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Home My WebLink AboutWQ0000672_2019 Residual Annual Report_20200228Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application r Annual Report what is the submittal r Residual Annual Report type?* r Additional Information r Other Annual Report 2019 Year* Date Paper Copy 2/28/2020 Received:* Project Number* WQ0000672 Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ........................................................................................................................................................................................................................................................................................................................................................................... Name * Enviro-Choice Recycling, LLC Email Address* envirochoicenc@gmail.com Project Information ......................................................................................... Submittal Type* r New Permit Application r Renewal r Annual Report r Other Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted? r Yes r Nor N/A Permit Number* WQ0000672 Applicant\Permittee * City of Lumberton Facility Name * City of Lumberton Phone Number* 9107385311 r Modification (Major or Minor) r Additional Information r Residual Annual Report r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. City of Lumberton RLAP, Land applications of Class B Residuals, Robeson County Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) ECR City of Lumberton Annual Report 20.77MB Final_Signed.pdf upload only 1 RJF docurrent. WItiple docurrents must be corrbined into one R7F file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required, be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been received. The paper copy shall include the following: o Application Form o All relevant attachments {talcs, soils report, specs, etc.] o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) Mailine address: Division of Water Resources ! Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W - = Raleigh, NC 27699-1617 S12 N.5alisburySt. For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560. * rJ By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/27/2020 PO Box 390 Lumberton, NC 28359 Phone: (910) 738-5311 Fax: (866) 768-8016 February 26, 2020 N.C. Environmental Quality-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Compliance Representative Subject: 2019 Annual Report for City of Lumberton Land Application Program (City of Lumberton W00000672) Dear Compliance Representative: Enclosed is (1) copy of the monitoring and reporting information as required in the referenced permit for the City of Lumberton, North Carolina. This report was compiled from land application records provided by the City of Lumberton and Enviro-Choice Recycling. The report includes: 1) a State required annual certification form and facility information page, 2) the 2019 annual application summary table, 3) annual residual sampling summary form and laboratory analysis reports, 4) field loading reports, 5) individual field summary sheets, 6) pathogen and vector reduction documentation, and 7) soil analysis reports. Should you need more information regarding this land application program, please contact me at 910-738-5311. Eric T. Locklear Enviro-Choice Recycling ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: W00000672 County: F •I'rt Name (as shown on permit): Robeson Year: of Lumberton acr y Land Application Operator: Enviro-Choice Recycling, LLC Phone: _ Land application of residuals as allowed by the permit occurred during the past calendar year? ® Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. 2019 910-738-5311 Part A - Residuals A lication Summa : Total number of application fields in the permit: 43 19 Total number of fields utilized for land application during the year: Total amount of dry tons applied during the year for all application sites: 1391 Total number of acres utilizes for land application during the year: 379.1 Part B - Annual Comoiance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. ® Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .I I I 1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." � � � _ Date Permittee Na a and Title type or print) Sig re o e nr, Itt e Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W00000672 Laboratory: Facility Name: City of Lumberton Residual Source WQ # or NPDES #: WWTP Name: City of Lumberton 1) Pace Analytical 2) ENCO 3) 4) 5) Residual Analysis Dare Parameter (mg/kg) Cone. Limit m k ° Sam le or Composite Date 2!4/19 6/28/19 8/20/19 11/11/19 Percent Solids (%) NA 3.3 2.5 2 3.4 Arsenic 75 9.6 0.076 0.0871 0.19 Cadmium 85 0.96 0.0075 0.0083 0.0287 Copper Chromium 4,300 NA 269 201 5.88 0.045 2.19 0.053 18.7 0.058 Lead 840 19 0.526 0.0765 0.469 Mercury 57 0.53 0.0055 0.0059 0.0101 Molybdenum Nickel 75 420 7.6 29.2 0.136 0.684 0.0284 0.154 0.199 1 Selenium 100 9.6 0.062 0.062 0.155 Zinc 7,500 665 14.6 9.47 27.8 Total Phosphorus NA 18700 130 270 132 TKN NA 55000 61000 49000 16000 Ammonia -Nitrogen Nitrate and Nitrite NA NA 405 382 110 0.12 6.4 1 0.072 67 0.13 ' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the matvtauai permit mr nwwms 4 111 �. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties foMubmitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer 7 �4 Date 'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQ Permit Number: W00000672 W WTP Name: City of Lumberton NPDES Number: NCLO24571 Monitoring Period: From l/l/2019 To 12/31/2019 11 a s wrer n2T 11n61- Please indicate level achieved and alternative performed: Class A. Alt. A (umeItem) ❑ Alt B (Alk'freatmt ny❑ Alt. C (Prior Testin )❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Patho tm s ❑ If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens": Compost 131 Heat Drying ❑ Heat Treatment ❑ Thetmophilic [IBeta Ray El Gamma Ray ❑ Pasteurization ❑ Class B: JAII. 1 I ) Fecal Density 211 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogeny': Lime Stabilization ❑ Air Drying ❑ I Com oscine ❑ lAujobic Digestion Anaerobic Digestion ❑ If applicable to alternative pe med (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Ex°eer ° Frequency Sample TecAnalytical Parameter in Sludge lvlinimuGeo. MeanNaximunj Units of Analysis Type 2 x 10 to the MPN 6th power CFU 23100 52900 78100 cfu/gttun 0 Quarterly Grab 222D-MF FecalColifotm toiagranto 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MP N per 4 grams (in lieu of fecal total solid (dry colifotm weight) v acaur nuraca.m. a Guu....... .41t.1 (VS reduction) ❑ ,.-.c. ..-.. ......_ _ .- _-. Alt. 2 (40-day bench) ❑ - jAlt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying- Stable) [3 Alt. 8 (Drying- Unstable) ❑ Alt. 9 (injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ® "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." Cl "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision In accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are si ntfica enalties for false certification including fine and im isonment " g P DiPC �� Lei G Preparer Name and Title (type or print) Land ApplieL>a9e and Title (if apphcablextype or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 337.50 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Patrick Bullard Predominant Soil Series: Norfolk (NoA) Acres Used: 62.5 Acres Permitted: 62.5 Site #: NC-RO-39 Field #: 9 1 - D to (Hea Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Residual vy Sample or Ana ysts 1 a 21 3 -41 51 61 7 B 9 10 111 12 Com- posite Date 2/4/19 6/28/19 8/20/19 %Solids 3.3 2.5 2 Arsenic 9.6 0.076 0.0871 Cadmium 0.96 0.0075 0.0083 Copper 269 5.88 2.19 Chromium201 0.045 0.053 Lead 19 0.526 0.0765 Mercury 0.53 0.0055 0.0059 Mo1yb- denum 7.6 0.136 0.0284 Nickel 29.2 0.684 0.154 Selenium 9.6 0.062 0.062 Zinc 665 14.6 9.47 Total Phos- 18700 130 270 horus M t I F; Id Loa in s (Calculates inWsiacre) Annual Heavy e a to g 10 11 12 Total _jj 2 3 4 5 6 7 6_ 9 DT/.Ac./ n A pp `•' Event 5.40 ,Arsenic 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.000 0.000 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 Chromiu 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Lead 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 IVolyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 denum Nickel 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Selenium 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Zinc 0.000 0.000 0.102 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 Total Phos- 0.000 0.000 2.916 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.916 horus in accordance "1 certify, under penalty of law, that this document was prepared under my direction or supervision with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-39-9 Acres Utilized: 62.5 Land Owner: Patrick Bullard Annual Dry Tons Applied: 334.8093 Site #: Acres Permitted: 62.5 Operator: Patrick Bullard Crnn I Name: Coastal Bermuda Predominant Soil Series: Wagram (W8B) Cation Exchange Capacity (non 503): Croo 1 Max. PAN: 264 Crop 2 Name: Crop 2 Max. PAN: Y ;: o O Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons % Solids Volume Applied r PP per Acre (Dry TonsIAC) Residual Sources (NPDES N. WQ#. Fem. Animal Waste, etc) Soil Cond. D (Dry. Wet, Moist Precip. Past 24 Hrs. inches v 3 e s �. c, c ° o m r^o °o o A n g n y o N nVNg 48000 'z a 3 B. mglkg Nitrate yid Nitrite mglkg PAN Applied ( Ibslacre) Name of Crop Type Receiving Residual Application PP Crop I Crop 2 Crop 1 Crop 2 8/28/191 1 266,600 2.5 0.445 W00000672 Dry 0 S 0.5 0.3 6.4 0.072 12.808 12.808 8129/19 341,000 2.5 0.569 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072 16.383 16383 8130/19 310,000 2.5 0.517 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072 14.893 14.893 9/03/19 297,600 2.5 0.496 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072 1 14.298 14.298 9/9/19 291,400 2.5 0.486 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072 14.000 14.000 9/10/19 310,000 2.5 0.517 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072 14.893 14.893 9111/19 310,000 2.5 0.517 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072 14.893 14.893 9/12/19 297,600 2.5 0.496 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072L14-29814.2981989/13/19 266,600 2.5 0,445 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072089116/19 266,600 2.5 0.445 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0,0728089/17/19 254,200 2.5 0.424 W00000672 D 0 S 0.5 0.3 48000 6.4 0A722130.000 0 S 0.5 0.3 48000 6.4 0,07200Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): TOTALS' 03211600As Cd Cu Cr Pb H Mo Nt Se Zn P .295 Lime Applied Annual lbs/acre 0.001 0.000 0.024 0.001 0.001 1 0.000 0.000 0.002 0.001 0.102 2.916 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ac 0.001 0.000 0.024 0.001 0.001 0.000 0.000 0.002 0.001 0.102 Permitted C. P. L. R.**** Permit PAN Limit Istl2nd Crop 1 264 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." !'l *Application Method: S - Surface, IN - Injection, INC - Incorporation 6 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, annerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 42.18 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Lyndon Bullard Predominant Soil Series: Norfolk (NoA) Acres Used: 7.4 Acres Permitted: 7.4 Site #: NC-RO-39 Field #: 8 R 'd I Anal sis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): es I on Sample or Com- posite Date y 1 2/4/19 2 6/28/19 3 8/20/19 4 5 6 7 8 —91 11 12 % Solids 3.3 2.5 2 Arsenic 9.6 0.076 0.0871 Cadmiuml 0.96 0.0075 10.0083, Copper 1 269 5.88 2.19 Chromiunj 201 0.045 0.053 19 0.526 0.0765 0.53 0.0055 0.0059 7.6 0.136 0.0284 29.2 0.684 0.154 ENickel 9.6 0.062 0.062 665 14.6 9.47 18700 130 270 , v_,._.-, n,r,.«,.r c:,,�d „a.�:....� n .A �rn�aron in msiacrec � II I III III I III I III I III I III I III I III I III I I►I I III III � I III I III I III I III I III I III I III I III I III I III I III I III ►III ,.• I III I III I I I III I III I III III I III I III I III I III I III I I III I III III I III I III I III I III I III I III I III I III III III I II I III III I III I III I III I III I III I III I III III I III III � I III I III I III I III I III I III I III I III I III I III I III III I III • 1111 1 111 fill 1111 1 111 1 111 1 111 1111 1111 1111 1 111 111 1 1 1 - �� I III III I III I III I III I III I III I III I III ItoI jmIII I III I III III I III I III I III I III ItoI I III I III I III I III III ® I III I III I I: I III I III I III I III I III I III I III I III I III I I: I III I III � I III I III I III I III I III I III I III I III I III "I certify, under penalty of law, that this document was prepareu under u•y wrccuvu V. eupc• ,101o•9 ..• a.� ..-- with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: City of Lumberton Land Owner: Lyndon Bullard Operator: Patrick Bullard Crn" 1 Name- Coastal Bermuda PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0000672 Field #: NC-RO-3" Acres Utilized: 7.4 Annual Dry Tons Applied: 41.9835 Site #: Acres Permitted: 7_4 Predominant Soil Series: Norfolk (NoA) Cation Exchange Capacity (non 503): _ CroD 1 Max. PAN: 299 Crop 2 Name: Crop 2 Max. PAN: r Volume applied Volume Residual Sources Soil Cond. Precip• v 3 < o o 3 Y. > 3 Nitrate PAN Applied Name of Crop Type Receiving Residual ° s K enter one Solids! ( ) */* Applied r PP per NPDES #, W ( 0#• Pall 24 v = ,c TKN c and ( Ibs/ecre) d ° Liquid Solids Acre Ferl.. Animal Dry D ( D,, Hrs. �' 8 „ �. ry e w Nitrite Application PP Cu. Yds Gallons (Dry TonslAc) Waste, etc) Moist inches e ' `; ' 'o' mg(kg 48000 opg mg/kg Crop I Crop 2 Crop I Crop 2 821/19 241,800 2 2.725 W00000672 Dry 0 S 0.5 0.3 6.4 0.072 78.492 78.492 827/19 260,400 2 2.935 W00000672 Dry 0 S 0.5 0.3 48000 6.4 0.072 84.530 84.530 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF sopp to this form): T<rrAls o 5ozzoo As Cd Cu Cr Pb H MD Ni Se Zn P 163.021 163.021 Lime A lied Annual lbs/acre 0.001 0.000 0.025 0.001 0.001 0.000 0.000 0.002 0.001 1 0.I08 1 3.078 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac 0.001 0,000 0.025 0,001 0,001 0.000 0.000 0.002 0.001 0.108 Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 299 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure afar qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface-0.5, Injection/Incorporation- 1.0 Date "* Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.I,.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 22.57 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Lyndon Bullard Predominant Soil Series: Goldsboro (GoA) Acres Used: 3.7 Acres Permitted: 3.7 Site #: NC-RO-39 Field #: 7 e..d TM.1 Phncnhnrus nse maIk9. % Solids use Raw Percent #): Keslunal Hnii ly D4l YALY �alY«.� varwm ...... .- p aj 9 10 11 12 Sample or 1 2 3 4 5 Aj 7 Com- posite Date 2/4/19 6/28/19 8/20/19 %Solids 3.3 2.5 2 Arsenic 9.6 0.076 0.0871 Cadmium 0.96 0.0075 0083 0FO.O284 Copper 269 5.88 Chromiu 201 0.045 Lead 19 0.526 Mercury 0.53 0.0055 Molyb- 7.6 0.136 en in Nickel 29.2 0.684 0.154 Selenium 9.6 0.062 0.062 Zinc 665 14.6 1 9.47 Total Phos- 18700 130 270 horus Annual IIeavy 1 MMI r.c.0 10 11 12 Total 1 2 3 4 5 6 7 a 9 DT/AcJ c c App. " Event Arsenic 0.000 0.000 6.10 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.000 0.000 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 hromiu 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Lead 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 m Nickel 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Selenium 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Zinc 0.000 0.000 0.116 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.116 Total Phos- 0.000 0.000 3.294 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.294 horus a _ ... "I certify, under penalty of law, tnat this aocumenl was prcPa. .2 la_�7-bza Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPV OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX W HEN NOT APPLICABLE. Facility Name: City of Lumberton Land Owner: Lyndon Bullard Operator: Patrick Bullard Crop I Name: Coastal Bermuda WQ Permit #: W00000672 Field #: NC-RO-39-7 Acres Utilized: 3.7 Annual Dry Tans Applied: 22:7515 Site #: Acres Permitted: 3.7 Predominant Soil Series: Goldsboro (GoA) Crop I Max. PAN: 264 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Volume applied Volumne) Volume Residual Sources Soil preclp v e Z 3 Nitrate PAN Applied Name of Crop Type ° s (enter Solids/ / Applied per (NpDES a, WQ#� Corot Past 24 3 a �_ a 8 'rKN m a� (Ibs/acrel Receiving Residual e1 o Liquid Solids Acre Fert.. Animal (�' Hrs. $. �. `: m Nitrite Application Q Wet. e ' ' Cu Yds Gallons (Dry TowAe) Wes' etc) Moist) ind+ea ' > > m9A9 48000 m9's9 mgncg Crop I Crop 2 Crop I Crop 2 820/19 272,8W 2 6.149 W00000672 D7 0 S 0.5 0.3 6.4 0.072 177110 177.1 IC 0 000 0.000 0.000 0.000 0.000 0000 0.000 0.000 0 000 0.000 0.000 0 000 0.000 0.000 0.000 0.000 0.000 0 000 0 000 0.000 0.000 0000 0.000 0.000 0 000 0 000 0 000 0.000 O:OW 0000 0.000 0000 0000 Residuals Applications forms on FORM FSF sup (Busch FORM FSF supp 10 this form): As C'd I C'u Cr I Pb I JJR I Mo I Ni I Se I In I P ]it .IN 1771tp Lime Applied TOTALS 01 27zsu9 A inual lbs/acre 0.046 0.005 1 1313 0.942 0094 0.003 0.037 0.143 0.046 3.246 88.761 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulativclbs/ac U046 0005 1.313 0942 0094 0003. 0.037 1 0.I43 0096 3296 Permitted C. P. L. R.***s Permit PAN Limit Ist2nd Crop( "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." A � w *Application Method: S - Surface, IN - Injection, INC - Incorporation '-Volatilization Rate: Surface -0.5, Injection/incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost-0.1, anaerobially digested -0.2. aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 20.59 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Rhonda Chong Predominant Soil Series: Wagram (WaB) Acres Used: 2.9 Acres Permitted: 2.9 Site #: NC-RO-39 Field #: 6 rue...,.. Mnfale and Total Phosphorus use mg/kg. % Solids use Raw Percent #): Kesluui i tr Kluly ara vaaa k..,....T �••� �--- - __ _ ____ __ _ 10 11 12 Sample or 1 2 3 4 5j _6j Com- posite Date 2/4/19 6/28/19 8/20/19 %Solids 3.3 2.5 2 Arsenic 9.6 0.076 0.0871 Cadmium 0.96 0.0075 0.0083 Copper 269 5.88 2.19 Chromiun 201 0.045 0.053 Lead 19 0.526 0.0765 Mercury 0.53 0.0055 0.0059 Molyb- 7.6 0.136 0.0284 denum Nickel 29.2 0.684 0.154 Selenium 9.6 0. 662 6062 Zinc 665 14.6 9.47 Total Phos- 18700 130 270 horus Annual rleavv ivierar r.c.0 ...oau...go �.............._..... ---- - 9 10 11 t2 Total 1 2 3 4 5 6 7 8 0 DT/Ac./ m App Event Arsenic 0.000 0.000 7.10 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.OU1 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.000 0.000 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 Chromium 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Lead 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.000 0.000 0.000 0.0 00 0. 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 num ickel 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 enium 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 inc !horus 0.000 0.000 0.134 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.134 otal hos- 0.000 0.000 3.834 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.834 d' t' or so ervision in accordance "1 certify, under penalty of law, that this document was prepared under my Irec lop p with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton Land Owner: Rhonda Chong Operator: Patrick Bullard _ , .1_�.... r,....a.,l ne., ud- WQ Permit #: WQ0000672 Field #: NC-RO-39-6 Acres Utilized: 2.9 Annual Dry Tons Applied: 20.6832 Site #: Acres Permitted: 2.9 Predominant Soil Series: Wagram (WaB) Cation Exchange Capacity (non 503): r.�.,. I May_ PAN: 264 Crop 2 Name: Crop 2 Max. PAN: Volume applied Volume Residual Sources Soil Cond. Precip. ,o a < o ? 3 a TKN 'Z Y 2 B Nitrate and PAN Applied Name of Crop Type Receiving Residual o $ ❑ (enter one) Solids/ o h Applied per (NPDES #, WQN, (Dry. Past 24 �. =: a M Nitrite l Ibs/acre) Application A Liquid Solids Acre Fert., Animal Wet Cu. Yds Gallons (Dry TonslAc) Waste, etc) Moist inches ' * o mgikg mglkg mgikg Crop I Crop 2 Crop I Crop 2 6.4 0.072 205.425 205.425 8/31/19 198,400 2.5 7.132 WQOODD672 Dry 0 S 0.5 0.3 48000 0.000 0.000 0.000 0.000 0.000 0A00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 a.000 Residuals .Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0 198400 As Cd Cu I Cr I Pb I HP I Mo I Ni Se I Zn I P 1205.425 1305.425 Lime Applied TOTALS. Annual lbs/acre 0.001 0.000 0.031 0.001 0.001 0.000 0.000 0.002 0.001 0.134 3,934 0.134 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac 0.001 0.000 0.031 0.001 0,001 0.000 0.000 0.002 0.001 Permitted C. P. L. R.**'k Permit PAN Limit 1 st(2nd Crop 264 ......:. --A ..... a r6af "I certify, under penalty of law, that this document was prepared under my direction or supervision in accuruance WHEN a 3y�.V... UGG Arq ,....., ..---• - quali8ed personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 *s**C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): ': P'.17 Ash$ Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Lacy Cummings Owner: Fannie Oxendine Predominant Soil Series: Norfolk (NoA) Acres Used: 39.7 Acres Permitted: 39.7 Site #: NC-RO-21 Field #: 1 D t ITJ Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Residual vy Analysts a a 8 9 10 11 72 Sample or t 2 3 4 5 6 7 Com- posite Date 2/4/19 6/28/19 8/20/19 % Solids 3.3 2.5 2 Arsenic 9.6 0.076 0.0871 Cadmium 0.96 0.0075 0.0083 269 5.88 2.19 201 0.045 0.053 19 0.526 0.0765 0.53 0.0055 0.0059 r 7 6 0.136 0.0284 29.2 0.684 0.154 9.6 0.062 0.062 665 14.6 9.47 Tota Phos- 19700 130 270 horns ------- ne..M cMa r ...,d:..aa !!`9lr..lafrrl in the/acrel nnQuar "navy n "a. r.c.0 s t o 1 2 ' Total 1 2 3 a 5 s 7 s DT/Ac./ 0 a App y Event Arsenic 0.000 0.000 5.40 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.000 0.000 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 hromiu 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Lead 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Mercury 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 enu Nickel 0.000 0.000 2 0.000 0.000 0.000 0.000 0-0 0.000 0.000 0.000 0.000 0.002 Selenium 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Zinc 0.000 OA00 2 !2.916 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.102 Total Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.916 horus a:.e r: nrvicinn in aoenrdance "I certify, under penalty of taw, tnat mts nOCUmenl wan p.cpa.cu ..y with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 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N aum(oA palldda aumlop ad6y dw3 j amM MWN < Z P^S d :NVd -xeW Z dwJ :(C(S nou) ApasdeJ a3usg3x3 uo[leJ 8'£ :Pallluuad sa-lay 8'£ :Pazl1UI) saaaV :aweN Z doi3 L£Z :NVd'xvtV I doa0 epnuuag Ielseoi .amaN I oaJ (.('i) .jnggau l :saljaS Ilos )usulwopaad Pielln9 13148d mopuadO :# allS Z£89.OZ :pallddV suoy tia lsnnoVr buogJ epuogd :dauMO puerl S-6£-OH-JN :# Plald ZL90000aM :# Mw.sad jlAI uoLagwn Ido ( :a :ameN Cllyaed '3'I1[VJ17ddV ,LON N3HM XOR HO NXV'lg V NI ..V/N-. V 3JV7d NO 031'lddV O'131d HJtl3 NOd 03j-LIWfl11S ONV 03.L3'IdWOJ 38 O.L WHOS 3INV78 SIH.L d0 AdOJ V 371VW 35tl3'Id WHOA Ax'VWWaS (119H NOIJLV31'lddV alVz rlVfIN 1V ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): _-; '-7 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Quindale Bullard Predominant Soil Series: Lynchburg (Ly) Ac Acres Used: 14.8 res Permitted: 14.8 Site #: NC-RO-39-4 Field #: 4 'd 1 An I is Data (Hea Metals and Total Phosphorus use mg/ , % Solids use Raw Percent #): Rest ua vy Sample or a yst 21 3 a 5 6 7 Al9 10 11 12 Com- posite Date 2/4/19 6/28/19 8120/19 % Solids 3.3 2.5 2 Arsenic 9.6 0.076 0.0871 Cadmium 0.96 0.0075 0,0083 Copper 269 5.88 2.19 hromi 201 0.045 0.053 Lead 19 0.526 0.0765 Mercury 0.53 0.0055 0.0059 Molyb- d nu 7.6 0.136 0.0284 Nickel 29.2 0.694 0.154 Selenium 9.6 0.062 0.062 Zinc 665 14.6 9.47 Total Phos- 18700 130 270 horus it____. _x_,.J CC.Jd r ..n d:n c !( ..I.... 1••6ul u. the a9nuuul llGav) 1awY• c •..•u ..+v.....ob.. ,�- - --- - . 9 10 11 12 Total 1 2 _31 5 6 __ 7 8 DT/Ac./ o d App. Event 5.30 Arsenic 0.000 0.000 0.001 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.000 0.000 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 hromiu 0.000 0.000 0.001 0.000 0 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Lead 0.000 0.000 0.001 0.000 00 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Mercury 0.000 0.000 0.000 0.000 00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb 0.000 0.000 0.000 0.000 00 W00000" 0.000 0.000 0.000 0.000 0.000 0.000 0.000 en Nickel 0.000 0.000 0.002 0.000 00 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Selenium 0.000 0.000 0.001 0.000 00 0.000 0.0000.0000.0000. Zinc 0.000 0.000 0.100 0.000 00 0.000 0.000 0.000 0.000 0.000 0.000 0.100 Total Phos- 0.000 0.000 2.862 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 2.862 horus _ A A:�....f:...... n .J (.l..rA. rp "I certify, under penalty of law, that tnts document was preparcu uuuc.....y..••�. •..,•• ..• �"19. .•----------__ with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier �v Date DENR FORM MFLSF (12/2006) (90OZ/ZL) ASA Wa03 aN30 a)gH 0utpe0r11 luelnllod antielnwn� :'H"I'd'O.+r+ h'0- aBpnis mvj `£'0- paisa3tp Spuatgoaav `Z'0- PalsaStp Spv!gojasue `I'0- isodwo0 :salgH uoNgzgujaulW *** 0'1 not .puodjoaut/u0tl3aful VO - aaejjnS :alvpl uoNvzll!11310Aa uoyvjodjoaul - ONI `uogaalul - NI aagpuS - S :P041aW uolleatlddVs M0 iatlddy pue-I jo wrguu5!S su0t)ej01A %UltA0U3j joj /uawuosudtut pug sauy jo tltitglssod ayl Sutpnlaut `uol)vwjojul asluj Stu itugns joj sallleuad luu3tjtu8ts aic ajay) ley; xtumv wv 1 pa"!tugns goUewjoju! ayi palenlena Pug paja4)e1 Cuadojd Iauuosjad pa3!lenb ajnsse of pauSlsap wa)s.(s a yltAt 33UUPJ0339 ul uolswadns jo uopaamp au japan paiodajd sum )uawnaop styi ley) `Mel jo ,i)louad japan AjIlia31„ dolD POZAS I l!w!l NVd I!uuad LfZ •»ra'H I'd'D P217luu2d 001'0 100.0 Z00-0 000.0 0000 100-0 100-o fmo 000'0 100'0 oe/sglanllelnwnOlualinO oe/sgl antielnuwO smA joud Z98'Z OOl'0 1000 Z00'0 000'0 000'0 100'0 100-0 U0'0 000'0 100'0 ajag/sql ivnuuy .iv ap alt>(l hay t V DMI'l 06'C51 996'£SI d uZ a5 !N oW 1-I 9d 1 3 11J pJ Sy S'IV101 :(iujoj slgl of ddns dStl WHOA 438)ly) ddns ASd 14ZlOd uu slelol suo!te ll"N s!vup!saa 000-0 000'0 000'0 000'o 000 0 000-0 77 (o0ro 0o00 000'0 000'0 0!w'o 000'0 000'o ono'o 000'0 0000 000'0 000'0 000'0 000'0 000'0 000'0 000'0 000'0 000 0 000'0 o00'n ILZ'fb ILZ'fb ZL0*0 4'9 0008v £'0 5'0 S 0 tiO ZL9000OOM ZOS'l Z 009`99Z 61/bl/8 ZZ£'IS ZZE'15 ZL00 h'9 0008v f'O 9'0 S 0 tiO ZL900000AN ZSL'I Z OOZ`9I£ 61/fl/8 ZLf'65 ZL£'6S ZLO'O 4'9 000817 BwBW E'O 5'0 S 0 tiO ZL900006M 190'Z Z 008`99E 61/01/8 o + = c o sa4au! sil{ ls!ow 7aM (a)a `QMA% Ivw:uy'.ilad Owsuol ka) way sP!I0S so01180 SPA'nJ P!nbrl o Z dwJ 1 dw:) ! do 6y!Bw BVBW u0!le3!Iddy al!A!N Ew(wae/Sgt de Z led #0M '# S3OdN) jad pa!!ddy % lsp!IoS (avo jalva) !enpa8u!n!aal g patlddtl NVdag P E dawd amoS !unp!sad awntoA palldde awnloA odAl dwOjo awey N > .. _ --__.---__'-'___ ._........ a...-. :NVd -xeW Z doj0 :aweNZdoAj LEZ :NVd-xwW 1u—J (COS uou) filaedeD a8uaya:3 vope0 '1 lugyou -1 :SauaS 1!oS luvululopajd 8'bl :PaN!uuad 9313V :# al!S Zf 1 I'6L'Pallddy Buoy Cjp pmmV S'bI :pazllU(1 sajaV p-6£-OU-3N :# Pla!A ZL900000M :# llwjad OM upuuuag is;s.03 s...nry i ......J piFlingN31.led uolvjadO pjellnEl alepu!110 nawuO pue'l uoljagwng jo fp:) :awgN M!1!3e9 '3'iHVOI7ddV ION NHHM XOR HO XNV'ifl V NI ,V/N,, V 33V'ld NO U31lddV (1731A HOV3 HOA Q3 L.LIWHIIS ONV a3.13'IdWOO 38 O.L WHOA )INV'19 SIHj. d0 AdOJ V 3)IV W 3SV3 Id WHOA AUVWWaS Q'I3L3 NOLLVJI IddV QNV'I'IVf NNV ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): e Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Quindale Bullard Predominant Soil Series: Rains (Ra) Acres Used: 5.1 Acres Permitted: 5.1 Site #: NC-RO-39 Field #: 3 ...A TM.1 Dhnen6nrns nae mQ/kp. % Solids use Raw Percent #): Kesluual Anal ass "Aw -r ,. a.. .-- — - ---a---- _- - o B 9 10 11 '12_ Sample or t 2 3 < 5 6 7 Com- posite Date 2/4/19 6/28/19 9/20/19 % Solids 3.3 2.5 2 Arsenic 9.6 0.076 0.0871 Cadmium 0.96 0.0075 0.0083 Copper 269 5.88 2.19 Chromiurr 201 0.045 0.053 Lead 19 0.526 10.0765 Mercury 0.53 0.0055 0.0059 Molyb- 7.6 0.136 0.0284 um Nickel 29.2 0.684 0.154 Selenium 9.6 0.062 0.062 Zinc 665 14.6 9.47 Total Phos- 18700 130 270 horns none� 11 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1111 1 111 1 111 1 111 1 111 1 111 1 11 '�.' 1 111 1 111 1 1 1 1 111 1 111 1 111 1 111 1 111 fill 1 111 1 11 1 111 1 1 1 ri . l 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 am 1 Ill 1 Itt 1 It 1 111 1 III 1 111 too 1 111 fill 1 111 1 111 1 111 I t 1 11 1111 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 t i l l 1 111 1 111 •' 1lll till 1lll 1lll fill fill fill 1111 till 1lll 1111 fill = fill 1111 111 1111 1111 fill 111 fill JIM 1111 fill fill 111 �: 1 III 1 ill 1 11 1 111 I oil EM 1 111 1 111 I 111 1 ill 1 ill 1 11 1 11 ® fill 1111 11: 1111 Ili fill 1111 1III 1111 1111 1III 1111 11: 1111 1111 ® 1111 1 11 1 111 1111 1 III 1111 1111 1 lit 1111 . .. "I certify, under pens ty o law, that tnls aocumenr r�ea p� epb. r with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-39-3 Acres Utilized: 5.1 Land Owner: Quindale Bullard Annual Dry Tons Applied: 22.7515 Site #: Acres Permitted: 5_I Operator: Patrick Bullard Cre I Numn• t'naetnl Rermuda Predominant Soil Series: Rains (Ra) Cation Exchange Capacity (non 503): Cron I Max. PAN: 194 Crop 2 Name: Crop 2 Max. PAN: Volume applied Volume Residual Sources SOil Precip. ,a o 0 3 Z 3 Nitrate PAN Applied Name of Crop Type ° Y o e (enter one) Solids/ % Applied per (NPDES #, WQ#. Cond. (Dry, Past 24 'a v " _• e^e ^ �. TKN c o o and (Ibs/acre ) Receiving Residual Application 0 Liquid Solids Acre Fen.. Animal Hrs. $ o, � �' ^ : io Nitrite Crop I Crop 2 Crop 1 Crop 2 Cu. Yds Gallons (DryTOnSIAC) Waste, etc) Wet, Moist "�� o 0 � 6. nvlkg 48000 mg/kg mp/kg 9/14/19 272,800 2 4.461 W00000672 Dry 0 S 0.5 0.3 6.4 0.072 128.491 128.491 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF sup ( attach FORM FSF supp to this form): Tornts 01 272800 As Cd Cu I Cr Pb Hg JMolNil SelZnl P Iz8.491 12a.491 Lime Applied Annual lbs/acre 0.001 0.000 0.020 0.000 0.001 0.000 0.000 0.001 0.001 1 0.085 1 2.430 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac 0.001 0.000 0,020 0.000 0.001 0.000 0.000 0.001 0.001 0.085 Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop I F194 "I certify, under penalty of law, that this document was prepared under my direction or supen ision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation j� e�,� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 16.64 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Bullard Lindbergh Predominant Soil Series: Goldsboro (GoA) Acres Used: 2.6 Acres Permitted: 2.6 Site #: NC-RO-39 Field #: 1B D—:B...,1 Anoh,c:c na*a i pavv Metals and Total Phosphorus use m2lkl=_, % Solids use Raw Percent #): Ell INNININ QA et in 11 ® 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 11 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 ,.. 1 1 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 11 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 11 1 111 111 1 111 1 111 1 111 1 111 1 111 1 11 1 1 1 1 111 1 111 1 111 1 111 ' 1 111 1 I l t 1 111 1 111 1 111 1 111 1 1 1 1 111 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 ® 1 11 1 111 1 11 1 111 1 111 1 111 1 111 1 111 111 1 111 1 111 1 111 1 11 ® 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ® 1 111 1 111 1 111 1 111 1 111 1 111 f 111 1 111 I llt R "1 certify, under penalty o aw, t at t is ocumen was preps e u with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-39-1 B Acres Utilized: 2.6 Land Owner: Bullard Lindbergh Annual Dry Tons Applied: 16.5466 Site #: Acres Permitted: 2_6 Operator: Patrick Bullard Predominant Soil Series: Goldsboro (GoA) Cation Exchange Capacity (non 503): _ Cro I Name- Coastal Bermuda Crop I Max. PAN: 299 Crop 2 Name: Crop 2 Max. PAN: P me applied Volume Residual Sources Soil Cond. PreciP. v o < c 3 > > Y Y -q 3 Nitrate PAN Applied Name of Crop Type Receiving Residual r one) Solids/ o A Applied per (NPDES #, WQ#,D ( Past 24 '� m w rt _n F TKN o 3 and A lication Solids Acre FerL. Animal ry• Nitrite pPLiquid Crop I Crop 2 Crop 1 Crop 2 Waste, etc) WetRrs.ds n o mglkg mglkg mglkg Gallons (Dry Tons/Ac) Moist Inches 48000 198,400 2 6.364 W00000672 Dry 0 S 0.5 0.3 6.4 0.072 183.302 183.302 0.000 0.000 0.0000.000 0.000 0.000 0.000 0.000 0.0000.000 0.000 0.000 lAnnual 0.000 0.000 0.000 0.000 0000 0.0000,000 0.000 0.0000.000 0.000 0.000 0.000 0000 0000 000 0.000 U.000 0.00il.000 Residuals A plications totals on FORM FSF' soup ( attach FORM FSF soon to this form):0 I9s400 As Cd Cu Cr Pb H MO Ni Se Zn P I83.302 183.3U2 Lime A lied re 0.001 0.000 0.028 0.001 0.001 1 0.000 1 0.000 0.002 0.001 0.121 3.456 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ac 0.001 0.000 0.028 0.001 0.001 0,000 0.000 0.002 (001 0.121 Permitted C. P. L. R.**** Permit PAN Limit i stl2nd Crop 299 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance wain a G o� ... qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 231.85 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Patrick Bullard Owner: Bullard Lindbergh Predominant Soil Series: Goldsboro (GoA) Acres Used: 39.7 Acres Permitted: 5.3 Site #: NC-RO-39-IA Field #: IA _ _.---:- .v_._ .,, , X4.+ot... A Tnrat Phncnhnrus use mg/kg. % Solids use Raw Percent #): tcestuuat nunry 1 n va.a �....o, 2 j .........., 3 -..- ----- 5 ----.---- 6 --- 7 - ... 8 9 102/4/19 LSample 6/28/19 8/20/19 3.3 2.5 2 9.6 0.076 0.0871 Cadmium 0.96 0.0075 0.0083 Copper 269 5.88 2.19 Chrommu 201 0.045 0.053 Lead 19 0.526 0.0765 Mercury 0.53 0.0055 0.0059 Molyb- deman 7.6 0.136 0.0284 Nickel 29.2 0.684 0.154 Selenium 9.6 0.062 0.062 Zinc 665 14.6 9.47 Total Phos- 18700 130 270 horus Annual neavy i..nrnN ..V.... o .sue 1- - - 9 10 11 12 3 4 5 6 7 6 � � 0 m r r 0.000 0.000 ?.84 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 LDA 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 0.000 0.000 0.001 0.000 0.000 0.000 0.0000.0000.000 0.000 0.000 0.000 0.001 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 d num Nickel 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.000 0.000 0.002 Selenium 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.000 0.000 0.001 Zinc 0.000 0.000 0.111 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.111 Total Phos- U.000 0.000 3.154 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.154 horus ---A . -i-,,,,, aivn„tinn nr c,,,,prvsinn in accordance "1 certify, under penalty of taw, mat mts (Jucumcu...nM PI. V".v.. - - •w -------- - with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". a-a;7aZ) Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: City of Lumberton Land Owner: Bullard Lindbergh Operator: Patrick Bullard Crop 1 Name: Coastal Bermuda PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0000672 Field #: NC-RO-39-1A Acres Utilized: 5.3 Annual Dry Tons Applied: 31.0249 Site #: Acres Permitted: 5_3 Predominant Soil Series: Goldsboro (GoA) Cation Exchange Capacity (non 503): _ Crop 1 Max. PAN: 299 Crop 2 Name: Crop 2 Max. PAN: m a A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/AC) Residual Sources (NPDES #, W Q#• Fert., Animal Waste, etc) Soil Cow' tDry' Wet. Moist PrcciP. Past 24 Hrs. inches ,o a * m g _ .0 < R. �_ ¢ f0 ! .. o o 0 3 rD `D m ' o 7 hN mg/kg 48000 Z > 3 o 3 w o rn o d mg/kg Nitrate and Nitrite m9/k9 PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application P Crop I Crop 2 Crop 1 Crop 2 8/9/2019 297,600 2.5 5.854 W00000672 Dry 0 S 0.5 0.3 6.4 0.072 169.603 168.603 0.000 0.000 0.000 0.000 0.000 0.000 00 0.000 0.000 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF su p ( attach FORM FSF supp to this form): TOTALS: 0 2976u0 As Cd Cu Cr Pb H MO Ni Se Zn P 168.603 168.603 Lime A lied Annual lbs/acre 0.001 0.000 0.026 0.001 0,001 0.000 0.000 0.002 0.001 0.111 3.154 Date Ibs/ac Prior Years Cumulative Ibsiac Current Cumulative lbs/ac 0.001 0.000 0.026 0.001 0.001 0.000 0000 0.002 0.001 0.111 Permitted C. P. L. R.***r Permit PAN Limit Ist/2nd Crop 299 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." n *Application Method: S -Surface, IN -Injection, INC -Incorporation **Volatilization Rate: Surface -0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Lacy Cummings Owner: Fannie Oxendine Predominant Soil Series: Goldsboro (GoA) Acres Used: 52.1 Acres Permitted: 52.1 Site #: NC-RO-21 Field #: 5 ., __u.__• A _ 1-. : nntu ruaa.n Mctale and Total Phnsnhorus use me/ke. % Solids use Raw Percent #): NONE • v..... WA .Zi ITMA i roM.nna it 'aiouiivreO in mciacrei Annua• "Wavy 8. 5 10� 11 12 Total � 3 4 5 8 7 DT/Ac./ r11.38 0 App. Event Arsenic 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.740 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.740 hromiu 0.553 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.553 Lead 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 n m Nickel 1 0.080 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.080 Selenium 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Zinc 1.830 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.830 Total Phos- 51.462 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 51.462 horus _a__ d: _....ai...... nn in arrn Ydaare "I certify, under penalty of taw, mar mis oucument wab Piepa.ca uuu..a ...y with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-21-5 Acres Utilized: 52.1 Land Owner: Fannie Oxendine Annual Dry Tons Applied: 71.6673 Site #: Acres Permitted: 52.1 Operator: Lacy Cummings Cr o i Name: Com Predominant Soil Series: Goldsboro (GoA) Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 148 Crop 2 Name: Crop 2 Max. PAN: ° ° g ° P Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons % Solids Volume PP per Applied r Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert.. Animal Waste, etc) Soil COS' (� Wet, Moist Precip. Pas124 Hts. Inches aD 3'� s 06 m. ' < o m a^ - ' o 0 g vp n e ° TKN mgtkg 55000 z > 4 3 o 3 m 2 o 0; mgtkg Nitrate and Nitrite mgtkg PAN Applied 1 Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 4/4119 31,000 3.3 0.082 W00000672 0 S 0.5 0.3 405 382 2.778 2,778 4/11/19 31,000 3.3 0.082 W00000672 0 S 0.5 0.3 1 55000 405 382 2.778 2.778 4/12/19 31.000 3.3 0.082 W00000672 0 S 0.5 0.3 1 55000 405 382 2.778 2.778 4-15-19 6,200 3.3 0.016 W00000672 0 S 0.5 1 0.3 55000 405 382 0.556 0.556 4/16119 37,200 3.3 0.098 W00000672 0 S 0.5 0.3 55000 405 382 3.333 3.333 4/17/19 24,800 3.3 0.066 WQOD00672 0 S 0.5 0.3 55000 405 382 2.222 2.222 4/18119 31000 3.3 0.082 W00000672 0 S 0.5 0.3 55000 405 382 2.778 2.778 422/19 68,200 3.3 0.180 W00000672 0 S 0.5 0.3 55000 405 382 6.111 6.111 4/23/19 49,600 3.3 0.131 W00000672 0 S 0.5 0.3 55000 405 382 4.445 4.445 4125/19 55,800 3.3 0.147 W00000672 0 S 0.5 0.3 55000 405 382 5.000 5.000 4/29/191 4130/19 1 80,600 74,400 3.3 3.3 0.213 0.197 W00000672 W00000672 0 U S S 0.5 0.5 0.3 0.3 55000 55000 405 405 382 382 7.222 6.667 7.222 6.667 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TALS 0 Szosoo Annual lbs/acre As 0.026 Cd O.D03 Cu 0.740 Cr 0.553 Pb 0.052 H 0.001 Mo 1 0.021 Ni 1 0.080 Se 1 U.026 Zn 1.830 P a6.G68-t6.66R 51.462 Lime Date Applied Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ae 0.026 0.003 0.740 U.553 0.052 0.001 0.021 U.080 0.026 1.830 Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop 148 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, injection/incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 162.03 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Lacy Cummings Owner: Fannie Oxendine Predominant Soil Series: Goldsboro (GoA) Acres Used: 45.9 Acres Permitted: 45.9 Site #: NC-RO-21 Field #: 2A __.-...:� n_#_ iuo.,.,., Marole and Tatal Phnsnharus use m9/k9. % Solids use Raw Percent #): C� i •. i it �� ® 1 11 1 11 1 111 1 111 1 111 1 111 1 1 1 1 I l l i 111 1 111 1 111 1 111 1 11 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 •• i i, file 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 1� 1111 1 111 1111 1111 1 lit 1 tit tilt 1 111 1 111 I I 1 1 Ill 1 ill 1111 1111 111� 1111 1111 1111 1111 1111 1111 1 lit 1111 1111 1 fll 111 1 tit tilt life 1111 1 111 1 tit 1111 1 1 1 1111 1 1 1 1111 1 tit 1111 l ill 111 1111 fill t 111 1 111 1 ill 1111 1111 1111 1111 1 111 111 ® t 111 lit 1111 111 1 111 1 111 1111 1 111 11 1 1 iii 1111 1 iii 111 1 111 1 Iil 1 11 1 111 lilt 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ® 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 ill 1 111 1 ill 1 111 1 ill 1 1 1 ill ® 1111 1 ill 1 111 1111 1111 1111 1111 1111 1 iii 1111 1 ,� nswww�w�s�w*le1T�lR#'fP!'17,f�'fLT�s! "I certify, under penalty of taw, Ina Inis aocum cut was prcpa, cu uuum ...� , -• • • •• --- ----- ----- - with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-21-2A Acres Utilized: 45.9 Land Owner: Fannie Oxendine Annual Dry Tons Applied: 162.1046 Site #: Acres Permitted: 45.9 Operator: Lacy Cummings ('enn 1 Namc• Cnm Predominant Soil Series: Norfolk (NoA) Cation Exchange Capacity (non 503): CroD 1 Max. PAN: 131 Crop 2 Name: Crop 2 Max. PAN: s .8 o 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAC) Residual Sources (NPDES C WOO. Fen.. Animal Waste, etc) Soil Cond. wry' Wet, Moist Precip• Past 24 Ho. inches ,a 2 v 0 = c o m m_ : ' c o 0 3 : a o' TKN rrog 55000 3 w° c g '-� mg/4 Nitrate and Nitrite �9 PAN Applied (Ibstacre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 511/19 74,400 3.3 0.223 W00000672 0 S 0.5 0.3 405 382 7.567 7.567 5/2119 105,400 3.3 0,316 W00000672 0 S 0.5 0.3 55000 405 382 10.720 10.720 513/19 55,800 3.3 0.167 W00000672 0 S 0.5 0.3 55000 405 1 382 5.676 5.676 5/4/19 43,400 3.3 O.I30 W00000672 S 0.5 0.3 55000 405 382 4.414 4.414 5/7/19 80,600 3.3 0.242 W00000672 S 0.5 0.3 55000 405 382 8.198 8.198 5/8119 80,600 3.3 0-242 W00000672 S 0.5 0.3 55000 405 382 8.198 8.198 5/9119 80,600 3.3 0.242 W00000672 RO S 0.5 0.3 55000 405 382 8.198 8.198 5/10/19 80,600 3.3 0.242 W00000672 S 0.5 0.3 55000 405 382 8.198 8.198 5/14/19 167,400 3.3 0.502 W00000672 S 0.5 0.3 55000 405 382 17.027 17.027 5/15/19 148,800 3.3 0,446 W00000672 S 0.3 0.3 55000 405 382 I5.135 15.135 5/16/19 148,800 3.3 0.446 W00000672 S 0.5 0.3 55000 405 382 15.135 1 15.135 5/17/19 111,600 3.3 0.335 W00000672 0 S 0.5 0.3 55000 405 382 11.351 11.351 Residuals Applications totals on FORM FSF supp ( attach FORM FSF so pp to this form): TOTALS, 0 117800a Annual lbs/acre AS 0.001 Cd 0.000 Cu 0.042 Cr 0.000 Pb 0.004 H 0.000 Mo 0.001 Ni 0.005 Se 0.000 Zn 0.103 P n9.xu n9s16 0.918 LimeA lied Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative Ibs/ac 0.001 0.000 0.042 0.000 0.004 0.000 0.001 0.005 0.000 0.103 Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 131 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation ,-�21117 -.2Z **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *`* Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 140.14 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: Lacy Cummings Owner: Fannie Oxendine Predominant Soil Series: Norfolk (NoA) Acres Used: 39.7 Acres Permitted: 39.7 Site #: NC-RO-21 Field #: 1 n...., Mon.,., N[nralc and Tatal Phnsnhorus use me/ke. % Solids use Raw Percent #): mom Annual neavy irrcrm .__ __ --- - 10 11 12 1 2 3 4 6 6 7 8 9 / 0 w c 0.000 3.53 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 m 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 kDA r 0.000 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Nickel 0.000 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 Zinc 0.000 0.103 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.103 Total Phos- 0.000 0.918 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.918 horu5 _ a: .•:...... cinn in neenrdanee "I certify, under penalty or law, that this document was prepared nnde....y ,..,• • • -- --- -___- _____ _ with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-21-1 Acres Utilized: 39.7 Land Owner: Fannie Oxendine Annual Dry Tons Applied: 89.5841 Site #: Acres Permitted: 39.7 Operator: Lacy Cummings Cron 1 Name: Corn Predominant Soil Series: Norfolk (NoA) Cation Exchange Capacity (non 503): Crop I Max. PAN: 131 Crop 2 Name: Crop 2 Max. PAN: Q • Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons % Solids Volume PP per Applied r Acre (Dry Tons/Ac) Residual Sources (NPDES #. WQtt, F ert., Animal Waste, etc) Soil Cond. wry' Wet, Moist)metres Precip. Past 24 Hrs. v 3'? o' a c. ' < o j0 » m _ : o 3 a ^ R = : R o' TKN mgtkg 55000 Z Y [ 3 o 3 w o m• m9fkg Nitrate and Nitrite nvft PAN Applied ( lWacm) Name of Crop Type Receiving Residual Application Crop I I Crop 2 Crop I Crop 2 5/18/19 43,400 3.3 0.150 0 S 0.5 0.3 405 382 5.104 5.104 5120/19 173,600 3.3 0.602 0 S 0.5 0.3 55000 405 382 20.415 20.415 5/22119 148,800 3.3 0.516 0 S 0.5 0.3 55000 405 382E76,555 8 17.498 5/23/19 130,200 3.3 0.451 0 S 0.5 0.3 55000 405 3821 15.311 529/19 6,200 3.3 0.021 0 S 0.5 0.3 55000 405 382 0.729 6/4119 148,800 3.3 0.516 0 S 0.5 0.3 55000 405 3828 17.498 0.000 0 S 0.5 0.3 55000 405 382 0.000 0.000 0 S 0.5 0.3 55000 405 382 0.000 0.000 0 S 0.5 0.3 55000 405 382 0.0oo 0.000 0 S 0.5 0.3 55000 405 382o 0.000 0.000 0 S 0.5 0.3 55000 405 3820 0.000 0.000 0 S 0.5 0.3 55000 405 3820 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 651000 As Cd Cu Cr Pb H Mo Ni Se Zn P5 76.555 Lime A lied Annual lbs/acre 0.001 0.000 0.042 0.000 0.004 0.000 0.001 0.005 0.000 0.103 0.91 0.103 Date lbs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ac 0.001 0 000 0.042 0.000 0.004 0.000 0.0(11 0.005 0.000 Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop 131 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface- 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 207.00 Permit #: WQ0000672 Cation Exchange Capacity (non 503 only): Operator: R.G. Hammonds Owner: R.G. Hammonds Predominant Soil Series: Goldsboro (GoA) Acres Used: 57.5 Acres Permitted: 57.5 Site #: NC-RO-20 Field #: 8 n_..- iu•....,., Morale and Tntal Phnsnhorus use m9/lifl. % Solids use Raw Percent #): Lg . i . Non NINE Hnuual heavy u.caa ... c.0 - .. __ ___ _ - 9 10 11 12 Total 1 j 2 3 4 5 6 7 8 y DT/Ac./ 0 v App.ti Event 3.60 Arsenic 0.000 0.001 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.000 0.042 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.042 Chromium0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 denum Nickel 0.000 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Selenium 0.000 0.000 0.000 0.000 0.000 0.0 00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Zinc 0.000 0.105 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.105 Total rhos- 0.000 0.936 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.o00 0.000 0.000 0.936 horus _�__ . a :.. ...:.... .. in oepardanee "I certify, under penalty of law, that this document was prepareu uuuer my n.. «.............t,... ••�•�•• --- -__... ______ with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-8 Acres Utilized: 57.5 Land Owner: R.G. Hammonds Annual Dry Tons Applied: 210.7101 Site #: Acres Permitted: 57.5 Operator: R.G. Hammonds Crop 1 Name: Soy Bean Predominant Soil Series: Goldsboro(GoA) Crop I Max. PAN: 176 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: a m ° Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre Dry Tons Ac) Residual Sources (NPDES 4, WQ#, Fert.. Animal Waste, etc) Soil Cond. D ( iy' Moen Precip. Past 24 Hrs. inches Y K'o '� `6°+. •-' 0 * °o o Bi _ g *_ c n " E= : ' 0• TKN mg/kg 61000 Z Y 4 o 3 m o m• mg/kg Nitrate and Nitrite mglkg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 6127/19 235,600 2.5 0.427 W00000672 0 S 0.5 0.3 110 0.12 15.653 15.653 6/28119 260,400 2.5 OA72 W00000672 0 S 0.5 0.3 61000 110 0.12 17.300 17.300 6129/19 241,800 2.5 0.438 W00000672 0 S 0.5 0.3 61000 110 0.12 16.065 16.065 7/1/19 229,400 2.5 0.416 W00000672 0 S 0.5 0.3 61000 110 0.12 15.241 15-241 7/2/19 260,400 2.5 0.472 W00000672 0 S 0.5 0.3 61000 110 0.12 17.300 17.300 7/3/19 266,600 2.5 0.483 W00000672 0 S 0.5 0.3 61000 110 0.12 17.712 17.712 7/8/19 248,000 2.5 0.450 W00000672 0 S 0.5 0.3 61000 110 0.12 16.477 16.477 71151191 1 279,000 2.5 0.506 W00000672 0 S 0.5 0.3 61000 110 0.12 18.536 18.536 0.000 0.000 0.000 0.000 0.000 0.000 0.00(1 2000 1 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS. 01 2011290 As Cd Cu Cr Pb HP Mo Ni Se Zn P 134.284 134.284 Lime Applied Annual lbs/acre 0.001 0.000 0.042 0.000 0:004 0.000 0.001 0.005 1 0.000 0.105 0.936 0.105 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ac 0.001 0.000 0.042 0.000 0.004 0.000 0.001 0.005 0.000 Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop F 176 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date 1** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading! Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 46.63 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: R.G. Hammonds Owner: R.G. Hammonds Predominant Soil Series: Goldsboro (GoA) Acres Used: 12.5 Acres Permitted: 12.5 Site #: NC-RO-20 Field #: 7 Recidnal Annlvsis Data (Heavv Metals and Total Phosahorus use mg/kg, % Solids use Raw Percent #): wMEMENNE" 0 NONE in Annual Haaw Mortal Field Load mPs fCaleuiated in ® 1111 1 11 1 Ilf 1111 1 111 1 111 1111 1 Itl 1 111 ! 111 1 111 ! IBI 111 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 .�.� 11 11�� 1111 1111 1111 1111 1111 1111 1111 1111 1111 1111 11� 111 1 111 1 111 1 111 1 111 1111 11l1 t 111 1111 1111 1 Itt 1111 1111 ®'' 1 111 1 11 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 11 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 moms 1 111 •E1 111 1 11 1 111 1 Ilt 1 111 1 tll 1 111 1 111 1 11 1 1 1 111 1 111 1 1 ® 1 111 1 11 1 111 1 111 1 11! 1 111 1 111 1 tl 1 111 1 111 1 111 1 11 1 11 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 I t 11 1 111 1 111 ® 1 111 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �•. I Itl 1 1 1111 1111 1111 1111 1111 1111 11 1 1111 1111 1111 1' 1 nnn�n�a� "I certify, under penalty of law, that this document was preparea unoer my alrecnon or supervisuwn in acco.uaucc with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier a1�1 ad Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-7 Acres Utilized: 12.5 Land Owner: R.G. Hammonds Annual Dry Tons Applied: 46.5889 Site #: Acres Permitted: 12.5 Operator: R.G. Hammonds Cron 1 Name: Sov Bean Predominant Soil Series: Goldsboro(GoA) Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 176 Crop 2 Name: Crop 2 Max. PAN: Volume applied Volume Residual Sources Soil Precip. ,o 0 0 Z 3 Nitrate PAN Applied Name of Crap Type ° Y (toter one Solids/ * Applied r pP per (NPDES #, WQ#. Cond. Past 24 0 .� A m - R 4KN 9 3 w o and Ibs/acre ( ) Receiving Residual L m Liquid Solids Acre Fen.. Animal �ry Hrs. s- a o, m 2 R Y ^ 2 o ,; Nitrite Application Cu. Yds Gallons (Dry Tons/Ac) Waste, tic) Wet, Moist " ' 0 m8tk9 55000 m9ik0 nVtk0 Crop I Crop 2 Crop I Crop 2 624/19 124,000 3.3 1.365 W00000672 0 S 0.5 0.3 405 382 46.312 46.312 625/19 148,800 3.3 1.638 W00000672 0 S 0.5 0.3 55000 405 382 55.575 55.575 6130/19 86,800 2.5 0.724 W00000672 0 S 0.5 0.3 61000 110 0.12 26.527 26.527 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0-000 0.000 0.000 1 U.000 0.000 0.000 0,000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF sopp to this torn): TOTALS: 0 siyeoo As Cd Cu Cr I Pb lHglMol Nil Se Zn P 128.414 128.41a LimeApplied Annual)bs/acre 0.001 0.000 0.044 0.000 0.004 0.000 0.001 1 0.005 1 0.000 1 0.109 U.970 Date lbs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac 0.001 0.000 0.044 0.000 0.004 0.000 0.001 0.005 i 0.00 0.109 Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 176 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface-0.5, Injection/Incorporation- 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Lumberton Total Dry Tons Applied (Annual): 20.44 W00000672 Cation Exchange Capacity (non 503 only): R.G. Hammonds Owner: R.G. Hammonds Predominant Soil Series: Norfolk (NoA) 6.7 Acres Permitted: 6.7 Site #: NC-RO-20 Field #: 6 De�:d.ml Analvc:c notes rflPaw Metals and Total Phosphorus use me/kg. % Solids use Raw Percent ft MINIM 0 I I 0 on • �� la!I�m A nnnal TIPaw Metal Field l.narlinns ! .a cu ate m S acre. 1 111 ! 111 ! 111 1 111 1 111 1 111 1 111 1 111 1 111 1111 1 111 1 111 1 111 1 111 1 111 1 111 ! 111 ! 111 1 111 1111 1 111 1 111 1 111 1 111 1 111 1 111 I Iff 11 . ! ! 1 IIII IIII 1 111 IIII IIII ! 111 IIII Iff! ! 111 11 �� •►Lii`JiYL'Y1 III 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 11 1 1 1 1 ®'' !III 1 11 IIII 1 111 1 111 1 111 1 111 1 111 1 111 1 111 IIII 1 111 1 !! 1 111 1 111 1 11! 1 111 1 111 1 111 1 111 1 111 111 1 111 1 111 1 111 1 111 � 111 111 IIII IIII 111f 1 111 1 111 f 111 1 111 I I f I11 I I11 1 II • 1 1 1 1 11• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 111 1 111 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® IIII 1 1:` 1 111 1 111 1 111 1 111 IIII 1 111 IIII IIII 1 111 I Ifl 11.` 1 111 1 ` 1 111 1 111 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 ' •. "I certify, under penalty of law, that this document was preparea Honer my alrecaon or superv,swH ul accuruauca with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier ate%—o�f� Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: City of Lumberton Land Owner: R.G. Hammonds Operator: R.G. Hammonds CroD 1 Name: Soy Bean PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQPermit#: WQ0000672 Field#: NC-RO-20-6 Annual Dry Tons .Applied: 20.4764 Site #: Predominant Soil Series: Norfolk (NoA) Crop I Max. PAN: 164 Crop 2 Name: Acres Utilized: 6.7 Acres Permitted: 6.7 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: '$ a c o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (DryTons/Ac) Residual Sources (NPDES #, WQ#, Fert.. Animal Waste, etc) $O1l Cond. (Dry Wet' moist) precip. Past 24 Hrs. inches v o v $ $, ' o ». _ » 0 5 m iv ` o' TKN mg/kg 55000 2 c R. mglkg Nitrate and Nitrite mg/kg pAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 W/O 130,200 3.3 2.674 W00000672 0 S 0.5 0.3 405 382 90.723 90.723 6/22119 18,600 3.3 0382 W00000672 0 S 0.5 0.3 1 55000 405 382 12.960 12.960 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF sapp ( attach FORM FSF sapp to this form): TOTALS 0 148800 As Cd Cu Cr Pb H Mo Ni Se Zn P 103.684 103.684 Lime A lied Annual lbslacre 0.000 0.000 0.033 0.000 0.003 0.000 0.001 0.004 0.000 0.089 0.793 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac 0.000 0.000 0.036 0.000 0.003 0.000 0.001 0.004 0.000 0.089 Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop t64 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Appher *Application Method: S - Surface, IN - Injection, INC - Incorporation Z7 2 ,) **Volatilization Rate: Surface - 0.5, Injection/Incorporation - L0 Dale *** Mineralization Rates: Compost -0.I, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 147.96 Permit #: W00000672 Cation Exchange Capacity (non 503 only): Operator: R.G. Hammonds Owner: Charles Brown Predominant Soil Series: Wakulla(WkB) Acres Used: 33.4 Acres Permitted: 33.4 Site #: NC-RO-20 Field #: 4 nat. tHnaw Metals and Total Phosphorus use ma/Ica. %Solids use Raw Percent #): ..,1 uaa.,., Metal F:a .na moc a cn a e m s acre '� 1111 1tl 1111 1111 1111 1111 1111 t111 1111 1111 1111 1111 111 '® 1 ell 1 111 1 ell SIT, 11 1 111 1 ell 1 111 1 111 1 111 1 111 1 111 1 11 1 111 .. 1 11 1 1 1 111 1 111 f e e l t e l l 1 111 1 111 1 111 1 111 1 111 111 1 1 1 111 1 lee 1 111 1 111 1 111 1 111 1 111 1 111 1 Ill 1 111 1 ell 1 1 1 Ile ®'' 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 I l l 1 1 ® 1 11 111 1 lee 1111 1 111 1 Ill 1111 1111 1111 1111 1 ell 1 ell 1 eel ® 1 111 1 11 1 111 1 ell 1 111 1 Ilf 1 111 1 111 1 111 1 lee 1 111 1 ell 1 11 1 Ile 111. 1111 1 eel 1 Ill 1 ell 1 111 1 Ill 1 111 1 Ill 1 ell Imam 111. ® 111 Ile 111 1 Ile 1 Ill 1 ell 1 ell 1 11 1 Ill 1111 1 Ill 1 ell a le ® 1 ell 1 ' 1 111 1 111 1 Ill 1 Ill 1 111 1 Ile 1 111 1 lee 1 111 1 Ill 1 ' 1 1 ® 1111 1 Ile 1111 1111 1 111 1111 1 111 1 ell 1 111 1 ell ' . "1 certify, under penalty of law, that this document was prepareu unuer my UNEMvu u. 3up—..�...... .�"•tea••-- with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ,4;:� _gg- Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" 1N A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-4 Acres Utilized; 33.4 Land Owner: Charles Brown Annual Dry Tons Applied: 149.0142 Site #: Acres Permitted: 33.4 Operator: R.G. Hammonds Crop I Name: C.. Bermudagrass Predominant Soil Series: Wakulla(WkB) Crop 1 Max. PAN: 196 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: o s A Volume Iced applied (enter one) Solids/ Liquid Cu. Yds GSIIODS % Solids Volume Applied Per Acre (Dry TonslAc) Residual Sources (NPDES #. WQ#. Ferl.. Animal Waste, etc) Soil Cond. ryW Moist) Precip. Past 24 Hrs. inches D 3' ;; �.°. « .°� o F V o = 9 a ` o' TKN mgtkg 61000 ? > B c $ �. mgfkg Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 384,400 2.5 1.200 W00000672 Dry 0 S 0.5 0.3 110 0.12 43.966 43.966 229,400 2.5 0.716 WQ0000672 Dry 0 S 0.5 0.3 61000 110 0.12 26.238 26.238 266,600 2.5 0.832 W00000672 Dry 0 S 0.5 0.3 61000 110 0.12 30.493 30.493 k712V 260,400 2.5 0.813 W00000672 Dry 0 S 0.5 0.3 61000 110 0.12 29.784 29.784 279,000 2.5 0.871 WQ0000672 Dry 0 S 0.5 0.3 61000 110 0.12 31.911 31.911 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 Residuals Applicalions tolals on FIRM FSF supp ( attach FORM FSF Sapp to this form): TOTALS. 0 ial9soo As Cd Cu Cr Pb II Mo Ni Se 7_n P 162.391 162.391 LinieA lied Annual lbs/acre 0.001 0.(i 0.052 0.000 0.005 0.000 0.001 0.006 0.001 0.129 1.152 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ac 0.001 0000 0.052 0.000 0.005 0.000 0.001 0.006 0.001 0.129 Permitted C. P. L. R.**** Permit PAN Limit Isd2nd Crop 196 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation :;2;�7-r9. *"Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Lumberton Total Dry Tons Applied (Annual): 96.83 W00000672 Cation Exchange Capacity (non 503 only): R.G. Hammonds Owner: R.G. Hammonds Predominant Soil Series: Wakulla(WkB) 26.1 Acres Permitted: 26.1 Site #: NC-RO-20 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): � t ttt t tt t ttt t tlt t ttt t ttt t ttt t ttt t ttt t tt t ttt t ttt t tt � t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt I t t ttt t ttt t ttt t ttt t t. I ttt t tlt t ttt t ttt t ttt t ttt t ttt t ttt I ttt t tlt t t � t ttt t Itt I ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t tt t ttt t tt t ttt t ttt t ttt ttt t ttt t ttt t ttt t ttt I ttt t ttt t tt. ® t tt t Itt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t tt t ttt I ttt t ttt t ttt t Itt t ttt t ttt t ttt t ttt t ttt t tt ® t ttt t tt t ttt t ttt t ttt t ttt t ttt t ttt t ttt ttt t ttt t ttt t tt � t ttt t ttt t ttt t t t t ttt t ttt t tlt ttt t ttt t tt t ttt t t t t t ttt t t: t tlt � t ttt t ttt t ttt t ttt t ttt t ttt t ttt t ttt t t: �® t t t •. t ttt t ttt t ttt I ttt t ttt t ttt t ttt t ttt t t t t tt t •. !!� "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier C � - -� Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton Land Owner: R.G. Hammonds Operator: R.G. Hammonds Crop 1 Name: Bermudagrass WQ Permit#: WQ0000672 Field#: NC-RO-20-3 Annul Dry Tons Applied: 96.9525 Site #: Predominant Soil Series: Wakulla(WkB) Crop 1 Max. PAN: 147 Crop 2 Name: Acres Utilized: 26.1 Acres Permitted. 26.1 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° A Volume applied enter one) Solids/ ( ) . Liquid Cu. Yds Gallons % Solids Volume Applied r pp per Acre (Dry Tons/Ac) Residual Sources NPDES M, W ( Q# Fert. Animal Wire• etc) Soil Cond. (Dry' Wet, Moist Precip. Past 24 Hrs. inches D 3 a M 'S w c > o m > 0 3 5 g = m * o TKN rnWkg 61000 z Y 3 '� c w' mgtkg Nitrate and Nitrite mgfkg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 7116/19 186,000 25 0.743 W00000672 Dry 0 S 0.5 0.3 110 0.12 27.224 27.224 7/17/19 248,000 2.5 0.991 W00000672 Dry 0 S OS 0.3 61000 110 0.12 36.299 36.299 7119/19 254,200 2.5 1.015 W00000672 Dry 0 S 0.5 0.3 61000 110 0.12 37.206 37 206 7/19/19 241,800 2.5 0.966 W00000672 Dry 0 S 0.5 0.3 61000 110 0.12 35.391 35391 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF su p ( attach FORM FSF supp to this form): TOTALS- 0 930000 As Cd Cu I Cr Pb Hg Mo Ni Se Zn P 136.121 136.121 Lime A lied Annual lbs/acre 0.001 0.000 0.044 0.000 0.004 0.000 0.001 0.005 0.000 0.108 0.965 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac 0.001 0.000 0.044 0.000 0.004 0.000 0 001 0.005 0.00(1 0.108 Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 147 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier IZ-"J. Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface-0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3. raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loadine Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Lumberton Total Dry Tons Applied (Annual): 63.64 W00000672 Cation Exchange Capacity (non 503 only): Ozzell Baker Owner: Ozzell Baker Predominant Soil Series: Norfolk (NOA) 14.8 Acres Permitted: 14.8 Site #: NC-RO-16 Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): t •. t t t t t: t t: �� ®� t t 1 I t • t t t �� Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total i 2 3 4 6 6 7 8 9 10 11 121 DT/Ac./ A Pp Event 4.30 Arsenic 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.000 0.000 0.000 0.161 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.161 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 denum Nickel 0.000 0.000 0.000 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Selenium 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Zinc 0.000 0.000 0.000 0.239 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.239 Total Phos- 0.000 0.000 0.000 1.135 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.135 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier �D Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-16-6 Acres Utilized: 14.8 Land Owner: Ozzell Baker Annual Dry Tons Applied: 63.2906 Site #: Acres Permitted: 14.8 Operator: Ozzell Baker Crop I Name: Fescue Predominant Soil Series: Norfolk (NoA) Crop I Max. PAN: 161 Crop 2 Name: Cation Exchange Capacity (non 503): Fescue Crop 2 Max. PAN: 161 ° '� ° Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry TonslAc) Residual Sources (NPDES #, W FeA.. Animal Waste, etc) $01I Cond. (Dry. WeL Moi Precip. Past 24 Hrs. inches Y m ' o E cL + o m : .°� 0 3 A a N= ♦ m * o TKN mg/kg 16000 z > o 3 9 2 m. mglkg Nitrate and Nitrite mglkg PAN Applied (Ibslacre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 12/6/19 192,200 3A 1.841 W00000672 Dry 0 S 0.5 0.3 67 0.13 17.726 17.726 12/10/19 254,200 3.4 2.435 W00000672 Dry 0 1� 0.5 0.3 16000 67 0.13 23.444 23.444 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORI11 FSF supp ( attach FORM FSF supp to this form): TOTALS 0 aa6aoo As Cd Cu Cr Pb Hg I Mo Ni Se Zn P 41.169 41.169 Lime Applied Annual lbs/acre 0.002 0.000 0.161 0.000 0.004 0.000 0.002 0.009 0.001 0.239 1.135 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ac 0.002 0.000 0.161 0.000 0.004 0.000 0.002 0.009 0.001 0.239 Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop 161 161 "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation v **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.I, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Lumberton Total Dry Tons Applied (Annual): 35.67 WQ0000672 Cation Exchange Capacity (non 503 only): Ozzell Baker _Owner: Ozzell Baker Predominant Soil Series: Rains Sandy (Ra) 8.7 Acres Permitted: 8.7 Site #: NC-RO-16 Field #: 5 d I An 1 ' Data (Hea Metals and Total Phosphorus use m /kg, %Solids use Raw Percent #): Rest ua vy a ysts 8 9 10 11 12 Sample or 1 2 3 4 5 6 Com- posite Date 214/19 6/28/19 8/20/19 I1/11/19 %Solids 3.3 2.5 2 1 3.4 Arsenic 9.6 0.076 0.08711 0.19 Cadmium 0.96 0.00 5 0.0083 0.0287 Copper 269 5.88 1 2.19 18.7 Chromitur 201 0.045 1 0.053 0.058 Lead 19 0.526 10.0765 0.469 Mercury 0.53 0.0055 10.0059 0.0101 Molyb- 7.6 0.136 0.0284 0.199 entim denum 29.2 0.684 0.154 1 9.6 0.062 0.062 0.155 665 14.6 9.47 27.8 L 18700 130 270 132 A Iq_ Icutaleu In tuaiacrc): nnua..,�a.y ... .2.... •V•3 _ y Y ...,, 7 8 9 10 11 12_ 1 4 5 6 App. 4.10 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 [Arsenic 0.000 0.000 0.000 0.153 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.153 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 um Nickel 0.000 0.000 0.000 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Selenium 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.001 Zinc 0.000 0.000 0.000 0.228 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.228 Total Phos- 0.000 0.000 0.000 1.082 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.082 "I certify, under penalty of law, that this aocument was prepared under rimy direction o. win.... ..... » with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier �� Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: City of Lumberton Land Owner: Ozzell Baker Operator: Ozzell Baker tom....., r Weme• FescLe PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: W00000672 Field #: NC-RO-16-5 Annual Dry Tons Applied: 36.0405 Site #: Predominant Soil Series: Rains Sandy (Ra) ('ran 1 Max_ PAN: 184 Crop 2 Name: Acres Utilized: 8.7 Acres Permitted: 8.7 Cation Exchange Capacity (non 503): Fescue Crop 2 Max. PAN: 184 Volume applied Volume Residual Sources Soil PreciP. .o -e e 3 c z 3 Nitrate PAN Applied Name of Crop Type o t G (enter one) Solids/ * /o Applied per (NPDES #. WQ#. Cond. past 24 0 4. 'o' A ^_ � *R I KN 'c 3 C and ( Ibs/acre) Receiving Residual d Liquid Solids Acre Fert.. Animal ( ry. D R io o Nitrite Application Waste, etc) Wet, ' G ngA0 mgikg mglkg C rap I Crop 2 Crop 1 Crop 2 Cu. Yds Gallons (Dry Tons/Ac) Moist) 1f1Ch� 12/t2/191 1 254,200 3.4 1 4.143 WQOOD0672 Dry U S 0.5 0.3 16000 67 0.13 39.881 39.881 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.Doo 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.000 o.000 o.00a Residuals Applications totals on FORM FSF supp ( attach FORM FSF Sapp to this form): TOTALS: 0 z5azoo As Cd I Cu Cr I Pb I H r Mo I Ni Se Zn P 39.x81 39.881 Lime Applied Annual lbs/acre 0.002 0.000 0.153 0.000 0.004 0.000 0.002 0.008 D.DOI 0.228 1.082 0.228 Date Ibs/ac Prior Years Cumulative Ibs/ac Current Cumulative Ibs/ac 1 0.002 0.000 0.153 0.000 0.004 0.000 0,002 0.008 0.001 Permitted C. P. L.R.**** Permit PAN Limit Isd2nd Crop 184 184 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to asaurc ...a. qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2,1-0420 **Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) Dosage Rate Evaluation Report PrOdUCt Type: LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID (LUAEDL) Sample Date 2/4/2019 Usage From 2/1/2019 To 6/30/2019 Report # 92416933 Parameter PPM(m9/kg) Lbs/Dr1►Ton PA-N (Injected) 17166 34.331 PA-N (Surface w/ Incorp.) 17166 34.331 PA-N (Surface w/o Incorp.) 16963 33.926 TKN (TKN) 55000 110 Ammonia Nitrogen (Am) 405 0.81 Nitrate Nitrogen (Nin) 382 0.764 Organic Nitrogen (Orn) 54595 109.19 Total Phosphorus (P) 18700 37.4 Total Phosphate (P205) 42823 85.646 Estimated Avail. P205 21505 43.01 Total Potassium (K) <4780 <9.56 Total Potash (K20) <5736 <11.472 Arsenic (As) <9.6 <0.019 Cadmium (Cd) <0.96 <0.002 Chromium (Cr) NR NR Copper(Cu) 269 0.538 Lead (Pb) 19 0.038 Mercury (Hg) 0.53 0.001 Molybdenum (Mo) 7.6 0.015 Nickel (Ni) 29.2 0.058 Selenium (Se) <9.6 <0.019 Zinc (Zn) 665 1.33 Aluminum (AI) 41200 82.4 Calcium (Ca) 11300 22.6 Iron (Fe) NR NR Sodium (Na) 9850 19.7 Sulfur (S) NR NR Magnesium (Mg) 1870 3.74 Manganese (Mn) NR NR Percent Solids: 3.30 % pH Level: 6.4 Calculations PA-N (ppm) _ [ (f1) (ppm Org. N) ] + [ (V1) (ppm Ammonia N) ] + (ppm Nitrate N) P x 2.3 =Total P205 Total P205 x .5 =Estimated available P205 Kxt2=K20 ppm or mg/kg x .002 = Ibs/dry ton. Biosolids/Residuals Application State: NORTH CAROLINA Organic Nitrogen Mineralization Rate (f1): For AEROBICALLY DIGESTED 30.00% Ammonia Nitrogen Non -Volatilized Fraction (V1): For Injected:1.00 For Surtace w/ Incorp.:1.00 For Surface w/o Incorp.:0.50 NR =Data not Reported to Synagro or Data not Required Notes: 2101 01 AEDLIQ Cantral # 74103 09:36:11 6/26/2019 laceAnalyficalo w .nacelaba.com February 13, 2019 Nate Roth Synagro Technologies Inc 284 Boger Rd Mocksville, NC 27028 RE: Project: Lumberton VWVfP 2/7/19 Pace Project No.: 92416933 Dear Nate Roth: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for samples} received by the laboratory on February 07, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lord Patton lorri. patton@pacelabs1 com 1(828)254-7176 Project Manager Enclosures ce: Lysa Finnerty, Synagro REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, out the written consent of Pace Analytical Services, LLC. Page 1 of 18 aceAnalytical w .pacalabs.mm Project: Lumberton WWiP 2/7/19 Pace Project No.: 92416933 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/N ELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia(VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)876-9092 This report shall not be reproduced, except in full, out the written consent of Pace Analytical Services, LLC. Page 2bf 18 aceAnalytical w .pacelabs.com Project: Lumberton WWiP 2/7/19 Pace Project No.: 92416933 Lab ID Sample ID 92416933001 LUMBERTON WWTP Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 6010D SH1 13 PASI-A EPA 7471B RDT 1 PASI-A SM 2540G-2011 KDF 1 PASI-C ASTM D2974-67 KDF 1 PASI-C EPA9045D ECH 1 PASI-A SM 2719B-2011 EWS 1 PASI-A EPA 350.1 Rev 2.01993 Mod. CJH1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A EPA 365.1 Rev 2.01993 MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, -LC. Page 3 of 18 ;aceAnalyticalo w .pacelabs,com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Lumberton WWTP 2/7/19 Pace Project No.: 92416933 Sample: LUMBERTON WWTP Lab ID: 92416933001 Collected: 02/04/19 11:00 Received: 02/07/19 09:55 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6D10 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B Aluminum 41200 mg/kg 95.7 1 02/11/19 09:37 02/12/19 01:56 7429-90-5 Arsenic ND mg/kg 9.6 1 02/11/19 09:37 02/12/19 01:56 7440-38-2 Cadmium ND mg/kg 0.96 1 02/11/19 09:37 02/12/19 01:56 7440-43-9 Calcium 11300 mg/kg 95.7 1 02/11/19 09:37 02/12/19 01:56 7440-70-2 Copper 269 mg/kg 4.8 1 02/11/19 09:37 02/12/19 01:56 7440-50-8 Lead 19.0 mg/kg 4.8 1 02/11/19 09:37 02/12/19 01:56 7439-92-1 Magnesium 1870 mg/kg 95.7 1 02/11/19 09:37 02/12/19 01:56 7439-95-4 Molybdenum 7.6 mg/kg 4.8 1 02/1111909:37 02/12/1901:56 7439-98-7 Nickel 29.2 mg/kg 4.8 1 02/11/19 09:37 02/12/19 01:56 7440-02-0 Potassium ND mg/kg 4780 1 02111/1909:37 02/12/19 01:56 7440-09-7 Selenium ND mg/kg 9.6 1 02/11/19 09:37 02/12/19 01:56 7782-49-2 Sodium 9850 mg/kg 4780 1 02/11/19 09:37 02/12/19 01:56 7440-23-5 Zinc 665 mg/kg 9.6 1 02/11/19 09:37 02/12/19 01:56 7440-66-6 7471 Mercury Analytical Method: EPA7471B Preparation Method: EPA7471B Mercury 0,63 mg/kg 0.12 1 02/11/1916:07 02112/1915:59 7439-97-6 254OG Total Percent Solids Analytical Method: SM 254OG-2011 Total Solids 3.3 % 0.10 1 02/08/19 16:31 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 96.7 % 0.10 1 02/08/19 16:25 9046pH Soil 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, N021NO3 Nitrogen, NO2 plus NO3 Nitrogen, Nitrate Nitrogen, Nitrite 365.1 Phosphorus, Total Phosphorus Date: 02/13/2019 11 :12 AM Analytical Method: EPA 9045D 6.4 Std. Units 0.10 1 02/08/1917:20 H3 Analytical Method: SM 2710B-2011 17000 mg/kg 0.12 1 02/12/1913:40 N2 Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. 405 mg/kg 269 1 02/08/1912:27 02/09/1915:55 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 65000 mg/kg 2350 2 02/09/19 01:19 02/12/19 02:17 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993 382 mg/kg 60.1 1 02/09/19 04:09 02/09/19 05:20 382 mg/kg 60.1 1 02/09/19 04:09 02/09/19 05:20 14797-55-8 ND mg/kg 30.1 1 02/09/19 04:09 02/09/19 05:20 14797-65-0 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 18700 mg/kg 255 10 02/07/19 19:20 02/07/19 22:22 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnalytical w ..pacelabaxm QUALITY CONTROL DATA Project: Lumberton WWfP 2/7/19 Pace Project No.: 92416933 Pace Analytical Services, LLC sBOO luncey Ave. Suite too Huntersville, NC 28078 (704)875-9092 QC Batch: 457445 Analysis Method: EPA 7471B QC Batch Method: EPA 7471B Analysis Description: 7471 Mercury Associated Lab Samples: 92416933001 METHOD BLANK: 2495015 Matrix: Solid Associated Lab Samples: 92416933001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury mg/kg ND 0.0060 02/1211915:32 LABORATORY CONTROL SAMPLE: 2495016 Spike Parameter Units Cone. Mercury mg/kg 0.083 LCS LCS %Rec Result % Rec Limits Qualifiers 0.083 100 80-120 MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2495017 2495018 MS MSD 92416976023 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual Mercury mg/kg ND 0.059 0.06 0.057 0.052 90 79 75-125 8 Results presentetl on this page are In the units Intllcatetl by the "Unlfs" column except where an alternate unit is presentetl to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/112019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 aceAnalytical www.pacela6s.com QUALITY CONTROL DATA Project: Lumberton WWTP 2/7119 Pace Project No.: 92416933 Pace Analytical Services, LLC 9600 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 457387 Analysis Method: EPA 6010D QC Batch Method: EPA3050B Analysis Description: 6010 MET Associated Lab Samples: 92416933001 METHOD BLANK: 2494691 Associated Lab Samples: 92416933001 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed Aluminum mg/kg ND 10.0 02112/1901:28 Arsenic mg/kg ND 1.0 02/12/19 01:28 Cadmium mg/kg ND 0.10 02/12/1901:28 Calcium mg/kg ND 10.0 02/12/19 01:28 Copper mg/kg ND 0.50 02/12/19 01:28 Lead mg/kg ND 0.50 02/12/19 01:28 Magnesium mg/kg ND 10.0 02/12/19 01:28 Molybdenum mg/kg ND 0.50 02/12/19 01:28 Nickel mg/kg ND 0.50 02/12/19 01:28 Potassium mg/kg ND 500 02/12/19 01:28 Selenium mg/kg ND 1.0 02/12/19 01:28 Sodium mg/kg ND 500 02/12/19 01:28 Zinc mg/kg ND 1.0 02/12/19 01:28 Qualifers LABORATORY CONTROL SAMPLE: Parameter 2494692 Units Spike Conn. LCS Result LCS % Rec %Rec Limits Qualifers MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2494693 2494694 MS MSD 92416931001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result % Rae %Rec Limits RPD Qua] Aluminum ni 15600 7080 7220 27800 28400 173 177 75-125 2 M1 Arsenic mg/kg ND 708 722 630 643 88 88 75-125 2 Cadmium mg/kg 1.9 708 722 652 669. 92 92 75-125 3 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, are: 02/13/2019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 aceAnalytical w .pacelabs.wm QUALITY CONTROL DATA Project: Lumberton WJVfP 2/7/19 Pace Project No.: 92416933 Pace Analytical Services, LLC 9600 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2494693 2494694 MS MSD 92416931001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conn. Result Result %Rec %Rec Limits RPD Qual Calcium mg/kg 9340 7080 7220 15900 16300 93 96 75-125 2 Copper mg/kg 278 708 722 976 994 98 99 75-125 2 Lead mg/kg 48.9 708 722 691 707 91 91 75-125 2 Magnesium mg/kg 2690 7080 7220 9380 9600 94 96 75-125 2 Molybdenum mg/kg 9.0 708 722 710 728 99 99 75-125 2 Nickel mg/kg 15.8 708 722 679 695 93 94 75-125 2 Potassium mg/kg ND 7080 7220 11000 11300 95 97 75-125 2 Selenium mg/kg ND 708 722 599 618 84 85 75-125 3 Sodium mg/kg ND 7080 7220 8410 8710 96 98 75-125 4 Zinc mg/kg 468 708 722 1090 1110 87 89 75-125 2 Results presented on this page are in the units intlicatetl by the "Units" column except where an alternate unit is presentetl to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 02/13/2019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAnalytical w .pacelabs.wrn QUALITY CONTROL DATA Project: Lumberton WVVTP 2/7/19 Pace Project No.: 92416933 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 457237 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92416933001 SAMPLE DUPLICATE: 2494016 92416878001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 4.5 - 4.4 1 SAMPLE DUPLICATE: 2494017 92417004001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 19.2 18.4 4 Results presentetl on this page are in the units Intllcatetl by the"Units" column except where an alternate unit is presentetl to [he right of [he result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/13/2019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 Ahd� IF aceAnalytical w .pacelabs.wrn QUALITY CONTROL DATA Project: Lumberton NNVTP 2/7/19 Pace Project No.: 92416933 QC Batch: 457221 Analysis Method: EPA 9045D QC Batch Method: EPA 9045D Analysis Description: 9045 pH Associated Lab Samples: 92416933001 SAMPLE DUPLICATE: 2493893 92416187001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.8 7.9 0 H3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Results presentetl on this page are in the units intlicatetl by the "Units" column except where an alternate unit is presentetl to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/13/2019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnalytical a'xwpacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9900 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Project: Lumberton VWVfP 2/7/19 Pace Project No.: 92416933 QC Batch: 457085 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod. QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia Associated Lab Samples: 92416933001 METHOD BLANK: 2493205 Matrix: Solid Associated Lab Samples: 92416933001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/kg NO 8.5 02/09/1915:26 LABORATORY CONTROL SAMPLE: 2493206 Spike LCS LCS % Rae Parameter Units Conc. Result % Rae Limits Qualifiers Nitrogen, Ammonia mg/kg 481 473 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2493207 2493208 MS MSD 92416187001 Spike Spike MS MSD MS MSD % Rao Parameter Units Result Conc. Conn. Result Result % Rec % Rao Limits RPD Qual Nitrogen, Ammonia mg/kg 4000 953 918 9370 9000 118 83 90-110 4 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2493209 2493210 MS MSD 92416556005 Spike Spike MS MSD MS MSD % Rao Parameter Units Result Conc. Conc. Result Result % Rao % Rao Limits RPD Qual Nitrogen, Ammonia mg/kg 5560 22200 21400 27200 26100 97 96 90-110 4 Results presentetl on this page are In the units intlicatetl by the"Units" column except where an alternate unit is presentetl to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02113/201911:12 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 18 aceAnaiytical www.pacelabs.cam QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Lumberton WVVTP 2/7I19 Pace Project No.: 92416933 QC Batch: 457266 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92416933001 METHOD BLANK: 2494217 Matrix: Solid Associated Lab Samples: 92416933001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/kg NO 50.0 02/12/19 01:50 LABORATORY CONTROL SAMPLE: 2494218 Spike LCS LCS %Rea Parameter Units Conc. Result %Rea Limits Qualifiers Nitrogen, Kjeldahl, Total mg/kg 1000 1070 107 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2494219 2494220 MS MSD 92416187001 Spike Spike MS MSD MS MSD % Rae Parameter Units Result Conc. Cone. Result Result % Rae % Rea Limits RPD Qual Nitrogen, Kjeldahl, Total mg/kg 10200 1790 1650 20200 22800 -42 112 90-110 12 M61R1 Results presen[etl on [his page are in [he units intlicatetl by the "Units" column except where an alternate unit is presentetl to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not 6e reprotluced, except in full, Date: 02/13/201911:12 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 18 aceAnalXical a .pacelebs.anm QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Lumberton VWVfP 2/7/19 Pace Project No.: 92416933 QC Batch: 457273 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite Associated Lab Samples: 92416933001 METHOD BLANK: 2494230 Matrix: Solid Associated Lab Samples: 92416933001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/kg ND 2.0 02/09/19 05:10 Nitrogen, Nitrite mg/kg ND 1.0 02/09/19 05:10 Nitrogen, NO2 plus NO3 mg/kg ND 2.0 02/09/19 05:10 LABORATORY CONTROL SAMPLE: 2494231 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrogen, Nitrate mg/kg 15 17.0 113 90-110 Nitrogen, Nitrite mg/kg 10 10.1 101 90-110 Nitrogen, NO2 plus NO3 mg/kg 25 27.1 108 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2494232 2494233 MS MSD 92416556006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/kg ND 659 663 532 488 81 74 90-110 9 Nitrogen, Nitrite mg/kg ND 436 441 356 354 75 74 90-110 1 Mt Nitrogen, NO2 plus NO3 mg/kg NO 1090 1100 887 842 76 71 90-110 5 MI Results presentetl on this page are in the units intlicatetl by the "Units" column except vMere an alternate unit is presentetl to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02113/2019 11:12 AM without the written consent of Pace Analytical Services, L-C. Page 12 of 18 aceAnalytical wwwpace/abs.cam QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: Lumberton WWiP 2/7/19 Pace Project No.: 92416933 QC Batch: 457001 Analysis Method: EPA 365.1 Rev 2.01993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92416933001 METHOD BLANK: 2492910 Matrix: Solid Associated Lab Samples: 92416933001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/kg ND 0,96 02107/1922:16 LABORATORY CONTROL SAMPLE: 2492911 Spike LCS LCS %Rec - Parameter Units Conc. Result %Rec Limits Qualifiers Phosphorus mg/kg 49 51.7 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2492912 2492913 MS MSD 92416609001 Spike Spike MS MSD MS MSD % Rao Parameter Units Result Conc. Conic. Result Result %Rec %Rec Limits RPD Qual Phosphorus mg/kg 14100 184 184 13800 13400 -141 -401 90-110 4 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2492914 2492915 MS MSD 92416464001 Spike Spike MS MSD MS MSD % Rao Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Phosphorus mg/kg 10200 49 49.9 12700 11200 5120 2100 90-110 12 M61R1 Results presenletl on this page are in the units intlicatetl by the "Units" column except where an alternate unit is presen[etl to the right of tM1e result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/13/2019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 aceAnalytical wmvpacelabs.com QUALIFIERS Project: Lumberton WWTP 2/7/19 Pace Project No.: 92416933 1113;i.I:IYYGl:69 DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 PQL- Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RED values. LCS(D) -Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RED -Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. PAST -A Pace Analytical Services -Asheville PAST-C Pace Analytical Services -Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. R1 RED value was outside control limits. Date: 02/13/2019 11:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 18 laceAnalyticale w .pacelabs.anm QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Lumberton WWTP 92416933 2/7/19 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92416933001 LUMBERTON WWTP EPA3050B 457387 EPA 601 OD 457494 92416933001 LUMBERTON WWTP EPA7471B 457445 EPA 7471B 457534 92416933001 LUMBERTON WWTP SM 2540G-2011 457411 92416933001 LUMBERTON WWTP ASTM D2974-87 457237 92416933001 LUMBERTON WWTP EPA 9045D 457221 92416933001 LUMBERTON WWTP SM 271OB-2011 457664 92416933001 LUMBERTON WWTP EPA 350.1 Rev 2.01993 457085 EPA 350.1 Rev 2.01993 457187 Mod, Mod. 92416933001 LUMBERTON WWTP EPA 351.2 Rev 2.01993 457266 EPA 351.2 Rev 2.01993 457561 92416933001 LUMBERTON WWTP EPA 353.2 Rev 2.01993 457273 EPA 353.2 Rev 2.01993 457274 92416933001 LUMBERTON WWTP EPA 365.1 Rev 2.01993 457001 EPA 365.1 Rev 2.01993 457029 Date: 02/13/2019 11:12 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 �w / cYceAnalyflcaj Document Name: Sample Condition Upon Receipt(SCUR) Document No.: Document Document Revised: February 7, 2018 Page i of 2 Issuing Authority: Pace Carolinas Quality Office Laboratory receiving saTples: Asheville Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Client Name: M R 92416933 r Project #: C) IIIII IIIIIIIIIIIillll Courier: ❑Fed Ex L UPS ❑LISPS ❑Client 8241 @33 ❑ Commercial ❑Pace ❑Other:_ Custody Seal Present? ❑Yes �o Sealslntactr s ❑No Date/Initials Person Examining Contents. -[I-) c) - 1cl Packing Material: ❑Bubble Wrap ❑Bobbie Rags ❑None ❑ Other Biological Tissue Frozen? Thermometer: n ❑Yes []No QN/A ? (Ct`II^^ Type of ice: ❑Wet ❑Blue❑'None ❑IR Gun ID: � W Cooler Temp (°C): (�(] - lA� Correction Factor; Add/Subtract (`C)_ �� Temp should be above freezing to 6°C Cooler Temp Corrected (°C): z�f.L— []samples out of temp criteria. Samples on ice, cooling process hasbegun USDA Regulated Soil (❑ N/A, water sample) Did samples c rlgpate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ��a o Hirai? Hues I�fS Comments/Discrepancy: Chain of Custody Present? ❑Yes ❑No ❑N/A 1, Samples An'ived within Hold Time? QYes []NO ❑N/A 2. Short Hold Time Analysis (02 hr.)? ❑Yes ❑No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes i QNa ❑N/A 41 Sufficient Volume? ❑Yes ❑No ❑N/A 5. Correct Containers Used? Dyes []No ❑N/A 6. -Pace Containers Used? LINO❑N/A Containers Intact? ,Q,/Fes I_IYes []No ❑N/A 7. Dissolved analysis: Samples Field Filtered? Elves ❑No QN/A 8. Sample labels Match COC? ❑No ❑N/A 9. III�Yes V -Includes Date/Time/ID/Analysis Matrix: P) Headspace In VOA Vials(>5-6mm)? ❑Yes []NO []NIA 10. Trip Blank Present? ❑Yes ❑Na N/A 11. Trip Blank Custody Seals Present? QYes ❑No N/A COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION{RESOLUTION Field Data Required? ❑Yes�No Person contacted: Date/Time: Project Manager SCURF Review: ! Date:c�27(. Project Manager SRF Review: Date: 7 Page 16 of 18 Document Name: Document Revised: February 7, 2018 / piceAnalytical Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No,: F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project k Wo# ; 92416%3 Due Dale 02/18/19 PM' lJP 82_5YNRGRO CLIENT: , 2 - = = z _ \ a a ? z z z — Q z 6 - z u z w 0 _ 'o a c mo 'o o o n n ¢ o E - i > - r a _ - w " x z x < - u u v c of as G a 2L a a E a ¢ o o v"i S a a. : E < E n h _ E E E E E E E E E E E E E v E a E E E E _ _ E = o e N Ln o 3 Y °a o n', N Y Y z s m E m G tp ro ca is 0 o 0 0 to o > 3 c > > a o a a a a a a > > 1 2 3 4 5 NN 6 \d S +NN 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot H Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers, Page 17 of 18 CHAIN -OF -CUSTODY / Analytical Request Document The Ch tiRof-Custody is a LEGAL DOCUMENT. AA RkvaM RaIda must Ip comPleled edMalely. f� ISedtionA Section Section Page• of _-_- RequiredCNntinrormatlem Required Project IntatmaYon: Inver" lnbnnation: compenr Synagro ReportracAttention: Mary Brewer Addrcas 284 Boger Rd. CopyTe: compenr Name: Synagro REGULATORY:AGENCY Mocksvllle, NC 27028 Addrom 2B4 Boger Rd, MGoksville,NC 27028 r, NPDES r GROUNDWATER r DRINKINGWA-ER r UST r RCRA r OTHER _— Emell To: Pumhesa Older No.: PPapa uote oiL. Gv7r, Phone. 338-7 1610 Fmc Pmisst Nema: - MonePntance W"' Sib Lc shore /a/r „.. --,. STATE;: ) J3 Fgtered (YINEmma Rego trued Due DetorTAT; Pmiect Numaar. Pee*P,om e: i; Re tutisted:Arialys(s Section Velld MatriX Codes 2 a- z - R.gmr.acu.nrinrom,eaen N3TSIX camp COLLECTED Preselveb'ves .� WIMYrAmR W ^ z U Z m < acwr wavasa : CEO _ �- L ncouQT It U IV L 8 3 SAMPLE ID 6 w to z z c AR y < z IT as c rJ _ (A.Z, Omf,)AR w p w 3 m ¢ N Z fJ Sorrow Ice MUST Be UNIQUE TosuE is _ Q w Oz u O^ m _. Q U Y R to s o 0 o E a ¢` a 0, z D = Q. A z o 79 o¢ r 2 ofT.T.TIMCTM�ME +' = = Z z z i O �' Pace Project NuJ Lab I.D. ' ^ �•i`^) % :/le X XI X F X I X1 XI X1 X X at, I a I .�t�.. SL G 6'+i pl 14 Mama 4-':Want Mama Mw,w • : ADOffIdNALCOM1A1EN75:,'"_ :-i,RELNWf5NE6BY/APFILYATI ON. - bAiE .:'11fAE :: - :ACCEPTED BY111FRLWTbN _::DATE '�:nME%;.. SAMPLE CAN0IT[ONS N Z171 v AJy L.. Main SAMPLERNAMEAND SIGNATURE -r;:' �:. :-:�..:':: PRMTName OI SAMPLER C V N G U ., A SIGNATURE OF SAMPLER: jj�(— ' DATESIDrrttl _ - Mh11Do 1 U -i......... rv...: o...,,.,...4......-... ,....P...: NET ao...........................,.,.�.,.......1.sv6......,......-.................,.a. Jo..... F-ALL-C-020.D.:08. 12-0..-2007 Cameron Testing Services, Inc. Laboratory Report Client: Synagro CTs Prof. Project: Lumberton WWTP _1. Regulatory Sample Information Sampled M. Goad Date 02/04/19 Received a Analyses and Results NC DENR #664 NC PHHS #37799 US EPA#NC01918 190200 Yes M. Sims Date 02/04/19 Lab !D Sample 1p v SR Analyte Result c E a w Std. Methods ro c a Reference a 190200 -1 -2 -3 -4 -5 -6 -7 190200 -1 -2 -3 -4 -5 -6 -7 nepori Review Manager Sludge Gr Fec. Coliform-S 78100 CFUIg 391 a0 02/05/19 ERP 9222D - MF <23100 CFUrg 23100 23100 CFU/g 23100 <23100 CFU/Q 23100 <39100 CFUrg 39100 157000 CFu19 39200 196000 CFUr9 39200 Geomean 52900 'fudge Gr TS (%) 2.56% % 0.01 02/05/19 ERP 2540 G -TS 4.32% % 0.01 4.33% % 0.01 4.32% % o.o1 2.56% % o.o1 2.55% % o.o1 2.55% % 0.01 Date D 19 to 219 S. Steele Str. Sanford NC 27330 919-208-4240 chris@camerontesting.com 0 C 0 O N H a CL > p c� c z 0 0 CL o -1- H z z a N 4 W .2 - M N O _ � O L 0 aa5 VOA r ',±r .- N a z LO lad Z16 c(DI U - q5 z (NIJ�7 aol T U -- Z o Xplevq o qaaE) / dwoo `.7 aLuil a}ea 7 N a o q 0 tit z 0gt! M -J- c� t9 Is- CV r Q G1 CL �o6 o o _cr a 2�SENCO Laboratories 9g Accurate. Timely. Respousive. luuavative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, August 7, 2019 Hunt Environmental Associates (HU017) Attn: Jordan Davis 3330 Saddletree Road. Lumberton, NC 28360 RE: Laboratory Results for Project Number: [none], Project Name/Desc: City of Lumberton ENCO Workorder(s): CC10937 Dear Jordan Davis, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, June 28, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OUCLC'=-:�CA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 27 PROJECT NARRATIVE Client: Hunt Environmental Associates (HU017) Project: City of Lumberton Lab ID: CC10937 Overview (� �Eo www.encolabs.com Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples No Comments Quality Control Remarks No Comments Other Comments The Plant Available Nitrogen (PAN) has been calculated via available data as 205.12 The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 27 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: WW-1 Lab ID: CC10937-01 Sampled: 06/28/19 10:30 Received: 06/28/19 14:05 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1010A NO PREP 07/12/19 07/08/19 11:04 07/10/19 14:26 EPA 6010D EPA 3010A 12/25/19 01/06/20 07/10/19 09:06 07/11/19 13:33 EPA 7470A EPA 7470A 07/26/19 08/02/19 07/05/19 10:52 07/08/19 09:31 EPA 8081E EPA 3510C 07/05/19 08/14/19 07/05/19 08:20 07/10/19 14:04 EPA 8151A EPA 3510C 07/05/19 08/12/19 07/03/19 15:50 07/08/19 15:03 EPA 8260D EPA 503013_MS 07/12/19 07/24/19 07/10/19 00:00 07/10/19 17:00 EPA 8270E EPA 3510C MS 07/05/19 08/14/19 07/05/19 11:40 07/18/19 14:50 EPA 9040C NO PREP 06/28/19 10:44 07/05/19 09:15 07/05/19 10:58 SW-846 Ch.7 Sec.3 NO PREP 07/12/19 07/09/19 14:00 07/10/19 11:38 SW-846 Ch.7 Sec.3 NO PREP 07/12/19 07/09/19 14:00 07/10/19 14:22 Client ID: WW-1 Lab ID: CC10937-02 Sampled: 06/28/19 10:30 Received: 06/28/19 14:05 Parameter Preparation Hold Date/Time(sl Prep Date/Time(s) Analysis Date/Time(s) CSU Method NO PREP 03/23/22 07/01/19 08:18 07/02/19 13:48 EPA 200.7 Same 12/25/19 07/01/19 08:18 07/02/19 10:04 EPA 245.1 EPA 245.1 07/26/19 07/01/19 10:18 07/05/19 10:50 EPA 353.2 NO PREP 06/30/19 10:30 06/28/19 12:56 06/28/19 17:16 EPA 353.2 NO PREP 07/26/19 07/02/19 11:18 07/02/19 11:18 EPA 353.2 NO PREP 03/23/22 07/02/19 11:18 07/02/19 11:18 EPA 9040C NO PREP 06/28/19 10:44 07/09/19 09:31 07/09/19 09:31 SM 2540B-2011 NO PREP 07/05/19 07/03/19 20:34 07/03/19 20:34 Client ID: WW-1 Lab ID: CC10937-02RE1 Sampled: 06/28/19 10:30 Received: 06/28/19 14:05 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 365.4 Same 07/26/19 07/01/19 12:15 07/05/19 18:00 Client ID: WW-1 Lab ID: CC10937-02RE2 Sampled: 06/28/19 10:30 Received: 06/28/19 14:05 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 351.2 Same 07/26/19 07/01/19 12:15 07/05/19 18:30 Client ID: WW-1 Lab ID: CC10937-02RE3 Sampled: 06/28/19 10:30 Received: 06/28/19 14:05 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 350.1 NO PREP 07/26/19 07/09/19 09:38 07/09/19 09:38 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 27 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: WW-1 Lab ID: CC10937-01 Anala Results Flag MDL POLL Units Method Notes Barium - TCLP 0.272 0.0500 0.250 mg/L EPA 6010D pH 7.2 1.0 1.0 pH Units EPA 9040C Q-01 Temperature for pH (deg. C) 23 pH Units EPA 9040C Q-01 Client ID: WW-1 Lab ID: CC10937-02 Anala Results Flag MDL POLL Units Method Notes Aluminum - Total 572 0.420 1.00 mg/kg EPA 200.7 Cadmium - Total 0.00753 1 0.00360 0.0100 mg/kg EPA 200.7 Calcium - Total 287 0.390 1.00 mg/kg EPA 200.7 Copper - Total 5.88 0.0160 0.100 mg/kg EPA 200.7 Lead - Total 0.526 0.0310 0.100 mg/kg EPA 200.7 Magnesium - Total 47.4 0.290 1.00 mg/kg EPA 200.7 Mercury - Total 0.00548 0.00150 0.00200 mg/kg EPA 245.1 Molybdenum - Total 0.136 0.0250 0.100 mg/kg EPA 200.7 Nickel- Total 0.684 0.0220 0.100 mg/kg EPA 200.7 Nitrate/Nitrite as N 0.12 0.041 0.10 mg/kg EPA 353.2 Nitrite as N 0.12 0.017 0.10 mg/kg EPA 353.2 pH 7.0 1.0 1.0 pH Units EPA 9040C Q-01 Potassium - Total 81.8 1.50 5.00 mg/kg EPA 200.7 Sodium - Total 429 4.00 5.00 mg/kg EPA 200.7 Sodium Adsorption Ratio 6.17 [blank] CSU Method Temperature for pH (deg. C) 22 pH Units EPA 9040C Q-01 Total Solids 2.5 0.0050 0.0050 % by Volume SM 2540B-2011 Zinc - Total 14.6 0.0440 0.100 mg/kg EPA 200.7 Client ID: WW-1 Lab ID: CC10937-02RE1 Anala Results Flag MDL POLL Units Method Notes Phosphorus 130 D 1.2 5.0 mg/kg EPA 365.4 Client ID: WW-1 Lab ID: CC10937-02RE2 Anala Results Flag MDL POLL Units Method Notes Total Kjeldahl Nitrogen 610 D 26 48 mg/kg EPA 351.2 Client ID: WW-1 Lab ID: CC10937-02RE3 Anala Results Flag MDL POLL Units Method Notes Ammonia as N 110 D 4.0 9.0 mg/kg EPA 350.1 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 27 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-1 Lab Sample ID:CC10937-01 Received: 06/28/19 14:05 Matrix: Waste Water Sampled:06/28/19 10:30 Work Order: CC10937 Project: City of Lumberton Sampled By:Jordan Davis TCLP Volatile Organics by GCMS ^ - ENCO Orlando Certified analyte [NC 424] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1-Dichloroethene [75-35-4]^ 0.094 UD mg/L 100 0.094 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH 1,2-Dichloroethane [107-06-2]1 0.063 UD mg/L 100 0.063 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH 2-Butanone [78-93-3]^ 0.45 UD mg/L 100 0.45 0.50 9G10012 EPA 8260D 07/10/19 17:00 MJH Benzene [71-43-2]1 0.071 UD mg/L 100 0.071 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH Carbon Tetrachloride [56-23-5]1 0.094 UD mg/L 100 0.094 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH Chlorobenzene [108-90-7]1 0.072 UD mg/L 100 0.072 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH Chloroform [67-66-3]1 0.080 UD mg/L 100 0.080 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH Tetrachloroethene [127-18-4]^ 0.076 UD mg/L 100 0.076 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH Trichloroethene [79-01-6]1 0.089 UD mg/L 100 0.089 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH Vinyl chloride [75-01-4]1 0.071 UD mg/L 100 0.071 0.10 9G10012 EPA 8260D 07/10/19 17:00 MJH Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 0.054 1 0.0500 107 % 41-142 9GIO012 EPA 8260D 0711011917:00 MJH Dlbromofluoromethane 0.056 1 0.0500 113 % 53-146 9GIO012 EPA 8260D 0711011917:00 MJH Toluene-d8 0.050 1 0.0500 99 % 41-146 9GIO012 EPA 8260D 0711011917:00 MJH TCLP Semivolatile Organics by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dichlorobenzene [106-46-7]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi 2,4,5-Trichlorophenol[95-95-4]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi 2,4,6-Trichlorophenol[88-06-2]^ 0.03 UD mg/L 5 0.03 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi 2,4-Dinitrotoluene [121-14-2]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi 2-Methylphenol[95-48-7]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi 3 & 4-Methylphenol[108-39-4/106-44-5]^ 0.04 UD mg/L 5 0.04 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi Hexachlorobenzene [118-74-1]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi Hexachlorobutadiene [87-68-3]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi Hexachloroethane [67-72-1]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi Nitrobenzene [98-95-3]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi Pentachlorophenol [87-86-5]^ 0.04 UD mg/L 5 0.04 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi Pyridine [110-86-1]^ 0.02 UD mg/L 5 0.02 0.05 9GO5024 EPA 8270E 07/18/19 14:50 jfi QL-02 Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes 2,4,6-Tribromopheno/ ND 5 0.250 % 33-145 9GO5024 EPA 8270E 0711811914:50 jfi QS-05 2-Fluorobiphenyl 0.11 5 0.250 43 % 32-116 9GO5024 EPA 8270E 0711811914:50 if/ 2-Fluorophenol 0.057 5 0.250 23 % 11-100 9GO5024 EPA 8270E 0711811914:50 if/ Nitrobenzene-d5 0.061 5 0.250 32 % 24-107 9GO5024 EPA 8270E 0711811914:50 if/ Phenol-d5 0.036 5 0.250 15 % 10-100 9GO5024 EPA 8270E 0711811914:50 if/ Terphenyl-d14 0.13 5 0.250 52 % 52-150 9GO5024 EPA 8270E 0711811914:50 if/ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 27 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-1 Lab Sample ID:CC10937-01 Received: 06/28/19 14:05 Matrix: Waste Water Sampled:06/28/19 10:30 Work Order: CC10937 Project: City of Lumberton Sampled By:Jordan Davis TCLP Pesticides by GC ^ - ENCO Orlando certified analyte [NC 424] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Chlordane (tech) [12789-03-6]1 0.00036 U mg/L 1 0.00036 0.00050 9GO5004 EPA 8081E 07/10/19 14:04 JJB Endrin [72-20-8]1 0.000014 U mg/L 1 0.000014 0.000050 9GO5004 EPA 8081E 07/10/19 14:04 JJB gamma-BHC [58-89-9]1 0.000021 U mg/L 1 0.000021 0.000050 9GO5004 EPA 8081E 07/10/19 14:04 JJB Heptachlor[76-44-8]^ 0.000026 U mg/L 1 0.000026 0.000050 9GO5004 EPA 8081E 07/10/19 14:04 JJB Heptachlor epoxide [1024-57-3]^ 0.000018 U mg/L 1 0.000018 0.000050 9GO5004 EPA 8081E 07/10/19 14:04 JJB Methoxychlor[72-43-5]^ 0.000020 U mg/L 1 0.000020 0.000050 9GO5004 EPA 8081E 07/10/19 14:04 JJB Toxaphene[8001-35-2]^ 0.00048 U mg/L 1 0.00048 0.00050 9GO5004 EPA 8081E 07/10/19 14:04 JJB Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 2,4,5,E-TCMX 0.0038 1 0.00500 76 % 36-142 9GO5004 EPA 6061E 0711011914:04 JJB Decachlorobipheny/ 0.0040 1 0.00500 81 % 34-159 9GO5004 EPA 8061B 0711011914:04 JJB TCLP Herbicides by GC ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 2,4,5-TP (Silvex) [93-72-1]^ 0.00044 U mg/L 1 0.00044 0.00050 9GO2035 EPA 8151A 07/08/19 15:03 RGG 2,4-D [94-75-7]^ 0.00027 U mg/L 1 0.00027 0.00050 9GO2035 EPA 8151A 07/08/19 15:03 RGG Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes 2,4-DCAA 0.0078 1 0.0100 78 % 37-134 9GO2035 EPA 8151A 0710811915:03 RGG TCLP Metals by 6000/7000 Series Methods ^ - ENCO Orlando Certified analyte [NC 424] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Mercury[7439-97-6]^ 0.000230 U mg/L 1 0.000230 0.00200 9GO5017 EPA 7470A 07/08/19 09:31 CRG Classical Chemistry Parameters ^ - ENCO Orlando Certified analyte [NC 424] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes pHA 7.2 pH Units 1 1.0 1.0 9GO5011 EPA 9040C 07/05/19 10:58 CSB Q-01 Reactive Cyanide [57-12-5] 250 U mg/L 1 250 9GO8014 3W-846 Ch.7 Sec.: 07/10/19 11:38 CSB Reactive Sulfide [57-12-5] 500 U mg/L 1 500 9GO8013 3W-846 Ch.7 Sec.: 07/10/19 14:22 CSB Temperature for pH (deg. Q 23 pH Units 1 9GO5011 EPA 9040C 07/05/19 10:58 CSB Q-01 TCLP Metals by 6000/7000 Series Methods ^ - ENCO Jacksonville certified analyte [NC 442] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Arsenic[7440-38-2]^ 0.200 U mg/L 1 0.200 0.500 9G10003 EPA 6010D 07/11/19 13:33 ACV Barium [7440-39-3]A 0.272 mg/L 1 0.0500 0.250 9G10003 EPA 6010D 07/11/19 13:33 ACV Cadmium [7440-43-9]1 0.0112 U mg/L 1 0.0112 0.0500 9G10003 EPA 6010D 07/11/19 13:33 ACV Chromium [7440-47-3]1 0.0450 U mg/L 1 0.0450 0.250 9G10003 EPA 6010D 07/11/19 13:33 ACV Lead [7439-92-1]^ 0.0950 U mg/L 1 0.0950 0.250 9G10003 EPA 6010D 07/11/19 13:33 ACV Selenium [7782-49-2]1 0.250 U mg/L 1 0.250 1.00 9G10003 EPA 6010D 07/11/19 13:33 ACV Silver[7440-22-4]^ 0.0185 U mg/L 1 0.0185 0.250 9G10003 EPA 6010D 07/11/19 13:33 ACV FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 27 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-1 Lab Sample ID:CC10937-01 Received: 06/28/19 14:05 Matrix: Waste Water Sampled: 06/28/19 10:30 Work Order: CC10937 Project: City of Lumberton Sampled By:Jordan Davis Classical Chemistry Parameters Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Flashpoint > 200 OF 1 9GO8010 EPA 1010A 07/10/19 14:26 SMA Description: WW-1 Lab Sample ID:CC10937-02 Received: 06/28/19 14:05 Matrix: Waste Water Sampled: 06/28/19 10:30 Work Order: CC10937 Project: City of Lumberton Sampled By:Jordan Davis (Metals by EPA 200 Series Methods ^ - ENCO Cary cediFed analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Aluminum [7429-90-5]^ 572 mg/kg 10 0.420 1.00 9GO1004 EPA 200.7 07/02/19 10:04 JDH Arsenic[7440-38-2]^ 0.0760 U mg/kg 10 0.0760 0.100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Cadmium [7440-43-9]^ 0.00753 J mg/kg 10 0.00360 0.0100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Calcium [7440-70-2]^ 287 mg/kg 10 0.390 1.00 9GO1004 EPA 200.7 07/02/19 10:04 JDH Copper[7440-50-8]^ 5.88 mg/kg 10 0.0160 0.100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Lead [7439-92-1]^ 0.526 mg/kg 10 0.0310 0.100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Magnesium [7439-95-4]^ 47.4 mg/kg 10 0.290 1.00 9GO1004 EPA 200.7 07/02/19 10:04 JDH Mercury [7439-97-6]^ 0.00548 mg/kg 10 0.00150 0.00200 9GO1023 EPA 245.1 07/05/19 10:50 RLF Molybdenum [7439-98-7]^ 0.136 mg/kg 10 0.0250 0.100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Nickel[7440-02-O]^ 0.684 mg/kg 10 0.0220 0.100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Potassium [7440-09-7]^ 81.8 mg/kg 10 1.50 5.00 9GO1004 EPA 200.7 07/02/19 10:04 JDH Selenium [7782-49-2]^ 0.0620 U mg/kg 10 0.0620 0.100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Sodium [7440-23-5]^ 429 mg/kg 10 4.00 5.00 9GO1004 EPA 200.7 07/02/19 10:04 JDH Zinc[7440-66-6]^ 14.6 mg/kg 10 0.0440 0.100 9GO1004 EPA 200.7 07/02/19 10:04 JDH Classical Chemistry Parameters ^ - ENCO Cary cediFed analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Ammonia as N [7664-41-7]^ 110 D mg/kg 90 4.0 9.0 9GO8023 EPA 350.1 07/09/19 09:38 MKS Nitrate as N [14797-55-8]^ 0.025 U mg/kg 1 0.025 0.10 9HO2031 EPA 353.2 07/02/19 11:18 ALT Nitrate/Nitrite as IN 0.12 mg/kg 1 0.041 0.10 9GO2017 EPA 353.2 07/02/19 11:18 MKS Nitrite as N [14797-65-0]^ 0.12 mg/kg 1 0.017 0.10 91`28026 EPA 353.2 06/28/19 17:16 NMN pH^ 7.0 pH Units 1 1.0 1.0 9GO9006 EPA 9040C 07/09/19 09:31 LBG Q-01 Phosphorus [7723-14-O]^ 130 D mg/kg 50 1.2 5.0 9GO1016 EPA 365.4 07/05/19 18:00 NMN Sodium Adsorption Ratio 6.17 [blank] 1 9GO1004 CSU Method 07/02/19 13:48 JDH Temperature for pH (deg. C) 22 pH Units 1 9GO9006 EPA 9040C 07/09/19 09:31 LBG Q-01 Total Kjeldahl Nitrogen^ 610 D mg/kg 100 26 48 9GO1015 EPA 351.2 07/05/19 18:30 NMN Total Solids^ 2.5 % by Volume 1 0.0050 0.0050 9GO3035 SM 254OB-2011 07/03/19 20:34 JOC FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 27 QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9GO1004 - EPA 3005A 0Nk"q09 www.encolabs.com Blank (9G01004-BLK3) Prepared: 07/01/2019 08:18 Analyzed: 07/02/2019 09:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Aluminum 0.0420 U 0.100 mg/kg Arsenic 0.00760 U 0.0100 mg/kg Cadmium 0.000360 U 0.00100 mg/kg Calcium 0.0390 U 0.100 mg/kg Copper 0.00160 U 0.0100 mg/kg Lead 0.00310 U 0.0100 mg/kg Magnesium 0.0290 U 0.100 mg/kg Molybdenum 0.00250 U 0.0100 mg/kg Nickel 0.00220 U 0.0100 mg/kg Potassium 0.150 U 0.500 mg/kg Selenium 0.00620 U 0.0100 mg/kg Sodium 0.400 U 0.500 mg/kg Zinc 0.00440 U 0.0100 mg/kg LCS (9G03004-BSI) Prepared: 07/01/2019 08:18 Analyzed: 07/02/2019 09:52 Spike Source %REC RPD Analvte Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes Aluminum 2.04 0.100 mg/kg 2.00 102 85-115 Arsenic 0.203 0.0100 mg/kg 0.200 102 85-115 Cadmium 0.0206 0.00100 mg/kg 0.0200 103 85-115 Calcium 2.03 0.100 mg/kg 2.00 102 85-115 Copper 0.196 0.0100 mg/kg 0.200 98 85-115 Lead 0.202 0.0100 mg/kg 0.200 101 85-115 Magnesium 2.13 0.100 mg/kg 2.00 106 85-115 Molybdenum 0.198 0.0100 mg/kg 0.200 99 85-115 Nickel 0.202 0.0100 mg/kg 0.200 101 85-115 Potassium 10.1 0.500 mg/kg 10.0 101 85-115 Selenium 0.202 0.0100 mg/kg 0.200 101 85-115 Sodium 10.3 0.500 mg/kg 10.0 103 85-115 Zinc 0.209 0.0100 mg/kg 0.200 104 85-115 Matrix Spike (9G03004-MS1) Prepared: 07/01/2019 08:18 Analyzed: 07/02/2019 09:55 Source: CC09943-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Lima Notes Aluminum 2.17 0.100 mg/kg 2.00 0.0420 U 109 70-130 Arsenic 0.194 0.0100 mg/kg 0.200 0.00760 U 97 70-130 Cadmium 0.0198 0.00100 mg/kg 0.0200 0.000360 U 99 70-130 Calcium 113 0.100 mg/kg 2.00 113 NR 70-130 QM-07 Copper 0.205 0.0100 mg/kg 0.200 0.00160 U 102 70-130 Lead 0.209 0.0100 mg/kg 0.200 0.00310 U 104 70-130 Magnesium 45.9 0.100 mg/kg 2.00 44.4 76 70-130 Molybdenum 0.207 0.0100 mg/kg 0.200 0.00428 101 70-130 Nickel 0.222 0.0100 mg/kg 0.200 0.0108 105 70-130 Potassium 15.4 0.500 mg/kg 10.0 4.58 108 70-130 Selenium 0.193 0.0100 mg/kg 0.200 0.00620 U 96 70-130 Sodium 36.5 0.500 mg/kg 10.0 25.8 107 70-130 Zinc 0.230 0.0100 mg/kg 0.200 0.0148 108 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 27 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9G01004 - EPA 3005A - Continued Matrix Spike Dup (9G01004-MSD3) Prepared: 07/01/2019 08:18 Analyzed: 07/02/2019 09:57 Source: CC09943-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Aluminum 2.21 0.100 mg/kg 2.00 0.0420 U 111 70-130 2 30 Arsenic 0.190 0.0100 mg/kg 0.200 0.00760 U 95 70-130 2 30 Cadmium 0.0202 0.00100 mg/kg 0.0200 0.000360 U 101 70-130 2 30 Calcium 115 0.100 mg/kg 2.00 113 77 70-130 1 30 Copper 0.207 0.0100 mg/kg 0.200 0.00160 U 103 70-130 0.9 30 Lead 0.208 0.0100 mg/kg 0.200 0.00310 U 104 70-130 0.003 30 Magnesium 46.3 0.100 mg/kg 2.00 44.4 96 70-130 0.8 30 Molybdenum 0.209 0.0100 mg/kg 0.200 0.00428 103 70-130 1 30 Nickel 0.224 0.0100 mg/kg 0.200 0.0108 107 70-130 1 30 Potassium 15.5 0.500 mg/kg 10.0 4.58 109 70-130 0.3 30 Selenium 0.191 0.0100 mg/kg 0.200 0.00620 U 96 70-130 1 30 Sodium 36.6 0.500 mg/kg 10.0 25.8 107 70-130 0.2 30 Zinc 0.232 0.0100 mg/kg 0.200 0.0148 109 70-130 0.7 30 Post Spike (9G03004-PS1) Prepared: 07/01/2019 08:18 Analyzed: 07/02/2019 09:59 Source: CC09943-02 Spike Source %REC RPD Awe Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes Aluminum 2.15 0.100 mg/L 2.00 -0.0124 108 80-120 Arsenic 0.187 0.0100 mg/L 0.200 -0.0175 94 80-120 Cadmium 0.0199 0.00100 mg/L 0.0200 -0.00100 99 80-120 Calcium 117 0.100 mg/L 2.00 113 192 80-120 QM-08 Copper 0.201 0.0100 mg/L 0.200 -0.000923 100 80-120 Lead 0.210 0.0100 mg/L 0.200 0.00161 104 80-120 Magnesium 47.3 0.100 mg/L 2.00 44.4 144 80-120 QM-08 Molybdenum 0.208 0.0100 mg/L 0.200 0.00428 102 80-120 Nickel 0.223 0.0100 mg/L 0.200 0.0108 106 80-120 Potassium 15.4 0.500 mg/L 10.0 4.58 108 80-120 Selenium 0.192 0.0100 mg/L 0.200 -0.0362 96 80-120 Sodium 36.9 0.500 mg/L 10.0 25.8 110 80-120 Zinc 0.233 0.0100 mg/L 0.200 0.0148 109 80-120 Batch 9GO1023 - EPA 245.1 Blank (9G01023-BLK3) Prepared: 07/01/2019 10:18 Analyzed: 07/02/2019 13:53 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.000150 U 0.000200 mg/kg LCS (9G01023-BSI) Prepared: 07/01/2019 10:18 Analyzed: 07/02/2019 13:56 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00536 0.000200 mg/kg 0.00500 107 85-115 Matrix Spike (9G03023-MS1) Prepared: 07/01/2019 10:18 Analyzed: 07/02/2019 14:01 Source: CC09943-02 Spike Source %REC RPD Analvte Result Flaq PQL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00497 0.000200 mg/kg 0.00500 0.000150 U 99 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 27 QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9G01023 - EPA 245.1 - Continued (� �Eo www.encolabs.com Matrix Spike Dup (9G01023-MSD3) Prepared: 07/01/2019 10:18 Analyzed: 07/02/2019 14:03 Source: CC09943-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00521 0.000200 mg/kg 0.00500 0.000150 U 104 70-130 5 30 Post Spike (9G03023-PSI) Prepared: 07/01/2019 10:18 Analyzed: 07/02/2019 14:06 Source: CC09943-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.92 0.200 ug/L 5.00 -0.230 118 75-125 Classical Chemistry Parameters - Quality Control Batch 9F28026 - NO PREP Blank (9F28026-BLKi) Prepared: 06/28/2019 12:56 Analyzed: 06/28/2019 14:03 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/kg LCS (9F28026-BSI) Prepared: 06/28/2019 12:56 Analyzed: 06/28/2019 13:56 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.98 0.10 mg/L 1.00 98 90-110 Matrix Spike (9F28026-MS3) Prepared: 06/28/2019 12:56 Analyzed: 06/28/2019 14:05 Source: CC09631-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.1 0.10 mg/kg 1.00 0.017 U 107 90-110 Matrix Spike (9F28026-MS2) Prepared: 06/28/2019 12:56 Analyzed: 06/28/2019 17:12 Source: CC09945-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/kg 1.00 0.017 U 103 90-110 Matrix Spike Dup (9F28026-MSD3) Prepared: 06/28/2019 12:56 Analyzed: 06/28/2019 14:06 Source: CC09631-02 Analvte Nitrite as N Batch 9G01004 - EPA 3005A Result Flag POL 1.0 0.10 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes mg/kg 1.00 0.017 U 104 90-110 3 10 Blank (9G03004-BLK3) Prepared: 07/01/2019 08:18 Analyzed: 07/02/2019 13:49 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Sodium Adsorption Ratio 0.00 U [blank] Batch 9G01015 - Same Blank (9G03015-BLK3) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 13:48 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9G01015 - Same - Continued Blank (9G03015-BLK1) Continued Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 13:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 0.26 U 0.48 mg/kg Blank (9G03015-BLK2) Prepared: 07/01/2019 12:15 Analyzed: 07/05/2019 17:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 0.26 U 0.48 mg/kg LCS (9G01015-BS1) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 14:20 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 12 0.48 mg/kg 12.1 103 90-110 LCS (9G01015-BS2) Prepared: 07/01/2019 12:15 Analyzed: 07/05/2019 17:05 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 12 0.48 mg/kg 12.1 100 90-110 Matrix Spike (9G03015-MS3) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 14:23 Source: CC07425-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 48 D 2.4 mg/kg 4.85 44 77 90-110 QM-07 Matrix Spike (9G01015-MS2) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 14:28 Source: CC06722-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 41 D 2.4 mg/kg 4.85 40 33 90-110 QM-07 Matrix Spike Dup (9Go1015-MSD3) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 14:25 Source: CC07425-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 50 D 2.4 mg/kg 4.85 44 124 90-110 5 10 QM-07 Batch 9G01016 - Same Blank (9G03016-BLK3) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 16:41 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 0.030 3 0.10 mg/kg Blank (9G01016-BLK2) Prepared: 07/01/2019 12:15 Analyzed: 07/05/2019 17:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 0.025 J 0.10 mg/kg LCS (9G01016-BS1) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 16:43 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9GO1016 - Same - Continued LCS (9G01016-BS3) Continued Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 16:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 1.5 0.10 mg/kg 1.60 96 80-120 LCS (9G03016-BS2) Prepared: 07/01/2019 12:15 Analyzed: 07/05/2019 17:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 1.6 0.10 mg/kg 1.60 97 80-120 Matrix Spike (9G03016-MSS) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 16:45 Source: CC07425-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 21 D 1.0 mg/kg 0.640 21 96 80-120 Matrix Spike Dup (9Go1016-MSD1) Prepared: 07/01/2019 12:15 Analyzed: 07/03/2019 16:47 Source: CC07425-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Phosphorus 21 D 1.0 mg/kg 0.640 21 85 80-120 0.3 25 Batch 9GO2017 - NO PREP Blank (9G02017-BLK3) Prepared: 07/02/2019 10:26 Analyzed: 07/02/2019 10:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/kg LCS (9G02017-BS1) Prepared: 07/02/2019 10:28 Analyzed: 07/02/2019 10:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 1.25 103 90-110 Matrix Spike (9G02017-MS1) Prepared: 07/02/2019 12:47 Analyzed: 07/02/2019 12:47 Source: CC09004-01RE1 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 110 5.0 mg/kg 25.0 87 110 90-110 Matrix Spike (9G02017-MS2) Prepared: 07/02/2019 10:41 Analyzed: 07/02/2019 10:41 Source: CC09631-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 39 2.0 mg/kg 10.0 28 105 90-110 Matrix Spike Dup (9G02017-MSDI) Prepared: 07/02/2019 12:48 Analyzed: 07/02/2019 12:48 Source: CC09004-01RE1 Analvte Nitrate/Nitrite as N Batch 9GO2042 - NO PREP Spike Source %REC Result Flaq POL Units Level Result %REC Limits RPD 120 5.0 mg/kg 25.0 87 151 90-110 8 RPD Limit Notes 10 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9G02042 - NO PREP - Continued Blank (9G02042-BLK1) Prepared: 07/02/2019 15:23 Analyzed: 07/02/2019 15:23 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.045 U 0.10 mg/kg LCS (9G02042-BSI) Prepared: 07/02/2019 15:25 Analyzed: 07/02/2019 15:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.96 0.10 mg/L 1.01 95 90-110 Matrix Spike (9G02042-MSS) Prepared: 07/02/2019 15:28 Analyzed: 07/02/2019 15:28 Source: CC09025-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 2.2 0.50 mg/kg 2.02 0.22 U 108 90-110 Matrix Spike (9G02042-MS2) Prepared: 07/02/2019 15:34 Analyzed: 07/02/2019 15:34 Source: CC09656-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.36 0.10 mg/kg 0.393 0.045 U 92 90-110 Matrix Spike Dup (9G02042-MSD1) Prepared: 07/02/2019 15:30 Analyzed: 07/02/2019 15:30 Source: CC09025-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 2.2 0.50 mg/kg 2.02 0.22 U 109 90-110 0.6 10 Batch 9G03035 - NO PREP Blank (9G03035-BLK1) Prepared & Analyzed: 07/03/2019 20:34 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 0.0050 U 0.0050 % by Volume LCS (9G03035-BS3) Prepared & Analyzed: 07/03/2019 20:34 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 1100 50 mg/L 1100 100 80-120 Duplicate (9G03035-DUPl) Prepared & Analyzed: 07/03/2019 20:34 Source: CC10133-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 0.21 0.0050 % by Volume 0.21 0.2 20 Batch 9G08023 - NO PREP Blank (9G08023-BLK1) Prepared: 07/08/2019 15:51 Analyzed: 07/08/2019 15:51 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.045 U 0.10 mg/kg FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 27 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9GO8023 - NO PREP - Continued (� �Eo www.encolabs.com LCS (9G08023-BS3) Prepared: 07/08/2019 15:53 Analyzed: 07/08/2019 15:53 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.95 0.10 mg/L 1.01 94 90-110 Matrix Spike (9G08023-MSS) Prepared: 07/08/2019 15:57 Analyzed: 07/08/2019 15:57 Source: CC09002-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.41 0.10 mg/kg 0.393 0.060 89 90-110 QM-07 Matrix Spike (9G08023-MS2) Prepared: 07/08/2019 16:02 Analyzed: 07/08/2019 16:02 Source: CC09004-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.47 0.10 mg/kg 0.393 0.11 92 90-110 Matrix Spike Dup (9G08023-MSD3) Prepared: 07/08/2019 15:58 Analyzed: 07/08/2019 15:58 Source: CC09002-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.42 0.10 mg/kg 0.393 0.060 91 90-110 2 10 Batch 9GO9006 - NO PREP LCS (9G09006-BSI) Prepared & Analyzed: 07/09/2019 09:31 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes pH 7.0 1.0 pH Units 7.01 99 99-101 Duplicate (9G09006-DUPS) Prepared & Analyzed: 07/09/2019 09:31 Source: CC10133-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes pH 8.5 1.0 pH Units 8.5 0.2 25 TCLP Volatile Organics by GCMS - Quality Control Batch 9G10012 - EPA 5030E MS Blank (9G10012-BLK1) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 10:43 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1-Dichloroethene 0.00094 U 0.0010 mg/L 1,2-Dichloroethane 0.00063 U 0.0010 mg/L 2-Butanone 0.0045 U 0.0050 mg/L Benzene 0.00071 U 0.0010 mg/L Carbon Tetrachloride 0.00094 U 0.0010 mg/L Chlorobenzene 0.00072 U 0.0010 mg/L Chloroform 0.00080 U 0.0010 mg/L Tetrachloroethene 0.00076 U 0.0010 mg/L Trichloroethene 0.00089 U 0.0010 mg/L Vinyl chloride 0.00071 U 0.0010 mg/L 4-Bromof/uorobenzene 0,057 mg/L 0.0500 114 41-142 Dibromof/uoromethane 0.060 mg/L 0.0500 121 53-146 RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Volatile Organics by GCMS - Quality Control Batch 9G10012 - EPA 5030E MS - Continued Blank (9G10012-BLK1) Continued Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 10:43 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Toluene-d8 0.054 mg/L 0.0500 108 41-146 Blank (9G10012-BLK3) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 13:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.094 UD 0.10 mg/L 1,2-Dichloroethane 0.063 UD 0.10 mg/L 2-Butanone 0.45 UD 0.50 mg/L Benzene 0.071 UD 0.10 mg/L Carbon Tetrachloride 0.094 UD 0.10 mg/L Chlorobenzene 0.072 UD 0.10 mg/L Chloroform 0.080 UD 0.10 mg/L Tetrachloroethene 0.076 UD 0.10 mg/L Trichloroethene 0.089 UD 0.10 mg/L Vinyl chloride 0.071 UD 0.10 mg/L 4-Bromofluorobenzene 0.053 mg/L 0.0500 105 41-142 Dibromofluoromethane 0,056 mg/L 0,0500 113 53-146 Toluene-d8 0.051 mg/L 0.0500 103 41-146 Blank (9G10012-BLK4) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 13:37 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.094 UD 0.10 mg/L 1,2-Dichloroethane 0.063 UD 0.10 mg/L 2-Butanone 0.45 UD 0.50 mg/L Benzene 0.071 UD 0.10 mg/L Carbon Tetrachloride 0.094 UD 0.10 mg/L Chlorobenzene 0.072 UD 0.10 mg/L Chloroform 0.080 UD 0.10 mg/L Tetrachloroethene 0.076 UD 0.10 mg/L Trichloroethene 0.089 UD 0.10 mg/L Vinyl chloride 0.071 UD 0.10 mg/L 4-Bromofluorobenzene 0.054 mg/L 0.0500 107 41-142 Dibromofluoromethane 0.056 mg/L 0.0500 112 53-146 Toluene-d8 0.050 mg/L 0.0500 101 41-146 Blank (9G10012-BLKS) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 14:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.094 UD 0.10 mg/L 1,2-Dichloroethane 0.063 UD 0.10 mg/L 2-Butanone 0.45 UD 0.50 mg/L Benzene 0.071 UD 0.10 mg/L Carbon Tetrachloride 0.094 UD 0.10 mg/L Chlorobenzene 0.072 UD 0.10 mg/L Chloroform 0.080 UD 0.10 mg/L Tetrachloroethene 0.076 UD 0.10 mg/L Trichloroethene 0.089 UD 0.10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Volatile Organics by GCMS - Quality Control Batch 9G10012 - EPA 5030E MS - Continued Blank (9G10012-BLKS) Continued Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 14:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Vinyl chloride 0.071 LID 0.10 mg/L 4-Bromofluorobenzene 0.053 m91L 0.0500 105 41-142 Dibromofluoromethane 0.055 m9/L 0.0500 111 53-146 Toluene-d8 0,050 m9/L 0,0500 100 41-146 Blank (9G10012-BLK6) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 16:02 Analvte Result Flao CQ Units 1,1-Dichloroethene 0.094 LID 0.10 mg/L 1,2-Dichloroethane 0.063 LID 0.10 mg/L 2-Butanone 0.45 LID 0.50 mg/L Benzene 0.071 LID 0.10 mg/L Carbon Tetrachloride 0.094 LID 0.10 mg/L Chlorobenzene 0.072 LID 0.10 mg/L Chloroform 0.080 LID 0.10 mg/L Tetrachloroethene 0.076 LID 0.10 mg/L Trichloroethene 0.089 LID 0.10 mg/L Vinyl chloride 0.071 LID 0.10 mg/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 0.053 m91L 0.0500 106 41-142 Dibromofluoromethane 0.057 m9/L 0.0500 114 53-146 Toluene-d8 0.051 m91L 0.0500 101 41-146 LCS (9G10012-BSI) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 08:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.018 0.0010 mg/L 0.0200 90 47-139 Benzene 0.014 0.0010 mg/L 0.0200 70 56-136 Chlorobenzene 0.015 0.0010 mg/L 0.0200 74 51-139 Trichloroethene 0.014 0.0010 mg/L 0.0200 71 62-135 4-Bromofluorobenzene 0.051 m91L 0.0500 102 41-142 Dibromofluoromethane 0.055 m9/L 0.0500 111 53-146 Toluene-d8 0.050 m91L 0.0500 100 41-146 Matrix Spike (9G30012-MSS) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 15:04 111 Source: AC04909-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.029 0.0010 mg/L 0.0200 0.00094 U 144 47-139 QM-07 Benzene 0.021 0.0010 mg/L 0.0200 0.00071 U 103 56-136 Chlorobenzene 0.021 0.0010 mg/L 0.0200 0.00072 U 106 51-139 Trichloroethene 0.021 0.0010 mg/L 0.0200 0.00089 U 105 62-135 4-Bromofluorobenzene 0.052 m9/L 0.0500 104 41-142 Dibromofluoromethane 0.056 m9/L 0.0500 112 53-146 Toluene-d8 0.049 m91L 0.0500 99 41-146 Matrix Spike Dup (9G30012-MSD1) Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 15:33 Source: AC04909-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Volatile Organics by GCMS - Quality Control Batch 9G10012 - EPA 5030E MS - Continued Matrix Spike Dup (9G30012-MSD3) Continued Prepared: 07/10/2019 00:00 Analyzed: 07/10/2019 15:33 Source: AC04909-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.029 0.0010 mg/L 0.0200 0.00094 U 146 47-139 16 QM-07 Benzene 0.021 0.0010 mg/L 0.0200 0.00071 U 106 56-136 14 Chlorobenzene 0.021 0.0010 mg/L 0.0200 0.00072 U 104 51-139 13 Trichloroethene 0.022 0.0010 mg/L 0.0200 0.00089 U 108 62-135 20 4-Bromofluorobenzene 0.052 m91L 0.0500 103 41-142 Dibromofluoromethane 0.057 mg/L 0.0500 114 53-146 Toluene-d8 0,050 m91L 0,0500 99 41-146 TCLP Semivolatile Organics by GCMS - Quality Control Batch 9G05024 - EPA 3510C MS Blank (9G05024-BLK3) Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 14:43 Analvte Result Flaq POL Units 1,4-Dichlorobenzene 0.0006 U 0.002 mg/L 2,4,5-Trichlorophenol 0.0008 U 0.002 mg/L 2,4,6-Trichlorophenol 0.001 U 0.002 mg/L 2,4-Dinitrotoluene 0.0006 U 0.002 mg/L 2-Methylphenol 0.0007 U 0.002 mg/L 3 & 4-Methylphenol 0.002 U 0.002 mg/L Hexachlorobenzene 0.0006 U 0.002 mg/L Hexachlorobutadiene 0.0008 U 0.002 mg/L Hexachloroethane 0.0006 U 0.002 mg/L Nitrobenzene 0.0006 U 0.002 mg/L Pentachlorophenol 0.002 U 0.002 mg/L Pyridine 0.0007 U 0.002 mg/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 2,4,6-Tribromophenol 0.034 m91L 0.0500 67 33-145 2-Fluorob/phenyl 0.037 m91L 0.0500 74 32-116 2-Fluorophenol 0.028 m91L 0.0500 55 11-100 Nitrobenzene-d5 0.028 m91L 0.0500 57 24-107 Phenol-d5 0.017 m91L 0.0500 34 10-100 Terphenyl-d14 0.041 m91L 0.0500 83 52-150 Blank (9G05024-BLK2) Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 15:15 Analvte Result Flaq POL Units 1,4-Dichlorobenzene 0.003 U 0.01 mg/L 2,4,5-Trichlorophenol 0.004 U 0.01 mg/L 2,4,6-Trichlorophenol 0.006 U 0.01 mg/L 2,4-Dinitrotoluene 0.003 U 0.01 mg/L 2-Methylphenol 0.004 U 0.01 mg/L 3 & 4-Methylphenol 0.008 U 0.01 mg/L Hexachlorobenzene 0.003 U 0.01 mg/L Hexachlorobutadiene 0.004 U 0.01 mg/L Hexachloroethane 0.003 U 0.01 mg/L Nitrobenzene 0.003 U 0.01 mg/L Pentachlorophenol 0.008 U 0.01 mg/L Pyridine 0.004 U 0.01 mg/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 27 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA TCLP Semivolatile Organics by GCMS - Quality Control Batch 9GO5024 - EPA 3510C MS - Continued Blank (9G05024-BLK2) Continued Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 15:15 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 2,4,6-Tribromophenol 0.16 m9/L 0.250 64 33-145 2-Fluorobiphenyl 0.18 m9/L 0.250 71 32-116 2-Fluorophenol 0.12 m9/L 0,250 49 11-100 Nitrobenzene-d5 0.13 m9/L 0.250 51 24-107 Phenohd5 0.079 m9/L 0.250 32 10-100 Terphenyl-d14 0.20 m9/L 0,250 80 52-150 Blank (9G05024-BLK3) Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 15:46 Analvte Result Flaa POL Units 1,4-Dichlorobenzene 0.003 U 0.01 mg/L 2,4,5-Trichlorophenol 0.004 U 0.01 mg/L 2,4,6-Trichlorophenol 0.006 U 0.01 mg/L 2,4-Dinitrotoluene 0.003 U 0.01 mg/L 2-Methylphenol 0.02 0.01 mg/L 3 & 4-Methylphenol 0.05 0.01 mg/L Hexachlorobenzene 0.003 U 0.01 mg/L Hexachlorobutadiene 0.004 U 0.01 mg/L Hexachloroethane 0.003 U 0.01 mg/L Nitrobenzene 0.003 U 0.01 mg/L Pentachlorophenol 0.008 U 0.01 mg/L Pyridine 0.004 U 0.01 mg/L Spike Source %REC RPD Level Result "/oREC Limits RPD Limit Notes 1-01 1-01 24,6-Tribromophenol 0,17 m9/L 0.250 68 33-145 2-Fluorobiphenyl 0.19 m9/L a250 77 32-116 2-Fluorophenol 0.12 m9/L 0,250 47 11-100 Nitrobenzene-d5 0.13 m9/L 0.250 51 24-107 Phenol-d5 0.078 m9/L 0.250 31 10-100 Terphenyl-d14 0.16 m9/L 0.250 65 52-150 LCS (9G05024-BS1) Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 16:17 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.04 0.002 mg/L 0.0500 70 10-101 Pentachlorophenol 0.02 0.002 mg/L 0.0500 43 5-139 2,4,6-Tribromophenol 0.036 m9/L 0.0500 71 33-145 2-Fluorobiphenyl a o47 m9/L a o500 93 32-116 2-Fluorophenol 0.032 m9/L a o500 64 11-100 Nitrobenzene-d5 0.031 m9/L 0.0500 61 24-107 Phenol-d5 0.021 m9/L a o500 43 10-100 Terphenyl-d14 0.048 m9/L ao500 95 52-150 Matrix Spike (9G05024-MS1) Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 17:50 Source: AC04868-01 Spike Source a/oREC RPD Analvte Result Flaq fQ Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.15 D 0.05 mg/L 0.250 0.02 U 62 10-101 R-01 Pentachlorophenol 0.12 D 0.05 mg/L 0.250 0.04 U 46 5-139 R-01 24,6-Tribromophenol 0.20 m9/L 0.250 81 33-145 R-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Semivolatile Organics by GCMS - Quality Control Batch 9G05024 - EPA 3510C MS - Continued Matrix Spike (9G05024-MSi) Continued Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 17:50 Source: AC04868-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 2-Fluorobiphenyl 0.21 m91L 0.250 83 32-116 R-01 2-Fluorophenol 0.13 m91L 0.250 53 11-100 R-01 Nitrobenzene-d5 0.13 m91L 0.250 52 24-107 R-01 Phenol-d5 0.11 m91L 0.250 43 10-100 R-01 Terphenyhd14 0.18 m91L 0.250 72 52-150 R-01 Matrix Spike Dup (9G05024-MSD1) Prepared: 07/05/2019 11:40 Analyzed: 07/10/2019 18:21 Source: AC04868-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.17 D 0.05 mg/L 0.250 0.02 U 70 10-101 12 18 R-01 Pentachlorophenol 0.09 D 0.05 mg/L 0.250 0.04 U 38 5-139 21 23 R-01 2,4,6-Tribromophenol 0.22 m91L 0.250 90 33-145 R-01 2-Fluorobiphenyl 0.21 m91L 0.250 85 32-116 R-01 2-Fluorophenol 0.16 m91L 0,250 65 11-100 R-01 Nitrobenzene-d5 0.18 m9/L 0.250 74 24-107 R-01 Phenol-d5 0.10 m91L 0.250 42 10-100 R-01 Terphenyl-d14 0.19 m91L 0.250 76 52-150 R-01 TCLP Pesticides by GC - Quality Control Batch 9G05004 - EPA 3510C Blank (9G05004-BLK3) Prepared: 07/05/2019 08:20 Analyzed: 07/10/2019 12:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chlordane (tech) 0.000072 U 0.00010 mg/L Endrin 2.8E-6 U 0.000010 mg/L gamma-BHC 4.2E-6 U 0.000010 mg/L Heptachlor 5.2E-6 U 0.000010 mg/L Heptachlor epoxide 3.6E-6 U 0.000010 mg/L Methoxychlor 4.0E-6 U 0.000010 mg/L Toxaphene 0.000096 U 0.00010 mg/L 2, 4,5, E-TCMX 0,00063 m91L 0,00100 63 38-142 Decachlorobiphenyl 0.00061 m91L 0.00100 61 34-159 Blank (9G05004-BLK2) Prepared: 07/05/2019 08:20 Analyzed: 07/10/2019 13:04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chlordane (tech) 0.00036 U 0.00050 mg/L Endrin 0.000014 U 0.000050 mg/L gamma-BHC 0.000021 U 0.000050 mg/L Heptachlor 0.000026 U 0.000050 mg/L Heptachlor epoxide 0.000018 U 0.000050 mg/L Methoxychlor 0.000020 U 0.000050 mg/L Toxaphene 0.00048 U 0.00050 mg/L 2,4,5,E-TCMX 0.0038 m91L 0.00500 77 38-142 Decachlorobiphenyl 0.0044 m91L 0.00500 88 34-159 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Pesticides by GC - Quality Control Batch 9GO5004 - EPA 3510C - Continued LCS (9G05004-BS3) Prepared: 07/05/2019 08:20 Analyzed: 07/10/2019 13:17 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Endrin 0.00069 0.000010 mg/L 0.00100 69 28-143 2,4,5,6-TCMX 0.00074 m91L 0.00100 74 38-142 Decachloroblphenyl 0.00074 m91L 0.00100 74 34-159 Matrix Spike (9G05004-MS1) Prepared: 07/05/2019 08:20 Analyzed: 07/10/2019 13:29 Source: CC10937-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Endrin 0.0043 0.000050 mg/L 0.00500 0.000014 U 86 28-143 2,4,5,E-TCMX 0.0056 m91L 0,00500 112 38-142 Decachlorobiphenyl 0.0036 m91L 0.00500 73 34-159 Matrix Spike Dup (9G05004-MSD1) Prepared: 07/05/2019 08:20 Analyzed: 07/10/2019 13:41 Source: CC10937-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Endrin 0.0040 0.000050 mg/L 0.00500 0.000014 U 80 28-143 7 22 2,4,5,E-TCMX 0.0048 m91L 0.00500 97 38-142 Decachlorobiphenyl 0.0042 m91L 0.00500 84 34-159 TCLP Herbicides by GC - Quality Control Batch 9GO2035 - EPA 3510C Blank (9G02035-BLK3) Prepared: 07/02/2019 16:00 Analyzed: 07/03/2019 18:10 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.000088 U 0.00010 mg/L 2,4-D 0.000054 U 0.00010 mg/L 2,4-DC4A[2C] 0.0024 m91L 0.00200 118 37-134 Blank (9G02035-BLK2) Prepared: 07/02/2019 16:00 Analyzed: 07/03/2019 19:01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.00044 U 0.00050 mg/L 2,4-D 0.00027 U 0.00050 mg/L 2, 4-DCAA 0.012 m91L 0.0100 118 37-134 Blank (9G02035-BLK3) Prepared: 07/03/2019 15:50 Analyzed: 07/08/2019 13:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.000088 U 0.00010 mg/L 2,4-D 0.000054 U 0.00010 mg/L 2,4-DCAA[2C] 0.0021 m91L 0.00200 106 37-134 Blank (9G02035-BLK4) Prepared: 07/03/2019 15:50 Analyzed: 07/08/2019 14:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 27 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA TCLP Herbicides by GC - Quality Control Batch 9G02035 - EPA 3510C - Continued Blank (9G02035-BLK4) Continued Prepared: 07/03/2019 15:50 Analyzed: 07/08/2019 14:12 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.000088 U 0.00010 mg/L 2,4-D 0.000054 U 0.00010 mg/L 2,4-DC4A[2C] 0.0019 m91L 0.00200 94 37-134 LCS (9G02035-BS3) Prepared: 07/02/2019 16:00 Analyzed: 07/03/2019 19:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.0017 0.00010 mg/L 0.00200 85 24-135 2,4-D 0.0020 0.00010 mg/L 0.00200 101 20-134 2,4-DC4A 0.0026 m91L 0.00200 129 37-134 Matrix Spike (9G02035-MS1) Prepared: 07/02/2019 16:00 Analyzed: 07/03/2019 19:52 Source: AC04894-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Limit Notes 2,4,5-TP (Silvex) 0.0021 0.00010 mg/L 0.00202 0.000089 U 106 24-135 2,4-D 0.0019 0.00010 mg/L 0.00202 0.000055 U 96 20-134 2, 4-DCAA 0.0025 m91L 0.00202 122 37-134 Matrix Spike (9G02035-MS2) Prepared: 07/02/2019 16:00 Analyzed: 07/03/2019 23:46 Source: AC04762-02 Spike Source %REC RPD Awe Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.0096 0.00050 mg/L 0.0100 0.00044 U 97 24-135 2,4-D 0.0092 0.00050 mg/L 0.0100 0.00027 U 92 20-134 2 4-DC4A [2CJ 0.012 m9/L 0.0100 124 37-134 Matrix Spike Dup (9G02035-MSD3) Prepared: 07/02/2019 16:00 Analyzed: 07/03/2019 20:18 Source: AC04894-02 Spike Source %REC RPD Analvte Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.0019 0.00010 mg/L 0.00204 0.000090 U 96 24-135 9 19 2,4-D 0.0018 0.00010 mg/L 0.00204 0.000055 U 90 20-134 6 19 2, 4-DCAA 0.0027 m91L 0.00204 133 37-134 TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 9G05017 - EPA 7470A Blank (9G05017-BLK1) Prepared: 07/05/2019 10:52 Analyzed: 07/08/2019 08:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Mma Notes Mercury 2.30E-5 U 0.000200 mg/L Blank (9G05017-BLK2) Prepared: 07/05/2019 10:52 Analyzed: 07/08/2019 08:36 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.000230 U 0.00200 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 9G05017 - EPA 7470A - Continued Blank (9G05017-BLK3) Prepared: 07/05/2019 10:52 Analyzed: 07/08/2019 08:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.000230 U 0.00200 mg/L LCS (9G05017-BSI) Prepared: 07/05/2019 10:52 Analyzed: 07/08/2019 08:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00503 0.000200 mg/L 0.00500 101 80-120 Matrix Spike (9G05017-MSS) Prepared: 07/05/2019 10:52 Analyzed: 07/08/2019 08:55 Source: AC04800-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.0494 0.00200 mg/L 0.0500 0.000384 98 75-125 Matrix Spike Dup (9G05017-MSD1) Prepared: 07/05/2019 10:52 Analyzed: 07/08/2019 09:37 Source: AC04800-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.0474 0.00200 mg/L 0.0500 0.000384 94 75-125 4 20 Matrix Spike Dup (9G05017-MSD2) Prepared: 07/05/2019 10:52 Analyzed: 07/08/2019 08:58 Source: AC04800-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.0275 0.00200 mg/L 0.0500 0.000384 54 75-125 57 20 QM-07, QM-11 Classical Chemistry Parameters - Quality Control Batch 9G05011 - NO PREP LCS (9G05031-BSI) Prepared & Analyzed: 07/05/2019 10:58 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes pH 7.0 1.0 pH Units 7.00 100 99-102 Duplicate (9G05011-DUPS) Prepared & Analyzed: 07/05/2019 10:58 Source: AC04891-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes pH 6.1 1.0 pH Units 6.1 0.08 10 Q-01 Temperature for pH (deg. Q 23 pH Units 24 2 200 Q-01 Batch 94G08013 - NO PREP Blank (9G08013-BLK3) Prepared: 07/09/2019 14:00 Analyzed: 07/10/2019 14:22 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Reactive Sulfide 500 U 500 mg/L LCS (9G08013-BS1) Prepared: 07/09/2019 14:00 Analyzed: 07/10/2019 14:22 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9GO8013 - NO PREP - Continued LCS (9G08013-BS3) Continued Prepared: 07/09/2019 14:00 Analyzed: 07/10/2019 14:22 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Reactive Sulfide 280 U 500 mg/L 249 113 50-150 Duplicate (9G08013-DUPl) Prepared: 07/09/2019 14:00 Analyzed: 07/10/2019 14:22 Source: CC10937-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Reactive Sulfide 500 U 500 mg/L 500 U 30 Batch 9GO8014 - NO PREP Blank (9G08014-BLK1) Prepared: 07/09/2019 14:00 Analyzed: 07/10/2019 11:38 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Reactive Cyanide 250 U 250 mg/L LCS (9G08014-BS3) Prepared: 07/09/2019 14:00 Analyzed: 07/10/2019 11:38 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Reactive Cyanide 36 LID 6200 mg/L 99.9 36 22-100 Duplicate (9G08014-DUPl) Prepared: 07/09/2019 14:00 Analyzed: 07/10/2019 11:38 Source: CC10937-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Reactive Cyanide 250 U 250 mg/L 250 U 30 TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 9G10003 - EPA 3010A Blank (9G10003-BLK3) Prepared: 07/10/2019 09:06 Analyzed: 07/11/2019 13:08 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.200 U 0.500 mg/L Barium 0.0587 1 0.250 mg/L Cadmium 0.0112 U 0.0500 mg/L Chromium 0.0450 U 0.250 mg/L Lead 0.0950 U 0.250 mg/L Selenium 0.250 U 1.00 mg/L Silver 0.0185 U 0.250 mg/L Blank (9G10003-BLK2) Prepared: 07/10/2019 09:06 Analyzed: 07/11/2019 13:10 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.200 U 0.500 mg/L Barium 0.0500 U 0.250 mg/L Cadmium 0.0112 U 0.0500 mg/L Chromium 0.0450 U 0.250 mg/L Lead 0.0950 U 0.250 mg/L Selenium 0.250 U 1.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 9G10003 - EPA 3010A - Continued Blank (9G10003-BLK2) Continued Prepared: 07/10/2019 09:06 Analyzed: 07/11/2019 13:10 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Silver 0.0185 U 0.250 mg/L Blank (9G10003-BLK3) Prepared: 07/10/2019 09:06 Analyzed: 07/11/2019 13:17 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.200 U 0.500 mg/L Barium 0.0500 U 0.250 mg/L Cadmium 0.0112 U 0.0500 mg/L Chromium 0.0450 U 0.250 mg/L Lead 0.0950 U 0.250 mg/L Selenium 0.250 U 1.00 mg/L Silver 0.0185 U 0.250 mg/L LCS (9G10003-BS1) Prepared: 07/10/2019 09:06 Analyzed: 07/11/2019 13:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 12.9 0.500 mg/L 12.5 103 80-120 Barium 12.6 0.250 mg/L 12.4 101 80-120 Cadmium 1.26 0.0500 mg/L 1.24 101 80-120 Chromium 12.6 0.250 mg/L 12.5 101 80-120 Lead 12.9 0.250 mg/L 12.5 103 80-120 Selenium 12.3 1.00 mg/L 12.5 98 80-120 Silver 2.44 0.250 mg/L 2.50 98 80-120 Matrix Spike (9G10003-MS1) Prepared: 07/10/2019 09:06 Analyzed: 07/11/2019 13:21 Source: BCO2614-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Arsenic 13.2 0.500 mg/L 12.5 0.200 U 106 75-125 Barium 13.0 0.250 mg/L 12.4 0.251 103 75-125 Cadmium 1.29 0.0500 mg/L 1.24 0.0112 U 104 75-125 Chromium 12.7 0.250 mg/L 12.5 0.0450 U 102 75-125 Lead 13.1 0.250 mg/L 12.5 0.0950 U 105 75-125 Selenium 12.5 1.00 mg/L 12.5 0.250 U 100 75-125 Silver 2.45 0.250 mg/L 2.50 0.0185 U 98 75-125 Matrix Spike Dup (9G10003-MSD1) Prepared: 07/10/2019 09:06 Analyzed: 07/11/2019 13:23 Source: BCO2614-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 13.2 0.500 mg/L 12.5 0.200 U 105 75-125 0.2 20 Barium 13.0 0.250 mg/L 12.4 0.251 103 75-125 0.2 20 Cadmium 1.29 0.0500 mg/L 1.24 0.0112 U 103 75-125 0.3 20 Chromium 12.8 0.250 mg/L 12.5 0.0450 U 102 75-125 0.1 20 Lead 13.1 0.250 mg/L 12.5 0.0950 U 105 75-125 0.08 20 Selenium 12.6 1.00 mg/L 12.5 0.250 U 101 75-125 0.3 20 Silver 2.45 0.250 mg/L 2.50 0.0185 U 98 75-125 0.08 20 Classical Chemistry Parameters - Quality Control Batch 9GOB010 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 27 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 94G08010 - NO PREP - Continued LCS (9G08010-BS1) Prepared: 07/08/2019 11:04 Analyzed: 07/10/2019 14:26 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Flashpoint 81.0 OF 81.0 100 98-102 Duplicate (9G08010-DUPl) Prepared: 07/08/2019 11:04 Analyzed: 07/10/2019 14:26 Source: BCO2680-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Flashpoint < 60 U OF 59.0 1.68 5 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 27 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. 3-01 Result may be biased high due to positive results in the associated method blank at a concentration above the MDL and/or greater than one-half the MRL. Q-01 Analysis performed outside of method - specified holding time. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QS-OS Surrogate recovery biased low and outside control limits due to suspected matrix effects, as evidenced by sample behavior during sample preparation (emulsion formation, excessive foaming). R-01 The Reporting Limit for this analyte has been raised to account for matrix interference. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 27 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OE -CUSTODY RECORD www.encolabs.com CSN,C� 1p775 Central Port Dr. 481U Executive Park Court, Suite 111 102-A Woodwinds Industrial GI Orlando, FL 32824 Jacksonville, FL MIS-6069 Cary, NC 27511 (407) 825.5314 Fax (407) 850-6945 (904) 296-3007 Fax (904) 296-6210 (919) 467-3090 Fax (919) 467-3515 Page Of Client Name Hunt Environmental AssociMs (H0017) Project Number [none] Requested Analyses Requested Turnaround Times Note : Rush requests subject to acceptance by the facility Standard _ Expedited Due / 1 y� (D W CL M Q > W a.d �` Co r 0 N c� CL J (] m O co CL J 0 W A !� co a m Z ]C a x 8 $ to m n m M X z_ 1*! m !E fA � U r a: (n l_ � o �; N m o z(n Address 3330 Saddletree Road. Project NamelDesc City of Luinbe rton City/ST/Zp Lumberton NC 28360 ' PO # ! Billing Into i-ef (910) 738-5311 Fax Reporting Contact Jordan Davis Sam fer(s) Name, Affiliation (Print body Hunt JSai�/rfe) Signature Site Location / Time Zane Lab Workorder cc 10937 Preservation (See Codes) (Combine as necessary) item k Sample ID (Field Identilication) -)-j Colleclico� Collection -Msf Comp / Grab Matrix (see codes) Total 4 of Containers Sample Comments WW-1 I b 3Q aVV\ 6 611 ra WW 9 x x x x x x x 30 a01 & �-i ra b M 5 x x x —Total # of Containers Sample Kit Prepared By D lelTme ad By Rea�' Dat�me �w�n1q/� A Receiv t rme ✓ ' . Com a tslSpeciai Reportng Requirements ed By DatelTme Rece y atemme e Relinquished By Daternme Received By DateMme #'s & Tem on Receipt ,,11� • `'t � Condition n Receipt Acceptable Unacceptable Matrix: OW -Groundwater SO -Soil OW-Drfnking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: Mae H-HCl N-HNO3 S-H2SO4 NO-NaOH O-Olhor {delail in comments) Note : All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com 10775 Central Port Dr. 4610 Executive Park Courl, Suite 111 102-A Woodwinds Industrial Cr Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511 OEM— G) (4071 B26-5314 Fax (407) 850-6945 (904) 296-3007 Fax (904) 296-6210 (919) 467-3090 Fax (919) 467-3515 Page of Client Name Project Number Requested Analyses Requested Turnaround Hunt Environmental Associates (HU017) [none] Times Address Project NamefDasc p, Note: Rush requests subject to 3'3.30 Saddletree Road. City of Lumberton acceptance by the facii@y Gi IST/Zip PO 9 I Billing Info m CL r ulmberton, NC 28360 a- U Standard Tel Fax Reporting Contacl ❑ 4 (91 O) 738-5311 Jordan Davis < 0 to N a U py Expedited Samplers) Name, Affiliation (Print) BNlin Co tact d M 7 �JT(�► /(n � i� �,/ �ojy Hunt a 0CL Due 1 /i a a ISa er(s) Signature Site Location ITime Zone = U a Lab Workorder C F v CC 10937 Preservation (See Codes) {Combine as necessary) Collection Matrix Totals of Item r Sample ID (Field Identification) Collection Date Time Ccmp f Grah (see codes) Containers Sample Comments WW-1 WW 9 X X X X WW WW 5 <-- Total # of Containers Sample Kit Prepared By Date/Time Reluishad By DatarT;me Received By t irne GommenlslSpecial Reporting Requirements inquished By DatelTime ed alelTi e Relinquished By Date/Time Received By Oatefrime Cuoler a's & Temps on Receipt Condition Up�eceipt V Acceptable Unacceptable Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: Hoe H-HCI N-hNO3 S-H2SO4 NO-NaOH O-Other (detail in comments) Note All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist Sample Preservation Verification ENCO Cary Work Order: CC10937 Project: City of Lumberton Client: Hunt Environmental Associates (HU017) Project #: [none] Logged In: 28-Jun-19 15:30 Logged By: John C King j Preservation Check Performed By: Date/Time: U k � I CT S L u CC10937-01 s, Pres (pH) PH Checked / Date{i€me pH Adjusted Reagent Used/Comments :omments =: requirement ip Control Adjusted J 250mLP+ZnAc+NaOH >y Y ,/ N 1 NA Y/ NA K 250mLP+NaOH >12 Y/ N I NA Y N I NA CC10937-02 Cont Type Pies (pH) PH Checked / pH Adjusted DateMme Reagent Used/Comments Requirement in Control Adiusted A 500mLP+H2SO4 <2 Y 1 N / NA Y / t)/ NA E 250mLP+HNO3 <2 Y N / NA 1 N / NA Lp ZF f t k 6 5 U0 —J-z Vw Rea ent Name ID 1 A-�N u-3 -i� 2 Rea ent Name 1D 3 4 Reagent Name ID 5 6 pH Strip ID: _ PH Strips C8J0741 C!\ELMNTIPn, I«wru_r-ieservauonunecK.rpt Page 1 of 1 2�SENCO Laboratories 9g Accurate. Timely. Respousive. luuavative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, August 29, 2019 Hunt Environmental Associates (HU017) Attn: Jordan Davis 3330 Saddletree Road. Lumberton, NC 28360 RE: Laboratory Results for Project Number: [none], Project Name/Desc: City of Lumberton ENCO Workorder(s): CC13867 Dear Jordan Davis, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, August 20, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OUCLC'=-:�CA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 12 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: WW-2 Lab ID: CC13867-01 Sampled: 08/20/19 10:30 Received: 08/20/19 15:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) CSU Method NO PREP 05/15/22 08/22/19 13:41 08/26/19 13:26 EPA 200.7 Same 02/16/20 08/22/19 13:41 08/23/19 12:33 EPA 245.1 EPA 245.1 09/17/19 08/26/19 08:24 08/27/19 14:07 EPA 351.2 Same 09/17/19 08/22/19 11:34 08/26/19 13:40 EPA 353.2 NO PREP 08/22/19 10:30 08/21/19 17:27 08/21/19 17:27 EPA 353.2 [CALC] 08/22/19 10:30 08/28/19 13:54 08/28/19 13:54 EPA 353.2 NO PREP 09/17/19 08/28/19 13:54 08/28/19 13:54 EPA 9040C NO PREP 08/20/19 10:44 08/23/19 13:25 08/23/19 13:25 SM 254OB-2011 NO PREP 08/27/19 08/27/19 12:20 08/27/19 12:20 Client ID: WW-2 Lab ID: CC13867-01RE1 Sampled: 08/20/19 10:30 Received: 08/20/19 15:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 350.1 NO PREP 09/17/19 08/23/19 15:55 08/23/19 15:55 EPA 365.4 Same 09/17/19 08/22/19 11:34 08/26/19 18:46 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 12 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: WW-2 Lab ID: CC13867-01 Anala Results Flag MDL POLL Units Method Notes Aluminum - Total 128 D 0.420 1.00 mg/kg EPA 200.7 Arsenic - Total 0.0871 ID 0.0760 0.100 mg/kg EPA 200.7 Cadmium - Total 0.00825 ID 0.00360 0.0100 mg/kg EPA 200.7 Calcium - Total 225 D 0.390 1.00 mg/kg EPA 200.7 Copper- Total 2.19 D 0.0160 0.100 mg/kg EPA 200.7 Lead - Total 0.0765 ID 0.0310 0.100 mg/kg EPA 200.7 Magnesium - Total 43.1 D 0.290 1.00 mg/kg EPA 200.7 Mercury - Total 0.00586 0.000150 0.000200 mg/kg EPA 245.1 Molybdenum - Total 0.0284 ID 0.0250 0.100 mg/kg EPA 200.7 Nickel- Total 0.154 D 0.0220 0.100 mg/kg EPA 200.7 Nitrate/Nitrite as N 0.072 1 0.041 0.10 mg/kg EPA 353.2 Nitrite as N 0.061 1 0.017 0.10 mg/kg EPA 353.2 pH 7.1 1.0 1.0 pH Units EPA 9040C Q-01 Potassium - Total 74.7 D 1.50 5.00 mg/kg EPA 200.7 Sodium - Total 507 D 4.00 5.00 mg/kg EPA 200.7 Sodium Adsorption Ratio 8.09 [blank] CSU Method Temperature for pH (deg. C) 24 pH Units EPA 9040C Q-01 Total Kjeldahl Nitrogen 490 D 13 24 mg/kg EPA 351.2 Total Solids 2.0 0.0050 0.0050 % by Volume SM 2540B-2011 Zinc - Total 9.47 D 0.0440 0.100 mg/kg EPA 200.7 Client ID: WW-2 Lab ID: CC13867-01RE1 Anala Results Flag MDL POLL Units Method Notes Ammonia as N 6.4 D 0.22 0.50 mg/kg EPA 350.1 Phosphorus 270 D 12 50 mg/kg EPA 365.4 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 12 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-2 Lab Sample ID:CC13867-01 Received: 08/20/19 15:20 Matrix: Waste Water Sampled:08/20/19 10:30 Work Order: CC13867 Project: City of Lumberton Sampled By:Jordan Davis Metals by EPA 200 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL P L Batch Method Analyzed By Notes Aluminum [7429-90-5]^ 128 D mg/kg 10 0.420 1.00 91-122033 EPA 200.7 08/23/19 12:33 JDH Arsenic [7440-38-2]^ 0.0871 JD mg/kg 10 0.0760 0.100 91-122033 EPA 200.7 08/23/19 12:33 JDH Cadmium [7440-43-9]^ 0.00825 JD mg/kg 10 0.00360 0.0100 91-122033 EPA 200.7 08/23/19 12:33 JDH Calcium [7440-70-2]^ 225 D mg/kg 10 0.390 1.00 91-122033 EPA 200.7 08/23/19 12:33 JDH Copper[7440-50-8]^ 2.19 D mg/kg 10 0.0160 0.100 91-122033 EPA 200.7 08/23/19 12:33 JDH Lead [7439-92-1]^ 0.0765 JD mg/kg 10 0.0310 0.100 91-122033 EPA 200.7 08/23/19 12:33 JDH Magnesium [7439-95-4]^ 43.1 D mg/kg 10 0.290 1.00 91-122033 EPA 200.7 08/23/19 12:33 JDH Mercury [7439-97-6]^ 0.00586 mg/kg 1 0.000150 0.000200 91-126008 EPA 245.1 08/27/19 14:07 KAH Molybdenum [7439-98-7]^ 0.0284 JD mg/kg 10 0.0250 0.100 91-122033 EPA 200.7 08/23/19 12:33 JDH Nickel[7440-02-O]^ 0.154 D mg/kg 10 0.0220 0.100 91-122033 EPA 200.7 08/23/19 12:33 JDH Potassium [7440-09-7]1 74.7 D mg/kg 10 1.50 5.00 91-122033 EPA 200.7 08/23/19 12:33 JDH Selenium [7782-49-2]^ 0.0620 UD mg/kg 10 0.0620 0.100 91-122033 EPA 200.7 08/23/19 12:33 JDH Sodium [7440-23-5]^ 507 D mg/kg 10 4.00 5.00 91-122033 EPA 200.7 08/23/19 12:33 JDH Zinc[7440-66-6]^ 9.47 D mg/kg 10 0.0440 0.100 91-122033 EPA 200.7 08/23/19 12:33 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL P L Batch Method Analyzed By Notes Ammonia as N [7664-41-7]^ 6.4 D mg/kg 5 0.22 0.50 91-123028 EPA 350.1 08/23/19 15:55 NMN Nitrate as N [14797-55-8] 0.041 U mg/L 1 0.041 0.10 [CALC] EPA 353.2 08/28/19 13:54 NMN Nitrate/Nitrite as IN 0.072 J mg/kg 1 0.041 0.10 91-128017 EPA 353.2 08/28/19 13:54 NMN Nitrite as N [14797-65-0]^ 0.061 J mg/kg 1 0.017 0.10 91-121021 EPA 353.2 08/21/19 17:27 NMN pH 7.1 pH Units 1 1.0 1.0 91-123041 EPA 9040C 08/23/19 13:25 JAH Q-01 Phosphorus[7723-14-O]^ 270 D mg/kg 500 12 50 91-122014 EPA 365.4 08/26/19 18:46 NMN Sodium Adsorption Ratio 8.09 [blank] 1 91-122033 CSU Method 08/26/19 13:26 JDH Temperature for pH (deg. C) 24 pH Units 1 91-123041 EPA 9040C 08/23/19 13:25 JAH Q-01 Total Kjeldahl Nitrogen 490 D mg/kg 50 13 24 91-122012 EPA 351.2 08/26/19 13:40 NMN Total Solids^ 2.0 % by Volume 1 0.0050 0.0050 91-127015 SM 254OB-2011 08/27/19 12:20 JOC FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 12 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9H22033 - EPA 3005A Blank (9H22033-BLKi) Prepared: 08/22/2019 13:41 Analyzed: 08/23/2019 12:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Aluminum 0.0420 U 0.100 mg/kg Arsenic 0.00760 U 0.0100 mg/kg Cadmium 0.000360 U 0.00100 mg/kg Calcium 0.0390 U 0.100 mg/kg Copper 0.00160 U 0.0100 mg/kg Lead 0.00310 U 0.0100 mg/kg Magnesium 0.0290 U 0.100 mg/kg Molybdenum 0.00250 U 0.0100 mg/kg Nickel 0.00220 U 0.0100 mg/kg Potassium 0.150 U 0.500 mg/kg Selenium 0.00620 U 0.0100 mg/kg Sodium 0.400 U 0.500 mg/kg Zinc 0.00440 U 0.0100 mg/kg Blank (9H22033-BLK2) Prepared: 08/22/2019 13:41 Analyzed: 08/23/2019 12:03 Spike Source %REC RPD Analvte Result Flao POL Uni Level Result %REC Limits RPD Limit Notes Aluminum 0.0420 U 0.100 mg/kg Arsenic 0.00760 U 0.0100 mg/kg Cadmium 0.000360 U 0.00100 mg/kg Calcium 0.0390 U 0.100 mg/kg Copper 0.00160 U 0.0100 mg/kg Lead 0.00310 U 0.0100 mg/kg Magnesium 0.0290 U 0.100 mg/kg Molybdenum 0.00250 U 0.0100 mg/kg Nickel 0.00220 U 0.0100 mg/kg Potassium 0.150 U 0.500 mg/kg Selenium 0.00620 U 0.0100 mg/kg Sodium 0.400 U 0.500 mg/kg Zinc 0.00440 U 0.0100 mg/kg LCS (9H22033-BS1) Prepared: 08/22/2019 13:41 Analyzed: 08/23/2019 12:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Lima Notes Aluminum 1.95 0.100 mg/kg 2.00 97 85-115 Arsenic 0.195 0.0100 mg/kg 0.200 97 85-115 Cadmium 0.0195 0.00100 mg/kg 0.0200 98 85-115 Calcium 2.06 0.100 mg/kg 2.00 103 85-115 Copper 0.192 0.0100 mg/kg 0.200 96 85-115 Lead 0.193 0.0100 mg/kg 0.200 96 85-115 Magnesium 1.97 0.100 mg/kg 2.00 99 85-115 Molybdenum 0.189 0.0100 mg/kg 0.200 95 85-115 Nickel 0.195 0.0100 mg/kg 0.200 97 85-115 Potassium 9.78 0.500 mg/kg 10.0 98 85-115 Selenium 0.202 0.0100 mg/kg 0.200 101 85-115 Sodium 10.1 0.500 mg/kg 10.0 101 85-115 Zinc 0.202 0.0100 mg/kg 0.200 101 85-115 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 12 QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9H22033 - EPA 3005A - Continued 0Nk"q09 www.encolabs.com Matrix Spike (9H22033-MS3) Prepared: 08/22/2019 13:41 Analyzed: 08/23/2019 12:19 Source: CC09063-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result "/oREC Limits RPD Limit Notes Aluminum 1.95 0.100 mg/kg 2.00 0.0420 U 98 70-130 Arsenic 0.179 0.0100 mg/kg 0.200 0.00760 U 90 70-130 Cadmium 0.0179 0.00100 mg/kg 0.0200 0.000360 U 89 70-130 Calcium 126 0.100 mg/kg 2.00 127 NR 70-130 QM-07 Copper 0.196 0.0100 mg/kg 0.200 0.00160 U 98 70-130 Lead 0.192 0.0100 mg/kg 0.200 0.00310 U 96 70-130 Magnesium 19.7 0.100 mg/kg 2.00 18.0 85 70-130 Molybdenum 0.193 0.0100 mg/kg 0.200 0.00400 94 70-130 Nickel 0.190 0.0100 mg/kg 0.200 0.00220 U 95 70-130 Potassium 10.3 0.500 mg/kg 10.0 0.492 98 70-130 Selenium 0.189 0.0100 mg/kg 0.200 0.00620 U 94 70-130 Sodium 36.1 0.500 mg/kg 10.0 26.7 94 70-130 Zinc 0.263 0.0100 mg/kg 0.200 0.0785 92 70-130 Matrix Spike Dup (9H22033-MSD1) Prepared: 08/22/2019 13:41 Analyzed: 08/23/2019 12:22 Source: CC09063-01 Spike Source "/oREC RPD Awe Resul Flaa POL Uni Level Result %REC Limits RPD Limit Notes Aluminum 1.97 0.100 mg/kg 2.00 0.0420 U 99 70-130 1 30 Arsenic 0.177 0.0100 mg/kg 0.200 0.00760 U 89 70-130 1 30 Cadmium 0.0181 0.00100 mg/kg 0.0200 0.000360 U 90 70-130 1 30 Calcium 130 0.100 mg/kg 2.00 127 158 70-130 3 30 QM-07 Copper 0.201 0.0100 mg/kg 0.200 0.00160 U 100 70-130 2 30 Lead 0.195 0.0100 mg/kg 0.200 0.00310 U 98 70-130 2 30 Magnesium 20.1 0.100 mg/kg 2.00 18.0 104 70-130 2 30 Molybdenum 0.195 0.0100 mg/kg 0.200 0.00400 96 70-130 1 30 Nickel 0.195 0.0100 mg/kg 0.200 0.00220 U 97 70-130 3 30 Potassium 10.5 0.500 mg/kg 10.0 0.492 100 70-130 2 30 Selenium 0.191 0.0100 mg/kg 0.200 0.00620 U 95 70-130 0.9 30 Sodium 36.9 0.500 mg/kg 10.0 26.7 103 70-130 2 30 Zinc 0.268 0.0100 mg/kg 0.200 0.0785 95 70-130 2 30 Post Spike (9H22033-PS1) Prepared: 08/22/2019 13:41 Analyzed: 08/23/2019 12:24 Source: CC09063-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Limi Notes Aluminum 2.04 0.100 mg/L 2.00 -0.00477 102 80-120 Arsenic 0.182 0.0100 mg/L 0.200 -0.0189 91 80-120 Cadmium 0.0185 0.00100 mg/L 0.0200 -0.00121 93 80-120 Calcium 125 0.100 mg/L 2.00 127 NR 80-120 QM-08 Copper 0.197 0.0100 mg/L 0.200 0.000782 98 80-120 Lead 0.196 0.0100 mg/L 0.200 -0.00124 98 80-120 Magnesium 19.5 0.100 mg/L 2.00 18.0 76 80-120 QM-08 Molybdenum 0.196 0.0100 mg/L 0.200 0.00400 96 80-120 Nickel 0.202 0.0100 mg/L 0.200 0.00219 100 80-120 Potassium 10.7 0.500 mg/L 10.0 0.492 102 80-120 Selenium 0.187 0.0100 mg/L 0.200 -0.0254 93 80-120 Sodium 36.3 0.500 mg/L 10.0 26.7 96 80-120 Zinc 0.276 0.0100 mg/L 0.200 0.0785 99 80-120 Batch 9H2600B - EPA 7470A FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 12 QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9H26008 - EPA 7470A - Continued (� �Eo www.encolabs.com Blank (9H26008-BLK3) Prepared: 08/26/2019 08:24 Analyzed: 08/27/2019 12:41 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.000150 U 0.000200 mg/kg LCS (9H26008-BSI) Prepared: 08/26/2019 08:24 Analyzed: 08/27/2019 12:44 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00489 0.000200 mg/kg 0.00500 98 85-115 Matrix Spike (9H26008-MS3) Prepared: 08/26/2019 08:24 Analyzed: 08/27/2019 12:48 Source: CC07246-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00480 0.000200 mg/kg 0.00500 0.000150 U 96 70-130 Matrix Spike Dup (9H26008-MSD3) Prepared: 08/26/2019 08:24 Analyzed: 08/27/2019 12:51 Source: CC07246-03 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.00494 0.000200 mg/kg 0.00500 0.000150 U 99 70-130 3 30 Post Spike (91-126008-PSI) Prepared: 08/26/2019 08:24 Analyzed: 08/27/2019 12:54 Source: CC07246-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.82 0.200 ug/L 5.00 0.0200 116 75-125 Classical Chemistry Parameters - Quality Control Batch 9H21021 - NO PREP Blank (9H23021-BLKi) Prepared: 08/21/2019 17:09 Analyzed: 08/21/2019 17:09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/kg LCS (9H21021-BSI) Prepared: 08/21/2019 17:18 Analyzed: 08/21/2019 17:18 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 103 90-110 Matrix Spike (9H23021-MS3) Prepared: 08/21/2019 17:11 Analyzed: 08/21/2019 17:11 Source: CC12765-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.83 0.10 mg/kg 1.00 0.29 54 90-110 QM-07 Matrix Spike (9H23021-MS2) Prepared: 08/21/2019 17:16 Analyzed: 08/21/2019 17:16 Source: CC12765-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/kg 1.00 0.046 98 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 12 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9H21021 - NO PREP - Continued Matrix Spike Dup (9H23021-MSD3) Prepared: 08/21/2019 17:12 Analyzed: 08/21/2019 17:12 Source: CC12765-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.85 0.10 mg/kg 1.00 0.29 55 90-110 1 10 QM-07 Batch 9H22012 - Same Blank (9H22012-BLK3) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 12:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 0.26 U 0.48 mg/kg LCS (9H22012-BSI) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 12:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 13 0.48 mg/kg 12.1 106 90-110 Matrix Spike (9H22012-MS1) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 12:31 Source: CC12414-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 5.4 0.48 mg/kg 4.85 1.1 89 90-110 QM-07 Matrix Spike (9H22012-MS2) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 12:40 Source: CC12681-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 5.6 0.48 mg/kg 4.85 0.45 106 90-110 Matrix Spike Dup (9H22012-MSD3) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 12:33 Source: CC12414-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 3.4 0.48 mg/kg 4.85 1.1 48 90-110 45 10 QM-07, QM-11 Batch 9H22014 - Same Blank (9H22014-BLK1) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 14:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 0.025 U 0.10 mg/kg LCS (9H22014-BSI) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 14:49 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 1.7 0.10 mg/kg 1.60 107 80-120 Matrix Spike (9H22014-MS1) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 15:18 Source: CC12414-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 6.6 D 0.50 mg/kg 0.640 5.8 124 80-120 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 12 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9H22014 - Same - Continued Matrix Spike Dup (9H22014-MSD3) Prepared: 08/22/2019 11:34 Analyzed: 08/26/2019 15:19 Source: CC12414-01 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Phosphorus 6.4 D 0.50 mg/kg 0.640 5.8 96 80-120 3 25 Batch 9H22033 - EPA 3005A Blank (9H22033-BLK3) Prepared: 08/22/2019 13:41 Analyzed: 08/26/2019 13:26 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Sodium Adsorption Ratio 0.00 U [blank] Blank (9H22033-BLK2) Prepared: 08/22/2019 13:41 Analyzed: 08/26/2019 13:26 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Sodium Adsorption Ratio 0.00 U [blank] Batch 9H2302B - NO PREP Blank (9H23028-BLKI) Prepared: 08/23/2019 12:56 Analyzed: 08/23/2019 12:56 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.045 U 0.10 mg/kg LCS (9H23028-BSI) Prepared: 08/23/2019 12:58 Analyzed: 08/23/2019 12:58 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.98 0.10 mg/L 1.01 97 90-110 Matrix Spike (9H23028-MS1) Prepared: 08/23/2019 13:01 Analyzed: 08/23/2019 13:01 Source: CC11197-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.17 0.10 mg/kg 0.393 0.045 U 42 90-110 QM-07 Matrix Spike (9H23028-MS2) Prepared: 08/23/2019 13:06 Analyzed: 08/23/2019 13:06 Source: CC11381-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 5.3 E 0.10 mg/kg 0.393 5.2 22 90-110 QM-07 Matrix Spike Dup (9H23028-MSD3) Prepared: 08/23/2019 13:03 Analyzed: 08/23/2019 13:03 Source: CC11197-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.19 0.10 mg/kg 0.393 0.045 U 48 90-110 13 10 QM-07, QM-11 Batch 9H23041 - NO PREP LCS (9H23041-BSI) Prepared & Analyzed: 08/23/2019 13:25 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes pH 7.0 1.0 pH Units 7.01 101 99-101 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 12 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9H23041 - NO PREP - Continued Duplicate (9H23041-DUPl) Prepared & Analyzed: 08/23/2019 13:25 Source: CC13867-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes pH 7.2 1.0 pH Units 7.1 2 25 Batch 9H27015 - NO PREP Blank (9H27015-BLK3) Prepared & Analyzed: 08/27/2019 12:20 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 0.0050 U 0.0050 % by Volume LCS (9H27015-BSI) Prepared & Analyzed: 08/27/2019 12:20 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 1100 50 mg/L 1100 99 80-120 Duplicate (9H27015-DUPl) Prepared & Analyzed: 08/27/2019 12:20 Source: CC13867-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Total Solids 1.9 0.0050 % by Volume 2.0 4 20 Batch 9H2B017 - NO PREP Blank (9H28017-BLK3) Prepared: 08/28/2019 13:11 Analyzed: 08/28/2019 13:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/kg LCS (9H28017-BSI) Prepared: 08/28/2019 13:09 Analyzed: 08/28/2019 13:09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 1.25 102 90-110 Matrix Spike (9H28017-MS3) Prepared: 08/28/2019 14:48 Analyzed: 08/28/2019 14:48 Source: CC31381-02RE3 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 5.9 0.50 mg/kg 2.50 3.1 111 90-110 QM-07 Matrix Spike (9H28017-MS2) Prepared: 08/28/2019 13:20 Analyzed: 08/28/2019 13:20 Source: CC11381-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 2.7 E 0.10 mg/kg 0.521 2.2 95 90-110 QM-07 Matrix Spike Dup (9H28017-MSD3) Prepared: 08/28/2019 14:49 Analyzed: 08/28/2019 14:49 Source: CC11381-02RE1 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 5.9 0.50 mg/kg 2.50 3.1 110 90-110 0.6 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 12 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. Q-01 Analysis performed outside of method - specified holding time. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 12 _ 0 10775 Central Port Dr. • 4810 Executive Park Court, Suite 111 102-A Woodwinds Industrial Ct. Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511 (407) 826-5314 Fax (407) 850-6945 (904) 296-3007 Fax (904) 296-6210 (919) 467-3090 Fax (919) 467-3515 Page Of Client Name Hunt Environmental Associates (HU017) Project Number [none] Requested Analyses Requested Turnaround Times subject to NoteacceptRusance ce by the acceptance by the facility _Standard Expedited a - Z C r5 Y a 610 .o a o tif'E U -3 Q �p a m N X ? 17 0 T c E r! Uo g = N CO_ in co y CDDue m z Address 3330 Saddletree Road. Project Name/Desc City of Lumberton City/ST/Zip Lumberton, NG 28360 PO If / Billing Info Tel (910) 738-5311 Fax Reporting Contact Jordan Davis Sampler(s) Name, Affiliation (Print) Billin Contact body Hunt Sample )Signature Site Location / Time Zone Lab Workorder CC13867 Preservation (See Codes) (Combine as necessary) Item # Sample ID (Field Identification) Collection Date Collection Time Comp / Grab Matrix (see codes) Total # of Containers Sample Comments WW-2 WW 5 X x x s <-- Total # of Containers Sample Kit Prepared By Date/Time Relingdished By Date/Time Received ey Date/rime ii 1�1f 3:y�„ Lam— to 7 % C&ments/Special Reporting Flequirements Relinquished By Date/Time 7,ecly Date/Time Relinquished By Datefrime Received By DateTme Cooler #'s & Temps on Receipt Condition U n Receipt I3' ` Acceptable Unacceptable Matrix: GW-Groundwater SO -Soil DW-Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air 6-61her (detail in comments) Preservation: I -Ice H-HCI N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in comments) Note : All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist Sample Preservation Verification ENCO Cary EJ�ICO Work Order: CC13867 Project: City of Lumberton Client: Hunt Environmental Associates (HU017) Project #: [none] Logged In: 20-Aug-19 15:26 Logged By: John C King Preservation Check Performed By: Date/Time:7� CC13867-01 Cont Type Pres (pH) pH Checked / pH Adjusted DateMme Reagent Used/Comments Requirement In Control Adjusted A 500mLP+H2SO4 <2 U / N / NA Y / / NA E 250mLP+HNO3 <2 / N / NA Y / / NA Rea.gent Name ID 1 2 pH Strip ID: jam_ Rea ent Name ID 3 4 Rea ent Name ID 5 6 C:\ELMNT\Print\wko_PreservationCheck.rpt Page 1 1 2�SENCO Laboratories 9g Accurate. Timely. Respousive. luuavative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, November 27, 2019 Hunt Environmental Associates (HU017) Attn: Jordan Davis 3330 Saddletree Road. Lumberton, NC 28360 RE: Laboratory Results for Project Number: [none], Project Name/Desc: City of Lumberton ENCO Workorder(s): CC17274 Dear Jordan Davis, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, November 11, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OUCLC'=-:�CA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 13 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: WW-2 Lab ID: CC17274-01 Sampled: 11/11/19 12:45 Received: 11/11/19 16:17 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) CSU Method NO PREP 08/06/22 11/12/19 13:30 11/14/19 14:37 EPA 200.7 Same 05/09/20 11/12/19 13:30 11/14/19 12:02 EPA 245.1 EPA 245.1 12/09/19 11/18/19 09:51 11/19/19 12:49 EPA 353.2 NO PREP 11/13/19 12:45 11/12/19 16:24 11/12/19 16:24 EPA 353.2 [CALC] 11/13/19 12:45 11/22/19 10:22 11/22/19 14:53 EPA 353.2 NO PREP 12/09/19 11/22/19 10:22 11/22/19 14:53 EPA 9040C NO PREP 11/11/19 12:59 11/15/19 13:20 11/15/19 13:20 SM 254OB-2011 NO PREP 11/18/19 11/12/19 15:55 11/12/19 15:55 Client ID: WW-2 Lab ID: CC17274-01RE1 Sampled: 11/11/19 12:45 Received: 11/11/19 16:17 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 351.2 Same 12/09/19 11/14/19 11:53 11/26/19 12:29 EPA 365.4 Same 12/09/19 11/14/19 11:53 11/26/19 14:07 Client ID: WW-2 Lab ID: CC17274-01RE2 Sampled: 11/11/19 12:45 Received: 11/11/19 16:17 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 350.1 NO PREP 12/09/19 11/15/19 10:36 11/15/19 10:36 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 13 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: WW-2 Lab ID: CC17274-01 Anala Results Flag MDL POLL Units Method Notes Aluminum - Total 625 D 1.05 2.50 mg/kg EPA 200.7 R-01 Cadmium - Total 0.0287 D 0.00900 0.0250 mg/kg EPA 200.7 R-01 Calcium - Total 407 D 0.975 2.50 mg/kg EPA 200.7 R-01 Copper- Total 18.7 D 0.0400 0.250 mg/kg EPA 200.7 R-01 Lead - Total 0.469 D 0.0775 0.250 mg/kg EPA 200.7 R-01 Magnesium - Total 82.6 D 0.725 2.50 mg/kg EPA 200.7 R-01 Mercury - Total 0.0101 0.000750 0.00100 mg/kg EPA 245.1 Molybdenum - Total 0.199 ID 0.0625 0.250 mg/kg EPA 200.7 R-01 Nickel - Total 1.00 D 0.0550 0.250 mg/kg EPA 200.7 R-01 Nitrate/Nitrite as N 0.13 0.041 0.10 mg/kg EPA 353.2 Nitrite as N 0.14 0.017 0.10 mg/kg EPA 353.2 pH 7.2 1.0 1.0 pH Units EPA 9040C Q-01 Potassium - Total 132 D 3.75 12.5 mg/kg EPA 200.7 R-01 Sodium - Total 668 D 10.0 12.5 mg/kg EPA 200.7 R-01 Sodium Adsorption Ratio 7.87 [blank] CSU Method Temperature for pH (deg. C) 14 pH Units EPA 9040C Q-01 Total Solids 3.4 0.50 0.50 % by Volume SM 2540B-2011 Zinc - Total 27.8 D 0.110 0.250 mg/kg EPA 200.7 R-01 Client ID: WW-2 Lab ID: CC17274-01RE3 Anala Results Flag MDL POLL Units Method Notes Phosphorus 6.5 D 0.12 0.50 mg/kg EPA 365.4 Total Kieldahl Nitrogen 16 D 0.52 0.96 mo/ka EPA 351.2 Client ID: WW-2 Lab ID: CC17274-01RE2 Anala Results Flag MDL POLL Units Method Notes Ammonia as N 67 D 4.5 10 mg/kg EPA 350.1 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 13 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-2 Lab Sample ID:CC17274-01 Received: 11/11/19 16:17 Matrix: Waste Water Sampled:11/11/19 12:45 Work Order: CC17274 Project: City of Lumberton Sampled By:Jordan Davis Metals by EPA 200 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL P L Batch Method Analyzed By Notes Aluminum [7429-90-5]^ 625 D mg/kg 25 1.05 2.50 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Arsenic[7440-38-2]^ 0.190 UD mg/kg 25 0.190 0.250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Cadmium [7440-43-9]^ 0.0287 D mg/kg 25 0.00900 0.0250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Calcium [7440-70-2]^ 407 D mg/kg 25 0.975 2.50 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Copper[7440-50-8]^ 18.7 D mg/kg 25 0.0400 0.250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Lead [7439-92-1]^ 0.469 D mg/kg 25 0.0775 0.250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Magnesium [7439-95-4]^ 82.6 D mg/kg 25 0.725 2.50 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Mercury [7439-97-6]^ 0.0101 mg/kg 5 0.000750 0.00100 9K18016 EPA 245.1 11/19/19 12:49 KAH Molybdenum [7439-98-7]^ 0.199 JD mg/kg 25 0.0625 0.250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Nickel[7440-02-O]^ 1.00 D mg/kg 25 0.0550 0.250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Potassium [7440-09-7]^ 132 D mg/kg 25 3.75 12.5 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Selenium [7782-49-2]^ 0.155 UD mg/kg 25 0.155 0.250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Sodium [7440-23-5]^ 668 D mg/kg 25 10.0 12.5 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Zinc [7440-66-6]^ 27.8 D mg/kg 25 0.110 0.250 9K12035 EPA 200.7 11/14/19 12:02 JDH R-01 Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL P L Batch Method Analyzed By Notes Ammonia as N [7664-41-7]^ 67 D mg/kg 100 4.5 10 9K14036 EPA 350.1 11/15/19 10:36 AKF Nitrate as N [14797-55-8] 0.041 U mg/L 1 0.041 0.10 [CALC] EPA 353.2 11/22/19 14:53 PDK Nitrate/Nitrite as IN 0.13 mg/kg 1 0.041 0.10 91<22022 EPA 353.2 11/22/19 14:53 AKF Nitrite as N [14797-65-0]^ 0.14 mg/kg 1 0.017 0.10 9K12037 EPA 353.2 11/12/19 16:24 PDK pH 7.2 pH Units 1 1.0 1.0 9K15023 EPA 9040C 11/15/19 13:20 BDC Q-01 Phosphorus[7723-14-O]^ 6.5 D mg/kg 5 0.12 0.50 9K14010 EPA 365.4 11/26/19 14:07 AKF Sodium Adsorption Ratio 7.87 [blank] 1 9K12035 CSU Method 11/14/19 14:37 JDH Temperature for pH (deg. C) 14 pH Units 1 9K15023 EPA 9040C 11/15/19 13:20 BDC Q-01 Total Kjeldahl Nitrogen 16 D mg/kg 2 0.52 0.96 9K14011 EPA 351.2 11/26/19 12:29 AKF Total Solids^ 3.4 % by Volume 100 0.50 0.50 9K12006 SM 254OB-2011 11/12/19 15:55 CBAL1 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 13 QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9K12035 - EPA 3005A 0Nk"q09 www.encolabs.com Blank (9K12035-BLK1) Prepared: 11/12/2019 13:30 Analyzed: 11/14/2019 11:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Aluminum 0.0420 U 0.100 mg/kg Arsenic 0.00760 U 0.0100 mg/kg Cadmium 0.000360 U 0.00100 mg/kg Calcium 0.0390 U 0.100 mg/kg Copper 0.00160 U 0.0100 mg/kg Lead 0.00310 U 0.0100 mg/kg Magnesium 0.0290 U 0.100 mg/kg Molybdenum 0.00250 U 0.0100 mg/kg Nickel 0.00220 U 0.0100 mg/kg Potassium 0.150 U 0.500 mg/kg Selenium 0.00620 U 0.0100 mg/kg Sodium 0.400 U 0.500 mg/kg Zinc 0.00440 U 0.0100 mg/kg LCS (9K12035-BSI) Prepared: 11/12/2019 13:30 Analyzed: 11/14/2019 11:21 Spike Source %REC RPD Analvte Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes Aluminum 2.07 0.100 mg/kg 2.00 103 85-115 Arsenic 0.190 0.0100 mg/kg 0.200 95 85-115 Cadmium 0.0194 0.00100 mg/kg 0.0200 97 85-115 Calcium 2.03 0.100 mg/kg 2.00 101 85-115 Copper 0.186 0.0100 mg/kg 0.200 93 85-115 Lead 0.198 0.0100 mg/kg 0.200 99 85-115 Magnesium 2.09 0.100 mg/kg 2.00 105 85-115 Molybdenum 0.183 0.0100 mg/kg 0.200 92 85-115 Nickel 0.191 0.0100 mg/kg 0.200 96 85-115 Potassium 10.4 0.500 mg/kg 10.0 104 85-115 Selenium 0.179 0.0100 mg/kg 0.200 90 85-115 Sodium 10.2 0.500 mg/kg 10.0 102 85-115 Zinc 0.193 0.0100 mg/kg 0.200 97 85-115 Matrix Spike (91(12035-MS1) Prepared: 11/12/2019 13:30 Analyzed: 11/14/2019 11:24 Source: CCO5217-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Lima Notes Aluminum 2.21 0.100 mg/kg 2.00 0.0448 108 70-130 Arsenic 0.203 0.0100 mg/kg 0.200 0.00760 U 101 70-130 Cadmium 0.0207 0.00100 mg/kg 0.0200 0.000360 U 103 70-130 Calcium 11.6 0.100 mg/kg 2.00 9.16 122 70-130 Copper 0.224 0.0100 mg/kg 0.200 0.0219 101 70-130 Lead 0.211 0.0100 mg/kg 0.200 0.00310 U 106 70-130 Magnesium 3.44 0.100 mg/kg 2.00 1.25 109 70-130 Molybdenum 0.199 0.0100 mg/kg 0.200 0.00250 U 100 70-130 Nickel 0.204 0.0100 mg/kg 0.200 0.00292 101 70-130 Potassium 15.1 0.500 mg/kg 10.0 3.98 111 70-130 Selenium 0.195 0.0100 mg/kg 0.200 0.00620 U 97 70-130 Sodium 29.3 0.500 mg/kg 10.0 17.7 116 70-130 Zinc 0.341 0.0100 mg/kg 0.200 0.134 103 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 13 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9K12035 - EPA 3005A - Continued Matrix Spike Dup (9KI2035-MSD3) Prepared: 11/12/2019 13:30 Analyzed: 11/14/2019 11:27 Source: CCO5217-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Aluminum 2.10 0.100 mg/kg 2.00 0.0448 103 70-130 5 30 Arsenic 0.191 0.0100 mg/kg 0.200 0.00760 U 96 70-130 6 30 Cadmium 0.0205 0.00100 mg/kg 0.0200 0.000360 U 102 70-130 1 30 Calcium 10.7 0.100 mg/kg 2.00 9.16 78 70-130 8 30 Copper 0.223 0.0100 mg/kg 0.200 0.0219 100 70-130 0.6 30 Lead 0.208 0.0100 mg/kg 0.200 0.00310 U 104 70-130 1 30 Magnesium 3.22 0.100 mg/kg 2.00 1.25 98 70-130 7 30 Molybdenum 0.196 0.0100 mg/kg 0.200 0.00250 U 98 70-130 1 30 Nickel 0.200 0.0100 mg/kg 0.200 0.00292 99 70-130 2 30 Potassium 14.1 0.500 mg/kg 10.0 3.98 101 70-130 7 30 Selenium 0.196 0.0100 mg/kg 0.200 0.00620 U 98 70-130 0.8 30 Sodium 27.5 0.500 mg/kg 10.0 17.7 98 70-130 6 30 Zinc 0.334 0.0100 mg/kg 0.200 0.134 100 70-130 2 30 Post Spike (9K12035-PSI) Prepared: 11/12/2019 13:30 Analyzed: 11/14/2019 11:29 Source: CCO5217-01 Spike Source %REC RPD Awe Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes Aluminum 2.20 0.100 mg/L 2.00 0.0448 108 80-120 Arsenic 0.187 0.0100 mg/L 0.200 0.00710 90 80-120 Cadmium 0.0205 0.00100 mg/L 0.0200 -4.86E-5 103 80-120 Calcium 10.8 0.100 mg/L 2.00 9.16 81 80-120 Copper 0.229 0.0100 mg/L 0.200 0.0219 104 80-120 Lead 0.205 0.0100 mg/L 0.200 0.000155 103 80-120 Magnesium 3.30 0.100 mg/L 2.00 1.25 102 80-120 Molybdenum 0.201 0.0100 mg/L 0.200 0.00131 100 80-120 Nickel 0.206 0.0100 mg/L 0.200 0.00292 101 80-120 Potassium 14.5 0.500 mg/L 10.0 3.98 105 80-120 Selenium 0.193 0.0100 mg/L 0.200 -0.000964 96 80-120 Sodium 27.7 0.500 mg/L 10.0 17.7 100 80-120 Zinc 0.335 0.0100 mg/L 0.200 0.134 101 80-120 Batch 9KIS016 - EPA 7470A Blank (9K38016-BLKl) Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:37 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Mma Notes Mercury 0.000150 U 0.000200 mg/kg LCS (9K18016-BSI) Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:39 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00495 0.000200 mg/kg 0.00500 99 85-115 Matrix Spike (9K38016-MS3) Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:50 Source: CC18168-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00548 0.000200 mg/kg 0.00500 0.000924 91 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 13 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 200 Series Methods - Quality Control Batch 9K18016 - EPA 7470A - Continued Matrix Spike Dup (9K18016-MSD3) Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:52 Source: CC18168-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.00546 0.000200 mg/kg 0.00500 0.000924 91 70-130 0.4 30 Post Spike (9KI8016-PSI) Prepared: 11/18/2019 09:52 Analyzed: 11/19/2019 11:54 Source: CC18168-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.60 0.200 ug/L 5.00 0.924 94 75-125 Classical Chemistry Parameters - Quality Control Batch 9KI2006 - NO PREP Blank (9K12006-BLKS) Prepared & Analyzed: 11/12/2019 15:55 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 0.0050 U 0.0050 % by Volume LCS (9K12006-BS3) Prepared & Analyzed: 11/12/2019 15:55 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 1100 50 mg/L 1100 96 80-120 Duplicate (9K12006-DUP3) Prepared & Analyzed: 11/12/2019 15:55 Source: CC16864-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Solids 3.2 0.25 % by Volume 3.1 3 20 Batch 9KI2035 - EPA 3005A Blank (9K12035-BLKS) Prepared: 11/12/2019 13:30 Analyzed: 11/14/2019 14:37 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sodium Adsorption Ratio 0.00 U [blank] Batch 9K12037 - NO PREP Blank (9K12037-BLKS) Prepared: 11/12/2019 16:16 Analyzed: 11/12/2019 16:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/kg LCS (9K32037-BS3) Prepared: 11/12/2019 16:37 Analyzed: 11/12/2019 16:37 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 103 90-110 Matrix Spike (9KI2037-MSI) Prepared: 11/12/2019 18:02 Analyzed: 11/12/2019 18:02 Source: CC18217-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 13 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9K12037 - NO PREP - Continued Matrix Spike (9K32037-MS3) Continued Prepared: 11/12/2019 18:02 Analyzed: 11/12/2019 18:02 Source: CC18217-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/kg 1.00 0.039 99 90-110 Matrix Spike (9K32037-MS2) Prepared: 11/12/2019 18:05 Analyzed: 11/12/2019 18:05 Source: CC18217-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/kg 1.00 0.037 99 90-110 Matrix Spike Dup (9K12037-MSD3) Prepared: 11/12/2019 18:03 Analyzed: 11/12/2019 18:03 Source: CC18217-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/kg 1.00 0.039 100 90-110 1 10 Batch 9K14010 - Same Blank (9K14030-BLK1) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:50 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Phosphorus 0.032 3 0.10 mg/kg Blank (9K14030-BLK2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 14:04 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 0.049 3 0.10 mg/kg LCS (91(14010-BS1) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:52 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 1.6 0.10 mg/kg 1.60 99 80-120 LCS (91(14010-BS2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 14:06 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 1.6 0.10 mg/kg 1.60 103 80-120 Matrix Spike (9K14010-MS1) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:54 Source: CC12339-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Phosphorus 1.7 0.10 mg/kg 0.640 0.99 108 80-120 Matrix Spike Dup (9K14010-MSD1) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 17:56 Source: CC12339-01 Analvte Phosphorus Batch 9K14011 - Same Spike Source %REC Result Flag POL Units Level Result %REC Limits RPD 1.7 0.10 mg/kg 0.640 0.99 111 80-120 1 RPD Limit Notes 25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 13 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9K14011 - Same - Continued Blank (9K14011-BLKI) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 0.26 U 0.48 mg/kg Blank (9K14031-BLK2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 12:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 0.26 U 0.48 mg/kg LCS (91(14011-BS3) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 12 0.48 mg/kg 12.0 103 90-110 LCS (91(34011-BS2) Prepared: 11/14/2019 11:53 Analyzed: 11/26/2019 12:27 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 13 0.48 mg/kg 12.0 108 90-110 Matrix Spike (9K34011-MSi) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:14 Source: CC12339-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 11 0.48 mg/kg 4.80 5.7 107 90-110 Matrix Spike (9K34011-MS2) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:19 Source: CC12555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 5.5 0.48 mg/kg 4.80 0.65 102 90-110 Matrix Spike Dup (9K14031-MSD3) Prepared: 11/14/2019 11:53 Analyzed: 11/25/2019 16:15 Source: CC12339-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 11 0.48 mg/kg 4.80 5.7 114 90-110 3 10 QM-07 Batch 9K14036 - NO PREP Blank (9K14036-BLKl) Prepared: 11/14/2019 19:53 Analyzed: 11/14/2019 19:53 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.045 U 0.10 mg/kg LCS (91(14036-BS3) Prepared: 11/14/2019 19:54 Analyzed: 11/14/2019 19:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 1.0 0.10 mg/L 1.01 100 90-110 Matrix Spike (9K34036-MS3) Prepared: 11/15/2019 15:07 Analyzed: 11/15/2019 15:07 Source: CC16549-01 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Notes Page 9 of 13 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9K14036 - NO PREP - Continued Matrix Spike (9K34036-MS3) Continued Prepared: 11/15/2019 15:07 Analyzed: 11/15/2019 15:07 Source: CC16549-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.36 0.10 mg/kg 0.393 0.045 U 92 90-110 Matrix Spike (9K14036-MS2) Prepared: 11/15/2019 15:38 Analyzed: 11/15/2019 15:38 Source: CC17919-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.70 0.10 mg/kg 0.393 0.37 84 90-110 QM-07 Matrix Spike Dup (9K14036-MSD3) Prepared: 11/15/2019 15:08 Analyzed: 11/15/2019 15:08 Source: CC16549-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.36 0.10 mg/kg 0.393 0.045 U 93 90-110 0.3 10 Batch 9KI5023 - NO PREP LCS (9K35023-BS3) Prepared & Analyzed: 11/15/2019 13:20 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes pH 6.9 1.0 pH Units 7.00 99 99-101 Duplicate (9K15023-DUP3) Prepared & Analyzed: 11/15/2019 13:20 Source: CC17274-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes pH 7.1 1.0 pH Units 7.2 1 25 Batch 9K22022 - NO PREP Blank (9K22022-BLKS) Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:50 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/kg LCS (9K22022-BS3) Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:51 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 98 90-110 Matrix Spike (9K22022-MS3) Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:55 Source: CC17274-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.47 0.10 mg/kg 0.521 0.13 64 90-110 QM-07 Matrix Spike (9K22022-MS2) Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 15:04 Source: CC17732-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 20 E 0.10 mg/kg 0.521 20 69 90-110 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 13 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9K22022 - NO PREP - Continued Matrix Spike Dup (9K22022-MSD3) Prepared: 11/22/2019 10:22 Analyzed: 11/22/2019 14:57 Source: CC17274-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.47 0.10 mg/kg 0.521 0.13 65 90-110 0.7 10 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 13 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. Q-01 Analysis performed outside of method - specified holding time. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. R-01 The Reporting Limit for this analyte has been raised to account for matrix interference. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 13 — 10775 CsnI4 Port Dr. 4810 Executive Park Court, Suite 111 102-A Woodwinds Industrial Ct. Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary. NO 27511 UE-0—M MIS (407) 826-5314 Fax (407) 850-6945 (904) 296-3007 Fax (904) 296-6210 (919) 467-3090 Fax (919) 467-3515 Page of Cl" raffEnviranmental Associates (HU017) Proipft VM L11�.]r taJ Requested Analyses Requested Turnaround Times Note: Rush requests sub)ecl to acceptance by the facility Standard Expedited Due ro Z 0 'z =azTe(910) z; 2 Q rn m i5 a C M o cn 0 E N 1w� Q o Ce N z Mp <4 z (Al Add+�ss�� Saditetree Read. JJ 33JJ - Pr°it�tiW&T-JumbeItm Ci Rber kin, NC 28360 PO tt I Billing Info 7385311 Fax RepJUEd°bavis Sa�(s) Name. Atfitiatinn Print) Ni Jo y. �ae j N Billi �9ptHUnt J Samp s) Signature Site Location / Time Zone Lat) Workorder C:C.17274 Preservation (See Codes) (Combine as necessary) (tern # Sample ID (Field Identification) Collection Date Collection Time Comp I Grab Matrix (see codes) Total 0 of Containers Sample Comments WW-2 [I I2:g3" (, VWV 5 x x x -- Total # of Containers lip mpie Kit Prepared By Date, 9me ReGnq - ed By Datelrme Received Date/rrne Co MedSpecial Reporting Requirements R quished By Dat&TIme ived y T Date>rme Relinquished By DatwTime eCeiv d By DalerTime Cooler N's & T ps on Receipt a — —1 V rondil7pon Receipt Acceptable Unacceptable Matrix: GW-Groundwater SO -Sail DW-Drinking Water SE -Sediment SW -Surface Water WIN -Wastewater A -Air O-Other (detail in comments) Preservation: I -ice H-f jCl N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in comments) Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this lorm, unless prior written agreements exist Sample Preservation Verification. ENCO Cary (9 Work Order: CC17274 Project: Client: Hunt Environmental Associates (HU017) Project #: Logged In: 11-Nov-19 1617 Logged By: Preservation Check Performed By: CC17274-01 City of Lumberton [none] John C King Date/Time: C (` f - l'(020 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments A 500mLP+H2SO4 <2 I N I NA YCN / NA E 250mLP+HNO3 {2 Y 1 N / NA ! N / NA Rea ent Name ID 1 �-(I'V0 2 d ) SC C{� pH Strip ID: 0 Rea ent Name ID 3 4 Rea ent Name ID 5 6 C:IELMNTIPrintlwko_PreservationCheck. rpt Page 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021583 Client: Delois/Pete Allen Advisor: Enviro-Choice Recycling ,u Predictive 688 Deep Branch Rd. 3330 Saddletree Rd Lumberton, NC 28360 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction _ Sampled County: Robeson "!'''w Links to Helpful Information Client ID: 434958 Advisor ID: 486968 Sampled: 11/14/2019 Received: 11/26/2019 completed: 01/28/2020 Farm: NC-RQ-17 Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field. Sample ID: NC01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.7 120 - 160 30 30 0 0 0 0 C 0 Note: 3 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 2.76 0.94 8.2 51 4.0 4.8 47 56 33 14 61 37 39 1440 1440 2345 0.2 2 Sample ID: NCO2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.5 120 - 160 50 40 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 2.37 0.97 7.9 51 3.8 4.8 36 49 34 15 67 30 35 1510 1510 1964 0.2 3 North Carolina T&RCLr Trust Fmui cswnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021583 Delois/Pete Allen Page 2 of 3 Sample ID: NC03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.7 120 - 160 50 40 0 0 0 0 C 0 Note: 3 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.52 0.97 8.0 49 4.1 4.8 36 49 32 14 64 30 35 1419 1419 2029 0.2 3 Sample ID: NC04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.6 120 - 160 40 30 0 0 0 0 C 0 Note: 3 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.60 0.95 7.8 50 3.9 4.8 44 55 32 14 63 30 35 1378 1378 2166 0.2 3 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21583 Delois/Pete Allen Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021589 Client: Patrick Ballard Advisor: Enviro-Choice Recycling ,u Predictive PO Box 1262 3330 Saddletree Rd Pembroke, NC 28372 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction Sampled County: Robeson Links to Helpful Information Client ID: 505231 Advisor ID: 486968 Sampled: 11/15/2019 Received: 11/26/2019 Completed: 01/29/2020 Farm: NC-RO-39 Sample ID: NC01A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.0 180-220 40 140 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.49 1.07 5.6 48 2.9 4.6 43 39 34 11 68 25 32 330 330 356 0.2 4 Sample ID: NC01 B Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.2 180-220 60 120 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.55 1.02 5.6 44 3.1 4.6 34 47 29 11 69 27 33 218 218 163 0.1 2 Sample ID: NCO2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.1 180-220 40 130 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.49 1.06 5.6 47 3.0 4.6 44 42 33 11 63 25 32 293 293 284 0.1 2 North Carolina All! Ta RCL, Trust Fwwi ckwnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021589 Patrick Ballard Page 2 of 4 Sample ID: NC03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.2 180-220 30 140 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.37 1.07 5.7 43 3.2 4.6 47 40 30 10 60 25 32 309 309 321 0.1 2 Sample ID: NC04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.1 180-220 30 130 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.61 1.03 5.6 47 3.0 4.6 49 44 32 11 62 28 34 307 307 327 0.1 2 Sample ID: NC05 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.2 180-220 60 140 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.97 1.04 5.2 41 3.1 4.5 32 39 27 10 68 19 28 208 208 195 0.2 4 Sample ID: NC06 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.0 180-220 40 130 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.02 1.02 5.3 45 2.9 4.6 42 42 31 11 62 23 31 255 255 227 0.1 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021589 Patrick Ballard Page 3 of 4 Sample ID: NC07 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 1.6 180-220 40 190 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.37 0.98 7.2 64 2.6 5.1 43 21 51 12 63 43 43 245 245 48 0.2 3 Sample ID: NC08 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.1 180-220 50 120 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.19 1.04 5.5 46 3.0 4.6 37 45 31 11 62 26 33 226 226 166 0.1 2 Sample ID: NC09 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 2.2 180-220 70 130 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.49 1.01 5.4 40 3.2 4.6 27 41 26 10 63 24 31 178 178 113 0.1 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21589 Patrick Ballard Page 4 of 4 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021590 Client: Carnell Locklear Advisor: Enviro-Choice Recycling ,u Predictive 3009 Daniel McLeod Rd. 3330 Saddletree Rd Red Springs, NC 28377 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction Sampled County: Robeson Links to Helpful Information Client ID: 275468 Advisor ID: 486968 Sampled: 11/03/2019 Received: 11/26/2019 Completed: 01/28/2020 Farm: NC-RO-28 Sample ID: NC01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.1 120 - 160 0 60 0 0 0 0 0 0 Note: 3 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.87 1.04 6.0 50 3.0 4.7 82 41 36 10 61 31 36 457 457 562 0.1 2 Sample ID: NCO2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.1 120 - 160 0 50 0 0 0 0 0 0 Note: 3 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.61 1.03 6.0 49 3.1 4.7 62 43 34 11 77 31 36 356 356 402 0.1 2 Sample ID: NC03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.2 120 - 160 0 50 0 0 0 0 0 0 Note: 3 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.74 1.05 6.2 49 3.2 4.7 67 43 35 11 61 32 36 410 410 470 0.1 2 North Carolina All! Ta RCL, Trust Fwwi ckwnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21590 Carnell Locklear Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021588 Client: Fannie Oxendine Advisor: Enviro-Choice Recycling ,u Predictive 7623 NC HWY 711 3330 Saddletree Rd Pembroke, NC 28372 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction Sampled County: Robeson Links to Helpful Information Client ID: 505230 Advisor ID: 486968 Sampled: 10/22/2019 Received: 11/26/2019 completed: 01/28/2020 Farm: NC-RO-21 Sample ID: NC01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 1.3 120 - 160 30 100 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.22 0.98 7.2 68 2.3 5.2 47 20 54 12 54 51 48 267 267 40 0.2 3 Sample ID: NCO2A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 1.3 120 - 160 40 100 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.22 1.02 7.1 68 2.3 5.2 43 20 54 13 51 46 45 323 323 230 0.1 1 Sample ID: NCO2B Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 1.3 180-220 30 190 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.37 1.00 7.2 70 2.2 5.2 45 19 56 13 50 51 48 263 263 74 0.1 1 North Carolina Tahacw Trust FwW Cswnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021588 Fannie Oxendine Page 2 of 3 Sample ID: NC03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 1.7 180-220 30 130 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.22 0.98 7.6 65 2.7 5.0 46 43 48 14 56 47 45 870 870 1206 0.1 1 Sample ID: NC04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 1.9 180-220 40 130 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.15 0.96 7.7 63 2.9 4.9 44 42 46 14 58 46 45 983 983 1342 0.1 1 Sample ID: NC05 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.1 120 - 160 30 50 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.44 0.96 7.7 58 3.2 4.9 46 45 41 14 59 44 43 1001 1001 1260 0.2 3 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21588 Fannie Oxendine Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021587 Client: Ronald G. Hammonds Advisor: Enviro-Choice Recycling ,u Predictive 1218 Hammonds Rd. 3330 Saddletree Rd Lumberton, NC 28360 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction Sampled County: Robeson Links to Helpful Information Client ID: 404031 Advisor ID: 486968 Sampled: 11/13/2019 Received: 11/26/2019 Completed: 01/28/2020 Farm: NC-RO-20 Sample ID: NC03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 1.3 180-220 30 190 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.37 1.02 7.1 67 2.3 5.2 46 18 54 12 50 46 45 309 309 130 0.1 1 Sample ID: NC04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 1.3 180-220 40 190 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.44 0.98 6.9 67 2.2 5.2 43 19 54 12 55 45 44 230 230 41 0.2 3 Sample ID: NC06 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 1.3 0 40 100 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.37 0.99 6.9 68 2.2 5.2 44 20 54 12 57 45 37 242 242 41 0.2 3 North Carolina Tahacw Trust FwW Cswnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021587 Ronald G. Hammonds Page 2 of 3 Sample ID: NC07 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 2.0 0 70 50 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 1.37 1.05 5.4 46 2.9 4.6 28 44 32 11 72 28 27 192 192 105 0.2 4 Sample ID: NC08 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 1.3 0 40 110 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.15 0.98 6.9 68 2.2 5.2 44 16 54 12 52 47 38 222 222 41 0.1 1 Sample ID: NC14 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 1.4 0 40 100 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.08 0.99 7.2 67 2.4 5.2 43 21 53 13 46 53 42 342 342 230 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21587 Ronald G. Hammonds Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021586 Client: David McLean Advisor: Enviro-Choice Recycling ,u Predictive 919 McLean Rd 3330 Saddletree Rd Lumberton, NC 28358 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction Sampled County: Robeson Links to Helpful Information Client ID: 505228 Advisor ID: 486968 Sampled: 10/29/2019 Received: 11/26/2019 Completed: 01/28/2020 Farm: NC-RO-18 Sample ID: NC01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.3 120 - 160 30 40 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.44 0.94 7.7 54 3.5 4.8 48 54 36 14 58 37 39 1309 1309 1815 0.1 1 Sample ID: NCO2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 2.3 120 - 160 50 40 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.08 0.96 7.5 53 3.5 4.8 39 50 35 15 63 36 39 1338 1338 1962 0.2 3 North Carolina Ta RCLP Trust Fwwi ckwnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21586 David McLean Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021584 Client: Ozzell/Arrin Baker Advisor: Enviro-Choice Recycling ,u Predictive 2996 Evergreen Church Rd 3330 Saddletree Rd Pembroke, NC 28372 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction Sampled County: Robeson Links to Helpful Information Client ID: 156712 Advisor ID: 486968 Sampled: 11/11/2019 Received: 11/26/2019 Completed: 01/29/2020 Farm: NC-RO-16 Sample ID: NC01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 2.3 180-220 0 140 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 3.19 1.03 7.4 51 3.6 5.0 139 40 39 9 55 42 42 621 621 914 0.1 1 Sample ID: NCO2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 2.1 120-200 0 70 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 3.47 0.99 7.0 53 3.3 5.0 134 32 41 10 52 42 42 628 628 928 0.2 3 Sample ID: NC03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.9 180-220 0 140 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.84 1.03 6.7 56 3.0 5.0 125 37 44 10 54 40 41 628 628 859 0.1 1 North Carolina All! Ta RCL, Trust Fwwi ckwnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021584 Ozzell/Arrin Baker Page 2 of 4 Sample ID: NC04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.9 180-220 0 140 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.92 1.02 6.7 56 3.0 4.9 129 38 44 10 56 39 40 619 619 830 0.1 1 Sample ID: NC05 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.8 180-220 0 150 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 3.01 1.04 6.8 57 2.9 5.0 128 35 45 10 60 38 40 594 594 802 0.2 3 Sample ID: NC06 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 1.9 120-200 0 70 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.76 0.98 6.8 56 3.0 5.0 124 34 43 10 61 37 39 581 581 829 0.2 3 Sample ID: NC07 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 1.9 120 - 160 0 70 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 3.01 1.03 6.8 56 3.0 5.0 127 36 44 10 59 39 40 636 636 821 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021584 Ozzell/Arrin Baker Page 3 of 4 Sample ID: NC08 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Small Grain (SG) 1.9 80-100 0 80 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.84 0.97 6.8 55 3.0 5.0 122 31 42 11 62 38 33 611 611 828 0.2 3 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21584 Ozzell/Arrin Baker Page 4 of 4 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021585 Client: Ozzell/Arrin Baker Advisor: Enviro-Choice Recycling ,u Predictive 2996 Evergreen Church Rd 3330 Saddletree Rd Pembroke, NC 28372 Lumberton, NC 28360 } Soil Report Mehllch-3 Extraction Sampled County: Robeson Links to Helpful Information Client ID: 156712 Advisor ID: 486968 Sampled: 11/12/2019 Received: 11/26/2019 completed: 01/29/2020 Farm: NC-RO-16 Sample ID: NC16 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.9 180-220 0 150 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 2.92 1.02 6.7 55 3.0 5.0 125 33 43 10 64 38 40 595 595 837 0.2 3 Sample ID: NC17 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.9 180-220 0 130 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 3.01 1.03 6.7 56 3.0 5.0 131 43 43 10 63 38 40 562 562 800 0.2 3 Sample ID: NC18 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.9 180-220 0 150 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.76 1.03 6.7 54 3.0 5.0 129 36 42 9 61 38 40 574 574 821 0.2 3 North Carolina All! Ta RCL, Trust Fwwi ckwnmisslan Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL021585 Ozzell/Arrin Baker Page 2 of 3 Sample ID: NC19 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 2.1 180-220 0 150 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 3.01 1.04 6.6 52 3.2 4.9 129 35 40 9 54 37 39 593 593 809 0.1 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO21585 Ozzell/Arrin Baker Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/obpart4.htn7 fsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/apronomi/uyrst.htm N IR - CH, OICE VW PO Box 390 Lumberton, NC 28359 Phone: (910) 738-5311 Fax: (866) 768-8016 February 26, 2020 N.C. Environmental Quality-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Compliance Representative Subject: 2019 Annual Report for City of Lumberton Land Application Program (City of Lumberton WQ0000672) Dear Compliance Representative: Lime calculations have been included in the Annual Report, but because of field conditions, lime was not applied in 2019. Lime has been calculated and scheduled for each field. Once conditions improve lime will be distributed. Should you need more information regarding this land application program, please contact me at 910-738-5311. Farm ID Field # Field Leasse/Owner Crop Lime Recommended Acerage Total Lime to Apply NC-RO-16 1 Ozzell Baker Bermuda Hay/Past 2.3 16.9 38.87 NC-RO-16 2 Ozzell Baker Bermuda Hay/Past 2.1 3.6 7.56 NC-RO-16 3 Ozzell Baker Bermuda Hay/Past 1.9 3.4 6.46 NC-RO-16 4 Ozzell Baker Bermuda Hay/Past 1.9 3.6 6.84 NC-RO-16 5 Ozzell Baker Bermuda Hay/Past 1.8 8.7 15.66 NC-RO-16 6 Ozzell Baker Fescue/Ograss/Tim 1.9 14.8 28.12 NC-RO-16 7 Ozzell Baker Corn, Grain 1.9 17.5 33.25 NC-RO-16 8 Ozzell Baker Small Grain (SG) 1.9 7.6 14.44 NC-RO-16 16 Ozzell Baker Bermuda Hay/Past 1.9 5 9.5 NC-RO-16 17 Ozzell Baker Bermuda Hay/Past 1.9 6 11.4 NC-RO-16 18 Ozzell Baker Bermuda Hay/Past 1.9 12.3 23.37 NC-RO-16 19 Ozzell Baker Bermuda Hay/Past 2.1 1.6 3.36 NC-RO-17 1 Delois Allen Corn, Grain 2.7 36.4 98.28 NC-RO-17 2 Delois Allen Corn, Grain 2.5 25.4 63.5 NC-RO-17 3 Delois Allen Corn, Grain 2.7 28 75.6 NC-RO-17 4 Delois Allen Corn, Grain 2.6 47.7 124.02 NC-RO-18 1 Bobby Pittman Corn, Grain 2.3 16.6 38.18 NC-RO-18 2 Floyd, Polly Nanatte McLean; McLean, Christopher; Parker, Judy Gray McLean; Vukovich, Gwendolyn A.M., Vukovich, Vanessa Lynn; Vukovich, Craig, Jr. Corn, Grain 2.3 49.3 113.39 NC-RO-20 3 Ronald Hammonds Bermuda Hay/Past 1.3 24.9 32.37 NC-RO-20 4 Ronald Hammonds Bermuda Hay/Past 1.3 31.2 40.56 NC-RO-20 6 Ronald Hammonds Soybean 1.3 6.7 8.71 NC-RO-20 7 Ronald Hammonds Soybean 2 13 26 NC-RO-20 8 Ronald Hammonds Soybean 1.3 73.2 95.16 NC-RO-20 14 Ronald Hammonds Soybean 1.4 10.6 14.84 NC-RO-21 1 Lacy Cummings Corn, Grain 1.3 36.1 46.93 NC-RO-21 2A Lacy Cummings Corn, Grain 1.3 38.4 49.92 NC-RO-21 2B Lacy Cummings Bermuda Hay/Past 1.3 5.1 6.63 NC-RO-21 3 Lacy Cummings Bermuda Hay/Past 1.7 3.4 5.78 NC-RO-21 4 Lacy Cummings Bermuda Hay/Past 1.9 11.3 21.47 NC-RO-21 5 Lacy Cummings Corn, Grain 2.1 15.1 31.71 NC-RO-28 1 Carnell Locklear Corn, Grain 2.1 11.6 24.36 NC-RO-28 2 Carnell Locklear Corn, Grain 2.1 56.9 119.49 NC-RO-28 3 Carnell Locklear Corn, Grain 2.2 10.4 22.88 NC-RO-39 1A Patrick Bullard Bermuda Hay/Past 2 5.3 10.6 NC-RO-39 1B Patrick Bullard Bermuda Hay/Past 2.2 2.6 5.72 NC-RO-39 2 Patrick Bullard Bermuda Hay/Past 2.1 1.4 2.94 NC-RO-39 3 Patrick Bullard Bermuda Hay/Past 2.2 5.1 11.22 NC-RO-39 4 Patrick Bullard Bermuda Hay/Past 2.1 14.8 31.08 NC-RO-39 5 Patrick Bullard Bermuda Hay/Past 2.2 3.8 8.36 NC-RO-39 6 Patrick Bullard Bermuda Hay/Past 2 2.9 5.8 NC-RO-39 7 Lyndon Bullard, Anissa Emanuel Bullard Bermuda Hay/Past 1.6 3.7 5.92 NC-RO-39 8 Lyndon Bullard Bermuda Hay/Past 2.1 7.41 15.54 NC-RO-39 9 Tracy Elizabeth Bullard I Bermuda Hay/Past 2.2 62.5 137.5 City of Lumberton Environmental Laboratory Specific Oxvoen Uptake Rate (SOUR) Worksheet Date & Analyst: It.LF ":R i Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: g Weight of dried solids: "g/L g Total Solids: SOUR Time (Minutes) Temperature aC Dissolved Oxygen (mg/L) 0 Q3.00 8.58 1 3.00 8.58 2 '2.00 _ 8.55 3 2.00 8.45 4 12.00 8.32 5 12.00 8.24 6 12.00 8.22 7 12.00 8.06 8 12,00 7.91 9 12.00 7,81 10 13.00 7.69 11 1 .00 7.60 12 13.00 7.36 13 13.00 7.34 14 13.00 1.21 15 0. Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 12.5 0.11 mg/L/minute 0.28 (mg/g)/hr If sewage sludge is > 20°C, SOUR = (mg/g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: "g/L 9 Total Solids: SOUR Temperature Dissolved oC Oxygen (mg/L) 7. 1 _• 3.0 12.0 7.34 7.21 ;1 12.00 _ 7.04 12.00 6.88 4.00 6.78 M97 4.00 8.83 4,00 6.50 4.00 6.38 .00� 624 4.0 - 6.10 4.0 5.93 A 4.0 4.0 5.83 5.72 14.OQ 5.57 14.004� Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test oC 13.5625 0.13 mg/L/minute 0.36 (mg/g)/hr If sewage sludge is > 20°C, SOUR = M(mglg)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes If result Is <_ 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: 0.23 g Total Solids: 22.52 g/L SOUR Time Temperature Dissolved (Minutes) or., Oxygen (mg/L) 4 15.00 5.68 5 _ 15.00 5.53 6 15.00 5.43 7 15.00 5.32 Oxygen Consumption Rate 0.12 SOUR 0.33 SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 15.25 mg/L/minute (mg/g)/hr If sewage sludge is > 20'C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes if result is 5 1.6 (mg/g)hr Version 1111/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet )ate & Analyst: - KCL Dig# 2 'IR.dIr#. Total Solids Sample volume used for total solids test: 10 mL Weight of dish: 89.04, 9 Weight of dish + dried solids: _ 89.26 g Weight of dried solids: 0.22 9 Total Solids: 21.88 g/L SOUR Time (Minutes) Temperature oC Dissolved Oxygen (mg/L) 0 14.00 8.14 41 1 14.00 8,11 2 3 14.00 14.00 7.89 7.84 4 14.00 7.76 5 14.00 7.66 6 14,00 7.56 7 14.00 7.43 8 14.00 7.34 9 14.05 7.23 10 14.00 7.11 JN 11 14.00 6.99 12 14.00 6.89 13 14.00 6.78 14 14.00 6.65 15 14.00 Oxygen Consumption Rate 61*111i SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 14 0.11 mg/Uminute 0.29 (mg/g)/hr If sewage sludge is > 20°C, SOUR = (mg/g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is 5 1.5 (mg/g)hr Vpersion 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: 0.22 g Total Solids: 22.31 g/L Oxygen Consumption Rate 0.09 SOUR 0.26 SOUR Temperature Correction Average Sewage Sludge Temperature During Test mg/Uminute (mg/g)/hr If sewage sludge is > 20°C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes if result is 5 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: 0.23 g Total Solids: 22.69 gk SOUR s) Temperature oC Dissolved Oxygen (mg/L) 13.00 _ 13.00 _ 3.00 9.50 1 9.49 9.40 3.00 9.37 3.00 13.00 9.22 9.18 ii 3.00 9.113.00 9.053.00 8.973.00 8.883.00 8 8813.00 8.69 8.58 13.06 13.0 8.48 13.00 8.39 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test oC 13 0.08 mg/L/minute 0.22 (mg/g)/hr If sewage sludge is > 20°C, SOUR = (mg/g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes If result is 5 1.6 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet (Date & Analyst; �p� :«e�t►sm�[m.,aawd�,'.; dx;:J Y �LiYtY ��nnrym Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: 0.22 9 Total Solids: 22.27 g/L SOUR Time (Minutes) Temperature oC Dissolved Oxygen (mg/L) 0 12.00 9.30 1 12.00 9.28 2 12.00 9.27 3 12.00 9.23 I 4 12.00 9.1 J 5 2AU� 9.09 6 7 8 12.00 12.00 -_ 13A0 9.01 - 95 8.88 9 1. 0 81 10 13.00 8,75 11 13.00 _ 8.68 12 13.00 8.60 13 13.00 8.52 14 13.00 8.44 15 13.00 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 12.5 0.07 mg/Uminute 0.18 (mg/g)/hr If sewage sludge is > 20°C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes if result is 5 1.5 (mg/g)hr version 11/1111 City of Lumberton Environmental Laboratory specific Oxygen uotake Rate (SOUR) Worksheet Date & Analyst: 5128/2019 07378m TO 1010# 2 Day 1 Total Solids f9gLSample volume used for total solids test:Weight of dish: Weight of dish + dried solids: Weight of dried solids:IL Total Solids: SOUR Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test V.LJ M mg/Uminute (mg/gYhr / If sewage sludge is > 20°C, SOUR = ( mg g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr version 11/l/t l City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: stionvu2milp .-'- "9,10 2 Day 2 Total Solids Sample volume used for total solids test: Weight of dish: Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR 5 111.4114 111.5028 0.0914 18.28 mL 9 9 g/L Time Temperature Dissolved (Minutes) Oxygen (mg/L) 'C 0 .8 1 2 21.00 5.661 3 21.00 5.42 5.22 4 uV 5 6 2 .00 _ 21.00 4.87 4.66 7 8 t 20 4.2 g 21.00 4.18 10 21.00 4.01 11 21.00 3.82 12 21.00 21.00 3.64 3.42 13 14 21.00 _ 3.23 15 21.00'. 3.04 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 21 0.19 0.64 mg/L/minute (mg/g)/hr If sewage sludge is > 20"C, SOUR = (mg/g)/hr If sewage sludge is < 20°C, SOUR = = (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Solids Sample volume used for total solids test: 99099999F&AmL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: MO.09g Total Solids: I 18.22 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) aC 0 22.00 4.71 1 2200. 4.58 2 + 22.00 4.49 3 22.00 4.33 4 22.00 4.11 5 22.00 3.96 6 22.00 3.80 7 22.00 3.56 8 2.0 3.36 g 22.00 3.22 10 22.00 3,41 11 22.00 3.32 12 22.00 3.19 13 22.00 2.98 14 2.00 2.8 15 22.00 2_64 Oxygen Consumption Rate SOUR Temperature Correction Average Sewage Sludge Temperature During Test 0.13 mg/L/minute 0.44 (mg/g)/hr if sewage sludge is > 200C, SOUR = ®(mg/g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is 5 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 5/31/2019 0724am TLS Dig# 2 Day 4 Total Solids Sample volume used for total solids test:Ng/L mL W eight of dish: g Weight of dish + dried solids: g Weight of dried solids: g Total Solids: SOUR Time (Minutes) Temperature oC Dissolved Oxygen (mg/L) 0 1 21. 0 21.00 4.94 4.19 2 21.00 3.65 3 21.00 3.44 3.23 3.03 4 21.00 5 2 .00 6 21.00 2.82 7 21.00 _2i61 2.20 2.00 1.80 g 21.00 9 21.00 10 21.00 11 a 21.0 12 21.00 1.58 13 21.00 1.38 14 21.00 1.14 15 21.00 0.95 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test oC 21 0.23 mg/L/minute 0.76 (mg/g)/hr If sewage sludge is > 20°C, SOUR = 0.72 (mg/g)/hr If sewage sludge is < 20°C, SOUR = 0,71 (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr Version 1111/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 6/3/2019 0727am KCL Dig# 2 Day 5 Total Solids Sample volume used for total solids test: 5 mL Weight of dish: 123.1040 g Weight of dish + dried solids: 123.193 g Weight of dried solids: 0.0894 g Total Solids: 17.88 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) °C 0 1 21 6.7 29.0 6.76 2 21.00 +6.66 3 21.00 6,51 4 21. 0 6.4 5 21.00 6.25 6 0 6.11 7 21.00 5. 8 g 21.00 5.9 g 21.00 5.81 10 21.00 5.75 11 2 . 0 21.00 5.68 5.61 12 13 21.00 5.49 14 21.00 5.37 15 21.00 5.23 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 21 0.10 0.35 mg/Uminute (mg/guhr If sewage sludge is > 20°C, SOUR = 0.33 (n1g/g)/hr If sewage sludge is < 20°C, SOUR = F0.33 (n1g/g)Ihr SOUR passes if result is 5 1.5 (mg/g)hr vertion 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 6/4/2019 6:56am KCL Dig# 2 ` T;al Solids Sample volume used for total solids test: 5 mL Weight of dish: Ag/L g Weight of dish + dried solids: g Weight of dried solids: g Total Solids: SOUR Time (Minutes) Temperature 0C Dissolved Oxygen (mg/L) 0 21.00 6.40 1 20.00 6.26 2 21.00 6.01 3 21.00 5.86 4 21.00 5.71 5 21.00 5.56 6 2 .00 5.40 _ _ 5.24 4.95 4.79 7 21.00 8 9 21.00 10 21.00 11 21.00 4.62 12 21.00 4.48 13 21.00 4.32 14 21.00 4.16 15 21.00 4.00 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test 0C 20.9375 0.16 mg/L/minute 0.53 (mg/g)/hr If sewage sludge is > 200C, SOUR = (mg/guhr If sewage sludge is < 200C, SOUR = (mg/g)/hr SOUR passes If result Is 5 1.5 (mg/g)hr Vern n 11/1111 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: c mL Weight of dish: 9 Weight of dish + dried solids: g Weight of dried solids: 0.0922 g Total Solids: 18.44 g/L SOUR Time (Minutes) Temperature 'C Dissolved Oxygen (mg/L) 0 21. 6.47 1 21.00 6.44 2 21.0C 6.28 3 21.00 6.12 5.95 4 21.00 5 1.00 7 8 9 #EE59621.00 21.00 21.00 1.00 8 5.49 5.38 5.27 10 11 12 1.00 21.00 1.00 5.11 4.96 4.81 13 14 15 1.00 21.00 00 4.66 4.50 Oxygen Consumption Rate SOUR S;UR Temperature Correction 0.15 mg/L/minute 0.47 (mg/g)/hr Average Sewage Sludge Temperature During Test oC 21 If sewage sludge is > 20°C, SOUR = o a5 (mg/g)/hr If sewage sludge is < 200C, SOUR = (mg/g)/hr SOUR passes if result Is 5 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: MMMjPL1 Total Solids Sample volume used for total solids test: 10; mL Weight of dish: 123.1043, g Weight of dish + dried solids: llllllllllL1.23.2759 g Weight of dried solids: 0.1716 g Total Solids: 17.16 g/L SOUR Oxygen Consumption Rate 0.25 SOUR IM: SOUR Temperature Correction Average Sewage Sludge Temperature During Test 24 mg/L/minute (mg/g)/hr If sewage sludge is > 20'C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes if result Is 5 1.5 (mg/g)hr Ver$ion 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst:___.1$C_� _ - _DIA#$. .Day 2 Total Solids Sample volume used for total solids test: Weight of dish: Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 25.00 3.47 1 25.00 2.29 2 25.00 1.26 3 25.00 0.56 4 25.00 0.46 5 25.00 0.06 6 25.00 0.05 7 25.00 0.04 8 25.00 0.03 9 25.00 0.03 _ 10 24.00 0.03 11 24.00 0.03 12 24.00 0.03 13 24.00 0.03 14 24.00 0.03 15 24.00 0.03 Oxygen Consumption Rate SOUR SOUR Temperature Correction mL 9 g/L 0.15 mg/L/minute 0.56 (mg/g)/hr Average Sewage Sludge Temperature During Test °C 24.625 If sewage sludge is > 20°C, SOUR = 0.45 (mg/g)/hr If sewage sludge is < 20°C, SOUR = 0.41 _ (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr Version 1111/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 7/9.Z"2 19 7;in KC ._ pig# 2 Day 3 Total Solids Sample volume used for total solids test: 10 mL Weight of dish: LE4126.9148 gWeight of dish + dried solids:27.0831 g Weight of dried solids: 0.1685 g Total Solids: 16.85 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 24.00 4.17 1 24.00 3.87 2 24.00 2.58 3 24.00 2.34 4 25.00 1.40 5 25.00 0.72 6 25.00 0.25 _ 7 25.00 0.25 g 25.00 0.25 g 25.00 0.25 10 25.00 0.24 11 25.00 0.24 12 25.00 0.23 13 25.00 0.23 14 25.00 _ 0.22 15 1 25.00 0.21 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test 0C 24.75 0.24 mg/L/minute 0.85 (mg/g)/hr If sewage sludge is > 20°C, SOUR = 0.67- (mg/g)/hr If sewage sludge is < 20°C, SOUR = 0.62 (mg/g)/hr SOUR passes if result is <_ 1.5 (rng/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxvoen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: 0.0855 g Total Solids: 17.1 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 1 2 23.00 - 11 23.00 23'00 23.00 :.73 .69 .02 .48 •98 3 4 23.00 5 23.00 .71 6 23.00 23.00 3.43 3.17 7 g 23.00 23.00_ .97 •79 g 10 11 23.00 23.011 .55 2.34 12 23.00 2.11 13 14 23.00 23�0 1.66 15 23.00 1.47 Oxygen Consumption Rate SOUR S6UR Temperature Correction Average Sewage Sludge Temperature During Test 0.30 mg/L/minute 1.06 (mg/g)/hr If sewage sludge is > 20°C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes If result Is 5 1.5 (mg/g)hr Vertion 11/1/11 City of Lumberton Environmental Laboratory Specific oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: �t K L DID# 2 Day 5 Total Solids Sample volume used for total solids test: Weight of dish: Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR 5 125.7517 125.8355 0.0838 16.76 mL 9 g/L Time (Minutes) Temperature Dissolved Oxygen (mg/L) ,C 0 1 00 _ 22.00 2.. .04 6.85 2 3 4 22.00 22.00 6,65 6.43 5 22.00 6.26 6 22.00 6.03 7 22.00 5.81 8 22.00 5.60 9 22.00 5.36 10 11 22.00 22.00 5.14 4.94 12 22.00 4.67 13 22.00 4.49 14 22.00 4.27 15 22.00 4.02 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test 0.21 0.77 mg/L/minute (mg/g)/hr if sewage sludge is > 20`C, SOUR = 0.70 (mg/g)/hr If sewage sludge is < 20°C, SOUR =F o.0r nxl/g)/hr SOUR passes if result is 5 1.5 (rng/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxvaen Uptake Rate (SOUR) Worksheet Date & Analyst: Dig# 2 Day 6 Total Solids Sample volume used for total solids test: 5 n1L Weight of dish: 92.9588 9 Weight of dish + dried solids: 93.0427 g Weight of dried solids: 0.0839 g Total Solids: E16.78 g/L SOUR Oxygen Consumption Rate 021 SOUR 0.74 SOUR Temperature Correction Average Sewage Sludge Temperature During Test mg/L/minute (mg/g)/hr If sewage sludge is > 20°C, SOUR = EN(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes If result Is 5 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: � ' Sam KCL Total Solids Sample volume used for total solids test: EA mL Weight of dish: g Weight of dish + dried solids: g Weight of dried solids: g Total Solids: g/L SOUR Time Temperature Dissolved (Minutes) Oxygen (mg/L) oC 0 22.00 _6. 1 22.00 6.63 2 22.00 _ 6.47__ 3 22.00 '' 6.31 4 22.00 _ 6.12 5 22.00 5.93 6 22.00 5.74 7 22.00 5.54 6 22.00 5.34 9 22.00 _ 5.14 10 22.00 4.92 4,73 11 22.00 - 12 22.00 4.52 13 22.00 - 4.30 14 22.00 ` 4.10 3,98 15 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test 0.19 0.70 mg/Uminute (mg/g)/hr If sewage sludge is > 20°C, SOUR = 01(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes If result Is 5 1.5 (mg/g)hr Vertion 11/1/11 City of Lumberton Environmental Laboratory Soeciflc Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: mL Weight of dish: g Weight of dish + dried solids:"g/L g Weight of dried solids: g Total Solids: SOUR Time (Minutes) Temperature oC Dissolved Oxygen (mg/L) 0 1 .00 2.00 4.62 4.23 2 22.00 3.94 3 22.00 3.62 4 5 22.00 22.00 3.34 3.01 6 22.00 2.70 7 22.00 2.36 8 22.00 1.96 9 22.00 1.75 10 22.00 1.41 11 22.00 1.08 12 22.00 0.78 13 14 22.00 23.00 0.45 0.18 15 23.00 0,16 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test oC 22.125 0.31 mg/Uminute 1.17 (mg/g)/hr If sewage sludge is > 20°C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes If result is 5 1.5 (mg/g)hr Version 1111/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: j�s:.u,,®_...AQ-_...:A"_.>AY11 ._...:: Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 7Tg/L 9 Weight of dried solids: g Total Solids: SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 20.00 5.00 1 20.00 3.94 2 20.00 2.62 3 20.00 2.46 4 21.00 2.18 5 21.00 1.96 6 21.00 1.71 7 21.00 1.42 8 21.00 1.13 9 21.00 0.92 10 21.00 0.67 11 21.00 0.18 12 21.00 0.15 13 21.00 0.14 14 21.00 0.13 15 21.00 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test oC 20.75 0.29 mg/Uminute 1.08 (mg/gYhr If sewage sludge is > 20°C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes If result is <_ 1.5 (mg/g)hr Version 1111/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 10/10/2019 7:22am KCL Dig#2. t.-� :ii Total Solids Sample volume used for total solids test: 5 mL Weight of dish: 125.7519 g Weight of dish + dried solids: 125.8282 g Weight of dried solids: 0.0763 g Total Solids: 15.26 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) aC 0 20.00 2.70 1 20.00 2.00 2 20.00 1.90 3 20.00 1.63 4 20.00 1.42 5 20.00 1.36 6 20.00 1.15 7 20.00 0.92 6 NMI 0.71 g " ,20.00 0.52 10 0.00 0.29 11 20.00 0.27 12 20.00 0.26 13 20.00 0.25 14 20.00 0.23 15 20.00 0.22 Oxygen Consumption Rate SOUR SOUR Temperature Correction 0.16 mg/L/minute 0.61 (mg/g)/hr Average Sewage Sludge Temperature During Test 20 If sewage sludge is > 20°C, SOUR = 0.61 (mg/g)/hr if sewage sludge is < 20°C, SOUR = 0 (mg/g)/hr SOUR passes If result is 5 1.5 (mg/g)hr Version 1111111 City of Lumberton Environmental Laboratory Specific Oxy-gen Uptake Rate (SOUR) Worksheet Date & Analyst: 10111/2019 7:17am KCL Dig# 2 Day 4 Total Solids Sample volume used for total solids test: 5 mL Weight of dish: 120.5344 g Weight of dish + dried solids: 120.6153 g Weight of dried solids: 0.0809 g Total Solids: 16.18 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) °C p 20.00 2.04 1 20.00 1.86 2 20.00 1.11 3 20.00 0.86 4 20.00 0.70 5 20.00 0.44 6 20.00 0.30 7 20.00 0.28 g 20.00 0.25 g 20.00 0.25 10 20.00 0.24 11 20.00 0.23 12 20.00 0.22 13 20.00 0.21 14 20.00 0.21 15 20.00 0.20 Oxygen Consumption Rate SOUR SOUR Temperature Correction 0.10 mg/Uminute 0.38 (mg/g)/hr Average Sewage Sludge Temperature During Test 20 if sewage sludge is > 20°C, SOUR = M(mg/g)/hr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes if result is:5 1.5 (mg/g)hr Version 11/1111 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: Total Solids Sample volume used for total solids test: . _'�' _� mL Weight of dish: 4_ 9 Weight of dish + dried solids: "'t 9 Weight of dried solids: 0.0800 g Total Solids: 16 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) 0C 0 21.00 4.45 1 21.00 4.40 2 21.00 3.90 3 21.00 3.75 4 1 21.00 3.60 5 21.00 3.30 6 21.00 3.00 7 21.00 2.91 8 21.00 2.76 9 21.00 2.50 10 21.00 2.31 11 21.00 1.00 12 21.00 0.70 13 21.00 0.19 14 21.00 0.12 15 21.00 0.06 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test 0C 21 0.32 mg/Uminute 1.18 (mg/g)/hr If sewage sludge is > 20°C, SOUR = M(mg/g)lhr(mg/g)/hr If sewage sludge is < 200C, SOUR = SOUR passes If result is 5 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: • J Total Solids Sample volume used for total solids test: mL Weight of dish: 9 Weight of dish + dried solids: 9 Weight of dried solids: Tg/L g Total Solids: SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 20.00 4.08 1 20.00 3.87 2 20.00 3.61 3 20.00 3.39 4 20.00 3.15 5 20.00 2.94 6 20.00 2.71 7 20.00 2.49 8 20.00 2.26 9 20.00 2.07 10 20.00 1.87 11 20.00 1.66 12 20.00 1.44 13 20.00 1.18 14 20.00 1.00 15 20.00 0.80 Oxygen Consumption Rate SOUR SOUR Temperature Correction 0.22 mg/Uminute 0.78 (mg/g)/hr Average Sewage Sludge Temperature During Test oC 20 if sewage sludge is > 20°C, SOUR = M(mg/g)lhr(mg/g)/hr If sewage sludge is < 20°C, SOUR = SOUR passes If result is 5 1.5 (mg/g)hr Version 1111/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 10/16/2019 7:20am KCL Dig# 2 Day 7 } Total Solids Sample volume used for total solids test: 5 mL Weight of dish: 12Mg/L g Weight of dish + dried solids: 12g Weight of dried solids: g Total Solids: SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 i .00 4.20 1 19.00 4.05 2 19.00 3.90 3 19.00 3.75 4 19.00 3.60 5 19.00 3.44 6 19.00 3.28 7 19.00 3.12 8 19.00 2.97 9 19.00 2.81 10 19.00 2.65 11 19.00 2.49 12 19.00 2.33 13 19.00 2.90 14 19.00 2.00 15 19.00 Oxygen Consumption Rate SOUR SOUR Temperature Correction 0.15 mg/Uminute 0.59 (mg/g)/hr Average Sewage Sludge Temperature During Test oC 19 If sewage sludge is > 20°C, SOUR = (mg/gyhr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is 5 1.5 (mg/g)hr Version 11/1/11