

U I 33I0WWin Sumn¢itEnvironmental TechnologiInc. QC SUMMARY REPORT
inStSt.
EFti llrtOtJIdeNTAL TECHNOt_ .ls;, Cuyahoga Falls, Ohio 44223
A afyfFcaf Labaradorjos TEL: [phone] FAXY [phone] Wb#: ]903U410
Website: http:lAvww.settek.com 20-Afar-19
Client: Synagro
Project: Sanford WWTP Batch[D: R95670
Sample ID 19030367-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mglL
Prep Date:
RunNo: 95670
Client ID: BatchQC
Batch ID: R95670
TestNo: SW9014
Analysis Date: 3/8/2019
SegNo: 1996905
Analyte
Result
PQL SPK value SPK Ref Val
%REC L.owl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample lD 19030367-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 95670
Client ID: BatchQC
Batch ID: R95670
Testhlo: SW9014
Analysis Date: 3/8/2019
SegNo: 1996906
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.07 0.476 10.00 0.1046 89.7 81.3 118 9.495 4.57 5
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitatioit range H Holding times for preparation or anal)
7 Anaiyte detected below quantitation limits M Manual integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 29 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM111 3310 Win St.
EhIVli±Q14Pdif dTAL-CCM dG70+ I!;S, IFd'C: Cuyahoga Falls, Ohio 44223
WO#: 19030410
A-'TaPyC1iG'2i Lri:.;rarcr°dA� TEL: (330J 253-8211 FAX: [phone]
Website: htt ://wwiv.setlek.cam 20 Mar-19
Client: Synagro
Project: Sanford WWTP BatchlD: R95672
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4620 25.0 4800 0 96.2 85 115
Sulfide, Reactive 4310 25.0 4800 0 89.8 75 125
Sample I❑ 19030367-001AMSD
SampType: MSD
TestCode:
Sulfide,React Units: mglL
Prep Date:
RunNe: 95672
Client ID: BatchQC
Batch ID: R95672
TestNo:
SW9034
Analysis Date: 3/8/2019
SegNo: 1996983
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Quai
Suifide, Reactive
4380 25.0
4800 0 91.2 75
125
4310 1.61 30
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal)
1
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
O RSD is greater than RSDlimit
P
Second column continnation exceeds Original
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 30 of 33

summilu
3310 WSummitEnvironmentIIl Technologies,Inc.
St.
QC 5 V MM� 1 ltl'li ORT
�c
6N'Jlit0NPM4TALTECHNOL.00F5,9KC
Cuyahoga Falls, Ohio44223
Amalfi al Laboratoriag
TEL: [phone] FAX.- [phone]
w0#: 19030410
Website: httn:/hvwtv.settek.com
20-Mar-19
Client:
Synagro
Project:
Sanford WWTP
BatchID: R95672
Sample ID 19030367-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg1L
Prep Date:
RunNo: 95672
3lient ID: BatchQC
Batch ID: R95672
TestNo: SW9034
Analysis Date: 3/8/2019
SegNo: 1996983
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowL snit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anall
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 31 of 33

DC4QACOC338 nev.47
Efrendve Daft:121OW15
SUMMIT Analysis Request / Chain of Custody
ENV' ROMMENTAL TKCHROLOGIES. IrM For Summit Environmental Technologies, Inc. use only
Page 32 of 33

SUMMIT summit Environmental Technologies, lnc.
3310 ff m S1.
ENVMONMENTAL Tr -CH d01 gG1FR, 1I4r ct.ipahogaFalls, Ohio 44223 Sample Log -in Check List
Ani-MyNcarl LnhoralorfeF TEL: [phone] FIX- [phone]
Website: ham:/hni,iv.settak.Com
Client Name: SYN-NC-27028 Work Order Number: 19030410 RoptNo: 1
Logged by: Christopher Livengood 318/2019 10:05:00 AM
Completed By: Christopher Livengood 31812019 11:01;20 AM
Reviewed By: Jennifer Woolf 3/12/2019 11:29:27 AM
Chain of Custody
1. Is Chain of Custody complete? Yes W No ❑ Not Present ❑
2. How was the sample delivered? UPS
LOg In
3.
Coolers are present?
Yes
No ❑
NA ❑
4.
Shipping container/cooler in good condition?
Yes
0
No ❑
Custody seals intact on shipping containerlcnier?
Yes
❑
No ❑
Not Present V
No. Seal Date:
Signed By:
5.
Was an attempt made to cool the samples?
Yes
No ❑
NA ❑
6,
Were all samples received at a temperature of >0' C to 6,0'C
Yes
N❑
No ❑
NA ❑
7.
Sample(s) in proper container(s)?
Yes
0
No ❑
$_
Sufficient sample volume for indicated test(s)?
Yes
❑
No ❑
g-
Are samples (except VOA and ONG) properly preserved?
Yes
✓❑
No �...�
10.
Was preservative added to bottles?
Yes
❑
No R1
NA ❑
1 1 . Is the headspace in the VOA vials less than 114 inch or 6 mm? Yes ❑ No ❑ No VOA Vials n
12, Were any sample containers received broken? Yes ❑ No d❑
13. Does paperwork match bottle labels? Yes EVI No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes IV] No ❑
15. Is it clear what analyses were requested? Yes EVI No ❑
16. Were all holding times able to be met? Yes ❑ No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17, Was client notified of all discrepancies with this order? Yes No ❑ NA❑
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
ECoolEerN��3.9
°C C�GoodNct
�IntactSeal No Seal ❑ate Signed By
Page 33 of 33

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: W00000543
WWTP Name: Bia Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 01/01/19 To 03/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (AIk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If anniienhle to alternative nerfnrmed fCla.ss A or Class Rl emmnlete the fnllnwinu mnnitorinn data --
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 611,
CFU
<12300
<42700
<45500
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tionwt, 1
Option/Alt, 2
Option/Alt, 3
Option/Alt, 4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503,32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title (t Ype or print)
a� 1i
Signature of Preparer* at
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
NC DENR #664
NC PHHS #37799
US EPA#NC01918
190245
Yes
J. zubeckIs 02/07/19
190245
-1
3mdge Gr Fec. Cofiform-S <31200
CFU/g 31200 02/08/19 ERP 9222D - MF
-2
<21600
CFU/g 21600
-2
<21900
CFulg 21900
-4
<13300
cFurg 1$3000
-5
<23600
CFUrg 23500
-6
<45500
CFUlg 45500
-7
<12300
CFO/g 123000
Geomean <42700
190245
-1
3ludge Gr TS (q/a) 3.21 %
0.01 02/08/19 ERP 2540 G -TS
-2
4.64%
0.01
-2
4.56%
0.01
-4
0.750%
0.01
-5
4.24%
0.01
-6
2.15%
0.01
-7
0.810%
0.01
Report
'
Review
Lab Director
219 S. Steele Str.
Sanford NC 27330 919-208-4240
[e-mail]

219 S. Steele Str. Cameron Testis Services, Inc. Chain.,of Custo�r
Sanford, NC 27330 g
Phone: [phone] NC WW/GW CerL #e54 NC PHHS Cert# 37799 US EPA NC01918 Page T of
Company: Email:
CTS lab use
Contact:
Phone
Sample TernLab ID f
Address (City,
Fax:
Ice (YIN)
State, Zip)
Notes:
Permit (YIN) I
—
Project:
Rush (YIN) -- Due:
Collected: Name: +
)
t�t ID
Signature:
Sample Inf rmation
Number of bottles
Requested Analysis
Sample 1D
Q o
x ?
}
o '°
m a
¢
Preservatives: (U)npreserved, H(C)I,
H2(S)O4, H(N)O3, (Na)Thiosulfate, Na(O}H,
CTS Lab
ID
O
~ U
N O itl
m m
J
>j
Q
Other (X), Indicate
ri
S
i
1.7
I
Relinquished.,
Received:
Daterrime
i
Rush work will require prior approval. Additional charges will apply

City of Sanford
Big Buffalo WWTP
Sludge Calculations
IN
VSR = 65.64686
W1
DISH
112.1637
W2
WET
212.2177
W3
DRY
112,7763
W4
ASH
112,3395
0.612269
PERCENT VOLITILE SOLIDS
0.713026
OUT
W1
DISH
112.7573
W2
WET
213.0170
W3
DRY
121.4449
W4
ASH
117.4443
PERCENT SOLIDS
8,665097
PERCENT VOLITILE SOLIDS
0.460495
PERCENT VOLITILE SOLIDS REDUCTION 65.64686
IS it above 38%

VSR
Grab Date: 1- 9 - 1 9
Lab Tech's Initials:
Sample I
RAS (IN)
Volume 100 MIS.
Dish #1 D
Crucible Weight f 1-1. 1 6 3 7
gm
Crucible & Liquid 2 Z. 1 7 7
gm
Dried I I �c� 3
gm
Burned ! z -33 ��
9m
DIGESTER
(OUT)
100 MIS.
K
9 -14 L
-N-
1f2.73 7
Zt�, of7b
M
gm
gm
gm
am
Date/Time In: I - 9 -19 / i t.4a n•.
Drying Oven
Date/Time Out: 1, f a - + `1 / Temp: 1 O'f °C
Time In: I - !a• cq 11;3%4--
Muffle Furnace
Time Out: 1- 1 a - 0 II'. S? Temp: sT- °C
Were the samples well mixed before analyzing? Yes No
Was the temp of the drying oven in the proper operating range? Yes —' o
If not what were the corrective actions?
Was the temp of the Muffle Furnace in the proper operating range? Yes ---- No
if not what were the corrective actions?
Samplers _rr73, -'�45'

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Bia Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 04/01/19 To 06/30/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt, 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicable to alternative nerformed !Class A or Class III comnlete the fallowinu monitarinu data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61h
CFU
<358000
<492000
<855000
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt, 4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Mt. 6
0ption/Alt. 7
Option/AIt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(incorporation)
No vector attraction reduction
alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T,1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.I 106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T,1107 have not been met," (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title (t� e or print)
a 11 jo
Signature of Preparer* 7 at
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T.1102 (26)

190761
BB!
Sludge Or Fec, Coliform-S <699000
CFUIg
59900
04/22/19 SB 9222D - MF
BB2
<358000
cFU1g
amo0
BB3
<855000
CFUIg
855000
B64
<641000
OFuto
541000
BB5
<444000
CFUIg
444000
BB6
<361000
CFUIg
361000
BB7
<441000
CFUIg
441000
Geomean <492000
190761
BB I
�Iudge Or TS (0/0) 0,167%
%
0.01
04/22/19 2540 G -TS
BB2
0.279%
%
0.01
BB3
0,117%
%
0.01
BB4
0.186%
%
0.01
BB5
0.225%
%
om
BB6
0,277%
%
ni
B87
0.227%
%
aat
Report
Review
Lab €?irectar
-
�Date
219 S. Steele Str. 919-208 4240
Sanford NC 27330 ahriQuarnerantesting.aorn

Rush work will require prior approval. Additional charges will apply

VSR
Grab Date:
K— k . f)
Lab Tech's Initials:
DIGESTED
Sample (IN)
L��S—
OUT
Volume 100 MIS.
100 MIS.
Dish #1 P
0
Crucible Weight t} 1. 3 9 8 S
Crucible & Liquid .z E I 910
Dried It),` IFY
Burned i11, S WO 7
Date/Time ln: +4-4-0 / ! 0- r
DateMme Out: 4 - s .1`i / (o : r - Drying Oven
Time In t 1'. rs Muffle Furnace
Time Out: l Z : 10
gm
gm
9m
grn
Were the samples well mixed before analyzing? Yes Z No
Was the temp of the drying oven in the proper operating range? Yes ►% No
If not what were the corrective actions?.
Temp; 10 4j °C
Temp: Y )'U'C
Was the temp of the Muffle Furnace in the proper operating range? Yes �No
If not what were the corrective actions?
Samplers S -4-r S
41

T►
W1
DISH
W2
WET
W3
DRY
W4
ASH
liI
W1
DISH
W2
WET
W3
DRY
W4
ASH
City of Sanford
Big Buffalo WWTP
Sludge Calculations
111,3985
211,3930
111.9188
111.5407
PERCENT VOLITILE SOLIDS
112.1613
212.1619
117.6435
115.2625
PERCENT SOLIDS
PERCENT VOLITILE SOLIDS
0,520329
0.726696
5.482715
0.4334315
PERCENT VOLITILE SOLIDS REDUCTION 71.12496
Is it above 38%
R
VSR 71.12496

ANNUAL, PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: W00000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 07/01/18 To 09/30/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
CIass A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce. Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If gnnlir�hln to a1farna4ivn narfnrmar1 Wince A or C incc IM rmmnlafe the fnllnwina mnnitnrina rintnr
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x 10 to the 61h
CFU
<32300
<32500
<32700
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.110) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
OptionlAlt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
fiection)
(locorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met,"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (PIease note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met, I am aware that there are significant penalties for false certification including fine and imprisonment."
_Scott Siletzky, WWTP Superintendent
Preparer Name jandTitle ( pe or print)
1,7 bb
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land AppIier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc, Laboratory Report
191388
Report
Review
219 S. Steele Sir,
Sanford NC 27330
NC DENR #654
NC PHHS #37799
US EPA #NC01918
191388
Yes
M. Sims 07/24/19
1 31udgE' Or Fec. Cofiform-S <32500
cFur9
32500 07/24/19 RL 9222D - MF
2 <32400
cFU/9
32400
3 <32600
CFU1g
32600
4 <32300
cFU19
32300
5 <32600
CFUrg
32600
6 <32700
Uft
32700
7 <32500
uurg
3250o
Geomean <32500
1 3ludge or TS (%) 3.07%
0.01 07/24/19 RL 2540 G -TS
2 3.09%
0.01
3 3.07%
0.01
4 3.10%
0.01
5 3,06%
0.01
6 3.06%
0.01
7 3.07%
0,01
--- Lab Diraotor --..__�_ _.__...._.... - ..�..
slate
919-208-4240
chrisC3a camerontesting, coin

Rush work will require prior approval. Additional charges will apply

City of Sanford
Big Buffalo WWTP
Sludge Calculations
IR
VSR w 75.38066
W1
DISH
111.4004
W2
WET
211,2381
W3
DRY
111,9092
W4
ASH
111.5717
0.509627
PERCENT VOLITILE SOLIDS 0.663325
+1lf,
W1
DISH
112.1637
W2
WET
21Z1379
W3
DRY
121.0136
W4
ASH
118,1230
PERCENT SOLIDS 8.852184
PERCENT VOLITILE SOLIDS 0.326625
PERCENT VOLITILE SOLIDS REDUCTION 75.38066
is it above 38%

Grab Date- 7 - 1 y - 19
Lab Tech'sInitials:
DIGESTER
RAS (IN)
Sample—
F OUT
Volume 100 MIS.
100 MIS.
Dish #L R
p
Crucible Weighl
Crucible & Liquid
Dried
Bumed
Ltany
211 .23,'i
111. 101E
lit.T717
9m
gm
gm
9M
112. 1637
212. l3 71
l21. DI��
1rYr.l23a
Date/Time in: '?r1 �-19 l g :r
Drying Oven
DatelTirne Out: 7 -11-19
-iq�19 Timelrl. LI_=_A_y_
-�—Muffle Pomace
aM
3m
jm
aM
Were the samples well mixed before analyzing? Yes ✓✓No
Was the temp of the drying oven in the proper operating range? Yes. / No
If not what were the corrective actions?
Temp: 10 4 OC
Ternp:.jJ0 OC
Was the temp of the Muffie Furnace in the proper operating range? Yes '�No
If not what were the corrective actions?
Samplers 70 7 C

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number; W00000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 10/01/19 To 12/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (timehemp) Alt, 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class 13 only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 61
CFU
<14800
<15500
<16700
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. I
Option/Alt, 2
(V S reduction) X
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3 Option/Mt. 4
(30-day bench) (Spec. 02 uptake)
Option/Alt 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CPR 503.32/15A NCAC 02T,1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certificat'a including fine and imprisonment."
Scott Siletzky, WWTP SuperintendentjiVlp4Q o�
Prepe Ti e (type or print) MnAp er Name and Title (if applicable) (type or print) !! r�
k JV
Signature of Preparer at Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS #37799
w US EPA #NC01918
Synagro o N 192049
Sanford WWTP Yes
Sample Information
M. Boyd 10/22/19 v J. Cameron 10/22/19
,a r
Analyses and Results
192049
-1
31udgE Or
Fec. Coliform-S <14800
CFU/Q
14800 10/23/19 RL 9222D . MF
-2
<15900
crutu
15900
-3
< 15400
CFU19
15400
-4
<15300
mig
15300
-5
<16700
CFUrg
16700
-6
<16400
CFU19
15400
-7
<15j400
CFUl9
15400
Geomean <15500
192049
01 -1
nudge Or
TS (%) 6.74%
OV 10/23/19 RL 2540 G -TS
-2
6.30%
0.01
-3
6.48%
0.01
-4
6.53%
0.01
-5
5.97%
0.01
-6
6.48%
0.01
-7
6.49%
a.o�
Report
Review
X,
Lab Director
Date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 chrisoo un terontesting.com

219 S. Steele Str.
Sanford, NC 27330
Prone: 919-208-424D
Cameron Testing Services, Inc.
NC WWIGW Cert. #654 NC PHHS Cert # 37799 US EPA NG01918
Chain of Custody
Page of
Company:
5ynagro
EmaU:
[e-mail]
CTS lab use only
Contact
'Melinda Boyd
{Ph°ne'
336-909-8627
Sample Temp
ici
� Lab iD ,
Address (City,
`284 Boger Rd.
Fa)c
Ice (YIN)
1
state, zip)
Mocltsville, NC 2702$
N°
Permit (YIN)
,
Project
S Gn✓�W� 1
Rush (YIN)
Due: i
Collected:
Name: Melinda Boyd
Signature:
Sample Information
Number of bottles
Requested Analysis
x
?
� ro
Preservatives: (U)npreserved, H(C)I,
CTS Lab
Sample ID
�'
N
¢O
H2(S)t74, H(N)43, (Na)Thiosulfate, Na(0)H,
ID
C, m >
Other (X), Indicate
rCCJ Cal. ���
lal�a .3� Cyr 5�- ►�
4n
Relinquished:
Received:
DatelTime
Hush work will require prior approval. Additional charges will apply

Vs R
Grab Date: t 0 -17 - ) I
Lab Tech's Initials:
Sample RAS (IN)
Volume 100 MIS.
Dish #1 A.
Crucible Weight 111 r 3 9 9 3
Igm
Crucible & Liquid Z i 1 9 Zd Igm
Dried j l I . $ j �� gm
Burned Fill
gm
DIGESTER
(OUT)
100 MIS.
Z12,tS7J
DatelTime In:1Q-i-7 -0 I f D :03 Drying Oven
DatelTlme 0Ut:10-) g.19 / }o; Ig,
Time in: I 1 : S 1 —Muffle Furnace
Time Out: l 2. _ L{ a
Were the samples well mixed before analyzing? Yes V No
Was the temp of the drying oven in the proper operating range? Yes' Na
If not what were the corrective actions?
Temp: 1 D `l 'C
Temp: 5-YP °C
Was the ternp of the Muffle Furnace in the proper operating range? Yes✓✓ No
If not what were the corrective actions?
Samplers SS

W1
DISH
111.3993
W2
WET
211.5420
W3
DRY
111.8150
W4
ASH
111.5468
City of Sanford
Big Buffalo WWTP
Sludge Calculations
VSR = 49.20719
0.415108
PERCENT VOLITILE SOLIDS 0.645177
W1
DISH
112.1644
W2
WET
212.1276
W3
DRY
119.6944
W4
ASH
116.0790
PERCENT SOLIDS T53278
PERCENT VOLITILE SOLIDS 0.480133
PERCENT VOLITILE, SOLIDS REDUCTION 49.20719
Is it above 38% V C S

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project: Sanford
Field
(skate -county -site -field)
Soil
pH
Lime Requirement
(from soil anal sis)
Tons/Acre
Applied
Date Applied
NC-CH-49-6
5.8
0.6
0.0
N C-C H-49-7
5.7
0.8
0.0
NC-CH-49-8
6.2
0.0
n/a
NC-CH-66-6
5.9
0.5
0.0
NC-CH-66-8
6.2
0.0
n/a
NC-CH-66-11
6.1
0.0
n/a
NC-CH-77-1
6.2
0.0
n/a
NC-CH-77-5
6.4
0.0
n/a
NC-CH-77-7
5.7
0.7
0.7
N C-C H-77-8
5.4
2.3
2.3
NC-CH-77-12
6.2
0.0
n/a
NC-CH-77-16
5.8
0.5
0.0
*Lime to be spread in first quarter 2020

SECTION 7

Page 1 of 1
Report No: 20-045-0766
Account No: 46463
Advisor: Synagro Central LLCI Kinston
Marshall Puryrear
284 Boger Road
Suite 204
Mocksville NC 27028
Waypoeint(!D
ANALYTICAL
Client: Henry Stinson
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-W6
www.waypointanalytical.com
Farm: CH-66
Date Received: 0211412020
Date of Report: 02/17/2020
Lab No Field ID
Sample ID
Soil Class HM% W IV pH
Ac
P-1
K-1
S-1
Mn-1
Zn-1
Zn-Al
Cu-1
CE'C
BS%
Ca%
Mg%
ESP Na SS-1 NO -N
24368
66-6
M-0 4.5
5.9
2.2
323
41
46
406
1280
1600
875
12.6
83
62
19
0.6 0.1
Crop Recommendations:
Rec Uom
Lime (Uacre)
N
P2 05
KZ 0
S
Mn
Mn-Al
Zn
Cu
B
Mg
Last Crop
1- Pasture
Iblacre
0.5
50
0
106
6
0
262
0
0
0
0
2-Adjust pH to 6.0
Iblacre
0.0
0
262
0
24369
66-8
MIN 2.4
6.2
1,1
160
20
29
238
720
720
550
9.1
88
69
17
1.1 0A
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
P205 K2
S
Mn
Mn-A!
Zo
Cu
B
Mg
Last Crop
1- Pasture
lb/acre
0.0
50
0
120
15
0
157
0
0
0
0
2-Adjust pH to 6.0
lb/acre
0.0
0
157
0
24370
66-11
MIN 2.6
6A
1.6
235
27
44
225
1040
1040
755
11.5
86
66
18
0.6 0.1
Crop Recommendations.
Rec Uom
Lime (Uacre)
N
P2 05
K2
S
Mn
Mn-AI
Zn
Cu
B
Mg
Last Crop
1- Pasture
Iblacre
0.0
50
0
120
7
0
150
0
0
0
0
2-Adjust pH to 6.0
Iblacre
0.0
0
150
0
Comment:
Test result units = CEC and Na in meg/100cm3; NO3 N in mg1dm3; W!V in glcm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of i
Report No: 20-045-0767
Account No: 46463
Advisor: Synagro Central LLCI Kinston
Marshall Puryear
284 Boger Road
Suite 204
Mocksville NC 27028
o
Waypointu
ANALYTICAL
Client: Henry Stinson
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalyt[cal.com
Farm: CH-49
Date Received: 02M 412020
Date of Report: 02/17/2020
Lab No Field 1D
Sample ID
Soil Class HM% W/V pH
Ac
P-1
K 1
S-1
Mn-1
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO- N
24371 6-7-8
49-6
MIN 2.8
5.8
2.5
409
124
40
125
863
863
580
13.0
B1
56
20
0.3 0
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
P2 05
K2 O
S
Mn
Mn-AI
Zn
Cu
B
Mg
Last Crop
1- Pasture
Iblacre
0.6
50
0
0
9
2
95
0
0
0
0
2-Adjust pH to 6.0
Iblacre
0.6
2
95
0
24372 6-7-8
49-7
MIN 2.2
5.7
2.3
180
38
42
238
575
575
390
10.7
79
60
17
0.8 0.1
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
P2O5
K2O
S
Mn
Mn-Al
Zn
Cu
B
Mg
Last Crop
1- Pasture
Iblacre
0.8
50
0
112
8
0
164
0
0
0
0
2-Adjust pH to 6.0
Iblacre
0.8
0
164
0
244373 6-7-8
49-8
MIN 3.0
6.2
1.4
377
82
29
363
818
818
735
11.4
88
62
22
0A D
Crop Recommendations:
Rec Uom
Lime (Vacre)
N
P2 05
K2 0
S
Mn
Mn-Al
Zn
Cu
B
Mg
Last Crop
1- Pasture
Iblacre
0.0
50
0
40
15
0
232
0
0
0
0
2-Adjust pH to 6.0
Iblacre
0.0
0
232
0
Comment:
Test result units = CEC and Na in megl100cm3; N0.,-N in mgldm3; WN in g1cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown an this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 20-045-0765
Account No: 46463
Waypoint"
-
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
ANALYTICAL
w+ww,waypointanalytical.coni
Advisor: Synagro Central LLC/ Kinston
Client: Paul
Price
Farm: CH-77
Marshall Puryear
284 Boger Road
Suite 204
Date Received: 02/14/2020
Mocksville NC 27028
Date of Report: 02/17/2020
Lab No Field lb
Sample f0
Soil Class HM% WN pH
Ac
P-1
K-1
S-1
Mn-1
Zn-1
Zn-AI
Cu-1 CEC BS% Ca% Mg%
ESP Na SS-1 NO3 N
24362 1-5-11-12-16
77-1
MIN 3A
6.2
1.7
669
143
27
294
1578
1578
825 13.9 88 58 25
0.3 0
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
P205
K20
S
Mn
Mn-Al
Zn
Cu 6 Mg
Last Crop
1- Pasture
Iblacre
0.0
50
0
0
16
0
190
0
0 0 0
24363 1-5-11-12-16
77-5
MIN 1,5
6.4
0.4
37
34
27
150
95
95
75 4.1 91 70 17
0.4 0
Crop Recommendations:
Rec Uom
Lame (t/acre)
N
P205
K20
S
Mn
Ma -Al
Zn
Cu B Mg
Last Crop
1- Pasture
Iblacre
0.0
50
40
85
16
0
101
0
0 0.5 0
24364 1-5-11-12-16
77-11
M-0 3.8
6.3
1.5
558
98
44
413
1328
1659
050 14.4 90 63 23
0.5 0.1
Crop Recommendations:
Rec Uom
Lime (t/acrej
N
P205
K20
S
Mn
Mn-Al
Zn
Cu B Mg
Last Crop
1- Pasture
Iblacre
0.0
50
0
0
7
0
260
0
0 0 0
24366 1-5-11-12-16
77-12
MIN 1.9
6.2
1.2
257
25
40
463
480
480
595 10.3 88 62 24
0.8 0.1
Crop Recommendadons:
Rec Uem
Lime (Vacre)
N
P205
K20
S
Mn
Mn-Al
Zn
Cu B Mg
Last Crop
1- Pasture
lb/acre
0.0
50
0
120
9
0
292
0
0 0 0
24367 1-5-11-12-16
77-16
M-0 4.6
5.8
2.4
393
39
50
438
1443
1803
935 12.8 81 60 19
0.5 0.1
Crop Recommendations:
Rec Uom
Lime (t/acre)
N
P205
K20
S
Mn
Mn-Al
Zn
Cu B Mg
Last Crop
1- Pasture
Iblacre
0.5
50
0
110
0
0
283
0
0 0 0
Comment:
Test result units = CEC and Na in meg110Dcm3; NC3 N in mg1dm3; WN in g/cm3
North Carolina division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.