WQ0020239_Residual Annual Report 2019_20200302

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0020239
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Drew Matthews
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0020239
ApplicantTermittee * Town of Hertford
Facility Name * Hertford WWTP
Phone Number*
2528839301
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Hertford Annual Report.pdf 1.8MB
upload only 1 RDF document. NL@iple documents must be combined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 3/2/2020

TOWN OF HERTFORD
2019 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0020239
Submitted by:
Soil Plus
P.O. Box 1396
Oxford, North Carolina 27565
February 21, 2020
SOIL PLUS

SOIL PLUS
February 21, 2020
NCDEQ-DWR
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2019 LAND APPLICATION ANNUAL REPORT
Town of Hertford "Class B" Program
NC Permit No.: WQ0020239
Soil Plus Project No. 200802.A10
Non -Discharge Branch:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Town of Hertford on behalf of Atlantic
Sewage Control. Soil Plus compiled this report using data gathered during the compliance
year. This data includes (1) certification form, (2) residual sampling, (3) field loading
calculations, (4) pathogen and vector attraction reduction documentation, (5) standard soil
fertility nutrient analysis.
The Town of Hertford conducted application events on permitted fields in Perquimans
County during 2019. A total of 26.07 dry tons or 273,000 gallons of permitted residual
biosolids were land applied to permitted fields. Soil samples have not been collected from
the fields utilized for land application. The Town's land application contractor is in the
process of collecting them now and results will be submitted as soon as they are available.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the Town of Hertford (252-426-8182) for further assistance.
Respectfully,
Drew Matthews, Soil Plus
Charles Jones, Town of Hertford
J. Bryan Smith, Atlantic OBX
P.O. Box 1396
Oxford, NC 27565
[phone]
dmatthews @s oilplus. net
www.soilplus.net

Town of Hertford
2019 Annual Land
Application of
Residual Biosolids
Report
WQ0020239
Hertford, NC
ANNUAL LAND
APPLICATION
CERTIFICATION FORM
Source Loading Summary
Field Loading Summary
ANNUAL RESIDUAL
SAMPLING SUMMARY
FORM
Nutrient Analysis
503 Metal Analysis
TCLP
FIELD LOADING
SUMMARY FORMS
Nixon Farm
ANNUAL PATHOGEN &
VECTOR ATTRACTION
REDUCTION FORM
Fecal Coliform Results
30-Day Bench Scale Test
SOIL SAMPLES
Nixon Farm

Town of Hertford
2019 Class B Annual Report
WQ Permit# WQ0020239
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0020239 Town of Hertford JBS Contracting Perquimans [phone]
Year: 2019
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the ❑d
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 12
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 26.07
Total number of acres utilizes for land application during the year: 30.2
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality L 1 1 "1
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this.permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.1he facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated
facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
impomela
sonment for knowing violations."
Hays le
Pen_�/ ttee Name and Title (type or print):
ryt Signature of Permittee Date
Pivvulga i�L a /o?O7D �"= 2/21/2020
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

Source Summary Report
Town of Hertford WWTP 273,000 26.07
Total 273,000 26.07
Tuesday, January 14, 2020 Page 1 of 1

Site# 1
YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used At:)blied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
1 6
70,000
6.68
1554
Corn, Grain
140
11.1%
2 18.8
133,000
12.70
9.42
Corn, Grain
123
7.7%
3 5.4
70,000
6.68
17.27
Corn, Grain
147
11.7%
Total 273,000 26.07
Page 1 of 1

Town of Hertford
2019 Class B Annual Report
WQ Permit# WQ0020239
Residual Sampling Summary Form
Field Loading Calculations
2019 Analytical
2019 TCLP

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. W00020239 Facility Name Town of Hertford Source Permit No. NCO021849 Source Name Town of Hertford W WLP
Laboratory 1 Merltech, Inc.
Laboratory 2
Sample or ComposimDate 9/10/2019
Parameter (mg/Kg) Class A Class B
Aluminum
N/A N/A
9,900
Ammonia Nitrogen
N/A
N/A
437
Arsenic
41
75
2.18
Cadmium
39
85
1.32
Calcium
N/A
N/A
30,400
Copper
1,500
4,300
263
Lead
300
840
27.7
Magnesium's
N/A
N/A
2,250
Mercury
17
57
024
Molybdenum
N/A
75
1,38
Nickel
420
N/A,
N/A
N/A
N/A
420
N/A
N/A
N/A
N/A
10
437
2.2
5.80
22,700
Nitrate -Nitrite Niurgev
Percent Solids
pH (no units)
Phosphoms
Potassium
N/A
N/A
2,050
PAN (Ini./Inc.)
N/A
N/A
7,193
--
PAN (Surface)'.
N/A
t N/A
6,974
Selenium
100
100
2.18
Sodium.
N/A
N/A
6,900
SAR
N/A
N/A
1.55
TKN,
N/A
I N/A
L_—
21,500
Zinc
� 2,800
7,500
904
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that ied personnel properly gathered and evaluated the information submitted. I am aware that there arc significant penalties for
subm' t f se information, including the possibility of fines and imprisonment for knowing violations."
2. 1-1 Zo20
ature of Preparer • Date
*Pmoarer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

FIELD LOADING ESTIMATES
Facility Town of Hertford WWTP
Sampling Date 9/10/2019
% Solids 2.29
Mineralization Rate 0.30
Gallons per DT 10,471.97
pH 5.8
Sodium Absorpotion 1.55 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 21,500 lbs./1,000 gal 4.11
Ammonia Nitrogen (mg/Kg) 437.00 lbs./1,000 gal 0.08
Nitrate -Nitrite (mg/Kg) 437.00 lbs./1,000 gal 0.08
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 6,974 lbs./1,000 gal 1.33
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 7,193 lbs./1,000 gal 1.37
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.39
Phosphorus lbs./1,000 gal 4.34
Calcium lbs./1,000 gal 5.81
Calcium lbs./1,000 gal 0.43
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
2.18
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.32
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
263.00
Copper lbs./1,000 gal
0.05
Lead (mg/Kg)
27.70
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.24
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
10.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
2.18
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
904.00
Zinc lbs./1,000 gal
0.17
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
21,500
6,974
13.95
14,526
21,500
7,193 14.39
14,307
14,526
2,179
4.36
12,347
14,307
2,146 4.29
12,161
12,347
926
1.85
11,421
12,161
912 1.82
11,249
11,421
428
0.86
10,992
11,249
422 0.84
10,827
10,992
206
0.41
10,786
10,827
203 0.41
10,624
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 10,714 21.43
Total 10,876 21.75

Meritech, Inc.
Environmental Laboratory
Laboratory,
Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Date
Report Date:
Project:
Sample Rcvd:
9/23/2019
Hertford WWTP
9/10/2019
Meritech Work Order # 091019129
Sample:
HF091019 Grab
9/10/19
Parameters
Results
Analysis Date
Reporting Limit
Method
%Total Solids
2,29
%
9/11/19
0-100
%
SM 2540B
Ammonia, Nitrogen
<437
mg/kg
9/16/19
437
mg/kg
EPA 350.1
TKN
21,500
mg/kg
9/17/19
20
mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
<437
mg/kg
9/13/19
437
mg/kg
EPA 353.2
Aluminum, total
91900
mg/kg
9/12/19
2,50
mg/kg
EPA 2003
Arsenic, total
<2.18
mg/kg
9/12/19
2.18
mg/kg
EPA 2003
Cadmium, total
1.32
mg/kg
9/12/19
0.200
mg/kg
EPA 2003
Calcium, total
30,400
mg/kg
9/21/19
10.0
mg/kg
EPA 2003
Copper, total
263
mg/kg
9/12/19
1.00
mg/kg
EPA 200.7
Lead, total
27.7
mg/kg
9/12/19
1.13
mg/kg
EPA 200.7
Magnesium, total
2,250
mg/kg
9/12/19
10.0
mg/kg
EPA 200.7
Mercury, total
0.240
mg/kg
9/17/19
0,02
mg/kg
EPA 245A
Molybdenum, total
1.38
mg/kg
9/12/19
0.500
mg/kg
EPA 200.7
Nickel, total
10.0
mg/kg
9/12/19
2.00
mg/kg
EPA 2003
Phosphorus, total
22,700
mg/kg
9/21/19
2.00
mg/kg
EPA 2003
Potassium, total
21050
mg/kg
9/12/19
20.0
mg/kg
EPA 2003
Selenium, total
<2.18
mg/kg
9/12/19
2.18
mg/kg
EPA 2003
Sodium, total
6,900
mg/kg
9/21/19
20.0
mg/kg
EPA 2003
Zinc, total
904
mg/kg
9/21/19
0.500
mg/kg
EPA 200.7
pH
SA
S.U.
9/11/19
1.0 - 14.0
S.U.
SM 4500-HB
1 hereby certify that /have reviewed and approve these data.
Laboratory�sentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#:
lient: SOII PIUS Phone: [phone]
Address: PO Box 1396 Fax: [phone]
Oxford, NC 27565 Email: [e-mail]
Project: Hertford WWTP
P.O.#:
Attention: Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
Circle all that apply: Email (preferred), Fax, Mail std(Xdays) a -s Da s
MERITECH 1 INC..
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
e n Ve
VV v �� a VY.meritech-labs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): Joshua Simkins
Lab Use Only
Start
End
comp?
crab?
#of
Cont.
Test(s) Required
On Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
HF091019
9/10/19
W; V;Ja
G
3
Residual Analysis (Al, Ammonia-N, As, Cd, Ca, Cu, Pb,
o
Mg, Hg, Mb, Ni, Nitrate -Nitrite N, %TS, pH, P, K, Se,
Na, TKN, Zn)
-e
Temperature Upon
Receipt:
Method
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples must be done in the field prior to preservation. ***
AG
Of
Shipment:
Comments: Please report Residual Analysis results in mg/kg
Please email results to [e-mail]
Compositor#
Jug #
[
UPS
Fed Ex
Are these results for regulatory purposes? Yes
No
report results in: mg/L [ mg/kg I_
ug/L
Hand Delive ry
Relinquished by: - Lit/ Date: O/
Time: x�
x
Re eiv � /a e: Ti e: a�
3n
f—V..
Other
Reli Dater:
Time: p [c /
Recei d b .+ oatel. Time:
Relinquished Date:
Time:
Received by Lab:�D;tee f Time „.?

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 1
Report Date: 9/25/2019
Project: Hertford WWTP
Date Sample Rcvd: 9/10/2019
Meritech Work Order # 091019130 Sample: HF091019 Grab 9/10/2019
1311 - TCLP Metals
Parameter Results Analysis Date Det. Limit Reg. Limit Method
Arsenic
<0.100
mg/L
9/16/2019
0.100
5.0
EPA
200.7
Barium
0,061
mg/L
9/16/2019
0.050
100.0
EPA
200.7
Cadmium
<0.020
mg/L
9/16/2019
0.020
1.0
EPA
2003
Chromium
<0.050
mg/L
9/16/2019
0.050
5.0
EPA
2003
Lead
<0.100
mg/L
9/16/2019
0.100
5.0
EPA
2003
Mercury
<0.02
mg/L
9/17/2019
0.02
0.2
EPA
245.1
Selenium
<0.100
mg/L
9/16/2019
0.100
1.0
EPA
2003
Silver
<0.050
mg/L
9/16/2019
0.050
5.0
EPA
200.7
TCLP Organics
Parameter Results Analysis Date Reporting Limit Method
Volatiles 8260
Semi Vol. 8270
Attached
Attached
9/12/2019
9/19/2019
-
8260
8270
Other Tests
Parameter
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.58 %
9/11/2019
0-100
%
SM 2540B
Cyanide, total
<0.500 mg/kg
9/20/2019
0.500
mg/kg
EPA 335.4
Sulfide
<10 mg/kg
9/17/2019
10.0
mg/kg
SM4500SZD
Ignitability
>140 °F
9/17/2019
EPA 1030
Corrositivity (pH)
5.9 S.U.
9/11/2019
1.0 - 14.0
S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
h.
Page 2
Contact: Drew Matthews Report Date: 9/25/2019
Client: Soil Plus
P.O. Box 1396 Project: Hertford WWTP
Oxford, NC 27565 Date Sample Rcvd: 9/10/2019
Meritech Work Order # 091019130 Sample: HF091019 Grab 9/10/2019
1311 - I Lur Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Endrin
Attached - - -
Chlordane
Attached
Toxaphene
Attached
Methoxychlor
Attached
Heptachlor
Attached
Lindane
Attached
Herbicides - SW-846 8151A
Parameter
2,4-D
20415-TP [Silvex)
Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Attached
Attached
hereby certify that 1 have reviewed and approve these data.
L6Wal5KYRipresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
Environmental Laboratories
Laboratory Certificate #165
Client: Soil Plus
Project: Hertford WWTP
Client Sample ID: 1IF091019
Sample Collection: 09/10/19
Meritech Sample ID: 091019130
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 09/12/19
Extraction:
09/11/19
Analyst: VWV
Repot Date:
09/16/19
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
<0,0100
mg/L
0.0100
100
10
Chloroform
<0,0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
<0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
<0.100
mg/L
0,100
200
10
Tetrachloroethylene
< 0,0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0,50
10
Vinyl Chloride
<0,0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 09/19/19
Extraction:
09/11/19
Analyst: PM
Report Date:
09/23/19
Parameter
Result
Units
Det, Limit
Reg. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0,13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0,100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0,100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0,100
0.13
10
I hereby certify that I have
reviewed and
approve
these data.
4 _u
�., Ay
Laboratory
Representative
642 Tamco Road *Reidsville, NC 27320
[phone] *[e-mail]

�, ♦ . C : "kc
LAboRATORIES, INC.
• •l /process Consultaflons
Toxicity Characteristic Leachate Procedure (TCLP) Analysis for Meritech, Inc. collected 10 September 2019)
0910I9130
EPA FIW Quantitation Results Characteristic
Number Contaminant Limit(me/L) m /L Level(me/L) EPA Method Analyst
I. TCLP PESTICIDESMERBICIDES
D-020 Chlordane 0.003 BQL OA30 8081 MG
D-016 2,4-13 1,000 BQL 10.0 8151 MG
D-012 Endrin 0.002 BQL 0.020 8081 MG
D-031 Heptachlor 0,0008 BQL 0,008 8081 MG
D-013 Lindane 0,040 BQL 0.400 8081 MG
D-014 Methoxychlor 1,000 BQL 10,0 8081 MG
D-OIS Toxaphene OA5 BQL 0.500 8081 MG
D-017 2,4,5-TP(Silvex) 0.100 BQL 1,00 8151 MG
Sample Number
Sample Date
Sample Time (hrs)
Sample Matrix
Date Analyzed
71853-01
09/10/19
1030
Sludge
09/20/ l9
mg/kg =milligrams per kilogram =parts per million (ppm) aQL = nclmv Quantitation Limits

Chain of Custody Record (COC)
NPDES#:
Client: Soil Plus Phone: [phone]
Address: PO Box 1396 Fax: [phone]
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
Oxford, NC 27565 Email: [e-mail]
642 Tamco Rd. Phone: [phone]
Project: Hertford WWTP
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
P.O.#'
Turn Around Time*
Attention: *RUSH work needs prior approval.
How would you like your report sent?
Std(10 days) 3-S Da s Jd-aR Hm
Circle all that apply:LEmail (preferred), Fax, Mail x
Sampling Dates & Times
Person Taking sample(Sign/Print):
Joshua Simkins
Lab USE only
Sample Location and/or ID #
Start End
comp? #of Tests) Required
Grab? Cont.
°^lee? pH OK?
Yes / No ClOK?
Date
Time
Date
Time
HF091019
9/10/19
G
1
Full TCLP (Ignitability, Corrositivity, Reactivity) i
Temperature Upon
Method Of
** Dechlormation (<0.5 ppm) of Ammonia, Cyanide,
Receipt:
Phenol and TKN samples must be done in the field priorto preservation.
Compositor#
Shipment:
UPS
Fed Ex
HandDelivery
EJz Other
Comments: Please report TCLP results in mg/L
Please email results to [e-mail] Jug #
Are these results for regulatory purposes? Yes W: No Report results in: mg/L I mg/kg ug/L
Da Time: � , 7 Receiv d y: Date: Time:
Relinquished by: G ( \
j '� - -
Date: Time: Received by Date: Time:
puish o, 0 - to,( '1
no ishe Date: Time: Received by Lab.,t ��: ,�iat�: /r Timet:/t

Town of Hertford
2019 Class B Annual Report
WQ Permit# WQ0020239
Land Application Field Summary Forms

PermitNumber WQ0020239
Facility Name Town of Hertford
LandOwner Ed Nixon
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# 1 County Perquimans Crop 1 Corn, Grain
Field Name 1 SoilSeries Tomotley Crop 1 Pan 140
Acres Permited 6.00 Soil Abbrevation: To Crop 2
Crop 2 Pan
Volume Acres Dry
Date Measurement Applied % Solids Used DT/Ac. Tons
04/16/2019 Gallons 70,000 2.29 6.00 1.11 6.68
Source
Town of Hertford WWTP
Soil Application
Condition Precip Method
Dry 0 Surface
Total
P
50.58
Nitrate- Crop 1
Volatilization Mineralization TKN Ammonia Nitrite PAN
0.50 0.30 21,500 437.00 437.00 15.54
Crop 2
PAN Crop
Crop 1
Total Volume Applied 70,000
Total Dry Tons 6.68
Sum Total P
50.58
Total 15.54
Total
Reported in Gallons Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.005 0.003
0.586
0.062
0.001
0.003
0.022
0.005
2.014
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year 0.098 0.063
3.150 0.154
0.395
0.007
0.114
0.259
0.130
9.534
Cumulative Total 0.102 0.066
3.736
0.456
0.007
0.117
0.281
0.135
11.549
Permitted CPLR 36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
2/2 1 /2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

PermitNumber WQ0020239
Facility Name Town of Hertford
LandOwner Ed Nixon
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# 1 County Perquimans Crop 1 Corn, Grain
Field Name 2 SoilSeries Augusta-CP Crop 1 Pan 123
Acres Permited 18.80 Soil Abbrevation: At Crop 2
Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2
Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
04/17/2019 Gallons 133,000 2.29 18.80 0.68 12.70 Town of Hertford WWTP Dry 0 Surface 30.67 0.50 0.30 21,500 437.00 437.00 9.42 Crop 1
Total Volume Applied
133,000
Total Dry Tons 12.70
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Current Year
0.003
0.002
0.355
0.037
Prior Year
0.113
0.074
3.600 0.157
0.456
Cumulative Total
0.116
0.076
3.956
0.493
Permitted CPLR
36
34
1338
267
Mercury Molybdenum
0.000 0.002
0.007 0.145
0.007 0.147
15
Sum Total P 30.67
Nickel
Selenium
Zinc
0.014
0.003
1.221
0.293
0.138
10.349
0.307
0.141
11.571
374
89
2498
Total 9.42 Total
Crop 1 Crop 2
PAN PAN
Lime (T/Ac.) Date (1bs./Ac.) (lbs./Ac.)
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
2/21 /2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

PermitNumber WQ0020239
Facility Name Town of Hertford
LandOwner Ed Nixon
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# 1 County Perquimans Crop 1 Corn, Grain
Field Name 3 SoilSeries Altavista-CP Crop 1 Pan 147
Acres Permited 5.40 Soil Abbrevation: Aa.A Crop 2
Crop 2 Pan
Volume Acres Dry
Date Measurement Applied % Solids Used DT/Ac. Tons
04/18/2019 Gallons 70,000 2.29 5.40 1.24 6.68
Source
Town of Hertford WWTP
Soil Application
Condition Precip Method
Dry 0 Surface
Total
P
56.20
Nitrate- Crop 1
Volatilization Mineralization TKN Ammonia Nitrite PAN
0.50 0.30 21,500 437.00 437.00 17.27
Crop 2
PAN Crop
Crop 1
Total Volume Applied 70,000
Total Dry Tons 6.68
Sum Total P
56.20
Total 17.27
Total
Reported in Gallons Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.005 0.003
0.651
0.069
0.001
0.003
0.025
0.005
2.238
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year 0.075 0.066
1.673 0.062
0.224
0.003
0.088
0.142
0.103
5.248
Cumulative Total 0.080 0.069
2.324
0.293
0.003
0.092
0.167
0.108
7.486
Permitted CPLR 36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
2/2 1 /2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

Town of Hertford
2019 Class B Annual Report
WQ Permit# WQ0020239
Pathogen & Vector Attraction Reduction Form
Fecal Coliform Results
30-Day Bench Scale Test

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Hertford WQ Permit Number: WQ0020239
W WTP Name: Town of Hertford VAVTP NPEDS Number: NCO021849
Monitoring Period: 01/01/2019 to 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate 'Process to Further Reduce Pathogens":
"Class B" Alternative: Altemative 1
If applicable to alternative performed ("Class B" only) indicate 'Process to Further Reduce Pathogens":
Fecal Coliform Minimum Gen. Mean Maximum # of Exceedences
Colonies Per Gram of
Total Solids(Dry 361 426 804 0
Weight)
Technique SAI 9222 D
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 3 (30-day bench)
Not .Applicable
Not Applicable
Frequency Sample Type
Grab Samples
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
i� requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Charles A. Jones, ORC
J. Bryan Smith Operator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
JZ�A��A2/21/2020
ignamre of Prep rer* Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, January 14, 2020

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 1
Contact: Drew Matthews Report Date: 9/19/2019
Client: Soil Plus
P.O. Box 1396 Project: Hertford WWTP
Oxford, NC 27565 Date Sample Rcvd: 9/10/2019
Meritech Work Order # 091019121 Sample: HF091019 (001) Grab 9/10/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids
2.48 %
9/11/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
367 col/g dry wt
9/10/19 130 col/g dry wt
SM 9222D
Meritech Work Order #
091019122 Sample:
HF091019 (002) Grab
9/10/19
Parameters
Results
Analysis Date Reporting Limit
Method
%Total Solids
Fecal Coliform (Sludge)
2.25
404
%
col/g dry wt
9/11/19 0-100 %
9/10/19 130 col/g dry wt
SM 2540B
SM 9222D
Meritech Work Order #
091019123
Sample:
HF091019 (003) Grab
9/10/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids
Fecal Coliform (Sludge)
2.27
<400
%
col/g dry wt
9/11/19 0-Inn %
9/10/19 400 col/g dry wt
SM 2540B
SM 9222D
Meritech Work Order #
091019124
Sample:
HF091019 (004) Grab
9/10/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids
2.29 %
9/11/19 0-100 %
SM 254OB
Fecal Coliform (Sludge)
<397 col/g dry wt
9/10/19 397 col/g dry wt
SM 9222D
Meritech Work Order #
091019125 Sample:
HF091019 (005) Grab
9/10/19
Parameters
Results
Analysis Date Reporting Limit
Method
%Total Solids 2.52 % 9/11/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 361 col/g dry wt 9/10/19 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Contact: Drew Matthews
Report Date:
9/19/2019
Client: Soil Plus
P.O. Box 1396
Project:
Hertford WWTP
Oxford, NC 27565
Date Sample Rcvd:
9/10/2019
Meritech Work Order # 091019126 Sample:
HF091019 (006)
Grab
9/10/19
Parameters Results
Analysis Date
Reporting Limit
Method
% Total Solids 2,26 %
9/11/19
0-100 %
SM 2540B
Fecal Coliform (Sludge) 804 col/g dry wt
9/10/19
130 col/g dry wt
SM 9222D
Meritech Worlc Order #
091019127 Sample:
HF091019 (007) Grab
9/10/19
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
2,43 %
9/11/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
374 col/g dry wt
9/10/19 130 col/g dry wt
SM 9222D
I hereby certify that /have reviewed and approve these data. (�� A , lVC{lY�(��f(1
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#:
3-202013
Client: Still Plus
phone: [phone]
MERITECH INC.
PO Box 1396
1
Address:
Fax: [phone]
ENVIRONMENTAL LABORATORIES
Oxford, NC 27565
Email: [e-mail]
642 Tamco Rd, Phone: [phone]
Project: Hertford W WTP
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:
Turn around Time*
*RUSH work needs prior approval.
How would you like your report sent? '...
��/�/�/���
YY YY
VY.meritech-labs.com
Circle all that apply: Email (preferred), Fax,
Mail Std (i0 days) 3-5 oa S 74-QR Hrc
�
Person Taking Sample (Sign/Print):
Joshua Simkins
x
Lab Use Only
Sampling Dates &Times
p g
Sample Location
and/or ID #
Start I
End
Comp. ,
#of
Test(s) Required '
on Ice?
Yes / No
pH OK?
CI OK?
Date
Time
Date
Time
Grab?
Cont.
HF091019
(001)
09/10/2019
�.'�
G
1
Fecal Coliform / %Total Solids
HF091019
(002)
09/10/2019
10
A G
1
Fecal Coliform / % Total Solids
HF091019
(003)
09/10/2019
(0 I
G
1
Fecal Coliform / % Total Solids
j
HF091019
(004)
9/10/2019
tp 7
G
1
Fecal Coliform / % Total Solids
HF091019
(005)
9/10/2019
1�
G
1
Fecal Coliform /%Total Solids
HF091019
(006)
9/10/2019
)Q i5
G
1
Fecal Coliform / % Total Solids-
HF091019
(007)
9/10/2019
��,�
G
1
Fecal Coliform / % Total Solids
0
Temperature Upon
-
Receipt:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol
and TKN samples must be done in the field prior to preservation. ***
Method of
Comments:
Compositor #
Shipment:
Please email results to [e-mail]
Jug #
UPS
Fed Ex
Are these results for regulatory purposes?
Yes-
No eport results in:
mg/L [ mg/kg 15. ug/L E:J?
Relinquished by: _ D
Time:
��
i
��
R cei* b :
pDat : Time: "
I 3'
Hand Delivery
_.
- —
I�
R by: Dat
TGOther
Re y:
Date: I, Time:
Relinqui 'ed by: Date:
Time:
Received by Lab. „-
�D t , Time:A

Meritec Inc.
All .Environmental Laboratory
Laboratory Certification No. 165
Contact: Drew Matthews Report Date: 10/14/2019
Client: Soil Plus
P.O. Box 1396 Project: Hertford WWTP
Oxford, NC 27565 Date Sample Rcvd: 8/21/2019
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 091019128 Sample: HF091019 Grab 9/10/19
Total Solids Volatile Solids % Volatile Solids
Week 1 1.17 0.580 0.493
Weelc 2 1.08 0.540 0.502
Weelc 3 0.880 0.470 0.536
Week 4 1.11 0.570 0.511
Week 5 1.08 0.540 0.503
Mass Balance Equation = -2.08%Volatile Solids Reduction as per EPA Part 503 Biosolids Rule
1 hereby certify that I have reviewed and approve these data.
Laborres ative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

32z =s
Chain of Custody Record (COQ
NPDES#:
Soil Plus Phone:
Address: PO Box 1396 Fax: [phone]
252-883-9301
INC*Client:
MERITECH, N
ENVIRONMENTAL LABORATORIES
Oxford, NC 27565 Email: [e-mail]
642TamcoRd, Phone:[phone]
Project:
Hertford WWTP
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
P.O.#:
Attention:
How would you like your report sent?
Circle all that apply:1 Email (preferred), I Fax, Mail
Turn Around Time*
*RUSH work needs prior approval.
Std(10 days), 3-5 Da s 24-nR Hrc
x
Sampling Dates &Times
Person Taking Sample(Sign/Print): JOs11Ua. Sirnkins
Lab Use Only
Sample Location
and/or ID #
Start
End
Comp?
Grab?
#of
Cont.
Test(s) Required
on lee?
Ygs / No
pH OK?
Cl OK?
Date
Time
Date
Time
HF091019
9/10/19
G
1
cY
30 Day Bench Scale Test D
Temperature Upon
r Receipt:
Method of
Shipment:
** Dechlorination (c0.5 ppm) of Ammonia, Cyanide,
Comments*
Please email results to [e-mail]
Are these results for regulatory purposes? Yes
Relinquished by: Da
9
R m b Da -a
_
Relinq she by: Date:
Phenol and TKN samples must be done in the field prior to preservation.
WI No : � port results in: mg/t
Time: ��`i 1�' Rec 0d by: ✓�_
Time: ` Recei db
. (ci
Time: Received by Lab: s-'
**
Compositor #
Jug# r�
1 mg/kg ug/L
C— Date:
C ^� '� N7
Date: Time:
D!thf t;1 Time:
[} UPS
Q: Fed Ex
Hand Delivery
Other

Town of Hertford
2019 Class B Annual Report
WQ Permit# WQ0020239
Soil Samples