NC0026051_Annual Performance_20200303

RECEIVED
Annual Report
Pretreatment ua epo t MAR 0 3 2020
Submission Requirements NCDEQ1D'"RINPDEs
PAR Year 2019
Name Submitting: Amy Moore Date: 2/28/2020
Cover Letter E'
Certification Statement(s) [a'
Narrative 2'
Pretreatment Program Info Database Sheet lzl"
Pretreatment Performance Summary (PPS) EZ1
Significant Non-compliance Report (SNCR)
Historical SNC Report Q-
Public Notice(s) dw
Q ` c-cckl3cc
Allocation Table (AT) C�
SIU Semi-annual Data Sheets
Waste Reduction Information
Compliance Schedules ❑ r\IP

°URHAM Engineering and
COUNTY
�O
Environmental Services
1881..:1 Utilities Division
February 28, 2020
Return Receipt Requested
Certified Mail#7017 3380 0000 2144 1106
Ms. Vivien Zhong
Division of Water Resources/PERCS Unit REG�,�VE D
1617 Mail Service Center f�
Raleigh, NC 27699-1617 MAR 0 3 2020
Re: 2019 Pretreatment Annual Report(PAR) NCDEQIDWRINPDES
Dear Ms. Zhong:
Please find enclosed two copies of the Durham County Pretreatment Annual Report(PAR)for the
period of January 1, 2019 through December 31, 2019. If you have any questions concerning the
PAR please contact me at(919) 560-9035.
Sincerely,
Amy M re
Laboratory& Compliance Manager
Encl: Pretreatment Annual Report(1) Copy
cc: Stephanie Brixey, Deputy Director of E&ES/POTW Director
5926 NC Highway 55 East,Durham,North Carolina 27713
[phone] I fax[phone] I dconc.gov
Equal Employment/Affirmative Action Employer

Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NC0026051
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1, 2019 to December 31, 2019
Person to contact
Regarding this report: Amy Moore
Phone#: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate and complete.
Amy MAillAtriADOCe
e Date
Laboratory& Compliance Manager

Pretreatment Annual Report
POTW: Durham County Triangle WWTP
NPDES #: NC002605I
WWTP: Triangle Wastewater Treatment Plant
Reporting Period: January 1, 2019 to December 31, 2019
Person to contact
Regarding this report: Amy Moore
Phone#: [phone]
I certify that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based upon my inquiry of the
person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate and complete.
Stephanie 3rixey Date
Deputy Director of E&ES/POTW Di ctor

DURHAM COUNTY
PRETREATMENT ANNUAL REPORT
NARRATIVE
GENERAL PROGRAM INFORMATION:
Durham County submitted revisions to the Enforcement Response Plan (ERP) on
February 11, 2020 in response to the Dental Amalgam Rule, that was approved February
13, 2020. Durham County submitted a revision of the Long Term Monitoring Plan
(LTMP) to the Division on September 5, 2013, that was approved by the Division on
October 8, 2013. Durham County submitted a revision of the Sewer Use Ordinance
(SUO) to the Division on December 18, 2012. A letter was received from the Division
on January 28, 2013, requesting additional information. The additional information was
submitted March 21, 2013 and approved by the Division on April 3, 2013. The Industrial
Waste Survey (IWS) was submitted to the Division on March 9, 2016. The Division
requested additional information that was submitted on May 27, 2016. The IWS was
approved by the Division on May 31, 2016. Durham County submitted a revision of the
Headwork's Analysis (HWA) on March 16, 2018, that was,approved by the Division on
May 2, 2018. A copy of the "Pretreatment Program Info Database" is included.
GENERAL PERMIT INFORMATION:
During the reporting period the following Industrial User Permits were issued, modified,
or renewed:
• Aurobindo USA, IUP DC-089 was renewed with an effective date of October 9,
2019. The permit was received by the Division on September 17, 2019. The
permit was approved by the Division by email on October 2, 2019.
• Cree, IUP DC-076 was renewed with an effective date of August 1, 2019. The
permit was received by the Division on July 18, 2019 and approved by email on
July 26, 2019.
• Cree RTP, IUP DC-040 was renewed with an effective date of August 1, 2019.
The permit was received by the Division on July 18, 2019 and approved by email
on July 26, 2019.
• Micross, IUP DC-085 was renewed with an effective date of October 21, 2019.
The permit was received by the Division on September 17, 2019 and approved by
email on October 2, 2019.
• PowerSecure, IUP DC-095 was renewed with an effective date of November 13,
2019. The permit was received by the Division on November 7, 2019 and
approved by email on December 3, 2019.

SIU INFORMATION:
1. AstraZeneca (formerly Pearl Therapeutics) (IUP DC-078) — No permit
violations occurred at this facility.
2. Aurobindo USA (IUP DC-089)—Aurobindo was issued a Notice of Violation on
February 5, 2019, for late reporting of the December 2018 monthly average flow.
The permit requires the summary of the monthly flow rate be submitted by the
last day of the following month. The report for December 2018 was received on
February 4, 2019. Aurobindo was issued a Notice of Violation on October 14,
2019 for exceeding the daily maximum of acetone on August 8, 2019 and for
exceeding the monthly average of acetone for August 2019. Aurobindo was
issued a Notice of Violation on October 31, 2019 for exceeding the daily
maximum of acetone on September 23, 2019 and for exceeding the monthly
average of acetone for September 2019. Additional samples were collected for
acetone in October, November and December 2019. Aurobindo discovered that
disposing of cleaning liquid waste to the sanitary sewer contributed to the
elevated levels of acetone. In November 2019, Aurobindo began collecting and
removing liquid cleaning waste off-site via hazardous waste disposal. Aurobindo
is currently in Significant Non-Compliance for exceeding the monthly average
Technical Review Criteria for the second semiannual period of 2019. The
Notices of Violation were issued in accordance with the ERP.
3. Bioi en (IUP DC-080) — Biogen was issued a Notice of Violation on January 7,
2020, for late reporting of the November 2019 monthly average flow. The permit
requires the summary of the monthly flow rate be submitted by the last day of the
following month. The report for November 2019 was received on January 2,
2020. The Notice of Violation was issued in accordance with the ERP.
4. Cintas (IUP DC-037)—Cintas was issued a Notice of Violation on June 13, 2019
for exceeding the daily maximum of Oil and Grease(non-polar and polar) on May
14, 2019. Cintas was issued a Notice of Violation on August 29, 2019, for the
daily pH minimum on July 23, 2019 and August 6, 2019. The Notices of
Violation were issued in accordance with the ERP.
S. Cree, Inc. (IUP DC-076) — Cree was issued a Notice of Violation on June 13,
2019, for failure to report the use and discharge of a biocide as a changed
condition. Cree submitted the appropriate biocide worksheet and received
Durham County approval for future use and discharge of the biocide. The Notice
of Violation was issued in accordance with the ERP.
6. Cree RTP (IUP DC-040)—No permit violations occurred at this facility.
7. JMC (IUP DC-023)—No permit violations occurred at this facility.

8. Micross (IUP DC-085)—Micross was issued a Notice of Violation on November
27, 2019, for exceeding the monthly average flow rate for the month of October
2019. The Notice of Violation was issued in accordance with the ERP.
9. Novan (IUP DC-0841—No permit violations occurred at this facility.
10. Phononic (IUP DC-0751—Phononic was issued a Notice of Violation on January
14, 2019, for late reporting of pH, molybdenum, and flow meter calibration
record. Monitoring results are due no later than the last day of the month
following the month in which the samples were collected. Flow meter calibration
reports are due within 15 days of the calibration. The pH and molybdenum
samples were analyzed on September 24, 2018. The flow meter was calibrated on
August 24, 2018. The report for pH, molybdenum and flow meter calibration was
received on December 14, 2018. Phononic was issued a Notice of Violation on
July 17, 2019, for exceeding the daily maximum on May 17, 2019 for nickel and
for late reporting of the TTO certification. Additional samples for nickel were
collected and within permit limits. The TTO certification for the first semiannual
period of 2019 was due on June 7, 2019. Durham County received the
certification on June 11, 2019. The Notices of Violation were issued in
accordance with the ERP.
11. PowerSecure (IUP DC-095) — PowerSecure was issued a Notice of Violation on
January 15, 2019, for the daily maximum of pH on a sample collected on
December 19, 2018. An additional pH sample was collected on January 18, 2019.
PowerSecure was issued a Notice of Violation for late reporting on January 22,
2019. The monthly average flow for November 2018 was received on January 4,
2019. PowerSecure was issued a Notice of Violation on September 19, 2019 for
late reporting of monthly average flow. The permit requires the summary of the
monthly flow rate be submitted by the last day of the following month. The flow
report for July 2019 was received September 3, 2019. The Notices of Violation
were issued in accordance with the ERP.
12. SCM Metal (IUP DC-005)—No permit violations occurred at this facility.
13. United Therapeutics (IUP DC-053) — United Therapeutics exceeded the
permitted flow limit for the months of January, February and March 2019. The
flow exceedance was due to a malfunction of the facility utilities and was not
process related; therefore, a Notice of Violation was not issued. No permit
violations occurred at this facility.
WASTE REDUCTION ACTIVITIES:
The Triangle Wastewater Treatment Plant participates in the following waste reduction
activities:

1. Recycling of plastic, glass, aluminum, newspaper and corrugated cardboard.
2. Recycling of used pens, markers, mechanical pencils, highlighters, scotch tape
dispensers and cores, and ink jet cartridges.
3. Recycling of used batteries.
4. Secondary containment for bulk storage of chemicals.
5. Recycling of used oil.
6. Reduction of paper generation.
7. Reduction of power consumption via automation. Logic controls are present that
operates the rotors used for aeration as well as the intensity of the Ultraviolet
Disinfection System.
Permit applications and inspection reports were reviewed for industrial waste reduction
activities information. The codes used in Part V, Waste Reduction Information of the
Industrial Waste Survey and Permit Application are used here. A copy of the code and
description is attached for reference.
Industry Name Code or description of waste reduction activity
AstraZeneca(formerly Pearl Therapeutics)
Aurobindo W19, W34, W36, W55, W62, W71
Biogen W13, W33, W34, W36, W39, W99
Cintas W13, W52
Cree W24, W32, W33, W34, W36, W39, W51, W54, W55,
W58, W67
Cree RTP W24, W32, W33, W34, W36, W51, W54, W55
JMC W24, W52, W81
Micross W21, W23, W33, W34, W36
Novan W14, W55, W61, W62, W72
Phononic W34
PowerSecure W3, W24, W31, W32, W34, W36
SCM W39
United Therapeutics W25, W52, W54, W55
WASTE REDUCTION CODES:

W 13 Improved maintenance scheduling recordkeeping, or procedures
W14 Changed production schedule to minimize equipment and feedstock
changeovers
W 19 Other changes in operating practices (explain briefly in comments)
W 21 Instituted procedures to ensure that materials do not stay in inventory
beyond shelf-life
W22 Began to test outdated material-continue to use if still effective
W23 Eliminated shelf-life requirements for stable materials
W24 Instituted better labeling procedures
W25 Instituted clearinghouse to exchange materials that would otherwise
be discarded
W29 Other changes in Inventory control (explain briefly in comments)
W31 Improved storage or stacking procedures
W32 Improved procedures for loading,unloading and transfer operations
W33 Installed overflow alarms or automatic shutoff valves
W34 Installed secondary containment
W35 Installed vapor recovery systems
W36 Implemented inspection or monitoring program of potential spill or
leak sources
W39 Other spill and leak prevention(explain briefly in comments)
W41 Increased purity of raw materials
W42 Substituted raw materials
W49 Other raw material modifications (explain briefly in comments)
W51 Instituted recirculation within a process
W52 Modified equipment, layout, or piping
W53 Use of a different process catalyst
W54 Instituted better controls on operating bulk containers to minimize
discarding of empty containers
W 5 5 Changed from small volume containers to bulk containers to
minimize discarding of empty containers
W58 Other process modifications (explain briefly in comments)
W59 Modified stripping/cleaning equipment
W60 Changed to mechanical stripping/cleaning devices (from solvents or
other materials)
W61 Changed to aqueous cleaners(from solvents or other materials)

W62 Reduced the number of solvents used to make waste more amenable
to recycling
W63 Modified containment procedures for cleaning units
W64 Improved draining procedures
W65 Redesigned parts racks to reduce drag out
W66 Modified or installed rinse systems _
W67 Improved rinse equipment design
W68 Improved rinse equipment operation
W71 Other cleaning and degreasing operation (explain briefly in
comments)
W72 Modified spray systems or equipment
W73 Substituted coating materials used
W74 Improved application techniques
W75 Changed from spray to other system
W78 Other surface preparation and finishing(explain briefly in comments)
W81 Changed product specifications
W82 Modified design or composition of product
W83 Modified packaging
W89 Other product modifications (explain briefly in comments)
W99 Other(specify in comments)
Additional Information:
There were no SIU's in Significant Non-Compliance (SNC) for the first semi-annual
period.
Aurobindo was in SNC for exceeding the monthly average Technical Review Criteria for
acetone during the second semiannual period. Subsequent acetone sampling was
conducted and met permit limits. The Public Notice is included with this submittal and
will be posted in the March 3, 2020 edition of the Durham-Herald Sun. Proof of
publication will be sent to the Division of Water Resources as soon as it is available.
First Flight Venture Center (FFVC), regulated by local permit number DCL-062 was in
SNC during the second semiannual period for mercury. Subsequent mercury sampling
was conducted and met permit limits. The Public Notice is included with this submittal
and will be posted in the March 3, 2020 edition of the Durham-Herald Sun. Proof of
publication will be sent to the Division of Water Resources as soon as it is available.

Pretreatment Program Info Database printed on: 12/20/2019
for Program Name Durham County IWC%at 7Q10 100.00
WWTP Name Triangle Stream Information
Program Approval Date 07/06/1995 70-i6 Flow cfs/mgd 0 / 0.00
Pretreatment Status 1Q10 Flow cfs/mgd 0.00 / 0.00
Full Stream Classification ws-iv
Region RRO Basin Number CPF05
County Durham \ Receiving Stream Name NORTHEAST CREEK
NPDES Number NC0026051
NPDES Effective Date Last PAR Rec 02/28/2019 PAR Due Date 03/01/2020 mercury
12/01/2011 1631
NPDES Expire Date Current Fiscal 08/16/2018 required
p 04/30/2016 Year PCI Done
POTW is Primary WWTP
TRUE Last Audit on 07/27/2016 Audit Year Next20/21 'yes
Design Flow mgd 12.0000 %Design mgd is SIU permitted 11.85 Permitted SIU flow(mgd)[Pt_SIU) 1.422
WWTP SIU's 13 Program Sills 13
VWVTP CIU's 12 Program CIUs 12 LTM YVSP I 1 SUO
date Inactive Date Next Due 04/01/2023 04/01/2021
Date Received by DWR 03/16/2018 09/05/2013 03/14/2016 12/20/2012 et/17/2013 21(((zoZO
Date Approved 05/02/2018 10/08/2013 05/31/2016 04/03/2013 04193/201.3 ZI ri31ZIJZ0
Adopt Date Required
Date Adopted 03/11/2013
Info in this Box from Pt _Contacts Date Date Date
PT_Pro Attended Attended Attended
Formal Name g.Prime Phonel ext Fax HWA Wksp IUP Wksp PAR Wksp
Ms.Stephanie BrixeyPrim1919-560 9034 1919-544-8590 II 16/22/2011 I 1/23/2007
[e-mail] Deputy Director of E&ESr'POTW 5926 NC Hwy 55 E 27713
Ms.Amy Moore 0iIN`II919-560-9035 I 19t t-511-- 011 2/9/2012 14/18/2012 11/19/2012
[e-mail] LABORATORY&COMPLIANCE
Ms.Laura Melton I 11919-560-9042 1 1919-544-8590 II I I I
[e-mail] Pretreatment Project Coordinator 5926 Highway 55 East 27713
Pretreatment Related NOVs from DWQ L DWR Central Office Contact'Vivien Zhong
3/24/2004 PAR-failure to enforce-nov/orders for SNC DWR Regional Contact ICheng Zhang

Chapter 9, PAR Guidance
Pretreatment Performance Summary (PPS)
1. Pretreatment Town Name: Durham County
2. "Primary" NPDES Number NCO() 26051 This Column
for office
or Non Discharge Permit#if applicable=> use only
EPA
WENDB
3. PAR begin Date,please enter 01/01/yy or 07/01/yy 3.=> 1/1/2019 PSSD
4. PAR end Date, please enter 06/30/yy or 12/31/yy 4.=> 12/31/2019 PSED
5. Total number of SIUs, includes CIUs 5.=> 13 sius
6. Number of CIUs 6.=> 12 clus
7. Enter the Higher Number, either (7a) or(7b)here=> 0 NOIN
7a. Number of SIUs not sampled by POTW 7a.=> 0
7b. Number of SIUs not inspected by POTW 7b.=> 0
8. Number of SIUs with no IUP, or with an expired IUP 8.=> 0 NOCM
9. Total Number of SIUs in SNC due to either IU Reporting violations or
IUP Limit violations. To avoid double counting some SIUs
Enter (9a+9b)- 9c here=> 1 PSNC
Enter the Number of SIUs in SNC for :
9a. IU Reporting violations 9a.=> 0 MSNC
9b. IUP Limit violations 9b._> 1 SNPS
9c. Both IU Reporting& Limit violations 9c.=> 0
10. Number of SIUs in SNC due to IU Reporting violations
that were not sampled or inspected by POTW 10.=> 0 SNIN
11. Number of SIUs in SNC due to violation of 11._> 0 SSNC
Compliance Schedule due dates
12. Number NOVs,NNCs, AOs, or similar assesed to SIUs 12.=> 13 FENF
13. Number Civil or Criminal Penalties assessed to SIUs 13.=> 0 JUDI
14. Number of SIUs included in public notice 14.=> 0 svPu
15. Number of SIUs from which penalties collected 15.=> 0 IUPN
16. Total Amount of Civil Penalties Collected 16.=> $ 0
17. Total Number of SIUs on a compliance schedule 17.=> 0 socs
Foot Notes: AO Administrative Order NOV Notice of Violation
CIU Categorical Industrial User PAR Pretreatment Annual Report
CO Consent Order POTW Public Operated Treatment Works
IUP Industrial User Pretreatment Permit SIU Significant Industrial User
NNC Notice of Non-Compliance SNC Significant Non-Compliance,formerly ANC

Pretreatment Annual Report (PAR) PAR covers this calendar year=> 2019
Significant Non-Compliance Report (SNCR) Control Authority=Program=Town Name => Durham County
WWTP =Wastewater Treatment Plant, use separate form for each WWTP. WWTP Name => Triangle WWTP
SIU= Significant Industrial User NPDES # => NC002605 1
SNC = Significant Non-Compliance
A SNCR Form must be submitted with every PAR,please write "None" if you had No SIUs in SNC during calendar year
SNC ? (Yes/No)
HIP Pipe Industry Name Parameter for each 6-month period.
# # or"Reporting" Jan. -June July- Dec.
DC-089 001 Aurobindo Acetone No Yes
Attach a copy of the Division's "SIUs in SNC Historical Report" for your POTW's SIUs behind this page .
Is the database correct? Notify the Division of any errors ! Database indicates SNC history for previous years.
EVERY SNC MUST be explained in the Narrative, How was, is, or will it be resolved?
REPEAT SNCs are serious matters that MUST be explained in the Narrative.
Fonn name: PAR,SNCR,2001
Date Revised: 1/4/2001

'l-1 S trisi
REPORT
Durham County
2012 2013 2014 2015 2016 2017 2018
1st half I 2nd half 1st half I 2nd half 1st half I 2nd half 1st half I 2nd half 1st half I 2nd half 1st half 12nd half 1st half I 2nd half
JMC (USA), Inc. PreviousNames:
IUP# DC-023 Pipe# 001 SIU Word Description'.
metals-433-Cr metal production
IUP Status:Active
Chromium I X I I I I XI I
failure to sample I I I I I XI I
pH IX I
Phononic PreviousNames:
IUP# DC-075 Pipe# 001 SIU Word Description:
Subpart A
IUP Status:Active
Reporting I I I XI I I I
An'X'in a semi-annual period indicates snc for the period for the respective parameter.
PRINTED ON: 12/20/2019 This information is compiled from many sources,and has not been verified. PAGE 26
Contact the local pretreatment coordinator or state pretreatment staff if errors are noted.

Public Notice
Durham County in accordance with Federal and State Regulations, is hereby giving public notice. Listed
below are users in significant noncompliance with national pretreatment regulations (40 CFR Part 403),
state pretreatment regulations (15 NCAC 2H.0900), or local pretreatment regulations during July 2019
through December 2019.
Aurobindo Pharma USA, located at 2929 Weck Drive and regulated by significant industrial user permit
number DC-089 was in status of significant noncompliance for exceeding the monthly average permit
limitation for acetone. A written notification title "Notice of Violation" was sent to the user's authorized
representative requiring them to notify the County of the cause of the violation. Subsequent acetone
sampling in 2019 met the permit limit.
First Flight Venture Center, located at 2 Davis Drive and regulated by local industrial user permit number
DCL-062 was in status of significant noncompliance for exceeding the permit limitation for mercury. A
written notification titled "Notice of Violation"was sent to the user's authorized representative requiring
them to notify the County of the cause of the violation.Subsequent mercury sampling completed in 2020
met the permit limit.

TVVWTP Allocation Table Printed: 2/27/2020, 2:05 PM
Allocation Table Page 1 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 09/17/19
Permits last modified: 11/07/19
Porw=> Triangle WWTP
NPDES#=> NC0026051
FLOW BOD
Industry Type Renewal Modification Date Permit Limits _ Permit Limits
IUP I INDUSTRY NAMES Permit Pipe of Effective Effective Permit Conc. Load
Count (please list alphabeticly) number number Industry Date Date Expires MGD gal/day , mg/1 lbs/daL_
1 AstraZeneca Pharmaceutics DC-078 001 439 D&E Pharmaceutical 01/01/17 01/31/18 12/31/21 0.00200 2,000
2 Aurobindo USA DC-089 001 439 D&E Pharmaceutical 10/09/19 10/08/24 0.0390 39,000 _monitor
3 Biogen DC-080 001 439 D&E Pharmaceutical-no CN 08/24/15 03/24/17 08/23/20 0.2500 I 250,000 monitor
4 Cintas DC-037 001 Full Service Laundry Facility 11/05/17 11/01/22 0.1200# 120,000 monitor
5 Cree(008,009) DC-076 469 Semi Conductor Mfg. 08/01/19 07/31/24 0.4510 451,000 _
Cree 008 008 (Combined Discharge) monitor
Cree 009 009 (Combined Discharge) _ monitor
6 Cree RTP DC-040 012 469 Semi Conductor Mfg. 08/01/19 07/31/24 0.3290 329,000
t� ,
7 JMC(USA)Inc DC-023 001 433 Cr Metal Production 07/02/17 07/01/22 0.0100 10,000
8 Micross Advanced DC-085 001 469 E R&D Semiconductor 10/21/19 10/20/24 0.0750 75,000
ii
9 Novan, Inc DC-084 001 439 E R&D Pharmaceutical 09/14/18 09/13/23 0.0200 I 20,000
10 Phononic DC-075 001 469 A Semi Conductor Mfg. 03/08/18 03/06/23 0.0200 20,000
tip
11 PowerSecure DC-095 001 433 Metal Finisher 11/13/19 _ 11/12/24 0.0060 6,000
12 SCM Metals DC-005 001 471.104A Powder Former 07/01/16 06/30/21 0.0500 50,000
13 United Therapeutics DC-053 001 (Combined Discharge) 05/25/15 05/08/18 05/24/20 0.0500 50,000 monitor
1111111..
002 Pharmaceutical t
Column Totals=> ( 1.4220 1,422,0001 0
Basis=> NPDES Design
MARL from HWA(lbs/day)=> NPDES Permitted Flow=> 12.0000 20016
Uncontrollable Loading(lbs/day)=> 5.3100 8281
otal Allowable for Industry(MAIL)(lbs/day)=> 6.6900 11735
Total Permitted to Industry(lbs/day)=> 1.4220 0
MAIL left(lbs/day)_> 5.2680 11735
'ercent Allow. Ind. (MAIL)still available(%)=> 78.7% 100.0%
Percent MARL still available(%)=> 43.9% 58.6%
5 Percent MARL(lbs/day)=> 0.6000 1001,

TVVVVTP Allocation Table Printed: 2/27/2020, 2:05 PM
Allocation Table Page 2 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 09/17/19
Permits last modified: 11/07/19
POTw=> Triangle WWTP
NPDES#=> NC0026051
TSS Ammonia Arsenic Cadmium Chromium Copper I
Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (please alphabeticN) number number mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/da
1 AstraZeneca Pharmaceutic DC-078 001
2 Aurobindo USA DC-089 001 monitor �.(monitor monitor monitor
3 Biogen DC-080 001 monitor monitor _ monitor_ _
4 Cintas DC-037 001 monitor monitor monitor monitory monitor
5 Cree(008,009) DC-076 _
Cree 008 008 monitor monitor monitor monitor
i
Cree 009 009 monitor
6 Cree RTP DC-040 012 monitor monitor monitor monitor monitor
7 JMC(USA)Inc DC-023 001 ��monitor r-------
0.0250 0.0021 0.6500 0.0542_ 0.0584
8 Micross Advanced DC-085 001 monitor monitor monitor
9 Novan,Inc DC-084 001 ' monitor' monitor
10 Phononic DC-075 001
11 PowerSecure DC-095 001 0.0700 0.0035 1.7100 0.0856 2.0700 0.1036
12 SCM Metals DC-005 001 ' monitor 4 0.5000 0.2085
13 United Therapeutics DC-053 001 monitor 'monitor monitor
_ 002
Column Totals=> 0 0, ( 0.0000 1 0.00561 1 0.13981 0.3705
Stream Stream Stream AS/Nit/TF
Basis=> Design Design Std Std Std inhibition
MAHL from HWA(lbs/day)=> 25020, 2502.00 0.8962 0.2987 4.8465 ' 23.6589
Uncontrollable Loading(lbs/day)=> 9964 1306.42 0.1329 0.0133 0.1771 1.9308
'otal Allowable for Industry(MAIL)(lbs/day)=> 15056 - 1195.58 0.7633 0.2854 4.6694 21.7281
Total Permitted to Industry(lbs/day)=> 0 0.00 0.0000 0.0056 0.1398 0.3705
MAIL left(lbs/day)_> 15056 1195.58 0.7633 0.2799 4.5296 21.3576
'ercent Allow.Ind.(MAIL)still available(%)=> 100.0% 100.0% 100.0% 98.0% 97.0% 98.3%
Percent MAHL still available(%)=> 60.2% 47.8% 85.2% 93.7% 93.5% 90.3%
5 Percent MAHL(lbs/day)=> 1251 125.10 0.0448 0.0149 0.2423 1.1829

TWVVTP Allocation Table Printed: 2/27/2020, 2:05 PM
Allocation Table 10/10/2018 REVISED Page 3 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 09/17/19
Permits last modified: 11/07/19
POTw- Triangle WWTP
NPDES#=> NC0026051
Cyanide Lead Mercury Molybdenum Nickel
Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (please list alphabeticly) number number mg/I lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day
1 AstraZeneca Pharmaceutics DC-078 001 0.000142 0.000002
2 Aurobindo USA DC-089 001 monitor 0.000142 0.000046 monitor
3 Biogen DC-080 001 0.000142 0.000296 1.. 1 monitor
4 Cintas DC-037 001 monitor 0.000142 0.000142 monitor monitor
iiii
5 Cree(008,009) DC-076 0.000142 0.000534
I
Cree 008 008 monitor monitor monitor 0.4570 monitor
Cree 009 009 monitor monitor
6 Cree RTP DC-040 012 monitor 0.000142 0.000390 monitor monitor
7 JMC(USA)Inc DC-023 001 0.0300 0.00250.1� 0.0133 0.0001420.000012 monitor_ 0.0167
8 Micross Advanced DC-085 001 monitor monitor 0.000142I 0.000089 monitor monitor
9 Novan, Inc DC-084 001 0.000142 0.000024 monitor_
10 Phononic DC-075 001 ~� 0.000142 0.000024 monitor 0.0200
iir
11 PowerSecure DC-095 r 001 0.50001 0.0250 0.4300 0.0215 0.000142 0.000007 monitor 1.0000 0.0500
12 SCM Metals DC-005 001 0.0300 0.0125 0.1000 0.0417 0.000142 0.000059 _ monitor monitor
13 United Therapeutics • DC-053 • 001 monitor 0.000142 0.000059 monitor��
002
Column Totals=> 0.0400 0.07661 0.0016841 0.4570 0.0867
Stream Stream Sludge Stream
Basis=> Std Std NPDES Ceiling HASL Std
MARL from HWA(lbs/day)=> 0.7950 3.1596 0.025829 22.9553 2.4843
Uncontrollable Loading(lbs/day)=> 0.0221 0.1949 0.003543 0.3366 0.3321
'otal Allowable for Industry(MAIL) (lbs/day)=> 0.7728 2.9647 0.022286 22.6188 2.1522
Total Permitted to Industry(lbs/day)=> 0.0400 0.0766 0.001684 0.4570 0.0867
MAIL left(lbs/day)=> 0.7328 2.8882 0.020602 22.1618 2.0655
'ercent Allow. Ind. (MAIL)still available(%)=> 94.8 % 97.4% 92.4% 98.0% 96.0%
Percent MAHL still available(%)=> 92.2 % 91.4% 79.8% 96.5 % 83.1 %
5 Percent MAHL(lbs/day)=> 0.0397 0.1580 0.001291 1.1478 0.1242

TVVVVTP Allocation Table Printed: 2/27/2020, 2:05 PM
Allocation Table Page 4 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 09/17/19
Permits last modified: 11/07/19
POTw=> Triangle WWTP
NPDES#=> NC0026051
Selenium Silver Zinc Total Nitrogen Total Phos.
Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load
Count (Please list h icy) number number mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/I lbs/day 1 mg/1 lbs/day _
1 AstraZeneca Pharmaceutics DC-078 001
2 Aurobindo USA DC-089 001 monitor monitor monitor
3 Ben DC-080 001 ' monitor monitor monitor
4 Cintas DC-037 001 monitor monitor monitor monitor
5 Cree(008,009) DC-076 _
Cree 008 008 monitor monitor monitor monitor monitor
Cree 009 009
6 Cree RTP DC-040 012 monitor monitor' monitor monitor' monitor
7 JMC(USA?Inc DC-023 001 0.0900` 0.0075� 0.5600 0.0467 monitor monitor
8 Micross Advanced DC-085 001 monitor monitor monitor monitor
9 Novan,Inc DC-084 001 monitor`� monitor��� monitor
10 Phononic DC-075 001
11 PowerSecure DC-095 001 0.2400 0.0120 1.4800 0.0741 I
I
12 SCM Metals DC-005 001 monitor monitor monitor monitor
13 United Therapeutics DC-053 001 monitor monito monitor
_ 002
Column Totals=> 0.0195 0.12081 0.00 0.00
1 0.00001 ( J I I ( 1 I
Sludge
Ceiling AS/Nit/TF AS/Nit/IF
Basis=> HASL inhibition inhibition Design Design
MAHL from HWA(lbs/day)=> 0.4219 12.3224 49.2894 4003.2000 650.00
Uncontrollable Loading(lbs/day)=> 0.0930 0.0443 18.1304 1988.6492 238.92
'otal Allowable for Industry(MAIL)(lbs/day)=> 0.3289 12.2781 31.1590 2014.55 411.08
Total Permitted to Industry(lbs/day)=> 0.0000 0.0195 0.1208 0.00 0.00
MAIL left(lbs/day)_> 0.3289 12.2585 31.0382 2014.55 411.08
'ercent Allow. Ind. (MAIL)still available(%)=> 100.0% 99.8% 99.6% 100.0% 100.0%
Percent MAHL still available(%)=> 78.0% 99.5% 63.0% 50.3% 63.2%
5 Percent MAHL(lbs/day)=> 0.0211 0.6161 2.4645 200.16 32.5000

TWVVTP Allocation Table Printed: 2/27/2020, 2:05 PM
Allocation Table Page 5 of 5
Headworks last approved: 05/02/18
Allocation Table updated: 09/17/19
Permits last modified: 11/07/19
POTw=> Triangle WWTP
NPDES#=> NC0026051
Chloride Fluoride
Industry Permit Limits Permit Limits
IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load
Count (please list alphabeticly) number number mg/I lbs/day mg/1 lbs/day
1 AstraZeneca Pharmaceutic DC-078 001
2 Aurobindo USA DC-089 001 monitor monitor
3 Biogen DC-080 001 monitor monitor
4 Cintas DC-037 001 monitor monitor
5 Cree(008,009) DC-076 7.0000 26.3294
Cree 008 008 monitor monitor
Cree 009 009 monitor monitor
6 Cree RTP DC-040 012 monitor 7.0000 19.2070
7 JMC(USA)Inc DC-023 001 monito monitor
8 Micross Advanced DC-085 001 monitor 6.0000 3.7530
9 Novan,Inc DC-084 001
10 Phononic DC-075 001 _
11 PowerSecure DC-095 001
12 SCM Metals DC-005 001 monitor_ monitor
13 United Therapeutics DC-053 001 monitor monitor
_ 002
Column Totals=> 1 0.0000 49.2894
Basis=> Stream Std NPDES
MARL from HWA(lbs/day)=> 16179.5562 100.3290
Uncontrollable Loading(lbs/day)=> 3844.2251 31.7881
otal Allowable for Industry(MAIL)(lbs/day)=> 12335.3311 68.5409
Total Permitted to Industry(lbs/day)=> 0.0000 49.2894
MAIL left(lbs/day)=> 12335.3311 19.2515
'ercent Allow. Ind. (MAIL)still available(%)=> 100.0% 28.1 %o
Percent MARL still available(%)=> 76.2% 19.2%
5 Percent MAHL(lbs/day)=> 808.9778 5.0164

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/28/2019 S AstraZeneca022819Se1 < 0.025 /20.7 mg/L < /
f
03/18/2019 P AstraZeneca031819PO < 0.025 /20.7 mg/L < / 1 `�ECENED
TW
Feb 2019 Week 4 < 0.025 / mg/L < / MAR 0 3 2020
Mar 2019 Week 3 < 0.025 / mg/L < / 1
Feb 2019 Average < 0.025 /8.2 mg/L < / NCDEQIDWRINPDES
Mar 2019 Average < 0.025 /8.2 mg/L < /
2019 Quarter 1 < 0.025 / mg/L < /
2019 1st 6 Months(Avg) < 0.025 / mg/L < /
2019 1st 6...(Max) < 0.025 / mg/L < /
2019 1st 6...(Min) < 0.025 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S AstraZeneca0119Flow 0.000001 / MGD /
02/28/2019 S AstraZeneca0219F1ow 0.000737 / MGD /
03/31/2019 S AstraZeneca0319F1ow 0.000218 / MGD /
04/30/2019 S AstraZeneca0419F1ow 0.000253 / MGD /
05/31/2019 S AstraZeneca0519F1ow 0.00234 / MGD /
06/30/2019 S AstraZeneca0619F1ow 0.001337 / MGD /
Jan 2019 Week 4 0.000001 / MGD /
Feb 2019 Week 4 0.000737 / MGD /
Mar 2019 Week 4 0.000218 / MGD /
Apr 2019 Week 4 0.000253 / MGD /
May 2019 Week 4 0.00234 / MGD /
Jun 2019 Week 4 0.001337 / MGD /
Jan 2019 Average 0.000001 /0.002000 MGD /
Feb 2019 Average 0.000737 /0.002000 MGD /
Mar 2019 Average 0.000218 /0.002000 MGD /
Apr 2019 Average 0.000253 /0.002000 MGD /
May 2019 Average 0.00234 /0.002000 MGD * /
Jun 2019 Average 0.001337 /0.002000 MGD /
2019 Quarter 1 0.000318 / MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page I of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: EffluentWastewater Oufall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
2019 Quarter 2 0.00131 / MGD /
2019 1st 6 Months(Avg) 0.000814 / MGD /
2019 1st 6...(Max) 0.002340 / MGD /
2019 1st 6...(Min) 0.000001 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled : 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 1 16.67 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/28/2019 S AstraZeneca022819Se1 < 7.5 / mg/L < /
f
1 03/18/2019 P AstraZeneca031819P0 < 7.5 / mg/L < /
TW
Feb 2019 Week 4 < 7.5 / mg/L < /
Mar 2019 Week 3 < 7.5 / mg/L < /
Feb 2019 Average < 7.5 / mg/L < /
Mar 2019 Average < 7.5 / mg/L < /
2019 Quarter 1 < 7.5 / mg/L < /
2019 1st 6 Months(Avg) < 7.5 / mg/L < /
2019 1st 6...(Max) < 7.5 / mg/L < /
2019 1st 6...(Min) < 7.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/28/2019 S AstraZeneca022819Se1 < 0.0025 /20.7 mg/L < /
f
03/18/2019 P AstraZeneca031819P0 < 0.005 /20.7 mg/L < /
TW
Feb 2019 Week 4 < 0.0025 / mg/L < /
Mar 2019 Week 3 < 0.005 / mg/L < /
Feb 2019 Average < 0.0025 /8.2 mg/L < /
Mar 2019 Average < 0.005 /8.2 mg/L < /
2019 Quarter 1 < 0.0038 / mg/L < /
2019 1st 6 Months(Avg) < 0.0038 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 6

•
AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2019 1st 6...(Min) < 0.0025 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # 14
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/28/2019 S AstraZeneca022819Sel < 0.0025 /20.7 mg/L < /
f
03/18/2019 P AstraZeneca031819PO < 0.005 /20.7 mg/L < /
TW
Feb 2019 Week 4 < 0.0025 / mg/L < /
Mar 2019 Week 3 < 0.005 / mg/L < /
Feb 2019 Average < 0.0025 /8.2 mg/L < /
Mar 2019 Average < 0.005 /8.2 mg/L < /
2019 Quarter 1 < 0.0038 / mg/L < /
2019 1st 6 Months(Avg) < 0.0038 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.0025 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
02/28/2019 S AstraZeneca022819Sel 0.000005 /0.000142 mg/L /
fHg
06/03/2019 P AstraZeneca060319PO 0.000001 /0.000142 mg/L /
TWHg
Feb 2019 Week 4 0.000005 / mg/L /
Jun 2019 Week 1 0.000001 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 6

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Feb 2019 Average 0.000005 / mg/L /
Jun 2019 Average 0.000001 / mg/L /
2019 Quarter 1 0.000005 / mg/L /
2019 Quarter 2 0.000001 / mg/L /
2019 1st 6 Months(Avg) 0.000003 / mg/L /
2019 1st 6...(Max) 0.000005 / mg/L /
2019 1st 6...(Min) 0.000001 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/28/2019 S AstraZeneca022819Se1 < 0.003 /3 mg/L < /
f
03/18/2019 P AstraZeneca031819PO < 0.005 /3 mg/L < /
TW
Feb 2019 Week 4 < 0.003 / mg/L < /
Mar 2019 Week 3 < 0.005 / mg/L < /
Feb 2019 Average < 0.003 /0.7 mg/L < /
Mar 2019 Average < 0.005 /0.7 mg/L < /
2019 Quarter 1 < 0.004 / mg/L < /
2019 1st 6 Months(Avg) < 0.004 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 6

. ' .
AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 T Sample e:: Effluent Wastewater
P Y OuP �all: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/28/2019 S AstraZeneca022819Sel <. 0.003 /20.7 mg/L < /
f
03/18/2019 P AstraZeneca031819PO < 0.005 /20.7 mg/L < /
TW
Feb 2019 Week 4 < 0.003 / mg/L < /
Mar 2019 Week 3 < 0.005 / mg/L < /
Feb 2019 Average < 0.003 /8.2 mg/L < /
Mar 2019 Average < 0.005 /8.2 mg/L < /
2019 Quarter 1 < 0.004 / mg/L g/-
< /
2019 1st 6 Months(Avg) < 0.004 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/28/2019 S AstraZeneca022819Se1 6.7 /6- 10 SU /
f
03/18/2019 P AstraZeneca031819PO 6.2 /6- 10 SU /
TW
Feb 2019 Week 4 6.7 / SU /
Mar 2019 Week 3 6.2 / SU /
Feb 2019 Average 6.7 / SU /
Mar 2019 Average 6.2 / SU /
2019 Quarter 1 6.45 / SU /
2019 1st 6 Months(Avg) 6.45 / SU /
2019 1st 6...(Max) 6.7 / SU /
2019 1st 6...(Min) 6.2 / SU /
2019 1st 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 6

•
AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outtalk 001
Sample Count: 2 Months Sampled : 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday.February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 6

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/26/2019 P Aurobindo022619POT 0.126 / mg/L /
W
03/05/2019 S Aurobindo030519Self < 0.025 / mg/L < /
Feb 2019 Week 4 0.126 / mg/L /
Mar 2019 Week 1 < 0.025 / mg/L < /
Feb 2019 Average 0.126 / mg/L /
Mar 2019 Average < 0.025 / mg/L < /
2019 Quarter 1 < 0.076 / mg/L < /
2019 1st 6 Months(Avg) < 0.076 / mg/L < /
2019 1st 6...(Max) 0.126 / mg/L /
2019 1st 6...(Min) < 0.025 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/26/2019 P Aurobindo022619POT 24.6 / mg/L /
W
03/05/2019 S Aurobindo030519Se1f 31.4 / mg/L /
Feb 2019 Week 4 24.6 / mg/L /
Mar 2019 Week 1 31.4 / mg/L /
Feb 2019 Average 24.6 / mg/L /
Mar 2019 Average 31.4 / mg/L /
2019 Quarter 1 28 / mg/L /
2019 1st 6 Months(Avg) 28 / mg/L /
2019 1st 6...(Max) 31.4 / mg/L /
2019 1st 6...(Min) 24.6 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/17/2019 S Aurobindo0119Flow 0.002286 / MGD /
02/20/2019 S Aurobindo0219F1ow 0.002486 / MGD /
03/31/2019 S Aurobindo0319F1ow 0.003131 / MGD /
04/17/2019 S Aurobindo0419F1ow 0.002672 / MGD /
05/15/2019 S Aurobindo0519F1ow 0.002117 / MGD /
06/19/2019 S Aurobindo0619F1ow 0.004203 / MGD /
Jan 2019 Week 3 0.002286 / MGD /
Feb 2019 Week 3 0.002486 / MGD /
Mar 2019 Week 4 0.003131 / MGD /
Apr 2019 Week 3 0.002672 / MGD /
May 2019 Week 3 0.002117 / MGD /
Jun 2019 Week 3 0.004203 / MGD /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 11
t

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jan 2019 Average 0.002286 /0.039 MGD /
Feb 2019 Average 0.002486 /0.039 MGD /
Mar 2019 Average 0.003131 /0.039 MGD /
Apr 2019 Average 0.002672 /0.039 MGD /
May 2019 Average 0.002117 /0.039 MGD /
Jun 2019 Average 0.004203 /0.039 MGD /
2019 Quarter 1 0.002634 / MGD /
2019 Quarter 2 0.002997 / MGD /
2019 1st 6 Months(Avg) 0.002816 / MGD /
2019 1st 6...(Max) 0.004203 / MGD /
2019 1st 6...(Min) 0.002117 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0' 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/26/2019 P Aurobindo022619POT 773 / mg/L /
W
03/05/2019 S Aurobindo030519Se1f 201 / mg/L /
Feb 2019 Week 4 773 / mg/L /
Mar 2019 Week 1 201 / mg/L /
Feb 2019 Average 773 / mg/L /
Mar 2019 Average 201 / mg/L /
2019 Quarter 1 487 / mg/L /
2019 1st 6 Months(Avg) 487 / mg/L /
2019 1st 6...(Max) 773 / mg/L /
2019 1st 6...(Min) 201 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/26/2019 P Aurobindo022619POT < 0.00008 / mg/L < /
W
03/05/2019 S Aurobindo030519Self < 0.001 / mg/L < /
Feb 2019 Week 4 < 0.00008 / mg/L < /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 11

•
Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
Mar 2019 Week 1 < 0.001 / mg/L < /
Feb 2019 Average < 0.00008 / mg/L < /
Mar 2019 Average < 0.001 / mg/L < /
2019 Quarter 1 < 0.00054 / mg/L < /
2019 1st 6 Months(Avg) < 0.00054 / mg/L < /
2019 1st 6...(Max) < 0.001 / mg/L < /
2019 1st 6...(Min) < 0.00008 / mg/L < /
2019 1st 6...(Count) 2 / / 1
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/26/2019 P Aurobindo022619POT 40 / mg/L /
W
03/05/2019 S Aurobindo030519Self 49 / mg/L /
Feb 2019 Week 4 40 / mg/L /
Mar 2019 Week 1 49 / mg/L /
Feb 2019 Average 40 / mg/L /
Mar 2019 Average 49 / mg/L /
2019 Quarter 1 44.5 / mg/L /
2019 1st 6 Months(Avg) 44.5 / mg/L /
2019 1st 6...(Max) 49 / mg/L /
2019 1st 6...(Min) 40 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/26/2019 P Aurobindo022619POT 1640 / mg/L /
W
03/05/2019 S Aurobindo030519Self 545 / mg/L /
Feb 2019 Week 4 1640 / mg/L /
Mar 2019 Week 1 545 / mg/L /
Feb 2019 Average 1640 / mg/L /
Mar 2019 Average 545 / mg/L /
2019 Quarter 1 1092.5 / mg/L /
2019 1st 6 Months(Avg) 1092.5 / mg/L /
2019 1st 6...(Max) 1640 / mg/L /
2019 1st 6...(Min) 545 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 11

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/26/2019 P Aurobindo022619POT 0.037 / mg/L /
W
03/05/2019 S Aurobindo030519Se1f 0.072 / mg/L /
Feb 2019 Week 4 0.037 / mg/L /
Mar 2019 Week 1 0.072 / mg/L /
Feb 2019 Average 0.037 / mg/L /
Mar 2019 Average 0.072 / mg/L /
2019 Quarter 1 0.054 / mg/L /
2019 1st 6 Months(Avg) 0.054 / mg/L /
2019 1st 6...(Max) 0.072 / mg/L /
2019 1st 6...(Min) 0.037 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/26/2019 P Aurobindo022619POT < 0.003 / mg/L < /
W
03/05/2019 S Aurobindo030519Self < 0.003 / mg/L < /
Feb 2019 Week 4 < 0.003 / mg/L < /
Mar 2019 Week 1 < 0.003 / mg/L < /
Feb 2019 Average < 0.003 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < /
2019 Quarter 1 < 0.003 / mg/L < /
2019 1st 6 Months(Avg) < 0.003 / mg/L < /
2019 1st 6...(Max) < 0.003 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/26/2019 P Aurobindo022619POT < 0.005 / mg/L < /
W
03/05/2019 S Aurobindo030519Se1f < 0.005 / mg/L < /
Feb 2019 Week 4 < 0.005 / mg/L < /
Mar 2019 Week 1 < 0.005 / mg/L < /
Feb 2019 Average < 0.005 / mg/L < /
Mar 2019 Average < 0.005 / mg/L < /
2019 Quarter 1 < 0.005 / mg/L < /
2019 1st 6 Months(Avg) < 0.005 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 11
I

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/26/2019 P Aurobindo022619POT < 0.05 / mg/L < /
W
03/05/2019 S Aurobindo030519Se1f 0.6 / mg/L /
Feb 2019 Week 4 < 0.05 / mg/L < /
Mar 2019 Week 1 0.6 / mg/L /
Feb 2019 Average < 0.05 / mg/L < /
Mar 2019 Average 0.6 / mg/L /
2019 Quarter 1 < 0.33 / mg/L < /
2019 1st 6 Months(Avg) < 0.33 / mg/L < /
2019 1st 6...(Max) 0.6 / mg/L /
2019 1st 6...(Min) < 0.05 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
02/26/2019 P Aurobindo022619POT < 0.005 / mg/L < /
W
03/05/2019 S Aurobindo030519Se1f < 0.005 / mg/L < /
Feb 2019 Week 4 < 0.005 / mg/L < /
Mar 2019 Week 1 < 0.005 / mg/L < /
Feb 2019 Average < 0.005 / mg/L < /
Mar 2019 Average < 0.005 / mg/L < /
2019 Quarter 1 < 0.005 / mg/L < /
2019 1st 6 Months(Avg) < 0.005 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Dale SamplelD Result/Limit Mass/Limit
Mercury-LL
03/05/2019 S Aurobindo030519Se1f 0.000014 /0.00142 mg/L /
06/10/2019 P Aurobindo061019POT 0.000093 /0.00142 mg/L /
WHg
Mar 2019 Week 1 0.000014 / mg/L /
Jun 2019 Week 2 0.000093 / mg/L /
Mar 2019 Average 0.000014 / mg/L /
Jun 2019 Average 0.000093 / mg/L /
2019 Quarter 1 0.000014 / mg/L /
2019 Quarter 2 0.000093 / mg/L /
2019 1st 6 Months(Avg) 0.000053 / mg/L /
2019 1st 6...(Max) 0.000093 / mg/L /
2019 1st 6...(Min) 0.000014 / mg/L /
2019 1st 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 11

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 T Sample e: E uent Wastewater Ou
P Type: .� all: 001�
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/26/2019 P Aurobindo022619POT < 0.005 / mg/L < /
W
03/05/2019 S Aurobindo030519Se1f < 0.003 / mg/L < /
Feb 2019 Week 4 < 0.005 / mg/L < /
Mar 2019 Week 1 < 0.003 / mg/L < /
Feb 2019 Average < 0.005 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < /
2019 Quarter 1 < 0.004 / mg/L < /
2019 1st 6 Months(Avg) < 0.004 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/26/2019 P Aurobindo022619POT < 0.001 / mg/L < /
W
03/05/2019 S Aurobindo030519SeIf < 0.003 / mg/L < /
Feb 2019 Week 4 < 0.001 / mg/L < /
Mar 2019 Week 1 < 0.003 / mg/L < /
Feb 2019 Average < 0.001 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < /
2019 Quarter 1 < 0.002 / mg/L < /
2019 1st 6 Months(Avg) < 0.002 / mg/L < /
2019 1st 6...(Max) < 0.003 / mg/L < /
2019 1st 6...(Min) < 0.001 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/26/2019 P Aurobindo022619POT < 0.005 / mg/L < /
W
03/05/2019 S Aurobindo030519Se1f < 0.005 / mg/L < /
Feb 2019 Week 4 < 0.005 / mg/L < /
Mar 2019 Week 1 < 0.005 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 11

•
Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
Feb 2019 Average < 0.005 / mg/L < /
Mar 2019 Average < 0.005 / mg/L < /
2019 Quarter 1 < 0.005 / mg/L < /
2019 1st 6 Months(Avg) < 0.005 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/26/2019 P Aurobindo022619POT 0.5 / mg/L /
W
03/05/2019 S Aurobindo030519Se1f 0.4 / mg/L /
Mar 2019 Week 1 0.4 / mg/L /
Feb 2019 Week 4 0.5 / mg/L /
Feb 2019 Average 0.5 / mg/L /
Mar 2019 Average 0.4 / mg/L /
2019 Quarter 1 0.5 / mg/L /
2019 1st 6 Months(Avg) 0.5 / mg/L /
2019 1st 6...(Max) 0.5 / mg/L /
2019 1st 6...(Min) 0.4 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/26/2019 P Aurobindo022619POT 56.23 / mg/L /
W
03/05/2019 S Aurobindo030519Self 66.4 / mg/L /
Feb 2019 Week 4 56.23 / mg/L /
Mar 2019 Week 1 66.4 / mg/L /
Feb 2019 Average 56.23 / mg/L /
Mar 2019 Average 66.4 / mg/L /
2019 Quarter 1 61.32 / mg/L /
2019 1st 6 Months(Avg) 61.32 / mg/L /
2019 1st 6...(Max) 66.4 / mg/L /
2019 1st 6...(Min) 56.23 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/26/2019 P Aurobindo022619POT < 2.5 /200 mg/L < /
W
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 11

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
03/05/2019 S Aurobindo030519Self < 2.5 /200 mg/L < /
Feb 2019 Week 4 < 2.5 / mg/L < /
Mar 2019 Week 1 < 2.5 / mg/L < /
Feb 2019 Average < 2.5 / mg/L < /
Mar 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 < 2.5 / mg/L < /
2019 1st 6 Months(Avg) < 2.5 / mg/L < /
2019 1st 6...(Max) < 2.5 / mg/L < /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/26/2019 P Aurobindo022619POT 7.3 /6.0- 10.0 SU /
W
03/05/2019 S Aurobindo030519Self 8.6 /6.0- 10.0 SU /
04/09/2019 P Aurobindo040919POT 6.91 /6.0- 10.0 SU /
W
04/16/2019 P Aurobindo041619POT 8.69 /6.0- 10.0 SU /
W
Feb 2019 Week 4 7.3 / SU /
Mar 2019 Week 1 8.6 / SU /
Apr 2019 Week 2 6.91 / SU /
Apr 2019 Week 3 8.69 / SU /
Feb 2019 Average 7.3 / SU /
Mar 2019 Average 8.6 / SU /
Apr 2019 Average 7.8 / SU /
2019 Quarter 1 7.95 / SU /
2019 Quarter 2 7.8 / SU /
2019 1st 6 Months(Avg) 7.88 / SU /
2019 1st 6...(Max) 8.69 / SU /
2019 1st 6...(Min) 6.91 / SU /
2019 1st 6...(Count) 4 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 11
I

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall:• 001
Sample Count: 4 Months Sampled: 3 Weeks Sampled: 4 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/26/2019 P Aurobindo022619POT 13 /66 °C /
W
03/05/2019 S Aurobindo030519Se1f 11.1 /66 °C /
Feb 2019 Week 4 13 / °C /
Mar 2019 Week 1 11.1 / °C /
Feb 2019 Average 13 / °C /
Mar 2019 Average 11.1 / °C /
2019 Quarter 1 12.1 / °C /
2019 1st 6 Months(Avg) 12.1 / °C /
2019 1st 6...(Max) 13 / °C /
2019 1st 6...(Min) 11.1 / °C /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/26/2019 P Aurobindo022619POT 55.7 / mg/L /
W
03/05/2019 S Aurobindo030519Se1f 66 / mg/L /
Feb 2019 Week 4 55.7 / mg/L /
Mar 2019 Week 1 66 / mg/L /
Feb 2019 Average 55.7 / mg/L /
Mar 2019 Average 66 / mg/L /
2019 Quarter 1 60.85 / mg/L /
2019 1st 6 Months(Avg) 60.85 / mg/L /
2019 1st 6...(Max) 66 / mg/L /
2019 1st 6...(Min) 55.7 / mg/L /
2019 1st 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 11

,
Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/26/2019 P Aurobindo022619POT 7.86 / mg/L /
W
03/05/2019 S Aurobindo030519Se1f 9.81 / mg/L /
Feb 2019 Week 4 7.86 / mg/L /
Mar 2019 Week 1 9.81 / mg/L /
Feb 2019 Average 7.86 / mg/L /
Mar 2019 Average 9.81 / mg/L /
2019 Quarter 1 8.835 / mg/L /
2019 1st 6 Months(Avg) 8.835 / mg/L /
2019 1st 6...(Max) 9.81 / mg/L /
2019 1st 6...(Min) 7.86 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
02/26/2019 P Aurobindo022619POT 115 / mg/L /
W
03/05/2019 S Aurobindo030519Self 45 / mg/L /
Feb 2019 Week 4 115 / mg/L /
Mar 2019 Week 1 45 / mg/L /
Feb 2019 Average 115 / mg/L /
Mar 2019 Average 45 / mg/L /
2019 Quarter 1 80 / mg/L /
2019 1st 6 Months(Avg) 80 / mg/L /
2019 1st 6...(Max) 115 / mg/L /
2019 1st 6...(Min) 45 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
03/05/2019 S Aurobindo030519Se1f < 0.0025 / mg/L < /
Mar 2019 Week 1 < 0.0025 / mg/L < /
Mar 2019 Average < 0.0025 / mg/L < /
2019 Quarter 1 < 0.0025 / mg/L < /
2019 1st 6 Months(Avg) < 0.0025 / mg/L < /
2019 1st 6...(Max) < 0.0025 / mg/L < /
2019 1st 6...(Min) < 0.0025 / mg/L < /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 11

Aurobindo USA
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfa11: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/26/2019 P Aurobindo022619POT 0.157 / mg/L /
W
03/05/2019 S Aurobindo030519Se1f 0.322 / mg/L /
Feb 2019 Week 4 0.157 / mg/L /
Mar 2019 Week 1 0.322 / mg/L /
Feb 2019 Average 0.157 / mg/L /
Mar 2019 Average 0.322 / mg/L /
2019 Quarter 1 0.24 / mg/L /
2019 1st 6 Months(Avg) 0.240 / mg/L /
2019 1st 6...(Max) 0.322 / mg/L /
2019 1st 6...(Min) 0.157 / mg/L /
2019 1st 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 11 of 11

Biogen
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
02/12/2019 S Biogen021219Se1f 0.01 / 12.19 mg/L 0.007 / lbs/day
04/30/2019 P Biogen043019POTW < 0.025 / 12.19 mg/L < 0.0204 / lbs/day
Feb 2019 Week 2 0.01 / mg/L 0.007 / lbs/day
Apr 2019 Week 4 < 0.025 / mg/L < 0.0204 / lbs/day
Feb 2019 Average 0.01 /4.83 mg/L 0.007 / lbs/day
Apr 2019 Average < 0.025 /4.83 mg/L < 0.0204 / lbs/day
2019 Quarter 1 0.01 / mg/L 0.007 / lbs/day
2019 Quarter 2 < 0.025 / mg/L < 0.0204 / lbs/day
2019 1st 6 Months(Avg) < 0.018 / mg/L < 0.0137 / lbs/day
2019 1st 6...(Max) < 0.025 / mg/L < 0.0204 / lbs/day
2019 1st 6...(Min) 0.010 / mg/L 0.0070 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Vass/Limit
Ammonia
02/12/2019 S Biogen021219Self 2.2 / mg/L 1.4788 / lbs/day
04/30/2019 P Biogen043019POTW 1.9 / mg/L 1.5497 / lbs/day
Feb 2019 Week 2 2.2 / mg/L 1.4788 / lbs/day
Apr 2019 Week 4 1.9 / mg/L 1.5497 / lbs/day
Feb 2019 Average 2.2 / mg/L 1.4788 / lbs/day
Apr 2019 Average 1.9 / mg/L 1.5497 / lbs/day
2019 Quarter 1 2.2 / mg/L 1.4788 / lbs/day 1
2019 Quarter 2 1.9 / mg/L 1.5497 / lbs/day
2019 1st 6 Months(Avg) 2.05 / mg/L 1.5143 / lbs/day
2019 1st 6...(Max) 2.2 / mg/L 1.5497 / lbs/day
2019 1st 6...(Min) 1.9 / mg/L 1.4788 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S Biogen0119Flow 0.066049 /0.375 MGD /
02/28/2019 S Biogen0219Flow 0.075941 /0.375 MGD /
03/31/2019 S Biogen0319Flow 0.079375 /0.375 MGD /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 11

Biogen
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
04/30/2019 S Biogen0419F1ow 0.105689 /0.375 MGD /
05/31/2019 S Biogen0519F1ow 0.102279 /0.375 MGD /
06/30/2019 S Biogen0619F1ow 0.105689 /0.375 MGD /
Jan 2019 Week 4 0.066049 / MGD /
Feb 2019 Week 4 0.075941 / MGD /
Mar 2019 Week 4 0.079375 / MGD /
Apr 2019 Week 4 0.105689 / MGD /
May 2019 Week 4 0.102279 / MGD /
Jun 2019 Week 4 0.105689 / MGD /
Jan 2019 Average 0.066049 /0.250 MGD /
Feb 2019 Average 0.075941 /0.250 MGD /
Mar 2019 Average 0.079375 /0.250 MGD /
Apr 2019 Average 0.105689 /0.250 MGD /
May 2019 Average 0.102279 /0.250 MOD /
Jun 2019 Average 0.105689 /0.250 MGD /
2019 Quarter 1 0.073788 / MGD /
2019 Quarter 2 0.104552 / MGD /
2019 1st 6 Months(Avg) 0.089170 / MGD /
2019 1st 6...(Max) 0.105689 / MGD /
2019 1st 6...(Min) 0.066049 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 OM(1 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg NI: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/12/2019 S Biogen021219SeIf 22 / mg/L 14.788 / lbs/day
04/30/2019 P Biogen043019POTW 113 / rng/L 92.169 / lbs/day
Feb 2019 Week 2 22 / mg/L 14.788 / lbs/day
Apr 2019 Week 4 113 / mg/L 92.169 / lbs/day
Feb 2019 Average 22 / mg/L 14.788 / lbs/day
Apr 2019 Average 113 / mg/L 92.169 / lbs/day
2019 Quarter 1 22 / mg/L 14.788 / lbs/day
2019 Quarter 2 113 / mg/L 92.169 / lbs/day
2019 1st 6 Months(Avg) 67.5 / mg/L 53.479 / lbs/day
2019 1st 6...(Max) 113 / mg/L 92.169 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 11

Bioffen
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
' BOD
2019 1st 6...(Min) 22 / mg/L 14.788 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/12/2019 S Biogen021219Self < 0.0005 / mg/L < 0.000336 / lbs/day
' 04/30/2019 P Biogen043019POTW < 0.00008 / mg/L < 0.000061 / lbs/day
Feb 2019 Week 2 < 0.0005 / mg/L < 0.000336 / lbs/day
Apr 2019 Week 4 < 0.00008 / mg/L < 0.000061 / lbs/day
Feb 2019 Average < 0.0005 / mg/L < 0.000336 / lbs/day
Apr 2019 Average < 0.00008 / mg/L < 0.000061 / lbs/day
2019 Quarter 1 < 0.0005 / mg/L < 0.000336 / lbs/day
2019 Quarter 2 < 0.00008 / mg/L < 0.000061 / lbs/day
2019 1st 6 Months(Avg) < 0.00029 / mg/L < 0.000199 / lbs/day
2019 1st 6...(Max) < 0.0005 / mg/L < 0.000336 / lbs/day
2019 1st 6...(Min) < 0.00008 / mg/L < 0.000061 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/12/2019 S Biogen021219Se1f 21.1 / mg/L 14.1835 / lbs/day
04/30/2019 P Biogen043019POTW 20 / mg/L 16.313 / lbs/day
Feb 2019 Week 2 21.1 / mg/L 14.1835 / lbs/day
Apr 2019 Week 4 20 / mg/L 16.313 / lbs/day
Feb 2019 Average 21.1 / mg/L 14.1835 / lbs/day
Apr 2019 Average 20 / mg/L 16.313 / lbs/day
2019 Quarter 1 21.1 / mg/L 14.1835 / lbs/day
2019 Quarter 2 20 / mg/L 16.313 / lbs/day
2019 1st 6 Months(Avg) 20.55 / mg/L 15.2483 / lbs/day
2019 1st 6...(Max) 21.1 / mg/L 16.3130 / lbs/day
2019 1st 6...(Min) 20 / mg/L 14.1835 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/12/2019 S Biogen021219Self 87.8 / mg/L 59.02 / lbs/day
04/30/2019 P Biogen043019POTW 122 / mg/L 99.51 / lbs/day
Feb 2019 Week 2 87.8 / mg/L 59.02 / lbs/day
Apr 2019 Week 4 122 / mg/L 99.51 / lbs/day
Feb 2019 Average 87.8 / mg/L 59.02 / lbs/day
Apr 2019 Average 122 / mg/L 99.51 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 11

Biogen
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
COD
2019 Quarter 1 87.8 / mg/L 59.02 / lbs/day
2019 Quarter 2 122 / mg/L 99.51 / lbs/day
2019 1st 6 Months(Avg) 104.9 / mg/L 79.26 / lbs/day
2019 1st 6...(Max) 122 / mg/L 99.51 / lbs/day
2019 1st 6...(Min) 87.8 / mg/L 59.02 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
02/12/2019 S Biogen021219Self < 0.05 / 12.19 mg/L < 0.0336 / lbs/day
04/30/2019 P Biogen043019POTW < 0.003 / 12.19 mg/L < 0.002 / lbs/day
Feb 2019 Week 2 < 0.05 / mg/L < 0.0336 / lbs/day
Apr 2019 Week 4 < 0.003 / mg/L < 0.002 / lbs/day
Feb 2019 Average < 0.05 /4.83 mg/L < 0.0336 / lbs/day
Apr 2019 Average < 0.003 /4.83 mg/L < 0.002 / lbs/day
2019 Quarter 1 < 0.05 / mg/L < 0.0336 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.002 / lbs/day
2019 1st 6 Months(Avg) < 0.0263 / mg/L < 0.0178 / lbs/day
2019 1st 6...(Max) < 0.05 / mg/L < 0.0336 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.0020 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/12/2019 S Biogen021219Self 0.22 / mg/L 0.1479 / lbs/day
04/30/2019 P Biogen043019POTW 0.19 / mg/L 0.155 / lbs/day
Feb 2019 Week 2 0.22 / mg/L 0.1479 / lbs/day
Apr 2019 Week 4 0.19 / mg/L 0.155 / lbs/day
Feb 2019 Average 0.22 / mg/L 0.1479 / lbs/day
Apr 2019 Average 0.19 / mg/L 0.155 / lbs/day
2019 Quarter 1 0.22 / mg/L 0.1479 / lbs/day
2019 Quarter 2 0.19 / mg/L 0.155 / lbs/day
2019 1st 6 Months(Avg) 0.21 / mg/L 0.1514 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 11

f
•
Bioeen
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfa11:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2019 1st 6...(Max) 0.22 / mg/L 0.1550 / lbs/day .
2019 1st 6...(Min) 0.19 / mg/L 0.1479 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate .
02/12/2019 S Biogen021219Self < 0.05 / 12.19 mg/L < 0.0336 / lbs/day
04/30/2019 P Biogen043019POTW < 0.003 / 12.19 mg/L < 0.002 / lbs/day
Feb 2019 Week 2 < 0.05 / mg/L < 0.0336 / lbs/day
Apr 2019 Week 4 < 0.003 / mg/L < 0.002 / lbs/day
Feb 2019 Average < 0.05 /4.83 mg/L < 0.0336 / lbs/day
Apr 2019 Average < 0.003 /4.83 mg/L < 0.002 / lbs/day
2019 Quarter 1 < 0.05 / mg/L < 0.0336 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.002 / lbs/day
2019 1st 6 Months(Avg) < 0.0263 / mg/L < 0.0178 / lbs/day
2019 1st 6...(Max) < 0.05 / mg/L < 0.0336 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.0020 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # 1/0
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/12/2019 S Biogen021219Self 0.000007 /0.000142 mg/L /
04/30/2019 P Biogen043019POTWH 0.000004 /0.000142 mg/L /
g
Feb 2019 Week 2 0.000007 / mg/L /
Apr 2019 Week 4 0.000004 / mg/L /
Feb 2019 Average 0.000007 / mg/L /
Apr 2019 Average 0.000004 / mg/L /
2019 Quarter 1 0.000007 / mg/L /
2019 • Quarter 2 0.000004 / mg/L /
2019 1st 6 Months(Avg) 0.000006 / mg/L /
2019 1st 6...(Max) 0.000007 / mg/L /
2019 1st 6...(Min) 0.000004 / mg/L /
2019 1st 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 11

Bio2en
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
02/12/2019 S Biogen021219Self < 0.003 / 1.77 mg/L < 0.001681 / lbs/day
04/30/2019 P Biogen043019POTW < 0.003 / 1.77 mg/L < 0.002039 / lbs/day
Feb 2019 Week 2 < 0.003 / mg/L < 0.001681 / lbs/day
Apr 2019 Week 4 < 0.003 / mg/L < 0.002039 / lbs/day
Feb 2019 Average < 0.003 /0.41 mg/L < 0.001681 / lbs/day
Apr 2019 Average < 0.003 /0.41 mg/L < 0.002039 / lbs/day
2019 Quarter 1 < 0.003 / mg/L < 0.001681 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.002039 / lbs/day
2019 1st 6 Months(Avg) < 0.003 / mg/L < 0.001860 / lbs/day
2019 1st 6...(Max) < 0.003 / mg/L < 0.002039 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < 0.001681 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SanrplelD Result/Limit Mass/Limit
Molybdenum
04/30/2019 P Biogen043019POTW < 0.001 / mg/L < 0.0008 / lbs/day
Apr 2019 Week 4 < 0.001 / mg/L < 0.0008 / lbs/day
Apr 2019 Average < 0.001 / mg/L < 0.0008 / lbs/day
2019 Quarter 2 < 0.001 / mg/L < 0.0008 / lbs/day
2019 1st 6 Months(Avg) < 0.001 / mg/L < 0.0008 / lbs/day
2019 1st 6...(Max) < 0.001 / mg/L < 0.0008 / lbs/day
2019 1st 6...(Min) < 0.001 / mg/L < 0.0008 / lbs/day •
2019 1st 6...(Count) 1 / 1 /
•
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 11

Biogen
SAMPLE O VER VIE W
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
02/12/2019 S Biogen021219Se1f < 0.025 / 12.19 mg/L < 0.0168 / lbs/day
04/30/2019 P Biogen043019POTW < 0.003 / 12.19 mg/L < 0.002 / lbs/day
Feb 2019 Week 2 < 0.025 / mg/L < 0.0168 / lbs/day
Apr 2019 Week 4 < 0.003 / mg/L < 0.002 / lbs/day
Feb 2019 Average < 0.025 /4.83 mg/L < 0.0168 / lbs/day
Apr 2019 Average < 0.003 /4.83 mg/L < 0.002 / lbs/day
2019 Quarter 1 < 0.025 / mg/L < 0.0168 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.002 / lbs/day
2019 1st 6 Months(Avg) < 0.014 / mg/L < 0.0094 / lbs/day
2019 1st 6...(Max) < 0.025 / mg/L < 0.0168 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < 0.0020 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/12/2019 S Biogen021219Self 0.7 / mg/L 0.497 / lbs/day
04/02/2019 S Biogen040219Self 0.6 / mg/L 0.406 / lbs/day
04/30/2019 P Biogen043019POTW 0.6 / mg/L 0.522 / lbs/day
Feb 2019 Week 2 0.7 / mg/L 0.497 / lbs/day
Apr 2019 Week 1 0.6 / mg/L 0.406 / lbs/day
Apr 2019 Week 4 0.6 / mg/L 0.522 / lbs/day
Feb 2019 Average 0.7 / mg/L 0.497 / lbs/day
Apr 2019 Average 0.6 / mg/L 0.464 / lbs/day
2019 Quarter 1 0.7 / mg/L 0.497 / lbs/day
2019 Quarter 2 0.6 / mg/L 0.464 / lbs/day
2019 1st 6 Months(Avg) 0.7 / mg/L 0.475 / lbs/day
2019 1st 6...(Max) 0.7 / mg/L 0.522 / lbs/day
2019 1st 6...(Min) 0.6 / mg/L 0.406 / lbs/day
2019 1st 6...(Count) 3 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
04/02/2019 S Biogen040219Self 5.8 / mg/L 4.058 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 11

Biogen
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
04/30/2019 P Biogen043019POTW 6.1 / mg/L 4.975 / lbs/day
Apr 2019 Week 1 5.8 / mg/L 4.058 / lbs/day
Apr 2019 Week 4 6.1 / mg/L 4.975 / lbs/day
Apr 2019 Average 5.95 / mg/L 4.517 / lbs/day
2019 Quarter 2 5.95 / mg/L 4.517 / lbs/day
2019 1st 6 Months(Avg) 5.95 / mg/L 4.517 / lbs/day
2019 1st 6...(Max) 6.1 / mg/L 4.975 / lbs/day
2019 1st 6...(Min) 5.8 / mg/L 4.058 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/12/2019 S Biogen021219Se1f < 2.5 /200 mg/L < /
04/30/2019 P Biogen043019POTW < 2.5 /200 mg/L < /
Feb 2019 Week 2 < 2.5 / mg/L < /
Apr 2019 Week 4 < 2.5 / mg/L < /
Feb 2019 Average < 2.5 / mg/L < /
Apr 2019 Average < 2.5 / mg/L < /
2019 Quarter I < 2.5 / mg/L < /
2019 Quarter 2 < 2.5 / mg/L < /
2019 1st 6 Months(Avg) < 2.5 / mg/L /
2019 1st 6...(Max) < 2.5 / mg/L /
2019 1st 6...(Min) < 2.5 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/12/2019 S Biogen021219Se1f 7.11 /5.5- 10.5 SU /
04/30/2019 P Biogen043019POTW 7.9 /5.5- 10.5 SU /
Feb 2019 Week 2 7.11 / SU /
Apr 2019 Week 4 7.9 / SU /
Feb 2019 Average 7.11 / SU /
Apr 2019 Average 7.9 / SU /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 11

Biogen
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2019 Quarter 1 7.11 / SU /
2019 Quarter 2 7.9 / SU /
2019 1st 6 Months(Avg) 7.51 / SU /
2019 1st 6...(Max) 7.9 / SU /
2019 1st 6...(Min) 7.11 / SU /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
04/30/2019 P Biogen043019POTW 26 /66 °C /
Apr 2019 Week 4 26 / °C /
Apr 2019 Average 26 / °C /
2019 Quarter 2 26 / °C /
2019 1st 6 Months(Avg) 26 / °C /
2019 1st 6...(Max) 26 / °C /
2019 1st 6...(Min) 26 / °C /
2019 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
04/02/2019 S Biogen040219Se1f 5.2 / mg/L 3.638 / lbs/day
04/30/2019 P Biogen043019POTW 5.46 / mg/L 4.453 / lbs/day
Apr 2019 Week 1 5.2 / mg/L 3.638 / lbs/day
Apr 2019 Week 4 5.46 / mg/L 4.453 / lbs/day
Apr 2019 Average 5.33 / mg/L 4.046 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 11

Bioien
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
2019 Quarter 2 5.33 / mg/L 4.046 / lbs/day
2019 1st 6 Months(Avg) 5.33 / mg/L 4.046 / lbs/day
2019 1st 6...(Max) 5.46 / mg/L 4.453 / lbs/day
2019 1st 6...(Min) 5.2 / mg/L 3.638 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/12/2019 S Biogen021219Self 1.3 / mg/L 0.8739 / lbs/day
04/30/2019 P Biogen043019POTW 1.34 / mg/L 1.093 / lbs/day
Feb 2019 Week 2 1.3 / mg/L 0.8739 / lbs/day
Apr 2019 Week 4 1.34 / mg/L 1.093 / lbs/day
Feb 2019 Average 1.3 / mg/L 0.8739 / lbs/day
Apr 2019 Average 1.34 / mg/L 1.093 / lbs/day
2019 Quarter 1 1.3 / mg/L 0.8739 / lbs/day
2019 Quarter 2 1.34 / mg/L 1.093 / lbs/day
2019 1st 6 Months(Avg) 1.32 / mg/L 0.9834 / lbs/day
2019 1st 6...(Max) 1.34 / mg/L 1.0930 / lbs/day
2019 1st 6...(Min) 1.3 / mg/L 0.8739 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
02/12/2019 S Biogen021219Self 23.8 / mg/L 15.998455 / lbs/day
04/30/2019 P Biogen043019POTW 80 / mg/L 65.25216 / lbs/day
Feb 2019 Week 2 23.8 / mg/L 15.998455 / lbs/day
Apr 2019 Week 4 80 / mg/L 65.25216 / lbs/day
Feb 2019 Average 23.8 / mg/L 15.998455 / lbs/day
Apr2019 Average 80 / mg/L 65.25216 / lbs/day
2019 Quarter 1 23.8 / mg/L 15.998455 / lbs/day
2019 Quarter 2 80 / mg/L 65.25216 / lbs/day
2019 1st 6 Months(Avg) 51.9 / mg/L 40.6253 / lbs/day
2019 1st 6...(Max) 80 / mg/L 65.25216 / lbs/day
2019 1st 6...(Min) 23.8 / mg/L 15.998455 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/12/2019 S Biogen021219Self < 0.0025 / mg/L < /
Feb 2019 Week 2 < 0.0025 / mg/L < /
Feb 2019 Average . < 0.0025 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 11

-1 ,•,•
Biogen
SAMPLE OVERVIEW 1
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
VOC
2019 Quarter 1 < 0.0025 / mg/L < /
2019 1st 6 Months(Avg) < 0.0025 / mg/L < /
2019 1st 6...(Max) < 0.0025 / mg/L < /
2019 1st 6...(Min) < 0.0025 / mg/L < /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
' 02/12/2019 S Biogen021219Self 0.305 / mg/L 0.205022 / lbs/day
04/30/2019 P Biogen043019POTW 0.588 / mg/L 0.479603 / lbs/day
Feb 2019 Week 2 0.305 / mg/L 0.205022 / lbs/day
Apr 2019 Week 4 0.588 / mg/L 0.479603 / lbs/day
Feb 2019 Average 0.305 / mg/L 0.205022 / lbs/day
Apr 2019 Average 0.588 / mg/L 0.479603 / lbs/day
2019 Quarter 1 0.305 / mg/L 0.205022 / lbs/day
2019 Quarter 2 0.588 / mg/L 0.479603 / lbs/day
2019 1st 6 Months(Avg) 0.447 / mg/L 0.342313 / lbs/day
2019 1st 6...(Max) 0.588 / mg/L 0.479603 / lbs/day
2019 1st 6...(Min) 0.305 / mg/L 0.205022 / lbs/day
2019 1st 6...(Count) 2 / 2 /
•
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page II of 11

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
01/22/2019 S Cintas012219Se1f 1.75 / mg/L 0.929234 / lbs/day
Jan 2019 Week 4 1.75 / mg/L 0.929234 / lbs/day
Jan 2019 Average 1.75 / mg/L 0.929234 / lbs/day
2019 Quarter 1 1.75 / mg/L 0.929234 / lbs/day
2019 1st 6 Months(Avg) 1.75 / mg/L 0.929234 / lbs/day
2019 1st 6...(Max) 1.75 / mg/L 0.929234 / lbs/day
2019 1st 6...(Min) 1.75 / mg/L 0.929234 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
01/04/2019 P Cintas010419POTW 3.1 / mg/L 2.4235 / lbs/day
01/22/2019 S Cintas012219Se1f 17.1 / mg/L 9.0799 / lbs/day
02/12/2019 S Cintas021219Self 12.3 / mg/L 7.6136 / lbs/day
03/22/2019 S Cintas032219Self 6 / mg/L 4.3742 / lbs/day
04/09/2019 S Cintas040919Se1f 7.3 / mg/L 5.5545 / lbs/day
05/14/2019 S Cintas051419Self 0.97 / mg/L 0.4984 / lbs/day
06/07/2019 S Cintas060719Self 6.2 / mg/L 3.9026 / lbs/day
Jan 2019 Week 1 3.1 / mg/L 2.4235 / lbs/day
Jan 2019 Week 4 17.1 / mg/L 9.0799 / lbs/day
Feb 2019 Week 2 12.3 / mg/L 7.6136 / lbs/day
Mar 2019 Week 4 6 / mg/L 4.3742 / lbs/day
Apr 2019 Week 2 7.3 / mg/L 5.5545 / lbs/day
May 2019 Week 2 0.97 / mg/L 0.4984 / lbs/day
Jun 2019 Week 1 6.2 / mg/L 3.9026 / lbs/day
Jan 2019 Average 10.1 / mg/L 5.7517 / lbs/day
Feb 2019 Average 12.3 / mg/L 7.6136 / lbs/day
Mar 2019 Average 6 / mg/L 4.3742 / lbs/day
Apr 2019 Average 7.3 / mg/L 5.5545 / lbs/day
May 2019 Average 0.97 / mg/L 0.4984 / lbs/day
Jun 2019 Average 6.2 / mg/L 3.9026 / lbs/day
2019 Quarter 1 9.63 / mg/L 5.8728 / lbs/day
2019 Quarter 2 4.82 / mg/L 3.3185 / lbs/day
2019 1st 6 Months(Avg) 7.57 / mg/L 4.7781 / lbs/day
2019 1st 6...(Max) 17.1 / mg/L 9.0799 / lbs/day
2019 1st 6...(Min) 0.97 / mg/L 0.4984 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S Cintas0119Flow 0.064517 /0.180 MGD /
02/28/2019 S Cintas0219F1ow 0.064855 /0.180 MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
03/31/2019 S Cintas0319F1ow 0.071779 /0.180 MGD /
04/30/2019 S Cintas0419Flow 0.070686 /0.180 MGD /
05/31/2019 S Cintas0519Flow 0.064506 /0.180 MGD /
06/30/2019 S Cintas0619Flow 0.058031 /0.180 MGD /
Jan 2019 Week 4 0.064517 / MGD /
Feb 2019 Week 4 0.064855 / MGD /
Mar 2019 Week 4 0.071779 / MGD /
Apr 2019 Week 4 0.070686 / MGD /
May 2019 Week 4 0.064506 / MGD /
Jun 2019 Week 4 0.058031 / MGD /
Jan 2019 Average 0.064517 /0.120 MGD /
Feb 2019 Average 0.064855 /0.120 MGD /
Mar 2019 Average 0.071779 /0.120 MGD /
Apr 2019 Average 0.070686 /0.120 MGD /
May 2019 Average 0.064506 /0.120 MGD /
Jun 2019 Average 0.058031 /0.120 MGD /
2019 Quarter 1 0.06705 / MGD /
2019 Quarter 2 0.064408 / MGD /
2019 1st 6 Months(Avg) 0.065729 / MGD /
2019 1st 6...(Max) 0.071779 / MGD /
2019 1st 6...(Min) . 0.058031 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date .SamplelD Result/Limit Mass/Limit
BOD
01/04/2019 P Cintas010419POTW 315 / mg/L 246.262 / lbs/day
01/22/2019 S Cintas012219Se1f 435 / mg/L 230.981 / lbs/day
02/12/2019 S Cintas021219Self 15.4 / mg/L 9.533 / lbs/day
02/14/2019 P Cintas021419POTW 709 / mg/L /
03/22/2019 S Cintas032219Se1f 237 / mg/L 172.781 / lbs/day
03/26/2019 P Cintas032619POTW 257 / mg/L /
04/09/2019 S Cintas040919Se1f 352 / mg/L 267.834 / lbs/day
04/25/2019 P Cintas042519POTW 626 / mg/L /
05/14/2019 S Cintas051419Self 104 / mg/L 53.44 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOD
05/16/2019 P Cintas051619POTW 270 / mg/L /
06/07/2019 S Cintas060719Se1f 204 / mg/L 128.408 / lbs/day
06/11/2019 P Cintas061119POTW 306 / mg/L /
Jan 2019 Week 1 315 / mg/L 246.262 / lbs/day
Jan 2019 Week 4 435 / mg/L 230.981 / lbs/day
Feb 2019 Week 2 362.2 / mg/L 9.533 / lbs/day
Mar 2019 Week 4 247 / mg/L 172.781 / lbs/day
Apr 2019 Week 2 352 / mg/L 267.834 / lbs/day
Apr 2019 Week 4 626 / mg/L /
May 2019 Week 2 104 / mg/L 53.44 / lbs/day
May 2019 Week 3 270 / mg/L /
Jun 2019 Week 1 204 / mg/L 128.408 / lbs/day
Jun 2019 Week 2 306 / mg/L /
1 Jan 2019 Average 375 / mg/L 238.621 / lbs/day
Feb 2019 Average 362.2 / mg/L 9.533 / lbs/day
Mar 2019 Average 247 / mg/L 172.781 / lbs/day
Apr 2019 Average 489 / mg/L 267.834 / lbs/day
May 2019 Average 187 / mg/L 53.44 / lbs/day
Jun 2019 Average 255 / mg/L 128.408 / lbs/day
2019 Quarter 1 328.1 / mg/L 164.889 / lbs/day
2019 Quarter 2 310.3 / mg/L 149.894 / lbs/day
2019 1st 6 Months(Avg) 319.2 / mg/L 158.463 / lbs/day
2019 1st 6...(Max) 709 / mg/L 267.834 / lbs/day
2019 1st 6...(Min) 15.4 / mg/L /
2019 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/22/2019 S Cintas012219Self 0.0012 / mg/L 0.000637 / lbs/day
Jan 2019 Week 4 0.0012 / mg/L 0.000637 / lbs/day
Jan 2019 Average 0.0012 / mg/L 0.000637 / lbs/day
2019 Quarter 1 0.0012 / mg/L 0.000637 / lbs/day
2019 1st 6 Months(Avg) 0.0012 / mg/L 0.000637 / lbs/day
2019 1st 6...(Max) 0.0012 / mg/L 0.000637 / lbs/day
2019 1st 6...(Min) 0.0012 / mg/L 0.000637 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/04/2019 P Cintas010419POTW 114 / mg/L 89.1233 / lbs/day
01/22/2019 S Cintas012219Self 101 / mg/L 53.6301 / lbs/day
Jan 2019 Week 1 114 / mg/L 89.1233 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
Jan 2019 Week 4 101 / mg/L 53.6301 / lbs/day
Jan 2019 Average 107.5 / mg/L 71.3767 / lbs/day
2019 Quarter 1 107.5 / mg/L 71.3767 / lbs/day
2019 1st 6 Months(Avg) 107.5 / mg/L 71.3767 / lbs/day
2019 1st 6...(Max) 114 / mg/L 89.1233 / lbs/day
2019 1st 6...(Min) 101 / mg/L 53.6301 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
01/22/2019 S Cintas012219Self 0.015 / mg/L 0.007912 / lbs/day
02/12/2019 S Cintas021219Self < 0.003 / mg/L < 0.001857 / lbs/day
03/22/2019 S Cintas032219Self 0.008 / mg/L 0.005978 / lbs/day
04/09/2019 S Cintas040919Se1f 0.026 / mg/L 0.019403 / lbs/day
05/14/2019 S Cintas051419Se1f < 0.003 / mg/L < 0.001285 / lbs/day
06/07/2019 S Cintas060719Se1f < 0.003 / mg/L < 0.001574 / lbs/day
Jan 2019 Week 4 0.015 / mg/L 0.007912 / lbs/day
Feb 2019 Week 2 < 0.003 / mg/L < 0.001857 / lbs/day
Mar 2019 Week 4 0.008 / mg/L 0.005978 / lbs/day
Apr 2019 Week 2 0.026 / mg/L 0.019403 / lbs/day
May 2019 Week 2 < 0.003 / mg/L < 0.001285 / lbs/day
Jun 2019 Week 1 < 0.003 / mg/L < 0.001574 / lbs/day
Jan 2019 Average 0.015 / mg/L 0.007912 / lbs/day
Feb 2019 Average < 0.003 / mg/L < 0.001857 / lbs/day
Mar 2019 Average 0.008 / mg/L 0.005978 / lbs/day
Apr 2019 Average 0.026 / mg/L 0.019403 / lbs/day
May 2019 Average < 0.003 / mg/L < 0.001285 / lbs/day
Jun 2019 Average < 0.003 / mg/L < 0.001574 / lbs/day
2019 Quarter 1 < 0.009 / mg/L < 0.005249 / lbs/day
2019 Quarter 2 < 0.01 / mg/L < 0.00742 / lbs/day
2019 1st 6 Months(Avg) < 0.009 / mg/L < 0.006335 / lbs/day
2019 1st 6...(Max) 0.026 / mg/L 0.019403 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < 0.001285 / lbs/day
2019 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/22/2019 S Cintas012219Self 0.104 / mg/L 0.055223 / lbs/day
02/12/2019 S Cintas021219Self 0.069 / mg/L 0.042958 / lbs/day
03/22/2019 S Cintas032219Self 0.086 / mg/L 0.062405 / lbs/day
04/09/2019 S Cintas040919Self 0.173 / mg/L 0.131634 / lbs/day
05/14/2019 S Cintas051419Self 70.5 / mg/L 36.226008 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfa11: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
06/07/2019 S Cintas060719Se1f 0.073 / mg/L 0.045761 / lbs/day
Jan 2019 Week 4 0.104 / mg/L 0.055223 / lbs/day
Feb 2019 Week 2 0.069 / mg/L 0.042958 / lbs/day
Mar 2019 Week 4 0.086 / mg/L 0.062405 / lbs/day
Apr 2019 Week 2 0.173 / mg/L 0.131634 / lbs/day
May 2019 Week 2 70.5 / mg/L 36.226008 / lbs/day
Jun 2019 Week 1 0.073 / mg/L 0.045761 / lbs/day
Jan 2019 Average 0.104 / mg/L 0.055223 / lbs/day
Feb 2019 Average 0.069 / mg/L 0.042958 / lbs/day
Mar 2019 Average 0.086 / mg/L 0.062405 / lbs/day
Apr 2019 Average 0.173 / mg/L 0.131634 / lbs/day
May 2019 Average 70.5 / mg/L 36.226008 / lbs/day
Jun 2019 Average 0.073 / mg/L 0.045761 / lbs/day
2019 Quarter 1 0.086 / mg/L 0.053529 / lbs/day
2019 Quarter 2 23.582 / mg/L 12.134468 / , lbs/day
2019 1st 6 Months(Avg) 11.834 / mg/L 6.094 / lbs/day
2019 1st 6...(Max) 70.5 / mg/L 36.226008 / lbs/day
2019 1st 6...(Min) 0.069 / mg/L 0.042958 / lbs/day
2019 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/04/2019 P Cintas010419POTW 0.13 / mg/L 0.1016 / lbs/day
01/22/2019 S Cintas012219Self < 0.05 / mg/L < 0.0265 / lbs/day
02/12/2019 S Cintas021219Se1f 1.7 / mg/L 1.0523 / lbs/day
03/22/2019 S Cintas032219Self < 0.05 / mg/L < 0.0365 / lbs/day
04/09/2019 S Cintas040919Self 1.5 / mg/L 1.1413 / lbs/day
05/14/2019 S Cintas051419Self 0.45 / mg/L 0.2312 / lbs/day
06/07/2019 S Cintas060719Self 0.48 / mg/L 0.3021 / lbs/day
Jan 2019 Week 1 0.13 / mg/L 0.1016 / lbs/day
1 Jan 2019 Week 4 < 0.05 / mg/L < 0.0265 / lbs/day
Feb 2019 Week 2 1.7 / mg/L 1.0523 / lbs/day
Mar 2019 Week 4 < 0.05 / mg/L < 0.0365 / lbs/day
Apr 2019 Week 2 1.5 / mg/L 1.1413 / lbs/day
May 2019 Week 2 0.45 / mg/L 0.2312 / lbs/day
Jun 2019 Week 1 0.48 / mg/L 0.3021 / lbs/day
Jan 2019 Average < 0.09 / mg/L < 0.0641 / lbs/day
Feb 2019 Average 1.7 / mg/L 1.0523 / lbs/day
Mar 2019 Average < 0.05 / mg/L < 0.0365 / lbs/day
Apr 2019 Average 1.5 / mg/L 1.1413 / lbs/day
May 2019 Average 0.45 / mg/L 0.2312 / lbs/day
Jun 2019 Average 0.48 / mg/L 0.3021 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30%2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2019 Quarter 1 < 0.48 / mg/L < 0.3042 / lbs/day
2019 Quarter 2 0.81 / mg/L 0.5582 / lbs/day
2019 1st 6 Months(Avg) < 0.62 / mg/L < 0.4131 / lbs/day
2019 1st 6...(Max) 1.7 / mg/L 1.1413 / lbs/day
2019 1st 6...(Min) < 0.05 / mg/L < 0.0265 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Li,,,it
Lead
01/22/2019 S Cintas012219Self 0.0187 / mg/L 0.00993 / lbs/day
02/12/2019 S Cintas021219Self 0.0169 / mg/L 0.010461 / lbs/day
03/22/2019 S Cintas032219Self 0.0154 / mg/L 0.011227 / lbs/day
04/09/2019 S Cintas040919Self 0.0275 / mg/L 0.020925 / lbs/day
05/14/2019 S Cintas051419Self < 0.0025 / mg/L < 0.001285 / lbs/day
06/07/2019 S Cintas060719Se1f 0.0093 / mg/L 0.005854 / lbs/day
Jan 2019 Week 4 0.0187 / mg/L 0.00993 / lbs/day
Feb 2019 Week 2 0.0169 / mg/L 0.010461 / lbs/day
Mar 2019 Week 4 0.0154 / mg/L 0.011227 / lbs/day
Apr 2019 Week 2 0.0275 / mg/L 0.020925 / lbs/day
May 2019 Week 2 < 0.0025 / mg/L < 0.001285 / lbs/day
Jun 2019 Week 1 0.0093 / mg/L 0.005854 / lbs/day
Jan 2019 Average 0.0187 / mg/L 0.00993 / lbs/day
Feb 2019 Average 0.0169 / mg/L 0.010461 / lbs/day
Mar 2019 Average 0.0154 / mg/L 0.011227 / lbs/day
Apr 2019 Average 0.0275 / mg/L 0.020925 / lbs/day
May 2019 Average < 0.0025 / mg/L < 0.001285 / lbs/day
Jun 2019 Average 0.0093 / mg/L 0.005854 / lbs/day
2019 Quarter 1 0.017 / mg/L 0.010539 / lbs/day
2019 Quarter 2 < 0.0131 / mg/L < 0.009354 / lbs/day
2019 1st 6 Months(Avg) < 0.0151 / mg/L < 0.009947 / lbs/day
2019 1st 6...(Max) 0.0275 / mg/L 0.020925 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.001285 / lbs/day
2019 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/03/2019 P Cintas010319POTWH 0.000013 /0.000142 mg/L /
g
01/22/2019 S Cintas012219Self 0.000002 /0.000142 mg/L /
Jan 2019 Week 1 0.000013 / mg/L /
Jan 2019 Week 4 0.000002 / mg/L /
Jan 2019 Average 0.000007 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
2019 Quarter 1 0.000007 / mg/L /
2019 1st 6 Months(Avg) 0.000007 / mg/L /
2019 1st 6...(Max) 0.000013 / mg/L /
2019 1st 6...(Min) 0.000002 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/22/2019 S Cintas012219Self 0 / mg/L 0.0136 / lbs/day
Jan 2019 Week 4 0 / mg/L 0.0136 / lbs/day
Jan 2019 Average 0 / mg/L 0.0136 / lbs/day
2019 Quarter 1 0 / mg/L 0.0136 / lbs/day
2019 1st 6 Months(Avg) 0.026 / mg/L 0.0136 / lbs/day
2019 1st 6...(Max) 0.026 / mg/L 0.0136 / lbs/day
2019 1st 6...(Min) 0.026 / mg/L 0.0136 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/22/2019 S Cintas012219Self 0.0279 / mg/L 0.014815 / lbs/day
02/12/2019 S Cintas021219Self 0.0274 / mg/L 0.01696 / lbs/day
03/22/2019 S Cintas032219Self 0.0211 / mg/L 0.015383 / lbs/day
04/09/2019 S Cintas040919Self 0.043 / mg/L 0.032718 / lbs/day
05/14/2019 S Cintas051419Self 25.6 / mg/L 13.154408 / lbs/day
06/07/2019 S Cintas060719Self 0.0235 / mg/L 0.014792 / lbs/day
Jan 2019 Week 4 0.0279 / mg/L 0.014815 / lbs/day
Feb 2019 Week 2 0.0274 / mg/L 0.01696 / lbs/day
Mar 2019 Week 4 0.0211 / mg/L 0.015383 / lbs/day
Apr 2019 Week 2 0.043 / mg/L 0.032718 / lbs/day
May 2019 Week 2 25.6 / mg/L 13.154408 / lbs/day
Jun 2019 Week 1 0.0235 / mg/L 0.014792 / lbs/day
Jan 2019 Average 0.0279 / mg/L 0.014815 / lbs/day
Feb 2019 Average 0.0274 / mg/L 0.01696 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 16
I

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Mar 2019 Average 0.0211 / mg/L 0.015383 / lbs/day
Apr2019 Average 0.043 / mg/L 0.032718 / lbs/day
May 2019 Average 25.6 / mg/L 13.154408 / lbs/day
Jun 2019 Average 0.0235 / mg/L 0.014792 / lbs/day
2019 Quarter 1 0.0255 / mg/L 0.015719 / lbs/day
2019 Quarter 2 8.5555 / mg/L 4.40064 / lbs/day
2019 1st 6 Months(Avg) 4.2905 / mg/L 2.20818 / lbs/day
2019 1st 6...(Max) 25.6 / mg/L 13.154408 / lbs/day
2019 1st 6...(Min) 0.0211 / mg/L 0.014792 / lbs/day
2019 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/04/2019 P Cintas010419POTW < 0.1 / mg/L < 0.039 / lbs/day
01/22/2019 S Cintas012219Se1f 0.2 / mg/L 0.106 / lbs/day
02/12/2019 S Cintas021219Self 0.1 / mg/L 0.074 / lbs/day
03/22/2019 S Cintas032219Self 0.1 / mg/L 0.08 / lbs/day
04/09/2019 S Cintas040919Self 0.2 / mg/L 0.152 / lbs/day
05/14/2019 S Cintas051419Self < 0.1 / mg/L < 0.026 / lbs/day
06/07/2019 S Cintas060719Self < 0.1 / mg/L < 0.031 / lbs/day
Jan 2019 Week 1 < 0.1 / mg/L < 0.039 / lbs/day
Jan 2019 Week 4 0.2 / mg/L 0.106 / lbs/day
Feb 2019 Week 2 0.1 / mg/L 0.074 / lbs/day
Mar 2019 Week 4 0.1 / mg/L 0.08 / lbs/day
Apr 2019 Week 2 0.2 / mg/L 0.152 / lbs/day
May 2019 Week 2 < 0.1 / mg/L < 0.026 / lbs/day
Jun 2019 Week 1 < 0.1 / mg/L < 0.031 / lbs/day
Jan 2019 Average < 0.1 / mg/L < 0.073 / lbs/day
Feb 2019 Average 0.1 / mg/L 0.074 / lbs/day
Mar 2019 Average 0.1 / mg/L 0.08 / lbs/day
Apr 2019 Average 0.2 / mg/L 0.152 / lbs/day
May 2019 Average < 0.1 / mg/L < 0.026 / lbs/day
Jun 2019 Average < 0.1 / mg/L < 0.031 / lbs/day
2019 Quarter 1 < 0.1 / mg/L < 0.075 / lbs/day
2019 Quarter 2 < 0.1 / mg/L < 0.07 / lbs/day
2019 1st 6 Months(Avg) < 0.1 / mg/L < 0.073 / lbs/day
2019 1st 6...(Max) 0.2 / mg/L 0.152 / lbs/day
2019 1st 6...(Min) < 0.1 / mg/L < 0.026 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
01/04/2019 P Cintas010419POTW 18.5 / mg/L 14.463 / lbs/day
01/22/2019 S Cintas012219Self 70.3 / mg/L 37.329 / lbs/day
02/12/2019 S Cintas021219Self 31.3 / mg/L 19.375 / lbs/day
03/22/2019 S Cintas032219Self 30.8 / mg/L 22.454 / lbs/day
05/14/2019 S Cintas051419Self 11.5 / mg/L 5.909 / lbs/day
06/07/2019 S Cintas060719Self 30.1 / mg/L 18.947 / lbs/day
Jan 2019 Week 1 18.5 / mg/L 14.463 / lbs/day
Jan 2019 Week 4 70.3 / mg/L 37.329 / lbs/day
Feb 2019 Week 2 31.3 / mg/L 19.375 / lbs/day
Mar 2019 Week 4 30.8 / mg/L 22.454 / lbs/day
May 2019 Week 2 11.5 / mg/L 5.909 / lbs/day
Jun 2019 Week 1 30.1 / mg/L 18.947 / lbs/day
Jan 2019 Average 44.4 / mg/L 25.896 / lbs/day
Feb 2019 Average 31.3 / mg/L 19.375 / lbs/day
Mar 2019 Average 30.8 / mg/L 22.454 / lbs/day
May 2019 Average 11.5 / mg/L 5.909 / lbs/day
Jun 2019 Average 30.1 / mg/L 18.947 / lbs/day
2019 Quarter 1 37.73 / mg/L 23.405 / lbs/day
2019 Quarter 2 20.8 / mg/L 12.428 / lbs/day
2019 1st 6 Months(Avg) 32.08 / mg/L 19.746 / lbs/day
2019 1st 6...(Max) 70.3 / mg/L 37.329 / lbs/day
2019 1st 6...(Min) 11.5 / mg/L 5.909 / lbs/day
2019 1st 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
01/04/2019 P Cintas010419POTW 16 / 100 mg/L 12.508532 / lbs/day
01/22/2019 S Cintas012219Self 29.7 / 100 mg/L 15.770436 / lbs/day
02/12/2019 S Cintas021219Self 16.9 / 100 mg/L 10.461012 / lbs/day
03/22/2019 S Cintas032219Self 22.4 / 100 mg/L 16.330334 / lbs/day
04/09/2019 S Cintas040919Self 10.4 / 100 mg/L 7.913272 / lbs/day
05/14/2019 S Cintas051419Self 224 / 100 mg/L * * 115.101074 / lbs/day
06/07/2019 S Cintas060719Self 19.2 / 100 mg/L 12.085501 / lbs/day
Jan 2019 Week 1 16 / mg/L 12.508532 / lbs/day
Jan 2019 Week 4 29.7 / mg/L 15.770436 / lbs/day
Feb 2019 Week 2 16.9 / mg/L 10.461012 / lbs/day
Mar 2019 Week 4 22.4 / mg/L 16.330334 / lbs/day
Apr 2019 Week 2 10.4 / mg/L 7.913272 / lbs/day
May 2019 Week 2 224 / mg/L 115.101074 / lbs/day
Jun 2019 Week 1 19.2 / mg/L 12.085501 / lbs/day
Jan 2019 Average 22.9 / mg/L 14.139484 / lbs/day
Feb 2019 Average 16.9 / mg/L 10.461012 / lbs/day 1
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
Mar 2019 Average 22.4 / mg/L 16.330334 / lbs/day
Apr 2019 Average 10.4 / mg/L 7.913272 / lbs/day
May 2019 Average 224 / mg/L 115.101074 / lbs/day
Jun 2019 Average 19.2 / mg/L 12.085501 / lbs/day
2019 Quarter 1 21.3 / mg/L 13.767579 / lbs/day
2019 Quarter 2 84.5 / mg/L 45.033282 / lbs/day
2019 1st 6 Months(Avg) 48.4 / mg/L 27.1672 / lbs/day
2019 1st 6...(Max) 224 / mg/L 115.101074 / lbs/day
2019 1st 6...(Min) 10.4 / mg/L 7.913272 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 1 14.29 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 1 14.29 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT HEM(Non-Polar)
01/04/2019 P Cintas010419POTW 26 / 100 mg/L 20.3264 / lbs/day
01/22/2019 S Cintas012219Se1f 8.4 / 100 mg/L 4.4603 / lbs/day
02/12/2019 S Cintas021219Self 14.3 / 100 mg/L 8.8516 / lbs/day
03/22/2019 S Cintas032219Se1f 6.1 / 100 mg/L 4.4471 / lbs/day
04/09/2019 S Cintas040919Self 7.5 / 100 mg/L 5.7067 / lbs/day
05/14/2019 S Cintas051419Self 103 / 100 mg/L * 52.9259 / lbs/day
06/07/2019 S Cintas060719Self < 2.5 / 100 mg/L < 1.5736 / lbs/day
Jan 2019 Week 1 26 / mg/L 20.3264 / lbs/day
Jan 2019 Week 4 8.4 / mg/L 4.4603 / lbs/day
Feb 2019 Week 2 14.3 / mg/L 8.8516 / lbs/day
Mar 2019 Week 4 6.1 / mg/L 4.4471 / lbs/day
Apr 2019 Week 2 7.5 / mg/L 5.7067 / lbs/day
May 2019 Week 2 103 m 52.9259 lbs/day
/ mg/L /
Jun 2019 Week 1 < 2.5 / mg/L < 1.5736 / lbs/day
Jan 2019 Average 17.2 / mg/L 12.3933 / lbs/day
Feb 2019 Average 14.3 / mg/L 8.8516 / lbs/day
Mar 2019 Average 6.1 / mg/L 4.4471 / lbs/day
Apr 2019 Average 7.5 / mg/L 5.7067 / lbs/day
May 2019 Average 103 / mg/L 52.9259 / lbs/day
Jun 2019 Average < 2.5 / mg/L < 1.5736 / lbs/day
2019 Quarter 1 13.7 / mg/L 9.5214 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT HEM(Non-Polar)
2019 Quarter 2 < 37.7 / mg/L < 20.0688 / lbs/day
2019 1st 6 Months(Avg) < 24.0 / mg/L < 14.0417 / lbs/day
2019 1st 6...(Max) 103 / mg/L 52.9259 / lbs/day
2019 1st 6...(Min) < 2.5 / mg/L < 1.5736 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 1 14.29 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/04/2019 P Cintas010419POTW 7.3 /6.0- 10.5 SU /
01/22/2019 S Cintas012219Self 9.4 /6.0- 10.5 SU /
02/12/2019 S Cintas021219Self 7 /6.0- 10.5 SU /
03/04/2019 S Cintas030419Self 7.7 /6.0- 10.5 SU /
03/22/2019 S Cintas032219Self 7 /6.0- 10.5 SU /
04/09/2019 S Cintas040919Se1f 6.6 /6.0- 10.5 SU /
05/14/2019 S Cintas051419Se1f 6.5 /6.0- 10.5 SU /
06/07/2019 S Cintas060719Self 6.7 /6.0- 10.5 SU /
Jan 2019 Week 1 7.3 / SU /
Jan 2019 Week 4 9.4 / SU /
Feb 2019 Week 2 7 / SU /
Mar 2019 Week 1 7.7 / SU /
Mar 2019 Week 4 7 / SU /
Apr 2019 Week 2 6.6 / SU /
May 2019 Week 2 6.5 / SU /
Jun 2019 Week 1 6.7 / SU /
Jan 2019 Average 8.35 / SU /
Feb 2019 Average 7 / SU /
Mar 2019 Average 7.35 / SU /
Apr 2019 Average 6.6 / SU /
May 2019 Average 6.5 / SU /
Jun 2019 Average 6.7 / SU /
2019 Quarter 1 7.68 / SU /
2019 Quarter 2 6.6 / SU /
2019 1st 6 Months(Avg) 7.28 / SU /
2019 1st 6...(Max) 9.4 / SU /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 11 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
2019 1st 6...(Min) 6.5 / SU /
2019 1st 6...(Count) 8 / /
Sample Count: 8 Months Sampled: 6 Weeks Sampled : 8 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
01/22/2019 S Cintas012219Se1f < 0.0025 / mg/L < 0.001327 / lbs/day
Jan 2019 Week 4 < 0.0025 / mg/L < 0.001327 / lbs/day
Jan 2019 Average < 0.0025 / mg/L < 0.001327 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.001327 / lbs/day
2019 1st 6 Months(Avg) < 0.0025 / mg/L < 0.001327 / lbs/day
2019 1st 6...(Max) < 0.0025 / mg/L < 0.001327 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.001327 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/04/2019 P Cintas010419POTW 22 /66 °C /
01/22/2019 S Cintas012219Self 20.5 /66 °C /
02/12/2019 S Cintas021219Self 24.1 /66 °C /
03/04/2019 S Cintas030419Self 33.2 /66 °C /
03/22/2019 S Cintas032219Self 27.1 /66 °C /
04/09/2019 S Cintas040919Self 30.6 /66 °C /
05/14/2019 S Cintas051419Self 15.4 /66 °C /
06/07/2019 S Cintas060719Self 36.8 /66 °C /
Jan 2019 Week 1 22 / °C /
Jan 2019 Week 4 20.5 / °C /
Feb 2019 Week 2 24.1 / °C /
Mar 2019 Week 1 33.2 / °C /
Mar 2019 Week 4 27.1 / °C /
Apr 2019 Week 2 30.6 / °C /
May 2019 Week 2 15.4 / °C /
Jun 2019 Week 1 36.8 / °C /
Jan 2019 Average 21.3 / °C /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 12 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Feb 2019 Average 24.1 / °C /
Mar 2019 Average 30.2 / °C /
Apr 2019 Average 30.6 / °C /
May 2019 Average 15.4 / °C /
Jun 2019 Average 36.8 / °C /
2019 Quarter 1 25.4 / °C /
2019 Quarter 2 27.6 / °C /
2019 1st 6 Months(Avg) 26.2 / °C /
2019 1st 6...(Max) 36.8 / °C /
2019 1st 6...(Min) 15.4 / °C /
2019 1st 6...(Count) 8 / /
Sample Count: 8 Months Sampled: 6 Weeks Sampled: 8 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/04/2019 P Cintas010419POTW 18.5 / mg/L 14.463 / lbs/day
01/22/2019 S Cintas012219Self 70.1 / mg/L 37.222 / lbs/day
02/12/2019 S Cintas021219Self 31.2 / mg/L 19.313 / lbs/day
02/14/2019 P Cintas021419POTW 49.1 / mg/L /
03/22/2019 S Cintas032219Self 30.7 / mg/L 22.381 / lbs/day
03/26/2019 P Cintas032619POTW 35.7 / mg/L /
04/09/2019 S Cintas040919Self 30.8 / mg/L 23.435 / lbs/day
04/25/2019 P Cintas042519POTW 23 / mg/L /
05/14/2019 S Cintas051419Self 11.4 / mg/L 5.858 / lbs/day
05/16/2019 P Cintas051619POTW 18.9 / mg/L /
06/07/2019 S Cintas060719Self 30.1 / mg/L 18.947 / lbs/day
06/11/2019 P Cintas061119POTW 19.1 / mg/L /
Jan 2019 Week 1 18.5 / mg/L 14.463 / lbs/day
Jan 2019 Week 4 70.1 / mg/L 37.222 / lbs/day
Feb 2019 Week 2 40.15 / mg/L 19.313 / lbs/day
Mar 2019 Week 4 33.2 / mg/L 22.381 / lbs/day
Apr 2019 Week 2 30.8 / mg/L 23.435 / lbs/day
Apr 2019 Week 4 23 / mg/L /
May 2019 Week 2 11.4 / mg/L 5.858 / lbs/day
May 2019 Week 3 18.9 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 13 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
Jun 2019 Week 1 30.1 / mg/L 18.947 / lbs/day
Jun 2019 Week 2 19.1 / mg/L /
Jan 2019 Average 44.3 / mg/L 25.843 / lbs/day
Feb 2019 Average 40.15 / mg/L 19.313 / lbs/day
Mar 2019 Average 33.2 / mg/L 22.381 / lbs/day
Apr2019 Average 26.9 / mg/L 23.435 / lbs/day
May 2019 Average 15.15 / mg/L 5.858 / lbs/day
Jun 2019 Average 24.6 / mg/L 18.947 / lbs/day
2019 Quarter 1 39.22 / mg/L 23.345 / lbs/day
2019 Quarter 2 22.22 / mg/L 16.08 / lbs/day
2019 1st 6 Months(Avg) 30.72 / mg/L 20.231 / lbs/day
2019 1st 6...(Max) 70.1 / mg/L 37.222 / lbs/day
2019 1st 6...(Min) 11.4 / mg/L /
2019 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/04/2019 P Cintas010419POTW 1.73 / mg/L 1.3525 / lbs/day
01/22/2019 S Cintas012219Se1f 5.6 / mg/L 2.9736 / lbs/day
02/12/2019 S Cintas021219Se1f 3.6 / mg/L 2.2284 / lbs/day
02/14/2019 P Cintas021419POTW 4.19 / mg/L /
03/22/2019 S Cintas032219Self 3.5 / mg/L 2.5516 / lbs/day
03/26/2019 P Cintas032619POTW 3.37 / mg/L /
04/09/2019 S Cintas040919Self 2.5 / mg/L 1.9022 / lbs/day
04/25/2019 P Cintas042519POTW 3.21 / mg/L /
05/14/2019 S Cintas051419Self 1.2 / mg/L 0.6166 / lbs/day
05/16/2019 P Cintas051619POTW 3.12 / mg/L /
06/07/2019 S Cintas060719Self 2.8 / mg/L 1.7625 / lbs/day
06/11/2019 P Cintas061119POTW 1.73 / mg/L /
Jan 2019 Week 1 1.73 / mg/L 1.3525 / lbs/day
Jan 2019 Week 4 5.6 / mg/L 2.9736 / lbs/day
Feb 2019 Week 2 3.895 / mg/L 2.2284 / lbs/day
Mar 2019 Week 4 3.435 / mg/L 2.5516 / lbs/day
Apr 2019 Week 2 2.5 / mg/L 1.9022 / lbs/day
Apr 2019 Week 4 3.21 / mg/L /
May 2019 Week 2 1.2 / mg/L 0.6166 / lbs/day
May 2019 Week 3 3.12 / mg/L /
Jun 2019 Week 1 2.8 / mg/L 1.7625 / lbs/day
Jun 2019 Week 2 1.73 / mg/L /
Jan 2019 Average 3.665 / mg/L 2.163 / lbs/day
Feb 2019 Average 3.895 / mg/L 2.2284 / lbs/day
Mar 2019 Average 3.435 / mg/L 2.5516 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 14 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Apr 2019 Average 2.855 / mg/L 1.9022 / lbs/day
May 2019 Average 2.16 / mg/L 0.6166 / lbs/day
Jun 2019 Average 2.265 / mg/L 1.7625 / lbs/day
2019 Quarter 1 3.665 / mg/L 2.2765 / lbs/day
2019 Quarter 2 2.427 / mg/L 1.4271 / lbs/day
2019 1st 6 Months(Avg) 3.046 / mg/L 1.9125 / lbs/day
2019 1st 6...(Max) 5.6 / mg/L 2.9736 / lbs/day
2019 1st 6...(Min) 1.2 / mg/L /
2019 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
01/04/2019 P Cintas010419POTW 268 / mg/L 209.517914 / lbs/day
01/22/2019 S Cintas012219Self 244 / mg/L 129.561833 / lbs/day
02/12/2019 S Cintas021219Self 91.4 / mg/L 56.576125 / lbs/day
02/14/2019 P Cintas021419POTW 916 / mg/L /
03/22/2019 S Cintas032219Self 60.7 / mg/L 44.252289 / lbs/day
03/26/2019 P Cintas032619POTW 108 / mg/L /
04/09/2019 S Cintas040919Self 206 / mg/L 156.743661 / lbs/day
04/25/2019 P Cintas042519POTW 224 / mg/L /
05/14/2019 S Cintas051419Self 69.4 / mg/L 35.660779 / lbs/day
05/16/2019 P Cintas051619POTW 400 / mg/L /
06/07/2019 S Cintas060719Self 222 / mg/L 139.738602 / lbs/day
06/11/2019 P Cintas061119POTW 66 / mg/L /
Jan 2019 Week 1 268 / mg/L 209.517914 / lbs/day
Jan 2019 Week 4 244 / mg/L 129.561833 / lbs/day
Feb 2019 Week 2 503.7 / mg/L 56.576125 / lbs/day
Mar 2019 Week 4 84.4 / mg/L 44.252289 / lbs/day
Apr 2019 Week 2 206 / mg/L 156.743661 / lbs/day
Apr 2019 Week 4 224 / mg/L /
May 2019 Week 2 69.4 / mg/L 35.660779 / lbs/day
May 2019 Week 3 400 / mg/L /
Jun 2019 Week 1 222 / mg/L 139.738602 / lbs/day
Jun 2019 Week 2 66 / mg/L /
Jan 2019 Average 256 / mg/L 169.539873 / lbs/day
Feb 2019 Average 503.7 / mg/L 56.576125 / lbs/day
Mar 2019 Average 84.4 / mg/L 44.252289 / lbs/day
Apr 2019 Average 215 / mg/L 156.743661 / lbs/day
May 2019 Average 234.7 / mg/L 35.660779 / lbs/day
Jun 2019 Average 144 / mg/L 139.738602 / lbs/day
2019 Quarter 1 281.4 / mg/L 109.97704 / lbs/day
2019 Quarter 2 197.9 / mg/L 110.714347 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 15 of 16

Cintas Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
2019 1st 6 Months(Avg) 239.6 / mg/L 110.293 / lbs/day
2019 1st 6...(Max) 916 / mg/L 209.517914 / lbs/day
2019 1st 6...(Min) 60.7 / mg/L /
2019 1st 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
01/22/2019 S Cintas012219Se1f 0.0472 / mg/L /
Jan 2019 Week 4 0.0472 / mg/L /
Jan 2019 Average 0.0472 / mg/L /
2019 Quarter 1 0.0472 / mg/L /
2019 1st 6 Months(Avg) 0.0472 / mg/L /
2019 1st 6...(Max) 0.0472 / mg/L /
2019 1st 6...(Min) 0.0472 / mg/L /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/22/2019 S Cintas012219Se1f 0.916 / mg/L 0.486388 / lbs/day
02/12/2019 S Cintas021219Se1f 1.06 / mg/L 0.656134 / lbs/day
03/22/2019 S Cintas032219Se1f 1.24 / mg/L 0.904001 / lbs/day
04/09/2019 S Cintas040919Se1f 1.18 / mg/L 0.897852 / lbs/day
05/14/2019 S Cintas051419Se1f 1.45 / mg/L 0.745074 / lbs/day
06/07/2019 S Cintas060719Se1f 1.34 / mg/L 0.843467 / lbs/day
Jan 2019 Week 4 0.916 / mg/L 0.486388 / lbs/day
Feb 2019 Week 2 1.06 / mg/L 0.656134 / lbs/day
Mar 2019 Week 4 1.24 / mg/L 0.904001 / lbs/day
Apr 2019 Week 2 1.18 / mg/L 0.897852 / lbs/day
May 2019 Week 2 1.45 / mg/L 0.745074 / lbs/day
Jun 2019 Week 1 1.34 / mg/L 0.843467 / lbs/day
Jan 2019 Average 0.916 / mg/L 0.486388 / lbs/day
Feb 2019 Average 1.06 / mg/L 0.656134 / lbs/day
Mar 2019 Average 1.24 / mg/L 0.904001 / lbs/day
Apr 2019 Average 1.18 / mg/L 0.897852 / lbs/day
May 2019 Average 1.45 / mg/L 0.745074 / lbs/day
Jun 2019 Average 1.34 / mg/L 0.843467 / lbs/day
2019 Quarter 1 1.072 / mg/L 0.682174 / lbs/day
2019 Quarter 2 1.323 / mg/L 0.828798 / lbs/day
2019 1st 6 Months(Avg) 1.198 / mg/L 0.755486 / lbs/day
2019 1st 6...(Max) 1.45 / mg/L 0.904001 / lbs/day
2019 1st 6...(Min) 0.916 / mg/L 0.486388 / lbs/day
2019 1st 6...(Count) 6 / 6 /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 16 of 16

•
Cree, Inc.(All)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 007
Sample Date SamplelD Result/Limit Mass/Limit
TTO
01/30/2019 CreeP7013019POTW 0.0051 /0.771 mg/L /
Jan 2019 Week 4 0.0051 / mg/L /
Jan 2019 Average 0.0051 / mg/L /
2019 Quarter 1 0.0051 / mg/L /
2019 1st 6 Months(Avg) 0.0051 / mg/L /
2019 1st 6...(Max) 0.0051 / mg/L /
2019 1st 6...(Min) 0.0051 / mg/L /
2019 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Ouijall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
03/12/2019 S CreeP8031219Se1f 0.119 / mg/L 0.43172 / lbs/day
Mar 2019 Week 2 0.119 / mg/L 0.43172 / lbs/day
Mar 2019 Average 0.119 / mg/L 0.43172 / lbs/day
2019 Quarter 1 0.119 / mg/L 0.43172 / lbs/day
2019 1st 6 Months(Avg) 0.119 / mg/L 0.43172 / lbs/day
2019 1st 6...(Max) 0.119 / mg/L 0.431720 / lbs/day
2019 1st 6...(Min) 0.119 / mg/L 0.431720 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
03/12/2019 S CreeP8031219Self 16.1 / mg/L 58.4092 / lbs/day
04/16/2019 P CreeP8041619POTW 17.5 / mg/L 34.8821 / lbs/day
Mar 2019 Week 2 16.1 / mg/L 58.4092 / lbs/day
Apr 2019 Week 3 17.5 / mg/L 34.8821 / lbs/day
Mar 2019 Average 16.1 / mg/L 58.4092 / lbs/day
Apr 2019 Average 17.5 / mg/L 34.8821 / lbs/day
2019 Quarter 1 16.1 / mg/L 58.4092 / lbs/day
2019 Quarter 2 17.5 / mg/L 34.8821 / lbs/day
2019 1st 6 Months(Avg) 16.8 / mg/L 46.6456 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of I

Cree, Inc.(AIJ)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
2019 1st 6...(Max) 17.5 / mg/L 58.4092 / lbs/day
2019 1st 6...(Min) 16.1 / mg/L 34.8821 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S CreeP80119F1ow 0.32746 / MGD /
02/28/2019 S CreeP80219F1ow 0.357994 / MGD /
03/31/2019 S CreeP80319F1ow 0.320237 / MGD /
04/30/2019 S CreeP80419Flow 0.256128 / MGD /
05/31/2019 S CreeP80519F1ow 0.255809 / MGD /
06/30/2019 S CreeP80619F1ow 0.283233 / MGD /
Jan 2019 Week 4 0.32746 / MGD /
Feb 2019 Week 4 0.357994 / MGD /
Mar 2019 Week 4 0.320237 / MGD /
Apr 2019 Week 4 0.256128 / MGD /
May 2019 Week 4 0.255809 / MGD /
Jun 2019 Week 4 0.283233 / MGD /
' Jan 2019 Average 0.32746 / MGD /
Feb 2019 Average 0.357994 / MGD /
Mar 2019 Average 0.320237 / MGD /
Apr 2019 Average 0.256128 / MGD /
May 2019 Average 0.255809 / MGD /
Jun 2019 Average 0.283233 / MGD /
2019 Quarter 1 0.33523 / MGD /
2019 Quarter 2 0.265057 / MGD /
2019 1st 6 Months(Avg) 0.300144 / MGD /
2019 1st 6...(Max) 0.357994 / MGD /
2019 1st 6...(Min) 0.255809 / MGD /
2019 1st 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/12/2019 S CreeP8031219Se1f < 0.0005 / mg/L < 0.001814 / lbs/day
Mar 2019 Week 2 < 0.0005 / mg/L < 0.001814 / lbs/day
Mar 2019 Average < 0.0005 / mg/L < 0.001814 / lbs/day
2019 Quarter 1 < 0.0005 / mg/L < 0.001814 / lbs/day
2019 1st 6 Months(Avg) < 0.0005 / mg/L < 0.001814 / lbs/day
2019 1st 6...(Max) < 0.0005 / mg/L < 0.001814 / lbs/day
2019 1st 6...(Min) < 0.0005 / mg/L < 0.001814 / lbs/day
2019 1st 6...(Count) 1 / I /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 9

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
03/12/2019 S CreeP8031219Self 139 / mg/L 504.2781 / lbs/day
04/16/2019 P CreeP8041619POTW 200 / mg/L 398.652 / lbs/day
Mar 2019 Week 2 139 / mg/L 504.2781 / lbs/day
Apr 2019 Week 3 200 / mg/L 398.652 / lbs/day
Mar 2019 Average 139 / mg/L 504.2781 / lbs/day
Apr 2019 Average 200 / mg/L 398.652 / lbs/day
2019 Quarter 1 139 / mg/L 504.2781 / lbs/day
2019 Quarter 2 200 / mg/L 398.652 / lbs/day
2019 1st 6 Months(Avg) 169.5 / mg/L 451.465 / lbs/day
2019 1st 6...(Max) 200 / mg/L 504.2781 / lbs/day
2019 1st 6...(Min) 139 / mg/L 398.652 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit •
Chromium
03/12/2019 S CreeP8031219Self < 0.003 / mg/L < 0.00907 / lbs/day
Mar 2019 Week 2 < 0.003 / mg/L < 0.00907 / lbs/day
Mar 2019 Average < 0.003 / mg/L < 0.00907 / lbs/day
2019 Quarter 1 < 0.003 / mg/L < 0.00907 / lbs/day
2019 1st 6 Months(Avg) < 0.003 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Max) < 0.003 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/12/2019 S CreeP8031219Self 0.051 / mg/L 0.185748 / lbs/day
Mar 2019 Week 2 0.051 / mg/L 0.185748 / lbs/day
Mar 2019 Average 0.051 / mg/L 0.185748 / lbs/day
2019 Quarter 1 0.051 / mg/L 0.185748 / lbs/day
2019 1st 6 Months(Avg) 0.051 / mg/L 0.185748 / lbs/day
2019 1st 6...(Max) 0.051 / mg/L 0.185748 / lbs/day
2019 1st 6...(Min) 0.051 / mg/L 0.185748 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
03/12/2019 S CreeP8031219Self < 0.004 / mg/L < 0.014512 / lbs/day
04/16/2019 P CreeP8041619POTW < 0.003 / mg/L < 0.004983 / lbs/day
Mar 2019 Week 2 < 0.004 / mg/L < 0.014512 / lbs/day
Apr 2019 Week 3 < 0.003 / mg/L < 0.004983 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 9

Cree. Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Mar 2019 Average < 0.004 / mg/L < 0.014512 / lbs/day
Apr 2019 Average < 0.003 / mg/L < 0.004983 / lbs/day
2019 Quarter 1 < 0.004 / mg/L < 0.014512 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.004983 / lbs/day
2019 1st 6 Months(Avg) < 0.003 / mg/L < 0.009747 / lbs/day
2019 1st 6...(Max) < 0.004 / mg/L < 0.014512 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < 0.004983 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
03/12/2019 S CreeP8031219Self 0.68 / mg/L 2.467 / lbs/day
04/16/2019 P CreeP8041619POTW 2.8 / mg/L 5.5811 / lbs/day
Mar 2019 Week 2 0.68 / mg/L 2.467 / lbs/day
Apr 2019 Week 3 2.8 / mg/L 5.5811 / lbs/day
Mar 2019 Average 0.68 / mg/L 2.467 / lbs/day
Apr 2019 Average 2.8 / mg/L 5.5811 / lbs/day
2019 Quarter 1 0.68 / mg/L 2.467 / lbs/day
2019 Quarter 2 2.8 / mg/L 5.5811 / lbs/day
2019 1st 6 Months(Avg) 1.74 / mg/L 4.0241 / lbs/day
2019 1st 6...(Max) 2.8 / mg/L 5.5811 / lbs/day
2019 1st 6...(Min) 0.68 / mg/L 2.4670 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
03/12/2019 S CreeP8031219Self < 0.0025 / mg/L < 0.00907 / lbs/day
Mar 2019 Week 2 < 0.0025 / mg/L < 0.00907 / lbs/day
Mar 2019 Average < 0.0025 / mg/L < 0.00907 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.00907 / lbs/day
2019 1st 6 Months(Avg) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Max) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st6...(Count) 1 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/12/2019 S CreeP8031219Self 0.000001 / mg/L /
04/15/2019 P CreeP8041519POTW 0.000006 / mg/L /
Hg
Mar 2019 Week 2 0.000001 / mg/L /
Apr 2019 Week 3 0.000006 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 9

•
Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Mar 2019 Average 0.000001 / mg/L /
Apr 2019 Average 0.000006 / mg/L /
1 2019 Quarter 1 0.000001 / mg/L /
2019 Quarter 2 0.000006 / mg/L /
2019 1st 6 Months(Avg) 0.000004 / mg/L /
2019 1st 6...(Max) 0.000006 / mg/L /
2019 1st 6...(Min) 0.000001 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/12/2019 S CreeP8031219Self 0.01 / mg/L 0.0348 /0.457 lbs/day
04/16/2019 P CreeP8041619POTW 0.011 / mg/L 0.0219 / 0.457 lbs/day
Mar 2019 Week 2 0.01 / mg/L 0.0348 / lbs/day
Apr 2019 Week 3 0.011 / mg/L 0.0219 / lbs/day
Mar 2019 Average 0.01 / mg/L 0.0348 / lbs/day
Apr 2019 Average 0.011 / mg/L 0.0219 / lbs/day
2019 Quarter 1 0.01 / mg/L 0.0348 / lbs/day
2019 Quarter 2 0.011 / mg/L 0.0219 / lbs/day
2019 1st 6 Months(Avg) 0.010 / mg/L 0.0284 / lbs/day
2019 1st 6...(Max) 0.011 / mg/L 0.0348 / lbs/day
2019 1st 6...(Min) 0.010 / mg/L 0.0219 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
03/12/2019 S CreeP8031219Self < 0.0025 / mg/L < 0.00907 / lbs/day
Mar 2019 Week 2 < 0.0025 / mg/L < 0.00907 / lbs/day
Mar 2019 Average < 0.0025 / mg/L < 0.00907 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.00907 / lbs/day
2019 1st 6 Months(Avg) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Max) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.009070 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 9

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2019 1st6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
03/12/2019 S CreeP8031219Self 1.4 / mg/L 5.079 / lbs/day
04/16/2019 P CreeP8041619POTW < 0.1 / mg/L < 0.1 / lbs/day
Mar 2019 Week 2 1.4 / mg/L 5.079 / lbs/day
Apr 2019 Week 3 < U.I / mg/L < 0.1 / lbs/day
Mar 2019 Average 1.4 / mg/L 5.079 / lbs/day
Apr 2019 Average < 0.1 / mg/L < 0.1 / lbs/day
2019 Quarter 1 1.4 / mg/L 5.079 / lbs/day
2019 Quarter 2 < 0.1 / mg/L < 0.1 / lbs/day
2019 1st 6 Months(Avg) < 0.7 / mg/L < 2.589 / lbs/day
2019 1st 6...(Max) 1.4 / mg/L 5.079 / lbs/day
2019 1st 6...(Min) < 0.1 / mg/L < 0.100 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
I
Nitrogen,Total
03/12/2019 S CreeP8031219Self 20.1 / mg/L 72.921 / lbs/day
04/16/2019 P CreeP8041619POTW 23 / mg/L 45.845 / lbs/day
Mar 2019 Week 2 20.1 / mg/L 72.921 / lbs/day
Apr 2019 Week 3 23 / mg/L 45.845 / lbs/day
Mar 2019 Average 20.1 / mg/L 72.921 / lbs/day
Apr 2019 Average 23 / mg/L 45.845 / lbs/day
2019 Quarter 1 20.1 / mg/L 72.921 / lbs/day
2019 Quarter 2 23 / mg/L 45.845 / lbs/day
2019 1st 6 Months(Avg) 21.55 / mg/L. 59.383 / lbs/day
2019 1st 6...(Max) 23 / mg/L 72.921 / lbs/day
2019 1st 6...(Min) 20.1 / mg/L 45.845 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
03/12/2019 S CreeP8031219Self < 2.5 / mg/L < /
04/16/2019 P CreeP8041619POTW 5 / mg/L /
Mar 2019 Week 2 < 2.5 / mg/L < /
Apr 2019 Week 3 5 / mg/L /
Mar 2019 Average < 2.5 / mg/L < /
Apr 2019 Average 5 / mg/L /
2019 Quarter 1 < 2.5 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 9

•
Cree, Inc.(All)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
2019 Quarter 2 5 / mg/L /
2019 1st 6 Months(Avg) < 3.75 / mg/L < /
2019 1st 6... Max 5 / mg/L /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
03/12/2019 S CreeP8031219Se1f 8.5 /5.0- 10.5 SU /
04/16/2019 P CreeP8041619POTW 8.3 /5.0- 10.5 SU /
Mar 2019 Week 2 8.5 / SU /
Apr 2019 Week 3 8.3 / SU /
Mar 2019 Average 8.5 / SU /
Apr 2019 Average 8.3 / SU /
2019 Quarter 1 8.5 / SU /
2019 Quarter 2 8.3 / SU /
I 2019 1st 6 Months(Avg) 8.4 / SU /
2019 1st 6...(Max) 8.5 / SU /
2019 1st 6...(Min) 8.3 / SU /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily NI TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
03/12/2019 S CreeP8031219Self < 0.005 / mg/L < 0.01814 / lbs/day
Mar 2019 Week 2 < 0.005 / mg/L < 0.01814 / lbs/day
Mar2019 Average < 0.005 / mg/L < 0.01814 / lbs/day
2019 Quarter 1 < 0.005 / mg/L < 0.01814 / lbs/day
2019 1st 6 Months(Avg) < 0.005 / mg/L < 0.018140 / lbs/day
2019 1st 6...(Max) < 0.005 / mg/L < 0.018140 / lbs/day
2019 1st 6...(Min) < 0.005 / mg/L < 0.018140 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 9

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/12/2019 S CreeP8031219Self < 0.0025 / mg/L < 0.00907 / lbs/day
Mar 2019 Week 2 < 0.0025 / mg/L < 0.00907 / lbs/day
Mar 2019 Average < 0.0025 / mg/L < 0.00907 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.00907 / lbs/day
2019 1st 6 Months(Avg) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Max) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.009070 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
03/12/2019 S CreeP8031219Se1f 17.4 /66 °C /
04/16/2019 P CreeP8041619POTW 19 /66 °C /
Mar 2019 Week 2 17.4 / °C /
Apr 2019 Week 3 19 / °C /
Mar 2019 Average 17.4 / °C /
Apr 2019 Average 19 / °C /
2019 Quarter 1 17.4 / °C /
2019 Quarter 2 19 / °C /
2019 1st 6 Months(Avg) 18.2 / °C /
2019 1st 6...(Max) 19 / °C /
2019 1st 6...(Min) 17.4 / °C /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/24/2019 P CreeP8012419POTW 30.7 / mg/L 68.106 / lbs/day
02/14/2019 P CreeP8021419POTW 29.2 / mg/L 106.178 / lbs/day
03/12/2019 S CreeP8031219Se1f 18.7 / mg/L 67.842 / lbs/day
03/21/2019 P CreeP8032119POTW 23.3 / mg/L 60.823 / lbs/day
04/16/2019 P CreeP8041619POTW 23 / mg/L 45.845 / lbs/day
05/16/2019 P CreeP8051619POTW 21.2 / mg/L 35.185 / lbs/day
06/18/2019 P CreeP8061819POTW 28.4 / mg/L 65.609 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 9

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SwnplelD Result/Limit Mass/Limit
TKN
Jan 2019 Week 4 30.7 / mg/L 68.106 / lbs/day
Feb 2019 Week 2 29.2 / mg/L 106.178 / lbs/day
Mar 2019 Week 2 18.7 / mg/L 67.842 / lbs/day
Mar 2019 Week 3 23.3 / mg/L 60.823 / lbs/day
Apr 2019 Week 3 23 / mg/L 45.845 / lbs/day
May 2019 Week 3 21.2 / mg/L 35.185 / lbs/day
Jun 2019 Week 3 28.4 / mg/L 65.609 / lbs/day
Jan 2019 Average 30.7 / mg/L 68.106 / lbs/day
Feb 2019 Average 29.2 / mg/L 106.178 / lbs/day
Mar 2019 Average 21 / mg/L 64.332 / lbs/day
Apr2019 Average 23 / mg/L 45.845 / lbs/day
May 2019 Average 21.2 / mg/L 35.185 / lbs/day
Jun 2019 Average 28.4 / mg/L 65.609 / lbs/day
2019 Quarter 1 25.48 / mg/L 75.737 / lbs/day
2019 Quarter 2 24.2 / mg/L 48.88 / lbs/day
2019 1st 6 Months(Avg) 24.93 / mg/L 64.227 / lbs/day
2019 1st 6...(Max) 30.7 / mg/L 106.178 / lbs/day
2019 1st 6...(Min) 18.7 / mg/L 35.185 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/24/2019 P CreeP8012419POTW 2.9 / mg/L 6.4335 / lbs/day
02/14/2019 P CreeP8021419POTW 2.09 / mg/L 7.5997 / lbs/day
03/12/2019 S CreeP8031219Self 1.6 / mg/L 5.8046 / lbs/day
03/21/2019 P CreeP8032119POTW 2.57 / mg/L 6.7088 / lbs/day
04/16/2019 P CreeP8041619POTW 2.47 / mg/L 4.9234 / lbs/day
05/16/2019 P CreeP8051619POTW 3.74 / mg/L 6.2071 / lbs/day
06/18/2019 P CreeP8061819POTW 2.49 / mg/L 5.7523 / lbs/day
Jan 2019 Week 4 2.9 / mg/L 6.4335 / lbs/day
Feb 2019 Week 2 2.09 / mg/L 7.5997 / lbs/day
Mar 2019 Week 2 1.6 / mg/L 5.8046 / lbs/day
Mar 2019 Week 3 2.57 / mg/L 6.7088 / lbs/day
Apr 2019 Week 3 2.47 / mg/L 4.9234 / lbs/day
May 2019 Week 3 3.74 / mg/L 6.2071 / lbs/day
Jun 2019 Week 3 2.49 / mg/L 5.7523 / lbs/day
Jan 2019 Average 2.9 / mg/L 6.4335 / lbs/day
Feb 2019 Average 2.09 / mg/L 7.5997 / lbs/day
Mar 2019 Average 2.085 / mg/L 6.2567 / lbs/day
Apr 2019 Average 2.47 / mg/L 4.9234 / lbs/day
May 2019 Average 3.74 / mg/L 6.2071 / lbs/day
Jun 2019 Average 2.49 / mg/L 5.7523 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 9

Cree. Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
2019 Quarter 1 2.29 / mg/L 6.6367 / lbs/day
2019 Quarter 2 2.9 / mg/L 5.6276 / lbs/day
2019 1st 6 Months(Avg) 2.551 / mg/L 6.2042 / lbs/day
2019 1st 6...(Max) 3.74 / mg/L 7.5997 / lbs/day
2019 1st 6...(Min) 1.6 / mg/L 4.9234 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
03/12/2019 S CreeP8031219Self 12.1 / mg/L /
Mar 2019 Week 2 12.1 / mg/L /
Mar 2019 Average 12.1 / mg/L /
2019 Quarter 1 12.1 / mg/L /
2019 1st 6 Months(Avg) 12.1 / mg/L /
2019 1st 6...(Max) 12.1 / mg/L /
2019 1st 6...(Min) 12.1 / mg/L /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/12/2019 S CreeP8031219Self 0.388 / mg/L 1.407625 / lbs/day
Mar 2019 Week 2 0.388 / mg/L 1.407625 / lbs/day
Mar 2019 Average 0.388 / mg/L 1.407625 / lbs/day
2019 Quarter 1 0.388 / mg/L 1.407625 / lbs/day
2019 1st 6 Months(Avg) 0.388 / mg/L 1.40763 / lbs/day
2019 1st 6...(Max) 0.388 / mg/L 1.407625 / lbs/day
2019 1st 6...(Min) 0.388 / mg/L 1.407625 / lbs/day
2019 1st 6...(Count) 1 / 1 /
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S CreeP90119Flow 0.019996 / MGD /
02/28/2019 S CreeP90219Flow 0.022201 / MGD /
03/31/2019 S CreeP90319Flow 0.02835 / MGD /
04/30/2019 S CreeP90419Flow 0.027041 / MGD /
05/31/2019 S CreeP90519Flow 0.0298 / MGD /
06/30/2019 S CreeP90619Flow 0.029292 / MGD /
Jan 2019 Week 4 0.019996 / MGD /
Feb 2019 Week 4 0.022201 / MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 9

Cree. Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Mar 2019 Week 4 0.02835 / MGD /
Apr 2019 Week 4 0.027041 / MGD /
May 2019 Week 4 0.0298 / MGD /
Jun 2019 Week 4 0.029292 / MGD /
Jan 2019 Average 0.019996 / MGD /
Feb 2019 Average 0.022201 / MGD /
Mar 2019 Average 0.02835 / MGD /
Apr 2019 Average 0.027041 / MGD /
May 2019 Average 0.0298 / MGD /
Jun 2019 Average 0.029292 / MGD /
2019 Quarter 1 0.023516 / MGD /
2019 Quarter 2 0.028711 / MGD /
2019 1st 6 Months(Avg) 0.026113 / MGD /
2019 1st 6...(Max) 0.0298 / MGD /
2019 1st 6...(Min) 0.019996 / MGD /
2019 1st 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
03/12/2019 S CreeP9031219Se1f 42.8 / mg/L /
04/16/2019 P CreeP041619POTW 22 / mg/L /
Mar 2019 Week 2 42.8 / mg/L /
Apr 2019 Week 3 22 / mg/L /
Mar 2019 Average 42.8 / mg/L /
Apr 2019 Average 22 / mg/L /
2019 Quarter 1 42.8 / mg/L /
2019 Quarter 2 22 / mg/L /
2019 1st 6 Months(Avg) 32.4 / mg/L /
2019 1st 6...(Max) 42.8 / mg/L /
2019 1st 6...(Min) 22 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/12/2019 S CreeP9031219Se1f 0.034 / mg/L /
Mar 2019 Week 2 0.034 / mg/L /
Mar 2019 Average 0.034 / mg/L /
2019 Quarter 1 0.034 / mg/L /
2019 1st 6 Months(Avg) 0.034 / mg/L /
2019 1st 6...(Max) 0.034 / mg/L /
2019 1st 6...(Min) 0.034 / mg/L /
2019 1st 6...(Count) 1 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page I of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
03/12/2019 S CreeP9031219Self 0.32 / mg/L /
04/16/2019 P CreeP041619POTW < 0.05 / mg/L < /
Mar 2019 Week 2 0.32 / mg/L /
Apr 2019 Week 3 < 0.05 / mg/L < /
Mar 2019 Average 0.32 / mg/L /
Apr 2019 Average < 0.05 / mg/L < /
2019 Quarter 1 0.32 / mg/L /
2019 Quarter 2 < 0.05 / mg/L < /
2019 1st 6 Months(Avg) < 0.19 / mg/L < /
2019 1st 6...(Max) 0.32 / mg/L /
2019 1st 6...(Min) < 0.05 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
03/12/2019 S CreeP9031219Self 0.000012 / mg/L /
04/15/2019 P CreeP9041519POTW 0.000029 / mg/L /
Hg
Mar 2019 Week 2 0.000012 / mg/L /
Apr 2019 Week 3 0.000029 / mg/L /
Mar 2019 Average 0.000012 / mg/L /
Apr 2019 Average 0.000029 / mg/L /
2019 Quarter 1 0.000012 / mg/L /
2019 Quarter 2 0.000029 / mg/L /
2019 1st 6 Months(Avg) 0.000021 / mg/L /
2019 1st 6...(Max) 0.000029 / mg/L /
2019 1st 6...(Min) 0.000012 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/12/2019 S CreeP9031219Se1f < 0.003 / mg/L < /
04/16/2019 P CreeP041619POTW < 0.001 / mg/L < /
Mar 2019 Week 2 < 0.003 / mg/L < /
Apr 2019 Week 3 < 0.001 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < /
Apr 2019 Average < 0.001 / mg/L < /
2019 Quarter 1 < 0.003 / mg/L < /
2019 Quarter 2 < 0.001 / mg/L < /
2019 1st 6 Months(Avg) < 0.002 / mg/L < /
' 2019 1st 6...(Max) < 0.003 / mg/L < /
2019 1st 6...(Min) < 0.001 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall:: 009
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
03/12/2019 S CreeP9031219Se1f 51.4 / mg/L /
04/16/2019 P CreeP041619POTW < 2.5 / mg/L /
Mar 2019 Week 2 51.4 / mg/L /
Apr 2019 Week 3 < 2.5 / mg/L < /
Mar 2019 Average 51.4 / mg/L /
Apr 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 51.4 / mg/L /
2019 Quarter 2 < 2.5 / mg/L < /
2019 1st 6 Months(Avg) < 26.95 / mg/L < /
2019 1st 6...(Max) 51.4 / mg/L /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SatnplelD Result/Limit Mass/Limit
pH
03/12/2019 S CreeP9031219Setf 7.1 /5.0- 10.5 SU /
04/16/2019 P CreeP041619POTW 7.4 /5.0- 10.5 SU /
Mar 2019 Week 2 7.1 / SU /
Apr 2019 Week 3 7.4 / SU /
Mar 2019 Average 7.1 / SU /
Apr 2019 Average 7.4 / SU /
2019 Quarter 1 7.1 / SU /
2019 Quarter 2 7.4 / SU /
2019 1st 6 Months(Avg) 7.25 / SU /
2019 1st 6...(Max) 7.4 / SU /
2019 1st 6...(Min) 7.1 / SU /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
03/12/2019 S CreeP9031219Se1f 20.5 / °C /
04/16/2019 P CreeP041619POTW 19 / °C /
Mar 2019 Week 2 20.5 / °C /
Apr 2019 Week 3 19 / °C /
Mar 2019 Average 20.5 / °C /
Apr2019 Average 19 / °C /
2019 Quarter 1 20.5 / °C /
2019 Quarter 2 19 / °C /
2019 1st 6 Months(Avg) 19.8 / °C /
2019 1st 6...(Max) 20.5 / °C /
2019 1st 6...(Min) 19 / °C /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Ala SA/Limit
TKN
01/24/2019 P CreeP9012419POTW 28.6 / mg/L /
02/14/2019 P CreeP9021419POTW 27.7 / mg/L /
03/21/2019 P CreeP9032119POTW 22.7 / mg/L /
04/16/2019 P CreeP041619POTW 15.5 / mg/L /
05/16/2019 P CreeP9051619POTW 28.7 / mg/L /
06/18/2019 P CreeP9061819POTW 36.7 / mg/L /
Jan 2019 Week 4 28.6 / mg/L /
Feb 2019 Week 2 27.7 / mg/L /
Mar 2019 Week 3 22.7 / mg/L /
Apr 2019 Week 3 15.5 / mg/L /
May 2019 Week 3 28.7 / mg/L /
Jun 2019 Week 3 36.7 / mg/L /
Jan 2019 Average 28.6 / mg/L /
Feb 2019 Average 27.7 / mg/L /
Mar 2019 Average 22.7 / mg/L /
Apr 2019 Average 15.5 / mg/L /
May 2019 Average 28.7 / mg/L /
Jun 2019 Average 36.7 / mg/L /
2019 Quarter 1 26.33 / mg/L /
2019 Quarter 2 26.97 / mg/L /
2019 1st 6 Months(Avg) 26.65 / mg/L /
2019 1st 6...(Max) 36.7 / mg/L /
2019 1st 6...(Min) 15.5 / mg/L /
2019 1st 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/24/2019 P CreeP9012419POTW 3.84 / mg/L /
02/14/2019 P CreeP9021419POTW 3.36 / mg/L /
03/21/2019 P CreeP9032119POTW 2.67 / mg/L /
04/16/2019 P CreeP041619POTW 2.43 / mg/L /
05/16/2019 P CreeP9051619POTW 4.52 / mg/L /
06/18/2019 P CreeP9061819POTW 4.07 / mg/L /
Jan 2019 Week 4 3.84 / mg/L /
Feb 2019 Week 2 3.36 / mg/L /
Mar 2019 Week 3 2.67 / mg/L /
Apr 2019 Week 3 2.43 / mg/L /
May 2019 Week 3 4.52 / mg/L /
Jun 2019 Week 3 4.07 / mg/L /
Jan 2019 Average 3.84 / mg/L /
Feb 2019 Average 3.36 / mg/L /
Mar 2019 Average 2.67 / mg/L /
Apr 2019 Average 2.43 / mg/L /
May 2019 Average 4.52 / mg/L /
Jun 2019 Average 4.07 / mg/L /
2019 Quarter 1 3.29 / mg/L /
2019 Quarter 2 3.673 / mg/L /
2019 1st 6 Months(Avg) 3.482 / mg/L /
2019 1st 6...(Max) 4.52 / mg/L /
2019 1st 6...(Min) 2.43 / mg/L /
2019 1st 6...(Count) 6 / /
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 010
Sample Date SamplelD Result/Limit Mass/Limit
TTO
01/30/2019 P CreeP10013019POTW 0.017 /0.771 mg/L /
03/15/2019 S CreeP10031519SeIf < 0.005 /0.771 mg/L < /
Jan 2019 Week 4 0.017 / mg/L /
Mar 2019 Week 3 < 0.005 / mg/L < /
Jan 2019 Average 0.017 / mg/L /
Mar 2019 Average < 0.005 / mg/L < /
2019 Quarter 1 < 0.011 / mg/L < /
2019 1st 6 Months(Avg) < 0.0110 / mg/L < /
2019 1st 6...(Max) 0.0170 / mg/L /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 5

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 010
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over DailyM: 0 0.00 #Over Mo AvgM: 0 0.00 #Over Wk AvgM: 0 0.00 #Over Qtr AvgM: 0
0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S Cree0119Flow 0.347456 /0.600 MGD /
02/28/2019 S Cree0219Flow 0.380196 /0.600 MGD /
03/31/2019 S Cree0319Flow 0.348587 /0.600 MGD /
04/30/2019 S Cree0419Flow 0.283169 /0.600 MGD /
05/31/2019 S Cree0519F1ow 0.285609 /0.600 MGD /
06/30/2019 S Cree0619Flow 0.312525 /0.600 MGD /
Jan 2019 Week 4 0.347456 / MGD /
Feb 2019 Week 4 0.380196 / MGD /
Mar 2019 Week 4 0.348587 / MGD /
Apr 2019 Week 4 0.283169 / MGD /
May 2019 Week 4 0.285609 / MGD /
Jun 2019 Week 4 0.312525 / MGD /
Jan 2019 Average 0.347456 /0.451 MGD /
Feb 2019 Average 0.380196 /0.451 MGD /
Mar 2019 Average 0.348587 /0.451 MGD /
Apr 2019 Average 0.283169 /0.451 MGD /
May 2019 Average 0.285609 /0.451 MGD /
Jun 2019 Average 0.312525 /0.451 MGD /
2019 Quarter 1 0.358746 / MGD /
2019 Quarter 2 0.293768 / MGD /
2019 1st 6 Months(Avg) 0.326257 / MGD /
2019 1st 6...(Max) 0.380196 / MGD /
2019 1st 6...(Min) 0.283169 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % #
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 1

Cree, Inc.(All1
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample ), e: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
03/12/2019 S Cree031219SeIf 0.66 /8 mg/L /
04/16/2019 P Cree041619POTW 2.5 /8 mg/L /
Mar 2019 Week 2 0.66 / mg/L /
Apr 2019 Week 3 2.5 / mg/L /
Mar 2019 Average 0.66 /7 mg/L /
Apr 2019 Average 2.5 /7 mg/L /
2019 Quarter 1 0.66 / mg/L /
2019 Quarter 2 2.5 / mg/L /
2019 1st 6 Months(Avg) 1.58 / mg/L /
2019 1st 6...(Max) 2.5 / mg/L /
2019 1st 6...(Min) 0.66 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/12/2019 S Cree031219SeIf 0.000002 /0.000142 mg/L /
04/16/2019 P Cree041619POTW 0.000008 /0.000142 mg/L /
Mar 2019 Week 2 0.000002 / mg/L /
Apr 2019 Week 3 0.000008 / mg/L /
Mar 2019 Average 0.000002 / mg/L /
Apr 2019 Average 0.000008 / mg/L /
2019 Quarter 1 0.000002 / mg/L /
2019 Quarter 2 0.000008 / mg/L /
2019 1st 6 Months(Avg) 0.000005 / mg/L /
2019 1st 6...(Max) 0.000008 / mg/L /
2019 1st 6...(Min) 0.000002 / mg/L /
2019 1st 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 2

Cree, Inc.(A11)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: All
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over
e Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
03/12/2019 S Cree031219Self < 2.5 /200 mg/L < /
04/16/2019 P Cree041619POTW < 2.5 /200 mg/L < /
Mar 2019 Week 2 < 2.5 / mg/L < /
Apr 2019 Week 3 < 2.5 / mg/L < /
Mar 2019 Average < 2.5 / mg/L < /
Apr 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 < 2.5 / mg/L < /
2019 Quarter 2 < 2.5 / mg/L < /
2019 1st 6 Months(Avg) < 2.5 / mg/L < /
2019 1st 6...(Max) < 2.5 / mg/L < /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 2

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1 1 2019 To 6'30/2019 Sample Type: Effluent Wastewater Oufall: 011
Sample Date SamplelD Result/Limit Mass/Limit
TTO
02/25/2019 P CreeRTPP11022519P < 0.025 / 1.37 mg/L < /
OTW
Feb 2019 Week 4 < 0.025 / mg/L < /
Feb 2019 Average < 0.025 / mg/L < /
2019 Quarter 1 < 0.025 / mg/L < /
2019 1st 6 Months(Avg) < 0.025 / mg/L < /
2019 1st 6...(Max) < 0.025 / mg/L < /
2019 1st 6...(Min) < 0.025 / mg/L < /
2019 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
03/15/2019 S CreeRTPP12031519Se < 0.025 / mg/L < 0.02353 / lbs/day
If
04/09/2019 S CreeRTPP12040919Se < 0.025 / mg/L < 0.024298 / lbs/day
If
Mar 2019 Week 3 < 0.025 / mg/L < 0.02353 / lbs/day
Apr 2019 Week 2 < 0.025 / mg/L < 0.024298 / lbs/day
Mar 2019 Average < 0.025 / mg/L < 0.02353 / lbs/day
Apr 2019 Average < 0.025 / mg/L < 0.024298 / lbs/day
2019 Quarter 1 < 0.025 / mg/L < 0.02353 / lbs/day
2019 Quarter 2 < 0.025 / mg/L < 0.024298 / lbs/day
2019 1st 6 Months(Avg) < 0.025 / mg/L < 0.023914 / lbs/day
2019 1st 6...(Max) < 0.025 / mg/L < 0.024298 / lbs/day
2019 1st 6...(Min) < 0.025 / mg/L < 0.023530 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
03/15/2019 S CreeRTPP12031519Se 2.6 / mg/L 2.4471 / lbs/day
If
04/16/2019 P CreeRTPP12041619P 2.7 / mg/L /
OTW
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 1

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
Mar 2019 Week 3 2.6 / mg/L 2.4471 / lbs/day
Apr 2019 Week 3 2.7 / mg/L /
Mar 2019 Average 2.6 / mg/L 2.4471 / lbs/day
Apr 2019 Average 2.7 / mg/L /
2019 Quarter I 2.6 / mg/L 2.4471 / lbs/day
2019 Quarter 2 2.7 / mg/L /
2019 1st 6 Months(Avg) 2.65 / mg/L 2.4471 / lbs/day
2019 1st 6...(Max) 2.7 / mg/L 2.4471 / lbs/day
2019 1st 6...(Min) 2.6 / mg/L /
2019 1st 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
03/15/2019 S CreeRTPP12031519Se < 0.0025 / mg/L < 0.002353 / lbs/day
if
04/09/2019 S CreeRTPP12040919Se < 0.0025 / mg/L < 0.00243 / lbs/day
if
Mar 2019 Week 3 < 0.0025 / mg/L < 0.002353 / lbs/day
Apr 2019 Week 2 < 0.0025 / mg/L < 0.00243 / lbs/day
Mar 2019 Average < 0.0025 / mg/L < 0.002353 / lbs/day
Apr 2019 Average < 0.0025 / mg/L < 0.00243 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.002353 / lbs/day
2019 Quarter 2 < 0.0025 / mg/L < 0.00243 / lbs/day
2019 1st 6 Months(Avg) < 0.0025 / mg/L < 0.002391 / lbs/day
2019 1st 6...(Max) < 0.0025 / mg/L < 0.002430 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.002353 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/17/2019 S CreeRTPP120119Flow 0.109076 /0.469 MGD /
02/21/2019 S CreeRTPP120219F1ow 0.11044 /0.469 MGD /
03/22/2019 S CreeRTPP120319Flow 0.112852 /0.469 MGD /
04/18/2019 S CreeRTPP120419F1ow 0.116538 /0.469 MGD /
05/15/2019 S CreeRTPP120519F1ow 0.126902 /0.469 MGD /
06/19/2019 S CreeRTPP120619F1ow 0.138923 /0.469 MGD /
Jan 2019 Week 3 0.109076 / MGD /
Feb 2019 Week 3 0.11044 / MGD /
Mar 2019 Week 4 0.112852 / MGD /
Apr 2019 Week 3 0.116538 / MGD /
May 2019 Week 3 0.126902 / MGD /
Jun 2019 Week 3 0.138923 / MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jan 2019 Average 0.109076 /0.329 MGD /
Feb 2019 Average 0.11044 /0.329 MGD /
Mar 2019 Average 0.112852 /0.329 MGD /
Apr 2019 Average 0.116538 /0.329 MGD /
May 2019 Average 0.126902 /0.329 MGD /
Jun 2019 Average 0.138923 /0.329 MGD /
2019 Quarter 1 0.110789 / MGD /
2019 Quarter 2 0.127454 / MGD /
2019 1st 6 Months(Avg) 0.119122 / MGD /
2019 1st 6...(Max) 0.138923 / MGD /
2019 1st 6...(Min) 0.109076 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Barium
03/15/2019 S CreeRTPP12031519Se 0.026 / mg/L 0.0244 / lbs/day
If
04/09/2019 S CreeRTPP12040919Se 0.028 / mg/L 0.0276 / lbs/day
If
Mar 2019 Week 3 0.026 / mg/L 0.0244 / lbs/day
Apr 2019 Week 2 0.028 / mg/L 0.0276 / lbs/day
Mar 2019 Average 0.026 / mg/L 0.0244 / lbs/day
Apr 2019 Average 0.028 / mg/L 0.0276 / lbs/day
2019 Quarter 1 0.026 / mg/L 0.0244 / lbs/day
2019 Quarter 2 0.028 / mg/L 0.0276 / lbs/day
2019 1st 6 Months(Avg) 0.027 / mg/L 0.0260 / lbs/day
2019 1st 6...(Max) 0.028 / mg/L 0.0276 / lbs/day
2019 1st 6...(Min) 0.026 / mg/L 0.0244 / lbs/day
2019 1st6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/15/2019 S CreeRTPP12031519Se < 0.0025 / mg/L < 0.002353 / lbs/day
If
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
04/09/2019 S CreeRTPP12040919Se < 0.00025 / mg/L < 0.000243 / lbs/day
if
Mar 2019 Week 3 < 0.0025 / mg/L < 0.002353 / lbs/day
Apr 2019 Week 2 < 0.00025 / mg/L < 0.000243 / lbs/day
Mar 2019 Average < 0.0025 / mg/L < 0.002353 / lbs/day
Apr 2019 Average < 0.00025 / mg/L < 0.000243 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.002353 / lbs/day
2019 Quarter 2 < 0.00025 / mg/L < 0.000243 / lbs/day
2019 1st 6 Months(Avg) < 0.00138 / mg/L < 0.001298 / lbs/day
2019 1st 6...(Max) < 0.0025 / mg/L < 0.002353 / lbs/day
2019 1st 6...(Min) < 0.00025 / mg/L < 0.000243 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
03/15/2019 S CreeRTPP12031519Se 86.6 / mg/L 81.5067 / lbs/day
If
04/16/2019 P CreeRTPP12041619P 136 / mg/L /
OTW
Mar 2019 Week 3 86.6 / mg/L 81.5067 / lbs/day
Apr 2019 Week 3 136 / mg/L /
Mar 2019 Average 86.6 / mg/L 81.5067 / lbs/day
Apr 2019 Average 136 / mg/L /
2019 Quarter 1 86.6 / mg/L 81.5067 / lbs/day
2019 Quarter 2 136 / mg/L /
2019 1st 6 Months(Avg) 111.3 / mg/L 81.5067 / lbs/day
2019 1st 6...(Max) 136 / mg/L 81.5067 / lbs/day
2019 1st 6...(Min) 86.6 / mg/L /
2019 1st 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Lintit
Chromium
03/15/2019 S CreeRTPP12031519Se < 0.001 / mg/L < 0.001176 / lbs/day
If
04/09/2019 S CreeRTPP12040919Se < 0.001 / mg/L < 0.001215 / lbs/day
If
Mar 2019 Week 3 < 0.001 / mg/L < 0.001176 / lbs/day
Apr 2019 Week 2 < 0.001 / mg/L < 0.001215 / lbs/day
Mar 2019 Average < 0.001 / mg/L < 0.001176 / lbs/day
Apr 2019 Average < 0.001 / mg/L < 0.001215 / lbs/day
2019 Quarter 1 < 0.001 / mg/L < 0.001176 / lbs/day
2019 Quarter 2 < 0.001 / mg/L < 0.001215 / lbs/day
2019 1st 6 Months(Avg) < 0.001 / mg/L < 0.001196 / lbs/day
2019 1st 6...(Max) < 0.001 / mg/L < 0.001215 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 14

r
Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfa11: 012
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
2019 1st 6...(Min) < 0.001 / mg/L < 0.001176 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/15/2019 S CreeRTPP12031519Se 0.041 / mg/L 0.038777 / lbs/day
If
04/09/2019 S CreeRTPP12040919Se 0.015 / mg/L 0.014482 / lbs/day
If
Mar 2019 Week 3 0.041 / mg/L 0.038777 / lbs/day
Apr 2019 Week 2 0.015 / mg/L 0.014482 / lbs/day
Mar 2019 Average 0.041 / mg/L 0.038777 / lbs/day
Apr 2019 Average 0.015 / mg/L 0.014482 / lbs/day
2019 Quarter 1 0.041 / mg/L 0.038777 / lbs/day
2019 Quarter 2 0.015 / mg/L 0.014482 / lbs/day
2019 1st 6 Months(Avg) 0.028 / mg/L 0.026629 / lbs/day
2019 1st 6...(Max) 0.041 / mg/L 0.038777 / lbs/day
2019 1st 6...(Min) 0.015 / mg/L 0.014482 / lbs/day
2019 1st6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/15/2019 S CreeRTPP12011519Se < 0.004 / mg/L < 0.003639 /0.05 lbs/day
If
01/28/2019 S CreeRTPP12012819Se < 0.004 / mg/L < 0.003639 / 0.05 lbs/day
If
02/15/2019 S CreeRTPP12021519Se < 0.004 / mg/L < 0.003684 /0.05 lbs/day
If
02/26/2019 S CreeRTPP12022619Se < 0.004 / mg/L < 0.003684 /0.05 lbs/day
If
03/15/2019 S CreeRTPP12031519Se < 0.004 / mg/L < 0.003765 /0.05 lbs/day
if
03/25/2019 S CreeRTPP12032519Se < 0.004 / mg/L < 0.003765 /0.05 lbs/day
If
04/09/2019 S CreeRTPP12040919Se < 0.004 / mg/L < 0.003888 /0.05 lbs/day
if
04/16/2019 P CreeRTPP12041619P < 0.003 / mg/L < /0.05
OTW
04/22/2019 S CreeRTPP12042219Se < 0.004 / mg/L < 0.003888 /0.05 lbs/day
If
05/02/2019 S CreeRTPP12050219Se < 0.004 / mg/L < 0.004233 /0.05 lbs/day
If
05/31/2019 S CreeRTPP12053119Se < 0.004 / mg/L < 0.004233 /0.05 lbs/day
If
06/14/2019 S CreeRTPP12061419Se < 0.004 / mg/L < 0.004634 /0.05 lbs/day
If
06/28/2019 S CreeRTPP12062819Se < 0.004 / mg/L < 0.004634 /0.05 lbs/day
If
Monday,February 17,2020 *Indicates Violation •*Indicates TRC Violation Page 4 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Jan 2019 Week 3 < 0.004 / mg/L < 0.003639 / lbs/day
Jan 2019 Week 4 < 0.004 / mg/L < 0.003639 / lbs/day
Feb 2019 Week 3 < 0.004 / mg/L < 0.003684 / lbs/day
Feb 2019 Week 4 < 0.004 / mg/L < 0.003684 / lbs/day
Mar 2019 Week 3 < 0.004 / mg/L < 0.003765 / lbs/day
Mar 2019 Week 4 < 0.004 / mg/L < 0.003765 / lbs/day
Apr 2019 Week 2 < 0.004 / mg/L < 0.003888 / lbs/day
Apr 2019 Week 3 < 0.003 / mg/L < /
Apr 2019 Week 4 < 0.004 / mg/L < 0.003888 / lbs/day
May 2019 Week 1 < 0.004 / mg/L < 0.004233 / lbs/day
May 2019 Week 4 < 0.004 / mg/L < 0.004233 / lbs/day
Jun 2019 Week 2 < 0.004 / mg/L < 0.004634 / lbs/day
Jun 2019 Week 4 < 0.004 / mg/L < 0.004634 / lbs/day
Jan 2019 Average < 0.004 / mg/L < 0.003639 / lbs/day
Feb 2019 Average < 0.004 / mg/L < 0.003684 / lbs/day
Mar 2019 Average < 0.004 / mg/L < 0.003765 / lbs/day
Apr 2019 Average < 0.004 / mg/L < 0.003888 / lbs/day
May 2019 Average < 0.004 / mg/L < 0.004233 / lbs/day
Jun 2019 Average < 0.004 / mg/L < 0.004634 / lbs/day
2019 Quarter 1 < 0.004 / mg/L < 0.003696 / lbs/day
2019 Quarter 2 < 0.004 / mg/L < 0.004252 / lbs/day
2019 1st 6 Months(Avg) < 0.004 / mg/L < 0.003974 / lbs/day
2019 1st 6...(Max) < 0.004 / mg/L < 0.004634 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 13 / 12 /
Sample Count: 13 Months Sampled: 6 Weeks Sampled: 13 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
03/15/2019 S CreeRTPP12031519Se 0.74 /8.0 mg/L 0.6965 / lbs/day
if
04/16/2019 P CreeRTPP12041619P 2.22 /8.0 mg/L /
OTW
Mar 2019 Week 3 0.74 / mg/L 0.6965 / lbs/day
Apr 2019 Week 3 2.22 / mg/L /
Mar 2019 Average 0.74 /7.0 mg/L 0.6965 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Apr 2019 Average 2.22 /7.0 mg/L /
2019 Quarter 1 0.74 / mg/L 0.6965 / lbs/day
2019 Quarter 2 2.22 / mg/L /
2019 1st 6 Months(Avg) 1.48 / mg/L 0.6965 / lbs/day
2019 1st 6...(Max) 2.22 / mg/L 0.6965 / lbs/day
2019 1st 6...(Min) 0.74 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
03/15/2019 S CreeRTPP12031519Se < 0.0013 / mg/L < 0.001176 / lbs/day
If
04/09/2019 S CreeRTPP12040919Se < 0.0013 / mg/L < 0.001215 / lbs/day
If
Mar 2019 Week 3 < 0.0013 / mg/L < 0.001176 / lbs/day
Apr 2019 Week 2 < 0.0013 / mg/L < 0.001215 / lbs/day
Mar 2019 Average < 0.0013 / mg/L < 0.001176 / lbs/day
Apr2019 Average < 0.0013 / mg/L < 0.001215 / lbs/day
2019 Quarter 1 < 0.0013 / mg/L < 0.001176 / lbs/day
2019 Quarter 2 < 0.0013 / mg/L < 0.001215 / lbs/day
2019 1st 6 Months(Avg) < 0.0013 / mg/L < 0.001196 / lbs/day
2019 1st 6...(Max) < 0.0013 / mg/L < 0.001215 / lbs/day
2019 1st 6...(Min) < 0.0013 / mg/L < 0.001176 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/15/2019 S CreeRTPP12031519Se 0.000001 /0.000142 mg/L /
if
04/09/2019 S CreeRTPP12040919Se < 0.000001 /0.000142 mg/L < /
if
04/16/2019 P CreeRTPP12041619P 0.000041 /0.000142 mg/L /
OTW
Mar 2019 Week 3 0.000001 / mg/L /
Apr 2019 Week 2 < 0.000001 / mg/L < /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Apr 2019 Week 3 0.000041 / mg/L /
Mar 2019 Average 0.000001 / mg/L /
Apr 2019 Average < 0.000021 / mg/L /
2019 Quarter 1 0.000001 / mg/L /
2019 Quarter 2 < 0.000021 / mg/L /
2019 1st 6 Months(Avg) < 0.000014 / mg/L < /
2019 1st 6...(Max) 0.000041 / mg/L /
2019 1st 6...(Min) < 0.000001 / mg/L < /
2019 1st 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 2 Weeks Sampled: 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/15/2019 S CreeRTPP12031519Se < 0.001 / mg/L < 0.0012 / lbs/day
if
04/09/2019 S CreeRTPP12040919Se < 0.001 / mg/L < 0.0012 / lbs/day
If
04/16/2019 P CreeRTPP12041619P < 0.001 / mg/L < /
OTW
Mar 2019 Week 3 < 0.001 / mg/L < 0.0012 / lbs/day
Apr 2019 Week 2 < 0.001 / mg/L < 0.0012 / lbs/day
Apr 2019 Week 3 < 0.001 / mg/L < /
Mar 2019 Average < 0.001 / mg/L < 0.0012 / lbs/day
Apr 2019 Average < 0.001 / mg/L < 0.0012 / lbs/day
2019 Quarter 1 < 0.001 / mg/L < 0.0012 / lbs/day
2019 Quarter 2 < 0.001 / mg/L < 0.0012 / lbs/day
2019 1st 6 Months(Avg) < 0.001 / mg/L < 0.0012 / lbs/day
2019 1st 6...(Max) < 0.001 / mg/L < 0.0012 / lbs/day
2019 1st 6...(Min) < 0.001 / mg/L < /
2019 1st 6...(Count) 3 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
03/15/2019 S CreeRTPP12031519Se < 0.0013 / . mg/L < 0.001176 / lbs/day
If
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
04/09/2019 S CreeRTPP12040919Se < 0.0013 / mg/L < 0.001215 / lbs/day
If
Mar 2019 Week 3 < 0.0013 / mg/L < 0.001176 / lbs/day
Apr 2019 Week 2 < 0.0013 / mg/L < 0.001215 / lbs/day
Mar 2019 Average < 0.0013 / mg/L < 0.001176 / lbs/day
Apr 2019 Average < 0.0013 / mg/L < 0.001215 / lbs/day
2019 Quarter 1 < 0.0013 / mg/L < 0.001176 / lbs/day
2019 Quarter 2 < 0.0013 / mg/L < 0.001215 / lbs/day
2019 1st 6 Months(Avg) < 0.0013 / mg/L < 0.001196 / lbs/day
2019 1st 6...(Max) < 0.0013 / mg/L < 0.001215 / lbs/day
2019 1st 6...(Min) < 0.0013 / mg/L < 0.001176 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SampleID Result/Limit Mass/Limit
Nitrate-Nitrite
03/15/2019 S CreeRTPP12031519Se 9 / mg/L 8.471 / lbs/day
If
04/16/2019 P CreeRTPP12041619P 2.8 / mg/L /
OTW
Mar 2019 Week 3 9 / mg/L 8.471 / lbs/day
Apr 2019 Week 3 2.8 / mg/L /
Mar 2019 Average 9 / mg/L 8.471 / lbs/day
Apr 2019 Average 2.8 / mg/L /
2019 Quarter 1 9 / mg/L 8.471 / lbs/day
2019 Quarter 2 2.8 / mg/L /
2019 1st 6 Months(Avg) 5.9 / mg/L 8.471 / lbs/day
2019 1st 6...(Max) 9 / mg/L 8.471 / lbs/day
2019 1st 6...(Min) 2.8 / mg/L /
2019 1st 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
03/15/2019 S CreeRTPP12031519Se 18.6 / mg/L 17.506 / lbs/day
if
04/16/2019 P CreeRTPP12041619P 11.2 / mg/L /
OTW
Mar 2019 Week 3 18.6 / mg/L 17.506 / lbs/day
Apr 2019 Week 3 11.2 / mg/L /
Mar 2019 Average 18.6 / mg/L 17.506 / lbs/day
Apr 2019 Average 11.2 / mg/L /
2019 Quarter 1 18.6 / mg/L 17.506 / lbs/day
2019 Quarter 2 11.2 / mg/L /
2019 1st 6 Months(Avg) 14.9 / mg/L 17.506 / lbs/day
2019 1st 6...(Max) 18.6 / mg/L 17.506 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
2019 1st 6...(Min) 11.2 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
03/15/2019 S CreeRTPP12031519Se < 2.5 /200 mg/L < /
if
04/16/2019 P CreeRTPP12041619P < 2.5 /200 mg/L < /
OTW
Mar 2019 Week 3 < 2.5 / mg/L < /
Apr 2019 Week 3 < 2.5 / mg/L < /
Mar 2019 Average < 2.5 / mg/L < /
Apr 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 < 2.5 / mg/L < /
2019 Quarter 2 < 2.5 / mg/L < /
2019 1st 6 Months(Avg) < 2.5 / mg/L < /
2019 1st 6...(Max) < 2.5 / mg/L < /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/15/2019 S CreeRTPP12011519Se 7.1 /5.0- 10.5 SU /
if
01/28/2019 S CreeRTPP12012819Se 7.1 /5.0- 10.5 SU /
if
02/15/2019 S CreeRTPP12021519Se 7.4 /5.0- 10.5 SU /
if
02/26/2019 S CreeRTPP12022619Se 7.4 /5.0- 10.5 SU /
if
03/15/2019 S CreeRTPP12031519Se 8.9 /5.0- 10.5 SU /
If
03/25/2019 S CreeRTPP12032519Se 7 /5.0- 10.5 SU /
if
04/09/2019 S CreeRTPP12040919Se 6.5 /5.0- 10.5 SU /
if
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Lima
pH
04/16/2019 P CreeRTPP12041619P 7.3 /5.0- 10.5 SU /
OTW
04/22/2019 S CreeRTPP12042219Se 8.9 /5.0- 10.5 SU /
If
05/02/2019 S CreeRTPP12050219Se 7.1 /5.0- 10.5 SU /
If
05/31/2019 S CreeRTPP12053119Se 6.6 /5.0- 10.5 SU /
If
Jan 2019 Week 3 7.1 / SU /
Jan 2019 Week 4 7.1 / SU /
Feb 2019 Week 3 7.4 / SU /
Feb 2019 Week 4 7.4 / SU /
Mar 2019 Week 3 8.9 / SU /
I Mar 2019 Week 4 7 / SU /
Apr 2019 Week 2 6.5 / SU /
Apr 2019 Week 3 7.3 / SU /
Apr 2019 Week 4 8.9 / SU /
May 2019 Week 1 7.1 / SU /
May 2019 Week 4 6.6 / SU /
Jan 2019 Average 7.1 / SU /
Feb 2019 Average 7.4 / SU /
Mar 2019 Average 7.95 / SU /
Apr 2019 Average 7.57 / SU /
May 2019 Average 6.85 / SU /
2019 Quarter 1 7.48 / SU /
2019 Quarter 2 7.28 / SU /
2019 1st 6 Months(Avg) 7.39 / SU /
2019 1st 6...(Max) 8.9 / SU /
2019 1st 6...(Min) 6.5 / SU /
2019 l st 6...(Count) 11 / /
Sample Count: 11 Months Sampled: 5 Weeks Sampled : 11 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily : 0 0.00
#Under Daily TRC: 0 0.00
Sample Dale SamplelD Result/Limit Mass/Limit
Selenium
03/15/2019 S CreeRTPP12031519Se < 0.0025 / mg/L < 0.002353 / lbs/day
if
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfal1: 012
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
04/09/2019 S CreeRTPP12040919Se < 0.005 / mg/L < 0.00486 / lbs/day
if
Mar 2019 Week 3 < 0.0025 / mg/L < 0.002353 / lbs/day
Apr 2019 Week 2 < 0.005 / mg/L < 0.00486 / lbs/day
Mar 2019 Average < 0.0025 / mg/L < 0.002353 / lbs/day
Apr 2019 Average < 0.005 / mg/L < 0.00486 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.002353 / lbs/day
2019 Quarter 2 < 0.005 / mg/L < 0.00486 / lbs/day
2019 1st 6 Months(Avg) < 0.0038 / mg/L < 0.003606 / lbs/day
2019 1st 6...(Max) < 0.005 / mg/L < 0.004860 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.002353 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/15/2019 S CreeRTPP12031519Se < 0.0013 / mg/L < 0.001176 / lbs/day
If
04/09/2019 S CreeRTPP12040919Se < 0.0013 / mg/L < 0.001215 / lbs/day
If
Mar 2019 Week 3 < 0.0013 / mg/L < 0.001176 / lbs/day
Apr 2019 Week 2 < 0.0013 / mg/L < 0.001215 / lbs/day
Mar 2019 Average < 0.0013 / mg/L < 0.001176 / lbs/day
Apr 2019 Average < 0.0013 / mg/L < 0.001215 / lbs/day
2019 Quarter 1 < 0.0013 / mg/L ,< 0.001176 / lbs/day
2019 Quarter 2 < 0.0013 / mg/L < 0.001215 / lbs/day
2019 1st 6 Months(Avg) < 0.0013 / mg/L < 0.001196 / lbs/day
2019 1st 6...(Max) < 0.0013 / mg/L < 0.001215 / lbs/day
2019 1st 6...(Min) < 0.0013 / mg/L < 0.001176 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Dale SamplelD Result/Limit Mass/Limit
Temperature
01/15/2019 S CreeRTPP12011519Se 16.7 /66 °C /
te
01/28/2019 S CreeRTPP12012819Se 17.8 /66 °C /
If
02/15/2019 S CreeRTPP12021519Se 19.4 /66 °C /
If
02/26/2019 S CreeRTPP12022619Se 19.6 /66 °C /
if
03/15/2019 S CreeRTPPI2031519Se 21.4 /66 °C /
if
03/25/2019 S CreeRTPP12032519Se 18.9 /66 °C /
If
04/09/2019 S CreeRTPP12040919Se 18.9 /66 °C /
if
Monday,February 17,2020 *Indicates Violation ••Indicates TRC Violation Page 11 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
04/16/2019 P CreeRTPP12041619P 17 /66 °C /
OTW
04/22/2019 S CreeRTPP12042219Se 19.6 /66 °C /
If
05/02/2019 S CreeRTPP12050219Se 21.7 /66 °C /
ff
05/31/2019 S CreeRTPP12053119Se 24.8 /66 °C /
If
Jan 2019 Week 3 16.7 / °C /
Jan 2019 Week 4 17.8 / °C /
Feb 2019 Week 3 19.4 / °C /
Feb 2019 Week 4 19.6 / °C /
Mar 2019 Week 3 21.4 / °C /
Mar 2019 Week 4 18.9 / °C /
Apr 2019 Week 2 18.9 / °C /
Apr 2019 Week 3 17 / °C /
Apr 2019 Week 4 19.6 / °C /
May 2019 Week 1 21.7 / °C /
May 2019 Week 4 24.8 / °C /
Jan 2019 Average 17.3 / °C /
Feb 2019 Average 19.5 / °C /
Mar 2019 Average 20.2 / °C /
Apr 2019 Average 18.5 / °C /
May 2019 Average 23.3 / °C /
2019 Quarter 1 19 / °C /
2019 Quarter 2 20.4 / °C /
2019 1st 6 Months(Avg) 19.6 / °C /
2019 1st 6...(Max) 24.8 / °C /
2019 1st 6...(Min) 16.7 / °C /
2019 1st 6...(Count) 11 / /
Sample Count: 11 Months Sampled: 5 Weeks Sampled: 11 Quarters Sampled: 2
# % # % # % #
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
03/15/2019 S CreeRTPP12031519Se 9.5 / mg/L 8.941 / lbs/day
ff
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 12 of 14

Cree. Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall:: 012
Sample Date SamplelD Result/Limit Mass/Limit
TKN
04/16/2019 P CreeRTPP12041619P 8.35 / mg/L /
OTW
Mar 2019 Week 3 9.5 / mg/L 8.941 / lbs/day
Apr 2019 Week 3 8.35 / mg/L /
Mar 2019 Average 9.5 / mg/L 8.941 / lbs/day
Apr 2019 Average 8.35 / mg/L /
2019 Quarter 1 9.5 / mg/L 8.941 / lbs/day
2019 Quarter 2 8.35 / mg/L /
2019 1st 6 Months(Avg) 8.93 / mg/L 8.941 / lbs/day
2019 1st 6...(Max) 9.5 / mg/L 8.941 / lbs/day
2019 1st 6...(Min) 8.35 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
03/15/2019 S CreeRTPP12031519Se 1.8 / mg/L 1.6941 / lbs/day
if
04/16/2019 P CreeRTPP12041619P 1.87 / mg/L /
OTW
Mar 2019 Week 3 1.8 / mg/L 1.6941 / lbs/day
Apr 2019 Week 3 1.87 / mg/L /
Mar 2019 Average 1.8 / mg/L 1.6941 / lbs/day
Apr 2019 Average 1.87 / mg/L /
2019 Quarter 1 1.8 / mg/L 1.6941 / lbs/day
2019 Quarter 2 1.87 / mg/L /
2019 1st 6 Months(Avg) 1.835 / mg/L 1.6941 / lbs/day
2019 1st 6...(Max) 1.87 / mg/L 1.6941 / lbs/day
2019 1st 6...(Min) 1.8 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
03/15/2019 S CreeRTPP12031519Se 0.844 / mg/L /
8'
04/09/2019 S CreeRTPP12040919Se 0.0025 / mg/L /
ff
Mar 2019 Week 3 0.844 / mg/L /
Apr 2019 Week 2 0.0025 / mg/L /
Mar 2019 Average 0.844 / mg/L /
Apr 2019 Average 0.0025 / mg/L /
2019 Quarter 1 0.844 / mg/L /
2019 Quarter 2 0.0025 / mg/L /
2019 1st 6 Months(Avg) 0.4233 / mg/L /
2019 1st 6...(Max) 0.844 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 13 of 14

Cree, Inc.(RTP)
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
VOC
2019 1st 6...(Min) 0.0025 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/15/2019 S CreeRTPP12031519Se 0.758 / mg/L 0.713419 / lbs/day
if
04/09/2019 S CreeRTPP12040919Se 0.239 / mg/L 0.232291 / lbs/day
If
Mar 2019 Week 3 0.758 / mg/L 0.713419 / lbs/day
Apr 2019 Week 2 0.239 / mg/L 0.232291 / lbs/day
Mar2019 Average 0.758 / mg/L 0.713419 / lbs/day
Apr2019 Average 0.239 / mg/L 0.232291 / lbs/day
2019 Quarter 1 0.758 / mg/L 0.713419 / lbs/day
2019 Quarter 2 0.239 / mg/L 0.232291 / lbs/day
2019 1st 6 Months(Avg) 0.499 / mg/L 0.472855 / lbs/day
2019 1st 6...(Max) 0.758 / mg/L 0.713419 / lbs/day
2019 1st 6...(Min) 0.239 / mg/L 0.232291 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 14 of 14

JMC (USA). Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
02/11/2019 S JMCO21119Self 0.109 / mg/L 0.000329 / lbs/day
Feb 2019 Week 2 0.109 / mg/L 0.000329 / lbs/day
Feb 2019 Average 0.109 / mg/L 0.000329 / lbs/day
2019 • Quarter 1 0.109 / mg/L 0.000329 / lbs/day
2019 1st 6 Months(Avg) 0.109 / mg/L 0.000329 / lbs/day
2019 1st 6...(Max) 0.109 / mg/L 0.000329 / lbs/day
2019 1st 6...(Min) 0.109 / mg/L 0.000329 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/11/2019 S JMCO21119Self 2.8 / mg/L 0.0085 / lbs/day
05/28/2019 P JMC052819POTW 4.4 / mg/L 0.0431 / lbs/day
Feb 2019 Week 2 2.8 / mg/L 0.0085 / lbs/day
May 2019 Week 4 4.4 / mg/L 0.0431 / lbs/day
Feb 2019 Average 2.8 / mg/L 0.0085 / lbs/day
May 2019 Average 4.4 / mg/L 0.0431 / lbs/day
2019 Quarter 1 2.8 / mg/L 0.0085 / lbs/day
2019 Quarter 2 4.4 / mg/L 0.0431 / lbs/day
2019 1st 6 Months(Avg) 3.6 / mg/L 0.0258 / lbs/day
2019 1st 6...(Max) 4.4 / mg/L 0.0431 / lbs/day
2019 1st 6...(Min) 2.8 / mg/L 0.0085 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S JMC0119F1ow 0.000318 / MGD /
02/28/2019 S JMCO219Flow 0.000205 / MGD /
03/31/2019 S JMC0319Flow 0.000268 / MGD /
04/30/2019 S JMC0419Flow 0.000203 / MGD /
05/31/2019 S JMC0519Flow 0.000317 / MGD /
06/30/2019 S JMC0619Flow 0.000284 / MGD /
Jan 2019 Week 4 0.000318 / MGD /
Feb 2019 Week 4 0.000205 / MGD /
Mar 2019 Week 4 0.000268 / MGD /
Apr 2019 Week 4 0.000203 / MGD /
May 2019 Week 4 0.000317 / MGD /
Jun 2019 Week 4 0.000284 / MGD /
Jan 2019 Average 0.000318 /0.01 MGD /
Feb 2019 Average 0.000205 /0.01 MGD /
Mar 2019 Average 0.000268 /0.01 MGD /
Apr 2019 Average 0.000203 /0.01 MGD /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
May 2019 Average 0.000317 /0.01 MGD /
Jun 2019 Average 0.000284 /0.01 MGD /
2019 Quarter 1 0.000264 / MGD /
2019 Quarter 2 0.000268 / MGD /
2019 1st 6 Months(Avg) 0.000266 / MGD /
2019 1st 6...(Max) 0.000318 / MGD /
2019 1st 6...(Min) 0.000203 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/11/2019 S JMCO21119Se1f < 0.00008 /0.04 mg/L < 0 / lbs/day
05/28/2019 P JMC052819POTW < 0.00008 /0.04 mg/L < 0.000001 / lbs/day
Feb 2019 Week 2 < 0.00008 / mg/L < 0 / lbs/day
May 2019 Week 4 < 0.00008 / mg/L < 0.000001 / lbs/day
Feb 2019 Average < 0.00008 /0.025 mg/L < 0 / lbs/day
May 2019 Average < 0.00008 /0.025 mg/L < 0.000001 / lbs/day
2019 Quarter 1 < 0.00008 / mg/L < 0 / lbs/day
2019 Quarter 2 < 0.00008 / mg/L < 0.000001 / lbs/day
2019 1st 6 Months(Avg) < 0.00008 / mg/L < 0.000000 / lbs/day
2019 1st 6...(Max) < 0.00008 / mg/L < 0.000001 / lbs/day
2019 1st 6...(Min) < 0.00008 / mg/L < 0.000000 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/11/2019 S JMCO21119Self 2450 / mg/L 7.3967 / lbs/day
05/28/2019 P JMC052819POTW 2370 / mg/L 23.2406 / lbs/day
Feb 2019 Week 2 2450 / mg/L 7.3967 / lbs/day
May 2019 Week 4 2370 / mg/L 23.2406 / lbs/day
Feb 2019 Average 2450 / mg/L 7.3967 / lbs/day
May 2019 Average 2370 / mg/L 23.2406 / lbs/day
2019 Quarter 1 2450 / mg/L 7.3967 / lbs/day
2019 Quarter 2 2370 / mg/L 23.2406 / lbs/day
2019 1st 6 Months(Avg) 2410 / mg/L 15.3187 / lbs/day
2019 1st 6...(Max) 2450 / mg/L 23.2406 / lbs/day
2019 1st 6...(Min) 2370 / mg/L 7.3967 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
1 02/11/2019 S JMCO21119Self 0.054 / I mg/L 0.000163 / lbs/day
05/28/2019 P JMC052819POTW 0.062 / I mg/L 0.000609 / lbs/day
Feb 2019 Week 2 0.054 / mg/L 0.000163 / lbs/day
May 2019 Week 4 0.062 / mg/L 0.000609 / lbs/day
Feb 2019 Average 0.054 /0.650 mg/L 0.000163 / lbs/day
May 2019 Average 0.062 /0.650 mg/L 0.000609 / lbs/day
2019 Quarter 1 0.054 / mg/L 0.000163 / lbs/day
2019 Quarter 2 0.062 / mg/L 0.000609 / lbs/day
2019 1st 6 Months(Avg) 0.058 / mg/L 0.000386 / lbs/day
2019 1st 6...(Max) 0.062 / mg/L 0.000609 / lbs/day
2019 1st 6...(Min) 0.054 / mg/L 0.000163 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/11/2019 S JMCO21119Self 0.103 / 1 mg/L 0.000311 / lbs/day
05/28/2019 P JMC052819POTW 0.019 / 1 mg/L 0.000184 / lbs/day
Feb 2019 Week 2 0.103 / mg/L 0.000311 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
May 2019 Week 4 0.019 / mg/L 0.000184 / lbs/day
Feb 2019 Average 0.103 /0.7 mg/L 0.000311 / lbs/day
May 2019 Average 0.019 /0.7 mg/L 0.000184 / lbs/day
2019 Quarter 1 0.103 / mg/L 0.000311 / lbs/day
2019 Quarter 2 0.019 / mg/L 0.000184 / lbs/day
2019 1st 6 Months(Avg) 0.061 / mg/L 0.000248 / lbs/day
2019 1st 6...(Max) 0.103 / mg/L 0.000311 / lbs/day
2019 1st 6...(Min) 0.019 / mg/L 0.000184 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/11/2019 S JMCO21119Self < 0.003 /0.04 mg/L < 0.000008 / lbs/day
05/28/2019 P JMC052819POTW < 0.003 /0.04 mg/L < 0.000025 / lbs/day
Feb 2019 Week 2 < 0.003 / mg/L < 0.000008 / lbs/day
May 2019 Week 4 < 0.003 / mg/L < 0.000025 / lbs/day
Feb 2019 Average < 0.003 /0.03 mg/L < 0.000008 / lbs/day
May 2019 Average < 0.003 /0.03 mg/L < 0.000025 / lbs/day
2019 Quarter 1 < 0.003 / mg/L < 0.000008 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.000025 / lbs/day
2019 1st 6 Months(Avg) < 0.003 / mg/L < 0.000016 / lbs/day
2019 1st 6...(Max) < 0.003 / mg/L < 0.000025 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < 0.000008 / lbs/day
2019 1st6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/11/2019 S JMCO21119Self < 0.05 / mg/L < 0.0002 / lbs/day
05/28/2019 P JMC052819POTW 0.52 / mg/L 0.0051 / lbs/day
Feb 2019 Week 2 < 0.05 / mg/L < 0.0002 / lbs/day
May 2019 Week 4 0.52 / mg/L 0.0051 / lbs/day
Feb 2019 Average < 0.05 / mg/L < 0.0002 / lbs/day
May 2019 Average 0.52 / mg/L 0.0051 / lbs/day
2019 Quarter 1 < 0.05 / mg/L < 0.0002 / lbs/day
2019 Quarter 2 0.52 / mg/L 0.0051 / lbs/day
2019 1st 6 Months(Avg) < 0.29 / mg/L < 0.0026 / lbs/day
2019 1st 6...(Max) 0.52 / mg/L 0.0051 / lbs/day
2019 1st 6...(Min) < 0.05 / mg/L < 0.0002 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
02/11/2019 S JMCO21119Se1f 0.0041 /0.260 mg/L 0.000012 / lbs/day
05/28/2019 P JMC052819POTW 0.0051 /0.260 mg/L 0.00005 / lbs/day
Feb 2019 Week 2 0.0041 / mg/L 0.000012 / lbs/day
May 2019 Week 4 0.0051 / mg/L 0.00005 / lbs/day
Feb 2019 Average 0.0041 /0.160 mg/L 0.000012 / lbs/day
May 2019 Average 0.0051 /0.164 mg/L 0.00005 / lbs/day
2019 Quarter 1 0.0041 / mg/L 0.000012 / lbs/day
2019 Quarter 2 0.0051 / mg/L 0.00005 / lbs/day
2019 1st 6 Months(Avg) 0.0046 / mg/L 0.000031 / lbs/day
2019 1st 6...(Max) 0.0051 / mg/L 0.000050 / lbs/day
2019 1st 6...(Min) 0.0041 / mg/L 0.000012 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
1 #Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/12/2019 S JMCO21219SelfHg 0.000027 /0.000142 mg/L /
05/29/2019 P JMC052919POTWHg 0.000007 /0.000142 mg/L /
Feb 2019 Week 2 0.000027 / mg/L /
•
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
May 2019 Week 4 0.000007 / mg/L /
Feb 2019 Average 0.000027 / mg/L /
May 2019 Average 0.000007 / mg/L /
2019 Quarter 1 0.000027 / mg/L /
2019 Quarter 2 0.000007 / mg/L /
2019 1st 6 Months(Avg) 0.000017 / mg/L /
2019 1st 6...(Max) 0.000027 / mg/L /
2019 1st 6...(Min) 0.000007 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
05/28/2019 P JMC052819POTW 0 / mg/L 0 / lbs/day
May 2019 Week 4 0 / mg/L 0 / lbs/day
May 2019 Average 0 / mg/L 0 / lbs/day
2019 Quarter 2 0 / mg/L 0 / lbs/day
2019 1st 6 Months(Avg) 0.003 / mg/L 0.0000 / lbs/day
2019 1st 6...(Max) 0.003 / mg/L 0.0000 / lbs/day
2019 1st 6...(Min) 0.003 / mg/L 0.0000 / lbs/day
2019 1st 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
02/11/2019 S JMCO21119Self 0.0085 /0.3 mg/L 0.000026 / lbs/day
05/28/2019 P JMC052819POTW 0.0007 /0.3 mg/L 0.000007 / lbs/day
Feb 2019 Week 2 0.0085 / mg/L 0.000026 / lbs/day
May 2019 Week 4 0.0007 / mg/L 0.000007 / lbs/day
Feb 2019 Average 0.0085 /0.2 mg/L 0.000026 / lbs/day
May 2019 Average 0.0007 /0.2 mg/L 0.000007 / lbs/day
2019 Quarter 1 0.0085 / mg/L 0.000026 / lbs/day
2019 Quarter 2 0.0007 / mg/L 0.000007 / lbs/day
2019 1st 6 Months(Avg) 0.0046 / mg/L 0.000016 / lbs/day
2019 1st 6...(Max) 0.0085 / mg/L 0.000026 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2019 1st 6...(Min) 0.0007 / mg/I, 0.000007 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/11/2019 S JMCO21119Self 102 / mg/L 0.308 / lbs/day
05/28/2019 P JMC052819POTW 51.1 / mg/L 0.501 / lbs/day
Feb 2019 Week 2 102 / mg/L 0.308 / lbs/day
May 2019 Week 4 51.1 / mg/L 0.501 / lbs/day
Feb 2019 Average 102 / mg/L 0.308 / lbs/day
May 2019 Average 51.1 / mg/L 0.501 / lbs/day
2019 Quarter 1 102 / mg/L 0.308 / lbs/day
2019 Quarter 2 51.1 / mg/L 0.501 / lbs/day
2019 1st 6 Months(Avg) 76.6 / mg/L 0.405 / lbs/day
2019 1st 6...(Max) 102 / mg/L 0.501 / lbs/day
2019 1st 6...(Min) 51.1 / mg/L 0.308 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/11/2019 S JMCO21119Self 107 / mg/L 0.323 / lbs/day
05/28/2019 P JMC052819POTW 56.4 / mg/L 0.553 / lbs/day
Feb 2019 Week 2 107 / mg/L 0.323 / lbs/day
May 2019 Week 4 56.4 / mg/L 0.553 / lbs/day
Feb 2019 Average 107 / mg/L 0.323 / lbs/day
May 2019 Average 56.4 / mg/L 0.553 / lbs/day
2019 Quarter 1 107 / mg/L 0.323 / lbs/day
2019 Quarter 2 56.4 / mg/L 0.553 / lbs/day
2019 1st 6 Months(Avg) 81.7 / mg/L 0.438 / lbs/day
2019 1st 6...(Max) 107 / mg/L 0.553 / lbs/day
2019 1st 6...(Min) 56.4 / mg/L 0.323 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/11/2019 S JMCO21119Se1f < 2.5 /200 mg/L < /
05/28/2019 P JMC052819POTW < 2.5 /200 mg/L < /
Feb 2019 Week 2 < 2.5 / mg/L < /
May 2019 Week 4 < 2.5 / mg/L < /
Feb 2019 Average < 2.5 / mg/L < /
May 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 < 2.5 / mg/L < /
2019 Quarter 2 < 2.5 / mg/L < /
2019 1st 6 Months(Avg) < 2.5 / mg/L < /
2019 1st 6...(Max) < 2.5 / mg/L < /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/11/2019 S JMCO21119SeIf 8.1 /6- 10.5 SU /
02/12/2019 S JMCO21219SelfHg 8.1 /6- 10.5 SU /
05/28/2019 P JMC052819POTW 7.5 /6- 10.5 SU /
Feb 2019 Week 2 8.1 / SU /
May 2019 Week 4 7.5 / SU /
Feb 2019 Average 8.1 / SU /
May 2019 Average 7.5 / SU /
2019 Quarter 1 8.1 / SU /
2019 Quarter 2 7.5 / SU /
2019 1st 6 Months(Avg) 7.9 / SU /
2019 1st 6...(Max) 8.1 / SU /
2019 1st 6...(Min) 7.5 / SU /
2019 1st 6...(Count) 3 / /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater O110l1: 001
Sample Count: 3 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
02/11/2019 S JMCO21119Se1f < 0.0003 /0.160 mg/L < 0.000001 / lbs/day
05/28/2019 P JMC052819POTW < 0.0003 /0.160 mg/L < 0.000002 / lbs/day
Feb 2019 Week 2 < 0.0003 / mg/L < 0.000001 / lbs/day
May 2019 Week 4 < 0.0003 / mg/L < 0.000002 / lbs/day
Feb 2019 Average < 0.0003 /0.090 mg/L < 0.000001 / lbs/day
May 2019 Average < 0.0003 /0.090 mg/L < 0.000002 / lbs/day
2019 Quarter 1 < 0.0003 / mg/L < 0.000001 / lbs/day
2019 Quarter 2 < 0.0003 / mg/L < 0.000002 / lbs/day
2019 1st 6 Months(Avg) < 0.0003 / mg/L < 0.000002 / lbs/day
2019 1st 6...(Max) < 0.0003 / mg/L < 0.000002 / lbs/day
2019 1st 6...(Min) < 0.0003 / mg/L < 0.000001 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/11/2019 S JMCO21119Se1f 12 /66 °C /
05/28/2019 P JMC052819POTW 32 /66 °C /
Feb 2019 Week 2 12 / °C /
May 2019 Week 4 32 / °C /
Feb 2019 Average 12 / °C /
May 2019 Average 32 / °C /
2019 Quarter 1 12 / °C /
2019 Quarter 2 32 / °C /
2019 1st 6 Months(Avg) 22 / °C /
2019 1st 6...(Max) 32 / °C /
2019 1st 6...(Min) 12 / °C /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/11/2019 S JMCO21119Self 5.04 / mg/L 0.015 / lbs/day
05/28/2019 P JMC052819POTW 5.28 / mg/L 0.052 / lbs/day
Feb 2019 Week 2 5.04 / mg/L 0.015 / lbs/day
May 2019 Week 4 5.28 / mg/L 0.052 / lbs/day
Feb 2019 Average 5.04 / mg/L 0.015 / lbs/day
May 2019 Average 5.28 / mg/L 0.052 / lbs/day
2019 Quarter 1 5.04 / mg/L 0.015 / lbs/day
2019 Quarter 2 5.28 / mg/L 0.052 / lbs/day
2019 1st 6 Months(Avg) 5.16 / mg/L 0.033 / lbs/day
2019 1st 6...(Max) 5.28 / mg/L 0.052 / lbs/day
2019 1st 6...(Min) 5.04 / mg/L 0.015 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/11/2019 S JMCO21119Self 0.072 / mg/L 0.0002 / lbs/day
05/28/2019 P JMC052819POTW 0.027 / mg/L 0.0003 / lbs/day
Feb 2019 Week 2 0.072 / mg/L 0.0002 / lbs/day
May 2019 Week 4 0.027 / mg/L 0.0003 / lbs/day
Feb 2019 Average 0.072 / mg/L 0.0002 / lbs/day
May 2019 Average 0.027 / mg/L 0.0003 / lbs/day
2019 Quarter 1 0.072 / mg/L 0.0002 / lbs/day
2019 Quarter 2 0.027 / mg/L 0.0003 / lbs/day
2019 1st 6 Months(Avg) 0.050 / mg/L 0.0002 / lbs/day
2019 1st 6...(Max) 0.072 / mg/L 0.0003 / lbs/day
2019 1st 6...(Min) 0.027 / mg/L 0.0002 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/11/2019 S JMCO21119Self 0.195 /0.9 mg/L 0.000589 / lbs/day
05/28/2019 P JMC052819POTW 0.049 /0.9 mg/L 0.000478 / lbs/day
Feb 2019 Week 2 0.195 / mg/L 0.000589 / lbs/day
May 2019 Week 4 0.049 / mg/L 0.000478 / lbs/day
Feb 2019 Average 0.195 /0.56 mg/L 0.000589 / lbs/day
May 2019 Average 0.049 /0.56 mg/L 0.000478 / lbs/day
2019 Quarter 1 0.195 / mg/L 0.000589 / lbs/day
2019 Quarter 2 0.049 / mg/L 0.000478 / lbs/day
2019 1st 6 Months(Avg) 0.122 / mg/L 0.000533 / lbs/day
2019 1st 6...(Max) 0.195 / mg/L 0.000589 / lbs/day
2019 1st 6...(Min) 0.049 / mg/L 0.000478 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 11 of 11

Micross Advanced Interconnect Technology.LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
P P
Ammonia
01/18/2019 S Micross011819Self 3.4 / mg/L 0.481 / lbs/day
03/28/2019 P Micross032819POTW 9.3 / mg/L 2.6242 / lbs/day
Jan 2019 Week 3 3.4 / mg/L 0.481 / lbs/day
Mar 2019 Week 4 9.3 / mg/L 2.6242 / lbs/day
Jan 2019 Average 3.4 / mg/L 0.481 / lbs/day
Mar 2019 Average 9.3 / mg/L 2.6242 / lbs/day
2019 Quarter 1 6.35 / mg/L 1.5526 / lbs/day
2019 1st 6 Months(Avg) 6.35 / mg/L 1.5526 / lbs/day
2019 1st 6...(Max) 9.3 / mg/L 2.6242 / lbs/day
2019 1st 6...(Min) 3.4 / mg/L 0.4810 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S Micross0119Flow 0.020156 /0.100 MGD /
02/28/2019 S Micross0219Flow 0.021663 /0.100 MGD /
03/31/2019 S Micross0319FIow 0.024757 /0.100 MGD /
04/30/2019 S Micross0419Flow 0.03001 /0.100 MGD /
05/31/2019 S Micross0519Flow 0.042725 /0.100 MGD /
06/30/2019 S Micross0619Flow 0.047782 /0.100 MGD /
Jan 2019 Week 4 0.020156 / MGD /
Feb 2019 Week 4 0.021663 / MGD /
Mar 2019 Week 4 0.024757 / MGD /
Apr 2019 Week 4 0.03001 / MGD /
May 2019 Week 4 0.042725 / MGD /
Jun 2019 Week 4 0.047782 / MGD I
Jan 2019 Average 0.020156 /0.075 MGD /
Feb 2019 Average 0.021663 /0.075 MGD /
Mar 2019 Average 0.024757 /0.075 MGD /
Apr 2019 Average 0.03001 /0.075 MGD /
May 2019 Average 0.042725 /0.075 MGD /
Jun 2019 Average 0.047782 /0.075 MGD /
2019 Quarter 1 0.022192 / MGD /
2019 Quarter 2 0.040172 / MGD /
2019 1st 6 Months(Avg) 0.031182 / MGD /
2019 1st 6...(Max) 0.047782 / MGD /
2019 1st 6...(Min) 0.020156 / MGD /
2019 1st 6...(Count) 6 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
% # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
01/18/2019 S Micross011819Self < 0.0005 / mg/L < 0.000071 / lbs/day
03/28/2019 P Micross032819POTW < 0.0001 / mg/L < 0.000028 / lbs/day
Jan 2019 Week 3 < 0.0005 / mg/L < 0.000071 / lbs/day
Mar 2019 Week 4 < 0.0001 / mg/L < 0.000028 / lbs/day
Jan 2019 Average < 0.0005 / mg/L < 0.000071 / lbs/day
Mar 2019 Average < 0.0001 / mg/L < 0.000028 / lbs/day
2019 Quarter 1 < 0.0003 / mg/L < 0.000049 / lbs/day
2019 1st 6 Months(Avg) < 0.0003 / mg/L < 0.000049 / lbs/day
2019 1st 6...(Max) < 0.0005 / mg/L < 0.000071 / lbs/day
2019 1st 6...(Min) < 0.0001 / mg/L < 0.000028 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
01/18/2019 S Micross011819Self 20 / mg/L 2.8294 / lbs/day
03/28/2019 P Micross032819POTW 37 / mg/L 10.4402 / lbs/day
Jan 2019 Week 3 20 / mg/L 2.8294 / lbs/day
Mar 2019 Week 4 37 / mg/L 10.4402 / lbs/day
Jan 2019 Average 20 / mg/L 2.8294 / lbs/day
Mar 2019 Average 37 / mg/L 10.4402 / lbs/day
2019 Quarter 1 28.5 / mg/L 6.6348 / lbs/day
2019 1st 6 Months(Avg) 28.5 / mg/L 6.6348 / lbs/day
2019 1st 6...(Max) 37 / mg/L 10.4402 / lbs/day
2019 1st 6...(Min) 20 / mg/L 2.8294 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
01/18/2019 S Micross011819Self 0.02 / mg/L 0.002829 / lbs/day
03/28/2019 P Micross032819POTW 0.042 / mg/L 0.01171 / lbs/day
Jan 2019 Week 3 0.02 / mg/L 0.002829 / lbs/day
Mar 2019 Week 4 0.042 / mg/L 0.01171 / lbs/day
Jan 2019 Average 0.02 / mg/L 0.002829 / lbs/day
Wednesday,February 26,2020 *Indicates Violation "Indicates TRC Violation Page 2 of 10

Micros Advanced Interconnect Technology. LLC 1
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall.• '001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Mar 2019 Average 0.042 / mg/L 0.01171 / lbs/day
2019 Quarter 1 0.031 / mg/L 0.00727 / lbs/day
2019 1st 6 Months(Avg) 0.031 / mg/L 0.007270 / lbs/day
2019 1st 6...(Max) 0.042 / mg/L 0.011710 / lbs/day
2019 1st 6...(Min) 0.02 / mg/L 0.002829 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
01/18/2019 S Micross011819Self < 0.002 / mg/L < 0.000347 / lbs/day
03/28/2019 P Micross032819POTW < 0.003 / mg/L < 0.000705 / lbs/day
Jan 2019 Week 3 < 0.002 / mg/L < 0.000347 / lbs/day
Mar 2019 Week 4 < 0.003 / mg/L < 0.000705 / lbs/day
Jan 2019 Average < 0.002 / mg/L < 0.000347 / lbs/day
Mar 2019 Average < 0.003 / mg/L < 0.000705 / lbs/day
2019 Quarter 1 < 0.002 / mg/L < 0.000526 / lbs/day
2019 1st 6 Months(Avg) < 0.002 / mg/L < 0.000526 / lbs/day
2019 1st 6...(Max) < 0.003 / mg/L < 0.000705 / lbs/day
2019 1st 6...(Min) < 0.002 / mg/L < 0.000347 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
01/18/2019 S Micross011819Self 0.88 /8 mg/L 0.1245 / lbs/day
03/28/2019 P Micross032819POTW 1.53 /8 mg/L 0.4317 / lbs/day
Jan 2019 Week 3 0.88 / mg/L 0.1245 / lbs/day
Mar 2019 Week 4 1.53 / mg/L 0.4317 / lbs/day
Jan 2019 Average 0.88 /6 mg/L 0.1245 / lbs/day
Mar 2019 Average 1.53 /6 mg/L 0.4317 / lbs/day
2019 Quarter 1 1.21 / mg/L 0.2781 / lbs/day
2019 1st 6 Months(Avg) 1.21 / mg/L 0.2781 / lbs/day
2019 1st 6...(Max) 1.53 / mg/L 0.4317 / lbs/day
2019 1st6...(Min) 0.88 / mg/L 0.1245 / lbs/day
2019 1st 6...(Count) 2 / 2 / •
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of I

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
01/18/2019 S Micross011819Self < 0.005 / mg/L < 0.000707 / lbs/day
03/28/2019 P Micross032819POTW < 0.005 / mg/L < 0.001411 / lbs/day
Jan 2019 Week 3 < 0.005 / mg/L < 0.000707 / lbs/day
Mar 2019 Week 4 < 0.005 / mg/L < 0.001411 / lbs/day
Jan 2019 Average < 0.005 / mg/L < 0.000707 / lbs/day
Mar2019 Average < 0.005 / mg/L < 0.001411 / lbs/day
2019 Quarter 1 < 0.005 / mg/L < 0.001059 / lbs/day
2019 1st 6 Months(Avg) < 0.005 / mg/L < 0.001059 / lbs/day
2019 1st 6...(Max) < 0.005 / mg/L < 0.001411 / lbs/day
2019 1st 6...(Min) < 0.005 / mg/L < 0.000707 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
01/17/2019 S Micross011719SelfHg 0.000008 /0.000142 mg/L /
03/28/2019 P Micross032819POTW 0.000003 /0.000142 mg/L /
Hg
06/10/2019 P Micross061019POTW 0.000007 /0.000142 mg/L /
Hg
Jan 2019 Week 3 0.000008 / mg/L /
Mar 2019 Week 4 0.000003 / mg/L /
Jun 2019 Week 2 0.000007 / mg/L /
Jan 2019 Average 0.000008 / mg/L /
Mar 2019 Average 0.000003 / mg/L /
Jun 2019 Average 0.000007 / mg/L /
2019 Quarter 1 0.000006 / mg/L /
2019 Quarter 2 0.000007 / mg/L /
2019 1st 6 Months(Avg) 0.000006 / mg/L /
2019 1st 6...(Max) 0.000008 / mg/L /
2019 1st 6...(Min) 0.000003 / mg/L /
2019 1st 6...(Count) 3 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 10

•
Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenu m
01/18/2019 S Micross011819Self 0.039 / mg/L 0.0055 / lbs/day
03/28/2019 P Micross032819POTW 0.034 / mg/L 0.0095 / lbs/day
Jan 2019 Week 3 0.039 / mg/L 0.0055 / lbs/day
Mar 2019 Week 4 0.034 / mg/L 0.0095 / lbs/day
Jan 2019 Average 0.039 / mg/L 0.0055 / lbs/day
Mar 2019 Average 0.034 / mg/L 0.0095 / lbs/day
2019 Quarter 1 0.036 / mg/L 0.0075 / lbs/day
2019 1st 6 Months(Avg) 0.036 / mg/L 0.0075 / lbs/day
2019 1st 6...(Max) 0.039 / mg/L 0.0095 / lbs/day
2019 1st 6...(Min) 0.034 / mg/L 0.0055 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/18/2019 S Micross011819Self 0.0261 / mg/L 0.003692 / lbs/day
03/28/2019 P Micross032819POTW 0.0023 / mg/L 0.000641 / lbs/day
Jan 2019 Week 3 0.0261 / mg/L 0.003692 / lbs/day
Mar 2019 Week 4 0.0023 / mg/L 0.000641 / lbs/day
Jan 2019 Average 0.0261 / mg/L 0.003692 / lbs/day
Mar 2019 Average 0.0023 / mg/L 0.000641 / lbs/day
2019 Quarter 1 0.0142 / mg/L 0.002166 / lbs/day
2019 1st 6 Months(Avg) 0.0142 / mg/L 0.002166 / lbs/day
2019 1st 6...(Max) 0.0261 / mg/L 0.003692 / lbs/day
2019 1st 6...(Min) 0.0023 / mg/L 0.000641 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
01/18/2019 S Micross011819Self 0.7 / mg/L 0.093 / lbs/day
03/28/2019 P Micross032819POTW 0.9 / mg/L 0.26 / lbs/day
Jan 2019 Week 3 0.7 / mg/L 0.093 / lbs/day
Mar 2019 Week 4 0.9 / mg/L 0.26 / lbs/day
Jan 2019 Average 0.7 / mg/L 0.093 / lbs/day
Wednesday,February 26,2020 *Indicates Violation "Indicates TRC Violation Page 5 of 10

Micross Advanced Interconnect Technology.LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Ou all. '001
P �
Sample Date SumplelD Result/Limit Mass/Limit
Nitrate-Nitrite
Mar 2019 Average 0.9 / mg/L 0.26 / lbs/day
2019 Quarter 1 0.8 / mg/L 0.176 / lbs/day
2019 1st 6 Months(Avg) 0.8 / mg/L 0.176 / lbs/day
2019 1st 6...(Max) 0.9 / mg/L 0.260 / lbs/day
2019 1st 6... Min 0.7 / mg/L0.093lbs/day
) /
2019 1st 6...(Count) 2 / 2 /
Sample Date SumplelD Result/Limit Mass/Limit
Nitrogen,Total
01/18/2019 S Micross011819Self 10.66 / mg/L 1.508 / lbs/day
03/28/2019 P Micross032819POTW 19 / mg/L 5.361 / lbs/day
Jan 2019 Week 3 10.66 / mg/L 1.508 / lbs/day
Mar 2019 Week 4 19 / mg/L 5.361 / lbs/day
Jan 2019 Average 10.66 / mg/L 1.508 / lbs/day
Mar 2019 Average 19 / mg/L 5.361 / lbs/day
2019 Quarter 1 14.83 / mg/L 3.435 / lbs/day
2019 1st 6 Months(Avg) 14.83 / mg/L 3.435 / lbs/day
2019 1st 6...(Max) 19 / mg/L 5.361 / lbs/day
2019 1st 6...(Min) 10.66 / mg/L 1.508 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
01/18/2019 S Micross011819Self 36.8 /200 mg/L /
03/28/2019 P Micross032819POTW < 2.5 /200 mg/L < /
Jan 2019 Week 3 36.8 / mg/L /
Mar 2019 Week 4 < 2.5 / mg/L /
Jan 2019 Average 36.8 / mg/L /
Mar 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 < 19.65 / mg/L < /
2019 1st 6 Months(Avg) < 19.65 / mg/L < /
2019 1st 6...(Max) 36.8 / mg/L /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/18/2019 S Micross011819Self 8.3 /5.5-10.5 SU /
03/28/2019 P Micross032819POTW 8.4 /5.5- 10.5 SU /
Jan 2019 Week 3 8.3 / SU /
Mar 2019 Week 4 8.4 / SU /
Jan 2019 Average 8.3 / SU /
Mar 2019 Average 8.4 / SU /
2019 Quarter 1 8.35 / SU /
2019 1st 6 Months(Avg) 8.35 / SU /
2019 1st 6...(Max) 8.4 / SU /
2019 1st 6...(Min) 8.3 / SU /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
01/18/2019 S Micross011819Self < 0.001 / mg/L < 0.000134 / lbs/day
03/28/2019 P Micross032819POTW < 0.0003 / mg/L < 0.000071 / lbs/day
Jan 2019 Week 3 < 0.001 / mg/L < 0.000134 / lbs/day
Mar 2019 Week 4 < 0.0003 / mg/L < 0.000071 / lbs/day
Jan 2019 Average < 0.001 / mg/L < 0.000134 / lbs/day
Mar 2019 Average < 0.0003 / mg/L < 0.000071 / lbs/day
2019 Quarter 1 < 0.0006 / mg/L < 0.000102 / lbs/day
2019 1st 6 Months(Avg) < 0.0006 / mg/L < 0.000102 / lbs/day
2019 1st 6...(Max) < 0.0010 / mg/L < 0.000134 / lbs/day
2019 1st 6...(Min) < 0.0003 / mg/L < 0.000071 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 10

•
Micross Advanced Intorconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/18/2019 S Micross011819Self 15.2 /66 °C /
03/28/2019 P Micross032819POTW 18 /66 °C /
Jan 2019 Week 3 15.2 / °C /
Mar 2019 Week 4 18 / °C /
Jan 2019 Average 15.2 / °C /
Mar2019 Average 18 / °C /
2019 Quarter 1 16.6 / °C /
2019 1st 6 Months(Avg) 16.6 / °C /
2019 1st 6...(Max) 18 / °C /
2019 1st 6...(Min) 15.2 / °C /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tin
01/18/2019 S Micross011819Self < 0.005 / mg/L < 0.000707357 / lbs/day
03/28/2019 P Micross032819POTW < 0.013 / mg/L < 0.003527090 / lbs/day
Jan 2019 Week 3 < 0.005 / mg/L < 0 / lbs/day
Mar 2019 Week 4 < 0.013 / mg/L < 0 / lbs/day
Jan 2019 Average < 0.005 / mg/L < 0 / lbs/day
Mar 2019 Average < 0.013 / mg/L < 0 / lbs/day
2019 Quarter 1 < 0.009 / mg/L < 0 / lbs/day
2019 1st 6 Months(Avg) < 0.009 / mg/L < 0 / lbs/day
2019 1st 6...(Max) < 0.013 / mg/L < 0 / lbs/day
2019 1st 6...(Min) < 0.005 / mg/L < 0 / lbs/day
2019 lst6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
01/18/2019 S Micross011819Self I0 / mg/L 1.415 / lbs/day
03/28/2019 P Micross032819POTW 18.1 / mg/L 5.107 / lbs/day
Jan 2019 Week 3 I 0 / mg/L 1.415 / lbs/day
Mar 2019 Week 4 18.1 / mg/L 5.107 / lbs/day
Jan 2019 Average I0 / mg/L 1.415 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 10

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
Mar 2019 Average 18.1 / mg/L 5.107 / lbs/day
2019 Quarter 1 14.05 / mg/L 3.261 / lbs/day
2019 1st 6 Months(Avg) 14.05 / mg/L 3.261 / lbs/day
2019 1st 6...(Max) 18.1 / mg/L 5.107 / lbs/day
2019 1st 6...(Min) 10 / mg/L 1.415 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
01/18/2019 S Micross011819Self 1.7 / mg/L 0.2405 / lbs/day
03/28/2019 P Micross032819POTW 3.01 / mg/L 0.8493 / lbs/day
Jan 2019 Week 3 1.7 / mg/L 0.2405 / lbs/day
Mar 2019 Week 4 3.01 / mg/L 0.8493 / lbs/day
Jan 2019 Average 1.7 / mg/L 0.2405 / lbs/day
Mar 2019 Average 3.01 / mg/L 0.8493 / lbs/day
2019 Quarter 1 2.355 / mg/L 0.5449 / lbs/day
2019 1st 6 Months(Avg) 2.355 / mg/L 0.5449 / lbs/day
2019 1st 6...(Max) 3.01 / mg/L 0.8493 / lbs/day
2019 1st 6...(Min) 1.7 / mg/L 0.2405 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
01/18/2019 S Micross011819Self 0.307 / mg/L /
Jan 2019 Week 3 0.307 / mg/L /
Jan 2019 Average 0.307 / mg/L /
2019 Quarter 1 0.307 / mg/L /
2019 1st 6 Months(Avg) 0.307 / mg/L /
2019 1st 6...(Max) 0.307 / mg/L /
2019 1st 6...(Min) 0.307 / mg/L /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
01/18/2019 S Micross011819Self 0.49 / mg/L 0.069321 / lbs/day
03/28/2019 P Micross032819POTW 0.381 / mg/L 0.107506 / lbs/day
Jan 2019 Week 3 0.49 / mg/L 0.069321 / lbs/day
Mar 2019 Week 4 0.381 / mg/L 0.107506 / lbs/day
Jan 2019 Average 0.49 / mg/L 0.069321 / lbs/day
Mar 2019 Average 0.381 / mg/L 0.107506 / lbs/day
2019 Quarter 1 0.436 / mg/L 0.088413 / lbs/day
Wednesday,February 26,2020 *Indicates Violation ••Indicates TRC Violation Page 9 of 10

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•
Novan, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
03/15/2019 S Novan031519Se1f 0.447 / mg/L /
Mar 2019 Week 3 0.447 / mg/L /
Mar 2019 Average 0.447 / mg/L /
2019 Quarter 1 0.447 / mg/L /
2019 1st 6 Months(Avg) 0.447 / mg/L /
2019 1st 6...(Max) 0.447 / mg/L /
2019 1st 6...(Min) 0.447 / mg/L /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S Novan0119Flow 0.00046 / MGD /
02/28/2019 S Novan0219Flow 0.000514 / MGD /
03/31/2019 S Novan0319Flow 0.000462 / MGD /
04/30/2019 S Novan0419F1ow 0.00034 / MGD /
05/31/2019 S Novan0519Flow 0.00047 / MGD /
06/30/2019 S Novan0619Flow 0.000406 / MGD /
Jan 2019 Week 4 0.00046 / MGD /
Feb 2019 Week 4 0.000514 / MGD /
Mar 2019 Week 4 0.000462 / MGD /
Apr 2019 Week 4 0.00034 / MGD /
May 2019 Week 4 0.00047 / MGD /
Jun 2019 Week 4 0.000406 / MGD /
Jan 2019 Average 0.00046 / MGD /
Feb 2019 Average 0.000514 / MGD /
Mar 2019 Average 0.000462 / MGD /
Apr 2019 Average 0.00034 / MGD /
May 2019 Average 0.00047 / MGD /
Jun 2019 Average 0.000406 / MGD /
2019 Quarter 1 0.000479 / MGD /
2019 Quarter 2 0.000405 / MGD /
2019 1st 6 Months(Avg) 0.000442 / MGD /
2019 1st 6...(Max) 0.000514 / MGD /
2019 1st 6...(Min) 0.00034 / MGD /
2019 1st 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
03/15/2019 S Novan031519Self < 0.001 / mg/L < /
Mar 2019 Week 3 < 0.001 / mg/L < /
Mar 2019 Average < 0.001 / mg/L < /
2019 Quarter 1 < 0.001 / mg/L < /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 6

Novan. Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
2019 1st 6 Months(Avg) < 0.001 / mg/L < /
2019 1st 6...(Max) < 0.001 / mg/L < /
2019 1st 6...(Min) < 0.001 / mg/L < /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
03/15/2019 S Novan031519SeIf 786 / mg/L /
05/01/2019 P Novan050119POTW 1990 / mg/L /
Mar 2019 Week 3 786 / mg/L /
May 2019 Week 1 1990 / mg/L /
Mar 2019 Average 786 / mg/L /
May 2019 Average 1990 / mg/L /
2019 Quarter 1 786 / mg/L /
2019 Quarter 2 1990 / mg/L /
2019 1st 6 Months(Avg) 1388 / mg/L /
2019 1st 6...(Max) 1990 / mg/L /
2019 1st 6...(Min) 786 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
03/15/2019 S Novan031519Self 0.146 / mg/L /
05/01/2019 P Novan050119POTW 0.099 / mg/L /
Mar 2019 Week 3 0.146 / mg/L /
May 2019 Week 1 0.099 / mg/L /
Mar 2019 Average 0.146 / mg/L /
May 2019 Average 0.099 / mg/L /
2019 Quarter 1 0.146 / mg/L /
2019 Quarter 2 0.099 / mg/L /
2019 1st 6 Months(Avg) 0.123 / mg/L /
2019 1st 6...(Max) 0.146 / mg/L /
2019 1st 6...(Min) 0.099 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
03/15/2019 S Novan031519Self Ig 0.000007 /0.000142 mg/L /
05/01/2019 P Novan050119POTWH 0.000029 /0.000142 mg/L /
g
Mar 2019 Week 3 0.000007 / mg/L /
May 2019 Week 1 0.000029 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 6

Novan, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Mar 2019 Average 0.000007 / mg/L /
May 2019 Average 0.000029 / mg/L /
2019 Quarter 1 0.000007 / mg/L /
2019 Quarter 2 0.000029 / mg/L /
2019 1st 6 Months(Avg) 0.000018 / mg/L /
2019 1st 6...(Max) 0.000029 / mg/L /
2019 1st 6...(Min) 0.000007 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
03/15/2019 S Novan031519Se1f < 0.003 / mg/L < /
Mar 2019 Week 3 < 0.003 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < /
2019 Quarter 1 < 0.003 / mg/L < /
2019 1st 6 Months(Avg) < 0.003 / mg/L < /
2019 1st 6...(Max) < 0.003 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
03/15/2019 S Novan031519Self < 0.003 / mg/L < /
Mar 2019 Week 3 < 0.003 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < /
2019 Quarter 1 < 0.003 / mg/L < /
2019 1st 6 Months(Avg) < 0.003 / mg/L < /
2019 1st 6...(Max) < 0.003 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 6

Novan, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
1 pH
03/15/2019 S Novan031519Self 7.1 /6.0- 10.0 SU /
05/01/2019 P Novan050119POTW 8 /6.0- 10.0 SU /
Mar 2019 Week 3 7.1 / SU /
May 2019 Week 1 8 / SU /
Mar 2019 Average 7.1 / SU /
May 2019 Average 8 / SU /
2019 Quarter 1 7.1 / SU /
2019 Quarter 2 8 / SU /
2019 1st 6 Months(Avg) 7.55 / SU /
2019 l st 6...(Max) 8 / SU /
2019 1st 6...(Min) 7.1 / SU /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
03/15/2019 S Novan031519Se1f < 0.0025 / mg/L < /
Mar 2019 Week 3 < 0.0025 / mg/L < /
Mar 2019 Average < 0.0025 / mg/L < /
2019 Quarter 1 < 0.0025 / mg/L < /
2019 1st 6 Months(Avg) < 0.0025 / mg/L < /
2019 1st 6...(Max) < 0.0025 / mg/L < /
2019 1st 6...(Min) < 0.0025 / mg/L < /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
03/15/2019 S Novan031519Self 23 /66 °C /
05/01/2019 P Novan050119POTW 28 /66 °C /
Mar 2019 Week 3 23 / °C /
May 2019 Week 1 28 / °C /
Mar 20.19 Average 23 / °C /
May 2019 Average 28 / °C /
2019 Quarter 1 23 / °C /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 6

Novan, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2019 Quarter 2 28 / °C /
2019 1st 6 Months(Avg) 25.5 / °C /
2019 1st 6...(Max) 28 / °C /
2019 1st 6...(Min) 23 / °C /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
03/15/2019 S Novan031519Se1f 13 / mg/L /
05/01/2019 P Novan050119POTW 24.1 / mg/L /
Mar 2019 Week 3 13 / mg/L /
May 2019 Week 1 24.1 / mg/L /
Mar 2019 Average 13 / mg/L /
May 2019 Average 24.1 / mg/L /
2019 Quarter 1 13 / mg/L /
2019 Quarter 2 24.1 / mg/L /
2019 1st 6 Months(Avg) 18.55 / mg/L /
2019 1st 6...(Max) 24.1 / mg/L /
2019 1st 6...(Min) 13 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
03/15/2019 S Novan031519Se1f 1.302 / mg/L /
Mar 2019 Week 3 1.302 / mg/L /
Mar 2019 Average 1.302 / mg/L /
2019 Quarter 1 1.302 / mg/L /
2019 1st 6 Months(Avg) 1.302 / mg/L /
2019 1st 6...(Max) 1.302 / mg/L /
2019 1st 6...(Min) 1.302 / mg/L /
2019 1st 6...(Count) 1 / /
Monday,February I7,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 6

Novan, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
03/15/2019 S Novan031519Se1f 0.481 / mg/L /
Mar 2019 Week 3 0.481 / mg/L /
Mar 2019 Average 0.481 / mg/L /
2019 Quarter 1 0.481 / mg/L /
2019 1st 6 Months(Avg) 0.481 / mg/L /
2019 1st 6...(Max) 0.481 / mg/L /
2019 1st 6...(Min) 0.481 / mg/L /
2019 1st 6...(Count) 1 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 6

Phononic
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S Phononic0119Flow 0.006171 / MGD /
02/28/2019 S Phononic0219F1ow 0.012204 / MGD /
03/31/2019 S Phononic0319Flow 0.007673 / MGD /
04/30/2019 S Phononic0419F1ow 0.015157 / MGD /
05/31/2019 S Phononic0519F1ow 0.01408 / MGD /
06/30/2019 S Phononic0619Flow 0.014578 / MGD /
Jan 2019 Week 4 0.006171 / MGD /
Feb 2019 Week 4 0.012204 / MGD /
Mar 2019 Week 4 0.007673 / MGD /
Apr 2019 Week 4 0.015157 / MGD /
May 2019 Week 4 0.01408 / MGD /
Jun 2019 Week 4 0.014578 / MGD /
Jan 2019 Average 0.006171 /0.020 MGD /
Feb 2019 Average 0.012204 /0.020 MGD /
Mar 2019 Average 0.007673 /0.020 MGD /
Apr 2019 Average 0.015157 /0.020 MGD /
May 2019 Average 0.01408 /0.020 MGD /
Jun 2019 Average 0.014578 /0.020 MGD /
2019 Quarter 1 0.008683 / MGD /
2019 Quarter 2 0.014605 / MGD /
2019 1st 6 Months(Avg) 0.011644 / MGD / I
2019 1st 6...(Max) 0.015157 / MGD /
2019 1st 6...(Min) 0.006171 / MGD /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Dale SamplelD Result/Limit Mass/Limit
Bismuth
01/02/2019 P Phononic010219POT < 0.005 / mg/L < /
W
01/16/2019 S Phononic011619Self 0.308 / mg/L /
02/21/2019 S Phononic022119Self 0.038 / mg/L /
03/14/2019 S Phononic031419Self 0.045 / mg/L /
04/24/2019 S Phononic042419Self 0.132 / mg/L /
05/17/2019 S Phononic051719Self 0.059 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 5

Phononic
SAMPLE OVERVIEW
1/1/2019 To 6/30%2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
06/17/2019 S Phononic061719Self 0.03 / mg/L /
Jan 2019 Week 1 < 0.005 / mg/L < /
Jan 2019 Week 3 0.308 / mg/L /
Feb 2019 Week 3 0.038 / mg/L /
Mar 2019 Week 2 0.045 / mg/L /
Apr 2019 Week 4 0.132 / mg/L /
May 2019 Week 3 0.059 / mg/L /
Jun 2019 Week 3 0.03 / mg/L /
Jan 2019 Average < 0.157 / mg/L < /
Feb 2019 Average 0.038 / mg/L /
Mar 2019 Average. 0.045 / mg/L /
Apr 2019 Average 0.132 / mg/L /
May 2019 Average 0.059 / mg/L /
Jun 2019 Average 0.03 / mg/L /
2019 Quarter 1 < 0.099 / mg/L < /
2019 Quarter 2 0.074 / mg/L /
2019 1st 6 Months(Avg) < 0.088 / mg/L < /
2019 1st 6...(Max) 0.308 / mg/L /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 7 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/02/2019 P Phononic010219POT 0.000005 /0.000142 mg/L /
WHg
06/03/2019 S Phononic060319SelfH 0.000002 /0.000142 mg/L /
g
Jan 2019 Week 1 0.000005 / mg/L /
Jun 2019 Week 1 0.000002 / mg/L /
Jan 2019 Average 0.000005 / mg/L /
Jun 2019 Average 0.000002 / mg/L /
2019 Quarter 1 0.000005 / mg/L /
2019 Quarter 2 0.000002 / mg/L /
2019 1st 6 Months(Avg) 0.000004 / mg/L /
2019 1st 6...(Max) 0.000005 / mg/L /
2019 1st 6...(Min) 0.000002 / mg/L /
2019 1st 6...(Count) 2 / /
•
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 5

Phononic
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
01/02/2019 P Phononic010219POT < 0.001 / mg/L < 0.0001 / lbs/day
W
06/17/2019 S Phononic061719Self < 0.003 / mg/L < 0.0004 / lbs/day
Jan 2019 Week 1 < 0.001 / mg/L < 0.0001 / lbs/day
Jun 2019 Week 3 < 0.003 / mg/L < 0.0004 / lbs/day
Jan 2019 Average < 0.001 / mg/L < 0.0001 / lbs/day
Jun 2019 Average < 0.003 / mg/L < 0.0004 / lbs/day
2019 Quarter I < 0.001 / mg/L < 0.0001 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.0004 / lbs/day
2019 1st 6 Months(Avg) < 0.002 / mg/L < 0.0002 / lbs/day
2019 1st 6...(Max) < 0.003 / mg/L < 0.0004 / lbs/day
2019 1st 6...(Min) < 0.001 / mg/L < 0.0001 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
01/02/2019 P Phononic010219POT 0.163 / mg/L 0.008388 /0.02 lbs/day
W
01/16/2019 S Phononic011619Self 0.098 / mg/L 0.005043 /0.02 lbs/day
02/21/2019 S Phononic022119Self 0.009 / mg/L 0.000916 /0.02 lbs/day
03/14/2019 S Phononic031419Self 0.062 / mg/L 0.012264 /0.02 lbs/day
04/24/2019 S Phononic042419Self 0.082 / mg/L 0.008199 /0.02 lbs/day
05/17/2019 S Phononic051719Self 0.962 / mg/L 0.092651 /0.02 lbs/day * *
06/17/2019 S Phononic061719Self 0.063 / mg/L 0.009433 /0.02 lbs/day
Jan 2019 Week 1 0.163 / mg/L 0.008388 / lbs/day
Jan 2019 Week 3 0.098 / mg/L 0.005043 / lbs/day
Feb 2019 Week 3 0.009 / mg/L 0.000916 / lbs/day
Mar 2019 Week 2 0.062 / mg/L 0.012264 / lbs/day
Apr 2019 Week 4 0.082 / mg/L 0.008199 / lbs/day
May 2019 Week 3 0.962 / mg/L 0.092651 / lbs/day
Jun 2019 Week 3 0.063 / mg/L 0.009433 / lbs/day
Jan 2019 Average 0.1305 / mg/L 0.006716 / lbs/day
Feb 2019 Average 0.009 / mg/L 0.000916 / lbs/day
Mar 2019 Average 0.062 / mg/L 0.012264 / lbs/day
Apr 2019 Average 0.082 / mg/L 0.008199 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 5

Phononic
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
May 2019 Average 0.962 / mg/L 0.092651 / lbs/day
Jun 2019 Average 0.063 / mg/L 0.009433 / lbs/day
2019 Quarter 1 0.083 / mg/L 0.006653 / lbs/day
2019 Quarter 2 0.369 / mg/L 0.036761 / lbs/day
2019 1st 6 Months(Avg) 0.2056 / mg/L 0.019556 / lbs/day
2019 1st 6...(Max) 0.962 / mg/L 0.092651 / lbs/day
2019 1st 6...(Min) 0.009 / mg/L 0.000916 / lbs/day
2019 1st 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 1 14.29 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 1 14.29 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
06/10/2019 S Phononic061019Se1f 7.3 /5.5- 10 SU /
Jun 2019 Week 2 7.3 / SU /
Jun 2019 Average 7.3 / SU /
2019 Quarter 2 7.3 / SU /
2019 1st 6 Months(Avg) 7.3 / SU /
2019 1st 6...(Max) 7.3 / SU /
2019 1st 6...(Min) 7.3 / SU /
2019 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
01/02/2019 P Phononic010219POT 0.592 / mg/L /
W
01/16/2019 S Phononic011619Self 0.624 / mg/L /
02/21/2019 S Phononic022119Self 0.053 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 5

,
Phononic
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
03/14/2019 S Phononic031419Se1f 0.128 / mg/L /
04/24/2019 S Phononic042419Se1f 0.149 / mg/L /
05/17/2019 S Phononic051719Se1f 0.366 / mg/L /
06/17/2019 S Phononic061719Se1f 0.098 / mg/L /
Jan 2019 Week I 0.592 / mg/L /
Jan 2019 Week 3 0.624 / mg/L /
Feb 2019 Week 3 0.053 / mg/L /
Mar 2019 Week 2 0.128 / mg/L /
Apr 2019 Week 4 0.149 / mg/L /
May 2019 Week 3 0.366 / mg/L /
Jun 2019 Week 3 0.098 / mg/L /
Jan 2019 Average 0.608 / mg/L /
Feb 2019 Average 0.053 / mg/L /
Mar 2019 Average 0.128 / mg/L /
Apr 2019 Average 0.149 / mg/L /
May 2019 Average 0.366 / mg/L /
Jun 2019 Average 0.098 / mg/L /
2019 Quarter 1 0.349 / mg/L /
2019 Quarter 2 0.204 / mg/L /
2019 1st 6 Months(Avg) 0.287 / mg/L /
2019 1st 6...(Max) 0.624 / mg/L /
2019 1st 6...(Min) 0.053 / mg/L /
2019 1st 6...(Count) 7 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 5

PowerSecure
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
02/05/2019 P PowerSecure020519P 30.6 / mg/L /
OTW
03/22/2019 S PowerSecure032219Se 5.38 / mg/L /
]f
Feb 2019 Week 1 30.6 / mg/L /
Mar 2019 Week 4 5.38 / mg/L /
Feb 2019 Average 30.6 / mg/L /
Mar 2019 Average 5.38 / mg/L /
2019 Quarter 1 17.99 / mg/L /
2019 1st 6 Months(Avg) 17.99 / mg/L /
2019 1st 6...(Max) 30.6 / mg/L /
2019 1st 6...(Min) 5.38 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S PowerSecure0119Flow 0.002436 / MGD /
02/28/2019 S PowerSecure0219F1ow 0.002324 / MGD /
03/31/2019 S PowerSecure0319F1ow 0.002224 / MGD /
04/18/2019 S PowerSecure0419F1ow 0.001935 / MGD /
05/31/2019 S PowerSecure0519F1ow 0.001794 / MGD /
06/19/2019 S PowerSecure0619F1ow 0.001691 / MGD /
Jan 2019 Week 4 0.002436 / MGD /
Feb 2019 Week 4 0.002324 / MGD /
Mar 2019 Week 4 0.002224 / MGD /
Apr 2019 Week 3 0.001935 / MGD /
May 2019 Week 4 0.001794 / MGD /
Jun 2019 Week 3 0.001691 / MGD /
Jan 2019 Average 0.002436 /0.006 MGD /
Feb 2019 Average 0.002324 0.006 MGD
g / /
Mar 2019 Average 0.002224 /0.006 MGD /
Apr 2019 Average 0.001935 /0.006 MGD /
May 2019 Average 0.001794 /0.006 MGD /
Jun 2019 Average 0.001691 /0.006 MGD /
2019 Quarter 1 0.002328 / MGD /
2019 Quarter 2 0.001807 / MGD /
2019 1st 6 Months(Avg) 0.002067 / MGD /
2019 1st 6...(Max) 0.002436 / MGD /
2019 1st 6...(Min) 0.001691 / MGD /
2019 1st 6...(Count) 6 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 9

PowerSecure
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/05/2019 P PowerSecure020519P 0.0068 /0.11 mg/L /
OTW
03/22/2019 S PowerSecure032219Se < 0.0005 /0.11 mg/L < /
If
Feb 2019 Week 1 0.0068 / mg/L /
Mar 2019 Week 4 < 0.0005 / mg/L < /
Feb 2019 Average 0.0068 /0.07 mg/L /
Mar 2019 Average < 0.0005 /0.07 mg/L < /
2019 Quarter 1 < 0.00365 / mg/L < /
2019 1st 6 Months(Avg) < 0.00365 / mg/L < /
2019 1st 6...(Max) 0.0068 / mg/L /
2019 1st 6...(Min) < 0.0005 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
02/05/2019 P PowerSecure020519P < 0.001 /2.77 mg/L < /
OTW
03/22/2019 S PowerSecure032219Se < 0.003 /2.77 mg/L < /
if
Feb 2019 Week 1 < 0.001 / mg/L < /
Mar 2019 Week 4 < 0.003 / mg/L < /
Feb 2019 Average < 0.001 / 1.71 mg/L < /
Mar 2019 Average < 0.003 / 1.71 mg/L < /
2019 Quarter 1 < 0.002 / mg/L < /
2019 1st 6 Months(Avg) < 0.002 / mg/L < /
2019 1st 6...(Max) < 0.003 / mg/L < /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 9

PowerSecure
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
2019 1st 6...(Min) < 0.001 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/05/2019 P PowerSecure020519P 0.121 /3.38 mg/L /
OTW
03/22/2019 S PowerSecure032219Se 0.076 /3.38 mg/L /
If
Feb 2019 Week 1 0.121 / mg/L /
Mar 2019 Week 4 0.076 / mg/L /
Feb 2019 Average 0.121 /2.07 mg/L /
Mar 2019 Average 0.076 /2.07 mg/L /
2019 Quarter 1 0.099 / mg/L /
2019 1st 6 Months(Avg) 0.099 / mg/L /
2019 1st 6...(Max) 0.121 / mg/L /
2019 1st 6...(Min) 0.076 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/05/2019 P PowerSecure020519P < 0.003 /0.60 mg/L < /
OTW
03/22/2019 S PowerSecure032219Se < 0.004 /0.60 mg/L < /
If
Feb 2019 Week 1 < 0.003 / mg/L < /
Mar 2019 Week 4 < 0.004 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 9

PowerSecure
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
Feb 2019 Average < 0.003 /0.50 mg/L < /
Mar 2019 Average < 0.004 /0.50 mg/L < /
2019 Quarter 1 < 0.003 / mg/L < /
2019 1st 6 Months(Avg) < 0.003 / mg/L < /
2019 1st 6...(Max) < 0.004 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
02/05/2019 P PowerSecure020519P 0.0024 /0.69 mg/L /
OTW
03/22/2019 S PowerSecure032219Se < 0.0025 /0.69 mg/L < /
If
Feb 2019 Week 1 0.0024 / mg/L /
Mar 2019 Week 4 < 0.0025 / mg/L < /
Feb 2019 Average 0.0024 /0.43 mg/L /
Mar 2019 Average < 0.0025 /0.43 mg/L < /
2019 Quarter 1 < 0.0025 / mg/L < /
2019 1st 6 Months(Avg) < 0.0025 / mg/L < /
2019 1st 6...(Max) < 0.0025 / mg/L < /
2019 1st 6...(Min) 0.0024 / mg/L /
2019 l st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 9

PowerSecure
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/05/2019 P PowerSecure0205I9P 0.0000036 /0.000142 mg/L /
OTWHg
03/22/2019 S PowerSecure032219Se < 0.0000005 /0.000142 mg/L < /
lf
Feb 2019 Week 1 0.0000036 / mg/L /
Mar 2019 Week 4 < 0.0000005 / mg/L < /
Feb 2019 Average 0.0000036 / mg/L /
Mar 2019 Average < 0.0000005 / mg/L < /
2019 Quarter 1 < 0.000002 / mg/L < /
2019 1st 6 Months(Avg) < 0.0000020 / mg/L < /
2019 1st 6...(Max) 0.0000036 / mg/L /
2019 1st 6...(Min) < 0.0000005 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/05/2019 P PowerSecure020519P < 0.001 / mg/L < /
OTW
03/22/2019 S PowerSecure032219Se < 0.003 / mg/L < /
If
Feb 2019 Week 1 < 0.001 / mg/L < /
Mar 2019 Week 4 < 0.003 / mg/L < /
Feb 2019 Average < 0.001 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < /
2019 Quarter 1 < 0.002 / mg/L < /
2019 1st 6 Months(Avg) < 0.002 / mg/L < /
2019 1st 6...(Max) < 0.003 / mg/L < /
2019 1st 6...(Min) < 0.001 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
02/05/2019 P PowerSecure020519P 0.021 / 1.3 mg/L /
OTW
03/22/2019 S PowerSecure032219Se < 0.0025 / 1.3 mg/L < /
if
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 9

PowerSecure
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Feb 2019 Week 1 0.021 / mg/L /
Mar 2019 Week 4 < 0.0025 / mg/L < /
Feb 2019 Average 0.021 / 1 mg/L /
Mar 2019 Average < 0.0025 / 1 mg/L < /
2019 Quarter 1 < 0.0118 / mg/L < /
2019 1st 6 Months(Avg) < 0.0118 / mg/L < /
2019 1st 6...(Max) 0.021 / mg/L /
2019 1st 6...(Min) < 0.0025 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/18/2019 P PowerSecure011819P 9.1 /6- I0 SU /
OTW
02/05/2019 P PowerSecure020519P 9 /6- I0 SU /
OTW
03/22/2019 S PowerSecure032219Se 8.7 /6- I0 SU /
If
Jan 2019 Week 3 9.1 / SU /
Feb 2019 Week 1 9 / SU /
Mar 2019 Week 4 8.7 / SU /
Jan 2019 Average 9.1 / SU /
Feb 2019 Average 9 / SU /
Mar 2019 Average 8.7 / SU /
2019 Quarter 1 8.93 / SU /
2019 1st 6 Months(Avg) 8.93 / SU /
2019 1st 6...(Max) 9.1 / SU /
2019 1st 6...(Min) 8.7 / SU /
2019 1st 6...(Count) 3 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 9

PowerSecure
SAMPLE OVERVIEW
Effluent Wastewater Ou
1/1/2019 To 6/30/2019 Sample Type: a11: 001ff1 tf
Sample Date SamplelD Result/Limit Mass/Limit
Silver
02/05/2019 P PowerSecure020519P 0.0011 /0.43 mg/L /
OTW
03/22/2019 S PowerSecure032219Se < 0.0025 /0.43 mg/L < /
If
Feb 2019 Week 1 0.0011 / mg/L /
Mar 2019 Week 4 < 0.0025 / mg/L < /
Feb 2019 Average 0.0011 /0.24 mg/L /
Mar 2019 Average < 0.0025 /0.24 mg/L < /
2019 Quarter 1 < 0.0018 / mg/L < /
2019 1st 6 Months(Avg) < 0.0018 / mg/L < /
2019 1st 6...(Max) < 0.0025 / mg/L < /
2019 lst 6...(Min) 0.0011 / mg/L /
2019 l st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/05/2019 P PowerSecure020519P 21 /66 °C /
OTW
03/22/2019 S PowerSecure032219Se 21.3 /66 °C /
If
Feb 2019 Week 1 21 / °C /
Mar 2019 Week 4 21.3 / °C /
Feb 2019 Average 21 / °C /
Mar 2019 Average 21.3 / °C /
2019 Quarter 1 21.2 / °C /
2019 1st 6 Months(Avg) 21.2 / °C /
2019 1st 6...(Max) 21.3 / °C /
2019 l st 6...(Min) 21 / °C /
2019 1st 6...(Count) 2 / /
MohdaY.February17,2020 *IndicatesViolation **Indicates TRC Violation Page 7 of 9

Pow erSecu re
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % #
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TTO
03/22/2019 S PowerSecure032219Se < 0.005 /2.13 mg/L < /
if
Mar 2019 Week 4 < 0.005 / mg/L /
Mar 2019 Average < 0.005 / mg/L /
2019 Quarter 1 < 0.005 / mg/L /
2019 1st 6 Months(Avg) < 0.005 / mg/L /
2019 1st 6...(Max) < 0.005 / mg/L /
2019 1st 6...(Min) < 0.005 / mg/L • /
2019 1st 6...(Count) 1 / /
Sample Count: 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/05/2019 P PowerSecure020519P 0.111 /2.61 mg/L /
OTW
03/22/2019 S PowerSecure032219Se 0.043 /2.61 mg/L /
If
Feb 2019 Week 1 0.111 / mg/L /
Mar 2019 Week 4 0.043 / mg/L /
Feb 2019 Average 0.111 / 1.48 mg/L /
Mar 2019 Average 0.043 / 1.48 mg/L /
2019 Quarter 1 0.077 / mg/L /
2019 1st 6 Months(Avg) 0.077 / mg/L /
2019 1st 6...(Max) 0.111 / mg/L /
2019 1st 6...(Min) 0.043 / mg/L /
2019 1st 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 9 •

PowerSecure
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
02/05/2019 S SCM020519Se1f 8.1 / mg/L 0.8752 / lbs/day
05/29/2019 P SCM052919POTW 6.5 / mg/L 1.0804 / lbs/day
Feb 2019 Week 1 8.1 / mg/L 0.8752 / lbs/day
May 2019 Week 4 6.5 / mg/L 1.0804 / lbs/day
Feb 2019 Average 8.1 / mg/L 0.8752 / lbs/day
May 2019 Average 6.5 / mg/L 1.0804 / lbs/day
2019 Quarter 1 8.1 / mg/L 0.8752 / lbs/day
2019 Quarter 2 6.5 / mg/L 1.0804 / lbs/day
2019 1st 6 Months(Avg) 7.3 / mg/L 0.9778 / lbs/day
2019 1st6...(Max) 8.1 / mg/L 1.0804 / lbs/day
2019 1st 6...(Min) 6.5 / mg/L 0.8752 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S SCM0119Flow 0.012801 /0.080 MGD /
02/28/2019 S SCM0219F1ow 0.014394 /0.080 MGD /
03/31/2019 S SCM0319Flow 0.013542 /0.080 MGD /
04/30/2019 S SCM0419F1ow 0.013441 /0.080 MGD /
05/31/2019 S SCM0519FIow 0.011951 /0.080 MGD /
06/30/2019 S SCM0619FIow 0.011058 /0.080 MGD /
Jan 2019 Week 4 0.012801 / MGD /
Feb 2019 Week 4 0.014394 / MGD /
Mar 2019 Week 4 0.013542 / MGD /
Apr 2019 Week 4 0.013441 / MGD /
May 2019 Week 4 0.011951 / MGD /
" Jun 2019 Week 4 0.011058 / MGD /
Jan 2019 Average 0.012801 /0.050 MGD /
Feb 2019 Average 0.014394 /0.050 MGD /
Mar 2019 Average 0.013542 /0.050 MGD /
Apr 2019 Average 0.013441 /0.050 MGD /
May 2019 Average 0.011951 /0.050 MGD /
Jun 2019 Average 0.011058 /0.050 MGD /
2019 Quarter 1 0.013579 / MGD /
2019 Quarter 2 0.01215 / MGD /
2019 1st 6 Months(Avg) 0.012865 / MGD /
2019 1st 6...(Max) 0.014394 / MGD /
2019 1st 6...(Min) 0.011058 / MGD /
2019 1st 6...(Count) 6 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/05/2019 S SCM020519SeIf < 0.0005 / mg/L < 0.000054 / lbs/day
04/23/2019 S SCM042319Self < 0.0005 / mg/L < 0.00005 / lbs/day
05/29/2019 P SCM052919POTW < 0.00008 / mg/L < 0.000012 / lbs/day
Feb 2019 Week 1 < 0.0005 / mg/L < 0.000054 / lbs/day
Apr 2019 Week 4 < 0.0005 / mg/L < 0.00005 / lbs/day
May 2019 Week 4 < 0.00008 / mg/L < 0.000012 / lbs/day
Feb 2019 Average < 0.0005 / mg/L < 0.000054 / lbs/day
Apr 2019 Average < 0.0005 / mg/L < 0.00005 / lbs/day
May 2019 Average < 0.00008 / mg/L < 0.000012 / lbs/day
2019 Quarter 1 < 0.0005 / mg/L < 0.000054 / lbs/day
2019 Quarter 2 < 0.00029 / mg/L < 0.000031 / lbs/day
2019 1st 6 Months(Avg) < 0.00036 / mg/L < 0.000039 / lbs/day
2019 1st 6...(Max) < 0.0005 / mg/L < 0.000054 / lbs/day
2019 1st 6...(Min) < 0.00008 / mg/L < 0.000012 / lbs/day
2019 1st 6...(Count) 3 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/05/2019 S SCM020519SeIf 23.6 / mg/L 2.5499 / lbs/day
05/29/2019 P SCM052919POTW 17 / mg/L 2.8257 / lbs/day
Feb 2019 Week 1 23.6 / mg/L 2.5499 / lbs/day
May 2019 Week 4 17 / mg/L 2.8257 / lbs/day
Feb 2019 Average 23.6 / mg/L 2.5499 / lbs/day
May 2019 Average 17 / mg/L 2.8257 / lbs/day
2019 Quarter 1 23.6 / mg/L 2.5499 / lbs/day
2019 Quarter 2 17 / mg/L 2.8257 / lbs/day
2019 1st 6 Months(Avg) 20.3 / mg/L 2.6878 / lbs/day
2019 1st 6...(Max) 23.6 / mg/L 2.8257 / lbs/day
2019 1st 6...(Min) 17 / mg/L 2.5499 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
02/05/2019 S SCM020519Self 0.192 /0.75 mg/L 0.020745 / lbs/day
04/23/2019 S SCM042319Self 0.433 /0.75 mg/L 0.043522 / lbs/day
05/29/2019 P SCM052919POTW 0.404 /0.75 mg/L 0.067151 / lbs/day
Feb 2019 Week 1 0.192 / mg/L 0.020745 / lbs/day
Apr 2019 Week 4 0.433 / mg/L 0.043522 / lbs/day
May 2019 Week 4 0.404 / mg/L 0.067151 / lbs/day
Feb 2019 Average 0.192 /0.50 mg/L 0.020745 / lbs/day
Apr 2019 Average 0.433 /0.50 mg/L 0.043522 / lbs/day
May 2019 Average 0.404 /0.50 mg/L 0.067151 / lbs/day
2019 Quarter 1 0.192 / mg/L 0.020745 / lbs/day
2019 Quarter 2 0.419 / mg/L 0.055337 / lbs/day
2019 1st 6 Months(Avg) 0.343 / mg/L 0.043806 / lbs/day
2019 1st 6...(Max) 0.433 / mg/L 0.067151 / lbs/day
2019 1st 6...(Min) 0.192 / mg/L 0.020745 / lbs/day
2019 1st 6...(Count) 3 / 3 /
Sample Count: 3 Months Sampled: 3 Weeks Sampled : 3 Quarters Sampled: 2
# % # % # % # 14
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/05/2019 S SCM020519Self < 0.005 /0.04 mg/L < 0.00054 / lbs/day
05/29/2019 P SCM052919POTW < 0.003 /0.04 mg/L < 0.000416 / Ibs/day
Feb 2019 Week 1 < 0.005 / mg/L < 0.00054 / lbs/day
May 2019 Week 4 < 0.003 / mg/L < 0.000416 / lbs/day
Feb 2019 Average < 0.005 /0.03 mg/L < 0.00054 / lbs/day
May 2019 Average < 0.003 /0.03 mg/L < 0.000416 / lbs/day
2019 Quarter 1 < 0.005 / mg/L < 0.00054 / lbs/day
2019 Quarter 2 < 0.003 / mg/L < 0.000416 / lbs/day
2019 1st 6 Months(Avg) < 0.004 / mg/L < 0.000478 / lbs/day
2019 1st 6...(Max) < 0.005 / mg/L < 0.000540 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < 0.000416 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
p p
mtt
Fluoride
02/05/2019 S SCM020519Self < 0.05 / mg/L < 0.0054 / lbs/day
05/29/2019 P SCM052919POTW < 0.05 / mg/L < 0.0083 / lbs/day
Feb 2019 Week 1 < 0.05 / mg/L < 0.0054 / lbs/day
May 2019 Week 4 < 0.05 / mg/L < 0.0083 / lbs/day
Feb 2019 Average < 0.05 / mg/L < 0.0054 / lbs/day
May 2019 Average < 0.05 / mg/L < 0.0083 / lbs/day
2019 Quarter 1 < 0.05 / mg/L < 0.0054 / lbs/day
2019 Quarter 2 < 0.05 / mg/L < 0.0083 / lbs/day
2019 1st 6 Months(Avg) < 0.05 / mg/L < 0.0069 / lbs/day
2019 1st 6...(Max) < 0.05 / mg/L < 0.0083 / lbs/day
2019 1st 6...(Min) < 0.05 / mg/L < 0.0054 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
02/05/2019 S SCM020519Self < 0.0025 /0.20 mg/L < 0.00027 / lbs/day
04/23/2019 S SCM042319Se1f < 0.0025 /0.20 mg/L < 0.000251 / lbs/day
05/29/2019 P SCM052919POTW 0.0016 /0.20 mg/L 0.000268 / lbs/day
Feb 2019 Week 1 < 0.0025 / mg/L < 0.00027 / lbs/day
Apr 2019 Week 4 < 0.0025 / mg/L < 0.000251 / lbs/day
May 2019 Week 4 0.0016 / mg/L 0.000268 / lbs/day
Feb 2019 Average < 0.0025 /0.10 mg/L < 0.00027 / lbs/day
Apr 2019 Average < 0.0025 /0.10 mg/L < 0.000251 / lbs/day
May 2019 Average 0.0016 /0.10 mg/L 0.000268 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.00027 / lbs/day
2019 Quarter 2 < 0.0021 / mg/L < 0.000259 / lbs/day
2019 1st 6 Months(Avg) < 0.0022 / mg/L < 0.000263 / lbs/day
2019 1st 6...(Max) < 0.0025 / mg/L < 0.000270 / lbs/day
2019 1st 6...(Min) 0.0016 / mg/L 0.000251 / lbs/day
2019 1st 6...(Count) 3 / 3 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 3 Months Sampled : 3 Weeks Sampled: 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
02/05/2019 S SCM020519Se1f 0.000008 /0.000142 mg/L /
05/28/2019 P SCM052819POTWHg 0.000013 /0.000142 mg/L /
Feb 2019 Week 1 0.000008 / mg/L /
May 2019 Week 4 0.000013 / mg/L /
Feb 2019 Average 0.000008 / mg/L /
May 2019 Average 0.000013 / mg/L /
2019 Quarter 1 0.000008 / . mg/L /
2019 Quarter 2 0.000013 / mg/L /
2019 1st 6 Months(Avg) 0.0000105 / mg/L /
2019 1st 6...(Max) 0.0000126 / mg/L /
2019 1st 6...(Min) 0.0000084 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Meeks Sampled: 2 Quarters Sampled : 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SanrplelD Result/Limit Mass/Limit
Molybdenum
02/05/2019 S SCM020519Self < 0.003 / mg/L < 0.0003 / lbs/day
05/29/2019 P SCM052919POTW < 0.001 / mg/L < 0.0002 / lbs/day
Feb 2019 Week 1 < 0.003 / mg/L < 0.0003 / lbs/day
May 2019 Week 4 < 0.001 / mg/L < 0.0002 / lbs/day
Feb 2019 Average < 0.003 / mg/L < 0.0003 / lbs/day
May 2019 Average < 0.001 / mg/L < 0.0002 / lbs/day
2019 Quarter 1 < 0.003 / mg/L < 0.0003 / lbs/day
2019 Quarter 2 < 0.001 / mg/L < 0.0002 / lbs/day
2019 1st 6 Months(Avg) < 0.002 / mg/L <. 0.0002 / lbs/day
2019 1st 6...(Max) < 0.003 / mg/L < 0.0003 / lbs/day
2019 1st 6...(Min) < 0.001 / mg/L < 0.0002 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
02/05/2019 S SCM020519Se1f < 0.0025 / mg/L < 0.00027 / lbs/day
04/23/2019 S SCM042319Self < 0.0025 / mg/L < 0.000251 / lbs/day
05/29/2019 P SCM052919POTW 3.53 / mg/L 0.586743 / lbs/day
Feb 2019 Week 1 < 0.0025 / mg/L < 0.00027 / lbs/day
Apr 2019 Week 4 < 0.0025 / mg/L < 0.000251 / lbs/day
May 2019 Week 4 3.53 / mg/L 0.586743 / lbs/day
Feb 2019 Average < 0.0025 / mg/L < 0.00027 / lbs/day
Apr 2019 Average < 0.0025 / mg/L < 0.000251 / lbs/day
May 2019 Average 3.53 / mg/L 0.586743 / lbs/day
2019 Quarter 1 < 0.0025 / mg/L < 0.00027 / lbs/day
2019 Quarter 2 < 1.7663 / mg/L < 0.293497 / lbs/day
2019 1st 6 Months(Avg) < 1.1783 / mg/L < 0.195755 / lbs/day
2019 1st 6...(Max) 3.53 / mg/L 0.586743 / lbs/day
2019 1st 6...(Min) < 0.0025 / mg/L < 0.000251 / lbs/day
2019 1st 6...(Count) 3 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/05/2019 S SCM020519Se1f 0.6 / mg/L 0.064 / lbs/day
05/29/2019 P SCM052919POTW 0.5 / mg/L 0.081 / lbs/day
Feb 2019 Week 1 0.6 / mg/L 0.064 / lbs/day
May 2019 Week 4 0.5 / mg/L 0.081 / lbs/day
Feb 2019 Average 0.6 / mg/L 0.064 / lbs/day
May 2019 Average 0.5 / mg/L 0.081 / lbs/day
2019 Quarter 1 0.6 / mg/L 0.064 / lbs/day
2019 Quarter 2 0.5 / mg/L 0.081 / lbs/day
2019 1st 6 Months(Avg) 0.5 / mg/L 0.073 / lbs/day
2019 1st 6...(Max) 0.6 / mg/L 0.081 / lbs/day
2019 1st 6...(Min) 0.5 / mg/L 0.064 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit 11ass/Limit
Nitrogen,Total
02/05/2019 S SCM020519Self 19.3 / mg/L 2.085 / lbs/day
05/29/2019 P SCM052919POTW 12.3 / mg/L 2.044 / lbs/day
Feb 2019 Week 1 19.3 / mg/L 2.085 / lbs/day
May 2019 Week 4 12.3 / mg/L 2.044 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
Feb 2019 Average 19.3 / mg/L 2.085 / lbs/day
May 2019 Average 12.3 / mg/L 2.044 / lbs/day
2019 Quarter 1 19.3 / mg/L 2.085 / lbs/day
2019 Quarter 2 12.3 / mg/L 2.044 / lbs/day
2019 1st 6 Months(Avg) 15.8 / mg/L 2.065 / lbs/day
2019 1st 6...(Max) 19.3 / mg/L 2.085 / lbs/day
2019 1st 6...(Min) 12.3 / mg/L 2.044 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/05/2019 S SCM020519Se1f 5.3 /200 mg/L /
05/29/2019 P SCM052919POTW < 2.5 /200 mg/L /
Feb 2019 Week 1 5.3 / mg/L /
May 2019 Week 4 < 2.5 / mg/L /
Feb 2019 Average 5.3 / mg/L /
May 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 5.3 / mg/L /
2019 Quarter 2 < 2.5 / mg/L < /
2019 1st 6 Months(Avg) < 3.9 / mg/L < /
2019 1st 6...(Max) 5.3 / mg/L /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
02/05/2019 S SCM020519Se1f 7.9 /6.0- 10.5 SU /
04/23/2019 S SCM042319Se1f 6.7 /6.0- 10.5 SU /
05/29/2019 P SCM052919POTW 7.4 /6.0- 10.5 SU /
Feb 2019 Week 1 7.9 / SU /
Apr 2019 Week 4 6.7 / SU /
May 2019 Week 4 7.4 / SU /
Feb 2019 Average 7.9 / SU /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 10
1

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
Apr 2019 Average 6.7 / SU /
May 2019 Average 7.4 / SU /
2019 Quarter 1 7.9 / SU /
2019 Quarter 2 7.05 / SU /
2019 1st 6 Months(Avg) 7.33 / SU /
2019 1st 6...(Max) 7.9 / SU /
2019 1st 6...(Min) 6.7 / SU /
2019 1st 6...(Count) 3 / /
Sample Count: 3 Months Sampled: 3 Weeks Sampled : 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
02/05/2019 S SCM020519Self < 0.005 / mg/L < 0.00054 / lbs/day
05/29/2019 P SCM052919POTW < 0.0005 / mg/L < 0.000083 / lbs/day
Feb 2019 Week 1 < 0.005 / mg/L < 0.00054 / lbs/day
May 2019 Week 4 < 0.0005 / mg/L < 0.000083 / lbs/day
Feb 2019 Average < 0.005 / mg/L < 0.00054 / lbs/day
May 2019 Average < 0.0005 / mg/L < 0.000083 / lbs/day
2019 Quarter 1 < 0.005 / mg/L < 0.00054 / lbs/day
2019 Quarter 2 < 0.0005 / mg/L < 0.000083 / lbs/day
2019 1st 6 Months(Avg) < 0.0028 / mg/L < 0.000312 / lbs/day
2019 1st 6...(Max) < 0.005 / mg/L < 0.000540 / lbs/day
2019 1st 6...(Min) < 0.0005 / mg/L < 0.000083 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
02/05/2019 S SCM020519Self 15.8 /66 °C /
04/23/2019 S SCM042319Self 19.3 /66 °C /
05/29/2019 P SCM052919POTW 27 /66 °C /
Feb 2019 Week 1 15.8 / °C /
Apr 2019 Week 4 19.3 / °C /
May 2019 Week 4 27 / °C /
Feb 2019 Average 15.8 / °C /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 10

SCM Metal Products, Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Apr 2019 Average 19.3 / °C /
May 2019 Average 27 / °C /
2019 Quarter 1 15.8 / °C /
2019 Quarter 2 23.2 / °C /
2019 1st 6 Months(Avg) 20.7 / °C /
2019 1st 6...(Max) 27 / °C /
2019 1st 6...(Min) 15.8 / °C /
2019 1st 6...(Count) 3 / /
Sample Count: 3 Months Sampled : 3 Weeks Sampled: 3 Quarters Sampled : 2
# % # % # % #
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M : 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/05/2019 S SCM020519Se1f 18.8 / mg/L 2.031 / lbs/day
05/29/2019 P SCM052919POTW 11.8 / mg/L 1.961 / lbs/day
Feb 2019 Week 1 18.8 / mg/L 2.031 / lbs/day
May 2019 Week 4 11.8 / mg/L 1.961 / lbs/day
Feb 2019 Average 18.8 / mg/L 2.031 / lbs/day
May 2019 Average 11.8 / mg/L 1.961 / lbs/day
2019 Quarter 1 18.8 / mg/L 2.031 / lbs/day
2019 Quarter 2 11.8 / mg/L 1.961 / lbs/day
2019 1st 6 Months(Avg) 15.3 / mg/L 1.996 / lbs/day
2019 1st 6...(Max) 18.8 / mg/L 2.031 / lbs/day
2019 1st 6...(Min) 11.8 / mg/L 1.961 / lbs/day
2019 1st 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Lirnit
Total Phosphorus
02/05/2019 S SCM020519Self 2.4 / mg/L 0.2593 / lbs/day
04/23/2019 S SCM042319Self 1.1 / mg/L 0.1106 / lbs/day
05/29/2019 P SCM052919POTW 1.73 / mg/L 0.2876 / lbs/day
Feb 2019 Week 1 2.4 / mg/L 0.2593 / lbs/day
Apr 2019 Week 4 1.1 / mg/L 0.1106 / lbs/day
May 2019 Week 4 1.73 / mg/L 0.2876 / lbs/day
Feb 2019 Average 2.4 / mg/L 0.2593 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 10

SCM Metal Products. Inc.
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfa11: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Apr 2019 Average 1.1 / mg/L 0.1106 / lbs/day
May 2019 Average 1.73 / mg/L 0.2876 / lbs/day
2019 Quarter 1 2.4 / mg/L 0.2593 / lbs/day
2019 Quarter 2 1.415 / mg/L 0.1991 / lbs/day
2019 1st 6 Months(Avg) 1.743 / mg/L 0.2191 / lbs/day
2019 1st 6...(Max) 2.4 / mg/L 0.2876 / lbs/day
2019 1st 6...(Min) 1.1 / mg/L 0.1106 / lbs/day
2019 1st 6...(Count) 3 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/05/2019 S SCM020519Self 0.0104 / mg/L /
Feb 2019 Week 1 0.0104 / mg/L /
Feb 2019 Average 0.0104 / mg/L /
2019 Quarter 1 0.0104 / mg/L /
2019 1st 6 Months(Avg) 0.0104 / mg/L /
2019 1st 6...(Max) 0.0104 / mg/L /
2019 1st 6...(Min) 0.0104 / mg/L /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/05/2019 S SCM020519Self 0.401 / mg/L 0.043326 / lbs/day
04/23/2019 S SCM042319Self 0.62 / mg/L 0.062318 / lbs/day
05/29/2019 P SCM052919POTW 0.61 / mg/L 0.101392 / lbs/day
Feb 2019 Week 1 0.401 / mg/L 0.043326 / lbs/day
Apr 2019 Week 4 0.62 / mg/L 0.062318 / lbs/day
May 2019 Week 4 0.61 / mg/L 0.101392 / lbs/day
Feb 2019 Average 0.401 / mg/L 0.043326 / lbs/day
Apr 2019 Average 0.62 / mg/L 0.062318 / lbs/day
May 2019 Average 0.61 / mg/L 0.101392 / lbs/day
2019 Quarter 1 0.401 / mg/L 0.043326 / lbs/day
2019 Quarter 2 0.615 / mg/L 0.081855 / lbs/day
2019 1st 6 Months(Avg) 0.544 / mg/L 0.069012 / lbs/day
2019 1st 6...(Max) 0.62 / mg/L 0.101392 / lbs/day
2019 1st 6...(Min) 0.401 / mg/L 0.043326 / lbs/day
2019 1st 6...(Count) 3 / 3 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 10

•
United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit 1
Ammonia
02/15/2019 S UTP1021519Se1f 2.2 / mg/L /
03/26/2019 P UTP1032619POTW 1.58 / mg/L 1.0896 / lbs/day
Feb 2019 Week 3 2.2 / mg/L /
Mar 2019 Week 4 1.58 / mg/L 1.0896 / lbs/day
Feb 2019 Average 2.2 / mg/L /
Mar 2019 Average 1.58 / mg/L 1.0896 / lbs/day
2019 Quarter 1 1.89 / mg/L 1.0896 / lbs/day
2019 1st 6 Months(Avg) 1.89 / mg/L 1.0896 / lbs/day
2019 1st 6...(Max) 2.2 / mg/L 1.0896 / lbs/day
2019 1st 6...(Min) 1.58 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
01/31/2019 S UTP10119F1ow 0.06101 / MGD /
02/28/2019 S UTP10219F1ow 0.076968 / MGD /
03/31/2019 S UTP10319F1ow 0.073998 / MGD /
04/30/2019 S UTP10419F1ow 0.04388 / MGD /
05/31/2019 S UTP10519F1ow 0.033802 / MGD /
06/30/2019 S UTP10619F1ow 0.034314 / MGD /
Jan 2019 Week 4 0.06101 / MGD / 1
Feb 2019 Week 4 0.076968 / MGD /
Mar 2019 Week 4 0.073998 / MGD /
Apr 2019 Week 4 0.04388 / MGD /
May 2019 Week 4 0.033802 / MGD /
Jun 2019 Week 4 0.034314 / MGD /
Jan 2019 Average 0.06101 /0.050 MGD * /
Feb 2019 Average 0.076968 /0.050 MGD * /
Mar 2019 Average 0.073998 /0.050 MGD * /
Apr 2019 Average 0.04388 /0.050 MGD /
May 2019 Average 0.033802 /0.050 MGD /
Jun 2019 Average 0.034314 /0.050 MGD /
2019 Quarter 1 0.070659 / MGD /
2019 Quarter 2 0.037332 / MGD /
2019 1st 6 Months(Avg) 0.053995 / MGD /
2019 1st 6...(Max) 0.076968 / MGD /
2019 1st 6...(Min) 0.033802 / MGD /
2019 1st 6...(Count) 6 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 3 50.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
02/15/2019 S UTP1021519Se1f 37.7 / mg/L /
03/26/2019 P UTP1032619POTW 103 / mg/L 71.032 / lbs/day
Feb 2019 Week 3 37.7 / mg/L /
Mar 2019 Week 4 103 / mg/L 71.032 / lbs/day
Feb 2019 Average 37.7 / mg/L /
Mar 2019 Average 103 / mg/L 71.032 / lbs/day
2019 Quarter 1 70.4 / mg/L 71.032 / lbs/day
2019 1st 6 Months(Avg) 70.4 / mg/L 71.032 / lbs/day
2019 1st 6...(Max) 103 / mg/L 71.032 / lbs/day
2019 1st 6...(Min) 37.7 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
02/15/2019 S UTP1021519Self < 0.0005 / mg/L < /
03/26/2019 P UTP1032619POTW < 0.00008 / mg/L < 0.000052 / lbs/day
Feb 2019 Week 3 < 0.0005 / mg/L < /
Mar 2019 Week 4 < 0.00008 / mg/L < 0.000052 / lbs/day
Feb 2019 Average < 0.0005 / mg/L < /
Mar 2019 Average < 0.00008 / mg/L < 0.000052 / lbs/day
2019 Quarter 1 < 0.00029 / mg/L < 0.000052 / lbs/day
2019 1st 6 Months(Avg) < 0.00029 / mg/L < 0.000052 / lbs/day
2019 1st 6...(Max) < 0.0005 / mg/L < 0.000052 / lbs/day
2019 1st 6...(Min) < 0.00008 / mg/L < /
2019 1st 6...(Count) 2 / I /
1 Sample Date SamplelD Result/Limit Mass/Limit
Chloride
02/15/2019 S UTP1021519Self 19.3 / mg/L /
03/26/2019 P UTP1032619POTW 157 / mg/L 108.2726 / lbs/day
Feb 2019 Week 3 19.3 / mg/L /
Mar 2019 Week 4 157 / mg/L 108.2726 / lbs/day
Feb 2019 Average 19.3 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
Mar 2019 Average 157 / mg/L 108.2726 / lbs/day
2019 Quarter 1 88.15 / mg/L 108.2726 / lbs/day
2019 1st 6 Months(Avg) 88.15 / mg/L 108.273 / lbs/day
2019 1st 6...(Max) 157 / mg/L 108.2726 / lbs/day
2019 1st 6...(Min) 19.3 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
02/15/2019 S UTP1021519Self < 12.5 / mg/L < /
03/26/2019 P UTP1032619POTW 233 / mg/L 160.68 / lbs/day
Feb 2019 Week 3 < 12.5 / mg/L < /
Mar 2019 Week 4 233 / mg/L 160.68 / lbs/day
Feb 2019 Average < 12.5 / mg/L < /
Mar 2019 Average 233 / mg/L 160.68 / lbs/day
2019 Quarter 1 < 122.8 / mg/L < 160.68 / lbs/day
2019 1st 6 Months(Avg) < 122.8 / mg/L < 160.69 / lbs/day
2019 1st 6...(Max) 233 / mg/L 160.68 / lbs/day
2019 1st 6...(Min) < 12.5 / mg/L < /
' 2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
02/15/2019 S UTP1021519Self < 0.004 / mg/L < /
03/26/2019 P UTP1032619POTW < 0.003 / mg/L < 0.001724 / lbs/day
Feb 2019 Week 3 < 0.004 / mg/L < /
Mar 2019 Week 4 < 0.003 / mg/L < 0.001724 / lbs/day
Feb 2019 Average < 0.004 / mg/L < /
Mar 2019 Average < 0.003 / mg/L < 0.001724 / lbs/day
2019 Quarter 1 < 0.003 / mg/L < 0.001724 / lbs/day
2019 1st 6 Months(Avg) < 0.003 / mg/L < 0.001724 / lbs/day
2019 1st 6...(Max) < 0.004 / mg/L < 0.001724 / lbs/day
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
02/15/2019 S UTP1021519Self < 0.05 / mg/L < /
03/26/2019 P UTP1032619POTW < 0.05 / mg/L < 0.0345 / lbs/day
Feb 2019 Week 3 < 0.05 / mg/L < /
Mar 2019 Week 4 < 0.05 / mg/L < 0.0345 / lbs/day
Wednesday,February 26,2020 * **
Indicates Violation Indicates TRC Violation Page 3 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
Feb 2019 Average < 0.05 / mg/L < /
Mar 2019 Average < 0.05 / mg/L < 0.0345 / lbs/day
2019 Quarter 1 < 0.05 / mg/L < 0.0345 / lbs/day
2019 1st 6 Months(Avg) < 0.05 / mg/L < 0.0345 / lbs/day
2019 1st 6...(Max) < 0.05 / mg/L < 0.0345 / lbs/day
2019 1st 6...(Min) < 0.05 / mg/L < /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury
05/17/2019 S UTP1051719Self 0 / mg/L /
May 2019 Week 3 0 / mg/L /
May 2019 Average 0 / mg/L /
2019 Quarter 2 0 / mg/L /
2019 1st 6 Months(Avg) 0.00000 / mg/L /
2019 1st 6...(Max) 0.00000 / mg/L /
2019 1st 6...(Min) 0.00000 / mg/L /
2019 1st 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
01/18/2019 S UTPI011819Self 0.000005 /0.000142 mg/L /
02/15/2019 S UTP1021519Self 0.000006 /0.000142 mg/L /
03/22/2019 S UTP1032219Self 0.000006 /0.000142 mg/L /
03/25/2019 P UTP1032519POTWHg 0.000056 /0.000142 mg/L /
04/18/2019 S UTP1041819Se1f 0.000002 /0.000142 mg/L /
06/14/2019 S UTP1061419Se1f 0.000005 /0.000142 mg/L /
Jan 2019 Week 3 0.000005 / mg/L /
Feb 2019 Week 3 0.000006 / mg/L /
Mar 2019 Week 4 0.000006 / mg/L /
Mar 2019 Week 4 0.000056 / mg/L /
Mar 2019 Week 4 0.000056 / mg/L /
Mar 2019 Week 4 0.000006 / mg/L /
Apr 2019 Week 3 0.000002 / mg/L /
Jun 2019 Week 2 0.000005 / mg/L /
Jan 2019 Average 0.000005 / mg/L /
Feb 2019 Average 0.000006 / mg/L /
Mar 2019 Average 0.000056 / mg/L /
Mar 2019 Average 0.000006 / mg/L /
Mar 2019 Average 0.000006 / mg/L /
Mar 2019 Average 0.000056 / mg/L /
Apr 2019 Average 0.000002 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Jun 2019 Average 0.000005 / mg/L /
2019 Quarter 1 0.000006 / mg/L /
2019 Quarter 1 0.000056 / mg/L /
2019 Quarter 1 0.000006 / mg/L /
2019 Quarter 1 0.000056 / mg/L /
2019 Quarter 2 0.000003 / mg/L /
2019 1st 6 Months(Avg) 0.0000134 / mg/L /
2019 1st 6...(Max) 0.0000563 / mg/L /
2019 1st 6...(Min) 0.0000016 / mg/L /
2019 1st 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 8 Weeks Sampled: 8 Quarters Sampled : 5
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
02/15/2019 S UTP1021519Self < 0.003 / mg/L < /
03/26/2019 P UTP1032619POTW < 0.001 / mg/L < 0.0007 / lbs/day
Feb 2019 Week 3 < 0.003 / mg/L < /
Mar 2019 Week 4 < 0.001 / mg/L < 0.0007 / lbs/day
Feb 2019 Average < 0.003 / mg/L < /
Mar 2019 Average < 0.001 / mg/L < 0.0007 / lbs/day
2019 Quarter 1 < 0.002 / mg/L < 0.0007 / lbs/day
2019 1st 6 Months(Avg) < 0.002 / mg/L < 0.0007 / lbs/day
2019 1st 6...(Max) < 0.003 / mg/L < 0.0007 / lbs/day
2019 1st 6...(Min) < 0.001 / mg/L < /
2019 1st 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
02/15/2019 S UTP1021519Self 0.5 / mg/L /
03/26/2019 P UTP1032619POTW 0.6 / mg/L 0.379 / lbs/day
Feb 2019 Week 3 0.5 / mg/L /
Mar 2019 Week 4 0.6 / mg/L 0.379 / lbs/day
Feb 2019 Average 0.5 / mg/L /
Mar 2019 Average 0.6 / mg/L 0.379 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 10
1

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2019 Quarter 1 0.5 / mg/L 0.379 / lbs/day
2019 1st 6 Months(Avg) 0.5 / mg/L 0.379 / lbs/day
2019 1st 6...(Max) 0.6 / mg/L 0.379 / lbs/day
2019 1st 6...(Min) 0.5 / mg/L /
2019 1st 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
02/15/2019 S UTP1021519Self 8.5 / mg/L /
03/26/2019 P UTP1032619POTW 8.06 / mg/L 5.558 / lbs/day
Feb 2019 Week 3 8.5 / mg/L /
Mar 2019 Week 4 8.06 / mg/L 5.558 / lbs/day
Feb 2019 Average 8.5 / mg/L /
Mar 2019 Average 8.06 / mg/L 5.558 / lbs/day
2019 Quarter 1 8.28 / mg/L 5.558 / lbs/day
2019 1st 6 Months(Avg) 8.28 / mg/L 5.558 / lbs/day
2019 1st 6...(Max) 8.5 / mg/L 5.558 / lbs/day
2019 1st 6...(Min) 8.06 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
02/15/2019 S UTP1021519Self 10.9 /200 mg/L /
03/26/2019 P UTP1032619POTW < 2.5 /200 mg/L < /
Feb 2019 Week 3 10.9 / mg/L /
Mar 2019 Week 4 < 2.5 / mg/L < /
Feb 2019 Average 10.9 / mg/L /
Mar 2019 Average < 2.5 / mg/L < /
2019 Quarter 1 < 6.7 / mg/L < /
2019 1st 6 Months(Avg) < 6.7 / mg/L < /
2019 1st 6...(Max) 10.9 / mg/L /
2019 1st 6...(Min) < 2.5 / mg/L < /
2019 1st 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
01/18/2019 S UTP1011819Se1f 9.1 /5.5- 10 SU /
02/15/2019 S UTP1021519Se1f 7.3 /5.5- 10 SU /
03/22/2019 S UTP1032219Se1f 7.6 /5.5-10 SU /
03/26/2019 P UTP1032619POTW 7.5 /5.5- 10 SU /
04/18/2019 S UTP1041819Se1f 6.6 /5.5- 10 SU /
05/17/2019 S UTP1051719Se1f 6.5 /5.5- 10 SU /
06/14/2019 S UTP1061419Se1f 6.8 /5.5- 10 SU /
Jan 2019 Week 3 9.1 / SU /
Feb 2019 Week 3 7.3 / SU /
Mar 2019 Week 4 7.55 / SU /
Apr 2019 Week 3 6.6 / SU /
May 2019 Week 3 6.5 / SU /
Jun 2019 Week 2 6.8 / SU /
Jan 2019 Average 9.1 / SU /
Feb 2019 Average 7.3 / SU /
Mar 2019 Average 7.55 / SU /
Apr 2019 Average 6.6 / SU /
May 2019 Average 6.5 / SU /
Jun 2019 Average 6.8 / SU /
2019 Quarter 1 7.88 / SU /
2019 Quarter 2 6.63 / SU /
2019 1st 6 Months(Avg) 7.34 / SU /
2019 1st 6...(Max) 9.1 / SU /
2019 1st 6...(Min) 6.5 / SU /
2019 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # 1/0
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
01/18/2019 S UTP1011819Self 19.5 /66 °C /
02/15/2019 S UTP1021519Se1f 22.4 /66 °C /
03/22/2019 S UTP1032219Se1f 19.7 /66 °C /
03/26/2019 P UTP1032619POTW 16 /66 °C /
04/18/2019 S UTP1041819Se1f 22.5 /66 °C /
05/17/2019 S UTP1051719Se1f 19.3 /66 °C /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 10

•
United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001 1
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
06/14/2019 S UTP1061419Se1f 24.6 /66 °C /
Jan 2019 Week 3 19.5 / °C /
Feb 2019 Week 3 22.4 / °C /
Mar 2019 Week 4 17.9 / °C /
Apr 2019 Week 3 22.5 / °C /
May 2019 Week 3 19.3 / °C /
Jun 2019 Week 2 24.6 / °C /
Jan 2019 Average 19.5 / °C /
Feb 2019 Average 22.4 / °C /
Mar 2019 Average 17.9 / °C /
Apr 2019 Average 22.5 / °C /
May 2019 Average 19.3 / °C /
Jun 2019 Average 24.6 / °C /
2019 Quarter 1 19.4 / °C /
2019 Quarter 2 22.1 / °C /
2019 1st 6 Months(Avg) 20.6 / °C /
2019 1st 6...(Max) 24.6 / °C /
2019 1st6...(Min) 16 / °C /
2019 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
02/15/2019 S UTP1021519Se1f 7.9 / mg/L /
03/26/2019 P UTP1032619POTW 7.51 / mg/L 5.179 / lbs/day
Feb 2019 Week 3 7.9 / mg/L /
Mar 2019 Week 4 7.51 / mg/L 5.179 / lbs/day
Feb 2019 Average 7.9 / mg/L /
Mar 2019 Average 7.51 / mg/L 5.179 / lbs/day
2019 Quarter 1 7.71 / mg/L 5.179 / lbs/day
2019 1st 6 Months(Avg) 7.71 / mg/L 5.179 / lbs/day
2019 1st 6...(Max) 7.9 / mg/L 5.179 / lbs/day
2019 1st 6...(Min) 7.51 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
02/15/2019 S UTP1021519Self 2 / mg/L /
03/26/2019 P UTP1032619POTW 2.49 / mg/L 1.7172 / lbs/day
Feb 2019 Week 3 2 / mg/L /
Mar 2019 Week 4 2.49 / mg/L 1.7172 / lbs/day
Feb 2019 Average 2 / mg/L /
Mar 2019 Average 2.49 / mg/L 1.7172 / lbs/day
2019 Quarter 1 2.245 / mg/L 1.7172 / lbs/day
2019 1st 6 Months(Avg) 2.245 / mg/L I.7172 / lbs/day
1 2019 1st 6...(Max) 2.49 / mg/L 1.7172 / lbs/day
2019 1st 6...(Min) 2 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
02/15/2019 S UTP1021519Se1f 46.3 / mg/L /
03/26/2019 P UTP1032619POTW 88 / mg/L 60.687845 / lbs/day
Feb 2019 Week 3 46.3 / mg/L /
Mar 2019 Week 4 88 / mg/L 60.687845 / lbs/day
Feb 2019 Average 46.3 / mg/L /
Mar 2019 Average 88 / mg/L 60.687845 / lbs/day
2019 Quarter 1 67.2 / mg/L 60.687845 / lbs/day
2019 1st 6 Months(Avg) 67.2 / mg/L 60.6878 / lbs/day
2019 1st 6...(Max) 88 / mg/L 60.687845 / lbs/day
2019 1st 6...(Min) 46.3 / mg/L /
2019 1st 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
02/15/2019 S UTP1021519Self 0.964 / mg/L /
03/26/2019 P UTP1032619POTW < 0.005 / mg/L < /
Feb 2019 Week 3 0.964 / mg/L /
Mar 2019 Week 4 < 0.005 / mg/L < /
Feb 2019 Average 0.964 / mg/L /
Mar 2019 Average < 0.005 / mg/L /
2019 Quarter 1 < 0.4845 / mg/L /
2019 1st 6 Months(Avg) < 0.4845 / mg/L < /
2019 1st 6...(Max) 0.964 / mg/L /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 10
1

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
02/15/2019 S UTP1021519Self 0.5 / mg/L /
03/26/2019 P UTP1032619POTW 0.996 / mg/L (1.686876 / lbs/day
Feb 2019 Week 3 0.5 / mg/L /
Mar 2019 Week 4 0.996 / mg/L 0.686876 / lbs/day
Feb 2019 Average 0.5 / mg/L /
Mar 2019 Average 0.996 / mg/L 0.686876 / lbs/day
2019 Quarter 1 0.748 / mg/L 0.686876 / lbs/day
2019 1st 6 Months(Avg) 0.748 / mg/L 0.686876 / lbs/day
2019 1st 6...(Max) 0.996 / mg/L 0.686876 / lbs/day
2019 1st 6...(Min) 0.5 / mg/L /
2019 1st 6...(Count) 2 / 1 /
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
01/18/2019 S UTP2011819Self 0.101 /20.7 mg/L /
02/15/2019 S UTP2021519Se1f < 0.005 /20.7 mg/L < /
03/26/2019 P UTP2032619POTW < 0.025 /20.7 mg/L < /
04/18/2019 S UTP2041819Se1f 0.016 /20.7 mg/L /
05/17/2019 S UTP2051719Self 0.083 /20.7 mg/L /
06/14/2019 S UTP2061419Self 0.207 /20.7 mg/L /
Jan 2019 Week 3 0.101 / mg/L /
Feb 2019 Week 3 < 0.005 / mg/L < /
Mar 2019 Week 4 < 0.025 / mg/L < /
Apr 2019 Week 3 0.016 / mg/L /
May 2019 Week 3 0.083 / mg/L /
Jun 2019 Week 2 0.207 / mg/L /
Jan 2019 Average 0.101 /8.2 mg/L /
Feb 2019 Average < 0.005 /8.2 mg/L < /
Mar 2019 Average < 0.025 /8.2 mg/L < /
Apr 2019 Average 0.016 /8.2 mg/L /
May 2019 Average 0.083 /8.2 mg/L /
Jun 2019 Average 0.207 /8.2 mg/L /
2019 Quarter 1 < 0.044 / mg/L < /
2019 Quarter 2 0.102 / mg/L /
2019 1st 6 Months(Avg) < 0.073 / mg/L < /
2019 1st 6...(Max) 0.207 / mg/L /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 6 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 10

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chloroform
05/17/2019 S UTP2051719Se1f 0.054 / mg/L /
06/14/2019 S UTP2061419Se1f 0.066 / mg/L /
May 2019 Week 3 0.054 / mg/L /
Jun 2019 Week 2 0.066 / mg/L /
May 2019 Average 0.054 / mg/L /
Jun 2019 Average 0.066 / mg/L /
2019 Quarter 2 0.06 / mg/L /
2019 1st 6 Months(Avg) 0.060 / mg/L /
2019 1st 6...(Max) 0.066 / mg/L /
2019 1st 6...(Min) 0.054 / mg/L /
2019 1st 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
01/18/2019 S UTP2011819Self < 0.05 /20.7 mg/L < /
02/15/2019 S UTP2021519Se1f < 0.05 /20.7 mg/L < /
03/22/2019 S UTP2032219Se1f < 0.05 /20.7 mg/L < /
03/26/2019 P UTP2032619POTW < 0.005 /20.7 mg/L < /
04/18/2019 S UTP2041819Se1f < 0.05 /20.7 mg/L < /
05/17/2019 S UTP2051719Se1f < 0.05 /20.7 mg/L < /
06/14/2019 S UTP2061419Se1f < 0.05 /20.7 mg/L < /
Jan 2019 Week 3 < 0.05 / mg/L < /
Feb 2019 Week 3 < 0.05 / mg/L < /
Mar 2019 Week 4 < 0.028 / mg/L < /
Apr 2019 Week 3 < 0.05 / mg/L < /
May 2019 Week 3 < 0.05 / mg/L < /
Jun 2019 Week 2 < 0.05 / mg/L < /
Jan 2019 Average < 0.05 /8.2 mg/L < /
Feb 2019 Average < 0.05 /8.2 mg/L < /
Mar 2019 Average < 0.028 /8.2 mg/L < /
Apr 2019 Average < 0.05 /8.2 mg/L < /
May 2019 Average < 0.05 /8.2 mg/L < /
Jun 2019 Average < 0.05 /8.2 mg/L < /
2019 Quarter 1 < 0.039 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2019 Quarter 2 < 0.05 / mg/L < /
2019 1st 6 Months(Avg) < 0.044 / mg/L < /
2019 1st 6...(Max) < 0.05 / mg/L < /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled : 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
01/18/2019 S UTP2011819Self < 0.05 /20.7 mg/L < /
02/15/2019 S UTP2021519Self < 0.05 /20.7 mg/L < /
03/22/2019 S UTP2032219Self < 0.05 /20.7 mg/L < /
03/26/2019 P UTP2032619POTW < 0.005 /20.7 mg/L < /
04/18/2019 S UTP2041819Se1f < 0.05 /20.7 mg/L < /
05/17/2019 S UTP2051719Se1f < 0.05 /20.7 mg/L < /
06/14/2019 S UTP2061419Se1f < 0.05 /20.7 mg/L < /
Jan 2019 Week 3 < 0.05 / mg/L < /
Feb 2019 Week 3 < 0.05 / mg/L < /
Mar 2019 Week 4 < 0.028 / mg/L < /
. Apr 2019 Week 3 < 0.05 / mg/L < /
May 2019 Week 3 < 0.05 / mg/L < /
Jun 2019 Week 2 < 0.05 / mg/L < /
Jan 2019 Average < 0.05 /8.2 mg/L < /
Feb 2019 Average < 0.05 /8.2 mg/L < /
Mar 2019 Average < 0.028 /8.2 mg/L < /
Apr 2019 Average < 0.05 /8.2 mg/L < /
May 2019 Average < 0.05 /8.2 mg/L < /
Jun 2019 Average < 0.05 /8.2 mg/L < /
2019 Quarter 1 < 0.039 / mg/L < /
2019 Quarter 2 < 0.05 / mg/L < /
2019 1st 6 Months(Avg) < 0.044 / mg/L < /
2019 1st 6...(Max) < 0.05 / mg/L < /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 7 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Count: 7 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
01/18/2019 S UTP2011819Se1f < 0.003 /3 mg/L < /
02/15/2019 S UTP2021519Se1f < 0.003 /3 mg/L < /
03/22/2019 S UTP2032219Se1f < 0.003 /3 mg/L < /
03/26/2019 P UTP2032619POTW < 0.005 /3 mg/L < /
04/18/2019 S UTP2041819Self < 0.003 /3 mg/L < /
05/17/2019 S UTP2051719Self < 0.003 /3 mg/L < /
06/14/2019 S UTP2061419Self < 0.003 /3 mg/L < /
Jan 2019 Week 3 < 0.003 / mg/L < /
Feb 2019 Week 3 < 0.003 / mg/L < /
Mar 2019 Week 4 < 0.004 / mg/L < /
Apr 2019 Week 3 < 0.003 / mg/L < /
May 2019 Week 3 < 0.003 / mg/L < /
Jun 2019 Week 2 < 0.003 / mg/L < /
Jan 2019 Average < 0.003 /0.7 mg/L < /
Feb 2019 Average < 0.003 /0.7 mg/L < /
Mar 2019 Average < 0.004 /0.7 mg/L < /
Apr 2019 Average < 0.003 /0.7 mg/L < /
May 2019 Average < 0.003 /0.7 mg/L < /
Jun 2019 Average < 0.003 /0.7 mg/L < /
2019 Quarter 1 < 0.003 / mg/L < /
2019 Quarter 2 < 0.003 / mg/L < /
2019 1st 6 Months(Avg) < 0.003 / mg/L < /
2019 1st 6...(Max) < 0.005 / mg/L < /
2019 1st 6...(Min) < 0.003 / mg/L < /
2019 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
01/18/2019 S UTP2011819Se1f < 0.025 /20.7 mg/L < /
02/15/2019 S UTP2021519Self < 0.025 /20.7 mg/L < /
03/22/2019 S UTP2032219Self < 0.025 /20.7 mg/L < /
03/26/2019 P UTP2032619POTW < 0.005 /20.7 mg/L < /
04/18/2019 S UTP2041819Self < 0.05 /20.7 mg/L < /
05/17/2019 S UTP2051719Self < 0.025 /20.7 mg/L < /
06/14/2019 S UTP2061419Self < 0.025 /20.7 mg/L < /
Jan 2019 Week 3 < 0.025 / mg/L < /
Feb 2019 Week 3 < 0.025 / mg/L < /
Mar 2019 Week 4 < 0.015 / mg/L < /
Apr 2019 Week 3 < 0.05 / mg/L < /
May 2019 Week 3 < 0.025 / mg/L < /
Jun 2019 Week 2 < 0.025 / mg/L < /
Jan 2019 Average < 0.025 /8.2 mg/L < /
Feb 2019 Average < 0.025 /8.2 mg/L < /
Mar 2019 Average < 0.015 /8.2 mg/L < /
Apr 2019 Average < 0.05 /8.2 mg/L < /
May 2019 Average < 0.025 /8.2 mg/L < /
Jun 2019 Average < 0.025 /8.2 mg/L < /
2019 Quarter 1 < 0.02 / mg/L < /
2019 Quarter 2 < 0.033 / mg/L < /
2019 1st 6 Months(Avg) < 0.026 / mg/L < /
2019 1st 6...(Max) < 0.05 / mg/L < /
2019 1st 6...(Min) < 0.005 / mg/L < /
2019 1st 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
04/18/2019 S UTP2041819Self 6.6 / SU /
Apr 2019 Week 3 6.6 / SU /
Apr 2019 Average 6.6 / SU /
2019 Quarter 2 6.6 / SU /
2019 1st 6 Months(Avg) 6.6 / SU /
2019 1st 6...(Max) 6.6 / SU /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
1/1/2019 To 6/30/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
pH
2019 1st 6...(Min) 6.6 / SU /
2019 1st 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
04/18/2019 S UTP2041819Se1f 22.5 / °C /
Apr 2019 Week 3 22.5 / °C /
Apr 2019 Average 22.5 / °C /
2019 Quarter 2 22.5 / °C /
2019 1st 6 Months(Avg) 22.5 / °C /
2019 1st 6...(Max) 22.5 / °C /
2019 1st 6...(Min) 22.5 / °C /
2019 1st 6...(Count) 1 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 5

r
AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S AstraZenenca0719F10 0.001946 / MGD /
w RECEIVED
09/03/2019 S AstraZeneca0819Flow 0.000488 / MGD /
09/30/2019 S AstraZeneca0919F1ow 0.000577 / MGD / MAR 0 3 1010
10/31/2019 S AstraZenecal019Flow 0.000374 / MGD /
11/30/2019 S AstraZenecal119Flow 0.00028 / MGD / NCDEQIDWRINPDES
12/31/2019 S AstraZenecal219Flow 0.001952 / MGD /
Jul2019 Week 4 0.001946 / MGD /
Sep 2019 Week 1 0.000488 / MGD /
Sep 2019 Week 4 0.000577 / MGD /
Oct 2019 Week 4 0.000374 / MGD /
Nov 2019 Week 4 0.00028 / MGD /
Dec 2019 Week 4 0.001952 / MGD /
Jul 2019 Average 0.001946 /0.002000 MGD /
Sep 2019 Average 0.000533 /0.002000 MGD /
Oct 2019 Average 0.000374 /0.002000 MGD /
Nov 2019 Average 0.00028 /0.002000 MGD /
Dec 2019 Average 0.001952 /0.002000 MGD /
2019 Quarter 3 0.001004 / MGD /
2019 Quarter 4 0.000869 / MGD /
2019 2nd 6 Months(Avg) 0.000936 / MGD /
2019 2nd 6...(Max) 0.001952 / MGD /
2019 2nd 6...(Min) 0.00028 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 5 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % #
04
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
COD
08/22/2019 S AstraZeneca082219Sel 25 / mg/L /
f
10/02/2019 P AstraZeneca100219PO 21 / mg/L /
TW
Aug 2019 Week 4 25 / mg/L /
Oct 2019 Week 1 21 / mg/L /
Aug 2019 Average 25 / mg/L /
Oct 2019 Average 21 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 5

r
AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
COD
2019 Quarter 3 25 / mg/L /
2019 Quarter 4 21 / mg/L /
2019 2nd 6 Months(Avg) 23 / mg/L /
2019 2nd 6...(Max) 25 / mg/L /
2019 2nd 6...(Min) 21 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
08/22/2019 S AstraZeneca082219Se1 < 0.0025 /20.7 mg/L < /
f
Aug 2019 Week 4 < 0.0025 / mg/L < /
Aug 2019 Average < 0.0025 /8.2 mg/L < /
2019 Quarter 3 < 0.0025 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2019 2nd 6...(Max) < 0.0025 / mg/L < /
2019 2nd 6...(Min) < 0.0025 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
08/22/2019 S AstraZeneca082219Sel < 0.0025 /20.7 mg/L < /
f
Aug 2019 Week 4 < 0.0025 / mg/L < /
Aug 2019 Average < 0.0025 /8.2 mg/L < /
2019 Quarter 3 < 0.0025 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2019 2nd 6...(Max) < 0.0025 / mg/L < /
2019 2nd 6...(Min) < 0.0025 / mg/L < /
2019 2nd 6...(Count) 1 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 5
4

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled : 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/22/2019 S AstraZeneca082219Se1 0.000003 /0.000142 mg/L /
f
10/02/2019 P AstraZeneca100219PO 0.000003 /0.000142 mg/L /
TWHg
Oct 2019 Week 1 0.000003 / mg/L /
Aug 2019 Week 4 0.000003 / mg/L /
Aug 2019 Average 0.000003 / mg/L /
Oct 2019 Average 0.000003 / mg/L /
2019 Quarter 3 0.000003 / mg/L /
2019 Quarter 4 0.000003 / mg/L /
2019 2nd 6 Months(Avg) 0.0000026 / mg/L /
2019 2nd 6...(Max) 0.0000027 / mg/L /
2019 2nd 6...(Min) 0.0000026 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
1 #Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
08/22/2019 S AstraZeneca082219Se1 < 0.003 /3 mg/L < /
f
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 /0.7 mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 1 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
08/22/2019 S AstraZeneca082219Sel < 0.003 /20.7 mg/L < /
f
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 /8.2 mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled : 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/22/2019 S AstraZeneca082219Sel 6.7 /6- 10 SU /
f
10/02/2019 P AstraZeneca100219P0 6.8 /6- 10 SU /
TW
Aug 2019 Week 4 6.7 / SU /
Oct 2019 Week 1 6.8 / SU /
Aug 2019 Average 6.7 / SU /
Oct 2019 Average 6.8 / SU /
2019 Quarter 3 6.7 / SU /
2019 Quarter 4 6.8 / SU /
2019 2nd 6 Months(Avg) 6.75 / SU /
2019 2nd 6...(Max) 6.8 / SU /
2019 2nd 6...(Min) 6.7 / SU /
2019 2nd 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 5

AstraZeneca Pharmaceuticals LP
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % #
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily : 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 5

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
08/09/2019 S Aurobindo080919Self 3.39 /5.59 mg/L /
08/29/2019 S Aurobindo082919SeIf 6.7 /5.59 mg/L * /
09/23/2019 S Aurobindo092319SeIf 9.33 /5.59 mg/L * * /
09/25/2019 S Aurobindo092519Se1f < 0.25 /5.59 mg/L < /
09/30/2019 S Aurobindo093019Se1f < 0.025 /5.59 mg/L < /
10/15/2019 S Aurobindo101519Self 0.141 /5.59 mg/L /
11/19/2019 S Aurobindo111919Self < 0.25 /5.59 mg/L < /
11/21/2019 S Aurobindo112119Self < 0.25 /5.59 mg/L < /
11/25/2019 S Aurobindo112519Self < 0.25 /5.59 mg/L < /
12/04/2019 S Aurobindo120419SeIf < 0.25 /5.59 mg/L < /
12/06/2019 S Aurobindo120619SeIf < 0.25 /5.59 mg/L < /
12/13/2019 S Aurobindo121319Self < 0.25 /5.59 mg/L < /
Aug 2019 Week 2 3.39 / mg/L /
Aug 2019 Week 4 6.7 / mg/L /
Sep 2019 Week 4 < 3.202 / mg/L < /
Oct 2019 Week 3 0.141 / mg/L /
Nov 2019 Week 3 < 0.25 / mg/L < /
Nov 2019 Week 4 < 0.25 / mg/L < /
Dec 2019 Week 1 < 0.25 / mg/L < /
Dec 2019 Week 2 < 0.25 / mg/L < /
Aug 2019 Average 5.045 /2.21 mg/L * * /
Sep 2019 Average < 3.202 /2.21 mg/L * * < /
Oct 2019 Average 0.141 /2.21 mg/L /
Nov 2019 Average < 0.25 /2.21 mg/L < /
Dec 2019 Average < 0.25 /2.21 mg/L < /
2019 Quarter 3 < 3.939 / mg/L < /
1 2019 Quarter 4 < 0.234 / mg/L < /
2019 2nd 6 Months(Avg) < 1.778 / mg/L < /
2019 2nd 6...(Max) 9.33 / mg/L /
2019 2nd 6...(Min) < 0.025 / mg/L < /
2019 2nd 6...(Count) 12 / /
Sample Count: 12 Months Sampled: 5 Weeks Sampled: 8 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 2 16.67 #Over Mo Avg C: 2 40.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: I 8.33 #Over Mo Avg C TRC: 2 40.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/09/2019 S Aurobindo080919Se1f 29.7 / mg/L /
08/27/2019 P Aurobindo082719POT 14.4 / mg/L /
W
Aug 2019 Week 2 29.7 / mg/L /
Aug 2019 Week 4 14.4 / mg/L /
Aug 2019 Average 22.05 / mg/L /
2019 Quarter 3 22.05 / mg/L /
2019 2nd 6 Months(Avg) 22.05 / mg/L /
2019 2nd 6...(Max) 29.7 / mg/L /
2019 2nd 6...(Min) 14.4 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/18/2019 S Aurobndo0719Flow 0.01091 / MGD /
08/21/2019 S Aurobindo0819FIow 0.007003 / MGD /
09/19/2019 S Aurobindo0919F1ow 0.004043 / MGD /
10/17/2019 S Aurobindo1019Flow 0.003148 / MGD /
11/20/2019 S Aurobindo 1119Flow 0.002466 / MGD /
12/19/2019 S Aurobindol219F1ow 0.002606 / MGD /
Jul2019 Week 3 0.01091 / MGD /
Aug 2019 Week 3 0.007003 / MGD /
Sep 2019 Week 3 0.004043 / MGD /
Oct 2019 Week 3 0.003148 / MGD /
Nov 2019 Week 3 0.002466 / MGD /
Dec 2019 Week 3 0.002606 / MGD /
Jul 2019 Average 0.01091 /0.039 MGD /
Aug 2019 Average 0.007003 /0.039 MGD /
Sep 2019 Average 0.004043 /0.039 MGD /
Oct 2019 Average 0.003148 /0.039 MGD /
Nov 2019 Average 0.002466 /0.039 MGD /
Dec 2019 Average 0.002606 /0.039 MGD /
2019 Quarter 3 0.007319 / MGD /
2019 Quarter 4 0.00274 / MGD /
2019 2nd 6 Months(Avg) 0.005029 / MGD /
2019 2nd 6...(Max) 0.01091 / MGD /
2019 2nd 6...(Min) 0.002466 / MGD /
2019 2nd 6...(Count) 6 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
08/09/2019 S Aurobindo080919Self 205 / mg/L /
08/27/2019 P Aurobindo082719POT 145 / mg/L /
W
Aug 2019 Week 2 205 / mg/L /
Aug 2019 Week 4 145 / mg/L /
Aug 2019 Average 175 / mg/L /
2019 Quarter 3 175 / mg/L /
2019 2nd 6 Months(Avg) 175 / mg/L /
2019 2nd 6...(Max) 205 / mg/L /
2019 2nd 6...(Min) 145 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/09/2019 S Aurobindo080919Self < 0.00008 / mg/L < /
08/27/2019 P Aurobindo082719POT < 0.00008 / mg/L < /
W
Aug 2019 Week 2 < 0.00008 / mg/L < /
Aug 2019 Week 4 < 0.00008 / mg/L < /
Aug 2019 Average < 0.00008 / mg/L < /
2019 Quarter 3 < 0.00008 / mg/L < /
2019 2nd 6 Months(Avg) < 0.00008 / mg/L < /
2019 2nd 6...(Max) < 0.00008 / mg/L < /
2019 2nd 6...(Min) < 0.00008 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/09/2019 S Aurobindo080919Se!f 37 / mg/L /
08/27/2019 P Aurobindo082719POT 37 / mg/L /
W
Aug 2019 Week 2 37 / mg/L /
Aug 2019 Week 4 37 / mg/L /
Aug 2019 Average 37 / mg/L /
2019 Quarter 3 37 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2019 2nd 6 Months(Avg) 37 / mg/L /
2019 2nd 6...(Max) 37 / mg/L /
2019 2nd 6...(Min) 37 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
08/09/2019 S Aurobindo080919Self 295 / mg/L /
08/27/2019 P Aurobindo082719POT 282 / mg/L /
W
Aug 2019 Week 2 295 / mg/L /
Aug 2019 Week 4 282 / mg/L /
Aug 2019 Average 288.5 / mg/L /
2019 Quarter 3 288.5 / mg/L /
2019 2nd 6 Months(Avg) 288.5 / mg/L /
2019 2nd 6...(Max) 295 / mg/L /
2019 2nd 6...(Min) 282 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/09/2019 S Aurobindo080919Se1f 0.034 / mg/L /
08/27/2019 P Aurobindo082719POT 0.046 / mg/L /
W
Aug 2019 Week 2 0.034 / mg/L /
Aug 2019 Week 4 0.046 / mg/L /
Aug 2019 Average 0.04 / mg/L /
2019 Quarter 3 0.04 / mg/L /
2019 2nd 6 Months(Avg) 0.040 / mg/L /
2019 2nd 6...(Max) 0.046 / mg/L /
2019 2nd 6...(Min) 0.034 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/09/2019 S Aurobindo080919Se1f < 0.003 / mg/L < /
08/27/2019 P Aurobindo082719POT < 0.003 / mg/L < /
W
Aug 2019 Week 2 < 0.003 / mg/L /
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 / mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
08/09/2019 S Aurobindo080919Self < 0.003 /5.59 mg/L < /
08/29/2019 S Aurobindo082919Se1f < 0.003 /5.59 mg/L < /
Aug 2019 Week 2 < 0.003 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 /2.21 mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: I
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Dale SamplelD Result/Limit .41ass/Limit
Fluoride
08/09/2019 S Aurobindo080919Se1f < 0.05 / mg/L < /
08/27/2019 P Aurobindo082719POT < 0.05 / mg/L < /
W
Aug 2019 Week 2 < 0.05 / mg/L < /
Aug 2019 Week 4 < 0.05 / mg/L < /
Aug 2019 Average < 0.05 / mg/L < /
2019 Quarter 3 < 0.05 / mg/L < /
2019 2nd 6 Months(Avg) < 0.05 / mg/L < /
2019 2nd 6...(Max) < 0.05 / mg/L < /
2019 2nd 6...(Min) < 0.05 / mg/L < /
2019 2nd 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
08/09/2019 S Aurobindo080919SeIf < 0.003 /5.59 mg/L < /
08/29/2019 S Aurobindo082919Self < 0.003 /5.59 mg/L < /
Aug 2019 Week 2 < 0.003 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 /2.21 mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/09/2019 S Aurobindo080919Se1f 0.000062 /0.00142 mg/L /
11/04/2019 P Aurobindol 10419POT 0.000048 /0.000142 mg/L /
WHg
Aug 2019 Week 2 0.000062 / mg/L /
Nov 2019 Week 1 0.000048 / mg/L /
Aug 2019 Average 0.000062 / mg/L /
Nov 2019 Average 0.000048 / mg/L /
2019 Quarter 3 0.000062 / mg/L /
2019 Quarter 4 0.000048 / mg/L /
2019 2nd 6 Months(Avg) 0.000055 / mg/L /
2019 2nd 6...(Max) 0.0000617 / mg/L /
2019 2nd 6...(Min) 0.0000483 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
08/09/2019 S Aurobindo080919Self < 0.003 /0.81 mg/L < /
08/29/2019 S Aurobindo082919Self < 0.003 /0.81 mg/L < /
Aug 2019 Week 2 < 0.003 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 /0.18 mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/09/2019 S Aurobindo080919SeIf < 0.001 / mg/L < /
08/27/2019 P Aurobindo082719POT < 0.001 / mg/L < /
W 1
Aug 2019 Week 2 < 0.001 / mg/L < /
Aug 2019 Week 4 < 0.001 / mg/L < /
Aug 2019 Average < 0.001 / mg/L < /
2019 Quarter 3 < 0.001 / mg/L < /
2019 2nd 6 Months(Avg) < 0.001 / mg/L < /
2019 2nd 6...(Max) < 0.001 / mg/L < /
2019 2nd 6...(Min) < 0.001 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
08/09/2019 S Aurobindo080919Se1f < 0.003 /5.59 mg/L < /
08/29/2019 S Aurobindo082919Se1f < 0.003 /5.59 mg/L < /
Aug 2019 Week 2 < 0.003 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 /2.21 mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 1 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/09/2019 S Aurobindo080919Se1f < 0.1 / mg/L < /
08/27/2019 P Aurobindo082719POT 0.5 / mg/L /
W
Aug 2019 Week 2 < 0.1 / mg/L < /
Aug 2019 Week 4 0.5 / mg/L /
Aug 2019 Average < 0.3 / mg/L < /
2019 Quarter 3 < 0.3 / mg/L < /
2019 2nd 6 Months(Avg) < 0.3 / mg/L < /
2019 2nd 6...(Max) 0.5 / mg/L /
2019 2nd 6...(Min) < 0.1 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/09/2019 S Aurobindo080919Se1f 31.6 / mg/L /
08/27/2019 P Aurobindo082719POT 18.9 / mg/L /
W
Aug 2019 Week 2 31.6 / mg/L /
Aug 2019 Week 4 18.9 / mg/L /
Aug 2019 Average 25.25 / mg/L /
2019 Quarter 3 25.25 / mg/L /
2019 2nd 6 Months(Avg) 25.25 / mg/L /
2019 2nd 6...(Max) 31.6 / mg/L /
2019 2nd 6...(Min) 18.9 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
08/09/2019 S Aurobindo080919Se1f 5 /200 mg/L /
08/27/2019 P Aurobindo082719POT < 2.5 /200 mg/L < /
W
Aug 2019 Week 2 5 / mg/L /
Aug 2019 Week 4 < 2.5 / mg/L < /
Aug 2019 Average < 3.75 / mg/L < /
2019 Quarter 3 < 3.75 / mg/L < /
2019 2nd 6 Months(Avg) < 3.75 / mg/L < /
2019 2nd 6...(Max) 5 / mg/L /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/09/2019 S Aurobindo080919Se1f 8.1 /6.0- 10.0 SU /
08/27/2019 P Aurobindo082719POT 8.6 /6.0- 10.0 SU /
W
Aug 2019 Week 2 8.1 / SU /
Aug 2019 Week 4 8.6 / SU /
Aug 2019 Average 8.35 / SU /
2019 Quarter 3 8.35 / SU /
2019 2nd 6 Months(Avg) 8.35 / SU /
2019 2nd 6...(Max) 8.6 / SU /
2019 2nd 6...(Min) 8.1 / SU /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/09/2019 S Aurobindo080919Se1f 24 /66 °C /
08/27/2019 P Aurobindo082719POT 24 /66 °C /
W
Aug 2019 Week 2 24 / °C /
Aug 2019 Week 4 24 / °C /
Aug 2019 Average 24 / °C /
2019 Quarter 3 24 / °C /
2019 2nd 6 Months(Avg) 24 / °C /
2019 2nd 6...(Max) 24 / °C /
2019 2nd 6...(Min) 24 / °C /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampleID Result/Limit Mass/Limit
TKN
08/09/2019 S Aurobindo080919Self 31.6 / mg/L /
08/27/2019 P Aurobindo082719POT 18.4 / mg/L /
W
Aug 2019 Week 2 31.6 / mg/L /
Aug 2019 Week 4 18.4 / mg/L /
Aug 2019 Average 25 / mg/L /
2019 Quarter 3 25 / mg/L /
2019 2nd 6 Months(Avg) 25 / mg/L /
2019 2nd 6...(Max) 31.6 / mg/L /
2019 2nd 6...(Min) 18.4 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
08/09/2019 S Aurobindo080919Se1f 5.41 / mg/L /
08/27/2019 P Aurobindo082719POT 2.77 / mg/L /
W
Aug 2019 Week 2 5.41 / mg/L /
Aug 2019 Week 4 2.77 / mg/L /
Aug 2019 Average 4.09 / mg/L /
2019 Quarter 3 4.09 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 11

Aurobindo USA
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
2019 2nd 6 Months(Avg) 4.09 / mg/L /
2019 2nd 6...(Max) 5.41 / mg/L /
2019 2nd 6...(Min) 2.77 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
08/09/2019 S Aurobindo080919Self 193 / mg/L /
08/27/2019 P Aurobindo082719POT 42 / mg/L /
W
Aug 2019 Week 2 193 / mg/L /
Aug 2019 Week 4 42 / mg/L /
Aug 2019 Average 117.5 / mg/L /
2019 Quarter 3 117.5 / mg/L /
2019 2nd 6 Months(Avg) 117.5 / mg/L /
2019 2nd 6...(Max) 193 / mg/L /
2019 2nd 6...(Min) 42 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/09/2019 S Aurobindo080919SeIf 0.156 / mg/L /
08/27/2019 P Aurobindo082719POT 0.272 / mg/L /
W
Aug 2019 Week 2 0.156 / mg/L /
Aug 2019 Week 4 0.272 / mg/L /
Aug 2019 Average 0.214 / mg/L /
2019 Quarter 3 0.214 / mg/L /
2019 2nd 6 Months(Avg) 0.214 / mg/L /
2019 2nd 6...(Max) 0.272 / mg/L /
2019 2nd 6...(Min) 0.156 / mg/L /
2019 2nd 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 11 of 11

Bioeen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/30/2019 P Biogen073019POTW < 0.05 / 12.19 mg/L < /
Jul 2019 Week 4 < 0.05 / mg/L < /
Jul2019 Average < 0.05 /4.83 mg/L < /
2019 Quarter 3 < 0.05 / mg/L < /
2019 2nd 6 Months(Avg) < 0.05 / mg/L < /
2019 2nd 6...(Max) < 0.05 / mg/L < /
2019 2nd 6...(Min) < 0.05 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/17/2019 S Biogen071719Se1f 1.7 / mg/L 1.4501 / lbs/day
07/30/2019 P Biogen073019POTW 2.01 / mg/L /
Jul 2019 Week 3 1.7 / mg/L 1.4501 / lbs/day
Jul 2019 Week 4 2.01 / mg/L /
Jul 2019 Average 1.86 / mg/L 1.4501 / lbs/day
2019 Quarter 3 1.86 / mg/L 1.4501 / lbs/day
2019 2nd 6 Months(Avg) 1.86 / mg/L 1.4501 / lbs/day
2019 2nd 6...(Max) 2.01 / mg/L 1.4501 / lbs/day
2019 2nd 6...(Min) 1.7 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S Biogen0719Flow 0.102279 /0.375 MGD /
08/31/2019 S Biogen0819Flow 0.098048 /0.375 MGD /
09/30/2019 S Biogen0919Flow 0.092797 /0.375 MGD /
10/31/2019 S Biogen1019Flow 0.094833 /0.375 MGD /
11/30/2019 S Biogen1119Flow 0.081354 /0.375 MGD /
12/31/2019 S Biogen1219Flow 0.087887 /0.375 MGD /
Jul 2019 Week 4 0.102279 / MGD /
Aug 2019 Week 4 0.098048 / MGD /
Sep 2019 Week 4 0.092797 / MGD /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 9

Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Oct 2019 Week 4 0.094833 / MGD /
Nov 2019 Week 4 0.081354 / MGD /
Dec 2019 Week 4 0.087887 / MGD /
Jul2019 Average 0.102279 /0.250 MGD /
Aug 2019 Average 0.098048 /0.250 MGD /
Sep 2019 Average 0.092797 /0.250 MGD /
Oct 2019 Average 0.094833 /0.250 MGD /
Nov 2019 Average 0.081354 /0.250 MGD /
Dec 2019 Average 0.087887 /0.250 MGD /
2019 Quarter 3 0.097708 / MGD /
2019 Quarter 4 0.088025 / MGD /
2019 2nd 6 Months(Avg) 0.092866 / MGD /
2019 2nd 6...(Max) 0.102279 / MGD /
2019 2nd 6...(Min) 0.081354 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/17/2019 S Biogen071719Self 10.8 / mg/L 9.213 / lbs/day
07/30/2019 P Biogen073019POTW 99.3 / mg/L /
Jul 2019 Week 3 10.8 / mg/L 9.213 / lbs/day
Jul2019 Week 4 99.3 / mg/L /
Jul 2019 Average 55.1 / mg/L 9.213 / lbs/day
2019 Quarter 3 55.1 / mg/L 9.213 / lbs/day
2019 2nd 6 Months(Avg) 55.1 / mg/L 9.213 / lbs/day
2019 2nd 6...(Max) 99.3 / mg/L 9.213 / lbs/day
2019 2nd 6...(Min) 10.8 / mg/L /
2019 2nd 6...(Count) 2 1
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/17/2019 S Biogen071719Self < 0.0005 / mg/L < 0.000427 / lbs/day
07/30/2019 P Biogen073019POTW < 0.00008 / mg/L < /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 9

•
Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
Jul 2019 Week 3 < 0.0005 / m < 0.000427 / lbs/day
Y
Jul 2019 Week 4 < 0.00008 / mg/L < /
Jul 2019 Average < 0.00029 / mg/L < 0.000427 / lbs/day
2019 Quarter 3 < 0.00029 / mg/L < 0.000427 / lbs/day
2019 2nd 6 Months(Avg) < 0.00029 / mg/L < 0.000427 / lbs/day
2019 2nd 6...(Max) < 0.0005 / mg/L < 0.000427 / lbs/day
2019 2nd 6...(Min) < 0.00008 / mg/L < /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/17/2019 S Biogen071719Self 28.2 / mg/L 24.0549 / lbs/day
07/30/2019 P Biogen073019POTW 80 / mg/L /
Jul 2019 Week 3 28.2 / mg/L 24.0549 / lbs/day
Jul2019 Week 4 80 / mg/L /
Jul 2019 Average 54.1 / mg/L 24.0549 / lbs/day
2019 Quarter 3 54.1 / mg/L 24.0549 / lbs/day
2019 2nd 6 Months(Avg) 54.1 / mg/L 24.0549 / lbs/day
2019 2nd 6...(Max) 80 / mg/L 24.0549 / lbs/day
2019 2nd 6...(Min) 28.2 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
07/17/2019 S Biogen071719Self 39.4 / mg/L 33.61 / lbs/day
07/30/2019 P Biogen073019POTW 130 / mg/L /
Jul 2019 Week 3 39.4 / mg/L 33.61 / lbs/day
Jul 2019 Week 4 130 / mg/L /
Jul 2019 Average 84.7 / mg/L 33.61 / lbs/day
2019 Quarter 3 84.7 / mg/L 33.61 / lbs/day
2019 2nd 6 Months(Avg) 84.7 / mg/L 33.61 / lbs/day
2019 2nd 6...(Max) 130 / , mg/L 33.61 / lbs/day
2019 2nd 6...(Min) 39.4 / mg/L /
2019 2nd 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/30/2019 P Biogen073019POTW < 0.005 / 12.19 mg/L < /
Jul 2019 Week 4 < 0.005 / mg/L < /
Jul 2019 Average < 0.005 /4.83 mg/L < /
2019 Quarter 3 < 0.005 / mg/L < /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 9

Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/17/2019 S Biogen071719Self < 0.05 / mg/L < 0.0427 / lbs/day
07/30/2019 P Biogen073019POTW < 0.05 / mg/L < /
Jul 2019 Week 3 < 0.05 / mg/L < 0.0427 / lbs/day
Jul 2019 Week 4 < 0.05 / mg/L < /
Jul 2019 Average < 0.05 / mg/L < 0.0427 / lbs/day
2019 Quarter 3 < 0.05 / mg/L < 0.0427 / lbs/day
2019 2nd 6 Months(Avg) < 0.05 / mg/L < 0.0427 / lbs/day
2019 2nd 6...(Max) < 0.05 / mg/L < 0.0427 / lbs/day
2019 2nd 6...(Min) < 0.05 / mg/L < /
2019 2nd 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/30/2019 P Biogen073019POTW < 0.005 / 12.19 mg/L < /
Jul 2019 Week 4 < 0.005 / mg/L < /
Jul 2019 Average < 0.005 /4.83 mg/L < /
2019 Quarter 3 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 9

Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : I
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/17/2019 S Biogen071719Self 0.000008 /0.000142 mg/L /
10/02/2019 P Biogen100219POTWH 0.000008 /0.000142 mg/L /
g
Jul 2019 Week 3 0.000008 / mg/L /
Oct 2019 Week 1 0.000008 / mg/L /
Jul 2019 Average 0.000008 / mg/L /
Oct 2019 Average 0.000008 / mg/L /
2019 Quarter 3 0.000008 / mg/L /
2019 Quarter 4 0.000008 / mg/L /
2019 2nd 6 Months(Avg) 0.0000083 / mg/L /
2019 2nd 6...(Max) 0.0000083 / mg/L /
2019 2nd 6...(Min) 0.0000083 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/30/2019 P Biogen073019POTW < 0.005 / 1.77 mg/L < /
Jul 2019 Week 4 < 0.005 / mg/L < /
Jul 2019 Average < 0.005 /0.41 mg/L < /
2019 Quarter 3 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 9
L

Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/30/2019 P Biogen073019POTW < 0.005 / 12.19 mg/L < /
Jul2019 Week 4 < 0.005 / mg/L < /
Jul2019 Average < 0.005 /4.83 mg/L < /
2019 Quarter 3 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/17/2019 S Biogen071719Self 0.4 / mg/L 0.333 / lbs/day
07/30/2019 P Biogen073019POTW 0.2 / mg/L /
Jul 2019 Week 3 0.4 / mg/L 0.333 / lbs/day
Jul2019 Week 4 0.2 / mg/L /
Jul 2019 Average 0.3 / mg/L 0.333 / lbs/day
2019 Quarter 3 0.3 / mg/L 0.333 / lbs/day
2019 2nd 6 Months(Avg) 0.3 / mg/L 0.333 / lbs/day
2019 2nd 6...(Max) 0.4 / mg/L 0.333 / lbs/day
2019 2nd 6...(Min) 0.2 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/17/2019 S Biogen071719Self 4.6 / mg/L 3.924 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 9

Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/30/2019 P Biogen073019POTW 7.19 / mg/L 5.956 / lbs/day
Jul 2019 Week 3 4.7 / mg/L 4.009 / lbs/day
Jul 2019 Week 4 7.19 / mg/L 5.956 / lbs/day
Jul2019 Average 5.95 / mg/L 4.982 / lbs/day
2019 Quarter 3 5.95 / mg/L 4.982 / lbs/day
2019 2nd 6 Months(Avg) 5.95 / mg/L 4.982 / lbs/day
2019 2nd 6...(Max) 7.19 / mg/L 5.956 / lbs/day
2019 2nd 6...(Min) 4.7 / mg/L 4.009 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
07/30/2019 P Biogen073019POTW < 2.5 /200 mg/L < /
Jul 2019 Week 4 < 2.5 / mg/L < /
Jul 2019 Average < 2.5 / mg/L < /
2019 Quarter 3 < 2.5 / mg/L < /
2019 2nd 6 Months(Avg) < 2.5 / mg/L < /
2019 2nd 6...(Max) < 2.5 / mg/L < /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/17/2019 S Biogen071719Self 6.3 /5.5- 10.5 SU /
07/30/2019 P Biogen073019POTW 7.8 /5.5- 10.5 SU /
Jul 2019 Week 3 6.3 / SU /
Jul 2019 Week 4 7.8 / SU /
Jul 2019 Average 7.05 / SU /
2019 Quarter 3 7.05 / SU /
2019 2nd 6 Months(Avg) 7.05 / SU /
2019 2nd 6...(Max) 7.8 / SU /
2019 2nd 6...(Min) 6.3 / SU /
2019 2nd 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 9

Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/30/2019 P Biogen073019POTW 30 /66 °C /
Jul2019 Week 4 30 / °C /
Jul 2019 Average 30 / °C /
2019 Quarter 3 30 / °C /
2019 2nd 6 Months(Avg) 30 / °C /
2019 2nd 6...(Max) 30 / °C /
2019 2nd 6...(Min) 30 / °C /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/17/2019 S Biogen071719Self 4.3 / mg/L 3.668 / lbs/day
07/30/2019 P Biogen073019POTW 6.97 / mg/L 5.773 / lbs/day
Jul 2019 Week 3 4.3 / mg/L 3.668 / lbs/day
Jul2019 Week 4 6.97 / mg/L 5.773 / lbs/day
Jul 2019 Average 5.64 / mg/L 4.721 / lbs/day
2019 Quarter 3 5.64 / mg/L 4.721 / lbs/day
2019 2nd 6 Months(Avg) 5.64 / mg/L 4.721 / lbs/day
2019 2nd 6...(Max) 6.97 / mg/L 5.773 / lbs/day
2019 2nd 6...(Min) 4.3 / mg/L 3.668 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/17/2019 S Biogen071719Self 0.83 / mg/L 0.708 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 9

Biogen
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/30/2019 P Biogen073019POTW 1.36 / mg/L /
Jul 2019 Week 3 0.83 / mg/L 0.708 / lbs/day
Jul2019 Week 4 1.36 / mg/L /
Jul 2019 Average 1.095 / mg/L 0.708 / lbs/day
2019 Quarter 3 1.095 / mg/L 0.708 / lbs/day
2019 2nd 6 Months(Avg) 1.095 / mg/L 0.7080 / lbs/day
2019 2nd 6...(Max) 1.36 / mg/L 0.7080 / lbs/day
2019 2nd 6...(Min) 0.83 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
m 4.862153 lbs/day
S Biogen071719Self 5.7 / mg/L /
07/30/2019 P Biogen073019POTW 121 / mg/L /
Jul 2019 Week 3 5.7 / mg/L 4.862153 / lbs/day
Jul 2019 Week 4 121 / mg/L /
Jul 2019 Average 63.4 / mg/L 4.862153 / lbs/day
2019 Quarter 3 63.4 / mg/L 4.862153 / lbs/day
2019 2nd 6 Months(Avg) 63.4 / mg/L 4.86215 / lbs/day
2019 2nd 6...(Max) 121 / mg/L 4.862153 / lbs/day
2019 2nd 6...(Min) 5.7 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/17/2019 S Biogen071719Self 0.158 / mg/L 0.134775 / lbs/day
07/30/2019 P Biogen073019POTW 0.612 / mg/L /
Jul 2019 Week 3 0.158 / mg/L 0.134775 / lbs/day
Jul 2019 Week 4 0.612 / mg/L /
Jul2019 Average 0.385 / mg/L 0.134775 / lbs/day
2019 Quarter 3 0.385 / mg/L 0.134775 / lbs/day
2019 2nd 6 Months(Avg) 0.385 / mg/L 0.134775 / lbs/day
2019 2nd 6...(Max) 0.612 / mg/L 0.134775 / lbs/day
2019 2nd 6...(Min) 0.158 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 9

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
08/06/2019 S Cintas080619Se1f 0.779 / mg/L 0.330911 / lbs/day
Aug 2019 Week 1 0.779 / mg/L 0.330911 / lbs/day
Aug 2019 Average 0.779 / mg/L 0.330911 / lbs/day
2019 Quarter 3 0.779 / mg/L 0.330911 / lbs/day
2019 2nd 6 Months(Avg) 0.779 / mg/L 0.330911 / lbs/day
2019 2nd 6...(Max) 0.779 / mg/L 0.330911 / lbs/day
2019 2nd 6...(Min) 0.779 / mg/L 0.330911 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/23/2019 S Cintas072319Self 7.4 / mg/L 1.0947 / lbs/day
07/26/2019 P Cintas072619POTW 4.9 / mg/L 2.9723 / lbs/day
08/06/2019 S Cintas080619Self 23.9 / mg/L 10.1525 / lbs/day
09/13/2019 S Cintas091319Self 22.8 / mg/L 14.045 / lbs/day
10/08/2019 S Cintas100819Self 8.8 / mg/L 5.2176 / lbs/day
11/08/2019 S Cintas110819Self 4.4 / mg/L 2.309 / lbs/day
12/10/2019 S Cintas121019Self 10.3 / mg/L 6.1583 / lbs/day
Jul 2019 Week 4 6.15 / mg/L 2.0335 / lbs/day
Aug 2019 Week 1 23.9 / mg/L 10.1525 / lbs/day
Sep 2019 Week 2 22.8 / mg/L 14.045 / lbs/day 1
Oct 2019 Week 2 8.8 / mg/L 5.2176 / lbs/day
Nov 2019 Week 2 4.4 / mg/L 2.309 / lbs/day
Dec 2019 Week 2 10.3 / mg/L 6.1583 / lbs/day
Jul2019 Average 6.15 / mg/L 2.0335 / lbs/day 1
Aug 2019 Average 23.9 / mg/L 10.1525 / lbs/day
Sep 2019 Average 22.8 / mg/L 14.045 / lbs/day
Oct 2019 Average 8.8 / mg/L 5.2176 / lbs/day
Nov 2019 Average 4.4 / mg/L 2.309 / lbs/day
Dec 2019 Average 10.3 / mg/L 6.1583 / lbs/day
2019 Quarter 3 14.75 / mg/L 7.0661 / lbs/day
2019 Quarter 4 7.83 / mg/L 4.5616 / lbs/day
2019 2nd 6 Months(Avg) 11.79 / mg/L 5.9928 / lbs/day
2019 2nd 6...(Max) 23.9 / mg/L 14.0450 / lbs/day
2019 2nd 6...(Min) 4.4 / mg/L 1.0947 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S Cintas0719Flow 0.07476 /0.180 MGD /
08/31/2019 S Cintas0819Flow 0.060525 /0.180 MGD /
09/30/2019 S Cintas0919Flow 0.059344 /0.180 MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 17

,
Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
10/31/2019 S Cintas1019Flow 0.063637 /0.180 MGD /
11/30/2019 S Cintas1119Flow 0.055508 /0.180 MGD /
12/31/2019 S Cintas1219Flow 0.060618 /0.180 MGD /
Jul 2019 Week 4 0.07476 / MGD /
Aug 2019 Week 4 0.060525 / MGD /
Sep 2019 Week 4 0.059344 / MGD /
Oct 2019 Week 4 0.063637 / MGD /
Nov 2019 Week 4 0.055508 / MGD /
Dec 2019 Week 4 0.060618 / MGD /
Jul 2019 Average 0.07476 /0.120 MGD /
Aug 2019 Average 0.060525 /0.120 MGD /
Sep 2019 Average 0.059344 /0.120 MGD /
Oct 2019 Average 0.063637 /0.120 MGD /
Nov 2019 Average 0.055508 /0.120 MGD /
Dec 2019 Average 0.060618 /0.120 MGD /
2019 Quarter 3 0.064876 / MGD /
2019 Quarter 4 0.059921 / MGD /
2019 2nd 6 Months(Avg) 0.062399 / MGD /
2019 2nd 6...(Max) 0.07476 / MGD /
2019 2nd 6...(Min) 0.055508 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
07/23/2019 S Cintas072319Se1f 388 / mg/L 57.399 / lbs/day
07/26/2019 P Cintas072619POTW 575 / mg/L 348.796 / lbs/day
08/02/2019 P Cintas080219POTW 1470 / mg/L /
08/06/2019 S Cintas080619Se1f 463 / mg/L 196.678 / lbs/day
09/13/2019 S Cintas091319Se1f 181 / mg/L 111.498 / lbs/day
09/17/2019 P Cintas091719POTW 770 / mg/L /
10/08/2019 S Cintas100819Se1f 241 / mg/L 142.891 / lbs/day
10/25/2019 P Cintas102519POTW 153 / mg/L /
11/08/2019 S Cintas110819Self 196 / mg/L 102.855 / lbs/day
11/21/2019 P Cintas112119POTW 220 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 17

•
Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
BOO
12/10/2019 S Cintas121019Self 387 / mg/L 231.385 / lbs/day
12/10/2019 P Cintas121019POTW 356 / mg/L /
Jul 2019 Week 4 481.5 / mg/L 203.097 / lbs/day
Aug 2019 Week 1 966.5 / mg/L 196.678 / lbs/day
Sep 2019 Week 2 181 / mg/L 111.498 / lbs/day
Sep 2019 Week 3 770 / mg/L /
Oct 2019 Week 2 241 / mg/L 142.891 / lbs/day
Oct 2019 Week 4 153 / mg/L /
Nov 2019 Week 2 196 / mg/L 102.855 / lbs/day
Nov 2019 Week 3 220 / mg/L /
Dec 2019 Week 2 371.5 / mg/L 231.385 / lbs/day
Jul 2019 Average 481.5 / mg/L 203.097 / lbs/day
Aug 2019 Average 966.5 / mg/L 196.678 / lbs/day
Sep 2019 Average 475.5 / mg/L 111.498 / lbs/day
Oct 2019 Average 197 / mg/L 142.891 / lbs/day
Nov 2019 Average 208 / mg/L 102.855 / lbs/day
Dec 2019 Average 371.5 / mg/L 231.385 / lbs/day
2019 Quarter 3 641.2 / mg/L 178.592 / lbs/day
2019 Quarter 4 258.8 / mg/L 159.044 / lbs/day
2019 2nd 6 Months(Avg) 450 / mg/L 170.214 / lbs/day
2019 2nd 6...(Max) 1470 / mg/L 348.796 / lbs/day
2019 2nd 6...(Min) 153 / mg/L /
2019 2nd 6...(Count) 12 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/06/2019 S Cintas080619Self 0.0013 / mg/L 0.000552 / lbs/day
Aug 2019 Week 1 0.0013 / mg/L 0.000552 / lbs/day
Aug 2019 Average 0.0013 / mg/L 0.000552 / lbs/day
2019 Quarter 3 0.0013 / mg/L 0.000552 / lbs/day
2019 2nd 6 Months(Avg) 0.0013 / mg/L 0.000552 / lbs/day
2019 2nd 6...(Max) 0.0013 / mg/L 0.000552 / lbs/day
2019 2nd 6...(Min) 0.0013 / mg/L 0.000552 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/26/2019 P Cintas072619POTW I20 / mg/L 72.7922 / lbs/day
12/10/2019 S Cintas121019Self 110 / mg/L 65.7684 / lbs/day
Jul 2019 Week 4 120 / mg/L 72.7922 / lbs/day
Dec 2019 Week 2 110 / mg/L 65.7684 / lbs/day
Jul2019 Average 120 / mg/L 72.7922 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
Dec 2019 Average 110 / mg/L 65.7684 / lbs/day
2019 Quarter 3 120 / mg/L 72.7922 / lbs/day
2019 Quarter 4 I I 0 / mg/L 65.7684 / lbs/day
2019 2nd 6 Months(Avg) 115 / mg/L 69.2803 / lbs/day
2019 2nd 6...(Max) 120 / mg/L 72.7922 / lbs/day
2019 2nd 6...(Min) 110 / mg/L 65.7684 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
07/23/2019 S Cintas072319Self < 0.003 / mg/L < 0.00037 / lbs/day
08/06/2019 S Cintas080619Self 0.009 / mg/L 0.003993 / lbs/day
09/13/2019 S Cintas091319Self 0.006 / mg/L 0.003511 / lbs/day
10/08/2019 S Cintas100819Self 0.006 / mg/L 0.003795 / lbs/day
11/08/2019 S Cintas110819Self < 0.003 / mg/L < 0.001312 / lbs/day
12/10/2019 S Cintas121019Se1f 0.01 / mg/L 0.005859 / lbs/day
Jul 2019 Week 4 < 0.003 / mg/L < 0.00037 / lbs/day
Aug 2019 Week 1 0.009 / mg/L 0.003993 / lbs/day
Sep 2019 Week 2 0.006 / mg/L 0.003511 / lbs/day
Oct 2019 Week 2 0.006 / mg/L 0.003795 / lbs/day
Nov 2019 Week 2 < 0.003 / mg/L < 0.001312 / lbs/day
Dec 2019 Week 2 0.01 / mg/L 0.005859 / lbs/day
Jul 2019 Average < 0.003 / mg/L < 0.00037 / lbs/day
Aug 2019 Average 0.009 / mg/L 0.003993 / lbs/day
Sep 2019 Average 0.006 / mg/L 0.003511 / lbs/day
Oct 2019 Average 0.006 / mg/L 0.003795 / lbs/day
Nov 2019 Average < 0.003 / mg/L < 0.001312 / lbs/day
Dec 2019 Average 0.01 / mg/L 0.005859 / lbs/day
2019 Quarter 3 < 0.006 / mg/L < 0.002625 / lbs/day
2019 Quarter 4 < 0.006 / mg/L < 0.003655 / lbs/day
2019 2nd 6 Months(Avg) < 0.006 / mg/L < 0.00314 / lbs/day
2019 2nd 6...(Max) 0.010 / mg/L 0.005859 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < 0.000370 / lbs/day
2019 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
07/23/2019 S Cintas072319Self 0.113 / mg/L 0.016717 / lbs/day
08/06/2019 S Cintas080619Self 0.156 / mg/L 0.066267 / lbs/day
09/13/2019 S Cintas091319Self 0.116 / mg/L 0.071457 / lbs/day
10/08/2019 S Cintas100819Self 0.102 / mg/L 0.060477 / lbs/day
11/08/2019 S Cintas110819Self 0.064 / mg/L 0.033585 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
12/10/2019 S Cintas121019Self 0.12 / mg/L 0.071747 / lbs/day
Jul 2019 Week 4 0.113 / mg/L 0.016717 / lbs/day
Aug 2019 Week 1 0.156 / mg/L 0.066267 / lbs/day
Sep 2019 Week 2 0.116 / mg/L 0.071457 / lbs/day
Oct 2019 Week 2 0.102 / mg/L 0.060477 / lbs/day
Nov 2019 Week 2 0.064 / mg/L 0.033585 / lbs/day
Dec 2019 Week 2 0.12 / mg/L 0.071747 / lbs/day
Jul2019 Average 0.113 / mg/L 0.016717 / lbs/day
Aug 2019 Average 0.156 / mg/L 0.066267 / lbs/day
Sep 2019 Average 0.116 / mg/L 0.071457 / lbs/day
Oct 2019 Average 0.102 / mg/L 0.060477 / lbs/day
Nov 2019 Average 0.064 / mg/L 0.033585 / lbs/day
Dec 2019 Average 0.12 / mg/L 0.071747 / lbs/day
2019 Quarter 3 0.128 / mg/L 0.05148 / lbs/day
2019 Quarter 4 0.095 / mg/L 0.05527 / lbs/day
2019 2nd 6 Months(Avg) 0.112 / mg/L 0.053375 / lbs/day
2019 2nd 6...(Max) 0.156 / mg/L 0.071747 / lbs/day
2019 2nd 6...(Min) 0.064 / mg/L 0.016717 / lbs/day
2019 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/23/2019 S Cintas072319Self < 0.05 / mg/L < 0.0074 / lbs/day
07/26/2019 P Cintas072619POTW 0.15 / mg/L 0.091 / lbs/day
08/06/2019 S Cintas080619Self < 0.05 / mg/L < 0.0212 / lbs/day
09/13/2019 S Cintas091319Self < 0.05 / mg/L < 0.0308 / lbs/day
10/08/2019 S Cintas100819Self 1.2 / mg/L 0.7115 / lbs/day
11/08/2019 S Cintas110819Se1f < 0.05 / mg/L < 0.0262 / lbs/day
12/10/2019 S Cintas121019Self 0.37 / mg/L 0.2212 / lbs/day
Jul 2019 Week 4 < 0.1 / mg/L < 0.0492 / lbs/day
Aug 2019 Week 1 < 0.05 / mg/L < 0.0212 / lbs/day
Sep 2019 Week 2 < 0.05 / mg/L < 0.0308 / lbs/day 1
Oct 2019 Week 2 1.2 / mg/L 0.7115 / lbs/day
Nov 2019 Week 2 < 0.05 / mg/L < 0.0262 / lbs/day
Dec 2019 Week 2 0.37 / mg/L 0.2212 / lbs/day
Jul 2019 Average < 0.1 / mg/L < 0.0492 / lbs/day
Aug 2019 Average < 0.05 / mg/L < 0.0212 / lbs/day
Sep 2019 Average < 0.05 / mg/L < 0.0308 / lbs/day
Oct 2019 Average 1.2 / mg/L 0.7115 / lbs/day
Nov 2019 Average < 0.05 / mg/L < 0.0262 / lbs/day
Dec 2019 Average 0.37 / mg/L 0.2212 / lbs/day
2019 Quarter 3 < 0.08 / mg/L < 0.0376 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outtalk 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2019 Quarter 4 < 0.54 / mg/L < 0.3196 / lbs/day
2019 2nd 6 Months(Avg) < 0.27 / mg/L < 0.1585 / lbs/day
2019 2nd 6...(Max) 1.2 / mg/L 0.7115 / lbs/day
2019 2nd 6...(Min) < 0.05 / mg/L < 0.0074 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
07/23/2019 S Cintas072319Se1f 0.0165 / mg/L 0.002441 / lbs/day
08/06/2019 S Cintas080619Self 0.016 / mg/L 0.006797 / lbs/day
09/13/2019 S Cintas091319Se1f 0.0099 / mg/L 0.006098 / lbs/day
10/08/2019 S Cintas100819Self 0.0162 / mg/L 0.009605 / lbs/day
11/08/2019 S Cintas110819Self 0.014 / mg/L 0.007347 / lbs/day
12/10/2019 S Cintas121019Se1f 0.019 / mg/L 0.01136 / lbs/day
Jul2019 Week 4 0.0165 / mg/L 0.002441 / lbs/day
Aug019 Week 1 0.016 / mg/L0.006797 lbs/day
/
Sep 2019 Week 2 0.0099 / mg/L 0.006098 / lbs/day
Oct 2019 Week 2 0.0162 / mg/L 0.009605 / lbs/day
Nov 2019 Week 2 0.014 / mg/L 0.007347 / lbs/day
Dec 2019 Week 2 0.019 / mg/L 0.01136 / lbs/day
Jul 2019 Average 0.0165 / mg/L 0.002441 / lbs/day
Aug 2019 Average 0.016 / mg/L 0.006797 / lbs/day
Sep 2019 Average 0.0099 / mg/L 0.006098 / lbs/day
Oct 2019 Average 0.0162 / mg/L 0.009605 / lbs/day
Nov 2019 Average 0.014 / mg/L 0.007347 / lbs/day
Dec 2019 Average 0.019 / mg/L 0.01136 / lbs/day
2019 Quarter 3 0.0141 / mg/L 0.005112 / lbs/day
2019 Quarter 4 0.0164 / mg/L 0.009437 / lbs/day
2019 2nd 6 Months(Avg) 0.0153 / mg/L 0.007275 / lbs/day
2019 2nd 6...(Max) 0.019 / mg/L 0.011360 / lbs/day
2019 2nd 6...(Min) 0.0099 / mg/L 0.002441 / lbs/day
2019 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/25/2019 P Cintas072519POTWH 0.000022 /0.000142 mg/L /
g
08/06/2019 S Cintas080619Self 0.000008 /0.000142 mg/L /
Aug 2019 Week 1 0.000008 / mg/L /
Jul 2019 Week 4 0.000022 / mg/L /
Jul 2019 Average 0.000022 / mg/L /
Aug 2019 Average 0.000008 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
2019 Quarter 3 0.000015 / mg/L /
2019 2nd 6 Months(Avg) 0.0000148 / mg/L /
2019 2nd 6...(Max) 0.0000219 / mg/L /
2019 2nd 6...(Min) 0.0000078 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/06/2019 S Cintas080619Se1f 0 / mg/L 0.0108 / lbs/day
11/08/2019 S Cintas110819Self 0 / mg/L 0.0163 / lbs/day
12/10/2019 S Cintas121019Self 0 / mg/L 0.0138 / lbs/day
Aug 2019 Week 1 0 / mg/L 0.0108 / lbs/day
Nov 2019 Week 2 0 / mg/L 0.0163 / lbs/day
Dec 2019 Week 2 0 / mg/L 0.0138 / lbs/day
Aug 2019 Average 0 / mg/L 0.0108 / lbs/day
Nov 2019 Average 0 / mg/L 0.0163 / lbs/day
Dec 2019 Average 0 / mg/L 0.0138 / lbs/day
2019 Quarter 3 0 / mg/L 0.0108 / lbs/day
2019 Quarter 4 0 / mg/L 0.015 / lbs/day 1
2019 2nd 6 Months(Avg) 0.026 / mg/L 0.0136 / lbs/day
2019 2nd 6...(Max) 0.031 / mg/L 0.0163 / lbs/day
2019 2nd 6...(Min) 0.023 / mg/L 0.0108 / lbs/day
2019 2nd 6...(Count) 3 / 3 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
07/23/2019 S Cintas072319Self 0.0206 / mg/L 0.003047 / lbs/day
08/06/2019 S Cintas080619Self 0.025 / mg/L 0.01062 / lbs/day
09/13/2019 S Cintas091319Self 0.0257 / mg/L 0.015831 / lbs/day
10/08/2019 S Cintas100819Self 0.0222 / mg/L 0.013163 / lbs/day
11/08/2019 S Cintas110819Self 0.02 / mg/L 0.010495 / lbs/day
12/10/2019 S Cintas121019Self 0.022 / mg/L 0.013154 / lbs/day
Jul 2019 Week 4 0.0206 / mg/L 0.003047 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall:• 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Aug 2019 Week 1 0.025 / mg/L 0.01062 / lbs/day
Sep 2019 Week 2 0.0257 / mg/L 0.015831 / lbs/day
Oct 2019 Week 2 0.0222 / mg/L 0.013163 / lbs/day
Nov 2019 Week 2 0.02 / mg/L 0.010495 / lbs/day
Dec 2019 Week 2 0.022 / mg/L 0.013154 / lbs/day
Jul 2019 Average 0.0206 / mg/L 0.003047 / lbs/day
Aug 2019 Average 0.025 / mg/L 0.01062 / lbs/day
Sep 2019 Average 0.0257 / mg/L 0.015831 / lbs/day
Oct 2019 Average 0.0222 / mg/L 0.013163 / lbs/day
Nov 2019 Average 0.02 / mg/L 0.010495 / lbs/day
Dec 2019 Average 0.022 / mg/L 0.013154 / lbs/day
2019 Quarter 3 0.0238 / mg/L 0.009833 / lbs/day
2019 Quarter 4 0.0214 / mg/L 0.012271 / lbs/day
2019 2nd 6 Months(Avg) 0.0226 / mg/L 0.011052 / lbs/day
2019 2nd 6...(Max) 0.0257 / mg/L 0.015831 / lbs/day
2019 2nd 6...(Min) 0.02 / mg/L 0.003047 / lbs/day
2019 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/23/2019 S Cintas072319Self 0.1 / mg/L 0.009 / lbs/day
07/26/2019 P Cintas072619POTW < 0.1 / mg/L < 0.03 / lbs/day
08/06/2019 S Cintas080619Se1f 0.2 / mg/L 0.072 / lbs/day
09/13/2019 S Cintas091319Se1f 0.1 / mg/L 0.041 / lbs/day
10/08/2019 S Cintas100819Self 0.1 / mg/L 0.031 / lbs/day
11/08/2019 S Cintas110819Self 0.1 / mg/L 0.039 / lbs/day
12/10/2019 S Cintas121019Self < 0 / mg/L < 0.012 / lbs/day
Jul 2019 Week 4 < 0.1 / mg/L < 0.02 / lbs/day
Aug 2019 Week 1 0.2 / mg/L 0.072 / lbs/day
Sep 2019 Week 2 0.1 / mg/L 0.041 / lbs/day
Oct 2019 Week 2 0.1 / mg/L 0.031 / lbs/day
Nov 2019 Week 2 0.1 / mg/L 0.039 / lbs/day
Dec 2019 Week 2 < 0 / mg/L < 0.012 / lbs/day
Jul 2019 Average < 0.1 / mg/L < 0.02 / lbs/day
Aug 2019 Average 0.2 / mg/L 0.072 / lbs/day
Sep 2019 Average 0.1 / mg/L 0.041 / lbs/day
Oct 2019 Average 0.1 / mg/L 0.031 / lbs/day
Nov 2019 Average 0.1 / mg/L 0.039 / lbs/day
Dec 2019 Average < 0 / mg/L < 0.012 / lbs/day
2019 Quarter 3 < 0.1 / mg/L < 0.038 / lbs/day
2019 Quarter 4 < 0 / mg/L < 0.027 / lbs/day
2019 2nd 6 Months(Avg) < 0.1 / mg/L < 0.034 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2019 2nd 6...(Max) 0.2 / mg/L 0.072 / lbs/day
2019 2nd 6...(Min) < 0.0 / mg/L < 0.009 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/23/2019 S Cintas072319Se1f 30.4 / mg/L 4.497 / lbs/day
07/26/2019 P Cintas072619POTW 26.7 / mg/L 16.196 / lbs/day
08/06/2019 S Cintas080619Se1f 87.3 / mg/L 37.084 / lbs/day
09/13/2019 S Cintas091319Self 0.59 / mg/L 0.363 / lbs/day
10/08/2019 S Cintasl00819Self 32.9 / mg/L 19.507 / lbs/day
11/08/2019 S Cintas110819Self 18.9 / mg/L 9.918 / lbs/day
12/10/2019 S Cintas121019Self 29.6 / mg/L 17.698 / lbs/day
Jul 2019 Week 4 28.55 / mg/L 10.347 / lbs/day
Aug 2019 Week 1 87.3 / mg/L 37.084 / lbs/day
Sep 2019 Week 2 0.59 / mg/L 0.363 / lbs/day
Oct 2019 Week 2 32.9 / mg/L 19.507 / lbs/day
Nov 2019 Week 2 18.9 / mg/L 9.918 / lbs/day
Dec 2019 Week 2 29.6 / mg/L 17.698 / lbs/day
Jul2019 Average 28.55 / mg/L 10.347 / lbs/day
Aug 2019 Average 87.3 / mg/L 37.084 / lbs/day
Sep 2019 Average 0.59 / mg/L 0.363 / lbs/day
Oct 2019 Average 32.9 / mg/L 19.507 / lbs/day
Nov 2019 Average 18.9 / mg/L 9.918 / lbs/day
' Dec 2019 Average 29.6 / mg/L 17.698 / lbs/day
2019 Quarter 3 36.25 / mg/L 14.535 / lbs/day
2019 Quarter 4 27.13 / mg/L 15.707 / lbs/day
2019 2nd 6 Months(Avg) 32.34 / mg/L 15.038 / lbs/day
2019 2nd 6...(Max) 87.3 / mg/L 37.084 / lbs/day
2019 2nd 6...(Min) 0.59 / mg/L 0.363 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
07/23/2019 S Cintas072319Self 11.9 / 100 mg/L 1.760426 / lbs/day
07/26/2019 P Cintas072619POTW 9 / 100 mg/L 5.459414 / lbs/day
08/06/2019 S Cintas080619Self 35.9 / 100 mg/L 15.249945 / lbs/day
09/13/2019 S Cintas091319Self 8.1 / 100 mg/L 4.989674 / lbs/day
10/08/2019 S Cintas100819Se1f 11.2 /100 mg/L 6.640562 / lbs/day
11/08/2019 S Cintas110819Self 14.5 / 100 mg/L 7.609157 / lbs/day
12/10/2019 S Cintas121019Self 18.6 /100 mg/L 11.12084 / lbs/day
Jul 2019 Week 4 10.5 / mg/L 3.60992 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,HEM(Polar)
Aug 2019 Week 1 35.9 / mg/L 15.249945 / lbs/day
Sep 2019 Week 2 8.1 / mg/L 4.989674 / lbs/day
Oct 2019 Week 2 11.2 / mg/L 6.640562 / lbs/day
Nov 2019 Week 2 14.5 / mg/L 7.609157 / lbs/day
Dec 2019 Week 2 18.6 / mg/L 11.12084 / lbs/day
Jul 2019 Average 10.5 / mg/L 3.60992 / lbs/day
Aug 2019 Average 35.9 / mg/L 15.249945 / lbs/day
Sep 2019 Average 8.1 / mg/L 4.989674 / lbs/day
Oct 2019 Average 11.2 / mg/L 6.640562 / lbs/day
Nov 2019 Average 14.5 / mg/L 7.609157 / lbs/day
Dec 2019 Average 18.6 / mg/L 11.12084 / lbs/day
2019 Quarter 3 16.2 / mg/L 6.864865 / lbs/day
2019 Quarter 4 14.8 / mg/L 8.456853 / lbs/day
2019 2nd 6 Months(Avg) 15.6 / mg/L 7.54715 / lbs/day
2019 2nd 6...(Max) 35.9 / mg/L 15.249945 / lbs/day
2019 2nd 6...(Min) 8.1 / mg/L 1.760426 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,SGT HEM(Non-Polar)
07/23/2019 S Cintas072319Self < 2.5 /100 mg/L < 0.3698 / lbs/day
07/26/2019 P Cintas072619POTW < 2.5 /100 mg/L < 1.5165 / lbs/day
08/06/2019 S Cintas080619Self 10.7 / 100 mg/L 4.5452 / lbs/day
09/13/2019 S Cintas091319Se1f 5.6 / 100 mg/L 3.4497 / lbs/day
10/08/2019 S Cintas100819Self < 2.5 / 100 mg/L < 1.4823 / lbs/day
11/08/2019 S Cintas110819Self < 2.5 / 100 mg/L < 1.3119 / lbs/day
12/10/2019 S Cintas121019Self 8.4 / 100 mg/L 5.0223 / lbs/day
Jul2019 Week 4 < 2.5 / mg/L < 0.9432 / lbs/day
Aug 2019 Week 1 10.7 / mg/L 4.5452 / lbs/day
Sep 2019 Week 2 5.6 / mg/L 3.4497 / lbs/day
Oct 2019 Week 2 < 2.5 / mg/L < 1.4823 / lbs/day
Nov 2019 Week 2 < 2.5 / mg/L < 1.3119 / lbs/day
Dec 2019 Week 2 8.4 / mg/L 5.0223 / lbs/day
Jul 2019 Average < 2.5 / mg/L < 0.9432 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 17

•
Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampielD Result/Limit Mass/Limit
Oil&Grease,SGT-HEM(Non-Polar)
Aug 2019 Average 10.7 / mg/L 4.5452 / lbs/day
Sep 2019 Average 5.6 / mg/L 3.4497 / lbs/day
Oct 2019 Average < 2.5 / mg/L < 1.4823 / lbs/day
Nov 2019 Average < 2.5 / mg/L < 1.3119 / lbs/day
Dec 2019 Average 8.4 / mg/L 5.0223 / lbs/day
2019 Quarter 3 < 5.3 / mg/L < 2.4703 / lbs/day
2019 Quarter 4 < 4.5 / mg/L < 2.6055 / lbs/day
2019 2nd 6 Months(Avg) < 5.0 / mg/L < 2.5283 / lbs/day
2019 2nd 6...(Max) 10.7 / mg/L 5.0223 / lbs/day
2019 2nd 6...(Min) < 2.5 / mg/L < 0.3698 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SampielD Result/Limit Mass/Limit
pH
07/23/2019 S Cintas072319Self 5.9 /6.0- 10.5 SU * /
07/26/2019 P Cintas072619POTW 6.2 /6.0- 10.5 SU /
08/06/2019 S Cintas080619Self 5.9 /6.0- 10.5 SU * /
08/23/2019 S Cintas082319Self 6.6 /6.0-10.5 SU /
09/13/2019 S Cintas091319Self 7.2 /6.0- 10.5 SU /
10/08/2019 S Cintas100819Self 7.6 /6.0- 10.5 SU /
11/08/2019 S Cintas110819Self 7 /6.0-10.5 SU /
12/10/2019 S Cintas121019Self 7.1 /6.0-10.5 SU /
Jul2019 Week 4 6.05 / SU /
Aug 2019 Week 1 5.9 / SU /
Aug 2019 Week 4 6.6 / SU / j
Sep 2019 Week 2 7.2 / SU /
Oct 2019 Week 2 7.6 / SU /
Nov 2019 Week 2 7 / SU /
Dec 2019 Week 2 7.1 / SU /
Jul 2019 Average 6.05 / SU /
Aug 2019 Average 6.25 / SU /
Sep 2019 Average 7.2 / SU /
Oct 2019 Average 7.6 / SU /
Nov 2019 Average 7 / SU /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 11 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
pH
Dec 2019 Average 7.1 / SU /
2019 Quarter 3 6.36 / SU /
2019 Quarter 4 7.23 / SU /
2019 2nd 6 Months(Avg) 6.69 / SU /
2019 2nd 6...(Max) 7.6 / SU /
2019 2nd 6...(Min) 5.9 / SU /
2019 2nd 6...(Count) 8 / /
Sample Count: 8 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 2 25.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/06/2019 S Cintas080619Self < 0.0025 / mg/L < 0.001062 / lbs/day
Y
Aug 2019 Week 1 < 0.0025 / mg/L < 0.001062 / lbs/day
Aug 2019 Average < 0.0025 / mg/L < 0.001062 / lbs/day
2019 Quarter 3 < 0.0025 / mg/L < 0.001062 / lbs/day
2019 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.001062 / lbs/day
2019 2nd 6...(Max) < 0.0025 / mg/L < 0.001062 / lbs/day
2019 2nd 6...(Min) < 0.0025 / mg/L < 0.001062 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/23/2019 S Cintas072319Self 36.3 /66 °C /
07/26/2019 P Cintas072619POTW 34 /66 °C /
08/06/2019 S Cintas080619Self 37.3 /66 °C /
08/23/2019 S Cintas082319Se1f 39 /66 °C /
09/13/2019 S Cintas091319Se1f 39.5 /66 °C /
10/08/2019 S Cintas100819Se1f 35 /66 °C /
11/08/2019 S Cintas110819Self 26.2 /66 °C /
12/10/2019 S Cintas121019Se1f 30.5 /66 °C /
Jul2019 Week 4 35.2 / °C /
Aug 2019 Week 1 37.3 / °C /
Aug 2019 Week 4 39 / °C /
Sep 2019 Week 2 39.5 / °C /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 12 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Oct 2019 Week 2 35 / °C /
Nov 2019 Week 2 26.2 / °C /
Dec 2019 Week 2 30.5 / °C /
Jul2019 Average 35.2 / °C /
Aug 2019 Average 38.2 / °C /
Sep 2019 Average 39.5 / °C /
Oct 2019 Average 35 / °C /
Nov 2019 Average 26.2 / °C /
Dec 2019 Average 30.5 / °C /
2019 Quarter 3 37.2 / °C /
2019 Quarter 4 30.6 / °C /
2019 2nd 6 Months(Avg) 34.7 / °C /
2019 2nd 6...(Max) 39.5 / °C /
2019 2nd 6...(Min) 26.2 / °C /
2019 2nd 6...(Count) 8 / /
Sample Count: 8 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/23/2019 S Cintas072319Se1f 30.4 / mg/L 4.497 / lbs/day
07/26/2019 P Cintas072619POTW 26.7 / mg/L 16.196 / lbs/day
08/02/2019 P Cintas080219POTW 90.6 / mg/L /
08/06/2019 S Cintas080619Se1f 87.1 / mg/L 36.999 / lbs/day
09/13/2019 S Cintas091319Se1f 0.52 / mg/L 0.32 / lbs/day
09/17/2019 P Cintas091719POTW 40.3 / mg/L /
10/08/2019 S Cintas100819Se1f 32.9 / mg/L 19.507 / lbs/day
10/25/2019 P Cintas102519POTW 18.8 / mg/L /
11/08/2019 S Cintas110819Se1f 18.8 / mg/L 9.866 / lbs/day
11/21/2019 P Cintas112119POTW 17.4 / mg/L /
12/10/2019 S Cintas121019Self 29.6 / mg/L 17.698 / lbs/day
12/10/2019 P Cintas121019POTW 20 / mg/L /
Jul 2019 Week 4 28.55 / mg/L 10.347 / lbs/day
Aug 2019 Week 1 88.85 / mg/L 36.999 / lbs/day
Sep 2019 Week 2 0.52 / mg/L 0.32 / lbs/day
Sep 2019 Week 3 40.3 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 13 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
TKN
Oct 2019 Week 2 32.9 / mg/L 19.507 / lbs/day
Oct 2019 Week 4 18.8 / mg/L /
Nov 2019 Week 2 18.8 / mg/L 9.866 / lbs/day
Nov 2019 Week 3 17.4 / mg/L /
Dec 2019 Week 2 24.8 / mg/L 17.698 / lbs/day
Jul 2019 Average 28.55 / mg/L 10.347 / lbs/day
Aug 2019 Average 88.85 / mg/L 36.999 / lbs/day
Sep 2019 Average 20.41 / mg/L 0.32 / lbs/day
Oct 2019 Average 25.85 / mg/L 19.507 / lbs/day
Nov 2019 Average 18.1 / mg/L 9.866 / lbs/day
Dec 2019 Average 24.8 / mg/L 17.698 / lbs/day
2019 Quarter 3 45.94 / mg/L 14.503 / lbs/day
2019 Quarter 4 22.92 / mg/L 15.69 / lbs/day
2019 2nd 6 Months(Avg) 34.43 / mg/L 15.012 / lbs/day
2019 2nd 6...(Max) 90.6 / mg/L 36.999 / lbs/day
2019 2nd 6...(Min) 0.52 / mg/L /
2019 2nd 6...(Count) 12 / 7 /
Sample Date SampleID Result/Limit Mass/Limit
Total Phosphorus
07/23/2019 S Cintas072319Self 2.8 / mg/L 0.4142 / lbs/day
07/26/2019 P Cintas072619POTW 2.97 / mg/L 1.8016 / lbs/day
08/02/2019 P Cintas080219POTW 9.09 / mg/L /
08/06/2019 S Cintas080619Se1f 6.6 / mg/L 2.8036 / lbs/day
09/13/2019 S Cintas091319Self 5.2 / mg/L 3.2032 / lbs/day
09/17/2019 P Cintas091719POTW 3.49 / mg/L /
10/08/2019 S Cintas100819Self 2.8 / mg/L 1.6601 / lbs/day
10/25/2019 P Cintas102519POTW 1.68 / mg/L /
11/08/2019 S Cintas110819Self 1.4 / mg/L 0.7347 / lbs/day
11/21/2019 P Cintas112119POTW 2.53 / mg/L /
12/10/2019 S Cintas121019Self 2.9 / mg/L 1.7339 / lbs/day
12/10/2019 P Cintas121019POTW 2.43 / mg/L /
Jul 2019 Week 4 2.885 / mg/L 1.1079 / lbs/day
Aug 2019 Week 1 7.845 / mg/L 2.8036 / lbs/day
Sep 2019 Week 2 5.2 / mg/L 3.2032 / lbs/day
Sep 2019 Week 3 3.49 / mg/L /
Oct 2019 Week 2 2.8 / mg/L 1.6601 / lbs/day
Oct 2019 Week 4 1.68 / mg/L /
Nov 2019 Week 2 1.4 / mg/L 0.7347 / lbs/day
Nov 2019 Week 3 2.53 / mg/L /
Dec 2019 Week 2 2.665 / mg/L 1.7339 / lbs/day
Jul2019 Average 2.885 / mg/L 1.1079 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 14 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Aug 2019 Average 7.845 / mg/L 2.8036 / lbs/day
Sep 2019 Average 4.345 / mg/L 3.2032 / lbs/day
Oct 2019 Average 2.24 / mg/L 1.6601 / lbs/day
Nov 2019 Average 1.965 / mg/L 0.7347 / lbs/day
Dec 2019 Average 2.665 / mg/L 1.7339 / lbs/day
2019 Quarter 3 5.025 / mg/L 2.0557 / lbs/day
2019 Quarter 4 2.29 / mg/L 1.3762 / lbs/day
2019 2nd 6 Months(Avg) 3.658 / mg/L 1.7645 / lbs/day
2019 2nd 6...(Max) 9.09 / mg/L 3.2032 / lbs/day
2019 2nd 6...(Min) 1.4 / mg/L /
2019 2nd 6...(Count) 12 / 7 /
Sample Dale SamplelD Result/Limit Mass/Limit
TSS
07/23/2019 S Cintas072319Self 76.9 / mg/L 11.376195 / lbs/day
07/26/2019 P Cintas072619POTW 177 / mg/L 107.368476 / lbs/day
08/02/2019 P Cintas080219POTW 1610 / mg/L /
08/06/2019 S Cintas080619Self 97.3 / mg/L 41.332024 / lbs/day
09/13/2019 S Cintas091319Self 104 / mg/L 64.064944 / lbs/day
09/17/2019 P Cintas091719POTW 1650 / mg/L /
10/08/2019 S Cintas100819Self 202 / mg/L 119.767271 / lbs/day
10/25/2019 P Cintas102519POTW 147 / mg/L /
11/08/2019 S Cintas110819Self 39 / mg/L 20.46601 / lbs/day
11/21/2019 P Cintas112119POTW 152 / mg/L /
12/10/2019 S Cintas121019Self 326 / mg/L 194.91364 / lbs/day
12/10/2019 P Cintas121019POTW 432 / mg/L /
Jul 2019 Week 4 127 / mg/L 59.372336 / lbs/day
Aug 2019 Week 1 853.7 / mg/L 41.332024 / lbs/day
Sep 2019 Week 2 104 / mg/L 64.064944 / lbs/day
Sep 2019 Week 3 1650 / mg/L /
Oct 2019 Week 2 202 / mg/L 119.767271 / lbs/day
Oct 2019 Week 4 147 / mg/L /
Nov 2019 Week 2 39 / mg/L 20.46601 / lbs/day
Nov 2019 Week 3 152 / mg/L /
Dec 2019 Week 2 379 / mg/L 194.91364 / lbs/day
Jul2019 Average 127 / mg/L 59.372336 / lbs/day
Aug 2019 Average 853.7 / mg/L 41.332024 / lbs/day
Sep 2019 Average 877 / mg/L 64.064944 / lbs/day
Oct 2019 Average 174.5 / mg/L 119.767271 / lbs/day
Nov 2019 Average 95.5 / mg/L 20.46601 / lbs/day
Dec 2019 Average 379 / mg/L 194.91364 / lbs/day
2019 Quarter 3 619.2 / mg/L 56.03541 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 15 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
2019 Quarter 4 216.3 / mg/L 111.71564 / lbs/day
2019 2nd 6 Months(Avg) 417.8 / mg/L 79.8984 / lbs/day
2019 2nd 6...(Max) 1650 / mg/L 194.913640 / lbs/day
2019 2nd 6...(Min) 39 / mg/L /
2019 2nd 6...(Count) 12 / 7 /
Sample Dale SamplelD Result/Limit Mass/Limit
VOC
08/06/2019 S Cintas080619Self 0.0235 / mg/L /
Aug 2019 Week 1 0.0235 / mg/L /
Aug 2019 Average 0.0235 / mg/L /
2019 Quarter 3 0.0235 / mg/L /
2019 2nd 6 Months(Avg) 0.0235 / mg/L /
2019 2nd 6...(Max) 0.0235 / mg/L /
2019 2nd 6...(Min) 0.0235 / mg/L /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/23/2019 S Cintas072319Self 1.1 / mg/L 0.162728 / lbs/day
08/06/2019 S Cintas080619Self 1.04 / mg/L 0.441781 / lbs/day
09/13/2019 S Cintas091319Self 0.956 / mg/L 0.588905 / lbs/day
10/08/2019 S Cintas100819Self 1 / mg/L 0.592907 / lbs/day
11/08/2019 S Cintas110819Self 1.4 / mg/L 0.734677 / lbs/day
12/10/2019 S Cintas121019Self 0.99 / mg/L 0.591916 / lbs/day
Jul 2019 Week 4 1.1 / mg/L 0.162728 / lbs/day
Aug 2019 Week I 1.04 / mg/L 0.441781 / lbs/day
Sep 2019 Week 2 0.956 / mg/L 0.588905 / lbs/day
Oct 2019 Week 2 1 / mg/L 0.592907 / lbs/day
Nov 2019 Week 2 1.4 / mg/L 0.734677 / lbs/day
Dec 2019 Week 2 0.99 / mg/L 0.591916 / lbs/day
Jul2019 Average 1.1 / mg/L 0.162728 / lbs/day
Aug 2019 Average 1.04 / mg/L 0.441781 / lbs/day
Sep 2019 Average 0.956 / mg/L 0.588905 / lbs/day
Oct 2019 Average 1 / mg/L 0.592907 / lbs/day
Nov 2019 Average 1.4 / mg/L 0.734677 / lbs/day
Dec 2019 Average 0.99 / mg/L 0.591916 / lbs/day
2019 Quarter 3 1.032 / mg/L 0.397805 / lbs/day
2019 Quarter 4 1.13 / mg/L 0.639833 / lbs/day
2019 2nd 6 Months(Avg) 1.081 / mg/L 0.518819 / lbs/day
2019 2nd 6...(Max) 1.4 / mg/L 0.734677 / lbs/day
2019 2nd 6...(Min) 0.956 / mg/L 0.162728 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 16 of 17

Cintas Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date Sample ID Result/Limit Mass/Limit
Zinc
2019 2nd 6...(Count) 6 / 6 /
Wednesday,February 26,2020 'Indicates Violation "'Indicates TRC Violation Page 17 of 17

Cree. Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
08/09/2019 S CreeP8080919Self 0.434 / mg/L 1.073706 / lbs/day
Aug 2019 Week 2 0.434 / mg/L 1.073706 / lbs/day
Aug 2019 Average 0.434 / mg/L 1.073706 / lbs/day
2019 Quarter 3 0.434 / mg/L 1.073706 / lbs/day
2019 2nd 6 Months(Avg) 0.434 / mg/L 1.07371 / lbs/day
2019 2nd 6...(Max) 0.434 / mg/L 1.073706 / lbs/day
2019 2nd 6...(Min) 0.434 / mg/L 1.073706 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/09/2019 S CreeP8080919Self 15.9 / mg/L 39.3362 / lbs/day
10/24/2019 P CreeP8102419POTW 15.6 / mg/L 38.771 / lbs/day
Aug 2019 Week 2 15.9 / mg/L 39.3362 / lbs/day
Oct 2019 Week 4 15.6 / mg/L 38.771 / lbs/day
Aug 2019 Average 15.9 / mg/L 39.3362 / lbs/day
Oct 2019 Average 15.6 / mg/L 38.771 / lbs/day
2019 Quarter 3 15.9 / mg/L 39.3362 / lbs/day
2019 Quarter 4 15.6 / mg/L 38.771 / lbs/day
2019 2nd 6 Months(Avg) 15.75 / mg/L 39.0536 / lbs/day
2019 2nd 6...(Max) 15.9 / mg/L 39.3362 / lbs/day
2019 2nd 6...(Min) 15.6 / mg/L 38.7710 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S CreeP80719Flow 0.26092 / MGD /
08/31/2019 S CreeP80819F1ow 0.288418 / MGD /
09/30/2019 S CreeP80919Flow 0.273264 / MGD /
10/31/2019 S CreeP81019Flow 0.286049 / MGD /
11/30/2019 S CreeP81119Flow 0.281232 / MGD /
12/31/2019 S CreeP81219Flow 0.285863 / MGD /
Jul 2019 Week 4 0.26092 / MGD /
Aug 2019 Week 4 0.288418 / MGD /
Sep 2019 Week 4 0.273264 / MGD /
Oct 2019 Week 4 0.286049 / MGD /
Nov 2019 Week 4 0.281232 / MGD /
Dec 2019 Week 4 0.285863 / MGD /
Jul 2019 Average 0.26092 / MGD /
Aug 2019 Average 0.288418 / MGD /
Sep 2019 Average 0.273264 / MGD /
Oct 2019 Average 0.286049 / MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 10

Cree, Inc.(AI1)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SampleID Result/Limit Mass/Limit
Average Flow for Month
Nov 2019 Average 0.281232 / MGD /
Dec 2019 Average 0.285863 / MGD /
2019 Quarter 3 0.280841 / MGD /
2019 Quarter 3 0.26092 / MGD /
2019 Quarter 3 0.26092 / MGD /
2019 Quarter 3 0.280841 / MGD /
2019 Quarter 4 0.284381 / MGD /
2019 2nd 6 Months(Avg) 0.279291 / MGD /
2019 2nd 6...(Max) 0.288418 / MGD /
2019 2nd 6...(Min) 0.26092 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Barium
08/09/2019 S CreeP8080919Self 0.039 / mg/L 0.0972 / lbs/day
Aug 2019 Week 2 0.039 / mg/L 0.0972 / lbs/day
Aug 2019 Average 0.039 / mg/L 0.0972 / lbs/day
2019 Quarter 3 0.039 / mg/L 0.0972 / lbs/day
2019 2nd 6 Months(Avg) 0.039 / mg/L 0.0972 / lbs/day
2019 2nd 6...(Max) 0.039 / mg/L 0.0972 / lbs/day
2019 2nd 6...(Min) 0.039 / mg/L 0.0972 / lbs/day
2019 2nd 6...(Count) I / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium.
08/09/2019 S CreeP8080919Self < 0.0005 / mg/L < 0.001237 / lbs/day
Aug 2019 Week 2 < 0.0005 / mg/L < 0.001237 / lbs/day
Aug 2019 Average < 0.0005 / mg/L < 0.001237 / lbs/day
2019 Quarter 3 < 0.0005 / mg/L < 0.001237 / lbs/day
2019 2nd 6 Months(Avg) < 0.0005 / mg/L < 0.001237 / lbs/day
2019 2nd 6...(Max) < 0.0005 / mg/L < 0.001237 / lbs/day
2019 2nd 6...(Min) < 0.0005 / mg/L < 0.001237 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/09/2019 S CreeP8080919Self 190 / mg/L 470.0557 / lbs/day
10/24/2019 P CreeP8102419POTW 140 / mg/L 347.9448 / lbs/day
Aug 2019 Week 2 190 / mg/L 470.0557 / lbs/day
Oct 2019 Week 4 140 / mg/L 347.9448 / lbs/day
Aug 2019 Average 190 / mg/L 470.0557 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 10

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SwnplelD Result/Limit Mass/Limit
Chloride
Oct 2019 Average 140 / mg/L 347.9448 / lbs/day
2019 Quarter 3 190 / mg/L 470.0557 / lbs/day
2019 Quarter 4 140 / mg/L 347.9448 / lbs/day
2019 2nd 6 Months(Avg) 165 / mg/L 409 / lbs/day
2019 2nd 6...(Max) 190 / mg/L 470.0557 / lbs/day
2019 2nd 6...(Min) 140 / mg/L 347.9448 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit ,
Chromium
08/09/2019 S CreeP8080919Self < 0.003 / mg/L < 0.006185 / lbs/day
Aug 2019 Week 2 < 0.003 / mg/L < 0.006185 / lbs/day
Aug 2019 Average < 0.003 / mg/L < 0.006185 / lbs/day
2019 Quarter 3 < 0.003 / mg/L < 0.006185 / lbs/day
2019 2nd 6 Months(Avg) < 0.003 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Max) < 0.003 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/09/2019 S CreeP8080919Self 0.169 / mg/L 0.418102 / lbs/day
Aug 2019 Week 2 0.169 / mg/L 0.418102 / lbs/day
Aug 2019 Average 0.169 / mg/L 0.418102 / lbs/day
2019 Quarter 3 0.169 / mg/L 0.418102 / lbs/day
2019 2nd 6 Months(Avg) 0.169 / mg/L 0.418102 / lbs/day
2019 2nd 6...(Max) 0.169 / mg/L 0.418102 / lbs/day
2019 2nd 6...(Min) 0.169 / mg/L 0.418102 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/09/2019 S CreeP8080919Self 0.008 / mg/L 0.020534 / lbs/day I
10/24/2019 P CreeP8102419POTW < 0.003 / mg/L < 0.006213 / lbs/day
Aug 2019 Week 2 0.008 / mg/L 0.020534 / lbs/day
Oct 2019 Week 4 < 0.003 / mg/L < 0.006213 / lbs/day
Aug 2019 Average 0.008 / mg/L 0.020534 / lbs/day
Oct 2019 Average < 0.003 / mg/L < 0.006213 / lbs/day
2019 Quarter 3 0.008 / mg/L 0.020534 / lbs/day
2019 Quarter 4 < 0.003 / mg/L < 0.006213 / lbs/day
2019 2nd 6 Months(Avg) < 0.005 / mg/L < 0.013374 / lbs/day
Wednesday,February 26,2020 *Indicates Violation "Indicates TRC Violation Page 3 of 10

Cree. Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
2019 2nd 6...(Max) 0.008 / mg/L 0.020534 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < 0.006213 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/09/2019 S CreeP8080919Self 0.47 / mg/L 1.1628 / lbs/day
10/24/2019 P CreeP8102419POTW 1.54 / mg/L 3.8274 / lbs/day
Aug 2019 Week 2 0.47 / mg/L 1.1628 / lbs/day
Oct 2019 Week 4 1.54 / mg/L 3.8274 / lbs/day
Aug 2019 Average 0.47 / mg/L 1.1628 / lbs/day
Oct 2019 Average 1.54 / mg/L 3.8274 / lbs/day
2019 Quarter 3 0.47 / mg/L 1.1628 / lbs/day
2019 Quarter 4 1.54 / mg/L 3.8274 / lbs/day
2019 2nd 6 Months(Avg) 1.01 / mg/L 2.4951 / lbs/day
2019 2nd 6...(Max) 1.54 / mg/L 3.8274 / lbs/day
2019 2nd 6...(Min) 0.47 / mg/L 1.1628 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/09/2019 S CreeP8080919Se1f < 0.0025 / mg/L < 0.006185 / lbs/day
Y
Aug 2019 Week 2 < 0.0025 / mg/L < 0.006185 / lbs/day
Aug 2019 Average < 0.0025 / ing/L < 0.006185 / lbs/day
2019 Quarter 3 < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Max) < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Min) < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/09/2019 S CreeP8080919Self < 0.000001 / mg/L < /
10/24/2019 P CreeP8102419POTW 0.000076 / mg/L /
Hg
Aug 2019 Week 2 < 0.000001 / mg/L < /
Oct 2019 Week 4 0.000076 / mg/L /
Aug 2019 Average < 0.000001 / mg/L < /
Oct 2019 Average 0.000076 / mg/L /
2019 Quarter 3 < 0.000001 / mg/L < /
2019 Quarter 4 0.000076 / mg/L /
2019 2nd 6 Months(Avg) < 0.0000385 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 10

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
2019 2nd 6...(Max) 0.0000764 / mg/L /
2019 2nd 6...(Min) < 0.0000005 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/09/2019 S CreeP8080919Se1f 0.024 / mg/L 0.0599 / lbs/day
Aug 2019 Week 2 0.024 / mg/L 0.0599 / lbs/day
Aug 2019 Average 0.024 / mg/L 0.0599 / lbs/day
2019 Quarter 3 0.024 / mg/L 0.0599 / lbs/day
2019 2nd 6 Months(Avg) 0.024 / mg/L 0.0599 / lbs/day
2019 2nd 6...(Max) 0.024 / mg/L 0.0599 / lbs/day
2019 2nd 6...(Min) 0.024 / mg/L 0.0599 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/09/2019 S CreeP8080919Self 0.0063 / mg/L 0.015586 / lbs/day
Aug 2019 Week 2 0.0063 / mg/L 0.015586 / lbs/day
Aug 2019 Average 0.0063 / mg/L 0.015586 / lbs/day
2019 Quarter 3 0.0063 / mg/L 0.015586 / lbs/day
2019 2nd 6 Months(Avg) 0.0063 / mg/L 0.015586 / lbs/day
2019 2nd 6...(Max) 0.0063 / mg/L 0.015586 / lbs/day
2019 2nd 6...(Min) 0.0063 / mg/L 0.015586 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/09/2019 S CreeP8080919Self 1.3 / mg/L 3.216 / lbs/day
10/24/2019 P CreeP8102419POTW 1.2 / mg/L 3.032 / lbs/day
Aug 2019 Week 2 1.3 / mg/L 3.216 / lbs/day
Oct 2019 Week 4 1.2 / mg/L 3.032 / lbs/day
Aug 2019 Average 1.3 / mg/L 3.216 / lbs/day
Oct 2019 Average 1.2 / mg/L 3.032 / lbs/day
2019 Quarter 3 1.3 / mg/L 3.216 / lbs/day
2019 Quarter 4 1.2 / mg/L 3.032 / lbs/day
2019 2nd 6 Months(Avg) 1.3 / mg/L 3.124 / lbs/day
2019 2nd 6...(Max) 1.3 / mg/L 3.216 / lbs/day
2019 2nd 6...(Min) 1.2 / mg/L 3.032 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 10

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall:• 008
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/09/2019 S CreeP8080919Self 25.3 / mg/L 62.592 / lbs/day
10/24/2019 P CreeP8102419POTW 22.3 / mg/L 55.423 / lbs/day
Aug 2019 Week 2 25.3 / mg/L 62.592 / lbs/day
Oct 2019 Week 4 22.3 / mg/L 55.423 / lbs/day
Aug 2019 Average 25.3 / mg/L 62.592 / lbs/day
Oct 2019 Average 22.3 / mg/L 55.423 / lbs/day
2019 Quarter 3 25.3 / mg/L 62.592 / lbs/day
2019 Quarter 4 22.3 / mg/L 55.423 / lbs/day
2019 2nd 6 Months(Avg) 23.8 / mg/L 59.007 / lbs/day
2019 2nd 6...(Max) 25.3 / mg/L 62.592 / lbs/day
2019 2nd 6...(Min) 22.3 / mg/L 55.423 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/24/2019 P CreeP8102419POTW < 2.5 / mg/L < /
Oct 2019 Week 4 < 2.5 / mg/L < /
Oct 2019 Average < 2.5 / mg/L < /
2019 Quarter 4 < 2.5 / mg/L < /
2019 2nd 6 Months(Avg) < 2.5 / mg/L < /
2019 2nd 6...(Max) < 2.5 / mg/L < /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/09/2019 S CreeP8080919Se1f 8.2 /5.0- 10.5 SU /
10/24/2019 P CreeP8102419POTW 8.1 /5.0- 10.5 SU /
Aug 2019 Week 2 8.2 / SU /
Oct 2019 Week 4 8.1 / SU /
Aug 2019 Average 8.2 / SU /
Oct 2019 Average 8.1 / SU /
2019 Quarter 3 8.2 / SU /
2019 Quarter 4 8.1 / SU /
2019 2nd 6 Months(Avg) 8.15 / SU /
2019 2nd 6...(Max) 8.2 / SU /
2019 2nd 6...(Min) 8.1 / SU /
2019 2nd 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 10

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
08/09/2019 S CreeP8080919Self < 0.005 / mg/L < 0.01237 / lbs/day
Aug 2019 Week 2 < 0.005 / mg/L < 0.01237 / lbs/day
Aug 2019 Average < 0.005 / mg/L < 0.01237 / lbs/day
2019 Quarter 3 < 0.005 / mg/L < 0.01237 / lbs/day
2019 2nd 6 Months(Avg) < 0.005 / mg/L < 0.012370 / lbs/day
2019 2nd 6...(Max) < 0.005 / mg/L < 0.012370 / lbs/day
2019 2nd 6...(Min) < 0.005 / mg/L < 0.012370 / lbs/day
i 2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/09/2019 S CreeP8080919Self < 0.0025 / mg/L < 0.006185 / lbs/day
Aug 2019 Week 2 < 0.0025 / mg/L < 0.006185 / lbs/day
Aug 2019 Average < 0.0025 / mg/L < ' 0.006185 / lbs/day
2019 Quarter 3 < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6 Months(Avg) < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Max) < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Min) < 0.0025 / mg/L < 0.006185 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Sulfate
08/09/2019 S CreeP8080919Self 306 / mg/L 757.0371 / lbs/day
Aug 2019 Week 2 306 / mg/L 757.0371 / lbs/day
Aug 2019 Average 306 / mg/L 757.0371 / lbs/day
2019 Quarter 3 306 / mg/L 757.0371 / lbs/day
2019 2nd 6 Months(Avg) 306 / mg/L 757.037 / lbs/day
2019 2nd 6...(Max) 306 / mg/L 757.0371 / lbs/day
2019 2nd 6...(Min) 306 / mg/L 757.0371 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 10

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/09/2019 S CreeP8080919Self 26.5 /66 °C /
10/24/2019 P CreeP8102419POTW 22 /66 °C /
Aug 2019 Week 2 26.5 / °C /
Oct 2019 Week 4 22 / °C /
Aug 2019 Average 26.5 / °C /
Oct 2019 Average 22 / °C /
2019 Quarter 3 26.5 / °C /
2019 Quarter 4 22 / °C /
2019 2nd 6 Months(Avg) 24.3 / °C /
2019 2nd 6...(Max) 26.5 / °C /
2019 2nd 6...(Min) 22 / °C /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # 14
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/12/2019 P CreeP8071219POTW 28.4 / mg/L 62.056 / lbs/day
08/09/2019 S CreeP8080919Self 23.9 / mg/L 59.128 / lbs/day
08/22/2019 P CreeP8082219POTW 22.6 / mg/L 57.865 / lbs/day
09/17/2019 P CreeP8091719POTW 37.9 / mg/L 70.487 / lbs/day
10/24/2019 P CreeP8102419POTW 21.1 / mg/L 52.44 / lbs/day
11/12/2019 P CreeP8111219POTW 22.2 / mg/L 51.101 / lbs/day
12/10/2019 P CreeP8121019POTW 23.4 / mg/L 48.789 / lbs/day
Jul 2019 Week 2 28.4 / mg/L 62.056 / lbs/day
Aug 2019 Week 2 23.9 / mg/L 59.128 / lbs/day
Aug 2019 Week 4 22.6 / mg/L 57.865 / lbs/day
Sep 2019 Week 3 37.9 / mg/L 70.487 / lbs/day
Oct 2019 Week 4 21.1 / mg/L 52.44 / lbs/day
Nov 2019 Week 2 22.2 / mg/L 51.101 / lbs/day
Dec 2019 Week 2 23.4 / mg/L 48.789 / lbs/day
Jul 2019 Average 28.4 / mg/L 62.056 / lbs/day
Aug 2019 Average 23.25 / mg/L 58.496 / lbs/day
Sep 2019 Average 37.9 / mg/L 70.487 / lbs/day
Oct 2019 Average 21.1 / mg/L 52.44 / lbs/day
Nov 2019 Average 22.2 / mg/L 51.101 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 10

Cree. Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 008
Sample Date SamplelD Result/Limit Mass/Limit
TKN
Dec 2019 Average 23.4 / mg/L 48.789 / lbs/day
2019 Quarter 3 28.2 / mg/L 62.384 / lbs/day
2019 Quarter 4 22.23 / mg/L 50.777 / lbs/day
2019 2nd 6 Months(Avg) 25.64 / mg/L 57.410 / lbs/day
2019 2nd 6...(Max) 37.9 / mg/L 70.487 / lbs/day
2019 2nd 6...(Min) 21.1 / mg/L 48.789 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/12/2019 P CreeP8071219POTW 2.05 / mg/L 4.4794 / lbs/day
08/22/2019 P CreeP8082219POTW 1.98 / mg/L 5.0696 / lbs/day
09/17/2019 P CreeP8091719POTW 2.18 / mg/L 4.0544 / lbs/day
10/24/2019 P CreeP8102419POTW 1.82 / mg/L 4.5233 / lbs/day
11/12/2019 P CreeP8111219POTW 2.97 / mg/L 6.8365 / lbs/day
12/10/2019 P CreeP8121019POTW 2.19 / mg/L 4.5662 / lbs/day
Jul 2019 Week 2 2.05 / mg/L 4.4794 / lbs/day
Aug 2019 Week 4 1.98 / mg/L 5.0696 / lbs/day
Sep 2019 Week 3 2.18 / mg/L 4.0544 / lbs/day
Oct 2019 Week 4 1.82 / mg/L 4.5233 / lbs/day
Nov 2019 Week 2 2.97 / mg/L 6.8365 / lbs/day
Dec 2019 Week 2 2.19 / mg/L 4.5662 / lbs/day
Jul2019 Average 2.05 / mg/L 4.4794 / lbs/day
Aug 2019 Average 1.98 / mg/L 5.0696 / lbs/day
Sep 2019 Average 2.18 / mg/L 4.0544 / lbs/day
Oct 2019 Average 1.82 / mg/L 4.5233 / lbs/day
Nov 2019 Average 2.97 / mg/L 6.8365 / lbs/day
Dec 2019 Average 2.19 / mg/L 4.5662 / lbs/day
2019 Quarter 3 2.05 / mg/L 4.4794 / lbs/day
2019 Quarter 3 2.08 / mg/L 4.562 / lbs/day
2019 Quarter 3 2.08 / mg/L 4.562 / lbs/day
2019 Quarter 3 2.05 / mg/L 4.4794 / lbs/day
2019 Quarter 4 2.327 / mg/L 5.3086 / lbs/day
2019 2nd 6 Months(Avg) 2.198 / mg/L 4.9216 / lbs/day
2.97m 6.8365 lbs/day
2nd 6...(Max) / /
( ) �
2019 2nd 6...(Min) 1.82 / mg/L 4.0544 / lbs/day
2019 2nd 6...(Count) 6 / 6 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/09/2019 S CreeP8080919Se1f 1.69 / mg/L 4.181022 / lbs/day
Aug 2019 Week 2 1.69 / mg/L 4.181022 / lbs/day
Wednesday,February 26,2020 *Indicates Violation *'Indicates TRC Violation Page 9 of 10
I

Cree. Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Oufall:: 008
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
Aug 2019 Average 1.69 / mg/L 4.181022 / lbs/day
2019 Quarter 3 1.69 / mg/L 4.181022 / lbs/day
2019 2nd 6 Months(Avg) 1.69 / mg/L 4.18102 / lbs/day
2019 2nd 6...(Max) 1.69 / mg/L 4.181022 / lbs/day
2019 2nd 6...(Min) 1.69 / mg/L 4.181022 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S CreeP90719Flow 0.029912 / MGD /
08/31/2019 S CreeP90819Flow 0.027839 / MGD /
09/30/2019 S CreeP90919F1ow 0.03102 / MGD /
10/31/2019 S CreeP91019Flow 0.035557 / MGD /
11/30/2019 S CreeP91119Flow 0.03958 / MGD /
12/31/2019 S CreeP91219Flow 0.037682 / MGD /
Jul 2019 Week 4 0.029912 / MGD /
Aug 2019 Week 4 0.027839 / MGD /
Sep 2019 Week 4 0.03102 / MGD /
Oct 2019 Week 4 0.035557 / MGD /
Nov 2019 Week 4 0.03958 / MGD /
Dec 2019 Week 4 0.037682 / MGD /
Jul 2019 Average 0.029912 / MGD /
Aug 2019 Average 0.027839 / MGD /
Sep 2019 Average 0.03102 / MGD /
Oct 2019 Average 0.035557 / MGD /
Nov 2019 Average 0.03958 / MGD /
Dec 2019 Average 0.037682 / MGD /
2019 Quarter 3 0.02943 / MGD /
2019 Quarter 3 0.029912 / MGD /
2019 Quarter 3 0.029912 / MGD /
2019 Quarter 3 0.02943 / MGD /
2019 Quarter 4 0.037606 / MGD /
2019 2nd 6 Months(Avg) 0.033598 / MGD /
2019 2nd 6...(Max) 0.03958 / MGD /
2019 2nd 6...(Min) 0.027839 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 10

Cree, Inc.(All) 11
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/09/2019 S CreeP9080919Self 50.2 / mg/L 13.2751 / lbs/day
Aug 2019 Week 2 50.2 / mg/L 13.2751 / lbs/day
Aug 2019 Average 50.2 / mg/L 13.2751 / lbs/day
2019 Quarter 3 50.2 / mg/L 13.2751 / lbs/day
2019 2nd 6 Months(Avg) 50.2 / mg/L 13.2751 / lbs/day
2019 2nd 6...(Max) 50.2 / mg/L 13.2751 / lbs/day
2019 2nd 6...(Min) 50.2 / mg/L 13.2751 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/09/2019 S CreeP9080919Se1f < 0.05 / mg/L < 0.0132 / lbs/day
10/24/2019 P CreeP9102419POTW < 0.05 / mg/L < /
Aug 2019 Week 2 < 0.05 / mg/L < 0.0132 / lbs/day
Oct 2019 Week 4 < 0.05 / mg/L < /
Aug 2019 Average < 0.05 / mg/L < 0.0132 / lbs/day
Oct 2019 Average < 0.05 / mg/L < /
2019 Quarter 3 < 0.05 / mg/L < 0.0132 / lbs/day
2019 Quarter 4 < 0.05 / mg/L < /
2019 2nd 6 Months(Avg) < 0.05 / mg/L < 0.0132 / lbs/day
2019 2nd 6...(Max) < 0.05 / mg/L < 0.0132 / lbs/day
2019 2nd 6...(Min) < 0.05 / mg/L < /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/09/2019 S CreeP9080919Self 0.000026 / mg/L /
10/24/2019 P CreeP9102419POTW 0.000065 / mg/L /
Hg
Aug 2019 Week 2 0.000026 / mg/L /
Oct 2019 Week 4 0.000065 / mg/L /
Aug 2019 Average 0.000026 / mg/L /
Oct 2019 Average 0.000065 / mg/L /
2019 Quarter 3 0.000026 / mg/L /
2019 Quarter 4 0.000065 / mg/L /
2019 2nd 6 Months(Avg) 0.0000455 / mg/L /
2019 2nd 6...(Max) 0.0000647 / mg/L /
2019 2nd 6...(Min) 0.0000262 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page I of 4

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
10/24/2019 P CreeP9102419POTW < 0.001 / mg/L < /
Oct 2019 Week 4 < 0.001 / mg/L < /
Oct 2019 Average < 0.001 / mg/L < /
2019 Quarter 4 < 0.001 / mg/L < /
2019 2nd 6 Months(Avg) < 0.001 / mg/L < /
2019 2nd 6...(Max) < 0.001 / mg/L < /
2019 2nd 6...(Min) < 0.001 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/24/2019 P CreeP9102419POTW 87 / mg/L /
Oct 2019 Week 4 87 / mg/L /
Oct 2019 Average 87 / mg/L /
2019 Quarter 4 87 / mg/L /
2019 2nd 6 Months(Avg) 87 / mg/L /
2019 2nd 6...(Max) 87 / mg/L /
2019 2nd 6...(Min) 87 / mg/L /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/09/2019 S CreeP9080919Self 7.6 /5.0- 10.5 SU /
10/24/2019 P CreeP9102419POTW 8.8 /5.0- 10.5 SU /
Aug 2019 Week 2 7.6 / SU /
Oct 2019 Week 4 8.8 / SU /
Aug 2019 Average 7.6 / SU /
Oct 2019 Average 8.8 / SU /
2019 Quarter 3 7.6 / SU /
2019 Quarter 4 8.8 / SU /
2019 2nd 6 Months(Avg) 8.2 / SU /
2019 2nd 6...(Max) 8.8 / SU /
2019 2nd 6...(Min) 7.6 / SU /
2019 2nd 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 4

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SarnplelD Result/Limit Mass/Limit
Temperature
08/09/2019 S CreeP9080919Self 25.8 / °C /
Aug 2019 Week 2 25.8 / °C /
Aug 2019 Average 25.8 / °C /
2019 Quarter 3 25.8 / °C /
2019 2nd 6 Months(Avg) 25.8 / °C /
2019 2nd 6...(Max) 25.8 / °C /
2019 2nd 6...(Min) 25.8 / °C /
2019 2nd 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/12/2019 P CreeP9071219POTW 80.2 / mg/L /
08/22/2019 P CreeP9082219POTW 28.7 / mg/L /
09/17/2019 P CreeP9091719POTW 20.5 / mg/L /
10/24/2019 P CreeP9102419POTW 14.2 / mg/L /
11/12/2019 P CreeP9111219POTW 20.1 / mg/L /
12/10/2019 P CreeP9121019POTW 16.2 / mg/L /
Jul 2019 Week 2 80.2 / mg/L /
Aug 2019 Week 4 28.7 / mg/L /
Sep 2019 Week 3 20.5 / mg/L /
Oct 2019 Week 4 14.2 / mg/L /
Nov 2019 Week 2 20.1 / mg/L /
Dec 2019 Week 2 16.2 / mg/L /
Jul 2019 Average 80.2 / mg/L /
Aug 2019 Average 28.7 / mg/L /
Sep 2019 Average 20.5 / mg/L /
Oct 2019 Average 14.2 / mg/L /
Nov 2019 Average 20.1 / mg/L /
Dec 2019 Average 16.2 / mg/L /
2019 Quarter 3 43.13 / mg/L /
2019 Quarter 4 16.83 / mg/L /
2019 2nd 6 Months(Avg) 29.98 / mg/L /
2019 2nd 6...(Max) 80.2 / mg/L /
2019 2nd 6...(Min) 14.2 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 4

Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 009
Sample Date SamplelD Result/Limit Mass/Limit
TKN
2019 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
07/12/2019 P CreeP9071219POTW 7.53 / mg/L /
08/22/2019 P CreeP9082219POTW 3.47 / mg/L /
09/17/2019 P CreeP9091719POTW 2.77 / mg/L /
10/24/2019 P CreeP9102419POTW 2.05 / mg/L /
11/12/2019 P CreeP9111219POTW 4.08 / mg/L /
12/10/2019 P CreeP9121019POTW 2.37 / mg/L /
Jul 2019 Week 2 7.53 / mg/L /
Aug 2019 Week 4 3.47 / mg/L /
Sep 2019 Week 3 2.77 / mg/L /
Oct 2019 Week 4 2.05 / mg/L /
Nov 2019 Week 2 4.08 / mg/L /
Dec 2019 Week 2 2.37 / mg/L /
Jul2019 Average 7.53 / mg/L /
Aug 2019 Average 3.47 / mg/L /
Sep 2019 Average 2.77 / mg/L /
Oct 2019 Average 2.05 / mg/L /
Nov 2019 Average 4.08 / mg/L /
Dec 2019 Average 2.37 / mg/L /
2019 Quarter 3 4.59 / mg/L /
2019 Quarter 4 2.833 / mg/L /
2019 2nd 6 Months(Avg) 3.712 / mg/L /
2019 2nd 6...(Max) 7.53 / mg/L /
2019 2nd 6...(Min) 2.05 / mg/L /
2019 2nd 6...(Count) 6 / /
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S Cree0719F1ow 0.290832 /0.600 MGD /
08/31/2019 S Cree0819F1ow 0.316257 /0.600 MGD /
09/30/2019 S Cree0919F1ow 0.304284 /0.600 MGD /
10/31/2019 S Cree1019Flow 0.321606 /0.600 MGD /
11/30/2019 S Cree1119Flow 0.320812 /0.600 MGD /
12/31/2019 S Cree1219Flow 0.285863 /0.600 MGD /
Jul2019 Week 4 0.290832 / MGD /
Aug 2019 Week 4 0.316257 / MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 4

Cree, Inc.(All)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample T e: Effluent Wastewater (Wall: All
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Sep 2019 Week 4 0.304284 / MGD /
Oct 2019 Week 4 0.321606 / MGD /
Nov 2019 Week 4 0.320812 / MGD /
Dec 2019 Week 4 0.285863 / MGD /
Jul 2019 Average 0.290832 /0.451 MGD /
Aug 2019 Average 0.316257 /0.451 MGD /
Sep 2019 Average 0.304284 /0.451 MGD /
Oct 2019 Average 0.321606 /0.451 MGD /
Nov 2019 Average 0.320812 /0.451 MGD /
Dec 2019 Average 0.285863 /0.451 MGD /
2019 Quarter 3 0.310271 / MGD /
2019 Quarter 3 0.290832 / MGD /
2019 Quarter 3 0.290832 / MGD /
2019 Quarter 3 0.310271 / MGD /
2019 Quarter 4 0.309427 / MGD /
2019 2nd 6 Months(Avg) 0.306609 / MGD /
2019 2nd 6...(Max) 0.321606 / MGD /
2019 2nd 6...(Min) 0.285863 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled : 6 Weeks Sampled : 6 Quarters Sampled : 5
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit /Ilas.s/Limit
Fluoride
08/09/2019 S Cree080919Self 0.42 /8.0 mg/L /
10/24/2019 P Cree102419POTW 1.38 /8.0 mg/L /
Aug 2019 Week 2 0.42 / mg/L /
Oct 2019 Week 4 1.38 / mg/L /
Aug 2019 Average 0.42 /7.0 mg/L /
Oct 2019 Average 1.38 /7.0 mg/L /
2019 Quarter 3 0.42 / mg/L /
2019 Quarter 4 1.38 / mg/L /
2019 2nd 6 Months(Avg) 0.9 / mg/L /
2019 2nd 6...(Max) 1.38 / mg/L /
2019 2nd 6...(Min) 0.42 / mg/L /
2019 2nd 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 3

•
Cree, Inc.(All)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: All
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
08/09/2019 S Cree080919Self 0.000003 /0.000142 mg/L /
10/24/2019 P Cree102419POTW 0.000075 /0.000142 mg/L /
Aug 2019 Week 2 0.000003 / mg/L /
Oct 2019 Week 4 0.000075 / mg/L /
Aug 2019 Average 0.000003 / mg/L /
Oct 2019 Average 0.000075 / mg/L /
2019 Quarter 3 0.000003 / mg/L /
2019 Quarter 4 0.000075 / mg/L /
2019 2nd 6 Months(Avg) 0.000039 / mg/L /
2019 2nd 6...(Max) 0.000075 / mg/L /
2019 2nd 6...(Min) 0.000003 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Oil& Grease,Total
10/24/2019 P Cree102419POTW 9.3 /200.0 mg/L /
Oct 2019 Week 4 9.3 / mg/L /
Oct 2019 Average 9.3 / mg/L /
2019 Quarter 4 9.3 / mg/L /
2019 2nd 6 Months(Avg) 9.3 / mg/L /
2019 2nd 6...(Max) 9.3 / mg/L /
2019 2nd 6...(Min) 9.3 / mg/L /
2019 2nd 6...(Count) 1 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 3

•
Cree, Inc.(A11)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: All
Sample Count: 1 Months Sampled : 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 3

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
08/09/2019 S CreeRTPP12080919Se < 0.05 / mg/L < /
If
Aug 2019 Week 2 < 0.05 / mg/L < /
Aug 2019 Average < 0.05 / mg/L < /
2019 Quarter 3 < 0.05 / mg/L < /
2019 2nd 6 Months(Avg) < 0.05 / mg/L < /
2019 2nd 6...(Max) < 0.05 / mg/L < /
2019 2nd 6...(Min) < 0.05 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/09/2019 S CreeRTPP12080919Se 3.9 / mg/L /
If
10/24/2019 P CreeRTPP12102419P 1.5 / mg/L /
OTW
Aug 2019 Week 2 3.9 / mg/L /
Oct 2019 Week 4 1.5 / mg/L /
Aug 2019 Average 3.9 / mg/L /
Oct 2019 Average 1.5 / mg/L /
2019 Quarter 3 3.9 / mg/L /
2019 Quarter 4 1.5 / mg/L /
2019 2nd 6 Months(Avg) 2.7 / mg/L /
2019 2nd 6...(Max) 3.9 / mg/L /
2019 2nd 6...(Min) 1.5 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Arsenic
08/09/2019 S CreeRTPP12080919Se < 0.005 / mg/L < /
If
' Aug 2019 Week 2 < 0.005 / mg/L < /
Aug 2019 Average < 0.005 / mg/L < /
2019 Quarter 3 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/17/2019 S CreeRTPP120719F1ow 0.149353 /0.469 MGD /
08/20/2019 S CreeRTPP120819Flow 0.143189 /0.469 MGD /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 11

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
09/18/2019 S CreeRTPP120919F1ow 0.135057 /0.469 MGD /
10/27/2019 S CreeRTPP 121019F1ow 0.106792 /0.469 MGD /
11/28/2019 S CreeRTPP121119Flow 0.162001 /0.469 MGD /
12/19/2019 S CreeRTPP121219Flow 0.115678 /0.469 MGD /
Jul 2019 Week 3 0.149353 / MGD /
Aug 2019 Week 3 0.143189 / MGD /
Sep 2019 Week 3 0.135057 / MGD /
Oct 2019 Week 4 0.106792 / MGD /
Nov 2019 Week 4 0.162001 / MGD /
Dec 2019 Week 3 0.115678 / MGD /
Jul 2019 Average 0.149353 /0.329 MGD /
Aug 2019 Average 0.143189 /0.329 MGD /
Sep 2019 Average 0.135057 /0.329 MGD /
Oct 2019 Average 0.106792 /0.329 MGD /
Nov 2019 Average 0.162001 /0.329 MGD /
Dec 2019 Average 0.115678 /0.329 MGD /
2019 Quarter 3 0.139123 / MGD /
2019 Quarter 3 0.149353 / MGD /
2019 Quarter 3 0.139123 / MGD /
2019 Quarter 3 0.149353 / MGD /
2019 Quarter 4 0.128157 / MGD /
2019 2nd 6 Months(Avg) 0.135345 / MGD /
2019 2nd 6...(Max) 0.162001 / MGD /
2019 2nd 6...(Min) 0.106792 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Barium
08/09/2019 S CreeRTPP12080919Se 0.015 / mg/L /
if
Aug 2019 Week 2 0.015 / mg/L /
Aug 2019 Average 0.015 / mg/L /
2019 Quarter 3 0.015 / mg/L /
2019 2nd 6 Months(Avg) 0.015 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 11

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Barium
2019 2nd 6...(Max) 0.015 / mg/L /
2019 2nd 6...(Min) 0.015 / mg/L /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/09/2019 S CreeRTPP12080919Se < 0.0005 / mg/L < /
If
Aug 2019 Week 2 < 0.0005 / mg/L < /
Aug 2019 Average < 0.0005 / mg/L < /
2019 Quarter 3 < 0.0005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0005 / mg/L < /
2019 2nd 6...(Max) < 0.0005 / mg/L < /
2019 2nd 6...(Min) < 0.0005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Alass/Limit
Chloride
08/09/2019 S CreeRTPP12080919Se 79.8 / mg/L /
if
10/24/2019 P CreeRTPP12102419P 80 / mg/L /
OTW
Aug 2019 Week 2 79.8 / mg/L /
Oct 2019 Week 4 80 / mg/L /
Aug 2019 Average 79.8 / mg/L /
Oct 2019 Average 80 / mg/L /
2019 Quarter 3 79.8 / mg/L /
2019 Quarter 4 80 / mg/L /
2019 2nd 6 Months(Avg) 79.9 / mg/L /
2019 2nd 6...(Max) 80 / mg/L /
2019 2nd 6...(Min) 79.8 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Dale SamplelD Result/Limit Mass/Limit
Chromium
08/09/2019 S CreeRTPP12080919Se < 0.001 / mg/L < /
If
Aug 2019 Week 2 < 0.001 / mg/L < /
Aug 2019 Average < 0.001 / mg/L < /
2019 Quarter 3 < 0.001 / mg/L < /
2019 2nd 6 Months(Avg) < 0.001 / mg/L < /
2019 2nd 6...(Max) < 0.001 / mg/L < /
2019 2nd 6...(Min) < 0.001 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 11

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/09/2019 S CreeRTPP12080919Se 0.033 / mg/L /
If
Aug 2019 Week 2 0.033 / mg/L /
Aug 2019 Average 0.033 / mg/L /
2019 Quarter 3 0.033 / mg/L /
2019 2nd 6 Months(Avg) 0.033 / mg/L /
2019 2nd 6...(Max) 0.033 / mg/L /
2019 2nd 6...(Min) 0.033 / mg/L /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/09/2019 S CreeRTPP12070919Se < 0.004 / mg/L < 0.004982 /0.05 lbs/day
if
07/23/2019 S CreeRTPP12072319Se < 0.004 / mg/L < 0.004982 /0.05 lbs/day
If
08/09/2019 S CreeRTPP12080919Se < 0.004 / mg/L < /
If
10/24/2019 P CreeRTPP12102419P < 0.003 / mg/L < /
OTW
Jul 2019 Week 2 < 0.004 / mg/L < 0.004982 / lbs/day
Jul 2019 Week 4 < 0.004 / mg/L < 0.004982 / lbs/day
Aug 2019 Week 2 < 0.004 / mg/L < /
Oct 2019 Week 4 < 0.003 / mg/L < /
Jul 2019 Average < 0.004 / mg/L < 0.004982 / lbs/day
Aug 2019 Average < 0.004 / mg/L < /
Oct 2019 Average < 0.003 / mg/L < /
2019 Quarter 3 < 0.004 / mg/L < /
2019 Quarter 3 < 0.004 / mg/L < 0.004982 / lbs/day
2019 Quarter 3 < 0.004 / mg/L < /
2019 Quarter 3 < 0.004 / mg/L < 0.004982 / lbs/day
2019 Quarter 4 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.004 / mg/L < 0.004982 / lbs/day
2019 2nd 6...(Max) < 0.004 / mg/L < 0.004982 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 4 / 2 /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of I I

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Count: 4 Months Sampled: 3 Weeks Sampled: 4 Quarters Sampled: 5
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
08/09/2019 S CreeRTPP12080919Se 0.46 /8.0 mg/L /
If
10/24/2019 P CreeRTPP12102419P 0.91 /8.0 mg/L /
OTW
Aug 2019 Week 2 0.46 / mg/L /
Oct 2019 Week 4 0.91 / mg/L /
Aug 2019 Average 0.46 /7.0 mg/L /
Oct 2019 Average 0.91 /7.0 mg/L /
2019 Quarter 3 0.46 / mg/L /
2019 Quarter 4 0.91 / mg/L /
2019 2nd 6 Months(Avg) 0.69 / mg/L /
2019 2nd 6...(Max) 0.91 / mg/L /
2019 2nd 6...(Min) 0.46 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/09/2019 S CreeRTPP12080919Se 0.005 / mg/L /
if
Aug 2019 Week 2 0.005 / mg/L /
Aug 2019 Average 0.005 / mg/L /
2019 Quarter 3 0.005 / mg/L /
2019 2nd 6 Months(Avg) 0.005 / mg/L /
2019 2nd 6...(Max) 0.005 / mg/L /
2019 2nd 6...(Min) 0.005 / mg/L /
2019 2nd 6...(Count) 1 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 1 I

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
08/09/2019 S CreeRTPP12080919Se 0.000001 / mg/L /
if
10/24/2019 P CreeRTPP12102419P 0.000008 / mg/L /
OTWHg
Aug 2019 Week 2 0.000001 / mg/L /
Oct 2019 Week 4 0.000008 / mg/L /
Aug 2019 Average 0.000001 /0.000142 mg/L /
Oct 2019 Average 0.000008 /0.000142 mg/L /
2019 Quarter 3 0.000001 / mg/L /
2019 Quarter 4 0.000008 / mg/L /
2019 2nd 6 Months(Avg) 0.0000048 / mg/L /
2019 2nd 6...(Max) 0.0000081 / mg/L /
2019 2nd 6...(Min) 0.0000014 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/09/2019 S CreeRTPP12080919Se < 0.003 / mg/L < /
If
10/24/2019 P CreeRTPP12102419P < 0.001 / mg/L < /
OTW
Aug 2019 Week 2 < 0.003 / mg/L < /
Oct 2019 Week 4 < 0.001 / mg/L < /
Aug 2019 Average < 0.003 / mg/L < /
Oct 2019 Average < 0.001 / mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 Quarter 4 < 0.001 / mg/L < /
2019 2nd 6 Months(Avg) < 0.002 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.001 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 11

Cree. Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type.• Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/09/2019 S CreeRTPP12080919Se < 0.0025 / mg/L < /
If
Aug 2019 Week 2 < 0.0025 / mg/L < /
Aug 2019 Average < 0.0025 / mg/L < /
2019 Quarter 3 < 0.0025 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2019 2nd 6...(Max) < 0.0025 / mg/L < /
2019 2nd 6...(Min) < 0.0025 / mg/L < /
2019 2nd 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/09/2019 S CreeRTPP12080919Se 2 / mg/L /
If
10/24/2019 P CreeRTPP12102419P 2.4 / mg/L /
OTW
Aug 2019 Week 2 2 / mg/L /
Oct 2019 Week 4 2.4 / mg/L /
Aug 2019 Average 2 / mg/L /
Oct 2019 Average 2.4 / mg/L /
2019 Quarter 3 2 / mg/L /
2019 Quarter 4 2.4 / mg/L /
2019 2nd 6 Months(Avg) 2.2 / mg/L /
2019 2nd 6...(Max) 2.4 / mg/L /
2019 2nd 6...(Min) 2 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/09/2019 S CreeRTPP12080919Se 16.2 / mg/L /
If
10/24/2019 P CreeRTPP12102419P 10.5 / mg/L /
OTW
Aug 2019 Week 2 16.2 / mg/L /
Oct 2019 Week 4 10.5 / mg/L /
Aug 2019 Average 16.2 / mg/L /
Oct 2019 Average 10.5 / mg/L /
2019 Quarter 3 16.2 / mg/L /
2019 Quarter 4 10.5 / mg/L /
2019 2nd 6 Months(Avg) 13.35 / mg/L /
2019 2nd 6...(Max) 16.2 / mg/L /
2019 2nd 6...(Min) 10.5 / mg/L /
2019 2nd 6...(Count) 2 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 11
L

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/24/2019 P CreeRTPP12102419P < 2.5 /200 mg/L < /
OTW
Oct 2019 Week 4 < 2.5 / mg/L < /
Oct 2019 Average < 2.5 / mg/L < /
2019 Quarter 4 < 2.5 / mg/L < /
2019 2nd 6 Months(Avg) < 2.5 / mg/L < /
2019 2nd 6...(Max) < 2.5 / mg/L < /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled : 1 Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/09/2019 S CreeRTPP12070919Se 8.8 /5.0- 10.5 SU /
if
07/23/2019 S CreeRTPP12072319Se 9 /5.0- 10.5 SU /
if
08/09/2019 S CreeRTPP12080919Se 7.5 /5.0- 10.5 SU /
If
10/24/2019 P CreeRTPP12102419P 8.2 /5.0- 10.5 SU /
OTW
Jul 2019 Week 2 8.8 / SU /
Jul 2019 Week 4 9 / SU /
Aug 2019 Week 2 7.5 / SU /
Oct 2019 Week 4 8.2 / SU /
Jul 2019 Average 8.9 / SU /
Aug 2019 Average 7.5 / SU /
Oct 2019 Average 8.2 / SU /
2019 Quarter 3 7.5 / SU /
2019 Quarter 3 8.9 / SU /
2019 Quarter 3 7.5 / SU /
2019 Quarter 3 8.9 / SU /
2019 Quarter 4 8.2 / SU /
2019 2nd 6 Months(Avg) 8.38 / SU /
2019 2nd 6...(Max) 9 / SU /
2019 2nd 6...(Min) 7.5 / SU /
2019 2nd 6...(Count) 4 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 11

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Count: 4 Months Sampled: 3 Weeks Sampled: 4 Quarters Sampled: 5
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
08/09/2019 S CreeRTPP12080919Se < 0.005 / mg/L < /
if
Aug 2019 Week 2 < 0.005 / mg/L < /
Aug 2019 Average < 0.005 / mg/L < /
2019 Quarter 3 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/09/2019 S CreeRTPP12080919Se < 0.0025 / mg/L < /
1f
Aug 2019 Week 2 < 0.0025 / mg/L < /
Aug 2019 Average < 0.0025 / mg/L < /
2019 Quarter 3 < 0.0025 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0025 / mg/L < /
2019 2nd 6...(Max) < 0.0025 / mg/L < /
2019 2nd 6...(Min) < 0.0025 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/09/2019 S CreeRTPP12070919Se 29.5 /66 °C /
if
07/23/2019 S CreeRTPP12072319Se 26.9 /66 °C /
1f
08/09/2019 S CreeRTPP12080919Se 29.7 /66 °C /
If
10/24/2019 P CreeRTPP12102419P 20 /66 °C /
OTW
Jul 2019 Week 2 29.5 / °C /
Jul 2019 Week 4 26.9 / °C /
Aug 2019 Week 2 29.7 / °C /
Oct 2019 Week 4 20 / °C /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 11

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
Jul2019 Average 28.2 / °C /
Aug 2019 Average 29.7 / °C /
Oct 2019 Average 20 / °C /
2019 Quarter 3 29.7 / °C /
2019 Quarter 3 28.2 / °C /
2019 Quarter 3 29.7 / °C /
2019 Quarter 3 28.2 / °C /
2019 Quarter 4 20 / °C /
2019 2nd 6 Months(Avg) 26.5 / °C /
2019 2nd 6...(Max) 29.7 / °C /
2019 2nd 6...(Min) 20 / °C /
2019 2nd 6...(Count) 4 / /
Sample Count: 4 Months Sampled: 3 Weeks Sampled : 4 Quarters Sampled : 5
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/09/2019 S CreeRTPP12080919Se 14.2 / mg/L /
if
10/24/2019 P CreeRTPPI2102419P 8.15 / mg/L /
OTW
Aug 2019 Week 2 14.2 / mg/L /
Oct 2019 Week 4 8.15 / mg/L /
Aug 2019 Average 14.2 / mg/L /
Oct 2019 Average 8.15 / mg/L /
2019 Quarter 3 14.2 / mg/L /
2019 Quarter 4 8.15 / mg/L /
2019 2nd 6 Months(Avg) 11.18 / mg/L /
2019 2nd 6...(Max) 14.2 / mg/L /
2019 2nd 6...(Min) 8.15 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
10/24/2019 P CreeRTPP12102419P 1.43 / mg/L /
OTW
Oct 2019 Week 4 1.43 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 11

Cree, Inc.(RTP)
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 012
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
Oct 2019 Average 1.43 / mg/L /
2019 Quarter 4 1.43 / mg/L /
2019 2nd 6 Months(Avg) 1.43 / mg/L /
2019 2nd 6...(Max) 1.43 / mg/L /
2019 2nd 6...(Min) 1.43 / mg/L /
2019 2nd 6...(Count) I / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/09/2019 S CreeRTPP12080919Se 0.702 / mg/L /
If
Aug 2019 Week 2 0.702 / mg/L /
Aug 2019 Average 0.702 / mg/L /
2019 Quarter 3 0.702 / mg/L /
2019 2nd 6 Months(Avg) 0.702 / mg/L /
2019 2nd 6...(Max) 0.702 / mg/L /
2019 2nd 6...(Min) 0.702 / mg/L /
2019 2nd 6...(Count) 1 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 11 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
07/11/2019 S JMC071119Se1f 0.064 / mg/L 0.000341 / lbs/day
10/03/2019 P JMC100319POTW 0.06 / mg/L 0.000615 / lbs/day
Jul 2019 Week 2 0.064 / mg/L 0.000341 / lbs/day
Oct 2019 Week 1 0.06 / mg/L 0.000615 / lbs/day
Jul 2019 Average 0.064 / mg/L 0.000341 / lbs/day
Oct 2019 Average 0.06 / mg/L 0.000615 / lbs/day
2019 Quarter 3 0.064 / mg/L 0.000341 / lbs/day
2019 Quarter 4 0.06 / mg/L 0.000615 / lbs/day
2019 2nd 6 Months(Avg) 0.062 / mg/L 0.000478 / lbs/day
2019 2nd 6...(Max) 0.064 / mg/L 0.000615 / lbs/day
2019 2nd 6...(Min) 0.060 / mg/L 0.000341 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
07/11/2019 S JMC071119Self 3.5 / mg/L 0.0187 / lbs/day
10/03/2019 P JMC100319POTW 2.2 / mg/L 0.0227 / lbs/day
Jul 2019 Week 2 3.5 / mg/L 0.0187 / lbs/day
Oct 2019 Week 1 2.2 / mg/L 0.0227 / lbs/day
Jul2019 Average 3.5 / mg/L 0.0187 / lbs/day
Oct 2019 Average 2.2 / mg/L 0.0227 / lbs/day
2019 Quarter 3 3.5 / mg/L 0.0187 / lbs/day
2019 Quarter 4 2.2 / mg/L 0.0227 / lbs/day
2019 2nd 6 Months(Avg) 2.85 mg/L0.0207 lbs/day
/ /
2019 2nd 6...(Max) 3.5 / mg/L 0.0227 / lbs/day
2019 2nd 6...(Min) 2.2 / mg/L 0.0187 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S JMC0719Flow 0.000371 / MGD /
08/31/2019 S JMC0819Flow 0.000259 / MGD /
09/30/2019 S JMC0919Flow 0.000214 / MGD /
10/31/2019 S JMC1019Flow 0.000403 / MGD /
11/30/2019 S JMC1119Flow 0.000165 / MGD /
12/31/2019 S JMC1219Flow 0.000255 / MGD /
Jul 2019 Week 4 0.000371 / MGD /
Aug 2019 Week 4 0.000259 / MGD /
Sep 2019 Week 4 0.000214 / MGD /
Oct 2019 Week 4 0.000403 / MGD /
Nov 2019 Week 4 0.000165 / MGD /
Dec 2019 Week 4 0.000255 / MGD /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
Jul 2019 Average 0.000371 /0.01 MGD /
Aug 2019 Average 0.000259 /0.01 MGD /
Sep 2019 Average 0.000214 /0.01 MGD /
Oct 2019 Average 0.000403 /0.01 MGD /
Nov 2019 Average 0.000165 /0.01 MGD /
Dec 2019 Average 0.000255 /0.01 MGD /
2019 Quarter 3 0.000281 / MGD /
2019 Quarter 4 0.000274 / MGD /
2019 2nd 6 Months(Avg) 0.000278 / MGD /
2019 2nd 6...(Max) 0.000403 / MGD /
2019 2nd 6...(Min) 0.000165 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/11/2019 S JMC071119Self < 0.00008 /0.04 mg/L < 0 / lbs/day
10/03/2019 P JMC 100319POTW < 0.00008 /0.04 mg/L < 0.000001 / lbs/day
Jul 2019 Week 2 < 0.00008 / mg/L < 0 / lbs/day
Oct 2019 Week 1 < 0.00008 / mg/L < 0.000001 / lbs/day
Jul 2019 Average < 0.00008 /0.025 mg/L < 0 / lbs/day
Oct 2019 Average < 0.00008 /0.025 mg/L < 0.000001 / lbs/day
2019 Quarter 3 < 0.00008 / mg/L < 0 / lbs/day
2019 Quarter 4 < 0.00008 / mg/L < 0.000001 / lbs/day
2019 2nd 6 Months(Avg) < 0.00008 / mg/L < 0.000001 / lbs/day
2019 2nd 6...(Max) < 0.00008 / mg/L < 0.000001 / lbs/day
2019 2nd 6...(Min) < 0.00008 / mg/L < 0.000000 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 11

r
JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/11/2019 S JMC071119Self 3800 / mg/L 20.2512 / lbs/day
10/03/2019 P JMC100319POTW 1760 / mg/L 18.1865 / lbs/day
Jul 2019 Week 2 3800 / mg/L 20.2512 / lbs/day
Oct 2019 Week 1 1760 / mg/L 18.1865 / lbs/day
Jul2019 Average 3800 / mg/L 20.2512 / lbs/day
Oct 2019 Average 1760 / mg/L 18.1865 / lbs/day
2019 Quarter 3 3800 / mg/L 20.2512 / lbs/day
2019 Quarter 4 1760 / mg/L 18.1865 / lbs/day
2019 2nd 6 Months(Avg) 2780 / mg/L 19.2189 / lbs/day
2019 2nd 6...(Max) 3800 / mg/L 20.2512 / lbs/day
2019 2nd 6...(Min) 1760 / mg/L 18.1865 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
07/11/2019 S JMC071119Self 0.062 /1 mg/L 0.00033 / lbs/day
10/03/2019 P JMC100319POTW 0.051 /1 mg/L 0.000526 / lbs/day
Jul2019 Week 2 0.062 / mg/L 0.00033 / lbs/day
Oct 2019 Week 1 0.051 / mg/L 0.000526 / lbs/day
Jul 2019 Average 0.062 /0.650 mg/L 0.00033 / lbs/day
Oct 2019 Average 0.051 /0.650 mg/L 0.000526 / lbs/day
2019 Quarter 3 0.062 / mg/L 0.00033 / lbs/day
2019 Quarter 4 0.051 / mg/L 0.000526 / lbs/day
2019 2nd 6 Months(Avg) 0.056 / mg/L 0.000428 / lbs/day
2019 2nd 6...(Max) 0.062 / mg/L 0.000526 / lbs/day
2019 2nd 6...(Min) 0.051 / mg/L 0.000330 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
07/11/2019 S JMC071119Self 0.014 / 1 mg/L 0.000075 / lbs/day
10/03/2019 P JMC100319POTW 0.009 / 1 mg/L 0.000096 / lbs/day
Jul 2019 Week 2 0.014 / mg/L 0.000075 / lbs/day
Oct 2019 Week 1 0.009 / mg/L 0.000096 / lbs/day
Jul 2019 Average 0.014 /0.7 mg/L 0.000075 / lbs/day
Oct 2019 Average 0.009 /0.7 mg/L 0.000096 / lbs/day
2019 Quarter 3 0.014 / mg/L 0.000075 / lbs/day
2019 Quarter 4 0.009 / mg/L 0.000096 / lbs/day
2019 2nd 6 Months(Avg) 0.012 / mg/L 0.000085 / lbs/day
2019 2nd 6...(Max) 0.014 / mg/L 0.000096 / lbs/day
2019 2nd 6...(Min) 0.009 / mg/L 0.000075 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/11/2019 S JMC071119Self < 0.003 /0.04 mg/L < 0.000013 / lbs/day
10/03/2019 P JMC100319POTW < 0.003 /0.04 mg/L < 0.000026 / lbs/day
Jul 2019 Week 2 < 0.003 / mg/L < 0.000013 / lbs/day
Oct 2019 Week 1 < 0.003 / mg/L < 0.000026 / lbs/day
Jul 2019 Average < 0.003 /0.03 mg/L < 0.000013 / lbs/day
Oct 2019 Average < 0.003 /0.03 mg/L < 0.000026 / lbs/day
2019 Quarter 3 < 0.003 / mg/L < 0.000013 / lbs/day
2019 Quarter 4 < 0.003 / mg/L < 0.000026 / lbs/day
2019 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000020 / lbs/day
2019 2nd 6...(Max) < 0.003 / mg/L < 0.000026 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < 0.000013 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of I I

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
2019 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/11/2019 S JMC071119Self 0.18 / mg/L 0.001 / lbs/day
10/03/2019 P JMC 100319POTW 0.14 / mg/L 0.0014 / lbs/day
Jul2019 Week 2 0.18 / mg/L 0.001 / lbs/day
Oct 2019 Week 1 0.14 / mg/L 0.0014 / lbs/day
Jul 2019 Average 0.18 / mg/L 0.001 / lbs/day
Oct 2019 Average 0.14 / mg/L 0.0014 / lbs/day
2019 Quarter 3 0.18 / mg/L 0.001 / lbs/day
2019 Quarter 4 0.14 / mg/L 0.0014 / lbs/day
2019 2nd 6 Months(Avg) 0.16 / mg/L 0.0012 / lbs/day
2019 2nd 6...(Max) 0.18 / mg/L 0.0014 / lbs/day
2019 2nd 6...(Min) 0.14 / mg/L 0.0010 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Dale SamplelD Result/Limit Alms/Limit
Lead
07/11/2019 S JMC071119Self 0.0031 /0.260 mg/L 0.000017 / lbs/day
10/03/2019 P JMC100319POTW 0.0018 /0.260 mg/L 0.000019 / lbs/day
Jul 2019 Week 2 0.0031 / mg/L 0.000017 / lbs/day
Oct 2019 Week 1 0.0018 / mg/L 0.000019 / lbs/day
Jul 2019 Average 0.0031 /0.160 mg/L 0.000017 / lbs/day
Oct 2019 Average 0.0018 /0.160 mg/L 0.000019 / lbs/day
2019 Quarter 3 0.0031 / mg/L 0.000017 / lbs/day
2019 Quarter 4 0.0018 / mg/L 0.000019 / lbs/day
2019 2nd 6 Months(Avg) 0.0025 / mg/L 0.000018 / lbs/day
2019 2nd 6...(Max) 0.0031 / mg/L 0.000019 / lbs/day
2019 2nd 6...(Min) 0.0018 / mg/L 0.000017 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 11

•
JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/11/2019 S JMC071119Self 0.000003 /0.000142 mg/L /
10/03/2019 P JMC100319POTWHg 0.000002 /0.000142 mg/L /
Jul2019 Week 2 0.000003 / mg/L /
Oct 2019 Week 1 0.000002 / mg/L /
Jul2019 Average 0.000003 / mg/L /
Oct 2019 Average 0.000002 / mg/L /
2019 Quarter 3 0.000003 / mg/L /
2019 Quarter 4 0.000002 / mg/L /
2019 2nd 6 Months(Avg) 0.0000025 / mg/L /
2019 2nd 6...(Max) 0.0000026 / mg/L /
2019 2nd 6...(Min) 0.0000024 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
07/11/2019 S JMC071119Self 0.0016 /0.3 mg/L 0.000009 / lbs/day
10/03/2019 P JMC100319POTW < 0.0003 /0.3 mg/L < 0.000003 / lbs/day
Jul 2019 Week 2 0.0016 / mg/L 0.000009 / lbs/day
Oct 2019 Week 1 < 0.0003 / mg/L < 0.000003 / lbs/day
Jul 2019 Average 0.0016 /0.2 mg/L 0.000009 / lbs/day
Oct 2019 Average < 0.0003 /0.2 mg/L < 0.000003 / lbs/day
2019 Quarter 3 0.0016 / mg/L 0.000009 / lbs/day
2019 Quarter 4 < 0.0003 / mg/L < 0.000003 / lbs/day
2019 2nd 6 Months(Avg) < 0.0009 / mg/L < 0.000006 / lbs/day
2019 2nd 6...(Max) 0.0016 / mg/L 0.000009 / lbs/day
2019 2nd 6...(Min) < 0.0003 / mg/L < 0.000003 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall.• 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2019 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/11/2019 S JMC071119Self 46.6 / mg/L 0.248 / lbs/day
10/03/2019 P JMC 100319POTW 25.4 / mg/L 0.262 / lbs/day
Jul 2019 Week 2 46.6 / mg/L 0.248 / lbs/day
Oct 2019 Week 1 25.4 / mg/L 0.262 / lbs/day
Jul 2019 Average 46.6 / mg/L 0.248 / lbs/day
Oct 2019 Average 25.4 / mg/L 0.262 / lbs/day
2019 Quarter 3 46.6 / mg/L 0.248 / lbs/day
2019 Quarter 4 25.4 / mg/L 0.262 / lbs/day
2019 2nd 6 Months(Avg) 36 / mg/L 0.255 / lbs/day
2019 2nd 6...(Max) 46.6 / mg/L 0.262 / lbs/day
2019 2nd 6...(Min) 25.4 / mg/L 0.248 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/11/2019 S JMC071119Self 51.6 / mg/L 0.275 / lbs/day
10/03/2019 P JMC 100319POTW 27.6 / mg/L 0.285 / lbs/day
Jul 2019 Week 2 51.6 / mg/L 0.275 / lbs/day
Oct 2019 Week 1 27.6 / mg/L 0.285 / lbs/day
Jul 2019 Average 51.6 / mg/L 0.275 / lbs/day
Oct 2019 Average 27.6 / mg/L 0.285 / lbs/day
2019 Quarter 3 51.6 / mg/L 0.275 / lbs/day
2019 Quarter 4 27.6 / mg/L 0.285 / lbs/day
2019 2nd 6 Months(Avg) 39.6 / mg/L 0.280 / lbs/day
2019 2nd 6...(Max) 51.6 / mg/L 0.285 / lbs/day
2019 2nd 6...(Min) 27.6 / mg/L 0.275 / lbs/day
2019 2nd 6... Count 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
10/03/2019 P JMC100319POTW < 2.5 /200 mg/L < /
Oct 2019 Week 1 < 2.5 / mg/L < /
Oct 2019 Average < 2.5 / mg/L < /
2019 Quarter 4 < 2.5 / mg/L < /
2019 2nd 6 Months(Avg) < 2.5 / mg/L < /
2019 2nd 6...(Max) < 2.5 / mg/L < /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/11/2019 S JMC071119Self 7.6 /6- 10.5 SU /
10/03/2019 P JMC 1003 1 9POTW 7.4 /6- 10.5 SU /
Jul 2019 Week 2 7.6 / SU /
Oct 2019 Week 1 7.4 / SU /
Jul 2019 Average 7.6 / SU /
Oct 2019 Average 7.4 / SU /
2019 Quarter 3 7.6 / SU /
2019 Quarter 4 7.4 / SU /
2019 2nd 6 Months(Avg) 7.5 / SU /
2019 2nd 6...(Max) 7.6 / SU /
2019 2nd 6...(Min) 7.4 / SU /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 11

•
.
JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
07/11/2019 S JMC071119Se1f < 0.0003 /0.160 mg/L < 0.000001 / lbs/day
10/03/2019 P JMC100319POTW < 0.0003 /0.160 mg/L < 0.000003 / lbs/day
Jul 2019 Week 2 < 0.0003 / mg/L < 0.000001 / lbs/day
Oct 2019 Week 1 < 0.0003 / mg/L < 0.000003 / lbs/day
Jul 2019 Average < 0.0003 /0.090 mg/L < 0.000001 / lbs/day
Oct 2019 Average < 0.0003 /0.090 mg/L < 0.000003 / lbs/day
2019 Quarter 3 < 0.0003 / mg/L < 0.000001 / lbs/day
2019 Quarter 4 < 0.0003 / mg/L < 0.000003 / lbs/day
2019 2nd 6 Months(Avg) < 0.0003 / mg/L < 0.000002 / lbs/day
2019 2nd 6...(Max) < 0.0003 / mg/L < 0.000003 / lbs/day
2019 2nd 6...(Min) < 0.0003 / mg/L < 0.000001 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Muss/Limit
Temperature
07/11/2019 S JMC071119Self 28 /66 °C /
10/03/2019 P JMC100319POTW 25 /66 °C /
Jul 2019 Week 2 28 / °C /
Oct 2019 Week 1 25 / °C /
Jul 2019 Average 28 / °C /
Oct 2019 Average 25 / °C /
2019 Quarter 3 28 / °C /
2019 Quarter4 25 / °C /
2019 2nd 6 Months(Avg) 26.5 / °C /
2019 2nd 6...(Max) 28 / °C /
2019 2nd 6...(Min) 25 / °C /
2019 2nd 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 11

JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/11/2019 S JMC071119Self 5.04 / mg/L 0.027 / lbs/day
10/03/2019 P JMC100319POTW 2.2 / mg/L 0.023 / lbs/day
Jul 2019 Week 2 5.04 / mg/L 0.027 / lbs/day
Oct 2019 Week 1 2.2 / mg/L 0.023 / lbs/day
Jul 2019 Average 5.04 / mg/L 0.027 / lbs/day
Oct 2019 Average 2.2 / mg/L 0.023 / lbs/day
2019 Quarter 3 5.04 / mg/L 0.027 / lbs/day
2019 Quarter 4 2.2 / mg/L 0.023 / lbs/day
2019 2nd 6 Months(Avg) 3.62 / mg/L 0.025 / lbs/day
2019 2nd 6...(Max) 5.04 / mg/L 0.027 / lbs/day
2019 2nd 6...(Min) 2.2 / mg/L 0.023 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus •
07/11/2019 S JMC071119Self < 0.01 / mg/L < 0.0001 / lbs/day
Jul 2019 Week 2 < 0.01 / mg/L < 0.0001 / lbs/day
Jul 2019 Average < 0.01 / mg/L < 0.0001 / lbs/day
2019 Quarter 3 < 0.01 / mg/L < 0.0001 / lbs/day
2019 2nd 6 Months(Avg) < 0.01 / mg/L < 0.0001 / lbs/day
2019 2nd 6...(Max) < 0.01 / mg/L < 0.0001 / lbs/day
2019 2nd 6...(Min) < 0.01 / mg/L < 0.0001 / lbs/day
2019 2nd 6...(Count) 1 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/11/2019 S JMC071119Self 0.058 /0.9 mg/L 0.000309 / lbs/day
10/03/2019 P JMC1003I9POTW 0.018 /0.9 mg/L 0.000186 / lbs/day
Jul 2019 Week 2 0.058 / mg/L 0.000309 / lbs/day
Oct 2019 Week 1 0.018 / mg/L 0.000186 / lbs/day
Jul 2019 Average 0.058 /0.56 mg/L 0.000309 / lbs/day
Oct 2019 Average 0.018 /0.56 mg/L 0.000186 / lbs/day
2019 Quarter 3 0.058 / mg/L 0.000309 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 10 of 11
l

•
JMC (USA), Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
2019 Quarter 4 0.018 / mg/L 0.000186 / lbs/day
2019 2nd 6 Months(Avg) 0.038 / mg/L 0.000248 / lbs/day
2019 2nd 6...(Max) 0.058 / mg/L 0.000309 / lbs/day
2019 2nd 6...(Min) 0.018 / mg/L 0.000186 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 11 of 11

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfa11: '001
Sample Date SamplelD Result/Limit Mass/Lim&
Ammonia
07/23/2019 S Micross072319Self 2.8 / mg/L 1.045 / lbs/day
09/25/2019 P Micross092519POTW 5.2 / mg/L 1.9119 / lbs/day
Jul 2019 Week 4 2.8 / mg/L 1.045 / lbs/day
Sep 2019 Week 4 5.2 / mg/L 1.9119 / lbs/day
Jul2019 Average 2.8 / mg/L 1.045 / lbs/day
Sep 2019 Average 5.2 / mg/L 1.9119 / lbs/day
2019 Quarter 3 4 / mg/L 1.4785 / lbs/day
2019 2nd 6 Months(Avg) 4 / mg/L 1.4785 / lbs/day
2019 2nd 6...(Max) 5.2 / mg/L 1.9119 / lbs/day
2019 2nd 6...(Min) 2.8 / mg/L 1.0450 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S Micross0719Flow 0.05185 /0.100 MGD /
08/31/2019 S Micross0819Flow 0.045827 /0.100 MGD /
09/30/2019 S Micross0919Flow 0.046106 /0.100 MGD /
10/31/2019 S Micross1019Flow 0.096777 /0.100 MGD /
11/30/2019 S Micross1119Flow 0.028159 /0.100 MGD /
12/31/2019 S Micross1219Flow 0.020123 /0.100 MGD /
Jul 2019 Week 4 0.05185 / MGD /
Aug 2019 Week 4 0.045827 / MGD /
2 19 Week 4 0.046106 MGD Sep 0 / /
Oct 2019 Week 4 0.096777 / MGD /
Nov 2019 Week 4 0.028159 / MGD /
Dec 2019 Week 4 0.020123 / MGD /
Jul 2019 Average 0.05185 /0.075 MGD /
Aug 2019 Average 0.045827 /0.075 MGD /
Sep 2019 Average 0.046106 /0.075 MGD /
Oct 2019 Average 0.096777 /0.075 MGD * /
Nov 2019 Average 0.028159 /0.075 MGD /
Dec 2019 Average 0.020123 /0.075 MGD /
2019 Quarter 3 0.047928 / MGD /
2019 Quarter 4 0.048353 / MGD /
2019 2nd 6 Months(Avg) 0.048140 / MGD /
2019 2nd 6...(Max) 0.096777 / MGD /
2019 2nd 6...(Min) 0.020123 / MGD /
2019 2nd 6...(Count) 6 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 Of

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 1 16.67 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
07/23/2019 S Micross072319Self < 0.001 / mg/L < 0.000373 / lbs/day
Jul 2019 Week 4 < 0.001 / mg/L < 0.000373 / lbs/day
Jul 2019 Average < 0.001 / mg/L < 0.000373 / lbs/day
2019 Quarter 3 < 0.001 / mg/L < 0.000373 / lbs/day
2019 2nd 6 Months(Avg) < 0.001 / mg/L < 0.000373 / lbs/day
2019 2nd 6...(Max) < 0.001 / mg/L < 0.000373 / lbs/day
2019 2nd 6...(Min) < 0.001 / mg/L < 0.000373 / lbs/day
2019 ' 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
07/23/2019 S Micross072319Self 15 / mg/L 5.5981 / lbs/day
09/25/2019 P Micross092519POTW 3I / mg/L 11.398 / lbs/day
Jul 2019 Week 4 15 / mg/L 5.5981 / lbs/day
Sep 2019 Week 4 31 / mg/L 11.398 / lbs/day
Jul2019 Average I5 / mg/L 5.5981 / lbs/day
Sep 2019 Average 31 / mg/L 11.398 / lbs/day
2019 Quarter 3 23 / mg/L 8.498 / lbs/day
2019 2nd 6 Months(Avg) 23 / mg/L 8.4981 / lbs/day
2019 2nd 6...(Max) 31 / mg/L 11.3980 / lbs/day
2019 2nd 6...(Min) 15 / mg/L 5.5981 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
07/23/2019 S Micross072319Self 0.002 / mg/L 0.000601 / lbs/day
Jul 2019 Week 4 0.002 / mg/L 0.000601 / lbs/day
Jul 2019 Average 0.002 / mg/L 0.000601 / lbs/day
2019 Quarter 3 0.002 / mg/L 0.000601 / lbs/day
2019 2nd 6 Months(Avg) 0.002 / mg/L 0.000601 / lbs/day
2019 2nd 6...(Max) 0.002 / mg/L 0.000601 / lbs/day
2019 2nd 6...(Min) 0.002 / mg/L 0.000601 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 9

Micross Advanced Interconnect Technology,LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
07/23/2019 S Micross072319Self 0.051 / mg/L 0.019146 / lbs/day
09/25/2019 P Micross092519POTW 0.068 / mg/L 0.025112 / lbs/day
Jul 2019 Week 4 0.051 / mg/L 0.019146 / lbs/day
Sep 2019 Week 4 0.068 / mg/L 0.025112 / lbs/day
Jul2019 Average 0.051 / mg/L 0.019146 / lbs/day
Sep 2019 Average 0.068 / mg/L 0.025112 / lbs/day
2019 Quarter 3 0.06 / mg/L 0.022129 / lbs/day
2019 2nd 6 Months(Avg) 0.060 / mg/L 0.022129 / lbs/day
2019 2nd 6...(Max) 0.068 / mg/L 0.025112 / lbs/day
2019 2nd 6...(Min) 0.051 / mg/L 0.019146 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
07/23/2019 S Micross072319Self < 0.003 / mg/L < 0.000933 / lbs/day
09/25/2019 P Micross092519POTW < 0.003 / mg/L < 0.000919 / lbs/day
Jul 2019 Week 4 < 0.003 / mg/L < 0.000933 / lbs/day
Sep 2019 Week 4 < 0.003 / mg/L < 0.000919 / lbs/day
Jul 2019 Average < 0.003 / mg/L < 0.000933 / lbs/day
Sep 2019 Average < 0.003 / mg/L < 0.000919 / lbs/day
2019 Quarter 3 < 0.003 / mg/L < 0.000926 / lbs/day
2019 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000926 / lbs/day
2019 2nd 6...(Max) < 0.003 / mg/L < 0.000933 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < 0.000919 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
07/23/2019 S Micross072319Self 0.69 /8 mg/L 0.2575 / lbs/day
09/25/2019 P Micross092519POTW 0.64 /8 mg/L 0.2353 / lbs/day
Jul 2019 Week 4 0.69 / mg/L 0.2575 / lbs/day
Sep 2019 Week 4 0.64 / mg/L 0.2353 / lbs/day
Jul 2019 Average 0.69 /6 mg/L 0.2575 / lbs/day
Sep 2019 Average 0.64 /6 mg/L 0.2353 / lbs/day
2019 Quarter 3 0.67 / mg/L 0.2464 / lbs/day
2019 2nd 6 Months(Avg) 0.67 / mg/L 0.2464 / lbs/day
2019 2nd 6...(Max) 0.69 / mg/L 0.2575 / lbs/day
2019 2nd 6...(Min) 0.64 / mg/L 0.2353 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : l
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
07/23/2019 S Micross072319Self < 0.005 / mg/L < 0.001866 / lbs/day
09/25/2019 P Micross092519POTW 0.0057 / mg/L 0.00211 / lbs/day
Jul 2019 Week 4 < 0.005 / mg/L < 0.001866 / lbs/day
Sep 2019 Week 4 0.0057 / mg/L 0.00211 / lbs/day
Jul 2019 Average < 0.005 / mg/L < 0.001866 / lbs/day
Sep 2019 Average 0.0057 / mg/L 0.00211 / lbs/day
2019 Quarter 3 < 0.0054 / mg/L < 0.001988 / lbs/day
2019 2nd 6 Months(Avg) < 0.0054 / mg/L < 0.001988 / lbs/day
2019 2nd 6...(Max) 0.0057 / mg/L 0.002110 / lbs/day
2019 2nd 6...(Min) < 0.005 / mg/L < 0.001866 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
08/02/2019 S Micross080219SelfHg 0.000057 /0.000142 mg/L /
09/24/2019 P Micross092419POTW 0.000012 /0.000142 mg/L /
Hg
11/04/2019 P Micross110419POTW 0.000014 /0.000142 mg/L /
Hg
Aug 2019 Week 1 0.000057 / mg/L /
Sep 2019 Week 4 0.000012 / mg/L /
Nov 2019 Week 1 0.000014 / mg/L /
Aug 2019 Average 0.000057 / mg/L /
Sep 2019 Average 0.000012 / mg/L /
Nov 2019 Average 0.000014 / mg/L /
2019 Quarter 3 0.000034 / mg/L /
2019 Quarter 4 0.000014 / mg/L /
2019 2nd 6 Months(Avg) 0.0000275 / mg/L /
2019 2nd 6...(Max) 0.0000567 / mg/L /
2019 2nd 6...(Min) 0.000012 / mg/L /
2019 2nd 6...(Count) 3 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Count: 3 Months Sampled: 3 Weeks Sampled: 3 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
07/23/2019 S Micross072319Self 0.017 / mg/L 0.0062 / lbs/day
Jul 2019 Week 4 0.017 / mg/L 0.0062 / lbs/day
Jul 2019 Average 0.017 / mg/L 0.0062 / lbs/day
2019 Quarter 3 0.017 / mg/L 0.0062 / lbs/day
2019 2nd 6 Months(Avg) 0.017 / mg/L 0.0062 / lbs/day
2019 2nd 6...(Max) 0.017 / mg/L 0.0062 / lbs/day
2019 2nd 6...(Min) 0.017 / mg/L 0.0062 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
07/23/2019 S Micross072319Self 0.0032 / mg/L 0.001187 / lbs/day
09/25/2019 P Micross092519POTW 0.0161 / mg/L 0.00592 / lbs/day
Jul 2019 Week 4 0.0032 / mg/L 0.001187 / lbs/day
Sep 2019 Week 4 0.0161 / mg/L 0.00592 / lbs/day
Jul2019 Average 0.0032 / mg/L 0.001187 / lbs/day
Sep 2019 Average 0.0161 / mg/L 0.00592 / lbs/day
2019 Quarter 3 0.0096 / mg/L 0.003553 / lbs/day
2019 2nd 6 Months(Avg) 0.0096 / mg/L 0.003553 / lbs/day
2019 2nd 6...(Max) 0.0161 / mg/L 0.005920 / lbs/day
2019 2nd 6...(Min) 0.0032 / mg/L 0.001187 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
07/23/2019 S Micross072319Self 0.5 / mg/L 0.202 / lbs/day
09/25/2019 P Micross092519POTW 0.7 / mg/L 0.239 / lbs/day
Jul 2019 Week 4 0.5 / mg/L 0.202 / lbs/day
Sep 2019 Week 4 0.7 / mg/L 0.239 / lbs/day
Jul 2019 Average 0.5 / mg/L 0.202 / lbs/day
Sep 2019 Average 0.7 / mg/L 0.239 / lbs/day
2019 Quarter 3 0.6 / mg/L 0.22 / lbs/day
2019 2nd 6 Months(Avg) 0.6 / mg/L 0.220 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 9

Micross Advanced Interconnect Technoloey, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2019 2nd 6...(Max) 0.7 / mg/L 0.239 / lbs/day
2019 2nd 6...(Min) 0.5 / mg/L 0.202 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
07/23/2019 S Micross072319Self 9.14 / mg/L 3.411 / lbs/day
09/25/2019 P Micross092519POTW 13.7 / mg/L 5.037 / lbs/day
Jul 2019 Week 4 9.14 / mg/L 3.411 / lbs/day
Sep 2019 Week 4 13.7 / mg/L 5.037 / lbs/day
Jul2019 Average 9.14 / mg/L 3.411 / lbs/day
Sep 2019 Average 13.7 / mg/L 5.037 / lbs/day
2019 Quarter 3 11.42 / mg/L 4.224 / lbs/day
2019 2nd 6 Months(Avg) 11.42 / mg/L 4.224 / lbs/day
2019 2nd 6...(Max) 13.7 / mg/L 5.037 / lbs/day
2019 2nd 6...(Min) 9.14 / mg/L 3.411 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
09/25/2019 P Micross092519POTW < 2.5 /200 mg/L < /
Sep 2019 Week 4 < 2.5 / mg/L < /
Sep 2019 Average < 2.5 / mg/L < /
2019 Quarter 3 < 2.5 / mg/L < /
2019 2nd 6 Months(Avg) < 2.5 / mg/L < /
2019 2nd 6...(Max) < 2.5 / mg/L < /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled: 1 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/23/2019 S Micross072319Self 6.8 /5.5- 10.5 SU /
09/25/2019 P Micross092519POTW 8.4 /5.5- 10.5 SU /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
pH
Jul2019 Week 4 6.8 / SU /
Sep 2019 Week 4 8.4 / SU /
Jul2019 Average 6.8 / SU /
Sep 2019 Average 8.4 / SU /
2019 Quarter 3 7.6 / SU / 1
2019 2nd 6 Months(Avg) 7.6 / SU /
2019 2nd 6...(Max) 8.4 / SU /
2019 2nd 6...(Min) 6.8 / SU /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
07/23/2019 S Micross072319Self < 0.001 / mg/L < 0.000373 / lbs/day
Jul 2019 Week 4 < 0.001 / mg/L < 0.000373 / lbs/day
Jul2019 Average < 0.001 / mg/L < 0.000373 / lbs/day
2019 Quarter 3 < 0.001 / mg/L < 0.000373 / lbs/day
2019 2nd 6 Months(Avg) < 0.001 / mg/L < 0.000373 / lbs/day
2019 2nd 6...(Max) < 0.001 / mg/L < 0.000373 / lbs/day
2019 2nd 6...(Min) < 0.001 / mg/L < 0.000373 / lbs/day
2019 2nd 6...(Count) I / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/23/2019 S Micross072319Self 24.4 /66 °C /
09/25/2019 P Micross092519POTW 25 /66 °C /
Jul 2019 Week 4 24.4 / °C /
Sep 2019 Week 4 25 / °C /
Jul 2019 Average 24.4 / °C /
Sep 2019 Average 25 / °C /
2019 Quarter 3 24.7 / °C /
2019 2nd 6 Months(Avg) 24.7 / °C /
2019 2nd 6...(Max) 25 / °C /
2019 2nd 6...(Min) 24.4 / °C /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
Tem peratu re
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tin
07/23/2019 S Micross072319Self 0.003 / mg/L 0.001171869 / lbs/day
09/25/2019 P Micross092519POTW < 0.013 / mg/L < 0.004595966 / lbs/day
Jul 2019 Week 4 0.003 / mg/L 0 / lbs/day
Sep 2019 Week 4 < 0.013 / mg/L < 0 / lbs/day
Jul 2019 Average 0.003 / mg/L 0 / lbs/day
Sep 2019 Average < 0.013 / mg/L < 0 / lbs/day
2019 Quarter 3 < 0.008 / mg/L < 0 / lbs/day
2019 2nd 6 Months(Avg) < 0.008 / mg/L < 0 / lbs/day
2019 2nd 6...(Max) < 0.013 / mg/L < 0 / lbs/day
2019 2nd 6...(Min) 0.003 / mg/L 0 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Titanium
07/23/2019 S Micross072319Se1f 0.001 / mg/L 0.0003 / lbs/day
Jul 2019 Week 4 0.001 / mg/L 0.0003 / lbs/day
Jul 2019 Average 0.001 / mg/L 0.0003 / lbs/day
2019 Quarter 3 0.001 / mg/L 0.0003 / lbs/day
2019 2nd 6 Months(Avg) 0.001 / mg/L 0.0003 / lbs/day
2019 2nd 6...(Max) 0.001 / mg/L 0.0003 / lbs/day
2019 2nd 6...(Min) 0.001 / mg/L 0.0003 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TKN
07/23/2019 S Micross072319Se1f 8.6 / mg/L 3.21 / lbs/day
09/25/2019 P Micross092519POTW 13 / mg/L 4.78 / lbs/day
Jul 2019 Week 4 8.6 / mg/L 3.21 / lbs/day
Sep 2019 Week 4 13 / mg/L 4.78 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 9

Micross Advanced Interconnect Technology, LLC
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type.• Effluent Wastewater Outfall: '001
Sample Date SamplelD Result/Limit Mass/Limit
TKN
Jul2019 Average 8.6 / mg/L 3.21 / lbs/day
Sep 2019 Average 13 / mg/L 4.78 / lbs/day
2019 Quarter 3 10.8 / mg/L 3.995 / lbs/day
2019 2nd 6 Months(Avg) 10.8 / mg/L 3.995 / lbs/day
2019 2nd 6...(Max) 13 / mg/L 4.780 / lbs/day
2019 2nd 6...(Min) 8.6 / mg/L 3.210 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
07/23/2019 S Micross072319Self 0.675 / mg/L 0.251914 / lbs/day
Jul 2019 Week 4 0.675 / mg/L 0.251914 / lbs/day
Jul2019 Average 0.675 / mg/L 0.251914 / lbs/day
2019 Quarter 3 0.675 / mg/L 0.251914 / lbs/day
2019 2nd 6 Months(Avg) 0.675 / mg/L 0.251914 / lbs/day
2019 2nd 6...(Max) 0.675 / mg/L 0.251914 / lbs/day
2019 2nd 6...(Min) 0.675 / mg/L 0.251914 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 9

Novan. Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
11/21/2019 P Novan112119POTW < 0.025 / mg/L < /
Nov 2019 Week 3 < 0.025 / mg/L < /
Nov 2019 Average < 0.025 / mg/L < /
2019 Quarter 4 < 0.025 / mg/L < /
2019 2nd 6 Months(Avg) < 0.025 / mg/L < /
2019 2nd 6...(Max) < 0.025 / mg/L < I
2019 2nd 6...(Min) < 0.025 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S Novan0719F1ow 0.000467 / MGD /
08/31/2019 S Novan0819F1ow 0 / MGD /
09/30/2019 S Novan0919Flow 0.000405 / MGD /
10/31/2019 S Novan1019Flow 0.000332 / MGD /
11/30/2019 S Novan1119Flow 0.000336 / MGD /
12/31/2019 S Novan1219Flow 0.000315 / MGD /
Jul 2019 Week 4 0.000467 / MGD /
Aug 2019 Week 4 0 / MGD /
Sep 2019 Week 4 0.000405 / MGD /
Oct 2019 Week 4 0.000332 / MGD /
Nov 2019 Week 4 0.000336 / MGD /
Dec 2019 Week 4 0.000315 / MGD /
Jul2019 Average 0.000467 / MGD /
Aug 2019 Average 0 / MGD /
Sep 2019 Average 0.000405 / MGD /
Oct 2019 Average 0.000332 / MGD /
Nov 2019 Average 0.000336 / MGD /
Dec 2019 Average 0.000315 / MGD /
2019 Quarter 3 0.000291 / MGD /
2019 Quarter 4 0.000328 / MGD /
' 2019 2nd 6 Months(Avg) 0.000309 / MGD /
2019 2nd 6...(Max) 0.000467 / MGD /
2019 2nd 6...(Min) 0 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
COD
09/09/2019 S Novan090919Self 657 / mg/L /
11/21/2019 P Novan112119POTW 747 / mg/L /
Sep 2019 Week 2 657 / mg/L /
Nov 2019 Week 3 747 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 5

Novan. Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
COD
Sep 2019 Average 657 / mg/L /
Nov 2019 Average 747 / mg/L /
2019 Quarter 3 657 / mg/L /
2019 Quarter 4 747 / mg/L /
2019 2nd 6 Months(Avg) 702 / mg/L /
2019 2nd 6...(Max) 747 / mg/L /
2019 2nd 6...(Min) 657 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
09/09/2019 S Novan090919Se1f 0.164 / mg/L /
11/21/2019 P Novan112119POTW 0.079 / mg/L /
Sep 2019 Week 2 0.164 / mg/L /
Nov 2019 Week 3 0.079 / mg/L /
Sep 2019 Average 0.164 / mg/L /
Nov 2019 Average 0.079 / mg/L /
2019 Quarter 3 0.164 / mg/L /
2019 Quarter 4 0.079 / mg/L /
2019 2nd 6 Months(Avg) 0.122 / mg/L /
2019 2nd 6...(Max) 0.164 / mg/L /
2019 2nd 6...(Min) 0.079 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
11/21/2019 P Novan112119POTW < 0.005 / mg/L < /
Nov 2019 Week 3 < 0.005 / mg/L < /
Nov 2019 Average < 0.005 / mg/L < /
2019 Quarter 4 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
11/21/2019 P Novan112119POTW < 0.005 / mg/L < /
Nov 2019 Week 3 < 0.005 / mg/L < /
Nov 2019 Average < 0.005 / mg/L < /
2019 Quarter 4 < 0.005 / mg/L < /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 5

Novan, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
09/09/2019 S Novan090919Se1f 0.000112 /0.000142 mg/L /
11/21/2019 P Novan112119POTWH 0.00004 /0.000142 mg/L /
g
Sep 2019 Week 2 0.000112 / mg/L /
Nov 2019 Week 3 0.00004 / mg/L /
Sep 2019 Average 0.000112 / mg/L /
Nov 2019 Average 0.00004 / mg/L /
2019 Quarter 3 0.000112 / mg/L /
2019 Quarter 4 0.00004 / mg/L /
2019 2nd 6 Months(Avg) 0.0000760 / mg/L /
2019 2nd 6...(Max) 0.000112 / mg/L /
2019 2nd 6...(Min) 0.0000399 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
11/21/2019 P Novan112119POTW < 0.005 / mg/L < /
Nov 2019 Week 3 < 0.005 / mg/L < /
Nov 2019 Average < 0.005 / mg/L < /
2019 Quarter 4 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 5

Novan, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfa11: 001
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
11/21/2019 P Novan112119POTW < 0.005 / mg/L < /
Nov 2019 Week 3 < 0.005 / mg/L < /
Nov 2019 Average < 0.005 / mg/L < /
2019 Quarter 4 < 0.005 / mg/L < /
2019 2nd 6 Months(Avg) < 0.005 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
pH
09/09/2019 S Novan090919Se1f 7.1 /6.0- 10.0 SU /
11/21/2019 P Novan112119POTW 7.9 /6.0- 10.0 SU /
Sep 2019 Week 2 7.1 / SU /
Nov 2019 Week 3 7.9 / SU /
Sep 2019 Average 7.1 / SU /
Nov 2019 Average 7.9 / SU /
2019 Quarter 3 7.1 / SU /
2019 Quarter 4 7.9 / SU /
2019 2nd 6 Months(Avg) 7.5 / SU /
2019 2nd 6...(Max) 7.9 / SU /
2019 2nd 6...(Min) 7.1 / SU /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mn Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/09/2019 S Novan090919Self 28 /66 °C /
11/21/2019 P Novan112119POTW 16 /66 °C /
Sep 2019 Week 2 28 / °C /
Nov 2019 Week 3 16 / °C /
Sep 2019 Average 28 / °C /
Nov 2019 Average 16 / °C /
2019 Quarter 3 28 / °C /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 5

Novan, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2019 Quarter 4 16 / °C /
2019 2nd 6 Months(Avg) 22 / °C /
2019 2nd 6...(Max) 28 / °C /
2019 2nd 6...(Min) 16 / °C /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
09/09/2019 S Novan090919Se1f 13.4 / mg/L /
11/21/2019 P Novan112119POTW 15.8 / mg/L /
Sep 2019 Week 2 13.4 / mg/L /
Nov 2019 Week 3 15.8 / mg/L /
Sep 2019 Average 13.4 / mg/L /
Nov 2019 Average 15.8 / mg/L /
2019 Quarter 3 13.4 / mg/L /
2019 Quarter 4 15.8 / mg/L /
2019 2nd 6 Months(Avg) 14.6 / mg/L /
2019 2nd 6...(Max) 15.8 / mg/L /
2019 2nd 6...(Min) 13.4 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
09/09/2019 S Novan090919Self 1.458 / mg/L /
Sep 2019 Week 2 1.458 / mg/L /
Sep 2019 Average 1.458 / mg/L /
2019 Quarter 3 1.458 / mg/L /
2019 2nd 6 Months(Avg) 1.458 / mg/L /
2019 2nd 6...(Max) 1.458 / mg/L /
2019 2nd 6...(Min) 1.458 / mg/L /
2019 2nd 6...(Count) 1 / /
Monday,February 17,2020 *Indicates Violation "Indicates TRC Violation Page 5 of 5

•
Phononic
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S Phononic0719F1ow 0.010648 / MGD /
08/31/2019 S Phononic0819F1ow 0.009552 / MGD /
09/30/2019 S Phononic0919Flow 0.01098 / MGD /
10/31/2019 S Phononic1019Flow 0.011201 / MGD /
11/30/2019 S Phononic1119Flow 0.00697 / MGD /
12/31/2019 S Phononic1219Flow 0.004116 / MGD /
Jul2019 Week 4 0.010648 / MGD /
Aug 2019 Week 4 0.009552 / MGD /
Sep 2019 Week 4 0.01098 / MGD /
Oct 2019 Week 4 0.011201 / MGD /
Nov 2019 Week 4 0.00697 / MGD /
Dec 2019 Week 4 0.004116 / MGD /
Jul 2019 Average 0.010648 /0.020 MGD /
Aug 2019 Average 0.009552 /0.020 MGD /
Sep 2019 Average 0.01098 /0.020 MGD /
Oct 2019 Average 0.011201 /0.020 MGD /
Nov 2019 Average 0.00697 /0.020 MGD /
Dec 2019 Average 0.004116 /0.020 MGD /
2019 Quarter 3 0.010393 / MGD /
2019 Quarter 4 0.007429 / MGD /
2019 2nd 6 Months(Avg) 0.008911 / MGD /
2019 2nd 6...(Max) 0.011201 / MGD /
2019 2nd 6...(Min) 0.004116 / MGD /
2019 2nd 6...(Count) 6 / /
Sample Count: 6 Months Sampled: 6 Weeks Sampled : 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
' Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
07/08/2019 P Phononic070819POT 0.066 / mg/L /
W
07/22/2019 S Phononic072219Self 0.044 / mg/L /
08/16/2019 S Phononic081619Se1f 0.089 / mg/L /
09/13/2019 S Phononic091319Self 0.056 / mg/L /
10/14/2019 S Phononic101419Se1f 0.136 / mg/L /
11/20/2019 S Phononic112019Self 0.158 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page I of 5

Phononic
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Bismuth
12/18/2019 S Phononic121819Self 0.096 / mg/L /
Jul 2019 Week 2 0.066 / mg/L /
Jul2019 Week 4 0.044 / mg/L /
Aug 2019 Week 3 0.089 / mg/L /
Sep 2019 Week 2 0.056 / mg/L /
Oct 2019 Week 2 0.136 / mg/L /
Nov 2019 Week 3 0.158 / mg/L /
Dec 2019 Week 3 0.096 / mg/L /
Jul 2019 Average 0.055 / mg/L /
Aug 2019 Average 0.089 / mg/L /
Sep 2019 Average 0.056 / mg/L /
Oct 2019 Average 0.136 / mg/L /
Nov 2019 Average 0.158 / mg/L /
Dec 2019 Average 0.096 / mg/L /
2019 Quarter 3 0.064 / mg/L /
2019 Quarter 4 0.13 / mg/L /
2019 2nd 6 Months(Avg) 0.092 / mg/L /
2019 2nd 6...(Max) 0.158 / mg/L /
2019 2nd 6...(Min) 0.044 / mg/L /
2019 2nd 6...(Count) 7 / /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/08/2019 P Phononic070819POT 0.000004 /0.000142 mg/L /
WHg
10/14/2019 S Phononic101419Se1f < 0.000001 /0.000142 mg/L < /
Jul 2019 Week 2 0.000004 / mg/L /
Oct 2019 Week 2 < 0.000001 / mg/L < /
Jul 2019 Average 0.000004 / mg/L /
Oct 2019 Average < 0.000001 / mg/L < /
2019 Quarter 3 0.000004 / mg/L /
2019 Quarter 4 < 0.000001 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0000022 / mg/L < /
2019 2nd 6...(Max) 0.0000039 / mg/L /
2019 2nd 6...(Min) < 0.0000005 / mg/L < /
2019 2nd 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 5
L

Phononic
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
10/14/2019 S Phononic101419Self < 0.003 / mg/L < 0.0004 / lbs/day
Oct 2019 Week 2 < 0.003 / mg/L < 0.0004 / lbs/day
Oct 2019 Average < 0.003 / mg/L < 0.0004 / lbs/day
2019 Quarter 4 < 0.003 / mg/L < 0.0004 / lbs/day
2019 2nd 6 Months(Avg) < 0.003 / mg/L < 0.0004 / lbs/day
2019 2nd 6...(Max) < 0.003 / mg/L < 0.0004 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < 0.0004 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Date SampleID Result/Limit Mass/Limit
Nickel
07/08/2019 P Phononic070819POT 0.113 / mg/L 0.009268 /0.02 lbs/day
W
07/22/2019 S Phononic072219Se1f 0.038 / mg/L 0.007454 /0.02 lbs/day
08/16/2019 S Phononic081619Se1f 0.091 / mg/L 0.012859 /0.02 lbs/day
09/13/2019 S Phononic091319Self 0.027 / mg/L 0.00271 /0.02 lbs/day
10/14/2019 S Phononic101419Se1f 0.086 / mg/L 0.012553 /0.02 lbs/day
11/20/2019 S Phononic112019Self 0.188 / mg/L 0.014622 /0.02 lbs/day
12/18/2019 S Phononic121819Self 0.134 / mg/L 0.009195 /0.02 lbs/day
Jul2019 Week 2 0.113 / mg/L 0.009268 / lbs/day
Jul 2019 Week 4 0.038 / mg/L 0.007454 / lbs/day
Aug 2019 Week 3 0.091 / mg/L 0.012859 / lbs/day
Sep 2019 Week 2 0.027 / mg/L 0.00271 / lbs/day
Oct 2019 Week 2 0.086 / mg/L 0.012553 / lbs/day
Nov 2019 Week 3 0.188 / mg/L 0.014622 / lbs/day
Dec 2019 Week 3 0.134 / mg/L 0.009195 / lbs/day
Jul2019 Average 0.0755 / mg/L 0.008361 / lbs/day
Aug 2019 Average 0.091 / mg/L 0.012859 / lbs/day
Sep 2019 Average 0.027 / mg/L 0.00271 / lbs/day
Oct 2019 Average 0.086 / mg/L 0.012553 / lbs/day
Nov 2019 Average 0.188 / mg/L 0.014622 / lbs/day
Dec 2019 Average 0.134 / mg/L 0.009195 / lbs/day
2019 Quarter 3 0.0673 / mg/L 0.008073 / lbs/day
2019 Quarter 4 0.136 / mg/L 0.012124 / lbs/day
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 5

Phononic
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2019 2nd 6 Months(Avg) 0.0967 / mg/L 0.009809 / lbs/day
2019 2nd 6...(Max) 0.188 / mg/L 0.014622 / lbs/day
2019 2nd 6...(Min) 0.027 / mg/L 0.002710 / lbs/day
2019 2nd 6...(Count) 7 / 7 /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/08/2019 P Phononic070819POT 7.2 /5.5- 10 SU /
W
10/14/2019 S Phononic101419Self 7.7 /5.5- 10 SU /
Jul2019 Week 2 7.2 / SU /
Oct 2019 Week 2 7.7 / SU /
Jul2019 Average 7.2 / SU /
Oct 2019 Average 7.7 / SU /
2019 Quarter 3 7.2 / SU /
2019 Quarter 4 7.7 / SU /
2019 2nd 6 Months(Avg) 7.45 / SU /
2019 2nd 6...(Max) 7.7 / SU /
2019 2nd 6...(Min) 7.2 / SU /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
07/08/2019 P Phononic070819POT 0.144 / mg/L /
W
07/22/2019 S Phononic072219Se1f 0.056 / mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 5

Phononic
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Tellurium
11/20/2019 S Phononic112019Se1f 0.269 / mg/L /
12/18/2019 S Phononic121819Se1f 0.325 / mg/L /
Jul 2019 Week 2 0.144 / mg/L /
Jul 2019 Week 4 0.056 / mg/L /
Aug 2019 Week 3 0.12 / mg/L /
Sep 2019 Week 2 0.165 / mg/L /
1 Week 2 0.193 mg/L /
Oct 20 9 /Nov 2019 Week 3 0.269 / mg/L /
Dec 2019 Week 3 0.325 / mg/L /
Jul2019 Average 0.1 / mg/L /
Aug 2019 Average 0.12 / mg/L /
Sep 2019 Average 0.165 / mg/L /
Oct 2019 Average 0.193 / mg/L /
Nov 2019 Average 0.269 / mg/L /
Dec 2019 Average 0.325 / mg/L /
2019 Quarter 3 0.121 / mg/L /
2019 Quarter 4 0.262 / mg/L /
2019 2nd 6 Months(Avg) 0.182 / mg/L /
2019 2nd 6...(Max) 0.325 / mg/L /
2019 2nd 6...(Min) 0.056 / mg/L /
2019 2nd 6...(Count) 7 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 5

PowerSecure
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Aluminum
08/26/2019 P PowerSecure082619P 3.83 / mg/L /
OTW
09/13/2019 S PowerSecure091319Se 3.89 / mg/L /
If
Aug 2019 Week 4 3.83 / mg/L /
Sep 2019 Week 2 3.89 / mg/L /
Aug 2019 Average 3.83 / mg/L /
Sep 2019 Average 3.89 / mg/L /
2019 Quarter 3 3.86 / mg/L /
2019 2nd 6 Months(Avg) 3.86 / mg/L /
2019 2nd 6...(Max) 3.89 / mg/L /
2019 2nd 6...(Min) 3.83 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S PowerSecure0719Flow 0.001538 / MGD /
08/21/2019 S PowerSecure0819Flow 0.001443 / MGD /
09/30/2019 S PowerSecure0919Flow 0.001365 / MGD /
10/17/2019 S PowerSecure1019Flow 0.001309 / MGD /
11/30/2019 S PowerSecure1119Flow 0.001286 / MGD /
12/19/2019 S PowerSecure1219Flow 0.001269 / MGD /
Jul2019 Week 4 0.001538 / MGD /
Aug 2019 Week 3 0.001443 / MGD /
Sep 2019 Week 4 0.001365 / MGD /
Oct 2019 Week 3 0.001309 / MGD /
Nov 2019 Week 4 0.001286 / MGD /
Dec 2019 Week 3 0.001269 / MGD /
Jul 2019 Average 0.001538 /0.006 MGD /
Aug 2019 Average 0.001443 /0.006 MGD /
Sep 2019 Average 0.001365 /0.006 MGD /
Oct 2019 Average 0.001309 /0.006 MGD /
Nov 2019 Average 0.001286 /0.006 MGD /
Dec 2019 Average 0.001269 /0.006 MGD /
2019 Quarter 3 0.001449 / MGD /
2019 Quarter 4 0.001309 / MGD /
2019 Quarter 4 0.001278 / MGD /
2019 Quarter 4 0.001309 / MGD /
2019 Quarter 4 0.001278 / MGD /
2019 2nd 6 Months(Avg) 0.001368 / MGD /
2019 2nd 6...(Max) 0.001538 / MGD /
2019 2nd 6...(Min) 0.001269 / MGD /
2019 2nd 6...(Count) 6 / /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page I of 8

PowerSecure •
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 5
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/26/2019 P PowerSecure082619P < 0.00008 /0.11 mg/L < /
OTW
09/13/2019 S PowerSecure091319Se < 0.0005 /0.11 mg/L < /
if
Aug 2019 Week 4 < 0.00008 / mg/L < /
Sep 2019 Week 2 < 0.0005 / mg/L < /
Aug 2019 Average < 0.00008 /0.07 mg/L < /
Sep 2019 Average < 0.0005 /0.07 mg/L < /
2019 Quarter 3 < 0.00029 / mg/L < /
2019 2nd 6 Months(Avg) < 0.00029 / mg/L < /
2019 2nd 6...(Max) < 0.0005 / mg/L < /
2019 2nd 6...(Min) < 0.00008 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
08/26/2019 P PowerSecure082619P < 0.001 /2.77 mg/L < /
OTW
09/13/2019 S PowerSecure091319Se < 0.003 /2.77 mg/L < /
if
Aug 2019 Week 4 < 0.001 / mg/L < /
Sep 2019 Week 2 < 0.003 / mg/L < /
Aug 2019 Average < 0.001 / 1.71 mg/L < /
Sep 2019 Average < 0.003 / 1.71 mg/L < /
2019 Quarter 3 < 0.002 / mg/L < /
2019 2nd 6 Months(Avg) < 0.002 / mg/L < /
2019 2nd 6...(Max) < 0.003 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 8

PowerSecure
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chromium
2019 2nd 6...(Min) < 0.001 I mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Copper
08/26/2019 P PowerSecure082619P 0.089 /3.38 mg/L /
OTW
09/13/2019 S PowerSecure091319Se 0.155 /3.38 mg/L /
If
Aug 2019 Week 4 0.089 / mg/L /
Sep 2019 Week 2 0.155 / mg/L /
Aug 2019 Average 0.089 /2.07 mg/L /
Sep 2019 Average 0.155 /2.07 mg/L /
2019 Quarter 3 0.122 / mg/L /
2019 2nd 6 Months(Avg) 0.122 / mg/L /
2019 2nd 6...(Max) 0.155 / mg/L /
2019 2nd 6...(Min) 0.089 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/26/2019 P PowerSecure082619P < 0.003 /0.60 mg/L < /
OTW
Aug 2019 Week 4 < 0.003 / mg/L < /
Aug 2019 Average < 0.003 /0.50 mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 8

PowerSecure •
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
2019 2nd 6...(Max) < 0.003 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Lead
08/26/2019 P PowerSecure082619P < 0.0003 /0.69 mg/L < /
OTW
09/13/2019 S PowerSecure091319Se < 0.0025 /0.69 mg/L < /
If
Aug 2019 Week 4 < 0.0003 / mg/L < /
Sep 2019 Week 2 < 0.0025 / mg/L < /
Aug 2019 Average < 0.0003 /0.43 mg/L < /
Sep 2019 Average < 0.0025 /0.43 mg/L < /
2019 Quarter 3 < 0.0014 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0014 / mg/I, < /
2019 2nd 6...(Max) < 0.0025 / mg/I < /
2019 2nd 6...(Min) < 0.0003 / mg/I < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Mercury- LL
08/26/2019 P PowerSecure082619P 0.0000299 /0.000142 mg/L /
OTWHg
09/13/2019 S PowerSecure091319Se < 0.0000005 /0.000142 mg/L < /
If
Aug 2019 Week 4 0.0000299 / mg/I, /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 8

PowerSecure
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
Sep 2019 Week 2 < 0.0000005 / mg/L < /
Aug 2019 Average 0.0000299 / mg/L /
Sep 2019 Average < 0.0000005 / mg/L < /
2019 Quarter 3 < 0.0000152 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0000152 / mg/L < /
2019 2nd 6...(Max) 0.0000299 / mg/L /
2019 2nd 6...(Min) < 0.0000005 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/26/2019 P PowerSecure082619P 0.003 / mg/L /
OTW
09/13/2019 S PowerSecure091319Se < 0.003 / mg/L < /
if
Aug 2019 Week 4 0.003 / mg/L /
Sep 2019 Week 2 < 0.003 / mg/L < /
Aug 2019 Average 0.003 / mg/L /
Sep 2019 Average < 0.003 / mg/L < /
2019 Quarter 3 < 0.003 / mg/L < /
2019 2nd 6 Months(Avg) < 0.003 / mg/L < /
2019 2nd 6...(Max) 0.003 / mg/L /
2019 2nd 6...(Min) < 0.003 / mg/L < / 1
2019 2nd 6...(Count) 2 / /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
08/26/2019 P PowerSecure082619P 0.0065 /1.3 mg/L /
OTW
09/13/2019 S PowerSecure091319Se 0.0127 / 1.3 mg/L /
If
Aug 2019 Week 4 0.0065 / mg/L /
Sep 2019 Week 2 0.0127 / mg/L /
Aug 2019 Average 0.0065 / 1 mg/L /
Sep 2019 Average 0.0127 / 1 mg/L /
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 8

PowerSecure
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 001 T Sample e: Effluent Wastewater Outtalk
P Y P
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
2019 Quarter 3 0.0096 / mg/L /
2019 2nd 6 Months(Avg) 0.0096 / mg/L /
2019 2nd 6...(Max) 0.0127 / mg/L /
2019 2nd 6...(Min) 0.0065 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
08/26/2019 P PowerSecure082619P 8.2 /6- 10 SU /
OTW
09/13/2019 S PowerSecure091319Se 8.4 /6- 10 SU /
If
Sep 2019 Week 2 8.4 / SU /
Aug 2019 Week 4 8.2 / SU /
Aug 2019 Average 8.2 / SU /
Sep 2019 Average 8.4 / SU /
2019 Quarter 3 8.3 / SU /
2019 2nd 6 Months(Avg) 8.3 / SU /
2019 2nd 6...(Max) 8.4 / SU /
2019 2nd 6...(Min) 8.2 / SU /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Silver
08/26/2019 P PowerSecure082619P < 0.0003 /0.43 mg/L < /
OTW
Wednesday.February 26.2020 *Indicates Violation **Indicates TRC Violation Page 6 of 8

PowerSecure
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Silver
09/13/2019 S PowerSecure091319Se < 0.0025 /0.43 mg/L < /
if
Aug 2019 Week 4 < 0.0003 / mg/L < /
Sep 2019 Week 2 < 0.0025 / mg/L < /
Aug 2019 Average < 0.0003 /0.24 mg/L < /
Sep 2019 Average < 0.0025 /0.24 mg/L < /
2019 Quarter 3 < 0.0014 / mg/L < /
2019 2nd 6 Months(Avg) < 0.0014 / mg/L < /
2019 2nd 6...(Max) < 0.0025 / mg/L < /
2019 2nd 6...(Min) < 0.0003 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
08/26/2019 P PowerSecure082619P 22 /66 °C /
OTW
09/13/2019 S PowerSecure091319Se 23.1 /66 °C /
if
Aug 2019 Week 4 22 / °C /
Sep 2019 Week 2 23.1 / °C /
Aug 2019 Average 22 / °C /
Sep 2019 Average 23.1 / °C /
2019 Quarter 3 22.6 / °C /
2019 2nd 6 Months(Avg) 22.6 / °C /
2019 2nd 6...(Max) 23.1 / °C /
2019 2nd 6...(Min) 22 / °C /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled : 2 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 8

PowerSecure • '
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TTO
09/16/2019 S PowerSecure091619Se 0.005 /2.13 mg/L /
If
Sep 2019 Week 3 0.005 / mg/L /
Sep 2019 Average 0.005 / mg/I. /
2019 Quarter 3 0.005 / mg/L /
2019 2nd 6 Months(Avg) 0.005 / mg/L /
2019 2nd 6...(Max) 0.005 / mg/L /
2019 2nd 6...(Min) 0.005 / mg/L /
2019 2nd 6...(Count) 1 / /
Sample Count: 1 Months Sampled: 1 Weeks Sampled : 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
08/26/2019 P PowerSecure082619P 0.385 /2.61 mg/L /
OTW
09/13/2019 S PowerSecure091319Se 0.252 /2.61 mg/L /
If
Aug 2019 Week 4 0.385 / mg/L /
Sep 2019 Week 2 0.252 / mg/L /
Aug 2019 Average 0.385 / 1.48 mg/L /
Sep 2019 Average 0.252 / 1.48 mg/L /
2019 Quarter 3 0.319 / mg/L /
2019 2nd 6 Months(Avg) 0.319 / mg/L /
2019 2nd 6...(Max) 0.385 / mg/L /
2019 2nd 6...(Min) 0.252 / mg/L /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Wednesday,February 26,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 8

SCM Metal Products. Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
09/13/2019 S SCM091319Se1f 4.1 / mg/L 0.8317 / lbs/day
09/24/2019 P SCM092419POTW 6.7 / mg/L 0.564 / lbs/day
Sep 2019 Week 2 4.1 / mg/L 0.8317 / lbs/day
Sep 2019 Week 4 6.7 / mg/L 0.564 / lbs/day
Sep 2019 Average 5.4 / mg/L 0.6978 / lbs/day
2019 Quarter 3 5.4 / mg/L 0.6978 / lbs/day
2019 2nd 6 Months(Avg) 5.4 / mg/L 0.6979 / lbs/day
2019 2nd 6...(Max) 6.7 / mg/L 0.8317 / lbs/day
2019 2nd 6...(Min) 4.1 / mg/L 0.5640 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S SCM0719F1ow 0.014838 /0.080 MGD /
08/31/2019 S SCM0819Flow 0.011116 /0.080 MGD /
09/30/2019 S SCM0919Flow 0.013139 /0.080 MGD /
10/31/2019 S SCM1019F1ow 0.010718 /0.080 MGD /
11/30/2019 S SCM1119Flow 0.014371 /0.080 MGD /
12/31/2019 S SCM1219Flow 0.008139 /0.080 MGD /
Jul 2019 Week 4 0.014838 / MGD /
Aug 2019 Week 4 0.011116 / MGD /
Sep 2019 Week 4 0.013139 / MGD /
Oct 2019 Week 4 0.010718 / MGD /
Nov 2019 Week 4 0.014371 / MGD /
Dec 2019 Week 4 0.008139 / MGD /
Jul 2019 Average 0.014838 /0.050 MGD /
Aug 2019 Average 0.011116 /0.050 MGD /
Sep 2019 Average 0.013139 /0.050 MGD /
Oct 2019 Average 0.010718 /0.050 MGD /
Nov 2019 Average 0.014371 /0.050 MGD /
Dec 2019 Average 0.008139 /0.050 MGD /
2019 Quarter 3 0.013031 / MGD /
2019 Quarter 4 0.011076 / MGD /
2019 2nd 6 Months(Avg) 0.012054 / MGD /
2019 2nd 6...(Max) 0.014838 / MGD /
2019 2nd 6...(Min) 0.008139 / MGD /
2019 2nd 6...(Count) 6 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 T Sample e: Effluent Wastewater Ou
P Y all: 001P �
Sample Count: 6 Months Sampled : 6 Weeks Sampled: 6 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
09/13/2019 S SCM091319Se1f < 0.0005 / mg/L < 0.000101 / lbs/day
09/24/2019 P SCM092419POTW < 0.00008 / mg/L < 0.000006 / lbs/day
Sep 2019 Week 2 < 0.0005 / mg/L < 0.000101 / lbs/day
Sep 2019 Week 4 < 0.00008 / mg/L < 0.000006 / lbs/day
Sep 2019 Average < 0.00029 / mg/L < 0.000054 / lbs/day
2019 Quarter 3 < 0.00029 / mg/L < 0.000054 / lbs/day
2019 2nd 6 Months(Avg) < 0.00029 / mg/L < 0.000054 / lbs/day
2019 2nd 6...(Max) < 0.0005 / mg/L < 0.000101 / lbs/day
2019 2nd 6...(Min) < 0.00008 / mg/L < 0.000006 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
09/13/2019 S SCM091319Self 15.2 / mg/L 3.0833 / lbs/day
09/24/2019 P SCM092419POTW 16 / mg/L 1.3469 / lbs/day
Sep 2019 Week 2 15.2 / mg/L 3.0833 / lbs/day
Sep 2019 Week 4 16 / mg/L 1.3469 / lbs/day
Sep 2019 Average 15.6 / mg/L 2.2151 / lbs/day
2019 Quarter 3 15.6 / mg/L 2.2151 / lbs/day
2019 2nd 6 Months(Avg) 15.6 / mg/L 2.2151 / lbs/day
2019 2nd 6...(Max) 16 / mg/L 3.0833 / lbs/day
2019 2nd 6...(Min) 15.2 / mg/L 1.3469 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Copper
09/13/2019 S SCM091319Self 0.06 /0.75 mg/L 0.01211 / lbs/day
09/24/2019 P SCM092419POTW 0.175 /0.75 mg/L 0.014732 / lbs/day
Sep 2019 Week 2 0.06 / mg/L 0.01211 / lbs/day
Sep 2019 Week 4 0.175 / mg/L 0.014732 / lbs/day
Sep 2019 Average 0.117 /0.50 mg/L 0.013421 / lbs/day
2019 Quarter 3 0.117 / mg/L 0.013421 / lbs/day
2019 2nd 6 Months(Avg) 0.117 / mg/L 0.013421 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Copper
2019 2nd 6...(Max) 0.175 / mg/L 0.014732 / lbs/day 1
2019 2nd 6...(Min) 0.060 / mg/L 0.012110 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
09/24/2019 P SCM092419POTW < 0.003 /0.04 mg/L < 0.00021 / lbs/day
Sep 2019 Week 4 < 0.003 / mg/L < 0.00021 / lbs/day
Sep 2019 Average < 0.003 /0.03 mg/L < 0.00021 / lbs/day
2019 Quarter 3 < 0.003 / mg/L < 0.00021 / lbs/day
2019 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000210 / lbs/day
2019 2nd 6...(Max) < 0.003 / mg/L < 0.000210 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < 0.000210 / lbs/day
2019 2nd 6...(Count) 1 / 1 /
Sample Count: 1 Months Sampled: I Weeks Sampled: 1 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
09/13/2019 S SCM091319Self < 0.05 / mg/L < 0.0101 / lbs/day
09/24/2019 P SCM092419POTW < 0.05 / mg/L < 0.0042 / lbs/day
Sep 2019 Week 2 < 0.05 / mg/L < 0.0101 / lbs/day
Sep 2019 Week 4 < 0.05 / mg/L < 0.0042 / lbs/day
Sep 2019 Average < 0.05 / mg/L < 0.0072 / lbs/day
2019 Quarter 3 < 0.05 / mg/L < 0.0072 / lbs/day
2019 2nd 6 Months(Avg) < 0.05 / mg/L < 0.0072 / lbs/day
2019 2nd 6...(Max) < 0.05 / mg/L < 0.0101 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 9

SCM Metal Products. Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2019 2nd 6...(Min) < 0.05 / mg/L < 0.0042 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Lead
09/13/2019 S SCM091319Self < 0.0025 /0.20 mg/L < 0.000507 / lbs/day
09/24/2019 P SCM092419POTW 0.0012 /0.20 mg/L 0.000101 / lbs/day
Sep 2019 Week 2 < 0.0025 / mg/L < 0.000507 / lbs/day
Sep 2019 Week 4 0.0012 / mg/L 0.000101 / lbs/day
Sep 2019 Average < 0.0019 /0.10 mg/L < 0.000304 / lbs/day
2019 Quarter 3 < 0.0019 / mg/L < 0.000304 / lbs/day
2019 2nd 6 Months(Avg) < 0.0019 / mg/L < 0.000304 / lbs/day
2019 2nd 6...(Max) < 0.0025 / mg/L < 0.000507 / lbs/day
2019 2nd 6...(Min) 0.0012 / mg/L 0.000101 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit 11as.s/Limit
Mercury-LL
09/13/2019 S SCM091319Self < 0.000001 /0.000142 mg/L < /
12/02/2019 P SCM120219POTWHg 0.000024 /0.000142 mg/L /
Sep 2019 Week 2 < 0.000001 / mg/L < /
Dec 2019 Week 1 0.000024 / mg/L /
Sep 2019 Average < 0.000001 / mg/L < /
Dec 2019 Average 0.000024 / mg/L /
2019 Quarter 3 < 0.000001 / mg/L < /
2019 Quarter 4 0.000024 / mg/L /
2019 2nd 6 Months(Avg) < 0.000012 / mg/L < /
2019 2nd 6...(Max) . 0.000024 / mg/L /
2019 2nd 6...(Min) < 0.000001 / mg/L < /
2019 2nd 6...(Count) 2 / /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 9
L

•
SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 2 Months Sampled: 2 Weeks Sampled: 2 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
09/13/2019 S SCM091319Self < 0.003 / mg/L < 0.0005 / lbs/day
09/24/2019 P SCM092419POTW < 0.001 / mg/L < 0.0001 / lbs/day
Sep 2019 Week 2 < 0.003 / mg/L < 0.0005 / lbs/day
Sep 2019 Week 4 < 0.001 / mg/L < 0.0001 / lbs/day
Sep 2019 Average < 0.002 / mg/L < 0.0003 / lbs/day
2019 Quarter 3 < 0.002 / mg/L < 0.0003 / lbs/day
2019 2nd 6 Months(Avg) < 0.002 / mg/L < 0.0003 / lbs/day
2019 2nd 6...(Max) < 0.003 / mg/L < 0.0005 / lbs/day
2019 2nd 6...(Min) < 0.001 / mg/L < 0.0001 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nickel
09/13/2019 S SCM091319Self < 0.0025 / mg/L < 0.000507 / lbs/day
09/24/2019 P SCM092419POTW 0.0017 / mg/L 0.000141 / lbs/day
Sep 2019 Week 2 < 0.0025 / mg/L < 0.000507 / lbs/day
Sep 2019 Week 4 0.0017 / mg/L 0.000141 / lbs/day
Sep 2019 Average < 0.0021 / mg/L < 0.000324 / lbs/day
2019 Quarter 3 < 0.0021 / mg/L < 0.000324 / lbs/day
2019 2nd 6 Months(Avg) < 0.0021 / mg/L < 0.000324 / lbs/day
2019 2nd 6...(Max) < 0.0025 / mg/L < 0.000507 / lbs/day
2019 2nd 6...(Min) 0.0017 / mg/L 0.000141 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
09/13/2019 S SCM091319Self 0.4 / mg/L 0.073 / lbs/day
09/24/2019 P SCM092419POTW 0.4 / mg/L 0.037 / lbs/day
Sep 2019 Week 2 0.4 / mg/L 0.073 / lbs/day
Sep 2019 Week 4 0.4 / mg/L 0.037 / lbs/day
Sep 2019 Average 0.4 / mg/L 0.055 / lbs/day
2019 Quarter 3 0.4 / mg/L 0.055 / lbs/day
2019 2nd 6 Months(Avg) 0.4 / mg/L 0.055 / lbs/day
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
2019 2nd 6...(Max) 0.4 / mg/L 0.073 / lbs/day
2019 2nd 6...(Min) 0.4 / mg/L 0.037 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Dale SamplelD Result/Limit Mass/Limit
Nitrogen,Total
09/13/2019 S SCM091319Self 5.2 / mg/L 1.055 / lbs/day
09/24/2019 P SCM092419POTW 13.4 / mg/L 1.128 / lbs/day
Sep 2019 Week 2 5.2 / mg/L 1.055 / lbs/day
Sep 2019 Week 4 13.4 / mg/L 1.128 / lbs/day
Sep 2019 Average 9.3 / mg/L 1.091 / lbs/day
2019 Quarter 3 9.3 / mg/L 1.091 / lbs/day
2019 2nd 6 Months(Avg) 9.3 / mg/L 1.091 / lbs/day
2019 2nd 6...(Max) 13.4 / mg/L 1.128 / lbs/day
2019 2nd 6...(Min) 5.2 / mg/L 1.055 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
09/13/2019 S SCM091319Self 8.4 /200 mg/L /
09/24/2019 P SCM092419POTW < 2.5 /200 mg/L < /
Sep 2019 Week 2 8.4 / mg/L /
1 Sep 2019 Week 4 < 2.5 / mg/L < /
Sep 2019 Average < 5.45 / mg/L < /
2019 Quarter 3 < 5.45 / mg/L < /
2019 2nd 6 Months(Avg) < 5.45 / mg/L < /
2019 2nd 6...(Max) 8.4 / mg/L /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
09/13/2019 S SCM091319Self 7.1 /6.0- 10.5 SU /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 9
L

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SampleID Result/Limit Mass/Limit
pH
09/24/2019 P SCM092419POTW 7.6 /6.0- 10.5 SU /
Sep 2019 Week 2 7.1 / SU /
Sep 2019 Week 4 7.6 / SU /
Sep 2019 Average 7.35 / SU /
2019 Quarter 3 7.35 / SU /
2019 2nd 6 Months(Avg) 7.35 / SU /
2019 2nd 6...(Max) 7.6 / SU /
2019 2nd 6...(Min) 7.1 / SU /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled: 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Selenium
09/13/2019 S SCM091319SeIf < 0.005 / mg/L < 0.001014 / lbs/day
09/24/2019 P SCM092419POTW < 0.0005 / mg/L < 0.000042 / lbs/day
Sep 2019 Week 2 < 0.005 / mg/L < 0.001014 / lbs/day
Sep 2019 Week 4 < 0.0005 / mg/L < 0.000042 / lbs/day
Sep 2019 Average < 0.0028 / mg/L < 0.000528 / lbs/day
2019 Quarter 3 < 0.0028 / mg/L < 0.000528 / lbs/day
2019 2nd 6 Months(Avg) < 0.0028 / mg/L < 0.000528 / lbs/day
2019 2nd 6...(Max) < 0.005 / mg/L < 0.001014 / lbs/day
2019 2nd 6...(Min) < 0.0005 / mg/L < 0.000042 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
09/13/2019 S SCM091319Self 25.7 /66 °C /
09/24/2019 P SCM092419POTW 28 /66 °C /
Sep 2019 Week 2 25.7 / °C /
Sep 2019 Week 4 28 / °C /
Sep 2019 Average 26.9 / °C /
2019 Quarter 3 26.9 / °C /
2019 2nd 6 Months(Avg) 26.9 / °C /
2019 2nd 6...(Max) 28 / °C /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 9

SCM Metal Products, Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
2019 2nd 6...(Min) 25.7 / °C /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled : 2 Quarters Sampled: 1
# % # % # % # 14
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
09/13/2019 S SCM091319Se1f 4.8 / mg/L 0.974 / lbs/day
09/24/2019 P SCM092419POTW 13 / mg/L 1.094 / lbs/day
Sep 2019 Week 2 4.8 / mg/L 0.974 / lbs/day
Sep 2019 Week 4 13 / mg/L 1.094 / lbs/day
Sep 2019 Average 8.9 / mg/L 1.034 / lbs/day
2019 Quarter 3 8.9 / mg/L 1.034 / lbs/day
2019 2nd 6 Months(Avg) 8.9 / mg/L 1.034 / lbs/day
2019 2nd 6...(Max) 13 / mg/L 1.094 / lbs/day
2019 2nd 6...(Min) 4.8 / mg/L 0.974 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
09/13/2019 S SCM091319Self 1.1 / mg/L 0.2231 / lbs/day
09/24/2019 P SCM092419POTW 1.98 / mg/L 0.1667 / lbs/day
Sep 2019 Week 2 1.1 / mg/L 0.2231 / lbs/day
Sep 2019 Week 4 1.98 / mg/L 0.1667 / lbs/day
Sep 2019 Average 1.54 / mg/L 0.1949 / lbs/day
2019 Quarter 3 1.54 / mg/L 0.1949 / lbs/day
2019 2nd 6 Months(Avg) 1.54 / mg/L 0.1949 / lbs/day
2019 2nd 6...(Max) 1.98 / mg/L 0.2231 / lbs/day
2019 2nd 6...(Min) 1.1 / mg/L 0.1667 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
09/13/2019 S SCM091319Self 0.0676 / mg/L /
Sep 2019 Week 2 0.0676 / mg/L /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 9
L

SCM Metal Products. Inc.
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Ou all: 001
ffl �
P YP
Sample Date SamplelD Result/Limit Mass/Limit
VOC
Sep 2019 Average 0.0676 / mg/L /
2019 Quarter 3 0.0676 / mg/L /
2019 2nd 6 Months(Avg) 0.0676 / mg/L /
2019 2nd 6...(Max) 0.0676 / mg/L /
2019 2nd 6...(Min) 0.0676 / mg/L /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit
Zinc
09/13/2019 S SCM091319Self 0.381 / mg/L 0.077284 / lbs/day
09/24/2019 P SCM092419POTW 0.801 / mg/L 0.067431 / lbs/day
Sep 2019 Week 2 0.381 / mg/L 0.077284 / lbs/day
Sep 2019 Week 4 0.801 / mg/L 0.067431 / lbs/day
Sep 2019 Average 0.591 / mg/L 0.072358 / lbs/day I
2019 Quarter 3 0.591 / mg/L 0.072358 / lbs/day
2019 2nd 6 Months(Avg) 0.591 / mg/L 0.072358 / lbs/day
2019 2nd 6...(Max) 0.801 / mg/L 0.077284 / lbs/day
2019 2nd 6...(Min) 0.381 / mg/L 0.067431 / lbs/day
2019 2nd 6...(Count) 2 / 2 /
Monday,February 17,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Ammonia
08/16/2019 S UTP1081619Self 3.9 / mg/L /
08/27/2019 P UTP1082719POTW 14.2 / mg/L 3.6736 / lbs/day
Aug 2019 Week 3 3.9 / mg/L /
Aug 2019 Week 4 14.2 / mg/L 3.6736 / lbs/day
Aug 2019 Average 9.05 / mg/L 3.6736 / lbs/day
2019 Quarter 3 9.05 / mg/L 3.6736 / lbs/day
2019 2nd 6 Months(Avg) 9.05 / mg/L 3.6736 / lbs/day
2019 2nd 6...(Max) 14.2 / mg/L 3.6736 / lbs/day
2019 2nd 6...(Min) 3.9 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Average Flow for Month
07/31/2019 S UTP10719Flow 0.042485 / MGD /
08/31/2019 S UTP10819Flow 0.036272 / MGD /
09/30/2019 S UTP10919Flow 0.036061 / MGD /
10/31/2019 S UTP11019Flow 0.030445 / MGD /
11/30/2019 S UTP11119Flow 0.022503 / MGD /
12/31/2019 S UTP11219Flow 0.026603 / MGD /
Jul 2019 Week 4 0.042485 / MGD /
Aug 2019 Week 4 0.036272 / MGD /
Sep 2019 Week 4 0.036061 / MGD /
Oct 2019 Week 4 0.030445 / MGD /
Nov 2019 Week 4 0.022503 / MGD /
Dec 2019 Week 4 0.026603 / MGD /
Jul 2019 Average 0.042485 /0.050 MGD /
Aug 2019 Average 0.036272 /0.050 MGD /
Sep 2019 Average 0.036061 /0.050 MGD /
Oct 2019 Average 0.030445 /0.050 MGD /
Nov 2019 Average 0.022503 /0.050 MGD /
Dec 2019 Average 0.026603 /0.050 MGD /
2019 Quarter 3 0.038273 / MGD /
2019 Quarter 4 0.026517 / MGD /
2019 2nd 6 Months(Avg) 0.032395 / MGD / 1
2019 2nd 6...(Max) 0.042485 / MGD /
2019 2nd 6...(Min) 0.022503 / MGD /
2019 2nd 6...(Count) 6 / /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page I of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Count: 6 Months Sampled: 6 Weeks Sampled: 6 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
BOD
08/16/2019 S UTP1081619Self 71 / mg/L /
08/27/2019 P UTP1082719POTW 277 / mg/L 71.662 / lbs/day
Aug 2019 Week 3 71 / mg/L /
Aug 2019 Week 4 277 / mg/L 71.662 / lbs/day
Aug 2019 Average 174 / mg/L 71.662 / lbs/day
2019 Quarter 3 174 / mg/L 71.662 / lbs/day
2019 2nd 6 Months(Avg) 174 / mg/L 71.662 / lbs/day
2019 2nd 6...(Max) 277 / mg/L 71.662 / lbs/day
2019 2nd 6...(Min) 71 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cadmium
08/16/2019 S UTP1081619Self < 0.0005 / mg/L < /
08/27/2019 P UTP1082719POTW < 0.00008 / mg/L < 0.000019 / lbs/day
Aug019 Week 3 < 0.0005 / mg/L <
g g /
Aug 2019 Week 4 < 0.00008 / mg/L < 0.000019 / lbs/day
Aug 2019 Average < 0.00029 / mg/L < 0.000019 / lbs/day
2019 Quarter 3 < 0.00029 / mg/L < 0.000019 / lbs/day
2019 2nd 6 Months(Avg) < 0.00029 / mg/L < 0.000019 / lbs/day
2019 2nd 6...(Max) < 0.0005 / mg/L < 0.000019 / lbs/day
2019 2nd 6...(Min) < 0.00008 / mg/L < /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
08/16/2019 S UTP1081619Self 28.5 / mg/L /
08/27/2019 P UTP1082719POTW 58 / mg/L 15.005 / lbs/day
Aug 2019 Week 3 28.5 / mg/L /
Aug 2019 Week 4 58 / mg/L 15.005 / lbs/day
Aug 2019 Average 43.25 / mg/L 15.005 / lbs/day
2019 Quarter 3 43.25 / mg/L 15.005 / lbs/day
2019 2nd 6 Months(Avg) 43.25 / mg/L 15.005 / lbs/day
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Chloride
2019 2nd 6...(Max) 58 / mg/L 15.0050 / lbs/day
2019 2nd 6...(Min) 28.5 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
COD
08/16/2019 S UTP1081619Self 285 / mg/L /
08/27/2019 P UTP1082719POTW 519 / mg/L 134.27 / lbs/day
Aug 2019 Week 3 285 / mg/L /
Aug 2019 Week 4 519 / mg/L 134.27 / lbs/day
Aug 2019 Average 402 / mg/L 134.27 / lbs/day
2019 Quarter 3 402 / mg/L 134.27 / lbs/day
2019 2nd 6 Months(Avg) 402 / mg/L 134.27 / lbs/day
2019 2nd 6...(Max) 519 / mg/L 134.27 / lbs/day
2019 2nd 6...(Min) 285 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Cyanide
08/16/2019 S UTP1081619Se1f < 0.004 / mg/L < /
08/27/2019 P UTP1082719POTW < 0.003 / mg/L < 0.000647 / lbs/day
Aug 2019 Week 3 < 0.004 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < 0.000647 / lbs/day
Aug 2019 Average < 0.003 / mg/L < 0.000647 / lbs/day
2019 Quarter 3 < 0.003 / mg/L < 0.000647 / lbs/day
2019 2nd 6 Months(Avg) < 0.003 / mg/L < 0.000647 / lbs/day
2019 2nd 6...(Max) < 0.004 / mg/L < 0.000647 / lbs/day
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 2 / 1 /
Sample Date .SamplelD Result/Limit Mass/Limit
Fluoride
08/16/2019 S UTP1081619Self < 0.05 / mg/L < /
08/27/2019 P UTP1082719POTW 0.23 / mg/L 0.0595 / lbs/day
Aug 2019 Week 3 < 0.05 / mg/L < /
Aug 2019 Week 4 0.23 / mg/L 0.0595 / lbs/day
Aug 2019 Average < 0.14 / mg/L < 0.0595 / lbs/day
2019 Quarter 3 < 0.14 / mg/L < 0.0595 / lbs/day
2019 2nd 6 Months(Avg) < 0.14 / mg/L < 0.0595 / lbs/day
2019 2nd 6...(Max) 0.23 / mg/L 0.0595 / lbs/day
2019 2nd 6...(Min) < 0.05 / mg/L < /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall:: 001
Sample Date SamplelD Result/Limit Mass/Limit
Fluoride
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Mercury-LL
07/19/2019 S UTP1071919Se1f 0.000016 /0.000142 mg/L /
08/16/2019 S UTP1081619Self 0.000002 /0.000142 mg/L /
08/26/2019 P UTP1082619POTWHg 0.00012 /0.000142 mg/L /
09/13/2019 S UTP1091319Self 0.000004 /0.000142 mg/L /
10/11/2019 S UTP1101119Se1f 0.000005 /0.000142 mg/L /
11/21/2019 S UTP1112119Se1f 0.000008 /0.000142 mg/L /
12/30/2019 S UTP1123019SelfHg 0.000003 /0.000142 mg/L /
Jul2019 Week 3 0.000016 / mg/L /
Aug 2019 Week 3 0.000002 / mg/L /
Aug 2019 Week 4 0.00012 / mg/L /
Sep 2019 Week 2 0.000004 / mg/L /
Oct 2019 Week 2 0.000005 / mg/L /
Nov 2019 Week 3 0.000008 / mg/L /
Dec 2019 Week 4 0.000003 / mg/L /
Jul 2019 Average 0.000016 / mg/L /
Aug 2019 Average 0.000061 / mg/L /
Sep 2019 Average 0.000004 / mg/L /
Oct 2019 Average 0.000005 / mg/L /
Nov 2019 Average 0.000008 / mg/L /
Dec 2019 Average 0.000003 / mg/L /
2019 Quarter 3 0.000036 / mg/L /
2019 Quarter 4 0.000005 / mg/L /
2019 2nd 6 Months(Avg) 0.000023 / mg/L /
2019 2nd 6...(Max) 0.00012 / mg/L /
2019 2nd 6...(Min) 0.000002 / mg/L /
2019 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Moh bdenum
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Molybdenum
08/16/2019 S UTP1081619Se1f < 0.003 / mg/L < /
08/27/2019 P UTP1082719POTW < 0.001 / mg/L < 0.0003 / lbs/day
Aug 2019 Week 3 < 0.003 / mg/L < /
Aug 2019 Week 4 < 0.001 / mg/L < 0.0003 / lbs/day
Aug 2019 Average < 0.002 / mg/L < 0.0003 / lbs/day
2019 Quarter 3 < 0.002 / mg/L < 0.0003 / lbs/day
2019 2nd 6 Months(Avg) < 0.002 / mg/L < 0.0003 / lbs/day
2019 2nd 6...(Max) < 0.003 / mg/L < 0.0003 / lbs/day
2019 2nd 6...(Min) < 0.001 / mg/L < /
2019 2nd 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrate-Nitrite
08/16/2019 S UTP1081619Se1f 0.2 / mg/L /
08/27/2019 P UTP1082719POTW 0.4 / mg/L 0.106 / lbs/day
Aug 2019 Week 3 0.2 / mg/L /
Aug 2019 Week 4 0.4 / mg/L 0.106 / lbs/day
Aug 2019 Average 0.3 / mg/L 0.106 / lbs/day
2019 Quarter 3 0.3 / mg/L 0.106 / lbs/day
2019 2nd 6 Months(Avg) 0.3 / mg/L 0.106 / lbs/day
2019 2nd 6...(Max) 0.4 / mg/L 0.106 / lbs/day
2019 2nd 6...(Min) 0.2 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Nitrogen,Total
08/16/2019 S UTP1081619Self 12 / mg/L /
08/27/2019 P UTP1082719POTW 45.4 / mg/L 11.745 / lbs/day
Aug 2019 Week 3 12 / mg/L /
Aug 2019 Week 4 45.4 / mg/L 11.745 / lbs/day
Aug 2019 Average 28.7 / mg/L 11.745 / lbs/day
2019 Quarter 3 28.7 / mg/L 11.745 / lbs/day
2019 2nd 6 Months(Avg) 28.7 / mg/L 11.745 / lbs/day
2019 2nd 6...(Max) 45.4 / mg/L 11.745 / lbs/day
2019 2nd 6...(Min) 12 / mg/L /
2019 2nd 6...(Count) 2 / I /
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
08/16/2019 S UTP1081619Self < 2.5 /200 mg/L < /
08/27/2019 P UTP1082719POTW < 2.5 /200 mg/L < /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
Oil&Grease,Total
Aug 2019 Week 3 < 2.5 / mg/L < /
Aug 2019 Week 4 < 2.5 / mg/L < /
Aug 2019 Average < 2.5 / mg/L < /
2019 Quarter 3 < 2.5 / mg/L < /
2019 2nd 6 Months(Avg) < 2.5 / mg/L < /
2019 2nd 6...(Max) < 2.5 / mg/L < /
2019 2nd 6...(Min) < 2.5 / mg/L < /
2019 2nd 6...(Count) 2 / /
Sample Count: 2 Months Sampled: 1 Weeks Sampled: 2 Quarters Sampled : 1
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
pH
07/19/2019 S UTP1071919Self 7.4 /5.5- 10 SU /
08/16/2019 S UTP1081619Se1f 8.9 /5.5- 10 SU /
08/27/2019 P UTP1082719POTW 7.9 /5.5- 10 SU /
09/13/2019 S UTP1091319Se1f 6.5 /5.5- 10 SU /
10/11/2019 S UTP1101119Se1f 7.9 /5.5- 10 SU /
11/21/2019 S UTP1112119Se1f 6.7 /5.5- 10 SU /
12/19/2019 S UTP1121919Se1f 6.3 /5.5- 10 SU /
Jul 2019 Week 3 7.4 / SU /
Aug 2019 Week 3 8.9 / SU /
Aug 2019 Week 4 7.9 / SU /
Sep 2019 Week 2 6.5 / SU /
Oct 2019 Week 2 7.9 / SU /
Nov 2019 Week 3 6.7 / SU /
Dec 2019 Week 3 6.3 / SU /
Jul2019 Average 7.4 / SU /
Aug 2019 Average 8.4 / SU /
Sep 2019 Average 6.5 / SU /
Oct 2019 Average 7.9 / SU /
Nov 2019 Average 6.7 / SU /
Dec 2019 Average 6.3 / SU /
2019 Quarter 3 7.68 / SU /
2019 Quarter 4 6.97 / SU /
2019 2nd 6 Months(Avg) 7.37 / SU /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 6 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Li,nit Mass/Limit
pH
2019 2nd 6...(Max) 8.9 / SU /
2019 2nd 6...(Min) 6.3 / SU /
2019 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled: 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Temperature
07/19/2019 S UTP1071919Self 22.5 /66 °C /
08/16/2019 S UTP1081619Self 25.1 /66 °C /
08/27/2019 P UTP1082719POTW 26 /66 °C /
09/13/2019 S UTP1091319Se1f 23.2 /66 °C /
10/11/2019 S UTP1101119Se1f 24.6 /66 °C /
11/21/2019 S UTP1112119Se1f 19.8 /66 °C /
12/19/2019 S UTP1121919Se1f 18.4 /66 °C /
Jul 2019 Week 3 22.5 / °C /
Aug 2019 Week 3 25.1 / °C /
Aug 2019 Week 4 26 / °C /
Sep 2019 Week 2 23.2 / °C /
Oct 2019 Week 2 24.6 / °C /
Nov 2019 Week 3 19.8 / °C /
Dec 2019 Week 3 18.4 / °C /
Jul2019 Average 22.5 / °C /
Aug 2019 Average 25.6 / °C /
Sep 2019 Average 23.2 / °C /
Oct 2019 Average 24.6 / °C /
Nov 2019 Average 19.8 / °C /
Dec 2019 Average 18.4 / °C /
2019 Quarter 3 24.2 / °C /
2019 Quarter 4 20.9 / °C /
2019 2nd 6 Months(Avg) 22.8 / °C /
2019 2nd 6...(Max) 26 / °C /
2019 2nd 6...(Min) 18.4 / °C /
2019 2nd 6...(Count) 7 I /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 7 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type.• Effluent Wastewater Outfall: 001
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C : 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C : 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC : 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC : 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
TKN
08/16/2019 S UTP1081619Self 11.9 / mg/L /
08/27/2019 P UTP1082719POTW 45 / mg/L 11.642 / lbs/day
Aug 2019 Week 3 11.9 / mg/L /
Aug 2019 Week 4 45 / mg/L 11.642 / lbs/day
Aug 2019 Average 28.45 / mg/L 11.642 / lbs/day
2019 Quarter 3 28.45 / mg/L 11.642 / lbs/day
2019 2nd 6 Months(Avg) 28.45 / mg/L 11.642 / lbs/day
2019 2nd 6...(Max) 45 / mg/L 11.642 / lbs/day
2019 2nd 6...(Min) 11.9 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
Total Phosphorus
08/16/2019 S UTP1081619Self 1.8 / mg/L /
08/27/2019 P UTP1082719POTW 4.47 / mg/L 1.1564 / lbs/day
Aug 2019 Week 3 1.8 / mg/L /
Aug 2019 Week 4 4.47 / mg/L 1.1564 / lbs/day
Aug 2019 Average 3.135 / mg/L 1.1564 / lbs/day
2019 Quarter 3 3.135 / mg/L 1.1564 / lbs/day
2019 2nd 6 Months(Avg) 3.135 / mg/L 1.1564 / lbs/day
2019 2nd 6...(Max) 4.47 / mg/L I.1564 / lbs/day
2019 2nd 6...(Min) 1.8 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
TSS
08/16/2019 S UTP1081619Self 79.6 / mg/L /
08/27/2019 P UTP1082719POTW 264 / mg/L 68.298595 / lbs/day
Aug 2019 Week 3 79.6 / mg/L /
Aug 2019 Week 4 264 / mg/L 68.298595 / lbs/day
Aug 2019 Average 171.8 / mg/L 68.298595 / lbs/day
2019 Quarter 3 171.8 / mg/L 68.298595 / lbs/day
2019 2nd 6 Months(Avg) 171.8 / mg/L 68.2986 / lbs/day
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 8 of 9
I

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 001
Sample Date SamplelD Result/Limit Mass/Limit
TSS
2019 2nd 6...(Max) 264 / mg/L 68.298595 / lbs/day
2019 2nd 6...(Min) 79.6 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
Sample Date SamplelD Result/Limit Mass/Limit
VOC
08/16/2019 S UTP1081619Self 0.0227 / mg/L /
Aug 2019 Week 3 0.0227 / mg/L /
Aug 2019 Average 0.0227 / mg/L /
2019 Quarter 3 0.0227 / mg/L /
2019 2nd 6 Months(Avg) 0.0227 / mg/L /
2019 2nd 6...(Max) 0.0227 / mg/L /
2019 2nd 6...(Min) 0.0227 / mg/L /
2019 2nd 6...(Count) 1 / /
Sample Date SamplelD Result/Limit Mass/Limit 1
Zinc
08/16/2019 S UTP1081619Se1f 0.22 / mg/L /
08/27/2019 P UTP1082719POTW 0.395 / mg/L 0.102189 / lbs/day
Aug 2019 Week 3 0.22 / mg/L /
Aug 2019 Week 4 0.395 / mg/L 0.102189 / lbs/day
Aug 2019 Average 0.308 / mg/L 0.102189 / lbs/day
2019 Quarter 3 0.308 / mg/L 0.102189 / lbs/day
2019 2nd 6 Months(Avg) 0.308 / mg/L 0.102189 / lbs/day
2019 2nd 6...(Max) 0.395 / mg/L 0.102189 / lbs/day
2019 2nd 6...(Min) 0.22 / mg/L /
2019 2nd 6...(Count) 2 / 1 /
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outtalk 002
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
07/19/2019 S UTP2071919Self < 0.005 /20.7 mg/L < /
08/16/2019 S UTP2081619Self 0.088 /20.7 mg/L /
08/27/2019 P UTP20827I9POTW < 0.25 /20.7 mg/L < /
09/13/2019 S UTP2091319Self 0.39 /20.7 mg/L /
10/11/2019 S UTP2101119Self 0.014 /20.7 mg/L /
11/21/2019 S UTP2112119Self 1.18 /20.7 mg/L /
12/19/2019 S UTP2121919Self 6.76 /20.7 mg/L /
Jul 2019 Week 3 < 0.005 / mg/L < /
Aug 2019 Week 3 0.088 / mg/L /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 9 of 9

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outtalk 002
Sample Date SamplelD Result/Limit Mass/Limit
Acetone
Aug 2019 Week 4 < 0.25 / mg/L < /
Sep 2019 Week 2 0.39 / mg/L /
Oct 2019 Week 2 0.014 / mg/L /
Nov 2019 Week 3 1.18 / mg/L /
Dec 2019 Week 3 6.76 / mg/L /
Jul 2019 Average < 0.005 /8.2 mg/L < /
Aug 2019 Average < 0.169 /8.2 mg/L < /
Sep 2019 Average 0.39 /8.2 mg/L /
Oct 2019 Average 0.014 /8.2 mg/L /
Nov 2019 Average 1.18 /8.2 mg/L /
Dec 2019 Average 6.76 /8.2 mg/L /
2019 Quarter 3 < 0.183 / mg/L < /
2019 Quarter 4 2.651 / mg/L /
2019 2nd 6 Months(Avg) < 1.241 / mg/L < /
2019 2nd 6...(Max) 6.76 / mg/L /
2019 2nd 6...(Min) < 0.005 / mg/L < /
2019 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Chloroform
07/19/2019 S UTP2071919Se1f 0.009 / mg/L /
08/16/2019 S UTP2081619Se1f 0.021 / mg/L /
09/13/2019 S UTP2091319Se1f 0.009 / mg/L /
10/11/2019 S UTP2101119Se1f 0.01 / mg/L /
11/21/2019 S UTP2112119Self 0.528 / mg/L /
12/19/2019 S UTP2121919Self 0.991 / mg/L /
Jul 2019 Week 3 0.009 / mg/L /
Aug 2019 Week 3 0.021 / mg/L /
Sep 2019 Week 2 0.009 / mg/L /
Oct 2019 Week 2 0.01 / mg/L /
Nov 2019 Week 3 0.528 / mg/L /
Dec 2019 Week 3 0.991 / mg/L /
Jul 2019 Average 0.009 / mg/L /
Aug 2019 Average 0.021 / mg/L /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 1 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Chloroform
Sep 2019 Average 0.009 / mg/L /
Oct 2019 Average 0.01 / mg/L /
Nov 2019 Average 0.528 / mg/L /
Dec 2019 Average 0.991 / mg/L /
2019 Quarter 3 0.013 / mg/L /
2019 Quarter 4 0.51 / mg/L /
2019 2nd 6 Months(Avg) 0.261 / mg/L /
2019 2nd 6...(Max) 0.991 / mg/L /
2019 2nd 6...(Min) 0.009 / mg/L /
2019 2nd 6...(Count) 6 / /
Sample Date SamplelD Result/Limit Mass/Limit
Ethyl acetate
07/19/2019 S UTP2071919Self < 0.05 /20.7 mg/L < /
08/16/2019 S UTP2081619SeIf < 0.05 /20.7 mg/L < /
08/27/2019 P UTP2082719POTW < 0.003 /20.7 mg/L < /
09/13/2019 S UTP2091319Self < 0.05 /20.7 mg/L < /
10/11/2019 S UTP2101119Se1f < 0.05 /20.7 mg/L < /
11/21/2019 S UTP2112119Se1f < 0.25 /20.7 mg/L < /
12/19/2019 S UTP2121919Se1f < 0.05 /20.7 mg/L < /
Jul2019 Week 3 < 0.05 / mg/L < /
Aug 2019 Week 3 < 0.05 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Sep 2019 Week 2 < 0.05 / mg/L < /
Oct 2019 Week 2 < 0.05 / mg/L < /
Nov 2019 Week 3 < 0.25 / mg/L < /
Dec 2019 Week 3 < 0.05 / mg/L < /
Jul 2019 Average < 0.05 /8.2 mg/L < /
Aug 2019 Average < 0.026 /8.2 mg/L < /
Sep 2019 Average < 0.05 /8.2 mg/L < /
Oct 2019 Average < 0.05 /8.2 mg/L < /
Nov 2019 Average < 0.25 /8.2 mg/L < /
Dec 2019 Average < 0.05 /8.2 mg/L < /
2019Quarter 3 < 0.038 mg/L < /
/2019 Quarter 4 < 0.117 / mg/L g/-
< /
2019 2nd 6 Months(Avg) < 0.072 / mg/L < /
2019 2nd 6...(Max) < 0.25 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 7 / /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 2 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Count: 7 Months Sampled : 6 Weeks Sampled : 7 Quarters Sampled : 2
# % # % # % #
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
Isopropyl acetate
07/19/2019 S UTP2071919Se1f < 0.05 /20.7 mg/L < /
08/16/2019 S UTP2081619Se1f < 0.05 /20.7 mg/L < /
08/27/2019 P UTP2082719POTW < 0.003 /20.7 mg/L < /
09/13/2019 S UTP2091319Se1f < 0.05 /20.7 mg/L < /
10/11/2019 S UTP2101119Self < 0.05 /20.7 mg/L < /
11/21/2019 S UTP2112119Self < 0.25 /20.7 mg/L < /
12/19/2019 S UTP2121919Self < 0.05 /20.7 mg/L < /
Jul 2019 Week 3 < 0.05 / mg/L /
Aug 2019 Week 3 < 0.05 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Sep 2019 Week 2 < 0.05 / mg/L < /
Oct 2019 Week 2 < 0.05 / mg/L < /
Nov 2019 Week 3 < 0.25 / mg/L < /
Dec 2019 Week 3 < 0.05 / mg/L < /
Jul 2019 Average < 0.05 /8.2 mg/L < /
Aug 2019 Average < 0.026 /8.2 mg/L < /
Sep 2019 Average < 0.05 /8.2 mg/L < /
Oct 2019 Average < 0.05 /8.2 mg/L < /
Nov 2019 Average < 0.25 /8.2 mg/L < /
Dec 2019 Average < 0.05 /8.2 mg/L < /
2019 Quarter 3 < 0.038 / mg/L < /
2019 Quarter 4 < 0.117 / mg/L < /
2019 2nd 6 Months(Avg) < 0.072 / mg/L < /
2019 2nd 6...(Max) < 0.25 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled : 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 3 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
Methylene Chloride
07/19/2019 S UTP2071919Se1f < 0.003 /3 mg/L < /
08/16/2019 S UTP2081619Se1f < 0.003 /3 mg/L < /
08/27/2019 P UTP20827I9POTW < 0.003 /3 mg/L < /
09/13/2019 S UTP2091319Se1f < 0.001 /3 mg/L < /
10/11/2019 S UTP2101119Se1f < 0.001 /3 mg/L < /
11/21/2019 S UTP2112119Se1f < 0.005 /3 mg/L < /
12/19/2019 S UTP2121919Se1f < 0.001 /3 mg/L < /
Jul2019 Week 3 < 0.003 / mg/L < /
Aug 2019 Week 3 < 0.003 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Sep 2019 Week 2 < 0.001 / mg/L < /
Oct 2019 Week 2 < 0.001 / mg/L < /
Nov 2019 Week 3 < 0.005 / mg/L < /
Dec 2019 Week 3 < 0.001 / mg/L < /
Jul 2019 Average < 0.003 /0.7 mg/L < /
Aug 2019 Average < 0.003 /0.7 mg/L < /
Sep 2019 Average < 0.001 /0.7 mg/L < /
Oct 2019 Average < 0.001 /0.7 mg/L < /
Nov 2019 Average < 0.005 /0.7 mg/L < /
Dec 2019 Average < 0.001 /0.7 mg/L < /
2019 Quarter 3 < 0.002 / mg/L < /
2019 Quarter 4 < 0.002 / mg/L < /
2019 2nd 6 Months(Avg) < 0.002 / mg/L < /
2019 2nd 6...(Max) < 0.005 / mg/L < /
2019 2nd 6...(Min) < 0.001 / mg/L < /
2019 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled : 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
#Under Daily TRC: 0 0.00
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
07/19/2019 S UTP2071919Se1f < 0.025 /20.7 mg/L < /
08/16/2019 S UTP2081619Self < 0.025 /20.7 mg/L < /
08/27/2019 P UTP2082719POTW < 0.003 /20.7 mg/L < /
09/13/2019 S UTP2091319Se1f < 0.025 /20.7 mg/L < /
10/11/2019 S UTP2101119SeIf < 0.025 /20.7 mg/L < /
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 4 of 5

United Therapeutics Corporation
SAMPLE OVERVIEW
7/1/2019 To 12/31/2019 Sample Type: Effluent Wastewater Outfall: 002
Sample Date SamplelD Result/Limit Mass/Limit
n-Amyl acetate
11/21/2019 S UTP2112119SeIf < 0.125 /20.7 mg/L < /
12/19/2019 S UTP2121919Se1f < 0.025 /20.7 mg/L < /
Jul 2019 Week 3 < 0.025 / mg/L < /
Aug 2019 Week 3 < 0.025 / mg/L < /
Aug 2019 Week 4 < 0.003 / mg/L < /
Sep 2019 Week 2 < 0.025 / mg/L < /
Oct 2019 Week 2 < 0.025 / mg/L < /
Nov 2019 Week 3 < 0.125 / mg/L < /
Dec 2019 Week 3 < 0.025 / mg/L < /
Jul2019 Average < 0.025 /8.2 mg/L < /
Aug 2019 Average < 0.014 /8.2 mg/L < /
Sep 2019 Average < 0.025 /8.2 mg/L < /
Oct 2019 Average < 0.025 /8.2 mg/L < /
Nov 2019 Average < 0.125 /8.2 mg/L < /
Dec 2019 Average < 0.025 /8.2 mg/L < /
2019 Quarter 3 < 0.019 / mg/L < /
2019 Quarter 4 < 0.058 / mg/L < /
2019 2nd 6 Months(Avg) < 0.036 / mg/L < /
2019 2nd 6...(Max) < 0.125 / mg/L < /
2019 2nd 6...(Min) < 0.003 / mg/L < /
2019 2nd 6...(Count) 7 / /
Sample Count: 7 Months Sampled: 6 Weeks Sampled: 7 Quarters Sampled: 2
# % # % # % # %
#Over Daily C: 0 0.00 #Over Mo Avg C: 0 0.00 #Over Wk Avg C: 0 0.00 #Over Qt Avg C: 0 0.00
#Over Daily C TRC: 0 0.00 #Over Mo Avg C TRC: 0 0.00 #Over Wk Avg C TRC: 0 0.00 #Over Qt Avg C TRC: 0 0.00
#Over Daily M: 0 0.00 #Over Mo Avg M: 0 0.00 #Over Wk Avg M: 0 0.00 #Over Qtr Avg M: 0 0.00
#Over Daily M TRC: 0 0.00 #Over Mo Avg M TRC: 0 0.00 #Over Wk Avg M TRC: 0 0.00 #Over Qtr Avg M TRC: 0 0.00
#Under Daily: 0 0.00
1 #Under Daily TRC: 0 0.00
Thursday,February 27,2020 *Indicates Violation **Indicates TRC Violation Page 5 of 5
I