WQ0003504_2019 Residual Annual Report_20200228

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Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0003504
Applicant\Permittee * SYNAGRO
Facility Name * City of Durham
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for City of Durham. The paper copy is being hand delivered today by Ryan Copeland.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
DURHAM NC 2019 Annual Report FINAL.pdf 20.86MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/28/2020

435 NNUiams COMP[, SuiLe 100
Baltimore, AID 21220
ynagro.com
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. W00003504
Dear NCDEQ:
Synagro is submitting one hard copy and one electronic copy of the above referenced report on
behalf of the City of Durham, NC.
If you have any questions or need additional information, please do not hesitate to contact Don
Greeley at [phone] or Ryan Copeland at (336) 60744941
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Don Greeley, City of Durham
Ryan Copeland,Synagxo
YOUR PARTNER FORA CLEANER, GREENER WORLD

CITY OF DURHAM, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003504
2019 ANNUAL REPORT

City of Durham, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0003504 County Durham Year2019
Facility Name (as shown on permit) North Durham WRF South Durham WRF Brown WTP, Williams WTP & Lick Creek W WTP
NPDES No. NC0023841 NC0047597 03-32-010(A), 03-32-010(B), NC0026310
Land Application Operator Svnaao Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES _NO. If NO, skip Part A. and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 175
Total number of fields utilized for land application during the year: 48
Total amount of dry tons applied during the year for all application sites: 5245.38
Total number of acres utilized for land application during the year: 1420.50
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
I1. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12, No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
A. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C —Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belied true, accurate, and complete. .
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Don Greeley Director of Water Management
Permittee Name and Title (type or print)
Signature ofPrepazer* Date
(if different from Pemvttee)
*Prepazer is defined in 40 CFR Part 503.9(r) and ISA NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
DURHAM,NC
DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
DRY METRIC
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
February 2019
1,092.00
Y
170.15
D
154.32
March 2019
21637,00
Y
379.79
D
344.47
April 2019
27219.00
Y
319.60
D
289.86
May 2019
11821,00
Y
256.14
D
232.32
June 2019
11349.00
Y
189.74
D
172.11
July 2019
41277,00
Y
551.15
D
499.90
August 2019
37112.00
Y
408.88
D
370.87
September 2019
2,693.00
Y
353.83
D
320.91
October 2019
1,924.00
Y
252.79
D
229.28
YEARLY TOTAL
211124.00
Y
21882,07
D
21614,04
DURHAM, NC S. DURHAM WWTP
ANAEROB.
DIGESTED
CAKE
DRY METRIC
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
April 2019
1,393.00
Y
198.28
D
179.81
May 2019
4731.00
Y
661.46
D
599.90
August 2019
21727.00
Y
383.56
D
347.89
September 2019
2,061.00
Y
289.88
D
262.93
October 2019
11086,00
Y
154.58
D
140.20
November 2019
925.00
Y
126.20
D
114.47
YEARLY TOTAL
12,923.00
Y
11813.96
D
1,645.20
DURHAM, NC BROWN WTP CAKE
DRY METRIC
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
March 2019
194.67
W
32.70
D
29.66
April 2019
81.64
W
13.72
D
12.44
May 2019
486.10
W
95.77
D
86.86
June 2019
82.95
W
16.34
D
14.82
July 2019
631.67
W
124.43
D
112.87
August 2019
351.77
W
64.02
D
58.07
September 2019
454.95
W
82.80
D
75.11
October 2019
529.42
W
88.42
D
80.19
November 2019
122.94
W
20.53
D
18.63
December 2019
63.56
W
10.62
D
9.63
YEARLY TOTAL
21999,67
W
549.35
D
498.28
1 /30/2020

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003504 Laboratory
Facility Name: DURHAM, NC PACE ANALYTICAL SERVICE INC.
NPDES# : NCO023841 Waypoint Analytical Virginia Inc.
or WQ# (residual only)
WWTP Name: NORTH DURHAM WWTP
Residuals Analysis Data
Product Type
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
Date Sampled (grab) or
01/07/19
02/20/19
04/22/19
06/19/19
07/24/19
09/11/19
11/06/19
Date Composited
Percent Solids
18,50
17,10
16,70
15,30
15,60
15,60
14,00
PARAMETERS (mglkg
dry weight)
Arsenic
<3.7
5,09
<5
<5
<5
5,07
4,56
Cadmium
1
<1
<1
<1
<1
1,1
1,18
Mercury
0,26
0,316
0,398
0,385
0, 617
0,358
0,432
Chromium
NR
23.5
31.1
36.2
30
32.4
22.8
Copper
383
353
324
353
382
437
507
Lead
19
19.1
16.4
16.7
17.3
24.8
22.8
Molybdenum
7.5
6,86
6,71
7,69
8,38
12.2
16.3
Nickel
19.1
2045
23.2
22.4
21.2
22.4
20.6
Selenium
3,8
<5
<5
<5
5,11
<5
7,06
Zinc
1990
2020
1940
2560
2990
3060
3530
Total Phosphorus
30200
33100
32100
26600
23700
28700
34500
TKN
54200
56700
55800
63500
57400
50900
69700
Ammonia -Nitrogen
6680
8130
8080
9020
11000
10400
14300
Nitrate and Nitrite
86.1
<4. 92
<5
30.8
<4.55
<4. 88
<32, 8
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
E
Date 212y/Z
DENR FORM RSSF (5/2003) Panted' Thursday- January 30 2020 at 16'28'17 for' 2012 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
WQ000300
Laboratory
Facility Name:
DURHAM, NC
PACE ANALYTICAL
SERVICE INC.
NPDES# :
NCO023841
Waypoint
Analytical Virginia Inc.
or WQ# (residual only)
WWTP Name:
NORTH DURHAM WWTP
Residuals Analysis
Data
Product Type
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
Date Sampled (grab) or
01/07/19
02/20/19
04/22/19
06/19/19
07/24/19
09/11/19
11/06/19
Date Composited
Percent Solids
18,50
17,10
16,70
15,30
15. 60
15 60
14 00
,
,
PARAMETERS (mg/kg
dry weight)
Aluminum
16000
15400
14600
11900
11200
14400
14000
Calcium
12500
14100
12900
12300
12900
14000
17400
Magnesium
5850
6000
6680
6660
5490
6930
8570
pH
6,40
8.50
8,30
8,10
8,40
8,50
8,30
Potassium
2250
2460
2700
3050
3000
3760
4940
Sodium
<1830
462
474
584
593
660
914
"I certify under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date 2�zy/2o
NR -Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) _Printed: Thursday - danuary 30 202o at 1829 47 for 2ot2 01

laceAnalyticalo
wxvrPa bbs.=
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 15, 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: Durham -North
Pace Project No.: 92413361
Dear Nate Roth:
Enclosed are the analytical results for samples) received by the laboratory on January 08, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
p`eo 7 —
Lord
Patton
lorri. [e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Page 1 of'16

Project: Durham -North
Pace Project No.: 92413361
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: WNC030
North Carolina Drinkinq Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
vrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Page 2 of 16

aceAnalXicale
W ,psccfab&wm
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Durham -North
92413361
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92413361001
Durham -North 1 of 6
EPA6010D
DS
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA9045D
SMK
1
PASI-A
SM 271 OB-2011
DMN
1
PASI-A
EPA 350.1 Rev 2.01993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.01993
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not 6e reprotlucetl, except in Full,
without the written consent of Pace Analytcal Services, LLC. Page 3 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersmile, NC 28078
p04j875-9092
ANALYTICAL RESULTS
Project: Durham -North
Pace Project No.: 92413361
Sample: Durham -North 1 of 6 Lab ID: 92413361001 Collected: 01/07/19 09:45 Received: 01/08119 12:45 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 30506
Aluminum
16000
mg/kg
36.5
1
01 /11/1909:20
01/13/1922:49
7429-90-5
Arsenic
ND
mg/kg
3.7
1
01/11/1909:20
01113/1922:49
7440-38-2
Cadmium
1.0
mg/kg
0.37
1
01/11/1909:20
01113/1922:49
7440-43-9
Calcium
12500
mg/kg
36.5
1
01/11/1909:20
01113/1922:49
7440-70-2
Copper
383
mg/kg
1.8
1
01/11/1909:20
01/13/1922:49
7440.50-8
Lead
19.0
mg/kg
1.8
1
01/11/1909:20
01/13/1922:49
7439-92-1
Magnesium
5850
mg/kg
36.5
1
01/11/1909:20
01/1311922:49
7439-95-4
Molybdenum
7.5
mg/kg
1.8
1
01/11/1909:20
0111311922:49
7439-98-7
Nickel
19A
mg/kg
1.8
1
01/11/1909:20
0111311922:49
7440-02-0
Potassium
2250
mg/kg
1830
1
01/11/19
09:20
01/13/19
22:49
7440-09-7
Selenium
IS
mg/kg
3.7
1
01/1111909:20
01/13/1922:49
7782-49-2
Sodium
ND
mg/kg
1830
1
01/11/1909:20
01/13/1922:49
7440-23-5
Zinc
1990
mg/kg
3.7
1
01/11/1909:20
01/13/1922:49
7440-66-6 BC
7471 Mercury Analytical Method: EPA 7471B Preparation Method: EPA 74716
Mercury
2540G Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365A Phosphorus, Total
Phosphorus
0.26
mg/kg
0.023 1
01/11/1921:31
17700
mg/kg
0.12 1
01/15/1911:49
N2
Analytical Method:
EPA 350.1
Rev 2.0
1993 Mod. Preparation Method:
EPA 350.1
Rev 2.0 1993 Mod.
6680
mg/kg
381 10 01112/1910:40
01/12/1916:28
7664-41-7
Analytical Method:
EPA 351.2
Rev 2.0
1993 Preparation Method:
EPA 351.2 Rev
2.0
1993
64200
mg/kg
2700 10 01/14/1911:34
01/15/19
05:56
7727-37-9
Analytical Method:
EPA 353.2
Rev 2.0
1993 Preparation Method:
EPA 353.2 Rev
2.0
1993
103
mg/kg
10.2 1 01/10/1901:57
01/10/19
03:50
86.1
mg/kg
10.2 1 01/10/1901:57
01/10/1903:50
14797-55-8
17.1
mg/kg
5.1 1 01/10/1901:57
01/10/1903:50
14797-65-0
Analytical Method:
EPA 365.1
Rev 2.0
1993 Preparation Method:
EPA 365.1 Rev
2.0
1993
30200
mg/kg
1020 100 01109/1920:23
01/10/1915:13
7723A4-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 16
---, . , _ 1..,.

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Durham -North
Pace Project No.: 92413361
QC Batch: 452089
Analysis Method: EPA 7471 B
QC Batch Method: EPA7471B
Analysis Description: 7471 Mercury
Associated Lab Samples: 92413361001
METHOD BLANK: 2472136
Matrix: Solid
Associated Lab Samples: 92413361001
Blank Reporting
Parameter Units
Result Limit
Analyzed
Qualifiers
Mercury mg/kg
ND 0.0060
01/14/1912:06
LABORATORY CONTROL SAMPLE: 2472137
Spike LCS
LCS
% Rec
Parameter Units
Cone. Result
% Rec
Limits Qualifiers
Mercury mg/kg
0.083 0.067
81
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472138 2472139
MS MSD
92413378001
Spike Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Cone Cone. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.0063
0,055 0.057 0.048
0.049
75 75 75-125 3
Rosults prosonfod on this pago aro in tho units intlicaWd by tho "Units" column oxcopf whom an alfomafo unit is prosonfod fo the Aght of No result
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotluced, except in full,
Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLQ Page 5 of 16

Project: Durham -North
Pace Project No.: 92413361
QC Batch: 451935
QC Batch Method: EPA 3050E
Associated Lab Samples: 92413361001
METHOD BLANK: 2471114
Associated Lab Samples: 92413361001
Parameter
Units
Aluminum
m9/k9
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum -
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 6010D
Analysis Description: 6010 MET
Matrix: Solid
Blank
Result
Reporting
Limit
Analyzed
Qualifiers
ND
10.0
01113/1922:18
ND
1.0
01/13/1922:18
ND
0.10
01/13/1922:18
ND
10.0
01/1311922:18
ND
0.50
01/13/1922:18
ND
0.50
01/13/1922:18
ND
10.0
01/13/1922:18
ND
0.50
01/13/1922:18
ND
0,50
01/13/1922:18
ND
500
01/13/19
22:18
ND
1.0
01/13/19
22:18
ND
500
01/13/19
22:18
ND
1.0
01/13/19
22:18
BC
LABORATORY CONTROL SAMPLE:
Parameter
2471115
Units
Spike
Conc.
LCS
Result
LCS
%Rec
%Rec
Limits
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Qualifers
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE:
2471116
2471117
MS
MSD
92413357001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum
mg/kg
55600
9280
8310
69300
63600
148
96
75-125
9 M1
Arsenic
mg/kg
ND
928
831
827
734
89
88
75-125
12
Cadmium
mg/kg
ND
928
831
848
758
91
91
75-125
11
Results presented on this page are in No units lntlieatotl by the "Units" column except wham an alternate unit is presented to tho right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotluced, except in full,
Date: 0111512019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16

QUALITY CONTROL DATA
Project: Durham -North
Pace Project No.: 92413361
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE
Parameter
DUPLICATE: 2411116
MS
92413357001 Spike
Units Result Cone,
MSD
Spike
Cone.
2411111
MS
Result
MSD
Result
MS
% Rec
MSD
% Rae
%Rec
Limits
RPD Qua]
Calcium
mg/kg
17500
9280
8310
27500
25000
107
90
75-125
9
Copper
mg/kg
393
928
831
1350
1220
103
99
75-125
10
Lead
mg/kg
23.2
928
831
865
770
91
90
75-125
12
Magnesium
mg/kg
3700
9280
8310
12700
11400
97
93
75-125
11
Molybdenum
mg/kg
11.7
928
831
900
804
96
95
75-125
11
Nickel
mg/kg
15.5
928
831
871
778
92
92
75-125
11
Potassium
mg/kg
ND
9280
8310
13000
11900
97
95
75-125
9
Selenium
mg/kg
ND
928
831
783
687
84
82
75-125
13
Sodium
mg/kg
ND
9280
8310
11100
10100
92
91
75-125
10
Zinc
mg/kg
1880
928
831
2770
2570
97
84
75-125
8
Results prosonwd on NIs pago aro in the units Intlitatotl by Cho "Units" Column oxtept whoro an altoma[o unit is prosantod to Cho tight of Cho rosult
Date: 01/15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotluceo, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 16

Project: Durham -North
Pace Project No.: 92413361
QC Batch: 451773
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92413361001
SAMPLE DUPLICATE: 2470313
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2470314
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92413062001 Dup
Units Result Result
% 1.1 0.80
92413381002 Dup
Units Result Result
% 96.7 96.7
RPD Qualifiers
35 D6
RPD Qualifers
0
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Rosults prosonWtl on NIs pago aro In the units intlicaWd by tho "Units" column oxcept whom an altomato unit is prosonfad to the right of tho result
REPORT OF LABORATORY ANALYSIS
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Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

aceAnalytical
w ..pacela6smm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Durham -North
Pace Project No.: 92413361
..... __... _....
QC Batch: 452172
QC Batch Method: EPA 9045D
Associated Lab Samples: 92413361001
SAMPLE DUPLICATE: 2472426
Parameter Units
PH at 25 Degrees C Std. Units
SAMPLE DUPLICATE: 2472427
Parameter
pH at 25 Degrees C
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
92413563001 Dup
Result Result RPD Qualifiers
5.2 5.3 0 H3
92413312001 Dup
Units Result Result RPD Qualifiers
Std. Units 6.8 6.8 0 H3
Rosults prosontotl on this pago aro in tho units indicated by Cho "Units" Column oxcopt whoro an alfomaco unit is prosontotl to tha right of Cho rosult
REPORT OF LABORATORY ANALYSIS
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Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Durham -North
Pace Project No.: 92413361
QC Batch: 452023
Analysis Method: EPA
350.1 Rev 2.0 1993
Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92413361001
METHOD BLANK: 2471582
Matra: Solid
Associated Lab Samples: 92413361001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/kg
ND 8.9
01/12/1915:09
LABORATORY CONTROL SAMPLE: 2471583
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
%Rec Limits
Qualifiers
Nitrogen, Ammonia mg/kg
472
464
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471594
2471585
MS
MSD
92413357001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result %Rec
%Rec
Limits
RPD Qual
Nitrogen, Ammonia mg/kg 13200
10300
10500 21800
22500 83
89
90-110
3 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471586
2471587
MS
MSD
92413358001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Nitrogen, Ammonia mg/kg ND
2320
2320 2210
2210 93
93
90-110
0
Rosults prosontod on this page am In tho units intlicatotl by tho "Units" column execpt whero an altomate unit is prosontetl to tho right of tho result
Date: 01 /15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Page 10 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Durham -North
Pace Project No.: 92413361
QC Batch: 452219
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Associated Lab Samples: 92413361001
METHOD BLANK: 2472536
Matrix: Solid
Associated Lab Samples: 92413361001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND 50.0
01/15/19
04:45
LABORATORY CONTROL SAMPLE: 2472537
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits
Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000
967
97
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472538
2472539
MS
MSD
92413357001
Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 62000
21200
19000 74700
74800
60
67
90-110
0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472540
2472541
MS
MSD
92413358001
Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result
%Rec
%Rec
Limits
RPD Qua[
Nitrogen, Kjeldahl, Total mg/kg 5230
5170
5170 8110
9500
56
83
90-110
16 M11R1
Rosults prcsuntotl on this pogo arc in Cho units intlicatod by No "Units" Column oxeopt whoro an altomato unit Is proson[od to tho right of Cho rosult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 16

i
Project: Durham -North
Pace Project No.: 92413361
QC Batch: 451629
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92413361001
QUALITY CONTROL DATA
Analysis Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
METHOD BLANK: 2469664
Matrix:
Solid
Associated Lab Samples: 92413361001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Nitrogen, Nitrate
mg/kg
ND
2.0
01/10/1903:42
Nitrogen, Nitrite
mg/kg
ND
0.98
01/10/19 03:42
Nitrogen, NO2 plus NO3
mg/kg
ND
2.0
01/10/19 03:42
Qualifiers
Pace Analytical Services, LLC
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2469665
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.9 15.8
106 90-110
Nitrogen, Nitrite
mg/kg
9.9 10.6
107 90-110
Nitrogen, NO2 plus NO3
mg/kg
24.8 26.4
107 90-110
MATRIX
SPIKE &MATRIX
SPIKE DUPLICATE:
2469666
2469667
MS
MSD
92413357001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone,
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Nitrogen,
Nitrate
mg/kg
ND
425
420
412
393
97
93
90.110
5
Nitrogen,
Nitrite
mg/kg
ND
286
280
305
308
100
102
90-110
1
Nitrogen,
NO2 plus NO3
mg/kg
ND
711
702
717
701
100
99
90-110
2
Rosults prosontotl on this page am in No units Intlicatotl try the "Units" column oxcopt where an altomate unit is prosontotl to tho tight of the rosult
REPORT OF LABORATORY ANALYSIS
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date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

Project: Durham -North
Pace Project No.: 92413361
QC Batch: 451598
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92413361001
METHOD BLANK: 2469443
Associated Lab Samples: 92413361001
Parameter Units
Phosphorus mg/kg
LABORATORY CONTROL SAMPLE: 2469444
Parameter Units
Phosphorus mg/kg
QUALITY CONTROL DATA
Analysis
Method:
EPA 365.1 Rev 2.0
1993
Analysis
Description:
365.1 Phosphorus,
Total
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 01/10/1913:45
Spike LCS
no. Result
49 52.3
Pace Analytical Services, LLC
98OD Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS %Rec
Rec Limits Qualifiers
107 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2469445 2469446
MS MSD
92413357001 Spike Spike MS MSD MS MSD %Rec
Parameter Units .Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phosphorus mg/kg 24300 1100 1100 23200 23300 -99 -88 90.110 1 M6
Rosults prosontod on this pago aro In tho unite lndicafod by tiro "Units" column oxcopt whom an altomate unit is prosontod to the right of fho result
REPORT OF LABORATORY ANALYSIS
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Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, L-C. Page 13 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Durham
-North
Pace Project No.: 92413361
DEFINITIONS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) -Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC -Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in Sw846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical
Services -
Asheville
PAS[-C
Pace Analytical
Services -
Charlotte
ANALYTE QUALIFIERS
gC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
late: 01l15/2019 01;37 PM out the written consent of Pace Analytical Services, LLG Page 14 of 16

9001
aceAnalytical
w,m:pawlabawiw
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Durham -North
Pace Project No.: 92413361
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92413361001 Durham -North I of EPA 3050B 451935 EPA6010D 451945
92413361001 Durham -North 1 of 6 EPA 7471 B 452089 EPA 7471 B 452120
92413361001 Durham -North 1 of SM 2540G-2011 452044
92413361001 Durham -North 1 of 6 ASTM D2974-87 451773
92413361001 Durham -North 1 of 6 EPA 9045D 452172
92413361001 Durham -North 1 of 6 SM 2710E-2011 452503
92413361001 Durham -North 1 of 6 EPA 350.1 Rev 2.0 1993 452023 EPA 350.1 Rev 2.0 1993 452144
Mod, Mod.
92413361001 Durham -North 1 of 6 EPA 351.2 Rev 2.0 1993 452219 EPA 351.2 Rev 2.0 1993 452403
92413361001 Durham -North 1 of 6 EPA 353.2 Rev 2.0 1993 451629 EPA 353.2 Rev 2.0 1993 451647
92413361001 Durham -North 1 of 6 EPA 365.1 Rev 2.0 1993 451598 EPA 365.1 Rev 2,0 1993 451656
REPORT OF LABORATORY ANALYSIS
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Ite: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 16

7i[8

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range Ratio
201&01-ANDCAK-NC
DURHAM, NC N. DURHAM WWTP ANAEROB,
1/7/2019
1/1/2019-2/28/2019 1.4510
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (1830 x 18.5000) + 100 = 338.55
Ca mg/I = (Ca mg/kg x %Solids) + 100 = (12500 x 18.5000) + 100 = 2312.5
Mg mg/I = (mg mg/kg x %Solids) + 100 = (5850 x 18.5000) + 100 = 1082.25
Na meq = Na mg/I + Molec.Wgt.Na = 338.55 + 23 = 14.7196
Ca meq = Ca mg/I + MoleaWgt.Ca = 2312.5 + 20 = 115.625
Mg meq = Mq mg/I + Molec.Wgt.Mg = 1082.25 + 12 = 90.1875
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 14.7196 + SgrRoot[0.5(115.625+g0.1875)] = 1.45102
Page 1
Printed: 1/30/2020
16:45

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypoi ntan a lytica Isom
3/1 /2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-052-0204
Project Description: Durham North
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/2112019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attacheAD A, of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 267 South Carolina 93007
Page 1 of 6

ry 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-052-0204
Client Project Description: Durham North
Lab No Client Sample ID
Durham
North
2 of 6
Durham
North
2 of 6
Durham
North
2 of 6
Durham
North
2 of 6
Durham
North
2 of 6
Durham
North
2 of 6
Durham
North
2 of 6
Durham
North
2 of 6
Matrix Date Collected Date Received Method Lab ID
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
WiN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
02/20/2019
10:15
02/21/2019
02/20/2019
10:15
02/21/2019
02/20/2019
10:15
02/21/2019
02/20/2019
10:15
02/21/2019
02/20/2019
10:15
02/21/2019
02/20/2019
10:15
02/21/2019
02/20/2019
10:15
02/21/2019
02/20/2019
10:15
02/21/2019
Page 2 of 6
SM-4500-NH3C
WTN
9045D
WiN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WiN
SM-4500-NH3C-TKN
WTN
SM-2540G
WTN

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7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 4W I
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-052-0204
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? ® Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? ® Yes 0 No
Sample containers intact? 40 Yes 0 No
Sufficient sample volume for indicated test(s)? ® Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. ® Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
F- High concentration container (48 hr) F- Low concentration EnCore samplers (48 hr)
F- High concentration pre -weighed (methanol -14 d) F- Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 4D No
Comments:
Signature: Brandi Watson Date &Time: 02/21/2019 11:03:19
Page 5 of 6

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Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 2/20/2019 3/1/20194/30/2019 0.3384
DIGESTED CAKE
Na mq/I = (Na mg/kg x %Solids) + 100 = (462 x 17.1000) + 100 = 79.002
Ca mq/I = (Ca mg/kg x %Solids) + 100 = (14100 x 17.1000) + 100 = 2411.1
Mg mg/I = (mg mg/kg x %Solids) + 100 = (6000 x 17.1000) + 100 = 1026
Na meq = Na mg/I + Molec.Wgt.Na = 79.002 + 23 = 3.43487
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2411.1 +20 = 120.555
Mg meq = Mg mg/I + Molec.Wgt.Mg = 1026 + 12 = 85.5
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.43487 + SgrRoot(0.5(120.555+g5.5)] = 0.338403
Page 1
Printed: 1/30/2020
16:45

7621 Whitepine Road, Richmond, VA 23237
Main 804443-9401 0 Fax [phone]
www.waypo inta nalytica I. com
5/1 /2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-114-0206
Project Description: North Durham
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/24/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minu':es of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Anal ysis(s). Results for solid matrices are reported on an as -
received basis unless othe wise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.wayp o f nta n a lytica I. c o m
Sample Summary Table
Report Number: 19414-0206
Client Project Description: North Durham
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
SM-4500-NH3C
WTN
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
9045D
WTN
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
4500NO3F-2011
WTN
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
6010D
WTN
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
SW-7471B
WTN
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
SM-4500-NH3C-TKN
WTN
66050
North
Durham
Solids
04/22/2019
09:45
04/24/2019
SM-254OG
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

rceport Number: 19-114-0206
Account Number: 46451
and To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : North Durham
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
wwwowayp o i nta nalyti ca I. co m
Lab Number: 66050 REPORT OF ANALYSIS Date Sampled: 4/22/2019 09:45:00
Sample Id North Durham
Date Received: 04/24/2019 00:00
:
Date Reported: 05/01/2019
Total Solids * 16.70 167000 100.0 ADM 04/25/2019 16:21
Moisture * 83,30
100.0 ADM 04/25l201916:21
Total Kjeldahl Nitrogen 5,58 55800 250
Phosphorus 3,21 JPJ 04l29/2019 09:37
32100 50.0 KKM 04/28/201918:18
Potassium 0,27 2700 50.0 KKM 04/28/201918:18
Sulfur 1,04 10400 50.0 KKM 04/28/201918:18
Calcium 1.29 12900 250 KKM 04/28/201918:18
Magnesium 0.67 6680 50.0 KKM 04/28/201918:18
Sodium 0.05 474 250 KKM 04/28/201918:18
Iron 47400 50.0 KKM 04/28/201918:18
Aluminum 14600
50.0 KKM 04/28/201918:18
Manganese
526 5.00 KKM 04/28/201918:18
Copper 324 2.50 KKM 04/28/201918:18
Zinc 1940 12.5 KKM 04/28/201918:18
Ammonia Nitrogen 0.81 8080 100 JPJ 04/26/2019 12:00
Organic N 4.77 47720 250 04/26/2019 12:00
Nitrate+Nitrite-N <5.00 5.00 ZBD 04130/201912:49
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use ofour clients, and maynof be reproduced in �^rhole or pad, normay any reference be made
(o the work the results, or the company in any advertisiny, news release, orofherpublic announcements without obtaining ourpriorviilten authorization.
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
Pauric McGroary
Agronomist
Page 3 of 6

Report Number: 19-114-0206
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number : 66050
Sample Id : North Durham
Project : North Durham
REPORT OFANALY% I
7621 Whitepine Road, Richmond, VA 23237
Main 804.743-9401 0 Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/22/2019 09:45:00
Date Received: 04/24/2019 00:00
Date Reported: 05/01/2019
Cadmium <1.00 1.00 KKM 04l28l201918:18 6010D
Chromium 31A 2.50 KKM 0412812019 18:18 6010D
Nickel 23.2 2.50 KKM 04128/201918:18 6010D
Lead 16.4 3.00 KKM 04/28/201918:18 6010D
Arsenic <5.00 5.00 KKM 04/28/201918:18 6010D
Mercury 0.398 0.0156 TJS 04/30/201912:21 SW-7471B
Selenium <5.00 5,00 KKM 04/28/201918:18 6010D
pH " 8.3 JSL 04/29/2019 06:46 9045D
Molybdenum 6.71 2,50 KKM 04/28/201918:18 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time �t �G MC 60wr
Our reports and letters are /orthe exclusive and confidential use of our clients, and may not be reproduced in whole or part, normay any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, orofherpublic announcements wihrouf obtaining owphor written authorization. AgrOnOmlSt
Page 4 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401°Fax [phone]
www.waypoi nta na lytica 1. com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-114-0206
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: �—
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers received F 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? ® Yes No
Sample containers intact? ® Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes No
Cooler/Samples arrived at the laboratory on ice. 0 Yes No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No 4D N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No 4D N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) F— Low concentration EnCore samplers (48 hr)
F— High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments:
Signature: Brandi Watson Date &Time: 04/24/2019 13:23:18
Page 5 of 6

SAMPLING LOG q
• '' -i, r� G '1 ,
'• ' C/•
•
A �` L CUSTOMER
LAt3 � SAMPLE I.A. SAMPLINq
n. ,�,_ LOCATION
..��ruyutsned by Sampler: v
Relinquished by; �+u
Relinquished by:
II"IIIII'IIIIIII��'II���illll�fifll���i�"II�11'II"II�'IIII�'�0�g12079 �C %119i
Smaaro Central LLC/ 19-714.0206
Durham � ����®��
North Durham
13:22:53 �®��
were used dur/rig the co/%ctlo - fn'q prO--_ �Bdures _
n of those samples
D....
SAMPLE sAMPLER-�-�`u9vv�
TypE ti OF SAMPLING
CONTAINERS DATE METHOb
SL/COME TIME pRESERVEp
� 9�ZZ/9 o9Ys lCE
bate Time
LI,g 231 o ReDreved by:
REMARKS;
ate I Time o,._._
SPECIALINST mare
RUCTIONS; � a � Tlmp Recleved by;
For NL �0� �oG
-- n„� —_ monitoring purposes, � � G
uAMPLE
l.D. PON:
SL7 SL2 NH4-N NO N Orpanlc ANALYSIS
�uPafhM '` Pd Cd Cr NI REQUEST
Pb
NU P� � p� B� � l� As Fly So pH taco, vDlatnD
—_ a ulv, Solids Mo
SL9: Total Solids (Moisture), Total KJeldahi Nitro
SL2: Basle Test SL1 plus Sulfur, Calcium,
gen, Phosphorus, and Potassium ' ,
Magnesium, Sodium, Iron, Aluminum, M
ahgaheso, Copper and 2lnc
CI
a
METHOD
SHIPpEb
C°v�
�U/-]-

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
ReportRange Ratio
2012-01-ANDCAK-NC
DURHAM, NC N. DURHAM WWTP ANAEROB,
4/22/2019
5/1/2019.6/30/2019 0.3436
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (474 x 16.7000) + 100 = 79.158
Ca mg/I = (Ca mg/kg x %Solids) + 100 = (12900 x 16.7000) + 100 = 2154.3
Mg mg/I = (mg mg/kq x %Solids) + 100 = (6680 x 16.7000) + 100 = 1115.56
Na meq = Na mg/I + Molec. Wgt. Na = 79.158 + 23 = 3.44165
Ca meq = Ca mg/I + Molec. Wgt.Ca = 2154.3 + 20 = 107.715
Mg meq = Mg mg/I + Molec.Wgt.Mg = 1115.56 + 12 = 92.9633
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.44165 + SgrRoot[0.5(107.715+92.9633)] = 0.343583
Page 1
Printed: 1/30/2020
16:46

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Pax 804-271-6446
www.waypointanalytical.com
6/28/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-172-0203
Project Description: DURHAM NORTH
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 6/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Anal ysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 5

0
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-172-0203
Client Project Description: DURHAM NORTH
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
DURHAM NORTH
DURHAM NORTH
DURHAM NORTH
DURHAM NORTH
DURHAM NORTH
DURHAM NORTH
DURHAM NORTH
DURHAM NORTH
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
06/19/2019
13:10
06/21/2019
06/19/2019
13:10
06/21/2019
06/19/2019
13:10
06/21/2019
06/19/2019
13:10
06/21/2019
06/19/2019
13:10
06/21/2019
06/19/2019
13:10
06/21/2019
06/19/2019
13:10
06/21/2019
06/19/2019
13:10
06/21/2019
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-747113
WTN
SM-4500-NH3C-TKN
WTN
SM-254OG
WTN
Page
2
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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range Ratio
2012-01-ANDCAK-NC
DURHAM, NC N. DURHAM WWTP ANAEROB.
6/19/2019
7/1/2019-7/31/2019 0,4106
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (584 x 15.3000) + 100 = 89.352
Ca.
mg/I
= (Ca
mg/kg x %Solids)
+ 100
= (12300 x
15.3000) + 100
= 1881.9
Mg
mg/I
= (mg
mg/kg x %
Solids) + 100
= (6660 x
15.3000) + 100 =
1018.98
Na meq = Na mg/I + Molec. Wgt.Na = 89.352 + 23 = 3.88487
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1881.9 + 20 = 94.095
Mg meq = Mg mg/I + Molec. Wgt.Mg = 1018.98 + 12 = 84.915
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.88487 + SgrRoot[0.5(94.095+g4.915)] = 0.410632
Page 1
Printed: 1/30/2020
16:46

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointan alytica l.com
8/14/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-207-0005
Project Description: Durham North
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincereyly�,
P ry� 6
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

Waypoint
v 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-207-000S
Client Project Description: Durham North
Lab No Client Sample ID Matrix Date Collected Date Received Method lab ID
Durham North
Durham North
Durham North
Durham North
Durham North
Durham North
Durham North
Durham North
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
WiN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
07/24/2019
11:00
08/05/2019
07/24/2019
11:00
08/05/2019
07/24/2019
11:00
08/05/2019
07/24/2019
11:00
08/05/2019
07/24/2019
11:00
08/05/2019
07/24/2019
11:00
08/05/2019
07/24/2019
11:00
08/05/2019
07/24/2019
11:00
08/05/2019
Page 2 of 6
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WrN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-254OG
WTN

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7621 Whitepme Road, Richmond, VA 23237
Main 804-743-9401°Fax [phone]
www.waypo i nta n a lyti ca l.co m
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-207-0005
Shipping Method
Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
Shipping container/cooler uncompromised?
Other:
Thermometer ID:
Yes 0 No
Number of coolers received
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (COC) present? Yes 0 No
COG agrees with sample label(s)? Yes 0 No
COC properly completed ® Yes 0 No
Samples in proper containers? Yes 0 No
Sample containers intact? Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? Yes 0 No
Cooler temperature in compliance? Yes 0 No
Cooler/Samples arrived at the laboratory on ice. Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
F— High concentration container (48 hr) CF— Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 40 No
Comments
Signature: jMaryAmend � Date &Time: 08/05/2019 12:42:38
Page 5 of 6

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Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012.01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 7/24/2019 8/1/2019.9/30/2019 0.4337
DIGESTED CAKE
Na mg/I = (Na mg/kg x °/a Solids) + 100 = (593 x 15.6000) + 100 = 92.508
Ca mg/I = (Ca mg/kg x °/a Solids) + 100 = (12900 x 15.6000) + 100 = 2012.4
Mg mg/I = (mg mg/kg x %Solids) + 100 = (5490 x 15.6000) + 100 = 856.44
Na meq = Na mg/I + Molec.Wgt.Na = 92.508 +23 = 4.02209
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2012.4 + 20 = 100.62
Mg meq = Mg mg/I + Molec.Wgt.Mg = 856.44 + 12 = 71.37
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.02209 + SgrRoot[0.5(100.62+71.37)] = 0.433725
Page 1
Printed: 1l30/2020
16:47

7621 Whitepine Road, Richmond, VA 23237
Main 804443-9401 0 Fax [phone]
www.waypointa nalytica I.com
9/20/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number. 19-255-0011
Project Description: North Durham
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/12/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense,. or the refund of the charges paid for performance of said analysis.
Page 1 0£ 6

e
0
7621 Whitepine Road, Richmond, VA 23237
Waypoint.
Main 804-743-94010Fax [phone]
ANALYTICALww .waypointanalytical.com
Sample Summary Table
.eport Number: 19-255-0011
;lient Project Description: North Durham
ib No Client Sample ID Matrix Date Collected Date Received Method Lab ID
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
3182
North
Durham
Solids
09/11/2019
09:15
09/12/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Vrginia
Page 2 0£ 6
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-2540G
WTN

Account Number: 46451
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ww w,wa y p o i n to n a l yti ca I. co m
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : North Durham
REPORT OFANALYSIS Date Sampled: 9/19/2019 09:15:00
Lab Number : 68182 Date Received: 09/12/2019 00:00
Sample Id : North Durham Date Reported: 09/20/2019
Total Solids *
Moisture *
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
15.60
84.40
5.09
2.87
0.38
1.27
1.40
0.69
0.07
1.04
4.05
50900
28700
3760
12700
14000
6930
660
21300
14400
620
437
3060
10400
40500
�4.88
250
50.0
50.0
50.0
250
50.0
250
50.0
50.0
5.00
2.50
12.5
100
250
4.88
ADM
ADM
JPJ
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
JPJ
09/16/2019 16:59
09/16/2019 16:59
09/192019 13:00
09/17l2019 20:03
09/17/2019 20:03
09l17/2019 20:03
09/17/2019 20:03
09/17/2019 20:03
09/17/2019 20:03
09/17/2019 20:03
09l17(2019 20:03
09/17/2019 20:03
09/17/2019 20:03
09/17/2019 20:03
09/19l2019 15:30
09l19/2019 13:00
09l19/2019 15:10
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letferssre for the exclusive and confidential use of our clients, and may not be 2produced in whole or pad, nonnay any reference be made
fo the work, the results, orfhe companyin any advertising, news release, or other public announcements rnfhout obtaining our prionvri(ten authorization.
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NOY-2011
Pauric McGroary
Agronomist
Page 3 of 6

Account Number: 46451
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number : 68182
Sample Id : North Durham
Project : North Durham
REPORT OFANALYSIS
Date Sampled: 9/11/2019 09:15:00
Date Received: 09/12/2019 00:00
Date Reported: 09/20/2019
Cadmium 1.10 1.00 BKN 09/17/2019 20:03 6010D
Chromium 32.4 2.50 BKN 09/17/2019 20:03 6010D
Nickel 22.4 2,50 BKN 09/17/2019 20:03 6010D
Lead 24.8 3.00 BKN 09/17/2019 20:03 6010D
Arsenic 5.07 5.00 BKN 09/17/2019 20:03 6010D
Mercury 0.358 0,0147 TJS 09/171201913:43 SW-7471B
Selenium <5.00 5,00 BKN 09/17/2019 20:03 6010D
pH' 8.5 JSL 09/18/2019 06:19 9045D
Molybdenum 12.2 2.50 BKN 09/17/2019 20:03 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time You mC G%ONy
Our reports and le((e�s are ror (he exclusive and confidential use of our clients, and may not be reproduced in whole or part, normay any reference be made Pauric McGroary
(o the wodc, the rasul(s, or Poe company in any advertising, news release, orotherpublic announcements without obtaining ou�prior vm(ten authorization. AgfenemlSt
Page 4 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax $04-271-6446
www.waypo i nta n alytical.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-2554011
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? 40 Yes 0 No
Number of coolers received F 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Required
Custody seals intact on sample bottles? 0 Yes 0 No fo Not Required
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? ® Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
F— High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments
Signature: Brandi Watson Date &Time: 09/12/2019 12:02:38
Page 5 of 6

SAMPLING LOG #
PROJECT
Phone: 336
Iilllllllillllllllllllllilllllllllllllllllllllllllllllllllll09 220 CORD & CUSTODY
Smonio Ceram LLC/12,02.08 RECORD
rmm,oumum
r arresr roar me proper field sampling procedures
were used during the collection of these samples,
u
A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD
LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
NamNo2t11 P� S�(GdMP I yl'�/4
Relinquished by Sampler: {� Date TIME)Recleved by: REMARKS: ,
CoPetj)IJO yl►I(IJ 16'0o
Relinquished by; l i 0< .017 � I Game Reol/ yesi by:
SPECIAL INSTRUCTIONSO
o Itorin u Dees,
Realeved by;
SLi: Total Solids (Moisture), Total KJeidahi Nitrogen, Phosphorus, and Potassium
St2: Basic Test SLi plus SuHur, Calolum, Magnesium, Sodium IYon, Aluminum, Manganese, Copper and Zino

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range Ratio
2012-01-ANDCAK-NC
DURHAM, NC N. DURHAM WWTP ANAEROB,
9/1112019
10/112019AO/31/2019 0.4484
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (660 x 15.6000) + 100 = 102.96
Ca
mg/I =
(Ca
mg/kg x
%Solids)
+
100
= (14000 x 15.6000) + 100
= 2184
Mg
mg/I
= (mg
mg/kg x
%
Solids) .
100
= (6930 x 15.6000) + 100 =
1081.08
Na meq = Na mg/I + Molec. Wgt. Na = 102.96 + 23 = 4.47652
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2184 + 20 = 109.2
Mg meq = Mg mg/I + Molec.Wgt.Mg = 1081.08 + 12 = 90.09
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.47652 + SgrRoot[0.5(109.2+g0.09)] = 0.448449
Page 1
Printed: 1/30/2020
16:47

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
11 /18/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-312-0011
Project Description: North Durham
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attacheAD rt ;A I ; . Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 0£ 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www,waypointa nalytical-com
Sample Summary Table
Report Number: 19-312-0011
Client Project Description: North Durham
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
SM-4500-NH3C
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
9045D
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
4500NO3F-2011
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
6010D
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
SW-7471B
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
SM-4500-NH3C-TKN
69539
North
Durham
Solids
11/06/2019
08:40
11/08/2019
SM-254OG
WTN: Waypoint Analytical -TN, Memphis, TN
Page 2 of 6
Lab ID

Waypoint
ANALYTICAL
46454
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By : Ryan Copeland
Report Number:19-312-0011
7621 Whitepine Road, Richmond, VA 23237
Main 804443-9401 0 Fax [phone]
www.waypoin to nalytical.com
Ryan Copeland
Project North Durham
Information :
REPORT OFANALYSZS
Report Date : 11/18/2019
Received : 11/08/2019
Pauric McGroary
Agronomist
Lab No : 69539
Sample ID :North Durham Matrix: Solids
Sampled: 11/6/2019 8:40
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 14300 m /Kg - d
9 rY 714 1 11/15/19 15:00 JPJ SM-4500-1\11-13C
Nitrate+Nitrite-N <32.8 mg/Kg - dry 32,8 Y 11/12/19 14:16 ZBD 4500NO3F-2011
Organic N 55400 mg/Kg - dry 1790 1 11/15/19 12:00 CALCULATION
pH 8.3 s.u.
1 11/12/19 05:08 JSL 9045D
Total Solids 14.0 % 0.010 1 11/11/19 16:35 ADM SM-254OG
Total Kjeldahl Nitrogen 69700 mg/Kg - dry 1790 1 11/15/19 12:00 JPJ iM-4500-1\11-13C-TKP
Phosphorus 34500 mg/Kg - dry 35.7 1 11/13/19 02:54 KKM 6010D
Aluminum 14000 mg/Kg - dry 35.7 1 11/13/19 02:54 KKM 6010D
Arsenic 4.56 mg/Kg - dry 3.57 1 11/13/19 02:54 KKM 6010D
Calcium 17400 mg/Kg - dry 179 1 11/13/19 02:54 KKM 6010D
Cadmium 1.18 mg/Kg - dry 0.714 1 11/13/19 02:54 KKM 6010D
Chromium 22,8 mg/Kg - dry 1,79 1 11/13/19 02:54 KKM 6010D
Copper 507 mg/Kg - dry 1.79 1 11/13/19 02:54 KKM 6010D
Iron 22000 mg/Kg - dry 35,7 1 11/13/19 02:54 KKM 6010D
Lead 22.8 mg/Kg - dry 2.14 1 11/13/19 02:54 KKM 6010D
Magnesium 8570 mg/Kg - dry 35.7 1 11/13/19 02:54 KKM 6010D
Manganese 764 mg/Kg - dry 3.57 1 11/13/19 02:54 KKM 6010D
Mercury 0.432 mg/Kg - dry 0.109
1 11/12/19 14:34 T75 SW-74716
Molybdenum 16.3 mg/Kg - dry 1.79 1 11/13/19 02:54 KKM 6010D
Nickel 20.6 mg/Kg - dry 1.79 1 11/13/19 02:54 KKM 6010D
Potassium 4940 mg/Kg - dry 35,7 1 11/13/19 02:54 KKM 6010D
Selenium 7.06 mg/Kg - dry 3.57 1 11/13/19 02:54 KKM 6010D
Sodium 914 mg/Kg - dry 179 1 11/13/19 02:54 KKM 6010D
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
MQL Method Quantitatlon Limit
Page 3 0£ 6

46451
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By : Ryan Copeland
Report Number:19-312-0011
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Ryan Copeland
Project North Durham
Information :
REPORTOFANALYSIS
Report Date : 11I /2019
S�Jj Received : 11/08/2019
*c X G0bNr
Pauric McGroary
Agronomist
Lab No : 69539 - Matrix: Solids
Sample ID : North Durham I Sampled: 11/6/2019 8:40
Test Results Units MQL DF Date ITime By Analytical
Analyzed Method
Zinc
3530
mg/Kg -dry
g,g3
Sulfur
15900
mg/Kg -
dry
35.7
Moisture 86.0 � 0.010
Qualifiers/ g Analy[e detected in blank
De£nitions
Page 4 0£ 6
1
11/13/19
02:54
KKM
6010D
1
11/13/19
02:54
KKM
6010D
Y 11/11/1916:35 ADM SM-2540G
H Beyond holding Gme

7621 Whitepme Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointa nalytica I.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-312-0011
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
40 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? 40 Yes 0 No
Number of coolers received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (COC) present? Yes 0 No
COC agrees with sample label(s)? Yes 0 No
COC properly completed ® Yes 0 No
Samples in proper containers? ®Yes 0 No
Sample containers intact? Yes 0 No
Sufficient sample volume for indicated test(s)? ® Yes 0 No
All samples received within holding time? ® Yes 0 No
Cooler temperature in compliance? ® Yes 0 No
Cooler/Samples arrived at the laboratory on ice. ® Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water" Sample containers properly preserved 0 Yes 0 No 0 N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
High concentration container (48 hr) I Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F- Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 40 No
Comments:
Signature: Brandi Watson Date &Time: 11/08/2019 13:12:44
Page 5 of 6

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Product Code Product Name Sample Date Report Range Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB, 11/6/2019 11/1/2019-12/31/2019 0.5283
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) + 100 = (914 x 14.0000) + 100 = 127.96
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (17400 x 14.0000) + 100 = 2436
Mg mg/I = (mg mg/kg x % Solids) + 100 = (8570 x 14.0000) . 100 = 1199.8
Na meq = Na mg/I + Molec.Wgt.Na = 127.96 + 23 = 5.56348
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2436 +20 = 121.8
Mg meq = Mg mg/I + Molec,Wgt.Mg = 1199.8 + 12 = 99.9833
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.56348 + SgrRoot[0.5(121.8+gg.9833)] = 0.52832
Page 1
Printed: 1/30/2020
16:48

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aceAnalytical
w .pacelabs.com
Pace Analytical Services, LLC
9800Kncey Ave. Suite too
Huntersville, NC 28078
[phone]
January 15, 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: Durham -South
Pace Project No.: 92413359
Dear Nate Roth:
Enclosed are the analytical results for samples) received by the laboratory on January O8, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C:�Zo�` 7�
Lord
Patton
lorri. patton@pacelabs. com
1(828)254-7176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Page 1 of 16
I

Project: Durham -South
Pace Project No.: 92413359
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORYANALYSIS
This report shall not be reprotlucetl, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
sa00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE AI ALYTECOUNT
Project: Durham -South
Pace Project No.: 92413359
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92413359001 Durham -South 1 of 6 EPA 601 OD DS 13 PASI-A
EPA 7471 B RDT 1 PASI-A
SM 2540G-2011 KDF 1 PASI-C
ASTM D2974-87 KDF 1 PASI-C
EPA9045D SMK 1 PASI-A
SM 271 OB-2011 DMN 1 PASI-A
EPA 350.1 Rev 2.01993 Mod. CJH1 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A
EPA 365.1 Rev 2.01993 NAL 1 PASI-A
REPORT OF LABORATORYANALYSIS
This report shall not be reproduced, except in full,
out
the written consent of Pace Analytical Services, LLC. Page 3 of 16

lytical
i
ANALYTICAL RESULTS
Project: Durham
-South
Pace Project No.: 92413359
Sample: DurhamSouth 1 of 6 Lab ID: 92413359001 Collected: 01 /07/19 09:15 Received: 01/08/19 12:45
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7471 Mercury
Mercury
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 01/15/2019 01:37 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services, LLC
9600 Kinsey Ave. Suite 100
Huntenwille, NC 28078
[phone]
Matrix: Solid
CAS No. Qual
21500
mg/kg
39.0
1
01/11/1909:20
01/13/1922:46
7429-90-5
ND
mg/kg
3.9
1
01/1111909:20
01/13/1922:46
7440-38-2
0,95
mg/kg
0,39
1
01/11/1909:20
01/13/1922:46
7440-43-9
18000
mg/kg
39.0
1
01/11/1909:20
01/13/1922:46
7440-70-2
368
ni
2.0
1
01/11/1909:20
01/13/1922:46
7440-50-8
231
mg/kg
2.0
1
01/11/1909:20
01/13/1922:46
7439-92-1
5630
ni
39.0
1
01/11/19
09:20
01/13/19
22:46
7439-95-4
8.0
mg/kg
2.0
1
01 /11119
09:20
01/13/19
22:46
7439-98-7
18.2
ni
2.0
1
01/11/1909:20
01113/1922:46
7440-02-0
2610
ni
1950
1
01111/1909:20
01/13/1922:46
7440-09-7
5.3
mg/kg
3.9
1
01/11/19
09:20
01 /13/19
22:46
7782-49-2
ND
ni
1950
1
01/11/1909:20
01/13/1922:46
7440-23-5
2270
mg/kg
3.9
1
01/1111909:20
01/13/1922:46
7440-66-6 BC
Analytical Method:
EPA 7471B Preparation
Method:
EPA 7471B
0.19
mg/kg
0.020
1
01/1111921:31
01/14/1912:17
7439-97-6
Analytical Method:
SM 254OG-2011
16.6
% 0.000010
1
01/10/1913:28
Analytical Method:
ASTM D2974-87
83A
%
0.10
1
01110/1913:20
Analytical Method:
EPA 9045D
7.5 Std. Units
0.10
1
01/15/19
10:46
H3
Analytical Method: SM 27106-2011
19000
mg/kg
0.12 1
01/15/1911:49
N2
Analytical Method:
EPA 350.1
Rev 2.0
1993 Mod. Preparation Method:
EPA 350.1
Rev 2.0
1993 Mod.
4610
mg/kg
435 10 01/12/1910:40
01/12/1916:27
7664-41-7
Analytical Method:
EPA 351.2
Rev 2.0
1993 Preparation Method:
EPA 351.2 Rev
2.0
1993
60100
mg/kg
2730 10 01/14/1911:34
01/1511905:54
7727-37-9
Analytical Method:
EPA 353.2
Rev 2.0
1993 Preparation Method:
EPA 353.2 Rev
2.0
1993
ND
mg/kg
11.9 1 01/10/1901:57
01/10/1903:49
ND
mg/kg
11.9 1 01/10/19
01:57
01/10/19
03:49
14797-55-8
ND
mg/kg
6.0 1 01/10/19
01:57
01/10/19
03:49
14797-65-0
Analytical Method:
EPA 365.1
Rev 2.0
1993 Preparation Method:
EPA 365.1 Rev
2.0
1993
28800
mg/kg
589 50 0110911920:23
01/10/1915:02
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
Page 4 of 16

i
QUALITY CONTROL DATA
Project: Durham -South
Pace Project No.: 92413359
QC Batch: 452089 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Associated Lab Samples: 92413359001
METHOD BLANK: 2472136 Matrix: Solid
Associated Lab Samples: 92413359001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg NO 0.0060 01/14/1912:06
LABORATORY CONTROL SAMPLE: 2472137
Parameter Units
Mercury mg/kg
Pace Analytical Services, LLC
9800 KinceyAve. Suite Ioo
Huntersville, NC 28078
[phone]
Spike LCS LCS %Rec
Conc. Result %Rec Limits Qualifiers
0.083 0.067 81 80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2472138
2472139
MS
MSD
92413378001 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result %Rec %Rec Limits RPD Qual
Mercury mg/kg 0.0063 0,055
0.057
0.048
0.049 75 75 75-125 3
Rosults prosontod on this pogo aro in tho units Intlicatetl by tho "Units" column oxcopt whom an altemato unit is prosontotl W tho tight of No rosult
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
ate: 01/15/2019 01:37 PM out the written consent of Pace Analytical Services, LLC. Page 5 of 16

aceAnalXical
w ..pacdabscom
QUALITY CONTROL DATA
Project: Durham -South
Pace Project No.: 92413359
utc ea[cn: 451935 Analysis Method: EPA 6010D
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Associated Lab Samples: 92413359001
MCTHOD BLANK: 2471114
Associated Lab Samples: 92413359001
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg1kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Matrix: Solid
Blank
Result Qua[
Reporting
Limit
Analyzed
LABORATORY CONTROL SAMPLE:
Parameter
2471115
Units
Spike
Cone.
LCS
Result
LCS
% Rae
%Rec
Limits
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE:
2471116
MS
- 92413357001
Spike
Parameter
Units
Result
Cone.
Aluminum
mg/kg
55600
9280
Arsenic
mg/kg
ND
928
Cadmium
mg/kg
ND
928
2471117
MSD
Spike
MS
MSD
MS
Conc.
Result
Result
%Rec
8310
69300
63600
148
831
827
734
89
831
848
758
91
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
if
iers
Qualif
iers
MSD %Rec
Rec Limits RPD Qual
96 75-125 9 M1
88 75-125 12
91 75-125 11
Rosults prosontotl on this page aro in tho snits intlicatotl by tho "Units" column oxeopt whom an altnmato unit is proson[otl to fho right of the rosult
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16

ac"Analytical
w ,Pawlab&wm
QUALITY CONTROL DATA
Project: Durham -South
Pace Project No.: 92413359
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
2471116
MS
92413357001
Spike
Parameter
Units
Result
Conc.
Calcium
mg/kg
17500
9280
Copper
mg/kg
393
928
Lead
mg/kg
23.2
928
Magnesium
mg/kg
3700
9280
Molybdenum
mg/kg
11.7
928
Nickel
mg/kg
15.5
928
Potassium
mg/kg
ND
9280
Selenium
mg/kg
ND
928
Sodium
mg/kg
ND
9280
Zinc
mg/kg
1880
928
Pace Analytical Services, LLC
9a00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MSD
Spike
Conc.
2471117
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
8310
27500
25000
107
90
75-125
9
831
1350
1220
103
99
75-125
10
831
865
770
91
90
75-125
12
8310
12700
11400
97
93
75-125
11
831
900
804
96
95
75-125
11
831
871
778
92
92
75-125
11
8310
13000
11900
97
95
75-125
9
831
783
687
84
82
75-125
13
8310
11100
10100
92
91
75-125
10
331
2770
2570
97
84
75-125
8
Rosults prosontatl on this page ate in tho units Intlleatotl by tho "Units" column oxeoptwhoro an al[omato unit is prosontotl co tho tight of tho result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Ctual
Date; 01l15/2019 01:37 PM out the written consent of Pace Analytical Services, LLC. Page 7 of 16

aceAnalXical
wW pacerabS=
Project: Durham -South
Pace Project No.: 92413359
QC Batch: 452172
QC Batch Method: EPA 9045D
Associated Lab Samples: 92413359001
SAMPLE DUPLICATE: 2472426
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2472427
Parameter
pH at 25 Degrees C
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
92413563001 Dup
Units Result Result
Std, Units 5.2 5.3
92413312001 Dup
Units Result Result
Std, Units 6.8 6.8
RPD Qualifiers
0 H3
RPD Qualifiers
0 H3
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Rosults prosentotl on thls pago are in No units Intllcatotl try tho "Units" column oxeopt whoro an altemato unit is prosentod ro the right of tho result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

aceAnalytical
w .pacdabs.com
Project: Durham -South
Pace Project No.: 92413359
CiG klatch: 452023
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92413359001
METHOD BLANK: 2471582
Associated Lab Samples: 92413359001
Parameter Units
Nitrogen, Ammonia mg/kg
LABORATORY CONTROL SAMPLE: 2471583
Parameter Units
Nitrogen, Ammonia mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntemville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 8.9 01/12/1915:09
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
472 464 98 90-110
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE: 2471584
2471585
MS
MSD
92413357001 Spike
Spike
MS
MSD MS MSD %Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qua]
Nitrogen, Ammonia
mg/kg 13200 10300
10500
21800
22500 83 89 90-110 3 M6
MATRIX SPIKE &MATRIX SPIKE
DUPLICATE: 2471586
2471587
MS
MSD
92413358001 Spike
Spike
MS
MSD MS MSD %Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia
mg/kg ND 2320
2320
2210
2210 93 93 90-110 0
Results prosontotl on this page aro in tho units indltaMd by the "Units" Column oxeopt whom an altomato unit is prosontod to tho right of Cho insult.
Date: 01/15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotluceo, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 16

aceAnalyiical
www.parelabscam
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Durham -South
Pace Project No.: 92413359
QC Batch: 452219
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2
TKN
Associated Lab Samples: 92413359001
METHOD BLANK: 2472536
Matrix:
Solid
Associated Lab Samples: 92413359001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
NO 50.0
01/15/19
04:45
LABORATORY CONTROL SAMPLE: 2472537
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
%Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000
967
97
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472538
2472539
MS
MSD
92413357001
Spike
Spike MS
MSD
MS MSD
%Rec
Parameter Units Result
Conc,
Conc. Result
Result
% Rec % Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 62000
21200
19000 74700
74800
60 67
90-110
0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472540
2472541
MS
MSD
92413358001
Spike
Spike MS
MSD
MS MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec % Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 5230
5170
5170 8110
9500
56 83
90-110
16 M1, R1
Results pmsontetl on this pago am in tho units inditatotl by tho "Units" column oxcept whoro an altomato unit is prosontotl to tho tight of the result
Date: 01/15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Page 11 of 16

aceAnalytical
w ,pacelabawm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Durham -South
Pace Project No.: 92413359
QC Batch: 451629
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2
Nitrate+
Nitrite
Associated Lab Samples: 92413359001
METHOD BLANK: 2469664
Matrix: Solid
Associated Lab Samples: 92413359001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 2.0
01/10/19
03:42
Nitrogen, Nitrite
mg/kg
ND 0.98
01/10/19
03:42
Nitrogen, NO2 plus NO3
mg/kg
ND 2.0
01/10/19
03:42
LABORATORY CONTROL SAMPLE: 2469665
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.9 15.8
106
90-110
Nitrogen, Nitrite
mg/kg
9.9 10.6
107
90-110
Nitrogen, NO2 plus NO3
mg/kg
24.8 26A
107
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2469666 2469667
MS MSD
92413357001
Spike Spike MS
MSD
MS MSD
% Rec
Parameter Units
Result
Conc. Conc. Result
Result
% Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/kg
ND
425 420 412
393
97 93
90A 10 5
Nitrogen, Nitrite ni
ND
286 280 305
308
100 102
90-110 1
Nitrogen, NO2 plus NO3 mg/kg
ND
711 702 717
701
100 99
90-110 2
Rosults prosontotl on thls pago aro in tho units intlicamtl by tho "Units" column oxtopt whom an altemato unit Is pmsentotl to tho right of tho result
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotluced, except in full,
Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

acek7alytical
www.pacelabaccm
Project: Durham -South
Pace Project No.: 92413359
QC Batch: 451598
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92413359001
QUALITY CONTROL DATA
Pace Analytical Services, LLC
sa00 Kincey Ave. Suite Too
Huntersville, NO 28078
[phone]
Analysis
Method:
EPA 365.1 Rev 2.0
1993
Analysis
Description:
365.1 Phosphorus,
Total
METHOD BLANK: 2469443 Matrix; Solid
Associated Lab Samples: 92413359001
Blank Reporting
Parameter Units Result Limit Analyzed
Phosphorus mg/kg ND 2.0 01110/1913:45
LABORATORY CONTROL SAMPLE:
2469444
Spike
LCS
Qualifers
LCS
%Rec
Rec Limits Qualifiers
107 90-110
MSD MS MSD % Rec
Result % Rec % Rec Limits RPD Qual
23300 -99 -88 90-110 1 M6
Rosults pmsonWtl on this pago aro in tho units Intlitatotl by tho "Units" column oxoopt whcro an altomato unit is prosontotl to tho right oTthe rosolt
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotlucetl, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, U.C. Page 13 of 16

"Analytical
www.pecelabscrom
QUALIFIERS
Project: Durham -South
Pace Project No.: 92413359
DEFINITIONS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL -Practical Quantitation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte ie
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) -Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U -Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical
Services -Asheville
PASI-C
Pace Analytical
Services -Charlotte
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/fNI accreditation for this parameter.
R1 RPD value was outside control limits.
Date: 01/15/2019 01:37 PM
REPORT OF LABORATORYANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 16

xogzzzl
aceAnaiytical
w ,pecelaftc
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Durham -South
Pace Project No.: 92413359
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
Durham-South1
of
EPA3050B
451935
EPA6010D
451945
Durham-SouthI
of
EPA 7471E
452089
EPA 7471B
452120
DurhamSouth 1
of 6
SM 2540G-2011
452044
Durham-South1
of
ASTM D2974-87
451773
DurhamSouth 1
of 6
EPA 9045D
452172
Durham -South 1
of 6
SM 2710E-2011
452503
Durham -South 1
of 6
EPA 350.1 Rev 2.0
1993
452023
EPA 350.1 Rev
2.0 1993
452144
Mod.
Mod.
DurhamSouth 1
of 6
EPA 351.2 Rev 2.0
1993
452219
EPA 351.2 Rev
2.0 1993
452403
Durham -South 1
of 6
EPA 353.2 Rev 2.0
1993
451629
EPA 353.2 Rev
2.0 1993
451647
DurhamSouth 1
of 6
EPA 365.1 Rev 2.0
1993
451598
EPA 365.1 Rev
2.0 1993
451656
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducetl, except in full,
Date: 01/15/2019 01:37 PM out the written consent of Pace Analytical Services, LLC. Page 15 of 16

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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2012.0&ANDCAK-NC
DURHAM, NC S. DURHAM WWTP ANAEROB.
1/7/2019
1/1/2019-2/28/2019
1.3202
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (1950 x 16.60001 + 100 = 323.1
Ca mg/I = (Ca mq/kg x % Solitls) + 100 = (18000 x 16.6000) + 100 = 2988
Mg mg/I = (mg mg/kq x %Solids) + 100 = (5630 x 16.6000) + 100 = 934.58
Na meq = Na mg/I + Molec. Wgt.Na = 323.7 + 23 = 14.0739
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2988 +20 = 149.4
Mg meq = Mg mg/I + Molec. Wgt.Mg = 934.58 + 12 = 77.8817
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 14.0739 + SgrRoot[0.5(149.4+77,gg17)] = 1.32022
Page 1
Printed: 1/30/2020
16:53

0
M 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-052-0205
Client Project Description: Durham South
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
durham south 2 of 6
durham south 2 of 6
durham south 2 of 6
durham south 2 of 6
durham south 2 of 6
durham south 2 of 6
durham south 2 of 6
durham south 2 of 6
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
02/20/2019
11:00
02/21/2019
02/20/2019
11:00
02/21/2019
02/20/2019
11:00
02/21/2019
02/20/2019
11:00
02/21/2019
02/20/2019
11:00
02/21/2019
02/20/2019
11:00
02/21/2019
02/20/2019
11:00
02/21/2019
02/20/2019
11:00
02/21/2019
Page 1 of 5
SM-4500-NH3C
WiN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-254OG
WTN

Report Number: 19-052-0205
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : Durham South
7621 whitepine Road, Richmond, VA 23237
Maln 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS Date Sampled: 2l20/2019 11:00:00
Lab Number: 64889 Date Received: 02/21/2019 00:00
Sample Id : durham south 2 of 6 Date Reported: 03/01/2019
iotai5ouas-
16.90
169000
100.0
CJR
02/26/201915:35
Moisture'
83.10
100.0
CJR
02/26/201915:35
Total Kjeldahl Nitrogen
5.98
59800
250
CLIP
02/28/2019
11:30
Phosphorus
3.25
32500
50.0
KKM
02/26/2019
21:40
Potassium
0.25
2520
50.0
KKM
02/26/2019
21:40
Sulfur
1.24
12400
50.0
KKM
02/26/2019
21:40
Calcium
1,84
18400
250
KKM
02/26/2019
21:40
Magnesium
0,55
5470
50.0
KKM
02/26/2019
21:40
Sodium
0.06
624
250
KKM
02127/201917:41
Iron
22200
50.0
KKM
02/26/2019
21:40
Aluminum
22800
50.0
KKM
02/26/2019
21:40
Manganese
852
5,00
KKM
02/26/2019
21:40
Copper
378
2,50
KKM
02/26/2019
21:40
Zinc
2470
12.5
KKM
02/27/201917:41
Ammonia Nitrogen
0,72
7160
100
ZBD
02/27/2019
14:00
Organic N
5,26
52640
250
02/27/2019
14:00
Nitrate+Nitrite-N
222
4.95
ZBD
02/26/201914:18
All values are on a dry weight basis
except
as noted by asterisk. Detection
limit on all
N series is on a wet
basis.
B - Analyte detected in blank
H - Beyond Holding
Time
I t �G
Our repodsand leftersare /or the exclusive and con/idenfial use of ourdients, and may not be reproduced in whole orpart, nor may any reference be made
to the Work, the results, or the cnmpanyin any advertising, nevss release, or otherpublic announcements vAthout obtaining ourpdonvrilfen authohzation.
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
Pauric McGroary
Agronomist
Page 2 of 5

Report Number: 19-052-0205
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : Durham South
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYS/S Date Sampled: 2/20l2019 11:00:00
Lab Number: 64889 Date Received: 02/21/2019 00:00
Sample Id : durham south 2 of 6 Date Reported: 03/01/2019
caammm <1.00 1.00 KKM 02/26/2019 21:40 6010D
Chromium 29.2 2.50 KKM 02/26/2019 21:40 6010D
Nickel 23.2 2.50 KKM 02/26/2019 21:40 6010D
Lead 17.8 3.00 KKM 02/26/2019 21:40 6010D
Arsenic 5.18 5.00 KKM 02/26/2019 21:40 6010D
Mercury 0.236 0.0141 US 02/261201911:08 SW-7471B
Selenium <5.00 5.00 KKM 02/26/2019 21:40 6010D
pH * 6.8 JSL 02/27/2019 08:36 9045D
Molybdenum 7,79 2.50 KKM 02/26/2019 21:40 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time � 6ewr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior antten authorization.
Agronomist
Page 3 of 5

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ww ,waypointanalytical,com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-052-0205
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers received
Custody seals intact on shipping container/cooler? 0 Yes 0 No fo Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (COC) present? 40 Yes 0 No
COC agrees with sample label(s)? Yes 0 No
COC properly completed Yes 0 No
Samples in proper containers? Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 40 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? Yes 0 No
Cooler/Samples arrived at the laboratory on ice. le Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
High concentration container (48 hr) F— Low concentration EnCore samplers (48 hr)
F— High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments:
Signature: Brandi Watson Date &Time: 02/21/2019 11:04:29
Page 4 of 5

( } Go\
\ \ \�/ \ k
> \ }
, o n m 2
\) � k
\ (m

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 2/20/2019 311/2019-4/30/2019 0,4252
DIGESTED CAKE
mg/kg x %Solids) + 100 = (624 x 16.9000) + 100 = 105.456
Ca
mg/I =
(Ca
mg/kq x
%Solids)
+
100 =
(18400 x 16.9000) + 100
= 3109.E
Mg
mg/I
= (mg
mg/kg x
%
Solids) +
100
= (5470 x 16.9000) + 100 =
924.43
Na meq = Na mg/I + Molec.Wgt.Na = 105.45E + 23 = 4.58504
Ca meq = Ca mg/I + Molec.Wgt.Ca = 3109.E +20 = 155.48
Mg meq = Mg mg/I + Molec.Wgt.Mg = 924.43 + 12 = 77.0358
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.58504 + SgrRoot[0.5(155.48+77.0358)] = 0.425238
Page 1
Printed: 1/30/2020
16:53

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
5/1 /2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19A 14-0207
Project Description: South Durham
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/24/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Anal ysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

1
M 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19414-0207
Client Project Description: South Durham
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
South Durham
South Durham
South Durham
South Durham
South Durham
South Durham
South Durham
South Durham
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
04/22/2019
10:10
04/24/2019
04/22/2019
10:10
04/24/2019
04/22/2019
10:10
04/24/2019
04/22/2019
10:10
04/24/2019
04/22/2019
10:10
04/24/2019
04/22/2019
10:10
04/24/2019
04/22/2019
10:10
04/24/2019
04/22/2019
10:10
04/24/2019
Page 2 of 6
5M-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-254OG
WTN

Report Number: 19-114-0207
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : South Durham
7621 Whltepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Lab Number: 66051 REPORT OFANALY0 Date Sampled: 4l22/2019 10:10:00
Date Received: 04/24/2019 00:00
Sample Id :South Durham Date Reported: 05/01/2019
•--•• ��••�� ro.ou ionuuu 1U0.0 ADM 04/25/2019 16:21
Moisture * 83.40 100.0 ADM 04/25/2019 16:21
Total Kjeldahl Nitrogen 5,94 59400 250 JPJ 04/29/2019 09:37
Phosphorus 2.85 28500 50.0 KKM 04/28/201918:23
Potassium 0,25 2450 50.0 KKM 04/28/201918:23
Sulfur 1.03 10300 50.0 KKM 04/28/201918:23
Calcium 1.66 16600 250 KKM 04/281201918:23
Magnesium 0,51 5060 50.0 KKM 04/28/201918:23
Sodium 0.07 663 250 KKM 04/281201918:23
Iron 20300 50.0 KKM 04/281201918:23
Aluminum 18700 50.0 KKM 04/28/201918:23
Manganese 884 5.00 KKM 04/281201918:23
Copper 316 2,50 KKM 04/28/201918:23
Zinc 2090 12.5 KKM 04/281201918:23
Ammonia Nitrogen 0.96 9640 100 JPJ 04/26/2019 12:00
Organic N 4.98 49760 250 04/26/2019 12:00
Nitrate+Nitrite-N 36.1 4.96 ZBD 04130/201912:50
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
?A4u�c
Our repods and letters are Ior the ezdusive and confidential use ofour c/rents, and may not be reproduced in whole or part, nor may any reference he made
to the v. ork, the resul(s, or the company in any advertising, news n:/ease, or o(her public announcements without obtaining our prior vmtten authohzatlon.
SM-2540G
SM-264OG
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
Pauric McGroary
Agronomist
Page 3 of 6

Report Number: 19-114-0207
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : South Durham
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYS/S Date Sampled: 4/22/2019 10:10:00
Lab Number: 66051 Date Received: 04/24/2019 00:00
Sample Id : South Durham Date Reported: 06/01/2019
��w^^^,ur„ <�.uu 1.00 KKM 04l28/201918:23 6010D
Chromium 33.6 2.50 KKM 04/281201918:23 601OD
Nickel 23.4 2,50 KKM 04128/201918:23 6010D
Lead 14.3 3,00 KKM 04128/201918:23 601OD
Arsenic <5.00 6,00 KKM 04/28/201918:23 6010D
Mercury 0.415 0.0151 TJS 04/30/201912:23 SW-7471B
Selenium <5.00 6,00 KKM 04128/201918:23 6010D
pH . 8.0 JSL 04/29/2019 06:46 9045D
Molybdenum 7,24 2,50 KKM 04/28/201918:23 6010D
Comments:
All
values are on a dry weight basis
except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte
detected in blank
H - Beyond Holding Time
Our reportssnd letters a2 for fhe eeclusive and confidential use orour clients, and may not he reproduced in whole orpart, nor may any reference be made
to fhe r^,rork, fhe results, or fbe company in any advertising, news release, oro(herpublic announcements vAthout obtaining ourpriorrm(len au(hodzatron.
Pauric McGroary
Agronomist
Page 4 of 6

7621 Whitepine Road, Richmond, VA 23237
Waypoint.
Main 804-743-9402 0 Fax [phone]
ANALYTICALwww.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-114-0207
Shipping Method
Fed Ex 0 US Postal Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes 0 No
Number of coolers received I
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (COC) present? Yes 0 No
COC agrees with sample label(s)? ® Yes 0 No
COC properly completed ® Yes 0 No
Samples in proper containers? ® Yes No
Sample containers intact? ® Yes 0 No
Sufficient sample volume for indicated test(s)? ® Yes 0 No
All samples received within holding time? ® Yes 0 No
Cooler temperature in compliance? 0 Yes No
Cooler/Samples arrived at the laboratory on ice. 0 Yes No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
High concentration container (48 hr) F- Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Brandi Watson Date &Time: 04/24/2019 13:25:16
Page 5 of 6

.._......._.......................
• ,a:, •� i G 1,
� :1.
A tl< L
Lqg #
SPECIAL
SAMPLE
I.D.
�v�thM
IIIIIIINIIIIIIINIIIINIIINIIIIIIIIIIIIIIIIIININIIIIIIIIIIIII < 2(1,g � A
Svnoaro Cenlrat ltc/ovrham t9'ii4-o2o�
Soulh Omham ��� X ®®�f"
13:24:24 ;�®�®
were used dvdpg the co/leenwr of these Beres
� amples,
vu:� t vMER � �� L�9L-'lq/�
SAMPLE I,b. SAMPLING SA PLER
SAMPLE
LOCATION � # OF
O,1RIIhM TYPE CONTAINERS SAMPLING METNOb
I S taf'R( �0 �/�,�p I DATE TIME PRESERWED
YZZ �y min l��
red by Sampler•
�� Date 7fine�
iedby; � Y 2Z )y -v� � Recleved by;
REMARKS:
bat
ed by: � •� f-I � ' nm° Reoleve
Dale Ttm¢ Reclev d by:
RUCTIONS;
I�IQD�� �o
For Ni—_ manifortng purposes. �G�"Q ���
PO#;
SL1 SL2 ANALYSIS REQUEST
NHQ-N NO3 N tlrgaalt:
N Cd Cr NI Pb
As Hg Se pH eaCO3 Solids Mo. CI Np2,p
SLR; Total Solids (Moisture), Total KJeldahf Nitrogen, Phosphorus, and Potassium � I
SL2; l3aslc Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper and 21nc
ME7HOD
SHIPPED
u�'1
co
u>

==
Sodiurn Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB, 4/22/2019 5/1/2019-6/30/2019 0.4695
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (663 x 16.6000) + 100 = 110.058
Ca
mg/I
= (Ca
mg/kg x
%Solids)
+
100 =
(16600 x 16.6000) + 100
= 2755.E
Mg
mg/I
= (mg
mg/kg x
%
Solids) +
100
= (5060 x 16.6000) + 100 =
839.96
Na meq = Na mg/I + Molec.Wgt.Na = 110.058 + 23 = 4.78513
Ca meq = Ca mg/I + Molec. Wgt.Ca = 2755.E + 20 = 137.78
Mg meq = Mn mg/I + Molec.Wgt.Mg = 839.9E + 12 = 69.9967
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.78513 + SgrRoot[0.5(137.78+69.9967)] = 0.469473
Page 1 Printed: 1/30/2020
16:54

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalytica I.co m
6/28/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-172-0204
Project Description: DURHAM SOUTH
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 6/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P.�:- n° c
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said ana/ysis.
Virginia 460014
°�_
Page 1 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalytical.com
Sample Summary Table
Report Number: 19-172-0204
Client Project Description: DURHAM SOUTH
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
67063 DURHAM SOUTH Solids 06/19/2019 13:40 06/21/2019
67053 DURHAM SOUTH Solids 06/19/2019 13:40 06/21/2019 SM-4500-NH3C WiN
67063 DURHAM SOUTH Solids O6/19/2019 13:40 06/21/2019 9046D WTN
67063 DURHAM SOUTH Solids 06/19/2019 13:40 O6/21/2019 4600NO3F-2011 WTN
67063 DURHAM SOUTH Solids 06/19/2019 13:40 06/21/2019 6010D yyTN
67063 DURHAM SOUTH Solids 06/19/2019 13:40 06/21/2019 SW-74716 WTN
67053 DURHAM SOUTH Solids 06/19/2019 13:40 06/21/2019 SM-4500-NH3C-TKN WTN
67053 DURHAM SOUTH Solids 06/19/2019 13:40 06/21/2019 SM-2640G WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: �1354
Page 2 of 6

Report Number: 19-172-0204
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010Fax [phone]
wwwwway p oin to na lytica 1. com
Oct: DURHAM SOUTH
Lab Number: 67053 REPORT OFANALYS/S Date Sampled: 6/19/2019 13:40:00
Sample Id DURHAM SOUTH
Date Received: 06/21/2019 00:00
:
Date Reported: 06/28/2019
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
17.00
83.00
5.45
2.98
0.25
1.15
1.78
0.51
0.08
0.89
4.56
54500
29800
2460
11500
17800
5060
802
21200
22400
1000
324
2440
8940
45660
34.7
250
50.0
50.0
50.0
250
50.0
250
50.0
50.0
5.00
2.50
12.5
100
250
5.00
CJR
CJR
JPJ
BKN
BKN
KKM
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
JPJ
06/26/2019 14:42
06/26/2019 14:42
06/27/2019 09:30
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 15:57
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 03:02
06/27/2019 14:00
06/27/2019 09:30
06/28/2019 14:02
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NOY-2011
Our reports and letters are /or the exclusive and confidential use of our clients, and may not be reproduced in v hole orpart normay any re7erence be made
to fhe work, the nsWts, orthe company in any advedising, news release, orotherpublic announcements vnthout obtaining our poor written authorization.
Pauric McGroary
Anrnnnmic+

Report Number: 19-172-0204
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytical.com
Oct: DURHAM SOUTH
Lab Number: 67053 REPORT OFANALYS/S Date Sampled: 6/19/2019 13:40:00
Sample Id :DURHAM SOUTH Date Received: 06/21/2019 00:00
Data RennMoA• nR79R/9n4o
•�� i.vu esrcry 06/27/201903:02 6010D
Chromium 28.2 2,50 BKN 06/27/2019 03:02 601 OD
Nickel 21.6 2.50 BKN 06/27/2019 03:02 6010D
Lead 15A 3.00 BKN 06/27/2019 03:02 6010D
Arsenic <5.00 5,00 BKN 06/27/2019 03:02 6010D
Mercury 0.281 0,0138 TJS 06126/201912:25 SW-74718
Selenium <5.00 5,00 BKN 06/27/2019 03:02 6010D
pH . 8.0 JSL 06/26/2019 07:43 9045D
Molybdenum
8.00 2.50 BKN 06/27/2019 03:02 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on ail N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
1 Gt��a It�G V��X
Our reports and le(ters are for the exclusive and confidential use of our clients, and may not be reproduced in r hole or part, normay any reference be made
to the work the 2sults, or the company in any advertising, news release, orotherpublic announcements t°nthout obtaining ourpnonvritten authohzafion.
Pauric McGroary
Agronomist

7621 Whitepine Road, Richmond, VA 23237
ANALYTICAL Main soa-743-9ao1 ^ Fax soa-z7l-saa6
www.waypointa n alytical.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/Durham
Report Number: 19-172-0204
Shipping Method
Fed Ex � US Postal � Lab
UPS 0 Client � Courier
Shipping container/cooler uncompromised? Yes
Number of coolers received � �
Custody seals intact on shipping container/cooler? � Yes
Custody seals intact on sample bottles? 0 Yes
Chain of Custody (COC) present? Yes
COC agrees with sample label(s)? Yes
COC properly completed Yes
Samples in proper containers? ®Yes
Other
Thermometer ID: '
No
No Not Required
0 No ®Not Required
No
No
No
No
Sample containers intact? ®Yes 0 No
Sufficient sample volume for indicated test(s)? ®Yes � No
All samples received within holding time? ®Yes � No
Cooler temperature in compliance? ®Yes � No
Cooler/Samples arrived at the laboratory on ice. Yes
Samples were considered acceptable as cooling � No
process had begun.
Water -Sample containers properly preserved � Yes � No N/A
Water -VOA vials free of headspace !� Yes � No N/A
Trip Blanks received with VOAs � Yes � No N/A
Soil VOA method 5035 —compliance criteria met � Yes 0 No N/A
I^ High concentration container 48 hr
( ) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d
j^ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes No
Comments: i
Signature: �Brandi Watson Date &Time: 06/21/2019 11:3T40 I
Pa aP S .,f c

SAMPLING LOG # ^ CHAIN OF CUSTODY
CUSTOMER: svwAGR® IIIIIIIIIIIIIIIGIIIININIIIIINIINIIIIIIIIINIIIIIIIInIIIIII1<z,�2o,9 RECORD RECORD
Swaaru Ceal,alLG Du,hau, n:n:iv —
0 ouawu+SOUTH p proper field sampling procedures
PROJECT MANAGER; 1�t l,.._ling the collection of these sarnples.
Phone: (336 bu7-'{yg4E t✓54N.�sn�,Ca�@��/ 1 CoP6ilrNo
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD
LAB # SAMPLE LD. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
U7JNtp1 yrycnkc 5L) wNP �Ii9/19 13.40 ice Goarn�oP3
Relinqulshed by Sampler:rf Date Time ReOlovod by: REMARKS:
V-`{AN CAPCU%NO oltotiq 1, e q
Relinquished by: Date Time Reefeved by:
Relinqulshed by: Date Time Recleved by
( BPS to 17,1 �S—
SPECIAL INSTRUCTIONS:
For N� monitoring purposes. POM
ANALYSIS REQUEST
SAMPLE
SL1
SL2
NFI -N
n
NO -N
a
Organic
N
Cd
Cr
NI
Pb
As
Hg
Se
pH
Caco
equiv.
VolaWe
SOIIdS
Me
Cl
NOa-N
atit�M
1400
A00010001400
1000
1040
1000
1000
1400m
pw
S@_5: Total Solids (Moisture), Totai KJeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basle Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

_v
-�k�— _
—
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range
Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 6/19/2019 7/1/2019.7131/2019
DIGESTED CAKE 0.5614
Na mg/1 = (Na mg/kg x % Solids) + 100 = (802 x 17.0000) + 100 = 136.34
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (17800 x 17.0000) + 100 = 3026
Mg mg/I = (mg mg/kg x % Solids) + 100 = (5060 x 17.0000) + 100 = 860.2
Na
meq =
Na
mg/I +
Molec.Wgt.Na
= 136.34 +23
= 5.92783
Ca
meq =
Ca
mg/I +
Molec. Wgt.Ca
= 3026 + 20 =
151.3
Mg meq = Mg mg/I + Molec. Wgt.Mg = 860.2 + 12 = 71.6833
SAR = Na meq * SgrRoot[0.5 x (Ca meq + Mg meq)j = 5,92783 + SgrRoot[0.5(151.3+71.6833)j = 0.561402
Page 1 Printed: 1/30/2020
16:54

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointanalyti ca l.com
8/14/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-207-0006
Project Description: Durham South
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 8/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalytiwl.com
Sample Summary Table
Report Number: 19-207-0006
Client Project Description; Durham South
lab No Client Sample ID Matrix Date Collected Date Received Method Lab IC
67561 Durham South Solids 07/24/2019 10:00 08/06/2019
67651 Durham South Solids 07/24/2019 10:00 08/06/2019 SM-4500-NH3C WTN
67661 Durham South Solids 07/24/2019 50:00 OS/06/2019 9046D WTN
67661 Durham South Solids 07/24/2019 10:00 OS/OS/2019 4500NO3F2011 WTN
67661 Durham South Solids 07/24/2019 10:00 08/06/2019 6010D tn/TN
67561 Durham South Solids 07/24/2019 10:00 08/OS/2019 SW-74716 WTN
67551 Durham South Solids 07/24/2019 10:00 OS/OS/2019 SM-4500-NH3C-TKN WTN
67661 Durham South Solids 07/24/2019 10:00 08/OS/2019 SM-2640G WTN
WTN: Waypoint Malytical - TN, Memphis, TN, Certification: #1364
Page 2 of 6

Report Number: 19-207-0006
Account Number: 46461
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : Durham South
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
w w w.wa y p o i n to n a l yti ca 1. c o m
Lab Number: 67551 REPORT OFANALYS/S We Sampled: 7/24/2019 10:00:00
Sample Id Durham South
Date Received: 08/05/2019 00:00
:
rlatn Rnnnr{nrl. n014ninnnn
Moisture
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
83.30
5.32
2.77
0.23
0.99
1.56
0.47
0.07
0.99
4.33
53200
27700
2290
9850
15600
4740
712
18100
22600
947
294
2300
9880
43320
<4.46
250
50.0
50.0
50.0
250
50.0
250
50.0
50.0
5.00
2.50
12.5
100
250
4.46
HUM
ADM
JPJ
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
JPJ
07/30/2019 15:06
012019 15:06
08/09/2019 11:30
OS/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/01/2019 12:43
08/13/2019 12:00
08/09/2019 11:30
08/12/2019 15:11
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
Our reponsand /afters are /or the exclusive and confidential use o1 our clients, and may riot be reproduced in v.ho/e or pan, nor may any re/erence be made
to the work, the results, orthe companyin any advenising, news re/ease, orother public announcements without obtaining ourpBorimiton authorization. PauflC MCGroary
Agronomist

Report Number: 19-207-0006
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : Durham South
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytical.com
Lab Number: 67551 REPORT OF ANALYSIS Date Sampled: 7/24/2019 10:00:00
Date Received: 08/05/2019 00:00
Sample Id :Durham South Date Renorted: 08/14/2019
i.vu t.uu BKN 08/01/2019 12:43 6010D
Chromium 33.9 2.50 BKN 08/011201912:43 6010D
Nickel 22.4 2,50 BKN 08/01/201912:43 6010D
Lead 14.3 3.00 BKN 08/01/201912:43 6010D
Arsenic <5.00 5.00 BKN 08/01/201912:43 6010D
Mercury 0.430 0.0148 TJS 08/061201914:13 SW-7471B
Selenium <5.00 5,00 BKN 08/011201912:43 6010D
pH * 8.3 JSL 08/12/2019 07:57 9045D
Molybdenum 7,30 2.50 BKN 08/01/201912:43 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any re/erence be made
to the war$ the 2su/ts, orlhe company in any advertising, news release, orother public announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist

7621 WhiLepine Road, Richmond, VA 23237
Main 804-743-9401 "Fax [phone]
ANALYTICAL www.wa
ypointanalytipl.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/Durham
Report Number: 19-207-0006
Shipping Method
Fed Ex � US Postal � Lab � Other:
UPS � Client � Courier Thermometer ID: '
Shipping container/cooler uncompromised? Yes � No
Number of coolers received � �
Custody seals intact on shipping container/cooler? � Yes � No ®Not Required
Custody seals intact on sample bottles? � Yes � No ®Not Required
Chain of Custody (COC) present? ®Yes � No
COC agrees with sample label(s)? ®Yes � No
COC properly completed ®Yes � No
Samples in proper containers? ®Yes � No
Sample containers intact? ®Yes � No
Sufficient sample volume for indicated test(s)? ®Yes n No
ui samples receroed within holding time? ®Yes � No
gooier temperature in compliance? ®Yes � No
�ooiensampies arnved at the laboratory on ice. ®yes � No
Samples were considered acceptable as cooling
process had begun.
vva[er - aampie containers properly preserved � Yes � No N/A
Water -VOA vials free of headspace � Yes � No N/A
Trip Blanks received with VOAs � Yes � No N/A
you vvv method 5035 —compliance criteria met � Yes � No ®N/A
High concentration container (48 hr) ^Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) i Low conc pre -weighed vials (Sod Ric _�a �i
opeciai precautions or instructions included?
Comments:
Yes No
Signature: (Mary Amend
Date &Time: 08/05/2019 12:4337 j
Page 5 of 6

9 3o 9 a5ed
1
I�
0
LL
EM
Imm
IBM
IBM

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP DIGESTED CAKE ANAEROB, 7/24/2019 8/1/2019-9/30/2019 0.5219
Na mg/I = (Na mg/kg x %Solids) + 100 = (712 x 16.7000) * 100 = 118.904
Ca
mg/1 =
(Ca
mg/kg x
%Solids)
+
100 =
(15600 x 16.7000) + 100
= 2605.2
Mg
mg/1
= (mg
mg/kg x
%
Solids) +
100
= (4740 x 16.7000) + 100 =
791.58
Na meq = Na mg/I + Molec. Wgt.Na = 118.904 + 23 = 5.16974
Ca meq = Ca mg/I + Molec. Wgt.Ca = 2605.2 + 20 = 130.26
Mg meq = Mg mg/I + Molec. Wgt.Mg = 791.58 + 12 = 65.965
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.16974 + SgrRoot[0.5(130.26+65.965)] = 0.521923
Page 1 Printed: 1/30/2020
16:54

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointanalytiw l.com
9/20/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number. 19-255-0012
Project Description: South Durham
Dear Mary Brewer.
Waypoint Analytical Virginia, Inc. received samples) on 9/12/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures pertormed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were pertormed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P,,,,:. ar"J�
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

0
•
7621 Whitepine Road, Richmond,
VA 23237
�•
Main
804743-9401 °Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Sample
Summary Yable
Report Number:
19-255-0012
Client
Project Description: South Durham
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab IO
68183
South
Durham
Solids
09/li/2019
09:46
09/12/2019
68183
South
Durham
Solids
09/il/2019
09:46
09/12/2019
SM-4600-NH3C
WTN
68183
South
Durham
Solids
09/11/2019
09:46
09/12/2019
9046D
WTN
68183
South
Durham
Solids
09/11/2019
09:46
09/12/2019
4600NO3F-2011
WTN
68183
South
Durham
Solids
09/11/2019
09:45
09/12/2019
6010D
WTN
68183
South
Durham
Solids
09/11/2019
09:46
09/12/2019
SW-74716
WTN
68183
South
Durham
Solids
09/11/2019
09:45
09/12/2019
SM-4500-NH3C-TKN
WTN
68183
South
Durham
Solids
09/11/2019
09:46
09/12/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 -Virginia
Page ? of 6

Report Number: 19-255-0012
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : South Durham
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.wa yp ointa na I yti cal. co m
REPORT OF ANALYSIS Date Sampled: 9/11/2019 09:45:00
Lab Number: Date Received: 09/1212019 00:00
Sample Id :Soouthuth Durham Date Reported: 09/20/2019
Moisture
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
83.10
5.43
3.50
0.30
1.16
1.79
0.58
0.09
1.00
4.43
54300
35000
2980
11600
17900
5760
853
19800
32500
862
340
2610
10000
44300
<4.49
250
50.0
50.0
50.0
250
50.0
250
50.0
50.0
5.00
2.50
12.5
100
250
4.49
AUM
ADM
JPJ
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
JPJ
09/16/2019
16:59
09/16/2019
16:59
09/19/2019
13:00
09/17/2019
20:08
09/17/2019
20:08
09/17/2019
20:08
09/17/2019
20:08
09/17/2019
20:08
09/17/2019
20:08
09/17/2019
20:08
09/17/2019
20:08
09/17/2019
20:08
09/1 '12019
20:08
09/17/2019
20:08
09/1 112019
15:30
09/112019
13:00
09/19/2019
15:12
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
SM-2540G
SM-254OG
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
601OD
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
Ouneports and letters are for the exclusive and confidential use ofour clients, and maynot be reproduced in whole or part, nor may anyrefen:nce be made
to the work, the results, or the company in any advedising, news release, oro(herpublic announcemen(s rnthout obtaining our prior whiten authohzation.
Pauric McGroary
Agronomist

Report Number: 19-255-0012
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : South Durham
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
wwwiwaypoin to na I ytica I. com
Lab Number: 68183 REPORT OF ANALYSIS Date Sampled: 9/11/2019 09:45:00
Sample Id : South Durham
Date Received: 09/12/2019 00:00
Date Reported: 09/20/2019
Cadmium <1.00 1.00 BKN 09/17/2019 20:08
Chromium 30.5 2,50 BKN 09/17/2019 20:08
Nickel 22.6 2.50 BKN 09/17/2019 20:08
Lead 18.2 3.00 BKN 09/17/2019 20:08
Arsenic 6.12 5,00 BKN 09/17/2019 20:08
Mercury 0.490 0,0148 TJS 09/17/201913:45
Selenium <5.00
5.00 BKN 09/17/2019 20:08
pH
* 8.4 JSL 09/18/2019 06:19
Molybdenum 17.9 2,50 BKN 09/17/2019 20:08
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
6010D
6010D
6010D
6010D
6010D
S W-7471 B
6010D
9045D
6010D
n1Cf
gala Ire V�
Our reportscnd letters are Ior the exclusive and confitlenfial use ofour clients, and may notbe reproduced in rvhole or part, normay anyre/e2nce be made to the work, tfie results, or the companyin any advertising, news release, oro(her public announcements rnthout obtaining our prior written aulhorization. Paurlc MCCifCary
Agronomist

m
7621 Whitepine Road, Richmond, VA 23237
Main 804743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.corn
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/Durham
Report Number: 19-255-0012
Shipping Method
Fed Ex � US Postal � Lab 0 Other:
UPS � Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes � No
Number of coolers received � �
Custody seals intact on shipping container/cooler? � Yes � No ®Not Required
Custody seals intact on sample bottles? � Yes � No ®Not Required
Chain of Custody (COC) present? Yes � No
COC agrees with sample label(s)? Yes 0 No
COC properly completed ®Yes � No
Samples in proper containers? ®Yes � No
Sample containers intact? ®Yes � No
Sufficient sample volume for indicated test(s)? ®Yes 0 No
All samples received within holding time? ®Yes � No
Cooler temperature in compliance? ®Yes 0 No
Cooler/Samples arrived at the laboratory on ice. ®Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No N/A
Water -VOA vials free of headspace � Yes � No ®N/A
Trip Blanks received with VOAs � Yes � No N/A
Soil VOA method 5035 —compliance criteria met 0 Yes � No ®N/A
� High concentration container (48 hr) Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) I— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes No
Comments:
Signature: Brandi Watson Date &Time: 09/12/2019 12:03:34
Page 5 of 6

U
z
CO
g
s
i
I
C.
mm
8
e
n
�to:
��
O
lu
`m
vj
s
J
ow
IL
C �
a
S
Ora
oLUC3
u
C
y
y
ui
3L
2
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z
5
O
w
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-=
w
o
mf
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00
4
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z
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cc
4
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[at
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b
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HEM
NEE
MEN
MEE
IBM
IBM
BENI
IBM
NEE
NEE
on
wmm
OEM

_ ,.
Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range Ratio
2012.02-ANDCAK-NC
DURHAM, NC S. DURHAM WWTP ANAEROB.
9/11/2019
10/1/2019-10/31/2019 0.5815
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (853 x 16.9000) + 100 = 144.157
Ca mg/I = (Ca mg/kg x %Solids) + 100 = (17900 x 16.9000) + 100 = 3025.1
Mg mg/I = (mg mg/kg x %Solids) + 100 = (5760 x 16.9000) + 100 = 973.44
Na meq = Na mg/I + Molec. Wgt.Na = 144.157 + 23 = 6.2677
Ca meq = Ca mg/I + Molec.Wgt.Ca = 3025.1 + 20 = 151.255
Mg men = Mg mg/I + Molec. Wgt.Mg = 973.44 + 12 = 81.12
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.2677 + SgrRoot[0.5(151.255+g1.12)] = 0.581471
Page 1 Printed: 1/30/2020
16:54

7621 Wfiitepine Road, Richmond, VA 23237
Main 804-743-9401°Fax [phone]
www.waypointanalyti p l.com
11/18/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref; Analytical Testing
Report Number: 19-312-0012
Project Description: South Durham
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 11/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were pertormed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures pertormed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were pertormed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, of laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalytical.com
Sample Summary Table
Report Number: 19-312-0012
Client Project Description: South Durham
Lab No Client Sample ID Matrix Date Collected Date Received Method
lab IC
69540 South Durham Solids 11/06/2019 07:25 il/08/2019
69540 South Durham Solids 11/06/2019 07:Z5 11/08/2019 SM-4600-NH3C WTN
69540 South Durham Solids il/06/2019 07:26 11/08/2019 9046D
WTN
69640 South Durham Solids 11/O6/2019 07:26 11/OS/2019 4500NO3F-2011 WiN
69640 South Durham Solids 11/06/2019 07:26 11/08/2019 6010D
WTN
69640 South Durham Solids 11/O6/2019 07:26 11/OS/2019 SW-7471B
WTN
69640 South Durham Solids il/06/2019 07:26 11/OS/2019 SM-4600-NH3C-TKN WTN
69540 South Durham Solids 11/O6/2019 07:26 il/08/2019 SM-2640G WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

46461
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 270Z8
Submitted By : Ryan Copeland
Report Number:l9-312-0012
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401'Fax [phone]
www.waypointa na lytical.com
Ryan Copeland
Project South Durham
Information
REPORT OFANALYSIS
Report Date: 11/18/2019
Received : il/08/2019
�aw�G l�` 6��/
Pauric McGroary
Agronomist
Lab No : 69540 Matrix: Solids
Sample ID :South Durham Sampled: 11/6/2019 7:25
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 10100 mg/Kg -dry 617 1 11/16/19 16:00 ]PJ SM-4500-NH3C
Nitrate+Nitrite-N <30.9 mg/Kg -dry 30.9 1 li/12/19 14:17 ZBD 4600NO3F2011
Organic N 46300 mg/Kg -dry 1640 1 11/16/19 12:00 G4LCULATION
pH 8.3 s.u. 1 11/12/19 06:08 7SL 9046D
Total Solids 16.2 � 0.010 1 11/11/19 16:35 ADM SM-2640G
Total Kjeldahl Nitrogen 56400 mg/Kg -dry 1640 1 il/16/19 12:00 ]P] iM-4600-NH3C-TIU
Phosphorus 43600 mg/Kg -dry 30.9 1 11/13/19 02:69 KKM 6010D
Aluminum 37000 mg/Kg -dry 30.9 1 11/13/19 02:69 KKM 6010D
Arsenic 6.23 mg/Kg -dry 3.09 1 11/13/19 02:69 KKM 6010D
Calcium 21000 mg/Kg -dry 164 1 11/13/19 02:69 KKM 6010D
Cadmium 0.914 mg/Kg -dry 0.617 1 11/13/19 02:59 KKM 6010D
Chromium 20.1 mg/Kg -dry 1.64 1 il/13/19 02:69 KKM 6010D '
Copper 377 mg/Kg -dry 1.64 1 11/13/19 02:69 KKM 6010D
Iron 18800 mg/Kg -dry 30.9 1 11/13/19 02:69 KKM 6010D
Lead 20.6 mg/Kg -dry 1.86 1 il/13/19 02:59 KKM 6010D
Magnesium 6790 mg/Kg -dry 30.9 1 il/Y3/19 02:69 KKM 6010D
Manganese 710 mg/Kg -dry 3.09 1 11/13/19 02:59 KKM 6010D
Mercury
0.572 mg/Kg -dry 0.0932 1 11/12/19 14:38 T]S SW-74716
Molybdenum 22,6 mg/Kg -dry 1.54 1 li/13/19 02:59 KKM 6010D
Nickel 18.8 mg/Kg -dry 1.64 1 11/13/19 02:69 KKM 6010D
Potassium 3150 mg/Kg -dry 30.9 1 11/13/19 OZ:69 KKM 6010D
Selenium
6.1Y mg/Kg -dry 3.09 1 11/13/19 02:69 KKM 6010D
Sodium 1130 mg/Kg -dry 154 1 li/13/19 02:69 KKM 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

46461
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC Z7028
Submitted By : Ryan Copeland
Report Number :l9-312-0012
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalytiwl.com
Ryan Copeland
Project South Durham
Information
REPORTOFANALYSIS
Report Date : 11/18/2019
Received : 11/OS/Z019
Pauric McGroary
Agronomist
Lab No : 69540 Matrix: Solids
Sample ID :South Durham Sampled: 11/6/2019 7:25
Test Results Units MqL DF Date/Time By Analytical
Analyzed Method
Zinc 2790 mg/Kg -dry 7.72
Sulfur 13000 mg/Kg -dry 30.9
Moisture 83 $
0.010
Qualifiers/ g Analyte detected in blank
Definitions
1
11/13/19
02:69
KKM
6010D
1
11/13/19
OZ:S9
KKM
6010D
1 11/11/1916:36 ADM SM-Z640G
H Beyond holding time
Page 4 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804743-9401 °Fax [phone]
ANALYTICAL www.waypointanaiytipl.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/Durham
Report Number: 19-312-0012
Shipping Method
0 Fed Ex � US Postal � Lab 0 Other:
UPS 0 Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes 0 No
Number of coolers received ��
Custody seals intact on shipping container/cooler? � Yes 0 No Not Required
Custody seals intact on sample bottles? � Yes � No Not Required
Chain of Custody (COC) present? ®Yes � No
COC agrees with sample label(s)? ®Yes � No
COC properly completed ®Yes 0 No
Samples in proper containers? ®Yes � No
Sample containers intact? ®Yes (� No
Sufficient sample volume for indicated test(s)? ®Yes � No
All samples received within holding time? ®Yes � No
Cooler temperature in compliance? ®Yes � No
Cooler/Samples arrived at the laboratory on ice. Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No ®N/A
Water -VOA vials free of headspace � Yes � No N/A
Trip Blanks received with VOAs � Yes � No N/A
Soil VOA method 5035 —compliance criteria met � Yes � No N/A
r High concentration container (48 hr) r— Low concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) � Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes No
Comments:
Signature: Brandi Watson Date &Time: 11/08/2019 13:13:51
Page 5 of 6

SAMPLING LOG ��LEAS
G 17621 Whitt
CUSTOME NAGRW: .1%
PROJECT
t. • • e
I�IIIIIIIIIII'III1IIIIIIIII�I�I�IIII�IIIIIIIIIIIIIIIIII�IIIIII ;eao 12019 F CUSTODY
Smaoro ComroI LLG Dwham 13:13:17 & ANALYSIS
South Durham CORD
I attest that the proper field sampling procedures
were used during the collection of these samples.
Y,w CqPau"
A & L CUSTOMER SAMPLING SAMPLE WWI SAMPLINQ METHOD METHOD
LAB H SAMPLE I.D. LOCAYION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
�MLFJZ //
SouAJO(LHAa STOI* ARp S ome Illa/iq 1:15 ICE (UI
by Sampler:
Railnquished by:
by:
Time Recieved by:
REMARKS:
SPECIAL INSTRUCTIONS:,, ++ �O �--� I f'• ,� ^Q /��
For IV mon orinapurposes. JQ �PgO,(NuMll C_�>
MOM
�IIML790MEEMM
SLi: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium ,
SL2: Basle Test SLi plus SUifur, Calolum, Magnesium, Sodium, Iron, Aluminum, Mangansse, Copper and Zino

Product Code Product Name Sample Date Report Range Ratio
2012.02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 11/6/2019 11/1/201942/31/2019 0.6957
DIGESTED CAKE
Na mg/I = (Na mg/kg x %Solids) + 100 = (1130 x 16.2000) + 100 = 183.06
Ca
mg/I =
(Ca
mg/kg x
%Solids)
+
100 =
(21000 x 162000) + 100
= 3402
Mg
mg/I
= (mg
mg/kg x
%
Solids) +
100
= (6790 x 16.2000) + 100 =
1099.98
Na meq = Na mg/I + Molec. Wgt. Na = 183.06 + 23 = 7.95913
Came
= Ca mg/I + Molec.Wgt.Ca = 3402 +20 = 170.1
Mg meq = Mg mg/I + Molec.Wgt.Mg = 1099.98 + 12 = 91.665
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.95913 + SgrRoot[0.5(170.1+91.665)j = 0.695705
Page 1 Printed: 1/30/2020
16:55

' •,
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003504 Laboratory
Facility Name; DURHAM, NC PACE ANALYTICAL SERVICE INC.
NPDES# : Waypoint Analytical Virginia Inc.
or WQ# (residual only)
WWTP Name: BROWN WTP
Residuals Analysis Data
Product Type WPC WPC 6'dPC WPC
Date Sampled (grab) or Ol/07 /19 04/16/19 07/24/19 11/06/19
Date Composited
Percent Solids 16. 60 19.70 18.20 16. 70
PARAMETERS (mglkg dry weight)
Arsenic 7.8 <25 8.78 5. 91
Cadmium <0.33 <5 2.99 6.53
Mercury o.097 O. o714 0.0606 <0.094
Chromium Nrt 20.1 29.4 7.9
Copper 116 97.5 1280 647
Lead 13.8 <15 5.02 8.68
Molybdenum 2.1 <12.5 3.12 2,76
Nickel 14.2 <12.5 48 a7.4
Selenium <3.3 <25 <25 <29.9
Zinc 27.7 62.5 65.6 122
Total Phosphorus 547 1100 886 1010
TKN 5230 12000 11800 16900
Ammonia -Nitrogen <45.7 508 714 1000
Nitrate and Nitrite <11.4 <5 <4. 71 <28. 6
"I certify under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date 2/�y>l�o�d

Permit Number: WO0003504
Facility Name: DURHAM, NC
NPDES#:
or WQ# (residual only)
WWTP Name: BROWN WTP
Residuals Analysis Data
Product Type vaPc caPc
Date Sampled (grab) or Ol/o7/19 09/16/19
Date Composited
Percent Solids 16.80 19.70
Laboratory
PACE ANALYTICAL SERVICE INC.
Waypoint Analytical Virginia Inc.
wPc vrPc
07/24/19 11/06/19
18.20 16.70
PARAMETERS (mg/kg dry weight)
Aluminum
13000
12300
9840
9130
Calcium
345
1250
790
1240
Magnesium
359
378
221
278
pH
4.50
4.30
9.80
6.20
Potassium
<1630
<250
125
217
SOdIUm
<1630
<1250
345
397
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
� �
Date �/�i�ZOZr7
NR -Data Not Reported or Data Not Required

94407
"Analyticalo
wwwpacelabamm
January 15, 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: Durham -Brown WTP
Pace Project No.: 92413358
Dear Nate Roth:
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for samples) received by the laboratory on January 08, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lord
Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORYANALYSIS
This report shall not be reprotluced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

Project: Durham -Brown WiP
Pace Project No.: 92413358
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianaINELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NO 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certifcation #: 40
South Carolina Certification #: 99030001
VirginiaIVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotluced, except in full,
without the written consent of Pace Analytcal Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NO 28078
(704)8759092
Page 2 of 16

Project: Durham -Brown WTP
Pace Project No.: 92413358
Lab ID Sample ID
92413358001 Durham-Brown1 of
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA6010D
DS
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 254OG-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
DMN
1
PASI-A
EPA 350.1 Rev 2.01993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.01993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducetl, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 16

Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Durham -Brown WTP
Pace Project No.: 92413358
Sample: Durham -Brown 1 of Lab ID: 92413358001 Collected: 01/07/1910:15 Received: 01/08/1912:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 30506
Aluminum 13000 mg/kg 32.6 1 01/11/1909:20 01113/1922:42 7429-90-5
Arsenic 7.8 mg/kg 3.3 1 01111/1909:20 01/12/1915:14 7440-38-2
Cadmium ND mg/kg 0,33 1 01/11/1909:20 01113/1922:42 744043-9
Calcium 345 mg/kg 32.6 1 01/11/1909:20 01113/1922:42 7440-70-2
Copper 116 mg/kg 1.6 1 01111/1909:20 01/13/1922:42 7440-50-8
Lead 13.8 mg/kg 1.6 1 01/11/1909:20 01/13/1922:42 7439-92-1
Magnesium 354 mg/kg 32.6 1 01/11/1909:20 01/13/1922:42 7439-95-4
Molybdenum 2A mg/kg 1.6 1 01/1111909:20 01/13A922:42 7439-98-7
Nickel 14.2 mg/kg 1.6 1 01/11/1909:20 01/13/1922:42 7440-02-0
Potassium ND mg/kg 1630 1 01/11/1909:20 01/13/1922:42 7440-09-7
Selenium ND mg/kg 3.3 1 01/11/1909:20 01/12/1915:14 7782-49-2
Sodium ND mg/kg 1630 1 01/1111909:20 01/13/1922:42 7440-23-5
Zinc 27.7 mg/kg 3.3 1 01/11/1909:20 01/13/1922:42 7440-66-6 BC
7471 Mercury Analytical Method: EPA 7471B Preparation Method: EPA 7471E
Mercury 0,097 mg/kg 0.027 1 01/11/1921:31 01114/1912.15 7439-97-6
254OG Total Percent Solids Analytical Method: SM 2540G-2011
Total Solids 16.8 % 0.000010 1 01/10/19 13:28
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 83.2 % 0.10 1 01/10/19 13:19
9045 pH Soil Analytical Method: EPA 9045D
pH at 25 Degrees C 4.5 Std. Units 0.10 1 01/15/19 10:50 H3
Plant Available Nitrogen Analytical Method: SM 271 OB-2011
Plant Available Nitrogen 1570 mg/kg 0.12 1 01/15/1911:49 N2
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia ND mg/kg 45.7 1 01/1211910:40 01/12/1915:17 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total 5230 mg/kg 258 1 01/14/1911:34 01/1511904:49 7727-37-9 M11R1
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3 ND mg/kg 11.4 1 01/10/19 01:57 01/10/19 03:47
Nitrogen, Nitrate ND mg/kg 11.4 1 01/10/19 01:57 01/10/19 03:47 14797.55-8
Nitrogen, Nitrite ND mg/kg 5.7 1 01/1011901:57 01/10/1903:47 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2,0 1993
Phosphorus 547 mg/kg 11.4 1 01/09/19 20:23 01/10/19 13:51 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
)ate: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 16

04017
aceAnalytical®
w .pawlabscam
Project: Durham -Brown WTP
Pace Project No.: 92413358
tic esaicn: 452089
QC Batch Method: EPA 7471E
Associated Lab Samples: 92413358001
METHOD BLANK: 2472136
Associated Lab Samples: 92413358001
Parameter Units
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 2472137
Parameter Units
Mercury mg/kg
Pace Analytical Services, LLC
9800Kincey Ave. Suite loo
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7471 B
Analysis Description: 7471 Mercury
Matrix: Solid
Blank
Reporting
Result
Limit
Analyzed
Qualifiers
NO 0.0060
01/1411912:06
Spike
LCS
LCS
%Rec
Conc.
Result
%Rec
Limits Qualifiers
0.083
0.067
81
80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2472138
2472139
MS
MSD
92413378001 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result %Rec %Rec Limits RPD Qua[
Mercury mg/kg 0.0063 0.055
0.057
0,048
0.049 75 75 75-125 3
Rosults presontotl on this page aro in No units Intlicatotl by the "llnits" column oxcept whora an altomafo unit is pmsontptl to tho right of tho result
Jate: 01/15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 5 of 16

QUALITY CONTROL DATA
Project: Durham -Brown WTP
Pace Project No.: 92413358
QC Batch Method: EPA 3050E
Associated Lab Samples: 92413358001
Analysis Method:
Analysis Description:
EPA 601 OD
6010 MET
METHOD BLANK: 2471114
Matrix: Solid
Associated Lab Samples: 92413358001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Aluminum
mg/kg
NO
10.0
01/13/19 22:18
Arsenic
mg/kg
NO
1.0
01/13/19 22:18
Cadmium
mg/kg
NO
0.10
01/13/19 22:18
Calcium
mg/kg
NO
10.0
01/13/19 22:18
Copper
mg/kg
ND
0.50
01/13/19 22:18
Lead
mg/kg
NO
0.50
01/13/19 22:18
Magnesium
mg/kg
ND
10.0
01/13/19 22:18
Molybdenum
mg/kg
NO
0.50
01/13/19 22:18
Nickel
mg/kg
NO
0.50
01/13/19 22:18
Potassium
mg/kg
NO
500
01/13/19 22:18
Selenium
mg/kg
NO
1.0
01/13/19 22:18
Sodium
mg/kg
ND
500
01/1311922:18
Zinc
mg/kg
NO
1.0
01/13/19 22:18
BC -
LAtioRgTORY CONTROL SAMPLE:
Parameter
2471115
Units
Spike
Conic.
LCS
Result
LCS
%Rec
% Rec
Limits
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifers
MArRIx SPIKE &MATRIX SPIKE DUPLICATE: 2471116 2471117
MS MSD
92413357001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qua]
Aluminum mg/kg 55600 9280 8310 69300 63600 148 96 75-125 9 M1
Arsenic mg/kg NO 928 831 827 734 89 88 75-125 12
Cadmium mg/kg NO 928 831 848 758 91 91 75-125 11
Results
prosonmtl on this page are in the units Indicated by the "Units" column except whom an alternate unit is presented to tho right of the result
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
)ate: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16

QUALITY CONTROL DATA
Project: Durham -Brown WTP
Pace Project No.: 92413358
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
1704)875-9092
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE:
2471116
4471117
MS
MSD
92413357001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
17500
9280
8310
27500
25000
107
90
75-125
9
Copper
mg/kg
393
928
831
1350
1220
103
99
75-125
10
Lead
mg/kg
23.2
928
831
865
770
91
90
75-125
12
Magnesium
mg/kg
3700
9280
8310
12700
11400
97
93
75-125
11
Molybdenum
mg/kg
11.7
928
831
900
804
96
95
75-125
11
Nickel
mg/kg
15.5
928
831
871
778
92
92
75-125
11
Potassium
mg/kg
ND
9280
8310
13000
11900
97
95
75-125
9
Selenium
mg/kq
ND
928
831
783
687
84
82
75-125
13
Sodium
mg/kg
ND
9280
8310
11100
10100
92
91
75-125
10
Zinc
mg/kg
1880
928
831
2770
2570
97
84
75-125
8
Rosulfs prosontntl on this pa90 aro in tho units intlicaWd by tho "Units" column except whom an altomato unit is prosontod to tho right of tho rosui[.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
)ate: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16

el
aceAnalXical
wrwWoefab&wm
Project: Durham -Brown WTP
Pace Project No,: 92413358
QC Batch: 451773
QC Batch Method: ASTM 1)2974-87
Associated Lab Samples: 92413358001
SAMPLE DUPLICATE: 2470313
Parameter Units
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Peroent Moisture
92413062001 Dup
Result Result RPD Qualifiers
1.1 0.80 35 D6
svlwrL.t uuHUCATE: 2470314
92413381002 Dup
Parameter Units Result Result
Percent Moisture % 96.7 96.7
RPD Qualifiers
0
Pace Analytical Services, LLC
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results pmsonWtl on this pago aro in the units intlicamtl by No "Units" column oxcopt whom an altomato unit is presontetl to tho right of tho insult
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
'ate: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, U.C. Page 8 of 16

00007
aceAnalXical
w zpacelablwm
Project: Durham -Brown WTP
Pace Project No.: 92413358
W� Dawn. 45L9 /L
QC Batch Method: EPA 9045D
Associated Lab Samples: 92413358001
SAMPLE DUPLICATE: 2472426
Parameter
pH at 25 Degrees C
�Alvlrlt uuPLICATE: 2472427
Parameter
PH at 25 Degrees C
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
92413563001 Dup
Units Result Result RPD Qualifiers
Std. Units 5.2 5.3 0 H3
92413312001 Dup
Units Result Result RPD Qualifiers
Std. Units 6.8 6.8 0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Rosults pmsontotl on this page arc in No units Intlicatatl by the "Units" column oxcept whom an aitomato unit is prosontotl to No right of Ne rosolb
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
ate: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
,t._- 7
Page 9 of 16

aceAnalXical
Project: Durham -Brown WTP
Pace Project No.: 92413358
W. Dawn. 4JLU23
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92413358001
METHOD BLANK: 2471582
Associated Lab Samples: 92413358001
Parameter Units
Nitrogen, Ammonia mg/kg
LABORATORY CONTROL SAMPLE: 2471583
Parameter Units
Nitrogen, Ammonia mpg
Pace Analytical Services, LLC
sa00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 8.9 01112/1915:09
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
472 464 98 90-110
Ivwl Rlx sF'IKE &MATRIX SPIKE DUPLICATE: 2471584 2471585
MS MSD
92413357001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 13200 10300 10500 21800 22500 83 89 90-110 3 M6
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2471586 2471587
MS MSD
92413358001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Ammonia mg/kg ND 2320 2320 2210 2210 93 93 90-110 0
Results prosentotl on this pago aro In tho units indicated by tho "Units" column txtopt where an altomato unit is prosontttl to tho right of tho rtsulC
Date: 01 /15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotlucee, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 16

Project: Durham -Brown WTP
Pace Project No.: 92413358
Wn. Dawn. 4JLL'19
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92413358001
METHOD BLANK: 2472536
Associated Lab Samples: 92413358001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
tAt3UKAlUKY CONTROL SAMPLE: 2472537
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 01/15/1904:45
Spike LCS LCS %Rec
Cone. Result %Rec Limits Qualifiers
1000 967 97 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2472538 2472539
MS MSD
92413357001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Kjeldahl, Total mg/kg 62000 21200 19000 74700 74800 60 67 90-110 0 M1
MAI KIX SPIKE &MATRIX SPIKE DUPLICATE: 2472540 2472541
MS MSD
92413358001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone, Cone. Result Result %Rec %Rec Limits RPD Qua[
Nitrogen, Kjeldahl, Total mg/kg 5230 5170 5170 8110 9500 56 83 90-110 16 M11R1
Rosults prosontotl on this page are in No units InGicatotl by No "Units" column oxcopt whoro an altamato unit is prosontatl to No right of tho rosult
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
late: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, U.C.
Page 11 of 16

aceAnalyiical
w ..pacdabxcom
Project: Durham -Brown WTP
Pace Project No.: 92413358
QC Batch: 451629
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92413353001
QUALITY CONTROL DATA
Analysis
Method:
EPA 353.2 Rev
2.0 1993
Analysis
Description:
353.2 Nitrate+
Nitrite
Ivle I rrUu tsLANK: 2469664
Matrix: Solid
Associated Lab Samples: 92413358001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Nitrogen, Nitrate
mg/kg
ND 2.0
01/10/19 03:42
Nitrogen, Nitrite
mg/kg
ND 0.98
01/10/19 03:42
Nitrogen, NO2 plus NO3
mg/kg
ND 2.0
01/10/19 03:42
Qualifiers
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 10o
Huntemville, NC 28078
[phone]
LAt3URATORY CONTROL SAMPLE:
2469665
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result %Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.9
15.8 106 90-110
Nitrogen, Nitrite
mg/kg
9.9
10.6 107 90-110
Nitrogen, NO2 plus NO3
mg/kg
24.8
26.4 107 90-110
MAl KIX
SPIKE & MATRIX
SPIKE DUPLICATE:
2469666
2469667
MS
MSD
92413357001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen,
Nitrate
mg/kg
ND
425
420
412
393
97
93
90-110
5
Nitrogen,
Nitrite
mg/kg
ND
286
280
305
308
100
102
90-110
1
Nitrogen,
NO2 plus NO3
mg/kg
ND
711
702
717
701
100
99
90-110
2
Rosulfs pmsontotl on this pa90 aro In Wn unlg indicatotl by tho "Units" column extopt whero an altomatt unit is premntod to tho right of tho result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
)ate: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Durham -Brown WTP
Pace Project No.: 92413358
QC Batch: 451598
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92413358001
METHOD BLANK: 2469443
Associated Lab Samples: 92413358001
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Solid
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 01/10/1913:45
LABORATORY CONTROL SAMPLE: 2469444
Spike LCS LCS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phosphorus mg/kg 49 52.3 107 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2469445 2469446
MS MSD
92413357001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc Conc. Result Result %Rec %Rec Limits RPD Qual
Phosphorus mg/kg 24300 1100 1100 23200 23300 -99 -88 90-110 1 M6
Rosults prcsonted on this pago arp in the nnifs intlicafetl by tho "Units" colomn oxeopt whom an altpmato unit is pmson[otl to the right of tho result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reprotlucetl, except in full,
ate: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Durham -Brown WTP
Pace Project No.: 92413358
DEFINITIONS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
112-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) -Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U -Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
PaceAnalytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical
Services -Asheville
PASI-C
Pace Analytical
Services -Charlotte
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a wncentration above 1/2 the reporting limit but below the
laboratory reporting limit.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELACffNI accreditation for this parameter.
R1 RPD value was outside control limits.
gate: 01/15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 16

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 1o0
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Durham -Brown WTP
Pace Project No.: 92413358
Sao w Sample ID QC Batch Method QC Batch Analytical
Analytical Method Batch
92413358001 Durham -Brown 1 of 4 EPA 30506
451935 EPA6010D 451945
92413358001 Durham -Brown 1 of 4 EPA 7471 B
452089 EPA 74716 452120
92413358001 Durham -Brown 1 of 4 SM 2540G-2011
452044
92413358001 Durham-Brown1 of ASTM D2974-87
451773
92413358001 Durham -Brown 1 of 4 EPA 9045D
452172
92413358001 Durham -Brown 1 of 4 SM 2710E-2011
452503
92413358001 Durham -Brown 1 of 4 EPA 350.1 Rev 2.0 1993 452023 EPA 350.1 Rev 2.0 1993 452144
Mod. Mod.
92413358001 Durham -Brown 1 of 4 EPA 351.2 Rev 2.0 1993 452219 EPA 351.2 Rev 2.0 1993 452403
92413358001 Durham -Brown 1 of 4 EPA 353.2 Rev 2.0 1993 451629 EPA 353.2 Rev 2,0 1993 451647
92413358001 Durham -Brown 1 of 4 EPA 365.1 Rev 2.0 1993 451598 EPA 365.1 Rev 2.0 1993 451656
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Ite 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 16
�..,

CHAIN-0F•CUST0DYAnalytical Request Document
LAB USE ONLY* AffixWorkon w®ll 92413358
aceMalytieale
Chalmo&Custodyls a LEGAL DOCUMENT, Complete all relevant fields
IF IIIII� II III,I'LII'I I III
Al1 1,L'$IiADEC 92413358 :
Company: SYNAGRO
Billing Information: Mary Brewer: 284 Tord, Mockwille
NC 27028
Address: 284 Boger Rd., Mocksville, NC 27028
-
ContainerPreservativeType'•
-
Wb Pro)ect'Manager.
IF
-
ReportTo: Nate Roth([e-mail])
Emaif To: [e-mail]
'• Preser alive Types: (1) nitric add, (2)suffuric add, (31 Tydrorhloac add, (4)Sodium hydroxide, (5) 211e acetate,
(6)methanol,(7)fodium bhuifate,(9) sodium thsosuNatq(S)hexane,0) ascorbic acid,(8)ammonlum sulfate,
Copy To: IF Finnerty([e-mail])
Site Collection info/Address:
(C) ammonium hydroxide, (D)TSP, (Ul Unpreserved, (D)Dther.
Analyses
Lab Profile/urie:
Cu
mar roject Name/ umber:
State: County/City: Time Zone Collected:
6
-
Lab Sainiple Racejpt Cheoklist
C toay seele Y e nt/I "toot Y N
C todY S gp turse present } tr4
'
/ I )PT f )MT I ICT f JET
Phone: aas+oa+azn
Site/Facility I N:
Compllance Monitoring?
Email: [e-mail]
(Xj Yes ( j No NC (%J SC ()
li ctors3.q atuYe PYasB t Y Y i7li
_
IL-C
a the Inca: t {N NA..
Collected By (print: Clay Flsacked Y
Purchase0rderd:
DW PWSID N:
Duracell; N:
DW Location Code:
a
C e t Bott1 s I( YA
S ffisi nt Vol a PI 27A'.-
9 apla Aacei na on Ice - H NA, -.
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Turnaround Date Required:
Immediately Packed on Ice:
[ % Yes ( j No
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VOA Readspace -Acceptable; N N I
USDA RegµlaCpd Soils ,_ 11'.
samples an Holdi gTl C�nT
pl pos
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Rush:
Field Filtered applicable):
[ ]Same Day [ )NeM Day
[ )Yes [ )No
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11431dual Chloriner.ei Y
( IArchNe:
[ )2Day [ 13 Day 1 )4Day I )S Day
-
Z
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-
V
N
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01 StiriPs: ,._ IF
( ) Ho!d:
Expedite Charges
( rgez Apply)
Analy515:
rn
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N
UO'
`.U,,
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P-'
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Sd pla PR Acceptable 'Y N (+R'
pH StYlpst'
Sulfido PYesent
'Matrix Codes (Insert in Matrix box helow): Drinking Water (DW), Ground Water(GIN), Wastewaisr(WW),
Product (P), Soil/Solid ($L), Oil (OL), Wipe (WP), Air (AR), Tissue (TS1, Bioassay (8), Vapor (Vf, Other(Off
= m
Q
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TyPeoff[e Used: et Blue `Dry None SHORTHOLD$ PRESENT(<72hours):':'Y
N N/A-:.
LAB Sample Temperature Info:"
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Yeap Blank Repaived: ❑
Packing Miterial Used:
Labffecking N:
II IFIIF
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_
'Them
Caolux 1''Tesp upon Rocoipt:'f3oC
"
Radchem 5ampie(s)s&eened {dOD cpm): - Y N NA
Samples receive ma:-.
CooleY 1-:Th rm Corr. -.Factor: 0 oC
C®ri I Co Yectad Tertpr oe -
FEDEX. UPS tent Courier; Pace Courier '.
-
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Date/Time:
MTIL LAB USE ONLY
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Relinquished by{o pony: (Signature)
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Received by/Company:(Signature)
Date/Time:
gcctnufn:
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Relinquished by/Company: (Signature)
Date/Time:
Received by/Company: (Signature)
Date/Time:
Non Conformance(s):
Pager
PB: fF 11.YES:/
NO
of:
—Page 1 0
16

3odium Absorption• Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-04-WPC-NC DURHAM, NC BROWN WTP CAKE 1/7/2019 1/1120194/30/2019 6.0081
mg/kg x %Solids) + 100 = (1630 x 16,8000) + 100 = 273.84
Ca
mg/I
= (Ca
mg/kg x
%
Solitls) +
100
= (345 x
16.8000I
+
100
= 57.96
Mg
mg/I
= (mg
m91k9 x
%
Solids) +
100
= (354 x
16.8000)
+
100
= 59,472
Na meq = Na mg/I + Molec. Wgt.Na = 273.84 + 23 = 11.9061
Ca meq = Ca mg/I + Molec.Wgt,Ca = 57.96 + 20 = 2.898
Mg meq = Mg mg/I + Molec.Wgt.Mg = 59.472 + 12 = 4.956
SAR = Na meq + SgrRoot(0.5 x (Ca meq + Mg meq)] = 11.9061 + SgrRoot[0.5(2.898+4,956)] = 6.00812
Page 1 Printed: 1/30/2020
17:00

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010Pax 804-271-6446
www,waypointanalytica I, com
4/26/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-107-0206
Project Description: Durham Brown
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/17/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 7

Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
wwwowaypointa nalytical. com
Client: Synagro Central LLC/ Durham CASE NARRATIVE
Project: Durham Brown
Lab Report Number: 19-107-0206
Date: 4/2512019
Metals Analysis Method 6010D
Sample 65936 (Durham Brown)
QC Batch No: 1.432601/L432245
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 2 of 7

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www,wayp o f nta n a lytica l.co m
Sample Summary Table
Report Number: 19407-0206
Client Project Description: Durham Brown
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019 SM-4500-NH3C WTN
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019 9045D VJTN
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019 4500NO3F-2011 WTN
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019 6010D WTN
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019 SW-7471B WTN
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019 SM-4500-NH3C-TKN WTN
65936 Durham Brown Solids 04/16/2019 09:00 04/17/2019 SM-2540G WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: �1354

Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
i Mocksville , NC 27028
Project : Durham Brown
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Lab Number: 65936 REPORT OFANALYSIS Date Sampled: 4/16/2019 09:00:00
Sample Id : Durham Brown
Date Received: 04/17/2019 00:00
Date Reported: 04/26/2019
Total Solids' 19.70 197000 100.0 ADM 04/19/2019 15:34
Moisture ` 80.30 100.0 ADM 04/19/2019 15:34
Total Kjeldahl Nitrogen 1.20 12000 250 JPJ 04/23/2019 10:00
Phosphorus 0.11 1100 250 KKM 04/24/2019 13:18
Potassium <0.03 <250 250 KKM 04124/201913:18
Sulfur 0.66 6610 250 KKM 04124/201913:18
Calcium <0.13 <1250 1250 KKM 04/241201913:18
Magnesium 0.04 378 250 KKM 04/241201913:18
Sodium <0.13 <1250 1250 KKM 04/24/201913:18
Iron 317000 250 KKM 04/241201913:18
Aluminum 12300 250 KKM 04124/201913:18
Manganese 599 25.0 KKM 04/24/201913:18
Copper 97.5 12.5 KKM 04/24/201913:18
Zinc <62.5 62.5 KKM 04/24/201913:18
Ammonia Nitrogen 0,05 508 100 JPJ 04/21/2019 16:00
Organic N 1,15 11492 250
04/21 /2019 16:00
Nitrate+Nitrite-N <5.00 5.00 ZBD 04/24/201914:20
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time
1 tr�tf(G
Our its and letters are for the exclusive and confidential use of our clients, and maynot be reproduced in whole or part, normay any reference be made to the rmrk, the results, or the company in any advertising, news n:/ease, or otherpublic announcemenw ts ithout obtaining ourphor written authorization.
SM-2540G
SM-264OG
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
601oD
6010D
6010D
6010D
SM-NI-NH3C
CALCULATION
4500NO3F-2011
Pauric McGroary
Agronomist
Page 4 of 7

rceporr rvumner: 19-107-0206
Account Number: 46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : Durham Brown
7621 Whitepine Road, Richmond, VA 23237
Main 804.743.9401 0 Fax [phone]
www°waypo inta n a lytica I, com
Lab Number: 65936 REPORT OFANALYS/S Date Sampled: 4/16/2019 09:00:00
Sample Id Durham Brown
Date Received: 04/17/2019 00:00
:
Data Rnnnrfori, ndfgrion4o
��� o.vv KKM 04l24l201913:18 6010D
Chromium 20A 12.5 KKM 04/241201913:18 6010D
Nickel <12.5 12.5 KKM 04/241201914:24 6010D
Lead <15.0 15.0 KKM 04/241201913:18 6010D
Arsenic <25.0 25.0 KKM 04/241201913:18 6010D
Mercury 0.0714 0,0144 US 04/23/201912:49 SW-7471B
Selenium <25.0 25.0 KKM 04/24/201913:18 6010D
pH * 4.3 JSL 04/23/2019 07:50 9045D
Molybdenum
<12.5 12.5 KKM 04l24/201913:18 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time
Our reprodcnd letters are for (he exclusive and confiden(ial use ofour clients, and maynot be reproduced in �°rho/e or paH, nonnay any reference be made
to the r,ork, the results, or (he companyin any advedisiny, news re/ease, or otherpublic announcernenfs vrithout obtaining curprior evri(ten authorization,
Pauric McGroary
Agronomist
Page 5 of 7

7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 ° Fax [phone]
w ,waypointanalyticaIsom
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-107-0206
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes 0 No
Number of coolers received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Not Required
Chain of Custody (COC) present? Yes 0 No
COC agrees with sample label(s)? Yes 0 No
COC properly completed Yes 0 No
Samples in proper containers? Yes 0 No
Sample containers intact? Yes 0 No
Sufficient sample volume for indicated test(s)? Yes 0 No
All samples received within holding time? Yes 0 No
Cooler temperature in compliance? Yes 0 No
Cooler/Samples arrived at the laboratory on ice. Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No 40 N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No40 N/A
F- High concentration container (48 hr) F- Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F' Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Brandi Watson Date &Time: 04/17l2019 14:06:34
Page 6 of 7

SAMPLING LOG #
SYNAGRO RI
1 (aaw
A @ L CUSTOMER SAMPLING SAMPLE
LAB # SAMPLE I,D, LOCATION ' TYP.E
0'ry'1141 &, in( a1M,p TAILE2 5L/Gm,n
Relinquished by Sampler: Date Time
INU gilt./,, lug
Relinquished by:
Relinquished by:
SrrL;IAL INSTRUCTIONS:
�X '6� For (V 9 purposes.
monitorin
csra
SAMPLE
(� Wa SL9 SL2 NH4•N NO3-N Organic Cd CP NI
pd2li�f� N
ABN OF CusT®®y
IIIIIII(0CeIIIIIILLC/,hll lillllllllllllllllllllllll 7201 •®���®�®LYS°8
SYnauro Central LLC/Durham
Durham eram 14:05:44
d sampling procedures
ectlon of these samples.
Ay 6��
o.�mr�trt
# OF SAMPLING METHOD METHOD
CONTAINERS DATE TIME PRESERVED SHIPPED
RDDIeVed by: REMARKS:
Rec ed by:
1 �r)ohe ICU (1 �'b :
PO#:
ANALYSIS REQUEST
Pb qs Fig Se H CaCO3 Volatllo
P e uiv. _Solids MO CI NOZ•N�
Bertunl l� P� per' P� p� 6� 1� I P� ap�
SLR; Total Solids (Moisture), Total KJeldahl Nitrogen, Phosphorus, and Potassium SL2; Bastc Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-04-WPC-NC DURHAM, NC BROWN WTP CAKE 4/16/2019 511/2019-7/3112019 3,5186
Na mg/I = (Na mg/kg x % Solids) + 100 = (1250 x 19.7000) + 100 = 246.25
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1250 x 19.7000) + 100 = 246.25
Mg mg/I = (mg mg/kg x % Solids) + 100 = (378 x 19.7000) + 100 = 74.466
Na meq = Na mg/I + Molec.Wgt.Na = 246.25 + 23 = 10.7065
Ca meq = Ca mg/I + Molec. Wgt.Ca = 246.25 + 20 = 12.3125
Mg meq = Mg mg/I + Molec.Wgt.Mg = 74.466 + 12 = 6.2055
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)j = 10.7055 + SgrRoot(0.5(12.3125+6.2055)j = 3.51857
Page 1 Printed: 1/30/2020
17:01

762i Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica Isom
8/14/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-207-0007
Project Description: Durham Brown
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, of laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page
1
of 7

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointa nalytical,com
Client: Synagro Central LLC/ Durham CASE NARRATIVE
Project: Durham Brown
Lab Report Number: 19-207-0007
Date: 8/13/2019
Metals Analysis Method 6010D
Sample 67552 (Durham Brown)
Analyte: Selenium
QC Batch No: L447907/L447869
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page
2
of
7

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointa nalytical-com
Sample Summary Table
Report Number:
19-207-0007
Client
Project Description:
Durham Brown
Lab No
Client Sample ID
Matrix
67552
Durham Brown
Solids
67552
Durham Brown
Solids
67552
Durham Brown
Solids
67552
Durham Brown
Solids
67552
Durham Brown
Solids
67552
Durham Brown
Solids
67552
Durham Brown
Solids
67552
Durham Brown
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: ;Y'1354
Date Collected
07/24/2019 10:30
07/24/2019 10:30
07/24/2019 10:30
07/24/2019 10:30
07/24/2019 10:30
07/24/2019 10:30
07/24/2019 10:30
07/24/2019 10:30
Page 3 of 7
Date Received
Method
lab ID
OS/05/2019
08/05/2019
SM-4500-NH3C
W7N
08/05/2019
9045D
WTN
08/05/2019
4500NO3F-2011
WTN
08/05/2019
6010D
WTN
OS/05/2019
SW-7471B
WTN
08/05/2019
SM-4500-NH3C-TKN
WTN
OS/05/2019
SM-254OG
WTN

Z
Y
N
U
C7
U
=
O
p
Z
N
O
O
O
O
O
O
O
O
O
O
O
LL
N
N
Z
O
M
O
O
O
O
O
O
O
O
O
O
O
O
D
O
00
O
(fl
(O
CO
O
In
(p
O
Cfl
CO
O
O
U
Z
UJ
O
J
O
m
m
o
m
ro
o
m
m
m
�n
o
o
m
m
o
0
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
O
O
rn
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O
m
m
m
m
m
CD
m
m
lcl
O
a

V V V
Account
Number:
46451
Send To: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Project : Durham Brown
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www.wayp oin to n a lytica I, coin
Lab Number: 67552
REPORT OFANALYSIS Date Sampled: 7/24/2019 10:30:00
Sample Id Durham Brown
Data Received: 08/05/2019 00:00
:
Date Reported: 08/14/2019
Cadmium 2.49 1.00 BKN 08/01/201912:48 6010D
Chromium 29.4 2,50 BKN 08/011201912:48 6010D
Nickel 48.0 2.50 BKN 08/01/201912:48 6010D
Lead 6,02 3.00 BKN 08101/201912:48 6010D
Arsenic 8.78 5,00 BKN 08/01/201912:48 6010D
Mercury 0.0606 0,0141 TJS 08/06/201914:14 SW-7471B
Selenium
<25.0 25.0 BKN 08/06/201915:25 6010D
pH * 4,8 JSL 08/12/2019 07:57 9045D
Molybdenum 3.12 2,50 BKN 08/01/201912:48 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reportssnd letters are for the exclusive and conliden(ial use of our clients, and may not be reproduced in whole orpart, normay any reference be made
(o the vrodc, the results, or the company in any advertising, news release, orotherpublic announcements rn(hout obtaining ourphor written authorization.
Pauric McGroary
Agronomist
Page 5 of 7

s
7621 Whitepme Road, Richmond, VA 23237
Waypoint Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypo inta n alytical.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-207-0007
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes 0 No
Number of coolers received
Custody seals intact on shipping container/cooler? 0 Yes 0 No 40 Not Required
Custody seals intact on sample bottles? 0 Yes 0 No Is Not Required
Chain of Custody (COC) present? Yes 0 No
COC agrees with sample label(s)? Yes 0 No
COC properly completed Yes 0 No
Samples in proper containers? ® Yes 0 No
Sample containers intact? ® Yes 0 No
Sufficient sample volume for indicated test(s)? ® Yes 0 No
All samples received within holding time? Yes 0 No
Cooler temperature in compliance? Yes 0 No
Cooler/Samples arrived at the laboratory on ice. Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No N/A
Water - VOA vials free of headspace 0 Yes 0 No N/A
Trip Blanks received with VOAs 0 Yes 0 No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A
High concentration container (48 hr) Low concentration Encore samplers (48 hr)
F- High concentration pre -weighed (methanol -14 d) 7- Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments:
Signature: Mary Amend Date &Time: 08/OS/2019 12:44:40
Page
6
0£
7

SAMPLING LOG) N
PROJECT MANAGER: �yu�`,NQ " 1cU1ND j
Phone: I & 6a7
10.207-0007
IIIIIIIIIIIIIIIIIIIIIIPill 111111111111111[till 111111111111111111077-26.2019 BS, IND, CHAIN OF CUSTODY
Snraaro Central LLCI Durham 10,51..09 RECORD & ANALYSIS
m,.a., wanwu RECORD
I attest that the proper field sampling procedures
were used during the collection of these samples.
A & L CUSTOMER SAMPLING BAMPLE # OF SAMPLING METHOD METHOD
LAB N SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
Nhll(1M t NuE0. Sl j 7/Zq,I0 �
10: 30 CE CooLER
� l t
Ralinqulehed by Sampler: Date Time Recleved by; REMARKS;
RYAN COPEI.A00 IZ0,00
by;
Relinquished by: pate jlme Recleved bye _
For ``1_ Uimonitoringpurposes,
POtf:
MEMO
0
0
ME
SLi: Total Solids (Moisture), Total Klsidahl Nitrogen, Phosphorus, and Potaeslum
312: Bas10 Tort SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zino

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-04-WPC-NC DURHAM, NC BROWN WTP CAKE 7/24/2019 81112019-9130/2019 1,1892
Na mg/I = (Na mg/kg x % Solids) + 100 = (345 x 18.2000) + 100 = 62.79
Ca mg/I = (Ca mg/kg x % Solids) . 100 = (790 x 18.2000) + 100 = 143.78
Mg mg/I = (mg mg/kg x % Solids) + 100 = (221 x 18.2000) + 100 = 40.222
Na meq = Na mg/I + Molec. Wgt. Na = 62.79 + 23 = 2.73
Ca meq = Ca mg/I + Molec.Wgt.Ca = 143.78 +20 = 7.189
Mg meq = Mg mg/I + Molec. Wgt.Mg = 40.222 + 12 = 3.35183
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)j = 2.73 + SgrRoot[0.5(7.189+3.35183)] = 1.18916
Page 1 Printed: 1/30/2020
17:01

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointa nalytical.com
11/18/2019
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-312-0010
Project Description: Durham Brown
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
f applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www,waypointa nalytical.com
Sample Summary Table
Report Number:
Client Project Description:
19-312-0010
Durham Brown
Lab No
Client Sample ID
Matrix
69538
Durham
Brown N&M
Solids
69538
Durham
Brown N&M
Solids
69538
Durham
Brown N&M
Solids
69538
Durham
Brown N&M
Solids
69538
Durham
Brown N&M
Solids
69538
Durham
Brown N&M
Solids
69538
Durham
Brown N&M
Solids
69538
Durham
Brown N&M
Solids
WiN: Waypoint Analytical - TN, Memphis, TN
Date Collected
11/06/2019 08:15
11/06/2019 08:15
11/06/2019 08:15
11/06/2019 08:15
11/06/2019 08:15
11/06/2019 08:15
11/06/2019 08:15
11/06/2019 08:15
Page 2 of 7
Date Received
Method
Lab ID
11/08/2019
11/08/2019
SM-4500-NH3C
WTN
11/08/2019
9045D
WTN
11/08/2019
4500NO3F-2011
WTN
11/08/2019
6010D
WTN
11/08/2019
SW-7471B
WTN
11/08/2019
SM-4500-NH3C-TKN
WTN
11/08/2019
SM-254OG
WFN

46451
Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
MOcksvllle , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointa na lytica Isom
Ryan Copeland
Project Durham Brown
Information :
Report Date : 11/18/2019
Received : 11/08/2019
Submitted By : Ryan Copeland
Report Number : 19-312-0010 REPORT OFANAL YSIS Pauric McGroary
Agronomist
Lab No : 69538 Matrix: Solids
Sample ID: Durham Brown N&M Sampled: 11/6/2019 8:15
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen - 1000 mg/Kg - dry 599 1 11/15/19 15:00 JPJ SM-4500-1\11-13C
Nitrate+Nitrite-N <28.6 mg/Kg - dry 28.6 1 11/12/19 14:16 ZBD 4500NO3F-2011
Organic N 15900 mg/Kg - dry 1500 1 11/15/19 12:00 CALCULATION
pH 6.2 s.u. 1 11/12/19 05:08 JSL 9045D
Total Solids 16.7 % 0.010 1 11/11/19 16:35 ADM SW2540G
Total Kjeldahl Nitrogen 16900 mg/Kg - dry 1500 1 11/15/19 12:00 JPJ iM-4500-1\11-13C-TKP
Phosphorus 1010 mg/Kg - dry 29.9 1 11/13/19 02:49 KKM 6010D
Aluminum 4130 mg/Kg - dry 29.9 1 11/13/19 02:49 KKM 6010D
Arsenic 5.91 mg/Kg - dry 2,99 1 11/13/19 02:49 KKM 6010D
Calcium 1240 mg/Kg - dry I50 1 11/13/19 02:49 KKM 6010D
Cadmium 6.53 mg/Kg - dry 0.599 1 11/13/19 02:49 KKM 6010D
Chromium 7,90 mg/Kg - dry 1.50 1 11/13/19 02:49 KKM 6010D
Copper 647 mg/Kg - dry 1.50 1 11/13/19 02:49 KKM 6010D
Iron 380000 mg/Kg - dry 299 10 11/13/19 17:20 KKM 6010D
Lead 8,68 mg/Kg - dry 1.80 1 11/13/19 02:49 KKM 6010D
Magnesium 278 mg/Kg - dry 29,9 1 11/13/19 02:49 KKM 6010D
Manganese 11900 mg/Kg - dry 15.0 5 11/13/19 17:05 KKM 6010D
Mercury <0.0940 mg/Kg - dry 0.0940 1 11/12/19 14:33 TJS SW-74716
Molybdenum 2,76 mg/Kg - dry 1.50 1 11/13/19 02:49 KKM 6010D
Nickel 87,4 mg/Kg - dry 1,50 1 11/13/19 02:49 KKM 6010D
Potassium 217 mg/Kg - dry 29.9 1 11/13/19 02:49 KKM 6010D
Selenium <29,9 mg/Kg - dry 29.9 10 11/13/19 17:20 KKM 6010D
Sodium 397 mg/Kg - dry 150 1 11/13/19 02:49 KKM 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page
3
of
7

Waypo
7621 Whitepine Road, Richmond, VA 23237
O
Main 804-743-9401 *Fax [phone]
46451 ANALYTICAL www.waypointanalytical.com
Synagro Central LLC/ Durham Ryan Copeland
Mary Brewer Project Durham Brown
284 Boger Road Report Date: 11/SS/2019
9 Information : Mocksville NC 27028 Received : 11/08/2019
,
T6wfta X "40wy/'
Submitted By : Ryan Copeland o0
Report Number :19-312-0010 REPORTOFANALYSLS Pauric MCGroary
Agronomist
Lab No: 69538
Matrix: Solids
Sample ID :Durham Brown N8cM Sampled: 11/6/2019 8:15
Test Results Units MQL OF Date I Time By Analytical
Analyzed Method
Zinc 122 mg/Kg -dry
Sulfur 3700 mg/Kg - dry
Moisture 83.3
qualifiers/ g gnalyte detected in blank
Definitions
Page 4 0£ 7
7.49
1
11/13/19
02:49
KKM
6010D
29.9
1
11/13/19
02:49
KKM
6010D
0.010 1 11/11/19 16:35 ADM SM-2540G
H Beyond holding time

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ww W.waypointa nalytica l.com
: �ynagro central LLC/ Durt
Project: Durham Brown
Lab Report Number: 19-312-0010
Date: 11/15/2019
Metals Analysis Method 601013
Sample 69538 (Durham Brown N&M)
Analyte: Selenium
QC Batch No: L463984IL463658
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 5 0£ 7

Wi•< sufl=
ANALYTICAL.
concentration container (48 hr)
High concentration pre -weighed (methanol .14 d
Special precautions or instructions included?
Comments:
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]"6
www.waypointa nalytical.com
Cooler Receipt Form
Customer Number: 46451
Customer Name: Synagro Central LLC/ Durham
Report Number: 19-312-0010
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Other:
0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
Number of coolers received
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of Custody (COC) present?
COC agrees with sample label(s)?
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
Process had begun.
Water - Sample containers properly preserved
Water - VOA vials free of headspace
Trip Blanks received with VOAs
Soil VOA method 5035 —compliance criteria met
High
U Yes No
N/A
O
— Low concentration EnCore samplers (48 hr)
1 Low conc pre -weighed vials (Sod Bis -14 d)
0 Yes No
0 Yes
Yes
(�
3M
a
Yes
0
0 Yes
Yes
0
No
0
No
0
No
0
No
0
No
(�
No
0
No
0
No
0
No
0
No
0
No
Signature: IBrandi Watson Date &Time: 111/08/2019 13:11:38
Page 6 of 7

SAMPLING LOG # n A & L
IIIIIIIIIIIIIIIIIIIII�III�IIII�IIIIII�IIII II�IIIII�I tlIII IIII i A201196 ®F CUS
T®DY
Ll 7621 N SWanroCentritLLClDutham 13:1103 D & ANALYSIS
Durham Brain
® Rlchmo IJEC ORD
CUSTOMER MAGRO -- - 89�%F4a
�4 41\j D l attest that the proper field sampling procedures
PROJECTm�MANAGER:—1, were used during the
collection of these samples,
Phone:
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OP SAMPLING METHOD METHOD
LA13 # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
Ova" f 13wnl STeMs& IFAItfiL SL(/CbmP 11(6'iq IC6 CooLa
Relinquished by Sampler: {� Date Time Recleved by: REMARKS: ,
KlAN C.oP&AtJO 11/7/1y I1:ou
Rellnquished by: t �) Phi Time As v y:
Relinquished by: PIRO Time Recle ed by:
SPECIAL INSTRUCTIONS:
h
For_ ' monitoring purposes. PO##: (W l
6Li: Tote) Solids (Moisture), Total KJeidahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Tast SL1 plus Sulfur, Calolum, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zino
Page 7 of 7

3odium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange
Ratio
2012-04WPC-NC DURHAM, NC BROWN WTP CAKE 11/6/2019 10/1/2019A2/31/2019 1.0809
Na mg/I = (Na mg/kg x % Solids) + 100 = (397 x 16.7000) + 100 = 66.299
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1240 x 16,7000) + 100 = 207.08
Mg mg/I = (mg mg/kg x % Solids) + 100 = (278 x 16.7000) + 100 = 46.426
Na meq = Na mg/I + Molec. Wgt.Na = 66.299 + 23 = 2.88257
Ca meq = Ca mg/I + Molec. Wgt.Ca = 207.08 + 20 = 10.354
Mg meq = Mg mg/I + Molec.Wgt.Mg = 46.426 + 12 = 3.86883
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.88257 + SgrRoot[0.5(10.354+3.86883)] = 1.08094
Paqe 1 Printed; 1/30/2020
17:02

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: VANCE
OWNER: ETHEL PRITCHE'1T PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 97.79
SITE #: NC AM 00021 FIELD# : AM 00021 0001 OPERATOR: ROGER TATE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 27.90 ACRES PERMITTED: 27.90
Page: 1
Lhne Applied "•
Date Lbs'Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry,
'Pons
Per
Residual
Site
Cond.
Dry, Wet,
inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
all-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
4124/19
384.00 (CY)
1 I3.763
16.90
1.959
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,800.p
77160.00 p
222.00 p
14330
CORN
4/25/19
303.00 (CY)
10,860
16.90
1.54G
DSDAND
MOIST
0-<1/2"
SUR
0.5
0.20
59,800.p
7,160.00 p
222.00 p
14330
CORN
Apr-19
687.00 (CS')
1 24.623
Total Gallons/Ac:
Total Wet Tons/Ac:
r ulni cuvi� iuyA�. L4.OL
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
100
0.036
0.007
0.205
2.650
0.125
0.002
0.055
0.163
0.035
17.314
227.82
Cumulative lbs/acre
0.148
0.040
1.143
10.254
0.559
0.025
0.249
0.585
0.133
85.763
DSDANDC =DURHAM, NC S. DURHAM W1V'fP ANAEROB. DIGESTED CAKE
X W 1sty 2a?2L40
(SIGNATURE OF LAND APPLIEK) DATE
"I certify, under penally of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified peronncl properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false infomration, including the possibility of fines and imprisonment for knowing violations.'
N/A —Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg " Volatilization Rate: Surface 0.5, InjectionAncorpomtion 1.0
° Application Method: SUR- Surface, INJ - Injection, SURIN - Incorporation •"' See Site pH & Lime Application Records Section of Report for Fields where Linre is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: HELENA
OWNER: GEORGE AMICK
PERMIT #:
W00003504
ANNUAL DRY TONS APPLIED: 53.84
SITE #: NC AM 00023 FIELD# :AM 00023 0001
OPERATOR:
ROGER TAPE
CATION EXCHANGE CAPACITY (NON-503):
RFSIDI TAT. SOt IRCE(SI' See list at bottom of tenor(
ACRES UTILIZED: 12.70 ACRES PERMHTED: 12.70
Page: 1
Lime Applied xxx
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Pons (WT) (specify)
�
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Net,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp"')
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
a
Rate"
Rate
Nitrite
5/1/19
184.00 (CY)
14.488
16.70
2.038
DNDAND
DRY
0-Q/2"
SUR
0.570.2055�800.p
8,080.00 p
5.00 p
13589
SOYBEANS
May-19
184.00 (CIq
14,488
S/1/19
200.00 (CY)
15.748
16.60
2.202
DSDAND
DRY
0-<I/2"
SUR
0.5p
9,640.00 p
36.10 p
14111
SOYBEANS
Alay-19
200.00 (C71
15.748
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 30.24
As
Cd
Cr
Cu
Pb
11g
Imo
Ni
Se
Zn
P
PAN
TOTALS:
121
Annual lbs(acre
0,042
0.008
0.275
2.712
0.130
0.003
0.059
0.198
0.042
17.110
256.33
Cumulative Ibs/acre
0.185
0.057
1.362
12.499
0,763
0.030
0.304
0.782
0.147
103.117
DNDANDC =DURHAM, NC N. DURHAM NW'fP ANAEROB. DIGESTED CAKE
DSUANDC =DURHAM, NC S. DURHAM W\lr['P ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPI,IER) DA"fE
"I certify, nnder penalty of law, that this document was prepared nnder my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infomration submitted. I am aware that there are significant penalties for submi(ting false infommtion, including the possibility offines and imprisonment for knowing violations."
N/A —Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mgd<g .x Volatilization Rate: Surface 0.5, Injectionfincorporation LO
e Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation 'x` See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY
NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: HELENA
OWNER:
GEORGE AMICK
PERMIT#:
\V00003504
ANNUAL DRYTONS APPLIED: 14.42
SITE M:
NC AM 00023 FIELD# : AM 00023 0002
OPERATOR:
ROGER TATE
CATION EXCHANGE CAPACITY (NON-503):
RE.SIDI JAL
SOURCE(S): See list at bottom of report
ACRES UTILIZED: 17.80 ACRES PERMITTED: 17.80
Page: 1
Lime Applied sss
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry,
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
till-
nation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
pnN
(ppnr)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
=
Rat0*
Rate
Nitrite
S/1/19
28.00 (CY)
1.573
16.70
0.221
DNDAND
DRY
0-<1/2"
SUIT
0.5
0.20
553800.p
$080.00 p
5.00 p
13589
SOYBEANS
May-19
28.00 (C51
1.573
5/l/19
75.00 (CY)
4.213
16.60
0.589
DSDAND
DRY
0-<I/2n
SUR
0.5
0.20
59,400.p
9,640.00 p
36.10 p
1 14808
ISOYBEANS
Play-19
75,00 (CY)
4.213
Total Gallons/Ac:
'1'ntnl Wet Tons/Ac:
'Total cubic Yas/ne: s.79
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
23
Annual lbs/acre
0.008
0.002
0.053
O.S16
0.024
<.001
0.012
0.038
0.008
3.321
47.78
Cumulative lbs/acre
0.042
0.008
0.294
2.448
0.174
0.010
0.063
0.152
0.041
24.608
DNDANDC=DURHAM, NC N. DUKHAM W\Vl'P ANAEROB. DIGESTEll CAKE
DSDANDC=llURHAM, NC S. DURI-UVVI \V\VTP ANAEROB. DIGESTED CAKE
�oPelflN�
(SIGNATURE OP LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assort that qualified personnel properly gathered and
evaluated the infomation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg " Volatilization Rate: Surface 0.5, hljectimdlncogtoration LO
3 Application Method: SUR - Surface, FNJ - Injection, SURIN - Incorporation "' See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: APPLNG
OWNER: GEORGE AMICK PERMIT #: NV00003504 ANNUAL DRY TONS APPLIED: 57.78
SITE #: NC AM 00023 FIELD# : AM 00023 0003 OPERATOR: ROGER TATE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 14.40 ACRES PERMITTED: 14.40
Page : 1
Lime Applied •"'
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (wT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(PAN
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rates*
Rate
Nitrite
5/7/19
212.00 (CY)
14.722
16.70
1071
ONDAND
DRY
0-<1/2"
SUR
0.5
0.20
55,800.p
8,080.00 p
5.00 p
13589
SOYBEANS
May-19
212.00 (CYO
14,722
5/7119
200.00 (CY)
13.889
16.60
1.942
DSDANll
DRY
0-<112"
SUR
0.5
0.20
59,400.p
9,640.00 p
36.10 p
14808
SOYBEANS
May-19
200.00 (C]1
13.889
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 28.61
As
Cd
Cr
Cu
Pb
118
Mo
Ni
Se
zo
P
PAN
TOTALS:
114
Annual Ibs/acre
0.040
0.008
0.259
2.569
0.123
0.003
0.056
0.187
0.040
16.151
243.62
Cumulative lbs/acre
0.197
0.060
1.388
13,536
0,878
0.042
0.369
0.907
0.214
111.321
DNDANDC =DURHAM, NC N. DURHAM MVTP ANAEIZOB. DIGESTED CAKE
DSDANUC =DURHAM, NC S. DURHAM W WI'P ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared ender my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibilityof fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg4:g '• Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - incorporation °# See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
PACILITYNAME: DURHAM, NC
PREDOMINANT SOIL SERIES: APPLING
OWNER: GEORGEAMICK
PERMIT#:
W00003504
ANNUAL DRY TONS APPLIED: 67.82
SITE #: NC AM 00023 FIELD# : AM 00023 0004
OPERATOR:
ROGER TATE
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTIL17ED: 14.50 ACRES PERMfITED: 14.50
Page:
Lane Applied •••
Date Lbs'Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vain-
Miner -
or Wet Tons (VT) (specify)
%
Tons
Cond.
Precip.
cation
lili-
all-
Ammonia
Nitrate
AN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
'ration
zation
TKN
Nitrogen
and
(ppinn)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
5/8/19
184.00 (CY)
12.690
16.70
1.785
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
551800.p
8,080.00 p
5.00 p
13589
SOYBEANS
Nlay-19
184.00 (CY)
12,690
5/8119
300.00 (CY)
20.690
16.60
2.893
DSDAND
DRY
0-<I/2n
SUR
0.5
0.20
59,400.p
9,640.00 p
36.10 p
14808
SOYBEANS
Nlay-19
300,00 (CY)
20,690
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 33.35
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
134
Annual lbs/acre
0.047
0.009
0.305
2.985
0.14I
0.004
0.066
0.218
0.047
19.016
279.47
Cumulative Ibs/acre
0.184
0.068
1.393
13.782
0.835
0.033
0.362
0.879
0.155
109.059
DNDANDC = DURIIAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
DSDANDC = DURHAM, NC S. DURHAM WW'1'P ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"1 certify, under penally of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are sip.Jrificant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg °° Volatilization Rate: Surface 0.5. bnjectionulneorpomtion 1.0
• Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Linre Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: HELENA
OWNER: GEORGE AMICK
PERMIT#:
W00003504
ANNUAL DRY TONS APPLIED: 129.01
SITE #: NC AM 00023 FIELD# : AM 00023 0005
OPERATOR:
ROGER TATE
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 30.60 ACRES PERMITTED: 30.60
Page: 1
Lime Applied "•
Date I.bs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
s
RateSY
Rate
Nitrite
5/3/19
59.50 (W)
1.944
19.70
0.383
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
SOYBEANS
\lay-19
59.50 (R')
1.944
5/2/19
100.00 (CY)
3.268
16.70
0.460
DSDAND
DRY
(-<I/2"
SUR
0.5
0.20
55,800.p
8,080.00 p
5.00 p
13589
SOYBEANS
5/3/19
212.00 (CY)
6.928
16.70
0.974
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
55,800. p
8,080.00 p
5.00 p
13589
SOYBEANS
Dlay-19
312,00 (CY)
10,196
5/2119
225.00 (CY)
7.353
16.60
1.028
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400. p
9,640.00 p
36.10 p
14808
SOYBEANS
5/3/19
300.00 (CY)
9.804
I6.60
L371
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
5%400. p
9,640.00 p
36.10 p
14808
SOYBEANS
Dlay-19
525,00 (CS')
17.157
Total Gallons/Ac:
Total Wet Tons/Ac: 1.94
TOTALS:
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs(acrc
0.057
0.012
0.266
2.520
0.127
0.003
0.064
0.188
0.057
15.639
229.64
112
Cumulative Ibs/acre
0.205
0.070
1.370
11.770
0.822
0.030
0.317
0.837
0.177
90.981
DBWPC =DURHAM, NC BROWN 1V'1'P CAKE
DNDANDC =DURHAM, NC N. DURHAM WM'P ANAEROB. DIGESTED CAKE
DSDANDC=DURIIAM, NC S. DURHAM WWTP ANAF.ROB. DIGESTED CAKE
X
�PCtRNO
.Z/�z J2a
(SIGNATURE OF LAND APPLIEK) DATE
"I certify, under penalty oflaw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infomation submitted. I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required
%=percent p=ppm
onng/kg
Volatilization Rate: Surface 0.5,
Injection/lncorporotion 1.0
* Application Method: SUR -Surface, INl -Injection,
SURIN -Incorporation
�*x
See Si[e pli &Lime Application Records
Section of Report for Fields
where Lime is to be appliCO in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: APPLING
OWNER: GEORGE AMICK
PERMIT#:
W00003504
ANNUAL DRY TONS APPLIED: 10.49
SITE #: NC AM 00023 FIELD# : AM 00023 0006
OPERATOR:
ROGER TATE
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 3.70 ACRES PERMITTED: 3.70
Page: 1
Lime Applied ss.
hte LbyAc
allons (G) or Cubic Yards (CY)
or Wet Tons ONT) (specify)
Dry
'Foils
Site
Inches
Appli-
Vola-
Miner -
DATE
%
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
or
MONTH
Total
I Per Acre
Solids
Per
Residual
D
Dry, wet,
Past 24
Method
nation
zation
TKN
Nitro en
g
and
(ppnm)
Crop
Acre
Source
Moist
flours
Rate'
Rote
Nitrite
75.00 (CY)
20.270
MM
28
DRY
0-<t/
S5P2/19 OR
0.5
0.20
59,400.p
%640.00 p
36.10 p
14808
SOYBEANS
Map-19
75,00 (C)LL
20.270
TotalWet Tons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
84
0.028
0.006
0.190
1.791
0.081
0.002
0.041
0.133
0.028
11.846
161.54
Cumulative Ibsracre
0.082
0.016
0.533
4.968
0.359
0.021
0,137
0.336
0.093
49.072
777777
DSDANDC =DURHAM, NC S. DURIIAM W WTP ArNAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIF,R) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I nor aware that there are significant penalties for submitting false fi foradion, including the possibility of fines and imprisonment for knowing violations."
NIA =Not Applicable NR=Not Reported or Not Required %—percent p=ppm or ng/kg a. Volatilization Rate: Surface 0.5. htiection/Incorporation 1.0
' Application Method: SUR- Surface, INJ - injection, SURIN - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: APPLhNG
OWNER: MASON BARNWELL PERMIT 9: NV00003504 ANNUAL DRY TONS APPLIED: 15.09
SITE #: NC AM 00024 FIELD# : AM 00024 0002 OPERATOR: ROGER TATE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 6.90 ACRES PERMITTED: 6.90
Page : I
Line Applied
Date Lba/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (1VT) (specify)
%
Tons
Cond.
Precip.
cation
till-
all-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, \Vet,
Pact 24
Method
nation
nation
TKN
Nitrogen
and
(ppnr)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Role"
Rate
Nitrite
4/25/19
106.00 (CY)
15.362
16.90
2,187
DSDAND
MOIST
0-4/2"
SUR
0.5
0.20
59,800.p
7,160.00 p
222.00 p
14330
CORN
Apr-19
106,00 (C)LIJ
15,362
I
t oral uauonslAc:
Total Wet Tons/Ac:
V V .., JV
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Ann u t lbsfacre
63
0.023
0.004
0.128
1.653
0.078
0.001
0.034
0.101
0.022
10.802
142.13
Cumulative Ibs/acre
0.174
0.056
1.321
12.131
0.752
0.033
0.332
0.705
0.165
107.175
ell
DSDANDC =DURHAM, NC S. DURHAM R�VTP ANAEKOB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE 111
"I certify, under penally of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false infonnation, including the possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or nigd:g Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surfacc, INJ - Injection, SURIN - Incoryoratimr +++ See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILI'fYNAME: DURHAM,NC
PREDOMINANT SOIL SERIES: APPLING
OWNER: MASON BARNWELL
PERMIT#:
W00003504
ANNUAL DRY TONS APPLIED: 7.12
SITE #: NC AM 00024 FIELD# : AM 00024 0003
OPERATOR:
ROGER TAXL
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 9.00 ACRES PERMITTED: 9.00
Page: I
Lime Applied ***
llate Lbs/Ac
allons (G) or Cubic Yards (CY)
Dn,
Site
Incites
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
nation
zation
TKN
Nitrogen
and
(plan)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
4/25/19
50.00 (CY)
5.556
16.90
0.791
DSDAND
MOIST
0-<1/2"
SUR
0.5
0.20
59,800.p
7,160.00 p
222.00 p
14330
CORN
Apr-19
50.00 (C)LIJ
5,556
Total Gallons/Ac:
Total Wet Pons/Ac:
1 Onl l,llplC TaSiHC: J.Jb
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibsracre
0.008
0.002
0,046
0.598
0.028
<.001
0.012
0.037
0.008
3.906
51.40
23
Cumulative lbs/acre
0.117
0.045
0.851
8.761
0.562
0.024
0.241
0,504
0.073
77,794
DSDANDC=DURHAM, NC S. llURIIAM W WTP ANAF,ROB. DIGESTED CAKE
(SIGNATURE OF LAND e1PPLIER) DATE
"I certify, under penalty of ]aw, that this document was prepared under my direction or supervision in accordance with a system designed to assure thfll qualified peronnel properly gathered and
evaluated the infan nation submitted. I ant aware that there are significant penalties for submitting false infomnation, including the possibility offines and imprisonment for knowing violations."
N/A —Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg ° Volatilization Rate: Surface 0.5, InjectionAncorporation LO
* Application Melbod: SUR - Surface, RE - Injection, SURIN - Incorporation :as See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURHMVI, NC
OWNER: HENRY THORPE
SITE #: NC OR 00005 FIELD# : OR 00005 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: VANCE
PERMIT#: W00003504 ANNUAL DRY IONS APPLIED: 135.84
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 44.70 ACRES PERMY17FED: 44.70
Page
Lime Applied '••
Dale Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATEor
Per
Residual
Dry, Wet,
Past 24
Method
zation
ration
TKN
Nitrogen
and
(pp"')
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
2/10119
574.00 (CY)
12.841
18.50
2.001
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
54,200.p
6,680.00 p
86A0 p
12930
FESCUE PASTURE
Feb-19
574.00 (Cl�
12,941
3113/19
67.25 (W)
1.504
16.80
0.253
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
5,230.Op
45.70 p
11.40 p
1071
FESCUE PASTURE
Mar-19
67.25 RV)
1.504
3/13/19
200M (CY)
4.474
17.10
0.644
DNDAND
DRY
0-<I/2"
S[TR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
Mar-19
200.00 (CY)
4.474
4/4/19
37.48 (W)
0.838
16.80
0.141
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
5,230.Op
45.70 p
11.40 p
1071
FESCUE PASTURE
Apr-19
37A8 (W)
0.838

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITYNAME: DURIIAM,NC
PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRY THORPE
PERMIT #:
NV00003504
ANNUAL DRY TONS APPLIED: 135.84
SITE #: NC GR 00005 FIELD# : OR 00005 0001
OPERATOR:
HENRY THORPE
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 44.70 ACRES PERMITTED: 44.70
Page : 2
Lime Applied '••
Date I.bs/Ac
Total
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola.
Miner -
or Wet Tons (WT) (specify)
�
Tons
Cold.
Precip.
cation
tih-
all-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
Gallons/Ac:
Total Wet Tons/Ac: 234
Total Cubic Yds/Ac: 17.32
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
70
Annual Ibs/acre
0.028
0.006
0.030
2.079
0.112
0.002
0.041
0.114
0.024
10.588
163.94
Cumulative lbs/acre
0.236
0.106
2.040
18.342
1.576
0.034
0.540
1.148
0.415
99.292
!
DNDANDC=llURHAM, NC N. DUItIIArM W WTP ANAEROB. DIGESTED CAKIi
DB WPC = DURHAM, NC BROWN WTP CAKB
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared ender my direction or supervision in accordance with a system designed to assure that qualified peronnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for }mowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=pptm or nrg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IM - Injection, SURIN - Incorporation *** See Site pl l & Lime Application Records Section of Report for Fields where Linre is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRY THORPE
PERMIT N:
W00003504
ANNUAL DRY TONS APPLIED: 124.80
SITE N: NC GR 00005 FIELDS : OR 00005 0002
OPERATOR:
HENRY THORPE
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 37.90 ACRES PERMITTED: 37.90
Page: 1
Lima Applied •••
Date Lbs/Ac
allons (0) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (NT) (specify)
Tons
Cond.
Prccip.
cation
lili-
all-
Ammonia
Nitrite
PAN
DATE or
pef
Residual
Dry, Net,
Past 24
Method
zalion
zaiion
TKN
Nitrogen
and
(ppnt)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
4/25/19
44.16 (N)
1.165
16.80
0.196
DBNPC
DRY
0-<I/2"
SUR
0.5
0.20
5,230.Op
45.70 p
11.40 p
1071
FESCUEPASTURE
Apr-19
44.16 (W)
1,165
4111/19
131.00 (CY)
3.456
17.10
0.498
DNDAND
MOIST
0-<I/2"
SUR
0.5
0.20
5G,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
4/18/19
300.00 (CY)
7.916
17.10
1.140
DNDAND
DRY
0-<1/2"
SUR
0.5
1120
56,700.p
8,130.00 p
4.92 p
13794
FESCUE PASTURE
4/23/19
384,00 (CY)
10.132
17.10
L459
DNDAND
DRY
0-<l/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
Apr-19
815.00 (C10
214504
Total Gallons/Ac:
Total Net Tons/Ao: 1.17
Total Cubic Yds/Ac: 21.50
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
86
Annual lbs/acre
0.035
0.006
0.146
2.232
0.124
0.002
0.043
0.133
0.032
12.523
205.24
Cumulative lbs/acre
0.231
0.112
2.801
18.257
1.934
0.034
0.693
1A82
0.482
107.912
DBNPC = DURIIAM, NC BRONN N1'P CAKE
DNDANDC = DURIIAM, NC N. DURHAM NWTP ANAEKOB. DIGESTED CAKE
X I�-i L.Lit�1� Z YZ 2O
(SIGNATURE OF LAND APPLIER) DATE
"1 certify, under penalty of Inv, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am alvare that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reportedor Not Required %=percent p=plain or mg/4 " Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
+ Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation s•a See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILI'TYNAME: DURHAM,NC
OWNER: HENRY THORPE
SITE #: NC GR 00005 FIELD# : GR 00005 0003
RESIDUAL, SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOX, SERIES: VANCE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 313.90
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 92.50 ACRES PERMITTED: 92.50
Page:
Lime Applied
Dale Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Inches
Appli-
Vola-
Miner -
or Wet Tons (N'1') (specify)
%
Tons
Precip.
cation
till-
allrTKW
Ammonia
Nitrate
PAN
DATE or
per
Residual
Past 24
Method
zalion
zabon
Nitrogen
and
(ppnr)
Crop
MONTH
Total
per Acre
Solids
Acre
Source
EDRY
Hours
Rate**
Rate
Nitrite
2/9/19
518.00 (CY)
5.600
Him
0.873
DNDAND0-<I/2"
SUR
0.5
0.20
54,200. p
6,680.00 p
86.I0 p
12930
FESCUE PASTURE
Feb-19
518.00 (CIT)
5.600
3118/19
22.34 (W)
0.242
16.80
0.0411
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
5,230.0p
45.70 p
IlAO p
1071
FESCUE PASTURE
3/19/19
17.63 (W)
0.191
16.80
0.0321
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
5,230.Op
45.70 p
11.40 p
1071
FESCUE PASTURE
3/21/19
22.34 (W)
0.242
16.80
0.0411
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
5,230.0p
45.70 p
11.40 p
1071
FESCUE PASTURE
3/22/19
44.10 (W)
0.477
16.80
0.080
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
5,230.0p
45.70 p
11.40 p
1071
FESCUE PASTURE
Mar-19
1 106.41 (W)
1,152
3/18/19
325.00 (CY)
3.514
17.10
0.506
DNDAND
MOIST
0.<1/2"
SUR
0.5
0.20
56,700. p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
3/19/19
153.00 (CY)
1.654
17.10
0.238
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
Mar-19
478.00 (CY)
5.168
411/19
256.00 (CY)
2.768
17.10
0.399
DNDAND
MOIST
0-<I/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
4/4/19
390.00 (CY)
4.216
ITIO
0.607
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,700.p
8,1MW p
4.92 p
13784
FESCUE PASTURE
418119
265.00 (CY)
2.865
17.10
0,413
DNDAND
MOIST
0-<I12"
SUR
0.5
020
56,700. p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
4/11/19
106,00 (CY)
1.146
17.10
0.165
DNDAND
MOIST
0-<I/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
Apr-19
1,01

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACR.ITYNAME: DURHAM,NC
PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRYTHORPE
PERMIT N:
W00003504
ANNUAL DRY TONS APPLIED: 313.90
SITE 0: NC OR 00005 FIELD# : OR 00005 0003
OPERATOR:
HENRY THORPE
CATION EXCIIANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 92.50 ACRES PERMITTED: 92.50
Page: 2
Lime Applied "*
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (R�'f) (specify)
Tons
Cond.
Precip.
cation
lili-
ali.
Ammonia
Nitrate
PAN
DATEor
per
Residual
Dry, Wet,
Past 24
Method
nation
nation
TKN
Nitrogen
and
(pPnm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
Total Gallons/Ac:
Total Wet'fons/Ac: 1.15
Total Cubic Yds/Ac: 2176
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
87
Annual Ibs/acre
0.033
0.007
0.109
2.357
0.127
0.002
0.046
0.134
0.031
12,887
207.01
Cumulative lbs/acre
0.225
0.087
1.580
14.905
1.052
0.029
0.337
1.063
0.233
98.121
DNDANDC = DURI-IAM, NC N. DURHAM W 1VTP ANAEROB. DIGESTED CAKE
DBWPC =DURHAM, NC BROWN 1VTP CAKE
X V�11'' LLA0/ t�fl2L%U
(SIGNATURE OF LAND APPLIER) DATE
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I ran aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for }mowing violations."
N/A=Not Applicable MR —Not Reported or Not Required %=percent P=ppm orungdcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: ENON
OWNER: HENRY THORPE
PERMIT#:
W00003504
ANNUAL DRY TONS APPLIED: 116.08
SITE #: NC OR 00005 FIELD# : OR 00005 0004
OPERATOR:
HENRY THORPE
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 47.60 ACRES PERMITTED: 47.60
Page: 1
Lime Applied "'
Date LbJAc
allons (0) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
all
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, 1Vet,
Past 24
Method
nation
zr[ior
TKN
Nitrogen
and
(pp"')
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
3/14/19
600.00 ICY)
12.605
17.10
1.815
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE,PASTURE
illar-19
600.00 (CI')
12,605
4/1/19
206.00 (CY)
4.328I
17.10
0.623
DNDAND
MOIST
0-<I/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
Apr-19
1 206.00 (CI')
4.328
1
Total Gallons/Ac:
Total Wet Tons/Ac:
-tool (;tlbiC YtlYAC:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual Ibs/acre
0.025
0.005
0.115
1.722
0.093
0.002
0.033
0.100
0.024
9.852 161.44
67
Cumulative Ibslacre
0.205
0.077
1.451
13.616
0.866
0.027
0.316
0.967
0.215
101.930
1.
DNDANDC =DURHAM, NC N. DURHAM WWTP ANAEKOB. DIGESTED CAKE
X ��i� CoPEW�O 2 /Z Zu
- (SIGNATURE, OF LAND APPLIEK) DATE
"[ certify, under penalty of law, that this document was prepared under my direction or supervisior in accordance with a system designed to assure that qualified peronnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg "" Volatilization Rate: Surface 0.5, Injectiorulneorporation 1.0
" Application Method: SUR - Surface, TNJ - Injection, SURIN - Incorporation $°" See Site pH R Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: HENRY THORPE
SITE #: NC OR 00005 FIELD# : GR 00005 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM71
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: NV00003504 ANNUAL DRY TONS APPLIED: 156.05
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 26.10 ACRES PERMITTED: 26.10
Page: I
LimeApplied
Date LbsrAc
T
allons (0) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (\VT)(specify)
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
Total
DATE or
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
3/19119
21.01 OV)
0.805
16.80
0.135
DBWPC
DRY
0-<I/2n
SUR
0.5
0.20
5,230.Op
45.70 p
11.40 p
1071
FESCUEPASTURE
Mar-19
21.01 (\i')
0.805
3/19/I9
434,00 (CY)
16.628
17.10
2.395
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
FESCUE, PASTURE
3/20/19
625.00 (CY)
1 23.946
17.10
3.449
DNDAND
MOIST
0-<1/2"
SUR
0.5
0.20
56,700. p
8,130.00 p
4.92 p
13114
FESCUE PASTURE
Mar-19
11059,00 (C\')
40,574
otal Gallons/Ac:
Total Wet Tons/Ac: 0.80
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Me
Ni
Se
Zn
P
PAN
Annual lbs/acre
0.062
0.012
0.275
4.157
0.227
0.004
0.081
0.243
0.059
23.616
387.00
161
Cumulative Ibs/acre
0.315
0.103
L880
21.389
1.283
0,032
OA32
1.382
0.310
126.832
DBWPC=DURHAM, NC BKOWN \VTP CAKE
DNllANDC=DURHAM, NC N. DURHAM MVTP ANAEROB. DIGESTF,D CAKE
(SIGNATURE OF LAND APPLIF,R) DATE
"I certify, under penalty of law, tbat this document was prepared ender my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %—percent p=ppm or mg/1:g ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR-Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Linre Application Records Section of Report for Fields where Linre is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NArME: DURHAM, NC
PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRYTHORPE
PERMIT#:
W00003504
ANNUAL DRY TONS APPLIED: 43.21
SITE #: NC OR 00005 FIELD# : GR 00005 0006
OPERATOR:
HENRY THORPE
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 9.50 ACRES PERMITTED: 9.50
Page : 1
Lime Applied **3
Uate L65/Ac
10181
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
'Pons
Cond.
Precip.
cation
till-
ali-
Antonia
Nitrate
PAN
DATE or
"Total
I
Solids
Per
Residual
Dry, Wet,
Past 24
Method
Zillion
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
3129/19
300.00 (CY)
31.579
17,10
4.548
DNDAND
MOIST
0-<1/2"
SUR
0.5
0.20
5G,700.p
8,130.00 p
4.92 p
13784
FESCUE PASTURE
Mar-19
300,00 (Cl'j
31,579
-
Uzumtstnc:
Total Wet Tons/Ac:
TOTALS:
As
Cd
Cr
Ca
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
125
0.046
0.009
0.214
3,211
0,174
0.003
0.062
0.186
0,045
18.374
301,08
Cumulative Ibs/acre
0.220
0.072
1.225
13.503
0.916
0.022
0.296
0.946
0.215
90.818
DNllANDC =DURHAM, NC N. DURHAM W WTP ANAEROB. DIGESTF,D CAKE
s_(CI�IArJD 2 IZ ZD
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of lmv, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infomration submitted I am mvare that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=plan or nig/I:g "' Volatilization Rate: Surface 0.5, Injection/lncorporalion 1.0
$ Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation +$ See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: RONALD WALKER
SITE #: NC OR 00006 FIELD# : OR 00006 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDO,MNANT SOIL SERIES: HERNDON
PERIM #: W00003504 ANNUAL DRY TONS APPLIED: 146.02
OPERATOR: DAVID WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 57.60 ACRES PERMITTED: 57.60
Page : I
Lime Applied «««
Date i,bs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (\VT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(I)pm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate#°
Rate
Nitrite
9/23/19
65.97 (W)
1.145
1820
0.208
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE PASTURE
Sep-19
65.97
9/23/19
225.00 (CY)
3,906
15.60L0.604DNDAND
ND
DRY
0-<I/2n
SUR
0.5
0.20
57,400.p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
9/24/19
265.00 (CY)
4.601
15.G0ND
DRY
0-<l/2"
SUR
0.5
0.20
57,400.p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
9/27/19
265,00 (CY)
4.601
15.60ND
DRY
0-<1/2"
SUR
0.5
0.20
575400. p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
9/30/19
265.00 (CY)
4.601
15.60
DRY
0-<1/2"
SUR
0.5
0,20
57,400.p
II,000.00 p
4.55 p
14785
FESCUE PASTURE
Sep-19
14020,00 (Clj
17.709
1 Otal (iallOnS/AC:
Total Wet Tons/Ac: 1.15
'V",. �,•V.V ....,..... y'.'1
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Ln
P
PAN
Annual lbs/ncre
0.027
0.006
0.152
2.3I1
0.083
0.003
0.040
0,119
0.034
13.941
110.65
70
Cumulative lbs/acre
0.298
0,164
1.925
19.094
1,202
0.036
0,483
1.217
0.318
100.775
DB\VPC=DURHAM, NC BROIVN WTP CAKE
DNDANDC =DURHAM, NC N. DURHAM Rr\VTP ANAEROB. DIGESTED CAKE
X �I"IrJ Wtf�Iv`/ IZ/�
(SIGNATURE OF LAND APPLISR) DATE
"I certify, under penalty oflaw, that this document was prepared undenny direction or supervision in accordance with a system desig.red to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A -Not Applicable NR=Not Reported or Not Required %=percent p=Finn or mg/kg *' Volatilization Rate: Surface 0.5, hljectionancorporalion 1.0
* Application Method: SUR - Surface, INJ - Injection, SURN - Incorporation sas See Site pH & Linre Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILTTYNAME: DURIIAM,NC
OWNER: RONALD WALKER
SITE #: NC OR 00006 FIELD# : OR 00006 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT'#; NV00003504 ANNUAL DRY TONS APPLIED: 59.77
OPERATOR: DAVID \VALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.80 ACRES PERMITTED: 8.80
Page: I
Lime Applied ***
Date Lbs/Ac
T
allons (G) or Cubic Yards (CY)
Dry,
Site
tactics
Appli-
Vola-
Miner -
or Wet Tons ff'f) (specify)
%
'rolls
Cond.
Precip.
cation
till-
Ili-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wel,
Past 24
Method
zalion
nation
TKIN
Nitrogen
and
(ppnn)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
9/24/19
39.65 (W)
4.506
18.20
0.820
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE HAY
9/26/19
20.93 OV)
2.378
18.20
0.433
DB\VPC
DRY
0-<I/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE HAY
Sep-19
60.58
9/25/19
212.00 (CY)
240911
15.60
3.161
DNDAND
DRY
0.<I/2"
SUR
0.5
0.20
57,400.p
1I5000.00 p
4.55 p
14785
FESCUE HAY
9/26/19
159.00 (CY)
18.068
15.60
2.374
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
57,400. p
11,000.00 p
4.55 p
14785
FESCUE HAY
Sep-19
371.00 (C]')
42,159
otal Gallons/Ac:
'Total Wet Tons/Ac: 6,88
Total Cubic YdslAc: 42,16
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
0.077
0.017
0.406
7.439
0.204
0.007
0.101
0.355
0.119
33.289
264.78
170
Cumulative lbs/acre
0.471
0.149
2.527
27.462
1.777
0,062
0.613
1.908
0.492
123.612
DBNPC = DUI2IIAM, NC BROWN \VTP CAKE
DNDANDC=DURHAM, NC N. DURHAM W\VTP ANAEKOB. DIGESTED CAKE
X (Zy�,J �oc�tio 2��2 Zu
(SIGNATURE OF LAND AYYLIER) DATE
"I certify, corder penalty oflmv, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR=Not Reportedor Not Required %=percent p=Plan or mg/kg •* Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURTN - Incorporation $#° See Site pH Pa Linre Application Records Section of Report for Fields where Lime is to be applied in 2020

FACR,ITY NAME: DURHAM, NC
OWNER: SUSAN WILLIAMS
SITE #: NC OR 00008 FIELD# : OR 00008 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: APPLING
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 226.39
OPERATOR: TOMMY POPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILT7ED: 48.50 ACRES PERMITTED: 48.50
Page: 1
Lime Applied
Date Lbs'Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (RrT) (specify)
/0
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
Total
I
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
TIGN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
Rater`
Rate
Nitrite
5/23/19
20.26 (W)
0.418
19.70
0.082
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000. p
508.00 p
5.00 p
2557
FESCUE HAY
5/24/19
59.86 (W)
1.2341
19.70
0.243
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
5/28/19
69.80 (W)
1.4391
19.70
0.284
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
Nay-19
149,92 (W)
3,091
5/23/I9
156.00 (CY)
3.216
16.60
0.450
DSDAND
DRY
0-<1rz°
SUR
0.5
0.20
595400.p
9,640.00 p
36.10 p
14808
FESCUE HAY
5/24/19
131.00 (CY)
2.701
16.60
0.378
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400. p
%640.00 p
36.10 P
14808
FESCUE HAY
5/28/19
500.00 (CY)
10.309
16.60
1.441
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400. p
9,640.00 p
36.10 p
14808
FESCUE HAY
5/29/19
515.00 (CY)
10.619
16.60
1.485
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
5%400. p
9,640.00 p
36.10 p
14808
FESCUE HAY
5/30119
106.00 (CY)
2.186
16.60
0.306
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
59,400. p
95640.00 p
36.10 p
14808
FESCUE HAY
Nay-19
L408.00 (C)L�
29.031

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURIIAM, NC PREDOMINANT SOIL SERIES: APPLING
OWNER: SUSAN WILLIAMS PERMIT #: AV00003504 ANNUAL DRY TONS APPLIED: 226.39
SITE #: NC OR 00008 FIELD# : OR 00008 0001 OPERATOR: TOMMY POPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 48.50 ACRES PERMITTED: 48.50
Page: 2
Lime Applied 44•
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or wet Tons (\VT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, \Vet,
Past 24
Method
nation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
+
Rate**
Rate
Nitrite
'Total Gallons/Ac:
Total Wet Tons/Ac: 309
V`u, �"V,y •V y^y
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS
Annual lbs/acre
123
0.071
0.014
0.297
2.684
0.134
0.003
0.074
0.205
0.071
17.042
232,69
Cumulative Ibsracre
0.329
0.112
2.302
23.250
1.196
0,038
0.520
1.338
0.365
136.336
;
DB\VPC = DURHAM, NC BRO\VN \VTP CAKE
DSDANDC=llURIIAM, NC S. DURHAM \V\\'TP ANAEROB. DIGESI'Ell CAKE
(SIGNATURE OF LAND APPLIER) DATE
"1 certify, under penalty oflaw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reportedor Not Required %=percent p=plan or mg/I:g as Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, IN7 - Injection, SURIN - Incorporation ' See Site pH & Lime Application Records Section of Report for Fields where Linie is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: APPLING
OWNER: SUSAN WILLIAMS PERMIT 9: W00003504 ANNUAL DRY TONS APPLIED: 40.95
SITE U: NC OR 00008 FIELD# : OR 00008 0002 OPERATOR: TOMMY POPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 38.10 ACRES PERMITTED: 38.10
Page: 1
Lune Applied "'
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
till-
ali-
rLamount
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
nation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Raley
Rate
Nitrite
5/22/19
39.66 (W)
1.041
19.70
0.205
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000. p
508.00 p
5.00 p
2557
FESCUE HAY
\lay-19
39,66 ()l1
1,041
5/22/19
131.00 (CY)
3.438
16.60
0.481
1 DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400. p
9,640.00 p
36.10 p
14808
FESCUE HAY
5/23/19
106.00 (CY)
2.782
16.60
0.389
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
59,400.p
9,640.00 p
36.10 p
14808
FESCUE HAY
Alay-19
237.00 (CI)
6,220
'I'oml Gallons/Ac:
Total Wet Tons/Ac: 1404
1mne,uure ruvtve. b.LL
As
Cd
Cr
Cu
Pb
Hg
Imo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
0.019
0.004
0.067
0.590
0.031
<.001
0.018
0.046
0.019
3.661
50.02
27
Cumulative Ibs/acre
0.256
0.100
2.356
20.512
1.040
0.039
0.477
1.260
0.297
132.794
llBWPC =DURHAM, NC BROWN NTP CAKE
DSDANDC =DURHAM, NC S. DURHAM W1V'TP ANAEROB. DIGESTED CAKE
X (11 �YLVINO _- Z�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I out aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not
Reported
or Not Required
%=percent p=ppm or
mg/kg
"#
Volatilization bate: Surface 0.5,
Injection/Incorporation 1.0
% Application Method: SUR -Surface,
INJ - hnjeclion,
SURIN - Incorporation
#k'
See Site pH & Linre Application Records
Section of Report for Fields
where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURI Vl5 NC PREDOMINANT SOIL SERIFS: CECIL
OWNER: WILLIAM DORSETI' PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 80.06
SITE #: NC OR 00012 FIELD# : OR 00012 0001 OPERATOR: WILLIAM DORSETT CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 16.90 ACRES PERMITTED: 16.90
Page : I
Lime Applied
llate Lb Ae
allons(G) or Cubic Yards(CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
fvmnonia
Nitrate
PAN
DATE or
per
Residual
llry, \Vet,
Past 24
Method
zation
zalion
TKN
Nitrogen
and
(ppm)
Crop
MONTH
total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
5/21/19
21.05 (W)
1.246
19.70
0.245
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
May-19
21,05 (\i')
1.246
5121/19
387.00 (CY)
22.899
16.60
3.202
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400.p
9,640.00 p
36.10 p
14808
FESCUE HAY
5/22/I9
156.00 (CY)
9.231
16.60
1.291
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400.p
9,640.00 p
36.10 p
14101
FESCUE, HAY
May-19
543.00 (CY)
32,130
Total Gallons/Ac:
Total Wet Tons/Ac: 1,25
Total Cubic Yds/Ac: 32.13
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
134
Annual Ibs/acre
0.057
0.011
0.312
2.887
0.136
0.004
0.071
0.216
0.057
18.808
256.59
Cumulative lbs/acre
0.227
0.079
1.624
14.148
0.969
0.030
0.355
1.053
0.225
99904
llB\VPC= DURI-IAM, NC BRO\VN \VTP CAKE
DSDANDC=DURHrVM, NC S. DURHAM \VWTP ANAEROB. DIGES'IEU CAKE
2�ULII v6t un 2�j2 f 60
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this docmnent was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infomration submitted. I am aware that there are sipirificant penalties for submitting false infomration, including the possibility of fines and imprisonment for }mowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/I:g ** Volatilization Rate: Surface 0.5. hnjectionRncorporralion 1.0
* Application Method: SUR - Surface, ]NJ - Injection, SURIN - Incorporation "'* See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACtL1TY NAME: DURIIAM, NC
OWNER: WILLIAM DORSETT
SITE #: NC OR 00012 FIELD# : OR 00012 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PRF.DOMNANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL. DRY TONS APPLIED: 24.77
OPERATOR: WILLIAM DORSETT CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 18.70 ACRES PERMITTED: 18.70
Page: 1
Lime Applied *Ps
Dale Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Itches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATEor
Per
Residual
Dry, Wet,
Past
Method
nation
nation
TKN
Nitrogen
and
(ppnr)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
11/22/19
84.74 (W)
4.532
16.70
0.757
DBWPC
DRY
"0-<I2"
SUR
0.5
0.20
163900.p
1,000.00 p
28.6O-T-[--5TOT
FESCUEHAY
NoiA9
84.74 (<{�
1216/19
40.34 (RD
2,157
16.70
0.360
DBWPC
DRY
"0-<l2"
SUR
0.5
0.20
16,900.p
13000.00 p
28.60 p
3709
FESCUE HAY
12/11/19
23.22 (W)
1.242
16.70
0.207
DBWPC
DRY
"0-<12"
SUR
0.5
0.20
16,900.p
1,000-00 p
28.60 p
3709
FESCUE HAY
Dec-19
63.56 (R')
3,399
total uauonslnc:
Total Wet Tons/Ac: 7,93
V VV"
As
Cd
Cr
Cm
Pb
Hg
Me
Ni
Se
Zn
P
PAN
TOTALS:
Aunal lbs/acre
10
0.016
0.017
0.021
1.714
0,023
<.001
0.007
0.232
0.079
0.323
2.68
Cumulative Ibs/acre
0.114
0.055
0.501
9.271
0.547
0.009
0.137
0.606
0.173
34.893
DBWPC = DURHAM, NC BROWN WTP CAKIi
X �R�LL r Latin 2 (2 Zo
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR- Surface, NJ -Injection, SURIN - Incorporation%$ See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILIT'YNAME: DURHAM,NC
OWNER: WILLIAM DORSETT
SITE #: NC OR 00012 FIELD# : OR 00012 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVR,LE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 166.32
OPERATOR: WILLIAM DORSETT CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 33.30 ACRES PERMITTED: 33.30
Page:
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
/
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
7atimi
ration
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
5115119
40.47 (W)
1.215
19.70
0.239
DBWPC
DRY
0-<M"
SUR
0.5
0.20
1$000.p
508.00 p
5.00 P
2557
SOYBEANS
5116/19
53.84 (NV)
1.617
19.70
0.319
DBWPC
DRY
0-<I/2"
SUR.
0.5
0.20
12,000. p
508.00 p
5.00 p
2557
SOYBEANS
5/17/19
63.94 (W)
1920
19.70
0.378
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 P
2557
SOYBEANS
5/20/19
20,18 (W)
0.606
19.70
0.119
DBWPC
DRY
0-<t/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 P
2557
SOYBEANS
May-19
178,43 (W)
5.358
5/16/19
156.00 (CY)
1L685
16.70
0.659
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
55,800.p
8,080.00 P
5.00 p
13589
SOYBEANS
5/17/19
212.00 (CY)
6.3661
16.70
0.895
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
55,800. p
8,080.00 p
5.00 p
13589
SOYBEANS
Play-19
368,00 (CI1
1L051
5/20119
440.00 (CY)
13.213
16.60
1.8471
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400. p
9,640.00 p
36.10 p
14808
SOYBEANS
5121/19
128.00 (CY)
3.344
16.60
0.537
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,400.p
9,640.00 p
36.10 p
14808
SOYBEANS
Nay-19
568.00 (CY)
17.057

FACILITY NAME: DURHAM, NC
OWNER: WILLIAMDORSETI'
SITE #: NC OR 00012 FIELD# : OR 00012 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: NV00003504 ANNUAL, DRY TONS APPLIED: 166.32
OPERATOR: WILLIAM DORSETT CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 33.30 ACRES PERMITTED: 33.30
Page : 2
Lime Applied «««
Date I.bsrAc
allons(G) or Cubic Yards(CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (VT) (specify)
%
'Pons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Net,
Past 24
Method
zation
nation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
total Uauonsrnc:
Total Wet Tons/Ac: 5,36
.......,,. Loll
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALSV,'••yVV.V
Annual lbs/acre
its
0.092
0.018
0.299
2,720
0.151
0,003
0.082
0.210
0.092
16.131
238.04
Cunudative Ibs/acrc
0-176
0.052
1.056
7.798
0.537
0.016
0.204
0.597
0.176
59.412
DBWPC = DURHAM, NC BRONN \V'1P CAKE
DNDANDC =DURHAM, NC N. DU12f--LAM N1VTP ANAEROB. DIGESTED CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAF.ROB. DIGESTED CAKE
X �2Y� WeEI�N� Z�IZ/Zu
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. lain aware that there are significant penalties for submitting false infomration, including the possibility of fines and imprisonment for }mowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or nrg/kg s Volatilization Rate: Surface 0.5, InjectionAncoryoration 1.0
° Application Method: SUR - Surface, INJ - Injection, SURW - hmorpomtion See Site pH & Linre Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: APPIdNG
OWNER: JAMES WILSON PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 14.23
SITE #: NC OR 00014 FIELD# : OR 00014 0001 OPERATOR: JAMES WILSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 4.40 ACRES PERMITTED: 4.40
Page: I
Lime Applied +++
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
D
Dry
Site
Inches
Vol--
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
cation
tili-
all-
Ammonia
Nitrate
AN
Total
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
nation
nation
'1'KN
Nitrogen
and
(ppmt)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
4/29/19
1001.00 (CY)
22.727
16.90
3.235
DSDANU
DRY
0-4/2"
SUR
0.5
0.20
59,800.p
7,160.00 p
222.00 p
14330
CORN
Apr-19
100.00 (C])
22.727
t oral uauonsrac:
Total Wet Pons/Ac:
44 J
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
0.034
0.006
0.189
2.446
0.115
0.002
0.050
0.150
0.032
15.981
210.27
93
Cumulative lbs(acrc
0.067
0.013
0.339
4.369
0.209
0.002
0.097
0.264
0.063
28.061
DSDANDC = DURHAM, NC S. llURHAM W WTP ANAEROB. DIGESTED CAKE
X ''I� WVEW9
(SIGNATURE OF LAND APPLIER) DATE
"I certify, trader penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including lire possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %—percent p=ppnt or ntg/kg ** Volatilization Rate: Surface 0.5, InjectimnAncorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH R Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: HELENA
OWNER: JAMES WILSON
PERMIT#:
NV00003504
ANNUAL DRY TONS APPLIED: 21.35
SITE #: NC OR 00014 FIELD# : OR 00014 0002
OPERATOR:
JAMES R4LSON
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 10.90 ACRES PERMITTED: 10.90
Page: 1
Lime Applied '"'
Date LbsmAc
allons(G) or Cubic Yards CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATEor
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp"')
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
4/29/19
150,00 (CY)
13.761
16.90
1.959
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
59,800.p
73160.00 p
222.00 p
14330
CORN
Apr-19
150.00 (CY)
13,761
Total Gallons
Total Wet Tons/Ac:
.oInt�uwoo .�y�.o. re.ro
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
56
0.020
0.004
0.114
1.481
0.070
<,001
0.031
0.091
0.020
9.676
127.32
Cumulative Ibsracre
0.045
0.009
0.226
2.909
0.140
0.001
0.065
0.176
0.042
18.649
'
DSDANllC =DURHAM, NC S. DURHAM V✓NTP ANAEROB. DIGESTED CARE
X � -V ulfrn 212 Zv
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I our aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.n
N/A=Not Applicable NR=Not Reported orNot Required %=percent p=plan or mg/kg s`• Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection,SURIN - Incorporation "'* See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITYNAME: DURHAM,NC
OWNER: JAMES \VILSON
SITE #: NC OR 00014 FIELD# : OR 00014 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HELENA
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 21.35
OPERATOR: JAMES WILSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: IOAO ACRES PERM Y ED: 10.40
Page: 1
Line Applied *••
Date Lbs/Ae
Iota[
allons (G) or Cubic Yards (CY)
Dry
Site
tactics
Appli-
Vola-
Miner -
or Net Tons (\VT) (specify)
%Per
Tons
Cond.
Precip.
cation
tif-
ali-
Ammonia
Nitrate
PAN
Total
I
DATE or
Solids
Residual
Dry, Net,
Past 24
Method
'ration
zation
TKN
Nitrogen
and
(Ran)
Crop
MONTH
Per Acre
Acre
Source
Moist
hours
Rate**
Rate
Nitrite
4/29/19
150.00 (CY)
1 14.423
16.90
2.053
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
59,800. p
77160.00 p
222.00 p
14330
CORN
Apr-19
150,00 (CY)
14,423
Uallons/Ac:
Total Net Tons/Ac:
VJ y~`
TOTALS:
As
Cd
Cr
Cn
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
59
0.021
0.004
0.120
1.552
0.073
<,001
0.032
0.095
0.021
10.142
133.44
j Cumulative Ibs/acre
0.049
0.009
0.241
3.098
0.149
0.001
0.070
0.187
0.045
19.853
I
i
DSDArNDC = DURHAM, NC S. DURHAM WW1'P ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLiER) DATE
"I certify, under penalty of Irv, that this document was prepared ender my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %—percent P III plan or nmg/Kg °# Volatilization Rate: Surface 0.5, hijectionQncorportion LO
` Application Method: SUR - Surface, INJ -Injection, SURW - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

Riff!"tIffs MR
FACILITY NAME: DURHAM,NC PREDOMINANT SOIL SERIES: HELENA
OWNER: JAMES WILSON PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 47.42
SITE #: NC OR 00014 FIELD# : OR 00014 0005 OPERATOR: JAMES WILSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 14.40 ACRES PERMITTED: 14.40
Page : I
Lune Applied "'
Date LWAc
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons OVT) (specify)
%
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp"')
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
hours
Rote"
Rate
Nitrite
4/30/19
181,00 (CY)
12.569
17.10
1.810
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,700.p
8,130.00 p
4.92 p
13784
CORN
Apr-19
181,00 (Clj
12,569
I
4/30/19
150.00 (CY)
10.417
16.90
1,483
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
59,800.p
7,160.00 p
222.00 p
14330
CORN
Apr-19
150.00 (Cl')
10.417
Total Gallons/Ac:
Total Wet Tons/Ac:
�uVy �^y uLL ry
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbsracre
92
0.034
0.007
0.172
2.399
0.122
0.002
0,048
0.143
0.033
14.638
216.21
Cumulative ]bs/aere
0.036
0.007
0.183
2.546
0.129
0.002
0.052
0.152
0.035
15,561
DNDANDC =DURHAM, NC N. DURHAM IV WTP ANAEROB. DIGESTED CAKE
DSDANDC =DURHAM, NC S. llURHAM MPfP ANAEROB. DIGESTED CAKE
Vi �A boNv �l�z/ZV
(SIGNATURE OF LAND APPI,IER) DATE
"I certify, under penalty of Imv, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I our aware that there are significant penalties for submitting false information, including the possibility of Ones and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=plan or mg/kg Volatilization Rate: Surface 0.5, InjectioMncorpomtion 1.0
Application Method: SUR - Surface, INJ - Injection, SUR1N - Incorporation *a' See Site pH & Linre Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITYNAME: DURHAM,NC
OWNER: RICIIARDVANHOOKPOA
SITE #: NC OR 00015 FIELD# : OR 00015 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: NV00003504 ANNUAL. DRY TONS APPLIED: 143.89
OPERATOR: RICHARD VANHOOK CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 32.20 ACRES PERMITTED: 32 20
Page: 1
Lime Applied ***
Date LbyAc
or
MONTH
allons (G) or Cubic
or Wet Tons (WT)
Yards (CY)
(specify)
%
Solids
D 6'
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
cation
catiAppon
Method
Vol--
till-
zalion
Miller-
ali-
zation
T'KN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
5/9/19
37.54 (W)
1.166
19.70
0.230
DBWPC
DRY
0-<1l2"
SUR
0.5
0.20
I2P000.p
508.00 p
5.00 p
2557
FESCUE HAY
May-19
37454 (W)
1.166
5/9/19
212.00 (CY)
6.584
16-70
0.926
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
55,800-p
8,080.00 p
5.00 p
13119
FESCUE HAY
5/10/19
162.00 (CY)
5.031
16.70
0.708
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
551800. p
83080.00
5.00
13589
p
p
FESCUE HAY
May-19
374,00 ICY
I1.615
519/19
300.00 (CY)
9.317
16.60
1.303
DNDAND
DRY
/2"
SUR
0.5
0.20
59,400. p
91640.00 p
36.10
14808
FESCUE HAY
5l10/19
300.00 (CY)
9.317
16.60
1.303
DSllAND
DRY
70<11n2l'
SUR
0.5
0.20
59,400. p
93640.00 p
p
36.10 p
14308
FESCUE HAY
May-19
600.00 (CY
18.634
Total Wet Tons/Ac: 1,17
Tmal (`chin vavre ^-
V
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
0.054
0.011
0.286
2.750
0.135
0.003
0,065
0.203
0.054
17.257
253.88
123
Cumulative lbs/acre
0.195
0.069
1.172
12.017
0.720
0.016
0.295
0.827
0.208
72.271
DBWPC=DURHAM, NC BROIVN WTP CAKE
DNDANDC = pURIIAM, NC N. DURHAM W\V'I'P ANAEROB. DIGESTED CAKE
DSDANDC=DURHAM, NC S. DURI IAM WWTP ANAEROB. DIGESTED CAKE
s ���i IAPEIJtN� Z IZ/Zo
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of Imv, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I anm aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
NIA -Not Applicable NR=Not Reported or Not Required %=percent p=pion or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

PACILITYNAME: DURHAM,NC
OWNER: RICHARD VANHOOK POA
SITE #: NC OR 00015 PIELD# : OR 00015 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 22,36
OPERATOR: RICHARD VANHOOK CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.50 ACRES PF.RMTrTFD- R 50
Page: I
Lune Applied +�•
Date LbsIAc
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (\VT) (specify)
%
Solids
Dry
D
Tons
Per
Acre
Residual
Source
Site
Cond.
Dry, wet,
Moist
Inches
Precip.
Past 24
Hours
cation
cation
Method
Vol--
till-
nation
Rate"
Miner.
11i-
nation
Rate
TKN
Ammonia
Nitrogen
Nitrate
and
Nitrite
PAN
(ppm)
Crop
Total
I Per Acre
5/15/19
\lay-19
159.00 (CY)
159.00 (C]1
18.706
18.706
16.70
2.631
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
555800. p
8,080.00 p
5.00 p
13589
FESCUE IIAY
Total
Gallnns/Am
Total wet'fons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbstacre
0.026
0.005
0.164
1.705
0.086
0.002
0.035
0.122
0.026
10.208
168.91
72
Cumulative ]bs/acre
0.153
0.064
1.157
10.706
0.550
0.013
0.261
0.748
0,170
63.018
llNDANllC = DUAHAM, NC N. DURHAM \VwTP ANAEROB. DIGESTED CAKE
0 1v
(SIGNATURE OF LAND APPLiER) DATE
"I certify, under penalty of law, tlmt this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for (mowing violations."
N/A =Not Applicable NR=Not Reportedor Not Required %=percent p=ppm or mg/kg Volatilization Rate: Surface 0.5. InjectionAncorporation 1.0
° Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: DURHAM, NC PREDOMINANT SOIL SERIES: APPLING
OWNER: FAIRCREST LAND&CATTLE PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 99.61
SITE #: NC OR 00070 FIELD# : OR 00070 0001 OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE($): See list at bottom of report ACRES UTILIZED: 26.60 ACRES PERMITTED: 26.60
Page:
Lime Applied tst
Ihfe LbsrAc
DATE or
MONTH
Gallons (G) or Cubic
or Wet Tons (WT)
Yards (CY)
(specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, wet,
Inches
Precip.
Past24
A h
pp -
cation
Method
Vola-
Will
nation
Miner -
ali.
zation
TKN
Ammonia
Nitrogen
g
Nitrate
and
PAN
(PVnn)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
Ride"
Rate
Nitrite
10/3/19
39.68 (w)
1.492
16,70
0.249
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
16,900.p
1,000.00 p
28.60
10/4/19
47.96 (W)
1.803
16.70
0.301
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
16,900.p
I,000.00 p
p
28.60
F'3709WHEAT
Oct-19
87,64 OAD
3,295
pWHEAT
10/1/19
312.00 (CY)
11.729
15.60
1.541
DNDAND
DRY
0-<l/2"
SUR
0.5
0.20
503900,p
IQ400.00 p
4.88
13305
R'HEAT
Oct-19
312,00 (CY)
11,729
p
10/2/19
309.00 (CY)
11.617
16.90
1.653
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
543300.p
105000.00 p
4.49
11164
WHEAT
Oct-19
309.00 (CY)
11.617
p
.,f,f n,u,..,v/A.,.
Total Wet Ti 3.29
'rnf AI nitdp va�in�
VV
TOTALS:
As
Cd
Cr
Cit
Pb
Hg
Me
Ni
Se
Zn
P
PAN
Annual Ibs/acre
0.042
0.014
0.209
3.183
0.146
0.003
0.100
0.240
0.065
18.197
205,31
91
Cumulative Ibsiacre
0.841
0.352
13.245
55,782
7.083
0.249
3.37G
5.474
0.839
435.530
DBWPC=DURHAM, NC BROWN \VTP CAKE
DNDANDC=llURHAM, NC N. DURHAM W1VTP ANAL'ROB. DIGESTED CAKE
DSDANDC=DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X C��RIJ �OClAllp IZ Zo
(SIGNATURE OP LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. 1 on aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
N/A —Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg " Volatilization Rate: Surface 0.5, InjectioMncorporation 1.0
• Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation '* Sec Site pit & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: FAIRCREST LAND & CATTLE
SITE #: NC OR 00070 FIELD# : OR 00070 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HELENA
PERMIT#: NV00003504 ANNUAL DRY TONS APPLIED: 102.66
OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 26.90 ACRES PERMITTED: 26.90
Page: 1
Lime Applied "•
Dale Lbs�Ac
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet
or Wet Tons 0WH (spccifY)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
tactics
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(Ppm)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
e
Rate"
Rate
Nitrite
10/7/19
24.07 (W)
0.895
16.70
0.149
DBNVPC
DRY
0-<I/2n
SUR
0.5
0.20
16,900.p
1,000.00 p
28.60
3709
WHEAT
10/8119
43.45 (W)
1,615
16.70
0.270
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
167900.p
11000.00 p
p
28.61
37119
WHEAT
10/11/19
102.43 (W)
3.808
16.70
0.636
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
163900,P
1,000.00 p
p
28.60
3709
WHEAT
10/15/19
82.47 (W)
3.066
16.70
0.512
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
16,900.p
11000.00 p
p
28.60
3709
WHEAT
10/21/19
67.26 (W)
2.500
16.70
0.418
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
16,900.p
1,000.00 p
p
28.60
3709
WHEAT
p
Oct-19
319.68 (%V)
11,884
10/7/19
75.00 (CY)
2.788
15.60
0,366
DNDAN=DRYO�<1/211
UR
0.5
0.20
50,900.p
10,400.00 p
4.88
13305
WHEAT
10/15/19
300.00 (CY)
it 152
15.60
L465
DNDANUR
0.5
0.20
503900.p
10,400.00 p
p
4.88
I3305
WHEAT
p
Oct-19
375,00 (CY)
13.940

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: HELENA
OWNER: FAIRCREST LAND & CATTLE PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 102.66
SITE #: NC OR 00070 FIELD# : OR 00070 0002 OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 26.90 ACRES PERMITTED: 26.90
Page: 2
Lime Applied rrr
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
DATE
%Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
or
MONTH
Total
I Per Acre
Solids
Per
Residual
Dry, Wd,
Past 24
Method
zation
zation
TKN
Nitro en
g
and
(ppm)
Crop
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
Total Wet Tons/Ac: 11,88
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
63
0.042
0.030
0.150
4.169
0.125
0.002
0.056
0.429
0.137
11.694
109.14
Cumulative Ibs/acre
0.723
0.405
10.467
44.558
6.504
0.180
2.244
4.878
0.687
304.119
DB\VPC = DURIiAM, NC BROWN \V1'P CAKE
DNDANDC=DURHAM, NC N. DURIIAM WWTP ANAEROB. DIGESTED CAKE
XC®PcurNo ZL�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gathered and
evaluated the info niation submitted I ann nvarc that there are significant penalties for submitting false infomnation, including the possibility of fines and imprisonment for knowing violations."
NIA =Not Applicable NR=Not Reported or Not Required, %=percent p=ppm or mg/kg *• Volatilization Rate: Surface 0.5, Injection/huorporation 1.0
" Application Method: SUR - Surface, INI - Injection, SURIN - Incorporation See Site pll & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: APPI,ING
OWNER: FAIRCREST LAND R CATTLE PERMIT N: W00003504 ANNUAL DRY TONS APPLIED: 78.83
SITE 9: NC OR 00070 FIELDS : OR 00070 0003 OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 30.70 ACRES PERMITTED: 30.70
Page : I
Lime Applied
Dale LbsrAc
DATE
allons (G) or Cubic Yards (CY)
or Wet Tons OVT) (specify)
%
Dry
Tons
Pere
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Mettrod
Vola-
tili-
zalion
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
H
Total
Total
I Per Acre
Solids
Moist
Hours
Rate**
Rate
Nitrite
10/8/19
300.00 (CY)
9.772
15.60
1.284
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
501900.p
10,400.00 p
4.88 p
13305
WHEAT
10/9/19
300.00 (CY)
9.772
15.60
1.284
DNDAND
DRY
0-<1f2"
SUR
0.5
0.20
50,900.p
10,400.00 p
4.88 p
13305
WHEAT
Oct-19
600,00 (CY]l
19,544
Total GallonslAc:
Total Wet Tons/Ac:
,v«, .6yA,
Cd
Cr
Cm
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:As
Annual lbsracre
68
0.026
0.006
0.166
2.244
0.127
0.002
0.063
0.115
0.026
15.715
147.39
Cumulative lbs/acre
0.570
0.397
11.609
39.620
5.128
0.349
2.017
5.290
0.615
286.532
DNDANDC = DURHAM, NC N. DURIiAM W W'lY ANAEROB. DIGESTED CAKE
I L Zo
(SIGNATURE OF LAND APPIdF,R) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance witb a system designed to assure [bat qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not
Applicable NR=Not Reported or Not Required
%=percent p=ppm or
mg0:g
**
Volatilization Rate: Surface 0.5,
LtjectioNlncoryoration 1.0
*
Application Method: SUR -Surface, INJ -Injection,
SURIN -Incorporation
""
See Site pH &Lime Applicatior Records
Section of Report for Pields
where Linre is to be applied in 2020

ANNUAL LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM,
NC
PREDOMINANT SOIL SERIES: HELENA
OWNER: FAIRCREST
LAND & CATTLE
PERMIT #: W00003504
ANNUAL DRY TONS APPLIED: 84.65
SITE #: NC OR 00070
FIELD# : OR 00070 0004
OPERATOR: WOLFGANG LOTZ
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):
See list at bottom of report
ACRES UTILIZED: 33.00 ACRES PERMITTED: 33.00
Page:
Lime Applied +•+
Date Lbs/Ac
DATF, or
MON'1'11
Gallons (0) or Cubic Yards (CY)
or Wet Tons (1VT) (specify)
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
till-
nation
Miner -
ali-
nation
TKN
Munonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
'Total
I Per Acre
Acre
Source
Moist
Hours
Rate'
Rate
Nitrite
19
22500 (CY)
6.818
15.60
0.896
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
50,900.p
10,400.00 p
4.88 p
13111
WHEAT
Oct-19
Oet-
225,00 (CSC
6,818
10/4/19
387.00 (CY)
11.727
16.90
1.669
DSDAND
DRY
0-<1/2"
SUIi
0.5
0.20
543300.p
10,000.00 p
4.49
13864
WHEAT
p
Oct-19 1
387.00 (CY)
11.727
Total Wet Tons/AG:
TMM rush:,. VAerA,..
VJ✓
TOTALS:
As
Cd
Cr
Cu
Ph
Hg
Mir
Ni
Se
Zn
P
PAN
Amoral lbs/acre
70
0.030
0.005
0.160
1.918
0.105
0-002
0.082
0.116
0-026
14.196
168.26
Cumulative Ibslacre
0.702
0,366
12.118
46.918
4.798
0.319
1.994
5.721
0.694
394.456
DNDANDC = DURHAM, NC N. DURIiAM WWTP ANAEROB. DIGESTED G1KE
DSDANllC = DURHAM, NC S. DURHAM R�VTP ANAEROB. llIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are signifi"nt penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppnr or nrg/kg as Volatilization Rate: Surface 0.5, InjectionAncorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SUR1N - Incorporation Sec Site pH & Lime Application Records Section of Report for Fields where Limc is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: WILLIAM FREEZE, SR.
SITE N: NC OR 00076 FIELDN :OR 00076 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLF
PERMIT#: NV00003504 ANNUAL DRY TONS APPLIED: 30.70
OPERATOR: WILLIAM LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60
Page: 1
Lime Applied ***
Dale L0Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or wet Pons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Sile
Cond.
Dry, wet,
Inches
Precip.
Past 24
A tli-
pl
cation
Method
Vola-
till-
nation
Miner -
all-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
m
(ppin)
Crop
Total
Per Acre
Acre
Source
Moist
Haurs
Rate**
Rate
Nitrite
11/6/19
150.00 (CY)
22.727
16.20
3.101
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,400.p
10,100.00 p
30.90 p
14341
FESCUE HAY
11/7/19
75.00 ICY)
11.364
16.20
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,400.p
1Q100.00 p
30.90 p
14341
FESCUE HAY
Nor-19
225.00 (CIS
34A91
_n
to wet I onsMc:
TOTALS:
As
Cd
Cr
Cu
Pb
Fig
Mo
Ni
Se
Zn
P
PAN
Annual Ibsracre
133
0.058
0.009
0.187
3.507
0.192
0.005
0.210
0.175
0.057
25.955
404.67
Cumulative lbsiacre
-.,,
.I
0.393
0.159
5.208
25.922
3.161
0.061
1.034
2.847
0.398
173.470
,.
DSDANDC = DURIIAM, NC S. DURHAM \i�VTP ANAEROF. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, tinder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infuriation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment forkiiowilig violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or nrg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

PACILITYNAME: DURHAM,NC
OWNER: WILLIAM BREEZE, SR.
SITE #: NC OR 00076 FIELD# : OR 00076 0013
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGF-VILLE
PERMIT#: W00003504 ANNUAL DRYTONS APPLIED: 47.31
OPERATOR: WILLIAM LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.20 ACRES PERMITTED: 7.20
Page : I
Lime Applied ttt
DateI LbsrAc
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
/
Solids
D 6
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Veto-
tili-
zation
Miner -
Ili-
zation
TKN
Munonia
Nitrogen
g
Nitrate
mid
PAN
(PPm)
Crop
Total
Per Acre
I
Acre
Source
Moist
Hours
Rate&°
Rate
Nitrite
11/8/19;38o2:0
(W)
5.306
1G.70
0.886
DBWPC
llRY
0-<11T
SUR
0.5
0.20
16,900.p
I,000.00 p
28.60 p
3709
FESCUE HAY
Nov-19
(W)
5,306
(CY)
41.667I
I6.20
5.685
DSDANll
DRY
0-<I/2"
SUR
0.5
0,20
56,400.p
10,100.00 p
30.90 p
14341
FESCUE HAY
Nov-19
Nov-19
300.00 (CSC
MOM
41.667
Total Wet TonslAc: 5,31
V
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
0.081
0.022
0.243
5.433
0.250
0.007
0,262
0.369
0.122
31.938
496.38
170
Cumulative Ibs/acre
0,543
0.158
8956
32.362
3.715
0.072
1.372
3.181
0.519
195.538
DB WPC = llURHAM, NC BROWN �VTP CAKE
DSDANDC=DURI-LAbI, NC S. DURHrLVI �',RVTP ANAEROB. DIGF-S'1'ED CAI:E
(SIGNATUREOF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false infomntion, including the possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reportedor Not Required %—percent p=plan or ng/kg +` Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation sea See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITYNAME: DURHAM,NC
OWNER: WILLiAMBREEZE,SR.
SITE #: NC OR 00076 FIELD# : OR 00076 0017
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 105.14
OPF,RATOR: WILLIAM LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 17.10 ACRES PERMITTED: 17.10
Page: I
Time Applied ***
Date LbsrAc
DATE or
MONTH
Total
Gallons (G) or Cubic
or Wet'I'ons (WT)
Yards (CY)
(specify)
/
Solids
D 4'
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
cation
catiAppon
Method
Vol--
tili-
zation
ali- -
ali-
zation
TKN
Ammonia
Nitrogen
g
Nitrate
and
PAN
(PP°n)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
Rate'*
Rate
Nitrite
10/29/19
74.65 (W)
4.365
66.70
0.729
DBWPC
DRY
07I/2"
SUR
0.5
0.20
I6,900.p
1,000.00 p
288 p
3709
FESCUE HAY
10/30/19
47.45 (W)
2.775
16.70
0.463
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
16,900.p
1,000.00
28.60
P
p
3709
FESCUE HAY
Oct-19
122,10 (NIT)
7.140
l0/29/19
212.00 (CY)
12.3981
16.90
1.765
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
547300. p
10,000.00
4.49
13864
p
p
FESCUE HAY
Oct-19
212,00 (CSC
12.398
11/5119
50.00 (CY)
2.924
16.20
0.399
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
56,400.p
10,100.00 p
30.90
14341
FESCUE HAY
11/6/19
350.00 (CY)
20.468
16.20
2.793
DSDAND
DRY
0-<1/2^
SUR
0.5
0.20
563400.p
103100.00 p
p
30.90 P
14341
FESCUE HAY
Nov-19
400.00
23392
Ti
iai rangy„ern...
Wet Pons/Ac: 7.14
Tntal r'nhinV eJAr
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibsracre
0.075
0.025
0.255
5.149
0.216
0.006
0.214
0.408
0.128
27.311
403.60
I49
Cumulative lbs/aere
0.495
0.178
7.655
29.248
3.710
0.067
1.436
3.048
0.510
187338
DBWPC = DURILIM, NC BROWN \VTP CAKE
DSDANllC=DURHAM, NC S. DURHAM W WTP ANAEROB. DIGESTL'D CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false infomnation, including the possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p -ppm or mg/kg r: Volatilization Rate: Surface 0.5, InjectioMncorporation 1.0
' Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation $*' See Site pH R Linne Application Records Section of Report for Fields where Linne is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: HELENA
OWNER: L.J. ROGERS, JR. PERMIT fl: W00003504 ANNUAL DRY TONS APPLIED: 9.85
SITE N: NC OR 00093 FIELDH : OR 00093 0007 OPERATOR: LARRY ROGERS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 3.90 ACRES PERMITTED: 3.90
Page: 1
Lime Applied ;si
Dafe Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT)(specify)
%
Tons
Cord.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp"')
crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
10/3/19
75.00 (CY)
19.231
15.60
2.527
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
50,900.p
10,400.00 p
4.88 p
13305
WHEAT
Oct-19
75,00 (CI')
19,231
'Coral Gallons/Ac:
Total wet Tons/Ac:
• V,V' �`•V.V ',........ +"�✓
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
67
0.026
0.006
0.164
2.208
0.125
0.002
0.062
0.113
0.025
15.463
145.03
Cumulative lbs/acn;
0.476
0.320
10.090
3L597
3.724
0.219
1.279
4.725
0.455
261.482
llNDANDC =DURHAM, NC N. DURHAM W\VIP ANAEROB. DIGESTED CAKE
X I I L,
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infomtation submitted. I am aware that there are significant penalties for submitting false infomtation, including the possibility of fines and imprisonment for }mowing violations."
N/A=Not Applicable NR=Not Reported or Not Required
%=percent p=ppm onng/}:g
*�
Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
° Application Method: SUR -Surface, INJ - Injection,
SURIN - Incogrorntion
$#§
See Sile pH &Lime
Application Records
Section of Report for Fields
where Lime is to be applied in 2020

ANNUAL
LAND APPLICATION
FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC
PREDOMINANT SOIL SERIES: VANCE
OWNER: L.J. ROGERS, JR
PERMIT#:
W00003504
ANNUAL DRY TONS APPLIED: 69.61
SITE #: NC OR 00093 FIELD# : OR 00093 0013
OPERATOR:
LARRY ROGERS
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report
ACRES UTILIZED: 30.50 ACRES PERMITTED: 30.50
Page: 1
Lune Applied ***
Date Lbs/Ac
allons (0) or Cubic Yards (CY)
Dry
Site
tactics
Appli-
Vola-
Miner -
or wet Tons (wT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, wet,
Past 24
Method
nation
zation
TKN
Nitrogen
and
(pp"')
Crop
MONTH
Total I
Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
10/3/19
337.00 (CY)
11.049
I5.60
1.452
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
501900. p
10,400.00 p
4.88 p
13311
WHEAT
Oct-19
337.00 (Cl�
11,049
I0/2/19
153.00 (CY)
5.016
16.90
0.714
DSDAND
DRY
0.<1/2"
SUR
0.5
0.20
54,300.p
10,000.00 p
4.49 p
13864
WHEAT
1014/19
25.00 (CY)
0.820
16.90
0, 117
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
54,300.p
10,000.00 p
4,49 p
13864
WHEAT
Oct-19
178A0 (Clj
5,836
Total Gallons/Ac:
Total Wet Tons/Ac:
l otel l;nblC YaSiAC: 16.ES`2
As
Cd
Cr
Cu
Pb
IIg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
0.025
0.005
0.145
1.834
0.102
0.002
0.065
0.103
0.023
13.221
141.48
62
Cumulative Ibs/acre
0.721
0.247
8.254
35.159
4.251
0.106
1.952
3.801
0.528
269.658
DNDArNDC =DURHAM, NC N. DURHAM N1V'fP ANAEROE. DIGESTED CAKL'
DSDANDC=DUI213AM, NC S. DURHAM wWTP ANAEKOE. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppnn or mg/kg "° Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
e Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation '°' Sec Site pH R Liue Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURI-IAM, NC
OWNER: SIDNEYTHOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMTr #: IV00003504 ANNUAL DRY IONS APPLIED: 579.45
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES U'1'ILIZF,D: 134.00 ACRES PERMITTED: 134.00
Page: 1
Lime Applied "'
Date LbWAc
alloas (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
lili-
ali-
Atumonia
Nitrate
PAN
DATE or
per
Residual
Dry, R'et,
Past 24
Method
nation
nation
TKN
Nitrogen
and
(PAN
Crop
MONTH
Total I
Per Acre
Solids
Acre
Source
Moist
Hours
Rate*"
Rate
Nitrite
6126/19
459.00 (CY)
3.425
16.70
0.482
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
55,800.p
8080.00 p
5.00 P
13589
FESCUE PASTURE
6/27/19
459.00 (CY)
3.425
16.70
0.482
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
555800. p
8:080.00 p
5.00 p
13589
FESCUE PASTURE
U28/19
75.00 (CY)
0.560
16.70
0,079
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
55,800.p
8,080.00 p
5.00 p
13589
FESCUE PASTURE
Jun-19
993,00 (C)L�
7,410
8/26/19
60.03 (W)
0.448
18.20
0.082
DBWPC
DRY
0-<I/2"
1 SUR
0.5
0,20
I13800. p
714.00 p
4.71 p
2579
I FESCUE PASTURE
829/19
IS.' (W)
0.139
1820
0.025
1DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUEPASTURE
8/30/19
18.: (W)
0.141
18.20
0.026
DBRTC
DRY
0-<l/2"
SUR
0.5
0,20
11,800. p
714.00 p
4.71 p
2579
FESCUE PASTURE
Aug-19
97,52 (R')
0,728
8128/19
159.00 (CY)
1.187
15.60
0.156
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
57,400.p
115000.00 p
4.55 p
14785
FESCUE PASTURE
8/29119
159.00 (CY)
1.187
15.60
0.156
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400. p
113000.00 p
4.55 p
14781
FESCUE PASTURE
8/30/19
159.00 (CY)
1.187
15.60
0.156
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,2100.p
11,000.00 p
4.55 p
14785
FESCUEPASTURE
Aug-19
477,00 (CY)
3.561
8/19/19
206.00 (CY)
1.537
16.70
0.216
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
8/20119
384.00 (CY)
2.866
16.70
0.403
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200. p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
MI/19
375,00 (CY)
2,799
16,70
0.394
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUEPASTURE
8/27/19
375.00 (CY)
2.799
16.70
0.394
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
8/28119
300.00 (CY)
2.239
16.70
0.315
DSDAND
MOIST
0-<I/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
8/29/19
300,00 (CY)
2.239
16.70
0.315
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
8130/19
300.00 (CY)
2.239
16.70
0.315
DSDAND
MOIST
0-<I/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
Aug-19
24240.00 (C)LS
16.718
9/3/19
31.55 (W)
0.235
1820
0.043
DBWPC
DR
0-<1/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE PASTURE
9/4/19
39.64 (W)
0.296
18,20
0.054
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800. p
714.00 p
4.71 p
2579
FESCUE PASTURE
9/5/19
38.87 (W)
0,290
18.20
0.053
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE PASTURE
9/10/19
39.83 (W)
0.297
1820
0.054
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE PASTURE
9/16/19
35.53 (W)
0.265
18.20
0.048
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
11,800-p
714.00 p
4.71 p
2579
FESCUE PASTURE
Sep-19
185,42 (11J
1,383
9/3/19
75.00 (CY)
0.560
16.70
0.079
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
535200, p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
Sep-19
1 75,00 (C7111
0.560

FACILITY NAMF,: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 579.45
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 134.00 ACRES PERMITTED: 134.00
Page : 2
Lime Applied
Date LbsrAc
Total
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Apph-
Vola-
Mincr-
I
or Wet Tons (\VT) (specify)
%
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, \Vet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppnt)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate'"
Rate
Nitrite
Gallons/Ac:
Total Wet Tons/Ac: 2.11
'lbtal Cubic YtlYAc: 28.25
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
110
Annual Ibs/acre
0.046
0.010
0.280
3.445
0.124
0.004
0.060
0.214
0.059
18.069
224.38
Cumulative Ibs/acre
0.352
0.178
2.802
20.052
1,589
0,041
0.605
1.691
0.358
99.030
llNDANDC=DURI-IAM, NC N. DURHAM W\VTP ANAEROB. DIGESTED CAKE
DB\VPC = DURHAM, NC BROWN \Vl'P CAKE
DSDANDC=DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF hAND APPLIER) DATE
"I certify, ender penalty of law, that this document was prepared ender my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I ant aware that there are significant penalties for submitting false infomtation, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR= Not Reported or Not Required %=percent p=ppm or mg/kg ' Volatilization Rate: Surface 0.5. Injeclion/huoryoration 1.0
" Application Method: SUR - Surface, 1NJ - Injection, SURIN - Incorporation •'• See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0004
�UQMTT AT mraicN- caa ncr ar hnnnn, nfrennA
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT #: NV00003504 ANNUAL DRY TONS APPLIED: 260.82
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 36.00 ACRES PERMITTED: 36.00
Page: I
Lime Applied ***
Dale Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppnr)
Crop
MONTH
Total I
Per Acre
Solids
Acre
Source
Moist
Hours
+
Rate"
Rate
Nitrite
7129{19
61.28 (W)
1.702
19.70
0.335
DBWPC
DRY
0-<I{T'
SUR
0.5
0.20
12,000.p
508.00 IT
5.00 p
2557
FESCUEHAY
J111-19
6L28 (R')
1.702
8/12/19
56.57 (W)
1.571
I8.20
0.286
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 IT
2579
FESCUE BAY
8115/19
28.77 (W)
0.799
18.20
0.145
DBWPC
DRY
0-<112"
SUR
0.5
0.20
11,800. p
714.00 IT
4.71 p
2579
FESCUE HAY
8/16/19
41.61 (W)
1.I$6
1820
0.210
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 IT
2579
FESCUE HAY
Aug-19
126.95 (\V)
3.526
8/6/19
78.00 ICY)
2.167
15.60
0.285
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
57,400.IT
11,000.00 IT
4.55 p
14785
FESCUE HAY
8/9/19
150.00 (CY)
4,167
15.60
0.547
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
57,400.p
11,000.00 p
4.55 IT
14785
FESCUE HAY
8/12119
309.00 (CY)
8.583
15.60
1.128
UNHAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400.IT
11,000.00 P
4.55 p
14785
FESCUE HAY
8113/19
384.00 (CY)
10.667
15.60
1.401
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400.IT
11,000.00 IT
4.55 p
14785
FESCUE HAY
8/15/19
275,00 (CY)
7,639
15.60
1.004
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400.p
11,000400 P
4.55 IT
14785
FESCUE HAY
Aug-19
14196,00 (CIS
33,223
8RG719
38UL
0.667
I6.70
1.500
DNDAND
DKY
0-<lY2"
SUR
0.5
0.20
53,200. p
9,880.00 p
4.46 p
13608
FESCUE HAY
8/19119
102.861
16.70
0.402
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUEHAY
Aug-19
483,528

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE N: NC PS 00001 FtELDfl : PS 00001 0004
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT N: W00003504 ANNUAL DRY TONS APPLIED: 260.82
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 36.00 ACRES PERM rrLD: 36.00
Page: 2
Lime Applied
Dale LbsrAc
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner-
orNetTons(WT)(specify)
Tons
Cond.
Precip.
cation
tfli-
ali-
Ammonia
Nitrate
PAN
DATE or
V,
Per
Residual
Dry, Wet,Past
24
Method
zalion
nation
TKN
Nitrogen
and
(ppni)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Bate
Nitrite
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC=DURHAM, NC N. DURHAM \V1VTP ANAEROB. DIGESTED CAKE
DSDANDC=DURHAM, NC S. DURI JAM W WTP ANAEROB. DIGESTED CAKE
� l.,e, LArf�
X L
(SIGNATURE Of LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I out aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %—percent p=ppm or mg/kg Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ-bijcetion, SURIN - Incorporation "* See Site pH & Little Application Records Section of Report for Fields where Little is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: SIDNEYTHOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIFS: FAIKVIEW
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 67.65
OPERATOR: SIDNEY T'HOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 23.10 ACRES PERMITTED: 23.10
Page: I
Lime Applied "'
IYute Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
/
Tons
Cond.
Prccip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
nation
TKN
Nitrogen
and
(ppnr)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
9/3119
200.00 (CY)
8.658
16,70
1.218
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
1 53,200.p
9,880.00 p
4.46 p
13608
FESCUE HAY
9/4/19
281.00 (CY)
12.165
16,70
1.711
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE HAY
Sep-19
481.00 (C)L)
20,823
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 20.82
As
Cd
Cr
Cn
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
80
Annual Ibslacrc
0.029
0.006
0.199
1.722
0.084
0.003
0.043
0.131
0.029
13.472
162.25
Cumulative Ibs/acre
0,487
0.221
2.658
20.279
1.803
0.045
0.779
1.841
0.566
106,837
DSDANDC=DURHAM, NC S. DURHAM RrIVTP ANAEKOB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIEIi) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infommtion submitted.I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
N/A —Not Applicable NR=Not Reported or Not Required %=percent p=plan or nrg/kg s: Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
` Application Method: SUR - Surface, INJ - Injection, SURLY - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURI-IAM, NC
OWNER: SIDNEYTHOMPSON
SITE N: NC PS 00001 FIELDN : PS 00001 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
DOMINANT SOIL SERIES: TOAST
PERMT#: NV00003504 ANNUAL DRY TONS APPLIED: 372.38
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 104.10 ACRES PERMITTED: 104.10
Page: 1
Lime Applied
Date Lb>�Ac
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cord.
Precip.
cation
lili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, We(,
Past 24
Method
zation
zation
'l'KN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rates
Rate
Nitrite
6/28/19
82.95 (W)
0.797
19.70
0.157
DBR'PC
DRY
0-<1/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
Jun-19
8295 (W)
0,797
6/28/19
356,00 (CY)
1 3.420I
16.70
0.481
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
55,800. p
8,080.00 P
5.00 p
13589
FESCUE HAY
Jun-19
356.00 (CN91
3,420
7/2/I9
65.35 (W)
0.628
19.70
0.124
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
7/3/19
64.21 (W)
0.617
19.70
0.122
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
7/10/19
98.03 (W)
0.942
19.70
0.186
DBWPC
DRY
0-<112"
SUR
0.5
0.20
12,000. p
508.00 p
5.00 P
2557
FESCUE, HAY
7/16/19
42,80 (W)
0.411
19.70
0.081
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
Sul-19
270,39 011)
2.598
7/1/19
203.00 (CY)
1.950
15.30
0.251
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
63,500. p
9,020.00 p
30.80 p
15437
FESCUE 14AY
713/19
384.00 (CY)
3.689
15.30
0.475
DNDAND
DRY
0-4/2"
SUR
0.5
0,20
63,500. p
91020.00 p
30.80 p
15437
FESCUE HAY
7/9119
300,00 (CY)
2.882
15.30
0,371
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
63,500. p
9,020.00 P
30.80 P
15437
FESCUE HAY
7/10/19
334.00 (CY)
3.208
15.30
0.413
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
63,500. p
91020.00 p
30.80 p
15437
FESCUE HAY
7/I1/19
353.00 (CY)
3.391
15.30
0.437
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
63,500. p
97020.00 p
30.80 p
15437
FESCUE HAY
7/12/19
234,00 (CY)
2.248
15.30
0.290
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
63,500.p
9,020.00 p
30.80 p
15437
FESCUEHAY
7/15/19
153.00 (CY)
1.470
15.30
0.189
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
63,500.p
93020.00 p
30.80 p
15437
FESCUE HAY
Jul-19
1,961,00 (CND
18,838

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: TOAST
OWNER: SIDNEY THOMPSON PERMIT 9: W00003504 ANNUAL DRY TONS APPLIED: 372.38
SITE 8: NC PS 00001 FIELDff : PS 00001 0006 OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 104.10 ACRES PERMITTED: 104.10
Page: 2
Lime Applied '•'
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Toils (WT) (specify)
/
Tons
Coll
Precip,
cation
lili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry,Wet,
Pasl24
Method
nation
zation
'1'KN
Nitrogen
and
(ppm)
Crop
MON'1'li
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate**
Rate
Nitrite
Total Gallons/Ac:
Total Wet Tons/Ac: 3,39
'Total Cubic Yds'Ac: 22.26
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.063
0.013
0.233
2.156
0117
0.002
0.060
0.148
0.063
14.378
161.49
91
Cumulative lbsracre
0.371
0.098
2.489
14.697
1.557
0.083
0.406
1.737
0.287
83.205
llBWPC= DURI-IAM, NC BROWN WTP CAKE
DNDe1NDC =DURHAM, NC N. DURHAM MVTP ANAL'120B. DIGESTED CAKE
DUin� 2�2�Zo
(SIGNATURE OF LAND APPLIF,R) DATE
"I certify, ander penalty oflaw, that tbis document was prepared ender my direction or supervision in necordance witb a system designed to assure that qualified personnel properly gathered and
evaluated the infomtation submitted. I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
NIA —Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/log ** Volatilization Rate: Surface 0.5, hijectiorvIncorporslion 1.0
* Application Method: SUR - Surface, INJ - Injection, SUR1N - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: SIDNEYTHOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0007
RFCtnI ]AI . SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDO.YIMANT SOIL SERIFS: FAIRVIEW
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 125.48
OPERATOR: SIDNEY THO.MPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 31.80 ACRES PERMITTED: 31,80
Page: 1
Lime Applied
Dafe LbsfAc
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Veto-
till-
zation
Miner -
all-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
+
Rate"
Rate
Nitrite
8/6/19
206.00 (CY)
6.478
15.60
0.851
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400. p
I I,000.00 p
4.55 P
14785
FESCUE PASTURE
817/19
23, (CY)
7.358
15.60
0.967
DNDAND
DRY
0-<l/2"
SUR
0.5
0.20
57,400.p
11,000.00 P
4.55 p
14785
FESCUE PASTURE
8/8/19
309.00 (CY)
9.717
15.60
1.277
DNDAND
MOIST
0-<I/2"
SUR
0.5
0.20
57,400. p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
8/9/19
206.00 ICY)
6,478
115.60
0.851
llNDAND
llRY
0-<I72"
SUR
0.5
0.20
57,400. p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
Aug-19
955.00 (CAT)
30,031
Total Cubic Yds/Ac: 30.03
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
117
Annual lbs/acre
0.039
0.008
0.237
3.015
0.137
0.005
0.066
0.167
0.040
23.596
187.03
Cumulative lbs/acre
0.237
0.104
L476
15.394
1.162
0.035
0.372
1.121
0.170
95.700
[
DNDANDC=DURHAM, NC N. DURHAM 1VWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIEK) DA1'L'
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false infomration, including the possibility of tines and imprisonment for knowing violations."
NIA =Not Applicable NR= Not Reported or Not Required %— percent p=ppm or nrg/kg •" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
• Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *"° Sec Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY Nr Y E: DURIIAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0009
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 119.20
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 38.80 ACRES PERMITTED: 38.80
Page : I
Lune Applied
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (1VT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATEor
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp"')
Crap
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
7/31/19
309.00 (CY)
7.964
15.30
1.026
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
63,500.p
9,020.00 p
30.80 p
15437
FESCUE PASTURE
Jul-19
309.00 ICY)
7.964
1
8/1/19
45.68 (W)
1.177
18.20
0.214
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUEPASTURE
8/5/19
41.06 (W)
1.058
18.20
0.193
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800. p
714.00 p
4.71 p
2579
FESCUE. PASTURE
Aug-19
86,74 OV)
2,235
8/1/19
309.00 (CY)
7.964
15,60
1.046
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400.p
11,000.00 P
4.55 p
14785
FESCUE PASTURE
8/5/19
150.00 (CY)
3-866
11.60
0.IN
DNDANO
MOIST
0-<I/2"
SUR
0.5
0.20
573400.p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
8/6/19
25.00 (CY)
0.644
IS.60
0.085
DNDAND
DRY
0-<IY2"
SUR
0.5
0.20
57,400, p
115000.00 p
4.55 p
14785
FESCUE PASTURE
Aug-19
484.00 (CI')
12,474

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0009
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIPPORD
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 119.20
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 38.80 ACRES PERMITTED: 38.80
Page: 2
Lime Applied ***
Date Lbs/Ac
Total
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Volz-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wct,
past 24
Method
nation
nation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
Gallons/Ac:
Total Wet Tons/Ac: 2,24
-1 Olal (;trbtc YtiSIAc: 20.44
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
0.034
0.007
0.197
3.018
0.095
0.003
0.046
0.155
0.047
15.109
133.00
82
Cumulative Ibs/acre
0.251
0.108
1.057
9.997
0.897
0.059
0.371
0.975
0.315
40.682
DNDANDC = DURI-IAM, NC N. llURHAM W WTP ANAEROB. DIGES"LED CARF" _ -
DBWPC=DURHAM, NC BROWN WTP CAK1i
(SIGNATURE OF LAND APPLiER) DATE
"I certify, under penally of law, that this document was prepared tinder my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for ]mowing violations."
N/A = NotApplicable NR=Not Reporledor Not Required %— percent p=plan or mg/kg ** Volatilization Rate: Surface 0.5. Injection/lncorpomtion 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation '** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILLI'Y NAME: DRAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0010
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: NV00003504 ANNUAL DRY TONS APPLIED: 270.87
OPERATOR: STDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 67.50 ACRES PERMI'Pl'Ell: 67.50
Page: I
Lime Applied "'
Dale Lbs/Ac
17
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Net Tans (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Net,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppnr)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
11ours
Ratees
Rate
Nitrite
9/11/19
41.17 (N)
0.610
18.20
0.111
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800. p
714.00 p
4.71 p
2579
FESCUE PASTURE
9/12/19
]01.81 (w1
1.509
1820
0.275
DBWPC
DRY
0-4/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE PASTURE
Sep-19
142,98 011)
2.118
9/10/19
200.00 (CY)
2.963
15.60
0.389
DNDAND
DRY
0-4/2"
SUR
0.5
0.20
57,400. p
11,000.00 p
4.51 p
14785
FESCUE PASTURE
9/11119
384.00 (CY)
5.689
15.60
0.741
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400. p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
9/16/19
309.00 (CYO
4.578
15.60
0.601
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
57,400.p
11,000.00 p
4.55 p
14711
FESCUEPASTURE
9/17/19
309.00 (CY)
4.578
15.60
0.601
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
57,400. p
11,000.00 p
4.55 p
14785
FESCUE PASTURE
Sep-19
1,202.00 (CV)
17.808
9/12/19
309.00 (CY)
4.578
16.70
0.644
DSDAND
DRY
0-<I/2"
SUR
0.5
0.20
53,200. p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
9/13119
309.00 (CSC
4.578
16.70
0.644
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE PASTURE
Sep-19
618.00 (CY)
9.156

FACR,ITYNArME: DURHAM,NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0010
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLII FOP
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 270.87
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 67.50 ACRES PERMITTED: 67.50
Page: 2
Lune Applied "'
Date LbsrAc
allons (G) or Cubic Yards ICY)
Dry,
Site
Inches
Appli-
Vola-
Miner-
orWetTons(NT)(specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
r
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Ace
Source
Moist i
Hours
Rule#i
Rate
Nitrite
r oral uauonsukc:
Total Wet Tons/Ac: 2.12
yVVV VJ V `V V
As
Cd
Cr
Cu
Pb
Hg
Me
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs(acre
106
0.043
0.009
0.250
3.532
0.122
0.004
0.060
0.194
0.056
19.966
182.93
Cumulative Ibs/aere
0.217
0.068
2.406
13.360
1.150
0.062
0.296
1.496
0.206
78.805
DBWPC =DURHAM, NC BROWN \V'1'P CAKE
DNDANllC =DURHAM, NC N. DUftf--TAM \VWTP ANAF,ROB. llIGESTED CAKE
DSDANDC=DURHAM, NC S. DURI LAM WWTP ANAEROB. DIGESTED CAKE
X 1 1n KV) I�/ZR
(SIGNATURE OF LAND APPLIER) DATE
"I certify, wider penalty oflaw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the info niation submitted. I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=pion or mg/kg °a Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: SIDNL'YTHOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0011
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 138.29
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 30.20 ACRES PERMITTED: 30.20
Page: I
Lime Applied ��•
Date Lbs'Ac
allons (G) or Cubic Yards(CY)
Dry
Site
Inches
pppli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
Ili-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zalion
nation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
7/22/19
58.89 (W)
11.9501
19.70
0.384
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
12,000.p
508-00 p
5.00 p
2557
FESCUE HAY
7/30/19
19.55 (\\D
0-647
19.70
0.128
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
3111-19
78.44 (W)
2.597
7/22/19
487-00 (CY)
16.126
15.30
2.078
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
63,500,p
9,020.00 p
30.80 p
11437
FESCUE HAY
7/29/19
409.00 (CY)
13.5431
15.30
1.745
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
63,SOO.p
9,020.00 p
30.80 p
15437
FESCUE HAY
JuI-19
896.00 (CS')
29.669
811/19
40.56 (W)
1.343
]8.20
0.244
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
11,800.p
714.00 p
4.71 p
2579
FESCUE HAY
Aug-19
40,56 (M�
L343
1 O[al Ua110115/AC:
Total Wet Tons/AC:
3.94
�MV`V •
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:V•"•
Annual lbs/acre
122
0.068
0.014
0.312
3.425
0.145
0.003
0.073
0.208
0.076
19.671
204,95
Cumulative lbs/acre
0.251
0.060
1.632
13.522
1.230
0.080
0.284
1.302
0.184
61.645
DBWPC=DURHAM, NC BROWN WTP CAKE
DNDANDC=DURHAM, NC N. DURHAM WNTP ANAEROB, llIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of Inv, that this document was prepared under my direction or supervision in accordance with a system designed to usarc tlmt qualified personnel properly gathered and
evaluated the information submitted. Iran aware that there are significant penalties for submitting false information, including the possibility offices and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or ing/kg * Volatilization Rote: Surface 0.5, InjectioMncorporation 1.0
° Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation e:r See Site pH & Linte Application Records Section of Report for Fields where Lime is to be applied in 2020

PACILITYNAME: DURHAM,NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0012
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL, SERIES: CLIFFORD
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 137.90
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE, CAPACITY (NON-503):
ACRES UTILIZED: 30.10 ACRES PERMITTED: 30.10
Page: I
Lime Applied '••
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miller.
or Wet Tons (WT) (specify)
%
Tons
Carl
Precip.
cation
tlli-
ali-
Ammonia
Nitrate
PAN
DATEor
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
9/10/19
100.00 (CY)
3.322
15.60
0.437
DNDAND
DRY
0-<I/2n
SUR
0.5
0.20
57,400.p
11,000.00 p
4.55 p
14785
FESCUE HAY
Se]
3,322
1
9/4/19
128.00 (CY)
4.252
16.70
0.598
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200. p
9,880.00 p
4.46 p
13608
FESCUE HAY
9/5/19
300.00 (CY)
9.967
16.70
1.402
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE HAY
9/9/19
459.00 (CY)
15.249
16.70
2.145
DSDAND
DRY
0-<1/2"
SUR
0.5
0.20
53,200.p
9,880.00 p
4.46 p
13608
FESCUE HAY
Sep-19
887,00 (C1')
29,468
Total Gallons/Ac:
Total Wet Tons/Ac:
.V,"y,♦V.V .V'•`VCr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbstacre
126
-
0.046
0.009
0.307
2.771
0.134
0.004
0.068
0.204
0.046
21.676
250.31
Cumulative lbs/acre
0.405
0,165
3.399
23976
2.460
0.060
0,648
2.202
0.344
131.338
DNDANDC = DURIIAM, NC N. DURHAM MVTP ANAEROB. DIGES'1'Ell CAKE
llSDANDC =DURHAM, NC S. DURHAM WN1'P ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A=Not Applicable NR=Not Reported or Not Required %=percent p=ppm or mg/kg Volatilization Rate: Surface 0.5, htjectioriancorporation 1.0
Application Method: SUR - Surface, IN7 - Injection, SURIN - Incorporation k4# See Site pH R Line Application Records Section of Report for Fields where Linte is to be applied in 2020

PACILITYNAME: DURHAM,NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0013
RESIDUAL SOURCE(S): Sec list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINMN'ISOIL SERIFS: FAIRVIEW
PERMIT #: NV00003504 ANNUAI. DRY TONS APPLIED: 63.22
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.20 ACRES PERMITTED: 16.20
Page: I
Lime Applied "•
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (1VT) (specify)
llry
Site
Inches
Appli.
Vola-
Miner -
Pons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
AN
Total
DATE or
Solids
per
Residual
Dry, \Vet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
m
(pp )
Cro p
MONTH
Per Acre
Acre
Source
Moist
Hours
Rate"
Rate
Nitrite
7/31119
86.08 (W)
5.314
19,70
1.047
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE
Jul-19
86.(18 OV)
5,314
7130/19
284.00 (CY)
17.531
15.30
2,259
1 DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
63,500.p
9,020.00 p
30.80 p
15437
FESCUE
7/31/19
75.00 (CY)
4.630
15.30
0.597
DNDAND
DRY
0-4/2"
SUR
0.5
0.20
633500.p
97020.00 p
30.80 p
11437
FESCUE
Jul-19
359.00 (CY)
22.161
t oral umionslnc:
Total Wet Tons/Ac: 5.31
TOTALS:
Cr
Cu
Pb
Hg
Me
Ni
Se
Zn
P
PAN
Annual lbs/acrc
0.081
0.016
0.249
2.220
0.127
0.002
0.070
0,154
0.081
14.752
154.22
94
Cumulative Ibs/acre
0.247
0.156
0.737
8.323
0,519
0.012
0.357
0.641
0,301
39.811
DB\VPC = DURFLVM, NC BRO\VN W'IP CAKE
llNDANDC=llURHAM, NC N. DUAHAM W\VTP ANAEROB. DIGESTED Gtu E
(SIGNATURF, OF LAND APPLIER) DATF.
"I certify, under penalty of law, that this document ryas prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for ]mowing violations."
N/A=Not Applicable NR=Not Reported
or Not Required
%=percent p=ppm
or mg/kg
a` Volatilization Rate: Surface 0.5,
Injectiondlncogroration 1.0
° Application Mclhod: SUR-Surface
INI -Injection,
SURIN -Incorporation
+�° See Site pH R; Lime Application Records
Section PR for Pields
where Lime is to be applied in 2020

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0014
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT#: W00003504 ANNUAL DRY TONS APPLIED: 123.59
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 27.70 ACRES PERMTITED: 27.70
Page: I
Lime Applied •••
Date T.byAc
Gallons (G) or Cubic Yards (CY)
or Wet Tons (1VT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%Tons
Cond.
Precip.
cation
till-
ali-
Anunmria
Nitrate
PAN
DATE or
MONTH
Total
I Per Acre
Solids
Residual
Dry, We
Past Past 24
Method
zation
zation
"fKN
Nitrogen
and
(ppnr)
Crop
Acre
Source
Moist
Hours
<
Rate""
Rate
Nitrite
7/15119
67.49 (W)
2.436
19.70
0.480
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUEHAY
7117/19
45.43 (W)
1.640
19.70
0.323
DBWPC
DRY
0-<1/2"
SUR
0.5
0,20
123000.p
508.00 p
5.00 p
2557
FESCUE HAY
7/19/19
22.56 (W)
0.814
19.70
0.160
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
12,000.p
508.00 p
5.00 p
2557
FESCUE HAY
Jul-19
135,48 (W)
4.890
7/15119
231.00 (CY)
8,339
15.30
1.075
1 DNDAND
I DRY
0-<I/2"
SUR
0.5
0.20
63,500.p
95020.00 p
30.80 p
15437
FESCUE IJAY
7/16/19
106.00 (CY)
3.827
15.30
0.493
DNDAND
DRY
0-<1/2"
SUR
0.5
0.20
633500.p
9,020.00 p
30.80 p
15437
FESCUE HAY
7/17/19
309.00 (CY)
11.155
15.30
1.437
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
63,500.p
9,020.00 p
30.80 p
15437
FESCUE HAY
7118/19
106.00 (CY)
3.827
15.30
0A93
DNDAND
DRY
0-<I/2"
SUR
0.5
0.20
63,500.p
9,020.00 p
30.80 p
11437
FESCUE FLAY
Jul-19
752.00 (CP)
27.148

FACB,ITY NA vm: DURHAM, NC
OWNER: SIDNEYTHOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0014
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOB, SERIES: FAIRVIEW
PERMIT#: W000035W ANNUAL DRY TONS APPLIED: 123.59
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 27.70 ACRES PERMITTED: 27.70
Page: 2
Lime Applied
Date LbsrAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT)(specify)
%
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
Total
DATE or
Solids
PerResidual
Dry, Wet,
Past 24
Method
zation
ration
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
Arc
Source
Moist
Hours
Rate"
Rate
Nitrite
Total Wet Tons/Ac: 4.89
1j
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
113
0.083
0.017
0.292
2.658
0.146
0.003
0.078
0.181
0.083
18.032
188.23
Cumulative lbs/acre
0.181
0.151
0.705
9.76I
0.420
0.012
0.238
0.618
0.164
44.697
DBWPC =DURHAM, NC BRO\VN WTP CAKE
DNDANDC =DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
�jrl l �DV� UllnJ`1
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gathered and
evaluated the information submitted. I our aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR= Not Reported or Not Required %=percent p=ppm or ng/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation °`" See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

a 3, s "'ram Summit Environmental Technologies, Inc.
0 v h 3310Win St.
,., :4zONPetENT.lL TEC: PUIOLDGI:=S, inc Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.. [phone]
l�
Website: hgR://www.settekcom
February 10, 2016
Nate Roth
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: (336) 99M450
RE: Durham
Dear Nate Roth:
Order No.: 16011604
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/28/2016 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted,
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Bachar Najm
Project Manager
3310 Win St,
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arizona A70788, Arkansas 88-0735, California 07256CA, Colorado, Connecricut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.S, Indiana C-OH-li. Kansas E-10347, Kentucky (Underground Storage Tank)
3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099,
New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio DriNdng Water 4170, Ohio VAP CL0052, Oklahoma
9940. Oregon OH100001, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-I1-5, Region 8 STMS-L,
USDA/APHiS P330-11-00244, Utah OH009232011A, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 8
Page 1 of 10

Summit Environmental Technologies, Inc. +
$ 5 ��IFIE 3310 Win St. Case Narrative
SRON Pi FNT1L _ 0Lo's: s r.c. Cuyahoga Falls, Ohio 44223
O ' .rzryt ray Lzbar.ruries TEL: [phone] FAX.- [phone] Wp 16011604
Website: httn.1l/ w settekcom Date: 2/10/2016
CLIENT: Synagro
Project: Durham
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including over Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting /certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Oria nal
Page 2 of 8
Page 2 of 10

Smnntit Gnviranmental technologies, in
�"PP�; _ r 3310Win Qualifiers and Acronyms
^nONp7�tiTa,Lfi Cuyahoga Falls, Ohio 4422 WO#: 16011604
M1, TEL: [phone] FAX: [phone]
Website: httn.•11www settek,.00 Date: 2/10/2016
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+),
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+),
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+),
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for repotting.
Please refer to the Analyfical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 8
Page 3 of 10

SSun-E Summit Environmental Technologies, Inc. W®rkorder
uA 3310 Win St. inONP7F\rAL3 dOL�v.: S �tr Cuyahoga Falls. Ohio 44223 Sample Summary
TEL: [phone] FAX.- [phone]
WO#: 16011604
Website: httn-//ww____. wseget-cn»,
10-Feb46
CLIENT: Synagro
Project: Durham
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
16011604-001 North Durham 1/26/2016 2:15:00 PM 1/28/2016 9:55:00 AM Sludge
Page 4 of 8
Page 4 of 10

If AM
'i � 'ill ONYIGITA d0lu .'S L.
4n3.f';'ra _nt._Y37J Pi
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX., (330) 2S3-4489
Website: hg2.-Ilwwwsettei-com
WO#: 16011604
DR d Date eport
e 2/10/2016
CLIENT: Synagro Tag Number:
Matrix: SLUDGE
Lab ID: 16011604-OOIA
Project: Durham
Client Sample ID North Durham
Analyses
RCI
PH (SW9045D)
pH
Collection Date: 1/26/,4016 2:15:OO PM
Result RL Qual Units DF Date Analyzed
8.22
SW9045D
s.u. @20.4C
Analyst: DHC
1 /29/2018 10:30:00 AM
Qua11i1C[S: * Value exceeds Maximum Contaminan[Level. E Value above quavtitatioa range
H Holdmg times for preparation or analysis exceeded M Manual Integration used to dMermine area response
MC Value is be]ow Nioimmn Compound Lmilc N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDImut
P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit ollglnal
D Samples with CalcVal< MDL I Analyte detected below ynanlilation limits Page 5 of 8
Page 5 of 10

Summit Emironmemal Technologies, Inc.
WO#: 16011604
3370 Win St.
r�N"tIRON MENTAL 'O. OLD=5,.'rc0 Cuyahoga Falls. Ohio44223 Date Reported: 2/10/2016
::raryErai Lsrcrsra.r:es TEL: [phone] FAX [phone]
Company: Synagro
Website: hit LlLvww settek co
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 1/28/2016
Project#: Durham
TCLP Metals Analysis (6010)
anent ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
North Durham 001 1/26/2016 TCLP Arsenic(AsI 0.500 ND mg/L Sludge EPA 6010C 1 5.00 1/29/2016 WK
North Durham 001 1/26/2016 TCLP Barium(Ba) 5.00 ND mg/L Sludge EPA 6010 C 1 100 1/29/2016 WK
North Durham 001 1/26/2016 TCLP Cadmium(Cd) 0.100 ND mg/L Sludge EPA 6010 C 1 1,00 1/29/2016 WK
North Durham 001 1/26/2016 TCLP Chromium(Cr) 0.200 ND mg/L Sludge EPA 6010 C 1 5.00 1/29/2016 WK
North Durham 001 1/26/2016 TCLP Lead(Pb) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 1/29/2016 WK
North Durham 001 1/26/2016 TCLP Selenium(Se) 0.500 ND mg/L Sludge EPA 6010 C 1 1.00 1/29/2016 WK
North Durham 001 1/26/2016 TCLP Silver(Ag) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 1/29/2016 WK
TCLP Mercury Analysis (1311/74701
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
North Durham 001 1/26/2016 TCLP Mercury 0.00500 ND mg/L Sludge EPA 7470 A 1 0.200 2/5/2016 MFW
SVOC SW-846: 8081-TCLP Pesticides
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Ru¢ Analyst
North Durham 001 1/26/2016 Chlordane, total 0.0250 ND mg/L Sludge EPA 8081 B 1 0.0300 2/8/2016 JBN
North Durham 001 1/26/2016 Toxaphene 0,0500 ND mg/L Sludge EPA 8081 B 1 0.500 2/8/2016 JBN
North Durham 001 1/26/2016 Endrin 0.00250 ND mg/L Sludge EPA 8081 B 1 0.0200 2/8/2016 JBN
North Durham 001 1/26/2016 gamma-BHC 0.00250 ND mg/L Sludge EPA 8081 B 1 0.400 2/8/2016 JBN
North Durham 001 1/26/2016 Heptachlor 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 2/8/2016 JBN
North Durham 001 1/26/2016 Heptachlor epoxide 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 2/8/2016 JBN
North Durham 001 1/26/2016 Methoxychlor 0.00250 ND mg/L Sludge EPA 8081 B 1 10.0 2/8/2016 JBN
VOC by GC/MS
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
North Durham 001 1/26/2016 1,1-Dichloroethene 0.100 ND mg/L Sludge EPA 8260 B 1 0.700 1/29/2016 MES
North Durham 001 1/26/2016 1,2-Dichloroethane 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
North Durham 001 1/26/2016 MEK 2.00 ND mg/L Sludge EPA 8260 B 1 200 1/29/2016 MES
North Durham 001 1/26/2016 Benzene 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
North Durham 001 1/26/2016 Carbon tetrachloride 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
North Durham 001 1/26/2016 Chlorobenzene 0.100 ND mg/L Sludge EPA 8260 B 1 100 1/29/2016 MES
North Durham 001 1/26/2016 Chloroform 0.100 ND mg/L Sludge EPA 8260 B 1 6,00 1/29/2016 MES
North Durham 001 1/26/2016 Tetrachloroethene 0,100 ND mg/L Sludge EPA 8260 B 1 0.700 1/29/2016 MES
North Durham 001 1/26/2016 Trichloroethene 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
North Durham 001 1/26/2016 Vinyl chloride 0.200 ND mg/L Sludge EPA 8260 B 1 0.200 1/29/2016 MES

Summit Enviromnental Technologies, Inc. WO�k: 16011604
MSUMMIT
3310 Win St.
^nONr1s T L =�Pt OLv ._5, i�.G Cuyahoga Falls, Ohio 44223 Date Reported: 2/10/2016
na,ytiez TEL: [phone] FAY: [phone] Company: S Yn `�' a o
P
Website: httnL// mw .seitekcom
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 1/28/2016
Project#: Durham
SVOC 8270 TCLP BNA List
Client ID# Lab H}# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
North Durham 001 1/26/2016 1,4-Dichlorobenzene 0.200 ND mg/L Sludge EPA 8270 C 2 7.50 2/2/2016 BAV
North Durham 001 1/26/2016 2,4,5-Trichlorophenol 0.500 ND mg/L Sludge EPA 8270 C 2 400 2/2/2016 BAV
North Durham 001 1/26/2016 2,4,6-Trichlorophenol 0.500 ND mg/L Sludge EPA 8270 C 2 2.00 2/2/2016 BAV
North Durham 001 1/26/2016 2,4-Dinitrotoluene 0.200 ND mg/L Sludge EPA 8270 C 2 0,130 2/2/2016 BAV
North Durham 001 1/26/2016 Cresols, Total 10.0 ND mg/L Sludge EPA 8270 C 2 200 2/2/2016 BAV
North Durham 001 1/26/2016 Hexachloro-1,3- 0.200 ND mg/L Sludge EPA 8270 C 2 0.500 2/2/2016 BAV
butadiene
North Durham 001 1/26/2016 Hexachlorobenzene 0.200 ND mg/L Sludge EPA 8270 C 2 0.130 2/2/2016 BAV
North Durham 001 1/26/2016 Hexachloroethane 0.200 ND mg/L Sludge EPA 8270 C 2 3.00 2/2/2016 BAV
North Durham 001 1/26/2016 Nitrobenzene 0.200 ND mg/L Sludge EPA 8270 C 2 2.00 2/2/2016 BAV
North Durham 001 1/26/2016 Pentachlorophenol 0,500 ND mg/L Sludge EPA 8270 C 2 100 2/2/2016 BAV
North Durham 001 1/26/2016 Pyridine 0.500 ND mg/L Sludge EPA 8270 C 2 5.00 2/2/2016 BAV
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst
North Durham 001 1/28/2016 214-D 5.00 ND mg/L Sludge EPA 8321 A 1 10.0 2/9/2016 BJH
North Durham 001 1/26/2016 21415-TP 0.500 ND mg/L Sludge EPA 8321 A 1 1.00 2/9/2016 BJH

Summit Ein ironmental Technologies, Inc.
WO#: 160ll604
Or
3310 Win St.
"MRONtt N C OLr ;=sr iitc Cuyahoga Falls, Ohio 44223 Date Reported: 2/10/2016
hraiy`ira. Lau�ratarie. TEL: [phone] FAX.- [phone]
Company: Synagro
Website: hum,,//www scuek c.,..,
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 1/28/2016
Project#: Durham
Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst
North Durham 001 1/26/2016 Flashpoint (140°F) >140 OF Sludge EPA 1010 1
1/29/2016 TAH
North Durham 001 1/26/2016 Cyanide, Reactive ND mg/Kg Sludge EPA 9014 1 0.500 2/1/2016 MS
North Durham 001 1/26/2016 Sulfide, Reactive ND mg/Kg Sludge EPA 9034 1 25.0 2/l/2016 MS

Summit Gnvit'onnieiittll `1'echttologies, 111c• Analysis Request/C11ain Of Custody
33111 Win StfCcl For tiunnnit Gnviruumcntul Ikchnologics. Inc. ow only _.--
C'uylihoga Falls, Ohio 44223 TO: 330.2S3.821 I Rap: 330.253.4489 p,ige _�oi�. SE I' No.
coo, a, - N: n (Pleaw Pdm) I r.leer Nalw - Analytical Pal"Im{rtcls and Methods
/'lvcks,JrllrtNL Z0 u
l'licnt Phnrte N�,.3 Repo" to ®. a
2 h m 1. nail 1'le, c l IIC�i� RGtiuils ✓ - Ouola N., •� q 0
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✓n/E Ida f�1 ---
S;nnpled byICheck if Ohio Vr\P camplcs ✓ ell
,c a y r r y natc "lime
li Snmpl@Identification ('ollecled Collected
0
Notc.JCouuucnts:
ht tail br Uide 1 uitc �t i k ci a
Roar Rcquc,tut I{, lyl i
White and yclt g ryi� ,:L� IJ ,u.� nrycory uqd.. i� h I,bu,ni�n

oc-;
Rat. 14
CZ1S'15
Summit Environmental Technologies, Inc,
Cooler Receept Form
initials of person inspecting c/ooler andfsamples:
C<Z-
TenG :� "'''�� f C�/ i t �i r� t,l
Order Number. O
Date Rece-wed:—.- )� )L(4 Time Received: Date cooher(s) opened and samples Inspected�Gp
Number of CooferyBoxes: NIA
Shipper. F'Ep!•� UPS DHL Airborne VS Postal Walk-ln pickup P Other._—_
Packaging: P nu gunwrd,,.,2p blap r Foam None gg5j J
Tape on cooler/box �- � N NIA
Custody Seals Intact Y
N
C-O-C in plastic ,- _
!ce_ Blue ice present / tn5;n / melted N/A _-
Sample Temperature tR Gun 4102292 CF D ' oC /S . v
C N;A
Radiological Testing Instrument seral#36t27 y ,,
(see page 2 forscan resuRs) cam' NIA
f Ted per sample for Radiological Testing, it sampee IS HOT, the Radiological Safety officer must be notified
Y
C-O-C filled out properly
N NIA
Samples in separate bags 4, / .
N- WA
Sample containers intact• N
WA
if no, &si broken samoiels7-
Sample label{s) ccmpiete (FD, date. eic.) � N
Label(s) agree wvjn C-O-C NIA
Y N N/A
Correct containers used / Y N
NIA
Sufficient sample received I N
VV WA
Samples received within holding time LYV N
Bubbles absent from 40 mL vials^ y
N A
"Samples with bubbles <6mm are acceptable. Indicate bubble size if>6mm.
Was C:O!n: contacted about samples y N
Vt CF4nt send new samples Y N
Client mntacb
Logged in
Page 1 of 2
Page 10 of 10

Summit Environmental Technologies, Inc,
3310Win St.
P;VIz4NFeiEtTL E l.,bLC�, s,trsG Cuyahoga Falls, Ohio44223
TEL: [phone] FAX.- [phone]
Website: hgp://www.settekcom
February 10, 2016
Nate Roth
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: South Durham
Dear Nate Roth:
Order No.: 16011606
Summit Environmental Technologies, Inc_ received 1 sampleks) on 1/28/2016 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Bachar Najm
Project Manager
3310 Win St,
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA. Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.S, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank)
3, Kentucky 90146, Louisiana 04061 and LAI2004A Maine 2012015, Maryland 339, Massachusetts M-OPH9231 Minnesota 409711, Montana CERT0099,
New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631. Ohio Drinking Water 4170. Ohio VAP CL0052, Oklahoma
9940, Oregon 01-12O0001, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L,
USDA/APHIS 1?330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 8

Summit Environmental Technologies, Inc. �1 3310 Win sr. Case Narrative
arrative
dInONPetE�Ts5.L 7_....:,lO aho , L3G._>.� uy ga Falls �tG- C Ohio 44223 Wp�: 16011606
„, .wna.7yt C2i L ccr,>r,r;aa. _
T EL• . 330 2�3 _ � _ ( 8 11 FAX- 330 _53 ( 4489
Website: ham://www settek com Date: 2/10/2016
CLIENT: Synagro
Project: South Durham
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the %dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting /certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 2 of 8

j 'm Val Sunmeit Environmental Technologies, in Qualifiers and Acronyms
vi�1 �L 3310Winw
FP?VIRO WhI EA'TAL iZ&t:O LaG. 35,.;rC Cuyahoga Falls, Ohio 4422 WO16011606 tSraiyrical iai;cea_ro:•;es TEL: [phone] FAX.' (330) 253-446
Website: htto://wwwsettekco Date: 2/10/2016
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit,
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in thi
list or for additional information regarding the use of these Qualifiers on reported data. s
Original
Page 3 of 8

CLIENT:
Project:
L
My
P
S Summit'Environmentallechnologies, Inc.
3310 Win St.
^ONP1FtiTAL Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX,- [phone]
Website: hhta:Ilwwwsettekcom
Synagro
South Durham
Workorder
fox
1 16
• 16011606
Lab SampleID Client Sample ID Taa No Date Collected Date Received lyI
Matrix
16011606-001 South Durham
1/26/2016 1:30:00 PM 1/28/2016 9:55:00 AM Sludge
Page 4 of 8

Summit Environmental Technologies. Inc.
"A Analytical Report
11 �s 3310 Win St.
Cuyahoga Falls, Ohio 44293 (base report)
-^M ^•��':'''='�!'=-=dcr.'r�."+as TEL: [phone] FAX., [phone] WO#: 16011606
Website: http://wwwsettekcom Date Reported: 2/10/2016
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/26/2016 1:30:00 PM
Lab ID: 16011606-OOIA
Project: South Durham
Client Sample ID South Durham
Analyses Result RL Qual Units DF Date Analyzed
RCI. SW9045D Analyst: DHC
PH (SW9045D)
pH 8,01 s.u. a20.3C 1 1/29/2016 10:30:00 AM
Qualifi¢rs: * Value exceeds Maximum Contaminant LcveL E Vatuc above quantrtatiov range
H Holding t®es for prcpamtiov or analysis exceeded M Maoual integration used m determine area rpponse
MC Value is be]ow Minimum Compound Limit. N Tentatively idemi5ed compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDSmit
P Second column con5rmationexceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
U Samples with CaleVal< MDL 7 Anal detected below yte gnantitatinn its Page 5 of 8

y r Summit Environmental Technologies, Inc. WO#: 16011606
w�» � II iiz I T 3310 Win St.
,.,,.IRON➢,tE..7Al +tC":..O LC ;.._5, c,C Cuyahoga Falls, Ohio 44223 Date Reported: 2/10/2016
?i,-afyBcai iaror�ro:^e, TEL: [phone] Fi1X.- [phone] Company: S o
P Y= Yn�
Website: hL2Z1www settek rom
Address: 284 Boer Rd.
Mocksville NC 27028
Received: 1/28/2016
Project#: South Durham
TCLP Metals Analysis (6010)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
South Durham 001 1/26/2016 TCLP Arsenic(As) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 1/29/2016 WK
South Durham 001 1/26/2016 TCLP Barium(Ba) 5.00 ND mg/L Sludge EPA 6010 C 1 100 1/29/2016 WK
South Durham 001 1/26/2016 TCLP Cadmium(Cd) 0.100 ND mg/L - Sludge EPA 6010 C 1 1.00 1/29/2016 WK
South Durham 001 1/26/2016 TCLP Chromium(Cr) 0.200 ND mg/L Sludge EPA 6010 C 1 5.00 1/29/2016 WK
South Durham 001 1/26/2016 TCLP Lead(Pb) 0.500 ND mg/L Sludge EPA 6010 C 1 5,00 1/29/2016 WK
South Durham 001 1/26/2016 TCLP Selenium(Se) 0.500 ND mg/L Sludge EPA 6010 C 1 1.00 1/29/2016 WK
South Durham 001 1/26/2016 TCLP Silver(Ag) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 1/29/2016 WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab EW Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
South Durham 001 1/26/2016 TCLP Mercury 0.00500 ND mg/L Sludge EPA 7470 A 1 0.200 2/5/2016 MFW
SVOC SW-846: 8081-TCLP Pesticides
client iD# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
South Durham 001 1/26/2016 Chlordane, total 0.0250 ND mg/L Sludge EPA 8081 B 1 0.0300 2/8/2016 JBN
South Durham Vol 1/26/2016 Toxaphene 0.0500 ND mg/L Sludge EPA 8081 B 1 0.500 2/8/2016 JBN
South Durham 001 1/26/2016 Endrin 0.00250 ND mg/L Sludge EPA 8081 B 1 0.0200 2/8/2016 JBN
South Durham 001 1/26/2016 gamma-BHC 0.00250 ND mg/L Sludge EPA 8081 B 1 0.400 2/8/2016 JBN
South Durham 001 1/26/2016 Heptachlor 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 2/8/2016 JBN
South Durham 001 1/26/2016 Heptachlor epoxide 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 2/8/2016 JBN
South Durham 001 1/26/2016 Methoxychlor 0,00250 ND mg/L Sludge EPA 8081 B 1 10.0 2/8/2016 JBN
VOC by GC/MS (8260)-TCLP
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
South Durham 001 1/26/2016 1,1-Dichloroethene 0.100 ND mg/L Sludge EPA 8260 B 1 0.700 1/29/2016 MES
South Durham 001 1/26/2016 1,2-Dichloroethane 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
South Durham 001 1/26/2016 MEK 2.00 ND mg/L Sludge EPA 8260 B 1 200 1/29/2016 MES
South Durham 001 1/26/2016 Benzene 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
South Durham 001 1/26/2016 Carbon tetrachloride 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
South Durham 001 1/26/2016 Chlorobenzene 0.100 ND mg/L Sludge EPA 8260 B 1 100 1/29/2016 MES
South Durham 001 1/26/2016 Chloroform 0.100 ND mg/L Sludge EPA 8260 B 1 6.00 1/29/2016 MES
South Durham 001 1/26/2016 Tetrachloroethene 0.100 ND mg/L Sludge EPA 8260 B 1 0.700 1/29/2016 MES
South Durham 001 1/26/2016 Trichloroethene 0,100 ND mg/L Sludge EPA 8260 B 1 0.500 1/29/2016 MES
South Durham 001 1/26/2016 Vinyl chloride 0.200 ND mg/L Sludge EPA 8260 B 1 0.200 1/29/2016 MES
Page 6 of 8

k Summit Emironmenial Technologies, Inc. fag WO#: 1601160E
N , ova" i v 3310 Win St.
'� ry .gnONriE J7tL c... oLC ,as, lrzc Cuyahoga Falls, Ohio 44223 Date Reported: 2/10/2016
,drayt;"cai LsaaraiodJe3. TEL: [phone] FAX. [phone] Company: Synagro
Website.• hLQL: /www settek com Address: 28
4 Boger Rd,
Mocksville NC 27028
Received: 1/28/2016
Project#: South Durham
SVOC 8270 TCLP BNA List
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
South Durham 001 1/26/2016 1,4-Dichlorobenzene 0.200 ND mg/L Sludge EPA 8270 C 2 7.50 2/2/2016 BAV
South Durham 001 1/26/2016 2,4,5-Trichlorophenol 0.500 ND mg/L Sludge EPA 8270 C 2 400 2/2/2016 BAV
South Durham 001 1/26/2016 2,4,6-Trichlorophenol 0,600 ND mg/L Sludge EPA 8270 C 2 2.00 2/2/2016 BAV
South Durham 001 1/26/2016 2,4-Dinitrotoluene 0.200 ND mg/L Sludge EPA 8270 C 2 0.130 2/2/2016 BAV
South Durham 001 1/26/2016 Cresols, Total 10.0 ND mg/L Sludge EPA 8270 C 2 200 2/2/2016 BAV
South Durham 001 1/26/2016 Hexachloro-1,3- 0.200 ND mg/L Sludge EPA 8270 C 2 0.500 2/2/2016 BAV
butadiene
South Durham 001 1/26/2016 Hexachlorobenzene 0.200 ND mg/L Sludge EPA 82700 2 0.130 2121201E BAV
South Durham 001 1/26/2016 Hexachloroethane 0.200 ND mg/L Sludge EPA 8270 C 2 3.00 2/2/2016 BAV
South Durham 001 1/26/2016 Nitrobenzene 0,200 ND mg/L Sludge EPA 8270 C 2 2.00 2/2/2016 BAV
South Durham 001 1/26/2016 Pentachlorophenol 0.500 ND mg/L Sludge EPA 8270 C 2 100 2/2/2016 BAV
South Durham 001 1/26/2016 Pyridine 0.500 ND mg/L Sludge EPA 8270 C 2 5.00 2/2/2016 BAV
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
South Durham 001 11261201E 214-D 5.00 ND mg/L Sludge EPA 8321 A 1 10,0 2/9/2016 BJH
South Durham 001 1/26/2016 21475-TP 0.500 ND mg/L Sludge EPA 8321 A 1 1.00 2/9/2016 BJH
Page 7 of 8

=E ! Summit EnvirooMental Technologies, Inc.
WO#: 16011606
3310 W n St.
LI ON�PIF VT'LL Y.�OU]> Cuyahoga Falls Ohio 44223 Date Reported: 2/10/2016
TLTI I'r fir'=� L'�o''-3ta"/�z TEL: [phone] FAX: [phone] Company: S a o
Website: httn://www.setlrkccm P 84
Address: 284 Boer Rd,
Mocksville NC 27028
Received: 1/28/2016
Project#: South Durham
Client ID# Lab ED# Collected Analyte Result Units Matrix Method DF RL Run Analyst
South Durham 001 1/26/2016 Flashpoint (140°F) >140 OF Sludge EPA 1010 1 1/29/2016 TAH
South Durham 001 1/26/2016 Cyanide, Reactive ND mg/Kg Sludge EPA 9014 1 0.500 2/1/2016 MS
South Durham 001 1/26/2016 Sulfide, Reactive ND mg/Kg Sludge EPA 9034 1 25.0 2/1/2016 MS
Pale 8 of 8

Summit Envilonment.411 Technologies, }nc. l nal gig like(Illest/Ch`i11 of Ca15%Ody
3310 Will stleel Fol Summit [invironnlunlul'lichnulugie�, lua u�c unl)
(uulhugu Falk, Ohio 4422 i O: 310,>51.321 1 Fax: [phone] I'nec of� SF..f \0 1
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Summit Environmental Technologies, Inc.
Cooler Receipt Form
Initials of person inspecting)1 cooler and
samples: � Client" ,_ I` 0 Y
,../ Order Number. L
Date Received:__ ! G Time Received: i, ` —
Date cooler(s) opened and samples inspecteu.
Number of Coo[ers1$oxes:
--�----- NIA
Shipper. FF� UPS OHL Airbome U$ Pcstal Walk-in Pickup P Other.
Packaging: P nur gubh�f€
P EDp4'r Foam None �i
Tape on cooter/b= �---
/ N NIACusandy Seats intact
C-O-C in plastic Y N 69
Y fce__ Blue ice d, � WA
,,���
present ! 6e: t / melted NIA
Sample Temperature IR Gun *t 60 9tg CF ,C _ f s•y ,
C wA
(see page 2 Testing InStrument serial 1 7 Y
(see page 2 forscan results] N/A
Use she9t per sample for Radfologleat TesUrg, Pf
Immedlat9ly, sample is HOT, the Radiological Safety Officer must be notiflod
C-O-C filled out properly ¢/
N N/A
Samplesin separate bags
N N/A
Sample containers intact
N N/A
If no, list broken samolPr<1,
Sample Pabei{sy eamalefe (ID, safe, etc)
N Label(s) agree with C-OC NIA
Y
L� N N/A
Correct containers used Y '
L/ N . NIA
Sufficient sample received j
1 N N/A
Samples received within holding time
N
$ubbl s absent from 40 mL vials^ �,,r
Y N LV -' Samples with bubbles <6mm are acceptable. Indicate bubble size if>5mm,
Was dient contacted about samph_s Y
N
Will Client send new samples Y
N
Logged to
Page a of 2

Enviromnenial Zechnologies, Inc.
3310 Win St.
q ON141E T L CXU0LC 5, c Cuyahoga Falls, Ohio 44223
' �krary+,-� .-.,ra arorles TEL: [phone] FAX., [phone]
Website: htI2:11www cettekcom
February 28, 2018
Clay Fisackerly
Synagro
284 Boger Rd-
Mocksville, NC 27028
TEL: [phone]
FAX: (336) 99M450
RE: Durham Brown
Dear Clay Fisackerly:
Order No-: 18011276
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/26/2018 for the
analyses presented in the following report,
Therewere no problems with the analytical events associated with this report unless noted
in the Case Narrative,
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call th
laboratory. e
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St,
Cuyahoga Falls, Ohio 44223
Arkansas 83-0735, California 07256CA, Colorado, Comecticut PH-0108, De]aware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Dlinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kenmcky 90146, Louisiana 04061, Maryland 339, Minnesota
4097] I, New Hampshire 2996, New jersey OH006, New York 11777, North Carolina 39705 and 631. North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-I1-5, Utah OH00923201 M, Virginia VELAP 9456, Washington
C891
Page 1 of 29

ci "'""' Summit Environmental Technologies. Inc. �p7
n 3310Win St, Case Narrative
Sra dIA0NP.9EP:TikL `_c#CdOLf�GdPS; 1Fzc, Cuyahoga Falls, Ohio 44223
.�,ra6yE^ai L rcrara-;�;c TEL: [phone] FAX.. [phone] w04: 18011276
Website: httnZL/ .,cette4com Date: 2/28/2018
CLIENT: Synago
Project: Durham Brown
WorkOrder Narrative:
18011276: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditation/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This reportis believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
18011216-001 a tclp-svoc-cpest(808lb): The associated MS and MSD pair exhibited high RPDs for all
analytes of interest; spike recoveries were acceptable.
18011276-00IA SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in the
LCS.
Analytical Sequence QC Notes:
CCV rr 6637 20PP tclp-voc-mstr_tclp(82601: The TCLP-VOC CCV (Batch R80303) exhibited high
recovery for Method -Specified CCC Vinyl chloride; All samples were ND for Vinyl chloride. All other
Method. Specified CCCs and SPCCs exhibited control.
Orin nal
Page 2 of 29

Summit Environmental Technologies, Inc.
E , I 3310 Win St. Case Narrative
�j - InO NY1E+.TAL 6 OLr �S, wc. Cuyahoga Falls, Ohio 44223
li drarftf....i i„n�rsrp.r,es TEL: [phone] FAX.- (330) 2534489 WD#' 18011276
Website: ha2:11 w_ wsettekco Date: 2/28/2018
CLIENT: Synagro
Project: Durham Brown
18011276-001amsd tclp-svoc-cpest(8081b): The Pesticide TCLP Sample MS and MSD pair exhibited
high RPDs for all analytes of interest; The MS and MSD exhibited results within the acceptance limits
for all analytes of interest individually.
Original
Page 3 of 29

S11171/17 t Emironmenlal Technologies. In
't'41ma il�'C° 3310 Win 5
Iff l +IR0 NM E NTAL: . NO L6G;ES 'C Cuyahoga Falls, Ohio 442I
P .4ra;yGrai Larcrsr�.•;ec TEL: [phone] FAx..- (330) 253446
Website: horn Iwww settek co
Qualifiers and Acronyms
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
WO#: 18011276
Date: 2/28/2018
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+),
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
1CV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly ufilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that no not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 29

S - M Summit Environmental Technologies, Inc. VV ®ik®PClei'
3310 Win St. ll
IRONYS�+.7AL OL S r.'G Cuyahoga Falls. Ohio 44223 Sample Summary
TEL: [phone] FAX.• [phone]
WOE: 18011276
Website: htfn//www cen kcom
2XFeb-I8
CLIENT: Synaa o
Project: Durham Brown
Lab SampleID Client Sample ID Tag No Date Collected Date Received
Matrix
18011276-001 Durham Brown TCLP 2018 1/24/2018 11:40:00 AM 1/26/2018 9a0:00 AM
Sludge
Page 5 of 29

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Summit Environmental Technologies, Inc.
Air 3310Win St. Analytical Report
lFWO ROWol E NTAL 3E OLD 'c5 ;'coO Cuyahoga Falls, Ohio 44223
a (base report)
^••�rrr..aa Lzbcralo"� TEL: [phone] FAX: [phone] WO#: 18011276
Website: htmLALwwse re y t k
com Date Reported: 2/28/2018
CLIENT:
Matrix:
Synagro
SLUDGE
Lab M 18011276-OOIA
Project: Durham Brown
Client Sample 1D Durham Brown TCLP 2018
Analyses
Result
Tag Number:
Collection Date: 1/24/2018 11:40:00 AM
RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERBSOLID SW7470A SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury ND 0.00200 mg/L 1 2/8/2018 10:27:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D Analyst: KMS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 2/7/2018 1:04:36 AM
TCLP Barium(Ba) ND 5,00 mg/L 1 2f7/2018 1:04:36 AM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 2/7/2018 1:04:36 AM
TCLP Chromium(Cr) ND 0.200 mg/L 1 2/7/2018 1:04:36 AM
TCLP Lead(Pb) ND 0.500 mg/L 1 2/7/2018 1:04:36 AM
TCLP Selenium(Se) ND 0.0500 mg/L 1 2/7/2018 1:04:36 AM
TCLP Silver(Ag) ND 0.500 mg/L 1 2f7/2018 1:04:36 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.0800 mg/L 2 2/9/2018 6:58:00 PM
2,4,5-Trichlorophenol ND 0.200 mg/L 2 2/9/2018 6:58:00 PM
2,4,6-Trichlorophenol ND 0.200 mg/L 2 2/9/2018 6:58:00 PM
2,4-Dinitrotoluene ND 0,0400 mg/L 2 2/9/2018 6:58:00 PM
o-Cresol ND 0.200 mg/L 2 2/9/2018 6:58:00 PM
m/p-Cresol(s) ND 0.200 mg/L 2 2/9/2018 6:58:00 PM
Cresols, Total ND 4.00 mg/L 2 2/9/2018 6:58:00 PM
Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 2/9/2018 6:58:00 PM
Hexachiorobenzene ND 0.0400 mg/L 2 2/9/2018 6:58:00 PM
Hexachloroethane ND 0.0800 mg/L 2 2/9/2018 6:58:00 PM
Nitrobenzene ND 0.0800 mg/L 2 2/9/2018 6:58:00 PM
Pentachlorophenol ND 0.200 mg/L 2 2/9/2018 6:58:00 PM
Pyridine ND 0.200 OL- mg/L 2 2/9/2018 6:58:00 PM
Surr: 2-Fluorophenol 57.9 10 - 109 %Rec 2 2/9/2018 6:58:00 PM
Surr: Phenol-d6 28.4 10 - 109 %Rec 2 2/9/2018 6:58:00 PM
Surr: Nitrobenzene d5 99.1 19 - 120 %Rec 2 2/9/2018 6:58:00 PM
Surr. 2,4,6-Tribromophenol 71.8 10 - 120 %Rec 2 2/9/2018 6:58:00 PM
Surr: 2-Fluorobiphenyl 89.9 22 - 117 %Rec 2 2/9/2018 6:58:00 PM -
Qualifiers: "' Value exceeds Maximum Contaminant Level, E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 29

iSummit Environmental Technologies, Inc,m
MIT 3310Win St. Analytical Report
p I ONF iG�TxL OLxn :ES.NtC Cuyahoga Falls, Ohio 44223 (base report)
TEL: [phone] FAX., [phone] W04: 18011276
Website: http://www settekco Date Reported: 2/28/2018
CLIENT:
Matrix:
Synagro
SLUDGE
an M 18011276-001A
Project: Durham Brown
Client Sample ID Durham Brown TCLP 2018
Analyses
Tag Number:
Collection Date: 1/24/2018 11:40:00 AM
Result RL Qual Units
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14 99.2 34 - 116
NOTES:
Possible low bias for Pyridine due to low recovery in the LCS.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW131118081)
SW8270D
%Rec
SW8081
DF Date Analyzed
SW3510C Analyst: BJH
2 2/9/2018 6:58:00 PM
SW3510C Analyst: JBN
Chlordane, total ND 0.0200 m /L
9 2 2 7/2018 9:35:00 PM
Toxaphene ND 0.0400 mg/L 2 2/7/2018 9:35:00 PM
Endrin ND 0.00200 QMR mg/L 2 2/7/2018 9:35:00 PM
gamma-BHC ND 0.00200 QMR mg/L 2 2/7/2018 9:35:00 PM
Heptachlor. ND 0.00200 QMR mg/L 2 2/7/2018 9:35:00 PM
Heptachlor epoxide ND 0.00200 QMR mg/L 2 2/7/2018 9:35:00 PM
Methoxychlor ND 0.00200 QMR m /L
9 2 2/7/2018 9:35:00 PM
Surr. TCMX 74.1 10 - 119 %Rec 2 2/7/2018 9:35:00 PM
Surr. DCB 46.6 10 - 119 %Rec 2 2/7/2018 9:35:00 PM
NOTES:
The associated MS and MSD pair exhibited high RPDs for all analytes of interest; spike recoveries were acceptable.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: JBN
TCLP HERBICIDES ANALYSIS (SW1311/8151)
274-D ND 1.00 mg/L 1 2/20/2018 4:30:00 PM
21415-TP ND 0.500 d mg/L 1 2/20/2018 4:30:00 PM
Surr: DCAA 89.3 20- 140 %Rec 1 2/20/2018 4:30: 00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst: MES
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.0500 mg/L 10 2/6/2018 8:06:00 PM
1,2-Dichloroethane ND 0.0500 mg/L 10 2/6/2018 8:06:00 PM
MEK 1.83 0.250 mg/L 10 2/6/2018 8:06:00 PM
Benzene ND 0.0500 mg/L 10 2/6/2018 8:06:00 PM
Carbon tetrachloride ND 0,0500 mg/L 10 2/6/2018 8:06:00 PM
Chlorobenzene ND 0.0500 mg/L 10 2/6/2018 8:06:00 PM
Qualifiers: Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits Original
p e1'y RL Reporting Detection Limit
Page 8 of 29

'•�� , r - ,-�, Swnmit Environmental Technologies. Inc. 4., 7 7� I.
3310Win St, A)maly �Ec`[�Y dti�0�6
'11 ONPI�STAL OLu =_5 'C Cuyahoga Falls, Ohio 44223 (base report)
'•�+; -�•-+:.acre;ar. ac TEL: [phone] FAX., [phone] WO#:
18011276
Website: htta,-11 ww.,eeaekcom Date Reported: 2/28/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/24/2018 11:40:00 AM
Lab ID: 18011276-001A
Project: Durham Brown
Client Sample ID Durham Brown TCLP 2018
Analyses Result
TCLP METALS, VOC, BNA, PEST,
HERB -SOLID
TCLP VOLATILES ANALYSIS
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr:4-Bromofluorobenzene
104
Surr: Dibromofluoromethane
102
Surc Toluene-d8
106
RCI-SOLID-W! IGNITABILITY1030
REACTIVE CYANIDE (9014/7.3.3,2)-SOLID
Cyanide, Reactive ND
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
RCI-SOLID-W/ IGNITABILITY1030
PH (SW9045D)
pH 6.2
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
RL Qual Units
SW8260B
DF Date Analyzed
S V1311M Analyst: MES
0.0500
mg/L
10
2/6/2010 8:06:00
PM
0.0500
mg/L
10
2/6/2018 8:06:00
PM
0.0500
mg/L
10
2/6/2018 8:06:00
PM
0.0200 QC+
mg/L
10
2/6/2018 8:06:00
PM
70 .130
%Rec
10
2/6/2018 8:06:00
PM
70 - 130
% Rec
10
2/6/2018 8:06:00
PM
70 - 130
% Rec
10
216/2018 8:06:00
PM
Quali£ers: "` Value exceeds Maximum Contaminant Level.
H Holding times for prepazation or analysis exceeded
MC Value is below Minimum Compound Limit,
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
SW9014 Analyst: MS
0.500 mg/Kg 1 2/Z2018 3:16:00 PM
SW1030 Analyst: AJT
1 1/29/2018 3:00:00 PM
SW9045D Analyst: DHC
s.u.@20.00 1 Z1Z2018 12:00:00 PM
SW9034 Analyst: MS
25.0 mg/Kg 1 2/Z2018 3:16:00 PM
E Value above quantitation range
M Manua] Integration used to determine azea response
N Tentatively identified compounds
0 RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 29

FN Sum
_Summit Environmental Technologies, Inc.Accreditation Program
�OLCG„ 3310 Win
5t.
,rc Cuyahoga Falls, Ohio 44223 AnalyteS Report
+'raly ,cai Laorara..es TEL: [phone] FAX: [phone]
WO#: 18011276
Website: http://www.,veitek.co
28-Feb-18
Client: Synagro State: NW
Project: Durham Brown Program Name: NC_WW_SCM
Sample ID Matrix Test Name
Analyte Status
1 $011276-OOlA Sludge Ignitability of Solids(SW-846:1030) Ignitability A
Sludge pH(SW9045D)
Hydrogen Ion (pH) A
Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U
Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Sludge TCLP Herbicides Analysis (SWlill/8151) 2,4,5-TP A
Sludge TCLP Herbicides Analysis (SWlill/8151) 214-D q
Sludge TCLP Herbicides Analysis (SWli 11/8151) DCAA A
Sludge TCLP Mercury Analysis (SW 1311/7470) Mercury A
Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis (SW1311/6010) Barium A
Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis (SWli 11/6010) Chromium A
Sludge TCLP Metals Analysis (SWli 11/6010) Lead q
Sludge TCLP Metals Analysis (SW131116010) Selenium A
Sludge TCLP Metals Analysis (SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis (SW131 1/8081) 2,2%3.3%4,4%5,5%6,6'- A
Decachlorobiphenyl
Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A
Sludge TCLP Pesticides Analysis (SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis (SW131 1/8081) gamma-BHC q
Sludge TCLP Pesticides Analysis (SW13 11/808 1) Heptachlor A
Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis (SW1311/808 1) Tetrachloro-m-xylene A
Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis (SWL311/8270) 1,4-Dichlorobemene A
Sludge TCLP Semi-Volatiles Analysis(SWI 311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW 1311/8270) 2,4,6-Tribromophenol A
Sludge TCLP Semi-Volatiles Analysis(SWI 311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW13 11/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2-Fluorobiphenyl A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorophenol A
NC_WW_SCM A Accredited NC_WW SCM U Unavailable
Original #1
Page 10 of 29

Summit Environmental Technologies. Inc. Accreditation Program
3310 Win St.
11nONs1GVTAL3 P�.OLGO �, Cuyahoga Falls, Ohio44223 Analyte$ Report
m a3ytrcai ise»xsra,-iec TEL: 330 ( ) 2 ,53-8211 FAX [phone] WO#: 18011276
Website: http:#/ .settelccom
28-Fe&18
Client: Synagro State: NW
Project: Durham Brown Program Name: NC_W W SCM
Sample ID Matrix Test Name
Analyte Status
1801127&001A Sludge TCLP Semi-Volatiles Analysis(SWI 311/8270) 2-Methylphenol A
Sludge TCLP Semi-Volatiles Analysis (SWI311/8270) 3,4-Methylphenol A
Sludge TCLP Semi-Volatiles Analysis (SW I311/8270) Cresols, Total
A
Sludge TCLP Semi-Volatiles Analysis (SWIM 1/8270) Hexachlorobenzene
A
Sludge TCLP Semi-Volatiles Analysis(SWI311/8270) Hexachlorobutadiene
A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane
A
Sludge TCLP Semi-Volatiles Analysis (SW 1311/8270 A
Nitrobenzene
Sludge TCLP Semi-Volatiles Analysis (SWI311/8270
Ni4obenzene-d5 A
Sludge TCLP Semi-Volatiles Analysis (SW I311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SWI311/8270) Phenol-d6
A
Sludge TCLP Semi-Volatiles Analysis (SWI311/8270) p-Tcrphenyl-d14 A
Sludge TCLP Semi-Volatiles Analysis(SWlill/8270) Pyridine
A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane
A
Sludge TCLP Volatiles Analysis 2-Butanone
A
Sludge TCLP Volatiles Analysis 4-Bromofluorobenzene A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride
A
Sludge TCLP Volatiles Analysis Chlorobenzene
A
Sludge TCLP Volatiles Analysis Chloroform
A
Sludge TCLP Volatiles Analysis Dibromofluoromethme
A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Toluene-d8
A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
NC_WW_SCM A Accredited NC_WW SCM U Unavailable
Original #1
Page 11 of 29

�a Summit Environmental Technologies, Inc.
m�:���ai' �� 3310 fyinSr. QC SUMMARY REPORT
t;il MONMENTAl TECHNOLOGIES, INC Cu}'nhoga Falls, Oltio 44223
._ _._ Ar>t lyl!_al l.gbaralorlrs TEL: [phone] E4X: [phone] WO#: 18011276
Website: hg2.//WUgV settek cop 28-Feb-18
Client: Synagro
Project: Durham Brown
BatchID: 30720
Sample ID ics 6638 20PPB SampType: LCS TestCode: tc[p-voc-mstr Units: mg/L Prep Date:
RunNo: 80303
Client ID: LCSS Batch ID: 30720 TestNo: SW8260B SW1311M Analysis Date: 2/6/2018
y SegNo: 1406740
Analyte Result PQL SPK value SPK Ref Val % REC Lowl-imil H]ghL]mil RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroelhene 0,0229 0.00500 0.0200 0 115 79A 131
1,2-Dichloroethane 0.0241 0.00500 0.0200
0 120 73.6 137
MEK 0.0955 0.0250 0.100
0 95.5 55.1 163
Benzene 0.0227 0.00500 0.0200 0 114 73A 132
Carbon tetrachloride 0.0228 0.00500 0.0200 0 114 63.7 139
Chlorobenzene 0.0207 0,00500 0.0200 0 103 72.3 139
Chloroform 0.0233 0.00500 0.0200 0 116 79.3 129
Tetrachloroethene 0.0192 0,00500 0.0200 0 96.0 56.2 187
Trichloroethene 0.0205 0.00500 0.0200 0 102 64.1 138
Vinyl chloride 0.0268 0.00200 0.0200 0 134 22.1 147
Surf:4-Bromofluorobenzene 51.7 50.00 103 80.4 126
Soft: Dibromo0uoromethane 51.6 50.00 103 70.3 125
Surr: Toluene-d8 53.6 50.00 107 82 117
Sample ID MB-30720 SampType: MBLK TestCode: tclp-voc-mstr Units: mg/L Prep Date: 2/5/2018 RunNo: 80303
Client ID: PBS Batch ID: 30720 TestNo: SW8260B SW1311M Analysis Date: 2/6/2018 SegNo: 1406858
Analyte Result PQL SPK value SPK Ref Val % REC LowLimit HighLimil RPD Ref Val % RPD RPDLimit Qua]
1,1-Dichloroethene ND 0.100
1,2-Dichloroethane ND 0.100
MEK ND 0.500
Benzene ND 0.100
Qualifiers: * Value exceeds Maximum Contaminant Level. B Arudyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minunum Compound Limit. ND Not Detected Original
P Second column confirmation exceeds - O RPD is greater than recovery
PI, Permit Limit R RPD outside acceptedd rerecovery limits
Page 12 of 29

'3 Summit Environmental Technologies, Inc.
g� 3310 Win St. QC SUMMARY REPORT
ENtIaONITNTAI TTGuJr0L00I $, INC Clp'ahoga Falls, Ohro 44223
AtOlyllval Ly6w3rwlor TEL:[phone] Fiff:[phone] WO#: 18011276
Website: h�:/hvulw settek tout 28-Feb-18
Client: Synagro
Project: Durham Brown
BatchlD:
Sample ID MB-30720 SampType: MBLK TestCode: tctp-voc-mstr Units: mg/L
Client ID: PBS Batch ID: 30720 TestNo: SW8260B SW1311M
Analyte Result PQL SPK value SPK Ref Val
Carbon tetrachloride ND 0,100
Chlorobenzene ND 0.100
Chloroform ND 0.100
Tetrachloroethene ND 0.100
Trichloroethene ND 0.100
Vinyl chloride ND 0.0400
Surr:4-Bromofluorobenzene 1020 1000
Surr: Dibromo0uoromethane 1000 1000
Surr. Toluene-d8 1050 1000
Sample ID 18011188.002aMS SampType: MS TestCode: tclp-voc-mstr Units: mg/L
Client ID: BatchQC Batch ID: 30720 TestNo: SW82608 SW1311M
Analyte
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Result PQL
SPK value SPK Ref Val
Prep Dale: 2!5/2018
Analysis Date: 2/6/2018
%REC LowLimit HighLimit RPD Ref Val
102
70
130
100
70
130
105
70
130
Prep Date:
Analysis Date: 2/6/2018
%REC LowLimit HighLimit RPD Ref Val
0.176
0.0500
0.200
0
88.0
39.9
160
0.215
0.0500
0.200
0
107
42.5
157
0.952
0.250
1.00
0
95.2
16.6
227
0.213
0,0500
0.200
0
107
38.1
155
0.150
0.0500
0.200
0
75.1
40.8
162
0.197
0.0500
0.200
0
98.4
35.7
168
0.214
0.0500
0.200
0
107
18.3
199
0.163
0.0500
0,200
0
81.5
10
261
30720
RunNo: 80303
SegNo: 1406858
%RPD RPDLimit Qual
RunNo: 80303
SegNo: 1406919
%RPD RPDLimit Qual
Qualifiers: " Value exceeds Maximum Contaminant Level. B Anall4e detected in the associated Method Blank E Value above quantitation range H Bolding tunes for preparation or analysis exceeded J Amtlyte detected below quantitation Limits
M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected
0 RSD is greaterrealer than RSDlimit
P Second column confirmation exceeds PI, Permit Limit R RPD outside accepted recovery limits
Original
Page 13 of 29

Summit Environmental Technologies, Irtc.
summov 3310IN17St. QC SUMMARY REPORT
@71VIHONt1rNTAl TfC14170L001 6 VC Cuyahoga Falls Otero 44223
Arulyllcnl Laborator p,5 TEL: [phone] FAX.. [phone] work: 18011276
Mebsite: &W.Wivww seltelrcoat
28-Feb-18
Client: Synagro -.
Project: Durharn Brown
Sample ID 18091188.002aMS SampType: MS
Client ID: BatchQC Batch ID: 30720
Analyte
Trichloroethene
Vinyl chloride
Surr: 4-Brom ofl uorobe nze ne
Surr. Dibromofluoromethane
Surr: Toluene-d8
TestCode: tclp-voc-mstr Units: mg/L
TestNo: SW8260B SW1311M
Bafc
I :
Prep Date:
Analysis Date: 2/6/2018
Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val
0.194 0.0500 0.200 0 97.0 23.8 175
0.197 0.0200 0.200 0 98.3 10 165
517 500.0 103 84.6 130
485 500.0 97.0 71.4 127
510 500.0 102 74.6 127
Sample ID 18011188-002aMSD SampType: MSD TestCode: tclp-voc-mstr units: mg/L
Client ID: BatchQC Batch ID: 30720 TestNo: SW8260B SW1311M
Analyte
Result PQL SPK value SPK Ref Val
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Brom ofl u o ro b e n ze n e
Surr: Dibromofluoromethane
Qualifiers:
Prep Date:
Analysis Date: 2/6/2018
30720
RunNo: 80303
SegNo: 1406919
%RPD RPDLimit Coal
QC+
RunNo: 80303
SegNo: 1406935
%RPD RPDLimit Qual
0.180 0.0500 0.200 0 90.0 39.9 160 0.176 2.13
0.212 0.0500 0.200 0 106 42.5 157 0.215 IA7
0.938 0.250 1.00 0 93.8 16.6 227 0.952 1.42
0.207 0.0500 0.200 0 103 38.1 155 0.213 3.10
0.147 0.0500 0.200 0 73.6 40.8 162 0.150 2.09
0.194 0.0500 0.200 0 97.0 35.7 168 0.197 1,43
0.207 0.0500 0.200 0 103 18.3 199 0.214 3.61
0.157 0.0500 0.200 0 78.6 10 261 0.163 3.69
0.185 0.0500 0.200 0 92.4 23.8 175 0.194 4.81
0.192 0,0200 0.200 0 95.8 10 165 0.197 2.63
503 500.0 101 84.6 130 0
499 500.0 99.7 71.4 127
0
* Value exceeds Maxhnum Contaminant Level. B Analyte detected in the associated Method Blank
H IIolding tunes for preparatiot or anal psis exceeded E Value above gitantitation range
7 J Analyte detected below gaantitation limits M Manual Lilegration used to detennvte
MC Value is below Minimum Compound Limit. ND Not Detected
P Second colanm continuation exceeds O RSD of greater than d recovery
t r
PL Permit Limn R RPD outside accepted recovep� limits
%REC LowLimit HighLimit RPD Ref Val
25
25
25
25
25
25
25
25
25
25
25
25
QC+
Original
Page 14 of 29
Analyte
Trichloroethene
Vinyl chloride
Surr: 4-Brom ofl uorobe nze ne
Surr. Dibromofluoromethane
Surr: Toluene-d8
TestCode: tclp-voc-mstr Units: mg/L
TestNo: SW8260B SW1311M
Bafc
I :
Prep Date:
Analysis Date: 2/6/2018
Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val
0.194 0.0500 0.200 0 97.0 23.8 175
0.197 0.0200 0.200 0 98.3 10 165
517 500.0 103 84.6 130
485 500.0 97.0 71.4 127
510 500.0 102 74.6 127
Sample ID 18011188-002aMSD SampType: MSD TestCode: tclp-voc-mstr units: mg/L
Client ID: BatchQC Batch ID: 30720 TestNo: SW8260B SW1311M
Analyte
Result PQL SPK value SPK Ref Val
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Brom ofl u o ro b e n ze n e
Surr: Dibromofluoromethane
Qualifiers:
Prep Date:
Analysis Date: 2/6/2018
30720
RunNo: 80303
SegNo: 1406919
%RPD RPDLimit Coal
QC+
RunNo: 80303
SegNo: 1406935
%RPD RPDLimit Qual
0.180 0.0500 0.200 0 90.0 39.9 160 0.176 2.13
0.212 0.0500 0.200 0 106 42.5 157 0.215 IA7
0.938 0.250 1.00 0 93.8 16.6 227 0.952 1.42
0.207 0.0500 0.200 0 103 38.1 155 0.213 3.10
0.147 0.0500 0.200 0 73.6 40.8 162 0.150 2.09
0.194 0.0500 0.200 0 97.0 35.7 168 0.197 1,43
0.207 0.0500 0.200 0 103 18.3 199 0.214 3.61
0.157 0.0500 0.200 0 78.6 10 261 0.163 3.69
0.185 0.0500 0.200 0 92.4 23.8 175 0.194 4.81
0.192 0,0200 0.200 0 95.8 10 165 0.197 2.63
503 500.0 101 84.6 130 0
499 500.0 99.7 71.4 127
0
* Value exceeds Maxhnum Contaminant Level. B Analyte detected in the associated Method Blank
H IIolding tunes for preparatiot or anal psis exceeded E Value above gitantitation range
7 J Analyte detected below gaantitation limits M Manual Lilegration used to detennvte
MC Value is below Minimum Compound Limit. ND Not Detected
P Second colanm continuation exceeds O RSD of greater than d recovery
t r
PL Permit Limn R RPD outside accepted recovep� limits
%REC LowLimit HighLimit RPD Ref Val
25
25
25
25
25
25
25
25
25
25
25
25
QC+
Original
Page 14 of 29

a `9 u m Summit Environmental Technologies Inc.
S QC SUMMARY REPORT
ENVIRONI RNTAl TCr'1tt10L0Gtc%;NC Cuyahoga Falls, Ohio 44223
Armlyllcst G,9borafaller TEL: [phone] FILY: [phone] WO#: 18011276
0 ebsite: ltup:/Avmnv settek coin
28-Feb-18
--
Client: Synagro —
Project: Durham Brown
BatehlD: 30720
Sample ID 18011 too-002aMSD SampType: MSD TestCode: tclp-voc-mstr Units: mg/L
Client ID: BatchQC Batch ID: 30720 TestNo: SW8260B SW1311M
Analyte
Sum Toluene-d8
Result PQL SPK value SPK Ref Val
516 500.0
Qnnlitiers: " Vahic exceeds Masinuun Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second colunut confimtation exceeds
Prep Date:
B Anal)4e detected in the associated Method Blank
J Anal}4e detected below gnantitation limits
ND Not Detected
PL Permit Limit
R
%RPD RPDLimit
0 25
B Value above r{uartli(a[ion range
M Mannat Integration used to determine
O RSD is greater than RSDlintit
R RPD outside accepted recovery limits
Qual
Original
Page 15 of 29

-V. - SammR Environmental Technologies, Inc.
��1�� 3310Win St. QC SUMMARY REPORT
ENVIHOMI5NTA1 TECHNOLOCHESF INC Cuyahoga Falls, Ohio 44223
Ar7t+lylfsa/(.a5�ra/arlc4 TEL: [phone] F41: [phone] WON: 18011276
Website: Liao://uww settek coin
-.- 28-Feh-18
Client: Synagro
Project: Durham Brown
BatchID: 30744
Sample ID 18011276.001ams SampType: ms TestCode: telp-svoc-epe Units: mg/L Prep Date: 2/6/2018 RunNo: 80413
Client ID: Durham Brown TCL Batch ID: 30744 TestNo: SW8081 SW3510C
Analysis Date: 217/2018 SegNo: 1412121
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit oust
Endrin 0.00553 0,00200 0.0200 0 27.6 20 157
gamma-BHC 0.00667 0.00200 0.0200 0 QMR
0
Heptachlor 33.4 22 137 QMR
.00566 0.00200 0.0200 0 28.3 24 121
Heptachlor epoxide 0.00571 0.00200 0.0200 0 28 5 27 121 QMR
Methoxychlor 0.00680 0.00200 0.0200 5.1 QMR
p
134.0 10 199 QMR
Sum TCMX 40,00 37.8 10 119
Surr. DCB 8,82 40.00 22.1 10 119
Sample ID 18011276-001amsd SampType: msd TestCode: tclp-svoc•cpe Units: mg/L Prep Date: 2/6/2018 RunNo: 80413
Client ID: Durham Brown TCL Batch ID: 30744 TestNo: SW8081 SW3510C
Analysis Date: 2/7l2018 SegNo: 1412122
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin 0.0103 0.00200 0.0200 0 51.3 20 157 30 R
. 599
0.00553 gamma-BHC 0.00981 0.00200 0.0200 0 49.0 22 137 0.00553 59.30 R
Heptachlor 0.00952 0.00200 0.0200 p
Heptachlor epoxide 0.0102 0.00200 0.0200 50.8 24 152 0.00566 50.9 30 R
0 63.8 27 199 0.00571 56.2 30 R
Methoxychlor 0.0128 0.00200 0.0200 0 63.8 10 199 0,00680 60.9 30 R
Surr. TCMX 20.1 40.00
NOTES: 50.3 10 119 0
DCB 12.9 40.00 32.2 10 119 0
The Pesticide TCLP Sample MS and MSD pair exhibited high RPDs for all analytes of interest; The MS
ndividually. and MSD exhibited results within the acceptance limits for all analytes of interest
i
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quaulitation range
II Holding times for preparation or analysis exceeded J Anal)4e detected below quantitation limits
MC Value is below Mini"", Compound Limit. ND Not Detected M Manuel realer Integration used to de[emiine
O RSD is greater than RSDlimit Original
P Second column confnnation exceeds PL Pernut Limit
R IZPD outside accepted recovery limits
Page 16 of 29

b ''` Summit Environmental Technologies, Inc.
Val a ofa m 331014finSt. QC SUMMARY REPORT
CNVIROKIENTAI Tf6tJU0L001 $, INC Cuyahoga Falls, 01do 44223
�, .... _ _ - �I rialyllcaf La6ar31orle:; TEL: [phone] F4X. [phone] WO#: 18011276
Mebsite: htlg.,11 vnqy settek cons 28-FeL-18
Clieut: Synagro
Project: DurhalnBrom Batcllll): 30768
Sample ID MB-30768 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM
Client ID: PBS Batch ID: 30768 TestNo: SW7470A SW7470A
Analyte Result PQL SPK value SPK Ref Val
TCLP Mercury ND 0.00200
Sample ID LCS-30768 SampType: LCS TestCode: HG_TCLP(74 Units: PPM
Client ID: LCSS Batch ID: 30768 TestNo: SW7470A SW7470A
Analyte Result PQL SPK value SPK Ref Val
TCLP Mercury 0.00406 0.00200 0.00400 0
Sample ID 18011527.001AMS SampType: MS TestCode: HG_TCLP(74 Units: PPM
Client ID: BatchQC Batch ID: 30768 TestNo: SW7470A SW7470A
Analyte Result PQL SPK value SPK Ref Val
TCLP Mercury 0.00456 0.00200 0.00400 0
Sample ID 18011527-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM
Client ID: BatchQC Batch ID: 30768 TestNo: SW7470A SW7470A
Analyte Result PQL
TCLP Mercury 0,00484 0.00200
Qualifiers: Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimuur Compound Limit.
P Second column confirmation exceeds
Prep Date: 2/7/2018 RunNo: 80370
Analysis Date: 2/8/2018 SegNo: 1410446
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[
Prep Date: 2/7/2018 RunNo: 80370
Analysis Date: 2/8/2018 SegNo: 1410447
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
102 80 120
Prep Date: 2/7/2018 RunNo: 80370
Analysis Date: 2/8/2018 SegNo: 1410455
%REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
114 75 125
Prep
Date:
2/7/2018
RunNo:
80370
Analysis
Date:
2/8/2018
SegNo:
1410456
SPK value SPK Ref ValLowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0.00400 0 121 75 125 0.00456 5.96 20
B Analyte detected in the associated Method Blank E Value above quantitation range
J Analyte detected below quantitation limits M Manual Integration used to detennine
ND Not Detected O RSD is greater than RSDlimit Original
PL Permit Lvnit R RPD outside accepted recovery limits
Page 17 of 29

Summit Eav„a,,»,e„talTeeh„aog,esS. QC SUMMARY REPORT
�� �R I4t' �� P71 �wz...r' ' w 3370 {ViminStt.
E.IIIHOMdFNTA1 T 61NOLO01 $, 1NC Cuyahoga Falls, Oh,o 44223
-.— _.. hrtulyllcnl Lvbarnlo,/, s TEL: [phone] FAX: [phone] WO#: 18011276
Website: bttU'11rmvrvsenekcoin 28-Feb-18
Client: Synagro
Project: DurhaniBrovn
BatchlD: 30768
Sample ID 18011527-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/7/2018 RunNo: 80370
Client ID: BatchQC Batch ID: 30768 TestNo: SW7470A SW7470A Analysis Date: 2/8/2018 SegNo: 1410456
Analyle Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[
Qualifiers: " Value exceeds Maxbnum Contaminant Level. B Analyte detected in the associated Method Blank
E Value above gimnlitation range
13 Holding limes for preparation or analysis exceeded J Analyle detected below quanlitation limits M Manual Integration used to determine
MC Value is below Mininnum Compound Limit. ND Not Detected Original
O RSD is greater than RSDlimil
P Second colunm confirmation exceeds PL Pemrit Limit R RPD outside accepted recovery limits
Page 18 of 29

�r Slannot Environmental Technologies, Inc. QC SUMMARY REPORT
m m
� 3310 iyina St.
ENVIRONIPAFtNTAL TECHNOLOGIES, INC CaJ'ahoga Falls, Ohio 44223
:... Analytical L.gbmdtarle-s TEL: [phone] FAX.- [phone] WOO: 18011276
Website: http 11wnaPsettek tort 28-Feb-18
Client: Synagro
Project: Durham Brown
BatchID: 30893
Sample ID mb-30893 SampType: mblk TeslCode: tclp-svoc-her Units: mg/L Prep Date: 2/9/2018
Sample ID Ics-30893 SampType: Ics TeslCode: tclp-svoc-her Units: mg/L Prep Date: 2/9/2018
Client ID: LCSS Batch ID: 30893 TestNo: SW8151A SW8151A Analysis Date: 2/20/2018
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
214-D ND 1.00 0.500 0 94.2 62.6 125
2,4,5-TP ND 0.500 0.500 0 91.0 52.5 128
Sum DCAA 499 500.0 99.9 20 140
QualiOm•s: ' Value exceeds Maximum Contaminant Level.
H Holding times for preparation or atalysis execeded
MC Value is below Minimum Compound Limit.
P Second colunm continuation exceeds
B fmal}4e detected in the associated Method Blank
J Analyte detected bcloty quantitation limits
ND Not Detected
PL Permit Limit
RunNo:
%RPD RPDLimit Qual
RunNo: 80862
SegNo: 1426790
%RPD RPDLimit
B Value ahove quantitation range
M Manual briegration used to detemtiue
O
Qual
Original
Page 19 of 29

Summit Environmental Technologies, Inc.
um331g0 FlSn St. QC SUMMARY REPORT
E7 VIHONIIf NTAI TECHNOLOGIES, i\C Cuyahoga Falls, Ohio 44223
-.-�. Arrulyllcaf L,aborstoNcs TEL: [phone] FAX: [phone] WO#: 18011276
JVebsile: _http.-//mtrw settelr cons
28-Feb-18
--
Client: Synagro — -
Project: Durham Brown
BatchID: 30893
Sample ID 18011410-001ams SampType: me TestCode: tclp-svoc-her Units: mg/L Prep Date: 2/9/2018
Client ID: BatchQC Batch ID: 30893 TestNo: SW8151A SW8151A Analysis Date: 212212018
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val
214-D ND 11.3 0.500 0 82.3 37 105
21415-TP ND 11.3 0.500
Surf: 2,4-Dichlorophenylacetic acid 451 0 90.2 38 140
500.0 90.3 20 140
Sample ID 18011410-001amsd SampType: msd Tea ode: tclp-svoc-her Units: mg/L Prep Date: 2/9/2018
Client ID: BatchQC Batch ID: 30893 TestNo: SW8151A SW8151A
Analysis Date: 2/22/2018
Analyte Result PQL SPK value SPK Ref Val %REC LoWLimit HighLimit RPD Ref Val
214-D ND 11.3 0.500 0 85.6 37 105 2,4,5-TP 0
ND 11.3 0.500 0 89.6 38 106 0
Sum 2A-Dichlorophenylaretic acid 481 500.0
96.2 20 140
Qualifiers: ° Value exceeds Maxinuun Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Cmnpound Limit.
P Second column continuation exceeds
B Analyte detected in the associated Method Blank
J Anal}1e detected below quanli[ation limits
ND Not Detected
YL Pemtit Limit
RunNo: 80998
SegNo: 1430808
%RPD RPDLimit Qual
HQC-
HQC-
H
RunNo: 80998
SegNo: 1430809
%RPD
RPDLimit
Qual
0
30
HQC-
0
30
HQC-
0
30
H
E Value above quantita[iou range
M Manual huegration used to determine
O RSD is greater than RSDhinil
R KPD outside accepted recovery limits
Original
Page 20 of 29

'`° MOIL"
Environmental Technologies, ]ae '
U 1� r 3310Win A QC SUMMARY REPORT
ENVIRONMENTAL TPCHNOLOOI S,;NB Cuyahoga Falls, Ohio 44223
A ovtyll 71 Lnboraforla•4 TEL: [phone] F.1X- [phone] WON: 18011276
Website: NW.Iluntroosetiek con
28-Feb-I8
Client: Synagro
Project: Durham Brown
BatchlD: R79971
Sample ID LCS-R79971 SampType: LCS
Client ID: LCSS Batch ID: R79971
Analyte Result
Ignitability 8.04
Qualifiers; * Value exceeds Maximum ContaminantLcvel-
H Holding tunes for Preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column continuation exceeds
TestCode: Ignitability_S Units:
TestNo: Sw1030
PQL SPK value SPK Ref Val
7.240 0
Prep Date:
Analysis Date: 1/2912018
REC LowLimit HighLimit RPD Ref Val
111 70 130
B Anal}4e detected in the associated Method Blaiilc
J Aualyte detected below gnantitaliou limits
ND Not Detected
PL Penuit Lunit
RunNo: 79971
SegNo: 1393806
%RPD RPDLimit Cual
E Vahte above quantitation range
M Manual Iunegntiou used to detemnine
O RSD is greater than RSDlhnit
R RPD outside accepted recovery limits
Original
Page 21 of 29

� c Sunrurit Environmental Technologies, Inc.
3310 IV,nSt.
QC SUMMARY REPORT
L JYIHONt1PNTJ11 ifCHtJOL9nl $, IMC Crryahoga Falls, Olno 44223
TI .4rt Iylcnl(.v oratorJor TEL: [phone] FkT(.[phone] woof: 18011276
If ebsrte: http //www settek co rr
.. 28-Feb-18
...
Bent: Synagro —
Project: Durham Brown
BatehfD: R80294
Sample ID MB-R80294 SampType: MBLK TestCode: Cyanide,Rea Units: mglL Pre Date:
p RunNo: 80294
ClientID: pBW
Batch ID: R80294 TestNo: SW9014
Analysis Date: 2/2l2018 SegNo: 1405936
Analyte Result PQL SPK value SPK Ref Val
%REC LovAimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS•R80294 SampType: LGS TestCode: Cyanide,Rea Units: mg/L Pre Date:
p RunNo: 80294
Client ID: LCSW
Batch ID: R80294 TestNo: SW9014
Analysis Date: 2/212018 Seq No: 1405938
Analyte Result PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 1.02 0.500 1.000 0 102 85 115
Sample ID 18011490-010AM5 SampType: MS TestCode: Cyanide,Rea Units: mg/L Pre Date:
80294
Client ID: BatchQC Batch ID: R80294 TestNo: SW9014 P SegRunNo: 14059
Analysis Date: 2/2l2018 SegNo: 1405941
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 1.08 0.500 1.000
0 108 81.3 118
Sample ID 18011410.010AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/L Pre Date:
Client ID: BafchQG Batch ID: R80294 TestNo: SW9014 P RunNo: 80294
Analysis Date: 2/2/2018 SegNo: 1405942
Analyte Result PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 1.04 0.500 1.000 0 104 81.3 118 1,084
3.76 5
Qualifiers: ° Value exceeds Maxinwm Contaminant Level. A Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded G Value above gnantitation range
7 J Analyle detected below quantitation limits M Manual Integration used to detemtine
MC Value is below Mininuun Compound Limit. ND Not Detected
O RSD is greater than o er Original Second column confirmation exceeds PL Permit Lunit
R RPD outside acceptedd recovery limits
Page 22 of 29

6 - T-' � Ssnnnit Environmental Technologies, Inc.
u r mall 0 1Vm Sf. QC SUMMARY REPORT
ENVIRON614NTAl TETW40L00i'S, INC Cuyahoga Falls Ohio 44223
dgnlyfleal L.gbQ) a/ot/t s TF.L: [phone] FifX.- [phone] WO#: 18011276
Website: hQ //ujmv sellek co n 28-Feb-18
Client: Syuagro
Project: Durham Brown
BatchED: R80294
Sample ID 18011410.090AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/L
Client ID: BatchQC Batch ID: R80294 TestNo: SW9014
Analyte
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 2/2/2018
REC LovrLimit HighLimit RPD Ref Val
Qualifiers; � Value exceeds btaxinmm Contaminant Level. B r1rml}1e detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minumum Compound Limit. ND Not Detected
P Second cultural continuation exceeds PL Permit Limit
RunNo: 80294
SegNo: 1405942
%RPD RPDLimit Dual
F, Value above quanti[atimi range
M Manual hnegration used to determine
O RSD is greater than RSDlimit
K RPD outside accepted recovery limits
Original
Page 23 of 29

i - ,� �� Summit Environmental Technologies, Gm.
.9mmmm 3310 l75n St. QC SUMMARY REPORT
EriVIHONIAFNTIq Tt•CHN0L901 $,i\C Cajahoga Falls, 01no 44223
Arnlyllc3l Lvb_ralop<:5 TEL: [phone]F y.-[phone] WO#: 18011276
lrebsite: hO.-Ilwmv settek can
28-Feb-18
Client: Synagro
Project: Dllrhaln Brown
BatchID: R80297
Sample ID MB•R80297 SampType: MBLK TestCode: Sulfide,React Units: mg/L
Client ID: PBW Batch ID: R80297 TestNo: SW9034
Analyte Result PQL SPK value SPK Ref Val
Sulfide, Reactive ND 25.0
Sample ID LCS•R80297 SampType: LCS TestCode: Sulfide,React Units: mglL
Client ID: LCSW Batch ID: R80297 TestNo: SW9034
Analyte Result PQL SPK value SPK Ref Val
Sulfide, Reactive 4670 25.0 4800 0
Sample ID 18011410.010AMS SampType: MS TestCode: Sulfide,React Units: ma
Client ID: BatchQC Batch ID: R80297 TestNo: SW9034
Analyte Result PQL SPK value SPK Ref Val
Sulfide, Reactive 4620 25.0 4800 0
Prep Date: RunNo: 80297
Analysis Date: 2/212018 SegNo: 1405979
%REC LOWLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Prep Date:
Analysis Date: 2/2/2018
%REC LowLimit HighLimit RPD Ref Val
97.3 85 115
Prep Date:
Analysis Date: 2/2/2018
%REC LowLimit HighLimit RPD Ref Val
96.2 75 125
RunNo: 80297
SegNo: 1405980
%RPD RPDLimit Coal
RunNo: 80297
SegNo: 1405982
%RPD RPDLimit Qual
Sample ID 18011410-010AMSD SampType: MSD TestCode: Suitide,React Units: tug/L Prep Date: Client ID: BatchQC RunNo: 80297
Batch ID: R80297 TestNo: SW9034
Analysis Date: 2/2/2018 SegNo: 1405983
Analyte Result PQL SPK value SPK Ref Val %REC LoWLimit HighLimit RPD Ref Val %RPD RPDLimit
Sulfide, Reactive 4410 25.0 4800 0 91.9 75 125 4620 4.65 30
Qualifiers: ' Value exceeds Maxinnun Contaminant Level. B Anal}1e detected in the associated Method Blank B
II Uolding tunes for preparation or analysis exceeded Value above quantitation range
S J Analyte detected below quantitation limits M Manua( Integration used to detemrinc
MC Value is below Minimum Compound Limit. ND Not Detected
P Second colunm confirmation exceeds C RSD is greater cepsthan d recovery
PL Pemtit Limit 12 APD outside accepted recovery limits
Qua
Original
Page 24 of 29

- Summit Environmental Technologies, Inc.
U& MN � 3310 Win St. QC SUMMARY REPORT
CNVIHONMENTAI TECHt OLOGI $, INC Cuyahoga Falls, Ohio 44223
.e, Arraly(lcal Labotatoijor TEL: [phone] FAX: [phone] WO#: 18011276
Mebsite: hnp-//wunv settek com 28-Feb-18
Client: Synagro
Project: Durham Brown
BatchfD: R80297
Sample ID
18011410.010AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R80297
Analyte
Result
TestCode: Sulfida,React Units: mg/L Prep Date: RunNo: 80297
TestNo: SW9034 Analysis Date: 2/2/2018 SegNo: 1405983
PQL SPK value SPK Ref Val % REC Lowt-imit Hight-imit RPD Ref Val % RPD RPDLiniit Qua]
Qualifiers: g Value exceeds Masinuun Contamutaut Level.
H Holding tunes for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column con6miation exceeds
B Anal}4e detected in the associated Medved Blank
J Aual}4e detected below quantitation limits
Nll Not Detected
YL Permit Limit
E Value above quantitation range
M Manual huegration used to delemtute
O RSD is greater than RSDlintit
R RPD outside accepted recovery limits
Original
Page 25 of 29

Suuvnil Environmental Technologies, Inc.
-I���-' 3310 IVirt St.
E tVIHOMid ENTAI TfCNt:OL001_$, iN0 Cuyahoga Falls, Ohio 44223
T-�e. Armlyllcal Laboratories TEL: [phone] FifX: [phone]
if ebsite: httD'//wtigr settek cam
Client: Synagro
Project: Durham Brown
Sample ID 18020385-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R80464
Analyle Result
pH 10.7
QC SUMMARY REPORT
WO#: 18011276
BatCI R80464
TestCode: pH_011(9045 Units: s.u.@21.8C Prep Date:
RunNo: 80464
TestNo: SW9045D Analysis Date: 2/12/2018
SegNo: 1413679
PQL SPK value SPK Ref Val %REC LowLimit Highl-imit RPD Ref Val %RPD RPDLimit Qual
0 0 10.7 0 10
Qualifiers: > Value exceeds Maxunnm Contaminant Level. B Fvral}4e detected in the associated Method Blank A Holding times for preparation or analysis exceeded J Anat}1e detected below quantitation Emits
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second colunm confirmation exceeds
PL Pemtit Lunil
E Value above quantitation range
M Manual Lmegration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 26 of 29

�gr��� ,��.7t t -. Stmmtit Fm)ironutental Technologies, hta QC SUMMARY REPORT
'.� � I 3310 Win St.
ENVIRONMENTAL TrCIJUOLOOI Sr AC Owahoga Falls, Oluo 44223
....,.,„. ..�mP rAnalyllc❑l LaboratorhF TEL: [phone] FAX [phone] WOH: 18011276
H ebsite: htta:/hnaw settek com 28-Feb-18
Client: Synagro
Project: Durham Brown BatchTD: R80464
Sample ID LCS•R80464 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@20.6C Prep Date: RunNo: 80464
Client ID: LCSW Batch ID: R80464 TestNo: SW9045D _ Analysis Date: 2/12/2018 SegNo: 1413497
Analyte Result PQL SPK value SPK Ref Val % REC Lovkimit HighLimit RPD Ref Val %RPD RPDLimit Qual
,.0
.3
r.0 u 101 98.6 101.4
Sample ID 18020179.001ADUP SampType: DUP TestCode: pH_NPW(450 Units: s.u.@19.2C Prep Date: RunNo: 80464
Client ID: BatchQC Batch ID: R80464 TestNo: SW9045D Analysis Date: 2/12/2018 SegNo: 1413499
Analyte Result PQL SPK value SPK Ref Val % REC Lowl-imit HighLimit RPD Ref Val % RPD RPDLimit Qual
..0
Qnalitiers: ° Vahte exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Mininuun Compotmd Limit.
P Second colunm confirmation exceeds
B Anal}1e detected in the associated Method Blank
J Analyte detected below quantitation limits
ND
Not Detected
PL Pennit Limit
11.2 0 5
E Value above quamitation range
M Mannal Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 27 of 29

;�y Snuim{I hirvlromnen/ol fea/rnolaglee. Gu.
2� QW0 t " M"' Y", f `" 4 3310 Win St.
1I ONh7ES7Al';c .0 .OLC., _5 Cuyahoga Falls, Ohio 44223
+�r %ri a i.rcraty es TEL: [phone]FAX' [phone] Sample Log -In Check List
Wehsite: Htrp•//www cettekcom
Client Name: SYN-NC-27028 Work Order Number. 18011276
RcptNo: 1
Logged by: Lori Douglas 1/26/2018 9:30:00 AM G)
Completed By: Christopher Livengood 1/26/2018 2:37:37 PM C
``LLa►t.�xr
Reviewed By: Jennifer Woolf 1/26/2018 6:11:54 PM r??*w
Chain of Custody
1. Is Chain of Custody complete? Yes 0 No
❑ Not Present ❑
z, How was the sample delivered? Fed Ex
Log In
3. Coolers are present? Yes No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present 7
No, Seal Date: Signed By:
5, Was an attempt made to cool the samples? Yes 0 No ❑ NA ❑
6. Were all samples received at a temperature of >06 C to 6.0°C Yes RI No ❑ NA ❑
7, Sample(s) in proper container(s)?
$, Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13, Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
8�ecial Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Person Notified:
Regarding:
Client Instructions:
18. (Additional remarks:
Cooler Information
Cooler No Tem
IS 4 n
Yes ❑ No ❑
Yes ❑ No 0
Yes No ElYes 0 No ❑
Yes No ❑
Yes 0 No ❑
Yes ❑ No ❑
Date
Va: ❑ entail ❑ Phone ❑ Fax
Seallntactj SeaIN � eal
NOt Present,
NA
NA
No VOA Vials ❑W
❑ In Person
Page 29 of 29
Date
Va: ❑ entail ❑ Phone ❑ Fax
Seallntactj SeaIN � eal
NOt Present,
NA
NA
No VOA Vials ❑W
❑ In Person
Page 29 of 29

SECTION 5

North & South Durham Sludge Fecal Coliform Analysis
2019 Summary
North Durham WRF
South Durham WRF

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQPermitNumber: WQ0003504
WWTPName: North Durham WRF
NPDES Number. NC0023841
Monitoring Period: From 01/01/19 To 02/28/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) _ Alt. 2/13 (Alk Treatment
_. Alt. 3/C (Prior Testing) —
Alt. 4/1) (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _
Alt. 6 (Equivalent to PFRP) —
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost — Heat Drying _ Heat Treatment _
Thermophilic _
Beta Ray — Gamma Ray — Pasteurization _
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens _
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization — Air Drying — Composting _ Aerobic Digestion
Anaerobic Digestion —
Parameter Allowable Level in Sludge ��' "" ` °`"'"" f°onrtorma data:
Pathogen Density No. of Frequency Sam 1,
P
Excee- of Type
Minimum Geo. Mean Maximum Units dences Analysis
Fecal 2x10to the 6th MPN 1278 4958 53892 MPN/g
Coliform power per gram of 0 Bi-monthly Grab
total solids
CFU ,,.,.,,
1000 MPN per graze of total
solids (dry weight)
Salmonella 3 MPN per 4 grams total
bacteria (in solids (dry weight)
lieu of fecal
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107)
Option/AltI I Option/Alt. 2
(VS reduction) X (40-day bench)
Option/Alt, 5 Option/Alt, 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9 Option/Alt. 10
(Injection) _ (Incorporation)
Technique
Please indicate option alternative performed:
Opti. 3 Option/Alt, 4
(30-day bberiench) (Spec. 02 uptake)
/Al _
Optiont. 7 Option/Alt. 8
(Drying —Stable) (Drying — Unstable)
CERTIFICATION STATEMENT (please check the appropriate statement)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15AtVCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503432/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/L5A KCAL 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly bather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment.' -
.John Dodson, Superintendent —North DurhamWRF
Prepazer Name and Title (print or type) Land Applier Name and Title if applicable)
/„i� ( PP ) (type or print)
gnature of Prepazer* L-//Daatt/ee Signature of Land APPTier (if applicable)
) Date
*Prepazer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T.1102 (26)
E

North Durham Water Reclamation Facility ;n
Sludge Report out
Jan '19
PRIMARY SLUDGE TO DIGESTER A PRIMARY SLUDGE TO DIGESTER - B
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons % Solids Lbs Dry % Vol Ibs VM
1 70,659 6 33,148 82 27,206 62,838 7.50 39,305 76.9 30,226
2 77,149 5.48 35,260 80.2 28,264 669870 7.40 41,269 81.2 33.519
3 71,160 5,00 29,674 78.0 23,131 70,715 8.35 49,245 80.1 39,421
4 60,777 5.70 28,892 81.9 23,666 73,750 8.50 52,281 82.9 43,315
TOTAL 279,745 5.55 1269973 80.5 102,267 2749173 7.94 1827101 80.3 146,481
WASTING TOTAL TO GBT
WEEK Gallons %Solitls Lbs Dry % Vol Ibs VM Gallons Ibs. D.S. Ibs. V.M.
1 1,240,181 1.50 155,147 65.5 101,621 1,232,116 154,138 1007960
2 11227,628 1.35 138,219 68.6 94,818 617,708 69,548 47,710
3 11222,663 1.93 196,292 69.6 136,669 1P031,422 165,590 1159292
4 11667,138 1.43 198,131 68.8 136,215 11594, 967 1899554 130,318
TOTAL 51357,610 1.55 687,789 68.1 4697323 4,476,213 578,829 394,280
ANAEROBIC SLUDGE TO PRESS TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM WEEK Gallons % Solids Lbs Dry % Vol Ibs VM
1 503,021 2.95 123,758 55.0 68,005 1 377,051 5.20 163,519 70.80 115,772
2 633,373 2.78 146,585 56.2 82,344 2 2469W 5.20 107,053 70.63 75,615
3 452,053 2.60 98,023 57.1 55,947 3 435,098 3.62 1319360 71.12 93,423
4 1,072,165 2.48 221,311 59.4 131,514 4 688,164 3.94 2267040 72,22 163,253
TOTAL 21660,612 2.70 589,677 56.9 337,810 TOTAL 11747,161 4.49 627,972 71.2 448,063
SOLIDS OFF PRESS
WEEK
Sum
Yds
%Solids
1
384
17.50
2
384
17.87
3
384
17.42
4
576
17,48
TOTAL
1728
17.57
Total Gallons to Anaerobic Dig. 2,301,079
Total Pounds of Dry Solitls to Anaerobic Dig. 937,046
Total Pounds of Vol. Solids to Anaerobic Dig. 696,810
Total Gallons from Anaerobic Dig. 21660,612
Total Ibs, of Dry Solids from Anaerobic Dig. 5897677
Total Ibs. of Vol. Solids from Anaerobic Dig. 337,810
Detention Time - Days 42
Gas Production 115487920
Ft3 of Gas Produced/lb of VM Added 2
% Reduction 52 (V)9 52 % (AMS)

North Durham Water Reclamation Facility
Sludge Report
Feb '19
PRIMARY SLUDGE
TO DIGESTER -
A
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
63,434
4
23,489
84
19,797
2
59,053
5.84
28,762
81.8
23,533
3
65,040
5.70
30,919
83.3
25,749
4
77,835
3.96
25,706
77.0
19,804
TOTAL
265,362
4.88
108,876
81.5
88,883
PRIMARY SLUDGE TO
DIGESTER - B
Gallons
% Solids
Lbs Dry
% Vol
281828
8.68
20,869
84.9
35,445
8.20
247240
85.3
71,992
3.88
23,296
87.2
671912
4,64
267280
84.3
2049177
6.35
94,685
85.4
in 76 %
out 60 %
Ibs VM
7,714
20,667
20,309
22,154
80,844
WASTING TOTAL
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons Bons Ibs. D.S. Ibs. V.M.
1 1,085,383 1.18 106,815 71.5 76,394 11071,451 1057444 75,413
2 1,119,679 1.12 104,587 71.9 75.156 1,066,025 99,575 71,555
3 11255,546 1,10 115,184 72.8 83,825 1,360,871 124,846 90,857
4 11225,577 1.10 112,434 72.9 81,987 1,0849798 99,519 72,570
TOTAL 476869185 1.13 439,020 72.3 317,362 47583,145 429,385 310,394
ANAEROBIC SLUDGE TO PRESS TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM WEEK Gallons % Solids Lbs Dry % Vol Ibs VM
1 647,428 2.64 142,548 59.3 84,531 1 3777735 3.72 117,192 73,01 85,562
2 539,956 2.58 116,183 59.4 69,036 2 353,563 4.44 130,849 73,99 96,812
3 711,921 2.28 135,076 60.9 82,261 3 406,965 3,64 123,545 74.63 92,201
4 690,365 2.36 135,880 60.7 82,452 4 334,245 3.76 104,734 74.66 78,192
TOTAL 2,589470 2.47 529,688 60.1 318,281 TOTAL 1,472,508 3.89 476,320 74.1 352,767
SOLIDS OFF PRESS
-
WEEK Yds %Solids
1 384 17.83
2 384 17.37
3 384 17.09
4 384 17.16
TOTAL 1536 17.36
SummaN
Total Gallons to Anaerobic Dig. 11942,047
Total Pounds of Dry Solids to Anaerobic Dig. 67g,882
Total Pounds of Vol. Solids to Anaerobic Dig. 522,494
Total Gallons from Anaerobic Dig. 2589,670
Total Ibs. of Dry Solids from Anaerobic Dig. 529,688
Total Ibs. of Vol. Solids from Anaerobic Dig. 318,281
Detention Time - Days 50
Gas Production 11557,103
Ft3 of Gas Produced/lb of VM Added 3
Reduction 53 (VX) 39 % (AMS)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQPermit Number: W
00003504
WWTP Name: North Durham WRF NPDES Number: NC002M41
Monitoring Period: From 03/01/19 To 04/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) _ Alt. 2B (Alk Treatment
Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _
Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying Heat Treatment Thermophilic _
Beta Ray _ Gamma Ray _ Pasteurization _
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens _
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Anaerobic Digestion
Composting Aerobic
_ Digestion
----
Pazameter
-- -- Al----•--• •- _• ��• •••_•. �.•as
lowable Level in Sludge
a or v,iass n com fete the following monitoring data:
Pathogen Density
No. of
Frequency
Sample
Analytical
Minimum Geo. Mean Maximum Units
Excee-
dences
of
Analysis
Type
Technique
Fecal
Coliform
2x10 to the 6`^ MPN
1402 22109 115942 MPN/g
0
Bi-monthly
Grab
9221 E
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
solids (dry weight)
N/o
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
ecrur nrrracnon Hetluction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction) X
Option/Alt. 5
(14-Day Aerobic)
Option/Alt, 9
(Injection)
Ophon/Alt. 2
(40-day bench)
Option/Mt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15AtVCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met.
aware that there are significant penalties for false certification including fine and imprisonment" I am
John Dodson, Superintendent —North Durham WRF
Prepazer Name and Title (print or type) Land Applier Name and Title if applicable) e or C PP ) (type print)
ignature of Prepazer* D Signature of Land Applier (if applicable)
*Prepazer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

North Durham Water Reclamation Facility in
Sludge Report out
Marl 9
PRIMARY SLUDGE TO DIGESTER m A PRIMARY SLUDGE TO DIGESTER B
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons % Solids Lbs Dry % Vol Ibs VM
1 76,718 5 33,399 77 25,804 67,808 6.52 36,872 81.4 30,006
2 68,497 5.28 30,163 81.9 24,715 67,808 6.64 377550 81.2 30,498
3 55,803 3,78 17,592 82.8 14,563 647669 5,14 27,722 79,2 21,945
4 82,429 3.32 22,801 78.8 17,971 849475 6,97 49,082 79.9 39,233
TOTAL 283,447 4.35 103,955 80,1 83,053 284,760 6.32 151,226 80.4 1217682
WASTING TOTAL TO GBT
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons Ibs. D.S. Ibs. V.M.
1 172307300 1.10 112,868 71.5 80,644 1,4105820 129,429 92,477
2 11388,981 1.18 136,692 69.5 95,056 193279543 130,646 90,851
3 1,3971908 1,13 131,159 71.9 94,336 11460,035 1367988 98,528
4 1,981,279 1.18 194,982 74.1 1449442 11727,989 170,055 125,977
TOTAL 5,998,468 1,15 575,700 71.8 414,478 5,926,386 567,117 407,833
ANAEROBIC SLUDGE TO PRESS TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM WEEK Gallons % Solids Lbs Dry % Vol Ibs VM
1 734,037 2.03 123,968 62.0 76,798 1 51%500 3.81 1657182 73.65 121,656
2 633,511 2.16 114,123 61.3 69,935 2 3639281 3.88 117,555 70.72 83,135
3 777,153 2.28 147,777 62.1 917711 3 447,444 4.24 158,330 73.67 116,644
4 868,491 2,30 1662594 61.9 103,155 4 480,035 4.34 173,866 71.86 124,935
TOTAL 3,013,192 2.19 552A62 61.8 341,598 TOTAL 1,810,260 4.07 614,932 72.5 446,370
SOLIDS OFF PRESS
WEEK
Yds
%Solids
1
384
11.40
2
384
16.03
3
384
16.36
4
480
16.24
TOTAL
1632
16.51
Summary
Total Gallons to Anaerobic Dig. 21378,467
Total Pounds of Dry Solids to Anaerobic Dig. 870,113
Total Pounds of Vol. Solids to Anaerobic Dig. 651,105
Total Gallons from Anaerobic Dig. 3,013,192
Total lbs. of Dry Solids from Anaerobic Dig, 552,462
Total lbs. of Vol. Solids from Anaerobic Dig. 341,598
Detention Time - Days 41
Gas Production 11831,023
Ft3 of Gas Produced/Ib of VM Added 3
Reduction 44 (VK) 48 % (AMB)

North Durham Water Reclamation Facility in
Sludge Report out
Apr'19
PRIMARY SLUDGE
TO DIGESTER - A
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
89,437
8
56,689
76
43,129
2
62,027
4,98
25,736
80.5
20,724
3
59,863
5.13
25,587
72.3
18487
4
60,880
5.26
26,693
78.0
20,820
TOTAL
272,207
5.84
134,704
76.7
103,159
WASTING TOTAL
WEEK
Gallons
%Solitls
Lbs Dry
%Vol
lbs VM
1
11469,677
1,20
147,085
70.9
104,342
2
11411,075
1.20
141,220
71.1
100,408
3
11343,707
1,13
127,007
67,5
85,730
4
11741,323
3.17
459,883
70.2
322,991
TOTAL
51965,782
1,68
875,196
69.9
613,471
ANAEROBIC SLUDGE TO PRESS
WEEK
Gallons
1
686,384
2
678,246
3
623,039
4
190162551
TOTAL
3,004,220
PRIMARY SLUDGE TO
DIGESTER -
B
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
581949
6.98
34,316
85.3
29,258
331559
6.90
19,312
86.0
16,613
7,620
124,262
4.18
43,354
74.1
32,103
224,390
6.02
96,982
81.8
77,974
TO GBT
Gallons
lbs. D.S.
lbs. V.M.
1,641,475
164,279
116,539
1, 446,671
144,783
1027941
1,348,187
127,431
86,016
1,939,472
512,214
359,745
6,375,805
948,707
665,241
Solids Lbs Dry %Vol Ibs VM TWAS FROM GRAVITY BELT THICKENER
ry
2.14
1222503
54.5
66,715
WEEK
Gallons
%Solitls
Lbs D
SOLIDS OFF
PRESS
WEEK
Yds
%Solids
1
384
16.24
2
384
16.22
3
384
16.07
4
528
16.29
TOTAL
1680
16.21
Summary
Total Gallons to Anaerobic Dig. 2,582,053
Total Pounds of Dry Solids to Anaerobic Dig. 1,113,483
Total Pounds of Vol. Solids to Anaerobic Dig. 8097256
Total Gallons from Anaerobic Dig. 37004,220
Total lbs, of Dry Solids from Anaerobic Dig. 585,650
Total lbs. of Vol. Solids from Anaerobic Dig. 348,499
Detention Time - Days 37
Gas Production 17967,956
Ft3 of Gas ProducedAb of VM Added 2
Reduction 45
(VKJ 57 % (AMB)
71.1
Vol Ibs VM
68.54 125,219
72.48 167,889
71.58 131,742
71.72 203,272
628,122

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQPermitNumber: W00003504
WWTP Name: North Durham WRF NPDES Number: NC0023841
Monitoring Period: From OS/Ol/19 To 6/30/19
Pathogen Reduction (40 CFR 50332/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) _
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP) _
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment _ Thermophilic _
Beta Ray _ Gamma Ray _ Pasteurization _
Class B:
Alt. (I) Fecal Density X Alt. (2) process to Significantly Reduce Pathogens _
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Anaerobic Digestion
If annlirahlr 4n oltn...., ..
Composting Aerobic Digestion
- ---
Pazameter
Fecal
Coliform
v,�nss
Allowable Level in Sludge
2x10 to the 6w MPN
power per gram of
a or class u coin lete the following monitoring data•
Pathogen Density
Minimum Geo. Mean Maximum Units
1055 16079 59040 MPN/g
No, of
Excee-
dences
0
Frequency
of
Analysis
Bi-monthly
Sample
Type
Analytical
Technique
Grab
9221 E
total solids
CFU
CFU/g
1000 MPN per gram of total
solids (dry weight)
MPN/g
Salmonella
bacteria (in
lieu of fecal
3 MPN per 4 grams total
solids (dry weight)
coliform)
ecror nrtract�on Reduction (40 CFR 50333/15A NCAC 02T.110'7) -Please indicate option/alternative performed:
Option/Alt. I
(VS reduction) X
Option/Alt 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. G
(Alk Stabilization)
Option/Alt. 10
(Incorporntion)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying —Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying —Unstable)
No vector attraction reduction alternafives were performed
"I certify, under penalty of ]aw, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/liA NCAC 02T.1107 have been met
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met.' (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
awaze that there aze significant penalties for false certification including fine and imprisonment
John Dodson, Superintendent —North DurhamWRF
Prepazer Name and Title (print or type) �,,� �
azure of Prepazer* Bate
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
*Prepazer is defined in 40 CFR Part 503.9(r) and liA NCAC 2T.1102 (26)
Date
�.,.—,—,=.—I
— �
—
....

North Durham Water Reclamation Facility
Sludge Report
May'19
PRIMARY SLUDGE
TO DIGESTER -A
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
48,165
5
20,165
81
16,249
2
46,665
6.12
23,818
81.7
197455
3
44,831
6.10
222807
78.8
177963
4
78,280
5.58
36,397
80.0
29,126
TOTAL
217,941
5.70
103,187
80.4
82,793
PRIMARY SLUDGE TO DIGESTER - B
Gallons
%Solids
Lbs Dry
%Vol
65,408
4,43
24,184
79.8
701974
6.56
38,830
77.0
541389
5.68
25,765
85.9
721315
5.95
35,885
88.9
263,086
5.66
124,664
82.9
in 10 %
out 60 %
Ibs VM
19,291
29,899
22,132
31,890
103,212
WASTING TOTAL
TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Gallons
Ibs. D.S.
Ibs. V.M.
1
1,320,783
1.30
143,199
71.7
102,674
1,047,304
113,549
81,414
2
11545,446
1.30
1675557
72.8
121,926
11431,883
155,245
112,966
3
11542,483
1.17
150,084
73.6
110,512
11569,681
152,730
112,460
4
21211,562
1.00
184,444
74.5
137,365
21206,820
184,049
137,070
TOTAL
67620,274
1,19
645,284
73.2
472,476
61255,689
605,572
443,911
ANAEROBIC SLUDGE TO PRESS
TWAS FROM GRAVITY
BELT THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
474,308
2.60
102,849
60.0
61,709
1
298,543
4,00
997594
73.75
73,451
2
713,424
2.63
156,682
60.0
94,009
2
453,401
4.72
178,480
73.88
131,861
3
604,498
2.77
139,482
60.0
83,736
3
430,726
7.82
280,914
71.92
202,034
4
8107259
2.70
182,454
61.3
111,844
4
4722381
5.33
209,787
74.85
1577025
TOTAL
21602,489
2.68
581,467
60.3
351,299
TOTAL
11655,051
5.47
768,775
73.6
564,371
SOLIDS OFF PRESS
WEEK
Ytls
%Solids
1
384
2
384
16.82
3
384
17.00
4
528
16.40
TOTAL
1680
16.74
Summary
Total Gallons to Anaerobic Dig. 2,136,078
Total Pountls of Dry Solids to Anaerobic Dig. 996,626
Total Pounds of Vol. Solids to Anaerobic Dig, 750,376
Total Gallons from Anaerobic Dig. 21602,489
Total Ibs. of Dry Solids from Anaerobic Dig. 581,467
Total Ibs. of Vol. Solids from Anaerobic Dig. 351,299
Detention Time - Days 45
Gas Production 21171,229
Ft3 of Gas ProduceWb of VM Added 3
%Reduction 50 (VK) 53 % (AMS)

North Durham Water Reclamation Facility
Sludge Report
Jun '19
PRIMARY SLUDGE
TO DIGESTER - A
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
62,440
5
24,684
81
197885
2
78,291
6,42
41,919
71.6
30,006
3
75,199
5.80
365375
74.5
27,107
4
99,499
5.03
41,699
83.7
34,912
TOTAL
315,429
5.56
144,677
77.7
1117910
PRIMARY SLUDGE TO DIGESTER - B
Gallons
%Solids
Lbs Dry
%Vol
491923
4.98
20,735
87.2
491761
4.62
19,173
85.6
44,962
6.06
22,724
82.1
67,405
6.93
38,929
79.5
212,051
5.65
101,561
83.6
in 76 %
out 63 %
Ibs VM
8,081
16,412
8,647
30,949
84,089
WASTING TOTAL
TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Gallons
Ibs. D.S.
Ibs. V.M.
1
11505,388
0.94
118,016
74.5
879875
11472,874
115,467
85,977
2
1,714,572
0.95
135,846
73.4
99,711
114457675
114541
84,073
3
11529,797
1.10
140,344
72.6
101,889
1,454,088
133,398
96,847
4
11663,249
1.05
145,651
71.9
104,723
11483,365
1297898
93,397
TOTAL
61413,006
1.01
5392856
73.1
394,198
5,8569001
493,304
360,294
ANAEROBIC SLUDGE TO PRESS
TWAS FROM GRAVITY
BELT THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
596,471
2.78
138,044
62.3
86,036
1
278,707
5.68
131,975
75.17
99,201
2
463,534
2.83
109,533
62.0
67,947
2
2725281
6.58
149,307
74.08
110,599
3
581,084
2.80
135,695
64.1
86,980
3
2957319
6,63
1639171
74.30
121,236
4
466,809
3,00
116,796
64.8
75,684
4
324,860
6.70
181,525
73.63
133,663
TOTAL
21107,898
2.85
500,068
63.3
3167647
TOTAL
11171,167
6.40
625,978
74.3
464,700
SOLIDS OFF PRESS
WEEK
Yds
%Solids
1
384
15.43
2
384
16.08
3
384
15.97
4
384
14.97
TOTAL
1536
15.61
$Ufn1T12ry
Total Gallons to Anaerobic Dig. 1,698,647
Total Pounds of Dry Solitls to Anaerobic Dig. 872,216
Total Pounds of Vol. Solids to Anaerobic Dig. 660,698
Total Gallons from Anaerobic Dig, 21107,898
Total Ibs. of Dry Solids from Anaerobic Dig. 500,068
Total Ibs. of Vol. Solids from Anaerobic Dig. 316,647
Detention Time - Days 57
Gas Production 11782,465
Ft3 of Gas Produced/lb of VM Added 3
Reduction 46 (VK) 52 % (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
W WTP Name: North Durham WRF NPDES Number: NCO023841
Monitoring Period: From 07/01/19 To 08/31/19
Pathogen Reduction (40 CFR 50332/15A NCAC 02T.110G) -Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens _
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting _ Aerobic Digestion
Anaerobic Digestion
nnrfn..nnrl r('loee a nr !`loco R1 rnm nlnkr Thr following mnni4nrino data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Gen. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6e'
MPN
310
4238
20737
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU/g
CFU
1000 MPN per gam of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction
(40 CFR 503.33/15A NCAC 02T.1107)
-Please indicate option/alternative
performed:
0ption/Alt. 1
Option/Alt. 2
Opfion/Alt. 3
Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(AlkStabilization)
(Drying — Stable)
(Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection) _
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 50332/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A KCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
John Dodson, Superintendent —North Durham WRF �'`�{('�/q�//�
repazer Na e an�d�Title (print or type) — Land Applier Name and Title (if applicable) (type or print)
ature of Prreepaz `�
rTM Date Signature of Land Applier (if applicable)
Date
'"Prepazer is defined in 40 CFR Part 503.9(r) and ISA NCAC 2T.1102 (26)

North Durham Water Reclamation Facility �� �s pro
Sludge Report out 63 pro
Jul'19
PRIMARY SLUDGE
TO DIGESTER -A
PRIMARY SLUDGE TO
DIGESTER-B
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
Gallons
%Solitls
Lbs Dry
%Vol
Ibs VM
t
91,745
5
38,066
83
31,757
52,725
5.63
24,735
79.5
19,658
2
89,902
4.80
35,990
78.1
28,115
53,554
6.54
29,210
83.8
24,478
3
124,374
3.88
40,246
82.2
33,083
52,523
5.14
22,515
85.5
19,251
a
116,723
5.34
51,959
77.9
40,463
74,806
6.30
39,305
84.8
33,316
TOTAL
422,744
4.76
166,261
80.3
133,418
233,608
5.90
115,765
83.4
96,702
WASTING TOTAL
TO GBT
WEEK
Gallons
%Solitls
Lbs Dry
%Vol
Ibs VM
Gallons
lbs. D.S.
lbs. V.M.
1
1,061,916
1.00
88,564
69.2
61,316
1,067,923
89,065
61,663
2
1,069,808
0.84
74,946
71.1
53,317
930,996
65,222
46,399
3
1,017,077
0.86
72,949
70.6
51,531
1,112,432
79,788
56,362
4
1,695,808
0.79
111,376
70.3
78,312
1,818,278
119,420
83,967
TOTAL
4,844,609
0.87
347,836
70.3
244,475
4,929,629
353,495
248,391
ANAEROBIC SLUDGE TO PRESS
TWAS FROM
GRAVITY
BELT THICKENER
wEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
t
392,884
3.13
102,668
65.8
67,522
1
187,445
6.36
99,425
73.58
73,157
2
469,901
2.95
115,610
61.0
70,551
2
181,954
5.36
81,294
72.10
58,613
3
431,787
3.26
117,396
61.2
71,846
3
197,336
5.71
94,045
71.81
67,538
a
742,145
3.13
193,422
63.9
123,669
4
298,717
5.82
144,948
71.76
104,020
TOTAL
2,036,717
3.12
529,096
63.D
333,588
TOTAL
865,452
5.81
419,713
72.3
303,328
SOLIDS OFF PRESS
WEEK
Ytls
%Solids
1
384
15.44
2
384
15.47
3
384
15.16
4
624
15.44
TOTAL
1776
15.38
Summary
Total Gallons to Anaerobic Dig. 1,521,804
Total Pounds of Dry Solids to Anaerobic Dig. 701,739
Total Pounds of Vol. Solids to Anaerobic Dig. 533,448
Total Gallons from Anaerobic Dig. 2,036,717
Total Ibs. of Dry Solids from Anaerobic Dig. 529,096
Total lbs. of Vol. Solitls from Anaerobic Dig. 333,588
Detention Time -Days 63
Gas Production 1,836,798
Ft3 of Gas Produced/Ib of VM Atltletl 3
Reduction 47 (VK) 37 % (AMB)

North Durham Water Reclamation Facility
Sludge Report
Aug '19
PRIMARY SLUDGE TO DIGESTER - A
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
1
76,501
5
31,518
82
25,750
2
70,163
4,22
24,694
79.6
1901
3
1167462
3.28
31,858
68A
21,689
4
977400
5.60
45,490
72.4
32,941
TOTAL
360,526
4.53
133,560
75.5
1009042
PRIMARY SLUDGE TO DIGESTER - B
Gallons
%Solitls
Lbs Dry
%Vol
40,781
5.46
18,570
85.2
43,532
6.25
22,691
84.8
442853
5.82
21,771
35.3
647488
5.70
30,656
83.5
193,654
5.81
93,689
84.7
in 74 %
out 65 %
Ibs VM
5,826
19,248
18,566
25,594
79,233
WASTING TOTAL
TO GBT
WEEK
Gallons
%Solitls
Lbs Dry
%Vol
Its VM
Gallons
lbs. D.S.
Ibs, V.M.
1
1,296,973
0.80
86,534
70.4
60,877
1126190
75,139
52,861
2
12877641
0.82
88,059
70.6
62,205
11671,697
114,324
809758
3
11314,352
0.85
93,174
71.8
66,876
11415,884
100,372
729042
4
11786,560
1.02
1515482
70.7
107,098
11759,956
149,227
105,503
TOTAL
51685,526
0.87
419,250
70.9
297,056
5,9737727
439,062
311,164
ANAEROBIC SLUDGE TO PRESS
TWAS FROM GRAVITY
BELT THICKENER
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
1
4162712
2.90
100,786
63.4
63,898
1
219,384
6,55
1197843
71.80
86,047
2
567,640
2.90
137,289
65.0
89,238
2
249,326
6.63
137,863
72.31
99,689
3
484,424
2.93
118,509
65.5
777663
3
2559946
6,65
141,950
72.53
102,949
4
778,110
2.92
189,275
64.7
122,366
4
3927538
5.32
174,164
72.13
125,625
TOTAL
21246,886
2.91
545,860
64.7
3535166
TOTAL
1,117, 194
6.29
573,820
72.2
414,310
SOLIDS OFF PRESS
WEEK
Yds
%Solids
1
384
2
384
15.18
3
384
15.20
4
528
15,37
TOTAL
1680
15.25
Summary
Total Gallons to Anaerobic Dig. 1,671,374
Total Pounds of Dry Solids to Anaerobic Dig. 801,069
Total Pounds of Vol. Solids to Anaerobic Dig. 593,585
Total Gallons from Anaerobic Dig. 21246,886
Total Ibs. of Dry Solids from Anaerobic Dig. 5457860
Total Ibs. of Vol. Solids from Anaerobic Dig, 353,166
Detention Time - Days 58
Gas Production 17467,703
Ft3 of Gas Produced4b of VM Added 2
Reduction 37 (VIQ 41 % (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
W WTP Name: North Durham WRF NPDES Number: NC002M41
Monitoring Period: From 09/01/19 To 10/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt 1/A (rime/temp) _ Alt. 2B (Alk Treatment) _ Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying _ Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
Alt. (1) Fecai Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
lia ncabte to
aaernanve eaurmeu
.-.a��L ..�••• •�•�•••--�•--••------_..._____ ____
Pathogen Density
No. f
Exceo-
Frequency
of
Sample
Type
Analytical
Technique
Parameter
Allowable Level in Sludge
Minimum Gen. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6�' MPN
71 I 4974 30018 MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/9
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107)
Option/Alt. 1 Option/AIt. 2
(VS reduction) X (40-day bench)
Option/Alt. 5 Option/Alt. 6
(14-Day Aerobic) (Alk Stabilization)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation)
Please indicate option/alternative performed:
Option/Alt. 3 Option/Alt 4
(30-day bench) (Spec. 02 uptake)
Option/Alt. 7 Option/Alt. 8
(Drying —Stable) (Drying —Unstable)
CERTIFICATION STATEMENT (please check the appropriate statement)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15AKCAC 02T.1107 have been met
certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment'"
John Dodson Superintendent —North Durham WRF
Prepazer Name and Title (print or type) Land Applier Name and Title (if applicable) (type or print)
LU
Ygnaeef Prepazer* Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Please indicate option/alternative performed:
Option/Alt. 3 Option/Alt 4
(30-day bench) (Spec. 02 uptake)
Option/Alt. 7 Option/Alt. 8
(Drying —Stable) (Drying —Unstable)
CERTIFICATION STATEMENT (please check the appropriate statement)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15AKCAC 02T.1107 have been met
certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment'"
John Dodson Superintendent —North Durham WRF
Prepazer Name and Title (print or type) Land Applier Name and Title (if applicable) (type or print)
LU
Ygnaeef Prepazer* Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North Durham Water Reclamation Facility in 77 %
Sludge Report out 64 %
Sep '19
PRIMARY SLUDGE TO DIGESTER -A PRIMARY SLUDGE TO DIGESTER -B
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons % Solids Lbs Dry % Vol Ibs VM
1 70,844 4 24,372 79 19,260 45,182 4,88 18,370 84.6 15,536
2 67,170 4.36 24,425 80.1 19,564 58,337 5.30 255786 87.0 22,424
3 65,508 5.02 27,426 81.7 22,402 707872 3.36 19,860 86.9 17,254
4 83,474 3.78 26,339 82.2 21,650 87,589 3.30 24,106 86.4 20,820
TOTAL 286,996 4.29 102,561 80.8 82,876 261,980 4,21 889122 86.2 76,034
WASTING TOTAL
TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Gallons
Ibs. D.S.
Ibs. V.M.
1
113137051
1.05
114,984
71.3
81,926
17592,698
1395473
99,374
2
11157,246
1,00
96,514
72.3
69,780
11093,122
91,166
65,913
3
192617186
1.10
115,701
73.0
84,416
17336,801
122,638
89,477
4
11405,062
1,20
140,619
74.1
104,198
11391,362
139,248
103,182
TOTAL
5t136,545
1,09
467,818
72.7
340,320
5,413,983
492,525
357,947
ANAEROBIC SLUDGE TO PRESS
TWAS FROM GRAVITY
BELT THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
451,075
3.00
112,859
63.9
729089
1
344,050
5.29
151,718
71.38
108,289
2
533,966
3.08
1367938
63.8
87,367
2
221,532
6,00
110,855
73.81
81,827
3
603,566
3.02
152,019
63.9
97,079
3
284,635
5.50
130,562
74.12
96,773
4
483,309
4
346,540
5.45
157,513
75.00
118,135
TOTAL
2,071,916
3.03
401,816
63.9
256,535
TOTAL
11196,757
5.56
550,648
73.6
4052023
SOLIDS OFF PRESS
WEEK
Ytls
%Solids
1
384
14.74
2
384
15.24
3
384
15.17
4
480
TOTAL
1632
15.05
Summary
Total Gallons to Anaerobic Dig. 11745,733
Total Pounds of Dry Solids to Anaerobic Dig. 741,331
Total Pounds of Vol. Solids to Anaerobic Dig. 563,933
Total Gallons from Anaerobic Dig. 2,071,916
Total Ibs. of Dry Solids from Anaerobic Dig. 401,816
Total Ibs. of Vol. Solids from Anaerobic Dig. 2565535
Detention Time - Days 55
Gas Production 11894,386
Ft3 of Gas Produced/lb of VM Added 3
% Reduction 46 (VK) 55 % (AMS)

North Durham Water Reclamation Facility in 77 yid
Sludge Report out 67 Rio
Oct'19
PRIMARY SLUDGE
TO DIGESTER -A
PRIMARY SLUDGE TO
DIGESTER-B
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
69,797
4
23,051
82
18,870
70,398
4.08
23,954
85.9
209586
2
66,395
3.74
20,710
79.8
16,530
71,065
3.58
21,218
83.6
17,730
3
87,967
5.30
38,883
77.5
30,127
705002
2.78
16,230
77.9
12,640
4
859128
5.36
38,072
80.3
307562
88,439
6.09
44,900
79.3
35,606
TOTAL
309,287
4.60
1207716
79.9
96,089
299,904
4,13
1069303
81.7
86,562
WASTING TOTAL
TO GBT
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
Gallons
Ibs, D.S.
Ibs. V.M.
1
1,149,884
1,05
1009695
73.4
73,885
11123,888
98,419
72,215
2
19197,291
1,02
101,851
74.2
75,533
113679403
116,322
86,265
3
11181,544
1.23
121,534
74.2
90,218
873,497
89,848
66,697
4
11463,272
1.30
158,648
71.4
113,275
11404,374
152,262
108,715
TOTAL
41991,991
1.15
482,728
73.3
3529911
417697162
456,851
333,892
ANAEROBIC SLUDGE TO PRESS
TWAS FROM GRAVITY
BELT THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
475,723
2.98
118,034
64.4
76,043
1
254,329
5.63
119,312
73.30
87,456
2
676,047
2.92
164,636
69.2
113,895
2
284,377
5.42
128,546
75,11
96,551
3
394,234
2.83
93,157
66.6
62,012
3
227,571
5.43
103,122
75.53
77,891
4
759,121
2.68
169,884
66.1
112,265
4
368,215
5.80
1789113
75.23
133,992
TOTAL
21305,125
2.85
5459712
66.6
364,215
TOTAL
11134,492
5,57
529,093
74.8
395,890
SOLIDS OFF PRESS
WEEK
Ytls
%Solids
1
384
14.02
2
384
13.15
3
384
13.20
4
576
13.86
TOTAL
1728
13.56
SummaN
Total Gallons to Anaerobic Dig.
1,743,683
Total Pounds of Dry Solitls to Anaerobic Dig.
756,112
Total Pounds of Vol. Solids to Anaerobic Dig.
578,541
Total Gallons from Anaerobic Dig.
2,3055125
Total Ibs. of Dry Solids from Anaerobic Dig.
5457712
Total Ibs. of Vol. Solids from Anaerobic Dig.
364,215
Detention Time - Days
55
Gas Production
21129,696
Ft3 of Gas Produced/lb of VM Added
4
% Reduction
40
(VK)
Ibs Polymer
$/Ib
Pounds of Polymer Used - GBT
$1.87
Pounds of Polymer Used - BFP
$1.87
Poly Cost $/DT

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
W WTP Name: North Durham WRF NPDES Number: NCO023841
Monitoring Period: From 11/01/19 To 12/31/19
Pathogen Reduction (40 CFR 50332/15A NCAC 02T.1106) "Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp)
Alt. 4/D (No Prior Test)
Alt. 2B (Alk Treatment)
Alt. 5/Process to Further Reduce Pathogens
Alt. 3/C (Prior Testing)
Alt. 6 (Equivalent to PFRP)
If applicable to alternative
performed (Class A only)
indicate "Process to Further
Reduce Pathogens":
Compost
Heat Drying _
Heat Treatment _
Thermopbilic
Beta Ray _
Gamma Ray _
Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting _ Aerobic Digestion
Anaerobic Digestion
If applicable to
alternative enormea uass
n or i,�ass n �o... .o.� ...� ..,..�...... ............ ..-•-•
No. f
Frequency
Sample
Analytical
Parameter
Allowable Level in Sludge
Pathogen Density
Exceo-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
468
2649
17284
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MIN per gram of total
MPN/9
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option alternative performed:
0 tiont. 1 Option/Alt, 2 Option/Alt. 3 Option/Alt14
/Al
(VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake)
Option/Alt, 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic) (A1kStabilizatiion) (Drying - Stable) (Drying -Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment "
John Dodson Superintendent -North Durham WRF
Prepazer Name and Title (print or type) <��-�`�
S afore of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Prepazer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North Durham Water Reclamation Facility in
Sludge Report out
Nov'19
PRIMARY SLUDGE TO DIGESTER - A PRIMARY SLUDGE TO DIGESTER - B
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons % Solids Lbs Dry % Vol Ibs VM
1 64,691 4 21,257 85 18,039 54,026 5.58 25,142 83.0 20,863
2 70,522 4.80 28,231 84.3 23,792 53,973 4.73 21,269 86.2 18,328
3 65,074 6.00 32,563 82.7 26,943 53,997 4.58 20,625 85.5 17,635
4 877781 6.53 47,769 80.4 38,394 67,552 4.85 27,324 85.1 23,260
TOTAL 288,068 5.33 129,821 83.1 107,168 229,548 4.94 94,361 85.0 80,086
WASTING TOTAL
TO GBT
WEEK
Gallons
%Solids
Lbs Dry
% Vol
Ibs VM
Gallons
Ibs. D.S.
Ibs. V.M.
1
11328,325
1.05
116,321
73.3
85,235
1,226,741
107,426
78,716
2
11279,124
0.93
99,567
74.3
73,978
768,341
59,808
44,437
3
11099,389
1.03
94,745
75.0
71,027
1,260,259
108,609
81,421
4
11343,423
1.13
126,980
75.0
95,278
11109,834
104,901
78,711
TOTAL
59050,261
1.04
437,614
74.4
325,518
4,365,174
380,744
283,285
ANAEROBIC SLUDGE TO PRESS
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM
1 484,741 2.75 111,175 65.6 72,931
2 327,347 2.53 69,162 65.3 45,163
3 606,554 2.60 131,525 65.6 86,237
4 628,014 2.47 1297195 66.6 86,087
TOTAL 2,046,656 2,59 4419057 65.8 2907417
SOLIDS OFF PRESS
WEEK Yds %Solids
1 384 13.15
2 384 14.25
3 384 13.88
4 480 14.25
TOTAL 1632 13.88
TWAS FROM GRAVITY BELT THICKENER
WEEK
SOLIDS OFF PRESS
WEEK Yds %Solids
1 384 13.15
2 384 14.25
3 384 13.88
4 480 14.25
TOTAL 1632 13.88
TWAS FROM GRAVITY BELT THICKENER
WEEK
TWAS FROM GRAVITY BELT THICKENER
WEEK
Gallons
%Solids
Lbs Dry
%Vol
1
250,311
5.22
108,903
74.45
2
190,755
5.32
84,636
75.28
3
279,460
5.80
135,180
76.06
4
305,574
5.56
1417696
75.40
TOTAL
1,026,100
5.48
470,415
75.3
$Unlnlary
Total Gallons to Anaerobic Dig. 1,543,716
Total Pounds of Dry Solids to Anaerobic Dig. 694,596
Total Pounds of Vol. Solids to Anaerobic Dig. 5417702
Total Gallons from Anaerobic Dig. 21046,656
Total Ibs. of Dry Solids from Anaerobic Dig. 441,057
Total Ibs. of Vol. Solids from Anaerobic Dig. 290,417
Detention Time - Days 63
Gas Production 2,4222804
Ft3 of Gas Produced/lb of VM Added 4
Reduction 46 (VK)
66 %
Ibs VM
81,078
63,714
102,818
106,839
354,449

North Durham Water Reclamation Facility
Sludge Report
Dec'19
PRIMARY SLUDGE TO DIGESTER - A
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
1
819971
5
31,311
82
25,631
2
85,117
4.46
31,660
79.4
257126
3
86,739
4.08
29,515
77.0
22,715
4
165,593
3.60
49,718
83.0
41,253
TOTAL
419,420
4.29
142,204
80.4
114,724
out 65 %
PRIMARY SLUDGE TO DIGESTER - B
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
55,383
5.80
267790
85.8
22,986
55,567
6.00
27,806
85.9
23,885
559549
6.38
29,557
85.6
25,289
79,408
5.98
39,570
85.4
337773
245,907
6.04
123,723
85.7
105,933
WASTING TOTAL
"
TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Gallons
Ibs. D.S.
Ibs. V.M.
1
959,007
1.28
101,976
74.7
76,125
11079,129
114,749
85,660
2
11136,428
1.13
106,625
73.2
77,996
855,912
807306
58,744
3
11181,594
1.38
135,499
71.3
96,543
1,142,772
1317047
93,371
4
11375,658
1.20
137,676
71.8
98,817
1,076,290
107,715
77,313
TOTAL
4,652,687
1.25
4819777
72.8
349,482
49154,103
433,818
315,088
ANAEROBIC SLUDGE TO PRESS
SOLIDS
OFF PRESS
WEEK
Gallons
%Solitls
Lbs Dry
%Vol
Ibs VM
WEEK
Yds
%Solids
1
693,941
2.38
137,452
65.4
89,859
1
384
15.06
2
513,396
2.55
109,184
65.9
71,952
2
336
15.73
3
7269069
2.55
154,413
64.7
99,905
3
432
14.75
4
640,601
2,65
141,579
63.6
90,044
4
384
15.16
TOTAL
21574,007
2,53
542,629
64.9
351,761
TOTAL
1536
15.18
WAS FROM GRAVITY BELT THICKENER
WEEK
Gallons
%Solitls
Lbs Dry
%Vol
Ibs VM
1
292,030
5.11
124,560
75.54
94,096
2
1947398
5.30
85,928
74.67
64,159
3
338,887
5.79
163573
73.09
119,552
4
2892955
5,91
1427978
72.78
104,052
TOTAL
19115,270
5.53
517,038
74.0
3814859
Summary
Total Gallons to Anaerobic Dig. 1,780,597
Total Pounds of Dry Solitls to Anaerobic Dig. 782,965
Total Pounds of Vol. Solids to Anaerobic Dig, 6029517
Total Gallons from Anaerobic Dig. 21574,007
Total Ibs. of Dry Solids from Anaerobic Dig, 542,629
Total Ibs. of Vol. Solids from Anaerobic Dig. 351,761
Detention Time - Days 54
Gas Production 214697720
Ft3 of Gas ProducedAb of VM Added 4
Reduction 45 (VK) 42 % (AMB)

North &South Durham Sludge Fecal Coliform Analysis
2019 Summary
North Durham WRF
Sample
Date
Sample Set#1
LPN
twy ytotmmds
Sample Set #2
nPN
troyrc 6Wd rds
Sample Set #3
t/vrt
tmyywafwrds
Sample Set#4
tPx
[wrr« vwalmws
Sample Set il5
WN
fwbanvwd ds
Sample Set#6
WN
Sample Set#7
vax
taarods
Geometric Mean
tra/a.1s
2/21/2019
40545
51500
1,613
41145
82395
1,278
53,892
42958
4/26/2019
1,402
84,211
463154
5,983
41,667
16,393
115,942
223109
6/25/2019
91434
52,805
54,422
59,040
i,055
11,814
13,927
16,079
8/1512019
31902
9,058
20,737
92375
310
11204
91581
4,238
10/1712019
30,018
11596
219164
2,676
711
2,285
17,078
4,974
12/12/2019
3,883
31828
1,587
468
21529
1,897
17,284
21649
South Durham WRF
Sample
.. Date
Sample Set #i
APN
trortwmylaawrds
Sample Set #2
UPI!
tmscffi aW+sads
Sample Set ik3
I,PN
LroCamykf&sods
21242
Sample Sel #4
n'PN
tw:sxmgra6mrds
1,798
Sample Set #5
neat
troyyklawds
,..
2,721
Sample Set #6
NPN
IOwam3tamsoFds
.,.,_..--,...--.,-,..ems. �,
974
Sample Set #7
GPM
troy gwafwms
r . ..
31465
Geometric Mean
emtrsts
11770
2/21/2019
1,345
1,095
4/25/2019
1,245
29
59
69
10
56
2,586
109
6/25/2019
301
1,428
355
11321
639
616
237
567
8/16/2019
506
338
27
10
10
31422
11288
154
10/17/2019
4,348
23
61226
212
16,216
1
84,656
782
i2J12/2019
3,620
8,374
12,987
1,204
1310m
6,771
2,551
5,231

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
W WTP Name: South Durham WRF NPDES Number: NCO047597
Monitoring Period: From 01/01/19 To 02/28/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) _ Alt, 2B (Alk Treatment) _ Alt. 3/C (Prior Testing)
Alt, 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt, 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying _ Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If a licable to
alternative ertormea �,�ass
a ur ua�� .. ��_" •�« •_•� ��••-•• •••------------
Pathogen Density
Eaceef
Freqofncy
Typee
-
Technique
Parameter
Allowable Level in Sludge
Minimum Gco. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6`s MPN
974 1770 3465 MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gran of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503-33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1 OptiowAlt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake)
Option/Alt, 5 Option/Alt. 6 Option/Alt. 7 Option/Alt, 8
(14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying —Unstable)
Option/Alt, 9 Option/Alt. 10
(Injection) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT
(please
check the
appropriate
statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332/15A NCAC 02T1106 and the vector attraction
X reduction requirement in40 CFR 50333/liA�VCA 02T1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332/15ANCAC 02T1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements-)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properl gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment"
Charles Cocker Superintendent— South Durham WRF
Preparer Name and Title (print o`rw e)
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
i
*Prepazer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T.1102 (26)

Youth Durham Water Reclamation Facility
Yludge Report
anuary'2019
D PRIMARY SLUDGE TO DIGESTER
P'I GRAVITY THICKENER
TO ANAEROBIC
DIGESTE
VEEK
Gallons
% Solids
Los Dry
% Vol
Ibs VM
-':. Gallons %
Solids
Lbs Dry
% Vol
Ibs VM
1
370,652
2A
740190
84.5
62,690
i -
2
375,660
3A
106,522
85.6
91,183
"
3
351,912
22
64,569
81.7
52,753
4
462,031
4.4
169,547
79.9
135,468
S
'OTAL
11560,256
3.1
414,828
82.9
342,094
TASTING
TO GRAVITY THICKENER
''•, TWASGBTTOANAEROBICDIGESTE
MEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
.' Gallons %
Solids
Lbs Dry
% Vol
Ibs VM
1
879,430
0,81
59,482
74.6
44,374
96,983
6.1
49,339
73.3
36,166
2
1,152,288
1.11
107,111
73A
78,582
'is 53,078
6.2
27,446
73.2
20,090
3
1,154,908
1.10
105,745
77.9
82,374
-�. 168,614
6.4
89,999
74.2
66,780
4
1,650,287
1,00
137,703
72A
99,702
`'- 238,175
6.4
127,128
74.2
94,329
TOTAL
4,836,912
1,01
4100041
74.6
305*032
556,850
6.3
293,912
73.7
217,364
D ANAEROBIC SLUDGE TO PRESS-.
SD SOLIDS
OFF PRESS
GRAVITY THICKENER TO GBT
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
', Yds %Solids
%Vol
Gallons
%Solids Lbs Dry %Vol
Ibs VM
1
520v4O8
1.9
820464
60.5
49,891
'-. 312
17.4
63.0
117,957
4.2 41$18 70.5
29,129
2
462,681
1.9
73,316
60.4
44,283
1':. 324
17,2
63.0
63,200
3.7 197502 72.0
14,042
3
4162084
1.9
65,933
60.5
39,889
"; 281
17.0
63.4
154,572
4.5 58,011 72.2
41,884
4
737,152
1.9
116,809
60.3
70,436
S'; 436
17.1
63.5
263,245
1.9 41,714 60.3
25,153
TOTAL
2,136,325
1.9
3380522
60A
204,499
a 11352
17.2
63.2
598,974
3.6 1600545 68.8
110,208
ANAEROBIC SLUDGE TO BEDS
`, SOLIDS OFF
DRYING
BEDS
Beds Yards
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM Cleaned %Solids Removed
1
2
3
4
TOTAL
Summary
otal Gallons to Anaerobic Dig. 2,117,106
btal Pounds of Dry Solids to Anaerobic Dig. 708,740
btal Pounds of Vol. Solids to Anaerobic Dig. 559,459
dotal Gallons from Anaerobic Dig, 2,1361325
Total Ibs. of Dry Solids from Anaerobic Dig, 338,522
Total Ibs. of Vol. Solids from Anaerobic Dig. 204,499
)etention Time - Days 59
3as Production Ft3 62280,119
,t3 of Gas Produced/lb of VM added 11.2
Gravity Thickener to GBT gallon values are 80
of the meter reading in the Wasting Building.
'/o Reduction 63
Ibs Polymer $/lb Poly Cost $/DT
pounds of Polymer Used - GBT $1,75
pounds of Polymer Used - BFP 20610 $1.75 41568 26,98

South Durham Water Reclamation Facility
Sludge Report
February'2019
SO PRIMARY SLUDGE TO DIGESTER
WEEK
Gallons
%Solids
Lbs Dry
% Vol
Ibs VM
1
490,835
3.0
122,807
85.4
104,877
2
419,822
3.3
115,543
83.3
96,248
3
325,285
3A
92,238
83.6
77,111
4
3533361
3.5
1030146
84.6
87,262
TOTAL 1,589,303 3.3 433,734 84.2 365,497
Gallons % Solids Lbs Dry %Vol Ibs VM
WASTING TO GRAVITY THICKENER
',TWAS
GBT TO ANAEROBIC DIGESTE
WEEK Gallons %Solids Lbs Dry
%Vol
Ibs VM '',.
Gallons
%Solids
Lbs Dry %Vol
Ibs VM
1 11159,970 0,81 78,181
73.3
57,301 "'
181,432
5.9
89,275 74.3
66,332
2 1,225,218 1,09 1117774
72.1
80,642 t
135,755
6.3
71,328 75.0
53,496
3 1,4501000 0.99 119,479
74.2
88,692 ''�.
168,169
6.2
86,957 74.8
653044
a 310,000 0.82 21,215
74.1
15,723 :
82,482
6A
44,026 75A
33,063
TOTAL 4,145,188 0.93 330,649
73.4
242,359
567,838
6.2
291,586 74.8
217,935
SO ANAEROBIC SLUDGE TO PRESS
i
SO SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK Gallons % Solids Lbs Dry
% Vol
Ibs VM
Yds
% Solids
% Vol
Gallons % Solids
Lbs Dry % Vol
Ibs VM
1 489,700 3.8 155,196
72.6
112,672 '.
304
17.3
64.1
217,006 1.9
34,387 62.1
21,354
2 508,836 1.9 80,630
61A
49,507
333
16.8
64.8
1710005 3.6
51,343 72.5
371223
3 514*443 2.0 85,809
61.8
53,030
! 352
16.6
65.9
2097826 3.5
61,248 73.5
45,017
4 474,684 2.0 79,177
63.4
50,198 /:
344
16.7
65.6
93,974 4.0
31,350 74.1
23,230
TOTAL 1,9879663 2.4 400,812
64.8
265,407 1:'
1,333
16.9
65.1
691,811 3.3
178,327 70.6
126,825
ANAEROBIC SLUDGE TO BEDS
el
SOLIDS OFF
DRYING BEDS
Beds
Yards
WEEK Gallons %Solids Lbs Dry
%Vol
Ibs VM I�
Cleaned
%Solids
Removed
1
2 74,235 1.9 11,763
61.2
73199
3
4
TOTAL 74,235 1.9 11,763
61.2
7,199 ;
Summary
Total Gallons to Anaerobic Dig.
2,157,141
Total Pounds of Dry Solids to Anaerobic Dig.
725,320
TWA$ GBTto Anaerobic Digester is 77
Total Pounds of Vol. Solids to Anaerobic Dig,
583,432
of the Gravity Thckenerto GBT value.
Total Gallons from Anaerobic Dig.
23061,898
Total Ibs. of Dry Solids from Anaerobic Dig,
4121576
Gravity Thickener to GBT gallon values
are 80%
Total Ibs. of Vol. Solids from Anaerobic Dig.
272,607-
of the meter reading
in the Wasting Building.
Detention Time - Days
52
Gas Production Ft3
4,092,459
Ft3 of Gas Produced/lb of VM added
7.0
% Reduction
59
% (VK)
53
% (LBS)
Ibs Polymer
$Ab
Poly Cost
$/DT
Pounds of Polymer Used - GBT
0
$1,75
0
Pounds of Polymer Used - BFP
21715
$1.75
4,751
23.71

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
WWTP Name: South Durham WRF NPDES Number: NC0047597
Monitoring Period: From 03/Ol/19 To 04/30/19
Pathogen Reduction (40 CFR 50332/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (All: Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Dtying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Pazameter
Allowable Leve] in Sludge
Paffiogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'"
MPN
10
109
2586
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU/g
CFU
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector AttraMion ReduMion (40 CFR 503.33/15A NCAC 02T.1107)
Option/Alt. 1
Option/Alt. 2
(VS reduction) X
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/AIt.9
Option/A1t.10
(Injection)
(Incorporation)
Please indicate option alternative performed:
Option/Alt. 3 Option/Alt. 4
(30-day bench) (Spec. 02 uptake)
Option/AIt. 7 Option/Alt. 8
(Drying —Stable) (Drying —Unstable)
CERTIFICATION STATEMENT (please check the appropriate statement)
No vector attraction reduction alternatives were performed
"I certify, under penalty of ]aw, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector amaction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector amaction
reduction requirement m 40 CFR 503.33/liA NCAC 02T.1107 have not been met"(Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properlyy gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
awaze ffiat there aze significant penalties for false certification including fine and imprisonment.'
Chazles Cocker, Superintendent —South Durham WRF
Prepazer N n e/a�nd Title�(pent o�e)
Signature of Prepazer* Date
Land Applier Name and Tite (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Prepazer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

South Durham Water Reclamation Facility
Sludge Report
March '2019
SD PRIMARY SLUDGE TO DIGESTER GRAVITY THICKENER TO ANAEROBIC DIGESTE
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM Gallons %Solids Lbs Dry %Vol Ibs VM
1 305,302 3.0 76,386 75.8 57,901
2 296,468 3.1 76,649 79.6 611012 ].
3 291,568 3.3 80,245 87A 70,134
4 419,658 3.2 1119998 87.2 973663 '.
TOTAL 1,312,995 3.2 345,279 82.5 286,710
WASTING TO GRAVITY THICKENER `: TWAS GBT TO ANAEROBIC DIGESTE
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM Gallons %Solids Lbs Dry %Val Ibs VM
1 797,094 0.91 60,751 72.2 43,870 128,559 6.9 73,981 75.1 55,559
2 1,1651658 1.19 115,284 74.0 85,267 '. 1545770 6.4 823610 74.3 610379
3 10260t382 0,96 100,431 73.0 73,346 ! 114,830 6.2 59,376 73.6 43,701
4 1 ,801 7091 0.82 1230143 73.4 90,421 140,900 6.0 70,506 74.8 52,739
TOTAL 5,024,224 0,97 399,609 73.2 292,903 1. 539,059 6.4 286,473 74.5 213,378
SD ANAEROBIC SLUDGE TO PRESS SD SOLIDS OFF PRESS GRAVITY THICKENER TO GBT
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Yds % Solids % Vol Gallons % Solids Lbs Dry % Vol Ibs VM
1 416,065 2.0 69,400 62.6 43,444 : 316 17.0 64.7 166,338 3A 43,005 73.8 31,738
2 494,668 2.0 82,511 63.6 52,477 321 16.1 63.9 201,563 3.6 60,517 73.5 44,480
3 445,763 2.0 74,353 63.3 47,066 311 16.2 65.8 149,131 3.1 389556 72.3 27,876
4 583,275 1.9 92,426 62.7 57,905 °I 419 16.4 65.5 182,984 3.3 50,361 66.7 33,566
TOTAL 1,939,771 2.0 318,689 63.1 200t891 1,367 16.4 65.0 700,016 3.3 192,439 71.6 137,660
ANAEROBIC SLUDGE TO BEDS 1. SOLIDS OFF DRYING BEDS
Beds Yards
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM + Cleaned %Solids Removed
1
2
3
4
TOTAL
Summary
Total Gallons to Anaerobic Dig. 1 *852,054
Total Pounds of Dry Solids to Anaerobic Dig. 631,752
Total Pounds of Vol. Solids to Anaerobic Dig. 500,089 Weeks 2 - 4 of TWAS GBT to Ana. Digester is 77 % of the
Total Gallons from Anaerobic Dig. 1,939,771
Gravity Thickener to GBT value.
Total Ibs. of Dry Solids from Anaerobic Dig. 318,689
Total Ibs. of Vol. Solids from Anaerobic Dig. 200,891 Gravity Thickener to GBT gallon values are 80 %
Detention Time - Days 67 of the meter reading in the Wasting Building
Gas Production Ft3 4,096,168
Ft3 of Gas Produced/lb of VM added 8.2
% Reduction 58 % (VK) 60 % (LBS)
Ibs Polymer $/Ib Poly Cost $/DT
Pounds of Polymer Used - GBT $1,75
Pounds of Polymer Used - BFP 31150 $1.75 5,513 34,59

South Durham Water Reclamation Facility
Sludge Report
April '2019
SD PRIMARY SLUDGE TO DIGESTER �IGRAVfTY THICKENER TO ANAEROBIC DIGESTE
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM "�. Gallons %Solids Lbs Dry %Vol Ibs VM
i 336,679 3.9 109,508 67.3 95,601 ':.',
2 289,229 3.4 82,014 84.7 69,466 '!
3 344,470 3.8 109,170 74.4 81,222 s
a 564,361 4.0 188,271 79.0 148,734 :�'
To7AL 1,534,740 3.8 488,963 81.4 395,023 '�''�
WASTING TO GRAVITYTHICKENER t�..TWAS GBT TO ANAEROBIC DIGESTE
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM '>', Gallons %Solids Lbs Dry °/, Vol Ibs VM
t 1,257,403 0.78 81,632 73.3 59,829 ;1 141,040 6.5 76,458 74.1 56,655
2 1,410,901 0.90 105,785 73.2 77,478 '.'i 179,385 6.2 92,756 73.3 67,990
3 1,560,517 0.93 121,669 67.7 82,338 �� 142,595 6.1 72,544 69.5 50,418
a 2,067,536 0.64 111,085 68.8 76,419 `.'!� 232,503 6.5 126,040 69.0 86,968
TOTo,L 6.296,357 0.81 420,170 70.8 296,064 �i 695,523 6.3 367,798 71.5 262,031
SD ANAEROBIC SLUDGE TO PRESS " SD SOLIDS OFF PRESS GRAVITY THICKENER TO GBT
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM Yds %Solids %Vol Gallons %Solids Lbs Dry %Vol Ibs VM
i 473,690 2.1 82,962 63.6 52,764 `;�< 370 18.2 71.2 183,170 3.8 58,050 73.0 42,377
2 420,665 2.0 70,167 fi2.3 43,714 a. 280 15.8 64.7 232,968 3.7 71,889 73.1 52,551
3 406,525 2.0 67,808 63.1 42,787 i. 279 16.0 65.3 185,189 3.7 57,146 71.3 40,745
a 657,510 2.1 115,156 62.2 71,627 (! 461 16.3 64.8 301,952 2.9 73,030 67.3 49,149
rornL 1,958,390 2.1 336,094 62.8 210,892 '; 1,390 16.6 66.5 903,279 3.5 260,115 71.2 184,822
ANAEROBIC SLUDGE TO BEDS 1SOLIDS OFF DRYING BEDS
Beds Yards
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM ': Cleaned %Solids Removed
t
z
3
a 70,700 2.4 14,151 63.5 8,986 �,..
roTAL 70,700 2.4 14,151 63.5 8,986
Summary
Total Gallons to Anaerobic Dig. 2,230,263
Total Pounds of Dry Solids to Anaerobic Dig. 856,760
Total Pounds of Vol. Solids to Anaerobic Dig. 657,054 TWAS GBT to Anaerobic Digester is 77%
Total Gallons from Anaerobic Dig. 2,029,090 of the Gravity Thckener to GBT value.
Total lbs. of Dry Solids from Anaerobic Dig. 35D,245
Total lbs. of Vol. Solids from Anaerobic Dig. 219,876 Gravity Thickener to GBT gallon values are 80
Detention Tme -Days 54 of the meter reading in the Wasting Building.
Gas Production Ft3 5,961,173
Ft3 of Gas Produced/Ib of VM added 9.1
Reduction 53 % (VK) 67 % (LBS)
Ibs Polymer $!Ib Poly Cost $/DT
Pounds of Polymer Used -GBT $1.75
Pounds of Polymer Used - BFP 3,030 $1.75 5,303 31.55
.-�-i:-- -- -.. _ t..- .-- ._.. -.T _..-...

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
WWTP Name: South Durham WRF NPDES Number: NC0047597
Monitoring Period: From OS/Ol/19 To 06/30/19
Pathogen Reduction (40 CFR 503.32/ISA NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP) _
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic _
Beta Ray _ Gamma Ray _ Pasteurization _
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens _
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion _
Anaerobic Digestion
Tfa nlirohln olh,,.
Pazameter
_. ________ _.__,,
Allowable Level in Sludge
.. ,,. �,.,,,,, ,, .,.,... .�' u.o iouow�u�monlionn�nata:
Paffio�en Density
No. of
Frequency
Sample
Analytical
Minimum Geo. Mean Maeimum Units
Escee-
dences
of
Analysis
Type
Technique
Fecal
Colifotm
2x10tothe6�' MPN
237 567 1428 MPN/g
0
Bi-monthly
Grab
9221E
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
vector pttraMion Hetlucfion (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1 Opflon/A1t.2 O tion/AIt.3
(VS reduction) X (40-day bench) 30 da bench Option/Alt. 4
( Y ) (Spec. O_ uptake)
Option/Alt. 5 Option/Alt. 6 O tion/Alt. 7
(14-Day Aerobic) (Alk Stabilization) (Dryup —Stable) (Dryin�ptUnstable)
Option/Alt. 9 Option/Alt. 10
(Injection) _ (Incorporation) _ No vector ath�action reducton alternatives were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/1 SA�VCAC 02T.1107 have been met: '
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A�VCAC OZT.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly bather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
awaze that there aze significant penalfies for false certificafion including fine and imprisonment"
Chazles Cocker. Superintendent— South Durham WRF
Prepazer Name and 'tle (print ors
Ci/sue' .,-� 2�2
Signature ofPrepazer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
*Prepazer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date
..— z ,,-.�- . � . --��. ..

South Durham Water Reclamation Facility
Sludge Report
May '2019
SD PRIMARY SLUDGE TO DIGESTER ;GRAVITY THICKENER TO ANAEROBIC DIGESTE
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons % Solids Lbs Dry % Vol Ibs VM
1 382,940 4.0 127,749 84.6 108,075
2 324,564 3.8 102,861 83.6 85,992
3 425,177 4.1 145,385 83.6 121,542 ,.,.
4 464,360 3A 129,738 84.8 110,018 'd
TOTAL 1,597,041 IS 5053732 84.2 425,626
WASTING TO GRAVffY THICKENER [TWAS GBT TO ANAEROBIC DIGESTE
WEEK Gallons % Solids Lbs Dry % Vol Ibs VMI Gallons %Solids Lbs Dry %Vol Ibs VM
t 1,568,762 0,84 109,640 70.2 76,924 162,853 6.3 85,566 69.6 59,554
2 1,24%084 0,84 87,562 69.6 60,921 ii. 1480078 13.0 160,546 65.0 104,409
3 1,005,127 0,79 66,523 70.7 47,041 i 156,913 6.8 88,989 71A 63,271
4 1,600,785 0.90 120,609 66.9 80,736 !?; 241,276 6A 127,777 71.5 91,361
TOTAL 51423,757 0.84 384,334 69.4 265,623 ,', 709,120 8.1 462,878 69.3 318,594
SO ANAEROBIC SLUDGE TO PRESS j SD SOLIDS OFF PRESS GRAVITY THICKENER TO GBT
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM ?11 Yds %Solids %Vol Gallons %Solids Lbs Dry %Vol Ibs VM
1 501,970 2.2 92,101 61.8 56,919 382 16.5 63.3 211,498 3.4 59,972 67.0 40,181
2 537,320 2.2 98,587 61.1 60,237 '. 419 16.5 63.0 192,310 4.0 64,155 60.3 38,685
3 492,798 2.3 940529 60.6 57,284397 16.7 63.2 203,783 4.0 67,982 66.7 45,344
4 820o258 2.3 157.342 62.7 98,653 659 16.6 63.7 313,346 3.9 100,612 66.6 667957
TOTAL 2,352,346 2.3 442*559 61.6 273,093 `4.. 1,856 16.6 63.3 920,937 3.8 292,721 65.2 191,168
ANAEROBIC SLUDGE TO BEDS Bni ms ncc nu we cone
Beds Yards
WEEK Gallons °/, Solids Lbs Dry %Vol Ibs VM '.I Cleaned %Solids Removed
1
2
3
4
TOTAL
Summary
Total Gallons to Anaerobic Dig.
21306,161
Total Pounds of Dry Solids to Anaerobic Dig.
9683610
Total Pounds of Vol. Solids to Anaerobic Dig.
744,221
Total Gallons from Anaerobic Dig.
21352,346
Total Ibs, of Dry Solids from Anaerobic Dig.
442*559
Total Ibs. of Vol. Solids from Anaerobic Dig,
2731093
Detention Time - Days
54
Gas Production Ft3
6,892,552
Ft3 of Gas Produced/lb of VM added
93
Reduction
59
%(VK)
Ibs Polymer
$/Ib
Pounds of Polymer Used - GBT
0
$1,75
Pounds of Polymer Used - BFP
3•435
$1.75
T WAS GBT to Anaerobic Digester is 77
of the Gravity Thckener to GBT value.
Gravity Thickenerto GBT gallon values are 80
of the meter reading in the Wasting Building.
Poly Cost $/DT
0
6,011 27,17

South Durham Water Reclamation Facility
Sludge Report
June'2019
SO PRIMARY SLUDGE TO DIGESTER
.'. GRAVITY THICKENER TO ANAEROBIC DIGESTE
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM ': Gallons % Solids Lbs Dry % Vol Ibs VM
1
322,339
4.6
123,662
81A
100,290
2
260,864
7.2
156,644
63.3
99,155 it
3
283,050
4.3
101,508
74.1
75,217
4
361,003
4.5
135,485
83.2
112,723
roTa 1,227,257 5.2 517,298 75.4 387,386
WASTING TO GRAVITY THICKENER
iTWAS GBT TO ANAEROBIC DIGESTI
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
�:' Gallons
%Solids
Lbs Dry
%Vol
SD ANAEROBIC SLUDGE TO PRESS
WEEK
Gallons
%Solids
Lbs Dry
%Vol
1
501,653
2.2
92,043
61.1
2
303,441
2.2
55,675
60.4
3
500,908
2.2
91,907
59.2
4
461,890
2.3
88,600
58.9
TOTAL,
1,767,892
2.2
328,225
59.9
ANAEROBIC SLUDGE TO BEDS
WEEK Gallons %Solids Lbs Dry %Vol
1
2
3
4
TOTAL
Summary
Ibs VM -
Yds
%Solids
%Vol
561238
362
16.7
63.6
33,628''
208
17.8
60.2
54409 ':
319
16.6
62.7
52,185
362
17.2
60.7
196,460 '!
1,251
17.1
61.8
SOLIDS OFF DRYING BEDS
Beds
Yards
Ibs VM
Cleaned
%Solids
Removed
Total Gallons to Anaerobic Dig. 1,821,430
Total Pounds of Dry Solids to Anaerobic Dig. 821,764
Total Pounds of Vol. Solids to Anaerobic Dig. 595,882
Total Gallons from Anaerobic Dig, 11767,892
Total Ibs. of Dry Solids from Anaerobic Dig. 328,225
Total Ibs. of Vol. Solids from Anaerobic Dig. 196,460
Detention Time - Days - 66
Gas Production Ft3 6,6900177
Ft3 of Gas Produced/lb of VM added 11.2
% Reduction 45 % (VK)
Ibs Polymer $/Ib
Pounds of Polymer Used - GET $1.75
Pounds of Polymer Used - BFP 2,665 $1 75
Ibs
VM
52,878
51,464
65,225
38,929
208,496
Gallons %Solids Lbs Dry %Vol Ibs VM
275
Ibs
VM
52,878
51,464
65,225
38,929
208,496
Gallons %Solids Lbs Dry %Vol Ibs VM
275
3.9
58,636
69.7
40,869
771,602 3.7 234,867 65.9 1547643
TWAS GBT to Anaerobic Digester is 77%
of the Gravity Thckener to GBT value.
Gravity Thickener to GMT gallon values are 80
of the meter reading in the Wasting Building.
Poly Cost $/DT
4,664 28.42

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQPermitNumber: W00003504
WWTP Name: South Durham WRF NPDES Number: NC0047597
Monitoring Period: From 07/01/19 To 08/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP) _
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic _
Beta Ray _ Gamma Ray _ Pasteurization _
Class B:
Alt. (I) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens _
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air D ng
rYi Composting Aerobic Digestion
Anaerobic Digestion
Tfo nl'nnl.le ..IF....
------
-- ----..----.- _............ .................a„
y �ou� �rxe xue xm�owm� momtonna data:
Pathogen Density
Pazameter
Allowable Level in Sludge
No. of
Frequency
Sample
Analytical
Minimum Geo. Mean Maximum Units
Excee-
dences
of
Analysis
Type
Technique
Fecal
Coliform
Zx10 to the 6`" MPN
power per gram of
10 li4 3422 MPN/g
0
Bi-monthly
Grab
9221 E
total solids
CFU
CFU/g
1000 MPN per gram of total
solids (dry weight)
�,IpLr/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
VeMor Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107)
Option/Alt. 1
Option/Alt. 2
(VS reduction) X
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(Injection) _
(Incorporntion)
Please indicate option/alternative performed:
Option/Alt. 3 Option/Alt. 4
(30-day bench) (Spec. 02 uptake)
Option/Alt. 7 Option/Alt. 3
(Drying —Stable) (Drying —Unstable)
CERTIFICATION STATEMENT (please check the appropriate statement)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 50333/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.3?/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/1>A NCAC 02T.1107 have not been met"(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properlyy bather and evaluate the information used to determine that the pathogen and vector ath�action reduction requirements have been met. I am
awaze dtai there aze significant penalties for false certification including fine and imprisonment
Chazles Cocker, Superintendent— South Durham WRF
Prepazer N�a�me an/dj�itle (print or Land Applier Name and Tille (if applicable) (type or print)
Signature of Prepazer* Date Si�ature of Land Applier (if applicable) Date
*Prepazer is defined in 40 CFR Part 503.9(r) and ISA NCAC 2T.1102 (26)

South Durham Water Reclamation Facility
Sludge Report
July '2019
SD PRIMARY SLUDGE TO DIGESTER '.GRAVITY THICKENER TO ANAEROBIC DIGESTE
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM ��, Gallons %Solids Lbs Dry %Vol Ibs VM
t 302,708 2.5 63, 115 86.0 54,279 :..
2 272,167 2.9 65,826 84.6 55,689
3 251,899 2.9 60,924 86.3 52,578 '�
a 405,218 3.2 108,144 84.2 91,058
TOTAL 1,231,992 2.9 298,010 85.3 253,603 '.
WASTING TO GRAVR'Y THICKENER lTWAS GBT TO ANAEROBIC DIGESTE
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM '�� Gallons %Solids Lbs Dry %Vol Ibs VM
t 979,541 1.02 83,713 67.8 56,764 + 133,546 5.2 57,916 69.1 40,020
2 979,956 1.02 83,351 68.7 57,299 155,237 6.8 88,038 68.6 60,394
3 954,150 1.07 84,942 69.0 58,647 ':. 190,822 6.4 101,853 69.3 70,584
a 1,401,243 1.05 122,485 43.9 53,740 221,237 5.9 108,862 67.1 73,046
TOTAL 4,314,890 1.04 374,491 62.4 226,449 '. 700.842 6.1 356,669 68.5 244,045
SD ANAEROBIC SLUDGE TO PRESS I SD SOLIDS OFF PRESS GRAVITY THICKENER TO GBT
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM Yds %Solids %Vol Gallons %Solids Lbs Dry °/, Vol Ibs VM
i 449,545 2.3 86,232 57.7 49,756 ', 295 17.3 59.8 173,437 4.1 59,305 61.0 36,176
2 449,778 2.3 66,276 58.0 50,040 `, 357 17.6 57.2 201,606 3.6 60,530 67.1 40,616
3 409,911 2.3 78,629 56.8 44,661 263 17.2 56.5 247,821 2.1 43,403 64.6 28,039
a 741,381 2.3 142,212 57.6 81,914 `, 571 17.0 57.8 287,321 4.1 98,247 64.6 63,467
roTAL 2,050,615 2.3 393,349 57.5 226,371 ', 1,486 17.3 57.8 910,185 3.5 261,485 64.3 168,298
ANAEROBIC SLUDGE TO BEDS ',SOLIDS OFF DRYING BEDS
Beds Yards
WEEK Gallons %Solids Lbs Dry % VoI Ibs VM '; Cleaned %Solids Removed
i
2
3
4
TOTAL
Summary
Total Gallons to Anaerobic Dig.
1,932,834
Total Pounds of Dry Solids to Anaerobic Dig.
654,679
Total Pounds of Vol. Solids to Anaerobic Dig.
497,648
Total Gallons from Anaerobic Dig.
2,050,615
Total lbs. of Dry Solids from Anaerobic Dig.
393,349
Total lbs. of Vol. Solids from Anaerobic Dig.
226,371
Detention Time -Days
gq
Gas Production Ft3
6,075,394
Ft3 of Gas Produced/Ib of VM added
12.2
Reduction
64
% (V!Q
Ibs Polymer
$/Ib
Pounds of Polymer Used -GBT
$1.75
Pounds of Polymer Used - BFP
2,760
$1.75
TWAS GBT to Anaerobic Digester is 77%
of the Gravity Thickenerto GBT value.
55 % (LBS)
Poly Cost $/DT
4,830 24.56
_..__--,-.--I ..... .. ,. _

South Durham Water Reclamation Facility
Sludge Report
August '2019
SD PRIMARY SLUDGE TO DIGESTER
GRAVITYTHICKENER TO ANAEROBIC DIGESTER
WEEK Gallons %Solids Lbs Dry
°/, Vol Ibs VM
Gallons
%Solids
Lbs Dry
%Vol Ibs VM
t 281,989 3.3 77,609
87.0
67,520
z 286,339 3.4 81,194
78.4
63,656
3 305,379 4.1 104,42t
80.4
83,955
a 444,299 3.5 127,838
82.8
105.786
rorAL 1,318,006 3.6 391,063
82.2
320,917
WASTING TO GRAVITY THICKENER
'ITWAS GBT TO ANAEROBIC DIGESTER
WEEK Gallons %Solids Lbs Dry
%Vol
Ibs VM
Gallons
%Solids
Lbs Dry
%Vol Ibs VM
t 915,388 1.02 7J,848
67.4
52,448
'. 147,592
6.3
77,548
68.3 52,965
2 875,741 1.02 74,706
68.0
50,775
131,049
6.3
68,856
67.3 46,340
a 880,528 1.03 75,922
67.1
50,914
147,753
7.0
86,258
68.2 58,828
a 1,280,151 1.09 115,957
68.8
79,800
i 178,010
5.9
87,592
68.1 59,650
TorAL 3,951,808 1.04 344,434
67.8
233,937
' 604,404
6.4
320,253
68.0 217,783
SD ANAEROBIC SLUDGE TO PRESS
SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK Gallons %Solids Lbs Dry
%Vol
Ibs VM
Yds
%Solids
%Vol
Gallons
%Solids Lbs Dry %Vol Ibs VM
t 456,021 2.4 91,277
57.5
52,484
348
17.5
58.9
197,569
3.9 64,261 66.4 42,669
2 403,691 2.3 77,436
57.9
44,835
'. 274
17.6
58.3
189,810
3.1 49,073 66.6 32,683
3 429,280 2.3 82,344
58.1
47,842
324
17.5
59.4
203,907
3.6 61,221 65.0 39,794
a 599,782 2.3 115,050
57.2
65,809
434
17.5
58.4
235,424
3.9 75,592 65.8 49,702
ioiAL 1,888,774 2.3 366,108
57.7
210,971
;, 1,380
17.5
58.8
826,710
3.6 250,148 66.0 164,848
ANAEROBIC SLUDGE TO BEDS
(SOLIDS OFF DRYING BEDS
Beds
Yards
WEEK Gallons %Solids Lbs Dry
%Vol
Ibs VM
� Cleaned
%Solids
Removed
t
2
3
4
TOTAL
Summary
Total Gallons to Maerobic Dig.
1,922,410
Total Pounds of Dry Solids to Anaerobic Dig.
711,316
Total Pounds of Uol. Solids to Anaerobic Dig.
538,700
Total Gallons from Anaerobic Dig.
1,888,774
Total lbs. of Dry Solids from Anaerobic Dig.
366,108
Total lbs. of Vol. Solids from Maerobic Dig.
210,971
Detention Time -Days
65
-
Gas Production Ft3
6,141,382
Ft3 of Gas Produced/Ib of VM added
11.4
% Reduction
61
% (VKJ
61 °/, (LBS)
Ibs Polymer
$!Ib
Poly Cost
$/DT
Pounds of Polymer Used -GBT
$1.75
Pounds of Polymer Usetl - BFP
3,110
$1.75
5,443
29.73

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ permit Number: W00003504
WWTP Name: South Durham WRF NPDES Number: NC0047597
Monitoring Period: From 09/01/19 To ]0/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (flme/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) _
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP) _
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying Heat Treatment _ Thermophilic _
Beta Ray _ Gamma Ray _ Pasteurization _
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting _ Aerobic Digestion
Anaerobic Digestion
Tfa nlirahlnM olio.
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10tothe6'^ MPN
1 782 84656 MPN/g
0
Bi-monthly
Grab
9221E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
colifonn
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternativeporformed: '
0ption/Alt. 1 Option/Alt. 2 Option/Alt. 3 O tion/Alt 4
(VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake)
Option/Alt.S Option/Alt.6 Option/Alt.7 0 hon/AIt.B
(14-Day Aerobic) (Alk Stabilization) (Drying— Stable) (Drying P Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met
"I certify, under penalty of ]aw, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/liA NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
awaze that there aze significant penalfies for false certification including fine and imprisonment
Chazles Cocker, Superintendent— Souffi Durham WRF
Preparer Name and itle (print o yN) Land Applier Name and Title (if applicable) (type or print)
Signature of Prepazer* Date Signature of Land Applier (if applicable) Date
*Prepazer is defined in 40 CFR Part 503.9(r) and liA NCAC 2T.1102 (26)

South Durham Water Reclamation Facility
Sludge Report
September '2019
SD PRIMARY SLUDGE TO DIGESTER
GRAVITY THICKENER TO ANAEROBIC DIGESTER
WEEK
Gallons
%Solids
Lbs Dry
% Vol
Ibs VM
Gallons
%Solids
Lbs Dry
% Vol
Ibs VM
1
303,007
3.3
83,394
86.7
72,302
2
305,389
3.8
96,784
86.2
83,428
3
320,882
3.5
93,666
85.3
79,897
4
432,689
3.8
137,128
83.7
114,776
TOTAL
1,361,968
3.6
410,971
85.5
350*403
WASTING TO GRAVITY THICKENER
TWAS GBT
TO ANAEROBIC DIGESTER
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
1
896,251
1.13
84,796
69.3
58,773
145,052
6.0
72,584
69.1
50,156
2
896,395
1,19
88,814
70.7
62,766
165,296
6.0
82,714
70A
58,231
3
928,866
1.18
91,423
73.9
670563
166,954
6.0
83,544
71.1
59,400
4
1,213,474
1.04
105,319
71.3
75,129
180,002
5.5
82,567
71A
58,705
TOTAL
3,934,986
1.14
370,352
71.3
2640231
657,304
5.9
321,409
70A
226,491
SD ANAEROBIC SLUDGE TO PRESS
SD SOLIDS OFF PRESS
WEEK Gallons % Solids Lbs Dry % Vol
Ibs VM
Yds
% Solids
% Vol
1 411,536 2.3 78,941 57.5
45,391
327
17.1
56.9
2 470,344 2.2 863299 57.0
49,190
349
16.9
57.1
3 4382252 2.3 84,065 58.8
490431
342
16.8
59.8
4 496,071 2.2 91,019 58.6
53,337
297
17A
59.7
TOTAL 1,8163203 2.3 340,324 58.0
197,349
1,315
17.0
58A
ANAEROBIC SLUDGE TO BEDS
SOLIDS OFF DRYING
BEDS
Beds
Yards
WEEK Gallons % Solids Lbs Dry % Vol
Ibs VM
Cleaned
% Solids Removed
7
2
3
4
TOTAL
SummarV
Total Gallons to Anaerobic Dig.
2,019,272
Total Pounds of Dry Solids to Anaerobic Dig.
732,380
Total Pounds of Vol. Solids to Anaerobic Dig.
576,894
Total Gallons from Anaerobic Dig.
118167203
Total Ibs. of Dry Solids from Anaerobic Dig.
340t324
Total Ibs. of Vol. Solids from Anaerobic Dig,
1973349
Detention Time - Days
60
Gas Production Ft3
61241,521
Ft3 of Gas Produced/lb of VM added
10.8
% Reduction
67
% (VK)
66 %
(LBS)
Ibs
Polymer
S/lb
Poly Cost
Pounds of Polymer Used - GBT
$1.75
Pounds of Polymer Used - BFP
2,760
$1,75
4,830
GRAVITY THICKENER TO GBT
Gallons
%Solids
Lbs Dry
%Vol
170,932
3.7
52,746
67.9
203,426
3.8
64,470
66.8
2417579
3.6
72,532
69.3
242,800
3.4
683848
68.2
858,737
3.6
258,596
68.1
6�L�iY
28.38
35,815
43,066
50,264
46,955
176,100

South Durham Water Reclamation Facility
Sludge Report
October '2019
SD PRIMARY SLUDGE TO DIGESTER"'GRAVITY
THICKENER TO ANAEROBIC DIGESTER
WEEK
Gallons
%Solids
Lbs Dry
°/, Vol
bs VM
i Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
t
303,757
3.6
91,200
86.7
79,071
2
314,933
3.7
97,182
86.3
83,868
"�.
s
307,930
2.9
74,476
86.4
64,347
a
426,708
4.2
149,467
79.fi
118,976
h.
TOTAL
1,353,328
3.6
412,325
84.8
346,262
WASTING TO GRAVITY THICKENER
"rTWAS GBT TO ANAEROBIC DIGESTER
wEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
I Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
t
914,865
1.04
79,570
72.0
57,262
":P. 122,665
6.0
61,382
70.5
43,274
2
910,097
1.15
87,212
71.1
62,014
', 183,802
5.9
90,442
71.0
64,214
3 -
909,701
1.11
84,095
71.7
60,324
'.�-. 120,776
6.0
60,436
73.4
44,360
a
1,300,308
1.17
126,838
72.0
91,285
"- 208,020
6.4
111,033
70.7
78,500
TOTAL
4,034,971
1.12
377,715
71.7
270,885
=, 635,263
6.1
323,292
71.4
230,348
SD ANAEROBIC SLUDGE TO PRESS
C. SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK
Gallons
%Solids
Lbs Dry
°/, Vol
Ibs VM
' Yds
%Solids
°/, Vol
Gallons
%Solids Lbs Dry %Vol
t
386,216
2.2
70,863
59.1
41,880
� 297
16.5
61.2
140,764
3.4 39,915 69.2
2
451,357
2.2
82,815
59.8
49,523
-! 303
16.3
62.7
222,705
3.8 70,580 69.9
s
303,471
2.0
50,619
60.9
30,827
349
16.4
63.7
140,870
3.8 44,645 70.4
a
626,280
2.1
109,687
60.4
66,251
':�' 457
16.9
63.5
278,334
4.1 95,174 70.0
roTAL
1,767,324
2.1
313,984
60.1
188,481
; 1,405
16.5
62.8
782,673
3.8 250,313 69.9
ANAEROBIC SLUDGE TO BEDS
! SOLIDS OFF DRYING BEDS
Beds
Yards
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
i' Cleaned
°/, Solids
Removed
t
z
3
4
TOTAL
Summary
Total Gallons to Anaerobic Dig. 1,988,591
Total Pounds of Dry Solids to Anaerobic Dig. 735,617
Total Pounds of Vol. Solids to Anaerobic Dig. 576,610
Total Gallons from Anaerobic Dig. 1,767,324
Total lbs. of Dry Solids from Anaerobic Dig. 313,984
Total lbs. of Vol. Solitls from Anaerobic Dig. 188,481
Detention Time -Days 63
Gas Production Ft3 6,533,262
Ft3 of Gas Produced/Ib of VM added 11.3
Reduction sa % �vx� s7 i ices)
Ibs Polymer $/Ib Poly Cost $/DT
Pounds of Polymer Used -GBT $1.75
Pounds of Polymer Used - BFP 3,150 $1.75 5,513 35.11
Ibs VM
27,621
49,335
31,430
66,621
175,008
-,..
_. �
��a
...-,- . ,-.
-
-�.-
�.�..
__�-.-
.�.
,�.,__

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQPermitNumber: W00003504
WWTP Name: South Durham WRF NPDES Number: NC0047597
Monitoring Period: From I1/Ol/19 To 12/31/19
Pathogen Reduction (40 CFR 503.32/ISA NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying _ Heat Treatment _ Thermophilic _
Beta RaY _ Gamma Ray _ pasteurization _
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens _
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion _
Anaerobic Digestion
If annlicahle +n alrn�narivo ,.o.n,..sa �l-�.,......_ n.___ n. . . .. .. ... .. ..�
eae me ronowm monrtonna tlata•
Pathogen Density
Minimum Geo. Mean Maximum Units
1204 5231 li095 MPN/g
Pazameter
Fecal
Coliform
Allowable Level in Sludge
2x10 to ffie 6v' MPN
power per gram of
No. of
Excee-
dences
0
Frequency
of
Analysis
Bi-monthly
Sample
Type
Grab
Analytical
Technique
9221 E
total solids
CFU
CFU/g
1000 MPN per gram of total
solids (dry weight)
MpN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
0ption/Alt 1 Option/Alt. 2 Option/Alt. 3 O tion/Alt. 4
(VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake)
Option/Alt 5 Option/Alt 6 0 tion/Alt. 7
(14-Day Aerobic) (Alk Stabilization) (Dryin —Stable) (Dryin�P Unstabtle)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector attacton
X reduction requirement m 40 CFR 503.33/liA�VCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A�VCAC 02T.1107 have not been met "(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properlyy gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
awaze ffiat there aze significant penalties for false certification including fine and imprisonment"
_ Chazles Cocker, Superintendent —South Durham WRF
Prepazer Name and Title (print or e)
Signature ofPrepazer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Prepazer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

South Durham Water Reclamation Facility
Sludge Report
November'2019
. SD PRIMARY SLUDGE TO DIGESTER GRAVITY THICKENER TO ANAEROBIC DIGESTER
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons % Solids Lbs Dry % Vol Ibs VM
1 286,628 3.5 83,667 86.0 71,953
2 303,608 3.6 91,155 87.4 79,670
3 291 t607 3.3 80,256 85.4 68,539 T..
4 390,401 3.8 123,726 88.0 108,879
TOTAL 1,272,245 3.6 3782804 86.7 329,041
WASTING TO GRAVITY THICKENER TWAS GBT TO ANAEROBIC DIGESTER
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Gallons % Solids Lbs Dry % Vol Ibs VM
1 9105121 1,08 82,031 74.1 60,766 .+', 162,166 6.1 82,500 72.0 59,400
2 910,035 1,22 92,291 78.0 72,005 113,896 6.8 64,593 73.6 47,540
3 910,000 1.04 79,092 75.2 59,460 ( 157,965 6.0 79,046 74.4 58,810
4 1,1511113 1,02 97,678 75.1 73,398 `. 1320610 5.5 60,275 75.2 45,327
TOTAL 3,881,270 1,09 351,091 75.6 265,630 566,637 6.1 286,414 73.S 211,077
SD ANAEROBIC SLUDGE TO PRESS -! SD SOLIDS OFF PRESS GRAVITY THICKENER TO GBT
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Yds % Solids % Vol Gallons % Solids Lbs Dry % Vol Ibs VM
1 402,316 2.1 70,462 61.3 43,193 261 16.6 63.3 212,527 4.3 76,216 69.4 52,894
2 361,948 2.2 66,410 60.4 40,112 " 261 16.7 64,0 143,734 4,0 47,950 65.7 31,503
3 475,290 2.2 87,206 61.3 53,457 327 16.9 63.6 211,053 4.3 75,688 73.6 550706
4 361,397 2.2 64,802 62.0 40,177 '' 280 17.0 64.8 178,472 4.5 662236 73.7 48,783
TOTAL I,600,951 2.2 2882880 61.3 176,939 12128 16.8 63.9 745,786 43 2663090 70.6 188,886
ANAEROBIC SLUDGE TO BEDS SOLIDS OFF DRYING BEDS
Beds Yards
WEEK Gallons % Solids Lbs Dry % Vol Ibs VM Cleaned % Solids Removed
1
2
3
4
TOTAL
Summary
Total Gallons to Anaerobic Dig. 11838,882
Total Pounds of Dry Solids to Anaerobic Dig. 665,218
Total Pounds of Vol. Solids to Anaerobic Dig, 540,118
Total Gallons from Anaerobic Dig, 1,600,951
Total lbs. of Dry Solids from Anaerobic Dig. 288,880
Total Ibs. of Vol. Solids from Anaerobic Dig, 176,939
Detention Time - Days 66
Gas Production Ft3 5,926,900
Ft3 of Gas Produced/lb of VM added 11,0
%Reduction 67 %(VK) 67%(LBS)
Ibs Polymer $/lb Poly Cost $/DT
Pounds of Polymer Used - GBT $1,78
Pounds of Polymer Used - BFP 23385 $1,75 4,174 28,90

Pounds of Polymer Used -GBT
Pounds of Polymer Used - BFP
South Durham Water Reclamation Facility
Sludge Report
December '2019
SD PRIMARY SLUDGE
TO DIGESTER
wEEK Gallons %Solids
Lbs Dry
% VOI
Ibs VM
i 306,261
3.8
97,060
85.6
83,035
z 338,093
3.0
64,591
87.4
73,932
s 293,070
3.5
85,547
84.9
72,629
a 398,835
3.2
106,441
88.6
94,307
TOTAL 1,336,259
3.4
373,639
86.6
323,90a
WASTING TO GRAVITY THICKENER
WEEK
Gallons
%Solids Lbs Dry
% VoI
Ibs VM
i
888,685
1.04
77,240
75.7
58,467
2
911,014
1.09
83,066
77.2
64,086
3
910,713
1.10
83,636
76.4
63,922
a
1,300,667
1.08
117,566
76.0
89,361
TOTAL
4,011,079
1.08
361,508
76.3
275,856
SD ANAEROBIC SLUDGE TO
PRESS
WEEK
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
i
479,263
2.2
87,935
61,5
54,080
2
474,800
2.1
83,156
87.7
72,928
3
576,731
2.2
105,819
62.7
66,348
a
380,385
2.1
66,621
62.9
41,904
TOTAL
1,971,179
2.2
343,531
68.7
235,261
ANAEROBIC SLUDGE TO BEDS
WEEK Gallons %Solids Lbs Dry %Vol Ibs VM
i
z
3
4
TOTAL
Summary
Total Gallons to Anaerobic Dig. 2,047,923
Total Pounds of Dry Solids to Anaerobic Dig. 711,303
Total Pounds of Vol. Solids to Anaerobic Dig. 579,665
Total Gallons from Anaerobic Dig. 1,911,179
Total lbs. of Dry Solids from Anaerobic Dig. 343,531
Total lbs. of VoI. Solitls from Anaerobic Dig. 235,261
Detention Time -Days - 61
Gas Production Ft3 6,233-,281
Ft3 of Gas Produced/Ib of VM added 10.g
Reduction 55 % (VK)
Ibs Polymer $/Ib
$1.75
2,520 $1.75
GRAVITY THICKENER TO ANAEROBIC DIGESTER
Gallons %Solids Lbs Dry %Vol Ibs VM
TWAS GBT TO ANAEROBIC DIGESTER
Gallons
%Solids
Lbs Dry
%Vol
Ibs VM
139,494
5.8
67,476
75.6
51,012
215,319
5.5
98,767
76.0
75,063
164,100
6.3
86,221
76.3
65,787
192,751
5.3
85,200
75.0
63,900
711,664
5.7
337,664
75.7
255,761
SD SOLIDS OFF PRESS
GRAVITY
THICKENER TO GBT
Yds
°/a Solids
%Vol
Gallons
%Solids
Lbs Dry
%Vol
327
16.9
64.8
160,735
5.0
67,026
74.2
350
16.8
65.3
228,404
4.3
81,910
74.7
389
16.6
66.2
231,896
4.7
90,899
74.5
251
16.4
64.9
193,383
4.8
77,415
74.2
1,317
16.7
65.3
814,418
4.7
317,250
74.4
SOLIDS OFF DRYING
BEDS
Beds
Yards
Cleaned
%Solids Removed
59 % (LBS)
Poly Cost $/DT
4,410 25.67
Ibs VM
49,734
61,187
67,719
57,442
236,082

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQPermitNumber: W00003504
WWTP Name: Brown WTP NPDES Number: 03-32-010(A) _
Monitoring Period: From Ol/Ol/2019 To 03/31/Z019
Pathogen ReduMion (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alteroative performed:
Class A:
Alt. I/A (time/temp) Alt 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment _ Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilizaffon Air Drying Composting Aerobic Digestion _
Anaerobic Digestion
If annlicahle to alrernar:vn nnrfn.,..�d mi.,��e,..r�......u�,.,..__._._.�_:_n___: ______�._
Parameter
- ---
Allowable Level in Sludge
-- -- ----- - ---- --._ �.._ ............ ...............- ua.a.
Pathogen Density
No. of
Fre uenc
4 Y
Sam le
P
Anal ical
Yt
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6`"
MPN
MPN/g
Coliform
power per gram of
total solids
CFU
517
1047
2690
CFU/g
0
4/Yr
Grab
9222D
1000 MPN per gram of total
MpNr/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option alternative performed:
Option/Alt. I Option/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake)
Opfion/Alt 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 3
(14-Day Aerobic) (Alk Stabilization) (Drying -Stable) (Drying- Unstable)
Option/Alt. 9 Option/Alt. 10
(Inlectron) _ (Incorporafion) _ No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met:'
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/1 SA NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC OZT.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
awaze that there aze significant penalties for false cerfification including fine and imprisonment"
Tom Lucas, Assiut Suroerintendent Brown WTP
Pr/e/p/p_}'er Na�me�an,�d Title (print ortype) / Land Applier Name and Title (if applicable) (type or print)
Signature of Prepazer* Date Signature of Land Applier (if applicable) Date
*Prepazer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
_ .,. -. __-u.,,—� �-.—.- ... - � — ��__ -

FECAL DATA SHEET
Lab result
Log
2078
3.32
Min
2690
3.43
Max
538
2.73
Geometric Mean
532
2.73
1033
3.01
517
2.71
1614
3.21
Average
3.02
511
2690
1047

Page 1
Contact: Nate Roth Report Date: 1/17/2019
Client: Synagro
284 Boger Road Project: Durham -Brown WTP
Mocksville, NC 27028 Date Sample Rcvd: 1/7/2019
Meritech Work Order # 01071911 Sample: Durham -Brown Feca11 of 4 Grab 1/7/19
Parameters Results AnaysisDate ReportingLimlt et
%Total Solids 17.5 % 1/8/19 0-100 o/n SM 2540B
Fecal Coliform (Sludge) 2,078 col/g drywt 1/7/19 258 col/g drywt SM 9222D
Meritech Work Order #
01071912 Sample:
Durham -Brown
Feca11 of 4 Grab
1/7/19
Parameters
Results
AnalysisDatg
Reporting►�imit
Method
°/a Total Solids
16.9 %
1/8/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,690 col/g drywt
1/7/19
258 col/g drywt
SM 4222D
Meritech Work Order #
01071913
Sample:
Durham -Brown
Feca11 of 4
Grab
1/7/19
Parameters
esu t
Analysis Date
Re on rrir{g
Limit
Method
%TotalSoIids
16.9
%
1/8/19
0-100
%
SM 2540B
Fecal Coliform (Sludge)
<538
col/g dry wt
1/7/19
538
col/g dry wt
SM 9222D
Meritech Work Order #
01071914
Sample:
Durham -Brown
Feca11 of4
Grab
1/7/19
Parameters
Results
�nalysisDate
Reporting Limit
et d
%Total Solids
17.1
%
1/8/19
0-100
%
SM 2540B
Fecal Coliform (Sludge}
<532
col/g dry wt
1/7/19
S32
col/g dry wt
SM 9222D
Meritech Work Order #
01071915 Sample:
Durham -Brown
Feca11 of 4 Grab
1/7/19
Parameters
R U15
Analysis Date
ReportingLirnit
et d
%Total Solids
17.6 %
1/8/19
0-100 %
SM 25408
Fecal Coliform (Sludge)
1,033 cot/g dry wt
1/7/19
258 col/g drywt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
-,--�—r.-.
.�
1
_ ..
�
__ _.
a
— _ -.

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No,165
Contact: Nate Rotb
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech Work Order # 01071916
Parameters Results
Page 2
Report Date: 1/17/2019
Project: Durham -Brown WTP
Date Sample Rcvd: 1/7/2019
Sample: Durham -Brown Fecal 1 of4 Grab
Ana�sis Date Reporting Limit
%Total Solids
Fecal Coliform (Sludge)
17.6
<517
%
col/g dry wt
1/8/19
1/7/19
0-100
514
%
col/g dry wt
Meritech Work Order #
01071917
Sample:
Durham -Brown
Fecal 1 of 4
Grab
Parameters
Its
Analysis Date
Reporting Limit
%Total Solids
16.9 %
1/8/19
0-100 %
Fecal Coliform (Sludge)
1,614 col/g dry wt
1/7/19
228 col/g dry wt
SM 2540B
SM 9222D
1/7/14
4ethod
SM 2540B
SM 4222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
Yel.[phone] fax.[336)342-1522

arona
Chain of Custody Record (COC)
NPDES#:
L Phone:
�
IT` IH/ INC.
Address: fir:-
-I�.� � Fax:
ENVIRONMENTAL LABORATORIES
I��OZ-Vnxj\ -e' �i( Email: Y'
i
t�
'm[A'ri
.
)�
` 642 Tamco Rd. Phone: [phone]
Project:
j �jt
�l L4
L -vti� Zi�jn {tyl�p
-
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:- i\IL5<.!L>Yit
TurnAround Time*
How would you like our report sent?
'RUSH
work needs prior approval,
www.meritechlabs.com
ch r es Apply
Circle all that apply: Email referred), Fax, Mail std
0
a s) 3-5 Days 2a-4aHrs
Sampling bates &Times
pers Takings mple (Si nfpri t): )
Itt
Lab use only
Sample Location and/or ID #
�� �✓
Start End
Date Time Date Time
Comp?
Grab?
#of
Cont.
Test(s) Required
on Ice?
Yes No
pH OK?
Cl OK?
3
13
S
�
Temperature Upon
Receipt:
Method of
" Dechlorination
(<0.5 ppm)
of Ammonia, Cyanide,
Phenol and TKN samples must be done in the field prior to preservation. "•"
j
Shipment:
Comments:
Compositor #
Jug #
UPS
Fed Ex
Are these results r regul ory purposes? Yes _
No Q Report results in: mg/L
mg/kg 13� ug(L IL
- Hand Delivery
Relinquished by: qq Date: � Time;
/f. c-.. —)!
C—z Received b y
Date:
Time:
Other
Relinquished by: Date: Time:
J
Received
Date:
Time:
Relinquished by: Date: Time:
Received b
f
"DQTp
�,I rime: }

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQPermitNumber: W00003504
WWTP Name: Brown WTP NPDES Number: 0332-010(A)
Monitoring Period: From 4/1/2019 To 6/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP) _
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying Heat Treatment Thermophilic _
Beta Ray _ Gamma Ray _ Pasteurization _
Class B: .
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion _
Anaerobic Digestion
If a Iicable to alternative erformed Class A or Class B com lete the followin 't '
Pazameter
Allowable Leve] in Sludge
mom on.,- �a,a:
Pathogen Density
No.
of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6`" MPN
Mprr/g
Coliform
power per gram of
total solids
CFU
380
1800
4587
CFU/g
0
4/Yr
Crab
9222D
1000 MPN per gram of total
MpNr/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option alternative performed:
Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake)
0 tion/Alt. 5 p Option/Alt 7 Option/Alt. 8
(14-Da Aerobic) (AIkSOtabilization) (Drying —Stable) (Drying —Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of ]aw, that the pathogen requirements in 40 CFR 503.32/1 iA NCAC 02T.1106 and the vector amaction
X reduction requrement m 40 CFR 503.33/ISA NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met " (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to detemrine that the pathogen and vector attraction reduction requirements have been met. I am
awaze that there aze significant penalties for false certification including fine and imprisonment."
Tom Lucas, .k�fsixet Superintendent Brown WTP
Pr azer N�a%me�and Title (print or type)
—�li �/2v/�207�a
Signature of Prepazer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
*Prepazer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T.1102 (26)
Date

FECAL DATA SHEET
Lab result
Log
4484
3.65
Min
380
2.58
Max
1934
3.29
Geometric Mean
4,587
3.66
3719
3.57
429
2.63
2537
3.40
Average
3.26
380
4587
1800
m. ,—�,�,
�
-
�—�---
-
.

� .�� �
.��
Page 1
Contact: Ryan Copeland
Report Date:
4/30/2019
Client: Synagro
284 Boger Road
Project:
Durham Brown Plant
Mocksville, NC 27028
Date Sample Rcvd:
4/16/2019
Meritech Work Order # 04161915 Sample:
D.B. Fecals 2 of 4
(1) Grab
4/16/19
Parameters Re ut
Analysis Date
Reporting Limit
t o
%Total Solids 22.3 o/o
4/18/19
0-100 %
SM 2540B
Fecal Conform (Sludge) 4,484 col/g dry wt
4/16/19
258 col/g dry wt
SM 9222D
Meritech Work Order #
04161916 Sample:
D.B. Fecals 2 of 4 (2) Grab
4/16/19
Parameters
ults
Ana sisDate RegortingLimit
Metho
%Total Solids
23,9 %
4/18/19 0-100 %
SM 2546B
Fecal Coliform (Sludge}
380 col/g drywt
4/16/19 2S8 col/g drywt
SM 9222b
Meritech Work Order #
04161917 Sample:
D.B. Fecals 2 of 4 (3) Grab
4/16/19
Parameters
a Its
Analysis Date $gporting�i imit
M t o
%Total Solids
23.5 %
4/18/19 0-100 %
SM 2546B
Fecal Coliform (Sludge}
1,934 col/g drywt
4/16/19 258 col/g dry wt
SM 9222D
Meritech Work Order # 04161918 Sample: D.B. Fecals 2 of 4 (4) Grab
Parameters Rents Analy Ss Date Remo ingLimit
%Total Solids 21.8 % 4/18/19 0-100
Feca] Coliform (Sludge) 4,587 col/g dry wt 4/16/19 258 col/g dry wt
Meritech Work Order # 04161919 Sample: D.B. Fecals 2 of 4 (5) Grab
Parameters Results Analysis Date Reporting Limit
%Total Solids 22.0 % 4/18/19 0-100
Fecal Coliform (Sludge) 3,719 col/g drywt 4/16/19 258 col/g drywt
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
4/16/19
Method
SM 2540B
SM 9222D
4/16/19
Met d
SM 2S46B
SM 9222D

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Report Date: 4/30/2019
Project: Durham Brown Plant
Date Sample Rcvd: 4/16/2019
Meritech Work Order # 04161920 Sample: D.B. Fecals 2 of 4 (6) Grab 4/16/19
Parameters its Ana�ysisDate R�ortirtgLimit Method
%Total Solids 21.2 % 4/18/19 0-100 % SM 25408
Fecal Coliform (Sludge) 429 col/g dry wt 4/16/19 252 col/g dry wt SM 9222D
Meritech Work Order # 04161922 Sample: D.B. Fecals 2 of 4 (7) Grab
4/16/19
Parameters
a ul
Analysis Date
Reporting Limit
Method
%Total Solids
21.5 %
4/18/19
0-100 %
SM 2540E
Fecal Coliform (Sludge)
2,537 co]/g drywt
4/16/19
228 col/g drywt
SM 9222D
I hereby certrJy that I have reviewed and approve these data.
aboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
.-..—.

Chain of Custody Record (COQ
Client: SyA
NPDES#;
Phone:
MER1
lT INC.
i
Address:. % q
Fax:
ENVIRONMENTAL LABORATORIES
M01KSViLL6
Imo(
Email:Q%PEiat9
CJS;tyF�fCo�o2j
642 Tamco Rd. Phone: [phone]
Project: pURHfhM
6{otdN iDD�Anri`
-__ -
Reidsville NC 27320 Fax: [phone]
p O #:
Email: [e-mail]
Attention: l`'�nn� I,`oPEtjkNO
Turn Around Time*
How would you
like your report
sent? *RUSH
work needs prior approval.
www.meritechiabs.com
Circle all that apply:
Email referred),
Fax, Mail Std 10 a s) S�s I 24•48H�rs
Sampling Dates &Times
Person TakingSample(Sign/Print):
Lab Use Only
Sample Location
and/or ID # Start End
Date Time Date Time
Comp?
Grab?
#of
Cont.
Test s Required
( ) Cj
yes
PH-O.P.
v..
vv—"
/.No
Cjog?
6-
i
i'�cst?
�a�
I S
2
1.
3
3.1
S
}�
�b
7e(npe(ature,Upop Receipt:
Method of
*** Dechforination (<O.S ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done
in the field prior to
preservation.
Comments:
Com osttor #
.
UPS
Fed Ex
AreAre these results for regulatory purposes? Yes
No
Report results
in: mg/h [a mg/kg
ug/L
Hand
Relinquished by: Time: '�-
KYP0 Date: 4 &l -
Received by:
Date:
Tim e:
Other
Relinquished by: Date; Time:
Received by:
Date:
Time:
s
Relinquished by: Date: 'rime:
v L b:
�Tr

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City ofDurham WQ Permit Number: W00003504
WWTPName: BrownWTP NPDESNumber: 03-32-010(A)
Monitoring Period: From 7/01/2019 To 9/30/2019
Pathogen Reduction (40 CFR 50332/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) _ Alt. 2B (Alk Treatment) _ Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost _ Heat Drying Heat Treatment Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization _
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class S only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting _ Aerobic Digestion
Anaerobic Digestion
tr., "r��tiie
Vector
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6t°
MPN
MPNr/g
Coliform
power per gram of
total solids
CFU
494
711
1507
CFU/g
0
4/Yr
Grab
9222D
1000 MPN per gram of total
MPNr/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option alternative performed:
0ption/AltI 1 Option/AltI 2 Option/Alt. 3 Option/AIt. 4
(VS reduction) (40-day bench) (M-day bench) (Spec. 02 uptake)
Option/Alt. 5 Option/Alt. 6 Option/Alt, 7 Option/Alt. 8
(14-Day Aerobic) (A1kStabilization) (Drying —Stable) (Drying —Unstable)
Option/Alt, 9 Option/Alt. 10
(Injection) _ (Incorporation) _ No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attractionX reduction requirement in 40 CFR 50333/15A*KCAC 02T.1107 have been met
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A KCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly bather and evaluate the information used to determine that the pathogen and vector attraction redu
aware that there are significant penalties for false certification including fine and imprisonment: " ction requirements have been met. I am
Tom Lucas, A59609W Superintendent Brown WTP
Pr w N e and Title (print or type) Land Applier Name and Title (if applicable) (type or print)
�2/;�
Signature of Prepazer* Date Signature of Land Applier (if applicable) Date
*Prepazer is defined in 40 CFR Part 503.9(r) and ISA NCAC 2T.1102 (26)

FECAL DATA SHEET
Lab result
Log
1507
3.18
Min
999
3.00
Max
988
2.99
Geometric Mean
497
2.70
494
2.69
508
2.71
494
2.69
Average
2.85
494
1507
711

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No, 165
Contact: Nate Roth Page
Report Date: 8/2/2019
Client: Synagrc
284 Boger Road Project: Durham -Brown
Mocksville, NC 27028 Date Sample Rcvd: 7/24/2019
Meritech Work Order # 07241977 Sample: Durham -Brown Fecal 1 Grab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 18.1 % 7/25/19 0400 % SM 2540B
Fecal Coliform (Sludge) 1,507 col/g dry wt 7/24/19 258 col/g dry wt SM 9222D
Meritech Work Order # 07241978 Sample: Durham -Brown Fecal 2 Grab 7/24/19
Parameters Results Ana ysisDate ReportingUral Method
% Total Solids 18.2 % 7/25/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 999 col/g dry wt 7/24/19 258 col/g dry wt SM 9222D
Meritech Work Order # 07241979 Sample: Durham -Brown Feca13 Grab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 18.4 % 7/25/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 988 col/g dry wt 7/24/19 258 col/g dry wt SM 9222D
Meritech Work Order # 07241980 Sample: Durham -Brown Fecal 4 Grab
Parameters Results Analysis Date Reng Limit
%Total Solids 18.3 % 7/25/19 0-100 %
Fecal Coliform (Sludge) 497 col/g dry wt 7/24/19 258 col/g dry wt
porti
Meritech Work Order # 07241981 Sample: Durham -Brown Fecal Grab
Parameters Results Analysis Date Re on rting Limit
% Total Solids 18.4 % 7/25/19 0400 %
Fecal Coliform (Sludge) <494 col/g dry wt 7/24/19 494 col/g dry wt
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.(336J342.1522
7/24/19
tbod
SM 2540B
SM 9222D
7/24/19
Method
SM 2540B
SM 9222D

Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Report Date: 8/2/2019
Project: Durham -Brown
Date Sample Rcvd: 7/24/2019
Meritech Worlc Order #
07241982 Sample:
Durham -Brown
Feca16 Grab
Parameter
Results
Analysis Date
RenortingLimit
%Total Solids
17.9 %
7/25/19
0400 %
Fecal Coliform (Sludge)
<508 col/g dry wt
7/24/19
508 col/g dry wt
Meritech Worlc Order # 07241983 Sample: Durham -Brown Fecal 7 Grab
Parameters Results Analysis Date Lte ou rung Limit
%Total Solids 18A % 7/25/19 0-100 %
Fecal Coliform (Sludge) <494 col/g dry wt 7/24/19 494 col/g dry wt
7/24/19
Method
SM 2540B
SM 9222D
7/24/19
tbod
SM 2540B
SM 9222D
I hereby certify that I have reviewed and approve these data. `—� C=A
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

e sna
Chain of Custody Record (COQ
C
Client: JN4U2Lr,)
JZB�
NPDES#:
Ph
MER IT INC.
1
Address:
,
{Sce"qL (awAn Fax:ne:
ENVIRONMENTAL LABORATORIES
fficj4; ; cn
A)C Email:
5)JyW,,L
642 Tamco Rd. Phone: [phone]
/noo
Project: {JtYtlm
2r JAJ
Reidsville NC27320 Fax: [phone]
P.O.#:
Email: info@meritech[abs.com
Attention:
Turn Around Time*
How would
you like your report sent? *Ruse work needs prior approval,
www.meritechlabs.com
Char esA I
Circle all that apply: Email referred), Fax, Mail std 0 as)
3-sDays za-aRHrs
Sampling Dates & Times
Person TakingSample(Sign/Print):
Lab Use Only
Sample Location
and/or ID #
Start End
Date Time Date Time
Comp?
If of
Test(s) Required
fees
pH OK?
Grab?
CoFnt.
Yes / No
N
Cl OK?
Z
P
3
ii
<U
-
Temperature Upon
?
Method of
"` Dechlorination <0.5 ppm} of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Receipt: j,. }
Shipment:
Comments:
Compositor
P
UPS
Fed Ex
Are these results for regulatory purposes? Yes -
No
Report results in: mg/L mg/kg
Jug #
ug/L
�- Hand DellVery
Relinquished by: Date: 7{ r Time:
- ; f�� IZylly
r Receivedb
I J� Y.
Date:
Time:
Other
Relinquished by: Date: Time:
Received by:
Date:
Time:
Relinquished by: Date: Time:
Receiv
b: t f

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: CityofDurham WQPermitNumber. W00003504
WWTP Name: Brown WTP NPDES Number: 03-32-010(A)
Monitoring Period: From 10/Ol/2019 To 12/31/19
Pathogen ReduMion (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt 1/A (timehemp) Alt. 2/B (Alk Treatment) Alt 3/C (Prior Testing)
Alt. 4/D (No Prior Test) _ Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Theanophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class S:
Alt (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class S only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Pazameter
Allowable Level in Sludge
Pathogen Density
No, of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
Coliform
2x10 to the 6`s
power per gam of
MPN
MpN/g
total solids
CFU
522
594
1089
CFU/g
0
4/Yr
Grab
9222D
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 gams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector AttraMion Reduction (40 CFR 503.33/15A NCAC 02T.110'/) -Please indicate option alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(AlkStabilization)
(Drying —Stable)
(Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection) _
(Incorporation) _
No vector attraction reduction
alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A�ICAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 50333/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system desiazned to ensure that qualified personnel
properlyy gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
awaze thai there aze significant penalties for false certification including fine and imprisonment"
Tom Lucas, Superintendent Brown WTP
Prepazer Name d Title (print or type)
�� �i Z/�f/ao»
Signature of Prepazer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
*Prepazer is defined in 40 CFR Part 503.9(r) and liA NCAC 2T.1102 (26)
Date
.-..
,..,
,
j ..._.__- ...
..

FECAL DATA SHEET
Lab result Log
538 2.73 Min
538 2.73 Max
551 2.74 Geometric Mean
522 2.72
532 2.73
544 2.74
1089 3.04
Average 2.77
522
1089
594
_
�—�

Contact Ryan Copeland
Client Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Report Date: 11/19/2019
Project: Durham -Brown
Date Sample Rcvd: 11/6/2019
Meritech Work Order # 11061969 Sample: Durham -Brown 1 Grab
11/6/19
Para__ meted e 1 Analvcsc
at Reporting imit Method
%Total Solids 16.9 % 11/8/19 0-100
Fecal Coliform (Sludge) <538 col/g dry wt 11/6/19 538 col/g dry wt SM 9222D
Meritech Work Order # 11061970 Sample: Durham -Brown 2 Grab
11/6/19
Paramet�r� e u Analysis Date Reportng imit th d
Me o
%Total Solids 16.9 % 11/8/19 0-100 %
Fecal Coliform [Sludge) <538 col/g dry wt 11 6 19 SM 2540B
/ / 538 col/gdrywt SM 9222D
Meritech Work Order # 11061971 Sample: Durham -Brown 3 Grab
11/6/19
Param terc R u t Analysr__s Datg ReDOrting Limit Method
%Total Solids 16.5 % 11/8/19 0-100
FecalColiform(Sludge) <551 col/gdrywt 11/6/19 551 col/gdrywt SM9222D
Meritech Work Order # 11061972 Sample: Durham -Brown 4 Grab
11/6/19
Parameters R c��1 Analysis Date Re or6in i it
R_g1 �n Method
%Total Solids 17.4 % 11/8/19 0-100 %
Fecal Coliform (Sludge) 522 col/g dry wt 11/6/19 130 col/g drywt SM 9222D
Meritech Work Order # 11061973 Sample: Durham -Brown 5 Grab
11/6/19
Parametgr� Resul
_its Analysis Date Re orting imit Method
%Total Solids 17.1 % 11/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <532 col/g drywt 11/6/19 532 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
-�.
— -- s
—��,---_T
—_ _,

Contact Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
:..
,, � ,� ,
Report Date:
Page 2
11/19/2019
Durham -Brown
11/6/2019
Meritech Work Order # 11061974 Sample: Durham -Brown 6 Grab 11/6/19
Para_m�Pr,�r� Real Analy icDat ReportinaLimit Method
%Total Solids 16.7 % 11/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <544 col/g drywt 11/6/19 544 col/g dry wt SM 9222D
Project:
Date Sample Rcvd:
Meritech Work Order # 11061975 Sample: Durham -Brown 7 Grab 11/6/19
Parameters a ul AnaIvsis Date Reoorting imi Method
%Total Solids 16.7 % 11/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 1,089 col/gdrywt 11/6/19 130 col/gdrywt SM 9222D
I hereby certify thatPhave reviewed and approve these data. � �( ��
LabordtoryRep esentative
642 Tamco Road, Reidsville, North Carolana 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
n NPDESlt:
SJiN
d, INC.
Client:
jlrfi Phone:_ 336-)0'1'MERITECH
®
Address: U4 Lffi I 2AO Fax:
"<-- ENVIRONMENTAL LABORATORIES
K<Jll-tC- (r Email: U)176005(Y91IJ 6po.co"9
642 Tamco Rd. Phone: [phone]
Project: Qnud P)Iwt I
Reidsville NC 27320 Fax: [phone]
P,O.g,
Email: [e-mail]
Attention: EN I.LQ_t M Turn Around Time'
How would you like your report sent? 'RUSH work needs prior approval.
www,meritechlabs.com
Circle all that apply; Email (prat red), Fax, Mail Sid 1 a s) - s zd-n9 Hrs
C
Sampling Dates
p g
Person Taking Sample(Sign/Print): n.
IWlN � Lab Use Only
Sample Location and/or ID 7i
C('
-ice?
Start End
Date Time Date Time
com ?
p
crab?
tt of
Cont.
Test S Required
1. )
On
/ No
pH OK?
Cl OK?
C
61
Z
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3
4
Temperature Upon Receipt:
t
Method of
}" De chlorination
<0.5 pm)
of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to emservation. ttR
1
Shipment:
Comments: Compositor It
Jug H
Q UPS
fed Ex
Are these results for regulatory purposes? Yes .' No Q. Report results in: mg/L mg/kg IJ ug/L Q
"Hand Delivery
Relinquished by: 1 �0 GI Date:' 6 Time: I�.-!'C Received by: Date: Time:
N 7 J
Other
Relinquished by: Date: Time: Received by: Date; Time:
Relinquished by: Date: Time:
ReSei ed by Lab, Doi

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project: DURHAM
Field
(state -coup -site-field code)
Soil pH
(from
Lime Requirement
soil anal sis)
Tons/Acre
Applied
Date Applied
NC-AM-21-01
6.4
0.0
tons/ac.
NC-AM-24-02
5.9
0.0 tons/ac.
NC-AM-24-03
6.3
0.0 tonslac.
NC-AM-23-01
5.5
0.8 tons/ac.
1.0 tonlac.
Ordered*
NC-AM-23-02
6.0
0.0 tons/ac.
NC-AM-23-03
6.1
0.0 tons/ac.
NC-AM-23-04
5.2
1.0 tons/ac.
1.0 ton/ac.
Ordered*
NC-AM-23-08
5.1
1.2 tons/ac.
1.5 ton/ac.
Ordered*
NC-AM-23-06
5.8
0.4 tons/ac.
0.5 ton/ac
Ordered*
NC-OR-06-01
6.4
0.0 tons/ac.
NC-OR-06-02
5.8
0.3 tons/ac.
0.5 ton/ac
Ordered*
NC-OR-08-01
5.5
0.6 tons/ac.
1.0 ton/ac.
Ordered*
NC-OR-08-02
5.7
0.7 tons/ac.
1.0 ton/ac.
Ordered*
NC-OR-12-01
5.9
0.0 tons/ac.
NC-OR-12-02
7.0
0.0 tons/ac.
NC-OR-12-06
5.5
0.8 tonslac.
1.0 ton/ac.
Ordered*
NC-OR-14-01
5.9
0.0 tons/ac.
NC-OR-14-02
6.3
0.0 tons/ac.
NC-OR-14-04
6.7
0.0 tons/ac.
NC-OR-14-05
6.7
0.0 tons/ac.
NC-OR-15-01
5.5
0.6 tons/ac.
1.0 ton/ac.
Ordered*
NC-OR-15-03
6.3
0.0 tons/ac.
NC-OR-70-01
7.4
0.0 tons/ac:
NC-OR-70-02
5.9
0.0 tons/ac.
NC-OR-70-03
5.8
0.3 tons/ac.
0.5 ton/ac
Ordered*
NC-OR-70-04
5.9
0.0 tons/ac.
NC-OR-76-06
5.1
1.0 tons/ac.
1.0 ton/ac.
11/18/2019
NC-OR-76-13
5.1
1.0 tons/ac.
1.0
ton/ac.
11/19/2019
NC-OR-76-17
5.3
0.8 tons/ac.
1.0
ton/ac.
11/18/2019
NC-OR-93-07
6.6
0.0 tons/ac.
NC-OR-93-13
5.6
0.5 tons/ac.
1.0 ton/ac.
Ordered*
NC-GR-05-01
5.8
0.4 tons/ac.
0.5 ton/ac
Ordered*
NC-GR-05-02
6.0
0.0 tons/ac.
NC-GR-05-03
6.2
0.0 tons/ac.
NC-GR-05-04
6.0
0.0 tons/ac.
NC-GR-05-05
5.8
0.3 tons/ac.
0.5 ton/ac
Ordered*
NC-GR-05-06
5.2
1.4 tons/ac.
1.5 ton/ac.
Ordered*
NC-PS-01-01
6.0
0.0 tons/ac.
NC-PS-01-04
6.0
0.0 tons/ac.
NC-PS-01-05
4.7
1.8 tons/ac.
2.0 tons/ac
Ordered*
NC-PS-01-06
6.3
0.0 tonslac.
NC-PS-01-07
5.7
0.3 tons/ac.
0.5 ton/ac
Ordered*
-,
�-��t
. ��
� ..
_
,�.
_
s� ,.�� -_

0.0
tons/ac.
0
0.0
tons/ac.
1
0.3
tons/ac.
0.5 ton/ac
Ordered"
0.6
tons/ac.
1.0 ton/ac.
Ordered"
0.0
tons/ac.
7NC-PS�01�14
0.0
tons/ac.
U66

SECTION

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY19-SL033833
61111 °1T°'va Predictive Client: Roger Tate Advisor: Hunter Copeland
8615 Harmony Ch Rd 502 US 13 N
Soil Deport Mehlich-3Extraction Efland, NC 27243 Windsor, NC27983
~. b Links to Helpful Information Sampled: Not Provided Sampled County: Alamance
Received: 06/17/2019
Farm: AM-21 /AM-24 Completed: 06/20/2019 Client ID: 405199 Advisor ID: 493394
Sample ID: AM21-1 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, grain 0.0 120- 160 0 10 0 0 0 0 0 0 Note: 3
2 - 0.0
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 co; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% S4 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0,32 1.05 9.391 0.9 6A 418 71 73 14 47 278 178 1215 1215 313 0.2 2
Sample ID: AM24-2 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, grain 0.0 120 - 160 0 40 0 0 0 0 0 0 Note: 3
2 - 0.0
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cmR; NO3-N in mg[dnr3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% Sol Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cum[ Na ESP SS-1 NO3-N
0,36 1.03 8.6 84 1 A 5.9 678 50 68 13 45 265 176 1609 1609 334 0.1 1
Sample ID: AM24-3 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, grain 0.0 120 - 160 0 10 0 0 0 0 0 0 Note: 3
2 - 0.0
Test Results [units -WN in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/do]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.32 1.05 11.8 91 1.0 6.3 537 74 78 10 44 268 173 1776 1776 296 0.1 1
North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- SteveTroxler,CommissionerofAgricu/ture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY19-SL033833
Roger Tate
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS % % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime, ou-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. if Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-AI1 Mn-availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
MnwFarmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z WO manganese index
M-mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Microrrutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pu bs.htm.
NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncaor,aov/agronomi/oboart4 htmffgnd information that P-1 phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer P205 phosphate
S-1 sulfur index
Test Results SS-1 soluble salt index
WN weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cud, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit rnaw.ncaor.govlapronomiluvrsf htrn

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomil Report No. FY19-SL033832
Predictive Client: Claude / Butch Lynch Advisor: Hunter Copeland
c 9129 Harmony Church Rd 502 US 13 N
o �
Soil Rep®r# Mehlich-3Extraction Mebane, NC27302 Windsor, NC27983
Links to Helpful Information Sampled: Not Provided Sampled County: Alamance
Received: 06/17/2019
Farm: AM-23 Completed: 06/21/2019 Client ID: 372306 Advisor ID: 493394
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop
production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is
designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for
Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by
DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where
they become toxic to crops c rown on a field.
Sample ID: AM23-1 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information
Lime History: 1-Soybean 0.8 0 0 100 0 0 0 0 0 0 Note: 3
2- 0.0
Test Results [units - WN in g/c0; CEC and Na in meq/100 cO; NO3-N in mg/drrr3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS4 NO3-N
0,32 1.06 7A 77 1.7 5.5 547 21 54 22 41 130 88 1366 1366 300 0A 1
Sample ID: 2 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information
Lime History: 1-Soybean 0.0 0 0 100 0 0 0 0 0 0 Note: 3
2- 0.0
Test Results [units - WN in g/cn3; CEC and Na in meq/100 GO; NO3-N in mg/dd]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-AI1 Mn-AI2 Zn-I Zn-AI Cum] Na ESP SS -I NO3-N
0,22 1.04 6.2 83 1.0 6.0 95 19 65 17 34 407 254 358 358 100 0.1 2
North Carolina
Tobacco Tmi fund Commksion
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.neagr,gov/agronomi/
Report No. FY19-SL033832
Claude / Butch Lynch
Page 2 of 3
Sample ID: 3
Recommendations:
Lime
Nutrients (Iblacre)
More
Crop
(tons/acre)
N P205
K20
Mg
S Mn
Zn
Cu
B Information
Lime History:
1-Soybean
0.0
0 0
90
0
0 0
0
0
0 Note: 3
2-
0.0
Test Results [units - WN
in g/cm3; CEC and Na in
meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P4 K4
Ca% Mg% S-I
Mn-I
Mn-AI1
Mn-Al2 Zn-I
Zn-AI
Cum]
Na ESP SS -I NO3-N
0.36 1.08 8.3
87 1.1 6.1
166 25
61 24 48
331
207
613
613
123
0.1 1
Sample ID: 4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S Mn
Zn
Cu
B Information
Lime History:
1-Soybean
1.0
0 0
80
0
0 0
0
0
0 Note: 3
9.
0.0
Test Results [units - WN
in 9/cm3; CEC and Na in
meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P-1 K-I
Ca% Mg % S-1
Mn-I
Mn-All
Mn-Al2 Zn4
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.32 1.20 5.669
1.8 5.2
435 27
49 17 50
247
158
1319
1319
274
0.1 2
Sample ID: 5
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P205
K20
Mg
S Mn
Zn
Cu
JB Information
Lime History:
1-Soybean
1.2
0 0
60
0
0 0
0
0
Note: 3
2-
0.0
Test Results [units - WN
in g/cm3; CEC and Na in
meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P-I K-1
Ca% Mg% S-I
Mn-I
Mn-All
Mn-Al2 Zn-1
Zn-Al
Cu-1
Na ESP SS -I NO3-N
0.36 1.11 5.9
67 2.0 5.1
194 38
49 14 63
514
318
674
674
129
0.1 2
Sample ID: 6
Recommendations:
Lime
Nutrients (Iblacre)
I
More
Crop
(tons/acre)
N P205
K20
Mg
S Mn
Zn
Cu
B Information
Lime History:
1-Soybean
0A
0 0
70
0
0 0
Z
0
0 Note: 3 Note:
2-
0.0
Test Results [units - WN
in g/cm3; CEC and Na in
meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P-I K-1
Ca% Mg% S-I
Mn-I
Mn-AI1
Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS -I NO3-N
0.27 1.10 10.5
84 1.7 5.8
502 34
61 21 67
329
207
2014
2014
327
0.1 1

NCDA&CS Agronomic Division Phone: [phone] Website:
Claude / Butch Lynch
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
No.FY19-SL033832
Page 3 of 3
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS % % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca % % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cum] copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (inunits of K-I potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50, If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mr -All Mn-availability index for crop 1
Mn-AI2 Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mmanganese index
MMO mineral -organic soil class
notations appear on the soil report, refer to Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs. htm.
NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr govlagronomiloboart4 htrrrttiTind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer P205 phosphate
S-I sulfur index
Test Results SS -I soluble salt index
WN weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Znd, Zn-AI, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel Zn-I zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr gov/agraromiluvrst htrn

ly�ur oew "uronomic mvision Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY19-SL033833
ay�`OLT° Predictive
Client:
Roger Tate
Advisor:
Hunter Copeland
8615 Harmony Ch Rd
502 US 13
N
Soil Report
Mehlich-3Extraction
Efland,NC27243
Windsor, NC
27983
�
"
wmvn an Links
to Helpful Information
Sampled:
Not Provided
Sampled County: Alamance
Received:
06/17/2019
Farm: AM-21 /AM-24
Completed:
06/20/2019
Client ID: 405199
Advisor ID:
493394
Sample ID: AM21-1
Recommendations:
Lime
Nutrients (Ib/acre)
Crop
(tons/acre)
N P2O5 K2O
Mg S Mn
Zn
Cu
B
More
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
10
0 0 0
0
0
2 -
0.0
0
Note: 3
Test Results [units - WN
in g/curl; CEC and Na in
meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P-1 K-I
Ca% Mg%
Sol Mn-I
Mn-AI1 Mn-Al2 Zn-1
Zn-AI
Cu-I Na
ESP
SS -I NO3-N
0,32 1,05 9.3
91 0.9 6A
418 71
73 14
47 278
178 1215
1215
313 0.2
2
Sample ID: AM24-2
Recommendations:
Lime
Nutrients (lb/acre)
Crop
(tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu
B
More
Information
Lime History:
1 -Corn, grain
0.0
120 - 160 0
40
0 0 0
0
2 -
0.0
0
0
Note: 3
Test Results [units - WN
in g/cm3; CEC and Na in
meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P-I K-I
Ca% Mg%
S-1 Mnd
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I Na
ESP
SS4 NO3-N
0,36 1,03 8.6
84 1A 5.9
578 50
68 13
45 265
176 1609
1609
334 0.1
1
Sample ID: AM24-3
Recommendations:
Lime
Nutrients (Iblacre)
Crop
(tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu
B
More
Information
Lime History:
1 -Corn, grain
0.0
120 -160 0
10
0 0 0
0
0
0
Note: 3
2 -
0.0
Test Results [units -WN
in g/cm3; CEC and Na in
meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P-I K-I
Ca% Mg%
S-I Mn-I
Mn-AI1 Mn-AI2 Zn-I
Zn-AI
Cu-I Na
ESP
SS -I NO3-N
0.32 1,05 11.8
91 1.0 6.3
537 74
78 10
44 268
173 1776
1776
296 0.1
1
Nlorth Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner ofAgriculfure

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomil Report No. FY19-SL033833
Roger Tate
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime, cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50, If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mmanganese index
MWO mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs,htm.
NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.noaar.aovla(7ronomiloboart4l)L(rdvind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer P205 phosphate
S-I sulfur index
Test Results SSW] soluble salt index
WN weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-1, Zn-AI, Cud, S-1, SS -I, Na, ESP, SS-1, NO3-N (not routine) Zn-I zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar aovlapronaniluvrst htm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomic Report No. FY19-SL033831
o� OLTO+, Predictive Client: Henry Thorpe Advisor:
c 5676 Old Roxboro Rd,
Soil Report Mehlich-3Extraction Oxford, NC27565
Links to Helpful Information Sampled: Not Provided Sampled County: Granville
Received: 06/17/2019
Farm: GR-5 / GR-1 Completed: 06/20/2019 Client ID: 279166 Advisor ID:
Sample ID: GR1-1 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1-Fescue/OGrass/Tlm, M 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12
0- 0.0
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dr&]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-I Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.36 0.94 7.7 86 1.1 6.1 122 38 57 26 52 489 310 398 398 209 0,1 1
Sample ID: GR5-1 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1-Fescue/OGrass/Tim, M 0.4 120-200 0 10 0 0 0 0 0 0 Note: 12
2 - 0.0
Test Results [units - WN in g/c0; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P4 K-I Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I It
0,46 0.90 9.8 84 1.5 5.8 305 73 55 26 55 234 157 1324 1324 224 0.1 1
Sample ID: GR5-3 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu IS
Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 40 0 0 0 0 0 0'Information
Note: 12
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% S4 Mn4 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0,27 1,00 9.1 89 1.0 6.2 299 50 55 32 46 194 131 1040 1040 236 0.2 2
North Carolina
l t :t
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculfure

Page 1 of 1
Report No: 19-347-0572
Account No: 07216 0 ' 2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Synagro Central LLC/ Durham Client:Henry Thorpe Farm: GR-5
Mary Brewer
284 Boger Road Submitted By: Synagro Central LLC/ Durham
Mocksville NC 27028 Date Received: 12/13/2019
Date of Report: 12/16/2019
Lab No Field ID Sample ID Soil Class HM% WN pH Ac P-I Kai S-I Mn-I Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-/ NO3 N
21410 Fld 2 GR-5-2 MIN 1.9 6.0 70.0 202 9 31 125 . 330 330 280 75.4 7 5 2 0.1 0.1
Comment:
Test result units =CEC and Na in meq/t00cm3; NO3 N in mgldm3; WN in g/cm3
North Carolina Division of Water Quality Cerliftcation #257, Analysis and fertility recommendations shovrn on this report are pedormetl in accortlance �vrthin NCDA guidelines, Analysis prepared by: Waypoin[Analytical Carolina, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No, FY19-SL033831
Henry Thorpe
Page 2 of 3
Sample ID: GR5-4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim,
M 0.0
120-200 0
50
0
0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN
in g/cO; CEC and Na in meq/100 crrr3; NO3-N
in mg/drr$]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P-I K-I
Ca% Mg%
S-1
Mn-1
Mn-All
Mn-AI2
Zn4
Zn-AI
Cu4
Na
ESP
SS-1 NO3-N
0.41 0,95 10.2
87 1 A 6.0
259 44
56 28
53
889
550
1147
1147
274
0.1
1
Sample ID: GR5-5
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-FescuelOGrass/Tim,
M 0.3
120-200 50
80
0
0
0
0
0
0
Note: 12
2-
0.0
Test Results [units - WN
in g/crn3; CEC and Na in meq/100 cd; NO3-N
in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P4 K-1
Ca% Mg%
S-I
Mn-1
Mn•All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.22 0,92 6.4
81 1.2 5.8
38 28
50 29
61
293
193
151
151
86
0.1
2
Sample ID: GR5-6
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim,
M 1.4
120-200 0
60
0
0
0
0
0
0
Note: 12
2-
0.0
Test Results [units - W/V
in g/cO; CEC and Na in meq/100 cm3; NO3-N
in mg/dO]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P4 K-1
Ca% Mg%
S-I
Mn-I
Mn-AI1
Mn-Al2
Zn-I
Zn-AI
Cum]
Na
ESP
SS4 NO3-N
0,56 0,90 9.9
76 2A 5.2
350 40
52 22
91
238
160
1946
1946
345
0.2
2

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr
Henry Thorpe
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50, If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncaqr.gov/aqronomi/pubs.htm.
No. FY19-SL033831
Page 3 of 3
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS %
% CEC occupied by basic cations
Ca %
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM %
percent humic matter
K-1
potassium index
Kz0
potash
Mg %
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-A 11
Mn-availability index for crop 1
Mn-A 12
Mn-availability index for crop 2
M n-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NOa-N
ORG
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH
nitrate nitrogen
weight per volume
zinc availability index
zinc index

Page 1 of 1
Report No: 19-347-0515
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
8.
ANALYTICAL
David Walker
2850 Daisy Lane, Wilson, INC 27896
Main 252-206-1721 ° Fax [phone]
wwwowaypointanalytica l.com
Farm: OR-6
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12/16/2019
Lab No Fleld lD Sample ID Sol] Class HM% WN pH Ac P-/ K-/ S-/ Mn-1 Zn-1 Zn-Al Cu-i CEC BS% Ca% Mg% ESP Na SS-/ NO3 N
21348 FId 12 OR-6-1 MIN 0.6 6.4 70.0 142 39 23 163 233 233 120 74.6 6 5 1 0.1 0.1
21349 FId 12 OR-6-2 MIN 0.2 5.8 70.0 164 34 46 200 383 383 130 74.2 6 4 1 0.1 0.1
,:omment:
Tesl result units =CEC and Na in megl100cm3; NO3 N in mgltlm3; WN in g/cm3
North Carolina Division of Water Quality Certification tK257, Analysis and fenility recommentlations sham on this report are pertormetl In accoNance �dthin NCDA guitlelines, Analysis prepared by Waypoint Analytical Carolina, Inc.

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr,gov/agronomi/
Report No. FY19-SL033839
LTLF , Predictive
Client:
Tom Pope Advisor:
SYNAGRO
c
7900 Tom Pope Loop
284 Boger Road
Soil Report Mehlich-3Extraction
c
Cedar Grove, NC27231
Mocksville, NC 27028
fi
CC11
a. rrrr Links to Helpful Information Sampled:
Not Provided
Sampled County: Orange
Received:
06/17/2019
Farm: OR-8 Completed:
06/26/2019
Client ID: 453101
Advisor ID: 499503
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or Z' to alert you
that copper and/or zinc
have accumulated in the soil and are approaching a
level that could be detrimental to
production. The C and Z symbols are printed on your report for soil test
Zn and Cu index levels
crop
of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This is
designed to be a "trigger" that allows enough time to either reduce the rate of application or
find another field for application of biosolids andlor waste
note
water. The CTL (critical toxic level) for
Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500.
Maintaining a pH of
6.0 or higher may reduce potential for toxicity, especially
for Zn. These levels are used by
DENR as a benchmark to determine when application of waste products should be stopped.
The CTL for copper and zinc was set to prevent levels
from accumulating to the point where
they become toxic to crops grownon a field.
Sample ID: OR8-1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20 Mg S Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.6
120-200 0
90 0 0 0 Z
0 0
Note: 12 Note:
2 - 0.0
Test Results [units -WN in g/cars; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P4 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI
Cu-I Na ESP SS-1 NO3-N
0,27 1,24 6.477 1.4 5.5 537 26
51 25
52 131 96 2093 2093
342 0.1 2
Sample ID: OR8-2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20 Mg S Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.7
120-200 0
60 0 0 0 Z
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-1
Ca% Mg%
S4 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI
Cu-I Na ESP SS -I NO3-N
0.36 0,92 13.0 85 2.0 5.7 552 41
55 28
61 324 211 3550 3550
539 0.1 1
North Carolina
To
Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- SteveTroxler,CommissionerofAgriculture

NCDA&CS Agronomic Division Phone: [phone] Website:
Tom Pope
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
No.FY19-SL033839
Page 2 of 2
Lime AG exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca % % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cum[ copper index
ESP exchangeable sodium percent
Fertilizer HM percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z WO mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.govlaoronomiloboart4 ht i rjnd information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer P205 phosphate
S-I sulfur index
Test Results SS -I soluble salt index
Wtv weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-1, Zn-Al, Cu-1, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit wNw ncapr.govlagronorniluvrst.htm

Page 1 of 1
Report No: 19-347-0521
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Client: David Pope / William Dorsett
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: OR-12
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12116/2019
Lab No
Field /D
Sample ID
Soil Class
HM% WN
pH
Ac
P-1
K-I
S-1
Mn4
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
21360
Fld 1-26
Or-12-1
MIN
0.8
5.9
70.0
472
14
37
75
963
963
270
75.7
7
5
2
0.1
0.1
21361
Fld 1-26
Or-12-2
MIN
0.6
7.0
0.0
128
15
33
181
573
573
150
8.4
100
63
34
1.9
0.2
21362
Fld 1-26
Or-12-6
MIN
1.0
5.5
70.0
22
16
33
394
120
120
50
73.4
5
3
1
0.1
0.1
Comment:
Test result units =CEC and Na In meq/100cm3; NO3 N In mg/dm3; WN in g/cm3
Nonh Carolina Division of Water Quality Certification #257, Anaysis and terfility recommendations sham on this report are performed in accordance vnthin NCDA guidelines, Analysis prepared by Waypoint Analytical Carolina, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY19-SL033830
rc� ULi°"�«, Predictive Client: Tom Wilson Advisor: Hunter Copeland
Wilson farm 502 US 13 N
SOII RepoMehlich-3Extraction 3503 Mt Zion Church Road Windsor, NC27983
1 Mebane, NC 27302
Links to Helpful Information Sampled: Not Provided
P Sampled County :Orange
Received: 06/17/2019
Farm: OR-14 Completed: 06/26/2019 Client ID: 311885 Advisor ID: 493394
Sample ID: OR14-1 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, grain 0.0 120 -160 0 0 0 0 0 0 0 0 Note: 3
2 - 0.0
Test Results [units -WN in g1cm3; CEC and Na in meq/100 cm3; NO3-N in mg/d0]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS4 NO3-N
0,36 1,08 10.4 89 1.1 5.9 309 133 72 11 88 427 273 481 481 171 0.1 1
Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, grain 0.0 120 - 160 0 0 0 0 0 0 0 0 Note: 3
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S4 Mn-I Mn-All Mn-AI2 Zn4 Zn-AI Cum[ Na ESP SS -I NO3-N
0,22 1,12 14.3 94 0.8 6.3 461 181 78 10 215 326 208 888 888 208 0.1 1
Sample ID: 4 Recommendations: Lime Nutrients (Ib/acre) I More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, grain 0.0 120 -160 0 0 0 0 pH$ 0 0 0 Note: 3 Note:
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 crrr3; NO3-N in mgfdm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% S-I Mn-I Mn-AI1 Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.22 1.13 15.0 97 0A 6.7 422 136 80 13 135 752 457 873 873 239 0.2 1
North Carolina
rri lw
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner ofAgricu/ture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY19-S1.033830
Tom Wilson
Page 2 of 3
Sample ID: 5
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S Mn Zn
Cu B Information
Lime History:
1 -Corn, grain
0.0
120- 160 0
0
0
0 0 0
0 0 Note: 3
2 -
0.0
Test Results [units - WN
in g/cm3; CEC and Na in
meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH
P-I K-I
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2 Zn-I Zn-Al
Cu-1 Na ESP SS -I NO3-N
0.22 1.23 11.7
95 0.6 6.5
359 147
77 12 94
339
213
567 567
162 0.1 1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/. Report No, FY19-SLO33830
Tom Wilson
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS % % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50, If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-AI1 Mn-availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-O mineral -organic soil class
notations appear on the soil report, refer to Note: Secondary Nutrients and Micronutnents In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs,htm.
NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www ncaor aov/agronorni/obUa t4 htmtif r nd information that P 1 phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate
S4 sulfur index
Test Results SS -I soluble salt index
WN weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index
remaining 16 [P-I, K-1, Ca%, Mg%, Mind, Mn-All, Mn-Al2, Zn-1, Zn-AI, Cu-I, 3-1, SS -I, Na, ESP, SS -I, NO3-N (not routine])Zn-I zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.govlaaronomiluvrst htm

NCDA&CS
733.2655 Website:
Client: Richal Vanhook
9202 Walnut Grove Road
Mehlich-3 Extraction Hurdle Mills, NC 27541
punormation Sampled• Not Provided Sampled County: Orange
Links to Helfl If
mic Division Phone:
Predictive
Soil Report
Report No. FY19-SL033828
Advisor: SYNAGRO
284 Boger Road
Mocksville, NC 27028
Received: 06/17/2019
Farm: OR-15 Completed: 06/20/2019 Client ID: 499502 Advisor ID: 499503
Sample ID: OR151 Recommendations: Lttne Nutrients (lb/acre) IMore
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn cu B Information
Lime History: 1-Fescue/OGrass/Tim, M 0.6 120-200 0 70 0 0 0 0 0 0 Note: 12
2 - 0.0
Test Results [units - WN in g1crrr3; CEC and Na in meq/100 crrr3; NO3-N in mg/dO]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0,46 0,82 6.5 78 1.4 5,5 117 33 52 23 64 323 211 293 293 116 0.1 2
Sample ID: OR153 Recommendations: Lime
Nutrients (lb/acre) I More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12
2 - 0.0
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH Pat K-1 Ca% Mg% Sal Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0,32 0,87 9.8 89 1.1 6.3 237 87 56 28 86 887 545 748 748 255 0.1 1
North Carolina
Tobacco Trust Fund Commlssion
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner ofAgricu/ture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronorni/ Report No, FY19-SL033828
Richal Vanhook
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS % % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca % % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM % percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50, If they Mg % % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-AI1 Mn-availability index for crop 1
Mn-AI2 Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mmanganese index
MWO mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrienls In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
n c a g r. g o vl a g ro n o m i /p u b s. h t m.
NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawnslgardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncaor.aovlanronomilobpart4 htti nd information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowners Guide to Fertilizer P205 phosphate
S-I sulfur index
Test Results SSW] soluble salt index
WN weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cud, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel Zn-I zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit wi ncagrgovlaeronomiluvrst wrn

Page 1 of 1
Report No: 19-347-0520
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Lab No
Field ID
21356
Fld
1-4
21357
Fld
1-4
21358
Fld
1-4
21359
Fld
1-4
Comment:
Sample ID
OR-70-1
OR-70-2
OR-70-3
OR-70-4
®Waypoint.e
F 2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
ANALYTICAL wwwswaypointanalytical.com
Client: Wolfgang Lots Farm: OR-70-
Submilted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12116/2019
Soil Class HM% WN pH Ac P-1 K-1 S-! Mn-I Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3N
MIN 0.4 7.4 0.0 160 17 21 106 333 333 75 7.0 100 65 32 0.7 0
MIN 0.5 5.9 70.0 651 16 44 356 2483 2483 565 76.3 8 6 2 0.1 0.1
MIN 1.0 5.8 70.0 758 24 35 256 2465 2465 505 76.5 9 6 2 0.1 0.1
MIN 0.5 5.9 70.0 528 35 44 150 1425 1425 215 74.6 6 4 2 0.1 0.1
Tesl result units =CEC and Na In meoJ100cm3; NO3 N In mgldm3; WN in glcm3
North Carolina Division of Water Quality CeNfiration #257, Analysis and fedility recommendations sham on this report are pedormed in accorclance enthin NCDA guidelines, Analysis prepared by Waypoint Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-347-0522
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Client: David Latta
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-17210Fax [phone]
www.waypointanalytical.com
Farm: OR -76
Submitted By: Synagro Central LLC/ Durham
Date Received: 12113/2019
Date of Report: 12/16/2019
Lab No
Field ID
Sample ID
Soil Class
HM% WN
pH
Ac
P4
K-1
S4
Mn4
Zn-I
Zn•AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO3 N
21364
Fld 6-17
OR-76-6
MIN
1.0
5.1
70.0
577
17
46
206
1695
1695
355
73.8
5
4
1
0.1
0.1
21365
Fld 6-17
OR-76-13
MIN
0.7
6.1
70.0
358
26
52
800
1280
1280
395
73.7
5
4
1
0.1
0.1
21366
Fld 6-17
OR-76-17
MIN
1.1
5.3
70.0
220
17
40
381
1010
1010
225
73.1
4
3
1
0.1
0.1
Comment:
Test result units =CEC and Na in megll Wrin3; NO3 N in mg/dm3; WN In glcm3
NoAh Carolina Division of Water Quality Certification #257, Analysis antl fedility recommendations sham on this report are performed in aaordance vnthin NCDA guidelines, Analysis prepared by: Waypoinl Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-347-0526
Account No: 07216 ' 2850 Daisy Lane, Wilson, NC 27896
Main 252-206-17210Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Synagro Central LLC/ Durham Client: U Rogers Farm: OR-93
Mary Breyer
284 Boger Road Submitted By: Synagro Central LLC/ Durham
Mocksville NC 27028 Date Received: 12113/2019
Date of Report: M16/2019
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K I S-1 Mn-I Zn-I Zn-AI Cud CEC BS% Ca% Mg% ESP Na SS-1 NO3 N
21379 FId 713 OR-93-7 MIN 0.2 6.6 70.0 77 20 17 175 408 408 90 78.8 11 7 4 0A 0.1
21380 FId 713 OR-93-13 MIN 1.1 _. 5.6 70.0 536 40 42 106 2495 2495 330 76.4 9 6 2 0.1 0.1
Comment:
Test result units =CEC and Na In meq/1 Ogcm3; NO3 N In mg/dm3; WN In g/cm3
North Carolina Division of Water Quality Cedifcation #257, Analysis and fertility recommendations sharm on this report are performed in accordance vnthin NCDA guidelines, Analysis prepared by Waypoint Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-347-0531
Account No: 072%
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Client: Sidney Thompson
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-17210Fax [phone]
www,wayp o i ntana lytica l.co m
Farm: PS-1
Submitted By: Synagro Central LLCI Durham
Date Received: 12113/2019
Date of Report: 12/1612019
Lab No
Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-I
K-1
S-1
Mn-1
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
21398
FId1-13
PS-1-1
MIN
1.3
6.0
70.0
151
8
29
125
150
150
90
72.3
3
2
1
0.1
0.1
21399
FId1-13
PS-1-4
MIN
1.0
6.0
70.0
157
12
31
131
173
173
95
73.1
4
3
1
0.1
0.1
21400
Fldt-13
PS-1-5
MIN
0.9
4.7
70.0
343
15
31
213
858
858
325
72.0
3
2
1
0.1
0
21401
FId1-13
PS-1-6
MIN
2.8
6.3
70.0
113
37
79
181
588
588
115
78.1
10
8
2
0.2
0.1
21402
Fld1-13
PS-1-7
MIN
2.0
5.7
70.0
277
11
35
113
538
538
185
73.1
4
3
1
0.1
0.1
21403
Fldi-13
PS-1-9
MIN
0.9
6.1
70.0
200
10
35
131
258
258
135
73.2
4
3
1
0.1
0.1
21404
FId1-13
PS-1-10
MIN
1.9
6.2
70.0
123
120
35
181
378
378
130
75.6
7
4
2
0.1
0
21405
FId1-13
PS-1-11
MIN
0.8
5.8
70.0
269
12
33
119
530
530
175
73.3
4
3
1
0.1
0.1
21406
FId1-13
PS-1-12
MIN
1.0
5.6
70.0
401
12
35
156
1268
1268
295
74.4
6
4
1
0.1
0.1
21408
FId1-13
PS-1-13
MIN
0.9
6.8
70.0
11
12
15
175
40
40
35
74.4
6
4
2
0.1
0.1
21409
FIdl-13
PS-1-14
MIN
0.6
5.9
70.0
200
10
31
131
273
273
120
72.8
4
3
1
0.2
0.1
Comment:
Test result units =CEC and Na in meq/1 Wcm3; NO3 N In mg/dm3; WN In g/cm3
North Carolina Division of Water Quality Certification #257, Analysis antl (ediliry recommendations shrnvn on this report are performed in accordance vrithln NCDA guidelines, Analysis prepared by Waypoint Analytical Carolina, Inc.