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HomeMy WebLinkAboutWQ0001048_Residual Annual Report 2019_20200227an&n&ma off&w�oo&zw g'ewe&z .0G9tZ,rc>t CMSD POST OFFICE BOX 477 GRIFTON, NORTH CAROLINA 28530 CHARLES M. SMITHWICK, JR. DISTRICT MANAGER Mr. Daryl Merritt DENR/DWR/Water Quality Section Non -Discharge Compliance/Enforcement Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Contentnea MSD Land Application Permit #WQ0001048 2019 Annual Report Dear Mr. Merritt, February 20, 2020 ,tg •" � %020 Pe�i�tin9 Unit Please find enclosed three (3) copies of the above referenced annual sludge land application program report for the Contentnea Metropolitan Sewerage District (CMSD), Permit Number WQ0001048, for your review. If you should need any additional information please contact me at (252)524-5584. Sincerely, (�4 '/ 'e--" Charles M. Smithwick, Jr. Land Application ORC Enclosure ANNUAL LAND APPLICATION CERTIFICATION FORM K�v WQ Permit#: 0JjpLJ<9 County: '.j7i+-;- Year: 70) C Facility Name (as shown on permit): Onnfen4noE )- (Y%d-D Land Application Operator: i-yxf rf). `JJ7 g-y)ui kj ( Phone: ,and application of residuals as allowed by the permit occurred during toe past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. I-`_,3 ;, 7 2020 - Total number of application fields in thepermit: Za Total number of fields utilized for land application during the year: 3 Total amount of dry tons applied during the year for all application sites: y-Z: 30 Total number of acres utilizes for land application during the year: Part B - Annual Compiance Statement: �n Facility was compliant during calendar year ZG>I i with all conditions of the land a�plicC� }gr'�tt" (including but not limited to items 1-13 below) issued by the Division of Water Resources. ❑ `Y'es ;U No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Yermitt Name and Title (type or print) Signature f�Permittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) EXPLANATIONS FOR DEVIATIONS FOR THE 2019 ANNUAL SLUDGE LAND APPLICATION REPORT 2-19-19 Monitoring Well #9 Total Organic Carbon 10.10 mg/L Monitoring Well #10 Chromium 16 ug/L Monitoring Well #14 Chromium 26 ug/L Copper 0.077 mg/L 10-14-19 Monitoring Well #9 Fecal Coliform 16/100 ml Monitoring Well #10 Fecal Coliform 35/100 ml Monitoring Well #14 Fecal Coliform 7/100 ml Monitoring Well #15 Fecal Coliform 12/100 ml Monitoring Well #18 Fecal Coliform 200/100 ml On June 11, 2019 Groundwater Management Associates, Inc. (GMA) performed a groundwater evaluation at the Contentnea Metropolitan Sewerage District (CMSD) residuals land application sites. GMA concluded "that historical reports of chromium concentrations exceeding the groundwater standards in the monitoring wells at the facility were most likely associated with excessive turbidity. As such, these chromium detections would be naturally occurring in the aquifer materials. The June 11, 2019 sampling results do not indicate the presence of groundwater contaminations by metals (such as chromium) associated with residuals land application areas. The CMSD implemented a redevelopment program for their monitoring well network that entailed repeated bailing of the wells to remove sediment and to reduce turbidity. The Fecal Coliform hits in the monitoring wells during the October 14, 2019 sampling event are believed to have been caused by contamination of the well casings due to continued exposure during the bailing and purging of the wells prior to the sampling event. The CMSD has had all wells disinfected in January 2020 to eliminate any contamination. CLASS A Ai... JAL DISTRIBUTION AND MARKETING/ SURFA, DISPOSAL CERTIFICATION AND SUMMARY FOnivi WQ PERMIT #: ;,,,jQOC O [C)4;S FACILITY NAME: CL�lliC�l�1l �. m,,�D PHONE: 'e,52--JZU-5Sg 4 COUNTY: Pj.}+ OPERATOR: CY)af j 2-) M, 6Mj01)( i CL)Tf - FACILITY TYPE (please check one): 13 Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes 09 No ❑ ---► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) s) ( include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bullring Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February March April May June.! July t,WTP t 400032o77 August September October November December Total from FORM DMSDF (sup) Totals: Annual (dry tons): Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Part C: Total Number of Form DMSDF (Supp)I Facility was compliant during the past calendar year with all conditions of the land application permit ❑ Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No P It No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." .x-19.?ci?a Signature of Permittee Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM DMSDF (12/2006) RESIDUAL SAMPLING SUMMARY LAB REPORTS ANNUAL RESIDUAL SAMri,ING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: L)QCAc�ol04� Laboratory: 1) �/1�ffC�I�me/�% Z�l✓1C Facility Name: L`�n}, rf,6`D 2) Residual Source WQ # or 3) NPDES #: 4) WWTP Name: Conken�-n eg-fr6D 5) Residual Anal sis Data Parameter (mg/kg) Conc. Limit m /k a Sample or Composite Date �l z� Percent Solids (%) NA Arsenic 75 < 2,5 Cadmium 85 Copper 4,300 Z�? Chromium NA Z3 Lead 840 vD, Mercury 57 l) .Z,5 Molybdenum 75 <6,CS Nickel 420 t 15 Selenium 100 Zinc 7,500 �� ) Total Phosphorus NA 313 jgp TKN NA ��,o Ammonia -Nitrogen NA r)5,5 Nitrate and Nitrite NA a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pe7r�� bmitting false information, including the possibility of fines and imprisonment for knowing violations." -?-I9-awc Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) �n1Ml� T o,n qp (@n� � �n�(�,no o oTmm (� 4 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS PH (not to be used for reporting) Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg t-alcium (dry wt. basis), mg/kg admium (dry wt. basis), mg/kg topper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt, basis), mg/kg Total Nitrogen, mg/kg (calc) Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Nitrate Nitrogen(dry wt.), mg/kg Nitrite Nitrogen(dry wt.), mg/kg Phosphorus, T. (dry wt.), mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 3.6 04/29/19 JMS 4500HB-11 19636 05/02/19 LFJ EPA200.7 <2.5 05/07/19 MTM 3113B-04 15246 05/02/19 LFJ EPA200.7 1.0 05/02/19 MTM 3113B-04 271 05/02/19 LFJ EPA200.7 23 05/02/19 LFJ EPA200.7 25 05/08/19 MTM 3113B-04 4394 05/02/19 LFJ EPA200.7 0.25 05/10/19 MTM EPA7471B 15 05/02/19 LFJ EPA200.7 6957 05/02/19 LFJ EPA200.7 < 5.0 05/09/19 MTM 3113B-04 3081 05/15/19 LFJ EPA200.7 721 05/02/19 LFJ EPA200.7 47426 05/06/19 SEJ 1.57 04/29/19 JTH 254OG-11 c 40560 05/03/19 TLH 351.2 R2-93 c 1755 05/01/19 KPG 350.1 R2-93 c 6858 05/01/19 DTL 353.2 R2-93 c 7.96 05/01/19 TLH 353.2 R2-93 c 33180 05/03/19 BLD 365.4-74 < 5.0 05/02/19 LFJ EPA200.7 Drinking Water ID: 3771- Wastewater IDi 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 04/29/19 DATE REPORTEI) : 05/15/19 A D y 1 REVIEWED BY: ✓/( c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. TCLP LAB REPORTS Orlando, FL The results set forth herein are provided by SGS North America Inc. Technical Report for Environment 1, Inc Contentnea Metro Sewage District; Grifton, NC 416 SGS Job Number: FA62888 Sampling Date: 03/26/19 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentlinc. com ATTN: Deedee Woolard Total number of pages in report: 14 e Hardeopy 2.0 Automated Report Test results contained within this data package meet the requirements General Manrice, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), N1(FLO02), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZO806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SGS is the sole authority for authorizing edits or modifications to this document Please share your ideas about $�V Unauthorized modification of this report is strictly prohibited. how we can serve you better at: Review standard terms at: http:/hvww.sgs.com/en/temis-and-conditions Eli S.US.CustomerCare(ii se; com 1 of 14 FA62888 Table of Contents Sections: _1_ Section1: Sample Summary................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 4 Section3: Sample Results........................................................................................................ 3.1: FA62888-1: SLUDGE SAMPLE ............................................................................... 6 Section4: Misc. Forms .......................................................................................................... 12 4.1: Chain of Custody........................................................................................................... 13 2of14 VG _ FA62888 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA62888 Contentnea Metro Sewage District; Grifton, NC Project No: 416 Sample Collected` Matrix Client Number Date Time By Received Code Type Sample ID FA62888-1 03/26/19 09:05 KH 03/30/19 SO Sludge SLUDGE SAMPLE Soil samples reported on a dry weight basis unless otherwise indicated on result page. 3of14 FA62888 Summary of Hits Page 1 of 1 Job Number: FA62888 Account: Environment 1, Inc Project: Contentnea Metro Sewage District; Grifton, NC Collected: 03/26/19 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA62888-1 SLUDGE SAMPLE Corrosivity as pH 6.3 su SW846 CHAP? Ignitability (Flashpoint) a > 200 Deg. F SW846 1010A MOD (a) Not ignitable. SGw 4 of 14 FA62888 SGS' Orlando, FL Sample Results Report of Analysis Section 3 1� SGS5of14 FA62888 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE. Lab Sample ID: FA62888-1 Date Sampled: 03/26/19 Matrix: SO - Sludge Date Received: 03/30/19 Method: SW846 8260B SW846 3510C Percent Solids: 2.1 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 B132660.D 10 04/04/19 19:23 CV 04/02/19 15:00 OP74421 VB5355 Run #2 Purge Volume Run #1 5.0 nd Run #2 VOA TCLP List CAS No. Compound Result I-IW# MCL RL 71-43-2 Benzene ND D018 0.50 0.010 78-93-3 2-Butanone (MEK) ND D035 200 0.050 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 108-90-7 Chlorobenzene ND D021 100 0.010 67-66-3 Chloroform ND D022 6.0 0.010 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 75-35-4 1,1-Dichloroethylene ND D029 0.70 0.010 127-18-4 Tetrachloroethylene ND D039 0.10 0.010 79-01-6 Trichloroethylene ND D040 0.50 0.010 75-01-4 Vinyl Chloride ND D043 0.20 0.010 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 106% 83-118% 17060-07-0 1, 2-Dichloroethane-D4 115% 79-125% 2037-26-5 Toluene-D8 99% 85-112% 460-00-4 4-Bromofluorobenzene 90% 83-118% TCLP Leachate method SW846 1311 MDL Units Q 0.0031 mg/1 0.020 mg/1 0.0036 mg/1 0.0020 mg/1 0.0030 mg/I 0.0026 mg/1 0.0031 mg/1 0.0032 mg/I 0.0022 mg/I 0.0035 mg/I 0.0041 mg/I ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound c� 6of14 FA62888 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA62888-1 Date Sampled: 03/26/19 Matrix: SO - Sludge Date Received: 03/30/19 Method: SW846 8270D SW846 3510C Percent Solids: 2.1 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 9I004720.1) 1 04/08/19 22:01 MV 04/06/19 08:30 OP74496 S9I171 Run #2 Initial Volume Final Volume Run #1 100 ml 1.01111 Run #2 ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Methylphenol ND D023 200 0.050 0.0056 mg/1 3&4-Methylphenol ND D024 200 0.050 0.0098 mg/I 87-86-5 Pentachlorophenol ND D037 100 0.25 0.050 mg/1 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.050 0.0074 mg/1 88-06-2 2,4,6-Trichlorophenol ND D042 2.0 0.050 0.0075 mg/1 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.050 0.0050 mg/1 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.050 0.0081 mg/1 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/1 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 0.0050 mg/1 67-72-1 Hexachloroethane ND D034 3.0 0.050 0.016 mg/1 98-95-3 Nitrobenzene ND D036 2.0 0.050 0.0093 mg/I 110-86-1 Pyridine ND D038 5.0 0.10 0.020 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 29% 14-67% 4165-62-2 Phenol-d5 24% 10-50% 118-79-6 2,4,6-Tribromophenol 79% 33-118% 4165-60-0 Nitrobenzene-d5 56% 42-108% 321-60-8 2-Fluorobiphenyl 56% 40-106% 1718-51-0 Terphenyl-dl4 74% 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 14 FA62888 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA62888-1 Date Sampled: 03/26/19 Matrix: SO - Sludge Date Received: 03/30/19 Method: SW846 8151A SW846 3510C Percent Solids: 2.1 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC061615.D 1 04/09/19 05:49 RS 04/06/19 11:00 01174497 GCC1434 Run #2 Run #1 Run #2 Initial Volume Final Volume 10.0 ml 5.0 nil Herbicide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 94-75-7 2,4-D ND D016 10 0.050 0.017 mg/I 93-72-1 2,4,5-TP (Silvex) ND D017 1.0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 93% 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1A1) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8of14 FA62888 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA62888-1 Date Sampled: 03/26/19 Matrix: SO - Sludge Date Received: 03/30/19 Method: SW846 8081B SW846 3510C Percent Solids: 2.1 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 KK93509.D 1 04/08/19 16:25 WH 04/06/19 08:00 OP74495 GKK2971 Run #2 Initial Volume Final Volume Run #1 100 ml 5.01111 Run #2 Pesticide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) ND D013 0.40 0.00010 0.000022 mg/1 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin ND D012 0.020 0.00020 0.000021 mg/1 76-44-8 Heptachlor ND D031 0.0080 0.00010 0.000026 mg/1 1024-57-3 Heptachlor epoxide ND D031 0.0080 0.00010 0.000020 mg/1 72-43-5 Methoxychlor ND D014 10 0.00020 0.000050 mg/1 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 71% 42-127% 2051-24-3 Decachlorobiphenyl 75% 27-127% ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/l/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9of14 FA62888 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA62888-1 Date Sampled: 03/26/19 Matrix: SO -Sludge Date Received: 03/30/19 Percent Solids: 2.1 (Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/l 1 04/11/19 04/12/19 LM SW846 6010D 2 2 SW846 3010A 4 SW846 3010A 4 Barium < 2.0 D005 D006 100 1.0 2.0 0.050 mg/1 mg/l 1 1 04/11/19 04/11/19 04/12/19 04/12/19 LM LM SW846 6010D SW846 6010D 2 SW846 3010A 4 Cadmium < 0.050 Chromium < 0.10 D007 5.0 0.10 mgA 1 04/11/19 04/12/19 LM SW846 6010D 2 SW846 3010A 4 Lead < 0.050 D008 5.0 0.050 mg/1 1 04/11/19 04/12/19 LM SW846 6010D 2 1 SW846 3010A 4 SW846 7470A 3 Mercury < 0.0050 D009 0.20 1.0 0.0050 0.10 mg/1 mg/1 1 1 04/04/19 04/11/19 04/04/19 64/12/19 Jc LM SW846 7470A SW846 6010D 2 SW846 3010A 4 Selenium < 0.10 DO10 Silver < 0.10 D011 5.0 0.10 mg/1 1 04/11/19 04/12/19 LM SW846 6010D 2 SW846 3010A 4 (1) Instrument QC Batch: MA15750 (2) Instrument QC Batch: MA15773 (3) Prep QC Batch: MP35316 (4) Prep QC Batch: MP35352 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/l/11) er%s 10 of 14 __au FA62888 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA62888-1 Date Sampled: 03/26/19 Matrix: SO -Sludge Date Received: 03/30/19 Percent Solids: 2.1 Project: Contentnea Metro Sewage District; Grifton, NC General Chemistry Analyte Result RL Units DF Corrosivity as pH 6.3 so 1 Cyanide Reactivity < 72 72 mg/kg 1 Ignitability (Flashpoint) a > 200 Deg. F 1 Solids, Percent 2.1 % 1 Sulfide Reactivity < 2400 2400 mg/kg 1 (a) Not ignitable. RL = Reporting Limit Page 1 of 1 Analyzed By Method 04/11/19 15:15 BW SW846 CHAP7 04/09/19 GW SW846 CHAP7 04/02/19 11:15 BW SW846 1010A MOD 04/11/19 15:22 AC SM19 254OG 04/09/19 11:55 AC SW846 CHAP7 _SGS 11 of 14 FA62888 SGS Orlando, FL Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 C (� 12of14 _VLIc FA62888 Environment 1, Inc. P.O. Box 7085, 114 Oakmont Dr. Greenville, NC 27858 nvironment I inc.com hone (252) 756-6208 • Fax (252) 756-0633 CLIENT: 416 Week:9 CMSD (SLUDGE & WELLS ACCT) CONTEN7NEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRTFCON NC 28530 (252)524-5584 CHAIN OF CUSTODY RECORD FA�ZOEof I DISINFECTION CHLORINE NEUTRNJZED AT COLLECTION CHLORINE pH CHECK (LAB) UV NONE P P P G G G G G CONTAINER TYPE, PIG CHEMICALPRESERVATION A A A A A A A A N A -NONE D-NAOH Z w o ¢ o b B-tea E-HCL o¢ Z z y. rn a a C-HLS0 F-ZINCACETATEINAOH o g 8 .o a¢ G-NATHIOSIAFATE 0 0 �" ¢ � u s a � U u F ,a rr�� F U F f- F a a ib 5 CLASSIFICATION: WASTEWATER(NPOES) DRNKINGWATER DWR(GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURINPMENT/DELIVERY Y N SAMPLES COLLECTED BY: (Please P it LL'' 71 �Q `emu .r7S SAMPLES RECEIVED IN LAB AT °C RECEI BY(SIG.) >F/I1ME COMMENTS: • RECEN (SIG.) E w T P. aw C. rU y7-0DATFJtM�v1EA. RECEIVED BY (SIG. q IQ - a Sampler must place a V for composite sample or a "G° for f 3� j /fGrab sample in the blocks above for each parameter requested. N2 365257 FA62888: Chain of Custody Page 1 of 2 bu __ 13of14 FA62888 SGS Sample Receipt Summary Job Number: FA62888 Client: ENVIROMENT 1, INC. Project: SLUDGE AND WELLS ACCT pate / Time Received: 3/30/2019 9:15:00 AM Delivery Method: FED EX Airbill Vs: 1001893324360003281100486845038270 Therm ID: IR 1; Therm CF: 0.4; # of Coolers: 2 Cooler Temps (Raw Measured) "C: Cooler 1: (1.8); Cooler 2: (2.2); Cooler Temps (Corrected) °C: Cooler 1: (2.2); Cooler 2: (2.6); Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 3. Temp criteria achieved 4. Cooler temp verification 5. Cooler media Trio Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC Y or N ® ❑ © ❑ 0 ❑ IR Gun Ice a Y or N N/A ❑ 0 ❑ ❑ 0 ❑ W or S NIA 3. Type Of TB Received ❑ ❑ Misc. Information Number of Encores: 25-Gram 5-Gram Test Strip Lot #s: pH 0-3 230315 Residual Chlorine Test Strip Lot #: sample mrormaoon 1. Sample labels present on bottles 2. Samples preserved properly 3. Sufficient volume/containers recvd for analysis: 4. Condition of sample 5. Sample recvd within HT 6. Dates/rimes/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? 12. Residual Chlorine Present? L. © ❑ nta ❑ ❑ ❑� ❑ ❑ ❑ ❑ ❑ ❑ 66 ❑ ❑ Number of 5035 Field Kits: Number of Lab Filtered Metals: pH 10A2 219813A Other. (Specify) shoot Technician: TRINITYM Date: 3/30/2019 9:15:00 AM Rev. Dale 0524117 Reviewer: Date: FA62888: Chain of Custody Page 2 of 2 14 of 14 __ SGS7 FA62888 LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION F —,D SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: �,�� WQ Permit #: tCIC�t I� Field #: Land Owner: (� ����-jam Annual Dry Tons Applied: Site #: Operator: Chorl e5rf)6t -T1- Predominant Soil Series: Crop 1 Name: &-01- -C(baCrop 1 Max. PAN: I")(v Crop 2 Name: Acres Utilized: Z,,gL/ Acres Permitted: Z, q4 Cation Exchange Capacity (non 503): 1-4.6 Crop 2 Max. PAN: �, � ° ° c ° Q Volume applied Pp � (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume A lied er PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. �rY. Wet Moist Precip. Past 24 Hrs. inches > b oo w, o � C o 7y w P w�. w , w. N w.. 0 TKN mg/kg Z�� o °C,° C, w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type P YP Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 71 .... . .... Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): .................. TOTALS: 2C As Cd Cu Cr Pb Hg Mo Ni SePZn P 3-1.52� Lime A lied lbs/acre O,Annual ,5 5 5O-Col? 0. U .OIO G ` 0► O Z3 G :.: ........... Date lbs/ac Prior Years Cumulative lbs/ac ,5a5 .5� I q-CQ� , Z2,&QS ,P'P .3b4 .4�3 '2. Z4 3 Current Cumulative lbs/ac CU 5l0 .5o(o I •h�f3 Ici 0,3b�3...Permitted C. P. L. R.**** ( 3U 1338 — z(P) t 5 — 4 Zu Permit PAN Limit 1st/2nd Crop P i Co "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informati9p, including the possibility of fines and imprisonment for knowing violations." Al Signature of Ladd Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: %n-i�n6a..-IYM6f� Total Dry Tons Applied (Annual): Z, 75L5 P— nit #• LoQW01C .I.td Cation Exchange Capacity (non 503 only): U. 5 rator: (' pi l9LCIL�Tr• Owner: ('Cn+M1 nta.N)6Dj Predominant Soil Series: Acres Used: Z• S(4 Acres Permitted: Z. S(-y Site #: 13 Field #: � pacifl„nl Analveic Data (Aeavv Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Com- posite Date 1 ,Zq,/q 2 3 4 5 6 7 8 9j LOJ 11 12 % Solids 1.515v Arsenic G 2 , 5 Cadmium I • D Copper Z71 Chromium Z3 Lead v5 Mercury p • Z5 Molyb- denum e 6.0 Nickel 1 r7 Selenium < 5. D Zinc 02I Total Phos- us 13,31 c6O nol FTeaw Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6_ L7J L8J 9 10,1 11 12 DT/Ac./ 6_�5,ia c App. Event mq&g Arsenic p Cn5 Cadmium 6.03Z OZ Copper D. 52 5 6z,5 Chromium. D14 5 c, 0415 Lead , C)LI4 O.OUS Mercury C) , D coo Molyb- 0)0 o CA 0 Nickel , &Zq O Selenium C-), D 10 C' 01 O Zinc Total Phos- phorus Z "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoruance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I ^— aware that there are significant penalties for submitting false information, including the possibility of fines and it sonment for knowing violations". &.4 ,,/ o�-�9ycye Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: lxt�ax CYl�2) WQ Permit #: 04q Field #: Z Acres Utilized: Z• (�, Z Land Owner: con+a--t Annual Dry Tons Applied: 13(4 0 Site #: Acres Permitted: L7, (p2 Operator: &)al Ienm, brn,A4.0Ct,1-Sr Predominant Soil Series: 16c+al U 5 Cation Exchange Capacity (non 503): Crop 1 Name: I ZOO 5iL-dSMIM Crop 1 Max. PAN: i SO Crop 2 Name: Crop 2 Max. PAN: ° +� ° ° Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. (D Wet Moist Precip. Past 24 Hrs. inches > 4.0 , R3 E' a w * O �J C o � * N w ., w * w * �• TKN mg/kg z �� q o � CO 5. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 24-�-1 za�O 1.,5 1. ZG Q WCC03 Zo-p Ar,4 10 0, 5 0.30 465bo 1-)55 gkoqe, z (. Cjq Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): TOTALS] �Z� :: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 6, z Lime Applied Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulativelbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Cro Cp(n O,C©3 d, py ,0I3 . ,0L Z 5.065 a.IGU 34, w O 3 s.gg5' -) i d. &V9 5•v�Q W-$GQ,31•1.3o► 1-06 0.35L1 Z 9��3 .G3L4 6 R o3 :::::::::::`>.'::::::::::: _ ........................... U '2 Z 7 15 - 37L1 �3ci Z4r1 ::::::::::::::::::::: : : : ::::: : : : : : ::: :::::: ............. .... ....................... Date lbs/ac G-25A lb� 1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, ,0cluding the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Cpnt"P14m,-fY 6D Total Dry Tons Applied (Annual): JQC4 Permit #: Of!�0 o(C49 Cation Exchange Capacity (non 503 only): (4- rator: Owner: 0nf-)1-C����r� G� IYl,?� Predominant Soil Series: P[ajc))(P h txvl es Used: Z. (p Acres Permitted: z 2 Site #: Field #: `z Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date L-11 21 3 4 5 6 7 8 9 10 11 12 % Solids 1v Arsenic < Z.,5 Cadmiuml 1.0 Copper I r) I Chromium Z3 Lead Zcj Mercury Molyb- deninn Nickel 15 Selenium <5.0 Zinc I 721 Total Phos- ^T A us 3319 C; ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 L4J L5 6 7 8 9 1 o 11 12 y DT/Ac./ {�Zy_loi o App • LA Event .;Wig. Arsenic p , Cadmium 0 , Op3 0, oc;3 Copper p, L)4 ,-)a4 Chromium O ; p(„ p O Lead c).6105 M.6106 Mercury p _ 1 O. Molyb- cionum , 13 0,013 Nickel p 03Cj1_3 SeleniumZinc 1.Q73 7 Total Phos- phorus Z 2 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and in onment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: C0nAQ-4nf0-rn6D WQ Permit C�(I Field #: 3 Acres Utilized: z.iz Land Owner: cliff`} (1�0�-fY1217 Annual Dry Tons Applied: Z , I G, 3 Site #: Acres Permitted: t�, 7 Z Operator: C�Gflfr�..5mi`Iuy.�iCYL7� Predominant Soil Series: ���� Cation Exchange Capacity (non 503): (4, 5 Crop 1 Name: -bffn-L1n0- Crop 1 Max. PAN: I -)L� Crop 2 Name: Cron 2 Max. PAN: o G +' a o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons oho Solids Volume A lied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist Precip. Past 24 firs. inches > b o a C o w w � * N' * N o 0 7y w ., � w * w f TKN mg/kg Z o El °R 0 mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Mb r.�, o. oco-1c�3Zo7� r p o.5 o3a D 5 �b 31.7Ji C° Q. sCCp Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): TOTALS: Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd —Crop As Cd Cu Cr Pb H Mo Ni Se Zn P L G, U O,COZ p; -) O. 53S' p, j 7 c (�.gS1 g,� 3 0- Z-P141 10.t418 c,Poo I 3 :..... . .:: -i5 1.23ci 54, 4 4a,ci ig 4 .423 , ZG3 ZG Ltd .................... 3C� `�....1.3 S - Zto7 15 3)4 S° ZUGg — .. ..... ti i0 Lime Applied.. Date lbs/ac ,i's -Fi 61W/h5 - �- -__„ ..u..— F, 11"=L.,y vi law, LL1216 LUIS uucument was prepares under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incoruoration -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: (r` +tr,4nr`C--m6D Total Dry Tons Applied (Annual): Z. q 3 Permit #: (^ )nfb-4n�l�� Cation Exchange Capacity (non 503 only): C/,5 •ator: Cl-pf �e6in. brn l l iU,77 Owner: r(j)+pn+n6DL m6Dt Predominant Soil Series: Acres Used: Z:7Z Acres Permitted: Z.-)z Site #: 6 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 Cl 2 3 4 5 6 7 8 91 10 11 12 % Solids i. -fi Arsenic <7.1j Cadmium (• O Copper 7­2 1 Chromium Z 3 Lead ZC Mercury C) , ZS Molyb- < 5.p Nickel 16 Selenium I <�j.© Zinc o Z I Total Phos- �' ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 11 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ � z5-1 G y o App. Event b.g6(.o Arsenic D. O•CL i Cadmium 0, WZ- Copper T O.43-) Chromi , 3--) . 637 Lead 6, p4D O, 040 Mercury p . © 4, COCA Molyb- Nickel , OZW U Selenium Zinc Total Phos- phorus 53•14 53� 4S� "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im cnment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION _LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Cbn+er4n.egL m6D WQ permit #: lO i 04,q Field #: y Acres Utilized: Land Owner: C0n+ff e0 m�tD Annual Dry Tons Applied: 0,-�ZC� Site #: 3 Acres Permitted: & 3u Operator: CLQl11e5M-6640 I• Predominant Soil Series: _} IU_j Cation Exchange Capacity (non 503): y• 5 Crop 1 Name: C a_ -A r r.cj&_ Crop 1 Max. PAN: I g© Crop 2 Name: Crop 2 Max. PAN: Y a� Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. (Dry, Wet, Moist Precip. Past 24 Hrs. inches y a b F" �" o� w * o C o ;n w �, � o — 7y w, Q °� N * o TKN mg/kg Z�� � o Q° o g w' mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 I� 510CX� 1.5 I • CCA NCCC337lS� 1, 000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALs: 5►CCO As Cd Cu Cr Pb H Mo Ni Se Zn P 3S,�7o Lime Applied Annual lbs/acre Prior Years Cumulative lbs/ac a. OO O COZ ` (aZ ,. jp(o 310 ' ::::..::.:::: (b � O . 016 OU3 d 0, 013 `I I.Z ©,`)} 1 4 G5U k(I-49 24 614 -)q 0-lid .-)SG ci.tZ3 0.43 0 Zqr ... 7(i to U.�iS U•i 472.`� , t�� Z •7GG (o j3 6 �+ 4 C ZC4,125 36 y 13 5 "7 15 — "X4 Qq 1. Date lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. Permit PAN Limit 1st/2nd Cro P •'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false :7M luding the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation JIF ova!r�/ 7 .t�'� **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: C6n+e-)4f)feci_-WOD Total Dry Tons Applied (Annual): 3. 33c) Permit #: Cation Exchange Capacity (non 503 only): U , 5 •ator: CitlfD�J1 Y�iCIL�S� Owner: CpI--)}en44-)� i� Predominant Soil Series: Acres Used: 3, 3 4 Acres Permitted: S.3Q Site #: 3 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6 7 8 9 10 11 12 % Solids Arsenic <2.5 Cadmium ) . p Copper Z-) I Chromium Z3 Lead Z5 Mercury p, Z-j Molyb- denum <5•0 Nickel 15 Selenium <!5.0 Zinc I Total Phos- -'---us "31�sv ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 1 2 3 4 5 6 7 8 9 10 11 12 App. Event I - CCD 1. O Arsenic C)Cj,5 Cadmium 6, CC;& D, Z Copper 6, 5tjZ Z Chromium 0,04(o Lead 0.0,50 . 050 Mercury In, p p, Molyb- denilm O <OIO Nickel 0,C 3C>01 Selenium 0,C>tO 61010 Zinc I. ULl1 I.LIUZ Total Phos- phorus .' (co (ol0 3bD "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and in onment for knowing violations". dIZ4 V Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION"- —LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Co-y l+n,@g- m `d Land Owner: Cn,-Fer�ne« f')517 Operator: 0—)006nn.6niwU 0-Jr Crop 1 Name: 'rv,, err WQ Permit #: tx_)=1041 Field #: Annual Dry Tons Applied: . �37 Site #• Predominant Soil Series: u(15 Crop 1 Max. PAN: IV( Crop 2 Name: 5 Acres Utilized: 3 7 (4 3 Acres Permitted: 3,--)L4 Cation Exchange Capacity (non 503) Crop 2 Max. PAN: u•5 o +' a; o at Q tQ Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons 00 % Solids t.M Volume Applied per PP P Acre (Dry Tons/Ac) ' O S ` Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) 9C 03 ')� Soil Cond. (Dry, Wet, Moist Precip. Past 24 Hrs. inches O a b 5 o' o w p C o �y w ; * N• * w o p.5 ;� w, co ?= * �• * * c. 0 o.3Z) TKN mg/kg Stud Z o B o0 0 o w• mg/kg 1-)56 Nitrate and Nitrite mg/kg 64b59rc PAN Applied lbs/acre ( ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Q • (1 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): . ToT' s. LU Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac etmitted C. P. L. R. **** Permit PAN Limit lst/2nd Crop P LLT _ As Cd Cu Cr Pb Hg I Mo Ni I Se Zn P v Z O, Co) , 7 01 O . ZZ D. o b. 0. 013 , Z4 �(o : 0. 1Z t}, 17 ci37 3�, p33 p�, 3• I4 i G.�72 I - ..... .... . l y L-1.1 '�u 7 .174 3lv•� U 055 Z� (L 5 5 0 .G85 i •u3b :::.:::::::::::......... ..... .................... (o I — Z )37y g9 4cg :: .................................................... Lime A lied Date lbs/ac i certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informatin30ncluding the possibility of fines and imprisonment for knowing violations." _ *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 JOV Signature of Land Applier Datex* Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Conien,�)co_ Cn67 Total Dry Tons Applied (Annual): Permit #: Cation Exchange Capacity (non 503 only): •ator: Cl�t(1>° �5rs�l ltt Cl j, f• Owner: CC�()4er4f)6DL rf-&-pj Predominant Soil Series: _Rcc+ob) Acres Used: 3,-?L4 Acres Permitted: i,')L4 Site #: -13 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 a-L _Iq 21 3 4 5 6 7 8 9 10 1j 12 % Solids i . 57 0 Arsenic C 7,5 Cadmium I ,D Copper z71 Chromium Z3 Lead Z l5 Mercwy 0 ,25 Molyb- denum <5, o Nickel I lj Selenium <6, p Zinc /)Z I Total Phos- _'--.:s 331S01 ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ App. Event 6,(4343 Arsenic 0,002 10, UO-z Cadmium O . Col Copper p D, Z,32 ChromiumO OZD GZ Lead Mercury Cp,Cjpp Molyb- Coo 4 Nickel O 13 3 Selenium 4 Zinc Z D lo32 Total Phos- phorus ZCf,OL4o I I I I I Zq•CX� "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im onment for knowing violations". card vtl Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: COnier4r q— n()dp WQ Permit #: G�_)Q�* jC)QR Field M 49 Acres Utilized: Land Owner: OC�nfEr)4n eC� fYi�-D Annual Dry Tons Applied: 3 (,) BCD Site #: c -ram II Acres Permitted: Operator: %t ittwo, 6ln4-ocqr— Predominant Soil Series: Cation Exchange Capacity (non 503): Crop 1 Name: }gl L�fr)(,iCl+C3.. Crop 1 Max. PAN: 17Z Crop 2 Name: Crop 2 Max. PAN: -2•-)3 4.5 ° + ° ° >~ ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist Precip. Past 24 Hrs. inches Y a w C o ,y w w �• � - N o o 7y m w * TKN mg/kg Z q o 0 °�°, o o P. mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre ( ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Z2 :: C) • �l4 (.v Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 5Z7LXJ .:<-::: »: As Cd Cu Cr Pb Hg Mo Ni Se Zn P n.-n I Lime Applied Annual lbs/acre -Z I Zug OZ ► (D,015 CO .0014 p.lotil 5� :::... D, I I.')")Z 41-11 5O -ZLID.�I`. (v I (v 'p3 . 53 Z� b� 5 5. 34 (� 13�(2 IUS 5. 3Z I o • 14:1�5 ,3 15 7 I Z Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit 1st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informati, inNluding the possibility of fines and imprisonment for knowing violations." Signature of Land *Application Method: S - Surface, IN - Injection, INC - Incorporation I ,A .2 U **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Cpnten�ne_&_rnbT Total Dry Tons Applied (Annual): i3.45o Permit #: ,,per I GUI Cation Exchange Capacity (non 503 only): 4.'5 rator: Cj 1� �,n, 6MtWj 0g Owner: �Pf)jen4ne� (��;�� Predominant Soil Series: Acres Used: -),-)3 Acres Permitted: 7_--23 Site #: C_TjaC } Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 U ZG- IGl 21 3 4 5 6 7 8 9 10 11 12 % Solids j .57`Jv Arsenic < Z, 5 Cadmium I.O Copper Z-) Chromium Z5 Lead Z15 Mercury C) , Z5 Molyb- deninn Nickel 15 Selenium <6.C) Zinc 7Z1 Total Phos- -'--Us 3►:6o ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event p, L1 fc 121 L3J4] L5J 6 7 8 9 10 11 12 � (p Arsenic Z Oc�Z Cadmium 0, 00 Copper O, ZL4Z Z42 Chromim Lead 0 0 1 0V Mercury p, C) D • p00 Molyb- demum oou Nickel 13 Selenium 0, OCqO 004 Zinc p. (ot. -5 ` u3 Total Phos- horus Zq, J�F) "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im onment for knowing violations". Signature of Land Applier 01 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION -__LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: C©Her I)*-CL [y)6 J7 WQ Permit #: 1x.)Q0W tC)44,g Field #: Land Owner: Ccn+eFQ m6t) Annual Dry Tons Applied: 0 • P0 Site #: Operator: C11ak-,) li)• bm'14-u i(ui. Predominant Soil Series: A l aao. Crop 1 Name: CQ=l�lri Klg= Crop 1 Max. PAN: 02 Crop 2 Name: C4 Acres Utilized: c `n- f Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 5.i5 6.15 4.5 o a� Q Volume applied (enter one) Solids/ Li Liquid 4 Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. D ( rY� We t Moist Precip. Past 24 Hrs. inches y b o� w * o o C o �y w �. c� .r po � , �, * N � �• 0 TKN mg/kg Z �o o g mg/kg Nitrate and Nitrite mg/kg PAN Applied (ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 -1q 4m6 i 574b ©,SfU U3 -) rndi& n 0,5 0,30 Q 1-66161-:5.124,31-551 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): . TOTALS: . ::::::::::::::: Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PA N Limit lst/2nd Crop As Cd Cu Cr Pb H Mo Ni Se Zn P J1.5� G. ooci O, WZ O, 4U I U• CZn D, py I • `p:�3 ©,p.4 O.OU3 , ao 1 ' :: 1. g-) U ,54. Zb.$19 5 :5 Z 1 0 ,141 10t, 6,W3(o 07)::::::::::::::::::::::::::::::::::::::::: 55 (F, �tG 5. IG3 Z(:�5% 5.5 b"L iUl Z• ��I 5,1o37 O • iy G51::.....:.:.`:.:.:...:.:.::.:.:.:... _ .3u i Z(or) 15 ,3-)L4 U g ::::::::::::::::::::::::::»:< :: : -17 Z' Lime Date A lied lbs/ac 2j i certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information in�ding the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation ^'! �-'ai4,7D **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: CC r)i �eCk. M &D Total Dry Tons Applied (Annual): 44, IQC) Permit Cation Exchange Capacity (non 503 only): y 5 •ator: Cbpf� f(�.5rfi �viC�iY Owner: CCU}en �a YYI Predominant Soil Series: A � Acres Used: 5.15 Acres Permitted: 5,15 Site #: C TQCj z1 Field #: Cr Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 21 3 L 4 5 6 7 8 9 10 11 12 % Solids Arsenic 2, 5 Cadmium i .O Copper Z-21 Chromium Z3 Lead Z5 Mercury C5, ZS Molyb- denlim Nickel f �j Selenium < Cj Zinc 721 Total Phos- ,,--is 33 i tal Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ c App. a Event ©. y zj Arsenic 6,0014©.L 1 Cadmium .CX>Z 002 Copper j Chromiiu C) 37 7 Lead O 4 Mercury 0.ODCO O Molyb- deflilm Nickel 0, 62Z j .OZ(4 Selenium C) • COfd Zinc L 174 1 1 C Total Phos- phorus 54-QF1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and irr onment for knowing violations". A Signature of Land Applier Jr Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION '&....,LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: �' cfillleL�. WQ Permit #: Field #: 13 Acres Utilized: 3• 20 Land Owner: Cef)+en�nlEg_ 1•f):51D Annual Dry Tons Applied: Site #: C ('Z-Q&Z Acres Permitted: 3,30 Operator: 11P1,►t1iJfCkl�r Predominant Soil Series: On �� Cation Exchange Capacity (non 503): Crop 1 Name: %ZL 2fmuei OL Crop 1 Max. PAN: Ito I Crop 2 Name: Crop 2 Max. PAN: o a) Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. (Dry' Wet' Moist Precip. Past 24 Hrs. inches > 5 � A w * o �J C o �, � — * N F) 4 7y w CD RL * 0 TKN mg/kg Z � q o � M 0 0 R. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 O 0-3L1 4c6&0 1755 Ug A(,i . (U . Lf-)(c Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: ZcFpv As Cd Cu Cr Pb H Mo Ni Se Zn P i . , �I Lime Applied Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop t� 1 1 D-Ol1 Z . L). , 0,04 0 ); 7 ..: >::::::::. ... 0, 3 ZO 0,229 t 7 7, i U Z• 33 3 0.013 1 • C?5 .4")� r q u Clf2 .......... L 3 ............... .. ... . . 32 v;3s�35 2.33 Z,357 :G� 1,06 2•GCti c, 4 Gu, ....................... -��....... Z Q ::: .............. �'' `' Date lbs/ac i certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informati "luding the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: m� Total Dry Tons Applied (Annual): j , 5-) ) Permit #: k C t.`O�IC�I� Cation Exchange Capacity (non 503 only): y. j rator: ( r0 {�. i f161� eCkj7�. Owner: (_pf) f e _n-0 Predominant Soil Series: j11 G� Acres Used: 13-bb Acres Permitted: 3.3C�. Site #: j _�> Field #: CMC(Cf-11 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 11 oq 21 3 L 41 L-51 L 61 7 8 9[io-I 11 12 % Solids -) Arsenic , 5 Cadmium 1 -0 Copper Z7 i Chromium Z-3 Lead Z5 Mercury L), Z) Molyb- denum <5Q Nickel 1,5 Selenium C5O Zinc '7Z Total Phos- us ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total© © © 0 0 0 •. Event • b • • rr ®®®®®®®®®®®♦ •• MEMO, MI • ®®®®�®®®®®®b ®®®®®®® • -• u Y iY owl ® • . P• EEEEEEEEEEEN� __ahorus__M-, "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im anment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION I. .,,D SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: LnieNner -m-,p WQ Permit #: 1JQ=1()49 Field #: Land Owner: i��FY1 Annual Dry Tons Applied: Z,CC4-1-S Site #• Operator: ��i�,.y7r Predominant Soil Series: Crop 1 Name: CCD&x1 ter Crop 1 Max. PAN: 17(p Crop 2 Name: Acres Utilized: 3. 0D Acres Permitted: 3-on Cation Exchange Capacity (non 503): (4- 5 Crop 2 Max. PAN: JtJ ° a- N s~ ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons a/o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, We t, Moist Precip. Past 24 Hrs. inches y 5 o' o w �, C o 7y �. �, �- * N' o 4 ;v � w •, � � * '- TKN mg/kg Z y q o a ao o o w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 -1 pe I [xx 1.5 ©• ( 1-�Cc�3ZU�� d C� : S o 3U c/ . o t �5.4io Z') • of 1 b • Lq q Residuals Applications totals on FOkM FSF supp ( attach FORM FSF supp to this form): TOTALS: As Cd Cu Cr Pb Hg Mo Ni Se Zn P Lime Applied Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd -Crop - 0 , CCU' L ool , , 0. Z O. 5 v O�OZ) . ' 7`1-Cb!'4&31q >:: >: 0,710 0•405 q • Q-'4 0- }k ) -�40 O,C210 Ca- '-n Z w) ic�l,• o, Zi 3 0,4cCCq-C,9-) 4.(, i •4si b , _ �SSS �.3ZZ (� 333....:...::.:.::::.:.:.......... u I ^8 L�� i 5 a3�u g�a Z4�i (o Date lbs/ac �"-, h 1 certuy, unaer penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informati n�ncluding the possibility of fines and imprisonment for knowing violations." Al Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: C cnit7-An>?c ff k2 Total Dry Tons Applied (Annual): -K 025 p-r*nit th 104 Cation Exchange Capacity (non 503 only): 4.5 rator: OyAt le-0. SrYl'a')OckATi Owner: C(� -- P11�1 0 m,`J 1� Predominant Soil Series: �+j� Acres Used: 6,00 Acres Permitted: & W Site #: Field #: IL..} Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 _Ic 121 3 4 5 6 7 8 9 10 11 12 % Solids Arsenic Z, cj Cadmium Copper 1 Chromium Z 3 Lead Z� Mercury & 7,5 Molyb- denum rj,D Nickel i Selenium <,j.O Zinc /)Z I Total Phos- us ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 121 3 L4 j5 6 7 8 9 10 11 J 12 DT/Ac./ App. Event 0. 0::eR Arsenic 0.O03 00 3 Cadmium p Co I ,Gb Copper Chromium D, 32 _ ,032 Lead O , 35 0 035 Mercury 000 DODO Molyb- denum p.a(?7 7 Nickel 0, t72l Selenium 7 .1X77 Zinc j pp7 I.007 Total Phos- horus 4h, la I4h,31q "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I a— -ware that there are significant penalties for submitting false information, including the possibility of fines and im �)nment for knowing violations". CA" W a1W;6�16 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION-' - --.LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: C��c �� WQ Permit #: LJQCWfWgg Field #:y 5 Acres Utilized: Z.31 Land Owner: ' ('fo Annual Dry Tons Apphed z, rj Site #: Acres Permitted: 2•39' Operator: Chakl ) (l.&n4-uli S• Predominant Soil Series: (� �;(-4-�r-(��►.y'1 Cation Exchange Capacity (non 503): f../. 5 Crop 1 Name: CQ ,, .faJ 13ermL Crop 1 Max. PAN: i") (0 Crop 2 Name: Crop 2 Max. PAN: ° ° d ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Pp P Acre (Dry TonslAc) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist Precip. Past 24 Hrs. inches y 4 � coo E o A a * C o 7� w w i -- * N' ?_ o � � P. o w * w * o' TKN mg/kg Z y El o 0 ac o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 i 31WO 1. 4�80 i��CC�3Z0"� rnoia+ 5 C� 5 a�30 4as�v I755 �5 U.11 S ........ ......... ..... .. . ....... ....... ....... 45`d Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):.................. .................... TOTA1s:ZCcv As Cd Cu Cr Pb Hg Mo Ni Se Zn P 34.11$ Lime Applied Annual lbs/acre Prior Years Cumulative lbs/ac 5, COLI (3,DaZ p;11-)7 0, 61 0- 742 0,u-I0 22510 q,102 Z.IL,,2 0 035 0, 0D 2.4Zg 6,346 i i5 Iw :. ::: ,Zino p L112 Z)•��a 1U�- Z.ZUIo d35 e7 • bU5 Cj01 4U� 1 .U1 `::`::"::::::::>::::: >::':::: ........... t-{ 133� — ZI�� I ' j -- 374 q Z 8 ..........:.......:.:.:.:.:.:.:.:.:.:.:.:. ......................... 7 1 � Date lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit lst/2 nd Cro p '•1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informat* ncluding the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Dame: Co fYl6�1 Total Dry Tons Applied (Annual): Z, UG, Permit #: ,LJQC)W I OL4 Cation Exchange Capacity (non 503 only): Lt, 6 rator: dt. ,m, jr ; iq— - Owner: (�C��}��}r� m � Predominant Soil Series: Pal6ffg_6�h Acres Used: Z,?�Cd Acres Permitted: -Z-34 Site #: �6 D Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 U- 121 3 L4 5 6 7 8 9 10 11 12 % Solids 1. Arsenic <' Z. -6 Cadmium 1.0 Copper I zi1 Chromium Z 3 Lead 25 Mercury ,25 Molyb- dcniirn �5.0 Nickel i 5 Selenium <5,() Zinc r?z 1 Total Phos- is I T� ial Heavy Metal Field Loadings (Calculated in lbs/acre): .. D - pp Event w �s a ®®®®®®®®®®• i • • Phos- __Rhorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im cnment for knowing violations". Cam" Al 07W ;wro Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION'- .. "LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: cb- f& )lea- rfa Land Owner: CCnferkeo�- g15D Operator: t�ejiil.6rn,10)ujgZ[. Crop 1 Name: `a IZ&KX&Z WQ Permit #: V3gC,pi(2%4 5 Field #: HIP Acres Utilized: Annual Dry Tons Applied: Z. 357 Site #: D Acres Permitted: Predominant Soil Series: A ICL6 C� Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 72 Crop 2 Name: Crop 2 Max. PAN: 2�4�8 4.5 ° a) r. ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons oho Solids Volume A lred er PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist)inches Precip. Past 24 Hrs. y 410 o 0 0' a '• 0 C o 7y - w .. ; = * � o 0 po r P, ., � * �• TKN mg/kg Z o El o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 -I Nei 3eobb 16A ,) I ►-1 W--) Afu 0 S 3' 5 0.30 PCs b 5.cro 7 ::': .'Y1 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS:F Annual lbs/acre0,004 Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R. * * * * Permit PAN Limit lst/2 nd Crop LLT As Cd Cu Cr Pb I Hg Mo Ni Se Zn P 7 0,CO2 , Qq 0.0y p CUg I , I U 2 l lql; o,v5s O�2 .45,0E Z-I1B 0.033 0.1,14 IZ O.L100 'l '> Z(oZ tl 71 �5, 53 Z2 33 O • IaZZ- 53� 64D`d i S130 :....:`. `'........ . . ...............:::.::::::: : 3 (v U 1 ' 7 15 ..: i Lime Date A lied lbs/ac KfCS-Gi Z/G2`�Jhn 1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informat!A iNluding the possibility of fines and imprisonment for knowing violations." ,W6 ,/ �7��Q•b *Application Method: S - Surface, IN - Injection, INC - Incorporation 100, ��9� ^f **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant LoadinLy Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Ccn fen. n-eam67 Total Dry Tons Applied (Annual): Permit #: Cation Exchange Capacity (non 503 only): rator: Owner: ��[{ ' (� Predominant So Acres Used: �, Cry Acres Permitted: 7,C �eg Site #: Z 357 W5 it Series: /-}�QCpQ Field #: 1(0 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 4X 2 3 4 5 6 7 8 9 10 11 12 % Solids 1. A Arsenic <Z,,5 Cadmium 1 - Q Copper �71 Chromium Z3 Lead ,Z,5 Mercury 0, L,5 Molyb- demim Nickel 15 Selenium C5.0 Zinc 7z 1 Total Phos- zs IUL ial Heavy Metal Field Loadings (Calculated in lbs/acre): Total IN a E NEINEE App. Event R! MOO r • __®_®®__®_®®_®_®®• M0 RIM ®®®®®®®® Ir •.' r ITT ® Y ®®®®®®®®®®®• , ' ® ®®®®®®®®®®®® P, "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im mment for knowing violations". (�;A7 4 �(/ 4; � -4 w 11 Signature of Land Applier 79 Baas Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION I ...,,,D SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: &f) I.er�he -map WQ permit #: "COOINq Field #: I-) Acres Utilized: 3-(,02 Land Owner: (rJ- 491vre)-K-& Annual Dry Tons Applied: S C� Z43 Site #: V Acres Permitted: 3, 4"z Operator: n�" I,l'Nfl. 6rilW1Jialy , Predominant Soil Series: A lgaQ, Cation Exchange Capacity (non 503): 4-15 Crop 1 Name: CnQ6iQ1-t30n- _dCL Crop 1 Max. PAN: 1'72 Crop 2 Name: Crop 2 Max. PAN: ° a� >~ ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist Precip. Past 24 Hrs. inches > K b �' o� w C o �; - * 4 7y CD ?j * w * o' TKN mg/kg Z �� iX o °� 0 �. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual g Application Crop 1 Crop 2 Crop 1 Crop 2 00Dv 1.5A 1.0�65 Ha-WWT) mcii�+ O S 0-5 0.30 40SPv Q55 6AC5.q(- J • O ' 5 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 6000O .::::::.:.:.:.:: As Cd Cu Cr Pb Hg Mo Ni Se Zn P tU2.c5 Lime Applied Annual lbs/acre 025 0,062 , 0056 5 P Date lbs/ac Years Cumulative lbs/ac '' '' ''''Prior iD I ZC3 0.64U O* Z l 3_ Zu5 ' . 3Z2 , LQ(, 7.G i5 i . cio Z A 4-) p . Q45 , S32 3. 2-2q 0.5 u ► r q ::::?:::::: `::.:.:.>:.:.:. »: ZIv7 i - ,3 U i $ 3 ............................................................................................. Z Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." w A *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Iniection/Incornoration - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Cn'l+ff4neCL m5p Total Dry Tons Applied (Annual): 13,CjZg Permit #: ;� pool CA; Cation Exchange Capacity (non 503 only): 4 5 rator: (y b{� �j((). �nj� J� i. Owner: Predominant Soil Series: Acres Used: �. (o"Z Acres Permitted: _toz Site #: Field #: 1 j Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite DateZr I 1 2 3 4 5 6 7 8 9 10 Li12 % Solids Arsenic < 2,6 Cadmium 1.Q Copper --) I Chromium 3 Lead 2 J Mercury Molyb- Nickel I Selenium Zinc 11) Z J Total Phos- zs 3 j A [al Heavy Metal Field Loadings (Calculated in lbs/acre): Total I 1 I L2]3 4 5 6 7 8 9 10 11 12 DT/Ac./ rt App. n Event o,5 7 Arsenic , 5 I I 16.006 Cadmium p , COZ Copper -d 13. ka Chromium , 05 D Lead , CGSu 6, C6LJ Mercury • bO { 1 Molyb- - C>,Oil O.Ot 1 Nickel ©• 3 1 1 0.633 Selenium p, b { I O+OI J Zincly� Total Phos- horus �Z.GYj "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im mment for knowing violations". Signature of Land Applier 40, Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION i —LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: ©n lF to lYl WQ Permit #: wq (50C t0(48 Field #: I q Acres Utilized: Land Owner: U'n ii°ll l /Yi(Z✓ Annual Dry Tons Applied: Cj, Zc, (, Site #: C-r�q�411 Acres Permitted: Operator: O)DA e5m, 6MiW-%,-kCL T. Predominant Soil Series: A hAa— Cation Exchange Capacity (non 503): C.�. Crop 1 Name: CCCZQl-jf- Crop 1 Max. PAN: jI 2 Crop 2 Name: Crop 2 Max. PAN: ° N Q Volume applied (enter on Solids/ Liquid Cu. Yds Gallons % Solids Volume A hed er PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist Precip. Past 24 Hrs. inches > b �' o� w C o iz w �. * 4 7d R w •, =' w R TKN mg/kg Z �F o El aq 0 w. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 , - i 51-1-)c9 1.5A Q, (Z 14 5 rnO15+ 0 5 C) ,'5 p , 5 >-6D v 4 bD I Rio 5q4 3 rz.bg (.o Cj., 7C Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 114=1.......: As Cd Cu Cr Pb Hiz Mo Ni Se Zn P so X Lime Applied Annual lbs/acre 6, DO I p , pU Z . 4Zct O. L3 4 0 ,1�4� Old v CX O. 023 O: UU$ 1.14 2"; 3 55 ;>:::.:::.:. Date lbs/ac Prior Years Cumulative lbs/ac 5 2 Q , coi p, n 4 D . C� C� -60 3 b ©v ®..GYM . abb 4 0.:::::::::: ::::::::::::: : , oo U (D • d)3 .603 , ok5 o . Cf3 6 -Y oo p , p 12 - , O3 Z . U1-L 1. a Z :: :::::: :::: »>:: »::::: ::.:.................. :::::::::. LA 1 Z 7 ► � — .................. 7U G yq Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop --f certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informationAc!0ing the possibility of fines and imprisonment for knowing violations." A a � *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Iniection/Incornoration - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: C(y)ttj-)4offi_ (Y),-17 Total Dry Tons Applied (Annual): ry.7!i, v Permit #: e�Cool 04'? Cation Exchange Capacity (non 503 only): Lt. 5 rator: Lf�l��m �p�y# � 7i t. Owner: Predominant Soil Series: (Qaa� Acres Used: 1.75 Acres Permitted: Site #: C=TiaC+j. Field #: IGj Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 42q-1G 121 jf- cae, 3 • Zc,_/Q 4 5 6 7 8 9 10 11 12 % Solids �_ 7`IO 1,611) 1.67b Arsenic , 5 < Z . 5 < Z.,5 Cadmium 1.0 1.0 i , 6) Copper Z7 I Z? 1 271 Chromium Z 3 Z 3 Lead 2-3 Z5 Z 5 Z`j Mercury C}•Z5 C),ZS Molyb- denum C60 <�5,b <6,o Nickel 1,5 15 151 Selenium <!�. o < 6. D < 6.0 Zinc 7 Z J 'i 21 ' Total Phos- as 331�& 331lO 331Ib tal Heavy Metal Field Loadings (Calculated in lbs/acre): App. Event r r ... ®.. .. • 1 • • L 1 ______®®_ • r W6 ma, "66 6 An _ . • . • � r r6W Mom • ► ®®___®®®® Total Phos- _phorusIMMMENEEMENEEN.1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and im mment for knowing violations". ��4 i6�_ Signature of Land Applier Date DENR FORM MFLSF (12/2006) PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: C(Y)4er)4irlf;P- WQ Permit Number: L)2�aao104S WWTP Name: ObniNPDES Number: M_M-&W-0 Monitoring Period: From -bounty i,?. P To TpeCPM% 31,Zolgi 'athogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) [I Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens ❑ ............ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion (� Anaerobic Di estion g .................................................. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- Frequency of Analysis Sample 'type Analytical Tech- Minim Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN < 11-j 1 1-7 < 1 Z1 C P� Clf b(3u�5 Q -7 C f� g2Z1 E-� CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." rto l e�ftl.,St"Ia—Ti . / c r rI. 401 CCACAdr— Prep r ame and Title (type or print) u.r,aature of Preparer* Date Cl�, i��• �mi�i�ic��%/nnd � a+rro6l.cXZG Land Applier Name and Title (i applicable)(type or print) 6" / .-;2-A-Ahad Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Enw,un[ME&M Flo himpumbd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Sample Analysis Method PARAMETERS #1 Date Analyst Code Total Residue, mg/1 14940 04/23/19 JTH 2540E-11 Fecal Coliform (MPN), /gram Solids < 121 04/22/19 JTH 9221E-06 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/22/19 DATE REPORTED : 04/25/19 REVIEWED BY: EAUT&MBM Flo MoTpumho GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPN), /gram Solids Sample Analysis Method #2 Date Analyst Code 15360 04/23/19 KDS 2540B-11 < 117 04/23/19 KDS 9221E-06 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/23/19 DATE REPORTED : 04/25/19 REVIEWED BY: EIMAnNE&M % hwPuMNA ■ 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Sample Analysis Method PARAMETERS #3 Date Analyst Code Total Residue, mg/l 15940 04/24/19 JTH 2540B-11 Fecal Coliform (MPH /gram Solids < 113 04/24/19 JTH 9221E-06 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/24/19 DATE REPORTED : 04/26/19 REVIEWED BY: Enwkwn[d % hwTP@T@%4 114 OAKMONT DRIVE PHONE (252) 756-6208 FAX (252) 756-0633 GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPH /gram Solids Sample Analysis Method #4 Date Analyst Code 16020 04/29/19 JTH 2540B-11 <113 04/29/19 JTH 9221E-06 ID#: 416 A DATE COLLECTED: 04/29/19 DATE REPORTED : 04/30/19 REVIEWED BY: oo oflnbM % hwPoTOW 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/I Fecal Coliform (MPH /gram Solids Sample Analysis Method ##5 Date Analyst Code 15420 04/30/19 KDS 254OB-11 <117 04/30/19 JTH 9221E-06 ID#: 416 A DATE COLLECTED: 04/30/19 DATE REPORTED : 05/02/19 REVIEWED BY: Mwkwn(M Flo hmpumW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPH /gram Solids Sample Analysis Method #6 Date Analyst Code 15500 05/02/19 JTH 2540B-11 <116 05/01/19 KDS 9221E-06 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 05/01/19 DATE REPORTED : 05/06/19 REVIEWED BY: Eflw'unflmid Flo hmpumW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/1 Fecal Coliform (MP1), /gram Solids Sample Analysis Method #7 Date Analyst Code 14980 05/06/19 JMH 2540B-11 <120 05/06/19 JMH 9221E-06 FAX (252) 756-6633 ID#: 416 A DATE COLLECTED: 05/06/19 DATE REPORTED : 05/08/19 REVIEWED BY: Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 7. 7. 7 7. 22 14-22-19/1310 1 7.54 7.49 7.43 7.2 7.1 70 6_9 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 4-22-19/1315 Windy Sammond 1.58 23 0.07 8.1 0.98 Dry Solids grees Celsius arees Celsius 4.37 mg Oxygen/hr 0.28 mg Oxygen/hr/g 23 degrees Celsius 0.86 Temperature Corrected Specific Oxygen Uptake Rate: 0.24 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 8.4 8.2 8 7.8 a� 7.6 m 7.4 m N 7.2 _N In 7 6.8 6.6 6.4 Oxygen Uptake Rate Chart y ==0.0729 + 8.196 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 11 Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time.- Sampled By: Analysis Date/Time: Analyzed By: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 8.23 8.19 8.14 8.09 8.03 7.97 7.96 7.87 7.84 7.75 7.71 7.64 7.57 7.49 7.42 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: CMSD W00001048 4/24/2019 22 4-24-19/1245 Andrew Edwards 4-24-19/1258 Windy Sammond 1.62 % 22 dE 22 dE 0.06 8.3 0.99 Dry Solids agrees Celsius. agrees Celsius 3.32 mg Oxygen/hr 0.20 mg Oxygen/hr/g 22 degrees Celsius 0.91 Temperature Corrected Specific Oxygen Uptake Rate: 0.19 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 FW Oxygen Uptake Rate Chart 8.4 8.2 8 7.8 7.2 7 I y =-0.0553� + 8.353 I� 6.8 ' ! 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name. C Biosolids Permit Number: V Date: Digester Temperature: Sampling Date/Time: 4 Sampled By: A Analysis Date/Time: 4 Analyzed By: V Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 8.08 8.08 7.97 7.94 7.91 7.9 7.84 7.81 7.77 7.71 7.63 7.4 7. 73 72 Slope: I ntercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 3D 0001048 -25-19/1350 ndrew Edwards indy Sammond 1.63 % Dry Solids 24 degrees Celsius 24 dearees Celsius 0.05 8.1 0.99 3.24 mg Oxygen/hr 0.20 mg Oxygen/hr/g 24 degrees Celsius 0.82 Temperature Corrected Specific Oxygen Uptake Ratej 0.16 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 E: A 8 7.8 0 E 7.6 x O 7.4 0 N N 0 7.2 7 Oxygen Uptake Rate Chart , -0.05 x+8.18 I i I I I j i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 8.86 8.75 8.74 8.7 8.61 8.52 8.46 8.37 8.31 8.26 8.2 d02 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: CMSD WQ0001048 5/1/2019 24 5-1-19/1350 Andrew Edwards 5-1-19/1400 Windy Sammond 1.6 23 22 % Dry Solids degrees Celsius degrees Celsius 3.50 mg Oxygen/hr 0.22 mg Oxygen/hr/g 23 degrees Celsius 0.86 Temperature Corrected Specific Oxygen Uptake Rate: 0.19 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 9 8.8 8.6 8.4 0 7.8 7.6 7.4 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name. CMSD Biosolids Permit Number: WQ0001048 Date: 5/2/2019 Digester Temperature: 25 Sampling Date/Time: 5-2-19/1325 Sampled By: Andrew Edwards Analysis Date/Time: 5-2-19/1333 Analyzed By: Windy Sammond Total Solids: 1.58 % Dry Solids Beginning Temperature: 23 degrees Celsius End Temperature: 22 degrees Celsius Dissolved Oxygen Level 8.42 8.42 8.41 8.41 8.37 8.35 8.32 8.29 8.28 8.25 8.23 8.22 8.2 8.19 8.18 8.16 Slope: I ntercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.02 8.4 0.99 1.16 mg Oxygen/hr 0.07 mg Oxygen/hr/g 23 degrees Celsius 0.86 Temperature Corrected Specific Oxygen Uptake Rate:1 0.06 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 8.5 8.45 8.4 8.35 8.3 a� a� a "'8.25 o N 8.2 N_ 8.15 8.1 8.05 8 Oxygen Uptake Rate Chart t y =-0.0194 + 8.458 J � I 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 8.2 8.2 8.2 8.2 8.2 8.22 8.22 8.21 8.19 8.17 8.16 8. 33 8.11 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 5/8/2019 25 5-8-19/1405 Andrew Edwards Sammond 1.54 % Dry Solids 24 degrees Celsius 23 dearees Celsius 0.01 8.3 0.89 0.58 mg Oxygen/hr 0.04 mg Oxygen/hr/g 24 degrees Celsius 0.82 Temperature Corrected Specific Oxygen Uptake Rate: 0.03 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 8.25 -- 8.2 E 08.15 0 8.1 8.05 8 Oxygen Uptake Rate Chart _-0.0097 + 8.282 I i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 8. 8. 8.3 8.3 C:7 8.32 8.31 8.29 8.27 8.24 8.22 8.19 8.16 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Andrew Edwards 5-9-19/1325 Windv Sammond 53 % Dry Solids 25 degrees Celsius 24 degrees Celsius 0.02 8.4 0.99 0.96 mg Oxygen/hr 0.06 mg Oxygen/hr/g 25 degrees Celsius 0.78 Temperature Corrected Specific Oxygen Uptake Ratel mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 8.35 M:lC3 a) E ,m8.25 a x O (D 8.2 0 U) �8.15 :M 8 Oxygen Uptake Rate Chart I i y -0.016 + 8.435 I i j 1 I 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Time (minutes) GROUNDWATER MONITORING LAB REPORTS GW-59A COMPLIANCE REPORT FORM Permit # U-)q0 0 (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. Will this monitoring report (GIN-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES N,ItQ IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. Y 4 Are any monitored constituents equal to or above the established standards? YV NO If the answer to question 4 is "NO'; skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: ( I #c) -T i O, i CJrrLj 1 �- t vPJ I �ILA (�1 I * 16 �rc�mi urn I to Lq) CCPP o 5 For the constituents identified in question 4 above, have standards been exceeded previously for the in the last two YES. NO same constituent(s) in the same well(s) years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported; and sample collection date for each occurrence (for the last two years).. loe)I+ Z 7,2-1; -To.(, IZ•Iur -q>' l tJ21I #tO Z2Z-.Q Clirtxf)fL'M iL4Uq/� l I4CinfC1T)%L M 65 1 "� I tvuq 1 t -rp C (' z , ru4-'q,� i, le--r--��r) C.11tOrniU 2-7R-I Ib-lt-I� i lt�gl� 1�.Drom �L Z-ZO-1 Ct-NVCM �M I ,Q, 18 Ztht4 TC1C F7 b(, ZD-l4 Cn(CM° I(Qct l i L -L �I � (r)(pni4m 9UU 6 Are the monitoring wells listed in section 5 located at or beyond. the review boundary? YES 1 If the answer is "YES" a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO'; monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 1�ttrif) Vtt era rnP i�-I`or c api ' ampGn a ,l:xxile!(I,�+�dhav r i r t (y 4-0d e f feel � et tat pr a^� a Qa�al u�cri as �;u:o� S �nc1.�2ar c�rktnS i�iJ h eme g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided of the top of the current GW-59 form. eg Wa_5bo9Avejalisr�tfro�.mationsear aiedand�e�nyfoFtitatc�n`b"mei tttl�thi a andcomp to o: hebest o mk�r owteoge� rehb(yconotlea pCrtkphoatrtytGeh_ oE Lnpj Slgndiure of Permittee (or Authorized Agent) Gate GW-59A 12/8/2003 SUBMIT FORM ON DW PAPER ONLY GROU�­ATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: L0 Permit Name (if different): Facility Address: qM County l' yl (Sla le) j2ip) Contact Person: Telephone#: �PP�t's1 Well Location/Site Name :\ 715� No, of wells to be sampled: Cp PERMIT Number: Expiration Date: 6I W'�X_ Non -Discharge UIC NPDESOther TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑,/Remediation: El Rotary Distributor S Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Date sample collected: Well Depth: ft. Well Diameter: Z in. Depth to Water Level B2546: ft. below measuring point Screened Interval: _aft. to Q ft. Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: gallons Samples for metals were collected unfiltered: r.YES ❑ NO and field acidified: X YES ❑ NO FIELD ANALYSES: pH 00400:units Temp. 000lo: 13 °C Spec. Cond. 00094: C/�i 3 µ Odor 00085: nc Appearance (� 1r If WELL WAS DRY at time ofMhos sampling, check here: ❑ LABORATORY INFORMATION Date sample analyzed: Z-1 IC9 Laboratory Name: EVj COEW)EATl If-f-, Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 C),C)(_o mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) OrthophoSphate 70507 D t C)�) mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 "7 LP mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 4rj units Ba - Barium 01007 ug/L TOC 00680 ) Q, 10 mg/L Ca - Calcium oog16 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 5 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <D. OI() mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 G(C`, �j ELMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia omio O. (p 1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 _ ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): IInfluent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Name and Title'- Please print or type GW-59 Rev.3-1-2016 for Nuulonzeu Agent) luaw) SUBMIT FORM ON AMOW PAPER ONLY GROUNMATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFOR Facility Name: Permit Name (if di Facility Address: (aiaiel Please Print Clearly or Type Contact Person: � fy r ' Telephone#: .Z6Z-62(4_515gU Well Location/Site Name: 6 cW ri eld" No. of wells to be sampled: (D PERMIT Number: Expiration Date: J-� ZQZQ Non -Discharge U40W- 104,0 UIC NPDES IUCCX`�37,n) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): d Date sample collected: 7-JC/-%c/ FIELD ANALYSES: If WELL WAS Well Depth: ft. Well Diameter: --in. pH 00400: 5 J units Temp. 000lo: R_ °C DRY at Depth to Water Level ersas: & Z ft. below measuring point Screened Interval: Z ft. to 9 ft. Spec. Cond. 000sa: Cf.CD µMhos time of Measuring Point is _0 ft. above land surface _ Relative M.P. Elevation: ft. Odor 00085: nwt sampling, Volume of water pumped/bailed before sampling: gallons Appearance OC 069 check here: ❑ Samples for metals were collected unfiltered: � YES El NO and field acidified: [A YES El NO late sample analyzed: Z 19-19 Laboratory Name: -f nyitCflr`Yle-)4 Zj 1M_Certification No. %d ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o5i ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 C ,' D rng/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 Q.ICj mg/L Other (Specify Compounds and Concentration Units): ssolved Solids:Total 70300 L�j mg/L Al -Aluminum 01105 mg/L PH (Lab) 00403 6 1 units Ba - Barium 01007 ug/L TOC 00680 � 4 -qj mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L . Arsenic 01002 ug/L Chromium: Total 01034 J iv ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <O, 0 i Q mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oosas_ mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 �A - ( µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 1 ( mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn -Manganese o1o55 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # UVr rcrtrreurauUrr aysterns umy (.viracn Lao rceports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee(or GW-59 Rev. 3-1-2016 SUBMIT FORM ON JW PAPER ONLY GROU1_.ATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Facility Name: Permit Name (if di Facility Address: A , n, (zip, or Contact Person:Telephone#: Well Location/Site Name: 16 No. of wells to be sampled: PERMIT Number: Expiration Date: /-� [WZ6J Non -Discharge LQtC0I0C4 cS UIC NPDES N4cpmlun Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): f C) Date sample collected: FIELD ANALYSES: WAS, Well Depth: ��j ft. Well Diameter: in. pH ooa00:� units Temp. 000lo: )L4 °C DRY at Depth to Water Level 825a6: 5ft. below measuring point �= g p Screened Interval: (P ft. to j3 ft. Spec. Cond. 000sa: �j� . CJ µ Mhos time of Measuring Point is Z ft. above land surface Relative M.P. Elevation: ft. Odor 00085: n (X)s sampling, check Volume of water pumped/bailed before sampling: 5 gallons Appearance CIW 69 here: ❑ Samples for metals were collected unfiltered: YES El �/ NO and field acidified: L]9 YES ❑ NO Date sample analyzed: n q— q Laboratory Name: Z IlV 1 (( ff—a) ' J: ( r - Certification No. j PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 Z /100mL Nitrate (NO3) as N 00620 0, 'Z_ mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 315o4 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) hoS Ortho p phate 70507 mg/L Other (Specify Compounds and Concentration Units): dissolved Solids:Total 70300 4b mg/L AI - Aluminum oil o5 mg/L pH (Lab) 00403 j . "j units Ba - Barium 01007 ug/L TOC 000sa L� • %T� mg/L Ca - Calcium oog16 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 Z� ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 Q. O"T7 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 Si . µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 Q ,O LP mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn. - Manganese o1o55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% rermmee for Autnonzea Agent) Name and I Itle - Please print or type GW-59 Rev.3-1-2016 of Permittee (or Authorized Agent) SUBMIT FORM ON )W PAPER ONLY GROUImuvvATER QUALITY MONITORING: COMPLIANCE REPORT FORM NFORMATION Facility Name: Permit Name (if di Facility Address: Crime (City) Please Print Clearly or (Slate) (Zip) act Person: �(�f�'Q,�(�]y D l Telephone#: -M-Z_5zq--!5 qC4 Location/Site Name: j n+&act 0(2 IgP 'f',6P,_IG j O No. of wells to be sampled: Cv ERMIT Number: Expiration Date: f-Ll_/oZID on -Discharge i,_Qc C0D1OQ'5? UIC PDES jQ_ t'_03715)-) Other YPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: EJ Rotary Distributor NrLand Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): j 'rj Date sample collected: Z Iq-I Cj Well Depth: 19 ft. Well Diameter: Z in. Depth to Water Level 825a6: p �, 5 ft. below measuring point Screened Interval: ?eft. to ft. Measuring Point is 2.above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: EYES ❑ NO and field acidified: [2(YES ❑ NO FIELD ANALYSES: pH 00400:11�._L units Temp. 000lo: I °C Spec. Cond. 000sa: S; µMhos Odor 00085: f7 On Appearance eal( If WELL WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: Z--Igp jqI Laboratory Name: uj (On g �) f`G Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1051 ug/L Coliform: MF Fecal 31616 21 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P o0665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 n , o3 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 5,?, units Ba - Barium 01007 ug/L TOC omm Cj.ZU mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 uglL Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <&C)10 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0 . mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): I Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% �l %` )m W) LQ(-d &P 1 0:�4, a1 C12� Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON OW PAPER ONLY GROUlimuvv'ATER QUALITY MONITORING: COMPLIANCE REPORT FORM ACILITY Facility Name: Permit Name (if different): Facility Address: oc - C,V �-4tr Print Clearly or Type County (City) (Slate) (Zip) Contact Person: Telephone#:z ��t i-�J ✓�u Well Location/Site Name: L'Q(ne sie(o n No. of wells to be sampled: PERMIT Number: Expiration Date: 1_31_ZpZC) Non -Discharge lccm UIC NPDES HGDO376-) ) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): )1-] Date sample collected: _19 /n Well Depth: 15? ft. Well Diameter: Z. in. Depth to Water Level 825a6: P 4 5 ft. below measuring point Screened Interval: z ft. to ft. Measuring Point is Z.33 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: gallons Samples for metals were collected. unfiltered: [?YES ❑ NO and field acidified: N YES ❑ NO FIELD ANALYSES: pH ooaoo: 5.0 units Temp. 000lo: 13 °C Spec. Cond. 000sa: Co / I j µ Mhos Odor 00085: nC.-J-) Appearance L'�( If WELL WAS DRY. at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: Z / �'{—) �j Laboratory Name: n\ji (-Cn ffl�� S�� (�• Certification No. J PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 1) mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 ©.)0 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 (,4 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 004o3 5. (� units Ba - Barium 01007 ug/L TOC 00680 �.Z� mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 1 D ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 (9 I. C4 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 �: mg/L Mg - Magnesium o0927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev. 3-1-2016 nt or type of Permiftee (or Authorized Agent) (Date) SUBMIT FORM O PAPER ONLY GROUNT"if1/ATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: }, Permit Name (if different): �_ mJ_ I Facility Address: QU) (,L)1 1'Pn (r).V! j��1 County (Slate) (zip) Contact Person::T)enef &—gtq-n Telephone#: z6Z sZy1 Well Location/Site Name: uj &.� R (16 4r I_--5 No. of wells to be sampled: PERMIT Number: Expiration Date: / —LJ W Z0 _ Non -Discharge UIC _ NPDES Other _ TYPE OF PERMITTED OPERATION BEING MONITORED _ ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge P ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): 119 Date sample collected: FIELD ANALYSES: WAS Well Depth: ! ft. Well Diameter: Z. in. pH 00000: 4. (D units Temp. 000lo: 13 °C DRY at Depth to Water Level 62646: ft. below measuring point Screened Interval eft. to / b ft. Spec. Cond. 000sa- µMhos time of Measuring Point is Z_ft. above land surface Relative M.P. Elevation: ft. Odor oo085: sampling, check Volume of water pumped/bailed before sampling: gallons Appearance Gear here: ❑ Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: [V YES ❑ NO LABORATORY INFORMATION Date sample analyzed: z �� �� Laboratory Name: Env) rOn1y)&)+'S) I Certification No. 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 i /100mL Nitrate (NO3) as N 00620 �U_�jC ` mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 1100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 < C).C)mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 12C) mg/L AI -Aluminum oilo5 mg/L pH (Lab) 00403 4. Ce units Ba - Barium 01007 ug/L TOC 00660 15. mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 5 Lj ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 C®= O10 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg -Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 j (�� µMhos K - Potassium 00937 mg/L VOC 7873 , method # Total Ammonia oo6lo (-j, 10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH,as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # t-or rtemeatation systems Unly (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% �e �n� Lar)1 Ate) t � i crm G2L Permittee (or Authorized Agent) Name and Title - Plea a print or type Sign GW-59 Rev.3-1-2016 Agent) (Date) 9 E1Mw'UT@1Efl&10 alp howp(mbd wa�tewat�r xarTio � OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS ID#: 416 DATE COLLECTED: 02/19/19 DATE REPORTED : 03/04/19 REVIEWED BY: Well #9 Well #10 Well #14 Well #15 Well #17 Analysis Method Date Analyst Code Fecal Coliform (MF), /100 Mls < 1 < 1 2 2 1 02/19/19 JMH 9222D-06 Ammonia Nitrogen as N, mg/l 0.61 0.08 0.06 0.19 0.07 02/20/19 TLH 350.1 R2-93 Nitrate Nitrogen as N, mg/1 0.06 0.80 0.82 0.82 0.11 02/20/19 BLD 353.2 R2-93 Total Organic Carbon, mg/l 10.10 4.93 4.03 9.24 5.21 02/28/19 SEJ 531OC-11 T-fal Dissolved Residue, mg/l 76 43 40 72 64 02/21/19 TBG 2540C-11 iI Chromium, ug/l <5.0 16 26 7 10 02/21/19 LFJ EPA200.7 i,opper, ug/l < 10 < 10 77 < 10 < 10 02/21/19 LFJ EPA200.7 Conductivity (at 25c), uMhos/cm 94.3 69.0 57.9 86.2 61.4 02/25/19 JMH 251OB-11 Total Ortho-Phosphate as P, mg/l 0.09 0.19 0.26 0.03 0.18 02/20/19 KDS 450OPE-11 EMIAnIMEW % hCOTPOTEW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Fecal Coliform (M[F), /100 Mls Ammonia Nitrogen as N, mg/l Nitrate Nitrogen as N, mg/l Total Organic Carbon, mg/l " ' it Dissolved Residue, mg/l it Chromium, ug/l Copper, ug/l Conductivity (at 25c), uMhos/cm Total Ortho-Phosphate as P, mg/l Well ##18 Analysis Method Date Analyst Code < 1 02/19/19 JMH 9222D-06 0.10 02/20/19 TLH 350.1 R2-93 < 0.04 02/20/19 BLD 353.2 R2-93 5.53 02/28/19 SEJ 531OC-11 120 02/21/19 TBG 2540C-11 <5.0 02/21/19 LFJ EPA200.7 <10 02/21/19 LFJ EPA200.7 163 02/25/19 JMH 251OB-11 < 0.01 02/20/19 KDS 450OPE-11 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 02/19/19 DATE REPORTED : 03/04/19 REVIEWED BY: GW-59A COMPLIANCE REPORT FORM Permit # ic(4s (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( - -I ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established. due date? 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question .1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Of ce for guidance. X 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is 'NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the I YES I NO ii same constituent(s) the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions. required by the Division involving this YES NO groundwater quality problem? ' If the answer to question 7 is "YES, describe those actions in the space provided below. If the answer to question 7 is "NO', contact the Regional Office within 90 days; an evaluation may be —4 rmmnliAnt fines and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit d form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. Pwr a� e�e�' ac°k owle�d' et at the above mfo matoii}w s'eVal�uate ndtt-eoatiorisubm�tted �n thin _-- Ven�nr>_G`oe�.tc.+ , p�anrl.:co"�mn1 {e to he es Qftm s�k11Q Ied9e. Signature of Permittee (or Authorized Agent) ,7- 31 Date GW-59A 12/8/2003 SUBMIT FORM ONAMLOW PAPER ONLY IGROURMATER QUALITY MONITORING: COMPLIANCE REPORT FORM ILI I Y INFORMATION Please Print Clearly or Type lity Name: ©nib­f�lf _ t^(i"-z nit Name (if different); ` en1 nda_ n_),)AD litynAddress: GHQb_)i 01�jO4LL -7 1�I-l�.l r,� IStreetf �C_ Z( TlJ t D53U County (Cilyf f5�ale1 i7-ii>, Contact Person: Telephone#: z5Z-5ZL4-Fj5<&L4 Well Location/Site Name:. &�tjj CD� p(prr� No. of wells to be sampled: PERMIT Number: Expiration Date: )-3j-ZDZU Non -Discharge jj =D1047, UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: ...I ­_ 1—r Mwlj, I tury WELL ID NUMBER (from Permit): G Date sample collected: (,-)-►�j FIELD ANALYSES: If WELL WAS Well Depth: g ft. Well Diameter: Z in. pH 00400:4_q units Temp. 000lo: z °C DRY at Depth to Water Level 82546: 3`�► ft. below measuring point Screened Interval: 3 ft. to g ft. Spec. Cond. 000sa: (a 5 C.� µMhos time ofsampling, Measuring Point is %. �j ft. above land surface Relative M.P. Elevation: ft. Odor 000ss: check Volume of water pumped/bailed before sampling: ,j gallons Samples Appearance here:❑ for metals were collected unfiltered: U YES ❑ NO and field acidified: M YES ❑ NO Date sample analyzed: 1_'-I I -ICI Laboratory Name: E.ny l (Qf-)ma* Z, f Certification No. 10_ PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. _ COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 ' /100mL Nitrate (NO3) as N 00620 C). 6 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 0. mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 t4 Lo mg/L AI - Aluminum oil o5 mg/L pH (Lab) 00403 L) .Cj units Ba - Barium 01007 ug/L TOC 00680 �•� Z mg/L Ca - Calcium oo91s mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 < 5. O ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 jQ mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 000ss l�. (tMhos K - Potassium 00937 mg/L VOC 7673 method # Total Ammonia ooslo C.CC mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total) Mn -Manganese 01055 lJg/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # r•or mememation systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% ittee (or Authorized Agent) kiame and Title - PI a e print or type GW-59 Rev.3-1-2016 of Permiftee (or %-t3)4:� (Date) SUBMIT FORM ON' W PAPER ONLY all'i W GROUNuvvATER QUALITY MONITORING: SUN=an- COMPLIANCE REPORT FORM 1 sa FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: j-�►- /�7_( Facility Name: 7() c4 Jtp_ 1 7 ,e )Di Non -Discharge OCC-3t )(JI's UIC Permit Name (if different): n i en �_ rii�l NPDES PtM5_Z(5_P Other Facility Address: qca U-),) � Qovjn�) (-j) TYPE OF PERMITTED OPERATION BEING MONITORED Catr-IWCn istreelj t4l_ i(( 1D 530 Count y _:�10--}- ❑Lagoon ❑Remediation: Infiltration Gallery (Cilyj - (SI.I.) (zip) / I ❑ Spray Field ❑ Remediation: Contact Person: 2Pnep-6 1`iy) Telephone#: ❑ Rotary Distributor 9 Land Application of Sludge Well Location/Site Name: 6 (-,� Fi P_1 d # U No. of wells to be sampled:- ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER from Permit): ( ) �(� Date sample collected: (0-1 I�I Well Depth: P � ft. Well Diameter: Z in. Depth to Water Level s2sas: z- ft- below measuring point Screened Interval: Z ft. to ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Volume of water before sampling: pumped/bailed p g: gallons Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: N YES ❑ NO FIELD ANALYSES: pH ooaoo:�� units Temp. o0010: � �C Spec. Cond. 00094: 5 .0 µMhos -Odor 000e5: none- Appearance CI.�Q'� If WELL WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: Laboratory Name: nyi fQnrnb-)-( ZI rc Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00565 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 Q. Quo mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 4. q units Ba - Barium 01007 ug/L TOC omm mg/L Ca - Calcium oo916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 uglL Arsenic 01002 ug/L Chromium: Total 01034 C) ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <Q, QIO mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 5,5 .c) )LMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia omio <C)-c-)4 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen. Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% �jgn� m ) Lanq Dvp1-I (t�- W ay_(_ Pemmittee (or Authorized Agent) Name and Title -. Ple se print or type GW-59 Rev.3-1-2016 SUBMIT FORM ON )W PAPER ONLY GROW ATER QUALITY MONITORING: COMPLIANCE REPORT FORM T� Facility Name: Permit Name (if di Facility Address: (Jt.M) Please Print Clearly or Type act Person: r It fib '(�-h Telephone#: Z5Z-570- S 4 Location/Site Name: S� O_� No. of wells to be sampled: (o PERMIT Number: Expiration Date: Non -Discharge L)Q oca OL I-3 UIC NPDESOther TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ water Source Heat Pump ❑ Other: o�rvrrr_umu trNrUKMA I IUN If WELL WELL ID NUMBER (from Permit): Date sample collected: (0-1 FIELD ANALYSES: WAS Well Depth: 13 ft. Well Diameter: Z in. pH oosao: q - 6 units Temp. 000io: IC( °C DRY at Depth to Water Level 82546:J.-T5 ft. below measuring point Screened Interval:ft. to 13 ft. Spec. Cond. 000sa: �j, Cj µMhos time of Measuring Point is Z ft. above land surface Relative M.P. Elevation: ft. Odor 000ss: r)QfL sampling, check Volume of water pumped/bailed before sampling: gallons Appearance cjto`( here:❑ Samples for metals were collected unfiltered: M YES ❑ NO and field acidified: D� YES ❑ NO Date sample analyzed: (p—I I-1 GI Laboratory Name: env+ FCn rn01A- _T_) Inc. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NOZ) as N 00615 mg/L Pb - Lead olosi Coliform: MF Fecal 31616 / I /100mL Nitrate (NO.) as N oosao ZCI rng/L Zn - Zinc 01092 Coliform: MF Total 31504 `t /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Certification No. K!) ug/L mg/L Orthophosphate 70507 3. alp mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 mg/L Al -Aluminum oiios mg/L pH (Lab) 00403 Lt, �j units Ba - Barium 01007 ug/L TOC oosao Z.L}Z mg/L Ca - Calcium oosls mg/L Chloride oosao mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 '� ug/L G ,ease and OIIS ooss2 mg/L Cu - Copper 01042 <0.01Q mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 �36.q-I µMhos K - Potassium 00937 mg/L VOC 71373 , method # Total Ammonia oosao <(j.Q�} mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) ug/L Mn - Manganese oioss TKN as N 00625 mg/L Ni - Nickel 01067 ug/L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: D­)a_-Q'�l0-)I (gf IiC ItCt� ittee (or Authorized Agent)Name and THIe -'Please print or type GW-59 Rev.3-1-2016 and that the lat--ratory analytical data lllty of fines and imprisonment for Knc I method # method # method # mg/L VOC Removal% (Date) SUBMIT FORM ON' iW PAPER ONLY GROUNuvvATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Facility Name: Permit Name (if di Facility Address: Contact Person: l} e nee-i`)mJ V-h Telephone#: Z,67-,5Z(45!%4 Well Location/Site Name: i nit�oec i-dZIGIu 1 G 1 O No. of wells to be sampled: (. PERMIT Number: Expiration Date: 1-31-2670 Non -Discharge U-)QWOtb4 UIC NPDES HC,0 737L5-7 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL WELL ID NUMBER (from Permit): Date sample collected: (,—I)—I c j FIELD ANALYSES: Well Depth: , ft. Well Diameter: Z in. pH 00400::5, ) units Temp. 000lo: Zo 'C Depth to Water Level 62546: ZZ-1 ft. below measuring point Screened Interval: 3 ft. to ft. Spec. Cond. 00094: µMhos Measuring Point is Z-j ft. above land surface Relative M.P. Elevation: ft: Odor 00085: Volume of water pumped/bailed before sampling: 5 gallons Appearance CITY Samples for metals were collected unfiltered: N YES ❑ NO and field acidified: M YES ❑ NO DRY at I time of sampling, here: ❑ ate sample analyzed: to 1)-)G I Laboratory Name: Envl (cn(Ye?I-:r nC• Certification No. IQ kRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo3a5 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 1 C> /100ml- Nitrate (NO3) as N 00620 ©, mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 0.C�(-k mg/L Other (Specify Compounds and Concentration Units): ;solved Solids:Total 70300 �? o mg/L Al - Aluminum o11 os mg/L pH (Lab) 00403 ,�. ` units Ba - Barium oloo7 ug/L TOC o0660 Q. mg/L Ca - Calcium 00916 mg/L - Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 �j ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <Q, Q jo mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) >ecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 , method # Total Ammonia 00610 0 319 1mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn -Manganese oloss ug/L TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # method # method # For. Remediation Systems Only. (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% � nm, Q-) pr-QADD -04C Cn etc_, Permittee (or Authorized Agen Name and Title'- Please print or type GW-59 Rev.3-1-2016 of Permittee (or Authorized Agent) SUBMIT FORM ON )dMDW PAPER ONLY GROUK_ATER QUALITY MONITORING: Iq mum COMPLIANCE REPORT FORM n 9-8 30 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: -P_(�_ m6c Non -Discharge UxPW=4-9 UIC NPDES Other Permit Name (if different): (,Z m�o Facility Address: G l l I e l­V5 —6cv, Lim TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery � (Street] ri m 1-a� �'j-5p County j (city) (Stale) (zip, ❑ Spray Field ❑ Remediation: Contact Person: �Q� �l^[ll Telephone#: Z-�J�-J�U ❑ Rotary Distributor M Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): I �) Date sample collected: FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: 2 in. pH 00400: 4t (o units Temp. 000lo: Zh °C DRY at Depth to Water Level szsas: 4;� ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 0009a: 3g• G µMhos time ofsampling, Measuring Point is Z 33 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: ncnt, check Volume of water sampling: before pumped/bailed um P P p g: gallons Appearance cJ�l( _ here: ❑ Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: [X YES El NO LABORATORY INFORMATION Date sample analyzed: (o—I �-I� Laboratory Name: e[yror)rner )+_T, I Irc• Certification No.�_ PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly.turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 Q-) mg/L Al -Aluminum o11os mg/L pH (Lab) 00403 4 • w units Ba - Barium 01007 ug/L TOC D0680 mg/L Ca - Calcium oo916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 < ).C)o mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 'S.q µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 CQ -CA mg/L Mg - Magnesium oo927 mg/L method # (Ammonia Nitrogen: NH3 as N; Ammonla Nitrogen, Total) Mn - Manganese oloss ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% of Permittee (or Authorized Agent) GW-59 Rev.3-1-2016 SUBMIT FORM ON �W PAPER ONLY GROUNLjvvATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if di Facility Address: (Stale) (zip) or Contact Person: Telephone#: Z6Z-'5ZCJ-6% Well Location/Site Name: No. of wells to be sampled: PERMIT Number: Expiration Date: I-I—LDII` Non -Discharge I,_x,` WID049 UIC NPDES N( 3,2LM Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): g Date sample collected: (Q) I-1�I FIELD ANALYSES: WAS Well Depth: lC) ft. Well Diameter: z in. pH ooaoo:$.rj units Temp. 00010: 19 'C DRY attime of Depth to Water Level 82546: ft. below measuringpoint P Screened Interval: ft. to 1 ft. 5 Q Sec. Cond. o009a: P 9� µMhos sampling,. Measuring Point is Z ft. above land surface Relative M.P. Elevation: ft. Odor 00065: norm' check Volume of water pumped/bailed before sampling: 5 gallons Appearance 0 ffA Ilr here:❑ Samples for metals were collected unfiltered: 09 YES ❑ NO and field acidified: N YES ❑ NO ------------- Date sample analyzed: L-) F-IG Laboratory Name: t--nxJI i-cy-v ul T t I OC Certification No. 16 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead most ug/L Coliform: MF Fecal 31616 ? (]� /100mL Nitrate. (NO.) as N 00620 O �j mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use WIN method for highly turbid samples) Orthophosphate 70507 Q. QZ mg/L Other (Specify Compounds and Concentration Units): dissolved Solids:Total 70300 Igs mg/L Al -Aluminum o1105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC oo660 G2. mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 �rj .Q ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 �O,Q mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 1�j µMhos K - Potassium 00937 mg/L VOC 7673 method # Total Ammonia 00610 �j.( mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3as N: Arnmonla Nitrogen, Total) Mn - Manganese o1os5 ug/L - , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% ittee (or Authorized Agent) Name and Title -'Please print or type GW-59 Rev.3-1-2016 of Permittee (or Authorized Agent) MRATmEqW Flo hmpumho OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Fecal Coliform (MF), /100 Ms Ammonia Nitrogen as N, mg/l Nitrate Nitrogen as N, mg/1 Total Organic Carbon, mg/l Total Dissolved Residue, mg/1 ital Chromium, ug/1 copper, ug/l Conductivity (at 25c), uMhos/cm Total Ortho-Phosphate as P, mg/1 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 06/11/19 DATE REPORTED : 07/08/19 REVIEWED BY: Well #9 Well #10 Well #14 Well #15 Well #17 Analysis Method Date Analyst Code < 1 1 4 10 < 1 06/11/19 MAR 9222D-06 0.99 <0.04 <0.04 0.38 <0.04 06/13/19 DTL 350.1 R2-93 0.15 0.55 0.29 0.19 0.48 06/12/19 AKS 353.2 112-93 7.82 3.89 2.42 9.22 1.73 06/13/19 SEJ 531OC-11 46 30 35 126 47 06/13/19 KDS 2540C-11 <5.0 <5.0 7 5 5 06/13/19 LFJ EPA200.7 < 10 < 10 < 10 < 10 < 10 06/13/19 LFJ EPA200.7 65.0 55.0 35.9 137 38.9 06/17/19 JMS 251OB-11 0.07 0.06 0.06 0.04 0.16 06/12/19 KDS 450OPE-11 �ooQ0000� % hCoTpumbd I I-t'1jMr\IVIV IV I VI U V L GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Well #18 Analysis Method PARAMETERS Date Analyst Code Fecal Coliform (W), /100 Mls >600 06/11/19 MAR 9222D-06 Ammonia Nitrogen as N, mg/l <0.04 06/13/19 DTL 350.1 R2-93 Nitrate Nitrogen as N, mg/1 0.05 06/12/19 AKS 353.2 R2-93 Total Organic Carbon, mg/1 7.92 06/13/19 SEJ 531OC-11 "Dtal Dissolved Residue, mg/l 108 06/13/19 KDS 2540C-11 otal Chromium, ug/l <5.0 06/13/19 LFJ EPA200.7 Copper, ug/1 <10 06/13/19 LFJ EPA200.7 Conductivity (at 25c), uMhos/cm 151 06/17/19 JMS 251OB-11 Total Ortho-Phosphate as P, mg/l 0.02 06/12/19 KDS 450OPE-11 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 06/11/19 ]GATE REPORTED : 07/08/19 REVIEWED BY: 'A - EmbbimmW % hCoTpumbd GREENVILLE, N.C. 27858 ID#: 416 Y FAX (252) 756-0633 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN DATE COLLECTED: 06/11/19 P.O. BOX 477 DATE REPORTED : 07/08/19 GRIFTON ,NC 28530 REVIEWED BY: .� Well #10 Well #14 Analysis Method PARAMETERS Date Analyst Code Total Chromium, ug/1 <5.0 <5.0 06/13/19 LFJ EPA200.7 Copper, ug/1 < 10 < 10 06/13/19 LFJ EPA200.7 GW-59A COMPLIANCE REPORT FORM Permit k d (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( i)I ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? x 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing is "Yes", the Regional Office YES NO identification plate, area overgrown, etc.)? If the answer contact for guidance. 4 Are any monitored constituents equal to or above the established standards? YTS NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. u-)204q �Coli �• ) I �/)cowl wel►#►5 �=eca cbo izfm l ►corY• ) �^ well # i� (ec (Cc�Li m Cbl �' adVlocrn �211 #Io a ecal tL>,2 l�(t_.I �(DalCot fM �I 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES '1l4/ NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). ;fcQ I Col i M 7 (�rni fGZLI g oel) 1� SjlGOri (� (l-I�l Iv811#K3 l/iCGm1 well*(4 � bi�i1�/ic-1 ZI�a iiZwp�5 i/) 11 Je) Io*Lj �� e 11 15 [al)OCm I I)ei) 4-0 l/icom I 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES tVQ X If the answer is "YES"' a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO". monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? X If the answer to question 7 is 'YES", describe those actions in the.space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation. fines, and/or penalties. 4000vig�-�eChfcmiuml �j ue i�ve been oldlt C C60-191,J4h ��� rr. p,j a reoult Y��M i alcttecl 4•h-e cN�e.rl CCk4.)n�j 5• [�e c�r� �rIC11�� do txl i eve J-h e-pPcalcc(icbrm elidif)-% ifvht LLe,(I� b� ,P- tt--,1a pl e l�c�etini r�F bfc �r� 2vzv g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. hlfereQj bZockno lw edge tha Vi ove i fo motion was luated'antl theAnfo r dMidnLsub`rF tied i "th s w��,� 4._ 9A)_is� e�and cotnPt�obes my Howled e irep�Compliange.ReportW p Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON )W PAPER ONLY 711AeM O OENFA1kWA__ i 1 0.-.O_... E GROUNDWATER QUALITY MONITORING: o I COMPLIANCE REPORT FORM s c s9 t: a s; B 6n s3o, FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: C(nlenlr_e_CL ft_�f17 Non -Discharge UIC Permit Name (if different): q NPDES NCC©�71j7� Other Facility A/d�dre/s�s/:ICJ j L° n -P 'v U-)-) TYPE OF PERMITTED OPERATION BEING MONITORED (�(11�Ty I E" QC Z�530 County A -1* ❑ Lagoon ❑ Remediation: Infiltration Gallery (City' (siaie' (Zip) ❑ Spray Field ❑ Remediation: Contact Person: Telephone#: 76 5_2q-� V-1 ❑ Rotary Distributor 56 Land Application of Sludge Well Location/Site Name: ,,.)Ljedq=0P,Q()6j_rC No. of wells to be sampled: F ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): G Date sample collected: jQ-jC..j --jq Well Depth: g ft. Well Diameter: Z in. De Depth to Water Level 825a6: p 5, � ft. below measuring point Screened Interval: 3 ft. to � ft. Measuring Point is Z . 5 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: Jr gallons Samples for metals were collected unfiltered: IX] YES ❑ NO and field acidified: YES ❑ NO FIELD ANALYSES: pH 00400:q.--7 units Temp. 000lo: Z3 °C Spec. Cond. 000sa: �(� µ Mhos Odor 000B5: ()Cj-) 'e- Appearance CjeQ r If WELL WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: to-10-ej Laboratory Name: F. n!j 000mcni Z) Certification No.)0 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N o0615 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 i /100mL Nitrate (NO3) as N 00620 GG (2)Q mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 315o4 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC oo68o mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium olo27 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 CO C) mg/L ORGANICS: (by GC, GCIMS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? lLidid Yes (1) ❑ No (0) Specific Conductance 00095 Z30 FtMhos K - Potassium 00937 mg/L VOC 7873 method # (ozoo c - Total Ammonia oo610 j . ­6y mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% u� rcn uuicc tui nuuiuuccu nyci u� GW-59 Rev.3-1-2016 IL:L:IL71 SUBMIT FORM ON' W PAPER ONLY GROUNDWATER QUALITY MONITORING: and I copy to: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: bn+tT)4')e-a ff),0 Permit Name (if different): n+cn 'eL— (nLiD Facility Address: Qoo ()J`I i f r'6 Q j 2PA County W- (Cay) (Statel (ZiP) ! ' Contact Person: J�jo_��j()jl� Telephone#: Z62-,2�-j�S�t Well Location/Site Name: ,-/) o-r P dd *4 No. of wells to be sampled: (o PERMIT Number: Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field El Remediation: ❑ Rotary Distributor di -and Application of Sludge ❑ Water Source Heat Pump ElOther: If WELL WELL ID NUMBER (from Permit): IQ Date sample collected: Id-Iq-ICf Well Depth: ft. Well Diameter: in. Depth to Water Level 8254e: C�) (o ft. below measuring point Screened Interval: ft. to 9 ft. Measuring Point is _3 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: gallons Samples for metals were collected unfiltered: [[] YES ❑ NO and field acidified: [A YES ❑ NO FIELD ANALYSES: pH 00400: U • 8 units Temp. 00010: Z3 °C Spec. Cond. oossa: 4,0. 3 µMhos Odor 000as: 000-e.. Appearance r )oo f— d fajr late sample analyzed: IO- 14-jCj Laboratory Name: FnO f on m ent TIt Ity 'ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead oio51 Coliform: MF Fecal 31616 135 /100mL Nitrate (NO3) as N 00620 O G 5 mg/L Zn - Zinc 01092, Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L Certification No. ) 3 ug/L mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 0,1(.0 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 6tZ mg/L Al -Aluminum o11os mg/L pH (Lab) 004o3 q• 9 units Ba - Barium 01007 ug/L TOC oosao Z •4 Co mg/L Ca - Calcium oos1B mg/L Chloride oosao mg/L Cd - Cadmium olo27 ug/L Arsenic 01002 ug/L Chromium: Total 01034 <-, ug/L DRY at time of sampling, here: ❑ Grease and Oils 00552 mg/L Cu - Copper 01042 Co,Q►0 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? �d Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 , method # A WOC, --I Total Ammonia ooelo C>. I (p mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen. Total) Mn -Manganese oloss ug/L TKN as N 00625 mg/L Ni - Nickel 010e7 ug/L method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% V V V-D'd mev. J- I-ZU 10 SUBMIT FORM ON) W PAPER ONLY GROUNDWATER QUALITY MONITORING: oR o ocEssl COMPLIANCE REPORT FORM S C _ENTER G 19BO -G306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: I-a)-ZO QZ Facility Name: f-en4-nf0'^-- [Y)L- (, Non -Discharge ,��ry Cw(��5 UIC Permit Name (if different): fl 0-Win-ea- Q Mb- NPDES Other Facility Address: _9QQ LL) j I �u �,�YA m , Po -Eck ED-) TYPE OF PERMITTED OPERATION BEING MONITORED r 1 4� estreeq �4C ZA!53( County �g Gallery � ❑ Lagoon El Infiltration (04y) tstaie, ,zlw ❑ Spray Field ❑ Remediation: Contact Person: I��nec `d 1 11 4_� Telephone#: Z-L52(.4-' %4 ❑ Rotary Distributor M Land Application of Sludge Well Location/Site Name: Cs }(yy g No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): % Ll Date sample collected: Well Depth: 1 ft. Well Diameter: Z in. Depth to Water Level 82546: 10. d� ft. below measuring point Screened Interval: &ft. to 1 ✓ ft. — Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: )] YES ❑ NO and field acidified: YES ❑ NO FIELD ANALYSES: pH 00400:4,'5 units Temp. 000m: ZJ C Spec. Cond. 0009a: i � µMhos Odor 000s5: nCy-)e_ Appearance cir If WELL WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: to- I( _K_ff Laboratory Name: F- nyI fcnmeo+ �1 lry--- Certification No. 1 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 o .b mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 g-% mg/L Al -Aluminum o11o5 mg/L pH (Lab) 00403 46 units Ba - Barium 01007 ug/L TOC omm mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic01002 ug/L Chromium: Total01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <G, QIO mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 9 Yes (1) ❑ No (0) Specific Conductance 00095 f 5 tlMhos K - Potassium 00937 mg/L VOC 7873 method # 6Z�QCJ L Total Ammonia oo610 Q.W mg/L Mg - Magnesium oo927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mglL VOC Removal% _Pharlt1fl. d A-W imkm 06c Penmttee (or Authorized Agent) Name and Title - PI ase print or type GW-59 Rev.3-1-2016 SUBMIT FORM ON PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM GAr`n ITV tntCnDRNATtnnt Please Facility Name: Permit Name (if different): Facility Address: qCC or County (city) fstatel (zip) ontact Person: J�e(� eP l Telephone#: Z,fZ-!5Z4-� fell Location/Site Name:I E*60eCf' JaP141-6091 O No. of wells to be sampled PERMIT Number: Expiration Date: I-,N-ZGZn Non -Discharge t,�[Q42 UIC NPDES NCCC)aZQ_n Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): 1,5 Date sample collected: Well Depth: ft. Well Diameter: c7_in, Depth to Water Level s254s: De p �• 5 ft. below measuring point Screened Interval: 3 ft. to �ft_ Measuring Point is Z.6 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: [%YES ❑ NO and field acidified: YES ❑ NO FIELD ANALYSES: pH 00aoo:4• C0 units Temp. 000lo: z� °C Spec. Cond. oo0s4: '� � • �-i µ Mhos Odor 00085: r-)or)t_ Appearance G(r—L F If WELL WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: ��}-iC }� I jp Laboratory Name: Envifo')n)c +-Tj Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 d•©(� mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 (}.(x% mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al -Aluminum o11os mg/L pH (Lab) 00403 •(� units Ba - Barium 01007 ug/L TOC oosso Cj.� mg/L Ca - Calcium oosss mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 (n ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 CQ •Q JQ mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 719oo ug/L Lab Report Attached? 1� Yes (1) ❑ No (0) Specific Conductance 00095 0-4 µMhos K - Potassium 00937 mg/L VOC 7873 method # %WOC_4 I Total Ammonia oosso ©, L4 90 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen. Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% C)af1 m �; ��czSc lCand l� lirnc c. Permittee (or Authorized Agent) Name and Title - P ease print or type GW-59 Rev.3-1-2016 SUBMIT FORM ON PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM CAf-ll ITV IAlCr)DI111ATIrlA1 Please Facility Name: (_a Permit Name (if different): Facility Address: C/CQ or Type County ntact Person: I�)trle. "-rnII vv-) Telephone#: 762-'5Z4- 5%4 'll Location/Site Name:. C(�nff P PJC[ #(Qi No. of wells to be sampled: (p PERMIT Number: Expiration Date: Non -Discharge 1,000IDOIC>< I d UIC NPDESOther TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor CvLand Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): Date sample collected: I C--14-jG FIELD ANALYSES: Well Depth: q ft. Well Diameter: in. pH 00400:4-9 units Temp. 000lo: Depth to Water Level 62546: I (p ft. below measuring point Screened Interval: Z ft. to ft. Spec. Cond. 00094: �5 I g µMhos Measuring Point is �.�j�j ft. above land surface Relative M.P. Elevation: ft. Odor 000e5: �C�l Volume of water pumped/bailed before sampling: gallons Appearance ld'e( Samples for metals were collected unfiltered: OYES ❑ NO and field acidified: [A YES ❑ NO LABORATORY INFORMATION Date sample analyzed: IC15-(4--�Cj L LaboratoryName: F fN) f(n jY 15_) 1 .T� �%1C Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 ' /100mL Nitrate (NO3) as N 00620 0 • (p mg/L Zn - Zinc D1092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 1�•.O� mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 5(� mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 la . units Ba - Barium 01007 ug/L TOC 006eo Z- I �0 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 C �J. (� ug/L If WELL DRY at time of sampling, here: ❑ Grease and Oils o0552 mg/L Cu - Copper 01042 C O • SIC) mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 1� Yes (1) ❑ No (0) Specific Conductance 00095 mj •� ELMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia o0610 �. I mg/L Mg - Magnesium oo927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen. Total) Mn - Manganese olos5 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Na GW-59 Rev.3-1-2016 - Please pnnt or type ica' W ou- SUBMIT FORM ON Y4111111111V/ PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if different): Facility Address: C(c):! ,� LPlease Print Clearly or 1 t h b (Slate) lzlp) County P1 +-f- act Person: enee 5-m� Telephone#: Z57 5ZLi- 55�_`4 Location/Site Name: I,k)C�D r I ei 6 4hj No. of wells to be sampled:—( _ PERMIT Number: Expiration Date: )-A,�►-L000 Non -Discharge k_QCCOI04q UIC NPDES I-IC�03ZC�7�i Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): 1,9 Date sample collected: Well Depth: �� ft. Well Diameter: Z in. Depth to Water Level 82546: -�, 1 (c ft. below measuring point Screened Interval: S ft. to la ft. Measuring Point is 2 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling:�:!! gallons Samples for metals were collected unfiltered: YES ❑ NO and field acidified: YES ❑ NO FIELD ANALYSES: pH 0oaoo: -0 units Temp. 000lo: ZZ °C Spec. Cond. 00094: 13Gi µMhos Odor 00085: Appearance G Q Y If WELL WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: I � I L4-1,: Laboratory Name: _ F_rw i ra) (�eit _.-L j nc - Certification No. C— PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo815 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 _E00 /100mL Nitrate (NO3) as N 00820 �� , QL mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00885 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 O . �J mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 1 mg/L Al - Aluminum o11os mg/L pH (Lab) 00403 5.0 units Ba - Barium 01007 ug/L TOC 0068D Q -L O mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium olo27 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 C)LC) mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? rLq_- Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oo810 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00825 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% _VV II-J -I-GU IV Efiw'w0)flmM % hC0TV@TMW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 z �. -----Wastewater TD: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 10/14/19 DATE REPORTED : 11/18/19 REVIEWED BY: -- Well #9 Well #10 Well #14 Well #15 Well #17 Analysis Method Date Analyst Code PARAMETERS Fecal Coliform (N1F), /100 Mls 16 35 7 12 < 1 10/14/19 HJO 9222D-06 Ammonia Nitrogen as N, mg/l 1.34 0.16 0.20 0.48 0.13 10/16/19 BLD 350.1 R2-93 Nitrate Nitrogen as N, mg/l <0.04 0.95 1.45 0.04 0,61 10/15/19 BLD 353.2 R2-93 Total Organic Carbon, mg/l 6.78 2.46 2.09 9.83 2.16 10/16/19 SEJ 531OC-11 tal Dissolved Residue, mg/I 53 42 87 119 50 10/15/19 MAR 2540C-11 tal Chromium, ug/1 <5.0 <5.0 <5.0 6 <5.0 10/25/19 LFJ EPA200.7 Copper, ug/l < 10 < 10 < 10 < 10 < 10 10/17/19 LFJ EPA200.7 Conductivity (at 25c), uMhos/cm 230 47.3 158 81.4 51.8 10/21/19 TMR 251OB-11 Total Ortho-Phosphate as P, mg/I 0.12 0.16 0.03 0.08 0.07 10/15/19 KDS 450OPE-11 RMUmNEW Flo hCupTOW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Well #18 Analysis Method PARAMETERS Date Analyst Code Fecal Coliform (MF), /100 MIS 200 10/14/19 HJO 9222D-06 Ammonia Nitrogen as N, mg/l 0.28 10/16/19 BLD 350.1 R2-93 Nitrate Nitrogen as N, mg/l <0.04 10/15/19 BLD 353.2 R2-93 Total Organic Carbon, mg/l 8.47 10/16/19 SEJ 531OC-11 otal Dissolved Residue, mg/1 133 10/15/19 MAR 2540C-11 otal Chromium, ug/l <5.0 10/25/19 LFJ EPA200.7 Copper, ug/l < 10 10/17/19 LFJ EPA200.7 Conductivity (at 25c), uMhos/cm 139 10/21/19 TMR 251OB-11 Total Ortho-Phosphate as P, mg/1 0.05 10/15/19 KDS 450OPE-11 Wastewater iD -0 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 10/14/19 DATE REPORTED : 11/18/19 REVIEWED BY: % howpud(d 114 OAKMONT UHIVE GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. $OX 477 GRIFTON, NC 28530 REVIEWED BY: VOLATILE ORGANICS m„ i, vmvnna g'7nno-1 i jNE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 416 ANALYST: KPG DATE COLLECTED: 10/14/19 DATE ANALYZED: 10/23/19 DATE REPORTED: 11/18/19 Page: 1 PARAMETERS, ug/1 Well #9 Well #10 Well #14 Well #1S Well #17 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 1. Benzene <0.50 <0.50 <0.50 <0.50 <0.50 2. Bromobenzene <0.50 <0.50 <0.50 <0.50 <0.50 3. Bromochloromethane <0.50 <0.50 <0.50 <0.50 <0.50 4. Bromodichloromethane <0.50 < 0.50 < 0.50 < 0.50 < 0.50 5. Bromoform < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 6. Bromomethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 7. N-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 S. Sec-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 9. Tert-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 10. Carbon Tetrachloride < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 11. Chlorobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 12. Chloroethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 13. Chloroform 1.022 < 0.50 < 0.50 < 0.50 < 0.50 14. Chloromethane <0.50 <0.50 <0.50 <0.50 <0.50 15. 2-Chlorotoluene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 16. 4-Chlorotoluene <0.50 <0.50 <0.50 <0.50 <0.50 17. Dibromochloromethane <0.50 <0.50 <0.50 <0.50 <0.50 18. 1,2-Dibromo-3-Chloropropane <0.50 <0.50 <0.50 <0.50 <0.50 19. 1,2-Dibromoethane <0.50 <0.50 <0,50 <0.50 <0.50 20. Dibromomethane <0.50 <0.50 <0.50 <0.50 <0.50 21. 1,2-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 22. 1,3-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 23. 1,4-Dichlorobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 24. Dichlorodifluoromethane <0.50 <0.50 <0.50 <0.50 <0.50 25. 1,1-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 . 1,2-Dichloroethane 26. <0.50 <0.50 <0.50 <0.50 <0.50 1,1-Dichloroeth 2ane <0.50 <0.50 <0.50 <0.50 <0.50 28. Cis-1,2-Diroeth ethane <0.50 <0.50 <0.50 <0,50 <0.50 29. trans-1,2-Dichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 30. 1,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 31. 1,3-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 32. 2,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 33. 1,1-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 34. Cis-1,3-Dichloropropene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 35. trans-1,3-Dichloropropene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 3 6. Ethylbenzene EthylbHexac <0.50 <0.50 <0.50 <0.50 <0.50 3. lorobutadiene <0.50 <0.50 <0.50 <0.50 <O.SO 38. Isopropylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 39. 4-Isopropyltoluene < 0.50 < 0.50 <0.50 < 0.50 < 0.50 40. Methylene Chloride < 0.50 <0.50 < 0.50 < 0.50 < 0.50 41. Naphthalene <0.50 < 0.50 < 0.50 < 0.50 < 0.50 42. Propylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 43. Styrene 44. 1,1,1,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 <0.50 <6.50 45. 1,1,2,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 4 6. Tetrachloroethene <0.50 <0.50 <0.50 <0.50 <0.50 4. Toluene <0.50 <0.50 <0.50 <0.50 <0.50 48. 1,2,3-Tricblorobenzene ElMnNEW Flo hcupumbo wastewater ID; 19 1_10 __,<wPHONE (252) 756-6208 114 OAKMONT DRIVE FAX (252) 756-0633 GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CLIENT ID: 416 CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN ANALYST: KPG 7 DATE COLLECTED: 10/14/19 Page: 2 P.O. BOX 47BOX 47 28530 DATE ANALYZED: 10/23/19 GRIFTONDATE REPORTED: 11/18/19 REVIEWED BY: VOLATILE ORGANICS emn mRTunnS 92.0OC-11 PARAMETERS, ug/l Well #9 Well #10 Well #14 Well #15 Well #17 49. 1,2,4-Trichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 50. 1,1,1-Trichloroethane <0.50 <.0.50 <0.50 <0.50 <0.50 51, 1,1,2-Trichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 52. Trichloroethene 53. Trichlorofluoromethane <0.50 <0.50 <0.50 <0.50 <0.50 54. 1,2,3-Trichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0,50 <0.50 <0.50 55. 1,2,4-Triinethylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 56. 1,3,5-Trirnethylbenzene <0.50 < 0.50 < 0.50 < 0.50 < 0.50 57, Vinyl Chloride < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 58. Total Xylenes 59. Methyl Tert Butyl Ether < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 EMMUTORHM Flo hCupumho 114 O l"MONT DRIVE GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELDS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 28530 REVIEWED BY: - r !4', wastewater ID: �0 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 416 VOLATILE ORGANICS STD. METHODS 620OC-11 ANALYST: KPG DATE COLLECTED: 10/14/19 Page: 3 DATE ANALYZED: 10/23/19 DATE REPORTED: 11/18/19 PARAMETERS, ug/l Well #18 1. Benzene < 0.50 2. Bromobenzene < 0.50 3. Bromochloromethane <0.50 4. Bromodichloromethane <0.50 5. Bromoform < 0.50 6. Bromomethane < 0.50 7. N-Butylbenzene <0.50 8. Sec-Butylbenzene <0.50 9. Tert-Butylbenzene <0.50 10. Carbon Tetrachloride <0.50 11. Chlorobenzene <0.50 12. Chloroethane < 0.50 13. Chloroform <0.50 14. Chloromethane < 0.50 15. 2-Chlorotoluene < 0.50 16. 4-Chlorotoluene < 0.50 17. Dibromochloromethane < 0.50 18. 1,2-Dibromo-3-Chloropropane < 0.50 19. 1,2-Dibromoethane < 0.50 20. Dibromomethane <0.50 21. 1,2-Dichlorobenzene < 0.50 22. 1,3-Dichlorobenzene < 0.50 23. 1,4-Dichlorobenzene < 0.50 24. Dichlorodifluoromethane <0.50 25. 1,1-Dichloroethane < 0.50 26, 1,2-Dichloroethane <0.50 27, 1,1-Dichloroethene < 0.50 28. Cis-1,2-Dichloroethene < 0.50 29. trans-1,2-Dichloroethene < 0.50 30. 1,2-Dichloropropane < 0.50 31. 1,3-Dichloropropane < 0.50 32. 2,2-Dichloropropane < 0.50 33. 1,1-Dichloropropene < 0.50 34. Cis-1,3-Dichloropropene <0.50 35. trans- 1,3-Dichloropropene < 0.50 36. Ethylbenzene < 0.50 37. Hexachlorobutadiene < 0.50 38. Isopropylbenzene < 0.50 39. 4-Isopropyltoluene < 0.50 40. Methylene Chloride <0.50 41. Naphthalene < 0.50 42. Propylbenzene < 0.50 < 0.50 43. 44. Styrene 1,1,1,2-Tetrachloroethane < 0.50 45. 1,1,2,2-Tetrachloroethane < 0.50 46. Tetrachloroethene < 0.50 47. Toluene <0.50 < 0.50 48. 1,2,3-Trichlorobenzene r 7- ' 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, C 28530 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 620OC-11 PARAMETERS, ug/l WaatewaC®r TDt 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 416 ANALYST: KPG DATE COLLECTED: 10/14/19 DATE ANALYZED: 10/23/19 DATE REPORTED: 11/18/19 Well ##18 49. 1,2,4-Trichlorobenzene < 0.50 50. 1,1,1-Trichloroethane < 0.50 51. 1,1,2-Trichloroethane < 0.50 52. Trichloroethene <0.50 53. Trichlorofluoromethane <0.50 54. 1,2,3-Trichloropropane < 0.50 55. 1,2,4-Trimethylbenzene < 0.50 56. 1,3,5-Trimethylbenzene < 0.50 57. Vinyl Chloride <0.50 58. Total Xylenes < 1.00 59. Methyl Tert Butyl Ether < 1.00 Page: 4 SOILS ANALYSIS LAB REPORTS LIME APPLICATION NCDA&CS Agro c Division Phone: (919) 733-2655 Website: www.nc lov/agronomi/ Report No. F' L006679 Client: CMSD Advisor: Chris Whitehurst Predictive PO Box 477 Ayden Nitrogen Grifton, NC 28530 PO Box 7 Soil Report Mehlich-3 Extraction Ayden, NC 28513 Sampled County: Pitt "•'"t•5`� �Links to Helpful Information Client ID: 147385 Advisor ID: 490477 Sampled:09/19/2019 Received: 09/27/2019 Completed: 10/04/2019 Farm: Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or " Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to Rrevent levels from accumulating to the point where they become toxic to crops grown on a field. Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 130 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.56 1.02 16.2 86 2.2 6.2 996 42 66 19 49 75 59 3558 3558 1265 0.2 1 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 170 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.94 17.4 89 1.8 6.4 1021 28 69 19 58 72 55 4450 4450 1505 0.3 2 Forth Carolina Tobakto ltkm 1 uwwd Ccwnmisslon Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Aaricu/ture NCDA&CS Agro-- c Division Phone: (919) 733-2655 Website: www.nc lov/agronomi/ Report No. F` ;L006679 Page 2 of 10 Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Bermuda hay/past., M 0.0 180-220 0 190 0 0 pH$ Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - W/V in g/crT?; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 1.12 16.8 96 0.6 7.0 991 20 74 22 55 67 42 3022 3022 844 0.3 2 Sample ID: 4 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.7 180-220 0 170 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.71 0.92 15.0 81 2.8 5.8 1002 28 63 17 142 71 60 2532 2532 1176 0.3 2 Sample ID: 5 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.8 180-220 0 80 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dM3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 0.81 19.6 84 3.2 5.8 1013 66 60 22 84 80 65 4192 4192 1842 0.3 2 Sample ID: 6 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 140 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.04 17.6 89 1.9 6.4 991 39 67 22 52 78 58 3997 3997 1224 0.2 1 NCDA&CS Agroi Division Phone: (919) 733-2655 Website: www.nc lov/agronomi/ Report No. F` L006679 Page 3 of 10 Sample ID: 7 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 130 0 0 pH$ Z 0 0 Note: 12 Note: 3 2 - 0.0 Test Results [units - WN in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/drri3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 1.09 14.7 94 0.9 6.8 845 44 70 22 47 83 54 2066 2066 579 0.2 1 Sample ID: 8 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 160 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.97 1.02 17.4 89 1.9 6.4 886 29 68 21 56 76 57 2882 2882 1251 0.3 2 Sample ID: 9 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 110 0 0 pH$ Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn4 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.13 17.6 95 0.9 6.9 884 49 71 23 35 100 63 3658 3658 959 0.1 1 Sample ID: 10 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 140 0 0 pH$ Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 1.07 19.6 95 1.0 6.9 978 37 71 23 36 80 51 5042 5042 1480 0.1 1 NCDA&CS Agro r Division Phone: (919) 733-2655 Website: www.nc lov/agronomi/ Report No. F 'L006679 Page 4 of 10 Sample ID: 11 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 150 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drrt3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.41 1.15 12.6 88 1.5 6.4 846 36 66 21 35 100 71 2779 2779 815 0.1 1 Sample ID: 12 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 130 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.04 16.9 90 1.7 6.5 871 41 69 20 42 84 60 4232 4232 1254 0.2 1 Sample ID: 13 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.6 180-220 0 140 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.92 1.02 11.3 81 2.2 5.8 843 40 61 19 52 85 68 1753 1753 580 0.2 2 Sample ID: 14 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.0 180-220 0 150 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.71 1.14 9.9 87 1.2 6.4 527 35 64 22 37 78 58 1034 1034 293 0.1 1 NCDA&CS Agror--' : Division Phone: (919) 733-2655 Website: www.nc ov/agronomil Report No. F) L006679 Page 5 of 10 Sample ID: 15 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 1.4 180-220 0 170 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS -I NO3-N 1.19 1.19 4.4 50 2.2 5.0 134 27 34 13 27 32 36 256 256 66 0.1 2 Sample ID: 16 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.4 180-220 0 160 0 20 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.94 1.13 5.3 36 3.4 4.5 116 31 23 10 23 31 36 230 230 55 0.1 2 Sample ID: 17 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 160 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dM3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS -I NO3-N 0.60 1.14 8.5 80 1.7 5.9 601 30 57 21 44 73 61 940 940 357 0.1 1 Sample ID: 18 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.3 180-220 0 140 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/cd; CEC and Na in meg1100 cm3; NO3-N in mg/drrt3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.51 1.01 14.4 85 2.2 5.9 1139 38 62 21 52 78 64 3350 3350 1119 0.1 1 NCDA&CS Agror--' : Division Phone: (919) 733-2655 Website: www.nc ov/agronomi/ Report No. Fly L006679 Page 6 of 10 Sample ID: 19 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 140 0 0 0 Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dM3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.81 1.00 15.9 90 1.5 6.4 1027 37 67 22 45 77 57 2826 2826 822 0.1 1 Sample ID: 20 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 120 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.14 1.11 10.2 93 0.7 6.7 294 46 68 23 33 100 67 662 662 175 0.1 1 Sample ID: 21 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 130 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.71 1.10 10.4 93 0.7 6.7 550 43 70 22 35 115 75 1197 1197 308 0.1 1 Sample ID: 22 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 2.4 180-220 0 130 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.66 0.94 11.7 66 4.0 5.1 1116 44 48 17 89 81 66 1923 1923 1300 0.1 1 NCDA&CS Agror--' ; Division Phone: (919) 733-2655 Website: www.nc ov/agronomi/ Report No. Fly L006679 Page 7 of 10 Sample ID: 23 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.6 180-220 0 160 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.60 1.00 12.9 80 2.5 5.8 1035 32 59 21 58 67 57 2794 2794 1023 0.1 1 Sample ID: 24 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 160 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.71 1.10 11.9 90 1.2 6.6 712 30 65 25 48 92 64 1823 1823 550 0.1 1 Sample ID: 25 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 150 0 0 pH$ Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.81 1.08 13.9 93 1.0 6.7 832 34 71 21 38 58 42 2885 2885 617 0.1 1 Sample ID: 26 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 170 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.87 1.03 13.3 86 1.9 6.1 854 28 70 14 43 61 53 3385 3385 1010 0.2 2 NCDA&CS Agror----0 ; Division Phone: (919) 733-2655 Website: www.nc ov/agronomi/ Report No. F) L006679 Page 8 of 10 Sample ID: 27 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 150 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dM3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.08 0.98 13.7 87 1.8 6.2 824 35 69 17 37 48 43 2653 2653 812 0.1 1 Sample ID: 28 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.0 180-220 0 160 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.80 1.10 10.3 83 1.8 6.0 666 30 65 17 33 75 62 1416 1416 409 0.1 1 Sample ID: 29 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 160 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.08 1.08 12.2 88 1.5 6.3 872 31 66 21 38 61 49 2180 2180 648 0.1 1 Sample ID: 30 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 170 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS -I NO3-N 2.52 1.04 13.9 88 1.7 6.2 784 26 67 20 35 62 51 2131 2131 653 0.1 1 NCDA&CS Agroi ; Division Phone: (919) 733-2655 Website: www.nc ov/agronomil Report No. F) L006679 Page 9 of 10 Sample ID: 31 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.0 180-220 0 170 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drr?]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.37 1.16 10.0 90 1.0 6.4 491 27 67 21 34 63 49 1266 1266 296 0.1 1 Sample ID: 32 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 1.0 180-220 0 150 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.60 1.15 9.4 75 2.4 5.6 895 33 55 18 44 74 61 1508 1508 513 0.1 1 Sample ID: 33 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.0 180-220 0 150 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.56 1.13 9.9 83 1.7 6.1 795 33 60 21 39 68 57 1565 1565 477 0.1 1 NCDA&CS Agror Division Phone: (919) 733-2655 Website: www.nc ov/agronomi/ Report No. F) L006679 Page 10 of 10 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations I Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmi#sfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WIV weight per volume Zn-AI zinc availability index The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-1, SS-1, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/agronomi1uyrst.htm Payment 1005633 Ayden Nitrogen 4728 Old NC 11 / P.O. Box 7 Ayden, NC 28513 252-746-2152 Fax 252-746-8472 Ayden Golf & Country Club 4343 Ayden Golf Club Road Ayden, NC 28513 Description Payment Received Discount Allowed Total Credit to Account Invoice # Amount 1017230 87.48 Date 02/18/2020 Customer ID 011256 Check 20444 87.48 Amount 87.48 0.00 87.48 Ayden Golf & Country Club - Balance after this payment 0.00 Payment 1005633 File 2 Copy Payment 1005633 Ayden Nitrogen 4728 Old NC 11 / P.O. Box 7 Ayden, NC 28513 252-746-2152 Fax 252-746-8472 Ayden Golf & Country Club 4343 Ayden Golf Club Road Ayden, NC 28513 Description Payment Received Discount Allowed Total Credit to Account Invoice # Amount 1017230 87.48 Date 02/18/2020 Customer ID 011256 Check 20444 87.48 Amount 87.48 0.00 87.48 Ayden Golf & Country Club - Balance after this payment 0.00 Payment 1005633 File Copy Payment 1005633 Ayden Nitrogen 4728 Old NC 11 / P.O. Box 7 Ayden, NC 28513 252-746-2152 Fax 252-746-8472 Ayden Golf & Country Club 4343 Ayden Golf Club Road Ayden, NC 28513 Description Payment Received Discount Allowed Total Credit to Account Invoice # Amount 1017230 87.48 Date 02/18/2020 Customer ID 011256 Check 20444 87.48 Amount 87.48 0.00 87.48 Ayden Golf & Country Club - Balance after this payment 0.00 Payment 1005633 Customer Copy NC,DA&CS.Agror Division Phone: (919) 733-2655 Website: www.nc, )v/agronomi/ Report No. FY _008558 Client: CMSD Advisor: Chris Whitehurst Y � �%Y' Predictive PO Box 477 Ayden Nitrogen T Grifton, NC 28530 PO Box 7 } Soil Report Mehlich-3 Extraction Ayden, NC28513 Sampled County: Pitt Links to Helpful Information Client ID: 147385 Advisor ID: 490477 Sampled:09/19/2019 Received: 10/08/2019 Completed: 10/16/2019 Farm: Sample ID: 37 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 160 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.12 12.6 94 0.7 6.9 541 31 67 26 41 89 57 836 836 300 0.1 1 Sample ID: 38 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 180 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dn13]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.14 1.19 10.9 94 0.7 6.8 142 22 69 24 31 61 42 451 451 116 0.1 1 Sample ID: 39 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.6 180-220 0 170 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dtrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.43 1.12 8.6 78 1.9 5.7 437 26 60 16 34 53 49 919 919 265 0.1 1 North Carolina Ii+Ma<ci� crust Furw,J C'i�nvni+.lcaro Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Agriculture NCDA&CS.Agron Division Phone: (919) 733-2655 Website: www.nce w/agronomil Report No. FY: 008558 Page 2 of 3 Sample ID: 40 Recommendations: Lime Nutrients (ID/acre) More Crop (tons/acre) N P2O5 K2O Mg- S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., M 0.0 180-220 0 160 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.19 1.11 9.4 87 1.2 6.3 269 32 65 21 39 66 52 597 597 217 0.1 1 NCDA&CS,Agron Division Phone: (919) 733-2655 Website: www.nci w/agronomi/ Report No. FY: .008558 Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-O mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm1#sfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume Zn-AI zinc availability index The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/agronomi/uyrst.htm SavedRx: LIME 2019-2020 ge-m-e- Soil Fertility Poweca Hy grower: CMSD Farm: WILEY GASKINS RD Field(s): Multiple Fields Tenn Lime - Fertilizer Application (Ibs/ac) F, 5.5 17. - 0 400 1578 2756 3934 5112 Lab: NCDA Equation: Lab - NCDA Commodity: Bermuda Grass Sample Dates: 2019-09-19 - 2018-10-12 Constraints: Target pH: 6 Crop Type: Pick Type Max Rate: N/A Multiplier: N/A Min Rate: 400.0 Ibs/ac Subtract: N/A Switch Rate: 400.0 Ibs/ac Minimum Application Rate: 400.0 Ibs/ac Total Product: 44471.15 Ibs Maximum Application Rate: 5112.1 Ibs/ac Total Product Bulk: 22.24 ton Average Application Rate: 1650.79 Ibs/ac Product Cost / Bulk: $0.0/ton Application Area: 26.94 ac Total Product Price: $0.0 Average Field Rate: 586.32 Ibs/ac Application Cost / Area: $0.0/ac Total Area: 75.85 ac Total Application Cost: $0.0 Total Cost: $0.0 Ayden Nitrogen 4728 Old NC 11 10/23/19 08:20 AM Ayden, NC 28513 1/2 252-746-2152 PlA1T61i11 h r-ertilizer Application Summary SavedRx: LIME 2019-2020 Soil Fertility Grower: CMSD Commodity: Bermuda Grass Farm: WILEY GASKINS RD Labs: NCDA Field(s): Multiple Fields Field Summary Field PLS ID .. County Area Centroid Pitt 2.06 ac 35.365487,-77.414558 1 Pitt 16.18 ac 35.360361,-77.418702 F Pitt 2.21 ac 35.358556,-77,418100 Pitt 2.35 ac 35.358478,-77.421019 4 Pitt 13.83 ac 35.367513,-77.419061 F-05 Pitt 14.34 ac 35.366959,-77.415219 F-06 Pitt 4.40 ac 35.365362,-77.416477 F-07 Pitt 15.91 ac 35.360321,-77.410402 F-08 I Pitt 14.40 ac 35.362013,-77.410097 Ayden Nitrogen 4728 Old NC 11 10/23/19 08:20 AM Ayden, NC 28513 2/2 252-746-2152 Statement Ayden Nitrogen Statement Date: 10/31/2019 4728 Old NC 11 / P.O. Box 7 ID: 010202 Ayden, NC 28513 Total Balance: $1,690.65 Phone 252-746-2152 Page: 1 Contentnea Metro Sewage Dist __- _ I Amount Remitted: Po Box 477 _... Griffon, NC 28530 J - Terms: Unless otherwise agreed in wrifing by Harvey Fertilizer & 0 " " Gas Co, interest will accrue at a periodic rate of 1.5% per j month. To avoid additional finance charges, payments must G be in office by last day of month. -- -- - - - - - - _ 1�-_-.,-Your Share ----I Date Number Description / Detail Quantity Price 1 Unit Extension / Prepaid Regular Balance Forward 0.00 0.00 10/25/2019 1017044 Charge Invoice - Due 11/24/2019 Dolomitic Lime - Bulk 9.150 Tons 51.000 [Tons 466.65 466.65 App Fees Materials 9.150 Each 14.000 /Each 128.10 128.10 Invoice Total 594.75 0.00 594.75 10/25/2019 1017045 Charge Invoice - Due 11/24/2019 Dolomitic Lime - Bulk 7.920 Tons 51.000 !Tons 403.92 403.92 App Fees Materials 7.920 Each 14.000 /Each 110.88 110.88 Invoice Total 514.80 0.00 514.80 10/25/2019 1017046 Charge Invoice- Due 11/24/2019 Dolomitic Lime - Bulk 8.940 Tons 51.000 [Tons 455.94 455.94 App Fees Materials 8,940 Each 14.000 ]Each 125.16 125.16 Invoice Total 581.10 0.00 581.10 Ending Total Balances 0.00 1,690.65 Current 1 - 30 31 - 60 61 - 90 Over 90 Unapplied Budget Billing Prepay Overall 1,690.65 0.00 0.00 0.00 0.00 0.00 0.00 0.00 -i,690.c Ayden Nitrogen Date: 10/31/2019 Contentnea Metro Sewage Dist