WQ0006101_Residual Annual Report 2019_20200226

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/26/2020
Received:*
Project Number* WQ0006101
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0006101
Applicant\Permittee * Synagro
Facility Name * City of Dunn
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
City of Dunn 2019 Annual Report
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
DUNN NC 2019 Annual Report FINAL.pdf 40.13MB
Upload only 1 RDF document. NL@iple documents must be combined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/21/2020

435 V/iliiarris Count, State 100
Baltimore, N D 21220
wwwsy7nagro.coin
FEBRUARY 21, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0006101
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Dunn, NC.
If you have any questions or need additional information, please do not hesitate to contact
Heather Adams at [phone] or Melvin Goad at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Heather Adams — City of Dunn
Melvin Goad - Synagro
YOUR PARTNER FORA CLEANER, GREENER WORLD

CITY OF DUNNI NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006101
2019 ANNUAL REPORT

City of Dunn, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00006101 County Harnett Year 2019
FacilityName (as shown on permit) Dunn WWTP & City of Dunn WTP NPDES No. NC0043176.03-43-010
.and Application Operator SYnaar'o Phone# (336) 99&7150
,and application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summary:
Total number of application fields in the permit: 13
Total number of fields utilized for land application during the year: 9
Total amount of dry tons applied during the year for all application sites: 174.84
Total number of acres utilized for land application during the year: 60.7
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
143 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T. 1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C —Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, ' chiding the possibility of fines and imprisonment for
knowing violations."
Heather Adams, Utilities Director
Permittee Name and Title (type or print) Signa Pr' aake
Signature of Preparer* Date Signadlre of Land AppPidr Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
DUNN, NC
DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT TONS
April 2019 7133000,00 G 65.41 D 59.34
September 2019 576,600.00 G 52089 D 47,98
YEARLY TOTAL 112897600000 G 118,30 D 107,32
2/5/2020

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
DUNN, NC
DUNN, NC WTP LIQUID
MONTH/YEAR
October 2019
YEARLY TOTAL
AMOUNT UNIT
502,200.00 G
502,200.00 G
DRY TONS UNIT
56.54 D
56.54 D
DRY METRIC
TONS
51.29
51.29
2/5l2020

ANNUAL RESIDUALS SAMPLINO SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006101
Facility Name: DUNN, NC
NPDES# : NCO043176
or WQ# (residual only)
WWTP Name: DUNN WWTP
Residuals Analysis Data
Product Type AEDLIQ
Date Sampled (grab) or 02/04/19
Date Composited
Percent Solids 2. 20
PARAMETERS (mg/kg dry weight)
Arsenic <14 . 4
Cadmium 1. 9
Mercury 1.2
Chromium NR
Copper 278
Lead 48.9
Molybdenum 9
Nickel 1588
Selenium <14 . 4
Zinc 468
Total Phosphorus 14900
TKN 63100
Ammonia -Nitrogen 584
Nitrate and Nitrite 1050
Laboratory
PACE ANALYTICAL SERVICE INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF P
DENR FORM RSSF (5/2003)
Printed: Thursday - February 6, 2020 at 09:00:41 for: 2188 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006101
Facility Name: DUNN, NC
NPDES# : NCO043176
or WQ# (residual only)
WWTP Name: DUNN WWTP
Residuals Analysis Data
Product Type AEDLIQ
Date Sampled (grab) or 02/04/19
Date Composited
Percent Solids 2. 20
PARAMETERS (mg/kg dry weight)
Aluminum
15600
Calcium
9340
Magnesium
2 690
pH
Potassium
6.00
<718 0
Sodium
<7180
Laboratory
PACE ANALYTICAL SERVICE INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date G/ /v,
(SIGNAI`URE OF PREPARER)
NR -Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Thursday -February 6, 2020 at 09:01:14 for: 2188 01

Analytical
www.pacelabs.com
February 137 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: DUNN WWTP 2/7/19
Pace Project No.: 92416931
Dear Nate Roth:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for samples) received by the laboratory on February 07, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
mil-° �
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 18

Analytical
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Project: DUNN WWTP 2/7/19
Pace Project No.: 92416931
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent 01 Pace Analytical Services, LLC.
Page 2 of 18

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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
DUNN WWTP 2/7/19
92416931
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92416931001
DUNN WWTP
EPA 601OD
SH1
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
ECH
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 18

Analytical
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ANALYTICAL RESULTS
Project: DUNN VWVfP 2/7/19
Pace Project No.: 92416931
Sample: DUNN WWTP Lab ID: 92416931001 Collected: 02/04/19 13:30 Received: 02/07/19 09:55
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA3050B
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
AS No. Qua[
Aluminum
15600
mg/kg
144
1
02/11/19
09:37
02/12/19
01:34
7429-90-5
Arsenic
ND
mg/kg
14A
1
02/11/19
09:37
02/12/19
01:34
7440-38-2
Cadmium
1.9
mg/kg
1 A
1
02/11/19
09:37
02/12/19
01:34
7440-43-9
Calcium
9340
mg/kg
144
1
02/11/19
09:37
02/12/19
01:34
7440-70-2
Copper
278
mg/kg
7.2
1
02/11/19
09:37
02/12/19
01:34
7440-50-8
Lead
48.9
mg/kg
7.2
1
02/11/19
09:37
02/12/19
01:34
7439-92-1
Magnesium
2690
mg/kg
144
1
02/11/19
09:37
02/12/19
01:34
7439-95-4
Molybdenum
9.0
mg/kg
7.2
1
02/11/19
09:37
02/12/19
01:34
7439-98-7
Nickel
15.8
mg/kg
7.2
1
02/11/19
09:37
02/12/19
01:34
7440-02-0
Potassium
ND
mg/kg
7180
1
02/11/19
09:37
02/12/19
01:34
7440-09-7
Selenium
ND
mg/kg
14.4
1
02/11/19
09:37
02/12/19
01:34
7782-49-2
Sodium
ND
mg/kg
7180
1
02/11/19
09:37
02/12/19
01:34
7440-23-5
Zinc
468
mg/kg
14A
1
02/11/19
09:37
02/12/19
01:34
7440-66-6
7471 Mercury
Mercury
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
1.2 mg/kg
Analytical
Method: SM 2540G-2011
2.2
Analytical Method: ASTM D2974-87
97.8
Analytical Method: EPA 9045D
6.0 Std. Units
Analytical Method: SM 2710E-2011
20100 mg/kg
0.18 1 02/11/1916:07
02/12/1915:55 7439-97-6
02/08/19 16:31
02/08/19 16:25
02/12/19 13:40
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
584 mg/kg
415 1 02/08/1912:27 02/09/1915:52 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
63100 mg/kg
3050 2 02/09/19 01:19 02/12/19 02:16 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
1050
mg/kg
89.1
1
02/09/19
04:09
02/09/19
05:17
1050
mg/kg
89.1
1
02/09/19
04:09
02/09/19
05:17 14797-55-8
ND
mg/kg
44.5
1
02/09l19
04:09
02/09/19
05:17 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
14900 mglkg 448 10 02/07/19 19:20 02/07l19 22:21 7723-14-0
REPORT OF LABORATORY ANALYSIS
N2
This report shall not be reproduced, except in full,
Date: 02/13/2019 11:11 AM without the written consent of Pace Analytical Services, LLC, Page 4 of 18

QD
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Project: DUNN VWVfP 2/7/19
Pace Project No.: 92416931
QC Batch: 457445
QC Batch Method: EPA 7471 B
Associated Lab Samples: 92416931001
METHOD BLANK: 2495015
Associated Lab Samples: 92416931001
Parameter
Mercury
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Solid
EPA 7471 B
7471 Mercury
Blank Reporting
Units Result Limit Analyzed
mg/kg ND 0,0060 02/12/1915:32
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2495016
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0,083 100 80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2495017
2495018
MS
MSD
92416976023
Spike
Spike
MS MSD MS MSD % Rec
Parameter Units Result
Cone.
Cone.
Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND
0,059
0,06
0,057 0,052 90 79 75-125 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2019 11:11 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: DUNN WW�P 2/7/19
Pace Project No.: 92416931
QC Batch: 457387 Analysis Method: EPA6010D
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Associated Lab Samples: 92416931001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 2494691
Matrix: Solid
Associated Lab Samples:
92416931001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Aluminum
mg/kg
ND
10.0
02/12/19
01:28
Arsenic
mg/kg
ND
1.0
02/12/19
01:28
Cadmium
mg/kg
ND
0,10
02/12/19
01:28
Calcium
mg/kg
ND
10.0
02/12/19
01:28
Copper
mg/kg
ND
0,50
02/12/19
01:28
Lead
mg/kg
ND
0,50
02/12/19
01:28
Magnesium
mg/kg
ND
10.0
02/12/19
01:28
Molybdenum
mg/kg
ND
0,50
02/12/19
01:28
Nickel
mg/kg
ND
0,50
02/12/19
01:28
Potassium
mg/kg
ND
500
02/12/19
01:28
Selenium
mg/kg
ND
1.0
02/12/19
01:28
Sodium
mg/kg
ND
500
02/12/19
01:28
Zinc
mg/kg
ND
1.0
02/12/19
01:28
LABORATORY CONTROL
SAMPLE: 2494692
Spike
LCS
LCS
%
Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Aluminum
mg/kg
500
493
99
80-120
Arsenic
mg/kg
50
45.2
90
80-120
Cadmium
mg/kg
50
46.9
94
80-120
Calcium
mg/kg
500
490
98
80-120
Copper
mg/kg
50
49.5
99
80-120
Lead
mg/kg
50
46.9
94
80-120
Magnesium
mg/kg
500
479
96
80-120
Molybdenum
mg/kg
50
51 A
102
80-120
Nickel
mg/kg
50
47.9
96
80-120
Potassium
mg/kg
500
ND
99
80-120
Selenium
mg/kg
50
42.9
86
80-120
Sodium
mg/kg
500
491J
98
80-120
Zinc
mg/kg
50
46.2
92
80-120
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE: 2494693
2494694
MS
MSD
92416931001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc,
Result
Result
% Rec
% Rec
Limits RPD Qua[
Aluminum
mg/kg 15600
7080
7220
27800
28400
173 177
75-125 2 M1
Arsenic
mg/kg ND
708
722
630
643
88 88
75-125 2
Cadmium
mg/kg 1.9
708
722
652
669
92 92
75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2019 11:11 AM out the written consent 01 Pace Analytical Services, LLC. Page 6 of 18

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Project:
Pace Project No.:
DUNN VWVfP 2/7/19
92416931
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX
Parameter
SPIKE DUPLICATE: 2494693
MS
92416931001 Spike
Units Result Conc.
MSD
Spike
Conc.
2494694
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
9340
7080
7220
15900
16300
93
96
75-125
2
Copper
mg/kg
278
708
722
976
994
98
99
75-125
2
Lead
mg/kg
48.9
708
722
691
707
91
91
75-125
2
Magnesium
mg/kg
2690
7080
7220
9380
9600
94
96
75-125
2
Molybdenum
mg/kg
9.0
708
722
710
728
99
99
75-125
2
Nickel
mg/kg
15.8
708
722
679
695
93
94
75-125
2
Potassium
mg/kg
ND
7080
7220
11000
11300
95
97
75-125
2
Selenium
mg/kg
ND
708
722
599
618
84
85
75-125
3
Sodium
mg/kg
ND
7080
7220
8410
8710
96
98
75-125
4
Zinc
mg/kg
468
708
722
1090
1110
87
89
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: DUNN WWTP 2/7/19
Pace Project No.: 92416931
QC Batch: 457237 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92416931001
SAMPLE DUPLICATE: 2494016
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2494017
Parameter
Percent Moisture
92416878001
Units Result
4.5
92417004001
Units Result
10 19.2
Dup
Result
4.4
Dup
Result
18A
RPD Qualifiers
1
RPD Qualifiers
53
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: DUNN VWVfP 2/7/19
Pace Project No.: 92416931
QC Batch: 457221 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92416931001
SAMPLE DUPLICATE: 2493893
Parameter Units
pH at 25 Degrees C Std, Units
92416187001 Dup
Result Result
7.8
RPD Qualifiers
7.9 0 H3
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page9of18

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QUALITY CONTROL DATA
Project: DUNN VWVfP 2/7/19
Pace Project No.: 92416931
QC Batch: 457085 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod,
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod, Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92416931001
METHOD BLANK: 2493205 Matrix: Solid
Associated Lab Samples: 92416931001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 8.5 02/09/19 15:26
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2493206
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 481 473 98 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2493207
MS
92416187001 Spike
Parameter Units Result Conc,
Nitrogen, Ammonia mg/kg 4000 953
2493208
MSD
Spike MS MSD MS MSD %Rec
Conc. Result Result % Rec % Rec Limits RPD Qual
918 9370 9000 118 83 90-110 4 M6
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2493209 2493210
MS MSD
92416556005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Ammonia mg/kg 5560 22200 21400 27200 26100 97 96 90-110 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/13, 019 11:11 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 18

Analytical
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Project: DUNN VWVfP 2/7/19
Pace Project No.: 92416931
QC Batch: 457266
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92416931001
METHOD BLANK: 2494217
Associated Lab Samples: 92416931001
Parameter
Nitrogen, Kjeldahl, Total
QUALITY CONTROL DATA
Analysis
Method:
EPA
351.2 Rev 2.0 1993
Analysis
Description:
351.2
TKN
Matrix: Solid
Blank Reporting
Units Result Limit Analyzed
mg/kg ND 50.0 02/12/19 01:50
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2494218
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 1070 107 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2494219 2494220
MS MSD
92416187001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc, Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 10200 1790 1650 20200 22800 -42 112 90-110 12 M6,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Analytical
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Project:
Pace Project No.:
DUNN VW�lrP 2/7/19
92416931
QC Batch: 457273
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92416931001
METHOD BLANK: 2494230
Associated Lab Samples: 92416931001
QUALITY CONTROL DATA
Analysis
Method:
EPA 353.2 Rev
2.0 1993
Analysis
Description:
353.2 Nitrate +
Nitrite
Matrix: Solid
Blank Reporting
Units Result Limit
Nitrogen,
Nitrate
mg/kg
ND
2.0
Nitrogen,
Nitrite
mg/kg
ND
1.0
Nitrogen,
NO2 plus NO3
mg/kg
ND
2.0
Analyzed
02/09/19 05:10
02/09/19 05:10
02/09/19 05:10
Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2494231
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 17.0 113 90-110
Nitrogen, Nitrite mg/kg 10 10.1 101 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 27A 108 90-110
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE:
2494232
2494233
MS
MSD
92416556005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc,
Result
Result
% Rec
% Rec
Limits
RPD Qua]
Nitrogen,
Nitrate
mg/kg
ND
659
663
532
488
81
74
90-110
9
Nitrogen,
Nitrite
mg/kg
ND
436
441
356
354
75
74
90-110
1 M1
Nitrogen,
NO2 plus NO3
mg/kg
ND
1090
1100
887
842
76
71
90-110
5 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/13/2019 11:11 AM out the written consent of Pace Analytical Services, LLC. Page 12 of 18

Analytical
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QUALITY CONTROL DATA
Project: DUNN VWVfP 2/7/19
Pace Project No.: 92416931
QC Batch: 457001 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365A Rev 2.0 1993 Analysis Description: 365A Phosphorus, Total
Associated Lab Samples: 92416931001
METHOD BLANK: 2492910 Matrix: Solid
Associated Lab Samples: 92416931001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 0.96 02/07/19 22:16
LABORATORY CONTROL SAMPLE: 2492911
Parameter Units
Phosphorus mg/kg
Spike LCS
Conc. Result
49 51.7
LCS
Rec
105
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
0ualifiers
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2492912 2492913
MS MSD
92416609001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 14100 184 184 13800 13400 -141 -401 90-110 4 M6
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2492914 2492915
MS MSD
92416464001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 10200 49 49.9 12700 11200 5120 2100 90-110 12 M63R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 13 of 18

Analytical
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QUALIFIERS
Project: DUNN WWTP 2/7/19
Pace Project No.: 92416931
DEFINITIONS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, INC 28o78
[phone]
PQL -Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) -Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC -Not Calculable.
SG - Silica Gel - Clean -Up
U -Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute,
LABORATORIES
PAST -A
Pace
Analytical
Services -Asheville
PASI-C
Pace
Analytical
Services -Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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Analytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
DUNN VWVfP 2/7/19
92416931
Analytical
Lab ID
Sample
ID
QC Batch Method
QC Batch
Analytical Method
Batch
92416931001
DUNN
WWTP
EPA3050B
457387
EPA
6010D
457494
92416931001
DUNN
WWTP
EPA 7471B
457445
EPA
7471B
457534
92416931001
DUNN
WWTP
SM 2540G-2011
457411
92416931001
DUNN
WWTP
ASTM D2974-87
457237
92416931001
DUNN
WWTP
EPA9045D
457221
92416931001
DUNN
WWTP
SM 2710B-2011
457664
92416931001
DUNN
WWTP
EPA 350.1 Rev 2.0
1993
457085
EPA
350.1 Rev
2.0
1993
457187
Mod,
Mod,
92416931001
DUNN
WWTP
EPA 351.2 Rev 2.0
1993
457266
EPA
351.2 Rev
2.0
1993
457561
92416931001
DUNN
WWTP
EPA 353.2 Rev 2.0
1993
457273
EPA
353.2 Rev
2.0
1993
457274
92416931001
DUNN
WWTP
EPA 365.1 Rev 2.0
1993
457001
EPA
365.1 Rev
2.0
1993
457029
REPORT OF LABORATORY ANALYSIS
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Date: 02/13/2019 11:11 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 18

AwAnalytical
Laboratory receiving samples:
Asheville / Eden❑
Courier:
❑ Commercial
Custody Seal Present?
Packing Material:
Client Name:
r
❑FedEx
❑Pace
❑Yes . No
❑Bubble Wrap
Document Name: Docum=Revised:February 7,2018
mple Condition Upon Receipt(SCUR) of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
Seals intact?
Project #: rWO## s 92416931
❑Client 1113"1I924931
82416
(]i�s ❑No �!!
Date/Initials Person Examining Contents:
[.None ❑ Other
Thermometer: �
IRGunID: ICiG�� Type of ice:
❑i a
Cooler Temp (°C): (c ltJ Correction Factor: Add/Subtract (°C)
Cooler Temp Corrected (°C): lb �
❑Wet ❑Blue
USDA Regulated Soil (❑ N/A, water sample)
Did samples ongi ate in a quarantine zone within the United States: CA, NY, or SC (check
❑Yes ❑r No
Chain of Custody Present? )30 es ❑No ❑N/,
Samples Arrived within Hold TimDe? Yes []No ❑N/
Short Hold Time Analysis (<72 hr.)? ❑Yes (3�No ❑N/
Rush Turn Around Time Requested? Oyes No ❑N/
Sufficient Volume? 13%es ❑No ❑N/
Correct Containers Used? ❑des [:]No ❑N/
-Pace Containers Used? ❑i Fes ❑No ❑Ni
W
Containers Intact? es []No ❑
Dissolved analysis: Samples Field Filtered? ❑Yes ❑No ©N,
Sample Labels Match COO [ 'yes ❑No ❑N,
t^
-Includes Date/Time/ID/Analysis Matrix: t�
Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No )3N
Trip Blank Present? ❑Yes []No ON
Trip Blank Custody Seals Present? ❑Yes ❑No (]n
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTIDN
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
--
Biological Tissue Frozen?
❑Yes ❑No [JN/A
QlJone
Temp
should be above freezing to 6°C
]Samples out of temp criteria. Samples on ice, cooling process
has begun
Lot ID of split containers:
Date/Time:
Field Data Required? ❑Yes No
Page 16 of 18
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTIDN
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
--
Biological Tissue Frozen?
❑Yes ❑No [JN/A
QlJone
Temp
should be above freezing to 6°C
]Samples out of temp criteria. Samples on ice, cooling process
has begun
Lot ID of split containers:
Date/Time:
Field Data Required? ❑Yes No
Page 16 of 18

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
iPacehialytical
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Check mark top half of box if pH and/ dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project #
WQ#:92416931
PMO L* Due Date: 02/18/19
CLIENT* 92-sYNAGRO
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pH Adjustment Log for Preserved Sarnples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time pre �rvation Amount of Preservative Lot R
adjusted added
Note:
Note:
Whenever there is a discrepancy
affecting
North Carolina compliance
samples, a copy of this Corm wmbe sent to the rvortn t.arouna vcn,vt. art k:l:�aZJ�15 wljl�� 110�4
Out of
hold, incorrect preservative, out
of temp,
incorrect containers.
Page 17 of 18

aceArratytic21
Section A
Rocuired Client Information:
CHAIN -OF -CUSTODY / Analytical Request Document
The Chairrot-Custody Is a LEGAL DOCUMENT. AA relevant fields must be completed accurately.
Section B Seetton C
Required Project information: Inwioe Information:
Page: of
Company.
Synagro
Report To:
AHantlon:
Mary Brewer
Address:
284Boger Rd.
Copy To:
Company Name: Synagro
REGULAT0137AGENCY.;}:;;'-;:`::':;;.-<:.;::::•.::...,....-
Mock$VIIIe, NC 27028
Address:
284 Boger Rd, Mocksville,NC 27028
1' NPDES r GROUNDWATER
r
DRINKING
WATER
r UST r RCRA
r OT14ER
Email To: , 6
Purchase Order No.:
PamCuole
L
Phone: 3 e6,790' 1610
Fax
FAIRReference:
Project Name:
Poea Project
MM Mer.
Slte'Loea IFfy
I".
Requested Due DaterrAT:
Project Number.
Paco ProNa a:IF
:.;:;:;'.Requested:Atiaty'si
ofiftered
(YIN)`;;I
Section D
Valid Matrix Codes
Requirea Caere lnfoun
meo
MAIJUX
CODE
a
OF
COLLECTED
Preservatives
•�:
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Issue
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SAMPLERNAMEANDSIGNATURE
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IF
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PRINT Name of SAMPLER
i V yr
dI AA
SIGNATURE of SAMPLER:
1%
DATE Signed
2 v
~cc
rJ
in
MMIDDlYYI:
!
'1.-e.,....N...:R.....t..,n,......Farm ............P.... NET s0..>n.>m...term ......,,,....0 .. ,... ...ro.. .. ts°6 .., r....... > ...... ..,n .«..,, 30 . art . FALL-0-020.e..06. 12-Oec-2007

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2188=01=AEDLIQ-NC DUNN, NC WWTP AEROBICALLY DIGESTED 2/4/2019 2/1/2019=12/31/2019 2A908
LIQUID
Na mgll = (Na mglkg x %Solids) = 100 = (7180 x 2.2000) = 100 = 157.96
Ca mgll = (Ca mg/kg x %Solids) _ 100 = (9340 x 2.2000) = 100 = 205.48
Mg mg/I = (mg mg/kg x %Solids) + 100 = (2690 x 2.2000) = 100 = 59.18
Na meq = Na mg/I = Molec.Wgt.Na = 157.96 = 23 = 6.86783
Ca meq = Ca mg/I = Molec.Wgt.Ca = 205.48 + 20 = 10.274
Mg meq = Mg mg/I = Molec.Wgt.Mg = 59.18 _ 12 = 4.93167
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.86783 = SgrRoot[0.5(10.274+4.93167)] = 2.49076
Printed: 2/6/2020
Page 1 09:02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006101
Facility Name: DUNN, NC
NPDES#:
or WQ# (residual only)
WWTP Name: DUNN WTP
Residuals Analysis Data
Product Type WPL
Date Sampled (grab) or 02/04/19
Date Composited
Percent Solids 2,70
PARAMETERS (mg/kg dry weight)
Arsenic <110 8
Cadmium <1.2
Mercury o . 2 5
Chromium NR
Copper 42.6
Lead 13.5
Molybdenum <5 a 9
Nickel 12,8
Selenium <11 . 8
Zinc 73 . 8
Total Phosphorus 1590
TKN 3780
Ammonia -Nitrogen <327
Nitrate and Nitrite <73. 5
Laboratory
PACE ANALYTICAL SERVICE INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penayfies for submitting false information, including the possibiply of fines and imprisonment for knowing violations."
Date
(SIGNATCJRE OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Thursday -February 6, 2020 at 09:00:53 for: 2188 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report,
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form,
Permit Number: W00006101
Facility Name: DUNN, NC
NPDES#:
or WQ# (residual only)
WWTP Name: DUNN WTP
Residuals Analysis Data
Product Type WPL
Date Sampled (grab) or 02/04/19
Date Composited
Percent Solids 2. 70
PARAMETERS (mg/kg dry weight)
Aluminum 118000
Calcium 978
Magnesium 1440
pH 5080
Potassium <5 9 0 0
Sodium <5900
Laboratory
PACE ANALYTICAL SERVICE INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penal#ies for submitting false information, includ the possibility of fines and imprisonment for knowing violations."
Date
RE OF PREPARER)
NR -Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Thursday - February 6, 202o at o9:01:06 for: 218s o2

Analytical
www.pacelabs.com
February 13, 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
Dear Nate Roth:
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for samples) received by the laboratory on February 07, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cr� ?�3
Lorri Patton
lorri. [e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
[phone]
Page 1 of 18

Analytical
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Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Analytical
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SAMPLE ANALYTE COUNT
Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92416932001 DUNN WTP EPA 601OD
SH1
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
ECH
1
PASI-A
SM 271OB-2011
EWS
1
PASI-A
EPA350.1 Rev 2.0 1993 Mod,
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
Sample: DUNN WTP Lab ID: 92416932001 Collected: 02/04/19 14:30 Received: 02/07/19 09:55
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed
[37[rliril_*>iL�ir
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix:
Solid
CAS No. Qual
Aluminum
118000
mg/kg
118
1
02/11/19
09:37
02/12/19
01:53
7429-90-5
Arsenic
ND
mglkg
11.8
1
02/11/19
09:37
02/12/19
01:53
7440-38-2
Cadmium
ND
mg/kg
1.2
1
02/11/19
09:37
02/12/19
01:53
7440-43-9
Calcium
978
mg/kg
118
1
02/11/19
09:37
02/12/19
01:53
7440-70-2
Copper
42.6
mg/kg
5.9
1
02/11/19
09:37
02/12/19
01:53
7440-50-8
Lead
13.5
mg/kg
5.9
1
02/11/19
09:37
02/12/19
01:53
7439-92-1
Magnesium
1440
mg/kg
118
1
02/11/19
09:37
02/12/19
01:53
7439-95-4
Molybdenum
ND
mg/kg
5.9
1
02/11/19
09:37
02/12/19
01:53
7439-98-7
Nickel
12.8
mg/kg
5.9
1
02/11/19
09:37
02/12/19
01:53
7440-02-0
Potassium
ND
mg/kg
5900
1
02/11/19
09:37
02/12/19
01:53
7440-09-7
Selenium
ND
mg/kg
11.8
1
02/11/19
09:37
02/12/19
01:53
7782-49-2
Sodium
ND
mg/kg
5900
1
02/11/19
09:37
02/12/19
01:53
7440-23-5
Zinc
73.8
mg/kg
11.8
1
02/11/19
09:37
02/12/19
01:53
7440-66-6
7471 Mercury
Analytical Method:
EPA 7471 B
Preparation
Method:
EPA 7471 B
Mercury
0.25
mg/kg
0.17
1
02/1111916:07
02/12/1915:57
7439-97-6
254OG Total Percent Solids
Analytical Method:
SM 2540G-2011
Total Solids
2.7
%
0,10
1
02/08/19
16:31
Percent
Moisture
Analytical Method:
ASTM D2974-87
Percent
Moisture
97.3
% 0,10 1 02/08/19 16:25
9045 pH Soil
Analytical Method:
EPA 9045D
PH at 25 Degrees C
5.8 Std.
Units
0.10 1
02/08/19 17:27
H3
Plant Available Nitrogen
Analytical Method:
SM 271 OB-2011
Plant Available Nitrogen
1130
mg/kg
0,12 1
02/12/19 13:40
N2
350.1 Ammonia
Analytical Method:
EPA 350.1 Rev 2.0
1993
Mod. Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod,
Nitrogen, Ammonia
ND
mg/kg
327 1 02/08/19
12:27
02/09/19 15:53
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method:
EPA 351.2 Rev 2.0
1993
Preparation Method:
EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
3780
mg/kg
1690 1 02/09/19
01:19
02/12/19 01:47
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method:
EPA 353.2 Rev 2.0
1993
Preparation Method:
EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND
mg/kg
73.5 1 02/09/19
04:09
02/09/19 05:19
Nitrogen, Nitrate
ND
mg/kg
73.5 1 02/09/19
04:09
02/09/19 05:19
14797-55-8
Nitrogen, Nitrite
ND
mg/kg
36.7 1 02/09/19
04:09
02/09/19 05:19
14797-65-0
365.1 Phosphorus, Total
Analytical Method:
EPA 365.1 Rev 2.0
1993
Preparation Method:
EPA 365A Rev 2.0 1993
Phosphorus
1590
mg/kg
36.5 1 02/07/19
19:20
02/07/19 22:56
7723-14-0
REPORT OF LABORATORY ANALYSIS
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Analytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DUNN WTP 2/7l19
Pace Project No.: 92416932
QC Batch: 457445
Analysis Method:
EPA 7471 B
QC Batch Method: EPA 7471 B
Analysis Description:
7471 Mercury
Associated Lab Samples: 92416932001
METHOD BLANK: 2495015
Matrix: Solid
Associated Lab Samples: 92416932001
Blank Reporting
Parameter Units
Result Limit
Analyzed
Qualifiers
Mercury mg/kg
ND 0,0060 02/12/1915:32
LABORATORY CONTROL SAMPLE: 2495016
Spike LCS
LCS
% Rec
Parameter Units
Conc. Result
% Rec
Limits Qualifiers
Mercury mg/kg
0,083 0,083
100
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2495017
2495018
MS MSD
92416976023
Spike Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Conc, Conc, Result
Result % Rec % Rec Limits RPD Qua]
Mercury mg/kg ND
0,059 0,06 0,057 0,052
90 79 75-125 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Analytical
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QUALITY CONTROL DATA
Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
QC Batch: 457387 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92416932001
METHOD BLANK: 2494691
Associated Lab Samples: 92416932001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
10.0
02/12/19
01:28
Arsenic
mg/kg
ND
1.0
02/12/19
01:28
Cadmium
mg/kg
ND
0.10
02/12/19
01:28
Calcium
mg/kg
ND
10.0
02/12/19
01:28
Copper
mg/kg
ND
0,50
02/12/19
01:28
Lead
mg/kg
ND
0,50
02/12/19
01:28
Magnesium
mg/kg
ND
10.0
02/12/19
01:28
Molybdenum
mg/kg
ND
0,50
02/12/19
01:28
Nickel
mg/kg
ND
0,50
02/12/19
01:28
Potassium
mg/kg
ND
500
02/12/19
01:28
Selenium
mg/kg
ND
1.0
02/12/19
01:28
Sodium
mg/kg
ND
500
02/12/19
01:28
Zinc
mg/kg
ND
1.0
02/12/19
01:28
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2494692
Units
Spike
Cone.
LCS
Result
LCS
% Rec
%Rec
Limits
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Qualif
iers
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE:
2494693
2494694
MS
MSD
92416931001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone,
Result
Result
% Rec
% Rec
Limits
RPD Qua]
Aluminum
mg/kg
15600
7080
7220
27800
28400
173
177
75-125
2 M1
Arsenic
mg/kg
ND
708
722
630
643
88
88
75-125
2
Cadmium
mg/kg
1.9
708
722
652
669
92
92
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Analytical
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Project:
Pace Project No.
DUNN WTP 2/7/19
92416932
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE &MATRIX
Parameter
SPIKE DUPLICATE: 2494693
MS
92416931001 Spike
Units Result Conc.
MSD
Spike
Conc,
2494694
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
9340
7080
7220
15900
16300
93
96
75-125
2
Copper
mg/kg
278
708
722
976
994
98
99
75-125
2
Lead
mg/kg
48.9
708
722
691
707
91
91
75-125
2
Magnesium
mg/kg
2690
7080
7220
9380
9600
94
96
75-125
2
Molybdenum
mg/kg
9.0
708
722
710
728
99
99
75-125
2
Nickel
mg/kg
15.8
708
722
679
695
93
94
75-125
2
Potassium
mg/kg
ND
7080
7220
11000
11300
95
97
75-125
2
Selenium
mg/kg
ND
708
722
599
618
84
85
75-125
3
Sodium
mg/kg
ND
7080
7220
8410
8710
96
98
75-125
4
Zinc
mg/kg
468
708
722
1090
1110
87
89
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2019 11:12 AM without the written consent 01 Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
QC Batch: 457237 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92416932001
SAMPLE DUPLICATE: 2494016
Parameter
Percent Moisture
92416878001
Units Result
4.5
SAMPLE DUPLICATE: 2494017
92417004001
Parameter Units Result
Percent Moisture % 19.2
Dup
Result
4A
Dup
Result
18A
RPD Qualifiers
1
RPD Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/13/2019 11:12 AM without the written consent 01 Pace Analytical Services, LLC.

Analytical
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QUALITY CONTROL DATA
Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
QC Batch: 457221 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92416932001
SAMPLE DUPLICATE: 2493893
Parameter
pH at 25 Degrees C
92416187001 Dup
Units Result Result
Std. Units 7.8
RPD Qualifiers
7.9 0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
QC Batch: 457085 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350A Ammonia
Associated Lab Samples: 92416932001
METHOD BLANK: 2493205 Matrix: Solid
Associated Lab Samples: 92416932001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 8.5 02/09/19 15:26
LABORATORY CONTROL SAMPLE: 2493206
Parameter
Nitrogen, Ammonia
Spike LCS
Units Conc. Result
mg/kg 481
LCS %Rec
% Rec Limits
473
98 90-110
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualif
iers
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2493207 2493208
MS MSD
92416187001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, Ammonia mg/kg 4000 953 918 9370 9000 118 83 90-110 4 M6
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2493209 2493210
MS MSD
92416556005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc, Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 5560 22200 21400 27200 26100 97 96 90-110 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Analytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: DUNN WTP 2/7/19
Pace Project No.: 92416932
QC Batch: 457266 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Associated Lab Samples: 92416932001
METHOD BLANK: 2494217 Matrix: Solid
Associated Lab Samples: 92416932001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 02/12/19 01:50
LABORATORY CONTROL SAMPLE: 2494218
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 1070 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2494219 2494220
MS MSD
92416187001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, Kjeldahl, Total mg/kg 10200 1790 1650 20200 22800 -42 112 90-110 12 M6,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project:
Pace Project No,
DUNN WfP 2/7/19
92416932
QC Batch: 457273
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92416932001
METHOD BLANK: 2494230
Associated Lab Samples: 92416932001
Parameter
Nitrogen, Nitrate
Nitrogen, Nitrite
Nitrogen, NO2 plus NO3
QUALITY CONTROL DATA
Analysis
Method:
EPA 353.2 Rev
2.0 1993
Analysis
Description:
353.2 Nitrate +
Nitrite
Matrix: Solid
Blank Reporting
Units Result Limit
mg/kg ND 2.0
mg/kg ND 1'0
mg/kg ND 2.0
LABORATORY CONTROL SAMPLE: 2494231
Parameter Units
Nitrogen, Nitrate mg/kg
Nitrogen, Nitrite mg/kg
Nitrogen, NO2 plus NO3 mg/kg
MATRIX SPIKE &MATRIX SPIKE DUPLICATE:
Parameter
Nitrogen, Nitrate
Nitrogen, Nitrite
Nitrogen, NO2 plus NO3
Analyzed
02/09/19 05:10
02/09/19 05:10
02/09/19 05:10
Spike LCS LCS
Cone. Result % Rec
2494232
MS
92416556005 Spike
Units Result Conc.
mg/kg ND 659
mg/kg ND 436
mg/kg ND 1090
15 17.0 113
10 10.1 101
25 27.1 108
MSD
Spike
Conc.
663
441
1100
2494233
Result
MS
Rec
Limits
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
fiers
-1
MSD
MS
MSD
%Rec
Result
%Rec
%Rec
Limits
RPD
488
81
74
90-110
9
354
75
74
90-110
1 M1
842
76
71
90-110
5 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Qual
This report shall not be reproduced, except in full,
Date: 02/13/2019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18

Analytical
wwwpacelabs.com
Project:
Pace Project No.
DUNN WTP 2/7/19
92416932
QUALITY CONTROL DATA
QC Batch: 457001 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92416932001
METHOD BLANK: 2492910
Associated Lab Samples: 92416932001
Parameter Units
Phosphorus mg/kg
LABORATORY CONTROL SAMPLE: 2492911
Parameter Units
Phosphorus mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 0,96 02/07/19 22:16
Spike LCS
Conc. Result
49 51.7
LCS
Rec
105
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Qualifiers
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2492912
2492913
MS
MSD
92416609001
Spike
Spike
MS MSD MS MSD % Rec
Parameter Units Result
Conc,
Conc,
Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 14100
184
184
13800 13400 -141 -401 90-110 4 M6
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2492914 2492915
MS MSD
92416464001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 10200 49 49.9 12700 11200 5120 2100 90-110 12 M6,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2019 11:12 AM without the written consent 01 Pace Analytical Services, LLC.
Page 13 of 18

Analytical
www.pacelabs.com
Project:
Pace Project No,
DEFINITIONS
DUNN WTP 2/7/19
92416932
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) -Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC -Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute,
LABORATORIES
PASI-A
Pace
Analytical
Services -Asheville
PASI-C
Pace
Analytical
Services -Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2019 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

Analytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
DUNN WTP 2/7/19
92416932
Analytical
Lab ID
Sample
ID
QC Batch Method
QC Batch
Analytical Method
Batch
92416932001
DUNN
WTP
EPA 3050B
457387
EPA
601 OD
457494
92416932001
DUNN
WTP
EPA 7471 B
457445
EPA
7471 B
457534
92416932001
DUNN
WTP
SM 2540G-2011
457411
92416932001
DUNN
WTP
ASTM D2974-87
457237
92416932001
DUNN
WTP
EPA9045D
457221
92416932001
DUNN
WTP
SM 271OB-2011
457664
92416932001
DUNN
WTP
EPA 350.1 Rev 2.0
1993
457085
EPA
350.1 Rev
2.0
1993
457187
Mod.
Mod,
92416932001
DUNN
WTP
EPA 351.2 Rev 2.0
1993
457266
EPA
351.2 Rev
2.0
1993
457561
92416932001
DUNN
WTP
EPA 353.2 Rev 2.0
1993
457273
EPA
353.2 Rev
2.0
1993
457274
92416932001
DUNN
WTP
EPA 365.1 Rev 2.0
1993
457001
EPA
365.1 Rev
2.0
1993
457029
Date: 02/13/2019 11:12 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

>- Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2� Issuing Authority: .. ehiai'W(Cc7l Document No.:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Lanoratory
Asheville ® .Greenwood n Huntersville Raleigh[]
WoMechanicsvillen
32 Sample,Condltta•n� r •
Upon Receipt_ Project
■ •� ® ■ ' ■
■ Commercial ■' ■•
Date/InitialsCustody Seal Present? [JYes ffNo Seals Intact? RY�es E]No
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Otlier
Thermometer; l !?I Type of Ice: ❑wet [:]Blue❑IR Gun ID: -
Cooler Temp (°C): i `� • u) Correction Factor: Add/Subtract (°C) l
Cooler Temp Corrected (°C): i
USDA Regulated Soil (❑ N/A, vratersample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check in
❑Yes QNo
Chain of Custody Present? []Yes ❑No ❑N/A
Samples Arrived within Hold Time? .[Yes ❑No ❑N/A
Short Hold Time Analysis (02 hr.)? Dyes [36o ❑N/A
Rush Turn Around Time Requested? ❑Yes No ❑N/A
Sufficient Volume? Oes ❑No ❑N/A
Correct Containers Used? [2Pes ❑No ❑N/A
-Pace Containers Used? 04es ❑No ❑N/A
eyes Intact? es ❑No QN/A
Dissolved analysis: Samples Field Filtered? Dyes ❑No /A
Sample Labels Match COO []Yes ❑No ❑N/A
-Includes Date/Time/ID/Analysis Matrix: f�
Headspace in VOA Vials (>5-6mm)? ❑Yes ONO []NIA
Trip Blank Present? []Yes ❑No [L]N/A
:T
Trip Blank Custody Seals Present? ❑Yes ❑No ON/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Biological T[ssue Frozen?
❑Yes ❑No [7N/A
[]Plone
Temp
should be above freezing to 6°C
]Samples out of temp criteria. Samples on ice, cooling process
has begun
Lot ID of split containers:
Person contacted: Date/Time: _
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes�No
pate:
Date: � r
Page 16 of 18
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Biological T[ssue Frozen?
❑Yes ❑No [7N/A
[]Plone
Temp
should be above freezing to 6°C
]Samples out of temp criteria. Samples on ice, cooling process
has begun
Lot ID of split containers:
Person contacted: Date/Time: _
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes�No
pate:
Date: � r
Page 16 of 18

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
..-P cehlalytical
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/ dechlormation is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project
W®#:92
PM: LJP
16932
Due Date: 02/18/19
CLIENT: 92-SYNAGRO
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pH Adjustment Log for Preserved Samples
Note:
Sample iD
Type of Preservative
pH upon receipt
Date preservation adjusted
Time pre=.�rvalion
adjusted
Amount of Preservative
added
Lot ti
m r.,.Hfi��rinn llffi�> li a
Whenever there
is a discrepancy
affecting
North Carolina compliance
samples, a
copy
or
uus corm Will Be sent w ule iYV11+1 �o� ������ ��•••• -•�•-•••----- ---
Out of
hold, incorrect preservative,
out
of temp,
incorrect containers.
Page 17 of 18

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Page 18 of 18

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report
Range
Ratio
2188-02-WPL-NC
DUNN, NC WTP LIQUID
2/4/2019
2/1/2019-12/31/2019
4.5868
Na mg/I = (Na mg/kg x %Solids) = 100 = (5900 x 2.7000) = 100 = 159.3
Ca mg/I = (Ca mg/kg x %Solids) = 100 = (978 x 2.7000) _ 100 = 26.406
Mg mg/I = (mg mg/kg x %Solids) = 100 = (1440 x 2.7000) = 100 = 38.88
Na meq = Na mg/I : Molec.Wgt.Na = 159.3 _ 23 = 6.92609
Ca meq = Ca mg/I + Molec.Wgt.Ca = 26.406 = 20 = 1.3203
Mg meq = Mg mg/I + Molec.Wgt.Mg = 38.88 _ 12 = 3.24
SAR = Na meq : SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.92609 = SgrRoot[0.5(1.3203+3.24)] = 4.58676
Printed: 2/6/2020
Page 1 09:02

FACILITY NAME : DUNN, NC
OWNER: RAY N DELORES EDWARDS
SITE #: NC CU 00010 FIELD# : CU 00010 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: AUTRYVILLE
PERMIT #: WQ0006101
OPERATOR: RAY N DELORES EDWARDS
ANNUAL DRY TONS APPLIED : 10.24
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.60 ACRES PERMITTED: 7.60
rage: 1
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
( Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/16/19
111,600.00 (G)J747684,2111
2,20
1.347
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
BERMUDAGRASS, COASTAL - HAY
Apr49
11100.00 (G)
14,684.211
Total Gallons/Ac: 14,684.21
As I Cd I Cr I Cu I Pb I Hg I Mo I Ni I Se ( Zn I P I PAN
TOTALS
Annuallbs/acre I 0.039 I 0.005 I NR I 0.749 I 0.132 I 0.003 0.024 I 0.043 ( 0.039 I 1.261 I 40.14 I 54
Cumulative lbs/acre
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
X
0.253 � 0.186 � 2.657 � 14.725 � 6.075 � 0.050 ( 0.590 � 1.710 � 0.191 � 44.462
s d
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME: DUNN, INC
OWNER: RAY N DELORES EDWARDS
SITE #: NC CU 00010 FIELD# : CU 00010 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: AUTRYVILLE
PERMIT #: WQ0006101
OPERATOR: RAY N DELORES EDWARDS
ANNUAL DRY TONS APPLIED : 10.24
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.30 ACRES PERMITTED: 6.30
rage: 1
Lune Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
0
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/16/19
ill 1 600,00 (G)
17714,2861
2,20
1.625
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
BERMUDAGRASS, COASTAL - HAY
Apr49
1119600.00 (G)
179714.286
Total Gallons/Ac: 17,714.29
TOTALS: I As I Cd I Cr I Cu I Pb I Hg I Mo ) Ni I Se I Zn ( P I PAN
Annuallbs/acre I I I 0.029 I 0.051 0.047 1.521 I 48.43 65
0.047 0.006 NR 0.904 0.159 0.004
Cumulative Ibs/acre
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
X
0.047 ( 0.006 � NR ( 0.904 � 0.159 � 0.004 � 0.029 � 0.051 � 0.047 � 1.521
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR
=Not
Reported
or Not
Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
* Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME: DUNN,NC
OWNER: RAY N DELORES EDWARDS
SITE #: NC CU 00010 FIELD# : CU 00010 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: AUTRYVILLE
PERMIT #: W00006101
OPERATOR: RAY N DELORES EDWARDS
ANNUAL DRY TONS APPLIED : 30.72
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.00 ACRES PERMITTED: 11.00
rage: 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PANT
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/10/19
86,800.00 (G)
7890,90,
2.20
0.724
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
BERMUDAGRASS, COASTAL - HAY
4/11/19
4%600.00 (G)
4509,09,
2.20
0.414
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
I,050.00 p
20097
I BERMUDAGRASS, COASTAL - HAY
4/11/19
1423600,00 (G)
12963,636
2,20
1.189
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
BERMUDAGRASS, COASTAL - HAY
4/12/19
55,800.00 (G)
5072.727
2,20
0.465
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
635100. p
584.00 p
1,050.00 p
20097
BERMUDAGRASS, COASTAL - HAY
Apr49
334,800.00 (G)
309436.363
Total Gallons/Ac: 30,436.36
As I Cd I Cr I Cu I Pb I Hg I Mo ( Ni I Se I Zn I P I PAN
TOTALS
Annuallbs/acre 0.080 ( 0.011 NR 1.552 0.273 0.007 I 0.050 I 0.088 I 0.080 2.614 I 83.21 112
Cumulative Ibs/acre
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
0.141 � 0.039 ( 1.218 � 3.836 � 0.790 � 0.022 � 0.209 � 0.603 � 0.127 ( 13.089
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not
Required
% =percent p =ppm or, mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SUR1N -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME: DUNN, IN
OWNER: RAY N DELORES EDWARDS
SITE #: NC CU 00010 FIELD# : CU 00010 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : AUTRYVILLE
PERMIT #: W00006101
OPERATOR: RAY N DELORES EDWARDS
ANNUAL DRY TONS APPLIED : 14.22
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.80 ACRES PERMITTED: 4.80
Page: 1
Lune Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
( Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/10/19
155X0.00 (G)
22794,1181
2.20
2.091
DUAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
BERMUDAGRASS, COASTAL - HAY
Apr-19
15500.00 (G)
229794.118
Total Gallons/Ac: 22,794.12
TOTALS: I As I Cd I Cr I Cu I Pb I Hg I Mo I Ni I Se I Zn I P I PAN
Annuallbs/acre 0.060 I 0.008 NR I 1.163 0.205 0.005 I 0.038 0.066 0.060 1.957 I 62.32 84
Cumulative Ibs/acre
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
0.060 ( 0.008 � NR � 1.163 � 0.205 � 0.005 � 0.038 � 0.066 � 0.060 � 1.957
or if
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME: DUNN,NC
OWNER: HAROLD EDRIDGE
SITE #: NC CU 00034 FIELD# : CU 00034 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: WQ0006101
OPERATOR: HAROLD ELDRIDGE
ANNUAL DRY TONS APPLIED : 17.61
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.80 ACRES PERMITTED: 4.80
rage: 1
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/27/19
93,000.00 (G)
19375.0001
2.20
1.777
DUAEDL
DRY
0-<1/2"
SUR
0.
63,100. p
584.00 p
1,05
97
FESCUE PASTURE
Sep49
93,000.00 (G)
19,375.000
10/3/19
8000.00 (G)
16791,66712.70
1.891
DUWPL
DRY
0-<1/2"
SUR
3,780.0 p
327.00 p
73.50 p
1618
FESCUE PASTURE
Oct49
80,600.00 (G)
16,791,667
Total Gallons/Ac: 369166.67
TOTALS:
As
Cd
Cr
Cu
Pb
lag
Iwo
Ni
Se
Zn
P
PAN
Annual lbs/acre
0.096
0.011
NR
1.149
0.225
0.005
0.054
0.105
0.096
1.943
58.98
78
Cumulative lbs/acre
0.332
0.080
1.655
10.164
1.368
0.058
0.383
0.862
0.276
17.662
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
x
N t o LA-0 04
(SIGNATURE OF LAND APPLIER) DATE
certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designe
"I d to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR =Not
Reported
or Not
Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method: SUR -Surface,
INJ -Injection,
BURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACiLITYNAME: DUNN,NC
OWNER: HAROLD EDRIDGE
SITE #: NC CU 00034 FIELD# : CU 00034 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: W00006101
OPERATOR: HAROLD ELDRIDGE
ANNUAL DRY TONS APPLIED : 15.64
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.00 ACRES PERMITTED: 4.00
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
( Per Acre
Solids
Acre
Source
Moist
Hours
Rate" **
Rate
Nitrite
9/26/19
8600.00 (G)
21700.000
2.20
1.991
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
FESCUE PASTURE
Sep49
86,800.00 (G)
21,700.000
10/3/19
%200.00 (G)
17050,000
( 2.70
1.920
DUWPL
DRY
0-<I/2"
SUR
0.5
0.40
3,780.0 p
327.00 p
73.50 p
1618
FESCUE PASTURE
Oct49
68,200.00 (G)
17,050.000
1
I
Total Gallons/Ac: 38,750.00
As
Cu
Cr
Cu
Pb
rigIwoNi
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
86
0.103
0.012
NR
1.270
0.247
0.006
0.058
0.112
0.103
2.147 65.43
Cumulative lbs/acre
0.287
0.067
1.359
8.067
1.042
0.049
0.312
0.672
0.241
13.734
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepazed under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not
Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME : DUNN, NC
OWNER: HAROLD EDRIDGE
SITE #: NC CU 00034 FIELD# : CU 00034 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GOLDSBORO
PERMIT #: W00006101
OPERATOR: HAROLD ELDRIDGE
ANNUAL DRY TONS APPLIED : 15.77
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.30 ACRES PERMITTED: 4.30
rage: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/26/19
8000.00 (G)
18744.1861
2.20
1.720
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00
FESCUE PASTURE
Sep49
80,600.00 (G)
18,744.186
T0097
10/3/19
74,400.00 (G)
17302.3261
2.70
1.948
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
3,780.0 p
327.00 p
1 73.50 p
1618
FESCUE PASTURE
Oct49
74,400.00 (G)
17,302.326
Total Gallons/Ac: 36,046.51
As
Cd
Cr
Cu
Pb
rig
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
75
0.095
0.011
NR
1.122
0.221
0.005
0.054
0.104
0.095
1.897 57.44
Cumulative lbs/acre
0.352
0.084
1.682
10.265
1.379
0.060
0.398
0.933
0.286
17.902
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DUNN, NC
OWNER: HAROLD EDRIDGE
SITE #: NC CU 00034 FIELD# : CU 00034 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NORFOLK
PERMIT #: WQ0006101
OPERATOR: HAROLD ELDRIDGE
ANNUAL DRY TONS APPLIED : 23.24
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.20 ACRES PERMITTED: 6.20
Page : 1
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/25/19
49,600.00 (G)
8000.000
2,20
0.734
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
FESCUE PASTURE
9/26/19
74,400.00 (G)
12000,0001
2.20
1.101
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
635100. p
584.00 p
15050,00 p
20097
FESCUE PASTURE
Sep49
124,000.00 (G)
20,000.000
10/3/19
49,600.00 (G)
8000,000
2.70
0.901
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
3,780.0 p
327.00 p
73.50 p
1618
I FESCUE PASTURE
10/4/19
5500.00 (G)
9000,000
2.70
1.013
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
35780,01)
327.00 p
73.50 p
1618
FESCUE PASTURE
Oct-19
105,400.00 (G)
179000.000
Total Gallons/Ac: 379000.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
tNR
80
0.098
0.012
1.183
0.231
0.005
0.056
0.107
0.098
2.000
60.76
Cumulative lbs/acre
0.368
0.086
1.655
10.046
1.397
0.057
0.382
0.893
0.289
17.528
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: DUNN,NC
OWNER: HAROLD EDRIDGE
SITE #: NC CU 00034 FIELD# : CU 00034 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GOLDSBORO
PERMIT #: WQ0006101
OPERATOR: HAROLD ELDRIDGE
ANNUAL DRY TONS APPLIED: 37.18
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.70 ACRES PERMITTED: 9.70
Page : 1
Lime Applied ***
Date
Lbs/Ac
T
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm )
Crop
p
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/25/19
192,200.00 (G)
19814.4331
2,20
1.818
DUAEDL
DRY
0-<1/2"
SUR
0.5
0.30
63,100. p
584.00 p
1,050.00 p
20097
FESCUE PASTURE
Sep49
192,200.00 (G)
199814,433
10/3/19
37,200,00 (G)
3835.052I
2,70
0.432
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
3,780.Op
327.00 p
73.50 p
1618
I FESCUE PASTURE
10/4/19
136,400.00 (G)
14061,856
2.70
1.583
DUWPL
DRY
0-<1/2"
SUR
0.5
0.40
3,780.0 p
327.00 p
73.50 p
1618
FESCUE PASTURE
Oc09
173,600.00 (G)
179896.908
otal (jallons/Ac: 37,711.34
As
Cd
Cr
Cu
Pb
Hg
Iwo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
80
0.100
0.012
NR
1.182
0.232
0.005
0.056
0.109
0.100
1.999 60.58
Cumulative Ibs/acre
0.344
0.084
1.613
10.446
1.433
0.057
0.377
0.882
0.283
18.006
DUAEDL = DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
DUWPL = DUNN, NC WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

Summit Environmental Technologies, Inc.
NUMM111 3310 Win St.
MVIRONtd@NTALTECHNOLOGIE5, We Cuyahoga Falls, Ohio 44223
Arralytical Laboratoollee TEL: [phone] FAX.• [phone]
Website: htto:/hvwiv.settek.com
March 155 2017
Chad M. Hayes
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Dunn WWTP
Dear Chad M. Hayes:
Order No.: 17030217
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/3/2017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Mazykmd
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon 0 00001, Rhode Island LA000317, South Carolina 92016001,
Texas TI04704466-11-5, Region 8 8TMS-L, USDA/APHIS P33041-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C
Page 1 of 50

Summit Environmental Technologies, Inc.
XUAMMIT 3310 Win St.
Fr4VIRONh1ENTALTECHNOLOGIES,INCO Cuyahoga Falls, Ohio44223
Arrafylrcal La4aralaries TEL: [phone] FAX: [phone]
Website: htto:11'wimsettek.com
CLIENT: Synagro
Project: Dunn WWTP
Case Narrative
WO#: 17030217
Date: 3/15/2017
WorkOrder Narrative:
17030217: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental -
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Comments:
ccv 20ppb c0306/ 1096834: Analytical Comments for voc-MSTR npw(8260), Sample ccv 20ppb
c0306/, Batch ID R66502 : The VOC CCV (Batch R66502) exhibited slightly high (120.51/6) recovery
For Method -Specified CCC Vinyl chloride; All samples were ND for Vinyl chloride. All other Method -
Specified CCCs and SPCCs exhibited control.
mb-25849 1098253: Analytical Comments for tclp-svoc-cpest tclp(8081), Sample mb-25849, Batch ID
25849 : The TCLP Pesticides Method Blank (Batch 25849) exhibited high recovery for Surrogate:
DCB; MB was ND for all analytes of interest.
lcs-25849 1098254: Analytical Comments for tclp-svoc-cpest tclp(8081), Sample lcs-25849, Batch ID
25849: The TCLP Pesticides LCS (Batch 25849) exhibited high recovery for Surrogate: DCB; All
Original
Page 2 of 50

SUMMIT
r-f fVIRONk1EN7AL IECHNOLOGlr:S, lNG.
Arrafyf,%F al Lahcqralqf-lg
Suntntit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: htto:lAvimsettek.com
CLIENT: Synagro
Project: Dunn WWTP
other analytes of interest exhibited recoveries within acceptance limits.
Case Narrative
WO#: 17030217
Date: 3/15/2017
Original
Page 3 of 50

SUMMIT
FNVIRONMENTAL MHNOLOGIES, INC
h7iefytiCaP Lab€rratrl�s
Summit Environmental Technologies, in
3310 Win 5
Cuyahoga Falls, Qhio 4422
TEL: [phone] FAX 1330J 253-445
Website: http:/hvwwsettek.co
Qualifiers and Acronyms
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
WO#: 17030217
Date: 3/15/2017
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
C The result is below the Mini
Mmum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC./+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
)CS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 50

U > IT
MVIRONMENTAL TECHNOLOGIES[ INC.
Analytical Laboratories
CLIENT: Synagro
Project: Dunn WWTP
Lab SampleID Client Sample ID
1703021M01 Dunn WWTP
SummitEnrironmental Technologies, Inc.
3310 Win St.
Cuyahoga Fans, Ohio 44223
TEL: [phone] FAX.[phone]
Website: htto:/hvivw,settek.com
Tag No Date Collected
3/2/2017 11:00:00 AM
Workorder
Sample Summary
WO#: 17030217
I S Mar-17
Date Received Matrix
3/3/2017 1:40:00 PM Sludge
Page 5 of 50

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, NC. Cuyahoga Falls, Ohio 44223
Arralyllcal Lsb#ratories TEL: [phone] FAX: [phone]
Website: hQ://www.settekeom
DATES REPORT
WO#: 17030217
I5-Mar-17
Client: Synagro
Project: Dunn WWTP
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
17030217-OOIA Dunn WWTP 3/2/2017 11:00:00 AM Sludge Ignitability of Solids (SW-846: 1030)
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)
3/8/2017 11:00:00 AM
3/10/2017 4:03:00 PM
3/6/2017 11:45:00 AM
3/6/2017 11:45:00 AM
SVOC 8270 TCLP BNA List 3/6/2017 5:29:57
PM
3/8/2017 8:30:00 AM
3/13/2017 4:46:00
PM
SVOC SW-846: 8081-TCLP Pesticide43/6/2017 5:29:57
PM
3/8/2017 7:00:00 AM
3/9/2017 5:09:00
PM
SVOC SW-846: 8151 Herbicides-TCL3/6/2017 5:29:57
PM
3/7/2017 10:30:00 AM
3/10/2017 10:26:00
PM
TCLP Mercury Analysis (1311/7470) 3/6/2017 5:29:57
PM
3/7/2017 11:00:00 AM
3/7/2017 6:31:00
PM
TCLP Metals Analysis (6010)
VOC
3/6/2017 5:29:57 PM 3/7/2017 9:50:48 AM 3/9/2017 10:09:47 AM
3/7/2017 11:51:00 PM
Original
Page 6 of 50

StawnitBnrh omnental Technologies, Inc. Analytical Report
SUMMIT 3310 Win St.
rFS'�rIRONMENTALTECHNOLdG1E5,INC. Cuyahoga Falls, Ohio44223 (base report)
ArralytTael Laboratories TEL: [phone] FAX.- [phone] WO#: 17030217
Website: httP.*11Wini?.settek.com Date Reported: 3/15/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2017 11:00:00 AM
Lab ID: 17030217-001A
Project: Dunn WWTP
Client Sample ID Dunn WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (1311/7470)
TCLP Mercury
ND 0.00200
SW7470A SW7470A Analyst: ALJ
mg/L 1 3/7/2017 6:31:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010C SW3010A Analyst: WK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As) ND 0,500 mg/L 1 3/9/2017 10:09:47 AM
TCLP Barium(Ba) ND 5,00 mg/L 1 3/9/2017 10:09:47 AM
TCLP Cadmium(Cd) ND 0,100 mg/L 1 3/9/2017 10:09:47 AM
TCLP Chromium(Cr) ND 0,200 mg/L 1 3/9/2017 10:09:47 AM
TCLP Lead(Pb) ND 0,500 mg/L 1 3/9/2017 10:09:47 AM
TCLP Selenium(Se) ND 0.500 mg/L 1 3/9/2017 10:09:47 AM
TCLP Silver(Ag) ND 0,500 mg/L 1 3/9/2017 10:09:47 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270C SW3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene ND 0,0800 mg/L 2 3/13/2017 4:46:00 PM
2,4,5-Trichlorophenol ND 0,200 mg/L 2 3/13/2017 4:46:00 PM
2,4,6-Trichlorophenol ND 0,200 mg/L 2 3/13/2017 4:46:00 PM
2,4-Dinitrotoluene ND 0.100 mg/L 2 3/13/2017 4:46:00 PM
Cresols, Total ND 4,00 mg/L 2 3/13/2017 4:46:00 PM
Hexachloro-1,3-butadiene ND 0.100 mg/L 2 3/13/2017 4:46:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 3/13/2017 4:46:00 PM
Hexachloroethane ND 0,0800 mg/L 2 3/13/2017 4:46:00 PM
Nitrobenzene ND 0,0800 mg/L 2 3/13/2017 4:46:00 PM
Pentachlorophenol ND 0,200 mg/L 2 3/13/2017 4:46:00 PM
Pyridine ND 0,200 mg/L 2 3/13/2017 4:46:00 PM
Surr: 2-Fluorophenol 63.0 10 - 109 %Rec 2 3/13/2017 4:46:00 PM
Surr: Phenol-d6 64.2 10 - 109 %Rec 2 3/13/2017 4:46:00 PM
Surr: Nitrobenzene-d5 67.5 19 - 120 %Rec 2 3/13/2017 4:46:00 PM
Surr: 2,4,6-Tribromophenol 77.6 10 - 120 %Rec 2 3/13/2017 4:46:00 PM
Surr: 2-Fluorobiphenyl 62.9 22 - 117 %Rec 2 3/13/2017 4:46:00 PM
Surr: p-Terphenyl-d14 75.8 34 - 116 %Rec 2 3/13/2017 4:46:00 PM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 50

IT SummitEnvironmental Technologies, C. Analytical Report
SUMM3310 Win St.
FNVIRONMENTAL TECHNOWG]ES, INN Cuyahoga Falls, Ohio 44223 (base report)
Arraiptical Laboratories TEL: [phone] FAX., [phone] WO#: 17030217
Website: http:11iniinv.settek.com Date Reported: 3/15/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2017 11:00:00 AM
Lab ID: 17030217-001A
Project: Dunn WWTP
Client Sample ID Dunn WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081A SW3510C Analyst: JBN
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total ND 0.0100 mg/L 1 3/9/2017 5:09:00 PM
Toxaphene ND 0.0200 mg/L 1 3/9/2017 5:09:00 PM
Endrin ND 0.00100 mg/L 1 3/9/2017 5:09:00 PM
gamma-BHC ND 0.00100 mg/L 1 3/9/2017 5:09:00 PM
Heptachlor ND 0.00100 mg/L 1 3/9/2017 5:09:00 PM
Heptachlor epoxide ND 0.00100 mg/L 1 3/9/2017 5:09:00 PM
Methoxychlor ND 0,00100 mg/L 1 3/9/2017 5:09:00 PM
Surr: TCMX 73.7 10 - 119 %Rec 1 3/9/2017 5:09:00 PM
Surr: DCB 89.9 10 - 119 %Rec 1 3/9/2017 5:09:00 PM
TCLP HERBICIDES ANALYSIS (SW846 1311/8151) SW8151A SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D ND 1.00 mg/L 1 3/10/2017 10:26:00 PM
214,5-TP ND 0.500 mg/L 1 3/10/2017 10:26:00 PM
Surr: DCAA 75.8 20 - 140 %Rec 1 3/10/2017 10:26:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B Analyst: MES
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
1,2-Dichloroethane ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
MEK ND 2.00 mg/L 1 3/7/2017 11:51:00 PM
Benzene ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Carbon tetrachloride ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Chlorobenzene ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Chloroform ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Tetrachloroethene ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Trichloroethene ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Vinyl chloride ND 0.200 QC+ mg/L 1 3/7/2017 11:51:00 PM
Surr: 4-Bromofluorobenzene 97.2 70 - 130 %Rec 1 3/7/2017 11:51:00 PM
Surr: Dibromofluoromethane 96.0 70 - 130 %Rec 1 3/7/2017 11:51:00 PM
Surr: Toluene-d8 100 70 - 130 %Rec 1 3/7/2017 11:51:00 PM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 8 of 50

U I V Summit Environmental Technologies, Inc.
3310 Win St. Analytical Report
FFWIRONh1EWALTECHNOLOGIESTgnc Cuyahoga Falls, Ohio44223 (base report)
ArraPytir_al LaboraiorJes TEL: [phone] FAX: [phone] WO#: 17030217
Website: ht 2.*1Aywiy.settek.com Date Reported: 3/15/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2017 11:00:00 AM
Lab ID: 17030217-001A
Project: Dunn WWTP
Client Sample ID Dunn WWTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.500 mg/Kg 1 3/6/2017 11:45:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: RMT
Ignitability Non-flammable. 1 3/8/2017 11:00:00 AM
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 6.5 s.u.@19.7C 1 3/10/2017 4:03:00 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND 25.0 mg/Kg 1 3/6/2017 11:45:00 AM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for prepazation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 9 of 50

U1 T Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVIRONNIENTALTEC11t4OLOG1'=S, 3NC Cuyahoga Falls, Ohio 44223 WO#: 17030217
APral'y Ucal .isbarsrarie57 TEL: [phone] FAX.- [phone]
Website: hgp:llwivw.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: 25824
Sample ID MB-25824
SampType: MBLK
TestCode:
Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/7/2017
RunNo: 66446
Client ID: PBW
Batch ID: 25824
TestNo:
SW6010C SW3010A
Analysis Date: 3/7/2017
SegNo: 1096699
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
ND
0.500
TCLP
Barium(Ba)
ND
5.00
TCLP
Cadmium(Cd)
ND
0.100
TCLP
Chromium(Cr)
ND
0.200
TCLP
Lead(Pb)
ND
0.500
TCLP
Selenium(Se)
ND
0.500
TCLP
Silver(Ag)
ND
0.500
Sample ID LCS-25824
SampType: LCS
TestCode:
Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/7/2017
RunNo: 66446
Client ID: LCSW
Batch ID: 25824
TestNo:
SW6010C SW3010A
Analysis Date: 3/7/2017
SegNo: 1096700
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
1.98
0.500
2.000
0
99.0
80
120
TCLP
Banum(Ba)
ND
5.00
2.000
0
102
80
120
TCLP
Cadmium(Cd)
1.99
0.100
2.000
0
99.6
80
120
TCLP
Chromium(Cr)
2.01
0.200
2.000
0
100
80
120
TCLP
Lead(Pb)
2.00
0.500
2.000
0
99.8
80
120
TCLP
Selenium(Se)
1.99
0.500
2.000
0
99.7
80
120
TCLP
Silver(Ag)
1.01
0.500
1.000
0
101
80
120
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 10 of 50

NUMMITSummit
Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVIRONMENTAL INC Cuyahoga Falls, Ohio 44223 WO#: 17030217
A"Iytleal taboratarles TEL: [phone] FAX.- [phone]
Website: http://wivw.settek.eom 15-Mar47
Client: Synagro
Project: Dunn WWTP BatchID: 25839
TCLP Mercury ND 0.00200
TCLP Mercury 0.00411 0.00200 0.00400 0 103 80 120
Sample ID 17021496408AMS
SampType: MS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 3/7/2017
RunNo: 66490
Client ID: BatchQC
Batch ID: 25839
TestNo:
SW7470A SW7470A
Analysis Date: 3/7/2017
SegNo: 1096551
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit
RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00416 0.00200 0.00400 0 104 75 125
Sample ID
17021496-008AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
25839
Analyte Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
Prep Date: 3/7/2017
Analysis Date: 3/7/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66490
SegNo: 1096552
%RPD RPDLimit Qual
i'CLP Mercury 0.00417 0.00200 0.00400 0 104 75 125 0.00416 0.240 20
Qualifiers: * Value exceeds Maximwn Contaminant Level.
H Holding times for preparation or analysis exceeded
B Analyte detected in the associated Method Blank
E Value above quantitation range
Original

U' T Summit Environmental Technologies, Inc.
S3310 Win St.
ENVI;Q4MMENTAL TECHN4LOGIc.S, INC Cuyahoga Falls, Ohio 44223
AnalytlCal taborainries TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Client: Synagro
Project: Dunn WWTP
Sample ID
17021496-008AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
25839
Analyte
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
QC SUMMARY REPORT
WO#: 17030217
I S-Mar-17
BatchID: 25839
Prep Date: 3/7/2017
Analysis Date: 3/7/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66490
SegNo: 1096552
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 12 of 50

ffJISUMMIT St
3310 Win St.
Summit Environmental Technologies,Inc. QC SUMMARY REPORT
ENVIRON141ENTAL TECHNOLOGIES. '. c Cuyahoga Falls, Ohio 44223 WO#: 17030217
lthPu ticaP iebOratarles TEL: [phone] FAX., [phone]
Website: httg:Ilivivw.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: 25848
Sample ID mb-25848
SampType: mblk
TestCode:
tclp-svoc-her
Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: PBW
Batch ID: 25848
TestNo:
SW8151A
SW8151A
Analysis Date: 3/10/2017
SegNo: 1099064
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0 0
2,4,5-TP ND 0,500 0 0
Surr: DCAA 320 500.0 64.0 20 140
Sample ID Ics-25848
SampType: Ics
TestCode:
tclp-svoc-her
Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: LCSW
Batch ID: 25848
TestNo:
SW8151A
SW8151A
Analysis Date: 3/1012017
SegNo: 1099065
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
214-D
ND
1.00 0.500
0 80.3
62.6
125
21475-TP
ND
0.500 0.500
0 79.6
52.5
128
Surr: DCAA
430
500.0
86.0
20
140
Sample ID 17030217-001ams
SampType: ms
TestCode:
tclp-svoc-her
Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: Dunn WWTP
Batch ID: 25848
TestNo:
SW8151A
SW8151A
Analysis Date: 3/1012017
SegNo: 1099066
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
214-D
ND
1.00 0.500
0 80.0
37
105
2,4,5-TP
ND
0.500 0.500
0 78.9
38
106
Surr: DCAA
416
500.0
83.2
20
140
Qualifiers: *
Value exceeds Maximmn Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confinnation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 13 of 50

ui, luSummit Environmental Technologies, Inc.us3310 Win St. QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls. Ohio 44223 WO#: 17030217
1lhafyf/aaa .fbOratcaries TEL: [phone] FAX., [phone]
Wehsite: htto:11Wwrv.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: 25848
Sample ID 17030217-001amsd
SampType: msd
TestCode:
tclp-svoc-her
Units: mg/L
Prep Date: 3/7/2017
RunNo: 66643
Client ID: Dunn WWTP
Batch ID: 25848
TestNo:
SW8151A
SW8151A
Analysis Date: 3/10/2017
SegNo: 1099067
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 75.9
37
105
0 0 30
2,4,5-TP
ND
0.500 0.500
0 74.7
38
106
0 0 30
Surr: DCAA
393
500.0
78.6
20
140
0
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 14 of 50

Inc
SUMMIT Summit Environmental Technologies, 3310 Win StSt. . QC SUMMARY REPORT
EPAuIROWENTAL TECHNOL GI,E1 S, WC Cuyahoga Falls, Ohio 44223 WO#: 17030217
Analytical Laborgfnries TEL: [phone] FAX.- [phone]
Website: http://rvwrv.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: 25849
Sample ID mb-25849
SampType: Aim
TestCode:
tclp-svoc-cpe
Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: PBW
Batch ID: 25849
TestNo:
SW8081A
SW3510C
Analysis Date: 3/9/2017
SegNo: 1098253
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00500
Toxaphene
ND
0,0100
Endrin
ND
0,000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0,000500
Surr: TCMX
8.23
Surr: DCB
11.9
d
10.00 82.3 10 119
10.00 119 10 119 S
Sample ID Ics-25849
SampType: Ics
TestCode:
tclp-svoc-cpe
Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: LCSW
Batch ID: 25849
TestNo:
SW8081A
SW3510C
Analysis Date: 3/9/2017
SegNo: 1098254
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00600
0.000500
0.00500
0
120
20
157
gamma-BHC
0.00426
0.000500
0.00500
0
85.3
22
137
Heptachlor
0.00553
0,000500
0,00500
0
111
24
121
Heptachlor epoxide
0,00565
0,000500
0.00500
0
113
27
152
Methoxychlor
0,00608
0,000500
0.00500
0
122
10
199
Surr: TCMX
10.5
10.00
105
10
119
Surr: DCB
14.1
10.00
141
10
119
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding tunes for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to detennine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
E`
Original
Page 15 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIT 3310 Win St.
rEMNIROMMENTALTECHUOLCGl1=S, INC Cuyahoga Falls, Ohio 44223 WO#: 17030217
4!ralyb1cal Laboratarie= TEL: [phone] FAX.• [phone]
Website: http://`wivw.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: 25849
Sample ID 17030215-001ams
SampType: ms
TestCode:
tclp-svoc-cpe
Units: mg/L
Prep Date: 3/8/2017
RUnNo: 66588
Client ID: BatchQC
Batch ID: 25849
TestNo:
SW8081A
SW3510C
Analysis Date: 3/9/2017
SegNo: 1098255
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0105
0.00100
0.0100
0
105
20
157
gamma-BHC
0,00712
0,00100
0.0100
0
71.2
22
137
Heptachlor
0,00878
0.00100
0.0100
0
87.8
24
121
Heptachlor epoxide
0,00969
0,00100
0.0100
0
96.9
27
152
Methoxychlor
0.0117
0,00100
0.0100
0
117
10
199
Surr: TCMX
12.0
20.00
60.0
10
119
Surr: DCB
22.3
20.00
112
10
119
Sample ID 17030215-001amsd
SampType: msd
TestCode:
tclp-svoc-cpe
Units: mg/L
Prep Date: 3/8/2017
RunNo: 66588
Client ID: BatchQC
Batch ID: 25849
TestNo:
SW8081A
SW3510C
Analysis Date: 3/9/2017
SegNo: 1098256
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00891
0.00100
0.0100
0
89.1
20
157
0.0105
16.7
30
gamma-BHC
0.00672
0.00100
0.0100
0
67.2
22
137
0,00712
5.78
30
Heptachlor
0,00825
0,00100
0.0100
0
82.5
24
121
0,00878
6.20
30
Heptachlor epoxide
0,00868
0,00100
0.0100
0
86.8
27
152
0.00969
10.9
30
Methoxychlor
0,00961
0.00100
0.0100
0
96.1
10
199
0.0117
19.9
30
Surr: TCMX
12.4
20.00
61.8
10
119
0
Surr: DCB
16.9
20.00
84.5
10
119
0
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manua] Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 16 of 50

1 T Summit Environmental Technologies, Inc.
NUMM3310 Win St.
ENVIRONb1$NTAI. TECfiNOL@GY=_5, "C Cuyahoga Falls, Ohio 44223
Analytha/ 1,4wnsrarier TEL: [phone] FAX: [phone]
Website: http://lviviv.settelc.com
Client: Synagro
Project: Dunn WWTP
Sample ID MB-25878
SampType: MBLK
TestCode:
SVOC-BNA_T Units: mg/L
Client ID: PBW
Batch ID: 25878
TestNo:
SW8270C SW3510C
Analyte
Result
PQL
SPK value SPK Ref Val
1,4-Dichlorobenzene
ND
0.0200
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0,0100
Cresols, Total
ND
1,00
Hexachloro-1,3-butadiene
ND
0,00400
Hexachlorobenzene
ND
0,0100
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0,0500
Pyridine
ND
0,0500
Surr: 2-Fluorophenol
0,335
Surr: Phenol-d6
0,343
Surr: Nitrobenzene-d5
0,376
Surr: 2,4,6-Tribromophenol
0,457
Surr: 2-Fluorobiphenyl
0,350
Surr: p-Terphenyl-d14
0,436
QC SUMMARY REPORT
WO#: 17030217
I S-Mar-17
BatchID: 25878
Prep Date: 3/8/2017
Analysis Date: 3/13/2017
%REC LowLimit HighLimit RPD Ref Val
0.5000
67.0
10
109
0.5000
68.6
10
109
0.5000
75.3
19
120
0.5000
91.4
10
120
0.5000
70.0
22
117
0.5000
87.2
34
116
RunNo: 66688
SegNo: 1099749
%RPD RPDLimit Qual
Sample ID
LCS-25878
SampType:
LCS
TestCode:
SVOC-BNA_T
Units:
mg/L
Prep
Date:
3/8/2017
RunNo:
66688
Client ID:
LCSW
Batch ID:
25878
TestNo:
SW8270C
SW3510C
Analysis
Date:
311312017
SegNo:
1099750
Analyte Result PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 17 of 50

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHN{iLOGIES$ INC Cuyahoga Falls, Ohio 44223
A.rsPkr cal Labvrotarles TEL: [phone] FAX.* [phone]
Website: http://wwiv.settek.com
Client: Synagro
Project: Dunn WWTP
QC SUMMARY REPORT
BatchID: 25878
WO#: 17030217
15-Mar-l7
Sample ID LCS-25878 SampType: LCS , TestCode: SVOC-BNA_T Units: mg/L Prep Date: 3/8/2017 RunNo: 66688
Client ID: LCSW Batch ID: 25878 TestNo: SW8270C SW3510C Analysis Date: 3/13/2017 SegNo: 1099750
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene
0.198
0.0200
0.2000
0
99.0
19.1
126
2,4,5-Trichlorophenol
0.257
0.0500
0.2000
0
128
11.7
151
2,4,6-Trichlorophenol
0.254
0.0500
0.2000
0
127
12.4
150
2,4-Dinitrotoluene
0.279
0.0100
0.2000
0
140
20.6
140
Cresols, Total
ND
1.00
0.4000
0
119
10
129
Hexachloro-1,3-butadiene
0.202
0,00400
0.2000
0
101
14.7
137
Hexachlorobenzene
0.215
0.0100
0.2000
0
107
12
139
Hexachloroethane
0.214
0.0200
0.2000
0
107
14.8
132
Nitrobenzene
0.233
0.0200
0.2000
0
116
15.6
138
Pentachlorophenol
0.201
0.0500
0.2000
0
101
10
156
Pyridine
0.0705
0.0500
0.2000
0
35.3
10
126
Surr: 2-171uorophenol
0.454
0.5000
90.7
10
147
Surr: Phenol-d6
0.464
0.5000
92.7
10
140
Surr: Nitrobenzene-d5
0.480
0.5000
95.9
10
169
Surr: 2,4,6-Tribromophenol
0.590
0.5000
118
10
185
Surr: 2-Fluorobiphenyl
0.442
0.5000
88.4
10
169
Surr: p-Terphenyl-d14
0.495
0.5000
99.0
10
179
Sample ID
17030030-001AMS
SampType:
MS
Client ID:
BatchQC
Batch ID:
25878
Analyte
Result
TestCode: SVOC-BNA_T Units: mg/L
TestNo: SW8270C SW3510C
PQL SPK value SPK Ref Val
Prep Date: 3/8/2017
Analysis Date: 3/13/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66688
SegNo: 1099752
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 18 of 50

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIs'tNIAENTALTECHWOL061£S,'WC Cuyahoga Falls, Ohio44223
nalytical laboratories TEL: [phone] FAX.d [phone]
Website: http://ivww.settek.com
Client: Synagro
Project: Dunn WWTP
QC SUMMARY REPORT
WO#: 17030217
I S-Mar-17
BatchID: 25878
Sample ID
17030030-001AMS
SampType:
M5
TestCode:
SVOC-BNA_T
Units:
mg/L
Prep
Date:
3/8/2017
Client ID:
BatchQC
Batch ID:
25878
TestNo:
SW8270C
SW3510C
Analysis
Date:
3/13/2017
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
1,4-Dichlorobenzene
0.416
0.0800
0.4000
0
104
29
112
2,4,5-Trichlorophenol
0,501
0.200
0.4000
0
125
53
123
2,4,6-Trichlorophenol
0,497
0.200
0,4000
0
124
50
125
2,4-Dinitrotoluene
0,524
0.0400
0,4000
0
131
57
128
Cresols, Total
ND
4,00
0.8000
0
119
20
125
Hexachloro-1,3-butadiene
0,393
0.0160
0.4000
0
98.2
22
124
Hexachlorobenzene
0.416
0,0400
0.4000
0
104
53
125
Hexachloroethane
0.458
0.0800
0,4000
0
115
21
115
Nitrobenzene
0,478
0.0800
0,4000
0
120
45
121
Pentachlorophenol
0,441
0.200
0,4000
0
110
35
138
Pyridine
ND
0,200
0.4000
0
21.3
10
126
Surr: 2-Fluorophenol
0,841
1.000
84.1
10
147
Surr: Phenol-d6
0.856
1.000
85.6
10
140
Surr: Nitrobenzene-d5
0.917
1.000
91.7
10
169
Surr: 2,4,6-Tribromophenol
1.04
1,000
104
10
185
Surr: 2-Fluorobiphenyl
0.806
1,000
80.6
10
169
Surr: p-Terphenyl-d14
0.919
1,000
91.9
10
179
RunNo: 66688
SegNo: 1099752
%RPD RPDLimit Qual
Sample ID
17030030-001AMSD
SampType:
MSD
TestCode:
SVOC-BNA_T
Units:
mg/L
Prep
Date:
3/8/2017
RunNo:
66688
Client ID:
BatchQC
Batch ID:
25878
TestNo:
SW8270C
SW3510C
Analysis
Date:
3/13/2017
SegNo:
1099753
Analyte
Result
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
S
S
mQMR
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contatninant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 19 of 50

SummitEnvironmental Technologies, Inc.
Ul I 3310 Win St.
r:NVIRON1de:NTAL TEC'HUOLOGIE1 S, INC Cuyahoga Falls, Ohio 44223
/6riafyticat t,sboramriea TEL: [phone] FAX: [phone]
Website: httn://wwiv.settek.com
Client: Synagro
Project: Dunn WWTP
Sample ID
17030030-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
25878
Analyte
Result
TestCode: SVOC-BNA T Units: mg/L
TestNo: SW8270C SW3510C
PQL SPK value SPK Ref Val
WO#: 17030217
15-Mar-17
BatchID: 25878
Prep Date: 3/8/2017
Analysis Date: 3/13/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66688
SegNo: 1099753
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.368
0.0800
0.4000
0
92.1
29
112
0.4164
12.2
30
2,4,5-Trichlorophenol
0.438
0.200
0.4000
0
110
53
123
0.5008
13A
30
2,4,6-Trichlorophenol
0.433
0.200
0.4000
0
108
50
125
0.4968
13.8
30
2,4-Dinitrotoluene
0.444
0.0400
0.4000
0
111
57
128
0.5244
16.7
30
Cresols, Total
ND
4.00
0.8000
0
103
20
125
0
0
30
HexachloroA 3-butadiene
0.345
0.0160
0.4000
0
86.2
22
124
0.3928
13.0
30
Hexachlorobenzene
0.370
0.0400
0.4000
0
92.6
53
125
0.4164
11.7
30
Hexachloroethane
0.391
0.0800
0.4000
0
97.8
21
115
0.4580
15.7
30
Nitrobenzene
0.413
0.0800
0.4000
0
103
45
121
0.4780
14.5
30
Pentachlorophenol
0.387
0.200
0.4000
0
96.7
35
138
0.4408
13.0
30
Pyridine
ND
0.200
0.4000
0
38.1
10
126
0
0
30
Surr: 2-Fluorophenol
0.788
1.000
78.8
10
147
0
Surr: Phenokd6
0.817
1.000
81.7
10
140
0
Surr: Nitrobenzene-d5
0.844
1.000
84.4
10
169
0
Surr: 2,4,6-Tribromophenol
0.959
1.000
95.9
10
185
0
Surr: 2-Fluorobiphenyl
0.762
1.000
76.2
10
169
0
Surr: p-Terphenyl-d14
0.830
1.000
83.0
10
179
0
Qualifiers: *
Value exceeds Maximmn Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for prepazation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
i7
Original
Page 20 of 50

�� SummitEnvironmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONh1ENTAL TECHNOL DIES, INC Cuyahoga Falls, Ohio 44223 WO#: 17030217
AnTalyliral C.aborWorles TEL: [phone] FAX: [phone]
Website: htto://www.settek.com 15-Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: R66453
Cyanide, Reactive ND 0.500
Cyanide, Reactive 1.01 0.500 1.000 0 101 85 110
Sample ID 17021495-008AMS
SampType: MS
TestCode:
Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 66453
Client ID: BatchQC
Batch ID: R66453
TestNo:
SW9014
Analysis Date: 3/6/2017
SegNo: 1095928
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.07 0.500 1.000 0 107 81.6 122
Sample ID
17021495-008AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R66453
Analyte Result
TestCode: Cyanide,Rea Units: mg/Kg
TestNo: SW9014
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 3/6/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66453
SegNo: 1095929
%RPD RPDLimit Qual
Cyanide, Reactive 1.05 0.500 1.000 0 105 81.6 122 1.072 2.46 5
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
B Analyte detected in the associated Method Blank
E Value above quantitation range
Original
Page 21 of 50

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St,
ENVIRONMENTAL TECHHOL00*81 INC Cuyahoga Falls, Ohio 44223
A!tafpticat tnborWorles TEL: [phone] FAX.- (330) 2534489
Website: httn://www.settek.com
Client: Synagro
Project: Dunn WWTP
Sample ID
17021495-008AMSD
SampType:
MSD
Client ID:
Batch=
Batch ID:
R66453
Analyte
Result
TestCode: Cyanide,Rea Units: mg/Kg
TestNo: SW9014
PQL SPK value SPK Ref Val
QC SUMMARY REPORT
WO#: 17030217
15-Mar-17
BatchID: R66453
Prep Date:
Analysis Date: 3/6/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66453
SegNo: 1095929
%RPD RPDLimit Qual
qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 22 of 50

IT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
ENVIF ]NWWAL WCHNOL GIGS, 3KC Cuyahoga Falls, Ohio 44223 WO#: 17030217
Rhalyilaai ijroarsJarJes TEL: [phone] FAX.- [phone]
Website: http://ivww.settek.com 15-Mar-17
Client: Synagro
Project: Dunn WWTP BatchID: R66473
Sulfide, Reactive ND 25.0
Sulfide, Reactive 2100 25.0 2250 0 93.3 85 130115
Sulfide, Reactive 2130 25.0 2250 0 94.7 80 120
Sulfide, Reactive 2140 25.0 2250 0 95.1 80 120 2130 0.468 30
Qualifiers: 'p Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
Original

UI T Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVIRONMENTAL TECHHOL DIES, iNC Cuyahoga Falls, Ohio 44223
Arra►yiicai tvb0ratar/e5 TEL: [phone] FAX: [phone] WO#: 17030217
Website: http://ivivw.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
Sample ID 17021495-008AMSD SampType: MSD
Client ID: BatchQC
Analyte
Batch ID: R66473
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
BatchID: R66473
Prep Date:
Analysis Date: 3/6/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66473
SegNo: 1-096277
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contatninant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 24 of 50

U', MMITSummit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTALTECHUCLOGIES, INC Cuyahoga Falls, Ohio44223 WO#: 17030217
h_rr is tical C trbtSXafories TEL: [phone] FAX: [phone]
Website: ham://www.settekcom 15-Mar47
Client: Synagro
Project: Dunn WWTP BatchID: R66500
Ignitability lon-flammable. 0 0 20
Ignitability !on -flammable. 0 0 20
Ignitability Ion -flammable. 0 0 20
Ignitability
Ion -flammable.
0 0 20
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 25 of 50

UMil IT Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVIRON1AENTAL TECHNOL GIE5, JNC Cuyahoga Falls, Ohio 44223
WO#: 17030217
Arrd?iylr`ca1 i';aborstarJes TEL: [phone] FAX. [phone]
Website: htti7:llivivw.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP BatchID: R66500
Ignitability lon-flammable. 0 0 20
Ignitability Ion -flammable. 0 0 20
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 26 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIT 3310 Win St.
ENVIR'OMPoIENTA:L T6CHNOLOGIc5S, 3NC Cuyahoga Falls, Ohio 44223 WO#: 17030217
Anjfgticaf Caborstories TEL: [phone] FAX.- [phone]
Website: hay.011www.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: R66500
Sample ID
17030373-001ATRIP
SampType:
DUP
TestCode:
Ignitability_S Units:
Prep
Date:
RunNo:
66500
Client ID:
BatchQC
Batch ID:
R66500
TestNo:
SW1030
Analysis
Date: 3/8/2017
SegNo:
1096797
Analyte
Ignitability
Result
Ion -flammable.
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
0
%RPD RPDLimit Qual
0 20
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 27 of 50

SummitEnvironmental Technologies, Inc. QC SUMMARY REPORT
SUMMINIL3310 Win St.
rcP4Vl t0NG1ENTAL TEGHNOLQOt�rS, 311C Cuyahoga Falls, Ohio 44223
11..rraiytfcaP Laboratories TEL: [phone] FAX.' [phone]
WO#: 17030217
Website: httv:lliviviv.settek.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
Sample ID Ics 20ppb L-0306
Client ID: LCSW
Analyte
SampType: LCS
Batch ID: R66502
Result
TestCode: voc-MSTR_n Units: mg/L
TestNo: SW8260B
PQL SPK value SPK Ref Val
BatchID: R66502
Prep Date:
Analysis Date: 3/7/2017
%REC LowLimit HighLimit RPD Ref Val
1,1-Dichloroethene
0.0200
0.00500
0.0200
0
100
71
138
Benzene
0.0191
0.00500
0.0200
0
95.7
75
137
Chlorobenzene
0,0192
0,00500
0,0200
0
95.9
77
132
Trichloroethene
0.0196
0.00500
0.0200
0
97.8
64
119
Surr: 4-B romofl u oro benzene
51A
50,00
103
70
130
Surr: Dibromofluoromethane
49.4
50,00
98.8
70
130
Surr: Toluene-d8
51.1
50.00
102
70
130
RunNo: 66502
SegNo: 1096835
%RPD RPDLimit Qual
Sample ID mblk
SampType: MBLK
TestCode:
voc-MSTR_n Units: mg/L
Prep Date:
RunNo: 66502
Client ID: PBW
Batch ID: R66502
TestNo:
SW8260B
Analysis Date: 3/7/2017
SegNo: 1096837
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
111-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0,00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0,00200
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
QC+
Original
Page 28 of 50

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
IS UIMMIT 3310 Win St.
ENVIRCNIdENTALTECHNOLOGIES,INC Cuyahoga Falls, Ohio WO#: 17030217
ll TEL: [phone] FAX.- [phone]
Website: http://www.settelc.com 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: R66502
Sample ID
mblk
SampType:
MBLK
TestCode:
voc-MSTR_n Units: mg/L
Prep
Date:
RunNo:
66502
Client ID:
PBW
Batch ID:
R66502
TestNo:
SW8260B
Analysis
Date: 3/7/2017
SegNo:
1096837
Analyte Result PQL SPK value 5PK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Surr:4-Bromofluorobenzene
48.9
50.00
97.9
70 130
Surr:
Dibromofluoromethane
50.8
50.00
102
70 130
Surr:
Toluene-d8
50.1
50.00
100
70 130
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 29 of 50

�� SummitEnvironmentalTechnologies,Inc. QC SUMMARY REPORT
3310 Win St.
EKVIRONb1ENTAl-T6CHHOLOGIESINC Cuyahoga Falls, Ohio44223 WO#: 17030217
Artalyticai t aborsfories TEL: [phone] FAX: [phone]
Website: hMp:AAwww.settek.com 15 Mar47
Client: Synagro
Project: Dunn WWTP
SatchID: R66502
Sample ID
17030217-001ams
SampType:
MS
TestCode:
tclp-voc-MST Units: mg/L
Prep
Date:
RunNo:
66502
Client ID:
Dunn WWTP
Batch ID:
R66502
TestNo:
SW8260B
Analysis
Date: 3/8/2017
SegNo:
1096853
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit
1,1-Dichloroethene
0.174
0.0100
0.200
0
86.9
39.9
160
1,2-Dichloroethane
0.170
0.0100
0.200
0
85.0
42.5
157
MEK
1.02
0.0500
1.00
0
102
16.6
227
Benzene
0.190
0.0100
0.200
0
94.8
38A
155
Carbon tetrachloride
0.188
0.0100
0.200
0
93.8
40.8
162
Chlorobenzene
0.200
0.0100
0.200
0
100
35.7
168
Chloroform
0.186
0.0100
0.200
0
93.2
18.3
199
Tetrachloroethene
0.197
0.0100
0.200
0
98A
10
261
Trichloroethene
0.191
0.0100
0.200
0
95.3
23.8
175
Vinyl chloride
0.232
0.0100
0.200
0
116
10
165
Surr:4-Bromofluorobenzene
513
500.0
103
84.6
130
Surr: Dibromofluoromethane
478
500.0
95.5
71 A
127
Surr: Toluene-d8
510
500.0
102
74.6
127
Sample ID
17030217-001amsd
SampType:
MSD
TestCode:
tclp-voc-MST Units: mg/L
Prep
Date:
RunNo:
66502
Client ID:
Dunn WWTP
Batch ID:
R66502
TestNo:
SW8260B
Analysis
Date: 3/8/2017
SegNo:
1096854
Analyte
Result
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
Qual
OC+
%RPD RPDLimit Qual
1,1-Dichloroethene
0.177
0.0100
0200
0
88.6
39.9
160
0.174
1.99
25
1,2-Dichloroethane
0.169
0.0100
0.200
0
84.4
42.5
157
0.170
0.590
25
MEK
1.01
0.0500
1.00
0
101
16.6
227
1.02
1.52
25
Benzene
0.186
0.0100
0.200
0
93.1
38A
155
0.190
1.76
25
Qualifiers: * Value exceeds Maximum Contaminant Level, B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for prepazation or analysis exceeded J Analyte detected below quanfitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 30 of 50

IT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
NUMM3310 Win St.
ENVIROWENTAL TECHNOLOGIES, iNC Cuyahoga Falls, Ohio 44223 WO#: 17030217
Amwtpt/ca! Laborataries TEL: [phone] FAX: [phone]
Website: hgp.s11www.settek.com IS Mar47
Client: Synagro
Project: Dunn WWTP
Sample ID
17030217-001amsd
SampType:
MSD
Client ID:
Dunn WWTP
Batch ID:
R66502
Analyte
Result
TestCode: tclp-voc-MST Units: mg/L
TestNo: SW8260B
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 3/8/2017
%REC LowLimit HighLimit RPD Ref Val
RunNo: 66502
SegNo: 1096854
%RPD RPDLimit Qual
Carbon tetrachloride
0.182
0.0100
0.200
0
91.1
40.8
162
0.188
2.97
25
Chlorobenzene
0.189
0.0100
0.200
0
94.3
35.7
168
0.200
5.87
25
Chloroform
0.184
0.0100
0200
0
92.2
18.3
199
0.186
1.08
25
Tetrachloroethene
0.180
0.0100
0200
0
90.2
10
261
0.197
8.70
25
Trichloroethene
0.186
0.0100
0.200
0
92.8
23.8
175
0.191
2.66
25
Vinyl chloride
0.223
0.0100
0.200
0
112
10
165
0.232
3.91
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for prepazation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
QC+
Original
Page 31 of 50

SUMMIlt
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVIRONMENTAL TECHUOLOC1SS, Cuyahoga Falls, Ohio 44223 WO#: 17030217
AWlytical Iabo moriaf TEL: [phone] FAX: [phone]
Website: http:/hvivw.settekcom 15-Mar47
Client: Synagro
Project: Dunn WWTP
BatchID: R66612
Sample ID LCS-R666I2
SampType: LCS
TestCode:
pH_0II(9045 Units: S.U. a@19.6C
Prep Date:
RunNo: 66612
Client ID: LCSW
Batch ID: R66612
TestNo:
SW9045D
Analysis Date: 3/10/2017
SegNo: 1098612
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0
0 100 90 110
Sample ID 17030430-001ADUP
SampType: DUP
TestCode:
pH_Oil(9045 Units: s.u.@20.1C
Prep Date:
RunNo: 66612
Client ID: BatchQC
Batch ID: R66612
TestNo:
SW9045D
Analysis Date: 3/10/2017
SegNo: 1098614
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
5.8
0 0
5.8 0.7 10
Qualifiers: *
Value exceeds Maximum Contatninant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Pen -nit Limit
R
RPD outside accepted recovery limits
Original
Page 32 of 50

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Page 33 of 50

ac•r
Roy. 16
t rrP�Cdl4'l! nilil� •.i-•!i x�!t
Summit Envisan untat technologies, Inc.
Cooler Receipt Form
Initials of person inspecting cooler and sample —
Order Number.
Client: -----�-�-
Date Received:__ Tirne Received: t3 qo Date cooler(%) opened and samples inspected33,
Number of Ooo1ersl8oxes:_1 NIA
Shipper ED EX UPS DHL Airborne US postal 'Waik•in Pickup Other:
Packaging: Peanuts f3ubbl Wr Paper Foam None Other_ �_
Tape an cooler/box: _CYD N N/A
A
Custody Seals intact
C-O-C in pl stic t Y l N NIA
Icelue ice presen absent 1 melted NIA
Sample Temperature IR Gun #t Of 20459 CF t7 _ c °C �. ') - ----°C N/A
Radiological Testing Instrument serial #35127 Y N Nf
(see page 2 for scan results)
••Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be notified
immediately.
C-O-C filled out properly N NIA
Samples in separate bags N NIA
Sample containers intact' r N NIA
if no, list broken sample(s)
Sample labels) complete (If7, date, etc.) �Y N NIA
Labels) agree with C-O-C ( Y:) N N/A
Correct containers used cy N NIA
Sufficient sample received N N/A
Samples received within holding time Y N
E3ubbles absent from 40 mL vials"* Y N NIA
" Samples with bubbles e6mm are acceptable. Indicate rubble size if y6mm.
Was client contacted about samples Y N
Will client send new samples Y N
Client contact: _
Logged in by:..._.
Comments:
Pa3e t of 2
Page 34 of 50

North Carolina wastewaterlGroundwater Laboratory Certification
Certified Raranetem Llsung
Lad Mama Sufnrni4 Cmtednmental Tecnnaloolea: Inc.
rM1'ddrese: 331 C Win Street
Cuyahoga Falls, O, 144[23-
TIe atravr. nz-�rtc'tt luR�u:rtlarg, h8Y1'1�.tlJly rn![ if+e reginrrmrrac nI 95A.hICA,C H.p80D, re per trr' oerF�firJ hr m"surelnent A tm wrometers wEc bo2or
-- CERTIFFED PARAMETERS
INORGANfc RESIDUE. SUSPENDED
13OD SM 2540 01997 (Acueousy
SM 5210 P-2C07 i'Aquepu5) t2ESfP]sJE, TOTAL
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EPA 3E!D,U. ROV 2.1, 1093 (Aqueou5) EPA t3JU.04 Rev.2 1. tgQ (AcueouSl
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EPA 200.8, Rev . 5 A, tsNuJAQueou;)
5'Jw S45 6020 G (Aqueous)
Ir.ACNY 4 EPh 200.7, Rev. 4,, 1954 (Aqueous)
Sfhf-E46 t5010 D (Acueousr
EPA `2008. Rev 5.4, 1094 (Argf,.ctt5)
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Certified Parameters Listi?1g
LauDlame: 5e_rmm-t.Enucmni�arl l-echr. � I,eettli� Number 631
Adclrers- 31I Alin tigr<v:,q El'ective,E'a`e: i?V201 7
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CERTIFIED PARAMETERS
$ul.'-u'�11y 15Ui4'!•' �S-{�'1gk
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RWN!346 602013 (,ArjijlKJ s,]
FPA 200,8 Rear. _, 4 15g4 IAZL*V rsl
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i,LR ORGANICS
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EPA 625 (Ari,eoae)
SW 946 827C © iAqueo4ts}
GHLORINA,TEDADD HEF2i KJDES
O-846 8151 ✓4 (Aquvuk€sI
C1aLCRKNATI I) R�iENOLICS
EPA 1653, Ruv_A.. 1N7-.I,°;.gminu ;
YJaTFr�f:TACtLE F'E^:�tJLt:l}F1t �Y�'u^C.+kROC}h�S
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Certified Parameters lAst'sng
Lao Knew Gum.mi;.Enwrapimenta17echnn�p"aos:Inc . Numl?er: (i31
Address: 331'1"4 Wan Stre-et f E(fectiw pAIC: 171.2�s17
Cuyahoya FsI , DH 4420e3- Exp„ wil Date 1213Lact 17
Dato 5F Laat AwrtenUaher:L I 1 Are0 t 6
lqm sbove.i aned laboratgrr ndY,rlM s(ul4 Mill lha IoquIf3R12rlls ur 1SA fJtly4=;.H 45[n. rs MUmtq•eorrtW ior.the messurmen! cS :hr, fwasrrxiDrs. I slec.bedcw.
--- _ CCRTIFIEDPARAMETEA2S-----,-.--
INORGANIC SILICA —
BOO EPA 2005 7 Rl nil 4.4 1974 (Aqueousi
SI,( 5210 D 2001 4^queouc) tivd 4E6EU10D GCqueouFy
CHLORIDE SULFATE
SW-846 905.6 A I;Acuenu>,) EPA 3UU. U, kilt 7.1, 1993 (A.qL ee<-s;
COD SVJA46905C A (Aaue�uEJ
SPA 522C C:.19117 (Cwgn eous) 5 U 1-FIDE
R 1JORIDE EW, 546 R034 (A0LJF(l0S)
rPA300.0.Rev, 2,11 15193 (Anuaows) METAL
SYY-846 DMIS A (ArWulycros TCLF METALS
INC MANIC. PH ENO. 1La O
SW446 L3I 1 ;A:tuenlLsj
€Ph 420,1. Rev 1979 (A.junru5) 4LUMNLM r 4�
NITROGEN, hr'RRTF "— O
EPA, Z5(1.T Ruv:4 4. 1594 (AgiJennr%) O
EPA 300.1y, P.tv. 2:1, 1M iAquentFs; MM646 GO Q0;AgLeow.51 d M
SV41,646 90, 5:A (Amiem.$) EPA 200 8. (tev4. 5 4- 1994 (Aqueous) N N
NITROGEN, NITRITE �
SW-846 6:)AI V I.Aqucoin
EPIN 300.0, I:e?, 2 1, 1993 (Aqueous) hTlh.fC)Nlr �- �
SVd�48 9050 A; �q !¢ous) am
EPA 20C:71 Rea. 4.4 19144 (kuccus)
WITROGEN. ND - NO2 SbW446 6010C lAqucaus;
LPA 340.7. Rev, 2,11 103 (f.qucousI EPA- 2Uu:C;,. Reu: 54. 19 4 {.Aqueou3)
SW -BAG €956 A VvVuoo=i 5 V446 6020 B (Aqueous)
NITROGENt TOTAL KJELDAHL ARSENIC:.
Stu 4500 Vcrq 9-1997 t$10 45D0Wrf3 DY 1997) {Aqucou) EPA 200.31 Sao. 6,4 1094 (Aquaousl
DIL 8 GREASE S'Jh-84[Aqueous)
EPA I b64 I�fev- B (Aqu.ea usy EPA 200.8. Rev..5.4 1994(Aquecus)
Sw•&46 9011 6 (Non•Aq.leoLgy slh-mrl Eia2r,,rt (Acoo?cus)
PHOSPHORJS, 101'AL BAR, UV.
EPA 200.7, rinv 4 c.('%4) IAauenu9) EPA 200.7: Rev. r, 4, 1950A (Atjuaxl!'
W-84R Ort 10 D (Aqueous) SWAS48 "m I(I n (Ac I loo l•5)
�2ESIDUE, DI55:)-vFn mn c. EPA 200:8_ RtV, 5.4, 1.$94 (AtluBnusl
OM 2540 C-1997 0Iu1cl�ruw 1 SW6431020 0. i,4tauenusI
RESICIUE, 5;13PENDED I)ERYLLIUM
Sh42540 D-1997 (Aqueolrs) PA 2G0:3: Rsx S 1994 (Aqusrnas)
R6SIDLE. TOTALEPA
6020 D (Aqueousi
SPA 2540 8-IS97 (Aqueous) BORON
Thi* comiiieetor requtes.mq;niz r.Ld m-
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Gertifed Partxlet�rs LiSk rig
Summit E'Itia Dnrsnntoi I hJ=,c;Jor lez, Inc
J(1(Yress. ISM 'VQi i w:ttuct
t UY00fla F211,, CH 44223-
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CERTimm PARAI19ETERS
I:.r4. 2C70.6., RE!V, 54.., 1904 0queoiis)
!;%'V-84U 6U20 N fAquvcu"sj
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Fri
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obquemmC
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4.41 W4° t tFAqueaut:I
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tuen9sb
r'1-ii.O M,IUNi T0TA1_
UPA 200 ;. Rev,
4 4 1354 tAquecuy}
`W-841�. E'D 10 [11^�gC.
OJS i
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5-4 1994 (Aqu'suus
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4As upoj �)
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4:4. 1 �4 (AquF;MAO
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4�-Fllf1%i0D'Aqueo'ls
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L'J 646 6020 3 ,AGLSou51
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EPA 205.8+ R. 5 4, 19'S4 fAz;UC L21
ti P-9.413 6020 E (Aquea us.I
P�T�+SS1Uh.1
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Certified Parameters Listing
Lah Name: a gmit EngernnnnMil I TOeh:n0logiea, Irle
Address: S310 Wki 5trc;;t
Uuyahogz Fa 's, OH 44223-
Fhe chxva �am1d �dU9r91orr, �aaina t1411 met. 11'e reyurgnrt„vrls uI' ISA N£P.G 1'H uEp11- is narr�6g5erIJ!!3rd,I3r the'tlaasu+urFnr aY rrr-acr id=rs us-0eq t4dow.
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S-T RONT IUM -
EPA ZUU.7 ;?ill: z 4 "1941AqueptlS;l
SN16840m 609C DIAcue auE;
EPA 200.8, Rev_ 5-Z. 1 q94 (Aqueous)
SW,a40 6O 0 B IAquaous)
THALI IWO
FPA Irn7_ Reu. 4.4. 3SJ=+4 (AUU00us)
SW-846. 6010 r7 IAtjth3n(r5)
EPA 2V0, F Fiev 054. 1 W4, (Aqueaug)
St -4146 6020E IA[ju8rir5',r
TIN
EPA 2001-7 Rev 4 c '9u4 l..Aqueai,)
EW-846 6C1 J D 1Aquc0us
VANADIUM
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WV-846 6020 3 jAclucc;us
Z!Nv
EPA e00 t3, R:cv. So4. 1994 1AqucousI
SL'1-5A0 6020.8 (Agwt:cius)
ORGANIC
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AG5UR8AB_E UK(;ANIC .;ALIDES
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F3A.SFNELJTRAUACID Uig(;ANICS
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( HLORINMUDACID HFkI3IC4IDE5;
M-0408151 A jA:lrmsruti)
CHLORMATED r H E NOLIC S
EPA 1.553. Rev. A. 1997 FAiFutrnix}
E1iTRAC7AUL2 PETROLEUM HYDROCARB04NF
MADEP, PABY 2004 gm I Oaupaus)
NONHALOGMATU3 VOCA71Le I UIiU>1NPC5
SW-8466D'5C IAqueiU9;l
Cxrlifir ale
0�1
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1239J2017
1 ti9s41©
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EP q 600 ;Aqueous)
SVJ=8461MV L4 (Aqueous)
POLYCHLORINATED SIVHFNYI.S MC 3s)
EPA 6CB (AcIve0us)
5 u�-B46 5002A ((AaLuWUS)
d� U RC3FAFi _E- C RGAN ICS
1 PA 624 IAcIEwous)
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SVJ=80 9020 E {Aqueous) O
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Carl dfied Parameters 'I is#ing
Lai Name 5omrnit EmmanmentalTeehnalag es, Crc
u.ddress' 3310 Win Street "f
Cuphoga Fa1Ia, OH 44223- 7
Tno above named iab®rSfirl he4jjg duly me[ tfw mgknromergs at 75A 4ii 24.050C. 1=-heretycerirrrn J:Jr me measureinan, oflho pararn�r; is-ec berloo.
CERTIFIED PARAMETERS
INOR13ANdC S1LIW%
BCD EPA 2007. Rev.'. 4.4: '1994 fAqueaus)
SM 521D 8-2001 (AquacJus GIIV•04G 63`C D IAqueous)
CI ILD RI D E SULFATE
SIN-846 43515 A tAquecus) EPA WC.04 Rev 2 10 1993 (Aqueaus.}
CODSVVA84a 905.6A (Actrmt;:)
SM 5220 C-1 r797 (Aqueou9) SULFIDE
FLUORIDE SW440" 91}34IAquems)
EPA 300.0, Rev, 2.1. 1993 (Aquaoas) METAL
SW-84B 905E A fAgaeous) TCLP MIETA.S
INORGANIC PHEYJ S GW-646 '311 (Aqueous)
CPA 420.1, Rev. 1S78 faqueaust ALUMINUM
N'TROGEN, NITRATE CPA 20G-7 :Rev. 5 4. 99-g4 P,Aclumas)
EPA 300n, Rev 2-1, 1E93 (Aqueous; S1V-84fi [SDI© D CAjvekaus;)
SLV4A' 6 9056.A (Aqueaus) EPA ?DO -A, Ray. `S A 1994 (ACIreaus)
NITROGEN, Nil RITE Swt w a"0:20 B (A.quecus)
EPA XU.U; L®v.2.1, 1993 (Aqueous) ANTIMONY
SW846 905E A;Aqueoas) EPA 200.7, Rev. 4.4. 1904 fAqueoual
N TR6GEN NO3 + NO2 SW-846.6010 D (Aquecus)
EPA 300 0, Rev, 2.1 1993 ,Aqueous} EPA 200 8, Rcv. 5.4, 15 94 JAsfue ousj
SW-046 9056 A fAqueraiu=) SW*845 G020 B (Aqueous)
4IVZO'3EN1 7(77ALIWELDAHL ARSENJC
SAY 45W Norg 5-1597 (SM 4$00 N113 D-1997) iP.gaeousl EPA 2DO 7, Rev 4,4_ 199c L4quEous?
NL & GREASE SWV 946 601C U (Aqueous)
EPA 1Ei'34 Rev. 8 (Aqueous') EPA 200 JJ Rev, 5.4, 199A (Aqueous)
W0448 K71 9 (:Non Aquaaush Sw 846 6E20 B (A'queou=4)
RHOSPhtlRUS, TOTAL BARp1UM
EPA200.7, Rev 4,4 (193+4) (AcueUu5) EPA 200.7 Rev. 4.4, 1994 dkziimcus)
S4'+ 846 6010 DiAcu+truus) SW-4340543010D(Aqueaus)
F:ESIDUE, DISSOLVED i&7 C EPA 203 8, Rev .5 4- 1994 (4quecus)
SM 2540 CA Aqueous) SW-fW 6f120 6 (Aquiem'31
RESIDUE, SUSPENDED &ERVytlfijm
SN' 2W D l W 7 iAquealss} EPA 21[jD 8. Rov 5.4, 1994 (aqueous)
+2ESIGUE, I-OTAL bWAS46 tic;20 B {Aqueous).
SM 2540 9-19,37 (Aqueousl 30RON
;erti(idate NL'r1.
lfective Q?ate
ExpiraCioil Dare.
Data of Las' Amendment:
631
i J11241.6
12.+31 f201.6
11I4I2Di6
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Certified Parameters Listing
L, h I�INO) r:o. it�wrrutrEnvironwetiLax Te:hrmlrk3ies, Irc,
ddrG"_6: 3310. Win Stfeel-
CuyaNNja Fsl1!,e, M! 442-93-
The aGcve Ir mer. Iz Garatcry, rraumy uWy rnu t 4tG req lrrn F; m n tan Nt 5 �w 6 Cq, is IiereF.:y cBrif>e+.", for Vic rnmurarin, of 7x V,trarnet+°: Ils^ed txldn
CERTIFIED FARAMETERS
EFTA 2016, Rev. 54. 1 99d ,;Aquemjs) u'A-BDIG 001 D (Agst=s)
S°NwW; C5620 Lq (Agaeousl PMOh'E5W
CADMIUM EPA2M W. RMw..4 �: 1e94 (Aq:3rspusJ
EPA 9af3.7, Rev 4.4, 1954 f, 4gt esu ) .rvINDP8466a°0 D dAqueaus)
SIN ,B46 6010 D tAqueousI I'dlANGANLSE
EPA
200_9, Rsa. 5:4E 1944 wAquieo33s)
S'VV.-E96 5020 S (Aqueous)
CALCIUM
-PA 2007, flea'. 4.4. 1994 lAquenlir.)
SN-841E604C D Agmous)
t1FIR7h9IMA TOTAL
EPA 20,17 Rev 4.4, 1994 (Aqutaous)
S1rw 9466PJ10 D gAquecus)
EPA 1a t!. Rev. 5 4, 1994 (Aaucous)
s4'O484t. U020.B (Aqueous)
COBALT
EPA 200.7, Ray: 4A -1994 (Aque€r ts;+
Z%VVzd4G 6010 D r,Aqueujsj
EPA 200Z, Rev 5.4, 1994 ?Aqueous)
SW-€i4C 6'1320 H (.rjueous
COPPER.
EPA 200 , Rey 4,4t 1994 iAquecus)
St+Op 845 6U 10 to (Aquew3ass)
EPA 2U0.8, Rey- 6.4, 1994 {Aguecus)
M-846 6020 R (Aqueous)
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Nrrrth CarcJItna W.astewater/Groundwater Laboratory Certifintlooi
ertmea ParartleterrS Listing
I b N� rttm. SurrinYPt Enwrcinmeitd)i'1 e hnahgi.ss, Inc
ixclress. -131G NNin Street
Cuyahoga Fa1Is, 041 44223
Tie tanve narnPn I r: nr�te, y. hauing
utu
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N r;t 2H Q [A
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cart �u .ar it. msas are^ser d: 1 7t e pnram Int. iiSiM ialt
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wTRO(+JTIL3M
EPA
: '01-s46 6010 O
I;Amwuus;
EPA, 200.8., Rcv-
SA, 19,94
(Aqueous)
Sa'V4466-12C B
(Aquecus.1
THA`, ILIUM
EPA200.7, Rev.
A 4,1 9e4
dAtu*ous)
5W841515010 C1
(Aquer us)
PA 2001, Rev
5A, 15194
(Aqueous)
SW- 46 6020 B
(Acura Us)
F,N
EPA 200,7, Rov.
4 4. 1 ftom
{Aqueousl
S%W-846 t 010 H
(,AqueCis)
tANADI UM
Er'aA.200.B, Raw.
{. , 1C944i,Alamus)
+SWc846J 602O E
(A.Inron .s ,
ZINC
FPA ZCG.8:," Rev.
64. 14.44
(Aqueous
SW4 846 6020 B
(Agrac,&aLis
OR0ANIG
�R�Av1Cs
S'a1 846t311 (AcueaLs}
AIDSOIRBA€3I ORCIANIC HAJIDES
EPA 1650, Rev, C 1497 (Aqueous)
6,ASE NEUTR ALeAmn, 0R-tc AN1C5
i*PA 625(Aquaous)
.Sat'' "-6a6 8270 G t 4quo.D.w8i
OHLORMATED ACID HERBICIDES
SVI-84£ 815' A (Aqueous,
GHLORINAT D PHENOLICS
EPA 1653, Rev, A 190 (Aque[ausy
ExmACTABLE PETROLELJtt I- YDROCARRONS
MADER May 2004, Raw e i aAQueo.Lmy
NONHALOGENATFD +l"3t_AT'I.E, ORGANIC$
SW-5468CJ15 C 4Aquewssil
RE
�TICIDES, ORGANCt_FILtORINE
=F A BDF (A lapous)
3u�rR945 1 1',x (AgUGous)
PClLYCi• LOPINATED BIPHENYLS 4PCBe
EPA 608 Aqucour;
-64a 8082A fAqueo s)
PLl: GLABLE, ORGANICS
kP�1624 4Aqueous)
Tr TAL ORGANIC HALIDES
S1 r,.846 510OX F (A.quoous)
TPH MESELRAd E ORGANICS
S4"3-846 8015 G (+M1qutsou_)
TIa1I �GASCLINEPANCE OROAN'ICS
S1nJ- 80115C:"f+4quems)
Vw LrATILE PETROLE)UMHYDROCARBONS
h Fi DER Mays 2ai:A, Rev 1,1 (ArxmFsus)
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IJate of Last Amen��meni-
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Febnlary 7, 2d17
ti31
fAs. Meegan Dougherty
5urnmit Environmental Technologies, Inc.
M 0 Win Street
Cuyahoga Falls, OH 44223
RilY L (.?t-trjr &P
1gIlII(.I% ti, lt1'kI;
Subje,�t NC y"iN1((G4V LG S xty-Day Paramt�ter Method Dacertiticativn Recomrrtartdatittn�
Zinc � EPA 200,7 and SWmU46 6010 D
17ear f�is. ❑cucherty:
The rerri$diai Proficiency `Testing (PT} resultisj far the kielcwI}ammeter Mi�thad(sj reported by your
laboratory far the North Carolina Wastewater! Groundwawer Laboratory Certification (NC VArWGW LCII
performance evaluation wastwere unacceptable and a sixtj:day parameter method decertification will be
recornmendea. The results reported and the true values as they appear in our records are as folicews:
Sfudy
t fi-3B
'A written C
Parameter C��ethcld
EPA 2�70.7i
SVtf�d4U UU.10 U
EPA 20U)
SWI 846 6010 D
Un1#s:
WAIL
Reported Tnsr; �1ccEptar��ce 'performance
Vatlie value Rarge _
600 495 421-569 I NQt AwWable
(till_ I ta6d7
for each unacceptable result
i40+J � 119(}-1610
be
iVot Acceptable
This is to no#ity yrou that the Laboratory �ottification branch of the North Carolina Division of Water
Rascurces, Water SC°ences Seetibn, is considering rewOri7rTlendirlg 7 petame4,r methadfsj
decertification to the Environmental Program Supervisor_ The recommendation. concerns the at:40ve
mentioned v4ationes}, This is not a decertification, it Is a notification of our intent to consider
decertification. You will be informed in a separate communication if decertification is Issued.
Con:aot me immediately at (919) 733-39t78 ext 251 if your records do not agree. with our, or if you have
fives#IQ.'15
S�ncorely,
ZI f
Todd Crawford
Technical Assistance & Compliance Specialist
NC VuVROW Laboratory Certification Brant
flttd�hmer,t
ec_ Cana Saitervrhite, .laso-r, 8n �illl, rvtosler irtle #(i31
411atEr Scierlc� SCG11011
NC Waslewater,IGrw,ncwat�r L�6urattity Ge•�ificailarl eranclt
'F+l;I il 5$r:-:� Ct!r,lec �a��1ah, hu!1i'• i;a•ol �� t76��-�n29
t:gwtlur!'1�7�•5?'?ze+tj;:r�rkEs:.itd,t�ti!e��'! hJ-rh.;,alryln9zie!1?
Fnctle' 9 `4-7IJ-3 Ll;l'. FA s 914-TTI-g2d i
!i•Irme! I_L4.tL�44e._y,,nc.;✓,r�ebaalfdiy�i5?o'nshWte[-ttlOdfcEsN�aher-fY64,l,CBS=dataPMa�gr.3�'BPILA6.11oIn.ig9741hOrafPN-cCr1irJt.n-brrtt
Page 10 of 16
Page 44 of 50

rr. 1 11 1 I I I I
February i, 2[}17
ti31
dvls Meegan Clougherty
Summ;t Environmental Technologies, Inc.
3310 Win Street
;uyahoga Fails, 4H 44223
ldta5" t car_ll r.:=
ti91C'1tt:Al. f.• f�LCir�1
Sttbject, NG WV'11'/G'�N �G Sixry•O�y Parameter Method Q�eceltifieation Recammendation�
Selenium — EPA 2011.7 and SW-646 6010 Q
Clear 11As_ C1�arlgher#y.
Thp remedial Proficiency Testing f?T) resuit(s} for the beharn� Parairneter Mathadi;s) reported by your
laboratory for the North Carolina Wastewateri Groundwater Laboratory Cerigication (NC WvvIGW LC)
performance evaluation wlvaslwere unacceptable and a sixty-day tarameter method decertificat on will be
recommended, The results reported and the true values as they appear in our records are as follows:
Study Parameter P1{etYidii t1n'its
thfl'i6M3B
a97iJ1��1
vrritlen
EPA 200.1!
EPA zaa.7!
S'J6r-$40 �it7�0 _D_
re Action Repoli (CM
Reported True ACCeptaaee 'Perf.;,rmanee
v;atue Vatue R.ar. a
sea 442 376-50e Not Acceptable
4701
t�9�rL
eac
h unacceptable result v
3a3 � 32i3-odd
to reissuing
Not >a,rceptable
This is io notify' you that the Laboratory Cortiflcation Branch o
f the North Carolina Givisian of UVati�r
Resources, Water Sciences SeCtitSn, 1$ considering recorninending a parameter rnetrodlIsI
decertification to the Environmental Precgram Supervisor, Thu reckmmendatinn concerns the above
mentioned vlolation(s). This is not a decertification, it is a cation of our intent to c4ttis dor
ducurtiftcation. You will be informed in a separate communication if decertification is issued.
Contact me immediately at (919) 733v39008 ext• 251
questions•
filttgl:ill 114:11!
cc'. Cana Sattcrvrrile, ,leson Smittl, Mastel Pile: JLf33'�
if your records do not agree with ours or ,:f you have
�incerely�,
Todd Crawford
Technical Assistance & Cvmplianc�: �cecialist
hC WV+IrGW LaULYatory C=itificaticn Branch
1V'ater �lentns Sk[uwn
►fC WaMvMOriGmundwbierLataara;glk Certltibtiun 9talech
1e)11.kkA,3il Laivi:�t'wdei• PaL;e!ah, N:.nh%�mli� 27CFr_.tc3e3
Lr�r:�+pr,r btu Reedy t>r�tt. Raad,.:�kllFjh; Nr;rili rar�ma
FhrrnE �79 r39.3�t]$1�P:{�4"4.r3ry ii241
Inlcrnal hlin:tt,lnalwatoK rocaurcegtwytcr•rosourteidlahratenstlepCes•fronle-ua4gii8potnt{ertificali4n•lar3nCh
Page 11 of 16
Page 45 of 50

February /, 2017
a31
As. Meegan Dougherty
i(Mmit Environmental Technologies, Inc.
3310 Win Street
Cuyah•:ga Falls, OFF 44223
CODPEV
�•t14'liE;lL 1 Iti''tr;lry
Subject: N� VVV"J/GVV t.� Sixty -Day Porarr:eter Metnad Decertillca#ian Recommendation:
Nickel •- EPA 200.7 and SVV-848 6010 D
Dear Iv9s• Doughe�iy•
The remedial fsr•oficitincy Yes#ing (PT;i resulti:s) for the below Parameter 141ethcd(s; repr~rte�1 byl your
laboratory for the North Carolina Wastrrvrateri Groundwater Laboratory Certification (NC VJV'J1GW LC)
performance evaluation vras1were unacceptable and a sixty-daV p aramete� method decertification will be
recommended• The results reported and the true values as they appear in our records are as follows:
8iudy
Paran�ete� Fulelhcsd I lJnits
Val�4
;T SW-t346 6�11 G 0 N91L 1 �'+56 9 t 8
0920i601 EPA 200 7) Wg1L 1620 1360
S'AL846 6010 ©- ura---
'� :tten Cvrraairtii� i+riitsn Report (CAR) Pur each un ceatatite result Will ba regL.
.4ccۥptance
_. F�anCe
$05-1 a3rJ
Performance
Not Acceptable
9200-1a2o �lot,.ptable
prig+ to reissu n9 ceriir�211en
�ec+r
Yhis is to notify You that the Latsora;ory• Certification Bran+rh of the North Carolina Division of Water
Rcsce�rces, Water Scsences aecl'ion, III& ndiny a parameter rr1Pthctdfs)
riecertlfication to the Environmental Program supervisor. The rac;,rnmend ation concerns the above
n-lenticned vioiation(s). This is not a decertification; it is a notification of our intent to consider
decertification. You will be informed in a separate communication if decertification is issued.
Contact me immediately at t;919j 733-3908 ext, 251 if your records do not agree with ours or ,f you have
questions.
incerely
f
Tt�dd Crawford
Technical assistance & Compliance Specialist
NC WINfG'JV Laboratory CArtification Branch
!'dt�chment
^C. fJana 5alter��hile; Jason Smifh, Master �ele #�r:i1
water Srierces SecEID+I
1''JS:;L�.•1 h.•'G :�'a,val.=rE.attdra!�ry Deli I .,_di�_�r 3r3t1alF
L::_.:1. .. ,.
`Un.- J. �..lill f:'.I fWj IsA I.. ,.�I_i iIT, II I SQUFCeSjQ 4ldtwacer-scs•ilmne-aa2C,7�kOr8tn f�' ,"1lrlGAldan ra arh
Page 12 of 16
Page 46 of 50

MRICH AM
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Page 13 of 16
Page 47 of 50

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SUMMIT
ENVIRONMENTALTa_GftHOLOGMS, ING
ArratyticaI La_boratorle
September 11, 2019
Melvin Goad
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: (336) 99M450
RE: Dunn, NC WTP
Dear Melvin Goad:
SummitEnt�ironmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL [phone] FAX.[phone]
Website: hQ.*1Aviviv.settek.com
Order No.: 19081720
Summit Environmental Technologies, Inc. received 1 sample(s) on 8/22/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
g Project Manaer
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-0H-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New Yorle 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon 0 00001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T10470446641-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 33

Summit Evironmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TcCHNOLOG] zS,R C Cuyahoga Falls, Ohio44223
Arupffy0cal LaboralorMe TEL: [phone] FAX: [phone]
Website: hLtjz://wwiv.settek.com
CLIENT: Synagro
Project: Dunn, NC WTP
Case Narrative
WO#: 19081720
Date: 9/1112019
WorkOrder Narrative:
19081720: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
For use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19081720-OOIA TCLP-SVOC_8270E: Possible low bias for Pyridine due to low recovery in the LCS.
19081720-OOIA TCLP-svoc-herb_TCLP(8151): The CCV exhibits high recoveries for 2,4-1). All
reported samples are ND for 2,4-D.
Original
Page 2 of 33

IS U M I Summit Environmental Technologies, In
3310 Win S
EP4VIROMrdlENTALTE-CHNOLQGi -B, 1Nrs Cuyahoga Falls, Ohio 442�
Anaf 0cal Laburalones TEL: [phone] FAX: [phone]
Website: http://`viviv.seUek.co.
Qualifiers and Acronyms
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
WO#: 19081720
Date: 9/11/2019
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/M[B+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC./+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL./+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV./+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
)CS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
)UP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
MC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 33

SUMMIT
ENVIRONMENTAL itCHPJOLGQIr!3, 9RC
Anatytical Labcralarj@s
CLIENT: Synagro
Project: Dunn, NC WTP
Lab SampleID Client Sample ID
19081720-001 Dunn, NC WTP
Em Summit ptronmental Technologies, Inc.
3310 Win St,
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: hQ://iviviv.settek.coni
Tag No Date Collected
8/21/2019 111500 AM
Workorder
Sample Summary
WO#: 19081720
II-Sep-19
Date Received Matrix
8/22/201910:20:00 AM Sludge
Page 4 of 33

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IT
Summit Environmental Technologies, Inc. Analytical Repo
SUMM3310 Win St.
ENWIFt0t4 ENTAL TECnNoLwu;s, Ne Cuyahoga Falls, Ohio 44223 (base report)
,A,nalyG`cat taboratdrip� TEL: [phone] FAX: [phone] Wo#: 19081720
Website: hgp://www.settek.com Date Reported: 9/11/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/21/2019 11:15:00 AM
Lab ID: 19081720-001A
Project: Dunn, NC WTP
Client Sample ID Dunn, NC WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury ND 0.00200 mg/L 1 8/26/2019 3:55:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 8/26/2019 5:59:26 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 8/26/2019 5:59:26 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 8/26/2019 5:59:26 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 8/26/2019 5:59:26 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 8/26/2019 5:59:26 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 8/26/2019 5:59:26 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 8/26/2019 5:59:26 PM
FLASHPOINT DETERMINATION (1010) SW1010 Analyst: TAH
Flashpoint (140°F) >140 °F 1 8/30/2019 12:31:30 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270 SW3510C Analyst: MES
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 8/28/2019 7:28:00 PM
2,4,5-Tr1chlorophenol ND 0.500 mg/L 2 8/28/2019 7:28:00 PM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 8/28/2019 7:28:00 PM
2,4-Dinitrotoluene ND 0.100 mg/L 2 8/28/2019 7:28:00 PM
Cresols, Total ND 10.0 mg/L 2 8/28/2019 7:28:00 PM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 8/28/2019 7:28:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 8/28/2019 7:28:00 PM
Hexachloroethane ND 0.200 mg/L 2 8/28/2019 7:28:00 PM
Nitrobenzene ND 0.200 mg/L 2 8/28/2019 7:28:00 PM
Pentachlorophenol ND 0.500 mg/L 2 8/28/2019 7:28:00 PM
Pyridine ND 0.500 QL- mg/L 2 8/28/2019 7:28:00 PM
Surr: 2-Fluorophenol 39.0 10 -109 m %Rec 2 8/28/2019 7:28:00 PM
Surr: Phenol-d6 43.2 10 - 109 %Rec 2 8/28/2019 7:28:00 PM
Surr: Nitrobenzene-d5 30.7 19 - 120 %Rec 2 8/28/2019 7:28:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal < MDL
Page 6 of 33

IT........ 17
it Evironmental Technologies, v,c. Analytical Report
SUMM3310 Win St.
ENVIRONMENTAL MCHNOI-n ,rc.s, lNr, Cuyahoga Falls, Ohio 44223 (base report)
AnafyriC7/_3borafanei. TEL: [phone] FAX..- [phone] WO#: 19081720
Website: http://ivlt�ui.settek.com Date Reported: 9/11/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/21/2019 11:15:00 AM
Lab ID: 19081720-001A
Project: Dunn, NC WTP
Client Sample ID Dunn, NC WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270 SW3510C Analyst: MES
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: 2,4,6-Tribromophenol 47.3 10 - 120 %Rec 2 8/28/2019 7:28:00 PM
Surr: 2-Fluorobiphenyl 42.1 22 - 117 %Rec 2 8/28/2019 7:28:00 PM
Surr: p-Terphenyl-d14 56.3 34 - 116 %Rec 2 8/28/2019 7:28:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND 0,0250 mg/L 10 8/28/2019 9:17:00 AM
Toxaphene ND 0,0500 mg/L 10 8/28/2019 9:17:00 AM
Endrin ND 0,00500 mg/L 10 8/28/2019 9:17:00 AM
gamma-BHC ND 0.00500 mg/L 10 8/28/2019 9:17:00 AM
Heptachlor ND 0.00500 mg/L 10 8/28/2019 9:17:00 AM
Heptachlor epoxide ND 0.00500 mg/L 10 8/28/2019 9:17:00 AM
Methoxychlor ND 0.00500 d mg/L 10 8/28/2019 9:17:00 AM
Surr: TCMX 71.7 10 - 119 %Rec 10 8/28/2019 9:17:00 AM
Surr: DCB 75.9 10 - 119 %Rec 10 8/28/2019 9:17:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: MES
TCLP HERBICIDES ANALYSIS (SW1311/8151)-SOLID
2,4-D ND 0.0100 QC+ mg/L 1 8/30/2019 5:28:00 PM
2A5-TP ND 0,00500 mg/L 1 8/30/2019 5:28:00 PM
Surr: DCAA 94.6 20 - 140 m %Rec 1 8/30/2019 5:28:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260 Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.125
mg/L
25
8/26/2019
3:04:00
PM
1,2-Dichloroethane
ND
0.125
mg/L
25
8/26/2019
3:04:00
PM
MEK
ND
2,50
mg/L
25
8/26/2019
3:04:00
PM
Benzene
ND
0.125
mg/L
25
8/26/2019
3:04:00
PM
Carbon tetrachloride
ND
0.125
mg/L
25
8/26/2019
3:04:00
PM
Chlorobenzene
ND
1.25
mg/L
25
8/26/2019
3:04:00
PM
Chloroform
ND
0.125
mg/L
25
8/26/2019
3:04:00
PM
Tetrachloroethene
ND
0.125
mg/L
25
8/26/2019
3:04:00
PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal < MDL
Page 7 of 33

,mr SunmzitEnwonmentalTechnologies,btc. Analytical Report
summ3310 Win St,
ENVIROtd A5WAL ECsinlOW GI;5,' 0 Cuyahoga Falls, Ohio 44223 (base report)
Arraly0cal Laboratari2c TEL: [phone] FAX.• [phone] WO#: 19081720
Website: htto:11Wwu?.settek.co7t Date Reported: 9/11/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/21/2019 11:15:00 AM
Lab ID: 19081720-OOIA
Project: Dunn, NC WTP
Client Sample ID Dunn, NC WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260 Analyst: CTB
TCLP VOLATILES ANALYSIS
Trichloroethene ND 0,125 mg/L 25 8/26/2019 3:04:00 PM
Vinyl chloride ND 0,0500 mg/L 25 8/26/2019 3:04:00 PM
Surr: 4-Bromofluorobenzene 89.4 70 - 130 %Rec 25 8/26/2019 3:04:00 PM
Surr: Dibromofluoromethane 88.1 70 - 130 %Rec 25 8/26/2019 3:04:00 PM
Surr: Toluene-d8 94.9 70 - 130 %Rec 25 8/26/2019 3:04:00 PM
RCI-SOLID-W/IGNITABILITY1030 SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.481 mg/Kg 1 8/27/2019 5:11:00 PM
RCI-SOLID-W/IGNITAOil ITY1030 SW9045D Analyst: DHC
PH (SW9045D)
pH 7.3 s.u.@19.5C 1 9/6/2019 10:53:00 AM
RCI-S0LID-W/IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 8/27/2019 5:11:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for prepazation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal < MDL
Page 8 of 33

Summit Environmental Technologies, Inc. Accreditation Program
SUMMIT 3310 Win St. Anal teS Report
EW111OWNIEUTAL TECHNOOGLFS, INC Cuyahoga Falls, Ohio 44223 1 p
Arralytical Laboratorlag TEL: [phone] FAX.* [phone] WO#: 19081720
Website: http./lAviviv.settek.com 114ep49
Client: Synagro State: NW
Project: Dunn, NC WTP Program Name: NC WW_SCM
Sample ID Matrix Test Name Analyte Status
1908172M01A Sludge Flashpoint Determination (1010) Flashpoint (140'F) A
Sludge pH (SW9045D) Hydrogen Ion (pH) A
Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U
Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Sludge TCLP Herbicides Analysis (SW1311/8151)-solid 2,4,5-TP A
Sludge TCLP Herbicides Analysis (SW1311/8151)-solid 2,4-D A
Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A
Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis (SW1311/6010) Barium A
Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis (SW1311/6010) Chromium A
Sludge TCLP Metals Analysis (SW1311/6010) Lead A
Sludge TCLP Metals Analysis (SW1311/6010) Selenium A
Sludge TCLP Metals Analysis (SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A
Sludge TCLP Pesticides Analysis (SW131118081) Endrin A
Sludge TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original #1
Page 9 of 33

l' � Summit Environmental Technologies Inc.
nsul"3310 Win St.
ENVInOUPd5NTAL TrCHNOL6r1r5, INC Cuyahoga Falls, Ohio 44223
,Anaflrtical Laboratorlos TEL: [phone] FAX.- [phone] Website: ham:11inviv.settek.com 114ep49
WO#: 19081720
Accreditation Program
Analytes Report
Client: ynagro State: NW
Project: Dunn, NC WTP Program Name: NC WW SCM
Sample ID Matrix Test Name Analyte Status
19081720-OOIA Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge
TCLP
Volatiles
Analysis
Sludge TCLP VolatIles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
NC WW SCM A Accredited NC WW SCM U Unavailable
Page 10 of 33
12-13ichloroethane
,
2-Butanone
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
A
A
A
A
A
A
A
A
A
Original # 1
NC WW SCM A Accredited NC WW SCM U Unavailable
Page 10 of 33
12-13ichloroethane
,
2-Butanone
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
A
A
A
A
A
A
A
A
A
Original # 1

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
M 1 3310 Win St.
ENVIROMME14TAL TECHNOLQGIES, NNC% Cuyahoga Falls, Ohio 44223
Anafy ticaf Laboralarim TEL: [phone] FAX.N [phone] WO#: 19081720
Website: http:Ilivivw.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39062
Sample ID MD-39062
SampType: MBLK
TestCode:
tclp-svoc-her
Units: Mg/L.
Prep Date: 8/22/2019
RunNo: 102772
Client ID: PBS
Batch ID: 39062
TestNo:
SW8151A
SW8151A
Analysis Date: 8/30/2019
SegNo: 2315678
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 0.000100 0 0
20
dQC+
Sample ID LCS-39062
SampType: LCS
TestCode:
tclp-svoc-her
Units: mg/L
Prep Date: 8/22/2019
RunNo: 102772
Client ID: LCSS
Batch ID: 39062
TestNo:
SW8151A
SW8151A
Analysis Date: 8/30/2019
SegNo: 2315679
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
224-D
0.00480 0.000100
0.00500
0 95.9
43.8
130
QC+
Sample ID LCSD-39062
SampType: LCSD
TestCode:
tclp-svoc-her
Units: mg/L
Prep Date: 8/22/2019
RunNo: 102772
Client ID: LCSS02
Batch ID: 39062
TestNo:
SW8151A
SW8151A
Analysis Date: 8/301201
9
SegNo: 2315680
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit
RPD Ref Val
%RPD RPDLimit Qual
214-D
0.00526 0.000100
0.00500
0 105
43.8
130 0.00480
9.15 30 QC+
2,4,5-TP
0.00478 0.0000500
0.00500
0 95.7
51.5
130 0.00450
6.14 30
Surr: DCAA
6.62
5.000
132
34.2
150
0
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or anal}
Original

U! 'T Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
EP,4%llrtON?iIE14TALTEC!INDL-QC.IFS.INC Cuyahoga Falls, Ohio44223 WO#: 19081720
ArraVilca.P Laboraionet` TEL: [phone] FAX..- [phone]
Website: htW://wwim.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39079
Sample ID MB-39079
SampType:
MBLK
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 8/26/2019
RunNo: 102459
Client ID: PBS
Batch ID:
39079
TestNo:
SW7470A SW7470A
Analysis Date: 8/26/2019
SegNo: 2300106
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
fCLP Mercury
ND 0.00200
Sample ID LCS-39079
SampType: LCS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 8/26/2019
RunNo: 102459
Client ID: LCSS
Batch ID: 39079
TestNo:
SW7470A SW7470A
Analysis Date: 8/26/2019
SegNo: 2300107
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit
RPD Ref Val
%RPD RPDLimit Qual
fCLP Mercury
0.00399 0.00200 0.00400
0 99.8
80 120
Sample ID 19081708-001AMS
SampType: MS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 8/26/2019
RunNo: 102459
Client ID: BatchQC
Batch ID: 39079
TestNo:
SW7470A SW7470A
Analysis Date: 8/26/2019
SegNo: 2300121
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1-CLP Mercury
0.00439 0.00200 0.00400
Sample ID
19081708-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
39079
Analyte Result
TCLP Mercury
0 110 75 125
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
Prep
Date:
8/26/2019
Analysis
Date:
8/26/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 102459
SegNo: 2300122
%RPD RPDLimit Qual
0.00421 0.00200 0.00400 0 105 75 125 0.00439 4.19 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
Value above
E quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 12 of 33
lding
H Hotimes for prepazation or anal;
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
UM
J 1 3310 Win St.
Ell` lP0NMEt4TAL FMiN0[-C G1: z$, INC Cuyahoga Falls, Ohio 44223 WO#: 19081720
ArraVii:c2l Laboratories TEL: [phone] FAX.P [phone]
Website: http:Ilivwiv.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
Sample ID
19081708-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
39079
Analyte
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PC)L SPK value SPK Ref Val
BatchID: 39079
Prep Date: 8/26/2019
Analysis Date: 8/26/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 102459
SegNo: 2300122
%RPD RPDLimit Qual
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal}
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 13 of 33

'1 SummitEnvironmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
EfIVIROtJtA>=NTAL'TECt161€)LCFG4LFS, 7N Cuyahoga Falls, Ohio 44223
4ntytFcaJ ibc�ratorJe� TEL: [phone] FAX. [phone] WO#: 19081720
Website: httn:lliviviv.settek.com 11-Sep-19
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39081
Sample ID MB-39081
SampType: MBLK
TestCode:
Mtl-TCLP-7(6
Units: mg/L
Prep Date: 8/26/2019
RunNo: 102434
Client ID: PBS
Batch ID: 39081
TestNo:
SW6010D
SW3010A
Analysis Date: 812612019
SegNo: 2299147
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
ND
0.500
TCLP
Barium(Ba)
ND
5.00
TCLP
Cadmium(Cd)
ND
0,100
TCLP
Chromium(Cr)
ND
0.200
TCLP
Lead(Pb)
ND
0,500
TCLP
Selenium(Se)
ND
0.0500
TCLP
Silver(Ag)
ND
0,500
Sample ID LCS-39081
SampType: LCS
TestCode:
Mtl-TCLP-7(6 Units: mg/L
Prep Date: 8/26/2019
RunNo: 102434
Client ID: LCSS
Batch ID: 39081
TestNo:
SW6010D SW3010A
Analysis Date: 8/26/2019
SegNo: 2299148
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
1.94
0.500
2.000
0
96.8
80
120
TCLP
Banum(Ba)
ND
5,00
2,000
0
102
80
120
TCLP
Cadmium(Cd)
1,84
0.100
2.000
0
92.0
80
120
TCLP
Chromium(Cr)
2.04
0.200
2,000
0
102
80
120
TCLP
Lead(Pb)
2.07
0,500
2.000
0
103
80
120
TCLP
Selenium(Se)
2,01
0.0500
2,000
0
101
80
120
TCLP
Silver(Ag)
2,15
0,500
2,000
0
107
80
120
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal}
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 14 of 33

U'Nt Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVIRONMENTAL TECHNIC LQGIEFS,INC Cuyahoga Falls, Ohio44223
ywfyUcat L7bcrralarias TEL: [phone] FAX.- [phone] WO#: 19081720
.
Website: http://wrvw.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39081
Sample ID 19081723-001AMS
Samp, ype: MS
TestCode:
MtI-1CLP-7(6
Units: Mg/L.
Prep Date: 8/26/2019
RunNo: 102434
Client ID: BatchQC
Batch ID: 39081
TestNo:
SW6010D
SW3010A
Analysis Date: 8/26/2019
SegNo: 2300646
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
2.33
0.500
2000.
0
117
70
130
TCLP
Barium(Ba)
ND
5,00
2,000
0,3035
104
70
130
TCLP
Cadmium(Cd)
2.00
0.100
2,000
0,001857
99.8
70
130
TCLP
Chromium(Cr)
2.14
0.200
2,000
0
107
70
130
TCLP
Lead(Pb)
2.17
0,500
2,000
0
109
70
130
TCLP
Selenium(Se)
2.41
0.0500
2,000
0
121
70
130
TCLP
Silver(Ag)
2,34
0,500
2.000
0
117
70
130
Sample ID 19081723-001AMSD
SampType: MSD
TestCode:
Mtl-TCLP-7(6
Units: mg/L
Prep Date: 8/26/2019
RunNo: 102434
Client ID: BatchQC
Batch ID: 39081
TestNo:
SW6010D
SW3010A
Analysis Date: 8/26/2019
SegNo: 2300647
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP
Arsenic(As)
2.32
0.500
2.000
0
116
70
130
2.332
0.309
20
TCLP
Barium(Ba)
ND
5.00
2.000
0,3035
103
70
130
0
0
20
TCLP
Cadmium(Cd)
1,99
0.100
2.000
0.001857
99.6
70
130
1.997
0.211
20
TCLP
Chromium(Cr)
2,12
0,200
2.000
0
106
70
130
2.140
1.13
20
TCLP
Lead(Pb)
2.17
0.500
2.000
0
109
70
130
2,173
0,0705
20
TCLP
Selenium(Se)
2.42
0.0500
2.000
0
121
70
130
2,412
0,414
20
TCLP
Silver(Ag)
2,32
0,500
2.000
0
116
70
130
2.341
0.834
20
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E
Value above quantitation range
H
Holding times for prepazation or anah
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
P
Second column confirmation exceeds
PL
Permit Limit
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 15 of 33

' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
PEA VIRONMEWALnCHNOWgJZZ; INC Czryahoga Falls, Ohio 44223 WO#: 19081720
Anatytfcal Lalsnratorlo TEL: [phone] FAX.- [phone]
Website: htW://wivw.settek.com 11-Sep49
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39118
Sample ID MB-39118
SampType: MBLK
TestCode:
TCLP-SVOC- Units: mg/L
Prep Date: 8/26/2019
RunNo: 102542
Client ID: PBS
Batch ID: 39118
TestNo:
SW8081 SW3510C
Analysis Date: 8/27/2019
SegNo: 2303594
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Chlordane, total
ND
0.00250
Toxaphene
ND
0,00500
Endrin
ND
0.000500
d
gamma-BHC
ND
0.000500
d
Heptachlor
ND
0.000500
d
Heptachlor epoxide
ND
0,000500
d
Methoxychlor
ND
0,000500
d
Surr: TCMX
4,39
20.00 21.9 10 119
Surr: DCB
8,97
20.00 44.8 10 119
Sample ID LCS-39118
SampType: LCS
TestCode:
TCLP-SVOC- Units: mg/L
Prep Date: 8/26/2019
RunNo: 102542
Client ID: LCSS
Batch ID: 39118
TestNo:
SW8081 SW3510C
Analysis Date: 8/281201
9
SegNo: 2303595
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit
RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00710
0.000500
0.0100
0
71.0
20
216
gamma-BHC
0.00609
0.000500
0.0100
0
60.9
20
197
Heptachlor
0,00619
0,000500
0.0100
0
61.9
20
200
Heptachlor epoxide
0,00610
0.000500
0.0100
0
61.0
20
200
Methoxychlor
0,0108
0,000500
0.0100
0
108
20
227
Surr: TCMX
8.74
20.00
43.7
20
143
Surr: DCB
11.6
20.00
58.0
20
151
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding tunes for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 16 of 33

U' T Summit Environmental Technologies, Inc. 3310 Win St, QC SUMMARY REPORT
EhVIfSONFAENTALTECHNOLQGIES,IWCuyahoga Falls, Ohio44223 WO#: 19081720
+� My,itfcal Laboralorl'as TEL: [phone] FAX.- [phone]
Website: httR://wiviv.settek.com 114ep-19
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39118
Sample ID 19081461-002ams
Samp, ype: MS
TestCode:
TCLP-SVOC- Units: Mg/L.
Prep Date: 8/26/2019
RunNo: 102542
Client ID: BatchQC
Batch ID: 39118
TestNo:
SW8081 SW3510C
Analysis Date: 8/28/2019
SegNo: 2303596
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00978
0.00500
0.0100
0
97.8
10
224
gamma-BHC
0,00908
0.00500
0,0100
0
90.8
10
192
Heptachlor
0.00977
0,00500
0,0100
0
97.7
10
197
Heptachlor epoxide
0.00848
0.00500
0,0100
0
84.8
10
208
Methoxychlor
0.0187
0,00500
0,0100
0
187
10
251
Surr: TCMX
11 A
20.00
57.0
10
157
Surr: DCB
12.8
20,00
64.2
10
194
Sample ID 19081461-002AMSD
SampType: MSD
TestCode:
TCLP-SVOC- Units: mg/L
Prep Date: 8/26/2019
RunNo: 102542
Client ID: BatchQC
Batch ID: 39118
TestNo:
SW8081 SW3510C
Analysis Date: 8/28/2019
SegNo: 2303597
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00918
0.00500
0.0100
0
91.8
10
224
0.00978
6.34
30
gamma-BHC
0.00841
0.00500
0.0100
0
84A
10
192
0.00908
7.58
30
Heptachlor
0.00917
0.00500
0,0100
0
91.7
10
197
0.00977
6.30
30
Heptachlor epoxide
0.00769
0,00500
0,0100
0
76.9
10
208
0.00848
9,77
30
Methoxychlor
0.0207
0,00500
0,0100
0
207
10
251
0,0187
10.1
30
Surr: TCMX
11.0
20,00
55A
10
157
0
Surr: DCB
13.2
20.00
66A
10
194
0
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal
7
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 17 of 33

MJ I MF Summit Environmental Technologies, Inc.
as U3310 Win St,
ENVI41ONP4EhITALTECHNf]L.GGI,.cS,INC Cuyahoga Falls, Ohio44223
AnaiyffaaP __,J fWarorJOS TEL: [phone] FAX: [phone]
Website: hto2://www.settek.com
Client: Synagro
Project: Dunn, NC WTP
Sample ID
MB-39131
SampType:
MBLK
TestCode:
TCLP-SVOC_
Units:
mg/L
Client ID:
PBS
Batch ID:
39131
TestNo:
SW8270
SW3510C
Analyte Result PQL SPK value SPK Ref Val
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.402
Surr: Phenol-d6
0.437
Surr: Nitrobenzene-d5
0.385
Sum 2,4,6-Tribromophenol
0.510
Surr: 2-171uorobiphenyl
0.482
Surr: p-Terphenykd14
0.596
CIZK►�i�1 i1%I: � ► � � �J �� ■
WO#: 19081720
II-Sep-l9
BatchID: 39131
Prep Date: 8/28/2019
Analysis Date: 8/28/2019
%REC LowLimit HighLimit RPD Ref Val
1.000
40.2
10
109
1.000
43.7
10
109
1.000
38.5
19
120
1.000
51.0
10
120
1.000
48.2
22
117
1.000
59.6
34
116
RunNo: 102576
SegNo: 2327666
%RPD RPDLimit Qual
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for prepazation or anal}
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 18 of 33

�' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
£ta4�lfi?C�NM1N71�LSE�HNULtG1a �F7C Cuyahoga Falls, Ohio44223
WO#: 19081720
Analyt/ca/ i:rbr3rafoxies TEL: [phone] FAX:[phone]
Website: httR:/hviviv.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
SatchID: 39131
Sample ID
LCS-39131
SampType:
LCS
TestCode:
TCLP-SVOC_
Units:
mg/L
Prep
Date:
8/28/2019
Client ID:
LCSS
Batch ID:
39131
TestNo:
SW8270
SW3510C
Analysis
Date:
8/281201
9
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
1,4-Dichlorobenzene
0.428
0.100
0.8000
0
53.5
19.1
126
2,4,5-Trichlorophenol
0,579
0.250
0,8000
0
72A
11.7
151
2,4,6-Trichlorophenol
0.569
0,250
0.8000
0
71
A
12.4
150
2,4-Dinitrotoluene
0.682
0,0500
0,8000
0
85.2
20.6
140
o-Cresol
0.493
0,250
0.8000
0
61.6
13.8
137
Cresols, Total
ND
5.00
1.600
0
63.0
10
129
Hexachloro-1,3-butadiene
0.411
0.0200
0,8000
0
51.4
14.7
137
Hexachlorobenzene
0,576
0,0500
0.8000
0
72.0
12
139
Hexachloroethane
0,374
0.100
0.8000
0
46.8
14.8
132
Nitrobenzene
0.453
0,100
0.8000
0
56.6
15.6
138
Pentachlorophenol
0,701
0.250
0.8000
0
87.6
10
156
Pyridine
ND
0.250
0.8000
0
9.95
1
130
Surr: 2-Fluorophenol
0,542
1,000
54.2
10
147
Surr: Phenol-d6
0,569
1.000
56.9
10
140
Surr: Nitrobenzene-d5
0,524
1.000
52A
10
169
Surr: 2,4,6-Tribromophenol
0,730
1,000
73.0
10
185
Surr: 2-Fluorobiphenyl
0.711
1,000
71.1
10
169
Surr: p-Terphenyl-d14
0,718
1.000
71.8
10
179
RunNo: 102576
SegNo: 2327667
%RPD RPDLimit Qual
Qualifiers: B
J
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
E
M
Value above quantitation range
Manual Integration used to determine area response
H
MC
Holding times for preparation or anal;
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Pen -nit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
m
Original
Page 19 of 33

l 1 T Summit Environmental Technologies, Inc.
3310 Win St.
EtWIR4NMENTALTECHN[5OGIES,MNrL Cuyahoga Falls, Ohio44223
Analytical Laboralor/es TEL: [phone] FAX: [phone]
Website: htW://ivww.settek.com
Client: Synagro
Project: Dunn, NC WTP
QC SUMMARY REPORT
BatchID: 39131
WO#: 19081720
Sample ID
MB-39131
SampType:
MBLK
TestCode:
svoc-BNA T
Units:
mg/L
Prep
Date:
8/28/2019
RunNo:
102576
Client ID:
PBS
Batch ID:
39131
TestNo:
SW8270
SW3510C
Analysis
Date:
8/28/2019
SegNo:
2305805
Il-Sep-19
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0,250
2,4,6-Trichlorophenol
ND
0,250
2,4-Dinitrotoluene
ND
0,0500
o-Cresol
ND
0.250
Cresols, Total
ND
5,00
Hexachloro-1,3-butadiene
ND
0,0200
Hexachlorobenzene
ND
0,0500
Hexachloroethane
ND
0,100
Nitrobenzene
ND
0,100
Pentachlorophenol
ND
0.250
Pyridine
ND
0,250
Sum 2-Fluorophenol
0.402
1,000
40.2
10
109
Sum Phenol-d6
0.437
1,000
43.7
10
109
Sum Nitrobenzene-d5
0.385
1,000
38.5
19
120
Sum 2,4,6-Tribromophenol
0,510
1.000
51.0
10
120
Surr:2-Fluorobiphenyl
0.482
1,000
48.2
22
117
Surr: p-Terphenyl-d14
0,596
1.000
59.6
34
116
Qualifiers: B Analyte detected
in the associated Method
Blank
E
Value above quantitation range
H
Holding times for preparation or anal}
J Analyte detected
below quantitation limits
M
Manual Integration used to determine
area
response
MC
Value is below Minimum Compound
ND Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Qual
Original
Page 20 of 33

' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
Ettlrll 0N1AENTALTECHN7L4Ci'�S, INC Cuyahoga Falls, Ohio 44223
Arralyticaf Laboratories TEL: [phone] FAX.- [phone] WO#: 19081720
Website: ht&Q7111vww.settek.com 11-Sep-19
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39131
Sample ID LCS-39131
SampType: LCS
TestCode:
svoc-BNA_T
Units: mg/L
Prep Date: 8/28/2019
RunNo: 102576
Client ID: LCSS
Batch ID: 39131
TestNo:
SW8270
SW3510C
Analysis Date: 8/28/2019
SegNo: 2305806
Analyte
Result
PQL
SPK value
SPK Ref Val
%REC Lowl-imit HighLimit
RPD Ref Val
%RPD RPDLimit
1,4-Dichlorobenzene
0.428
0.100
0.8000
0
53.5
36.4
130
2,4,5-Trichlorophenol
0.579
0,250
0,8000
0
72A
31.7
132
2,4,6-Trichlorophenol
0,569
0.250
0.8000
0
71.1
31.1
133
2,4-Dinitrotoluene
0.682
0,0500
0,8000
0
85.2
43.3
130
o-Cresol
0,493
0.250
0.8000
0
61.6
32.9
130
Cresols, Total
ND
5.00
1.600
0
63.0
31.7
130
Hexachloro-1,3-butadiene
0,411
0,0200
0.8000
0
51A
31A
130
Hexachlorobenzene
0,576
0.0500
0.8000
0
72.0
43.1
130
Hexachloroethane
0.374
0,100
0.8000
0
46.8
36.5
130
Nitrobenzene
0.453
0,100
0,8000
0
56.6
39.5
130
Pentachlorophenol
0.701
0,250
0,8000
0
87.6
34
130
Pyridine
ND
0.250
0,8000
0
9.95
10
130
Surr: 2-Fluorophenol
0,542
1.000
54.2
17.1
130
Surr: Phenokc!6
0.569
1.000
56.9
10
130
Surr: Nitrobenzene-d5
0.524
1.000
52A
32.6
130
Surr:2,4,6-Tribromophenol
0.730
1,000
73.0
4,43
130
Surr:2-Fluorobiphenyl
0,711
1.000
71A
41.8
130
Sum p-Terphenyl-d14
0,718
1.000
71.8
36.4
130
Qualifiers: B
J
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
E
M
Value above quantitation range
Manual Integration used to determine area response
H
MC
Holding times for preparation or anal;
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Qual
Original
Page 21 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIT 3310 Win St,
FNVIRMMENTAL TECDiNfJLi;WGIF.S, INCCuyahoga Falls, Ohio 44223
WO#: 19081720
AnadytdcaP ialberatorlee TEL: [phone] FAX:[phone]
Website: htW:Iliviviv.setteic.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
BatchID: 39131
Sample ID 19081561-001AMS SampType: MS TestCode: svoc-BNA T Units: mg," Prep Date: 8/28/2019 RunNo: 102576
Client ID: BatchQC Batch ID: 39131 TestNo: SW8270 SW3510C Analysis Date: 8/28/2019 SegNo: 2305808
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene
0.308
0.200
0.8000
0
38.5
33.8
126
W
2,4,5-Trichlorophenol
ND
0,500
0.8000
0
50.5
28.7
144
W
2,4,6-Trichlorophenol
ND
0.500
0,8000
0
47.7
12.8
153
W
2,4-Dinitrotoluene
0.476
0.100
0.8000
0
59.6
20.4
155
W
o-Cresol
ND
0,500
0.8000
0
44.3
10
148
W
Cresols, Total
ND
10.0
1,600
0
45.2
10
148
W
Hexachloro-1,3-butadiene
0.295
0.0400
0,8000
0
36.9
29
126
W
Hexachlorobenzene
0.414
0,100
0.8000
0
51.7
33.7
134
W
Hexachloroethane
0.240
0,200
0.8000
0
30.0
32.8
132
SW
Nitrobenzene
0,292
0.200
0,8000
0
36.5
20
158
W
Pentachlorophenol
0,504
0.500
0,8000
0
63.0
10
176
W
Pyridine
ND
0,500
0,8000
0
7,25
10
130
SmW
Surr:2-Fluorophenol
0.382
1.000
38.2
3,39
130
W
Surr: Phenol-d6
0.413
1.000
41.3
5
130
W
Surr: Nitrobenzene-d5
0,350
1.000
35.0
14.5
154
W
Surr: 2,4, 6-Tribromophenol
0,526
1,000
52.6
19.5
130
W
Surr:2-Fluorobiphenyl
0.523
1.000
52.3
34A
130
W
Surr: p-Terphenyl-d14
0.572
1.000
57.2
8.86
156
W
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal}
7
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 22 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ISUMMIT3310 Win St.
ERVll?ONMENTAL 7ECHNaut i1=S,1AGC Cuyahoga Falls, Ohio 44223 WO#: 19081720
A.mar ra'caf Laboraiarles TEL: [phone] FAX.- [phone]
Website: htW:Illviviv.settek.com 11-Sep-19
Client: Synagro
Project: Dunn, NC WTP
SatchID: 39131
Sample ID
19081561-001AMSD
SampType:
MSD
TestCode:
svoc-BNA T
Units:
mg/L
Prep
Date:
8/28/2019
RunNo:
102576
Client ID:
BatchQC
Batch ID:
39131
TestNo:
SW8270
SW3510C
Analysis
Date:
8/28/2019
SegNo:
2305809
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene
0.442
0.200
0.8000
0
55.2
33.8
126
0.3080
35.7
30
RW
2,4,5-Trichlorophenol
0,557
0.500
0,8000
0
69.6
28.7
144
0.4036
32.0
30
RW
2,4,6-Trichlorophenol
0.534
0,500
0,8000
0
66.7
12.8
153
0,3816
33.2
30
RW
2,4-Dinitrotoluene
0.610
0,100
0.8000
0
76.3
20.4
155
0,4764
24.7
30
W
o-Cresol
0.500
0,500
0.8000
0
62.5
10
148
0,3544
34.1
30
RW
Cresols, Total
ND
10.0
1,600
0
62.9
10
148
0
0
30
RW
Hexachloro-1,3-butadiene
0,434
0.0400
0,8000
0
54.3
29
126
0.2952
38.2
30
RW
Hexachlorobenzene
0,498
0.100
0,8000
0
62.3
33.7
134
0,4136
18.5
30
W
Hexachloroethane
0.378
0,200
0.8000
0
47.2
32.8
132
0.2404
44A
30
RW
Nitrobenzene
0.433
0.200
0.8000
0
54.1
20
158
0,2920
38.9
30
RW
Pentachlorophenol
0.636
0,500
0.8000
0
79A
10
176
0,5036
23.2
30
W
Pyridine
ND
0.500
0,8000
0
11A
10
130
0
0
30
RmW
Surr:2-Fluorophenol
0,560
1,000
56.0
3,39
130
0
W
Surr: Phenol-d6
0.584
1.000
58A
10
130
0
W
Surr: Nitrobenzene-d5
0.520
1,000
52.0
14.5
154
0
W
Surr: 2,4,6-Tribromophenol
0.675
1,000
67.5
19.5
130
0
W
Surr:2-Fluorobiphenyl
0,700
1.000
70.0
34.4
130
0
W
Surr: p-Terphenyl-d14
0.661
1.000
66A
8,86
156
0
W
Qualifiers: B
J
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
E
M
Value above quantitation range
Manual Integration used to determine area response
H
MC
Holding times for prepazation or anal;
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 23 of 33

M1 I T Summit Environmental Technologies Inc.
SU3310 Win St.
Eltb(IROtJtddEtJTALTECHH©L-OGiE ,]7.I^ Cuyahoga Falls, Ohio44223
Af atytfcal Laborarcrlcs TEL: [phone] FAX. [phone]
Website: htL2://wwlv.settek.com
Client: Synagro
Project: Dunn, NC WTP
QC SUMMARY REPORT
WO#: 19081720
Sample ID
LCS-102476
SampType:
LCS
TestCode:
tclp-voc-mstr Units: mg/L
Prep
Date:
RunNo:
102476
Client ID:
LCSS
Batch ID:
R102476A
TestNo:
SW8260
Analysis
Date: 8/26/2019
SegNo:
2301194
ll-Sep-l9
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene
0.0239
0.00500
0.0200
0
119
79.4
131
1,2-Dichloroethane
0.0208
0,00500
0,0200
0
104
73.6
137
MEK
ND
0.100
0,100
0
99.4
55.1
163
Benzene
0.0207
0,00500
0,0200
0
103
73.1
132
Carbon tetrachloride
0.0181
0.00500
0,0200
0
90.4
63.7
139
Chlorobenzene
ND
0.0500
0,0200
0
108
72.3
139
Chloroform
0,0198
0.00500
0.0200
0
99.0
79.3
129
Tetrachloroethene
0.0241
0,00500
0.0200
0
121
56.2
187
Trichloroethene
0,0218
0.00500
0.0200
0
109
64.1
138
Vinyl chloride
0,0193
0.00200
0,0200
0
96.5
22.1
147
Surr:4-Bromofluorobenzene
49.1
50.00
98A
80.4
126
Surr: Dibromofluoromethane
44.4
50.00
88.8
70.3
125
Surr: Toluene-d8
48.9
50.00
97.8
82
117
Sample ID
MB-102476
SampType:
MBLK
TestCode:
tclp-voc-mstr Units: mg/L
Prep
Date:
RunNo:
102476
Client ID:
PBS
Batch ID:
R102476A
TestNo:
SW8260
Analysis
Date: 8/2612019
SegNo:
2301199
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene ND 0.00500
1,2-Dichloroethane ND 0.00500
MEK ND 0,100
Benzene ND 0,00500
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 24 of 33

UMM , V Summit Environmental Technologies, Inc. QC SUMMARY REPORT
1
3310 Win St,
ENVIPON MENTAL TECHN[] W.011E$, INC Cuyahoga Falls, Ohio 44223
JireaVytdeaP La6arator/as TEL: [phone] FAX: [phone]
WO#: 19081720
Website: http://www.settekcom 11-Sep49
Client: Synagro
Project: Dunn, NC WTP
Sample ID
MB-102476
SampType:
MBLK
TestCode:
tclp-voc-mstr Units: mg/L
Client ID:
PBS
Batch ID:
R102476A
TestNo:
SW8260
Analyte Result PQL SPK value SPK Ref Val
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
45.9
Surr: Dibromofluoromethane
43.2
Surr: TolueneA8
47.4
BatchID: R102476A
Prep Date:
Analysis Date: 8/26/2019
%REC LowLimit HighLimit RPD Ref Val
50.00
91.8
70
130
50.00
86.5
70
130
50.00
94.9
70
130
RunNo: 102476
SegNo: 2301199
%RPD RPDLimit Qual
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for prepazation or anal}
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 25 of 33

U'T Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
EP4VlrE NFd1r=NTALTEiCHNOLCIGIES,IPfC Cuyahoga Falls, Ohio44223
ltrpalyTdCaP i abo:ratard� TEL: [phone] FAX.• [phone] WO#: 19081720
Website: httg:llwlviv.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP BatchID: R102547
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4620 25.0 4800 0 96.2 85 115
Sulfide, Reactive 4460 25.0 4800 0 92.9 75 125
Sulfide, Reactive 4590 25.0 4800 0 95.6 75 125 4460 2.87 30
Qualifiers: B Analyte detected in the associated Method Blank
Value above quantitation range
H Holding times for preparation or anal}
Original

Ur> I lt Summit Environmental Technologies, Inc.
3310 Win St,
EP4l(liltOldME14TALTr:CHNDWGIES, INC. Cuyahoga Falls, Ohio 44223
Arrafy0caf Laboratories TEL: [phone] FAX.- (330) 2534489
Client: Synagro
Project: Dunn, NC WTP
Sample ID
19081915-003AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R102547
Analyte
Result
QC SUMMARY REPORT
WO#: 19081720
Website: httn://ivivw.settek.com II-Sep-I9
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
BatchID: R102547
Prep Date:
Analysis Date: 8/27/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 102547
SegNo: 2303711
%RPD RPDLimit Qual
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 27 of 33

' Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIP 014ME14TAL TECH NOLOG IFS, INC Cuyahoga Falls, Ohio 44223
WO#: 19081720
+�rrnlyilcal r.a�bc�raf�rles TEL: [phone] FAX. [phone]
Website: http://wu�rv.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP BatchID: R102648
Cyanide, Reactive ND 0.485
Cyanide, Reactive 9.12 0.490 10.00 0 91.2 85 115
Cyanide, Reactive 0.513 0.490 0.5000 0 103 50 150
Cyanide, Reactive 9.35 0.490 10.00 0.08112 92.7 81.3 118
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or anal;
Original

I,T SummitEnvironmental Technologies, Inc. QC SUMMARY REPORT
IS3310 Win St.
FFVI{ICitltdl tiTALiECtlNc�fL�a1�„7MC Cuyahoga Falls, Ohio44223
AwrwYVt/cal Laborafcrdes TEL: [phone] FAX: [phone] WO#: 19081720
Website: httn:11www.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
EatchID: R102648
Sample ID 19081915-003AMS
SampType: MS
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 102648
Client ID: BatchQC
Batch ID: R102648
TestNo:
SW9014
Analysis Date: 8/27/2019
SegNo: 2311030
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID
19081915-003AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R102648
Analyte
Cyanide, Reactive
Result
TestCode: Cyanide,Rea Units: mg/L
TestNo: SW9014
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 8/27/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 102648
SegNo: 2311031
%RPD RPDLimit Qual
8.91 0.485 10.00 0.08112 88.3 81.3 118 9.353 4.85 5
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal}
7
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 29 of 33

3SU , Nt Summit Environmental Technologies, 3310 Win St,
QC SUMMARY REPORT
RE+4V1{iL+NMENTAL TECHH©f 64CS, 1P:C Cuyahoga Falls, Ohio 44223
WO#: 19081720
ArraVlrtfcaV Labaratarls>s TEL: [phone] FAX. [phone]
Website: http://www.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
Sample ID
LCS-R102659
SampType:
LCS
TestCode:
FlashPt_S(10 Units: °F
Client ID:
LCSS
Batch ID:
R102659
TestNo:
SW1010
Analyte Result PQL SPK value SPK Ref Val
Flashpoint (140°F)
137
135.4
SatchID: R102659
Prep Date:
Analysis Date: 8/30/2019
%REC LowLimit HighLimit RPD Ref Val
0 101 98 102
RunNo: 102659
SegNo: 2311257
%RPD RPDLimit Qual
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding titnes for preparation or anal}
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P
Second column confinnation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 30 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
Pt4k+I12L tAr:WTALTECHN OLO(3]ES, INC Cuyahoga Falls, Ohio 44223
WO#: 19081720
AnaPytFCad iaboralaries TEL: [phone] FAX:[phone]
Website: htW:Ilwwli:.settek.com 114ep49
Client: Synagro
Project: Dunn, NC WTP
BatchID: R102891
Sample ID
LCS-R102891
SampType:
LCS
TestCode:
pH_14PW(450 Units: s.u.@20.1C
Prep
Date:
Client ID:
LCSW
Batch ID:
R102891
TestNo:
SW9045D
Analysis
Date: 9/6/2019
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
pH 7.0 7.0 0 100 98.6 101.4
Sample ID
19082236-002ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R102891
Analyte
pH
TestCode: pH_NPW(450 Units: s.u.@19.2C
TestNo: SW9045D
Prep Date:
Analysis Date: 9/6/2019
Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
7.3
RunNo: 102891
SegNo: 2322523
%RPD RPDLimit Qual
RunNo: 102891
SegNo: 2322525
%RPD RPDLimit Qual
7.3 0.4
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal}
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
5 H
Original
Page 31 of 33

Analysis Request/Chain of Custody
4489 For Summit f nvironmenUil 7ec:hnologies. I •. rn r.I wn A�
- -
k"age of tiI;T
Y.
Analytical Parameters and Methods
!7
4.
Y
Som
y
C
�
L'
v
G
TIMM
P6 .L
y
[�u
goo
W
ago ti
°$WAWA
^ goo
- .
v.
4%Ma
lints
9
i
CIC
Cotleeted
u°
v,
a
I'Ic:.Mlint :1,ralY�wl
Iim
X54
kcf
:1S&f
Date 'lime NoteslCununems:
,uuc a/5amplc Ory'gm
�rj h' NG =OI(COhINLLANCE
Yf:S NC7
airrijicd5rIl)NRFQUiRF.T IUS NO
RL �Ok'Ti�V4U'OR')'TUSrATC•(D11'oNI.V)
YEN NO
byes, plcaw firmjLe PWS, STU,
Simi he appraw4I pk l p Z: s u01;41 Pn n6�k, ti1,.,,n
`— will
hyi;4t, rllana� f irq+ a4 f)K'-+FwY%Idemir
y,�mnrlca W the Iatu7rnYpry. The cletu rcl:urtiy the i �. 1214
_ age f 1
Page 32 of 33

U,Y summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLQGiFfi, INC- Cuyahoga Falls, Ohio 44223
Analytteal Laboratonee TEL: [phone] FAX. [phone]
Website: hQ:11www.settek.coni
Client Name: SYWNC-27028
Logged by: John A.Semenik
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
Work Order Number: 19081720
8/22/2019 10:20:00 AM
8/22/2019 1:37:08 PM
8/22/2019 2:53:33 PM
Sample Log -In Check List
� �
l .V ph ae,
RcptNo: 1
Chain of Custody
1, Is Chain of Custody complete? Yes ❑�/ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3, Coolers are present? Yes ❑d No ❑ NA ❑
4, Shipping container/cooler in good condition? Yes ❑d No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes � No ❑ NA ❑
7, Sample(s) in proper container(s)? Yes 0 No ❑
8, Sufficient sample volume for indicated test(s)? Yes 0 No ❑
9, Are samples (except VOA and ONG) properly preserved? Yes 0 No ❑
10. Was preservative added to bottles? Yes ❑ No 0 NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials ❑�
12, Were any sample containers received broken? Yes ❑ No❑
13. Does paperwork match bottle labels? Yes ❑ No ❑
(Note discrepancies on chain of custody)
14, Are matrices correctly identified on Chain of Custody? Yes No ❑
15. Is it clear what analyses were requested? Yes No ❑
16. Were all holding times able to be met? Yes R1 No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA 0
Person Notified: i Date
By Whom: Via: ❑ eMail ❑Phone ❑Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed By
1
3.7
Good
Not Present
Page 33 of 33

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period:
of Dunn WWTP
From 01/01/19
WQ Permit Number: WQ 0006101
NPDES Number: NC 0043176
To 12/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved "Ald alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaeroc
biDigestion
Air Drying
Composting
Aerobic Digestion
If applicable to alternative performed (Class A or Class Bl complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61'
MPN
MPN/g
Coliform
power per gram
of total solids
43,100
435100
4300
CFU/g
0
1X/yr,
Grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction) X
Option/Alt. 5
(14-Day Aerobic)
Option/Alt, 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Mt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench)
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
(Spec,
Option/Alt. 4
02 uptake)
Option/Alt, 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false. certification including fine and imprisonment."
)
onrie Dukes, WWTP Supervisor
Prepares Nameand Title (type or print)
Signature of Preparer* ate
Land Applies Name and Title (if applicable) (type or print)
Signature of Land Applior (if applicable)
Date
*Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc.
Synagro
Dunn WWTP
Laboratory Report
Yes
190Aul
M. Sims
190201 -1 'sludge cr Fec. Coliform-S <43100 CFUl9 43100 02/05/19 ERP
-2 <43100 CFU/o 43100
-3 <43100 CFUl9 43100
4 <431 00 CFU/9 43100
'5 <43100 CFUl9 43100
-6 <43100 CFU/g 43100
-7 <43100 CFUlg 43100
Geomean <43100
190201 -1 3�uage Gr Ts (%) 2.32% 0.01
-2 2.32% 0.01
-3 2.32% 0.01
42.32% 0.01
-5 2.32% 0.01
-6 2.32% 0101
-7 2.32% 0401
Report
Review
Project Manager
Date
NC DENR #654
NC PHHS #37799
US EPA #NC01918
02/04119
9222D - MF
02/05/19 ERP 2540 G -TS
219 S. Steele 5tr.
919-208-4240
Sanford NC 27330 [e-mail]

an S. , NC str. Cameron Testing Services, Inc. y
Sanford, NC 27330 Chain of Custody
Phone. [phone] NC WW/GW Cert. #654 NC PHHS Cert # 37799 US EPA NCO1918 Page of
Company ll� , EmailIvN
til t -, _CfS dab use t
NIII
1CO�1taCt
pa SnpTemp
t - ---- f
'IN1 l7 �l
Address City„� W`� !c {Y3` a
State £l�I �z ' ti 11 ilt�l it l l �; �,
a M2 p�iIt V�i �ti t. 7 N --
Notes �SAe�mrt IN) i { } 11 R Y ,4t
�57� ).
Protect NN
��\- 1,1
—
wN
t' Rush (Y1M Due
Cgil�ecetl Name:
9 re Si
.O'C��
V,�WKIt t Illy k < , , tip f?;,r �:a . , ,,.�n 6 i k
IN
, a ,� , C { .. Y.. t1 r�+� ls. » 3., • ,l.,x. < u ` ; a _` 3lll tVr s S ' Y
Sa 1 w 1 ei ORn -u� It.r at[on .; z , l l
s ,ti. >.t -c.. .� �. ,l11.. .�.
_., i„rf,w„Yc tau 1 s t, l.. 11�5:2 na t .ta�5
tv. .., �S�.. �y l �aa4}.: ;�
.. .,,,N . ,F �� ,%a' .fr �? iti t.,iININNI;;lf?; n I `1,1
s cL f ? o "' a Preservatives. (U)npresenred,, H(C)I
Sample ID E ; ?- c� �,
s�w� l=
j= o 1 aD N o o i �! o H2(S)04, H(N)03; (Na)Thiosulfate; Na(0)H',,l
> Other(X), Indicate11k { ,
- i ;--- ---1------�----I---�---�--------lam-- - ; � � -
I IN
,- ---
I
-r
--
�- -t---- --- - - _ _--- -
Reli°'
n u`ishe
t,
Rece"IN, NI
,. , lIN
Ut , 1... t
�ued:�
J
Rush work will require prior approval. Additional charges will apply

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period:
of Dunn WTP
of Dunn WTP
From 01/01/19
WQ Permit Number: WQ 0006101
NPDES Number. 03-43-010
To 12/31/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaeroon
Air Drying
Composting
Aerobic Digestion
If applicable to alternative performed (Class A or Class Bl complete the followinn monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 611
MPN
MPN/g
Coliform
power per gram
of total solids
<83,100
<1022000
<116,000
CFU/g
0
l X/yr.
Grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench)
(Spec.
were performed X
No vector attraction reduction alternatives
"I certify,
under penalty
of law, that the pathogen requirements
in 40
CFR
503.32/15A NCAC 02T.1106 and the vector attraction
X reduction
requirement in 40 CFR 503.33/15A NCAC 02T.1107
have
been
met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Ian Stroud, WTP
Preparer Nam
of Preparer*
or print)
(D API
Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
C 2T.1102

Cameron Testing Services, Inc.
i� Synagro
P �ec1
Dunn WTP
Laboratory Report
Sample Information
M. Goad teat 08/21/19 ey d'
MV
x ,.
Analyses and Results
191581
Yes
J. Cameron
191581 1 nudge cr Fec. Coliform-S <83100 CFU/g 83100 08/21/19
2 <11600 CFU/g 116000
3 <13800 CFU/g 138000
4 <89700 CFU/g 89700
5 <90800 CFU/g 90800
6 <10600 CFU/g 106000
7 <99800 CFU/g 99800
Geomean <102000
191581 01 1 Sludge Gr TS (%) 1.20% 0.01 08/21/19
2 0.859% 0.01
3 0.724% 0.01
4 1.12% 0.01
5 1.10% 0.01
6 0.945% 0.01
7 1.00% 0.01
Report '
Review
Project Manager Date
219 S. Steele Str.
Sanford NC 27330
NC DENR #654
NC PHHS #37799
US EPA#NC01918
08/21/19
RL 9222D - MF
RL 2540 G -TS
919-208-4240
chris�camerontesting.com

219 Sanford,
Steele Cameron Testing Services, Inc.
Sanford, NC 27330 Chain of Custody
Phone: [phone] NC WW/GW Cert. #654 NC PHHS Cert # 37799 US EPA NCO 1918 Page Of
Company: , Synagro Email
4evin Goad i [e-mail] CTS lab use Only
Melvin Phone: Sample Temp
_ 336-909=8627 (C) Lab ID l
Address (City, 284 Boger Rd. Fax: Ice (Y/N) j
State, zip) MoCksville, NC 27028 - - Notes: Permit (Y/N)I - -- -- —
M. 919 799-0766--
Praject:
Tvnn WT7 Rush (Y/N) Due:
Collected: Name: Melvin Goad Signature:
Sample Information Number of bottles Requested Analysis
Sample ID E � c� LO a Preservatives: (U)npreserved, H(C)I, CTS Lab
❑ V N N m o¢ J H2(S)04, H(N)031 (Na)Thiosulfate, Na(0)H, ID
0 °' i 00 > Other (X), Indicate
r
LCrtyL _l ( 2 .%� lrjl_
- I
- - - - -I D
I
elves•
Rush work will require prior approval. Additional charges will apply

Agricultural Lime Application Log
Year. 2019
Proiect: Dunn WWTP
Field
Soil
Lime Recommendation
Tons/Acre
Date
(state -county -site -field)
PH
from soil analysis)
Applied
Applied
NC-CU-10-01
6.8
O.OT/AC
N/A
N/A
NC-CU40-03
6.3
O.OT/AC
N/A
N/A
NC-CU40-04
6.2
O.OT/AC
N/A
N/A
NC-CU40-05
6.4
O.OT/AC
N/A
N/A
NC-CU-34-01
6.0
O.OT/AC
N/A
N/A
NC-CU-34-02
5.9
1.1T/AC
1.1T/AC
NC-M34=03
6.0
O.OT/AC
N/A
N/A
NC-CU-34-04
6.0
O.OT/AC
N/A
N/A
NC-CU-34-05
6.4
O.OT/AC
N/A
N/A
* Ag lime will be applied v
when field
and crop conditions are suitable.

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY19-SL029723
�uLru
� "��.acGN�
PredlCttve
Client:
Ray Edwards
Advisor:
Synagro
7001 Main St
284 Boger
Rd
Soil
Report
Mehlich-3 Extraction
Wade, NC 28395
Mocksville,
NC
27028
wJ~
�n`c
Sampled County: Cumberland
F�unnEo,a�.
Links to Helpful Information
Sampled:
04/08/2019
Received:
04/15/2019
Farm: Not Provided
Completed:
04/23/2019
Client ID: 249287
Advisor
ID:
404711
Sample ID: CM101
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M
0.0
180-220 0
190
0
0
pH$
0
0
0
Note: 12 Note:
2 -
0.0
Test Results [units - W/V
in g/crrr3; CEC and Na in meq/100 cn73; NO3-N
in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC
BS% Ac pH
P-I K-1
Ca% Mg%
S-I Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS -I NO3-N
0.56 1.25
6.7
94 0.4 6.8
300 21
69 24
36 120
78
989
989
164
0.1
1
Sample ID: CM103
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Bermuda hay/past., M
0.0
180-220 0
190
0
0
0
0
$
0
Note: 12 Note:
2 -
0.0
Test Results [units - WN
in g/cm3; CEC and Na in meq/100 cn73; NO3-N
in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC
BS% Ac pH
P-I K-I
Ca% Mg%
S-I Mn-I
Mn-All
Mn-AI2
Zn-1
Zn-AI
Cu-1
Na
ESP
SS -I NO3-N
0.36 1.31
4.1
86 0.6 6.3
97 20
58 26
26 140
97
153
153
21
0.1
2
Sample ID: CM104
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., M
0.0
180-220 0
210
0
0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units -W/V
in g/crrr3; CEC and Na in meq/100 cn73; NO3-N
in mg/drift
Soil Class:
Mineral
HM% W/V
CEC
BS% Ac pH
P-1 K-1
Ca% Mg%
S-I Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.41 1.36
4.1
85 0.6 6.2
201 14
59 25
27 78
61
413
413
118
0.1
2
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, CommissionerofAgriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.neagr.gov/agronomi/ Report No. FY19-SL029723
Ray Edwards
Page 2 of 3
Sample ID: CM105 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past., M 0.0 180-220 0 200 0 25 0 0 0 0 Note: 12
2 - 0.0
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K=1 Ca% Mg% S-I Mn-I Mn-AI1 Mn=AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.27 1.41 3.5 88 0.4 6.4 123 17 58 28 22 124 85 182 182 46 0.1 3

NCDA&CS Agronomic Division Phone: (919) 733=2655 Website: www.neagr.gov/agronomi/
Report No. FY19=SL029723
Ray Edwards
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report
Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-AI1
Mn-availability index for crop 1MnwAI2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs,htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncapr.gov/apronomi/obpart4.htmYlfsfind information that
P=I
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-I
sulfur index
Test Results
SSW]
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-1, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine]
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncaprgov/aoronomi/uvrst.htm

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.govlagronomi/
Report No. FY20-SL0072lO
I. �!"'
~,�Y`{^
Client:
Harold Eldridge
Advisor;
Synagro
,5 4,l, Predictive
8373 Rhodes Pond RdAl
.
S na ro
l _ I
,f/i'
K,.,�t�F� Soil
Report
Mehiich-3 Extraction
Dunn, NC 28334
284 Boger Rd.
Mocksville,
NC 27028
Sampled County: Cumberland
Links to Helpful Information
Client ID; 295037
Advisor
ID; 503079
sampled:09/26/2019 Received: 10/01/2019 Completed: 10/08/2019
Farm:
Sample ID: C 3401
Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop (tonslacre)
N P2O6
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History,
1-Fescue/OGrass/Tim, M
0.0
l20-200 0
100
0 0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN
In glcm3; CEC and Na In meq/100
cm3; NO3•N
In mg/dm3]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH P-1
K-I
Ca% Mg%
Sal
Mn-I
Mn-All Mn•Al2
Zn-I
Zn-AI
Cum[
Na ESP
SS -I NO3-N
1.67 1.26 T5
83 1.3 6.0 163
21
57 24
39
79
64
218
218
140
0.1 1
Sample ID: CU3402
Recommendations;
Lim®
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O9
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, E
1.1
50-70 0
30
0 0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN
In glcm3; CEC and Na in meq/100
cm3; NO3-N
In mgldm3]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH PM]
Kul
Ca% Mg%
Sol
Mn-I
Mn•Al1 Mn•AI2
Zn-1
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
0.66 1.38 6A
80 1.3 5.9 210
33
52 25
41
109
75
264
264
152
0.1 2
Sample ID: CU3403
Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M
0.0
120=200 0
80
0 0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units • WN
In g1cm3; CEC and Na in meq/100
cm3; NO3-N
In mg/d0]:
Soil Class,
Mineral
HM% WN CEC
Bs% Ac pH Pal
Kul
Ca% Mg%
Sal
Mn-1
Mn-AI1 Mn•AI2
Zn-I
`Zn-AI
Cum[
Na ESP
SS -I NO3-N
1.61 1.21 7.9
82 1 A 6.0 151
31
57 23
53
55
50
286
28&
159
0.1 1
iunt i er.,i Curi!!iti�u�n
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality,
- Sfeve Troxler, Commissioner of Apriculfure

NCDA&CS Agronomic Division Phone; [phone]
Webslte: www.ncagr.gov/agronomi/
Report
No. FY20-SL007210
Harald Eldridge
Page 2 of 3
Sample ID: CU3404
Recommendations;
Lime
Nutr
ents (lb/acre)
More
Crop (tons/acre)
• N P205
K20
Mg
S
Mn
Zn
Cu
B Information
Lime History:
1-Fescue/OGrass/Tim, M
0.0
120-200 0
60
0
0
0
0
0
0 Note: 12
2 -
0.0
Test Results [units • WN
In glad, CEC and Na In meq/100
cm3, NO3-N
In mg/dm3];
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH Pal
Kul
Ca% Mg%
Sol
Mn-I
Mn-AI1
Mn•AI2
Zn-1
Zn-Al
Cu•I Na
ESP SS•I NO3wN
0,97 1.33 5,7
79 142 600 268
38
52 23
51
71
60
218
218
239 0A
2
Sample ID: CU3405
Recommendations:
Lime
Nutrients I /acre)
More
Crop (tons/acre)
N P208
K20
Mg
S
Mn
Zn
Cu
B Information
Lime History:
1-Fescue/OGrass/Tim, M
0.0
120-200 0
60
0
0
0
0
0
0 Note: 12
2 -
040
Test Results [units - WN
In glcd, CEC and Na in meq/100
cd, NO3-N
In mg/ddj:
Soil Class:
Mineral
HM% W/V CEC
BS% Ac PH Pal
Kw1
Ca% Mg%
Sol
Mn•i
Mn•A11
MnvAl2
Zn-I
ZnwAI
Cu•I Na
ESP SSwI NO3-N
1.02 1.28 805
89 180 6A 229
41
57 29
57
83
60
322
322
225 041
1