WQ0030998_Residual Annual Report 2019_20200228

Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subrrittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Robert T. Branch
Email Address*
[e-mail]
Project Information
Application Type* r New
r Renewal
r Annual Report
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQoo30998
Applicant/Permittee * Triple S Farms & Cleaning, Inc.
Applicant/Permittee PO Box 709 Veulaville, NC 28518
Address*
Facility Name * Triple S Farms & Cleaning, Inc.
Phone Number*
336.312-9007
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.

For new and modification permit applications, a paper copy may he required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper application is required,
be advised, applications accepted for pre -review until both the paper and electronic copies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (talcs, soils report, specs, etc.)
o One full-size e-rei-ieering plan set
o One 11x17" engineer ng 1'- an set
o One extra set of specifications
o Fee (if required)
Mailing address:
--------------------------------------------
By U.S. Postal Service
Division of Water Resources
--------------------------------------------
Non-discharge Branch
1617 Mail Service Center
-------------------------------------------
Raleiah. NC 27699-1617
Division of Water Resources
Non -Discharge Branch
Att: Nathaniel Thornburg, 9"
512 N.5alisburySt.
Raleish. NC 276Q4--117O
Floor, Office #942W
For questions or problems contact Tessa Monday attessa.monday[)ncdenr.Rov or 919.707.3560.
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Forrn Engineering Rans, Specifications, Calculations, Etc.)
SSS_FARMS_2019_AR Final.pdf 10.45MB
Upload only 1 FDF docurrent. Multiple docurrents rrust be corrbined into one FDF file.
* V By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature *
Submission Date Is filled inautomatically once submtted.

2019 ANNUAL REPORT
TRIPLE S FARMS & CLEANING, INC.
LAND APPLICATION PROGRAM
PERMIT #WQ0030998
Prepared For:
Triple S Farms & Cleaning, Inc.
Post Office Box 709
Beulaville, NC 28518
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
February 2020

BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone]
February 25, 2020
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2019 LAND APPLICATION ANNUAL REPORT
Triple S Farms & Cleaning, Inc.
Permit No. WQ0030998
Branch Residuals & Soils Project No. 2007-70
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Triple S Farms & Cleaning, Inc. This data includes: 1) Certification Forms and Facility
Information, 2) Annual Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7)
Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils
Lab Data 10) 2019 Application Summary Table, and 11) 2019 Application Condition Summaries.
A total of 2,860,677 gallons (292.65dry tons) of Class B lime -stabilized biosolids or Class B fecal and
injected/incorporated biosolids were land applied to 116.4 acres in 2019. This material was divided as follows:
• 221,000 gallons (20.46 dry tons) from Beulaville WWTP,
• 1,039,700 gallons (106.22 dry tons) from Clayton Little Creek WRF,
0 126,000 gallons (2.68 dry tons) from Kenansville WWTP,
0 0 gallons (0 dry tons) from Rose Hill WWTP,
0 587,000 gallons (70.25 dry tons) from Warsaw WWTP,
• 37,800 gallons (4.07 dry tons) from Southwest Plantation WWTP, and
• 849,177 gallons (88.97 dry tons) from Wallace WWTP.
If any further information is required regarding this land application program, please do not hesitate to contact
me at [phone].
Since ely,
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures
cc: Town of Beulaville Town of Kenansville
Town of Rose Hill Town of Warsaw
Southwest Plantation Town of Wallace
Town of Clayton

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Forms and Facility Information
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2019 Application Summary Table
XI 2019 Application Condition Summaries

CERTIFICATION FORMS AND FACILITY INFORMATION

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0030998 County: Duplin Year: 2019
Facility Name (as shown on permit): Triple S Farms & Cleaning
Land Application Operator: Triple S Farms & Cleaning Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
Yes No -If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - ReSidualC Annlirntinn C..MMaM.J•
Total number of application fields in thepermit:
9
Total number of fields utilized for land application during the year:
8
Total amount of dry tons applied during the year for all application sites:
292.65
Total number of acres utilizes for land application during the year:
116.4
Y■ & " - cauuuu, w,uwauce Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. p Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .l 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of flues and imprisonment for knowing violations.,, //� A 0
Mr. Eric R. Smith, Owner
Permittee Name and Title (type or print)
Date
See Attached �Ja�� � �f���✓�� �� „��'.
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 07T 11 M 176)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BEULAVILLE
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes p No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .l 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature o eparer* Date
(if different rom Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF CLAYTON
Part B - Annual Comuiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes p No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Si Lure mure of Preparer* Date
different from Perri
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF KENANSVILLE
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. p ides D No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
l) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
- a2.c2��2Q�p
Signature 8f Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
SOUTHWEST PLANTATION
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T . 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .l I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of firs ndysoisonment for knowing violations."
2
-2 }'ZrJ
Date
(if di rent from Permittee)
* Prd0arer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WALLACE
Part B - Annual Comaiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed an each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. 1l11 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
(� a 4 2 •C�,�Zv Lv
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL. LAND APPLICATION CERTIFICATION FORM
TOWN OF WARSAW
Part B - Annual Comoiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. p Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
I ) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and Iime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. i l l I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
poslibility of fines and imprisonment for knowing violations."
0
Signdture of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORMS

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NPDFS #:
NCO026018
WWTP Name: Town of Beulaville WWTP
Residual AnaIvsis Data
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or C mposite Date
9/23/2019
Percent Solids (%)
NA
2.22
Arsenic
75
<13.5
Cadmium
85
<13.5
Copper
4,300
459.00
Chromium
NA
18.60
Lead
840
28.10
Mercury
57
2.61
Molybdenum
75
<13.5
Nickel
420
<13.5
Selenium
100
<13.5
Zinc
7,500
1650.00
Total Phosphorus
NA
16,400
TKN
NA
40,100
Ammonia -Nitrogen
NA
<4.5
Nitrate and Nitrite
NA
199
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
0
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
M:KID CnORA OCQC Mn/nnn0%

ANNUAL RESIDUAL, SAMPLING SUMMARY FORTNI[
Please note that your permit may contain additional parameters to he analyzed. The parameters can be reported in FCaRi'dili'RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WQ0023178
Town of Clayton
NC0025453
WWTP Name: Little Creek Water Reclamation Facility
Residual Analvsis Data
Laboratory: ]) Waypoint Analytical
2}
3)
4)
5)
Parameter
(mg�g)
Conc.
Limit
7
m )
Sample or Composite Date
ii23no19
i
Percent Solids (%)
NA
2.45
Arsenic
75
<5.00
Cadmium
85
<1.00
Copper
4,300
191.00
Chromium
NA
NA
—
----
Lead
840
10.60
Mercury
57
0.29
-j---
Molybdenum
75
5.19
—
--�-
Nickel
420
I2.60
Selenium 1
100
<5.00
'
—
Zinc
7,500
573.00
Total Phosphorus
NA
27,300
l
TKN
NA
32,800
Ammonia -Nitrogen
NA
4,400
Nitrate and and Nitrite
NA
4,040
---
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUM1VIARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - l3
WQ Permit Number: WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WO # or
NPDES #:
NCO036668
WWTP Name: Town of Kenansville WWTP
Residual Analvsis Data
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
Parameter
(mgtkg)
Ceiling
Conc.
Limit
Sample or Composite Date
6/5/2019
Percent Solids (%a)
NA
0.51
Arsenic
75
<19.2
Cadmium
85
<39.2
Copper
4,300
806.00
Chromium
NA
<39.2
Lead
840
<39.2
Mercury
57
4.71
Molybdenum
75
<39.2
Nickel
420
<39.2
Selenium
100
<39.2
Zinc
7,500
971.00
Total Phosphorus
NA
20,600
TKN
NA
33,400
Ammonia -Nitrogen
NA
<19.6
Nitrate and Nitrite
NA
2,500
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature &Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
aa5 a baD
Date

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NPDES #:
WWTP Name: Southwest Plantation WWTP
Daaidual Analvek date
Laboratory: I) Environmental Chemists
2)
3)
4)
5)
Parameter
(mgtkg)
Ceiling
Conc.
Limit
Sam le or Composite Date
4nz<2019
Percent Solids (%)
NA
2.58
Arsenic
75
<7.79
Cadmium
85
<7.79
Copper
4,300
60.10
Chromium
NA
<7.79
Lead
840
0.79
Mercury
57
<0.698
Molybdenum
75
<7.79
Nickel
420
0.79
Selenium
100
0.79
Zinc
7,500
477.00
Total Phosphorus
NA
19.E
TKN
NA
82,900
Ammonia -Nitrogen
NA
2,410
Nitrate and Nitrite
NA
105
"I certify, under penalty of law at this document was prepared under my direction or supervision in accordance with a system designed
'
to assure that qua le onpe2properly gathered and evaluated the information submitted. I am aware that there a
Signature of
*Preparer is,#fined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
Z'Zs- 2
Date
MKID Cr"MIA OCCG 11919lVW%

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
811 1•"
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NPDES #:
NC0003450
WWTP Name: Town of Wallace WWTP
Residual Analvsis Data
Laboratory: 1) Environmental Chemists, Inc.
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite
Date
1/15/2019
6/52019
9/18/2019
18H WW
iD7Y
Percent Solids M
NA
2.57
2.65
231
036
Arsenic
75
<223 1
<31.6
4330
4330
Cadmium
85
<22.3
<31.6
4330
4330
Copper
4,300
926.00
906.00
935.00
644.00
Chromium
NA
30.20
3250
43.30
43.30
Lead
840
59.40
57.30
5930
<623
Mercury
57
2.01
1
2.20
1.99
.631
Molybdenum
75
<13.4
<31.6
4330
4330
Nickel
420
23.00
<31.6
4330
4330
Selenium
100
<22.3
<31.6
4330
4330
Zinc
7,500
1590.00
1400.00
1390.00
1040.00
Total Phosphorus
NA
17.900
25,800
34,500
19,100
TKN
NA
7.020
37,500
44,100
35,000
Ammgenonia-Nitro
NA
1,960
1,200
4
4
Nitrate and Nitrite
I NA
3,900
390
1,180
7,580
" I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for sMbmitting false information, including the possibility of fines and imprisonment for knowing violations:'
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
2-(D -- Z02-D
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0030998 Laboratory:
Facility Name: Triple S Farms & Cleaning
Residual Source WQ # or
NPDES #:
NCO021903
WWTP Name: Town of Warsaw WWTP
Residual Analysis Data
1) Environmental Chemists
2)
3)
4)
5)
Parameter
(mpg)
Ceiling
Conc.
Limit
Sample or C mposite Date
9/24/2019
Percent Solids (%)
NA
2.S7
Arsenic
75
<10.40
Cadmium
85
<10.40
Copper
4,300
223.00
Chromium
NA
14.80
Lead
840
24.50
Mercury
57
0.70
Molybdenum
75
<10.40
Nickel
420
<10.40
Selenium
100
<10.40
Zinc
7,500
599.00
Total Phosphorus
NA
13.200
TKN
NA
26,800
Ammonia -Nitrogen
NA
<3.48
Nitrate and Nitrite
NA
10
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penapies for subm#tti* false information, including the possibility of fines and imprisonment for knowing violations."
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 132.49
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series NoA
Acres Used: 34.2 Acres Permitted: 34.2 Site #: 1 Field #: I
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
K20191-19 9-024-0208 WL20191-11R2019 In-1 w1I0to i- wunmo Irainio in um-imn Irnln-
Sample
-- - -
----- -
-�
v-.
•.l\LU 17 I1.
1.77-VLY'UL
or Com-
posite
6/5/19
1/23/19
1/15/19
9/23/19
1/15/19
9/24/19
9/23/19
9/24/19
1/23/19
Date
% Solids
0.51
2.45
2.57
2.22
1 2.57
2.87
2.22
2.87
2.45
Arsenic
39.20
5.00
22.30
13.50
22.30
10.40
13.50
10.40
5.00
Cadmium
39.20
1.00
22.30
13.50
22.30
10.40
13.50
10.40
1.00
Chromium
39.20
0.00
30.20
18.60
30.20
14.80
18.60
14.80
0.00
Copper
806.00
191.00
926.00
459.00
926.00
223.00
459.00
223.00
191.00
Lead
39.20
10.60
59.40
28.10
59.40
24.50
28.10
24.50
10.60
Mercury
4.71
0.29
2.01
2.61
2.01
0.70
2.61
0.70
0.29
Molyb-
denum
39.20
5.19
13.40
13.50
13.40
10.40
13.50
10.40
5.19
Nickel
39.20
12.60
23.00
13.50
23.00
10.40
13.50
10.40
12.60
Selenium
39.20
5.00
22.30
13.50
22.30
10.40 1
13.50
10.40
5.00
Zinc
971.00
573.00
1590.00
1650.00
1590.00
599.00
1650.00
599.00
573.00
Total
Phos-
20,600
27,300
17,900
16,400
17,900
13,200
16,400
13,200
27,300
horus
Annual Heavy Metal Field Loadines (Calculated in lbs/acre):
m> =
o
0.03
0.19
1.20
0.19
0.75
0.55
0.22
0.50
0.25
0
o. �
e'
Arsenic
0.00
0.00
0.05
0.01
0.03
0.0I
0.01
0.01
0.00
0.13
Cadmium
0.00
0.00
0.05
0.01
0.03
0.01
0.01
0.01
0.00
0.12
Chromium
0.00
0.00
0.07
0.01
0.05
0.02
0.01
0.01
0.00
0.17
Copper
0.04
0.07
2.22
0.17
1.39
0.24
0.20
1 0.22
0.09
4.66
Lead
0.00
0.00
0.14
0.01
0.09
0.03
0.01
0.02
0.01
0.32
Mercury
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.01
Molyb-
den m
0.00
0.00
0.03
0.01
0.02
0.01
0.01
0.01
0.00
0.09
Nickel
0.00
0.00
0.06
0.01
0.03
0.01
0.01
0.01
0.01
0.14
Selenium
0.00
0.00
0.05
0.01
0.03
0.01
0.01
0.01
0.00
0.13
Zinc
0.05
0.22
3.82
0.62
2.39
0.65
0.71
0.60
0.28
1
9.35
Total
Phos-
1.08
10.63
43.01
6.13
26.88
14.41
7.10
13.30
13.54
136.08
horus
low .•w
I ceriuy, unaer penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inc uding a ssibili of fines and imprisonment for knowing violations"
AAA
Signature of Land Applier nnte

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 24.33
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 8.48 Acres Permitted: 8.48 Site #: 1 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
K2019 1-19 L2019 1-19 SWP 2019 1- WL2019 3-
Sample
orCom-
posite
Date
6/5/19
1/15/19
4/22/19
9/18/19
% Solids
0.51
2.57
2.58
2.31
Arsenic
39.20
22.30
7.79
14.40
Cadmium
39.20
22.30
7.79
14.40
Chromium
39.20
30.20
7.79
32.30
Copper
806.00
926.00
60.10
935.00
Lead
39.20
59.40
7.79
59.30
Mercury
4.71
2.01
0.70
1.99
Molyb-
denum
39.20
13.40
7.79
14.40
Nickel
39.20
23.00
7.79
21.30
Selenium
39.20
22.30
7.79
14.40
Zinc
971.00
1590.00
477.00
1390.00
Total
Phos-
horns
20,600
17,900
19,600
34,500
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
o
mo =
v
g
a.09
0.61
0.16
2.01
y
�
y
Arsenic
0.01
0.03
0.00
0.06
0.09
Cadmium
0.01
0.03
0.00
0.06
0.09
Chromium
0.01
0.04
0.00
0.13
0.18
Copper
0.15
1.12
0.02
3.77
5.05
Lead
0.01
0.07
0.00
0.24
0.32
Mercury
0.00
0.00
0.00
0.01
0.01
Molyb-
denum
0.01
0.02
0.00
0.06
0.08
Nickel
0.01
0.03
0.00
0.09
0.12
Selenium
0.01
0.03
0.00
0.06
0.09
Zinc
0.18
1.93
0.15
5.60
7.85
Total
Phos-
3.72
21.68
6.27
138.96
170.62
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I a aware that there are significant penalties for submitting false information,
inc ding the p sibilit f mes and imprisonment for knowing violations"
Signature of Land Applier natP

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 51.86
Permit #: WQ 30998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 21 Acres Permitted: 21 Site #: 1 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WR2019 10-19 9-024-0208 C19-024-020 C19-024-02 CI9-024_w cio.ma.w
Sample
orCom-
posite
Date
9/24/19
1/23/19
1/23/19
1/23/19
-- --
1/23/19
- - -- --
1/23/19
% Solids
2.87
2.45
2.45
2.45
2.45
2.45
Arsenic
10.40
5.00
5.00
5.00
5.00
5.00
Cadmium
10.40
1.00
1.00
1.00
1.00
1.00
Chromium
14.80
1 0.00
0.00
0.00
0.00
0.00
Copper
223.00
191.00
191.00
191.00
191.00
191.00
Lead
24.50
10.60
10.60
10.60
10.60
10.60
Mercury
0.70
0.29
0.29
0.29
0.29
0.29
Molyb-
denum
10.40
5.19
5.19
5.19
5.19
5.19
Nickel
10.40
12.60
12.60
12.60
12.60
12.60
Selenium
10.40
5.00
5.00
5.00
5.00
5.00
Zinc
599.00
573.00
573.00
573.00
573.00
573.00
Total
Phos-
horus
13,200
27,300
27,300
27,300
27,300
27,300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�o
0
0.28
0.23
1.02
0.26
0.26
0.41
a
�-
Arsenic
0.01
0.00
0.01
0.00
0.00
0.00
0.03
Cadmium
0.01
0.00
0.00
0.00
0.00
0.00
0.01
Chromiutr
0.01
0.00
0.00
0.00
0.00
0.00
0.01
Copper
1 0.13
0.09
0.39
0.10
0.10
0.15
0.96
Lead
0.01
0.00
0.02
0.01
0.01
0.01
0.06
Mercury
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Molyb-
denum
0.01
0.00
0.01
0.00
0.00
0.00
0.03
Nickel
0.01
0.01
0.03
0.01
0.01
0.01
0.06
Selenium
Selenium
0.01
0.00
0.01
0.00
0.00
0.00
0.03
Zinc
0.34
0.27
1.17
0.30
0.30
0.46
2.84
Total
Phos-
7.52
12.70
55.86
14.34
14.24
22.13
126.79
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
incl ding a po IbiWilnes and imprisonment for knowing violations"
c:............ .ri __J A__,:__ _

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 9.81
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 4.14 Acres Permitted: 4.14 Site #: 1 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C19-024-0208 9-024-0208
IRNMEN10000010
®
11
11
•
Phos-
MorusiMMENEEMENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
M.
swim
'Total
.�.
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including th oss-ibility of fines and imprisonment for knowing violations"
Signature of Land ADDlier t1��P

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Triple S Farms Total Dry Tons Applied (Annual): 35.40
Permit #:
WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator:
Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used:
11.2 Acres Permitted: 11.2 Site #: 1 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C19-024.0208 9-024-0208
Sample
or Com-
1/23/19
1/23/19
posite
Date
% Solids
2.45
2.45
Arsenic
5.00
5.00
Cadmium
1.00
1.00
Chromium
0.00
0.00
Copper
191.00
191.00
Lead
10.60
10.60
Mercury
0.29
0.29
Molyb-
denum
5.19
5.19
Nickel
12.60
12.60
Selenium
5.00
5.00
Zinc
573.00
573.00
Total
Phos-
27,300
27,300
horus
rinnuai ,heavy wietai r iela Loanin s Calculated in lbs/acre :
' uOrly#=
'
t
t
----------
mom
t a
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am a are that there are significant penalties for submitting false information,
inclu g the ssi kity of f and imprisonment for knowing violations"
:25--r
Signature of Land Applier nnti-

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 2.71
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series GoA
Acres Used: 13.95 Acres Permitted: 13.95 Site #: 1 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
SWP 2019 1-19 P 2019 1-19
Sample
or Com- 4/22/19 4/22/19
posite
Date
% Solids 2.58 2.58
Arsenic 7.79 7.79
Cadmium 7.79 7.79
Chromium 7.79 7.79
Copper 60.10 60.10
Lead 7.79 7.79
Mercury 0.70 0.70
Molyb- 7.79 7.79
denum
Nickel 7.79 7.79
Selenium 7.79 7.79
Zinc 477.00 477.00
Total
Phos- 19,600 19,600
horns
A
nnual
Heavy Metal ri 0 Loadings (Calculated
in lbs/acre):
-e
� y w
0.10 0.10
O
Arsenic
0.00
0.00
0.00
Cadmium
0.00
0.00
ChromiuTT
0.00
0.00
0.00
Copper
0.01-F
0.01
0.00
0.02
Lead
0.00
1 0.00
0.00
Mercury
0.00
0.00
0.00
Molyb-
0.00
denum
0.00
0.00
Nickel
0.00
0.00
0.00
Selenium
0.00
0.00
0.00
0.09
0.09
0.19
[Zinc
Total
Phos- 3.81 3.81
phorus 7 62
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
incl ing the oss' 11*ty off es and imprisonment for knowing violations"
%cmafilPa nfT --A A-..-1:..-

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 6.67
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 14.5 Acres Permitted: 14.5 Site #: I Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
B201910-19
Non
• ..Phos-
Total
. 11
h
. .
P .
1:
. .
1:
--i cernry, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possi ility of fi d imprisonment for knowing violations"
% 1,
Sienature of Land AnnliPr r`

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 29.38
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series GoA
Acres Used: 8.93 Acres Permitted: 8.93 Site #: 1 Field #: 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use m&g, % Solids use Raw Percent #):
WR2019 10-19 K2019 1-19 WR2019 10-
amp e
or Com-
posite
9/24/19
6/5/19
9/24/19
Date
Solids
2.87
0.51
2.87
Arsenic
10.40
39.20
10.40
Cadmium
10.40
39.20
10.40
Chromium
14.80
39,20
14.80
Copper
223.00
806.00
223.00
Lead
24.50
39.20
24.50
Mercury
0.70
4.71
0.70
Molyb-
denum
10.40
39.20
10.40
Nickel
10.40
39.20
10.40
Selenium
10.40
39.20
10.40
Zinc
599.00
971.00
599.00
Total
Phos-
13,200
20,600
13,200
Chorus
Annual
Heavy Metal Field Loadings
(Calculated
in lbs/acre):
�? 0
1.27 0.11 1.90
"Ga
�
Arsenic
0.03 10.01
0.04
0.08
Cadmium
0.03 1
0.01
0.04
0.08
Chromium
0.04
0.01
0.06
0.10
Copper
0.57
0.18
0.85
1.60
Lead
0.06
0.01
0.09
0.16
Mercury
0.00 1
0.00
0.00
0.01
Molyb-
denum
0.03
0.01
0.04
0.08
Nickel
0.03
0.01
0.04
0.08
Selenium
0.03
0.01
0.04
0.08
Zinc
1.53
0.22
2.28
4.03
Total
Phos-
33.61
4.71
50.24
88.56
[_
PhoruLl______L
_j
I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inc ding a po {bility nes and imprisonment for knowing violations"
Signature of Land Aonlier n�+A

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As —
Arsenic
Cd
— Cadmium
Cr —
Chromium
Cu
— Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients (lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
Owner: Eric Smith
)perator: Eric Smith
Crop 1 Name: Bermudagmss
WQ Permit #: WQ0030998
.nnual Dry Tons Applied: 132.49
Predominat Soil Series
Crop 1 Max PAN:
NoA
Field #: I Acres Utilized: 34.20
Site #: 1 Acres Permitted: 34.20
Cation Exchange Capacity (non 503): NA
299.00 Crop 2 Name: Small Grain
Crop 2 Max. PAN 50.00
C7
w
7 CD
c
ISPecify
Totals
Per Acre
Solids
As
Decimal
Volume
A lied r
Pp
Acre
DT/Ac
Residual Sources
(NPDES #, W #,
Q
Fert., Animal Waste.
etc.)
Site
Cond.
(Dry,
Wet'
Moist)
Preci p'
Past 24
Hrs.
t,c�
>
3
�.
o
. 0
'
o
a : --
F; IF
+ N
» ^
=1
;v q
� rs M
; N
`
�'
TKN
z >
^ R
o
> >
Nitrate
and
Nitrite
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Gal'
Cu.Yd.
Re port
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Ian-19
42,000
1,228
0.51
0.03
Kenansville WWTP
S
030
0.30
33,400
20
2,500
0.65
X
web-19
65,200
1,906
2.45
0.19
LiltleCreek WRF
S
0.50
0.30
82,800
4,400
4,040
11.59
X
zeb-19
384.000
11,228
2.57
1.20
Wallace WWTP
IN
1.00
0.30
7,020
1,960
3,900
17.73
X
dar-19
69,000
2,018
2.22
1 0.19
eeulaville WWTP
S
0.50
0.30
40,100
5
199
4.57
X
star--19
240.000
7,018
2.57
0.75
Wallace WWTP
IN
1.00
0.30
7,020
1,960
3,900
11.08
X
kpr-19
156,000
4,561
2.87
0.55
Warsaw WWTP
S
0.50
0.30
26,800
3
10
8. 99
X
4ay-19
80.000
2,339
2.22
0.22
9eulavillc WWTP
S
0.50
0.30
40,100
5
199
5.30
X
un-19
144,000
4,211
2.87
0.50
Warsaw WWTP
S
0.50
0.30
26,800
3
10
8.11
X
)ec-19
83,0W
2.427
2.45
0.25
Little- Creek WRF
S
0.50
0.30
82,800
4,400
4.040
14.76
X
OTALS:
36,936
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
nnuallbs/acre
0.13
0.12
0.17
4.66
0.32
0.01
0.09
0.14
0.13
9.35
136.08
37.85
44.73
Date
lbs/ac
urrent Cumulative Ibs/acre
0.77 0.74 NA 44.44 4.25 0.08 NA 1.51 0.92 8
0.64 0.61 NA 39.77 3.94 0.07 NA 1.37 0.79 E2t.48
36 34 NA 1,338 267 15 NA 374 89
299 50_00
for Years Cumulative lbs/acre
srmitted C. P. L. R.****
:rmit PAN Limit- Ist/2nd Crop
cernry, ureter penalty or taw, that this document was prepared under my direction or supervision in accordance with a system
xigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
;niftcant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
f *Application Method: S - Surface IN - Injection, INC - Incorporation PP , J ► potation
**Volitilization Rate: Surface - 0.5 Iniectio � n/Incorporatton -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name:
Owner:
Dperator:
Triple S Farms
Eric Smith
Eric Smith
Crop 1 Name: Bermudograss
WQ Permit #: WQ0030998
.nnual Dry Tons Applied: 24.33
Field #:
Acres Utilized: 8.48
Site #: 2 Acres Permitted: 9.48
Predominat Soil Series FoA Cation Exchange Capacity (non 503): NA
Crop 1 Max PAN: 276.00 Crop 2 Name: Small Grain Crop 2 Max. PAN 50.00
C1
o
o c^o
c
Totals
Per Acre
% Solids
As
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert ,Animal Waste,
etc.)
Site
Cond.
(Dry,
Wet,
Moist)
Precip.
Past 24
Hrs.
trxhes
o
3 L,
�'
0 n
t '
g
a ^:
+� N
a
C
* iv
# 5'
TKN
_z a
3
i3 3
a„ o
g
Nitrate
and
Nitrite
PAN Applied
PP
(lbs/acre)
Must Select
Crop I or Crop 2
.SpeciN,
Gal.
Cu.Yd.
Report
TotalsDecimal
n Gal.
Crop I
Crop 2
Crop I
Crop 2
Jan-19
36,000
4,245
0.51
0.09
Kenansville WWTP
S
0.50
0.30
33,400
20
2,500
2.26
X
Feb-19
48,000
5,660
2.57
0.61
Wallace WWTP
IN
1.00
0.30
7,020
1,960
3,900
8.94
X
Jul-19
12,600
1,486
2.58
0.16
Soud vest Planation
S
0.50
0.30
82,900
2,410
105
1 8.14
X
Jul-19
177,177
20,894
2.31
2.01
Walbee WWTP
IN
1.00
0.30
44.100
2,810
1,180
65.96
1 X
'OTALS:
32.285
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime Applied
.nnuallbs/acre
0.09
0.09
0.18
5.05
0.32
0.01
0.08
0.12
0.09
7.85
170.62
74.10
11?0
Date
Ibs/ac
'urrent Cumulative lbs/acre
0.69 0.67 NA 36.29 3.58 0.07 NA 1.33 0.75 69.91
0.59 0.58 NA 31.24 3.26 0.06 NA 1.21 0.66 62.06
36 34 NA 1,338 267 15 NA 374 89 2,498
F 776 1 50.00
rior Years Cumulative lbs/acre
ermitted C. P_ L. R.****
ermit PAN Limit Ist/2nd Crop
t certtty, under penalty of taw, that this document was prepared under my direction or supervision in accordance with a system
esigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
gnificic)ant penalties for submitting f se information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #: 1 Acres Utilized: 21.00
Owner: Eric Smith .nnual Dry Tons Applied: 51.86 Site #: 3 Acres Permitted: 21.00
3perator: Eric Smith Predominat Soil Series FoA Cation Exchange Capacity (non 503): NA
Crop 1 Name: Bermudagrass. Crop 1 Max PAN: 276.00 Crop 2 Name: small Grain Crop 2 Max. PAN 50•00
ol7
.. !
7 a
SP=1
Totals
Per Acre
%Solids
As
Decimal
Volume
Applied per
Acre
DT(Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(Dry,
Wet,
Moist)
Precip
Past 24
Hrs.
t,u
�
3 a
n.
ry
* �'
'
c
* N
7a a
=
*
* 7
TKN
Z a
• B
a o
g
Nitrate
and
Nitrite
PAN Applied
PP
(]bs/acre}
Must Select
Crop 1 or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop I
Crop 2
Jan-19
50,000
2,381
2.87
0.28
Warsaw WWTP
S
0.50
030
26,800
3
10
4.59
X
Mar-19
47,300
2 276
2.45
0.23
tittle Creek WRF
S
0.50
0.30
82,800
4,400
4,040
13.84
X
Sep-19
210,300
10,014
2.45
1.02
t.inle creek WRF
S
0.50
0.30
82,800
4,400
4,040
60.90
1 X
Oct-19
54,000
2,571
2.45
0.26
UttL- Creek WRF
S
0.50
030
82,800
4,400
4,040
15.64
X
V0v-19
53,600
2,552
2A5
0.26
LinleCreek WRF
S
0.50
0.30
82,800
4,400
4,040
15.52
X
Dec-19
83.300
3,967
2.45
0.41
Little Creek WRF
S
0.50
0.30
82,800
4,400
4,040
24.12
X
'OTALS:
23,762
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
.nnuallbs/acre
0.03
0.01
0.01
0.96
0.06
0.00
0.03
0.06
0.03
2.84
126.79
90.37
44.23
Date I
Ibs/ac
urrent Cumulative lbs/acre
0.37 0.33 NA 18.27 1.62 0.04 NA 0.61 0.43 36.74
0.34 0.32 NA 17.31 1.56 0.04 NA 0.55 0.40 33.90
36 34 NA 1,338 267 15 NA 374 89 2,498
1 276 50.00
rior Years Cumulative lbs/acre
=itted C. P. L. R.****
!rmit PAN Limit Ist/2nd Crop
1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
.signed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
gnificant penalties for submitti false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
t;�D **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
Owner: Eric Smith
Operator: Eric Smith
Crop I Name: Small Grain
WQ Permit #: WQ0030998 Field #:
.nnual Dry Tons Applied: 9.81 Site #:
Predominat Soil Series FoA
Crop 1 Max PAN: 115.00 Crop 2 Name:
Acres Utilized: 4.14
4 Acres Permitted: 4.14
Cation Exchange Capacity (non 503): NA
Fescue Crop 2 Max. PAN 50.00
t7
o m
co
Specify
Totals
Per Acre
% Solids
AS
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert.. Animal Waste,
etc.)
Site
Cond.
(Dry'
Wet.
Moist)
Preci p
Past 24
Hrs.
t„c
a
3
a `_'-.
0 n
a o•
o
p
+ '
#
`;
5
� R
� d
; N
}
�'
TKN
Z
3
a a
g
Nitrate
and
Nitrite
PAN Applied
PP
(Ibs/acre)
Must Select
Crop I or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop I
Crop 2
Crop 1
Crop 2
Mar-19
30,00D
7,246
2.45
0.74
UnL-Creek WRF
S
0.50
0.30
82,800
4,400
4,040
44.06
X
Sep-l9
66.000
15,942
2.45
1.63
Little Creek WRF
S
0.50
0.30
82,800
4,400
4,040
96.94
X
'OTALS:
23,188
As
Cd
Cr
Cu
Pb
HR
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime Applied
►nnuallbs/acre
0.02
0.00
0.00
0.90
0.05
0.00
0.02
0.06
0.02
2.71
129.35
96.94
44.06
Date
Ibs/ac
:urrent Cumulative 1bs/acre
0.18 0.17 NA 11.07 0.76 0.02 NA 0.57 0.24 31.21
0.16 0.16 NA 10.17 0.71 0.02 NA 0.51 0.21 28.50
36 34 NA 1,338 267 IS NA 1 374 89 2,498
1 115 50.00
'rior Years Cumulative Ibs/acre
'etmitted C. P. L. R.****
lermitPA limitlsinnaCrop
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
esigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
ignificant penalties ting false information, including the possibility of fines and imprisonment for knowing violations."
t' ,r *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - OA
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
Acres Utilized: 11.20
Site #: 5 Acres Permitted: 11.20
)perator: Eric Smith Predominat Soil Series FoA Cation Exchange Capacity (non 503): NA
WQ Permit #: WQ0030998 Field #:
Owner: Eric Smith ,nnual Dry Tons Applied:
Crop 1 Name:
Fescue
35.40
Crop 1 Max PAN: 207.00 Crop 2 Name: Small Grain
Crop 2 Max. PAN 50.00
o 0
Fr o
Specify
Totals
Per Acre
%Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert,Animal Waste,
etc.)
Cond.
(Dry,
Wet,
Moist)
Precip'
Past 24
Firs.
t„c
3 4J
� �
�r �'
o
¢ o'
>
� �
:;
z '
� �,
F
;
o
TKN
? >
3 �
tro o
cz
o �•
Nitrate
and
Nitrite
PAN Applied
(]bs/acre)
Must Select
Crop l or Crop 2
Gal.
CUM&
Report
Totals
in Gal.
Crop I
Crop 2
Crop l
Crop 2
tan-19
280,700
25,063
2.45
2.56
little Creek WRF
S
0.50
0.30
82,800
4,400
4,040
152.40
X
4ov-19
65,800
5,875
2.45
0.60
little Creek WRF
S
0.50
030
82,800
4,400
4,040
35.73
X
OTALS:
30,938
As
Cd
Cr
Cu
Pb
Hit
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
nnuallbs/acre
0.03
0.01
0.00
1.21
0.07
0.00
0.03
0.08
0.03
3.62
172.58 1
152.40
35.73
Date
lbs/ac
urrent Cumulative lbs/acre
0.47 0.44 NA 20.91 2.01 0.05 NA 0.83 0.51 3931
0.44 0.43 NA 19.71 1.94 0.05 NA 0.75 0.48 35.69
36 34 NA 1,338 267 15 NA 374 89 2,498
F207 50.00
for Years Cumulative Ibs/acre
:rmitted C. P. L. R.****
:rmit PAN Limit lst/2nd Crop
certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
:signed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
;nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
��--7IN*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD RRVI IARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
WQ Permit #: W00030998 Field #:
Owner: Eric Smith nnual Dry Tons Applied: 2.71 Site #:
)perator: Eric Smith Predominat Soil Series GoA
Crop 1 Name: Forest Crop 1 Max PAN: 60.00 Crop 2 Name:
I Acres Utilized:
13.95
6 Acres Permitted:
13.95
Cation Exchange Capacity (non 503):
NA
#N/A Crop 2 Max. PAN
#N/A
� O _
w
s c
Specify
Totals
Per Acre
°°Solids
Decimal
Volume
Applied per
Acne
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,(Dry
Site
Cond.
Moist)
Prccip
Past 24
Hrs.
t, .
-o
g �
_
* c
°
'
o
;u ':
m
+ N
* w
�
a n
R
# p
Et
_
TKN
z Y
• �
o a
CV m.
Nitrate
and
Nitrite
mWice
PAN Applied
PF
(lbs/acre)
Must Select
Crop 1 or Crop
F P
2
Gal.
Cu.Yd.
Report
Totalsetc.)Wet
n Gal.
Crop 1
Crop 2
Crop 1
Crop 2
'eb-19
12,600
903
2.58
0.10
Southwest Plantation
S
0.50
0.30
82,900
2,410
105
4.95
X
kpr--19
12,600
903
2.58
0.10
Southwest Plantation
S
0.50
0.30
82,900
2,410
105
4.95
X
'-Hg
DTALS:
1,806
As
Cd
Cr
Cu
Pb
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
nnuallbs/acre
0.00
0.00
0.00
0.02
0.00
0.00
0.00
0.00
0.00
0.19
7.62
9.90
0.00
Date
Ibs/ac
arrent Cumulative lbs/acre
0.05 0.05 NA 0.29 0.05 0.00 NA 0.06 0.05 1.48
0.04 0.04 NA 1 0.26 0.04 1 0.00 NA 0.06 0.04 1.30
36 34 NA 1,338 267 t5 NA 374 89 2,498 _
60 1 #NIA
for Years Cumulative lbs/acre
xmitted C. P. L. R.****
:rmit PAN Limit 1 st/2nd Crop
certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
;signed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
mificant penaltXobmittin a se information, including the possibility of fines and imprisonment for knowing violations."
_ *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rat
DENR FORM FSF N2MnnF1

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #• W00030998
Owner: Eric Smith ,nnual Dry Tons Applied:
Dperator: Eric Smith Predominat Soil Series
Crop 1 Name: Bermudagrass
Field #: I Acres Utilized: 14.50
Site #: 7 Acres Permitted: 14.50
Cation Exchange Capacity (non 503): NA
Crop 1 Max PAN: 276.00 Crop 2 Name: MIA Crop 2 Max. PAN #N/A
6.67
FoA
oG
n)
'Specify!
Totals
Per Acre
%Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fenn, Animal Waste,
etc.)
Site
Cond.
(Dry'
Wet,
Moist)
Preci p
Past 24
Hrs.
a
-Z
a
c G
c
=
N
3
TKN
z a
o a
q g
Nitrate
and
Nitrite
PAN Applied
pp
(lbs/acre)
Must Select
Crop 1 or Crop 2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop I
Crop 2
Oct-19
72,000
4,966
2.22
0.46
1t i ine wwrP
S
0.50
0.30
40,100
5
199
11.24
X
'OTALS:
4,966
As
Cd
Cr
Cu
Pb
Ha
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
0.01
0.01
0.02
0.42
0.03
0.00
0.01
0.01
0.01
1.52
15.08
11.24
0.00
Date
Ibs/ac
Innuallbs/acre
utrent Cumulative Ibs/acre
0.01 0.01 NA 0.42 0.03 0.00 NA 0.01 0.01 1.52
0.00 0.00 NA 0.00 0.00 0.00 NA 0.00 0.00 0.00
36 34 NA 1.338 267 15 NA 374 89 2.498
276 #N/A
nor Years Cumulative lbs/acre
ermitted C. P. L. R.****
ermit PAN Limit Ist(2nd Crop
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
esigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
gnificant penaltTW
submit ' false information, including the possibility of fines and imprisonment for knowing violations."
� *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Iniection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms
Owner: Eric Smith
Operator: Eric Smith
Crop 1 Name: Bermudagnus
WQ Permit #: WQW30998 Field #:
.nnual Dry Tons Applied: 29.38 Site #:
Predominat Soil Series GoA
Crop 1 Max PAN: 299.00 Crop 2 Name:
I Acres Utilized:
8.93
9 Acres Permitted:
8.93
Cation Exchange Capacity (non 503):
NA
Small Grain Crop 2 Max. PAN
50.00
C7
o
Fr o
Totals
Per Acre
�O Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #. WQ#.
Fen.., Animal Waste,
etc.)
Site
Cond.
(Dry,
Wet,
Moist)
Precip
Past 24
Hrs.
Inches
b
o
�.
o
a =.
o
c
;n `
*
S
;
=
* n
; ^
o
n
TKN
Z a
3
c
�•
Nitrate
and
Nitrite
PAN Applied
PP
(ibs/acre)
Must Select
Crop I or Crop 2
rRepon
Crop I
P
Crop 2
P
Crop 1
p
Crop 2
p
Jan-19
95,000
10,638
2.87
1.27
Warsaw WWTP
S
0.50
0.30
26,800
3
10
2070
X
Sep-19
48,000
5,375
0.51
0.11
Kenansville WWTP
S
0.50
0.30
33,400
20
2,500
2.86
X
Sep-19
142,000
15,901
2.87
1.90
Warsaw WWTP
S
0.50
0.30
26,800
3
10
30.64
X
"OTALS:
31,915
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P IPAN
1
PAN 2
Lime Applied
innualIbs/acre
0.08
0.08
0.10
1.60
0.16
0.01
0.08
0.08
0.08
4.03
88.56
33.51
20.50
Date
lbs/ac
:urrent Cumulative lbs/acre
0.16 0.25 NA 4.20 0.36 0.01 NA 0.25 0.25 8.57
0.09 0.17 NA 2.60 0.19 0.00 NA 0.17 0.17 4.54
36 34 NA 1,338 267 15 NA 374 89 2,498
299 50.00
'rior Years Cumulative Ibs/acre
'ermitted C. P. L. R.****
'ermit PAN Limit I st/2nd Crop
1 certify, under penalty or law, that this document was prepared under my direction or supervision in accordance with a system
esigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
ignificant penalties for subm� 'ng false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method. S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

RESIDUAL ANALYSIS LAB SHEETS

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms
Beulaville WWTP
B2019 10-19
9/23/2019
10/8/2019
Annual 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.22
Nitrogen (TKN)*
4.010
40,100.000
Phosphorus
1.640
16,400.000
Potassium
0.364
3,640.000
Sulfur
0.000
Calcium
2.070
20,700.000
Magnesium
0.178
1,780.000
Sodium
0.595
5,950.000
Iron
---
Aluminum
---
6,350.000
Manganese
---
Copper
---
459.000
1,500
Zinc
---
1,650.000
2,800
Ammonia Nitrogen*
0.000
4.500
Nitrate N / Nitrite N*
---
199.000
Cadmium
---
13.500
39
Chromium
---
18.600
1,200
Nickel
---
13.500
420
Lead
---
28.100
300
Arsenic
---
13.500
41
Mercury
---
2.610
17
Selenium
---
13.500
100
pH
3.650
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.010
Molybdenum
---
13.500
75
Chloride
---
Boron
Available P2O5
Specific Gravity

Beulaville WWTP
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms
Annual 2019
Date Reported: 10/8/2019 Report No: B2019 10-19
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
24.460
PAN Inj.
24.464
P
32.800
K
7.280
Lime (estimated)
0.000
Secondary Nutrients
Calcium
41.400
Magnesium
3.560
Sodium
11.900
SAR
1.585
Chloride
0.000
Iron
0.000
Alumium
12.700
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
2.22
pH
3.650
Min Rate
0.300
Metals
Arsenic
0.027
Cadmium
0.027
Chromium
0.037
Copper
0.918
Lead
0.056
Mercury
0.005
Molybdenum
0.027
Nickel
0.027
Seleniun
0.027
Zinc
3.300
2015
2016
2017
2018
0.30
24.06
2019
0.15
8.42
2020
0.08
3.58
2021
0.04
1.66
2022
2023
2024
2025

Environmental Chemists, Inc.
enviroc em6602 Windmill Way, Wilmington, NC 2W5 •
710 Bowsertown Road, Manteo, NC 27950.392.52.4 Lab 910/Fa., 424 Fax
gam' 25_ 473.57p2 Lab/Fae
?55-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
infoCaenvironmentalchemists.com
Town of Beulaville Date of Report: Oct 08, 2019
Post Office Box 130
Beulaville NC 28518 Customer PO #: Attention: Angie Miller Customer ID: 08100015Report #: 2019-16107
Project ID: Sludge
Lab 1D Sample 1D: Collect Date/Time Matrix
19-41363 Site: Sludge Sampled by
9/23/2019 2:00 PM Solid/Sludge client
Test Method
Sludge Residuals Results Date Analyzed
Aluminum EPA 200.7
6350 mg/kg 10/01/2019
Arsenic EPA 200.7
<13.5 mg/kg 10/01/2019
Cadmium EPA 200.7
<13.5 mg/kg 10/01/2019
Calcium EPA 200.7
20700 mg/kg 10/02/2019
Chromium EPA 200.7
18.6 mg/kg 10/01/2019 Copper EPA zao.7
Lead EPA 200.7 459 mg/kg 10/01/2019
Magnesium EPA 200.7 28.1 mg/kg 10/01/2019
EPA 200.7
Molybdenum 1780 mg/kg 10/01/2019
<13.5 mg/kg 10/01/2019
Nickel EPA zoo 7
<13.5 mg/kg 10/01/2019
Potassium EPA 200.7
3640 mg/kg 10/01/2019
Selenium EPA 200.7
<13.5 mg/kg 10/01/2019
Sodium EPA 200.7
Zinc EPA 200.7 5950 mg/kg 10/01/2019
Nitrate+Nitrite-Nitrogen EPA353.2 1650mg/kg 10/01/2019
Total Solids N SM 2540 B 199 mg/kg . 09/28/2019
PH SM 4500 H t3 2.22% 09/26/2019
Ammonia Nitrogen SM 4500 NH3 C 3.65 units 10/04/2019
Total Kjeldahl Nitrogen (TKN) SM asao ors B <4.5 mg/kg 09/26/2019
Total Phosphorus SM 4500 P F 40100 mg/kg 09/27/2019
Mercury swags 7471s 16400 mg/kg 10/03/2019
Comment: Results reported on a dry weight basis. pH reported on an as received basis. g/kg 09/28/2019
Reviewed by

• r
ENVIRONMENTAL CHEMISTS, INC 910.392.0223 252.473.5702
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATON # 94 NCDHHS: DLS CERTIFICATION # 37729 Info®environmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Town of Beulavlile
ADDRESS:
e PROJECT NAME: Annual Sludge
JREPORTNO:
CONTACT NAME:
PO NO:
REPORT TO: PHONE/FAX:
COPY TO:
Sampled By: r
email:
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge,
Collection & Otf�er.
Sample Identification
PRESERVATION
op a _c (7 c p W
o
D e
CL
E E ` a = E m z v $ S ANALYSIS REQUESTED
Time Temp �, S 3 z z=
Slud
� 9 �
C P
a
f� 3Gi
G G `� x Fu LP
C P
G G X Nutrients/Metals
C P
G G x I
C P
G G
C P
G G
C P
G G
C P
G G
C P
G G
C P
G G
DOlvered By: Comments: Received By:
Time: 5` �_

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Clayton
Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
19-024-0208
1/23/2019
2/6/2019
Annual 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
-2.45
Nitrogen (TKN)*
8,280
82,800.000
Phosphorus *
2.730
27,300.000
Potassium
0.590
5,900.000
Sulfur
0.000
0.000
Calcium
2.070
20,700.000
Magnesium
0.528
5,280.000
Sodium
0.187
1,870.000
Iron
---
Aluminum
---
8,200.000
Manganese
---
Copper
---
191.000
1,500
Zinc
---
573.0O0
2,800
Ammonia Nitrogen*
0.440
4,400.000
Nitrate N / Nitrite N*
---
4,040.000
Cadmium
---
1.000
39
Chromium
---
1,200
Nickel
---
12.600.
420
Lead
---
10.600
300
Arsenic
---
5:0W
41
Mercury
---
0.290
17
Selenium
---
5:00.0
100
H
.5
Calcium Carbonate E . (es
t)
0.000
Organic Nitrogen
7.840
Molybdenum
---
5.1W
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340

Wastewater Treatment Plant
Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2019
Date Reported: 2/6/2019 Report No: 19-024-0208
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
59.520
PAN Inj.
63.920
P
54.600
K
11.800
Lime (estimated)
500.000
Secondary Nutrients
Calcium
41.400
Magnesium
10.560
Sodium
3.740
SAR
0.469
Chloride
0.000
Iron
0.000
Alumium
16.400
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.45
pH
5.800
Min Rate
0.300
Metals
Arsenic
0.010
Cadmium
0.002
Chromium
0.000
Copper
0.382
Lead
0.021
Mercury
0.001
Molybdenum
0.010
Nickel
0.025
Seleniun
0.010
Zinc
1.146

Waypdlont,(2)
ANALYTICAL
2/6/2019
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 19-024-0208
Project Description: Holding Tank
Waypoint Analytical Virginia, Inc. received sample(s) on 1/24/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P..µ 'r 6.7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007

(2)
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-024-0208
Client Project Description: Holding Tank
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
64533
Holding Tank
Solids
01/23/2019
10:30
01/24/2019
64533
Holding Tank
Solids
01/23/2019
10:30
01/24/2019
SM-4500-NH3C
WTN
64533
Holding Tank
Solids
01/23/2019
10:30
01/24/2019
9045D
WTN
64533
Holding Tank
Solids
01/23/2019
10:30
01/24/2019
4500NO3F-2011
WTN
64533
Holding Tank
Solids
01/23/2019
10:30
01/24/2019
6010D
WTN
64533
Holding Tank
Solids
01/23/2019
10:30
01/24/2019
SW-7471B
WTN
64533
Holding Tank
Solids
01/23/2019
10:30
01/24/2019
SM-4500-NH3C-TKN
WTN
64533
Holding Tank
Solids
O1/23/2019
10:30
01/24/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 19-024-0208
Account Number: 46546
Send To: Town Of Clayton
POB 879
Clayton, NC 27528
Lab Number: 64533
Sample Id : Holding Tank
Waypoint(2)
ANALYTICAL
Project: Holding Tank
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 1/23/2019 10:30:00
Date Received: 01 /24/2019 00:00
Date Reported: 02/06/2019
Arsenic
<5.00
5.00
CCR
01/29/2019 20:39
Mercury
0.290
0.0154
TJS
01/29/201911:49
Selenium
<5.00
5.00
CCR
01/29/2019 20:39
pH *
5.8
JSL
01/30/2019 08:49
Molybdenum
5.19
2.50
CCR
01/29/2019 20:39
Silver
<2.50
2.50
CCR
01/29/2019 20:39
Sodium Absorption Ratio "
2.99
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series
is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding Time
Pofi&
601 OD
SW-7471 B
601 OD
9045D
601 OD
6010D
CALCULATION
X 1011rf
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made
to the work the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization
Pauric McGroary
Agronomist

Report Number: 19-024-0208
Account Number: 46546
Send To: Town Of Clayton
POB 879
Clayton , NC 27528
Lab Number: 64533
Sample Id : Holding Tank
Waypoint(2)
ANALYTICAL
Project: Holding Tank
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 1/23/2019 10:30:00
Date Received: 01 /24/2019 00:00
Date Reported: 02/06/2019
Total Solids "
2.45
24500
100.0
CJR
01/29/2019 15:55
SM-254OG
Moisture `
97.50
100.0
CJR
01/29/2019 15:55
SM-2540G
Total Kjeldahl Nitrogen
8.28
82800
250
CLP
01/31/2019 14:30
SM-4500-NH3C-TKN
Phosphorus
2.73
27300
50.0
CCR
01/29/2019 20:39
6010D
Potassium
0.59
5900
50.0
CCR
01/29/2019 20:39
6010D
Calcium
2.07
20700
250
KKM
01/30/201913:48
6010D
Magnesium
0.53
5280
50.0
CCR
01/29/2019 20:39
601OD
Sodium
0.19
1870
250
CCR
01/29/2019 20:39
601OD
Aluminum
8200
50.0
CCR
01/29/2019 20:39
6010D
Copper
191
2.50
CCR
.01/29/2019 20:39
601OD
Zinc
573
12.5
CCR
01/29/2019 20:39
601OD
Ammonia Nitrogen
0.44
4400
100
ZBD
01/31/2019 12:15
SM-4500-NH3C
Organic N
7.84
78400
250
DH
01/31/2019 12:15
CALCULATION
Nitrate+Nitrite-N
4040
4.68
ZBD
02/01/2019 09:43
4500NO3F-2011
Cadmium
<1.00
1.00
CCR
01/29/2019 20:39
601OD
Nickel
12.6
2.50
CCR
01/29/2019 20:39
601OD
Lead
10.6
3.00
CCR
01/29/2019 20:39
601OD
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet
basis.
B-Analyte detected in blank
H - Beyond Holding Time
pwic-
MC V0~1
Our reports and letters are for the evclusrve and confidential use of our clients and may not be reproduced rn whole or part nor may any reference be made Pauric McGroary
to the work the results, or the company in any advertising news release, or other public announcements without obtaining our prior written authorization
Agronomist

Waypoint-W
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46646
Customer Name: Town Of Clayton
Report Number: 19-024-0208
Shipping Method
Fed Ex US Postal Lab
UPS Client Courier
Other:
Thermometer ID:
Shipping container/cooler uncompromised?
10 Yes
No
Number of coolers received
I '
Custody seals intact on shipping container/cooler?
Yes
No
Not Required
Custody seals intact on sample bottles?
Yes
No
Not Required
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
No
Water - Sample containers properly preserved
Yes
No
N/A
Water - VOA vials free of headspace
Yes
No
N/A
Trip Blanks received with VOAs
Yes
No
N/A
Soil VOA method 5035 — compliance criteria met
Yes
No
N/A
High concentration container (48 hr) Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
I. No
Comments:
Signature: Brandi Watson
Date & Time: 01/24/2019 12:52:05

WASTEWATER SAMPLE TRH
•
19-024 ozos
Waypo
����������������,��
46546
Town Of Clavlon
01-24-2019
7021 Whilehine Road Richmond VA 23237 TO: 804-743 Holdina Tank
12:51:29
'ODY Account #
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Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen. ' 0
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium. Oil and Grease (EPA), _ 2y 5
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
�3`N

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms
Kenansville WWTP
K2019 1-19
6/5/2019
6/5/2019
Annual 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
0.51
Nitrogen (TKN)*
3.340
33,400.000
Phosphorus
2.060
20,600.000
Potassium
0.598
5,980.000
Sulfur
0.000
Calcium
2.490
24,900.000
Magnesium
0.304
3,040.000
Sodium
2.000
20,000.000
Iron
---
Aluminum
---
8,530.000
Manganese
---
Copper
---
806.000
1,500
Zinc
---
971.000
2,800
Ammonia Nitrogen*
0.002
19.600
Nitrate N / Nitrite N*
---
2,500.000
Cadmium
---
39.200
85
Chromium
---
39.200
1,200
Nickel
---
39.200
420
Lead
---
39.200
300
Arsenic
---
39.200
41
Mercury
---
4.710
17
Selenium
---
39.200
100
pH
7.390
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.338
Molybdenum
---
39.200
75
Chloride
---
Boron
Available P2O5
Specific Gravity

Kenansville WWTP
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms
Annual 2019
Date Reported: 6/5/2019 Report No: K2019 1-19
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
25.048
PAN Inj.
25.067
P
41.200
K
11.960
Lime (estimated)
0.000
Secondary Nutrients
Calcium
49.800
Magnesium
6.080
Sodium
40.000
SAR
2.269
Chloride
0.000
Iron
0.000
Alumium
17.060
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
% Solids
0.51
pH
7.390
Min Rate
0.300
Metals
Arsenic
0.078
Cadmium
0.078
Chromium
0.078
Copper
1.612
Lead
0.078
Mercury
0.009
Molybdenum
0.078
Nickel
0.078
Seleniun
0.078
Zinc
1.942
2015
2016
2017
2018
0.30
20.03
2019
0.15
7.01
2020
0.08
2.98
2021
0.04
1.38
2022
2023
2024
2025

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Wa}; Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(ez em ironmentalchemists.com
Town of Kenansville
Date of Report: Jul 05, 2019
PO Box 370
Customer PO #:
Kenansville NC 28349
Customer ID: 09020018
Attention: Gary Benson
Report #: 2019-09017
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-23013 Site: sludge
6/5/2019
10:15 AM Solid/Sludge Garry Benson
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW 846 Method 80818/3510
<0.02 mg/L
06/10/2019
Endrin (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
06/10/2019
Heptachlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
06/10/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
06/10/2019
Lindane (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
06/10/2019
Methoxychlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
06/10/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
06/10/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 827013510
<0.050 mg/L
06/12/2019
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
06/12/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
06/12/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.003 mg/L
06/10/2019
2,4-D (TCLP)
SW846 Method 8151A
<0.003 mg/L
06/10/2019
1,1-Dichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
1,2-Dichloroethane (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Benzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019

Environmental Chemists, Inc.
enviroch6
em
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, lvlanteo, NC 27954 • 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info a environmentalchemists.com
Town of Kenansville
Date of Report: Jul 05, 2019
PO Box 370
Customer PO #:
Kenansville NC
28349
Customer ID: 09020018
Attention: Gary Benson
Report #: 2019-09017
Project ID: Sludge
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
06/12/2019
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
06/28/2019
Sulfide
SM 4500 S D
0.11 mg/kg
06/27/2019
Ignitabillty
SW 846 method 1010
>195 °F
06/10/2019
pH
SW 846 Method 9045D
7.39 units
06/27/2019
Sludge Residuals
Aluminum
EPA 200.7
8530mg/kg
06/07/2019
Arsenic
EPA 200.7
<39.2 mg/kg
06/07/2019
Cadmium
EPA 200.7
<39.2 mg/kg
06/07/2019
Calcium
EPA 200.7
24900 mg/kg
06/07/2019
Chromium
EPA 200.7
<39.2 mg/kg
06/07/2019
Copper
EPA 200.7
806 mg/kg
06/07/2019
Lead
EPA 200.7
<39.2 mg/kg
06/07/2019
Magnesium
EPA 200.7
3040 mg/kg
06/07/2019
Molybdenum
EPA 200.7
<39.2 mg/kg
06/07/2019
Nickel
EPA 200.7
<39.2 mg/kg
06/07/2019
Potassium
EPA 200.7
5980mg/kg
06/07/2019
Selenium
EPA 200.7
<39.2 mg/kg
06/07/2019
Sodium
EPA 200.7
20000 mg/kg
06/07/2019
Zinc
EPA 200.7
971 mg/kg
06/07/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
2500 mg/kg
06/10/2019
Total Solids (%)
SM 2540 B
0.51 %
06/06/2019
Ammonia Nitrogen
SM 4500 NH3 C
<19.6 mg/kg
06/07/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
33400 mg/kg
06/07/2019
RannrtS )nia_noni7

rF"w'— 44 k Environmental Chemists, Inc.
enviroChem1 6602 Windmill Wa}; Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertmvn Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
Sid 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL R CONSULTING CHEMISTS infota environmentxlchemists.com
Town of Kenansville Date of Report: Jul 05, 2019
PO Box 370 Customer PO #:
Kenansville NC 28349 Customer ID: 09020018
Attention: Gary Benson Report #: 2019-09017
Project ID: Sludge
Total Phosphorus SM 4500 P F 20600 mg/kg 06/11/2019
Mercury SW8467471B <4.71 mg/kg 06/09/2019
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
06/14/2019
Barium
EPA 200.7
<1.0 mg/L
06/14/2019
Cadmium
EPA 200 7
<1.0 mg/L
06/14/2019
Chromium
EPA 200.7
<1.0 mg/L
06/14/2019
Lead
EPA 200 7
<1.0 mg/L
06/14/2019
Selenium
EPA 200 7
<1.0 mg/L
06/14/2019
Silver
EPA 200 7
<1.0 mg/L
06/18/2019
Mercury
EPA 2451
<0.0002 mg/L
06/22/2019
Comment: Sludge residual reported on a dry weight basis
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Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Jacksonville WWTP
SWP 2019 1-19
4/22/2019
5/21/2019
Annual 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.58
Nitrogen (TKN)*
8.290
82,900.000
Phosphorus
1.960
19,600.000
Potassium
0.362
3,620.000
Sulfur
0.000
Calcium
0.601
6,010.000
Magnesium
0.197
1,970.000
Sodium
1.000
10,000.000
Iron
---
Aluminum
---
1,170.000
Manganese
---
Copper
---
60.100
1,500
Zinc
---
477.000
2,800
Ammonia Nitrogen*
0.241
2,410.000
Nitrate N / Nitrite N*
---
105.000
Cadmium
---
7.790
39
Chromium
---
7.790
1,200
Nickel
---
7.790
420
Lead
---
7.790
300
Arsenic
---
7.790
41
Mercury
---
0.698
17
Selenium
---
7.790
100
pH
6.940
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
8.049
Molybdenum
---
7.790
75
Chloride
---
Boron
Available P2O5
Specific Gravity

Jacksonville WWTP
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Annual 2019
Date Reported: 5/21/2019 Report No:
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
50.914
PAN Inj.
53.324
P
39.200
K
7.240
Lime (estimated)
0.000
Secondary Nutrients
Calcium
12.020
Magnesium
3.940
Sodium
20.000
SAR
4.582
Chloride
0.000
Iron
0.000
Alumium
2.340
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
SWP 2019 1-19
Physical Characteristics
% Solids
2.58
pH
6.940
Min Rate
0.300
Metals
Arsenic
0.016
Cadmium
0.016
Chromium
0.016
Copper
0.120
Lead
0.016
Mercury
0.001
Molybdenum
0.016
Nickel
0.016
Seleniun
0.016
Zinc
0.954
2016
2017
2018
2019
0.30
48.29
2020
0.15
16.90
2021
0.08
7.18
2022
0.04
3.32
2023
2024
2025
2026

,enviroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Environmental Services
Date of Report: May 21, 2019
PO Box 1054
Customer PO #:
Jacksonville NC 28541
Customer ID: 14110017
Attention: Sonny Scozzari
Report #: 2019-06498
Project ID: Bear Trail Golf Course
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-16389 Site: Sludge
4/22/2019
6:00 PM Solid/Sludge Client
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW 846 Method 808113/3510
<0.02 mg/L
05/03/2019
Endrin (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
05/03/2019
Heptachlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
05/03/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
05/03/2019
Lindane (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
05/03/2019
Methoxychlor (TCLP)
SW 846 Method 8081 B/3510
<0.0005 mg/L
05/03/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
05/03/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
Cresol (TCLP)
SW 846 method 8270/3510
0.223 mg/L
05/06/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
0.223 mg/L
05/06/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
05/06/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
pH
SW 846 Method 9045D
6.94 units
04/24/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.003 mg/L
05/09/2019
2,4-D (TCLP)
SW846 Method 8151A
<0.003 mg/L
05/09/2019
1, 1 -Dichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
1,2-Dichloroethane (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Benzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
M 710 Bowser -town Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoCenvironmentalchemists.com
Environmental Services
Date of Report: May 21, 2019
PO Box 1054
Customer PO #:
Jacksonville NC 28541
Customer ID: 14110017
Attention: Sonny Scozzari
Report #: 2019-06498
Project ID: Bear Trail Golf Course
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
05/08/2019
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
05/07/2019
Analyzed outside of hold time. RL elevated due to matrix interference.
Sulfide
sM 4500 S o
4.83 mg/kg
05/0812019
Analyzed outside of hold time.
Ignitability
SW 846 method 1010
>195 °F
04/30/2019
Sludge Residuals
Aluminum
EPA 200.7
1170 mg/kg
04/25/2019
Arsenic
EPA 200.7
<7.79 mg/kg
04/25/2019
Cadmium
EPA 200.7
<7.79mg/kg
04125/2019
Calcium
EPA 200.7
6010 mg/kg
04/25/2019
Chromium
EPA 200.7
<7.79 mg/kg
04/25/2019
Copper
EPA 200.7
60.1 mg/kg
04/25/2019
Lead
EPA 200.7
<7.79 mg/kg
04/25/2019
Magnesium
EPA 200.7
1970 mg/kg
04/25/2019
Molybdenum
EPA 2007
<7.79mg/kg
04/25/2019
Nickel
EPA 200 7
<7.79 mg/kg
04/25/2019
Potassium
EPA 200 7
3620 mg/kg
04/25/2019
Selenium
EPA 200.7
<7.79 mg/kg
04/25/2019
Sodium
EPA 200.7
10000 mg/kg
04/25/2019
Zinc
EPA 200.7
477 mg/kg
04/25/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
105 mg/kg
05/02/2019
Total Solids (%)
SM 2540 s
2.58 %
04/24/2019

F"I"" —.- Environmental Chemists, Inc.
envirochem 6602 Windmill Way Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
'$e'' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info ta em•ironmentalchemists.com
Environmental Services
Date of Report: May 21, 2019
PO Box 1054
Customer PO #:
Jacksonville NC 28541
Customer ID: 14110017
Attention: Sonny Scozzari
Report #: 2019-06498
Project ID: Bear Trail Golf Course
Ammonia Nitrogen SM 4500 NH3 C
2410 mg/kg
04/30/2019
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B
82900 mg/kg
05/02/2019
Total Phosphorus SM 4500 P F
19600 mg/kg
05/07/2019
Mercury SWe46 7471E
<0.698 mg/kg
04/26/2019
TCLP Metals
Arsenic
EPA 200.7
<1.0mg/L
05/08/2019
Barium
EPA 200.7
<1.0 mg/L
05/07/2019
Cadmium
EPA 200.7
<1.0 mg/L
05/07/2019
Chromium
EPA 200.7
<1.0 mg/L
05/07/2019
Lead
EPA 200 7
<1.0 mg/L
05/07/2019
Selenium
EPA 200.7
<1.0 mg/L
05/07/2019
Silver
EPA 200.7
<1.0 mg/L
05/08/2019
Mercury
EPA245.1
<0.0002 mg/L
05/12/2019
Comment:
Sludge residuals reported o a dry eight basis.
1 No � ����
Reviewed by:
ran

u ENVIRONMENTAU CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTERICATION # 94 N DHHS: DLS CERTIFICATION # 37729
COLLECTION AND CI AIN OF CUSTODY
CLIENT: wowPROJECT
NAME: EF U
ADDRESS: �CG�iu-ra
/ f�^
CONTACT NAME:
REPORT TO:
COPY TO:
Sampled By:
SAMPLE TYPE:'1 = I
Collection
Sample Identffioation
C
a a o `" €
mt-' E �t9 t E
Date Time Temp
oa
U 0 `
Eflfuent
C P
G G
Eflfuent
C P
_
G G
Eflfuent -Grab
C P
C P
G G
Effluent (Quarterly)
C P
G G
C P
G G
GL
4
C ' P
G G
C P
G G
C P
255-A Wilmington Hwy
Jacksonville, NC 28540
OFFICE: 910-347-5863 Lab/Fax
ENT REPORT NO: c� �p �9-0(V66
PO NO:
PHONE/FAX:
E-MAIL:
ifluent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
PRESERVATION
oW
o o z o o = ANALYSIS REQUESTED
z z = = x z - ~o
3s�
X
X
X
X
- DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacte is must be dechlorinated
Transfer I
2.
Temperature when Received:
Delivered By:
Comments:
Accepted:
Received By:
BOD, TSS
Ammonia
X 1 I Fecal
Total Phosphorus
Total Nitrogen
z ppm or less) in the field at the time of collection.
Received By: Date/Time
Resample Requested -
Date: Time: -Z3-C Time: JGv
_ TURNAROUND:

Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL20191-19
Date Sampled:
1/15/2019
Date Reported:
2/7/2019
Reporting Period:
1st Quarter 2019
Parameter
%
PPM
i Weight
Solids*
2.57
Nitrogen (TKN)*
0.702
7,020.000
Phosphorus
1.790
17,900.000
Potassium
0.337
3,370.000
Sulfur
0.000
Calcium
3.020
30,200.000
Magnesium
0.331
3,310.000
Sodium
0.441
4,410.000
Iron
---
Aluminum
---
11,600.000
Manganese
---
EPA
Monthly Limits
Copper
---
926.000
1,500
Zinc
---
1,590.000
2,800
Ammonia Nitrogen*
0.196
1,960.000
Nitrate N / Nitrite N*
---
3,900.000
Cadmium
---
22.300
85
Chromium
---
30.200
1,200
Nickel
---
23.000
420
Lead
---
59.400
300
Arsenic
---
22.300
41
Mercury
---
2.010
17
Selenium
---
2�2.300 '
100
pH
5.580
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
0.506
Molybdenum
---
13.4(()
75
Chloride
---
Boron
Available P205
Specific Gravity
Wercent Solids are an average of Fecal data collected on January 16, 2019.

roo"W--- 49
4-
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
Attention:
Lab ID Sample ID:
19-02160 Site: sludge
Test
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+ N itrite-Nitrogen
Total Solids (%)
pH
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Feb 07, 2019
Customer PO #:
Customer ID: 15060009
Report #: 2019-00865
Project ID: Wallace WWTP
Collect Date/Time Matrix Sampled by
1/15/2019 10:40 AM Solid/Sludge David Verdin/Brent Dean
Method Results Date Analyzed
EPA 200.7
11600mg/kg
01/22/2019
EPA 200.7
<22.3mg/kg
01/22/2019
EPA 200.7
<22.3 mg/kg
01/22/2019
EPA 200.7
30200 mg/kg
01/23/2019
EPA 200.7
30.2mg/kg
01/22/2019
EPA 200.7
926mg/kg
01/22/2019
EPA 200.7
59.4mg/kg
01/22/2019
EPA 200.7
3310 mg/kg
01/23/2019
EPA 200.7
<13.4 mg/kg
01/25/2019
EPA200.7
23.0mg/kg
01/22/2019
EPA 200 7
3370 mg/kg
01/23/2019
EPA 200 7
<22.3 mg/kg
01 /30/2019
EPA 200.7
4410 mg/kg
01 /24/2019
EPA 200.7
1590 mg/kg
01/22/2019
EPA 353.2
3900 mg/kg
02/04/2019
SM 2540 B
2.29 %
01/17/2019
SM 4500 H B
5.58 units
01/17/2019
SM 4500 NH3 C
1960 mg/kg
01/23/2019
SM 4500 Org B
7020 mg/kg
01/23/2019
SM 4500 P F
17900 mg/kg
01/29/2019
SW8467471B
2.01 mg/kg
01/26/2019
Reoort # 2019-00865

Facility: Triple S Farms
Source: Wallace WWTP
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Wallace, North Carolina
Triple S Farms
Wallace WWTP
WL2019 2-19
6/5/2019
6/25/2019
2nd Quarter 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.65
Nitrogen (TKN)*
3.750
37,500.000
Phosphorus
2.580
25,800.000
Potassium
0.424
4,240.000
Sulfur
0.000
Calcium
2.370
23,700.000
Magnesium
0.284
2,840.000
Sodium
1.200
12,000.000
Iron
---
Aluminum
---
11,900.000
Manganese
---
Copper
---
906.000
1,500
Zinc
---
1,400.000
2,800
Ammonia Nitrogen*
0.120
1,200.000
Nitrate N / Nitrite N*
---
390.000
Cadmium
---
31.600
39
Chromium
---
32.500
1,200
Nickel
---
31.600
420
Lead
---
57.300
300
Arsenic
---
31.600
41
Mercury
---
2.200
17
Selenium
---
31.600
100
H
6.820
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.630
Molybdenum
---
31.600
75
Chloride
---
Boron
Available P2O5
Specific Gravity
Percent Solids is an average of Fecal Solids collected
on June 6, 2019.

Environmental Chemists, Inc.
,e,nvir
,�ochem
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
Attention:
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, i\4anteo, NC 27954 • 252.473.5702 Lab/Fax
235-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info (,ym ironmentalchemists.coin
Date of Report: Jun 25, 2019
Customer PO #:
Customer ID: 15060009
Report #: 2019-08949
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-22817 Site: sludge 6/5/2019 10:05 AM Solid/Sludge Will Barr
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200 7 11900 mg/kg 06/07/2019
Arsenic EPA 200.7 <31.6 mg/kg 06/07/2019
Cadmium
EPA 200 7
<31.6 mg/kg
06/07/2019
Calcium
EPA 200.7
23700 mg/kg
06/07/2019
Chromium
EPA 200 7
32.5 mg/kg
06/07/2019
Copper
EPA 200 7
906 mg/kg
06/07/2019
Lead
EPA 200 7
57.3 mg/kg
06/07/2019
Magnesium
EPA 200.7
2840 mg/kg
06/07/2019
Molybdenum
EPA 200 7
<31.6 mg/kg
06/07/2019
Nickel
EPA 200 7
<31.6 mg/kg
06/07/2019
Potassium
EPA 200 7
4240 mg/kg
06/07/2019
Selenium
EPA 200.7
<31.6 mg/kg
06/07/2019
Sodium
EPA 200.7
12000 mg/kg
06/07/2019
Zinc
EPA 200.7
1400 mg/kg
06/07/2019
Nitrate+ N itrite-N itrogen
EPA 353.2
390 mg/kg
06/19/2019
Total Solids (%)
SM 2540 B
2.55 %
06/06/2019
pH
SM 4500 H B
6.82 units
06/18/2019
Ammonia Nitrogen
SM 4500 NH3 C
1200 mg/kg
06/07/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
37500 mg/kg
06/07/2019
Total Phosphorus
SM 4500 P F
25800 mg/kg
06/11 /2019
Mercury
SW8467471B
2.20mg/kg
06/09/2019
Rannrt 8 ')m o-naoeo _

Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL2019 3-19
Date Sampled:
9/18/2019
Date Reported:
10/8/2019
Reporting Period:
3rd Quarter 2019
Parameter
%
PPM
Dry Weight
Solids*
2.31
Nitrogen (TKN)*
4.410
44,100.000
Phosphorus
3.450
34,500.000
Potassium
0.394
3,940.000
Sulfur
0.000
Calcium
2.210
22,100.000
Magnesium
0.312
3,120.000
Sodium
0.500
5,000.000
Iron
---
Aluminum
---
12,400.000
Manganese
---
EPA
Monthly Limits
Copper
---
935.000
1,500
Zinc
---
1,390.000
2,800
Ammonia Nitrogen*
0.281
2,810.000
Nitrate N / Nitrite N*
---
1,180.000
Cadmium
---
14.400
39
Chromium
---
32.300
1,200
Nickel
---
21.300
420
Lead
---
59.300
300
Arsenic
---
14.400
41
Mercury
---
1.990
17
Selenium
---
14.400
100
pH
6.600
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.129
Molybdenum
---
14.400
75
Chloride
---
Boron
Available P2O5
Specific Gravity
Percent Solids are an average of Fecal solids collected on September 19, 2019.

[envirroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
710 Bwwsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inroCi em•ironmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Oct 08, 2019
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2019-15734
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-40315 Site: Sludge 9/18/2019 10:15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 2007
12400mg/kg
09/25/2019
Arsenic
EPA 200 7
<14.4 mg/kg
09/25/2019
Cadmium
EPA 200 7
<14.4 mg/kg
09/25/2019
Calcium
EPA 200 7
22100 mg/kg
09/25/2019
Chromium
EPA 200-7
32.3 mg/kg
09/25/2019
Copper
EPA 200 7
935 mg/kg
09/25/2019
Lead
EPA 200 7
59.3 mg/kg
09/25/2019
Magnesium
EPA 200 7
3120 mg/kg
09/25/2019
Molybdenum
EPA 2007
<14.4 mg/kg
09/25/2019
Nickel
EPA 200 7
21.3 mg/kg
09/25/2019
Potassium
EPA 200 7
3940 mg/kg
09/25/2019
Selenium
EPA 2007
<14.4mg/kg
09/25/2019
Sodium
EPA 200 7
5000 mg/kg
09/2512019
Zinc
EPA 200 7
1390 mg/kg
09/25/2019
Nitrate+Nitrite-Nitrogen
EPA 353 2
1180 mg/kg
09/23/2019
Total Solids (%)
SM 254e B
2.16 %
09/19/2019
pH
SM 4500 H B
6.60 units
10/01/2019
Ammonia Nitrogen
SM 4500 NH3 C
2810 mg/kg
09/22/2019
Total Kieldahl Nitrogen (TKN)
SM 4500 Org B
44100 mg/kg
09/19/2019
Total Phosphorus
SM 4500 P F
34500 mg/kg
10/03/2019
Mercury
SW8467471B
1.99 mg/kg
09/21/2019
Report # 2019-15734 Parma 1 M .1

Facility:
Triple S Farms
Source:
Wallace WWTP
Location:
Wallace, North Carolina
Contractor:
Triple S Farms
Type of Analysis:
Wallace WWTP
Report No:
WL2019 4-19
Date Sampled:
11/19/2019
Date Reported:
12/4/2019
Reporting Period:
4th Quarter 2019
Parameter
%
PPM
i Weight
Solids*
T. 0.36
Nitrogen (TKN)*
3.500
35,000.000
Phosphorus
1.910
19,100.000
Potassium
1.010
10,100.000
Sulfur
0.000
Calcium
2.810
28,100.000
Magnesium
0.478
4,780.000
Sodium
1.640
16,400.000
Iron
---
Aluminum
---
9,310.000
Manganese
---
EPA
Monthly Limits
Copper
---
644.000
1,500
Zinc
---
1,040.000
2,800
Ammonia Nitrogen*
0.003
31.300
Nitrate N / Nitrite N*
---
7,580.000
Cadmium
---
62.500
85
Chromium
---
62.500
1,200
Nickel
---
62.500
420
Lead
---
62.500
300
Arsenic
---
62.500
75
Mercury
---
5.310
17
Selenium
---
62.500
100
pH
6.790
Calcium Carbonate Eq. (est)
Organic Nitrogen
3.497
Molybdenum
---
62.500
75
Chloride
---
Boron
Available P205
Specific Gravity
IYercent solids are the average of fecal values collected on November 19, 2019.

1 '
6e�nZviropehe]m
ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Nianteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, INC 28540 • 910.347.5813 Lab/Fax
infow em iriinmentalehemists coni
Date of Report: Dec 04, 2019
Customer PO #:
Customer ID: 09010063
Report #: 2019-19452
Project ID: WWTP Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
1949384 Site: Sludge 11/19/2019 9:35 AM Solid/Sludge David Verdin
Test Method Results Date Analyzed
Sludge Residuals
Aluminum
EPA 2007
9310mg/kg
11/27/2019
Arsenic
EPA 200 7
<62.5 mg/kg
11/27/2019
Cadmium
EPA 200.7
<62.5mg/kg
11/27/2019
Calcium
EPA 200 7
28100 mg/kg
11/27/2019
Chromium
EPA 200.7
<62.5mg/kg
11/27/2019
Copper
EPA 200 7
644 mg/kg
11/27/2019
Lead
EPA 200.7
<62.5mg/kg
11/27/2019
Magnesium
EPA 2007
4780mg/kg
11/27/2019
Molybdenum
EPA 2007
<62.5mg/kg
11/27/2019
Nickel
EPA 200.7
<62.5 mg/kg
11/27/2019
Potassium
EPA 200 7
10100 mg/kg
11/27/2019
Selenium
EPA 2007
<62.5mg/kg
11/27/2019
Sodium
EPA 200.7
16400 mg/kg
11/27/2019
Zinc
EPA 200 7
1040 mg/kg
11/27/2019
Nitrate+Nitrite-Nitrogen
EPA 353 2
7580 mg/kg
11/26/2019
Total Solids (%)
SM 2540 B
0.32 %
11/20/2019
pH
SM 4500 H B
6.79 units
11/20/2019
Ammonia Nitrogen
SM 4500 NH3 C
<31.3 mg/kg
11 /23/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
35000 mg/kg
11/24/2019
Total Phosphorus
SM 4500 P F
19100 mg/kg
12/02/2019
Mercury
SW84674718
<5.31 mg/kg
11/21/2019
Comment: Results, except pH, reported on a dry weight basis.
pH reported on an as received basis.
Reviewed by: K0 1 X* ow,

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms
Warsaw WWTP
WR2019 10-19
9/24/2019
10/8/2019
Annual 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.87
Nitrogen (TKN)*
2.680
26,800.000
Phosphorus
1.320
13,200.000
Potassium
2.160
21,600.000
Sulfur
0.000
Calcium
1.800
18,000.000
Magnesium
0.122
1,220.000
Sodium
0.206
2,060.000
Iron
Aluminum
7,940.000
Manganese
---
Copper
---
223.000
1,500
Zinc
---
599.000
2,800
Ammonia Nitrogen*
0.000
3.480
Nitrate N / Nitrite N*
---
10.400
Cadmium
---
10.400
39
Chromium
---
14.800
1,200
Nickel
---
10.400
420
Lead
---
24.500
300
Arsenic
---
10.400
41
Mercury
---
0.697
17
Selenium
---
10.400
100
pH
6.790
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
2.680
Molybdenum
---
10.400
75
Chloride
---
Boron
Available P2O5
Specific Gravity

Warsaw WWTP
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms
Annual 2019
Date Reported: 10/8/2019 Report No: WR2019 10-19
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
16.102
PAN Inj.
16.106
P
26.400
K
43.200
Lime (estimated)
0.000
Secondary Nutrients
Calcium
36.000
Magnesium
2.440
Sodium
4.120
SAR
0.678
Chloride
0.000
Iron
0.000
Alumium
15.880
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
Physical Characteristics
% Solids
2.87
pH
6.790
Min Rate
0.300
Metals
Arsenic
0.021
Cadmium
0.021
Chromium
0.030
Copper
0.446
Lead
0.049
Mercury
0.001
Molybdenum
0.021
Nickel
0.021
Seleniun
0.021
Zinc
1.198
2016
2017
2018
2019
0.30
16.08
2020
0.15
5.63
2021
0.08
2.39
2022
0.04
1.11
2023
2024
2025
2026

envirochem
iSh!
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill WaY, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, N,Ianteo, NC 27954 • 252.473.5702 Lab/Fax
255- 1 Wilmington Highway, Jacksonville, NIC 28540 • 910.347.5843 Lab/Fax
info ei,em•ironmentalc hemists.com
Town of Warsaw
Date of Report: Oct 08, 2019
P.O. Box 464
Customer PO #:
Warsaw NC
28398
Customer ID: 09070029
Attention Greg Hughes
Report #: 2019-16108
Project ID: Sludge
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-41365 Site: Sludge
9/24/2019 10:05 AM Solid/Sludge Greg Hughes
Test
Method
Results Date Analyzed
Sludge Residuals
Aluminum
EPA 200 7
7940 mg/kg
10/01/2019
Arsenic
EPA 200 7
<10.4 mg/kg
10/01/2019
Cadmium
EPA 200 7
<10.4 mg/kg
10/01/2019
Calcium
EPA 200 7
18000 mg/kg
10/01/2019
Chromium
EPA 200 7
14.8 mg/kg
10/01/2019
Copper
EPA 200 7
223 mg/kg
10/01/2019
Lead
EPA 200 7
24.5 mg/kg
10/01/2019
Magnesium
EPA 2007
1220mg/kg
10/01/2019
Molybdenum
EPA 200 7
<10.4 mg/kg
10/01/2019
Nickel
EPA 200 7
<10.4 mg/kg
10/01/2019
Potassium
EPA 200 7
2160 mg/kg
10/01/2019
Selenium
EPA 200 7
<10.4 mg/kg
10/01/2019
Sodium
EPA 200 7
2060 mg/kg
10/01/2019
Zinc
EPA 200 7
599 mg/kg
10/01/2019
Nitrate+Nitrite-Nitrogen
EPA 353 2
10.4 mg/kg
09/27/2019
Total Solids (%)
SM 2540 B
2.87 %
09/26/2019
pH
SM 4500 H B
6.79 units
10/04/2019
Ammonia Nitrogen
SM 4500 NH3 C
<3.48 mg/kg
09/26/2019
Total Kieldahl Nitrogen (TKN)
SM 4500 Org B
26800 mg/kg
09/27/2019
Total Phosphorus
SM 4500 P F
13200 mg/kg
10/03/2019
Mercury
Sw8467471B
0.6970 mg/kg
09/28/2019
Comment: Sludge residuals, except pH reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:

ENVIRONMENTAL CHEMISTS, I N C 910.392.0223 252.473.5702
Analytical 8 Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
rnl I =rTlnki AKIM nuASKI r%r- �..ev�...
CLIENT: Town of Warsaw
yr
PROJECT NAME: Annual Sludge
ADDRESS:
CONTACT NAME:
REPORT TO:
COPY TO:
REPORT NO: I ? - lC r c P
PO NO:
PHONE/FAX:
email:
Sampled By:
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO
= Soil, SL = Sludge, Other:
Collection
a
br
PRESERVATION
Sample Identification
E o�
a
cc
W
o I, m m
E
c
o n
r E a
W
z
°z
e
y o 0 o w
ANALYSIS REQUESTED
D t
Time Temp
c
'j v
" _' z
_= z o
GJ lv f9
Sao
C
Pf
Sludge
G
G
X
I
F I
P U' 1
C
LP
G
G
X
Nutrients/Metals
C
P
G
G
X
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
#dp
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
,D
Temperature when Received:
1, Accepted:
Rejected:
Resample Regue ed:
Delivered
Received By:
Date: L`j
Time: q
Comments::
TU A OUND:

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS

A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES:
TOWN OF CLAYTON
AND
TOWN OF WALLACE
TCLP DATA WAS PROVIDED FOR THE FOLLOWING ADDITIONAL FACILITIES:
TOWN OF KENANSVILLE
AND
SOUTHWEST PLANTATION

WaypRlnt.(2)AYTICAL
12/6/2019
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 19-330-0001
Project Description: Holding Tank-TCLP
Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
i', - a' 6-7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

0
76214U(2) hitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number:
Client Project Description:
19-330-0001
Holding Tank-TCLP
Lab No Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
SW-1311 (ZHE)
WTN
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
6010D
WTN
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
7470A
WTN
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
8081A
WTN
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
8151A
WTN
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
8260E
WTN
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
8270C
WTN
69694 Holding Tank
TCLP
11/25/2019 09:00
11/26/2019
SW-1311
WTN
WTN: Waypoint Analytical - TN, Memphis, TN

Waypointe
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number :19-330-0001
Lab No : 69694
Sample ID : Holding Tank
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank-TCLP
Information :
REPORT OFANAL YSIrS
Report Date : 12/06/2019
Received : 11/26/2019
Pof« OF owr
Pauric McGroary
Agronomist
Matrix: TCLP
Sampled: 11/25/2019 9:00
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
TCLP Herbicide Extraction
Combined
1
12/02/19 14:10
SAI
SW-1311
TCLP Metals Extraction
Combined
1
12/02/19 14:10
SAI
SW-1311
TCLP Pesticide Extraction
Combined
1
12/02/19 14:10
SAI
SW-1311
TCLP SVOC Extraction
Combined
1
12/02/19 14:10
SA]
SW-1311
TCLP VOC ZHE Extraction
Combined
1
12/02/19 14:08
SA]
SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
L466809
12/03/19 09:30
Prep Method: 3005A
Test
Results
Units
MQL
DF
Date I Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.025
mg/L
0.025
1
12/04/19 17:17
BKN
L467150
TCLP Barium
<0.025
m9/L
0.025
1
12/04/19 17:17
BKN
L467150
TCLP Cadmium
<0.0050
mg/L
0.0050
1
12/04/19 17:17
BKN
L467150
TCLP Chromium
<0.010
mg/L
0.010
1
12/04/19 17:17
BKN
L467150
TCLP Lead
<0.010
mg/L
0.010
1
12/04/19 17:17
BKN
L467150
TCLP Selenium
<0.050
mg/L
0.050
1
12/04/19 17:17
BKN
L467150
TCLP Silver
<0.005
mg/L
0.005
1
12/04/19 17:17
BKN
L467150
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

�s
f
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
46546
Town Of Clayton
POB 879 Project Holding Tank-TCLP Report Date : 12/06/2019
Information : Received : 11/26/2019
Clayton , NC 27528
Pam« OF 60wr
Report Number :19-330-0001 REPORT OPANALYSIS Pauric McGroary
Agronomist
Lab No : 69694 Matrix: TCLP
Sample ID: Holding Tank Sampled: 11/25/2019 9:00
Analytical Method: 7470A Prep Batch(es): L466826 12/03/19 10:00
Prep Method: 7470A
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
TCLP Mercury
Analytical Method: 8081A
Prep Method: 3510C
Test
<0.0200
Results
mg/L
Prep Batch(es):
Units
0.0200
L467187
MQL
1 12/03/19 14:58
12/04/19 15:40
DF Date I Time
Analyzed
KKM
By
L466914
Analytical
Batch
TCLP Endrin
<0.004000
mg/L
0.004000
10
12/04/19 23:50
VIC
L467309
TCLP gamma-BHC
<0.004000
mg/L
0.004000
10
12/04/19 23:50
VIC
L467309
TCLP Methoxychlor
<0.004000
mg/L
0.004000
10
12/04/19 23:50
VIC
L467309
TCLP Toxaphene
<0.03000
mg/L
0.03000
10
12/04/19 23:50
VIC
L467309
TCLP Chlordane
<0.02000
mg/L
0.02000
10
12/04/19 23:50
VIC
L467309
TCLP Heptachlor Epoxide
<0.004000
mg/L
0.004000
10
12/04/19 23:50
VIC
L467309
TCLP Heptachlor
<0.004000
mg/L
0.004000
10
12/04/19 23:50
VIC
L467309
Surrogate: Decachlorobiphenyl
76.15
Limits: 36-116%
10 12/04/19 23:50 VIC
L467309
Surrogate: Tetrachloro-m-xylene
69.03
Limits: 25-123%
10 12/04/19 23:50 VIC
L467309
Analytical Method: 8151A
Prep Batch(es):
L466978
12/03/19 17:30
Prep Method: 8151A
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP 2,4-D <0.0200 mg/L 0.0200 1 12/05/19 14:42 VIC L467401
TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 12/05/19 14:42 VIC L467401
Surrogate: DCAA 105.4 Limits: 20-120% 1 12/05/19 14:42 VIC L467401
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypo'16 t
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number : 19-330-0001
Lab No : 69694
Sample ID : Holding Tank
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank-TCLP
Information :
REPORT OFANAL YSIS
Report Date: 12/06/2019
Received : 11/26/2019
Pw« or owr
Pauric McGroary
Agronomist
Matrix: TCLP
Sampled: 11/25/2019 9:00
Analytical Method: 82608
Prep Batch(es):
L467010 12/03/19 21:08
Prep Method: 5030E
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Benzene
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP Carbon Tetrachloride
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP Chlorobenzene
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP Chloroform
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP 1,4-Dichlorobenzene
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP 1,2-Dichloroethane
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP 1,1-Dichloroethene
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP Methyl Ethyl Ketone (MEK)
<0.200
mg/L
0.200
1
12/04/19 00:31 ASH
L467064
TCLP Tetrachloroethene
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP Trichloroethene
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
TCLP Vinyl Chloride
<0.0100
mg/L
0.0100
1
12/04/19 00:31 ASH
L467064
Surrogate: 4-BromoFluorobenzene
96.0
Limits: 71-137%
1 12/04/19 00:31 ASH
L467064
Surrogate: DibromoFluoromethane
106
Limits: 70-128%
1 12/04/19 00:31 ASH
L467064
Surrogate: 1,2-Dichloroethane - d4
111
Limits: 63-136%
1 12/04/19 00:31 ASH
L467064
Surrogate: Toluene-d8
102
Limits: 70-130%
1 12/04/19 00:31 ASH
L467064
Analytical Method: 8270C
Prep Batch(es):
L467124 12/04/19 13:15
Prep Method: 3S10C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
TCLP 3&4 Methylphenol
<0.100
mg/L
0.100
1
12/04/19 23:28 BGV
L467329
TCLP 2,4-Dinitrotoluene
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions

s
O
7621 Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www,waypointanalytical.com
46546
Town Of Clayton
POB 879 Project Holding Tank-TCLP Report Date : 12/06/2019
Information : Received : 11/26/2019
Clayton , NC 27528
Pam« P 6a-vr
Report Number :19-330-0001
Lab No : 69694
Sample ID : Holding Tank
REPORT OFANALYSIS
Pauric McGroary
Agronomist
Matrix: TCLP
Sampled: 11/25/2019 9:00
Analytical Method: 8270C
Prep Batch(es):
L467124 12/04/19 13:15
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Hexachlorobenzene
<0.050
mg/L.
0.050
1
12/04/19 23:28 BGV
L467329
TCLP Hexachlorobutadiene
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
TCLP Hexachloroethane
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
TCLP Nitrobenzene
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
TCLP Pentachlorophenol
<0.100
mg/L
0.100
1
12/04/19 23:28 BGV
L467329
TCLP Pyridine
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
TCLP 2,4,5-Trichlorophenol
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
TCLP 2,4,6-Trichlorophenol
<0.050
mg/L
0.050
1
12/04/19 23:28 BGV
L467329
Surrogate: TCLP 2,4,6-Tribromophenol
59.8
Limits: 42-102%
1 12/04/19 23:28 BGV
L467329
Surrogate: TCLP 2-Fluorobiphenyl
47.5
Limits: 24-86%
1 12/04/19 23:28 BGV
L467329
Surrogate: TCLP 2-Fluorophenol
29.4
Limits: 13-37%
1 12/04/19 23:28 BGV
L467329
Surrogate: TCLP 4-Terphenyl-d14
61.9
Limits: 30-122%
1 12/04/19 23:28 BGV
L467329
Surrogate: TCLP Nitrobenzene-d5
49.2
Limits: 25-78%
1 12/04/19 23:28 BGV
L467329
Surrogate: TCLP Phenol-d6
17.1
Limits: 9-27%
1 12/04/19 23:28 BGV
L467329
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions

Waypoint
ANALYTICAL
Client: Town Of Clayton
Project: Holding Tank-TCLP
Lab Report Number: 19-330-0001
Date: 12/5/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Separatory Funnel Extraction 8081 Method 3510C
Sample 69694 (Holding Tank)
QC Batch No: L467187/L467187
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Separatory Funnel Extraction Method 3510C
QC Batch No: 1-467124/1-467124
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Metals Analysis (TCLP) Method 6010D
Analyte: Silver
QC Batch No: 1-467150/1-466809
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.

VUa(DWhitepineY��'��
Road, Richmond, VA 23237
-7621
Main 804-743-9401 1 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Shipment
Receipt Form
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 19-330-0001
Shipping Method
Fed Ex US Postal Lab
Other
UPS Client Courier
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
No
Number of coolers/boxes received
r 1
Custody seals intact on shipping container/cooler?
Yes
No Not Present
Custody seals intact on sample bottles?
Yes
No Not Present
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
is Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Yes
No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Yes
No N/A
Water - VOA vials free of headspace
Yes
No N/A
Trip Blanks received with VOAs
Yes
No N/A
Soil VOA method 5035 — compliance criteria met
Yes
No N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
0 No
Comments:
Signature: Brandi Watson
Date & Time: 11/26/2019 10:58:22

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:env�7iirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fat
710 Bowserto%vn I2oad, Manteo, NC 27934 • 252.473.5702 Lab/Fax
255-A Wilminc ton Highway Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoii,etrvironmentalchemists.corll
Branch Residuals/Bob Branch
Date of Report: Feb 14, 2019
Customer PO #:
Customer ID: 15060009
Attention:
Report #: 2019-00869
Project ID: Wallace WWTP
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-02172 Site: sludge
1/15/2019
10:38 AM Solid/Sludge David Verdin/Brent Dean
Test
Method
Results
Date Analyzed
Chlordane (TCLP)
SW846 Method 8081B/3510
<0.02 mg/L
01/28/2019
Endrin (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
01/28/2019
Heptachlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
01/28/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
01/28/2019
Lindane (TCLP)
SW 846 Method 80816/3510
<0.0005 mg/L
01/28/2019
Methoxychlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
01/28/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
01/28/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/25/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/25/2019
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
Hexachlorobenzene (TCLP)
SW 846 method 8270t3510
<0.050 mg/L
01/25/2019
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
01/25/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/25/2019
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
01/24/2019
2,4-D
SW846 Method 8151A
<0.003 mg/L
01/24/2019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
02/05/2019
Sulfide
SM 4500 S D
0.26 mg/kg
02/13/2019
Ignitability
SW 846 method 1010
>210 °F
01/22/2019
Report # . 2019-00869
Page 1 of 2

PPPP'P"_ _7qq1
envirochem
Ism
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertow-n Road, klanteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, JacksonN-ille, NC 28540 • 910.347.5843 Lab/Fat
info, em•ironrnentalchemist;.coni
Date of Report: Feb 14, 2019
Customer PO #:
Customer ID: 15060009
Report #: 2019-00869
Project ID: Wallace WWTP
pH
SW 846 Method 9045D
6.64 units
01/28/2019
TCLP Metals
Arsenic
EPA 200.7
<1.0mg/L
01/30/2019
Barium
EPA 200.7
<1.0mg/L
01/30/2019
Cadmium
EPA 2007
<1.Omg/L
01/30/2019
Chromium
EPA 200.7
<1.0 mg/L
01/30/2019
Lead
EPA 200.7
<1.0 mg/L
01/30/2019
Selenium
EPA200.7
<1.0mg/L
01/30/2019
Silver
EPA 200 7
<1.0 mg/L
01/30/2019
Mercury
EPA 2451
<0.0002mg/L
01/26/2019
Comment:
Reviewed by:
Report #: 2019-00669 Page 2 of 2

TCLP Volatiles
Client: Environmental Chemist, Inc. Laboratory ID:UB06009-002
Description: 19-02172 Matrix: Aqueous
Date Sampled:01/15/2019 1038
Date Received:0210612019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1311/5030B 8260D 10 02/06/20191848 JM1 96842
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Benzene
71-43-2
8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7
8260D
ND
0.050
mg/L
1
Chloroform
67-66-3
8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.050
mg/L
1
Tetra chloroethene
127-18-4
8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6
8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4
8260D
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
96 70-130
1,2-Dichloroethane-d4
96 70-130
Toluene-d8
100 70-130
LOO = Limit of Ouantilation B = Detected in the method blank E = Quanbtation of compound exceeded the calibration range
NO = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc. Page: 5 of 36
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
n 4 I _Q

6602
mington
ENVIRONMENTAL CHEMISTS, I N C OFFICE: Windmill 3 2 02 3'IFAX 910- 92-44245
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
C171 I FrTIM nNn rWAIM ni: rl ICTnnv
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: ��� DU ?�Oct
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Jerry James, Public Works
email: [e-mail]
Sampled Bv:1-.JAL.,ie ' i i�/1 P_n an SAMPLE TYPE- 1 = Inflnnn4 F o Ffflnnnt W = WWII cT - ca.e en - c..:: of _ c:..,i,...
Sample Identification
p
Collection
E a
m~
0. 2
E 0
A o
o
8 -a
t E
M m
g 2
Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp"
o
Z
=
o
"_
Z
_
o
$
o
''
w
o
Sludge
-15 /
1035
C
P
�
X
full tcl , rci
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
RSEOTyed By:
Date/Time
2.
i Kesample Kequested:
Delivered By: Received By: Date:_ (- �5'1 1 Time:
Comments: TURNAROUND:

Lnviroe-hem::
ANALYTICAL & CONSULTING CHEMISTS
Town of Kenansville
PO Box 370
Kenansville NC
Attention: Gary Benson
Lab ID Sample ID:
19-23013 Site: sludge
Test
Environmental Chemists, Inc.
6602 Windmill Wly, Wilmington, NC 28405 e 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, iL•lanteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info!a. em ironmentalchemists.com
Date of Report: Jul 05, 2019
Customer PO #:
28349 Customer ID: 09020018
Report #: 2019-09017
Project ID: Sludge
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1, 1 -Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
Collect Date/Time Matrix
6/5/2019 10:15 AM Solid/Sludge
Method
SW 846 Method 8081 B/3510
SW 646 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081 B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
SW845 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
Results
Sampled by
Garry Benson
Date Analyzed
<0.02 mg/L
06/10/2019
<0.0005 mg/L
06/10/2019
<0.0005 mg/L
06/10/2019
<0.0005 mg/L
06/10/2019
<0.0005 mg/L
06/10/2019
<0.0005 mg/L
06/10/2019
<0.05 mg/L
06/10/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.250 mg/L
06/12/2019
<0.050 mg/L
06/12/2019
<0.003 mg/L
06/10/2019
<0.003 mg/L
06/10/2019
<0.01 mg/L
06/12/2019
<0.01 mg/L
06/12/2019
<0.01 mg/L
06/12/2019
<0.01 mg/L
06/12/2019

L
[envltrrochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bow-sertown Road, Manteo, NC 279.54 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info rremvironnientalchemists.com
Town of Kenansville
Date of Report: Jul 05, 2019
PO Box 370
Customer PO #:
Kenansville NC
28349
Customer ID: 09020018
Attention: Gary Benson
Report #: 2019-09017
Project ID: Sludge
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
06/12/2019
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
06/12/2019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
06/28/2019
Sulfide
SM 4500 S D
0.11 mg/kg
06/27/2019
Ignitability
SW 846 method 1010
>195 °F
06/10/2019
pH
SW 846 Method 9045D
7.39 units
06/27/2019
Sludge Residuals
Aluminum
EPA 200.7
8530 mg/kg
06/07/2019
Arsenic
EPA 200.7
<39.2 mg/kg
06/07/2019
Cadmium
EPA 200.7
<39.2 mg/kg
06/07/2019
Calcium
EPA 200.7
24900 mg/kg
06/07/2019
Chromium
EPA 200.7
<39.2 mg/kg
06/07/2019
Copper
EPA 200.7
806 mg/kg
06/07/2019
Lead
EPA 200.7
<39.2 mg/kg
06/07/2019
Magnesium
EPA 200.7
3040 mg/kg
06/07/2019
Molybdenum
EPA 200.7
<39.2 mg/kg
06/07/2019
Nickel
EPA 200.7
<39.2mg/kg
06/07/2019
Potassium
EPA 200.7
5980 mg/kg
06/07/2019
Selenium
EPA 200.7
<39.2 mg/kg
06/07/2019
Sodium
EPA 200.7
20000 mg/kg
06/07/2019
Zinc
EPA 200.7
971 mg/kg
06/07/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
2500 mg/kg
06/10/2019
Total Solids (%)
SM 2540 B
0.51 %
06/06/2019
Ammonia Nitrogen
SM 4500 NH3 C
<19.6 mg/kg
06/07/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 org B
33400 mg/kg
06/07/2019

6e�nZvitrochem]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fa\
710 Bowsertovm Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoOt environmentxlchemists.com
Town of Kenansville Date of Report: Jul 05, 2019
PO Box 370 Customer PO #:
Kenansville NC 28349 Customer ID: 09020018
Attention: Gary Benson Report #: 2019-09017
Project ID: Sludge
Total Phosphorus SM 4500 P F 20600 mg/kg 06/11/2019
Mercury swe467471E <4.71 mg/kg 06/09/2019
TCLP Metals
Arsenic
EPA 200 7
<1.0 mg/L
06/14/2019
Barium
EPA 200.7
<1.0 mg/L
06/14/2019
Cadmium
EPA 200 7
<1.0 mg/L
06/14/2019
Chromium
EPA 200.7
<1.0 mg/L
06/14/2019
Lead
EPA 200.7
<1.0 mg/L
06/14/2019
Selenium
EPA 200 7
<1.0 mg/L
06/14/2019
Silver
EPA 200.7
<1.0 mg/L
06/18/2019
Mercury
EPA 245 1
<0.0002 mg/L
06/22/2019
Comment: Sludge residual reported on a dry weight basis
A
Reviewed by: n ,

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
/. - Y 50fi-
CLIENT: Town of Kenansville
PROJECT NAME: Annual Sludge
REPORT NO: O
ADDRESS:
CONTACT NAME: Garry Benson
PO NO:
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled BV: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
m
m
N
a
a o IT
°
c c7
2 o`
cci a
c
o 6
v E
ccPRESERVATION
o w
m M
z
ANALYSIS REQUESTED
Date
Time
Temp
z
z
=
o
0
i
0
z
o
~
w
o
Sludge
. 3
SI
C
�I�
ti�
Full TCLP/RCl/Nutrients/Metals
-
-_
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
- 5-
2.
Temperature when Received: S Accepted: / Rejected: Resample Requested:
Delivered By: Received By: Date: Time:

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
rsM,
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Environmental Services
Date of Report: May 21, 2019
PO Box 1054
Customer PO #:
Jacksonville NC 28541
Customer ID: 14110017
Attention: Sonny Scozzari
Report #: 2019-06498
Project ID: Bear Trail Golf Course
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-16389 Site: Sludge
4/22/2019
6:00 PM Solid/Sludge Client
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW 846 Method 8081B/3510
<0.02 mg/L
05/03/2019
Endrin (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
05/03/2019
Heptachlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
05/03/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
05/03/2019
Lindane (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
05/03/2019
Methoxychlor (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
05/03/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
05/03/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
Cresol (TCLP)
SW 846 method 8270/3510
0.223 mg/L
05/06/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
0.223 mg/L
05/06/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
05/06/2019
o-Cresol (TCLP)
SW 846 method 8270f3510
<0.050 mg/L
05/06/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
05/06/2019
Pyridine (TCLP)
SW 846 method 827013510
<0.050 mg/L
05/06/2019
pH
SW 846 Method 9045D
6.94 units
04/24/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.003 mg/L
05/09/2019
2,4-D (TCLP)
SW846 Method 8151A
<0.003 mg/L
05/09/2019
1, 1 -Dichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
1,2-Dichloroethane (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Benzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019

7�1
envitrochem.-I
a
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4.124 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax
info Genvironmentalchemists.com
Environmental Services
Date of Report: May 21, 2019
PO Box 1054
Customer PO #:
Jacksonville NC 28541
Customer ID: 14110017
Attention: Sonny Scozzari
Report #: 2019-06498
Project ID: Bear Trail Golf Course
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
05/08/2019
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Trichloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
05/08/2019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
05/07/2019
Analyzed outside of hold time. RL elevated due to matrix interference.
Sulfide
SM 4500 S D
4.83 mg/kg
05/08/2019
Analyzed outside of hold time.
Ignitability
SW 846 method 1010
>195 °F
04/30/2019
Sludge Residuals
Aluminum
EPA 200.7
1170 mg/kg
04/25/2019
Arsenic
EPA 200.7
<7.79 mg/kg
04/25/2019
Cadmium
EPA 200.7
<7.79 mg/kg
04/25/2019
Calcium
EPA 200.7
6010 mg/kg
04/25/2019
Chromium
EPA 200.7
<7.79mg/kg
04/25/2019
Copper
EPA 200.7
60.1 mg/kg
04/25/2019
Lead
EPA 200.7
<7.79 mg/kg
04/25/2019
Magnesium
EPA 200.7
1970 mg/kg
04/25/2019
Molybdenum
EPA 200.7
<7.79 mg/kg
04/25/2019
Nickel
EPA 200.7
<7.79 mg/kg
04/25/2019
Potassium
EPA 200.7
3620 mg/kg
04/25/2019
Selenium
EPA 200.7
<7.79 mg/kg
04/25/2019
Sodium
EPA 200.7
10000 mg/kg
04/25/2019
Zinc
EPA 200.7
477 mg/kg
04/25/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
105mg/kg
05/02/2019
Total Solids (%)
SM 2540 a
2.58 %
04/24/2019

Environmental Chemists, Inc.
6enviro -hem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Ivlanteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
infoCem•ironmentalchemists.com
Environmental Services
Date of Report: May 21, 2019
PO Box 1054
Customer PO #:
Jacksonville NC 28541
Customer ID: 14110017
Attention: Sonny Scozzari
Report #: 2019-06498
Project ID: Bear Trail Golf Course
Ammonia Nitrogen SM 4500 NH3 C
2410 mg/kg
04/30/2019
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B
82900 mg/kg
05/02/2019
Total Phosphorus SM 4500 P F
19600 mg/kg
05/07/2019
Mercury SW8467471B
<0.698mg/kg
04/26/2019
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
05/08/2019
Barium
EPA 200.7
<1.0mg/L
05/07/2019
Cadmium
EPA 200.7
<1.0 mg/L
05/07/2019
Chromium
EPA 200 7
<1.0 mg/L
05/07/2019
Lead
EPA 200.7
<1.0 mg/L
05/07/2019
Selenium
EPA 200.7
<1.0mg/L
05/07/2019
Silver
EPA 200.7
<1.0 mg/L
05/08/2019
Mercury
EPA 245 1
<0.0002 mg/L
05/12/2019
Comment:
Sludge residuals reported o a dry eight basis.
f bura
Reviewed : b
Y
l�

y� ENVIRONMENTAL CHEMISTS INC
Analytical & Consulting Chemists NCDENR: DWQ CERTERICATION # 94 N DHHS: DLS CERTIFICATION # 37729
COLLECTION AND CIRAIN OF CUSTODY
CLIENT: PROJECT NAME: EF -LUENT
ADDRESS: _ �L%Gc.Cb / �� f�" F CONTACT NAME:
REPORT TO:
COPY TO:
255-A Wilmington Hwy
Jacksonville, NC 28540
OFFICE: 910-347-5863 Lab/Fax
REPORT NO: �p /G!'V bel" W
c,�
PO NO: !� d -5 !S —
PHONE/FAX:
E-MAIL:
Sampled By:
SAMPLE
TYPE:'1
= Influent, E = Effluent, W = Well, ST = Stream,
SO = Soil, SL = Sludge, Other:
Collection
w
PRESERVATION
Sample Identification
a a 0
E> E `o C7
_
"
`o
= m
o m m z o 0 0 o m
ANALYSIS REQUESTED
Date
Time
Temp
CL
`"
E
t z Z = _ = z
o
Eflfuent
C
P
X
G
G
BOD, TSS
Eflfuent
C
P
X
G
G
Ammonia
Eflfuent -Grab
C
P I
G
G I X
Fecal
C
P
G
G
Effluent (Quarterly)
C
P
G
G X
Total Phosphorus
C
P
G
G X
Total Nitrogen
�LP,
4
C '
P
G
G 31
C
P
G
G
C
P
NOTICE - DECHLORINATION:
Samples for Ammonia, TKN, Cyanide, Phenol
and
Bacte is must be dechlorinated (0.2 ppm or less) in the field
at the time of collection.
Transfer
Reli uished By:
Da e/Time
Received By:
Date/Time
Temperature when Received: Accepted: F
Delivered By: Received By
Comments: --
;ample Requested:
Date: �-Z3-(�_Time:
__ TURNAROUND:

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Town of Beulaville, Town of Clayton, Town of Kenansville, Town of Warsaw, and Southwest
Plantation meet pathogen reduction and vector attraction reduction requirements through lime
stabilization. The Town of Wallace met pathogen reduction through fecal density and vector
attraction reduction through injection or incorporation.
The forms for these facilities are marked appropriately.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Beulaville WWTP
Monitoring Period:
WQ Permit Number: WQ0030998
NPDES Number: NCO026018
12/31/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative erformed•
From
1/1/2018
To
Class A:
t A
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
P
Alt. C(Prior Testin) ❑
A1t.D (No Prior Test) ElProcess
to Farther Reduce Pathogens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Hea!pryin ❑
Heat Treatment ❑ Thermo hilic ❑
Beta Ra ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens C1
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air R!jing ❑
CompostingCompostigg ❑
JAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to
alternative performed
(Class A or Class B) complete the
llowing monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
Fre uenc
9 y
of Analysis
Sam le
p
Tencesype
na y uca
Tech -
ninne
MinimumGeo.
Mean
Maximu
Units
Fecal ( oliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
V
3 MPN per 4 grams
total solid (dry
wei ht)
ec tion or ttraction Reduc(15A NCAC 02T .1id7i - Please indinatp niternativa narfnrm&A-
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ jAlt.
4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying -Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
..�.j. _ AX: avri a AW11% A & ti 1 r'LVILEN r tp,ense cnecK me appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
--ams aeterminadon has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aw re that there are
significant penalties for false certification including fine a impriso en '
Mr. Stanley Miller, WWTP ORC
Preparer Name and Title (type or print) Land Ap Her Na an tle (if V tcable)(type or print)
Signature of P arer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
1,VWTP Name: Clayton Little Creek WRF NPDES Number: NCO025453
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
I Process to Further Reduce Patho engs ❑
If applicable to alternative rformed (Class A only) Indicate "Process to Further Reduce Patbogens":
Compost ❑
Heat Drying Cl
Heat Treatment ❑
Themiophilic ❑
Beta Ray ❑
Gamma Raj ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
I Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Di estion ❑
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech-
ninue
Minimu
Geo. Mean
Maximu
Units
Fecal CoIiform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacterial
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationE]
Alt 7 (Drying -Stable) D
JAIt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Mr. James 0. Warren, WRF ORC
Pre er,Nrame and Title (type or print)
/�)) r
L/� /
nature of Preparer*
f
Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Kenansville WWTP NPDES Number: NCO036668
Monitoring Period: From 1 / 112019 To 12/31 /2019
Pathogen Reduction (15A NCAC 02T .1106) • Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑ Process to Further Reduce Patho ens ❑
If applicable to alternative erformed Class A only) indicate "Process to Further Reduce Pathogens":
Com ost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑
BetLgay ❑ Gamma Ray ❑ Pasteurization ❑
Class B:
JAIt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Patlio ens
p
If applicable to alternative peiformed (Class B only) indicate "Process to Significantl • Reduce Pathogens":
Lime Stabilization El Air Drying ❑
omposting ❑ Aerobic Di
estion ❑
Anaerobic Digestion ❑
If applicable to
alternative peifor•med (Class A or Class B) com lete the
followin monitor•in
data:
Parameter
Allowable Level
Pathogen Density
13 �
um er o
Frequency
Sample
Analytical
in Sludge
g
Mi
E1Cee_
Tech-
2gnrpu x 10 to the
MI,N
ninuc
6th power
per gram of
Fecal Coliform
total solids
CRJ
1000 mpn per gram
of total solid (dry
wei t)
Salmonella bacteria
3 MPN per 4 !grams
(in lieu of fecal
total solid y
AC (12T
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
------- - v as.. 4-aii1 A tFicax CIAXAM uic App[-Upi-late Statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if
you check this statement attach an explanation why you have not met one or both of the
"'Phis determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine _,nd imprisoMfient "- //
Mr. Garry Benson, WWTP ORC 1a 47 X
Preparer Name and Title (type or print) Land Applier Nam nd Titl • applicable)(type or print)
a a_�
Signature o Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Southwest Plantation WWTP NPDES Number: WQ0029601
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
11
Class A:
Alt. A (timeItem) ❑
1 Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Patio en ❑
If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thenno hilic ❑
Beta Ray ❑
1 Gamma RaX ❑
Pasteurization ❑
Class B:
I Alt. (1) Fecal Densi ❑
Alt. (2) Process to Sjgnificantly Reduce Pathogens O
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying ❑
Composting ❑
JAerobic Digestion ❑
Anaerobic Digestion
If applicable to
alternative perfa
med (Class A or Class B) complete the
Ilowing monitoring dntn:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
denceR Escee-
Frequency
of Analysis
Sample
Type
na yuca
Tech-
Minimu
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
Itotal solids
MPN
CFU
1000 mpn per gram
of total solid (dry
wei t)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weiaht
FT
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. O: uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk Stabilization p
Alt 7 (Drying- Stable) ❑
JAlt. 8 (Drying- Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
Ckat'i IFICAT10N STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Sonny Scozzari, ORC
Preparer Name d itle (t or print) Land Applier Name and Title (if applicable)(type or print)
Signature f Preparer*1111JDate Signature of Land Applier (if applicable) Date
*Prepa r is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NC0003450
Monitoring Period: From 1/1/20I9 To 3/31/2019
PQfhnoan RWIRIPHA" fl SA NrAr (12T -1166) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑ I
Process to Farther Reduce Pathogen gs ❑
If applicable to alternative petformed (Class A only) indicate "Process to Further Reduce Patho ens":
Compost. ❑
Heat Drying [3
Heat Treatment ❑
Thermo hilic [3Beta
Ray❑
Gamma Ra ❑
Pasteurization [3Class
B:
Alt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative pet -formed (CIass B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting D Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to
alternative performed (Class A or Class B) complete the
llowing
monitoring data:
Allowable Level Pathogen Density
Number o
Excee-
Frequency Sample na ytica
Tech -
Parameter
in Sludge Minimu Geo. Mean Maximu Units
of Analysis T e
yPnioue
2 x 10 to the
MPN
62
7l
76
MPN/
0
Quarterly
Grab
SM 9221 C
E
6th power
Gram
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
I
coliform)
weight)
Vector Attraction Reduction (15A NCAC 02'1' .11u7) - Ylease inmcate alternative performeu.
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying -Stable) ❑ jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land A plier ORC
Prepare Name and Title (type or print) Land Applier Name and Tit (if appl' a le)(type or print)
12
a,(00, �D V� 7 -(P
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/20061

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPD)✓S Number: NC0003450
Monitoring Period: From 4/l/2019 To 6/30/2019
Uo+hnnan Varinrtinn 11 SA WA C`. (12T -1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ I
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) El
Alt.D (No Prior Test) ❑
Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost_13 Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density El I
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ lAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed
(Class A or Class B) complete the
following monitoring
data:
Allowable Level
Pathogen Density
um er o
Excee-
Frequency
Sample
na ytica
Tech -
Minimum
Geo. Mean
Maximuni
Units
Parameter
in Sludge
of Analysis
Type
2 x 10 to the
MPN
675
1,431
4,045
MPN/
0
Quarterly
Grab
sM 9221 C
E
6th power
Gram
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
weight)
Vector Attraction Reduction 115A NCAC 02T .1107) - Please indicate alternative performed.
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ 1 Alt. 4 (Spec. OZ uptake) L3
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying- Stable) ❑ jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
J vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land Applier Name a# Title (if p icable)(type or print)
�ht Q .
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
nr-NR FnRM PVRF OPT (191900BI

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NC0003450
Monitoring Period: From 7/1/2019 To 9/30/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) E37
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑ I
Process to Further Reduce Patho engs ❑
If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat ing ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ray ❑
Gamma RaX ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density_Ell
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significautl • Reduce Pathogens":
Lime Stabilization ❑
Air Drying El Composting❑
Aerobic Digestion ❑
Anaerobic Di estion ❑
If applicable to alternative performed (Class A or Class B) complete the
Ilowing monitoring
data:
Allowable Level
Pathogen Density
um er o
Excee-
Frequency
Sample
na yt�ca
Tech -
Parameter
in Sludge
Minimu
Geo. Mean
aximu
Units
of Analysis
a
Typenioue
2 x 10 to the
MPN
1,442
3,743
21,177
MPN/
0
Quarterly
Grab
SM 9221
C E
6th power
Gram
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per A grams
(in lieu of fecal
total solid (dry
coliform)
weight)
Vertnr Attraction Reduction t15A NUAU UZY .11U/1 - Please inaicate alternative periuruieu:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench)
JAIL 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (A1k. Stabilization❑
jAlt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Prep er Name and Title (type or print) Land A plier Name anl Title (if p licable)(type or print)
2-b-2-02D �2 a l0"ac�
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
nFNR FORM PVRF n9T m w9nm

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NC0003450
Monitoring Period:
To 12/31 /2019
Pathoeen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
From 10/1/2019
Class A:
Alt. A (time/tern) ❑
Alt B (Alk Treatment) ❑ I
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) 0
Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ray 17
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density El
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Signiftcnntly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
lAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative perfoi•med (Class A or Class B) complete the foflowingmonitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
«m er o
flenceR fiscee-
Frequency
of Analysis
Sample
Type
na yttca
Tech-
ninelp
nimut
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
2,128
5,780
10,000
MPN!
Gram
0
Quarterly
Grab
SM 9221
C E
CFU
1000 mpn per gram
of total solid (dry
wei lit
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternntive performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ I
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met:'
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith Land Applier ORC
Prep er Name and Title (type or print) Land A plier N e a Title (i p icable)(type or print)
hol to us Z - - zozo
� a
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
nt=nirl GnR&A Pvm= noY t1wonnm

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Warsaw WWTP NPDES Number: WQ0021903
Monitoring Period: From 1 / 1 /20l 9 To 12/31 /2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and nitPrnativP narfnrmaA•
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment) ❑
Alt. C (Prior Testin ❑
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Patho ens ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
Beta Ra ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Densi ❑
Alt. (2) Process to Significantly Reduce Pathogens El
Itapplicable plicable to alternative rformed (Class B only) indicate "Process to Significantly Reduce Potho ens":
Lime Stabilization El
Air Drying ❑
Composting Q
lAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to
alternative performed
(Class A or Class B) complete the
following monitoring
data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number of
Excee-
encer
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
tI--L-- ♦
3 MPN per 4 grams
total solid (dry
weight)
vecLUr ALLMcnon Reduction (15A NUAU UZY .11W) - Please indicate alternative performed: - -
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. StabilizationCl
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
UNn I it JR-A 11UN a 1 ArEIVIL :N•r (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
my direction and supervision in
the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have bee met. I a aware that there are
significant penalties for false certification including fine anAimprisonmA411
Mr. Greg Hughes, WWTP ORC�L
Pre ilrer Name and, p (type or print) La Applie Na a and T ;ho. (if applicable)(type or print)
Signs ure of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Town of Beulaville, Town of Clayton, Town of Kenansville, Town of Warsaw, and Southwest
Plantation meet pathogen reduction and vector attraction reduction requirements through lime
stabilization. The Town of Wallace met pathogen reduction through fecal density and vector
attraction reduction through injection or incorporation.
Documentation of these activities are found in the following section.

T*Ie s Farms WQ0030998
Lime Stabilirntion Documentation Month N.(a. r-
MENNEN
Signature of Operator
• EPA 40 CFR Part 503 for lime stabiliaatioa Mquircs lirne mixed with sevmre sludge to have a pH of 12 or greater alter 2 hours and memtsm it pH of 11.5 for the following 22 hours.
pH alma . actual pH values that love not been temperature corrected.
pH cameea - pH values have been temperature corrected -
AD temperature units we in Celsius.
Y1
N
tT
�O
M
O
Q
O
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N
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Cn CV un
N c� M M M '7
o
un
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^'
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CV
N
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p
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O
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'
r
n
�wocoocococooc00000
O
N
N
N
N
N
N
N
M
M
M
M
M
M
M
M
M
N
N
t'V
LLL=7
8
a+
Fy

Triple S Farms WQ0030998
Lime Stabilization Documentation
Mouth G:.V
®arm®����
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Signature OLlDpemtor
• EPA 40 CFR Part 503 for lime stabilization requires lime muted with sewage sludge to have a pH of 12 or greater after 2 hours and maintain a pH of 11.5 fbr the following 22 hours•
pH aww — actual pH values that have not been temperature corrected
pH ca radw m pH values have been tengmrattae corrected.
All temperamm units are in Celsius.
C,
O
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T*feSFarms WQ0030998
pbilizattioa DocumentationFacUlty Name Town of Baulevlk Lime 5Month V e• 4 E k
r
_■_..■.—■■..—..■■.—■..■■—■■_
_■_-.■.—■...—..■■.—■■.■■—■■_
lsi�
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Signature of
EPA 40 CFR Part 503 for lime stabilization requires lime matted with sewage sludge to have a pH of 12 or gamer abr 2 houn and maintain a pH of 11.5 for the following 22 how.
pH mutt - acbW pH vahtesthat have not been bovendm cortocted
pH eaiftw — pH values have bean tanperomm corrected.
Allteroperaque units ere in Celsius.
�t
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I I I /i / r '—)
Slucllge Stabilization Record
:Tm� n of Clayton
little Creel. Water Reclamation Facility
1'oluntc Treated: i ", ' j,
Volume used: 37 Gy(j � 36%
Time
Time / Date ,H
I Correction
Final
i Temp.
I
Factor
Initial
��•ss' //moo/rs lo,/Y
- r �,b�.
---�
After Addition
jY 3° / 3u
12 7y
/S. 7 ° c
Two firs. After addition
NSO //30M,
12.65r
-`1,r xe.°3
7b�
/s--
24 flrs. after .addition I0
ct 1/3,/iq ��Z.��
_S,S'Xa.o3
1-Z
is
Datc/ TimeBuffet•
-30-11 v:ni
,
P
c'
r
I Reading
I '7. _
INIv
11.
Int:i4ZY- Slope -jy )5-
U—at c/ _Time
�uffer
Reading itl�
/L. ys
Int: Wj Slope ;'g.75 s

Brnett Lime Company' Inc* CERTIFIED PUBLIC WEIGHER
`" 095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 S, Bartow, FL 33830 DELIVERY TICKET N0.
❑ 1100 Airport Rd, Eastaboga, AL 36260 52114
SHIPMENT DATE
S Clayton jo-van of) SHIPMENT WEIGHTS
LD P.(),. Bo G'tG
��•, 7 y`;t
C Ic�YEi�i�.11L• 2, ~
T
0
S C<l:? y tor, VVYTH,
H 1_fttIe C:tej lk kV.
1000 Durham Street L z t.
P
Clayton, NC, 2 7 `2.0
T
Ln
w
PROJECT NO.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CU5TQlylJj JyO.
BLC ORDER LOT NO CUSTOMER PURCHASE ORDER NO.
SHIPPED VIA TERMS
t ,.1
r-
I s� .- .- 1 ? 1 t f .. , . 1� •t� � t t�v
Net 30
ORDERED
1
z 1 Tanker CAL—FLO' Slurry
if
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED -_
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
CAL=FLQ
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
FT S Y S, E M e, S L t, x R Y
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
Slurry
6 [Fq� CAter Treatment
Drink�ngWaterTreatmentAddltive
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
)Z�-J'
Tested In accordance with
Standard ANSI/NSF60
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE
Calcium Hydroxide
"'FPEv�EN`. 650 mg/L Maximum Use level
SPECIAL INSTRUCTIONS DRIVER
NAME TANKER NO.
, �t
V� qLU
id 11 �fl Z -:3 111 ►
.�
OF
z
CUSTOMER SIGNATURE

Sludge Stabilization Record
Town of Clayton
Little Creek Water Reclamation Facility
Date: ,5�6�/ y Location: Hold%hy 7Q„'k -7?5
Volume Treated: 33/1 ooc Alkali Used: C G Ui
1/.o�x,3o,oO'0
Volume Used: �--5, G
Time
Time / Date
pH
Correction
Factor
Final
pH
Temp.
Initial
After Addition
a'' s'l�-!i
Jz �d
,25• `r
Two Hrs. After Addition
/'ZO
� a J2.
;-0 z-y� pA
3-2-
Iz •�
24 1Irs. after Addition
$�� sly/��
il,/c�
•a33
12,133,2
.1
Preparers 't.�:�f . --•tip%r .�
Date/ Time
Buffer
( Reading
INIv
D
/0.Oj-
z,O
Int:^f& Slope ?s- Y;y
Date/ Time
Buffer
Reading
NIN,
Ys'
.2t;1Y
Int: t,.;ui Slope,_S'9./f Ijv%

Burnett Lime Company, Inc.
© 7095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 5, Bartow, FL 33830 .
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE •
g [; i �� t,7ri f T,t Fit• _
0 Af n _ t c-curt 1-1
L F r_ . r-rr._ n7n-.
, a U
D n.,4011 �,-
T
Lel
S C hil, r,=tf 1P"TP
H
I 10 DiIt11 ,,i
P
T
0
CUSTOMER NO. I . BLC ORDER
PROJECT NO.
CUSTOMER PURCHASE ORDER NO.
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
5L 6 23
SHIPMENT WEIGHTS
Ln
Ln
0
.
L7
w
Cr
H
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
`t t
1 1 1 Tanker CAL —FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING CAL = F LO
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT SYSTEM 6 SLURRY
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS CAL'FLO•Slurry
w Drinking Water Treatment Additive
Tested in accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE r Standard ANSI/NSF60
Gkaum Hydrodde
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE L�EaFNDE�` j 650 mg/L MaZum Use Level
SPECIAL INSTRUCTIONS DRIVER NAME TANKER NO.
`ti •:ZL t 1 J tt '
VIN #
H
w
Z
CUSTOMER SIGNATURE

Sludge Stabilization Record
To« n of Clayton
Little Creel; Water Reclamation 17'acility
Date: -�-/ 1 Location:
Il'•3C,o",o
Volume Treutecl; .Clow Alkali Used: C-14��
Volume Used: y5- (o'v
"time
--- — -
Time / Date ' pH
I I — -
ir5l3S/y"/-ly
Correction
Factor
Final Temp.
( PH '
Initial
-s.y -0..e3
--- -�
After ;addition
- o, lzq
12,110
T1No 1-lrs. After Addition
z3o
�2 ys
-o,C)3
Z0,
13Z
rz,3i 4
24 I-Irs. after Addition ,w3o/y-3 •0.03Z�Z
n
Date/ Time
i q-1 /I
I(
Buffer
_
Reading
7 0 '7
Niv
_ p 3
/Z, `/-
12., 7._Z
-32y,c
Int:!;&r9lnpe -5
Date/ Time
Buffer
Reading
111N,
07
0 , O
10.0 7
' 7Z, 3
4-06Zgc
IZ ,'VS
12
-32-7-7
Int:�� Slope 'SYr78' yy

rnett Lime
:- 095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 5, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
—1--1
S Clavton (Tcw�u on
0 Ann: Accounts Pa able
D P.O. Box 8789
Gtayton,N 27520
T
0
S C'laytL7II WWTP
H Little Greek V RF
I
P 1000 Durbam Street Ext.
C:1_ayten, TM;C: 2752.0
T
0
Company, Inc.
�wq
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
52622
SHIPMENT WEIGHTS
�
�Cl l f
F6t l�`, �-
o
l7
I of L�
�
R
0 OL6
_!U
PROJECT NO. BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTQ.�E,� O. �BLCjj
LOT NNQ, CUSTOMER PURCHASE ORDER NO. SHIPP D VIA TERMS
��" �L11UU rr �I/
�ltnWR-� col `� Nlet _0
ORDERED • DESCRIPTION
b
1 1 Tanker CAL —FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING CALTE� F T O
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT S T S TE M S SLURRY
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS CAL`11.06Slurry
rt Drinking Water Treatment Additive
Tested In accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE ° Standard ANSI/NSF6Om CUlciuHydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE `��F"E .E, 6SO mg/L Maximum Use Level
it414 i ��] � 11V �7 L►7 IN
n_�+,a EQ6D6o
HieY w Z 151 (s, S O u� .5N14 11 ) � V q5
CUSTOMER SIGNATURE

Sludge Stabilization Record
Town of Clayton
Little Creek Water Reclamation Facility
Date: J� Z� 1 � Location:
Volume Treated: 327, 1,06, Alkali Usecl: Gt0c 3
Volume Used:
Time
Time / Date
pH
I Correction
( Final
Temp.
Factor
pH
Initial
09Uo psi fj
11.
/P-
After Addition
(>= 12.00 after temp.
correction)
r ZvG s
Two I-lrs. After Addition
(>= 12.00 after temp.
correction )
/ /cc% sll`�/� 1
i . 9 'L
-4-9
i Z • v5f'
Zi . l
24 Hrs. after Addition
(>= 11.50 after temp.
_
ROK 7
correction )
1 zOS 'S 3v I
< < �
12-
v�
Preparer:-Telrrz4) `1�217--
Date/ Time
Buffer
Reading
11v
z ,P OW1
7.
15.1
7, ve)
-173. q
'32,O.'2-
Int: lys Slope - S5'.c7
Date/ Time Buffer
Reading
1IN•
I 10, n
Int: W1 Sloped 9 ?

0
B�urnett Lime Company, Inc.
7095 Hwy 11, Campobello, SC 29322
0 5200 US Hwy 17 S, Bartow, FL 33830 .
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE •
SHIPMENT WEIGHTS
S
O
L
D
T
O
S
H
I
P
T
O
PROJECT NO
CUSTOMER NO. BLC ORDER LOT NO. I CUSTOMER PURCHASE ORDER NO.
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
53
LU
Cr
Fa -
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
1 1 I Tanker CAL —FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING GAL=- =FLO
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT S Y S T E M L S L V a a t
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
Slurry
AND OFF-LOADING AREA CLEANLINESS o s cF�, Cater Treatment
�t !. Drinking Water TreatmentAddttive
" Tested in accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE • ' °) Standard ANSI/NSF60
i 4 Calcium Hydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE `°ErE�oE�` 650 mg/L Maximum Use Level
71 111 7,111
r�
VIN #
CUSTOMER SIGNATURE

Sludge Stabilization Record
Town of Clayton
Little Creel: Water Reclamation Facility
Date: 2Z 20/g Location: 6 rXiz/z l
Volume Treated: .Z �'/, 20 a Alkali Used: Ica Ce,3
Volume Used: �6 0
Time
Time / Date
pli
Correction
Final
Temp.
Factor
pH
Initial
0�30
6.3y
. o z
G .36
2S. g
After Addition
�/Z
(>= 12.00 after temp.
p8o0j?/z ��
So
. o36
correction )
Two Hrs. After Addition
1000 /,/����
/I, /o
� I ��
!
(>= 12.00 after temp.
2 9 . %
correction )
I
24 Hrs. after Addition
0�00 '7l� ����}
i2.o6
0.o y
IZ , ►
26 y
(>= 11.50 after temp.
correction )
Preparer: Q�t..' -/ t �1Svn
Date/ Time
Buffer
Reading
NIN,
'-/. v
Y,o
/6 -, F
7.0
,o
0,7
to.p
io of
9-
4, !
/Z.yy' 12-6L "3R.1Int:
Slope 6,17 90v
Date/Time
Buffer
Reading
INIv
2Nv
". Q/
91 c`t
- 45'. N
l
r> t
49-i
ZZ, 6.
1 7 .r
l ��`�
*3/ . ,0
Int:i. Slope .SY.,7.3 =i f

B rnett Lime Company, Inc.
095 Hwy 11, Campobello, SC 29322.
❑ 5200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
S C'la��tr
0 .-Uhl . i _ L ,. tits
D }ay, n
T
0
S
H
I
P
T
0
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
52624
SHIPMENT WEIGHTS
In
O
l7
PROJECT NO.
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
CUSTOMER NO. BLC ORDER LOT NO. CUSTOMER PURCHASE ORDER NO. SHIPPED VIA TERMS
t
--- — • - .__ 1
cam'
ORDEREDDESCRIPTION
1 1 Tanker CAL—FLO' Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
CAL--FLO
BEGINNING TANK LEVEL FT ENDING TANK LEVEL
FT SYSTEM 6 SLURRY
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS
4 Slurry
t� k �Fq �? faterTreatment
4 Drinking Water Treatment Additive
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE
R Tested in accordance with
• ' ° Standard ANSI/NSF60
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE
Caidum Hydroxide
`°�PENOE�`` 6so mg/L Maximum use Level
0 ju 7)
CUSTOMER SIGNATURE

Sludge Stabilization Record
Town of Clayton
Little Creek Water Reclamation Facility
Date: f 3o//q Location: ro'k #'/
Volume Treated: -3o Dl L?60 Alkali Used: C /j f O 3 030
Volume Used:__fi�6 G
Time
Time / Date
pH
Correction
Final
Temp.
/o/S�%/.3�/!9
Factor
P11
Initial
?.�/
I l y
After Addition
(>= 12.00 after temp.
/-7� N
lvyv 3�
,z. �s
� q
!z, zy
�-7,
correction )
;
Two Firs. After Addition
(>= 12.00 after temp.
12 qe /.3e/
.
/
12 ..3�3
7- 9. l
correction )
24 Hrs. after Addition
/ t7-5
7-3i ly
�l• S�
2� "zs = Z'
Z.�Yo.,3
ii. 89tp•o6
27, f
(>= 11.50 after temp.
correction )
�
Prepares: L7g L"; d %¢74.:730,,
U
Date/ Time
Buffer
Reading
NIN•
7/36//9100$_
2.00
7.06
0 . �
7/3el /o J4-S
l 0 . o /
- / P.2. 9
713,1/1a6
/a.6S
—318.8
Int:.OW Slope -SP 1,q
Date/ Time
I Buffer
Reading
NIN•
73,L G�tiS
7.6<
-7.0 /
-7,0
715, I
/G•dt
!-,,03
-17V7
7 2, <q 'V
ssYs
, 2-- 9
-3�2,z
Int:� Slope SS' zV

Burnett�Line Company, Inc.
©1095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
S
0 Aun- Accoui t� i
C Y 0
D
clll 1y to!j. NC
T
0
H LIzfle CJ edl ',` 1-1
I l��.lfl �ut�i".�4ik `.si�.r•�
�ay L -
T
0
CUSTOMER NO. BLC ORDER LOT NO.
,_Utlt
PROJECT NO.
CUSTOMER PURCHASE ORDER NO.
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
5?6?5
SHIPMENT WEIGHTS
Ln
to
0
z
C7
LL
Of
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
SHIPPED VIA TERMS
l
1 1 1 Tanker CAL —FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING EKi
F LO'BEGINNING TANKLEVEL FT ENDING TANK LEVEL FT L U R R Y
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
5. �Eq` CAL-"O' Slurry
AND OFF-LOADING AREA CLEANLINESS .t � �rink(ngWater TreatmentAdditive
Tested In accordance with
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE • ' Standard ANSI/NSF60
a Calcium Hydroxide
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE yCpNDEN� • 650 mg/L Maximum Use Level
INSTRUCTIONSSPECIAL DRIVER NAME TANKER NO.
i l VIN #
W I I
z
/
,/ 1 t7
CUSTOMER SIGNATURE

Sludge Stabilization Record
Town of Clayton
Little Creek Water Reclamation Facility
Date: /O Location: �IGC�� �GL�jIC
Volume Treated: r°l7f 6 G� Alkali Used:
Volume Used. W, /&P
Time
Time /Date Al
Correction
�
Final
Temp.
Factor
PH
' -7 Zq
Initial
_
/03S�io -l5 7 3S
�3s`D o6
After Addition
12.30
Two Ilrs. After Addition
{
13ly//0.7-1
fZ. lq
i� 19'� 0.0C
-
� 2, Z
24 I-Irs. after Addition
//20//041_/5
I. it 0.03
12,01
Z61
Preparer•.� .,� U
Date/ Time
Buffer
Reading
iINlN.
-A-5
Int: G � ` Slope
Date/ Time
Buffer
Reading
i IN,
1G1.0V
16.
5
7
Int: %{'1- Slope:. y%-

B rnett Lime
095 Hwy 11, Campobello, SC 29322
❑ 5200 US Hwy 17 S, Bartow, FL 33830
❑ 1100 Airport Rd, Eastaboga, AL 36260
SHIPMENT DATE
)0-7-1r
s Clayton joiiw of)
0 Athi: Accounts Payable
L P.O. Box 8 789
D
Clayton, NC 27520
T
O
s Clay -ton NvNM
H Little Creek NVRF
1 1.000 Durham Street Ext.
P Clayton, NC 27520
T
O
CUST"O. BLC ORDER LOT NO.
VVVVOo
1 1 1
Company, Inc.
C
PROJECT NO.
CUSTOMER PURCHASE ORDER NO.
4�k C . )-C --1- 4
CERTIFIED PUBLIC WEIGHER
DELIVERY TICKET NO.
52626
SHIPMENT WEIGHTS
I
BILL FREIGHT CHARGES TO:
BURNETT LIME CONSIGNEE
_ SHIPPED VIA TERMS
Net 30
Tanker CAL -FLOG Slurry
DRIVER MUST FIND OPERATOR ON DUTY AT END OF OFF-LOADING
NO DILUTION WATER NEEDED
AUTOMATIC DILUTION METER TURNED "ON"
INITIAL WATER METER READING
FINAL WATER METER READING
BEGINNING TANK LEVEL FT ENDING TANK LEVEL FT CAL =FLO'
S.Y5 TE M a SLV R RY
*OPERATOR REQUESTED TO INSPECT SLURRY DILUTION ACCURACY
AND OFF-LOADING AREA CLEANLINESS o! �E4r CAL FLO- Slurry
Wt Drinking Water Treatment Additive
Tested in accordance wM
OPERATOR UNABLE TO INSPECT UNLOADING PROCEDURE Standard ANSI/NSF60
Calcium Hydroxide -
OPERATOR INITIALS IF DIFFERENT FROM CUSTOMER SIGNATURE y�E'ENOES 650mg/LMaximumUse Level
!L -y— I VIN # l L L L L
Z� L�b, 1 V 0 Lh y r

N
Q.
Pern2itee
Land Application permit i\c:
A Lit.4i,ITTk. S'J .A$dI,I A'I 1(),N OF 14'AS7f ,'%VArER BIOSOL.13)S
$aich We {gsHons} ; [�,1�1� Lbs. of Limey
�mtr►e�ts:
Datevlwrp
P �+
7
0
i

Permit=
Land Appheation Perm.it -tq, - �:
A LKALINE STABILIZ.4-TION 010WASTEWATEM SIOSOLIDs
Batch Size (gallons) - - l—, -
Lbs.0fLime , nt�IL�
tti
Cm
Ir
..........
... ... .......
C., L
CA, 1 7
o v: i
1 �r N 1 cv I N I o I �� `� a a_ I �" Y `^ 1"' —
�2
CX
Ig!
I

Triple S Farins If Q0030998
FaciliLime Stabilization Documentation z0 9
ty• Mame Southwest PlSouthwestmatmn�ar Trail Bear
men
SignaturCFR
�503
• EPA time stabilization requires lotre nuxed wnh sewage sludge to have a pit of 12 or greater for 2 hours and maintain a pit of I 15 for the following 22 hours
pll.rw actual pi valises that hate not been ictnperatute cormcmd
p11.— w v pit values have been temperature corrected
All temperature units arc in Celsius
15
v1
N
C.,
�D
M
O
t-
d'
^t
00
V1
N
cN
iD
m
O
M
,D
a..
N
r!1
00
•--s
d'
r
O
M
.D
t71
M
M
M
M
N
N
�CD
N
•--r
.--r
•--�
O
O
O
O
O
O
CD•-+
N
N
N
M
M
en
M'
c 1;
ti
C
t3
0
0=
C
O
a
C
O
C
O
G
C
C
O
O
O
0
0
0
O
o
C
O
C
C
O
O
V
U
O
Ch
w
"D
to
d
cry
N
O
7
M
t-
1.0
to
d
M
N
O
M
W
t�
1.0
h
d'
M
O
4
7
M
M
M
M
M
M
M
M
M
M
N
N
f V
N
N
N
N
N
N
N++
r+
.—.
-
--s
•--�
8
rL
I"'

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Jan-19
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
1/16/19
71
1.851
2
1/16/19
66
1.820
3
1/16/19
76
1.881
4
1/16/19
62
1.792
5
1/16/19
75
1.875
6
1/16/19
72
1.857
7
1/16/19
75
1.875
Totall 12.951
Averagel 1.850
Most Probable Number / Gram 1 71 Fecal Coliform
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

envirochem
rM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
infoCu environmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Feb 07, 2019
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2019-00865
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-02161 Site: 1 1/15/2019 10:24 AM Solid/Sludge David Verdin/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.56 % 01/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 <71 MPN/g 01/16/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-02162 Site: 2 1/15/2019 10:26 AM Solid/Sludge David Verdin/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.73 % 01/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 <66 MPN/g 01/16/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-02163 Site: 3 1/15/2019 10:28 AM Solid/Sludge David Verdin/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.39 % 01/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 <76 MPN/g 01/16/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-02164 Site: 4 1/15/2019 10:30 AM Solid/Sludge David Verdin/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.92 % 01/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 <62 MPN/g 01/16/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-02165 Site: 5 1/15/2019 10:32 AM Solid/Sludge David Verdin/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.42 % 01/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 <75 MPN/g 01/16/2019

Environmental Chemists, Inc.
envitroche 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Branch Residuals/Bob Branch Date of Report: Feb 07, 2019
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2019-00865
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-02166 Site: 6 1/15/2019 10:34 AM Solid/Sludge David Verdin/Brent Dean
Test Method Results Date Analyzed
Total Solids SM 2540 G 2.51 % 01/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 <72 MPN/g 01/16/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-02167 Site: 7 1/15/2019 10:36 AM Solid/Sludge David Verdin/Brent Dean
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.43 % 01/17/2019
Fecal Density SM 9221C E MPN 24 hr 503 <75 MPN/g 01/16/2019
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: Kou�',Qa

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO:
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: AnthonyColon, Public Works
email: [e-mail]
Samnlpd Rv- .�! -1 \ br.,l.n . Af, _ 4 1_ . SAMPI F TYPF 1 = Inflnant F c Fffluant W = wA CT = Rtremr„ Cr1 = Cna CI
Sample Identification
Collection
m
m
y F
N .O
E
v
m _
C (�
c
v a
m
C =
O1
v E
0 W
ca
Q
'' z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
i
=
o
_
o
=
p
i
~
W
o
Sludge
- -
logo
C
P
����
X
ff
nutrients/metals • V
G
G
1
1-15-6
0 211
C
P
' 1
X
fecal density/ %TS
G
G
2
-15-19
Ing
C
P
X
Ifecal density/ %TS
G
G
3
- 15-1
l 0 43
C
P
>
}
X
fecal density/ %TS
G
G
4
-15-
)030
C
P
v 1
X
fecal density/ %TS
G
G
5
1-15-)9
103Z
C
P
o f
X
fecal density/ %TS
G
G
6
-15-M
I ojq
C
P
X
fecal density/ %TS
G
G
7
-15-11
C
P
dCab�
X
fecal density/ %TS
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
-
I-15-201AR
429fI
Temperature when Received: 9 ( Accepted: ( Rejected: Resample Requested:
Delivered By: Received By: -,- 1 i%l� l t. -�' t� Date: `) ci Time: i'
Comments: ARbUND:
t

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Jun-19
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
6/6/19
744
2.872
2
6/6/19
4,045
3.607
3
6/6/19
2,933
3.467
4
6/6/19
1,712
3.234
5
6/6/19
675
2.829
6
6/6/19
1,545
1 3.189
7
6/6/19
779
1 2.892
Totall 22.089
Averagel 3.156
Most Probable Number / Gram 1 1,431 Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

41
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill 4Vay, Wilmington, NC 25405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, 1%9anteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inforrenvironmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Jun 25, 2019
Customer PO #:
Customer ID: 15060009
Attention: Report #: 2019-08949
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-22818 Site: Sludge 1 6/5/2019 10:07 AM Solid/Sludge Will Barr
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.69 % 06/06/2019
Fecal Density SM 9221C E MPN 24 hr 503 744 MPN/g 06/06/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-22819 Site: Sludge 2 6/5/2019 10:09 AM Solid/Sludge Will Barr
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 2.72 % 06/06/2019
Fecal Density SM 9221C E MPN 24 hr 503 4045 MPN/g 06/06/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-22820 Site: Sludge 3 6/5/2019 10:11 AM Solid/Sludge Will Barr
Test Method Results Date Analyzed
Total Solids (%)
SM 2540 G
2.66 %
06/06/2019
Fecal Density
SM 9221C E MPN 24 hr 503
2933 MPN/g
06/06/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-22821 Site: Sludge 4
6/5/2019 10:13 AM
Solid/Sludge Will Barr
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.63 %
06/06/2019
Fecal Density
SM 9221C E MPN 24 hr 503
1712 MPN/g
06/06/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-22822 Site: Sludge 5
6/5/2019 10:15 AM
Solid/Sludge Will Barr
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 G
2.67 %
06/06/2019
Fecal Density
SM 9221C E MPN 24 hr 503
675 MPN/g
06/06/2019

envirochem
sn+
ANALYTICAL & CONSULTING CHEMISTS
pp"'W-. - -77qq1
Branch Residuals/Bob Branch
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
into(I enviroil men talc hemists.com
Date of Report: Jun 25, 2019
Customer PO #:
Customer ID: 15060009
Report #: 2019-08949
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-22823 Site: Sludge 6 6/5/2019 10:17 AM Solid/Sludge Will Barr
Test Method Results Date Analyzed
Total Solids SM 2540 G 2.59 % 06/06/2019
Fecal Density SM 9221C E MPN 24 hr 503 1545 MPN/g 06/06/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-22824 Site: Sludge 7 6/5/2019 10:19 AM Solid/Sludge Will Barr
Test Method Results Date Analyzed
Total Solids SM 2540 G 2.57 % 06/06/2019
Fecal Density SM 9221C E MPN 24 hr 503 779 MPN/g 06/06/2019
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:

6602
Windml Way
ENVIRONMENTAL CHEMISTS, I N C OFFI E: 910I392-0223'IFAX 910-392-44245
7 e t cio� ..
Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: q /
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: AnthonyColon, Public Works
email: [e-mail]
Sampled By: / SAMPLE TYPE: I = Influent. E = Effluent. W = Well_ ST = Stream_ Sn = Snit Si = Ahiffno nthor•
Sample Identification
Collection
m m
E F
N
a
E a
U
E
� o
Li a
S-j
1 a
U E
2 W
00 �
g i
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
i
-j
=
o
i
0
z
0
i
o
~
w
o
Sludge
G-s-I g
a
C
P
1
'L�'�,1X
nutrients/metals
G
G
- -I
Iau'1
C
P
X
fecal density/ %TS
G
G
2
C -5-19
C
P
41
X
fecal density/ %TS
G
G
3
G-S-1
e ►
C
P
�'�
X
fecal density/ %TS
G
G
4
-5- 6
t
C
P
�
X
fecal density/ %TS
G
G
5)
-$-t�
t D l S
C
P
ti
v
X
fecal density/ %TS
G
G
ti
C
P
X
fecal density/ %TS
G
G
7
- i10I
C
P
gti�
2�
X
fecal density/ %TS
G
G
C
E-
--G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
G -S - f g
1&-,44
35-
2.
T.. ..a..... ...1-_._
.
1 CIII pera Lure When r
Delivered By:
Comments:
rime: 1 y V

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Sep-19
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
9/19/19
3,709
3.569
2
9/19/19
2,967
3.472
3
9/19/19
3,559
3.551
4
9/19/19
4,070
3.610
5
9/19/19
1,442
3.159
6
9/19/19
2,113
3.325
7
9/19/19
21,177
4.326
Totall 25.012
Averagel 3.573
Most Probable Number / Gram 3,743 Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

ro"7 41 Environmental Chemists, Inc.
1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
s�.i 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS into icenvironmentalchemists.com
Branch Residuals/Bob Branch Date of Report: Oct 08, 2019
Customer PO #:
Customer ID: 15060009
Attention, Report #: 2019-15734
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-40316 Site: #1 9/18/2019 10:15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-40317 Site: #2
Test
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.13 % 09/19/2019
3709 MPN/g 09/19/2019
Collect Date/Time Matrix Sampled by
9/18/2019 10:15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.36 % 09/19/2019
Fecal Density SM 9221C E MPN 24 hr 503 2967 MPN/g 09/19/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-40318 Site: #3 9/18/2019 10:15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.22 % 09/19/2019
Fecal Density SM 9221C E MPN 24 hr 503 3559 MPN/g 09/19/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-40319 Site: #4 9/18/2019 10:15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.31 % 09/19/2019
Fecal Density SM 9221C E MPN 24 hr 503 4070 MPN/g 09/19/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-40320 Site: #5 9/18/2019 10:15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
Ski 922 iG E IVI N 24 hr 503
2.29 % 09/19/2019
1442 MPN/g 09/19/2019
RPnnrt It 901Q-1571d o.,..e 9 . f I

envirochem
SM
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
Attention -
Lab ID Sample ID:
19-40321 Site: #6
Test
Total Solids (%)
Fecal Density
Lab ID Sample ID:
19-40322 Site: #7
Test
Total Solids (%)
Fecal Density
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, klanteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info a-em-ironmentalchemists.com
Date of Report: Oct 08, 2019
Customer PO #:
Customer ID: 15060009
Report #: 2019-15734
Project ID: Wallace WWTP
Collect Date/Time Matrix Sampled by
9/18/2019 10:15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Method Results Date Analyzed
SM 2540 B 2.32 % 09/19/2019
SM 9221C E MPN 24 hr 503 2113 MPN/g 09/19/2019
Collect Date/Time Matrix Sampled by
9/18/2019 10.15 AM Solid/Sludge Lisa Cottle/Ralph Ezzell
Method Results Date Analyzed
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.55 % 09/19/2019
21177 MPN/g 09/19/2019
Comment: Results reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report # : 2019-15734

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
Info ® environmentalchemists.com
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: 3
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, ORC
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Anthony Colon, Public Works
email: [e-mail]
Sampled By: C-77 f t E SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
2L
H
a
y
o a
a 6 m
U
r
g
0 a
o Im
"
¢
m
-' z
PRESERVATION
ANALYSIS REOUESTED
Date
Time
Temp
_
i
U
=
N
o
=
o
z
a
W
o
Sludge
C
P
�
X
nutrients/metals
I Pil I
d; IS
G
G
1)
C
P
���
X
fecal density/ %TS
G
G
2)
C
P
�
X
fecal density/ %TS
G
G
3)
C
P
�1b3�
X
fecal density/ %TS
G
G
4)
C
P
`
�31�
X
fecal density/ %TS
G
G
5
C
P
3�
X
fecal density/ %TS
G
Gu
6)
C
P
X
fecal density/ %TS
G
G
7)
C
P
ti
X
fecal density/ %TS
G
G
C
P
TF
I
I
G
G
Transfer
Relinquished By:
Date/Time
Received By:
DateMme
1.
tC
2.
Temperature when Received: Accepted:
Delivered By: Received By:
Comments:
Resample
TU
Time:— _
UND:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NCO020702
Nov-19
Environmental Chemists, Inc.
Lab #
Date Analyzed
Most Probable Number
per gram
Log
1
11/20/19
10,000
4.000
2
11/20/19
5,807
3.764
3
11/20/19
5,625
3.750
4
11/20/19
7,500
3.875
5
11/20/19
6,429
3.808
6
11/20/19
6,429
3.808
7
11/20/19
2,128
3.328
Totall 26.333
Averagel 3.762
Most Probable Number / Gram 5,780 Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

envirochem
G1.4
ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, t%,Ianteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
inro a,em'ironmentutchemists.conl
Date of Report: Dec 04, 2019
Customer PO #:
Customer ID: 09010063
Report #: 2019-19452
Project ID: WWTP Sludge
Lab ID
Sample ID:
Collect Date/Time
Matrix
Sampled by
19-49371
Site: 1
11/19/2019 9:35 AM
Solid/Sludge
David Verdin
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
0.18 %
11/20/2019
Fecal Density
SM 9221C E MPN 24 hr 503
<10000 MPN/g 11/20/2019
Lab ID
Sample ID:
Collect Date/Time
Matrix
Sampled by
19-49378
Site: 2
11/19/2019 9:35 AM
Solid/Sludge
David Verdin
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
0.31 %
11/20/2019
Fecal Density
SM 9221C E MPN 24 hr 503
<5807 MPN/g 11/20/2019
Lab ID
Sample ID:
Collect Date/Time
Matrix
Sampled by
19-49379
Site: 3
11/19/2019 9:35 AM
Solid/Sludge
David Verdin
Test
Method
Results
Date Analyzed
Total Solids (%) SM 2540 B 0.32 % 11/20/2019
Fecal Density SM 9221C E MPN 24 hr 503 <5625 MPN/g 11/20/2019
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-49380 Site: 4 11/19/2019 9:35 AM Solid/Sludge David Verdin
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
0.24 %
<7500 MPN/g
11/20/2019
11/20/2019
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
19-49381 Site: 5
11/19/2019 9:35 AM
Solid/Sludge David Verdin
Test
Method
Results Date Analyzed
Total Solids (%)
SM 2540 B
0.28 %
11/20/2019
Fecal Density
SM 9221C E MPN 24 hr 503
<6429 MPN/g
11/20/2019

• •
ANALYTICAL & CONSULTING CHEMISTS
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Environmental Chemists, Inc.
6602 Windmill k- a}; Iilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowscrtovvn Road, Manteo, NC 279-94 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(u en%ironnlentalcheiuists.coni
Date of Report: Dec 04, 2019
Customer PO #:
Customer ID: 09010063
Report #: 2019-19452
Project ID: WWTP Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-49382 Site: 6 11/19/2019 9:35 AM Solid/Sludge David Verdin
Test Method Results Date Analyzed
Total Solids (%
Fecal Density
Lab ID Sample ID:
19-49383 Site:7
Test
SM 2540 B
SM 9221 C E MPN 24 hr 503
Collect Date/Time
11 /19/2019 9:35 AM
Method
0.28 % 11/20/2019
<6429 MPN/g 11/20/2019
Matrix Sampled by
Solid/Sludge David Verdin
Results Date Analyzed
Total Solids (%) SM 2540 B 0.94 % 11/20/2019
Fecal Density SM 9221C E MPN 24 hr 503 2128 MPN/g 11/20/2019

ENVIRONMENTAL CHEMISTS i N C 6602 Windmill Way, Wilmington, NC 25405
/ Office: 910-392-0223 Fax: [phone]
Analytical & Consulting Chemists NCDENR: DWQ certification #94 NHCDHHS: DLS certification #37729 [e-mail]
Collection and Chain of Custody
Client: Town of Wallace WWTP
Project name: WWTP LTMP-sludge samples
Report No: i C — I C1 L-}
Address: PO Box 849
Contact name:
PO No:
Wallace, NC 28466
Report To: Brent Dean, ORC
Phone/Fax: Brent 910-284-7969
Copy to:
Email: [e-mail]
Sampled by: t i �%
SAMPLE TYPE: 1= Influent,
E= Effluent,
W=Well, ST= stream, SO= Soil, SL=Sludge, Other:
Sample Identification
collection
a
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date
time
temp
v
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=
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(_
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X
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2. sludge
j_ .. 9
G
P
X
Fecal Density,%TS
3. sludge
—1 _1
G
P
X
Fecal Density,%TS
4. sludge
G
P
`
X
Fecal Density,%TS
5. sludge
(_
09sr2
G
P
I
X
Fecal Density,%TS
6.sludge
i_(q.M
G
P
X
Fecal Density,%TS
7. sludge
-49
091S5G
P
X
Fecal Density,%TS
Transfer
Relinquished By:
Date/time
Received By:
Date/time
2
temp when received: C U71 t C Accepted: Rejected: Resample:
delivered By: Received by: date/time \ l q (C'/ Soo
Comments: turnaround:

B 17-IS 91usymm
Jan. 21, 2020 lc 24PU 9 37701 .z
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1 -0.24
16 -0.27
15 -0.30
14 -0.33
13 .0.36
12 -0.39
11 -0.42
i 0 .0.45
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Jan.21.2020 3:58PM �v
71n4y3r rbl PA
No.0207 P. 4
Tamp C
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0.45
39
38
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0,39
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Jan. 21, 2020 3:58PM
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No.0207 P. 5
Temp C 8aclor
40 0.45
39 0.42
38 0.39
371 0.36
361 0.33
34
0.27
33
0.24
32
0.21
31
0.18
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28
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jai. L I mu j:59pm
-----No. 0207
F.0
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lamp C
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14
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13
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12
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11
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10
-0.45

SOIL ANALYSIS REPORTS

SOIL SAMPLE ANALYSES
The Town of Beulaville, the Town of Warsaw, the Town of Clayton, the Town of Kenansville and
Southwest Plantation met pathogen reduction and vector attraction reduction requirements through
lime stabilization. The soil pH will continue to be raised through the continued application of lime
stabilized biosolids to these application fields.

PE
LA"U",
I
O+J
Location
Dixie Chemical - Beulaville
Sample Summary
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm Field 1 32.85 acres 34.908716,-78.012548
Sample Date: 2019-10-18 Soil Lab: Waters NC
Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy
01 '27/20 0142 PM
Beulaville, NC 28518

8
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Sample Summary
Location
Dixie Chemical - Beulaville
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm Field 2 9.06 acres 34.912564,-78.013934
Sample Date: 2019-10-18 Soil Lab: Waters NC
Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy 0112T20 01 :43 PM
Beulaville, NC 28518

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Location
Dixie Chemical - Beulaville
Sample Summary
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm Field 3A 14.85 acres 34.911282,-78.015917
Sample Date: 2019-10-18 Soil Lab: Waters NC
1 /1 Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy
Beulaville. NC 28518
01 /2720 01:44 PM

m
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Sample Summary
Location
Dixie Chemical - Beulaville
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm Field 3B 7.5 acres 34.912407,-78.017559
Sample Date: 2019-10-18 Soil Lab: Waters NC
1 /1 Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy
Beulaville, NC 28518
aln_ooa_iaan
01 /27i20 01.45 PM

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
"I wzpra &nq'Crawt1 :..
jY
W U�v Sc l e4AAC&
HARVEYS-BEULAVILLE [601261 Grower: TRIPLE S FARMS Page 1
Farm: TRIPLE S FARM / FIELD 3B
1060 S NC 41 & 111 LID: D2FF2589189 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 10/18/2019 Processed: 10/22/2019
Sample ID
22
LablDP-I
825164QW
199
K-I
Mg (%)
13
Ca (%)
75
pHw
Ac
S-I
Zn-I
Zn-AI
532
Mn-I
Mn-AI
Cu-I
CEC
10.0
BS (%) HM (%) Soil Class
9t] 0.76 Min
46
5.9
1.0
60
532
41
34
285
23
825165QW
184
52
16
74
6.2
0.6
52
522
522
44
40
312
8.8
93
0.67
Min
24
825166OW
232
64
12
76
6.0
0.8
55
622
622
41
42
345
9.5
92
0.75
Min
Explanation of Symbols - % (percent), -1 (Index); CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter)
NCDA Soil Fertility Recommendations (Ibs/A)
. • . , Lime N P2O5 K2O Mg s B
Tons/Acre Nitrogen Phosphate Potash Magnesium Sulfur Boron
22 BERMUDA PASTURE M j 0.3 220 120
23 BERMUDA PASTURE M 220 110
Zn Mn Cu See Note
Zinc Manganese Copper
12
12
24
BERMUDA PASTURE M
220
80
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is Gmiled to the lee assessed on the referenced sample.

Sample Summary
Location
Dixie Chemical - Beulaville
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm Field 4 5.49 acres 34.913876,-78.019044
Sample Date: 2019-10-18 Soil Lab: Waters NC
1 /1 Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy
Beulaville, NC 28518
ni n nno ncen
01/27/20 01:46 PM

A RS Ic RAL
O IE Nc.
HARVEYS-BEULAVILLE [601261
1060SNC41 &111
BEULAVILLE, NC 28518
TRI741 P-1
25 825167QW 115
26 1825168QW 1 107
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
Grower: TRIPLE S FARMS
Farm: TRIPLE S FARM / FIELD 4
LID: D2FF2589195
Test Method: Mehlich III
K-1 Mg (%) Ca (°k) pHw Ac S-1 Zn-I Zn-AI Mn-I
95 10 50 fr-5
,3 2.0 35 310 310 34
31 8 46 , 5.0 2.2 21 216 216 38
Explanation of Symbols - % (percent), -1 (Index); CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter)
"Improv& ,W(�ro-wth:..
W i�t e ScACPE/
Page 1
Target pH: 6
Received: 10/18/2019
Processed: 10/22/2019
Mn-AI Cu-I
CEC
BS (%) HM (%) Soil Class
30 182
6.2
68 1,22 Min
32
140
5.1
57
0.46
Min
NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID Crop Lime N P205 K20 Mg S B Zn Mn Cu See Note
Tons/Acre Nitrogen Phosphate Potash tNagnesium Sutfur Boron Zinc Manganese Copper
25 BERMUDA PASTURE M 1.1 220 30 12
26 BERMUDA PASTURE M
1.4
220
160
25
20
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agncutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited to the fee assessed oo the referenced sample.

Sample Summary
Location
Dixie Chemical - Beulaville
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm Field 5 13.56 acres 34.91382,-78.016318
Sample Date: 2019-10-18 Soil Lab: Waters NC
1 / I Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy
Beulaville, NC 28518
ni n nno 30an
01 /27/20 01:47 PM

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
"IwLprov&-CrowJ :..
Wa�VSGEell Pijl
HARVEYS-BEULAVILLE [601261 Grower: TRIPLE S FARMS Page 1
Faun: TRIPLE S FARM / FIELD 5
1060 S NC 41 & 111 LID: D2FF2589191 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 10/18/2019 Processed: 10/22/2019
825169QW
P4
K-1
Mg (%)
Ca
pHw
5.7
Ac
S-1
Zn-I
Zn-AI
406
Mn-I
47
Mn-AI
Cu-I
295
CEC
BS (%)
HM (%) Soil Class
0.85 Min
27
200
109
8
64
1.4
39
406
38
7.1
80
28
825170QW
432
99
10
75
5.7
1.4
64
944
944
75
54
510
13.0
89
0.63
Min
29
825171QW
297
42
7
76
5.4
1.4
56
681
681
50
39
458
9.7
85
0.92
Min
30
825172OW
338
71
8
63
4.9
2.8
74
798
798
66
49
535
10.9
74
0.77
Min
31
825173OW
428
47
9
78
5.6
1.4
70
938
938
69
51
540
12.6
89
0.56
Min
F_
1-_
I-, _.
I
-
I
I I
1_1
- I
I
Explanation of Symbols - % (percent), -1 (Index); CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter)
NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID Crop Lime N P2O5 K2O Mg S B Zn M Mn Cu See Note
Tons/Acre Nitrogen Phosphate Potash Magnesium Sulfur Boron Zinc Manganese Copper
27 BERMUDA PASTURE M 0.5 220 20 12
28
BERMUDA PASTURE M
I 0.5
220
30
4
12
29
BERMUDA PASTURE M
0.7
220
140
12
30
BERMUDA PASTURE M
1.8
220
70
12
31
BERMUDA PASTURE M
0.6
220
120
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety. Waters Agricutural Laboratones has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is lInied to the fee assessed on the referenced sample.

YIPI rJJ
Putro H
im
i
li&
f
�5
4
64
5
4,
i
ti

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
«rWtPr0'VC4Aq, (5rOU`t�V. . .
wUl,soce4'1�'
HARVEYS-BEULAVILLE [601261
1060 S NC 41 & 111
BEULAVILLE, NC 28518
° e
32 825174QW
33 825175QW.
P-I
64
59
K-1
64
76
Grower: TRIPLE S FARMS
Fans: TRIPLE S FARM / FIELD 7
LID: D2FF2589194
Test Method: Mehlich III
Mg (°k) Ca (°�) pHw j Ac S-I
1 8 33 4.9 3.8 27
9 28 5.1 2.8 42
Zn-I
145
114
Zn-AI
145
114
Mn-I
31
22
Received: 10/18/2019
Mn-AI Cu-[ CEC
28 95 7.0
23 90 5.0
Page 1
Target pH: 6
Processed: 10/22/2019
BS (%) HM (%) Soil Class
45 1.81 Min
44 1.47 Min
34
825176QW
36
117
7
17
5.0
4.6
32
68
68
16
19
50
6.0
34
2.61
Min
35
825177QW
43
89
7
22
4.6
4.6
31
98
98
19
21
58
6.3
36
2.60
Min
36
825178QW
19
49
7
37
4.6
2.8
100
108
108
16
19
55
5.4
48
0.91
Min
37
825179QW
32
23
5
40
4.7
2.8
51
118
118
19
21
68
5.3
48
3.36
Min
38
825180QW
55
45
6
36
4.6
4.0
45
141
141
25
24
82
7.3
45
2.00
Min
Explanation of Symbols - % (percent), -1 (Index); CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity). CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter)
NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID
32
Crop Lime
Tons/Acre
BERMUDA PASTURE M 2.5
N
Nitrogen
P2O5 K2O
Phosphate I Potash
Mg
Magnesium
S B Zn
Sulfur Boron Zinc
Mn
Manganese
Cu
Copper
See Note
220
20
80
12
33
BERMUDA PASTURE M
1.7
220
20
60
25
12
34
BERMUDA PASTURE M
2.9
220
60
20
25
12
35
BERMUDA PASTURE M
3.2
220
30
40
25
12
36
BERMUDA PASTURE M
2.0
220
90
110
25
12
37
BERMUDA PASTURE M
1.9
220
70
180
25
12
38
BERMUDA PASTURE M
2.8
220
20
120
25
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirety Waters Agriculural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is limited io the fee assessed on the referenced sampte.

E ... --.
LY3 k/
Sample Summary
Location
Dixie Chemical - Beulaville
Grower Farm Field Area Centroid
Triple S Farms Triple S Farm Field 9 12.38 acres 34.904472,-78.010869
Sample Date: 2019-10-18 Soil Lab: Waters NC
Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy
Beulaville, NC 28518
01n_Ooa_e4aan
0112T20 01 :48 PM

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
" I wLpsra &YLq' Cv-awth .. .
wa�,soce+l�.1
HARVEYS-BEULAVILLE [601261 Grower: TRIPLE S FARMS Page 1
Farm: TRIPLE S FARM / FIELD 9
1060 S NC 41 & 111 LID: D2FF2589193 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 10/18/2019 Processed: 10/22/2019
Sample ID
39
LablD
825181QW
P-1
K-I
195
Mg (%)
15
Ca (%)
pHw
Ac
S-1
Zn-I
Zn-AI
306
Mn-I
Mn-AI
Cu-I
270
950
CEC
10.9
18.5
BS (%)
a
HM (%) Soil Class
1.63 Min
275
87
6,1
6.3
1.0
40
306
59
51
91
40
825182QW
401
194
10
84
0.2
104
1438
1438
75
57
99
1.54
Min
41
825183QW
188
131
14
65
5.8
1.0
63
320
320
44
36
290
8.0
87
1.17
Min
42
825184QW
220
67
12
69
6.2
0.8
29
288
288
75
59
235
5.7
86
0.59
Min
43
825185QW
258
93
13
76
6.4
0.2
32
299
299
62
48
258
6.1
97
1.28
Min
44
825186QW
186
101
14
59
5.9
1.0
31
215
215
53
41
228
5.6
82
0.97
Min
Explanation of Symbols - % (percent), -1 (Index); CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter)
Sample ID
39
40
Crop
BERMUDA PASTURE M
BERMUDA PASTURE M
NCDA Soil Fertility Recommendations (Ibs/A)
Lime N P2O5 K2O Mg S B
Tons/Acre Nitrogen Phosphate Potash Magnesium Sulfur Boron
�220 -t t
220
Zn Mn Cu See Note
Zinc Manganese Copper
12
12
41
BERMUDA PASTURE M
0.3
220
12
42
BERMUDA PASTURE M
220
80
12
43
BERMUDA PASTURE M
220
30
12
44
BERMUDA PASTURE M
I 0.3
220
30
12
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only in its entirely- Waters Agncutural Laboratories has no control over the manner in which samples are taken, therefore, analysis is based solely on the sample as received. Laboratory liability is kmsW to the fee assessed on the referenced sample-

2019 APPLICATION SUMMARY TABLE

TRIPLE S FARMS
LAND APPLICATION PROGRAM
PERMIT NO. WQ0030998
2019 APPLICATION SUMMARY
: ..........
...
.
:/Site'::'
I ..... :
......
d
.......
::A
..c ....
Date
..........
..........
.........
.
y .....
.............
.............................
... ** ...
-.Dr.7669:
y ......
*
........
.....
....
...
Source
PAN
Eric Smith
1
1
34.2
I
Jan- 19
42,000
0.03
0.89
Small Grain
Kenansville WWTP
82.58
Feb- 19
65,200
0.19
6.66
Small Grain
Little Creek WRF
Feb- 19
384,000
1.20
41.08
Small Grain
Wallace WWTP
Mar-19
69,000
0.19
6.39
Bermudagrass
Beulaville WWTP
Mar-19
240,000
0.75
25.68
Bermudagrass
Wallace WWTP
Apr- 19
156,000
0.55
18.67
Bermudagrass
Warsaw WWTP
May-19
80,000
0.22
7.41
Bermudagrass
Beulaville WWTP
Jun- 19
144,000
1 0.50
17.23
Bermudagrass
Warsaw WWTP
Dec-19
83,000
0.25
8.48
Small Grain
Little Creek WRF
2
8.48
Jan- 19
36,000
0.09
0.77
Small Grain
Kenansville WWTP
85.30
Feb- 19
48,000
0.61
5.14
Small Grain
Wallace WWTP
Jul- 19
12,600
0.16
1.36
Bermudagrass
Southwest Plantatior
Jul-19
177,177
2.01
17.08
Bermudagrass
Wallace WWTP
3
21
Jan- 19
50,000
1 0.28
5.98
Small Grain
Warsaw WWTP
134.60
Mar-19
47,800
0.23
4.88
Bermudagrass.
Little Creek WRF
Sep-19
210,300
1.02
21.49
Bermudagrass.
Little Creek WRF
Oct- 19
54,000
0.26
5.52
Bermudagrass.
Little Creek WRF
Nov-19
53,600
0.26
5.48
Small Grain
Little Creek WRF
Dec- 19
83,300
0.41
8.51
Small Grain
Little Creek WRF
4
4.14
Mar-19
30,000
0.74
3.06
Fescue
Little Creek WRF
141.01
Sep-19
66,000
1.63
6.74
Small Grain
Little Creek WRF
5
11.2
Jan-19
280,700
2.56
28.68
Fescue
Little Creek WRF
188.13
Nov-19
65,800
0.60
6.72
Small Grain
Little Creek WRF
6
13.95
Feb- 19
12,600
0.10
1.36
Forest
Southwest Plantation
9.90
Apr- 19
12,600
0.10
1.36
Forest
Southwest Plantation
7
14.5Oct-1
9
72,000
0.46
6.67
Bermudagrass
Beulaville WWTP
11.24
9
8.93
Jan-19
95,000
1.27
11.37
Small Grain
Warsaw WWTP
54.01
Sep-19
48,000
0.11 1
1.02 1
Bermudagrass
Kenansville WWTP
Sep-19
142,000
1.90 1
16.99 1
Bermudagrass I
Warsaw WWTP
Fields Applied to: 8 116.4
Total
Town of Beulaville
Town of Clayton Little Creek WRF
Town of Kenansville
Town of Rose Hill
Southwest Plantation
Town of Wallace
Town of Warsaw
Gallons
Dry Tons
Metric
Tons
Permit Limit Dry Tons
2,860,677
292.65
266.05
NA
221,000
20.46
18.60
38
1,039,700
106.22
96.56
80
126,000
1 2.68
2.44
38
0
0.00
0.00
38
37,800
4.07
3.70
5
849,177
88.97
80.89
330
587,000
70.25
63.87
38
Branch Residuals Soils, LLC Confidential 2/11/2020 Page 1

2019 APPLICATION CONDITION SUMMARIES

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Beulaville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.22
Residual Report No.: B2019 10-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/20/19
1
25,200
Dry
Cool,Clear
0.00
3/25/19
1
43,800
Dry
Warm,Clear
0.00
Total Gallons
69,000

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Beulaville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.22
Residual Report No.: B2019 10-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/10/19
1
80,000
Dry
Warm,Clear
0.00
Total Gallons
80,000

Triple S Farms
Beulaville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Beulaville WWTP
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Surface
Field: 7
Percent Solids: 2.22
Residual Report No.: B2019 10-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/7/19
7
72,000
Dry
Warm,Clear
0.00
Total Gallons
72,000

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/4/19
1
29,700.0
Dry
Cool,Cloudy
0.01
2/5/19
1
35,500.0
Dry
Warm,Clear
0.00
Total Gallons
65,200.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Small Grain
Date
Field No.
Subl;eld
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/11/19
1
29,900.0
Dry
Warm,Cloud3
0.14
12/12/19
1
53,100.0
Dry
Cool,Clear
0.00
Total Gallons
1
1 83,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Bermudagrass.
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/15/19
3
47,800.0
Dry
Warm,Clear
0.00
Total Gallons
47,800.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Bermudagrass.
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/10/19
3
17,500.0
Dry
Jlot,Clear
0.00
9/11/19
3
18,000.0
Dry
Hot,Clear
0.00
9/12/19
3
30,000.0
Dry
Hot,Clear
0.00
9/13/19
3
17,600.0
Dry
Hot,Clear
0.00
9/16/19
3
29,500.0
Dry
Hot,Clear
0.00
9/17/19
3
32,000.0
Dry
Hot,Clear
0.00
9/19/19
3
23,800.0
Dry
Warm,Clear
0.00
9/20/19
3
23,900.0
Dry
Warm,Clear
0.00
9/23/19
3
12,000.0
Dry
Warm,Clear
0.00
9/25/19
3
6,000.0
Dry
Hot,Clear
0.00
Total Gallons
210,300.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Bermudagrass.
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/29/19
3
18,000.0
Dry
Warm,Clear
0.00
10/30/19
3
18,000.0
Dry
Cool,Cloudy
0.02
10/31/19
3
18,000.0
Dry
Cool,Cloudy
0.02
Total Gallons
54,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/12/19
3
12,000.0
Dry
Warm,Clear
0.00
11/13/19
3
11,800.0
Dry
Cool,Cloudy
0:46
11/14/19
3
18,000.0
Moist
Cool,Clear
0.00
11/22/19
3
11,800.0
Dry
Cool,Clear
0.00
Total Gallons
53,600.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
12/5/19
3
41,500.0
Dry
Cool,Clear
0.00
12/6/19
3
41,800.0
Dry
Cool,Clear
0.00
Total Gallons
83,300.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Surface
Field: 4
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/19/19
4
30,000.0
Dry
Cool,Clear
0.00
Total Gallons
30,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Surface
Field: 4
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/18/19
4
48,000.0
Dry
Hot,Clear
0.00
10/28/19
4
18,000.0
Dry
Warm,Clear
0.00
Total Gallons
66,000.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Surface
Field: 5
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/31/19
5
65,300.0
Dry
Cool,Clear
0.00
2/1/19
5
48,000.0
Dry
Cool,Clear
0.00
2/4/19
5
24,000.0
Dry
Cool,Cloudy
0.01
3/13/19
5
59,800.0
Dry
Cool,Clear
0.00
3/14/19
5
83,600.0
Dry
Cool,Clear
0.00
Total Gallons
280,700.0

Town of Clayton
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2019
Little Creek WRF
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Surface
Field: 5
Percent Solids: 2.45
Residual Report No.: 19-024-0208
Crop: Small Grain
Date
Field No.
Subrield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/4/19
5
18,000.0
Dry
Cool,Clear
0.00
11/5/19
5
18,000.0
Dry
Cool,Clear
0.00
11/7/19
5
18,000.0
Dry
Warm,Clear
0.00
11/8/19
5
11,800.0
Dry
arm,Cloud
0.47
Total Gallons
65,800.0

Triple S Farms
Kenansville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Kenansville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 0.51
Residual Report No.: K2019 1-19
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/3/19
1
42,000
Dry
Cool,Cloudy
0.06
Total Gallons
42,000

Triple S Farms
Kenansville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Kenansville WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 0.51
Residual Report No.: K2019 1-19
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/9/19
2
36,000
Dry
Warm,Clear
0.00
Total Gallons
36,000

Triple S Farms
Kenansville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Kenansville WWTP
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 0.51
Residual Report No.: K2019 1-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/25/ 19
9
48,000
Dry
Hot,Clear
0.00
Total Gallons
48,000

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Southwest Plantation
Farmer: Eric Smith
Acres: 13.95
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.58
Residual Report No.: SWP 2019 1-19
Crop: Trees
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/21/19
6
12,600
Moist
Cool,Cloudy
0.05
Total Gallons
12,600

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Southwest Plantation
Farmer: Eric Smith
Acres: 13.95
Site/Tract: 1
Application Method: Surface
Field: 6
Percent Solids: 2.58
Residual Report No.: SWP 2019 1-19
Crop: Forest
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/25/19
6
12,600
Dry
Warm, Clear
0.00
Total Gallons
12,604

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Southwest Plantation
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.58
Residual Report No.: SWP 2019
1-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/15/19
2
12,600
Dry
Hot, Clear
0.00
Total Gallons
12,600

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2019
Wallace WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 2.57
Residual Report No.: WL2019 1-19
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/6/19
1
18,000
Dry
Warm,Clear
0.00
2/7/19
1
78,000
Dry
Warm,Clear
0.00
2/8/19
1
48,000
Dry
Warm,Clear
0.00
Total Gallons
144,000

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2019
Wallace WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 2.57
Residual Report No.: WL2019 1-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/25/19
1
24,000
Dry
Warm,Clear
0.00
3/28/19
1
102,000
Dry
Cool,Clear
0.00
3/29/19
1
114,000
Dry
Warm,Clear
0.00
Total Gallons
240,000

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2019
Wallace WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Injected
Field: 2
Percent Solids: 2.57
Residual Report No.: WL2019 1-19
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/7/19
2
18,000
Dry
Warm,Clear
0.00
2/8/19
2
30,000
Dry
Warm,Clear
0.00
Total Gallons
48,000

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2019
Wallace WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Injected
Field: 2
Percent Solids: 2.31
Residual Report No.: WL2019 3-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/22/19
2
24,000
Moist
Hot,Clear
0.00
7/23/19
2
102,000
Dry
Warm,Clear
0.00
7/24/19
2
51,177
Dry
Hot,Cloudy
1.45
Total Gallons
177,177

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Warsaw WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.87
Residual Report No.: WR2019 10-19
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/25/ 19
1
90,000
Dry
Hot,Clear
0.00
4/26/19
1
66,000
Dry
Warm,Clear
0.00
Total Gallons
156,000

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Warsaw WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 2.87
Residual Report No.: WR2019 10-19
Crop: sermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/14/19
1
44,000
Dry
Warm,Clear
0.00
6/17/19
1
100,000
Dry
Hot,Clear
0.00
Total Gallons
144,000

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Warsaw WWTP
Farmer: Eric Smith
Acres: 21
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids: 2.87
Residual Report No.: WR2019 10-19
Crop: Small Grain
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/22/19
3
50,000
Dry
Cold,Clear
0.00
Total Gallons
50,000

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Warsaw WWTP
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.87
Residual Report No.: WR2019 10-19
Crop: Small Gram
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/23/19
9
95,000
Dry
Cool,Clear
0.00
Total Gallons
95,000

Triple S Farms
Warsaw, North Carolina
Triple S Farms
WQ0030998
Annual 2019
Warsaw WWTP
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 2.87
Residual Report No.: WR2019 10-19
Crop: sermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/30/19
9
78,000
Dry
Hot,Clear
0.00
10/1/19
9
64,000
Dry
Hot,Clear
0.00
Total Gallons
142,000