WQ0011244_Residual Annual Report 2019_20200226

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/26/2020
Received:*
Project Number* WQ0011244
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0011244
Applicant\Permittee * Synagro
Facility Name * city of Oxford
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Oxford 2019 Annual Report
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
OXFORD NC 2019 Annual Report FINAL.pdf 29.04MB
Upload only 1 RDF document. NL@iple documents must be combined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/21/2020

435 Williams Court, Suite 100
Baltimore, MD 21220
www—syilagro.coin
FEBRUARY 21, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0011244
Dear NCDEQ:
SYNAGRO
Synagro is submitting 1 copy and 1 electronic copy of the above referenced report on behalf of
the City of Oxford, NC.
If you have any questions or need additional information, please do not hesitate to contact Amy
Ratliff at [phone] or Ryan Copeland at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Amy Ratliff, City of Oxford
Ryan Copeland, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF OXFORD, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0011244
2019 ANNUAL REPORT

City of Oxford, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0011244 County Granville Year 2019
Facility Name (as shown on permit) City of Oxford WWTP NPDES No. NC0025054
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summary:
Total number of application fields in the permit: 26
Total number of fields utilized for land application during the year: 14
Total amount of dry tons applied during the year for all application sites: 733.83
Total number of acres utilized for land application during the year: 286.4
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
143 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C —Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."A��T Do+1;4T Pif�r P"�;"PAr A,,, n
� TU 1 Z1,tillfy-o
an
d Titl
pe or print)
arer*
Permittee)
Signature ofPrep
(if different from
Signature of
(if different
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
OXFORD, NC
OXFORD, NC AEROB. DIGESTED LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
April 2019 551,800.00 G 80.54 D 73.05
May 2019 620,000.00 G 90.48 D 82.07
June 2019 725,400,00 G 105.87 D 96.03
August 2019 2,424,200.00 G 367.84 D 333.63
September 2019 5277000600 G 25.95 D 23.51
October 2019 6631400400 G 32.64 D 29.61
November 2019 620,000.00 G 30.51 D 27.66
YEARLY TOTAL 6,131, 800.00 G 733.83 D 665.56
1 /30/2020

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0011244
Facility Name: OXFORD, NC
NPDES# : NCO025054
or WQ# (residual only)
WWTP Name: OXFORD
Residuals Analysis Data
Product Type
Date Sampled (grab) or
Date Composited
Percent Solids
Laboratory
PACE ANALYTICAL SERVICE INC.
Waypoint Analytical Virginia Inc.
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
01/07/19
07/24/19
09/11/19
11/06/19
3.50
4.17
1.18
3.56
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
<1.7
0.66
NR
393
0.843
57.6
<1
295
0.363
467
<1
56
<2.78
0.55
52.2
461
23.2
11.7
15.5
<17.4
1880
20.2
8.33
1901
1550
<5
25.6
10.4
12.8
1450
<5
33.9
8.94
17.6
<13.9
1820
24300
16400
19100
20300
62000
67900
74200
59400
13200
11900
22500
13600
<56.7
<4.76
<4.74
<128
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalty for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF PI�PARER)
Date 2/1 Z
DENR FORM RSSF (5/2003) Printed: Saturday - February 1, 2020 at 15:54:34 for: 2049 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0011244
Facility Name: OXFORD, NC
NPDES# . NCO025054
or WQ# (residual only)
WWTP Name: OXFORD
Residuals Analysis Data
Product Type AEDLIQ
Date Sampled (grab) or 01/07/19
Date Composited
Percent Solids
PARAMETERS (mg/kg dry weight)
Aluminum
Calcium
Magnesium
pH
Potassium
Sodium
Laboratory
PACE ANALYTICAL SERVICE INC.
Waypoint Analytical Virginia Inc.
AEDLIQ AEDLIQ AEDLIQ
07/24/19 09/11/19 11/06/19
3.50 4.17 1.18 3.56
55600
48000
47100
54700
17500
15500
15300
15400
3700
3140
3940
4560
7.40
<8700
7.50
2660
7.20
3780
7.70
2920
<8700
1350
4720
2310
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
TURF OF PREPARER)
NR -Data Not Reported or Data Not Required
Date
DENR FORM RSSF-B (7/2002) Printed: Saturday -February 1, 2020 at 15:55:48 for: 2049 01

Analytical
www.pacelabs.com
January 15, 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: Oxford VWVfP 1/7/19
Pace Project No.: 92413357
Dear Nate Roth:
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for samples) received by the laboratory on January 08, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254J176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
out the written consent of Pace Analytical Services, LLC.
Page 1 of 16

Project:
Analytical
www.pacelabs.com
Oxford WWTP 1/7/19
Pace Project No.: 92413357
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent 01 Pace Analytical Services, LLC. Page 2 of 16

Analytical
www.pacelabs.cnm
Project:
Pace Project No.
Oxford WWiP 1/7/19
92413357
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92413357001 Oxford 1 of 4 EPA 6010D
DS
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D �
SMK
1
PASI-A
SM 2710B-2011
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 16

Analytical
www.pacelabs.com
Project:
Pace Project No.:
Oxford VVVVfP 1/7/19
92413357
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Oxford 1 of 4
Lab ID:
92413357001 Collected: 01/07/19 13:30
Received: 01/08/19 12:45 Matrix: Solid
Results reported on a "dry
weight" basis and are
adjusted for percent moisture, sample size
and any dilutions.
Parameters
Results
Units Report Limit DF
Prepared Analyzed CAS Nc
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7471 Mercury
Mercury
2540G Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 6010D Preparation Method: EPA 30508
Qual
55600
mg/kg
174
1
01/11/19
09:20
01/13/19
22:24
7429-90-5 M1
ND
mg/kg
17.4
1
01/11/19
09:20
01/13/19
22:24
7440-38-2
ND
mg/kg
1.7
1
01/11/19
09:20
01/13/19
22:24
7440-43-9
17500
mg/kg
174
1
01/11/19
09:20
01/13/19
22:24
7440-70-2
393
mg/kg
8.7
1
01/11/19
09:20
01/13/19
22:24
7440-50-8
23.2
mg/kg
8.7
1
01 /11
/19
09:20
01 /13/19
22:24
7439-92-1
3700
mg/kg
174
1
01/11/19
09:20
01/13/19
22:24
7439-95-4
11.7
mg/kg
8.7
1
01/11/19
09:20
01/13/19
22:24
7439-98-7
15.5
mg/kg
8.7
1
01/11/19
09:20
01/13/19
22:24
7440-02-0
ND
mg/kg
8700
1
01/11/19
09:20
01/13/19
22:24
7440-09-7
ND
mg/kg
17.4
1
01/11/19
09:20
01/13/19
22:24
7782-49-2
ND
mg/kg
8700
1
01/11/19
09:20
01/13/19
22:24
7440-23-5
1880
mg/kg
17.4
1
01/11/19
09:20
01/13/19
22:24
7440-66-6 BC
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
0.66 mg/kg 0.11 1 01/11/19 21:31 01/14/19 12:13 7439-97-6
Analytical Method: SM 2540G-2011
3.5 % 0.000010 1 01/10/1913:28
Analytical Method: ASTM D2974-87
96.5 % 0.10 1 01/10/1913:19
Analytical Method: EPA 9045D
7.4 Std. Units 0.10 1 01/15/19 10:57 H3
Analytical Method: SM 2710E-2011
21200
mg/kg
0.12 1
01/15/1911:49 N2
Analytical Method:
EPA 350.1
Rev 2.0 1993 Mod. Preparation Method:
EPA 350.1 Rev 2.0 1993 Mod.
13200
mg/kg
255 1 01/12/1910:40
01/12/1915:12 7664-41-7 M6
Analytical Method:
EPA 351.2
Rev 2.0 1993 Preparation Method: EPA
351.2 Rev 2.0 1993
62000
mg/kg
2380 2 01/14/19 11:34
01/15/19 05:51 7727-37-9 M1
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
ND
mg/kg
56.7
1
01/10/19
01:57
01l10/19
03:44
ND
mg/kg
56.7
1
01/10/19
01:57
01/10/19
03:44
14797-55-8
ND
mg/kg
28.3
1
01/10/19
01:57
01/10/19
03:44
14797-65-0
Analytical Method:
EPA 365.1
Rev 2.0 1993
Preparation
Method:
EPA 365.1
Rev
2.0
1993
24300
mg/kg
1320 25
01/09/1920:23
01/10/1914:59
7723-14-0 M6
Date: 01/15/2019 01:37 PM
REPORT OF LABORATORYANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 16

Analytical
www.pacelabs.com
Project: Oxford VW1rfP 1/7/19
Pace Project No.: 92413357
QC Batch: 452089
QC Batch Method: EPA 7471 B
Associated Lab Samples: 92413357001
METHOD BLANK: 2472136
Associated Lab Samples: 92413357001
Parameter
Mercury
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Solid
EPA 7471 B
7471 Mercury
Blank Reporting
Units Result Limit Analyzed
mg/kg ND 0.0060 01/14/1912:06
LABORATORY CONTROL SAMPLE: 2472137
Parameter Units
Mercury mg/kg
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Spike LCS LCS %Rec
Conc. Result %Rec Limits Qualifiers
0.083 0.067 81 80-120
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2472138
MS
92413378001 Spike
Parameter Units Result Conc.
Mercury mg/kg 0.0063 0.055
2472139
MSD
Spike MS
Conc. Result
0.057 0.048
MSD MS MSD %Rec
Result %Rec %Rec Limits RPD
0.049 75 75 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Qual
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 16

Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Oxford WWi'P 1/7/19
Pace Project No.: 92413357
QC Batch: 451935 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92413357001
METHOD BLANK: 2471114
Associated Lab Samples: 92413357001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed Qualifiers
Aluminum
mg/kg
ND
10.0
01/13/19
22:18
Arsenic
mg/kg
ND
1.0
01/13/19
22:18
Cadmium
mg/kg
ND
0,10
01/13/19
22:18
Calcium
mg/kg
ND
10.0
01/13/19
22:18
Copper
mg/kg
ND
0,50
01/13/19
22:18
Lead
mg/kg
ND
0.50
01/13/19
22:18
Magnesium
mg/kg
ND
10.0
01/13/19
22:18
Molybdenum
mg/kg
ND
0.50
01/13/19
22:18
Nickel
mg/kg
ND
0,50
01/13/19
22:18
Potassium
mg/kg
ND
500
01/13/19
22:18
Selenium
mg/kg
ND
1.0
01/13/19
22:18
Sodium
mg/kg
ND
500
01/13/19
22:18
Zinc
mg/kg
ND
1.0
01/13/19
22:18 BC
LABORATORY CONTROL SAMPLE:
Parameter
2471115
Units
Spike
Conc.
LCS
Result
LCS
% Rec
%Rec
Limits
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE &MATRIX
SPIKE DUPLICATE:
2471116
2471117
MS
MSD
92413357001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc,
Result
Result
% Rec
% Rec
Limits
RPD Qua]
Aluminum
mg/kg
55600
9280
8310
69300
63600
148
96
75-125
9 M1
Arsenic
mg/kg
ND
928
831
827
734
89
88
75-125
12
Cadmium
mg/kg
ND
928
831
848
758
91
91
75-125
11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16

Analytical
www.pacela6s.com
Project:
Pace Project No.:
Oxford VW1ffP 1/7/19
92413357
MATRIX SPIKE &MATRIX SPIKE DUPLICATE:
__�ii�i�'i
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
QUALITY CONTROL DATA
2471116
MS
92413357001
Spike
Units
Result
Conc.
mg/kg
17500
9280
mg/kg
393
928
mg/kg
23.2
928
mg/kg
3700
9280
mg/kg
11.7
928
mg/kg
15.5
g2g
mg/kg
ND
9280
mg/kg
ND
928
mg/kg
ND
9280
mg/kg
1880
928
MSD
Spike
Conc.
8310
831
831
8310
831
831
8310
831
8310
831
2471117
MS
Result
27500
1350
865
12700
900
871
13000
783
11100
2770
MSD
Result
25000
1220
770
11400
804
778
11900
687
10100
2570
MS
Rec
107
103
91
97
96
92
97
84
92
97
MSD
Rec
90
99
90
93
95
92
95
82
91
84
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Rec
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
9
10
12
11
11
11
9
13
10
8
Qual
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 16

Analytical
tvww.pacelabs.com
Project: Oxford WWTP 1/7/19
Pace Project No.: 92413357
QC Batch: 451773
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92413357001
SAMPLE DUPLICATE: 2470313
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2470314
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92413062001
Units Result
1.1
92413381002
Units Result
96.7
Dup
Result
0.80
Dup
Result
96.7
RPD Qualifiers
35 D6
RPD Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 16

Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Oxford WWTP 1/7/19
Pace Project No.: 92413357
OC Batch: 452172 Analysis Method: EPA 9045D
OC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92413357001
SAMPLE DUPLICATE: 2472426
92413563001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.2 5.3 0 H3
SAMPLE DUPLICATE: 2472427
92413312001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.8 6.8 0 H3
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 16

Analytical
www,pacelabs.com
QUALITY CONTROL DATA
Project: Oxford WV�ffP 1/7/19
Pace Project No.: 92413357
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 452023 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92413357001
METHOD BLANK: 2471582 Matrix: Solid
Associated Lab Samples: 92413357001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 8.9 01/12/19 15:09
LABORATORY CONTROL SAMPLE: 2471583
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 472 464 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471584 2471585
MS MSD
92413357001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Ammonia mg/kg 13200 10300 10500 21800 22500 83 89 90-110 3 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471586 2471587
MS MSD
92413358001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND 2320 2320 2210 2210 93 93 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16

Analytical
www.pacela6s.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford WWTP 1/7/19
Pace Project No.: 92413357
QC Batch: 452219
Analysis
Method: EPA
351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis
Description: 351.2 TKN
Associated Lab Samples: 92413357001
METHOD BLANK: 2472536
Matrix: Solid
Associated Lab Samples: 92413357001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND 50.0
01/15/19
04:45
LABORATORY CONTROL SAMPLE: 2472537
Spike
LCS
LCS
%Rec
Parameter Units
Conc.
Result
%Rec
Limits
Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000
967
97
90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2472538
2472539
MS
MSD
92413357001
Spike
Spike MS
MSD
MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 62000
21200
19000 74700
74800
60
67
90-110
0 M1
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2472540
2472541
MS
MSD
92413358001
Spike
Spike MS
MSD
MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 5230
5170
5170 8110
9500
56
83
90-110
16 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORYANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Oxford VVVVfP 1/7/19
Pace Project No.: 92413357
QC Batch: 451629 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate +Nitrite
Associated Lab Samples: 92413357001
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 2469664 Matrix: Solid
Associated Lab Samples: 92413357001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/kg ND 2.0 01/10/19 03:42
Nitrogen, Nitrite mg/kg ND 0.98 01/10/19 03:42
Nitrogen, NO2 plus NO3 mg/kg ND 2.0 01/10/19 03:42
LABORATORY CONTROL SAMPLE: 2469665
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 14.9 15.8 106 90-110
Nitrogen, Nitrite mg/kg 9.9 10.6 107 90-110
Nitrogen, NO2 plus NO3 mg/kg 24.8 26.4 107 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2469666 2469667
MS MSD
92413357001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD
Nitrogen, Nitrate mg/kg ND 425 420 412 393 97 93 90-110 5
Nitrogen, Nitrite mg/kg ND 286 280 305 308 100 102 90-110 1
Nitrogen, NO2 plus NO3 mg/kg ND 711 702 717 701 100 99 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Qual
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 16

Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Oxford VWVfP 1/7/19
Pace Project No.: 92413357
QC Batch: 451598 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92413357001
METHOD BLANK: 2469443 Matrix: Solid
Associated Lab Samples: 92413357001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 01/10/1913:45
LABORATORY CONTROL SAMPLE: 2469444
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phosphorus mg/kg 49 52.3 107 90-110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2469445 2469446
MS MSD
92413357001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Phosphorus mg/kg 24300 1100 1100 23200 23300 -99 -88 90-110 1 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project:
Oxford WWTP 1/7/19
Pace Project No.: 92413357
DEFINITIONS
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL -Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) -Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
)UP - Sample Duplicate
RPD - Relative Percent Difference
NC -Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
WNitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A
Pace
Analytical
Services -Asheville
PAST-C
Pace
Analytical
Services -Charlotte
ANALYTE QUALIFIERS
gC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2019 01:37 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 16

Analytical
www.pacela6s.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Oxford VW�ffP 1/7/19
92413357
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92413357001
Oxford 1
of
4
EPA 3050B
451935
EPA
6010D
451945
92413357001
Oxford 1
of
4
EPA 7471 B
452089
EPA
7471 B
452120
92413357001
Oxford 1
of
4
SM 2540G-2011
452044
92413357001
Oxford 1
of
4
ASTM D2974-87
451773
92413357001
Oxford 1
of
4
EPA 9045D
452172
92413357001
Oxford 1
of
4
SM 2710B-2011
452503
92413357001
Oxford 1
of
4
EPA 350.1 Rev 2.0
1993
452023
EPA
350.1 Rev
2.0
1993
452144
Mod.
Mod.
92413357001
Oxford 1
of
4
EPA 351.2 Rev 2.0
1993
452219
EPA
351.2 Rev
2.0
1993
452403
92413357001
Oxford 1
of
4
EPA 353.2 Rev 2.0
1993
451629
EPA
353.2 Rev
2.0
1993
451647
92413357001
Oxford 1
of
4
EPA 365.1 Rev 2.0
1993
451598
EPA
365.1 Rev
2.0
1993
451656
Date: 01/15/2019 01:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 16

CHAIN -OF -CUSTODY Analytical Request Document
aceAnalytical
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
Company: SYNAGRO Billing Information: Mary Brewer: 284 Boger rd, Mocksville
Address: 284 Boger Rd., Mocksville, NC 27028 NC 27028
Report To: Nate Roth ([e-mail]) Email To: [e-mail]
Copy To: Lysa Finnerty ([e-mail]) Site Collection Info/Address:
Custom P ect Nome/Number: State: County/City: Time Zone Collected:
(J �C� I /� LL 1 1 v / I ]PT ( )MT [ )CT [ )ET
Phone:[phone] SiteJFacility I #:
Email: [e-mail]
Collected By (print): Clay Fisackerly Purchase Order #
Quote M
Col�yFed 8y (s�ture)i ll. (I (Turnaround Date F
ompliance Monitoring?
CJ Yes ( )NO NC (X] SC ( J
W PWS ID #:
W Location Code:
nmediately Packed on Ice:
X ) Yes [ ] No
Sample Di�sal: ush: Field
[X] Dispose as appropriate [ ] Return ( ) Same Day [ ] Next Day [ ] Yes ( ] No
[ ] Archive: ( ] 2 Day [ 13 Day [ ] 4 Day [ ) 5 Day
[ ]Hold: (Expedite Charges Apply) Analysis:
Matrix Codes (insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid,(SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Comp / Collected (or Composite End Res # of
Customer Sample ID Matrix' Grab Composite Start) _ _ CI Ctns
Date Time Date Time
X A 1 C 14 SL Cix� t-�-R I�
Filtered (if applicable):
Customer Remarks /,Special Conditions/ Possible Hazards:
Relinquished byJLompany: (Signature)
Relinquished by/Company: (Signature}
Received
Date/Time:
Date�me: Received by/Company: (Signature)
rx
•' Preservative Types: (1) nitric add, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, pi zinc acetate,
(6j methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (8) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
i[eanfo:;`
1 Therm Corr.G:Factori G'oC
1 Coi=ected Temp: �_oC
e19of16

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report
Range
Ratio
2049-01-AEDLIQ-NC
OXFORD, NC AEROB. DIGESTED LIQUID
1/7/2019
1/1/2019=8/26/2019
2.9093
Na mg/I = (Na mg/kg x %Solids) _ 100 = (8700 x 3.5000) = 100 = 304.5
Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (17500 x 3.5000) = 100 = 612.5
Mg mg/I = (mg mg/kg x %Solids) = 100 = (3700 x 3.5000) _ 100 = 129.5
Na meq = Na mg/I _ Molec.Wgt.Na = 304.5 = 23 = 13.2391
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 612.5 = 20 = 30.625
Mg meq = Mg mg/I = Molec.Wgt.Mg = 129.5 = 12 = 10.7917
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 13.2391 = SgrRoot[0.5(30.625+10.7917)] = 2.90929
Printed: 2/1 /2020
Page 1 15:56

Waypaint,
ANALYTICAL
8/14/2019
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-207-0003
Project Description: Oxford N & M
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94�1 °Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 8/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability
in
any claim relating to analyses performed
shall be limited to, at laboratory's
option, repeating the
analysis in question
at
laboratory's expense, or the refund of the
charges paid for performance of
said analysis.
Virginia 460014
Page 1 of 6

Wa ©int.
y�
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Mein 804-743-9401 °Fax $04-271-6446
www.waypaintenalyticaLcom
Sample Summary Table
Report Number: 19-207-0003
Client Project Description: Oxford N & M
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
67548
Oxford
N
&
M
Solids
07/24/2019
12:30
08/05/2019
67548
Oxford
N
&
M
Solids
07/24/2019
12:30
08/05/2019
SM-4500-NH3C
WTN
67548
Oxford
N
&
M
Solids
07/24/2019
12:30
O8/05/2019
9045D
WTN
67548
Oxford
N
&
M
Solids
07/24/2019
12:30
08/05/2019
4500NO3F-2011
WTN
67548
Oxford
N
&
M
Solids
07/Z4/2019
12:30
O8/05/2019
6010D
WTN
67548
Oxford
N
&
M
Solids
07/24/2019
12:30
08/05/2019
SW-7471B
WTN
67548
Oxford
N
&
M
Solids
07/24/2019
12:30
08/05/2019
SM-4500-NH3C-TKN
WTN
67548
Oxford
N
&
M
Solids
07/24/2019
12:30
08/05/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number: 19-207-0003
Account Number: 46478
Send To: Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
�I��,:
��
ANALYTICAL
Project : Oxford N & M
7621 Whitepine Roadr Richmond, VA 2323i
Main SU4-743-94�1 °Fax $04-271-6446
www.waypointanalytical.com
REPORT OFANALYS/S Date Sampled: 7/24/2019 12:30:00
Lab Number : 67548 Date Received: 08/05/2019 00:00
Sample Id : Oxford N & M Date Reported: 08/14/2019
Total Solids * 4.17 ADM 07/30/2019 15:06 SM-2540G
Moisture * 95.80 ADM 07/30/2019 15:06 SM-2540G
Total Kjeldahl Nitrogen 6.79 67900 250 JPJ 08/09/2019 11:30 SM-4500-NH3C-TKN
Phosphorus 1.64 16400 50.0 BKN 08/01/201912:17 6010D
Potassium 0.27 2660 50.0 BKN 08/01/201912:17 6010D
Sulfur 0.84 8390 50.0 BKN 08/01/201912:17 6010D
Calcium 1.55 15500 250 BKN 08/01/201912:17 6010D
Magnesium 0.31 3140 50.0 BKN 08/01/201912:17 6010D
Sodium 0.14 1350 250 BKN 08/01/201912:17 6010D
Iron 16700 50.0 BKN 08/01/201912:17 6010D
Aluminum 48000 50.0 BKN 08/01/201912:17 6010D
Manganese 520 5.00 BKN 08/01/201912:17 6010D
Copper 295 2.50 BKN 08/01/201912:17 6010D
Zinc 1550 12.5 BKN 08/01/201912:17 6010D
Ammonia Nitrogen 1.19 11900 100 JPJ 08/13/2019 12:00 SM-4500-NH3C
Organic N 5.60 56000 250 08/09/2019 11:30 CALCULATION
Nitrate+Nitrite-N <4.76 4.76 ZBD 08/12/201915:08 4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H -Beyond holding time I ��G �� ��OK�
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, normayany reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number:
Account Number
19-207-0003
46478
Send To: Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
1N� v�lnt...
��
ANALYTICAL
Project : Oxford N & M
?621 Whitepine Raad, Richmond, VA 23237
Main $04-743-94p1 °Fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS Date Sampled: 7/24/2019 12:30:00
Lab Number : 67548 Date Received: 08/05/2019 00:00
Sample Id : Oxford N & M Date Reported: 08/14/2019
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Molybdenum
Comments:
<1.00
1.00
BKN
08/01/201912:17
57.6
2.50
BKN
08/01/201912:17
19.1
2.50
BKN
08/01/201912:17
20.2
3.00
BKN
08/01/201912:17
<5.00
5.00
BKN
08/01/201912:17
0.843
0.0157
TJS
08/06/201914:07
<5.00
5.00
BKN
08/01/201912:17
7.5
JSL
08/12/2019
07:57
8.33
2.50
BKN
08/01/201912:17
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H -Beyond holding time
Our reports
and
letters are for
the exclusive and confidential use
of our clients, and may
not be reproduced in whole or part,
nor may
any reference be made
to the work,
the
results, or the
company in any advertising. news
release, or other public
announcements without obtaining
our prior
written authorization.
6010D
6010D
. � C1�7
6010D
6010D
SW-7471 B
6010D
6010D
Pauric McGroary
Agronomist
Page 4 of 6

Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypoi nta nalytical.com
Cooler Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 19-207-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other
UPS � Client � Courier Thermometer ID: ��
Shipping container/cooler uncompromised? � Yes 0 No
--
Number of coolers received 1
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes 0 No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
COC properly completed � Yes � No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes 0 No
Sufficient sample volume for indicated test(s)? � Yes � No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No • N/A
Water -VOA vials free of headspace � Yes � No � N/A
Trip Blanks received with VOAs � Yes � No � N/A
Soil VOA method 5035 —compliance criteria met � Yes � No � N/A
� High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes � No
Comments:
Signature: Mary Amend Date &Time: �08/05/2019 12:40:19
Page 5 of 6

SAMPLING LOG #
PROJECT MANACaER:
Phone: � ��
r llllll IIIII IIII IIIII I III IIIII III IIIIII III IIIII 11�� I I IIII a6426 20193
,� (� Svnanro Central LLCI Oxford 1p:38:41
�� OXPORO N8M
,r ' I � � �� Ir„
�. �� n•.. I i `
�. , ,� ��
! attest that the proper field sampling procedures
were used during the collection of These samples.
GJ � �
AHMr,,.cn
A & L CUSTOMER R.00AT�ON sTYP.E CONTAINERS DATE P�TIME PRES RUED H APED
LAB # SAMPLE LD.
�•�. � �GflMP V
Relinquished by 5ampfer. ����
Relinquished by:
Relinquished by: �P S
Date Time Recleved by:
Date Tfine Reoleved by:
Date _ Time Recleved by;
SF"ECIAL INSTRUCTIONS: � �
��'�� For ' " � monitaring purposes.
ANALYSIS REQUEST
SAMPLE Organic
I•D' SL1 SL2 NH4-N NOs-N N Cd Cr Ni P6 As Hg Se
PO#:
pH
SL1: Total Solids (Moisture, Total Kjeldahl NIlrogen, Phosphorus, and Potassium .
SL2: Basic Tess SLi plus Sulfur, Calcium, Magnesium, Sodfum, Iron, Aluminum, Manganese, Capper and Zinc
REMARKS:
vu,nwc MO
5ollds
�i7

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2049-01-AEDLIQ-NC
OXFORD, NC AEROB. DIGESTED LIQUID
7/24/2019
8127/2019-9/2/2019
0.5265
Na mg/I = (Na mg/kg x %Solids) _ 100 = (1350 x 4.1700) _ 100 = 56.295
Ca mg/I = (Ca mglkg x %Solids) _ 100 = (15500 x 4.1700) _ 100 = 646.35
Mg mg/I = (mg mg/kg x %Solids) _ 100 = (3140 x 4.1700) _ 100 = 130.938
Na meq = Na mg/I = Molec.Wgt.Na = 56.295 = 23 = 2.44761
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 646.35 + 20 = 32.3175
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 130.938 _ 12 = 10.9115
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.44761 = SgrRoot[0.5(32.3175+10.9115)] = 0.526465
Printed: 2/1 /2020
Page 1 15:57

Waypoint.
ANALYTICAL
9/20/2019
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-255-0009
Project Description: Oxford
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 9/12/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P�� M` c�°"d`
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

W� oint..
Yp
ANALYTICAL
Report Number: 19-255-0009
Client Project Description: Oxford
7621 Whitepine Road, Richmond, VA 23237
Main $q4-743-9401 °Fax $Q4-271-6446
www.waypaintanalytical.cam
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
SM-4500-NH3C
WTN
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
9045D
WTN
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
4500NO3F-2011
WTN
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
6010D
WTN
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
SW-7471B
WTN
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
SM-4500-NH3C-TKN
WTN
68180
Oxford
Solids
09/11/2019
08:15
09/12/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 -Virginia
Page 2 of 6

Report Number: 19-255-0009
Account Number: 46478
Send To: Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
a Dint_..,
��
ANALYTICAL
Project :Oxford
7621 UVhitepine Road, Richmond, VA 23237
Main $U4-743-94U1 °' Fax [phone]
www.waypaintanalyficaLcom
REPORT OF ANALYSIS Date Sampled: 9/11/2019 08:15:00
Lab Number : 68180 Date Received: 09/12/2019 00:00
Sample Id :Oxford Date Reported: 09/20/2019
Total Solids
Moisture
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
1.18
ADM
09/16/201916:43
SM-2540G
98.80
ADM
09/16/201916:43
SM-2540G
7.42
74200
250
JPJ
09/19/201913:00
SM-4500-NH3C-TKN
1.91
19100
50.0
BKN
09/17/201919:52
6010D
0.38
3780
50.0
BKN
09/17/201919:52
6010D
0.96
9570
50.0
BKN
09/17/201919:52
6010D
1.53
15300
250
BKN
09/17/201919:52
6010D
0.39
3940
50.0
BKN
09/17/201919:52
6010D
0.47
4720
250
BKN
09/17/201919:52
6010D
15300
50.0
BKN
09/17/201919:52
6010D
47100
50.0
BKN
09/17/201919:52
6010D
626
5.00
BKN
09/17/201919:52
6010D
467
2.50
BKN
09/17/201919:52
6010D
1450
12.5
BKN
09/17/201919:52
6010D
2.25
22500
100
JPJ
09/19/201915:30
SM-4500-NH3C
5.17
51700
250
09/19/201913:00
CALCULATION
<4.74
4.74
ZBD
09/19/201915:09
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H -Beyond holding time
Our reports
and
letters are
for
the exclusive and confidential use
of our clients, and may
not be reproduced in whole or part,
nor may
any reference be made
to the work,
fhe
results, or
the
company in any advertising, news
release, or other public
announcements without obtaining
our prior
written authorization.
1"'� V���
Pauric McGroary
Agronomist
Page 3 of 6

Report Number: 19-255-0009
Account Number: 46478
Send To: Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
1a o�nt.
��
ANALYTICAL
Project :Oxford
7621 Whitepine Road, Richmond, VA 23237
Main $04-743-94(]1 °Fax $04-271-5446
www.waypointa nalytical.com
REPORT OFANALYS/S Date Sampled: 9/11/2019 08:15:00
Lab Number : 68180 Date Received: 09/12/2019 00:00
Sample Id :Oxford Date Reported: 09/20/2019
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Molybdenum
Comments:
<1.00
1.00
BKN
09/17/201919:52
56.0
2.50
BKN
09/17/201919:52
12.8
2.50
BKN
09/17/201919:52
25.6
3.00
BKN
09/17/201919:52
<5.00
5.00
BKN
09/17/201919:52
0.363
0.0157
TJS
09/17/201913:41
<5.00
5.00
BKN
09/17/201919:52
7.2
JSL
09/18/2019
06:19
10.4
2.50
BKN
09/17/201919:52
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H -Beyond holding time
Our reports
and
letters
are
for
the exclusive and confidential use
of our clients, and may
not be reproduced in whole or part,
nor may
any reference be made
to the work,
the
results.,
or
the
company in any advertising, news
release, or other public
announcements without obtaining
our prior
written authorization.
6010D
6010D
6010D
SW-7471 B
6010D
9045D
6010D
m` Geo"�'
Pauric McGroary
Agronomist
Page 4 of 6

Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypoi nta na lytical.com
Cooler Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 19-255-0009
Shipping Method
Fed Ex � US Postal � Lab � Other
UPS 0 Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? � Yes � No
Number of coolers received 1
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes 0 No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
COC properly completed � Yes 0 No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes � No
Sufficient sample volume for indicated test(s)? � Yes 0 No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes 0 No � N/A
Water -VOA vials free of headspace � Yes � No � N/A
Trip Blanks received with VOAs � Yes 0 No � N/A
Soil VOA method 5035 —compliance criteria met � Yes � No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson Date &Time
Page 5 of 6
09/12/2019 12:00:29

VUV
I VIYl4..!
1. mar
y
PROJECT MANAGER: _.�`_
Phone:
(NJ
CHAINi i Sil7 ji, `'fi
RECORD
•rd
properI attest Mat the
field • f procedures
were used during the collection of these samples.
1
CUSTOMER SAMPLING SAMPLE #OF SAMPLING METHOD METHOD
LAB # SAMPLE WeLOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
I
Rallnquished by:
Rellnqulshed by:
SPECIAL INSTRUCTIO1�fS: .
mnnitnrina oul`Oos@5.
REMARKS:
alpAj ®C
APO#:
f
SLI* Total Solids (Moisture), Total Kleldahl Nitrogen, Phosphorus, and Potassium
S1.2,* Basic Test SLi •lus Suffur, calcium, Magnesium,sodium, • r. - - copper and
R
I�
'Page 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report
Range
Ratio
2049=01-AEDLIQ-NC
OXFORD, NC AEROB. DIGESTED LIQUID
9/11/2019
9/3/2019-11/30/2019
0.9534
Na mg/I = (Na mg/kg x %Solids) = 100 = (4720 x 1.1800) _ 100 = 55.696
Ca mg/I = (Ca mg/kg x %Solids) = 100 = (15300 x 1.1800) _ 100 = 180.54
Mg mg/I = (mg mg/kg x %Solids) = 100 = (3940 x 1.1800) = 100 = 46.492
Na meq = Na mgll = Molec.Wgt.Na = 55.696 + 23 = 2.42157
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 180.54 _ 20 = 9.027
Mg meq = Mg mgll = Molec.Wgt.Mg = 46.492 _ 12 = 3.87433
SAR = Na meq - SgrRoot(0.5 x (Ca meq + Mg meq)] = 2.42157 = SgrRoot[0.5(9.027+3.87433)] = 0.953441
Printed: 2/1 /2020
Page 1 15:57

Waypoint.
ANALYTICAL
11/18/2019
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-312-0007
Project Description: Oxford
7621 Whitepine Road, Richmond, VA 23237
Main Sp4-743-94Q1 °Fax $04-271-6446
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 11/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pawta m` C��/
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

i
�� ����„
vp
ANALYTICAL
Report Number: 19-312-0007
Client Project Description: Oxford
Lab No Client Sample ID
7621 Whitepine Road, Richmond, VA 23237
Main $p4-743-941)1 °Fax SQ4-271-6446
www.waypointa nalyfical. com
Sample Summary Table
Matrix Date Collected Date Received Method
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
69535
Oxford
N&M
Solids
11/06/2019
09:30
11/08/2019
WTN: Waypoint Analytical - TN, Memphis, TN
SM-4500-NH3C
9045D
4500NO3F-2011
6010D
SW-74716
SM-4500-NH3C-TKN
SM-2540G
Lab ID
WTN
WTN
WTN
WTN
WTN
WTN
WTN
Page 2 of 6

Wa a►int,
vp
ANALYTICAL
46478
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By : Ryan Copeland
Report Number : 19-312-0007
Lab No : 69535
Sample ID :Oxford N&M
7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 °Fax $04-271-6446
www.waypointanalyfical.cam
Ryan Copeland
Project Oxford
Information
REPORT OFANALYSIS
Report Date : 11/18/2019
Received : 11/08/2019
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: il/6/2019 9:30
Test Results Units MQL DF Date /Time By Analytical
Analyzed Method
Ammonia Nitrogen 13600 mg/Kg -dry 2780 1 11/15/19 15:00 JPJ SM-4500-NH3C
Nitrate+Nitrite-N <128 mg/Kg -dry 128 1 11/12/19 14:12 ZBD 4500NO3F-2011
Organic N 45800 mg/Kg -dry 6940 1 11/15/19 12:00 CALCULATION
pH 7,7 s.u. 1 11/12/19 05:08 JSL 9045D
Total Solids 3.56 % 0.010 1 li/11/19 16:35 ADM SM-2540G
Total Kjeldahl Nitrogen 59400 mg/Kg -dry 6940 1 il/15/19 12:00 JPJ iM-4500-NH3C-TKP
Phosphorus 20300 mg/Kg -dry 139 1 11/13/19 02:34 KKM 6010D
Aluminum 54700 mg/Kg -dry 139 1 11/13/19 02:34 KKM 6010D
Arsenic <13.9 mg/Kg -dry 13.9 1 11/13/19 02:34 KKM 6010D
Calcium 15400 mg/Kg -dry 694 1 11/13/19 02:34 KKM 6010D
Cadmium <2.78 mg/Kg -dry 2.78 1 11/13/19 02:34 KKM 6010D
Chromium 52.2 mg/Kg -dry 6.94 1 11/13/19 02:34 KKM 6010D
Copper 461 mg/Kg -dry 6.94 1 11/13/19 02:34 KKM 6010D
Iron 21500 mg/Kg -dry 139 1 11/13/19 02:34 KKM 6010D
Lead 33.9 mg/Kg -dry 8.33 1 11/13/19 02:34 KKM 6010D
Magnesium 4560 mg/Kg -dry 139 1 11/13/19 02:34 KKM 6010D
Manganese 564 mg/Kg -dry 13.9 1 11/13/19 02:34 KKM 6010D
Mercury 0.550 mg/Kg -dry 0.406 1 11/12/19 14:29 TJS SW-7471B
Molybdenum g,94 mg/Kg -dry 6.94 1 11/13/19 02:34 KKM 6010D
Nickel 17.6 mg/Kg -dry 6.94 1 11/13/19 02:34 KKM 6010D
Potassium 2920 mg/Kg -dry 139 1 11/13/19 02:34 KKM 6010D
Selenium <13.9 mg/Kg -dry 13.9 1 11/13/19 02:34 KKM 6010D
Sodium 2310 mg/Kg -dry 694 1 11/13/19 02:34 KKM 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

1Na aint,
v�
ANALYTICAL
46478
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By : Ryan Copeland
Report Number : 19-312-0007
Lab No : 69535
Sample ID :Oxford N&M
7621 Whitepine Raad, Richmond, VA 23237
Main $04-743-9401 °Fax [phone]
www.waypointanalyfical.com
Ryan Copeland
Project Oxford
Information
REPORT OFANALYSIS
Test Results Units MQL
Zinc
1820
mg/Kg
-dry
34.7
Sulfur
10000
mg/Kg
-dry
139
Moisture 96.4 % 0.010
Report Date : 11/18/2019
Received : 11/08/2019
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11/6/2019 9:30
DF Date /Time By Analytical
Analyzed Method
1
11/13/19
02:34
KKM
6010D
1
11/13/19
02:34
KKM
6010D
1 11/11/1916:35 ADM SM-2540G
Qualifiers/ g Analyte detected in blank H Beyond holding time
Definitions
Page 4 of 6

Waypaint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypo i nta n a l yti ca I. co m
Cooler Receipt Form
Customer Number: 46478
Customer Name: Synagro Central LLC/ Oxford
Report Number: 19-312-0007
Shipping Method
Fed Ex � US Postal 0 Lab � Other
UPS � Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? � Yes � No
Number of coolers received � 1
Custody seals intact on shipping container/cooler? � Yes 0 No � Not Required
Custody seals intact on sample bottles? � Yes � No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
COC properly completed � Yes � No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes � No
Sufficient sample volume for indicated test(s)? � Yes � No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes 0 No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved 0 Yes 0 No � N/A
Water -VOA vials free of headspace 0 Yes � No � N/A
Trip Blanks received with VOAs 0 Yes � No � N/A
Soil VOA method 5035 —compliance criteria met 0 Yes 0 No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson Date &Time
Page 5 of 6
11/08/2019 13:03:03

t,
pry..•
W
4
9
�r-

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2049=01=AEDLIQ-NC
OXFORD, NC AEROB. DIGESTED LIQUID
11/6/2019
12/1/2019=12/31/2019
0.7903
Na mg/I = (Na mg/kg x %Solids) _ 100 = (2310 x 3.5Ei00) _ 100 = 82.236
Ca mg/I = (Ca mg/kg x %Solids) = 100 = (15400 x 3.5600) - 100 = 548.24
Mg mg/I = (mg mg/kg x %Solids) = 100 = (4560 x 3.5600) _ 100 = 162.336
Na meq = Na mg/I = Molec.Wgt.Na = 82.236 + 23 = 3.57548
Ca meq = Ca mg/I = Molec.Wgt.Ca = 548.24 = 20 = 27.412
Mg meq = Mg mg/I = Molec.Wgt.Mg = 162.336 _ 12 = 13.528
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.57548 = SgrRoot[0.5(27.412+13.528)] = 0.790269
Printed: 2/1 /2020
Page 1 15:57

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Q

FACILITY NAME: OXFORD, NC
OWNER: HENRY THORPE
SITE #: NC GR 00001 FIELD# : GR 00001 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: WQ0011244
OPERATOR: HENRY THORPE
ANNUAL DRY TONS APPLIED : 149.33
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 46.10 ACRES PERMITTED: 46.10
rage: 2
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli.
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
Total Gallons/Ac:
Total Wet Tons/Ac:
._,
30,663.77
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
145
0.097
0.010
0.070
2.639
0.153
0.004
0.074
0.097
0.097
11.639 150.89
Cumulative lbs/acre
0.226
0.089
2.814
19.203
1.629
0.032
0.548
0.904
0.677
110,105
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: EDWARD DENNY
SITE #: NC GR 00004 FIELD# : GR 00004 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: W00011244
OPERATOR: EDWARD DENNY
ANNUAL DRY TONS APPLIED : 29.86
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.50 ACRES PERMITTED: 8.50
Page : 1
Lune Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/6/19
495600,00 (G)
5835.294
3.50
0.852
OXAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
6/18/19
435400.00 (G)
5105.882
3.50
0.745
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
I FESCUE HAY
6/24/19
11100.00 (G)
13129,412
3.50
1.916
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
Jun-19
204,600.00 (G)
24,070.588
Total Gallons/Ac: 249070.59
Total Wet Tons/Ac:
1 uiai Cuvi� i U.UV
As
Cu
Cr
Cu
Pb
Hg
Iwo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
150
0.122
0.012
NR
2.761
0.163
0.005
0.082
0.109
0.122
13.209 170.74
Cumulative lbs/acre
0.233
0.074
2.152
14.214
0.779
0.023
0.279
0.777
0.288
57.905
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME: OXFORD, NC
OWNER: EDWARD DENNY
SITE #: NC GR 00004 FIELD# : GR 00004 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: WQ0011244
OPERATOR: EDWARD DENNY
ANNUAL DRY TONS APPLIED : 126.69
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 52.50 ACRES PERMITTED: 52.50
rage: 1
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
5/29/19
117,800.00 (G)
2243,810
3.50
0.327
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
131200.00 p
56.70 p
21297
FESCUE PASTURE
5/30/19
8600.00 (G)
1653,333
3.50
0.241
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
135200.00 p
56.70 p
21297
FESCUE PASTURE
5/31/19
142,600,00 (G)
2716,190
3.50
0.396
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
13,200.00 p
56.70 p
21297
FESCUE PASTURE
May-19
3479200.00 (G)
69613,333
6/3/19
161,200.00 (G)
3070.476
3.50
0.448
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
13,200.00 p
56.70 p
21297
I FESCUE PASTURE
6/4/19
1052400,00 (G)
2007.619
3.50
0.293
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
( FESCUE PASTURE
6/5/19
111,600.00 (G)
2125,714
3.50
0.310
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
( FESCUE PASTURE
6/6/19
933000,00 (G)
1771,429
3.50
0.259
OXAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
62,000. p
135200.00 p
56.70 p
21297
I FESCUE PASTURE
6/18/19
49,600.00 (G)
944,762
3.50
0.138
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13200.00 p
56.70 p
21297
FESCUE PASTURE
Jun49
520,800*00 (G)
99920,000

FACILITY NAME: OXFORD, NC
OWNER: EDWARD DENNY
SITE #: NC GR 00004 FIELD# : GR 00004 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: WQ0011244
OPERATOR: EDWARD DENNY
ANNUAL DRY TONS APPLIED : 126.69
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 52.50 ACRES PERMITTED: 52.50
rage: 2
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
(
DATE or
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1 offal liallons/Ac: 16,533.33
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
0.084
0.008
NR
1.897
0.112
0.003
0.056
0.075
0.084
9.073 117.27
103
Cumulative ]bs/acre
0.175
0.055
1.698
11.472
0.602
0.017
0.213
0.581
0.269
47.595
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p =ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, INC
OWNER: HERBERT P. MORTON
SITE #: NC GR 00013 FIELD# : GR 00013 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: WQ0011244
OPERATOR: HERBERT P. MORTON
ANNUAL DRY TONS APPLIED : 8.24
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.70 ACRES PERMITTED: 11.70
rage: 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/9/19
371200,00 (G)
3179.487
1.18
0.156
OXAEDL
DRY
0-<I/2"
SUR
0.5
0.30
745200. p
22,500.00 p
4.74 p
26765
FESCUE PASTURE
9/10/19
1305200,00 (G)
11128,2051
1.18
0.548
OXAEDL
DRY
0-<I/2"
SUR
0.5
0.30
74,200. p
225500.00 p
4.74 p
26765
FESCUE PASTURE
Sep49
167,400.00 (G)
14,307.692
Total Gallons/Ac:
Total Wet Tons/Ac:
14,307.69
i vial �uuiv iu�. V.VV
As
Cd
Cr
Cu
Pb
rigMo
Ni
Se
Zn
P
PAN
TOTALS
Annual lbs/acre
38
0.007
0.001
0.079
0.658
0.036
<.001
0.015
0.018
0.007
2.042
26.89
Cumulative lbs/acre
0.150
0.106
4.053
22.305
2.728
0.045
0.698
1.260
1.067
85.244
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR
=Not
Reported
or Not
Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
* Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

FACILITY NAME: OXFORD, NC
OWNER: HERBERT P. MORTON
SITE #: NC GR 00013 FIELD# : GR 00013 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: W00011244
OPERATOR: HERBERT P. MORTON
ANNUAL DRY TONS APPLIED : 7.93
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 13.20 ACRES PERMITTED: 13.20
rage: 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
'Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/4/19
93,000.00 (G)
7045.455
1.18
0.347
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
747200. p
22,500.00 p
4.74 p
26765
FESCUE PASTURE
9/9/19
%200.00 (G)
5166,667
1.18
0.254
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
74,200. p
22,500.00 p
4.74 p
26765
FESCUE PASTURE
Sep-19
161,200.00 (G)
12,212.122
Total Gallons/Ac:
Total Wet Tons/Ac:
12,212.12
As
Cu
Cr
Cu
Pb
rig
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
32
0.006
0.001
0.067
0.561
0.031
<.001
0.013
0.015
0.006
1.743
22.95
Cumulative Ibs/acre
0.165
0.112
3.879
22.898
2.851
0.046
0.669
1.214
1.100
83.219
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
X
T
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: HERBERT P. MORTON
SITE #: NC GR 00013 FIELD# : GR 00013 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : GEORGEVILLE
PERMIT #: W00011244
OPERATOR: HERBERT P. MORTON
ANNUAL DRY TONS APPLIED : 9.76
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.50 ACRES PERMITTED: 8.50
rage: 1
Lune Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/3/19
1172800.00 (G)
13858.824
1.18
0.682
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
74,200. p
22,500.00 p
4.74 p
26765
FESCUE
9/4/19
495600.00 (G)
5835,294
1.18
0.287
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
74,200. p
22,500.00 p
4.74 p
26765
FESCUE
9/9/19
315000.00 (G)
3647,059
1.18
0.179
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
74,200. p
22,500.00 p
4.74 p
26765
FESCUE
Sep-19
198,400.00 (G)
239341.177
Total Gallons/Ac:
Total Wet Tool
23,341.18
As
Cu
Cr
Cu
Pb
rig
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
61
0.011
0.002
0.129
1.073
0.059
<.001
0.024
0.029
0.011
3.331
43.87
Cumulative lbs/acre
0.104
0.073
2.682
15.649
1.794
0.029
0.496
0.821
0.699
53.149
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: HERBERT P. MORTON
SITE #: NC GR 00013 FIELD# : GR 00013 0004 B
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00011244
OPERATOR: HERBERT P. MORTON
ANNUAL DRY TONS APPLIED : 30.19
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.60 ACRES PERMITTED: 7.60
Page : 1
Lime Applied ***
Date Lbs/Ac
DATE or
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/29/19
99,200.00 (G)
13052.632
4.17
2.270
OXAEDL
DRY
0-<l/2"
SUR
0.5
0.30
67,900. p
11,900.00 p
4.76 p
22755
FESCUE HAY
8/30/19
74,400.00 (G)
9789,474
4.17
1.702
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
67,900. p
11,900.00 p
4.76 p
22755
FESCUE HAY
Aug-19
173,600.00 (G)
22,842.106
Total Gallons/Ac:
Total Wet Tons/Ac:
22,842.11
As
Cu
Cr
Cu
Pb
rig
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
181
0.040
0.008
0.458
2.343
0.160
0.007
0.066
0.152
0.040
12.313 130.28
Cumulative lbs/acre
0.107
0.055
1.651
10.311
0.726
0.024
0.206
0.523
0.142
77
52.239
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: ROBERT CERWIN
SITE #: NC GR 00060 FIELD# : GR 00060 0001
RESIDUAL SOURCE(S): See list at bottom of report
PREDOMINANT SOIL SERIES : IREDELL
PERMIT #: WQ0011244
OPERATOR: JAKE ISLEY
ANNUAL DRY TONS APPLIED : 95.01
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 43.30 ACRES PERMITTED: 43.30
rage: 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
Rate
Rate
Nitrite
8/13/19
1059400,00 (G)
2434,180
3.50
0.355
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/14/19
1613200.00 (G)
3722.864
3.50
0.543
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
I FESCUE HAY
8/15/19
130,200.00 (G)
3006,928
3.50
0.439
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
627000. p
13,200.00 p
56.70 p
21297
I FESCUE HAY
8/16/19
130,200.00 (G)
3006,928
3.50
0.439
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/19/19
124,000.00 (G)
2863,741
3.50
0.418
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
Aug49
651,000.00 (G)
15,034.641
Total Gallons/Ac:
Total Wet Tons/Ac:
15,034.64
.um. �uuA� . uwn�. v.vv
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS
Annual lbs/acre
93
0.076
0.007
NR
1.725
0.102
0.003
0.051
0.068
0.076
8.251
106.64
Cumulative Ibs/acre
0.229
0.073
2.959
18.994
2.193
0.053
0.378
0.971
0.863
77.335
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** 0ee Site pH &Lime
Application Records Section of Report for
Fields where Lime 40s to be applied in 2020

FACILITY NAME: OXFORD, NC
OWNER: ROBERT CERWIN
SITE #: NC GR 00060 FIELD# : GR 00060 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LIGNUM
PERMIT #: W00011244
OPERATOR: JAKE ISLEY
ANNUAL DRY TONS APPLIED : 104.06
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 31.90 ACRES PERMITTED: 31,90
rage: 1
Lune Applied ***
Date Lbs/Ac
DATE or
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/5/19
8600.00 (G)
2721.003
3,50
0,397
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/6/19
11700.00 (G)
3692.790
3,50
0.539
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/7/19
136,400.00 (G)
4275,862
3.50
0.624
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/8/19
15500.00 (G)
4858,934
3.50
0.709
OXAEDL
DRY
0-<1/2"
SUR
0.5
0,30
6200. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/9/19
11100.00 (G)
3498.433
3.50
0.511
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/12/19
105,400.00 (G)
3304.075
3,50
0.482
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
Aug49
713,000.00 (G)
22,351.097
Total Gallons/Ac:
Total Wet Tons/Ac:
22,351.10
rRi
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
139
0.114
0.011
NR
2.564
0.151
0.004
0.076
0.101
0.114
12.266
158.54
Cumulative Ibs/acre
0.315
0,103
3,678
22,707
2.930
0.060
0,501
1,257
0.456
109,474
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER )
DATE
"I certify,
under penalty of law, that
this document was prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel
properly gathered and
evaluated
the information submitted.
I at aware that
there are significant penalties for
submitting false information, including the possibility
of fines and imprisonment for
knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not
Required
% =percent p =ppm or mg/kg
k
Application
,
-Inj,
-
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
*** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: ROBERT CERWIN
SITE #: NC GR 00060 FIELD# : GR 00060 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: ENON
PERMIT #: W00011244 ANNUAL DRY TONS APPLIED: 42.55
OPERATOR: JAKE ISLEY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.20 ACRES PERMITTED: 16.20
rage: 1
Lune Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/26/19
136,400.00 (G)
8419,753
3.50
1.229
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
13,200.00 p
56.70 p
21297
FESCUE PASTURE
8/27/19
130,200.00 (G)
8037,037
4.17
1.398
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
67,900. p
11,900.00 p
4.76 p
22711
FESCUE PASTURE
Aug49
266,600.00 (G)
169456.790
Total Gallons/Ac:
Total Wet Tons/Ac:
456.79
16,
i uLai �uui� iuw��. V.VV
As
Cd
Cr
Cu
Pb
rigMo
Ni
Se
Zn
P
PAN
TOTALS
Annual lbs/acre
116
0.057
0.007
0.161
1.790
0.113
0.004
0.052
0.091
0.057
8.953
105.56
Cumulative lbs/acre
0.184
0.062
2.778
14.582
1.444
0.035
0.281
0.941
0.239
83.824
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
�1
IGNATURE OF LAND APPLIER )
(S
DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered acid
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR —Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: ROBERT CERWIN
SITE #: NC GR 00060 FIELD# : GR 00060 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : ENON
PERMIT #: W00011244
OPERATOR: JAKE ISLEY
ANNUAL DRY TONS APPLIED : 34.50
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.90 ACRES PERMITTED: 11.90
Page : 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/27/19
12,400.00 (G)
1042.017
4.17
0.181
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
67,900. p
11,900.00 p
4.76 p
22755
FESCUE PASTURE
8/28/19
148,800.00 (G)
12504.2021
4.17
2.174
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
67,900. p
11,900.00 p
4.76 p
22755
I FESCUE PASTURE
8/29/19
37,200.00 (G)
3126.0501
4.17
0.544
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
67,900. p
11,900.00 p
4.76 p
22755
FESCUE PASTURE
Aug-19
198,400.00 (G)
16,672.269
Total Gallons/Ac:
Total Wet Tons/Ac:
16,672.27
As
Cd
Cr
Cu
Pb
rig
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
132
0.029
0.006
0.334
1.710
0.117
0.005
0.048
0.111
0.029
8.987
95.09
Cumulative lbs/acre
0.163
0.061
2.572
13.883
0.944
0.040
0.253
0.771
0.240
66.945
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: ROBERT CERWIN
SITE #: NC GR 00060 FIELD# : GR 00060 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : ENON
PERMIT #: W00011244
OPERATOR: JAKE ISLEY
ANNUAL DRY TONS APPLIED : 37.10
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.70 ACRES PERMITTED: 11.70
rage: 1
Lime Applied ***
Date Lbs/Ac
DATE or
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/21/19
11100.00 (G)
9538.462
3.50
1.392
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/22/19
14200.00 (G)
12188.034
3.50
1.779
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
Aug-19
254,200.00 (G)
213726.496
Total Gallons/Ac:
Total Wet Tons/Ac:
21,726.50
As
Cu
Cr
Cu
Pb
rig
Iwo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
135
0.110
0.011
NR
2.492
0.147
0.004
0.074
0.098
0.110
11.923
154.11
Cumulative Ibs/acre
0.291
0.084
2.881
20.506
1.442
0.054
0.431
1.015
0.450
91.625
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, NC
OWNER: ROBERT CERWIN
SITE #: NC GR 00060 FIELD# : GR 00060 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: ENON
PERMIT #: WQ0011244
OPERATOR: JAKE ISLEY
ANNUAL DRY TONS APPLIED : 24.43
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.20 ACRES PERMITTED: 7.20
Page : 1
Lime Applied ***
Date Lbs/Ac
DATE or
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
( Per Acre
Solids
Acre
Source
Moist
Hours
Rate
Rate
Nitrite
8/20/19
124,000.00 (G)
17222,222
3.50
2.514
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
FESCUE HAY
8/21/19
37,200.00 (G)
5166.667
3.50
0.754
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
62,000. p
13,200.00 p
56.70 p
21297
I FESCUE HAY
8/22/19
6,200.00 (G)
861.111
3.50
0.126
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
6200. p
13,200.00 p
56.70 p
21291
FESCUE HAY
Aug-19
1 1679400.00 (G)
23,2500000
Total Gallons/Ac:
23,250.00
Total Wet Tons/Ac:
ULa. �uV,� . uWn�. v.vv
TOTALS: As Cu Cr Cu Pb rigMo Ni Se Zn P PAN
Annual lbs/acre 145
0.118 0.012 NR 2.667 0.157 0.004 0.079 0.105 0.118 12.759 164.92
Cumulative lbs/acre 0.280 0.075 2.436 18.095 1.247 0.044 0.388 0.899 0.399 80.468
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
X
T
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p =ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
X
T
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p =ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : OXFORD, INC
OWNER: ROBERT CERWIN
SITE #: NC GR 00060 FIELD# : GR 00060 0007
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : ENON
PERMIT #: W00011244
OPERATOR: JAKE ISLEY
ANNUAL DRY TONS APPLIED : 34.17
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.10 ACRES PERMITTED: 16.10
Page : 1
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
10/30/19
74,400.00 (G)
4621.118
1.18
0.227
DL
MOIST
0-<1/2"
SUR
0.5
0.30
74,200. p
22,500.00 p
4.74 p
26765
FESCUE HAY
Oct-19
741400.00 (G)
4,621.118
7
11/4/19
2175000,00 (G)
13478.261
1.18
0.663
OXAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
742200. p
22,500.00 p
4.74 p
26765
I FESCUE HAY
11/5/19
2605400.00 (G)
16173.913
1.18
0.796
OXAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
74,200. p
22,500.00 p
4.74 p
26765
I FESCUE HAY
11/6/19
142,600.00 (G)
8857,143
1.18
0.436
OXAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
74200. p
225500.00 p
4.74 p
26765
FESCUE HAY
Nov49
620,000.00 (G)
38,509.317
Total Gallons/Ac:
Total Wet Tons/Ac:
43,130.43
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
114
0.021
0.004
0.238
1.982
0.109
0.002
0.044
0.054
0.021
6.155 81.07
Cumulative lbs/acre
0.021
0.004
0.238
1.982
0.109
0.002
0.044
0.054
0.021
6.155
OXAEDL =OXFORD, NC AEROB. DIGESTED LIQUID
x C ;�-Eii�� lil
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A
=Not Applicable NR
=Not
Reported
or Not Required
% =percent p =ppm or mg/kg
** Volatilization Rate:
Surface 0.5, Injection/Incorporation
1.0
*
Application Method:
SUR -Surface,
INJ -Injection,
SURIN -Incorporation
*** See Site pH &Lime
Application Records Section of Report for
Fields where Lime is to be applied in 2020

���
'r.44VIRr�Nh1Eh11'11L�E�1•kCa€5Lt3G1;=5, jrl�:
,+�rrar,Frh=a.1 �n�arr�rc�rje a
July 24, 2018
Clay Fisackerly
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Oxford TCLP 2018
Summit Environnsental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.• [phone]
Website: htto://www.settelc.com
Dear Clay Fisackerly: Order No.: 18061305
Summit Environmental Technologies, Inc. received 1 sample(s) on 6/22/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
�,, .�.. .
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware,. Florida NELAC E87688, Georgia E87688, Idaho OH00923, IDinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 27

Summit Environmental Technologies, Inc.
fn SUMMIT 3310 Win St.
rNVlf#ONMENTAL TECHNOLOGIES, ihtc_ Cuyahoga Falls, Ohio 44223
Anzfylrcal Laboratories TEL: [phone] FAX: [phone]
Website: hyp:llwww.settek.com
CLIENT: Synagro
Project: Oxford TCLP 2018
WorkOrderNarrative:
Case Narrative
WOit: 18061305
Date: 7/24/2018
18061305: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this reportare noted below.
Prep Sample Comments:
18061305-OOlA 391811: Prep Comments for MtlPrep_TCLP(3010A), Sample 18061305-OOlAa
Sample had a yellow tint, had limited volume, and was filtered after digestion.
18061305-001A 3918574 Prep Comments for SVPrep BNATot TCLP(3510), Sample 18061305-
001A: Sample is a soapy solution, Limited volume
18061305-001A 391855: Prep Comments for SVPrep_CPest_TCLP(3510), Sample 18061305-001A:
Sample is a soapy solution, Original pH of sample is acidic, sample was neutralized prior to extraction,
Limited volume
Original
Page 2 of 27

SumnsitEnvirownental Technologies, In
' 3310 Win
�"PfgrIR�7NFdENT�,L�ffG3iPat7L��.=S, iIV�C Cuyahoga Falls, Ohio442�
.+�,xr�f�th��.P Lahars�t�r7�;� TEL: [phone] FAX.• (330) 253-44E
Website.• http://wwwsettek.co.
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
WO#: 18061305
Date: 7/24/2018
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
r The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+),
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+),
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 27

SUMMIMF
,ArrafyN'cal Laboratories
CLIENT: Synagro
Project: Oxford TCLP 2018
Lab SampleID Client Sample ID
18061305-001 Oxford TCLP 2018
Summit Environmental Technologies, Inc,
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Tag No Date Collected
6/21/2018 12:30:00 PM
Workorder
Sample Summary
WO#: 18061305
Date Received Matrix
6/22/2018 10:20:00 AM Sludge
Page 4 of 27

Summit Environmental Technologies, Inc.
UMMIT 3310 Win St.
UYIVIRONloIENTAL TEC"NOLOG'I=S, INC_ Cuyahoga Falls, Ohio 44223
. nafyhlca,(Laberataries� TEL: [phone] FAX: [phone]
Website: http://Www.settek.com
DATES REPORT
W O#: 18061305
24-Jul-18
Client: Synaglo
Project: Oxford TCLP 2018
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
18061305-OOlA Oxford TCLP 2018 6/21/2018 12:30:00 PM Sludge Ignitability of Solids (SW-846: 1030) 7/23/2018 2:00:00 PM
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP Herbicides Analysis (SW1311/87/1/2018 6:00:00 PM
7/9/2018 5:18:00 PM
6/25/2018 2:29:00 PM
6/25/2018 2:29:00 PM
7/3/2018
TCLP Mercury Analysis (SW1311/7477/t/2018 6:00:00 PM
7/9/2018 5:18:00 PM
6/25/2018 2:29:00 PM
6/25/2018 2:29:00 PM
12:30:00 PM 7/11/2018 7:20:00 PM
7/3/2018 10:55:00 AM 7/3/2018 3:43:00 PM
TCLP
TCLP
Metals Analysis (SW1311/6010:7/1/2018 6:00:00 PM
7/2/2018 3:20:00 PM
7/5/2018 8:34:41 PM
TCLP
Pesticides Analysis (SW1311/8(7/1/2018 6:00:00 PM
7/2/2018 1:00:00 PM
7/11/2018 2:30:00 PM
TCLP
Semi-Volatiles Analysis 7/1/2018 6:00:00 PM
7/2/2018 11:15:00 AM
7/9/2018 12:18:00 PM
(SW1311/8270)
TCLP
Volatiles
Analysis
7/1/2018 6:00:00 PM
7/4/2018 2:16:00 AM
Original
Page 5 of 27

ff1summill
FKVIROWAEN AL TECHUOLOGIES, INC
Anafy rzl Lztbar-s�orips
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Analytical Report
(base report)
WO#: 18061305
idjebstte: kitty://ivww.settek.com Date Reported: 7/24/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 6/21/2018 12:30:00 PM
Lab ID: 18061305-OOIA
Project: Oxford TCLP 2018
Client Sample ID Oxford TCLP 2018
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1'311/7470)
TCLP Mercury
ND 0.0100
SW7470A SW7470A Analyst: EAM
mg/L 1 7/3/2018 3:43:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: KMS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 2.50 mg/L 1 7/5/2018 8:34:41 PM
TCLP Barium(Ba) ND 25.0 mg/L 1 7/5/2018 8:34:41 PM
TCLP Cadmium(Cd) ND 0.500 mg/L 1 7/5/2018 8:34:41 PM
TCLP Chromium(Cr) ND 1.00 mg/L 1 7/5/2018 8:34:41 PM
TCLP Lead(Pb) ND 2.50 mg/L 1 7/5/2018 8:34:41 PM
TCLP Selenium(Se) ND 0.250 mg/L 1 7/5/2018 8:34:41 PM
TCLP Silver(Ag) ND 2.50 mg/L 1 7/5/2018 8:34:41 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.160 mg/L 2 7/9/2018 12:18:00 PM
2,4,5-Trichlorophenol ND 0.400 mg/L 2 7/9/2018 12:18:00 PM
2,4,6-Trichlorophenol ND 0.400 mg/L 2 7/9/2018 12:18:00 PM
2,4-Dinitrotoluene ND 0.0800 mg/L 2 7/9/2018 12:18:00 PM
o-Cresol ND 0.400 mg/L 2 7/9/2018 12:18:00 PM
m/p-Cresol(s) ND 0.400 mg/L 2 7/9/2018 12:18:00 PM
Cresols, Total ND 8.00 mg/L 2 7/9/2018 12:18:00 PM
Hexachloro-1,3-butadiene ND 0.0320 mg/L 2 7/9/2018 12:18:00 PM
Hexachlorobenzene ND 0.0800 mg/L 2 7/9/2018 12:18:00 PM
Hexachloroethane ND 0.160 mg/L 2 7/9/2018 12:18:00 PM
Nitrobenzene ND 0.160 mg/L 2 7/9/2018 12:18:00 PM
Pentachlorophenol ND 0.400 mg/L 2 7/9/2018 12:18:00 PM
Pyridine ND 0.400 mg/L 2 7/9/2018 12:18:00 PM
Surr: 2-Fluorophenol 25.2 10 - 109 %Rec 2 7/9/2018 12:18:00 PM
Surr: Phenol-d6 27.0 10 - 109 %Rec 2 7/9/2018 12:18:00 PM
Surr: Nitrobenzene-d5 31.6 19 - 120 %Rec 2 7/9/2018 12:18:00 PM
Surr: 2,4,6-Tribromophenol 33.4 10 - 120 %Rec 2 7/9/2018 12:18:00 PM
Surr: 2-Fluorobiphenyl 41.8 22 - 117 %Rec 2 7/9/2018 12:18:00 PM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 6 of 27

Sanzuazit Environmental Technologies, Inc.
ffISUMMIT 3310 Al'in St.
i`,1rIRCfh1►,tEMIhLT�ttC�raL�u!€, 114c Cuyahoga Falls, Ohio44223
An3lyf€ral Laboratories TEL: [phone] FAY., [phone]
CLIENT: Synagro
Matrix: SLUDGE
Lab ID: 18061305-001A
Project: Oxford TCLP 2018
Client Sample ID Oxford TCLP 2018
Analyses
Analytical Report
(base report)
WO#: 18061305
ATebsrte: lattp:/hvwwsettelc.cO171 Date Reported: 7/24/2018
Tag Number:
Collection Date: 6/21/2018 12:30:00 PM
Result RL Qual Units
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
Surr: p-Terphenyl-d14
89.7 34 - 116
DF Date Analyzed
SW8270D SW3510C Analyst: BJH
%Rec 2 7/9/2018 12:18:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW3510C Analyst: JBN
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND 0.0200 mg/L 1 7/11/2018 2:30:00 PM
Toxaphene ND 0.0400 mg/L 1 7/11/2018 2:30:00 PM
Endrin ND 0,00200 mg/L 1 7/11/2018 2:30:00 PM
gamma-BHC ND 0.00200 mg/L 1 7/11/2018 2:30:00 PM
Heptachlor ND 0,00200 mg/L 1 7/11/2018 2:30:00 PM
Heptachlor epoxide ND 0,00200 mg/L 1 7/11/2018 2:30:00 PM
Methoxychlor ND 0.00200 mg/L 1 7/11/2018 2:30:00 PM
Surr: TCMX 35.1 10 - 119 %Rec 1 7/11/2018 2:30:00 PM
Surr: DCB 56.0 10 - 119 %Rec 1 7/11/2018 2:30:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: JBN
TCLP HERBICIDES ANALYSIS (SW1311/8151)
214-D ND 1.00 d mg/L 1 7/11/2018 7:20:00 PM
21415-TP ND 0.500 d mg/L 1 7/11/2018 7:20:00 PM
Surr: DCAA 83.7 20 - 140 %Rec 1 7/11/2018 7:20:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1, 1 -Dichloroethene
ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
1,2-Dichloroethane ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
MEK ND 2.50 mg/L 100 7/4/2018 2:16:00 AM
Benzene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Carbon tetrachloride ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Chlorobenzene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Chloroform ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Tetrachloroethene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Trichloroethene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Vinyl chloride ND 0.200 mg/L 100 7/4/2018 2:16:00 AM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 27

Summit Environmental Technologies, Inc.
SUMM111 3310 Win St.
r1tkt1R0NFAEN`FAL IECIMOLOGIEa, INN Cuyahoga Falls, Ohio 44223
Arraryfil'raf r'_abarBT*ori?q TEL: [phone] FAX., [phone]
CLIENT: Synagro
Matrix: SLUDGE
Lab ID: 18061305-001A
Project: Oxford TCLP 2018
Client Sample ID Oxford TCLP 2018
Analyses Result
Analytical Report
(base report)
WO#: 18061305
Websate: http://wla tiv.settelc.cona Date Reported: 7/24/2018
Tag Number:
Collection Date: 6/21/2018 12:30:00 PM
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
Sum 4-Bromofluorobenzene 107 70 - 130 %Rec 100 7/4/2018 2:16:00 AM
Sum DibromofIuoromethane 106 70 - 130 %Rec 100 7/4/2018 2:16:00 AM
Sum Toluene-d8 105 70 - 130 %Rec 100 7/4/2018 2:16:00 AM
RCI-SOLID-W/ IGNITABILITY1030 SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.500 mg/Kg 1 6/25/2018 2:29:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW1030 Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable 1 7/23/2018 2:00:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9045D Analyst: DHC
PH (SW9045D)
pH 6.8 s.u.@21.7C 1 7/9/2018 5:18:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 6/25/2018 2:29:00 PM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 8 of 27

Summit Environmental Technologies, Inc. Accreditation Program
frsummly 3310 Win St. Anal teS Report
Ft`{VIRON hiENTAL TECHNOLOCIES, INC Cuyahoga Falls, Ohio 44223 y p
Arrar'yfir-ai Laboratories TEL: [phone] FAX: [phone] WO#: 18061305
Website: http://www.settek.coin 244048
Client: Synagro State: NW
Project: Oxford TCLP 2018 Program Name: NC_WW SCM
Sample ID Matrix Test Name Analyte Status
18061305-001A Sludge Ignitability of Solids (SW-846: 1030) Ignitability A
Sludge pH (SW9045D) Hydrogen Ion (pH) A
Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U
Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Sludge TCLP Herbicides Analysis (SW1311/8151) 2,455-TP A
Sludge TCLP Herbicides Analysis (SW1311/8151) 2,4-D A
Sludge TCLP Herbicides Analysis (SW1311/8151) DCAA A
Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A
Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis (SW1311/6010) Barium A
Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis (SW1311/6010) Chromium A
Sludge TCLP Metals Analysis (SW1311/6010) Lead A
Sludge TCLP Metals Analysis (SW1311/6010) Selenium A
Sludge TCLP Metals Analysis (SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis (SW1311/8081) 2,2',333%454%525%636'- A
Decachlorobiphenyl
Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A
Sludge TCLP Pesticides Analysis (SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis (SW1311/8081) Tetrachloro-m-xylenc A
Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,54richlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Tribromophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorobiphenyl A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorophenol A
NC_WW_SCM
A Accredited NC WW SCM U Unavailable
Original # 1
Page 9 of 27

Sannanit Environmental Technologies, Inc. Accreditation Program
SUMMINt 1 3310 Win St. Anal tes Report
"WIRONh1EN'I`AL 1ECHNOLQGIES, irx, Cuyahoga Falls, Ohio 44223 Y 1�
Arrar'trti r'a.t tabaratori , TEL: [phone] FAX.• [phone] WO#: 18061305
Website: http://Www.settek.coni 24-M48
Client: Synagro State: NW
Project: Oxford TCLP 2018 Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
18061305-001A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Methylphenol A
Sludge, TCLP Semi-Volatiles Analysis (SW1311/8270) 3,4-Methylphenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene-d5 A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Phenol-d6 A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) p-Terphenyl-04 A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis 4-Bromofluorobenzene A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Dibromofluoromethane A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Toluene-d8 A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
NC WW SCM A Accredited NC WW SCM
U Unavailable
Original # 1
Page 10 of 27

IT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
ERA&VIRONMENTALTECHNOLOGIE.S, ]PqC Cuyahoga Falls, Ohio 44223
A.tafyUcal Lzbflratc;4e TEL: [phone] FAX.• [phone] WO#: 18061305
Website: http://Www.settek.com 244W48
Client: Synagro
Project: Oxford TCLP 2018
BatchIDa 32833
Sample ID
mb-32833
SampType:
MBLK
TestCode:
tclp-voc-MST
Units: mg/L
Prep
Date:
7/1/2018
RunNo:
86054
Client ID:
PBS
Batch ID:
32833
TestNo:
SW8260B
SW1311M
Analysis
Date:
7/3/2018
SegNo:
1616959
Analyte Result
PQL SPK value SPK Ref Val
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0,0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0,00200
Surr: 4-Bromofluorobenzene
50.0
Surr: Dibro mofl uorom ethane
48.7
Surr: Toluene-d8
51.3
%REC LowLimit HighLimit RPD Ref Val
50.00
100
70
130
50.00
97.5
70
130
50.00
103
70
130
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit,
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 11 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
u i or 3310 Win St.
ENVIRONMENTAL TEiHNOLOG;E51AMC Cuyahoga Falls, Ohio44223
11��1y6'ca.t LabflratorJe.� WO#: 18061305
TEL: [phone] FAX. [phone]
Website: httn:llwww.settek.com 244W48
Client: Synagro
Project: Oxford TCLP 2018
SatchIDa 32833
Sample ID
MB-32833
SampType:
MBLK
TestCode:
tclp-voe-mstr
Units: mg/L
Prep
Date:
7/1/2018
RunNo:
85971
Client ID:
PBS
Batch ID:
32833
TestNo:
SW8260B
SW1311M
Analysis
Date:
7/2/2018
SegNo:
1615558
Analyte Result
PQL SPK value SPK Ref Val
1,1-Dichloroethene
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0,0500
Tetrachloroethene
ND
0,0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
488
Surr: Dibromofluorom ethane
412
Surr: Toluene-d8
509
%REC LowLimit HighLimit RPD Ref Val
500.0
97.5
70
130
500.0
82A
70
130
500.0
102
70
130
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 12 of 27

ummilu Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St,
EN IRtiN1A F7 NTAL TEC9NOLOG4SS. INC Cuyahoga Falls, Ohio 44223 WO#: 18061305
A:rratyTTrat.taboraxonv� TEL: [phone] FAX* [phone]
Website: http://www.settek.com 244ul48
Client: Synagro
Project: Oxford TCLP 2018 BatchID: 32855
TCLP Mercury ND 0.00200
TCLP Mercury 0.00363 0.00200 0.00400 0 90.8 80 120
Sample ID 18061322-001AMS
SampType: MS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 7/3/2018
RunNo: 86042
Client ID: BatchQC
Batch ID: 32855
TestNo:
SW7470A SW7470A
Analysis Date: 7/3/2018
SegNo: 1616627
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00391 0.00200 0.00400 0 97.8 75 125
Sample ID 18061322-001AMSD
SampType: MSD
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 7/3/2018
RunNo: 86042
Client ID: BatchQC
Batch ID: 32855
TestNo:
SW7470A SW7470A
Analysis Date: 7/3/2018
SegNo: 1616628
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00381 0.00200 0.00400 0 95.2 75 125 0.00391 2.59 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitat ion limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 13 of 27

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St,
ENVIRONMENTAL Tt=£OUOLCCIE.S, NC Cuyahoga Falls, Ohio 44223
Analytical LsbDratorle,S TEL: [phone] FAX.- [phone]
Website: http://www.settek.eom
Client: Synagro
Project: Oxford TCLP 2018
Sample ID
18061322-001AMSD
SampType:
MSD
Client ID:
Batch=
Batch ID:
32855
Analyte
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
QC SUMMARY REPORT
BatchID0 32855
Prep
Date:
7/3/2018
Analysis
Date:
7/3/2018
%REC LowLimit HighLimit RPD Ref Val
WO#: 18061305
244W48
RunNo: 86042
SegNo: 1616628
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 14 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
U I Nt 3310 Win St.
ENVIRONIAr.NTAL TSC4N0L0[i1E51 1141C Cuyahoga Falls, Ohio 44223
. nalyticaf Laboratories TEL: [phone] FAX: [phone] WO#: 18061305
Website: httl2:llwww.settek.com 244ul48
000000
Client: Synagro
Project: Oxford TCLP 2018
BatchID: 32886
Sample ID mb-32886 SampType: mblk TestCode: tclp-svoc-her Units: mg/L Prep Date: 7/3/2018 RunNo: 86440
Client ID: PBS Batch ID: 32886 TestNo: SW8151A SW8151A Analysis Date: 7/11/2018 SegNo: 1632755
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D ND 1.00 0 0
21415-TP ND 0,500 0 0
Sum DCAA 365 500.0 73.1 20 140
Sample ID Ics-32886 SampType: Ics TestCode: tclp-svoc-her Units: mg/L Prep Date: 7/3/2018 RunNo: 86440
Client ID: LCSS Batch ID: 32886 TestNo: SW8151A SW8151A Analysis Date: 7/11/2018 SegNo: 1632756
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
214-D
ND
1.00 0.500
0 72.9
62.6
125
21415-TP
ND
0,500 0.500
0 78.9
52.5
128
Surr: DCAA
449
500.0
89.9
20
140
Sample ID
18061305-001ams
SampType:
ms
Client ID:
Oxford TCLP
2018
Batch ID:
32886
Analyte
Result
TestCode:
tclp-svoc-her
Units:
mg/L
TestNo:
SW8151A
SW8151A
PQL SPK value SPK Ref Val
Prep Date: 7/3/2018
Analysis Date: 7/11/2018
%REC LowLimit HighLimit RPD Ref Val
2,4-D
ND
1.00 0.500
0 82.7
37
105
2,415-TP
ND
0.500 0.500
0 86.1
38
106
Surr: DCAA
486
500.0
97.1
20
140
RunNo: 86440
SegNo: 1632760
%RPD RPDLimit Qual
Qualifiers: �
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit,
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 15 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIT 3310 Win St.
ENV1 tC N1AE:NTAL`rEiC"t.IQL0G1E.S, Al2 Cuyahoga Falls, Ohio 44223
A!1w1yP,°aa.f Laiavrat®rJss TEL: [phone] FAX. [phone]
WO#: 18061305
Website: httl2:llwww.settek.com 244W48
Client: Synagro
Project: Oxford TCLP 2018
Sample ID
18061305-001amsd
SampType:
msd
Client ID:
Oxford TCLP
2018
Batch ID:
32886
Analyte
Result
BatchIDa 32886
TestCode:
tclp-svoc-her
Units:
mg/L
Prep
Date:
7/3/2018
RunNo:
86440
TestNo:
SW8151A
SW8151A
Analysis
Date:
7/11/2018
SegNo:
1632761
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 84.9
37
105
0 0 30
27415-TP
ND
0.500 0.500
0 89.6
38
106
0 0 30
Sum DCAA
502
500.0
100
20
140
0
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 16 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summlir 3310 Win St.
ENVI� ONNIENTAL TECHNOLOGIES, iCY Cuyahoga Falls, Ohio 44223
l::rCa.P,p4`caf Lzbcratonas TEL: [phone] FAX.• [phone] WO#: 18061305
Website: http://www.settekcom 244W48
Client: Synagro
Project: Oxford TCLP 2018
BatchID: R85806
Sample ID 18061330-001AMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 85806
Client ID: BatchQC Batch ID: R85806 TestNo: SW9014 Analysis Date: 6/25/2018 SegNo: 1608659
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
9.74 0.500 10.00 0 97.4 81.6 122
Sample ID
18061330-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R85806
Analyte
Cyanide, Reactive
Result
TestCode: Cyanide,Rea Units: mg/Kg
TestNo: SW9014
PQL SPK value SPK Ref Val
9.62 0.500 10.00
Prep Date:
Analysis Date: 6/25/2018
%REC LowLimit HighLimit RPD Ref Val
RunNo: 85806
SegNo: 1608660
%RPD RPDLimit Qual
0 96.2 81.6 122 9.739 1.20 5
Qualifiers: +
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 17 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
UMMIT 3310 Win St.
tEP VIROh1 ENTAl- TfCHNOLOGI�E& ';%c Cuyahoga Falls, Ohio 44223
Atft�.Py6°mot I�a�rcaraa'orle� TEL: [phone] FAX.• [phone]
WO#: 18061305
Website: http://Www.settek.Com 244W48
Client: Synagro
Project: Oxford TCLP 2018
BatchIDa R85806
Sample ID MB-R85806
SampType: MBLK
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 85806
Client ID: PBW
Batch ID: R85806
TestNo:
SW9014
Analysis Date: 6/25/2018
SegNo: 1608644
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive
ND 0.500
Sample ID LCS-R85806
SampType: LCS
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 85806
Client ID: LCSW
Batch ID: R85806
TestNo:
SW9014
Analysis Date: 6/25/2018
SegNo: 1608645
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.91 0.500 10.00
0 99.1
85 115
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below qua11LA tion limits
M
Manual integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 18 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMINt 3310 Win St.
EUVIR4N?404TAL iECHNOLOGIE�S,;NC Cuyahoga Falls, Ohio44223
WO#: 18061305
A,*raYyrtfral.CzfaArarvrde� TEL: [phone] FAX.' [phone]
Website: hgQ:Ilwww.settek.com 244W48
Client: Synagro
Project: Oxford TCLP 2018
Sample ID
18061330-001AMS
SampType:
MS
Client ID:
BatchQC
Batch ID:
R85822
Analyte
Sulfide, Reactive
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
BatchlDa R85822
Prep Date:
Analysis Date: 6/25/2018
%REC LowLimit HighLimit RPD Ref Val
4630 25.0 4800 40.00 95.6 80 120
Sample ID
18061330-001AMSD
SampType:
MSD
Client ID:
Batch=
Batch ID:
R85822
Analyte
Sulfide, Reactive
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 6/25/2018
%REC LowLimit HighLimit RPD Ref Val
RunNo: 85822
SegNo: 1609030
%RPD RPDLimit Qual
RunNo: 85822
SegNo: 1609031
%RPD RPDLimit Qual
4740 25.0 4800 40.00 97.9 80 120 4630 2.35 30
Qualifiers: 'k
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 19 of 27

1wr Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summ3310 Win St.
P-WIRONMENTAL Ti ECHt40LQGt1=S, W2 Cuyahoga Falls, Ohio 44223
�trtalyUcaf Laborarorje5 TEL: [phone] FAX.- [phone] WO#: 18061305
Website: hgR:11www.settek.com 244W48
Client: Synagro
Project: Oxford TCLP 2018
BatchID0 R85822
Sample ID MB-R85822
SampType: MBLK
TestCode:
Sulfide,React Units: mg/L
Prep Date:
RunNo: 85822
Client ID: PBW
Batch ID: R85822
TestNo:
SW9034
Analysis Date: 6/25/2018
SegNo: 1609015
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
Sample ID LCS-R85822
Client ID: LCSW
Analyte
Sulfide. Reactive
ND 25.0
SampType: LCS
Batch ID: R85822
Result
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
4660 25.0 4800
Prep Date:
Analysis Date: 6/25/2018
%REC LowLimit HighLimit RPD Ref Val
0 97.1 85 115
RunNo: 85822
SegNo: 1609016
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for prepazation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 20 of 27

lir
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summ3310 Win St.
EN
"+�I C?NIdEtJTAL TfChlE40LaGaEs, INC Cuyahoga Falls, Ohio 44223
WO#: 18061305
Rr?&IyUcaP Laboralor s TEL: [phone] FAX.- [phone]
Website: httl2:llwww.settek.com 244ul48
Client: Synagro
Project: Oxford TCLP 2018
BatchID: R86179
Sample ID CHECK 7
SampType: LCS
TestCode:
PH_S(9045D) Units: s.u.@22.3C
Prep Date:
RunNo: 86179
Client ID: LCSS
Batch ID: R86179
TestNo:
SW9045D
Analysis Date: 7/9/2018
SegNo: 1623498
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0 0 99.6 90
110
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 21 of 27

Summit Environmental Technologies, Inc.
summlir 3310 Win St.
ENVIRONMENTAL TEC"NOLOG ES, AC Cuyahoga Falls, Ohio 44223
krWyUcaf Lzbaratardes TEL: [phone] FAX.- [phone]
Website: http:11www.settek.com
Client: Synagro
Project: Oxford TCLP 2018
QC SUMMARY REPORT
BatchIDa R86179
WO#: 18061305
244W48
Sample ID CHECK 7
SampType: LCS
TestCode:
PH_OIL(9045 Units: s.u.@22.2C
Prep Date:
RunNo: 86179 -
Client ID: LCSW
Batch ID: R86179
TestNo:
SW9045D
Analysis Date: 7/9/2018
SegNo: 1622920
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0
0 99.3 90 110
Sample ID 18070425-001ADUP
me 1
SampType: DUP
TestCode:
pH_Oil(9045 Units: s.u.@22.9C
Prep Date:
RunNo: 86179
Client ID: BatchQC
Batch ID: R86179
TestNo:
SW9045D
Analysis Date: 7/9/2018
SegNo: 1623459
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
5.4
5.3 0.7 10
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 22 of 27

Summit Environmental Technologies, Inc.
ummlir
3310 Win St, QC SUMMARY REPORT
ENVIRONMENTAL TECrµNOLGGIE.S. iNC Cuyahoga Falls, Ohio 44223 WO#: 18061305
Ar?a?yfI'Ca( L.abo.r.910 eF TEL: [phone] FAX.' [phone]
Website: http:11www.settek.com 244W48
Client: Synagro
Project: Oxford TCLP 2018 BatchlD. R86179
Sample ID LCS-R86179 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@21.8C Prep Date: RunNo: 86179
Client ID: LCSW Batch ID: R86179 TestNo: SW9045D Analysis Date: 7/9/2018 SegNo: 1622722
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 7.0 7.0 0 101 98.6 101.4
Sample ID 18061704-005ADUP SampType: DUP TestCode: pH_NPW(450 Units: s.u.@20.8C Prep Date: RunNo: 86179
Client ID: BatchQC Batch ID: R86179 TestNo: SW9045D Analysis Date: 7/9/2018 SegNo: 1622724
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 6.9 6.8 0.4 5
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 23 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIT 3310 Win St.
EUVI "tONMENTAL TECAiNOLCWi'S. AC Cuyahoga Falls, Ohio 44223
Ilritrtyf!fcai' t_aborarordes TEL: [phone] FAX. [phone]
WO#: 18061305
Website: hQ://www.settek.com 244u148
Client: Synagro
Project: Oxford TCLP 2018
SatchID: R86713
Sample ID LCS-R86713
SampType: LCS
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 86713
Client ID: LCSS
Batch ID: R86713
TestNo:
SW1030
Analysis Date: 7/23/2018
SegNo: 1645842
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
7.41
Sample ID
18061305-001ADUP
SampType:
DUP
Client ID:
Oxford TCLP 2018
Batch ID:
R86713
Analyte
Ignitability
Result
non-flammable
Sample ID
18070553-001ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R86713
Analyte
Ignitability
Result
Sample ID
18070827-001ADUP
SampType:
DUP
Client ID:
Batch=
Batch ID:
R86713
Analyte Result
Ignitability
non-flammable
7.240
TestCode: Ignitability_S Units:
TestNo: SW1030
0 102 70 130
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 712312018
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 7/23/2018
%REC LowLimit HighLimit RPD Ref Val
0
Prep Date:
Analysis Date: 7/23/2018
%REC LowLimit HighLimit RPD Ref Val
i
RunNo: 86713
SegNo: 1645844
%RPD RPDLimit Qual
0 20
RunNo: 86713
SegNo: 1645846
%RPD RPDLimit Qual
0 20
RunNo: 86713
Seq No: 1645848
%RPD RPDLimit Qual
0 20
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 24 of 27

Summit Environmental Technologies, Inc.
3310 Win St.
EPWIROWAENTAI. TECWJOLOGIES; INC Cuyahoga Falls, Ohio 44223
na0yLicat Lzboraranes TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Oxford TCLP 2018 BatchID: R86713
Sample ID
18070827-001ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R86713
Analyte
Result
Sample ID
18070849-001ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R86713
Analyte Result
Ignitability
non-flammable
Sample ID
18070849-002ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R86713
Analyte
Ignitability
Result
non-flammable
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 7/23/2018
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 7/23/2018
%REC LowLimit HighLimit RPD Ref Val
0
Prep Date:
Analysis Date: 7/23/2018
%REC LowLimit HighLimit RPD Ref Val
WO#: 18061305
244W48
RunNo: 86713
SegNo: 1645848
%RPD RPDLimit Qual
RunNo: 86713
SegNo: 1645850
%RPD RPDLimit Qual
0 20
RunNo: 86713
SegNo: 1645852
%RPD RPDLimit Qual
0 20
Qualifiers: "
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 25 of 27

ON%
P

Sznmaait Environmental Technologies, bxc.
T3310 i�T�in St.
fP€1rIRC�NAtENTAL'ffCt�N�SL�GdE�, ��d�. CuyuhognFalls, Ohio 44223
l�asaf�frasl Cahare�rle� TEL: [phone] FAX.• [phone]
Yfjebsite: htt>,://ivww.settek.com
Client Name: SYN-NC-27028
Work Order Number: 18061305
Sample Log -In Check List
RcptNo: 1
Logged by: Christopher Livengood 6/22/2018 10:20:00 AM ����� ��
Completed By: Christopher Livengood 6/22/2018 1:47:05 PM ,l�{�'��.
Reviewed By: Jennifer Woolf 6/25/2018 12:30:58 PM � �'� +���
Chain of Custody
1. Is Chain of Custody complete? Yes❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Log In
3, Coolers are present? Yes❑ No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes � No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑�
No. Seal Date: Signed By:
5, Was an attempt made to cool the samples? Yes ❑� No ❑ NA ❑
g, Were all samples received at a temperature of >0° C to 6.0°C Yes 0 No ❑ NA ❑
7_ Sample(s) in proper container(s)? Yes � No ❑
$. Sufficient sample volume for indicated test(s)? Yes � No ❑
g, Are samples (except VOA and ONG) properly preserved? Yes❑ No ❑
10. Was preservative added to bottles? Yes ❑ No ❑ NA❑
NA
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials
12. Were any sample containers received broken? Yes ❑ No ❑�
13. Does paperwork match bottle labels? Yes � No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes � No ❑
15. Is it clear what analyses were requested? Yes 0 No ❑
16. Were all holding times able to be met? Yes � No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA ❑�
Person Notified: Date
By Whom: Via: ❑ eMail ❑Phone ❑Fax ❑ In Person
Regarding:
Client Instructions
18. Additional remarks:
Additional sample reed on 7-13-18/10:25 via UPS in cooler w/ ice temp. of 4.2°
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed By
1
4.3
Good
Not Present
Page 27 of 27

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP
WWTP Name: Oxford W\
Monitoring Period: From
1/1/2019
WQ Permit Number: W00011244
NPDES Number: 1NC0025054
To 3/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.11061-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Beta Ray
Class B:
Alt. (1) Fecal Density X
Heat Drying
Gamma Ray
Heat Treatment
Pasteurization
Alt. (2) Process to Significantly Reduce Pathogens
Thermophilic
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaeroon
bic Digesti
Air Drying
Composting
Aerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the followinE monitorinS data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
675
15109
2,313
CFU/g
0
4 /Yr
grab
SM9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
colifann
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Infection)
(40-day bench)
Option/Alt. 2
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) X
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
(Spec.
Option/Alt. 4
02 uptake)
Option/Alt, 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been
"I certify, under penalty of law, that Lite pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Title
of Preparer*
print)
Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A
NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Report Date:
Project:
Date Sample Rcvd:
Page 1
1/17/2019
Qxford
2019
Meritech Work Order # 01071904 Sample: Oxford Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 4.05 % 1/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 1,347 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
Meritech Work Order # 01071905 Sample: Oxford Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 4.04 % 1/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 675 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
Meritech Work Order # 01071906 Sample: Oxford Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.93 % 1/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 2,313 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
Meritech Work Order # 01071907 Sample: Oxford Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 4.01 % 1/8/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 2,040 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
Meritech Work Order # 01071908 Sample: Oxford Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 4.06 % 1/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 896 col/g dry wt 1/7/19 258 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[33b)342-47�k8 fax.[336)342-1522

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Report Dace:
Project:
Date Sample Rcvd:
Page 2
1/17/2019
Oxford
2019
Meritech Work Order # 01071909 Sample: Oxford Fecal 1 of 4 Gra6 1/7/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 4M % 1/8/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 682 col/g dry wt 1/7/19 252 col/g dry wt SM 9222D
Meritech Work Order # 01071910 Sample: Oxford Feca11 of 4 Grab 1/7/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 4J6 % 1/8/19 0-100 % SM2540B
Fecal Coliform (Sludge) 765 col/g dry wt 1/7/19 228 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[336)342-1522

sisr,a
Chain of Custody R'�e'cord(COC)-
NPDES#:
Client:;; �.� � �° °�'.J Phone:
�°'°o
I
1 �r 1 � r
Address: :� ;�.
Fax:
ENVIRONMENTAL LABORATORIES
fi t: C 1 [ (
Email:
642 Tamco Rd. Phone: [phone]
Project:
NL
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: info@a meritechlabs.com
Attention: � �', ��
Turn Around Time*
*RUSH
work needs prior approval,
How would you like your report sent?
Charges A I
WWW.
Circle all that apply: Emai preferred) Fax, Mail
Std 10da s) 3-5 Days 24-48Hrs
,
Sampling Dates &Times
Per onTakin .Sam e Si nJPr' t .,
7tp. ' `i; �;
` 7. �
Lab Use Only
Sample Location
and/or ID #
Start
End
Comp?
#of
On Ice?
pH OK?
Test
s) Required
Yes / No
Date
Time
Date
Time
Grab?
Cont.
CI OK?
IrA
l
6
°
Temperature Upon
Receipt:
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples must be done in the
field prior to preservation.
"**
Comments:
F
Compositor #
Shipment,
Jug #
UPS
Fed Ex
Are these resin or regulatory purposes? Yes
No I
Report
results in: mg/L
E mg/kg ( ug/L `' 6 f Vt 4,
Hand Delivery
Relinquished bit' ": Date:
,dime:
Received by:
Date:
Time:
�{
4�11 Other
Relinquished by: ate:
Time:
Recei 5y'
Date;
Time:
Relinquished by: Date:
Time:
Receiv b
y
Time,:

Lab result Log
1347 3,13
675 2,83
2313 3,36
21040 3,31
896 2,95
682 2,83
785 2,89
Average 304
FECAL DATA SHEET
Min
Max
Geometric Mean
675
2313
1109

Contact: Nate Roth
Client; Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
2/11/2019
Oxford WWTP
1/7/2019
Vector Attraction Reduction / Aerobicall Digested Sludge 30 Day Test)
Meritech Worlc Order # 01071925
Total Solids
Sample: Oxford Composite
Volatile Solids
Week 1 1.23 0.680
Week 2 1.26 Q.700
Week 3 1.25 Q.710
Week 4 1.21 0.690
'11Ueek S 1.25 Q.710
Van I�leeck Reduction (%}: -6,35
I hereby certify that 1 have reviewed and approve these data.
°[� Volatile Solids
642 Tamco Road, Reidsville, North Carolina 2732Q
tel.[phone] fax.[phone]
0.557
0.557
0.5 71
Q.572

8/9/18
Chain of Custody Record (COC)
NPDES#:
I'MElTECINC.
�T
Client: �,�:��-.�'�"'?...J Phone:
,�
Address: 2
Fax:
;N. ..'.
ENVIRONMENTAL LABORATORIESc�..
642 Tamco Rd. Phone; 33&3424748
Project:
2 i `z- L I(J
`=
Reidsville NC 27320 Fax: 33&3424522
Email: [e-mail]
Attention: �.l '`
�
Around iora
�
wrkneedsprn
*RUSH work needs prior approval,
Wow would you like your report
sent?
C arpesAoDlv
www.meritechiabs.com
std 10 Oa s) 3.5 DaVS 1 24.48Hrs
Circle all that apply: mail tpreferred) ,
Fax, Mail
.
�•Em
Sampling Dates & Times
Perk n Takin mple ign/Print} ''
,I Ta
Lab Use Only
Sample Location
and/or ID #
Start End
Date Time Date Time
Comp?
40f,
k
SIt Req
'
u i'ed
On Ice?
Yes / No
pH OK?
Grab?
Cont.
Cl OK?
It
t �
}
�
, ...ion
'j ,r,...
1
tJtr.
id'10
1 # 4-�
P 'I
1� � ..J
f � d
'1
` ..
Temperature Upon
Receipt: 7 4/"
Method of
Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples
must be done in the field prior
to preservation."*
Shipment:
Comments:
Compositor #
Qt UPS
Jug#
Fed Ex
Are ti Ae results for ,reguIAtory,{�urposes? Yes
No
Report results in: mg/L �i mg/kg ug/L
Hand Delivery
Relinquished by* y Date:
„. ) i
"Time:
Received by:
Date: Time;
Other
Relinquished by: V Date:
Time:
Rece' AF1by:
Date: Time:
Relinquished by: Date:
Time:
R ved Lab:
D 1 Time:

%VS R
(older, more conservative method)
%VS in 0.5570 Enter in
o decimal form
/oVS out 0.5720
%VSR—_
((%VS in - (%VS in x %VS out))
%VSR= -6.29
(method from p.132 of WH manual)
%VS in
%VSR= -2.69
Results must be either greater than 38%; less than 17% fora 40-day scale test; test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
City of Oxford WWTP WQ Permit Number: WQ0011244
Oxford WWTP
Monitoring Period:
From 4/1/2019
NPDES Number: NC0025054
To 6/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.11061-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Beta Ray
Class B:
Alt. (1) Fecal Density X
Heat Drying
Gamma Ray
Heat Treatment
Pasteurization
Alt. (2) Process to Significantly Reduce Pathogens
Thermophilic
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaerobic Digestion
Air Drying
Composting
Aerobic Digestion
If applicable to alternative performed (Class A or Class Bl complete the following monitorin¢ data:
Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo. Mean Maximum Units dences Analysis
Fecal 2x10 to the 01 MPN MPN/g
Coliform power per gram
of total solids
CFU 230 249 263 CFU/g 0 4 /Yr grab SM9222D
1000 MPN per gram of MPN/g
total solids (dry weight)
Salmonella 3 MPN per 4 grams total
bacteria (in solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Alt, 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) X
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
WWTP
id Title (1
of Preparer*
print) Land Applier Name and Title (if applicable) (type or print)
® Date
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Alt, 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) X
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
WWTP
id Title (1
of Preparer*
print) Land Applier Name and Title (if applicable) (type or print)
® Date
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
Page 1
2019
Qxford
7J24/2019
Meritech Worlc Order # 07241993 Sample: Oxford Fecals Feca11 Grab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.80 % 7/25/19 0400 % SM 2540B
Fecal Coliform (Sludge) 239 col/g dry wt 7/24/19 258 col/g dry wt SM 9222D
Meritech Work Order # 07241994 Sample: Oxford Fecals Feca12 Grab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3AS % 7/25/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 263 col/g dry wt 7/24/19 258 col/g dry wt SM 9222D
Meritech Work Order # 07241995 Sample: Oxford Fecals Feca13 Grab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.58 % 7/25/19 0400 % SM 2540B
Fecal Coliform (Sludge) <254 col/g dry wt 7/24/19 254 col/g dry wt SM 9222D
Meritech Worlc Order # 07241996 Sample: Oxford Fecals Fecal 4 Grab 7/24J19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.95 % 7/25/19 0-100 % SM 2540B
Fecal Coliform (Sludge) < 2 3 0 col/g dry wt 7/24/19 230 col/g dry wt SM 9222D
Meritech Work Order # 07241997 Sample: Oxford Fecals Fecal 5 Grab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.67 % 7/25/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 248 col/g dry wt 7/24/19 258 col/g dry wt SM 9222D
64Z Tamco Road, Reidsville, North Carolina 27320
tel.(33b}342-4748 fax.{336)342-1522

Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
Meritech Worlc Order # 0724199$ Sample: Oxford Fecals Fecal 6 Grab
Parameters Results Analysis Date Reporting Linnit
% Total Solids 3.65 % 7/25/19 0400 %
Fecal Coliform (Sludge) <249 col/g dry wt 7/24/19 249 col/g dry wt
Page 2
2019
Oxford
7/24/2019
7/24/19
Method
SM 2540E
SM 9222DI
Meritech Warlc Order # 07241999 Sample: Oxford Fecals Fecal 7 Grab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3,51 % 7/25/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 259 col/g dry wt 7/24/19 258 col/g dry wt SM 9222D
C hereby certify Chat I have reviewed and approve these data.
64Z Tamco Raad, Reidsville, North Carolina Z73Z0
teL[336)34Z-4748 fax.(336)34Z-15ZZ

e 9 78
Chain of Custody Record (COC)
T
NPDES#:
MERIT 1
Client:
Phone:
, e
Address: gv�=ffl-
Fax:
ENVIRONMENTAL LABORATORIES
Email:
Vwptmm
l'�Gv'q
642TamcoRd. Phone:[phone]
Project:
10Xo2f3
.+
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
Attention: `�``NV?f�
Turn Around Time
*RUSH work needs prior approval,
How would you like your report Sent?
Char es Apply
�i�a w.mer��echl�bs.c®I'i1
Circle all that apply: Email referred), Fax, Mail
Std 10
s) 3-5 Days 24-48Hrs
Sampling Dates & Times
Person Taking (Sign/Print):
Lab Use Only
Sample Location and/or ID #
Start
End
comp?
#of
Test(s) Required
On Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Yi=S / No
Cl OK?
9
yI�
Temperature Upon
Receipt: 1 i n
Method Of
*** Dechlorination (<O.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples
must be done in the field prior to
preservation.
Shipment:
Comments:
Compositor #
Jug #
UPS
Fed Ex
Are these results for regulatory purposes? Yes
LJ
No ID
Report results in:
mg/L
[ mg/kg
77'ug/L
Nand Delivery
Relinquished by: �.d� Date:
c'7 y I
Time:
i�j_y5
Received by:
Date:
Time:
.., Other
Relinquished by: Date:
Time:
Received by:
Date:
Time:
Relinquished by: Date: Time:
R ed by Date:
T" ! f

Lab result Log
239 2,38
263 2.42
254 2,40
230 2,36
248 2,39
249 2,40
259 2,41
Average 2.40
FECAL DATA SHEET
Min
Max
Geometric Mean
230
263
249

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
8/29/2019
Oxford
7/24/2019
Vector Attraction Reduction /Aerobically Digested Sludge (30 Day Test)
Meritech Worlc Order # 07241992
Total Solids
Sample: Oxford Composite
Volatile Solids
Week 1 1A3 0.540
Week 2 0.720 0.390
Week 3 0.680 0.370
Week 4 0.280 0.160
Week 5 1.05 0.580
Van Kleecic Reduction (%): -10.58
I hereby certify that I have reviewed and approve these data.
7/24/19
%Volatile Solids
0.529
0.544
O.S42
0.590
0.554
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[33b}342-4748 fax.{336}342-1522

e/4/18
Chain of Custody Record (COC)
NPDES#:
Client: I� �'�'-�
Phone:
MERITECH1 ��
Address. N og
Fax:
ENVIRONMENTAL LABORATORIES
Email:
AL��r�a
642 Tamco Rd. Phone: [phone]
l'
Project: C
;,;-
Reidsville NC 27320 Fax: [phone]
P.Q.#:
Email: [e-mail]
Attention:
Turn Around Time*
*RUSH
work needs prior approval,
How would you like your
report sent?
Char es A I
www.meritechiabs.com
�/�
Circle all that apply: Email
Std 10 a s) 3-5 Da s 24-48Hrs
referred), Fax, Maif.
Sampling Dates & Times
Person Taking Sample (Sign/Print):
Lab Use Only
Sample Location and/or ID #
Start
End
comp?
it of
Test(s) Required
On Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Yes No
CI OK?
or toe,
Low
Temperature Upon
Receipt: k.,b4 "
Method
Of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples
must be done in the
field prior to preservation. ***
Shipment:
Comments:
Compositor #
UPS
Jug #
Fed Ex
Are these results for regulatory purposes? Yes
No (
Report
results in: mg/L mg/kg ug/L
QHand Delivery
Relinquished by: Q� Date:l f / �lG
t� d-
Time:
Received by:
Date:
Time:
1
Other
Relinquished by: Date:
Time:
Received by:
Date:
Time:
Miss
Relinquished by: Date: Time:
Receive y Lab: e:
i
CD"
IS

%VS R
(older, more conservative method)
%VS in 1 0,52901 Enter in
o
/oVS out 1 Ov55401 decimal form
%VSR_
((%VS in - (%VS in x %VS out))
%VSR= -10.60
(method from p.132 of WH manual)
%VS in
%VSR= -4.73
Results must be either greater than 38%; less than 17% fora 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period
City of Oxford WWTP WQ Permit Number: WQ0011244
Oxford WWTP
From 7/1/2019
NPDES Number: NC0025054
To 9/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Beta Ray
Class B:
Alt. (1) Fecal Density X
Heat Drying
Gamma Ray
Heat Treatment
Pasteurization
Alt. (2) Process to Significantly Reduce Pathogens
Thermophilic
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaerobic Digestion
Air Drying
Composting
Aerobic Digestion
If applicable to alternative performed (Class A or Class Bl comulete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
733
741
745
CFU/g
0
4 /Yr
grab
SM9222D
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Alt, 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench) X
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/1 SA NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Lewis, WWTP
da and Title 6r*�pprint) � Land Applier Name and Title (if applicable) (type or print)
of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
Page 1
9/11/2019
Oxford
9J4/2019
Meritech Worlc Order # 09041940 Sample: Qxford Fecals Fecal 1 Grab 9/4/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.23 % 9/6/19 0400 % SM 2540B
Fecal Coliform (Sludge) <739 col/g drywt 9/4/19 739 col/g dry wt SM 9222D
Meritech Worlc Order # 09041941 Sample: Oxford Fecals Fecal 2 Grab 9/4/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.23 % 9/6/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <739 col/gdry wt 9/4/19 739 col/gdrywt SM 9222D
Meritech Work Order # 09041942 Sample; Oxford Fecals Feca13 Grab 9/4 j19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.22 % 9/6/19 0400 % SM 2540B
Fecal Coliform (Sludge) <745 col/g dry wt 9/4/19 745 col/g dry wt SM 9222D
Meritech Work Order # 09041943 Sample: Oxford Fecals Fecal 4 Grab 9/4/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.24 % 9/6/19 0400 % SM 2540B
Fecal Coliform (Sludge) <733 col/g dry wt 9/4/19 733 col/g dry wt SM 9222D
Meritech Work Order # 09041944 Sample: Qxford Fecals Fecal 5 Grab 9/4 j19
9
Parameters Results Analysis Date Reporting Limit Method
........................................................._..............................a.._..........._........._... -....__........_......_.........................
% Total Solids 122 % 9/6/19 0-100 % SM 2540B
Fecal Coliform (Sludge) <745 col/g drywt 9/4/19 745 col/g drywt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.{336)34Z-4748 fax.{336)34Z-1522

Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Envlironmental Laboratory
Laboratory Certification No.165
Report Date
Projecfi:
Date Sample Rcvd:
Page 2
9/11/2019
Oxford
2019
Meritech Work Order # 09041945 Sample: Oxford Fecals Fecal 6 Grab 9/4/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.22 % 9/6/19 0400 % SM 2540B
Fecal Coliform (Sludge) <745 col/g dry wt 9/4/19 745 col/g dry wt SM 9222D
Meritech Work Order # 09041946 Sample: Oxford Fecals Feca17 Grab 9/4/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.23 % 9/6/19 0-100 % SM 2540E
Fecal Coliform (Sludge) <739 col/g dry wt 9/4/19 739 col/g dry wt SM 9222D
I hereby certify that I have teviewed and approve these data.
Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(33b)342-4748 fax.(336�342-1522

si9na
Chain of Custody Record (COC)
NPDES#:
MERITECH,i. Co
Client:-�
Phone:
Address: i +`� p6mr. ,,ql
Fax:
ENVIRONMENTAL LABORATORIES
r o;; iu'c ��
Email:
642Tamco Rd. Phone: [phone]
Project: r�"D
;i
`i }
: Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: {� !"C110k
Turn Around Time*
Wc
*RUSH work needs prior approval,
www.meritechlabs.com
How would you like your report sent?
'
char es Ao Div
Stcl 10
Circle all that apply: Email (pr erred) , Fax, Mail
s) 3-5 DaVS 24-48Hrs
Sampling Dates & Times
Person Taking Sample (SignfPrint :
Lab 115E Only
Sample Location and/or ID #
Start
End
comp?
#of
Test(s) Required
On Ice?
pH OK.
Time
Date
Time
Crab?
Cont.
Yes / No
CI OK?
f({€�late
lr
p
Ci3.• l�
3
�
I
i
Temperature Upon
Receipt:
Method Of
*** aechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN
samples must be done in the
field prior to preservation. ***
%''
Shipment:
Comments:
Compositor #
UPS
Jug#
Fed Ex
Are these results for regulatory purposes? Yes
No
Report
results in: mgf L ( mg/k
ug/L [.
'Delivery
Relinquished by: ;� ' x Date: c.
i,Hand vpt;Li4 '(y i
Time: z
= �
Received b y:
Date: I
Time:
Other
Relinquished by: Date:
Time:
Received by:
Date:
Time:
Relinquished by: Date:
Time:
eve
ale
Ti e

Lab result Log
739 2.87
739 2,87
745 2.87
733 2,87
745 2,87
745 2.87
739 2,87
Average 2.87
FECAL DATA SHEET
Min 733
Max 745
Geometric Mean 741

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Vector Attraction Reduction / Aerobi
Report Date
Project:
Date Sample Rcvd:
10/10/2019
Oxford
92019
Sludge (30 Day Test
Meritech Worlc Order # 09Q41939 Sample: Oxford Effluent Composite 9/4/19
Total Solids Volatile Solids % Volatile Solids
Week 1 1.10 O.b44 OS80
Weelr 2 0.970 0.570 0,591
Week 3 1.14 O.b70 0.589
Week4 1.Q0 0.570 0.571
Week 5 0.940 0.560 0.594
Kleecic Reduction (%): -5.81
I hereby certify that I have reviewed and approve these data. I �
Laboratory Representative
642 Tamca Road, Reidsville, North Carolina 27320
tel.(336)34Z-4748 fax.[phone]

5.9-20I6
Milliiiiiii
Chain of Custody Record (COC)
Clients
+
NPDES#:
Phone:
INC.
MERITELACHA+1
p
Address
61
Fax:
„
ENVIRONMENTAL LABORATORIES
��C74 dG�yi
r d.1t
Email: f r�l't1
� S:s� � e;.�.�j
'° �4tr'
"
642 Tamco Rd. Phone: [phone]
Project: gg
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:
Turn Around Time*
How would you I*Ikpy ur
*RUSH work needs prior approval.
report sent?
w1/w.meI'itc ClabS.C®li"iti
Std 10
5) s 24-48Hrs
Circle
all that apply Email (pr
_
erred) , Fax, Mail
Sampling Dates �z Times
Person Taking
Sample (Sign/Print):
...
; ::.I a4:1Js.:Ondy::::.
Sample Location and/or ID #
Start
End
comp?
#of
Test(s) i
orrice?. Yes:;.:.PH:-OK?.
Date
Time
Date
Time
Grab?
Cont.
I e u red
Cl OKP?
777
EFF
1J�
1V c 3
G�j
..........
..
L3�'i�iJi�ti
1 Fc�v-Zv+�.+
..
Temperature, Upon Receipt:
***
4i
Method of
Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field
prior to preservation.
Shipment:
Comments:
Corripositor,#:::':`:
UPS
Fed Ex
Are these results for regulatory purposes? Yes
No [
Report
results in: mg/L mg/kg
ug/L
Hand Deiivery
Relinquished by: ��� Date: �y Time:
L,? 1` d�j$
9
Received by:
Date:
Time;
,a
Other
Relinquished by: Date: Time:
Received by:
Date:
rime:
Relinquished by: Date: Time:
eive ab: a e:
Time:
Ell

%VSR
(older, more conservative method)
%VS in 1 0.5800 Enter in
%VS Out 1 0.5940 "-' decimal form
%VSR-_
((%VS in - (%VS in x %VS out))
%VSR= -5.95
(method from p.132 of WH manual)
%VS in
%VSR= -2.41
Results must be either greater than 38%; less than 17%fora 40-day scale test; test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City Of Oxford WWTP
WWTP Name: Oxford WWTP
WQ Permit Number: WQ0011244
NPDES Number: NC 0025054
Monitoring Period: From 10/1/2019 To 12/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.11061- ease indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class Bl complete the followinu mnnitnrinu data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
1.823
4,682
7,554
CFU/g
0
4 /Yr
Grab
9222D
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Alt, 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
.
(30-day bench) X
Option/Alt3
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt, 8
(Drying — Unstable)
were performed
No vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 021.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Antoine Leis. WWTP Superintendent
Ir
.�.
�.
rt
Land Applier Name and Title (if applicable) (type or print)
IMI
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Pa
503.9(r) and 15A NCAC 2T.1102 (26)

Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
Page 1
11/19/2019
Oxford
11/6/2019
Meritech Work Order # 11061977 Sample: Oxford 1 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Meth
od
% TotaI Solids 3.49 % 11/8/19 0400 % SM 2540B
Fecal Coliform (SIudge) 1,823 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061978 Sample: Oxford 2 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.46 % 11/8/19 0400 % SM 2540B
Fecal Coliform (SIudge) 5,255 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061979 Sample: Oxford 3 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.53 % 11/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 6,696 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061980 Sample: Oxford 4 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% TotaI Solids 3.72 % 11/8/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 4,399 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061981 Sample: Oxford 5 Grab
Parameters Results Analysis Date
% Total Solids 3.49 % 11/8/19
Fecal Coliform (Sludge) 7,554 col/g dry wt 11/6/19
Re orting Limit Method
0-100 % SM 2540B
508 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[336)342-1522

fi
'may'
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
Page 2
11/19/2019
Oxford
11/6/2019
Meritech Work Order # 11061982 Sample: Oxford 6 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.51 % 11/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 4,144 col/g dry wt 11/6/19 508 col/g dry wt SM 9222D
Meritech Work Order # 11061983 Sample: Oxford 7 Grab 11/6/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.58 % 11/8/19 0400 % SM 2540B
Fecal Coliform (Sludge) 5,587 col/g dry wt 11/6/19 494 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data,
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone]$ fax.[phone]

8�9�18
Chain of Custody Record (COC)
NPDES#:
C
Client: J�1fsGt�
Phone:5�(,'%U��wg5w
MERITECH IIVC.
1
Address: ZOOL) 15CG�C� !j'I)
Fax:
ENVIRONMENTAL LABORATORIES
Io( ✓SV W ALL ML
Email: dPRAnfO
i
642Tamco Rd. Phone: [phone]
Project:y�OM
"
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
ln
Attention: (Z AP z'C1 m)
Turn Around Time*
How would you like your report
*RUSH work needs prior approval,
sent? Char Anply
www.meritechiabs.com
Circle all that apply CEI preferred),
Fax, Mail Std, da
es
s) 3-5 Des 2rs
Sampling Dates & Times
Person Taking Sample (Sign/Print): r7 ,I�
�1��
Lab Use Only
Sample Location and/or ID #
L
Start
End
Comp?
#of
Test(s) Required
Yes
pH ?
Date
Time
Date
Time
Grab?
Cont.
es N
/ No
Cl OK?
v�r-�n ���
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F
2
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< L,
5
Temperature Upon
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples must be done in the field prior to preservation. ***
Receipt: NO
Shipment,
Comments:
Compositor #
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes
❑
No ❑ Report results in: mg/L ❑ mg/kg
❑ ug/L ❑
Hand Delivery
Relinquished by: U Date:
Lo�F
Time:
7- t
Received b
y.
Date:
Time:
❑ Other
Relinquished by: Date:
Time:
Received by:
Date:
Time:
Relinquished by: Date: Time:
Received Lab; a r,
--qme:�

Lab result Log
1823 3,26
5255 3,72
6696 3,83
41399 3,64
7554 3,88
4144 3,62
5587 3,75
Average 167
FECAL DATA SHEET
Min
Max
Geometric Mean
1823
7554
4682

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No,165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Vector Attraction Reduction / Aerobicall
Meritech Work Order # 11061976
Sample: Oxford Grab
Total Solids Volatile Solids
Week 1 1.09 0.590
Week 2 1.26 0.730
Week 3 1.22 0.700
Week 4 1.13 0.650
Week 5 1.03 0.590
Van Kleeck Reduction (%): -12.91
I hereby certify that I have reviewed and approve these data.
Report Date: 12/12/2019
Project: Oxford
Date Sample Rcvd: 11/6/2019
Sludge (30 Dav Test
�o Volatile Solids
0.540
0.577
0.570
0.572
0.570
ILI Ai I �_� _ I .�
642 Tamco Road, Reidsville, North Carolina 27320
tel.[336)342-4748 fax.[phone]

5-9.2016
Chain of Custody Record (COC)
NPDES#:
MEpA RITECH, INC.
1'
Client: si)(�{Z�
Phone,
Address: Zcb 0 � P—�
� Fax:
ENVIRONMENTAL LABORATORIES
IV�b(.IC5�1Ci-(� N�-
Email:(.De4
642 Tamco Rd. Phone: [phone]
Project:
OpFao
' /
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: ��I�rJ �FI=1l�rtil(�
Turn Around Time*
HOW WOUId OU lil<
y yaur
7
report sent.
*RUSH
work needs prior approval.
VVWW.merlteCillabS.C®m
Circle all that apply: Email ( ferred), Fax, Mail
Std 10
Al
rs) s z5
Sampling Dates &Times
p g
Person Taking Sample (Sign/Print):
Vi 'A-;,n
Lab Use Only
Sample Location
and/or ID #
Start
End
Comp?
Grab?
#of
Cont,
Test(s)
Required
On Ice? Yes
/ No
pH OK?
CI OK?
Date
Time
Date
Time
nn
Eti
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O -:ors =,= 1)GtNIrr
IiAt, N
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L�-1 � C/�JT =Jr2
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Temperature upon Receipt:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
1 )
Method of
Shipment:
Comments:
Compositor #
Jug #
❑ UPS
❑ Fed Ex
Are these results for regulatory purposes? Yes 116
No ❑ Report
results in: mg/L
❑ mg/kg
We
❑ ug/L ❑
Hand Delivery
Relinquished by: N ? Date: I Time: `�
l
. �5 Received by:
Date:
Time:
❑ Other
Relinquished by: Date: Time:
Received by:
Date:
Time:
Relinquished by: Date: Time:
Re ed by L
D
TirmS—�

%VS R
(older, more conservative method)
%VS in 1 0,54001 Enter in
o
/oVS out 1 0.5700 decimal form
%VSR_
((%VS in - (%VS in x %VS out))
%VSR= -12.92
(method from p.132 of WH manual)
%VS in
%VSR= -5.56
Results must be either greater than 38%; less than 17% fora 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

Agricultural Lime Application Log
Year: 2019
Project:
OXFORD
Field
(state-county,site field code)
Soil pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date Applied
NC-GR-1-1
6.1
0.0 tons/ac.
NC-GR-4-3
6.0
0.0 tons/ac.
NC-GR-4-2
6.5
0.0 tons/ac.
NC-GR-13-1
5.9
0.1 tons/ac.
NC-GRA3-2
5.9
0.1 tons/ac.
NC-GRA 3-3
6.0
0.0 tons/ac.
NC-GR-134B
5.7
0.3 tons/ac.
.5T/Acre
Ordered
NC-GR-60-01
5.7
0.3 tons/ac.
.5T/Acre
Ordered
NC-GR-6M2
6.0
0.0 tons/ac.
NC-GR-6M3
5.0
1.0 tons/ac.
IT/Acre
Ordered
NC-GR-60-04
5.4
0.7 tons/ac.
1T/Acre
Ordered
NC-GR-60-05
5.3
0.8 tons/ac.
1T/Acre
Ordered
NC-GR-60-06
5.6
0.4 tons/ac.
.5T/Acre
Ordered
NC-GR-6M7
6.3
0.0 tons/ac.

NCDA&CS Agronomic Division Phone: (919)
733-2655
Website: www.ncagr.gov/agronomi/
Report No. FY19-SL033831
predlctive
Client:
Henry Thorpe
Advisor:
�G�pULTURR�o
.. `'°2,�G
5676 Old Roxboro Rd.
2�° _
�
Soil
Report
Mehlich-3 Extraction
Oxford, NC 27565
wo b
,�
�, ,: ` �°,c
Sampled County
:Granville
.��� a��. Links to Helpful Information
Sampled:
Not Provided
Received:
06/17/2019
Farm: GR-5 / GR-1
Completed:
06/20/2019
Client ID: 279166
Advisor ID:
Sample ID: GR1-1
Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim,
M 0.0
120-200 0
60
0
0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WN
in g/crrt3; CEC and Na in meq/100 crrr3; NOs-N
in mg/drrt�]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P-I K-I
Ca% Mg%
S-I Mn-I
Mn-AI1
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.36 0.94 7.7
86 1.1 6.1
122 38
57 26
52 489
310
398
398
209 0.1 1
Sample ID: GR5-1
Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N PzOS
Kz0
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim,
M 0.4
120-200 0
10
0
0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - WN
in g/crrr3; CEC and Na in meq/100 crrr3; NOs-N
in mg/drrr3]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P-I K-I
Ca% Mg%
S-I Mn-I
Mn-AI1
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NOs-N
0.46 0.90 9.8
84 1.5 5.8
305 73
55 26
55 234
157
1324
1324
224 0.1 1
Sample ID: GR5-3
Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N P2Os
Kz0
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim,
M 0.0
120-200 0
40
0
0
0
0
0 0
Note: 12
2 _
0.0
Test Results [units - WN
in g/crrr3; CEC and Na in meq/100 crrr�; NOs-N
in mg/drrr�]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P-I K-I
Ca% Mg%
S-I Mn-I
Mn-AI1
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.27 1.00 9.1
89 1.0 6.2
299 50
55 32
46 194
131
1040
1040
236 0.2 2
Reprogramming of the laboratory -information -management system that -makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, CommissionerofAgriculture

NCDA&CS Agronomic Division Phone: (919)
733=2655 Website: www.ncagr.gov/agronomi/
Report No. FY19-SL033831
Henry Thorpe
Page 2 of 3
Sample ID: GR54
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim,
M 0.0
120-200 0
50
0
0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN
in g/crrr3; CEC and Na in meq/100 cm3; NO3-N
in mg/dnft
Soil Class:
Mineral
HM% W/V CEC
BS% Ac pH
P-1 K-I
Ca% Mg%
S-I
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.41 0.95 10.2
87 1 A 6.0
259 44
56 28
53
889
550
1147
1147
274
0.1
1
Sample ID: GR5-5
Recommendations:
Lime
Nutrients (Ib/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim,
M 0.3
120-200 50
80
0
0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units - W/V
in g/crrt3; CEC and Na in meq/100 cm3; NO3-N
in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P-1 K-1
Ca% Mg%
S-I
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.22 0.92 6A
81 1.2 5.8
38 28
50 29
61
293
193
151
151
86
0.1
2
Sample ID: GR5-6
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim,
M 1 A
120-200 0
60
0
0
0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN
in g/crrt ; CEC and Na in meq/100 cn73; NO3-N
in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC
BS% Ac pH
P-1 K-1
Ca% Mg%
S-I
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.56 0.90 9.9
76 2A 5.2
350 40
52 22
91
238
160
1946
1946
345
0.2
2

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. M9-SL033831
Henry Thorpe Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
I exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.html s#ind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizes
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/agronomi/uvrst.htm
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
Kz0 potash
Mg % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn-availability index for crop 1
Mn-A
Mn-I
12 Mn-availability index for crop 2
manganese index
M-O mineral -organic soil class
N nitrogen
Na sodium
NOs-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-I
phosphorus index
PzOs
S-I
SSW
phosphate
sulfur index
soluble salt index
WN weight per volume
Zn-AI zinc availability index
Zn-I zinc index

Page 1 of 1
Report No: 19-347-0532
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Alaypoi nt0
ANALYTICAL
Client: Eddie Denny
2850 Daisy Lane, Wilson, NC 27896
Main 252-2064721 ° Fax [phone]
www.waypointanalytical.com
Farm: GRA
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12/16/2019
Lab No Field ID Sample ID Soil Class HM•/ W/V pH Ac P-I K / S-I Mn-1 Zn-1 Zn Al Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N
21410 Fid 3 GR4-3 MIN 1.9 6.0 70.0 202 9 31 125 330 330 280 75A 7 5 2 0.1 0.1
Comment.
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY19-SL033838
�°ULTU�
4�G '9NdC Predictive Client: Eddy Denny Advisor: SYNAGRO
Y2� ,- °2�G 6633 Old Roxboro Rd 284 Boger Road
aS o i I Report Mehlich-3 Extraction Oxford, NC 27565 Mocksville, NC 27028
M
�, '�. ,:' �" Sampled County :Granville
���� ern. Links to Helpful Information Sampled: Not Provided
Received: 06/17/2019
Farm: GR-4 Completed: 06/20/2019 Client ID: 422576 Advisor ID: 499503
Sample ID: GR4-2 Recommendations: Lime Nutrients (Ib/acre) More
Crop (tons/acre) N PzOs Kz0 Mg S Mn Zn Cu B Information
Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 80 80 0 0 0 0 0 0 Note: 12
2 - 0.0
Test Results [units - WN in g/crrr�; CEC and Na in meq/100 cm3; NOs-N in mg/dnr3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-AI1 Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.32 1.04 9.7 90 1.0 6.5 24 30 54 35 44 935 571 313 313 140 0.1 1
ni_._,.� r-�_,.�:_._.
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: (919) 733=2655 Website: www.ncagr.gov/agronomi/
Report No. FY19-SL033838
Eddy Denny
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report
Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. Kd and P-I values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SSd levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-AI1
Mn-availability index for crop 1Mn=AI2
Mn-availability index for crop-2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
n-
MMnm I
manganese index
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs,htm.
NOs-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htrrrlsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-I
sulfur index
Test Results
SS -I
soluble salt index
WN
weight per volume
0 o
The first seven values [soil class, HM /o, W/V, CEC, BS /o, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mnd, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cud, Sd, SSd, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/agronomi1uyrst.htm

Page 1 of 1
Report No: 19-347.0524
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Naypol t T.,
ANALYTICAL
Client: Herb Morton
2850 Daisy Lane, Wilson, NC 27896
Main 252-2064721 ° Fax [phone]
www.waypointanalytical.com
Farm: GR-13
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12/16/2019
Lab No
Field /D
Sample ID
Soil Class
HM% W/V
pH
Ac
P4
K l
S-I
Mn-I
Zn-1
Zn-AI
Cu-I
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
21371
Fld
1-4
GR-13A
MIN
0.9
5.9
70.0
189
26
37
481
1060
1060
690
76.3
8
6
2
0.1
0.1
21372
Fld
1-4
GR-13-2
WO
3.6
5.9
70.0
137
14
29
525
378
472
560
75.6
8
6
1
0.1
0.1
21373
Rd
1-4
GR-13-3
MIN
1.3
6.0
70.0
97
17
29
575
513
513
425
76.6
9
7
2
0.1
0.1
21375
Fld
1-4
GRA3-413
MIN
1.1
5.7
70.0
133
22
42
200
543
543
250
74.3
6
5
1
0.1
0.1
Comment:
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water C2uality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-347-0512
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
maypolt T.,0
ANALYTICAL
Client: Jake Isley
2850 Daisy Lane, Wilson, NC 27896
Main 252-2064721 ° Fax [phone]
www.waypointanalyncal.com
Farm: GR-60
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12/16/2019
Lab No
Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-1
K I
S-I
Mn-I
Zn-I
Zn-AI
Cu-I
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
21336
Rd 1-7
GR-60 1
M-0
3.8
5.7
70.0
202
9
35
156
313
391
135
72.7
4
3
1
0.1
0.1
21337
Rd 1-7
GR-60 2
MIN
2.7
6.0
70.0
23
6
37
613
60
60
65
73.2
4
3
1
0.1
0.1
21338
Rd 1-7
GR-60 3
ORG
8.3
5.0
70.0
244
11
46
200
510
847
260
72.4
3
3
1
0.2
0.1
21339
Fld 1-7
GR-60 4
MIN
0.4
5A
70.0
369
13
52
150
705
705
265
73.5
5
4
1
0.2
0.2
21340
Fld1-7
GR-605
MIN
1A
5.3
70.0
217
12
58
175
468
468
240
72.7
4
3
1
0.2
0.1
21342
Ad 1-7
GR-60 6
MIN
0.8
5.6
70.0
256
11
37
181
440
440
175
73.0
4
3
1
0.2
0.1
21343
Fld 1-7
GR-60 7
MIN
0.9
6.3
70.0
227
11
64
450
1073
1073
430
79.0
11
8
3
0.2
0.2
Comment:
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are pertormed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.