WQ0021826_Residual Annual Report 2019_20200226

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/26/2020
Received:*
Project Number* WQ0021826
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0021826
Applicant\Permittee * Synagro
Facility Name * City of Roxboro
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Roxboro 2019 Annual Report
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
ROXBORO NC 2019 Annual Report FINAL.pdf 25.34MB
upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/21/2020

435 Williams Court, Suite 100
Baltimore, Xff) 21220
wwwsynagro.com
FEBRUARY 2 [, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0021826
Dear NCDEQ:
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Roxboro, NC.
If you have any questions or need additional information, please do not hesitate to contact
Thomas Warren at [phone] ext. 22 or Ryan Copeland at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Thomas Warren, City of Roxboro
Ryan Copeland, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF ROXBOROI NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0021826
2019 ANNUAL REPORT

City of Roxboro, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNectorRttraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00021826 County Person Year 2019
Facility Name (as shown on permit) City of Roxboro WWTP & WTP NPDES No. NCO021024
Land Application Operator Svnagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summary:
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: 6
Total amount of dry tons applied during the year for all application sites: 478.97
Total number of acres utilized for land application during the year: 62.6
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited. to items
143 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T . 1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C —Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information,. including the possibility of fines and imprisonment for
knowing violations."
Thomas S. Warren, Assistant City Manager
Pennittee Name and Title (type or print) Signature of Pe 'tt Date
Signature of Preparer* Date Signatuh o d Appli Date
if different from Permittee) (if different from Pbrmiftee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
ROXBORO,NC
ROXBORO, NC WWTP AEROB. DIGESTED CAKE
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT
February 2019 256400 Y 57.14 D
June 2019 1,890.00 Y 421.83 D
YEARLY TOTAL 21146400 Y 478097 D
DRY METRIC
TONS
51.82
382.62
434444
1 /30/2020

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ002104V
Facility Name: ROXBORO, NC
NPDES# . NCO021024
or WQ# (residual only)
WWTP Name. ROXBORO WWTP
Residuals Analysis Data
Product Type
Date Sampled (grab) or
Date Composited
Percent Solids
Laboratory
PACE ANALYTICAL SERVICE INC.
Waypoint Analytical Virginia Inc.
AEDCAK
AEDCAK
AEDCAK
AEDCAK
01/07/19
06/19/19
08/07/19
11/06/19
26.50
24.40
23.80
19.50
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
<3.1
1.2
0.3
1.31
0.413
<5
5.67
1.59
0.526
6.36
1.26
0.6
NR
429
427
45
53.2
524
32.4
533
39.7
7.1
17.5
873
5
32.9
6.14
24.8
892
<5
43.3
7.16
29.7
5.86
1060
40.7
8.36
16.8
6.62
1050
12600
16500
19400
20400
36200
54100
48300
44400
2710
6930
12400
3230
<7.5
102
23
34.6
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X (SIGNATURE OF OF P
DENR FORM RSSF (5/2003) Printed: Wednesday - February 5, 2020 at 18:58:13 for: 2102 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0021826
Facility Name: ROXBORO, NC
NPDES# : NCO021024
or WQ# (residual only)
WWTP Name: ROXBORO WWTP
Residuals Analysis Data
Product Type
Date Sampled (grab) or
Date Composited
Percent Solids
AEDCAK
O1/07/19
PARAMETERS (mg/kg dry weight)
Aluminum
Calcium
Magnesium
pH
Potassium
Sodium
Laboratory
PACE ANALYTICAL SERVICE INC.
Waypoint Analytical Virginia Inc.
AEDCAK AEDCAK AEDCAK
06/19/19 08/07/19 11/06/19
26.50 24.40 23.80 19.50
20200
22800
26500
20300
13600
12300
15100
16200
3160
3160
3420
3460
7.60
7.90
8.60
8.30
2830
1670
1920
2550
<1550
601
715
892
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(SIGNATURE OF PREPARE
NR -Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Wednesday -February 5, 2020 at 18:58:39 for: 2102 01

Analytical
www,pacelabs.com
January 15, 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: Roxboro WWTP
Pace Project No.: 92413364
Dear Nate Roth:
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for samples) received by the laboratory on January 08, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
lorri.Patton@pacelabs0com
1(828)254J176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Page 1 of 16

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Project:
Pace Project No
Roxboro WWTP
92413364
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC. Page 2 of 16

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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Roxboro VWVfP
92413364
Analyses
Lab ID
Sample ID
Method.
Analysts
Reported
Laboratory
92413364001
Roxboro 1 of 4
EPA 601 OD
IDS
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 2710E-2011
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 16

Analytical
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Project:
Pace Project No
Roxboro VWVfP
92413364
ANALYTICAL RESULTS
Sample: Roxboro 1 of4 Lab ID: 92413364001 Collected: 01/07/19 14:30 Received: 01/08/19 12:45
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 30506
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
CAS No.
Aluminum
20200
mg/kg
30.9
1
01/11/19
09:20
01/13/19
22:55
7429-90-5
Arsenic
ND
mg/kg
3A
1
01/11/19
09:20
01/13/19
22:55
7440-38-2
Cadmium
1.2
mg/kg
0,31
1
01/11/19
09:20
01/13/19
22:55
744043-9
Calcium
13600
mg/kg
30.9
1
01/11/19
09:20
01/13/19
22:55
7440-70-2
Copper
429
mg/kg
1.5
1
01/11/19
09:20
01/13/19
22:55
7440-50-8
Lead
39.7
mg/kg
1.5
1
01/11/19
09:20
01/13/19
22:55
7439-92-1
Magnesium
3160
mg/kg
30.9
1
01/11/19
09:20
01/13/19
22:55
7439-954
Molybdenum
7A
mg/kg
1.5
1
01/11/19
09:20
01/13/19
22:55
7439-98-7
Nickel
17.5
mg/kg
1.5
1
01/11/19
09:20
01/13/19
22:55
7440-02-0
Potassium
2830
mg/kg
1550
1
01/11/19
09:20
01/13/19
22:55
7440-09-7
Selenium
5.0
mg/kg
3A
1
01/11/19
09:20
01/13/19
22:55
778249-2
Sodium
ND
mg/kg
1550
1
01/11/19
09:20
01/13/19
22:55
7440-23-5
Zinc
873
mg/kg
3A
1
01/11/19
09:20
01/13/19
22:55
7440-66-6
7471 Mercury
Mercury
2540G Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
Analytical Method: EPA 74716 Preparation Method: EPA 74716
0.30 mg/kg 0.013 1 01/11/1921:31 01/14/1912:24 7439-97-6
Analytical Method: SM 2540G-2011
26.5 % 0.000010 1 01/10/1913:28
Analytical Method: ASTM D2974-87
73.5 % 0.10 1 01/10/1913:20
Analytical Method: EPA 9045D
Qual
13�
7.6 Std, Units 0.10 1 01/15/19 10:59 H3
Analytical Method: SM 2710E-2011
11400 mg/kg 0.12 1 01/15/1911:49 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
2710 mg/kg
34.3 1 01 /12/19 10:40 01 /12l19 15:30 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
36200 mg/kg
1890 10 01/14/19 11:34 01/15/19 05:58 7727-37-9
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3 ND mg/kg 7.5 1 01/10/19 01:57 01/10/19 03:52
Nitrogen, Nitrate ND mg/kg T5 1 01/10/19 01:57 01/10/19 03:52 14797-55-8
Nitrogen, Nitrite ND mg/kg 3.8 1 01/10/19 01:57 01/10/19 03:52 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus 12600 mg/kg 363 50 01/09/19 20:23 01/10/19 15:14 7723A4-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, I.I.C. Page 4 of 16

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Roxboro VWVfP
Pace Project No.: 92413364
QC Batch: 452089
Analysis
Method:
EPA 7471 B
QC Batch Method: EPA 7471 B
Analysis
Description:
7471 Mercury
Associated Lab Samples: 92413364001
METHOD BLANK: 2472136
Matrix: Solid
Associated Lab Samples: 92413364001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/kg
ND 0.0060 01/14/1912:06
LABORATORY CONTROL SAMPLE: 2472137
Spike
LCS
LCS %Rec
Parameter
Units
Conc.
Result
%Rec Limits Qualifiers
Mercury
mg/kg
0.083
0.067
81 80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE:
2472138
2472139
MS
MSD
92413378001
Spike
Spike
MS MSD MS MSD %Rec
Parameter Units
Result
Conc.
Conc.
Result Result %Rec %Rec Limits RPD Qual
Mercury mg/kg
0.0063
0.055
0.057
0.048 0.049 75 75 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 16

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QUALITY CONTROL DATA
Project: Roxboro WWTP
Pace Project No.: 92413364
QC Batch: 451935 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92413364001
METHOD BLANK: 2471114 Matrix: Solid
Associated Lab Samples: 92413364001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aluminum mg/kg ND 10.0 01/13/19 22:18
Arsenic mg/kg ND 1.0 01/13/19 22:18
Cadmium mg/kg ND 0,10 01/13/19 22:18
Calcium mg/kg ND 10.0 01/13/19 22:18
Copper mg/kg ND 0,50 01/13/19 22:18
Lead mg/kg ND 0.50 01/13/19 22:18
Magnesium mg/kg ND 10.0 01/13/19 22:18
Molybdenum mg/kg ND 0.50 01/13/19 22:18
Nickel mg/kg ND 0,50 01/13/19 22:18
Potassium mg/kg ND 500 01/13/19 22:18
Selenium mg/kg ND 1.0 01/13/19 22:18
Sodium mg/kg ND 500 01/13/19 22:18
Zinc mg/kg ND 1.0 01/13/19 22:18 BC
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2471115
Units
Spike
Conc.
LCS
Result
LCS
% Rec
%Rec
Limits
Qualifiers
Aluminum
mg/kg
500
458
92
80-120
Arsenic
mg/kg
50
44.2
88
80-120
Cadmium
mg/kg
50
44A
89
80-120
Calcium
mg/kg
500
457
91
80-120
Copper
mg/kg
50
47.2
94
80-120
Lead
mg/kg
50
44.6
89
80-120
Magnesium
mg/kg
500
448
90
80-120
Molybdenum
mg/kg
50
48A
97
80-120
Nickel
mg/kg
50
45.2
90
80-120
Potassium
mg/kg
500
ND
92
80-120
Selenium
mg/kg
50
42.3
85
80-120
Sodium
mg/kg
500
468J
94
80-120
Zinc
mg/kg
50
45.0
90
80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2471116
2471117
MS
MSD
92413357001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits RPD Qual
Aluminum mg/kg
55600
9280
8310
69300
63600
148
96
75-125 9 M1
Arsenic mg/kg
ND
928
831
827
734
89
88
75-125 12
Cadmium mg/kg
ND
928
831
848
758
91
91
75A25 11
Results presented on this page are in
the units indicated by the "Units"
column
except where
an alternate
unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16

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QUALITY CONTROL DATA
Project: Roxboro VWVfP
Pace Project No.: 92413364
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2471116
MS
Parameter
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
92413357001
Spike
Units
Result
Conc.
mg/kg
17500
9280
mg/kg
393
928
mg/kg
23.2
928
mg/kg
3700
9280
mg/kg
11.7
928
mg/kg
15.5
928
mg/kg
ND
9280
mg/kg
ND
928
mg/kg
ND
9280
mg/kg
1880
928
MSD
Spike
Conc.
8310
831
831
8310
831
831
8310
831
8310
831
2471117
MS
Result
27500
1350
865
12700
900
871
13000
783
11100
2770
MSD
Result
25000
1220
770
11400
804
778
11900
687
10100
2570
MS
Rec
107
103
91
97
96
92
97
84
92
97
MSD
Rec
90
99
90
93
95
92
95
82
91
84
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Rec
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
G7��
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
9
10
12
11
11
11
9
13
10
8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 16

Analytical
www.pacela6s.com
Project:
Pace Project No.
Roxboro WWTP
92413364
QUALITY CONTROL DATA
QC Batch: 451773 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92413364001
SAMPLE DUPLICATE: 2470313
92413062001
Parameter Units Result
Percent Moisture % 1.1
SAMPLE DUPLICATE: 2470314
Parameter
Percent Moisture
92413381002
Units Result
% 96.7
Dup
Result
0.80
Dup
Result
96.7
RPD Qualifiers
35 D6
RPD Qualifiers
0
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 16

Analytical
www.pacela6s.com
Project:
Pace Project No
Roxboro WWTP
92413364
QUALITY CONTROL DATA
QC Batch: 452172 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92413364001
SAMPLE DUPLICATE: 2472426
Parameter Units
pH at 25 Degrees C Std. Units
SAMPLE DUPLICATE: 2472427
Parameter Units
pH at 25 Degrees C Std. Units
92413563001
Result
5.2
92413312001
Result
~�:]
Dup
Result RPD Qualifiers
5.3 0 H3
Dup
Result RPD Qualifiers
6.8 0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 16

Analytical
www.pacela6s.com
Project: Roxboro WWTP
Pace Project No.: 92413364
QC Batch: 452023
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92413364001
METHOD BLANK: 2471582
Associated Lab Samples: 92413364001
Parameter
Nitrogen, Ammonia
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Matrix: Solid
Blank Reporting
Units Result Limit Analyzed
mg/kg ND 8.9 01/12/1915:09
LABORATORY CONTROL SAMPLE: 2471583
Spike LCS
Parameter Units Conc. Result
Nitrogen, Ammonia mg/kg 472
Qualifiers
LCS %Rec
Rec Limits
464 98 90-110
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE &MATRIX SPIKE DUPLICATE:
2471584
2471585
MS
MSD
92413357001
Spike
Spike
MS MSD MS MSD %Rec
Parameter Units
Result Conc.
Conc.
Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg
13200 10300
10500
21800 22500 83 89 90-110 3 M6
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2471586
MS
92413358001 Spike
Parameter Units Result Conc.
Nitrogen, Ammonia mg/kg ND 2320
2471587
MSD
Spike MS MSD MS MSD %Rec
Conc. Result Result %Rec %Rec Limits RPD
2320 2210 2210 93 93 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Qual
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 16

Analytical
www.pace/a6s.com
QUALITY CONTROL DATA
Project: Roxboro WWfP
Pace Project No.: 92413364
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 452219
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA
351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Associated Lab Samples:
92413364001
METHOD BLANK: 2472536
Matrix: Solid
Associated Lab Samples:
92413364001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
ND 50.0
01/15/19
04:45
LABORATORY.CONTROLSRMPLE:
2472537
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
1000
967
97
90-110
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE: 2472538
2472539
MS
MSD
92413357001
Spike
Spike MS
MSD
MS
MSD
%Rec
Parameter
Units Result
Conc.
Conc. Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total
mg/kg 62000
21200
19000 74700
74800
60
67
90-110
0 M1
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE: 2472540
2472541
MS
MSD
92413358001
Spike
Spike MS
MSD
MS
MSD
%Rec
Parameter
Units Result
Conc.
Conc. Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total
mg/kg 5230
5170
5170 8110
9500
56
83
90-110
16 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

Analytical
www.pacelabs.com
Project: Roxboro VWVfP
Pace Project No.: 92413364
OC Batch: 451629
OC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92413364001
METHOD BLANK: 2469664
Associated Lab Samples: 92413364001
Parameter
Nitrogen, Nitrate
Nitrogen, Nitrite
Nitrogen, NO2 plus NO3
QUALITY CONTROL DATA
Analysis
Method:
EPA 353.2 Rev
2.0 1993
Analysis
Description:
353.2 Nitrate +Nitrite
Matrix: Solid
Blank Reporting
Units Result Limit Analyzed
mg/kg ND 2.0 01/10/19 03:42
mg/kg ND 0.98 01/10/19 03:42
mg/kg ND 2.0 01/10/19 03:42
LABORATORY CONTROL SAMPLE: 2469665
Spike LCS LCS
Parameter Units Conc. Result %Rec
Nitrogen, Nitrate mg/kg 14.9 15.8
Nitrogen, Nitrite mg/kg 9.9 10.6
Nitrogen, NO2 plus NO3 mg/kg 24.8 26.4
Qualifiers
Rec
Limits
106 90-110
107 90-110
107 90-110
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX
SPIKE &MATRIX SPIKE
DUPLICATE:
2469666
2469667
MS
MSD
92413357001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen,
Nitrate
mg/kg
ND
425
420
412
393
97
93
90-110
5
Nitrogen,
Nitrite
mg/kg
ND
286
280
305
308
100
102
90-110
1
Nitrogen,
NO2 plus NO3
mg/kg
ND
711
702
717
701
100
99
90-110
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 16

Analytical
tvww.pecela6s.com
Project: Roxboro VWVfP
Pace Project No.: 92413364
QC Batch: 451598
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92413364001
QUALITY CONTROL DATA
Analysis Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
METHOD BLANK: 2469443 Matrix: Solid
Associated Lab Samples: 92413364001
Blank Reporting
Parameter Units Result Limit Analyzed
Phosphorus mg/kg ND 2.0 01/10l1913:45
LABORATORY CONTROL SAMPLE: 2469444
Parameter Units
Phosphorus mg/kg
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Spike LCS LCS %Rec
Conc. Result %Rec Limits Qualifiers
49 52.3 107 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE:
2469445
2469446
MS
MSD
92413357001
Spike
Spike
MS MSD MS MSD %Rec
Parameter Units
Result Conc.
Conc.
Result Result %Rec %Rec Limits RPD Qual
Phosphorus mg/kg
24300 1100
1100
23200 23300 -99 -88 90-110 1 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

Analytical
www.pacetabs.com
QUALIFIERS
Project:
Roxboro WWTP
Pace Project No.: 92413364
DEFINITIONS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
PQL -Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
.CS(D) - Laboratory Control Sample (Duplicate)
MS(D) -Matrix Spike (Duplicate)
)UP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 far the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
WNitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute,
PAST -A
Pace
Analytical
Services -Asheville
PAST-C
Pace
Analytical
Services -Charlotte
ANALYTE QUALIFIERS
gC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:38 PM out the written consent of Pace Analytical Services, LLC. Page 14 of 16

Analytical
www.pacelabs.com
Project:
Pace Project No
Roxboro VWVfP
92413364
Lab ID
Sample ID
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
92413364001
Roxboro 1
of
4
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method
EPA 3050B
EPA 7471 B
SM 2540G-2011
ASTM D2974-87
EPA 9045D
SM 2710E-2011
EPA 350.1 Rev 2.0 1993
Mod.
EPA 351.2 Rev 2.0 1993
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch Analytical Method
451935 EPA 6010D
452089 EPA 7471 B
452044
451773
452172
452503
452023 EPA 350.1 Rev 2.0 1993
Mod.
452219 EPA 351.2 Rev 2.0 1993
EPA
353.2
Rev
2.0
1993
451629
EPA
365.1
Rev
2.0
1993
451598
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
Analytical
Batch
451945
452120
452144
452403
451647
451656
Date: 01/15/2019 01:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 16

CHAIN -OF -CUSTODY Analytical Request Document LAB USEONLY- AffixWork WO# ' 92413364
aceAna/y4ical0 II I III I I III I II I I II I III
Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevant fields
Company: SYNAGRO Billing Information: Mary Brewer: 284 Boger rd, Mocksville ALL sHADL 92413364
Address: 284 Boger Rd., Mocksville, NC 27028 NC 27028
Container Preservative Type" Lab:ProjectManager:
Report To: Nate Roth (rroth@synagro,com) Email To: mbrewer@synagro,com
Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric add, (4) sodium hydroxide, (5) zinc acetate,
Copy To: Lysa Finnerty ([e-mail]) Site Collection Info/Address: (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic add, (a) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Cther
Analyses Lab Profile/Line: 0 q
Custo r Project Name/Number: State: County/City: Time Zone Collected:
Lab Sample Receipt Checklist.. Lk)/ [ ]PT [ )MT [ )CT ( ]ET Custody Seals Present/Intact +N
Phone:236�4o3d32a Site/Facility ID #: Compliance Monitoring? m Custody Signatures Present Y NNA
Email: [e-mail] [XI Yes ( ] No NC [X) SC[ ] Collector Signature Present V%P NA
Bottles intact - `') N NA
Collected By (print): Clay Fisackerly Purchase Order # : DW PWS ID if:
Correct eotties , IT NA
Quote #: DW Location Code: Sufficient Volume IT NA
Col ed By nature): Turnaround Date Required: Immediately Packed on Ice: Samples. Received on Ice V/N hA
[ X ]Yes [ ) No VOA Headspace Accepta'nleY NCNe'?`1
N USDA Regulated &oils - Y t7
Sample D' osal: Rush: Field Filtered (if applicable): N n Samples in Holding Time 4LY-,'N tdA
[X] Dispose as appropriate I J Return ( ) Same Day [ ] Next Day [ ] Yes ( ] No z to Residual Chlorine Present Y N +A i
( ]Archive: M Cl: Strips:
( ] 2 Day [ ] 3 Day [ ] 4 Day [ ) 5 Day Z a7 O v p Sample.pH Acceptable i
Y N N
[ )Hold: (Expedite Charges Apply) Analysis: - (a) U) ,:� I—;. pH Stripst -
` Matrix Codes Insert in Matrix box below): Drinking Water DW , Ground Water GW , Wastewater WW , ui � c - Li Sulfide Present Y 1d 2x
( ) g ( ) ( ) ( ) U 2 n
O / ( ) ( ) p ( ) ( ) ( ) yO P ( ) ( ) Y )� 3 Lead Acetate Strips:
Product P , Soil Solid SL , Oil OL , Wipe WP , Air (AR), Tissue TS , Bioassa B , Vapor V , Other OT - N d 2
Q-
CO
Comp/ Collected (or Res #of , Z t1 L LAB USE ONLY:
Composite End 0 Cts Lab Sample / .Comments:
Customer Sample ID Matrix' Grab Composite Start) CI Ctns o I E ,z` 'Z o ^ !
Date Time Date Time 0 CD E Y O Q L` i
CAD d to t` Q I-F— i1 d EL
j SL 1AW x x X. x x x x x x
Customer Remarks Special Conditions Possible Hazards: Packing Material Used h Blue Dry None SHORT HOLDS PRESENT (<72 hours) : Y N/A LAB Sample Temperature Info:
/ P / T e'of Ice Used: Get B Lab.TraCkin #: Temp Blank' Received: Y N
g g Therm !DO: ri / 6C24S
Cooler 1 Temp Upon Receipt:{Ijj�C
- SamplesTaceivedvia "' - Cooler 1 Therm Corr. Factor: C.oC-
RadChem sample(s) screened (<500 cpm): Y N NA cooler 1 corrected Temps
FEDEX UPS (lien . courier+ Pace Courier Comments:
Relin5di d by/Co a : (Signal . e) Date/Time: Receive (j/Comp y:. Signature }� Djte/T,''me: MTJL LAB USE ONLY
N /1Li i (J I +Isllci /��s Tabled: `
Relinquished k / ompany: (Signature) l Date/Time: Received by/Company: (Signature) Date/Time: Acctnum: 4,
r Trip Blank Received:. 'N.'
Template: HCL ' McOH , .TSP Other
Prelogin:
Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM: Noin Conformance(s): Page:
PB: YES J. NO of: ---Pagel(
of 16

Sodium Absorption Ratio Calculation (SAR)
i
Product Code Product Name Sample Date Report Range Ratio
2102=01=AEDCAK-NC ROXBORO, NC WWTP AEROB, DIGESTED 1/7/2019 1/1/2019=6/30/2019 1.5974
CAKE
Na mg/I = (Na mg/kg x %Solids) = 100 = (1550 x 26.5000) = 100 = 410.75
Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (13600 x 26.5000) = 100 = 3604
Mg mg/I = (mg mg/kg x %Solids) _ 100 = (3160 x 26.5000) + 100 = 837.4
Na meq = Na mg/I = Molec.Wgt.Na = 410.75 _ 23 = 17.8587
Ca meq = Ca mg/I = Molec.Wgt.Ca = 3604 = 20 = 180.2
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 837.4 = 12 = 69.7833
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 17.8587 = SgrRoot[0.5(180.2+69.7833)] = 1.59738
Printed: 2/5/2020
Page 1 18:57

Waypai nt .�
ANALYTICAL
6/28/2019
Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-172-0205
Project Description: ROXBORO WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 6/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory`s expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
jj ,..,�, ,..
.�".
Page 1 of 7

Vila hint....
��
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main $Q4-743-9401 °Fax $04-271-6446
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-172-0205
Client Project Description: ROXBORO WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
SM-4500-NH3C
WTN
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
9045D
WTN
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
4500NO3F-2011
WTN
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
6010D
WTN
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
SW-74716
WTN
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
SM-4500-NH3C-TKN
WTN
67054
ROXBORO
WWTP
Solids
06/19/2019
09:45
06/21/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 7

Report Number: 19-172-0205
Account Number: 46487
Send To: Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville , NC 27028
� 0►111t ,
��
ANALYTICAL
7621 Whitepine Raad, Richmond, VA 23237
Main $04-743-9401 °Fax $Q4-271-6446
www.waypaintanalyfical.corn
Project : ROXBORO WWTP
REPORT OFANALYS/S Date Sampled: 6/19/2019 09:45:00
Lab Number : 67054 Date Received: 06/21/2019 00:00
Sample Id : ROXBORO WWTP Date Reported: 06/28/2019
Total Solids "
Moisture
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
24.40
CJR
06/26/201914:42
75.60
CJR
06/26/201914:42
5.41
54100
250
JPJ
06/27/2019
09:30
1.65
16500
50.0
BKN
06/27/2019
03:17
0.17
1670
50.0
BKN
06/27/2019
03:17
0.73
7320
50.0
KKM
06/27/201916:02
1.23
12300
250
BKN
06/27/2019
03:17
0.32
3160
50.0
BKN
06/27/2019
03:17
0.06
601
250
BKN
06/27/2019
03:17
23900
50.0
BKN
06/27/2019
03:17
22800
50.0
BKN
06/27/2019
03:17
1240
5.00
BKN
06/27/2019
03:17
427
2.50
BKN
06/27/2019
03:17
892
12.5
BKN
06/27/2019
03:17
0.69
6930
100
JPJ
06/27/201914:00
Organic N 4.72 47170 250 06/27/2019 09:30
Nitrate+Nitrite-N 102 4.98 ZBD 06/28/201914:02
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H -Beyond holding time%,tG
Our reports
and
letters
are
for
the exclusive and confidential use
of our clients, and may
not be reproduced in whole or part,
nor may any reference be made
to the work,
the
results,
or
fhe
company in any advertising, news
release, or other public
announcements without obtaining
our prior written authorization.
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
1'}� V���
Pauric McGroary
Agronomist
Page 3 of 7

Report Number: 19-172-0205
Account Number: 46487
Send To: Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville , NC 27028
7621 Whitepine Road, Richm©nd, VA 23237
Main $04-743-9401 °Fax $04-271-6446
www.waypointanalytical.com
Project : ROXBORO WWTP
REPORT OF ANALYSIS Date Sampled: 6/19/2019 09:45:00
Lab Number : 67054 Date Received: 06/21/2019 00:00
Sample Id : ROXBORO WWTP Date Reported: 06/28/2019
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Molybdenum
Comments:
1.31
1.00
BKN
06/27/2019
03:17
45.0
2.50
BKN
06/27/2019
03:17
24.8
2.50
BKN
06/27/2019
03:17
32.9
3.00
BKN
06/27/2019
03:17
<5.00
5.00
BKN
06/27/2019
03:17
0.413
0.0147
TJS
06/26/201912:26
<5.00
5.00
BKN
06/27/2019
03:17
7.9
JSL
06/26/2019
07:43
6.14
2.50
BKN
06/27/2019
03:17
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H -Beyond holding time
Our reports
and
letters are
for
the exclusive and confidential use
of our clients, and may
not be reproduced in whole or part,
nor may
any reference be made
to the work,
the
results, or
the
company in any advertising, news
release, or other public
announcements without obtaining
our prior
written authorization.
6010D
6010D
6010D
6010D
SW-7471 B
6010D
9045D
6010D
m` ��"�
Pauric McGroary
Agronomist
Page 4 of 7

7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 °Fax 804-271-b446
www.waypoi nta nalytical.com
Cooler Receipt Form
Customer Number: 46487
Customer Name: Synagro Central LLC/ Roxboro
Report Number: 19-172-0205
Shipping Method
Fed Ex � US Postal � Lab � Other
UPS � Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? ®Yes � No
Number of coolers received 1
Custody seals intact on shipping container/cooler? 0 Yes � No � Not Required
Custody seals intact on sample bottles? � Yes � No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
COC properly completed � Yes 0 No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes � No
Sufficient sample volume for indicated test(s)? � Yes � No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No � N/A
Water -VOA vials free of headspace � Yes 0 No � N/A
Trip Blanks received with VOAs � Yes 0 No � N/A
Soil VOA method 5035 —compliance criteria met � Yes � No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
(— High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson Date &Time: 06/21/2019 11:39:59
Page 5 of 7

AMPLING LOG 0G 1
CUSTOMER:
SA
PROJECT MANAGER:
�R�
U (�
Phone: � 5�b � SJ��MPLING SAMPLE # OF
A.& L CUSTOMER LOCAT{ON TYPE CONTAINERS
LAB # SAMPLE I.D. SL .
sn� 1 LAMP i
Date Ti e Recieved by:
Relinquished by Sampler: n �N r. fpll9
w Date Time Recieved by:
D Relinquished by:
o Dale Time Recieved
Relinquished by:
l
SPECIAL INSTRUCTIONS: �U
For ! monitoring purposes.
(STATE
ANALYSIS REQUEST
Svnaaro Central LM Roxboro
ROJCBoRO WWTP
old sampling procedures
were usea gantry urc w1lection of these samples.
iZypw (,,Innp
SAM
PLER
SAMPLING METHOD METHOD
pAIE TIME, PRESERVED SHIPPED
SLR: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium an anew, Co er and Zlnc
SL2: Basic Test SL1 plus Sulfur, Caicium, Magnesium, Sodium, Iron, Aluminum, M 9 PP
OF
US {) �
. r CORD i''h ANALYSIS
'i _ 1`
1�2019
RECORD
REMARKS:

i
SAMPLING LOG #
wwmmER, SYNAGRO
PROJECTMANAaER; ✓t•-� 0 a 01
A
Q
1
C^ArkWv" %kl
• ���. •••�
III��IIII11�lIIIIflIIIIIIIIIIIIIIIIIE111IIIIIIHill IIIIIN457
062, 20,96
Svnagro-ADM 11:40:34
ADM NG2
Reflnqulshed by Sampler: Date Time Reoleved by; RF�iVWRK6:
mel
Rellnqulshed,by: Date Time Reolewd by;
by;
Time
3PECI�II.INSTRUCTI0N6;
For mombring purposes. POP,
ANALYSIS REQUEST
SAMPLE p enl CeCO® Vbleale Mo CI NO-N
LD• SLIT,L'2 NH.-N NOjrN Cd Cr NI Pb An Hg 8e PH ulv. Solids
a
AP 1#0 1#0;Oor00100 joog'1���too 'low loot �
NG �.
. i .
1
SL1: Total Sollde (Moisture), Tote) Keldahl Nitrogen, Phosphorus, and Potassium "
SL.2: Basic Teat SLi plus Sulfur, Calclum, Magrleelum, Sodlum, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2102=01-AEDCAK-NC ROXBORO, NC WWTP AEROB. DIGESTED 6/19/2019 7/1/2019-8/30/2019 0.6159
CAKE
Na mg/I = (Na mg/kg x %Solids) = 100 = (601 x 24.4000) = 100 = 146.644
Ca mg/I = (Ca mg/kg x %Solids) + 100 = (12300 x 24.4000) : 100 = 3001.2
Mg mg/I = (mg mg/kg x %Solids) _ 100 = (3160 x 24.4000) _ 100 = 771.04
Na meq = Na mg/I = Molec.Wgt.Na = 148.644 + 23 = 6.37583
Ca meq = Ca mg/I = Molec.Wgt.Ca = 3001.2 _ 20 = 150.06
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 771.04 = 12 = 84.2533
SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.37583 _ SgrRoot[0.5(150.06+64.2533)] = 0.615924
Printed: 2/5/2020
Page 1 18:57

Waypoint..
ANALYTICAL
8/19/2019
Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-221-0010
Project Description: Roxboro WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 8/9/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P,�� ro° c�"d�
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to ana/yses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

Wa vint,:
Yp
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main $t)4-743-94Q1 °Fax $Q4-271-6446
www.waypainta nalytical. com
Sample Summary Table
Report Number: 19-221-0010
Client Project Description: Roxboro WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
6777g
Roxboro
WWTP
Solids
08/07/2019
09:00
08/09/Z019
6777g
Roxboro
WWTP
Solids
OS/07/Z019
09:00
08/09/2019
SM-4500-NH3C
WTN
6777g
Roxboro
WWTP
Solids
08/07/2019
09:00
O8/09/2019
9045D
WTN
6777g
Roxboro
WWTP
Solids
08/07/2019
09:00
08/09/2019
4500NO3F-2011
WTN
6777g
Roxboro
WWTP
Solids
08/07/2019
09:00
O8/09/2019
6010D
WTN
6777g
Roxboro
WWTP
Solids
08/07/Z019
09:00
08/09/Z019
SW-7471B
WTN
6777g
Roxboro
WWTP
Solids
08/07/2019
09:00
08/09/2019
SM-4500-NH3C-TKN
WTN
6777g
Roxboro
WWTP
Solids
08/07/2019
09:00
O8/09/Z019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number:
Account Number
Submitted By:
19-221-0010
46487
Ryan Copeland
Send To: Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville , NC 27028
�I��,:
��
ANALYTICAL
7621 Whitepine Raad, Richmond, VA 23237
Main 81)4-743-9401 °Fax [phone]
wwvu,waypaintanalyfical.cam
Project :Roxboro WWTP
REPORT OFANALYS/S Date Sampled: 8/7/2019 09:00:00
Lab Number : 67778 Date Received: 08/09/2019 00:00
Sample Id : Roxboro WWTP Date Reported: 08/19/2019
Total Solids
Moisture
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
23.80
ADM
08/13/201916:41
76.20
ADM
08/13/201916:41
4.83
48300
250
JPJ
08/16/2019
08:00
1.94
19400
50.0
BKN
08/14/201919:27
0.19
1920
50.0
BKN
08/16/201914:24
0.77
7720
50.0
BKN
08/14/201919:27
1.51
15100
250
BKN
08/14/201919:27
0.34
3420
50.0
BKN
08/14/201919:27
0.07
715
250
BKN
08/16/201914:24
29500
50.0
BKN
08/14/201919:27
26500
50.0
BKN
08/14/201919:27
1370
5.00
BKN
08/14/201919:27
524
2.50
BKN
08/14/201919:27
1060
12.5
BKN
08/14/201919:27
1.24
12400
100
JPJ
08/18/201913:00
3.59
35900
250
08/16/2019
08:00
23.0
4.80
ZBD
08/16/201914:30
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H -Beyond holding time
Our reporfs
and
letters
are
for
the exclusive and confidential use
of our clients, and may
not be reproduced in whole or part,
nor may
any reference be made
to the work,
the
results,
or
the
company in any advertising, news
release, or other public
announcements withouf obtaining
our prior
written authorization.
P���
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
Pauric McGroary
Agronomist
Page 3 of 6

Report Number: 19-221-0010
Account Number: 46487
Submitted By: Ryan Copeland
Send To: Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville , NC 27028
�'��-,:
��
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main $U4-743-9401 °Fax 504-27I-6446
www.►nraypointanalytical.com
Project :Roxboro WWTP
REPORT OF ANALYSIS Date Sampled: 8/7/2019 09:00:00
Lab Number : 67778 Date Received: 08/09/2019 00:00
Sample Id :Roxboro WWTP Date Reported: 08/19/2019
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Molybdenum
Comments:
1.59
1.00
BKN
08/14/201919:27
6010D
53.2
2.50
BKN
08/14/201919:27
6010D
29.7
2.50
BKN
08/14/201919:27
6010D
43.3
3.00
BKN
08/14/201919:27
6010D
5.67
5.00
BKN
08/14/201919:27
6010D
0.526
0.0143
TJS
08/14/2019
16:27
SW-7471 B
5.86
5.00
BKN
08/14/201919:27
6010D
8.6
JSL
08/15/2019
07:49
9045D
7.16
2.50
BKN
08/14/201919:27
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H -Beyond holding time
Our reports
and
letters are
for
the exclusive and confidential use
of our clients, and may
not be reproduced in whole or part,
nor may
any reference be made
to the work,
the
results, or
the
company in any advertising, news
release, or other public
announcements without obtaining
our prior
written authorization.
Pauric McGroary
Agronomist
Page 4 of 6

7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypoi ntana lytical.com
Cooler Receipt Form
Customer Number: 46487
Customer Name: Synagro Central LLC/ Roxboro
Report Number: 19-221-0010
Shipping Method
0 Fed Ex 0 US Postal � Lab � Other
® UPS � Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? •Yes � No
Number of coolers received 1'
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes � No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
COC properly completed � Yes � No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes � No
Sufficient sample volume for indicated test(s)? � Yes 0 No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No ®N/A
Water -VOA vials free of headspace � Yes 0 No � N/A
Trip Blanks received with VOAs 0 Yes � No � N/A
Soil VOA method 5035 —compliance criteria met � Yes 0 No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson � Date &Time: j08/09/2019 14:05:29
Page 5 of 6

SAMPLING LOG #
A&L CUSTOMER
SAMPLING SAMPLE
LOCATION TYPE
iriT
Lv —
s--
�
Relinquished by Sampler: ��
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS:
For
monitoring purposes.
46487 r, r ,F ,
0. r 0
RECORD
• • r • -♦urL
usedwere aaring me com9crionof •le
SAMPLER
#OF SAMPLINGii. METHOD
CONTAINERSDATE TIME PRESERVED SHIPPED
MP F j1/1 9:U4g
mmwNN
Recieved by:
Reoleved by:
I�J�OPJPJ�
SLR: Tots! Solids (Moisture), Total Kjeldahl Niirogen, Phosphorus, and Potassium
5L2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iran, Aluminum, Manganese, Capper and Zlnc
i
REMARKS:
Sottds
�VVI)
• mm

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
210M1-AEDCAK-NC ROXBORO, NC WWTP AEROB. DIGESTED 8/7/2019 9/1/2019-10/31/2019 0.6651
CAKE
Na mg/I = (Na mg/kg x %Solids) = 100 = (715 x 23.8000) _ 100 = 170.17
Ca mg/I = (Ca mg/kg x %Solids) = 100 = (15100 x 23.8000) = 100 = 3593.8
Mg mg/I = (mg mg/kg x %Solids) + 100 = (3420 x 23.8000) + 100 = 813.96
Na meq = Na mg/I + Molec:Wgt.Na = 170.17 = 23 = 7.3987
Ca meq = Ca mg/I + Molec.Wgt.Ca = 3593.8 _ 20 = 179.69
Mg meq = Mg mg/I + Molec.Wgt.Mg = 813.96 _ 12 = 67.83
SAR = Na meq + SgrRoot(0.5 x (Ca meq + Mg meq)] = 7.3987 = SgrRoot[0.5(179.69+67.83)] = 0.665066
Printed: 2/5/2020
Page 1 18:57

Waypoint .
ANALYTICAL
11/18/2019
Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-312-0009
Project Description: Roxboro
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointanalytieal.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 11/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for pertormance of said analysis.
Page 1 of 6

Wa aint,:
Yp
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main R04-743-9401 °Fax $p4-271-6446
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-312-0009
Client Project Description: Roxboro
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/O8/2019
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/08/2019
SM-4500-NH3C
WTN
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/08/2019
9045D
WTN
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/08/2019
4500NO3F-2011
WTN
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/08/Z019
6010D
WTN
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/08/2019
SW-7471B
WTN
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/O8/2019
SM-4500-NH3C-TKN
WTN
69537
roxboro
N&M
Solids
11/06/2019
10:40
11/08/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

Wa Dint.,:
��
ANALYTICAL
:C:i�
7621 Whitepine Raad, Richmond, VA 23237
Main $04-743-9401 °Fax $04-271-6446
www.waypainta nalyfical.com
Synagro Central LLC/ Roxboro Ryan Copeland
Mary Brewer Project Roxboro Report Date : 11/18/2019
284 Boger Road Information : Received : 11/08/2019
Mocksville , NC 27028
Pam« m� �'�d``
Submitted By : Ryan Copeland
REPORTOFANALYSIS Pauric McGroary
Report Number : 19-312-0009 Agronomist
Lab No : 69537 Matrix: Solids
Sample ID : roxboro N&M Sampled: 11/6/2019 10:40
Test Results Units MQL DF Date /Time By Analytical
Analyzed Method
Ammonia Nitrogen 3230 mg/Kg -dry 513 1 11/15/19 15:00 ]PJ SM-4500-NH3C
Nitrate+Nitrite-N 34.6 mg/Kg -dry 25.6 1 11/12/19 14:14 ZBD 4500NO3F-2011
Organic N 41200 mg/Kg -dry 1280 1 11/15/19 12:00 CALCULATION
pH 8.3 s.u. 1 11/12/19 05:08 JSL 9045D
Total Solids 19.5 % 0.010 1 11/11/19 16:35 ADM SM-2540G
Total Kjeldahl Nitrogen 44400 mg/Kg -dry 1280 1 11/15/19 12:00 JPJ iM-4500-NH3C-TKP
Phosphorus 20400 mg/Kg -dry 25.6 1 11/13/19 02:44 KKM 6010D
Aluminum 20300 mg/Kg -dry 25.6 1 11/13/19 02:44 KKM 6010D
Arsenic 6.36 mg/Kg -dry 2.56 1 11/13/19 02:44 KKM 6010D
Calcium 16200 mg/Kg -dry 128 1 11/13/19 02:44 KKM 6010D
Cadmium 1.26 mg/Kg -dry 0.513 1 11/13/19 02:44 KKM 6010D
Chromium 32.4 mg/Kg -dry 1.28 1 11/13/19 02:44 KKM 6010D
Copper 533 mg/Kg -dry 1.28 1 11/13/19 02:44 KKM 6010D
Iron 23800 mg/Kg -dry 25.6 1 11/13/19 02:44 KKM 6010D
Lead 40.7 mg/Kg -dry 1.54 1 11/13/19 02:44 KKM 6010D
Magnesium 3460 mg/Kg -dry 25.6 1 11/13/19 02:44 KKM 6010D
Manganese 1000 mg/Kg -dry 2.56 1 11/13/19 02:44 KKM 6010D
Mercury 0.600 mg/Kg -dry 0.0810 i 11/12/19 14:32 TJS SW-7471B
Molybdenum 8.36 mg/Kg -dry 1.28 1 11/13/19 02:44 KKM 6010D
Nickel 16.8 mg/Kg -dry 1.28 1 11/13/19 02:44 KKM 6010D
Potassium 2550 mg/Kg -dry 25.6 1 11/13/19 02:44 KKM 6010D
Selenium 6.62 mg/Kg -dry 2.56 1 11/13/19 02:44 KKM 6010D
Sodium 892 mg/Kg -dry 128 1 11/13/19 02:44 KKM 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

Wa Dint..:
Yp
ANALYTICAL
46487
Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By : Ryan Copeland
Report Number : 19-312-0009
7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 °Fax [phone]
www.waypointa nalyiical.com
Ryan Copeland
Project Roxboro
Information
REPORT OFANAL YSIS
Report Date : 11/18/2019
Received : 11/08/2019
Pauric McGroary
Agronomist
Lab No : 69537 Matrix: Solids
Sample ID : roxboro N&M Sampled: 11/6/2019 10:40
Test Results Units MQL DF Date /Time By Analytical
Analyzed Method
Zinc 1050 mg/Kg -dry 6.41 1 li/13/19 02:44 KKM 6010D
Sulfur 8100 mg/Kg -dry 25.6 1 11/13/19 02:44 KKM 6010D
Moisture 80.5 % 0.010 1 11/11/1916:35 ADM SM-2540G
Qualifiers/ g
Definitions
Analyte detected in blank
H Beyond holding time
Page 4 of 6

� i
► � a
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypo i nta n a l yti ca I. co m
Cooler Receipt Form
Customer Number: 46487
Customer Name: Synagro Central LLC/ Roxboro
Report Number: 19-312-0009
Shipping Method
Fed Ex � US Postal � Lab � Other
• UPS � Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? ®Yes � No
Number of coolers received 1
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes � No � Not Required
Chain of Custody (COC) present? � Yes 0 No
COC agrees with sample label(s)? � Yes � No
COC properly completed � Yes 0 No
Samples in proper containers? � Yes 0 No
Sample containers intact? � Yes � No
Sufficient sample volume for indicated test(s)? � Yes � No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No ®N/A
Water -VOA vials free of headspace � Yes � No � N/A
Trip Blanks received with VOAs � Yes 0 No � N/A
Soil VOA method 5035 —compliance criteria met � Yes 0 No � N/A
� High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson Date &Time
Page 5 of 6
11 /08/2019 13:10:25

19 312-0009
l A Oro Central � - ,•� .
•
Oro
aluesir mat the proper o r sampling procedures
PROJECT MANAGER: IS lig were used during Mill collecHonof
3E
Pho SAMPLER
. �.r
s 11
#r rr
A
A SAMPLE IwD* LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
r
d �'
Relinquished by Sampler: A(16Q
I.ic71 imffils■�1TM
G
RElVL4RiSS:
ad
Time Recleved O)k
SPECIAL INSTRUCTIONS: ���
For monitoring purposes.
ATE
S�►tNiPLE Organi
�•C' SH.j SL2 PtH�-Pd NO,,N Yd Cd Cr Ml
Tame
MMe WITWE
rotauas� fly® CI ND�-i�
Solids
0
SL1: Total Soiids (Maistur'e), Total Kjeldahl Nitrogen, Phosphorus, and Potassium .
Sli Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iran, Aluminum, Manganese, Copper and Zinc
Page 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2102-01-AEDCAK-NC ROXBORO, NC 1NWTP AEROB. DIGESTED 11/6/2019
CAKE
Na mgll = (Na mg/kg x %Solids) _ 100 = (892 x 19.5000) - 100 = 173.94
Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (16200 x 19.5000) - 100 = 3159
Mg mg/I = (mg mg/kg x %Solids) _ 100 = (3460 x 19.5000) _ 100 = 674.7
Na meq = Na mg/I _ Molec.Wgt.Na = 173.94 = 23 = 7.56261
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 3159 _ 20 = 157.95
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 674.7 = 12 = 56.225
11 /1 /2019-12/31 /2019
SAR = Na meq _ SgrRoot(0.5 x (Ca meq + Mg meq)] = 7.56261 = SgrRoot[0.5(157.95+56.225)] = 0.730806
0.7308
Printed: 2/5/2020
Page 1 18:57

FACILITY NAME: R%J BUIO,NC
OWNER: RONALD CARVER
SITE #: NC PS 00024 FIELD# : PS 00024 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: WQ0021826
OPERATOR: RONALD CARVER
ANNUAL DRY TONS APPLIED : 181.01
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 23.30 ACRES PERMITTED: 23.30
rage: 1
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
2/6/19
256.00 (CY)
10.987
26.50
2.452
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
p
11410
FESCUE HAY
Feb49
256.00 (CY)
10.987
7,50
6/4/19
405.00 (CY)
17.382I
26.50
3.880
ROAEDC
DRY
0-<I/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
I FESCUE HAY
6/5/19
150.00 (CY)
6.438
26.50
1.437
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
FESCUE HAY
Jun49
555.00 (CY)
21820
Total Gallons/Ac:
Total Wet Tons/Ac:
i vLui �uvav iu,u n�.. JY.Ol
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS
Annuallbs/acre
177
0.048
0.019
NR
6.665
0.617
0.005
0.110
0.272
0.078
13.564 195.77
Cumulative lbs/acre
1.251
0.269
10.087
62.078
6.175
0.161
1.084
5.966
0.812
110.985
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
r�
l.�(JCi�+M'']
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME : ROXBORO, NC
OWNER: RONALD CARVER
SITE #: NC PS 00024 FIELD# : PS 00024 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826
OPERATOR: RONALD CARVER
ANNUAL DRY TONS APPLIED : 26.78
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.40 ACRES PERMITTED: 4.40
Page : 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/5/19
120.00 (CY)
27.273
26.50
6.087
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p710
FESCUE PASTURE
Jun49
120.00 (CY)
27.273
Total Gallons/Ac:
Total Wet Tons/Ac:
�._1 N7A1 /A
1 VLW VUULV LLL]l
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
0.038
0.015
NR
5.223
0.483
0.004
0.086
0.213
0.061
10.628
153.39
139
Cumulative lbs/acre
0.799
0.161
6.829
43.591
4.262
0.107
0.746
4.544
0.483
76.302
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not
Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME: ROXBORO, NC
OWNER: RONALD CARVER
SITE #: NC PS 00024 FIELD# : PS 00024 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: W00021826
OPERATOR: RONALD CARVER
ANNUAL DRY TONS APPLIED : 23.44
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.30 ACRES PERMITTED: 4.30
rage: 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/6/19
105.00 (CY)
24.419
26.50
5.450
ROAEDC
DRY
0-<I/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
FESCUE PASTURE
Jun49
105.00 (CIl
24.419
Total Gallons/Ac:
Total Wet Tons/Ac:
a utaa
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
124
0.034
0.013
NR
4.676
0.433
0.003
0.077
0.191
0.055
9.516 137.34
Cumulative lbs/acre
0.847
0.160
6.936
41.481
4.075
0.106
0.738
4.410
0.451
71.502
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAVE: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0001 A
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826
OPERATOR: PAUL BAILEY
ANNUAL DRY TONS APPLIED : 183.02
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.20 ACRES PERMITTED: 20.20
rage: 1
Lune Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/18/19
477.00 (CY)
23.614
26.50
5.270
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
FESCUE HAY
6/24/19
343.00 (CY)
16.980
26.50
3.790
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
FESCUE HAY
Jun49
820.00 (CY)
40.594
Total Gallons/Ac:
Total Wet Tons/Ac:
a ucu �uvav aua�u. YV.J7
As
Cu
Cr
Cu
Pb
rig
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
207
0.056
0.022
NR
7.774
0.719
0.005
0.129
0.317
0.091
15.819 228.32
Cumulative lbs/acre
1.548
0.283
11.312
65.065
7.062
0.157
1.300
7.450
0.734
112,483
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
C
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0001 B
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: WQ0021826
OPERATOR: PAUL BAILEY
ANNUAL DRY TONS APPLIED : 23.66
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 3.10 ACRES PERMITTED: 3.10
Page : 1
Lime Applied ***
Date Lbs/Ac
DATE or
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/24/19
56.00 (CY)
18.065
26.50=ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
FESCUE HAY
6/25/19
50.00 (CY)
16.129
26.50
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
FESCUE HAY
Jun-19
106.00 (CY)
34.194
Total Gallons/Ac:
Total Wet Tons/Ac:
As
Cu
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
174
0.047
0.018
NR
6.548
0.606
0.005
0.108
0.267
0.076
13.325 192.32
Cumulative lbs/acre
0.935
0,191
7.599
48.525
4.719
0.124
0.832
4.697
0.585
86.946
ROAEDC = ROXBORO, NC WWTP AEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: ROXBORO, NC
OWNER: PAUL BAILEY
SITE #: NC PS 00025 FIELD# : PS 00025 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00021826
OPERATOR: PAUL BAILEY
ANNUAL DRY TONS APPLIED : 41.07
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.30 ACRES PERMITTED: 7.30
rage: 1
Lime Apphed ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
or Wet Tons WT s eci
( ) (p fy)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/25/19
184.00 (CY)
25.205
26.50
5.626
ROAEDC
DRY
0-<1/2"
SUR
0.5
0.30
36,200. p
2,710.00 p
7.50 p
11410
FESCUE PASTURE
Jun-19
184.00 (CY)
25.205
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 25.21
TOTALS As Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
0.035
0.014
NR
4.827
0.447
0.003
0.080
0.197
0.056
9.822
141.77
128
Cumulative lbs/acre
0.583
0.115
4.894
33.884
2.865
0.063
0.547
3.314
0.393
60.060
ROAEDC = ROXBORQ NC WWTP AEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not
Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

Summit Environmental Technologies, Inc.
3310 Win St.
�t14rIPE�liJl41@Nl',hL TL-li9�t+ii7l-C)Cdt S,1N1•;
Anau`�rtltr�l Cal�vxsl�t'te�
January 21, 2019
Nate Roth
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 99&7150
FAX: (336) 99&8450
RE: Roxboro WWTP
Crryahoga Falls, Ohio 44223
TEL: [phone] FAX.• [phone]
Website: http://wwwsettek.com
Dear Nate Roth: Order No.: 19010531
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/10/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-1 l-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 28

Summit Environmental Technologies, Inc, Case Narrative
33I0 Win St.
�N�rl(��tdfi�riTaL TECl�H�L[jC�l� ,, �Ft4;. Cuyahoga Falls, Ohio 44223 WO#: 19010531
.rlfi�fyfr`C.�f L�bdrBrdr��rs TEL: (330% 253-8211 FAX.• [phone]
Website: htto:/hvww.settek.cotn Date: 1/21/2019
CLIENT: Synagro
Project: Roxboro WWTP
WorkOrder Narrative:
19010531: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc.., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19010531-OOlA SVOC-BNA_TCLP(8270d): Possible low bias for Pyridine due to low recovery in
CCV; Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
19010531-OOlA SVOC-BNA TCLP(8270d): Sample exhibited low recovery of Surrogates: 2-
Fluorophenol, Phenol-d6 possibly due to matrix effect.
Analytical Sequence QC Notes:
ccv 250 18712 re svoc-cPEST_npw(8081): CCV exhibits high recovery for endrin. All samples are ND
CCV 40ng 14287 SVOC-MSTR_S(8270): The CCV (Batch R93442) exhibited high recovery for
Hexachlorobutadiene and Pentachlorophenol. The associated samples are ND for the analytes with
Original
Page 2 of 28

IY Summit Environmental Technologies, Inc. Case Narrative
SUMM3310 Win St.
EFWMONPA NTAL TEC3iN(}t_Cfi3JESt INC. Cuyahoga Falls, Ohio 44223 WO#: 19010531
AnMyto'cal t-aboral000s TEL: [phone] FAX: [phone]
Wehsite: http://www.settek.com Date: 1/21/2019
CLIENT: Synagro
Project: Roxboro WWTP
high recoveries.
CCV 40ng 14287 SVOC-MSTR S(8270): The CCV (Batch R93442) exhibited low recovery for
Pyridine. Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Check shows
adequate instrument sensitivity for reporting purposes.
MB-35513 SVOC-BNA_TCLP(8270): MB-35513 exhibited low recovery of Surrogate: 2-Fluorophenol.
MB-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
LCS-35513 SVOC-BNA_TCLP(8270): LCS-35513 exhibited low recovery of Surrogate: 2-
Fluorop6enol.
LCS-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
Original
Page 3 of 28

SUMM111
EPtVIFTONWNTnL T[ClitaDL[ OWS, INC
Anarytical Labaratorles
Summit Environmental Technologies, In
3310 Win 5
Cuyahoga Falls, Ohio 4421
TEL: [phone] FAX: [phone]
Website: h0:11www.settek.co,
Qualifiers and Acronyms
These commonly used Qualifiers and Acronyms mayor may not be present in this report.
Qualifiers
WO#: 19010531
Date: 1/21/2019
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC./+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
W Samples were received outside temperature limits (0' — 6° C). Not Clean Water Act compliant.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
dB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
)CS Quality Control Sample CRQL Contract Required Quantitation Limit
)UP Duplicate FL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 28

SUMMIMF
ENVIrtOtJtilr:NmrALtC-CliNO10C.irS, INC
AnafyfI of iaboraroi as
CLIENT: Synagro
Project: Roxboro WWTP
Lab SampleID Client Sample ID
19010531-001 Roxboro TCLP 2019
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX. [phone]
Website: http:1Avwiv.settekcom
Tag No Date Collected
1/7/2019 2:30:00 PM
Workorder
Sample Summary
WO#: 19010531
Date Received
1/10/2019 10:15:00 AM
21-Tan-19
Matrix
Solid
Page 5 of 28

SUMMIT
ENVI i10AMENTALTECH OLOGIr$,.INC
1.nc�Py�c�c� i�Vs�rr�lr�rJ�4
SummitEnvironmental Technologies, Inc.
3310 Win St,
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.• (330) 2534489
Website: n9pv1/www.settek.com
DATES REPORT
WO#: 19010531
2I-Jan49
Client: Synagro
Project: Roxboro WWTP
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
19010531-OOlA Roxboro TCLP 2019 1/7/2019 2:30:00 PM Solid Ignitability of Solids (SW-846: 1030)
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP
Herbicides Analysis (SW1311/81/10/2019
5:44;59
PM
TCLP
Mercury Analysis (SW1311/7471/10/2019
5:44:59
PM
TCLP
Metals Analysis (SW1311/6010:1/10/2019
5:44:59
PM
TCLP
Pesticides Analysis (SW1311/8(1/10/2019
5:44:59
PM
TCLP Semi-Volafiles Anali
1/10/2019 5:4459 PM
1/11/2019 5:00:00 PM
1/16/2019 11:30:00 A
1/14/2019 8:25:00 AM
1/11/2019 11:00:00 AM
1/17/2019 3:09:04 PM
1/14/2019 11:38:00 AM
1/14/2019 11:08:00 AM
1/18/2019 6:04:00 PM
1/16/2019 4:39:00 PM
1/14/2019 4:13:06 PM
1/11/2019 11:45:00 A 1/16/2019 12:50:00 PM
1/14/2019 10:45:00 A 1/16/2019 1:25:00 AM
Tif
1/10/2019 546:19 PM 1/14If) 019 3606:00 PM
Original
Page 6 of 28

Sunvnit Environmental Technologies, Inc.
SUMM111 3310 Win St,
EPttrIRONN11=WA.L TECliN01 Cl WSf INC Cuyahoga Falls, Ohio 44223
AiTafyt;cal Lataorarortas TEL: [phone] FAX.• [phone]
CLIENT: Synagro
Matrix: SOLID
Lab ID: 19010531-001A
Project: Roxboro WWTP
Client Sample ID Roxboro TCLP 2019
Analyses
Analytical Report
(base report)
WO#: 19010531
Websate: http://ivww.settekcona Date Reported: 1/21/2019
Tag Number:
Collection Date: 1/7/2019 2:30:00 PM
Result RL Qual Units
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00500
DF Date Analyzed
SW7470A SW7470A Analyst: DNS
mg/L 1 1/16/2019 4:39:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 1.25 mg/L 1 1/14/2019 4:13:06 PM
TCLP Barium(Ba) ND 12.5 mg/L 1 1/14/2019 4:13:06 PM
TCLP Cadmium(Cd) ND 0.250 mg/L 1 1/14/2019 4:13:06 PM
TCLP Chromium(Cr) ND 0.500 mg/L 1 1/14/2019 4:13:06 PM
TCLP Lead(Pb) ND 1.25 mg/L 1 1/14/2019 4:13:06 PM
TCLP Selenium(Se) ND 0.125 mg/L 1 1/14/2019 4:13:06 PM
TCLP Silver(Ag) ND 1.25 mg/L 1 1/14/2019 4:13:06 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.0800 mg/L 2 1/16/2019 1:25:00 AM
2,4,5-Trichlorophenol ND 0.200 mg/L 2 1/16/2019 1:25:00 AM
2,4,6-Trichlorophenol ND 0.200 mg/L 2 1/16/2019 1:25:00 AM
2,4-Dinitrotoluene ND 0.0400 mg/L 2 1/16/2019 1:25:00 AM
o-Cresol ND 0.200 mg/L 2 1/16/2019 1:25:00 AM
Wp-Cresol(s) ND 0.200 mg/L 2 1/16/2019 1:25:00 AM
Cresols, Total ND 4.00 mg/L 2 1/16/2019 1:25:00 AM
Hexachloro-1,3-butadiene ND 0.0160 QC+ mg/L 2 1/16/2019 1:25:00 AM
Hexachlorobenzene ND 0.0400 mg/L 2 1/16/2019 1:25:00 AM
Hexachloroethane ND 0.0800 mg/L 2 1/16/2019 1:25:00 AM
Nitrobenzene ND 0.0800 mg/L 2 1/16/2019 1:25:00 AM
Pentachlorophenol ND 0.200 QC+ mg/L 2 1/16/2019 1:25:00 AM
Pyridine ND 0.200 QC- mg/L 2 1/16/2019 1:25:00 AM
Surr: 2-Fluorophenol 5.64 10 - 109 S %Rec 2 1/16/2019 1:25:00 AM
Surr: Phenol-d6 6.56 10 - 109 S %Rec 2 1/16/2019 1:25:00 AM
Surr: Nitrobenzene-d5 45.8 19 - 120 %Rec 2 1/16/2019 1:25:00 AM
Surr: 2,4,6-Tribromophenol 12.5 10 - 120 %Rec 2 1/16/2019 1:25:00 AM
Surr: 2-Fluorobiphenyl 44.0 22 - 117 %Rec 2 1/16/2019 1:25:00 AM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 28

SwnmitEnvironmental Technologies, Inc. Analytical Report
SUMMIT
3310 Win St.EPW1110tWENTAL TECHWOLOC11 S, Cuyahoga Falls, Ohio 44223 (base report)
Arratyb1cai Laboratcrose TEL [phone] F,4X.• [phone] WO#: 19010531
bfl'ebsite: http://ivrvrv,settelc.con7 Date Reported: 1/21/2019
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/7/2019 2:30:00 PM
Lab ID: 19010531-001A
Project: Roxboro WWTP
Client Sample ID Roxboro TCLP 2019
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14 107 34 - 116 %Rec 2 1/16/2019 1:25:00 AM
NOTES:
Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Check shows adequate instrument sensitivity for reporting
purposes.
Sample exhibited low recovery of Surrogates: 2-Fluorophenol, Phenol-d6 possibly due to matrix effect.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND 0.0250 mg/L 10 1/16/2019 12:50:00 PM
Toxaphene ND 0.0500 mg/L 10 1/16/2019 12:50:00 PM
Endrin ND 0.00500 QC+ mg/L 10 1/16/2019 12:50:00 PM
gamma-BHC ND 0,00500 mg/L 10 1/16/2019 12:50:00 PM
Heptachlor ND 0.00500 mg/L 10 1/16/2019 12:50:00 PM
Heptachlor epoxide ND 0,00500 mg/L 10 1/16/2019 12:50:00 PM
Methoxychlor ND 0,00500 mg/L 10 1/16/2019 12:50:00 PM
Surr: TCMX 23.0 10 - 119 %Rec 10 1/16/2019 12:50:00 PM
Surr: DCB 35.0 10 - 119 %Rec 10 1/16/2019 12:50:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: MES
TCLP HERBICIDES ANALYSIS (SW1311/8151)
214-D ND 1.00 mg/L 1 1/18/2019 6:04:00 PM
21415-TP ND 0.500 mg/L 1 1/18/2019 6:04:00 PM
Surr: DCAA 94.6 20 - 140 %Rec 1 1/18/2019 6:04:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst' CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.125 mg/L 25 1/14/2019 3:06:00 PM
1,2-Dichloroethane ND 0.125 mg/L 25 1/14/2019 3:06:00 PM
MEK ND 0.625 mg/L 25 1/14/2019 3:06:00 PM
Benzene ND 0.125 mg/L 25 1/14/2019 3:06:00 PM
Carbon tetrachloride ND 0.125 mg/L 25 1/14/2019 3:06:00 PM
Chlorobenzene ND 0.125 mg/L 25 1/14/2019 3:06:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 8 of 28

IT
Summit Environmental Technologies, Inc. Analytical Report
SUMM3310 Win St.
EPd'.rli?OANI�t4maL rrweiimol Ctti;l fi, rir` Cuyahoga Falls, Ohio 44223 (base report)
Arrafytical Laboratories TEL: [phone] FAX: [phone] WO#: 19010531
Website: http:11ivwiv.settek.con? Date Reported: 1/21/2019
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/7/2019 2:30:00 PM
Lab ID: 19010531-001A
Project: Roxboro WWTP
Client Sample ID Roxboro TCLP 2019
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311 M Analyst: CTB
TCLP VOLATILES ANALYSIS
Chloroform ND 0.125 mg/L 25 1/14/2019 3-106-100 PM
Tetrachloroethene ND 0.125 mg/L 25 1/14/2019 3:06:00 PM
Trichloroethene ND 0.125 mg/L 25 1/14/2019 3-106:00 PM
Vinyl chloride ND 0.0500 mg/L 25 1/14/2019 3:06:00 PM
Surr: 4-Bromofluorobenzene 97.6 70 - 130 %Rec 25 1/14/2019 3-106-100 PM
Surr: Dibromofluoromethane ill 70 - 130 %Rec 25 1/14/2019 3:06:00 PM
Surr: Toluene-d8 103 70 - 130 %Rec 25 1/14/2019 3:06:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.495 mg/Kg 1 1/14/2019 11:38:00 AM
RCI-SOLID-W/ IGNITABILITY1030 SW1030 Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable 1 1/11/2019 11 -1 00-1 00 AM
RCI-SOLID-W/ IGNITABILITY1030 SW9045D Analyst: VVK
PH (SW9045D)
pH 7.0 s.u.@20.3C 1 1/17/2019 3:09:04 PM
RCI-SOLID=W/ IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 1/14/2019 11:08:00 AM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 28

Summit Environmental Technologies, Inc. Accreditation Program
SUMM111 3310 Win St. Analptes Report
ENWROUNI =NTAL Ttt;fiC+�(5I OS, INC Cuyahoga Falls, Ohio 44223 J Y
Analyticai Laboratorios TEL: [phone] FAX: [phone] WO#: 19010531
Website: hgp://www.settek.com 2I4an49
Client: Synagro State: NW
Project: Roxboro WWTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
19010531-001A Solid Ignitability of Solids (SW446: 1030) Ignitability A
Solid pH (SW9045D) Hydrogen Ion (pH) A
Solid Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U
Solid Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Solid TCLP Herbicides Analysis (SW1311/8151) 2A5-TP A
Solid TCLP Herbicides Analysis (SW1311/8151) 254-D A
Solid TCLP Herbicides Analysis (SW1311/8151) DCAA A
Solid TCLP Mercury Analysis (SW1311/7470) Mercury A
Solid TCLP Metals Analysis (SW1311/6010) Arsenic A
Solid TCLP Metals Analysis (SW1311/6010) Barium A
Solid TCLP Metals Analysis (SW1311/6010) Cadmium A
Solid TCLP Metals Analysis (SW1311/6010) Chromium A
Solid TCLP Metals Analysis (SW1311/6010) Lead A
Solid TCLP Metals Analysis (SW1311/6010) Selenium A
Solid TCLP Metals Analysis (SW1311/6010) Silver A
Solid TCLP Pesticides Analysis (SW1311/8081) 2,2',3,3',4,4',5,5'16,6'- A
Decachlorobiphenyl
Solid TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A
Solid TCLP Pesticides Analysis (SW1311/8081) Endrin A
Solid TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A
Solid TCLP Pesticides Analysis (SW1311/8081) Heptachlor A
Solid TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A
Solid TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A
Solid TCLP Pesticides Analysis (SW1311/8081) Tetrachloro-m-xylene A
Solid TCLP Pesticides Analysis (SW1311/8081) Toxaphene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,64ribromophenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorobiphenyl A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorophenol A
Original # 1
Page 10 of 28

- SUMMINt
tes Summit Technologies, Inc. Accreditation Program
3310 Win St. Anal Report
EIVti HIONtdENTAL TECHNOI QGiF5, INC Cuyahoga Falls, Ohio 44223 Y
Anafyticad Laborato6oe TEL: [phone] FAX: [phone] WO#: 19010531
Website: http://www.settek.com 214un49
Client: Synagro State: NW
Project: Roxboro WWTP Program Name: NC WW SCM
Sample ID Matrix Test Name Analyte Status
19010531-001A Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Methylphenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 3,4-Methylphenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene-d5 A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Phenol M A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) p-Terphenyl-dM A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A
Solid TCLP Volatiles Analysis 1,1-Dichloroethene A
Solid TCLP Volatiles Analysis 1,2-Dicbloroethane A
Solid TCLP Volatiles Analysis 2-Butanone A
Solid TCLP Volatiles Analysis 4-Bromofluorobenzene A
Solid TCLP Volatiles Analysis Benzene A
Solid TCLP Volatiles Analysis Carbon tetrachloride A
Solid TCLP Volatiles Analysis Chlorobenzene A
Solid TCLP Volatiles Analysis Chloroform A
Solid TCLP Volatiles Analysis Dibromofluoromethane A
Solid TCLP Volatiles Analysis Tetrachloroethene A
Solid TCLP Volatiles Analysis Toluene-d8 A
Solid TCLP Volatiles Analysis Trichloroethene A
Solid TCLP Volatiles Analysis Vinyl chloride A
Original # 1
Page 11 of 28

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
fflsummly 3310 Win St,
EN4+1ROAhtENTAL I cCHNOLOGIES, JNC" Cuyahoga Falls, Ohio 44223
dnafy0eat Lataaratnr0gs, TEL: [phone] FAX.• [phone] WO#: 19010531
Website: http:11Www.settek.com 214an49
Client: Synagro
Project: Roxboro WWTP
BatchID6 35472
Sample ID MB-35472 SampType: MBLK TestCode: tclp-voc-mstr Units: mg/L Prep Date: 1/10/2019 RunNo: 93332
Client ID: PBS Batch ID: 35472 TestNo: SW8260B SW1311M Analysis Date: 1/11/2019 SegNo: 1903835
Analyte Result
PQL SPK value SPK Ref Val
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
464
Surr: Dibromofluorom ethane
602
Surr: Toluene-d8
496
%REC LowLimit HighLimit RPD Ref Val
500.0
92.8
70
130
500.0
120
70
130
500.0
99.2
70
130
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 12 of 28

mmilu
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIi OAPalEt4TAL IrEECH OLOGI S, DhG� Cuyahoga Falls, Ohio 44223
WO#: 19010531
ArWyr}cal iaboratordets TEL: [phone] FAX.• [phone]
Website: http:Ilwww.settek.com 214an49
Client: Synagro
Project: Roxboro WWTP BatchID: 35523
Sample ID Ics-35523 SampType: LCS TestCode: tclp-svoc-her Units: mg/L Prep Date: 1/11/2019 RunNo: 93601
Client ID: LCSS Batch ID: 35523 TestNo: SW8151A SW8151A Analysis Date: 1/18/2019 SegNo: 1914631
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 78.4
43.8
130
21475-TP
ND
0.500 0.500
0 62.9
51.5
111
Surr: DCAA
357
500.0
71.4
34.2
150
Sample ID mb 35523 SampType: MBLK TestCode: tclp-svoc-her Units: mg/L Prep Date: 1/11/2019 RunNo: 93601
Client ID: PBS Batch ID: 35523 TestNo: SW8151A SW8151A Analysis Date: 1/18/2019 SegNo: 1914632
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
214-D ND 1.00 0 0 d
21415-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 20 140
Sample ID 19010307-001ams SampType: MS TestCode: tclp-svoc-her Units: mg/L Prep Date: 1/11/2019 RunNo: 93601
Client ID: Batch= Batch ID: 35523 TestNo: SW8151A SW8151A Analysis Date: 1/18/2019 SegNo: 1914634
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
214-D ND 1.00 0.500 0 100 37 105 W
214,5-TP ND 0.500 0.500 0 89.8 38 106 W
Sum DCAA 567 500.0 113 20 140 W
Qualifiers: * Value exceeds Maximum Contaminant Level, B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 13 of 28

IT
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St,
SUMM
Er%kVliLOj4NIENTALnCItN€ FOGir.io_q, Nvr! Cuyahoga Falls, Ohio 44223 WO#: 19010531
fn Analydca/ La oratories TEL: [phone] FAX: [phone]
Website: httl2://www.settelc.com 214an49
Client: Synagro
Project: Roxboro WWTP
BatchID6 35523
Sample ID 19010307-001amsd SampType: MSD TestCode: tclp-svoc-her Units: mg/L Prep Date: 1/11/2019 RunNo: 93601
Client ID: Batch= . Batch ID: 35523 TestNo: SW8151A SW8151A Analysis Date: 1/18/2019 SegNo: 1914646
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 83.7
37
105
0 0
30 W
21415-TP
ND
0.500 0.500
0 71.5
38
106
0 0
30 W
Surr: DCAA
453
500.0
90.6
20
140
0
W
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 14 of 28

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
fn summint 3310 Win St,
EN'VIIIOMAENTAL TcC�bra 1C[��o�S, JKC Cuyahoga Falls, Ohio 44223
Anayyt€Cal Labcraiar� es TEL: [phone] FAX.• [phone] WO#: 19010531
Website: http://www.settek.com 214an49
Client: Synagro
Project: Roxboro WWTP
BatchIDa 35549
Sample ID MB-35549 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/16/2019 RunNo: 93469
Client ID: PBS Batch ID: 35549 TestNo: SW7470A SW7470A Analysis Date: 1/16/2019 SegNo: 1909423
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
Sample ID MB2-35549
Client ID: PBS
Analyte
TCLP Mercury
ND 0.00200
SampType: MBLK
Batch ID: 35549
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
ND 0.00500
Prep
Date:
1/16/2019
Analysis
Date:
1/16/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 93469
SegNo: 1909424
%RPD RPDLimit Qual
Sample ID LCS-35549
SampType: LCS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: LCSS
Batch ID: 35549
TestNo:
SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909425
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit
RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00401 0.00200 0.00400
0 100
80 120
Sample ID 19010659-002AMS
SampType: MS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: Batch=
Batch ID: 35549
TestNo:
SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909440
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00468 0.00200 0.00400 0.000380 108
75 125
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 15 of 28

MMIT
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIh O.WelVeITAL C CHNi€]LOGIt5, INC Cuyahoga Falls, Ohio 44223-
�.nalyt/cai LaSorarcrigs TEL: [phone] FAX.- [phone] WO#: 19010531
Website: htW://www.settekcom 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID
19010659-002AMS
SampType:
MS
Client ID:
Batch=
Batch ID:
35549
Analyte
Result
Sample ID
19010659-002AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
35549
Analyte
TCLP Mercury
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
BatchIDa 35549
Prep
Date:
1/16/2019
RunNo:
93469
Analysis
Date:
1/16/2019
SegNo:
1909440
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Prep
Date:
1/16/2019
RunNo:
93469
Analysis
Date:
1/16/2019
SegNo:
1909441
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
0.00462 0.00200 0.00400 0.000380 106 75 125 0.00468 1.29 20
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 16 of 28

MMIT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St,
ENIVIrI ONNIENTAL'rc.CHNO[_GGIF.3, JKC Cuyahoga Falls, Ohio 44223
Ar7afy0caf Lrybcralorles TEL: [phone] FAX: [phone] WO#: 19010531
Website: htW:Ilwww.settelc.com 214an49
Client: Synagro
Project: Roxboro WWTP BatchID: R93297
Ignitability 8.08 7.240 0 112 70 130
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 17 of 28

mmlir
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St.
ENVIRONMENTAL tEOHNOL(4G H75. INC Cuyahoga Falls, Ohio 44223
Arrjl�r[leal Laboratories TEL: [phone] FAX.• [phone] WO#: 19010531
Website: httv://www.settelc.com 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID 19010440-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R93297
Analyte
Result
Sample ID 19010531-001ADUP SampType: DUP
Client ID: Roxboro TCLP 2019 Batch ID: R93297
Analyte
Ignitability
Result
non-flammable
Sample ID
19010532-001ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R93297
Analyte
Ignitability
Result
non-flammable
Sample ID
19010533-001ADUP
SampType:
DUP
Client ID:
Batch=
Batch ID:
R93297
Analyte
Ignitability
Result
non-flammable
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
BatchID0 R93297
Prep Date:
Analysis Date: 1/11/2019
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 1/11/2019
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 1/11/2019
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 1/11/2019
%REC LowLimit HighLimit RPD Rre
ef Val
RunNo: 93297
SegNo: 1902697
%RPD RPDLimit Qual
RunNo: 93297
SegNo: 1902699
%RPD RPDLimit Qual
0 20
RunNo: 93297
SegNo: 1902701
%RPD RPDLimit Qual
0 20
RunNo: 93297
SegNo: 1902703
%RPD RPDLimit Qual
0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 18 of 28

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIT 3310 Win St.
EC�htirl{i WAIENTAL'IrEECH QLOGIES IW" Cuyahoga Falls, Ohio 44223 fflAnd +Aral LabatalorOeg TEL: [phone] FAX* [phone] WO#: 19010531
Website: hU:Ilwww.settelc.com 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID
19010534-001ADUP
SampType:
DUP
Client ID:
Batch=
Batch ID:
R93297
Analyte
Ignitability
Result
non-flammable
Sample ID
19010535-001ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R93297
Analyte
Ignitability
Result
non-flammable
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
BatchID9 R93297
Prep Date:
Analysis Date: 1/11/2019
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 1/11/2019
%REC LowLimit HighLimit RPD Ref Val
91
RunNo: 93297
SegNo: 1902705
%RPD RPDLimit Qual
0 20
RunNo: 93297
SegNo: 1902707
%RPD RPDLimit Qual
0 20
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blanlc
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 19 of 28

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summilu 3310 Win St.
EKWIROWMENTAL rECHNQLCbr15 , 1 ^ Cuyahoga Falls, Ohio 44223
Asps(yOcaf Laborator)e� TEL: [phone] FAX.- [phone] WO#: 19010531
Website: hQ://www.settek com 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID 19010535-01AMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg
Client ID: Batch= Batch ID: R93390 TestNo: SW9014
Analyte Result PQL SPK value SPK Ref Val
Cyanide, Reactive
8.98 0.490 10.00
Sample ID
19010535-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R93390
Analyte
Cyanide, Reactive
Result
I:. � 11�Z'Iic ciZl7
Prep Date:
Analysis Date: 1/14/2019
%REC
LowLimit HighLimit RPD Ref Val
0 89.8 81.6 122
TestCode: Cyanide,Rea Units: mg/Kg
TestNo: SW9014
PQL SPK value SPK Ref Val
9.09 0.495 10.00
Prep Date:
Analysis Date: 111412019
%REC LowLimit HighLimit RPD Ref Val
0 90.9 81.6 122
RunNo: 93390
SegNo: 1906045
%RPD RPDLimit Qual
RunNo: 93390
SegNo: 1906046
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 20 of 28

mmlySummit Environmental Technologies, Inc. QC SUMMARY REPORT
fflsuPORT Win St,
ENVIT OWMENTAL 17ECHNOLGG15 v INC Cuyahoga Falls, Ohio 44223
A.rpa1}�r}cal Labo,raiorapfi TEL: [phone] FAX: [phone] WO#: 19010531
Website: hQ.O11www.settek.com 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID LCS SampType: LCS TestCode: Cyanide,Rea Units: mg/L
Client ID: LCSW Batch ID: R93390 TestNo: SW9014
Analyte Result PQL SPK value SPK Ref Val
Cyanide, Reactive
9.57 0.490 10.00
BatchID: R93390
Prep Date:
Analysis Date: 1/14/2019
%REC LowLimit HighLimit RPD Ref Val
0 95.7 85 115
RunNo: 93390
SegNo: 1906029
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 21 of 28

MMIT
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffl SU3310 Win St,
EhVInOtAIE'NTALTZMLNOLOGIFS, IM't; Cuyahoga Falls, Ohio 44223 WO#: 19010531
Ana(yOcat' Labcralor)efi TEL: [phone] FAX: [phone]
Website: h=:Ilwww.settek.com 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID 19010535-001AMS SampType: MS
Client ID: BatchQC Batch ID: R93465
Analyte
Sulfide, Reactive
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
4210 25.0 4800
Sample ID 19010535-001AMSD SampType: MSD
Client ID: Batch= Batch ID: R93465
Analyte
Sulfide, Reactive
Result
BatchIDa R93465
Prep Date:
Analysis Date: 1/14/2019
%REC LowLimit HighLimit RPD Ref Val
0 87.7 80 120
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
4320 25.0 4800
Prep Date:
Analysis Date: 1/14/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 93465
SegNo: 1908916
%RPD RPDLimit Qual
RunNo: 93465
SegNo: 1908917
%RPD RPDLimit Qual
0 90.0 80 120 4210 2.58 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 22 of 28

MM111
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
IS U3310 Win St,
Ef%�VlitOt4?AlENTALlr�tCH?4€ LDGlt_S,. Jfif" Cuyahoga Falls, Ohio 44223 WO#: 19010531
In Ao8tyr/eat Laboraloaos TEL: [phone] FAX: [phone]
Website: hgp:11www.settek.com 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID MB-R93465
Client ID: PBW
Analyte
Sulfide, Reactive
Sample ID LCS-R93465
Client ID: LCSW
Analyte
Sulfide, Reactive
SampType: MBLK
Batch ID: R93465
Result
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
ND 25.0
SampType: LCS
Batch ID: R93465
Result
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
4
620 25.0 4800
BatchID0 R93465
Prep Date.
Analysis Date: 1/1412019
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 1/14/2019
%REC LowLimit HighLimit RPD Ref Val
0 96.2 85 115
RunNo: 93465
SegNo: 1908902
%RPD RPDLimit Qual
RunNo: 93465
SegNo: 1908903
%RPD RPDLimit C2ual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 23 of 28

�. �� Summit Environmental Technologies, Inc.
ffl 3310 Win St.
E<;kWIRONPal ENTAL I EMMOLGG155; 1N,r. Cuyahoga Falls, Ohio 44223
Ar7a(yrkai LaboratorJes TEL: [phone] FAX: [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Roxboro WWTP BatchID: R93510
pH 7.0 7.0 0 101 90 110
WO#: 19010531
21-Jan49
Sample ID CHECK 7 SampType: LCS TestCode: pH_S(9045D) Units: s.u.@21.00 Prep Date: RunNo: 93510
Client ID: LCSS Batch ID: R93510 TestNo: SW9045D Analysis Date: 1/17/2019 SegNo: 1911706
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0 101 90 110
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 24 of 28

mmlir
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
su3310 Win St,
EN4+I 0APolENTALItC ENOLOGirS, INC Cuyahoga Falls, Ohio 44223
Anal tical taboralorje!; TEL: [phone] FAX.• [phone] WO#: 19010531
Website: http://Www.settek.com 214an49
Client: Synagro
Project. Roxboro WWTP
BatchID0 R93510
Sample ID LCS-R93510 SampType: LCS TestCode: pH_Oil(9045 Units: s.u.@21.6C Prep Date: RunNo: 93510
Client ID: LCSW Batch ID: R93510 TestNo: SW9045D Analysis Date: 1/17/2019 SegNo: 1911010
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0 101 90 110
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 25 of 28

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffl SUMM111 3310 Win St.
lENiVir`tONPilENTALTEiG}6NOLOGiF13; INP. Cuyahoga Falls, Ohio44223 WO#: 19010531
d.natyr)caY LaboralorOvs TEL: [phone] FAX: [phone]
Website: hQ:Ilwww.settek.com 214an49
Client: Synagro
Project: Roxboro WWTP
Sample ID 19010626-004ADUP SampType: DUP
Client ID: BatchQC Batch ID: R93510
Analyte
pH
Result
7.5
TestCode: pH_NPW(450 Units: s.u.@20.1C
TestNo: SW9045D
PQL SPK value SPK Ref Val %REC
BatchID9 R93510
Prep Date:
Analysis Date: 1/17/2019
LowLimit HighLimit RPD Ref Val
RunNo: 93510
SegNo: 1911018
%RPD RPDLimit Qual
7.6 1.1 5 W
Qualif►ers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 26 of 28

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Swm»2it Envi14012127ental Technologies, Lac.
SUMMIT 3310 YVin St.
ENVIRONMENTAL lrl_CHN0LQC;,1r5, +Ne^ Cuyahoga Falls, Ohio 44223
a„i/yt/cai Laboraloelos TEL: [phone] FAX: [phone]
TVebsite: httn:11www.settek.com
Client Name: SYN-NC-27028
Logged by: Rachel Thomas
Work Order Number: 19010531
Sample Log -In Check List
' �` til� ry�MlGrt
Completed By: Christopher Livengood 1/10/2019 2:38:03 PM
Reviewed By: Jennifer Woolf - 2 1/11/2019 9:41:16 AM '71 W+4fl
Chain of Custody
1, Is Chain of Custody complete? Yes No -1 Not Present ❑
2. How was the sample delivered? UPS
RcptNo: 1
1/10/2019 10015:00 AM
Log In
3. Coolers are present? Yes k No ❑ NA ❑
4• Shipping container/cooler in good condition? Yes❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes 0 No ❑ NA ❑
6, Were all samples received at a temperature of >0° C to 6.0°C Yes 0 No ❑ NA ❑
7• Sample(s) in proper container(s)? Yes � No ❑
8. Sufficient sample volume for indicated test(s)? Yes 0 No ❑
9, Are samples (except VOA and ONG) properly preserved? Yes No ❑
10. Was preservative added to bottles? Yes ❑ No V NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials❑
12. Were any sample containers received broken? Yes ❑ No 0
13. Does paperwork match bottle labels? Yes No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes 0 No ❑
15. Is it clear what analyses were requested? Yes 0 No ❑
16. Were all holding times able to be met? Yes 0 No ❑
(If no, notify customer for authorization.)
Special Handlin_g (if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA W
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed_
1
2.1
Good
Not Present
Page 28 of 28

ANNUAL PATHOGEN AND VECTOR ATTRACTION
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (021 Rules)
Facility Name: City of Roxboro WWTP
WWTP Name: Roxboro WWTP
Monitoring Period: From O1/O1/2019
WQ Permit Number: WQ 0021826
NPDES Number: NC 0021024
To 3/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Beta Ray
Class B:
Alt. (1) Fecal Density X
Heat Drying
Gamma Ray
Heat Treatment
Pasteurization
Alt. (2) Process to Significantly Reduce Pathogens
Thermophilic
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaerogeston
bic Dii
Air Drying
Composting
Aerobic Digestion
If annlicable to alternative performed (Class A or Class Bl complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6tn
CFU
382
11478
91667
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x10to the 6"
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Alt, 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) X
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
(Spec.
Option/Alt. 4
02 uptake)
Option/Alt. 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify,
under penalty
of law, that the pathogen requirements
in 40
CFR
503.32/15A NCAC 02T.1106 and the vector attraction
X reduction
requirement in 40 CFR 503.33/15A NCAC 02T.1107
have
been
met."
"I certify, under penalty of law, that Lite pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and
vector attraction reduction requuements have been met. I am aware that there are significant penalties }-or false
certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
Preparer Name and Title
Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* � Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
IM,

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.16S
Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Report Date:
Project:
Date Sample Rcvd:
Page 1
1/17/2019
Roxboro
2019
Meritech Work Order # 01071918 Sample: Roxboro Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 24,0 % 1/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 91,667 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
Meritech Work Order # 01071919 Sample: Roxboro Fecal 1 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2490 % 1/8/19 0"100 % SM 2540B
Fecal Coliform (Sludge) 20,833 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
Meritech Worlc Order # 01071920 Sample: Roxboro Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 212 % 1/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 47,414 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
Meritech Work Order # 01071921 Sample: Roxboro Fecal 1 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% TotaI Solids 218 % 1/8/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 382 col/g drywt 1/7/19 258 col/g dry wt SM 9222D
Meritech Work Order # 01071922 Sample: Roxboro Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2397 % 1/8/19 0400 % SM 2540E
Fecal Coliform (Sludge) 1,151 col/g drywt 1/7/19 258 col/g drywt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Report Date:
Project:
Date Sample Rcvd:
Page 2
1/17/2019
Roxboro
2019
Meritech Worlc Order # 41471923 Sample: Roxboro Fecal 1 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 22.9 % 1/8/19 0=100 % SM 2540B
Fecal Coliform (Sludge) 26,201 col/g dry wt 1/7/19 252 col/g dry wt SM 9222D
Meritech Work Order # 41071924 Sample: Roxbora Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 23.9 % 1/8/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 25,105 col/gdrywt 1/7/19 228 col/gdrywt SM 9222D
I hereby certify that I have reviewed and approve these data.
Representative
642 Tamco Road, Reidsville, North Carolina Z7320
tel,(336}342-4748 fax.{336)342-15ZZ

8/9/18
Chain of Custodv Record
ENVIRONMENTAL
•A LABORATORIES
. •. 4748
Emailm .•
Sampling Dates &Times
Sample location and/or ID # Start I End
Date I Time I Date I Time
N PDES#:
Client: v Phone:
�7 Address: 1'..�' ,''- Feet Fax:
Emailp
Project:�i���' -- --
P.O.#:
How would you like your report sent?
Circle all that apply: F,r6ail(4referred), Fax, Mail
Comp? # of
Grrab? Cont.
L•.='
estk) Req u 1
T-'
Turn Around Time*
*RU5H work needs prior approval,
Std (10 days! 13 -
Lab Ilse Clnly
On Ice? pH OK?
Yes I No Cl OK?
Temperature Upon
IVIethOd Of *** Dechlorination (<O.S ppm} of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** `'�•
Comments: Compositor #
Shipment:
UPS Jug #
Fed Ex Are these results for regulatory purposes? Yes 01 No Report results in: mg/Li: mg/kg ug/L`
Relinquished by: 1 c;, Date: Time: Recei d hy: Date: Time:
Hand Delivery
other Relinquished by: Date: Time: Rec ved by: ate: Tithe:
Relinquished by: Date: Time: Recei b b: i LVe ( r) Time:

Lab result Log
91667 4096
20883 4032
47414 4068
382 2058
1151 3,06
26201 4,42
25105 4,40
Average 4.06
FECAL DATA SHEET
Min
Max
Geometric Mean
382
91667
11478

20IV
503 VECTOR ATTRACTION
This is our worksheet showing that in using the 503,33(b)(option3) that we are within the vector attraction reduction limit of 15%
Reduction
Formula
In - (In x Out)
-.010
.58 - .24
-0.01
.36
-.028 x 100 Q
In - (In x Out) -
,64- (.64 x .65) -
,64 - ,42 -
.22 - -,045 x
In -Out n
.58 - .60 n
-,020 n
-0.03 n
In - (In x Out)
.58- (. 58 x .60)
,58 - .35
,230 -0.13 x
0
Reduction
-2.8 First Quarter
-4.6 Second Quarter
100 � -13.0 Third Quarter
-8.7 Fourth Quarter
2019
2019
2019
2019

DIGESTER
"COOLER"
SLUDGE
ROXBORO WWTP LAB
TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 25406 and 2540E
Analyst: Nicki Dalton, Crystal Shotwell
DATE / TIME
OF
TEST
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH + WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
(Total)
Time
In
Oven
(Total)
Time
Out
Oven
WEIGHT
DISH + DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
(grams)
WEIGHT
VOLATILE
SOLIDS
(grams)
%
VOLATILE
SOLIDS
(Volatile)
Time
In
Oven
(Volatile)
Time
Out
Oven
ANALYST
INITIALS
RPD's
if Needed
10/1/2019
10/1/2019
7
35
82.4126
117.1204
34.7078
9:43 AM
10:43 AM
82.4116
-.0010
Blank
82,4121
-.0005
Blank
11:20 AM
12:20 PM
ND
8:20 AM
10/1/2019
8
35
77.8688
112,3689
34,5001
9:43 AM
10:43 AM
78.1506
.2818
0.82
77.9804
.1702
60
11:20 AM
12:20 PM
ND
0%
10/1/2019
5
1 35 1
77.8271
112.1130
34.2859 1
9:43 AM
10:43 AM
78.1087
.2816
0.82 1
77.9395
.1692
60 1
11:20 AM
12:20 PM
ND
10/8/2019
10/8/2019
7
35
82,4118
115.7411
33.3293
8:57 AM
9:57 AM
82.4117
-.0001
Blank
82.4117
.0000
Blank
11:10 AM
12:10 PM
ND
7:10 AM
10/8/2019
8
35
77,8680
111,3668
33,4988
8:57 AM
9:57 AM
78.1043
.2363
0.71
77.9557
.1486
63
11:10 AM
12:10 PM
ND
0%
10/8/2019
5
35
77.8264
111.2203
33.3939
8:57 AM
9:57 AM
78.0620
.2356
0.71
77.9136
.1484
63
11:10 AM
12:10 PM
ND
10/15/2019
10/15/2019
7
35
82.4124
117,2827
34.8703
8:25 AM
9:25 AM
82.4120
-.0004
Blank
82.4117
.0003
Blank
10:30 AM
11:30 AM
ND
6:32 AM
10/15/2019
8
35
77.8691
111.5977
33.7286
8:25 AM
9:25 AM
78,0947
.2256
0.67
77,9522
.1425
63
10:30 AM
11:30 AM
ND
0%
10/15/2019
5
35
77.8272
111.9440
34.1168
8:25 AM
9:25 AM
78.0559
.2287
0.67
77.9116
.1443
63
10:30 AM
11:30 AM
ND
10/22/2019
10/22/2019
7
35
82.4133
117.9999
35.5866
7:47 AM
8:47 AM
82.4129
-.0004
Blank
82.4125
.0004
Blank
9:53 AM
10:53 AM
ND
6:27 AM
10/22/2019
8
35
77.8706
112.5698
34.6992
7:47 AM
8:47 AM
78,0880
.2174
0.63
77.9496
.1384
64
9:53 AM
10:53 AM
ND
0%
10/22/2019
5
35
77.8284
112,0036
34,1752
7:47 AM
8:47 AM
78,0422
.2138
0.63
77,9064
.1358
64
9:53 AM
10:53 AM
ND
10/29/2019
10/29/2019
7
35
82.4129
118.2713
35.8584
8:30 AM
9:30 AM
82.4125
-.0004
Blank
82.4122
.0003
Blank
10:35 AM
11:35 AM
ND
6:18 AM
10/29/2019
8
35
77.8705
111.4256
33.5551
8:30 AM
9:30 AM
78.0737
.2032
0.61
77.9466
.1271
63
10:35 AMV12:OO
ND
0%
10/29/2019
5
35
77.8283
111.4990
33.6707
8:30 AM
9:30 AM
78.0316
.2033
0.60
77.9045
.1271
63
10:35 AM
ND
11/6/2019
11/6/2019
7
35
82.4119
116.7761
34.3642
8:45 AM
9:45 AM
82.4114
-.0005
Blank
82.4116
-.0002
Blank
11:00 AM
ND
6:00 AM
11/5/2019
8
35
77.8698
111.8033
33.9335
8:45 AM
9:45 AM
78.0690
.1992
0.59
77.9447
.1243
62
11:00 AM
:
ND
0%
11/5/2019
5
35
77,8274
112.8232
34,9958
8:45 AM
9:45 AM
78,0336
.2062
0.59
77.9051
.1285
62
11:00 AM
12:00 PM
ND
VSR
0
x - Blank
2019 (Fourth Quarter) VECTOR ATTRACTION CALCULATIONS

ANNUAL PATHOGEN AND VECTOR ATTRACTION
Facility Name.
WWTP Name:
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
of Roxboro WWTP
Roxboro WWTP
Monitoring Period: From
WQ Permit Number. WQ 0021826
NPDES Number: NC 0021024
04/01/2019 To 06/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaeroc geston
biDii
Air Drying
Composting
Aerobic Digestion
Tf annlirahle to alternative nerfnrmed (Glace A nr Class Rl cmm�lete the following monitorinL data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10to the 6th
CFU
347
643
6,749
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x10 to the 6th
CFU
CFU/g
power per gram of
total solids I solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/1
(VS reductioAlt. n)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench) .
Option/Alt2
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) X
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
(Spec.
Option/Alt. 4
02 uptake)
Option/Alt, 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties for false
certification including fine and imprisonment."
Derek Clayton WWTP Superintendent
Preparer Name and Title Land Applier Name and Title (if applicable) (type or print)
% Gam--, 2
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
MocksviIle, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Dafie Sample Rcvd:
Page 1
6/14/2019
Roxboro
2019
Meritech Work Order # 06051950 Sample: Roxboro Fecal 2 of 4 Grab 6/5/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 26.2 % 6/7/19 0A00 % SM 2540B
Fecal Coliform (Sludge) 347 col/g dry wt 6/5/19 228 col/g dry wt SM 9222D
Meritech Work Order # 06051951 Sample; Roxboro Feca12 of 4 Grab 6/5/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 22.9 % 6/7/19 0400 % SM 2540B
Fecal Coliform (Sludge) 6,749 col/g dry wt 6/5/19 228 col/g dry wt SM 9222D
Meritech Worlc Order # 06051952 Sample: Roxboro Fecal 2 of 4 Grab 6/5/19
Parameters Results Analysis Date Reportinng„Limit Method
% Total Solids 215 % 6/7/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <404 col/g dry wt 6/5/19 404 col/g dry wt SM 9222D
Meritech Work Order # 06051953 Sample: Roxboro Fecal 2 of 4 Grab 6/5/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 253 % 6/7/19 0400 % SM 2540B
Fecal Coliform (Sludge) <354 col/g dry wt 6/5/19 354 col/g dry wt SM 9222D
Meritech Work Order # 06Q51954 Sample: Roxboro Fecal 2 of 4 Grab 6J5/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 22.2 % 6/7/19 0400 % SM 2540B
Fecal Coliform (Sludge) <410 col/g dry wt 6/5/19 410 cal/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone]$1'ax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Report Date:
Project;
Date Sample Rcvd:
Meritech Worlc Order # 06051955 Sample: Roxboro Fecal Z of 4 Grab
Parameters Results Analysis Date Reporting Limit
% Total Solids 23.5 % 6/7/19 0400 %
Fecal Coliform (Sludge) 774 col/g dry wt 6/5/19 2Z8 col/g dry wt
Page 2
6/14/2019
Roxboro
2019
6/5/19
Method
SM 2540B
SM 9222D
Meritech Worl� Order # 06051956 Sample: Roxboro Fecal 2 of 4 Grab 6/5/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 21,3 % 6/7/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <427 col/g dry wt 6/5/19 427 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory
642 Tamca Road, Reidsville, Narth Carolina 27320
tel.[phone] fax.(336)34Z-15ZZ

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Lab result Log
347 2.54
6749 3,83
404 2461
354 2055
410 2061
774 2089
427 2063
Average 2.81
FECAL DATA SHEET
Min
Max
Geometric Mean
347
6749
643

ANNUAL PATHOGEN AND VECTOR ATTRACTION
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period
of Roxboro WWTP
WQ Permit Number:
Roxboro WWTP NPDES Number:
From 07/O1/2019 To 09/30/2019
0021826
NC 0021024
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Beta Ray
Class B:
Alt. (1) Fecal Density X
Heat Drying
Gamma Ray
Heat Treatment
Pasteurization
Alt. (2) Process to Significantly Reduce Pathogens
Thermophilic
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaeroon
bic Digesti
Air Drying
Composting
Aerobic Digestion
If annlicable to alternative performed (Class A or Class Bl complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6th
CFU
316
351
380
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x10 to the 61h
CFU
CFU/g
power per gram of
total solids I solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Mt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) X
Option/Alt. 3
Option/Alt. 7
(Drying —Stable)
(Spec.
Option/Alt. 4
02 uptake)
Option/Alt, 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties }'or false
certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
,�Pr�eparer Name and Title Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Environmental Laboratory
Laboratory Certification No.165
Page 1
Report Date: 8/16/2019
Project: Roxboro WWTP
Date Sample Rcvd: 8/7/2019
Meritech Worlc Order # 080719Q5 Sample: Roxboro Fecal 1 Grab 8 j7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 27.2 % 8/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <334 cal/g dry wt 8/7/19 334 col/g dry wt SM 9222D
Meritech Worl� Order # 08071906 Sample: Roxboro Fecal 2 Grab 8/7/19
Parameters Results Analysis Date Reporting Limit Method
Total Solids 25.2 % 8/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) <361 col/g dry wt 8/7/19 361 col/g dry wt SM 9222D
Meritech Work Order # 08071907 Sample: Roxboro Feca13 Grab 8/7J19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 28.8 % 8/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 316 col/g dry wt 8/7/19 228 col/g dry wt SM 9222D
Meritech Work Order # 08fl719Q8 Sample: Roxboro Fecal 4 Grab 8/7/19
Parameters Results Analysis Date Reporting -Limit Method
% Total Solids 24.5 % 8/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <371 col/g dry wt 8/7/19 371 col/g dry wt SM 9222D
Meritech Work Order # 08071909 Sample: Roxboro Feca15 Grab 8/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 25A % 8/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) <358 col/g dry wt 8/7/19 358 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, NorCh Carolina 27320
tel.[phone] fax.[phone]

r,
%i
EN
-111
Contact: jan Copeland
CIient: Synagro
284 Boger Road
Mocksville, NC 27028
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project;
Date Sample Rcvd:
Page 2
8/16/2019
Roxboro WWTP
8/7/2019
Meritech Worlc Order # 08071910 Sample: Roxboro Fecal 6 Grab 8 J7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 26.6 % 8/8/19 0,100 % SM 2540B
Fecal Coliform (Sludge) <342 col/g dry wt 8/7/19 342 col/g dry wt SM 9222D
Meritech Worlc Order # 08071911 Sample: Roxboro Fecal 7 Grab 8/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 23.9 % 8/8/19 0"100 % SM 2540E
Fecal Coliform (Sludge) <380 col/g drywt 8/7/19 380 col/g dry wt SM 9222D
1 hereby certify that 1 have reviewed and approve these data.
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

8/9)78
Chain of Custody Record (COC)
client:`
NPDES#:
Phone*
MERITECHINC.
d
JI'
Address: � , e t-�`CL 6` oito
Fax:
ENVIRONMENTAL LABORATORIES
1 �ir�S iu.0 N�
Email: CLCOCOLAi#�+7
S"A;461to..io 140
642 Tamco Rd. Phone: [phone]
Project: Z1, 'r..o W u TIP
Reidsville NC 27320 Fax: [phone]S22
P.O.#:
Email: [e-mail]
Attention: �`�4N t 21 O
Turn Around Time*
*RUSK work needs prior approval,
Haw would you like your report
sent?
iarges Anniv
www.meritechiabs.com
Circle all that apply Ema' (preferred),
Std 10 s) 3-5 Da s 24-48Hrs
Fax, Mail a
E
Sampling Dates & Times
Person Taking Sample (Sign/Print):
Lab use only
Sample Location and/or ID #
Start
End
Comp?
#of
Test(s) Required
On Ice?
pH OK?
Time
Date
Time
Grab?
Cont.
e/'No
Cl OK?
=��7l�Sax
q•zio
��t�Z- C3
� iD
ID
CAP
Temperature Upon
Receipt•
*** Dechlorination (<0.5 Ammonia, Cyanide, Phenol TKN
be done "**
Method of
ppm) of
and samples
must in the field prior
to preservation.
Comments:
Compositor #
Jug #
Shipment.
UPS
Fed Ex
Are these results for regulatory purposes? Yes
Imo,
No
Report results in:
mg/� ;
mg/kg ' ug/L
Hand Delivery
Relinquished by: y Date: a. ..ju
Zai„ ,c 1
Time: r �.
i g .
Received by:
Date: Time:
QOther
Relinquished by: Date:
Time:
Received by:
Date: Time:
Relinquished by: Date: Time:
Rece
D t yrge:<

Lab result Log
334 2052
361 2.56
316 2050
371 2057
358 2055
342 2053
380 2058
Average 2.55
FECAL DATA SHEET
Min 316
Max 380
Geometric Mean 351

ANNUAL PATHOGEN AND VECTOR ATTRACTION
Facility Name:
WWTP Name:
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
City of Roxboro WWTP WQ Permit Number:
Roxboro WWTP
NPDES Number
Monitoring Period: From 10/O1/2019 To 12/31/2019
0021826
NC 0021024
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaero
Air Drying
Composting
Aerobic Digestio
If apnlicable to alternative nerformed (Class A or Class Bl complete the following monitorine data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61'
CFU
221649
321511
421320
CFU/g
0
4/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU
CFU/g
2x10 to the 6tn
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) . X
(Spec.
were performed
No vector attraction reduction alternatives
"I certify,
under penalty
of law, that the pathogen requirements
in 40
CFR
503.32/15A NCAC 02T.1106 and the vector attraction
X reduction
requirement in 40 CFR 503.33/15A NCAC 02T.1107
have
been
met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties }.or false
certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
Preparer Name and Title
Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* I Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
Page 1
11/19/2019
Roxboro
11/6/2019
Meritech Work Order # 11061984 Sample: Roxboro 1 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 19.7 % 11/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 304,569 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061985 Sample: Roxboro 2 Grab
Parameters Results Analysis Date
% Total Solids 19.7 % 11/8/19
Fecal Coliform (Sludge) 284,264 col/g dry wt 11/6/19
Reporting Limit Method
0-100 % SM 25408
508 col/g dry wt SM 9222D
Meritech Work Order # 11061986 Sample: Roxboro 3 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 19.7 % 11/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 299,492 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061987 Sample: Roxboro 4 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 19A % 11/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 221,649 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 110619$8 Sample: Roxboro 5 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 19.5 % 11/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 374,359 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date
Project:
Date Sample Rcvd:
Page 2
11/19/2019
Roxboro
11/6/2019
Meritech Work Order # 11061989 Sample: Roxboro 6 Grab 11/6/19
Parameters Results Analvsis Date Reporting Limit Method
% Total Solids 19A % 11/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 391,753 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061990 Sample: Roxboro 7 Grab
Parameters Results Analysis Date
% Total Solids 19.7 % 11/8/19
Fecal Coliform (Sludge) 421,320 col/g drywt 11/6/19
I hereby certify than have reviewed and approve these data.
Reporting Limit Method
0-100 % SM 2540B
494 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.(336)34Z-1522

8�9�18 Chain of Custody Record (COC) C� n NPDES#:
MERITE Client: ✓rT�(ZiJ Phone:��(a"�L�%-��C�
C H1 I N C' Address: ,� DUN Bocce _ a24n Fax:
ENVIRONMENTAL LABORATORIES IMi�LI«�l�.r_r �- EmaillcoPG� wo C ��IfiQ�4- )'60,�
642Tamco Rd. Phone: [phone] Project: ► 0'yD�
Reidsville NC 27320 Fax: [phone]
Email: [e-mail] n Turn Around Time*
Attention: 2Y(Fc� �: �( AfS� *RUSH work needs prior approval,
How would you li t? your report sent? Char es A I
www.meritechlabs.com Circle all that apply: Em 1(preferred), Fax, Mail Stcl 1"a s) 3-5 Da s 24-48Hrs
Sampling Dates & Times Person Taking Sample (Sign/Print): ny n Sample Location and/or ID # Lab Use Only
art End
Comp? #of Test(s) Required On Ice? pH OI<?
Date Time Date Time Grab? Cont. Yes / No Cl OK?
Y,i,,
5
�p,�p r Cu
Temperature Upon
Receipt:
Method of *** Dechlorination 1<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** 1 i
Shipment: Comments: Compositor #
❑ UPS
Jug #
❑ Fed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Relinquished by: Date: ' /C Time: ) Received by: Date: Time:
r)C
Hand Delivery _ j
❑ Other Relinquished by: Date: Time: Received by: Date: Time:
Relinquished by: Date: Time: Receiv y L b: f ,) t Time:;

Lab result Log
304569 5,48
284264 5,45
299492 5,48
2211649 5,35
374359 5,57
391753 5,59
421320 5,62
Average 5051
FECAL DATA SHEET
Min
Max
Geometric Mean
221649
421320
321511

Agricultural Lime Application Log
Year. 2019
Project: Roxboro
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date Applied
NC-PS-24-01
5.8
0.2 tons/ac.
.5T/Acre
Ordered
NC-PS-24-02
4.9
1.1 tons/ac.
1.2T/Acre
Ordered
NC-PS-24-03
6.1
0.0 tons/ac.
NC-PS-25-1A
6A
0.0 tons/ac.
NC-PS-25-1 B
6.2
0.0 tons/ac.
NC-PS-25-2
5.5
0.5 tons/ac.
.5T/Acre
Ordered

Page 1 of 1
Report No: 19-347-0527
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
ivaypol t..
ANALYTICAL
Client: Ronnie Carver
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: PS-24
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12/16/2019
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-I Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NOIN
21381 Fid 1-3 PS-24-1 MIN 0.6 5.8 70.0 232 11 37 113 398 398 145 72.8 4 3 1 0.2 0.1
21382 Rd 1-3 PS-24-2 MIN 1.1 4.9 70.0 250 11 44 194 588 588 275 72.1 3 2 1 0.1 0.1
21383 Rd 1-3 PS-24-3 MIN 0.8 6.1 70.0 192 11 31 131 243 243 125 73.0 4 3 1 0.1 0.1
Comment:
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-347-0525
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Lab No Field lD .Sample ID
21376 Fld 1-2 PS-25-1A
21377 Rd 1-2 PS-25-18
21378 Fld 1-2 PS-25-2
Comment:
Maypoint M
ANALYTICAL
Client: Paul Bailey
Soil Class HM% W/V pH Ac P-I
MIN 0.8 6.4 70.0 82
WO 4.7 6.2 70.0 137
MIN 0.6 5.5 70.0 80
2850 Daisy Lane, Wilson, NC 27896
Main 252-2064721 ° Fax [phone]
wwwowaypointa na lytica l.com
Farm: PS-25
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12/16/2019
Mn-1 Zn-1 Zn-AI Cu-I CEC BS% Ca% Mg% ESP Na SS-1 NO N
14 31 1600 293 293 330 76.3 8 6 2 0.1 0.1
13 29 238 318 397 425 76A 8 6 2 0.1 0.1
27 35 94 218 218 215 76.8 9 5 3 0.1 0.1
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are pertormed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.