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CL § (D 2 n 'r g = 7 S } R m o 2o < ID ■ g aM _�a� K § § g k ■ 2 M ■ a) CL § 2 CL 2 R r+ c ° M CD 0 § � - 2 lu 2 +CL = £ koCD � 2 �k CLR ƒ 2 ƒ m ƒ E m r+ 'D (Am Q o E v Q cr B 2 .] 0.A VQ .§ / c m ■ 21, J o n) F r e 0 c C 2 o ° .] (A E, r CL E 2 E G J2 t ® r E o g rp V M § m g § S ■ o k0m J k CD m o § .§ 2 2 gu § � k IL n ■ � o cr �E � Tier 1 Checklist Sampling Event Number SD000282 Sample Date Sampler Outfall Number Contract Laboratory Results Parameter (Units) 3/14/2016 Antwoine Howard RNC-SD001 or RNC SD002 ESC Lab Sciences Value Benchmark Values Benchmark Exceedance? BOD 17.9 30 mg/L NO COD 61 120 mg/L NO pH 6.75 Standard (6-9) NO Nitrate -Nitrite 0.67 10 mg/L NO Phosphorus,Total 0.46 2 mg/L NO Kjeldahl Nitrogen, I KN 3 20 mg/L NO Suspended Solids(TSS) 46.8 100 mg/L NO Tier I Checklist Stormwater inspection conducted within 2 weeks? Yes List of possible Causes leaves, product on ground from unloading/operations Potential Solutions housekeeping Actions Taken (include dates of implementation) inform Area supervisor Keep a record of all Tier 1 actions with facility SWPPP Ph' Tier 2 Checklist In addition to repeating t e steps or Tier 1, mont y samp ing is require or a parameters at every outfall where an exceedance was recorded until 3 consecutive sampling events results are below benchmarks. Sampling Event Number SD000282 Sample Date 3/14/2016 Sampler Antwoine Howard Outfall Number RNC-SD001 or RNC SDO02 Contract Laboratory ESC Lab Sciences Results RNC SD001 Parameter (Units) Value Benchmark Values Benchmark Exceedance? BOD 17.9 30 mg/L NO COD 61 120 mg/L NO pH 6.8 Standard (6-9) NO Nitrate -Nitrite 0.67 10 mg/L NO Phosphorus,Total 0.46 2 mg/L NO Kjeldahl Nitrogen, TKN 3 20 mg/L NO Suspended Solids(TSS) 46.8 100 mg/L NO Results RNC SDO02 Parameter (Units) Value Benchmark Values Benchmark Exceedance? BOD 0 30 mg/L NO TSS 0 100 mg/L NO Total Kjeldahl Nitrogen 0 20 mg/L NO Nitrate -Nitrite 0 10 mg/L NO Total Phosphorus 0 2 mg/L NO COD 0 120 mg/L NO pH 0 Standard NO * Keep a record of all Tier 1 actions with facility SWPPP Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 1 of 5 Raleigh, NC A Raleigh -Durham International 0 7:47 AM EDT on March 24, 2016 (GMT -04001 Weather History for KRDU - March, 2016 March 14 2016 View Monday, March 14, 2016 Daily Weekly Monthly Custom Actual Average Record Temperature Mean Temperature 69 OF 51 OF Max Temperature 80 OF 63 OF 86 OF (1973) Min Temperature 58 OF 39 OF 16 OF (1926) Degree Days Heating Degree Days 0 14 Month to date heating degree days 123 224 Since 1 July heating degree days 2266 2796 Cooling Degree Days 4 0 Month to date cooling degree days 22 0 Year to date cooling degree days 22 1 Growing Degree Days 18(Base 50) Moisture Dew Point 61 OF Average Humidity 73 Maximum Humidity 100 Minimum Humidity 45 Precipitation Precipitation 1.87 in 0.13 in 2.00 in (1999) Month to date precipitation 3.01 1.88 Year to date precipitation 9.42 8.61 https://www.wunderground. com/history/airport/KRDU1201613114IDailyHistory.html?req_... 3/24/2016 a a Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 2 of 5 Actual Average Record Snow Snow Tin 0.10 in T in (1951) Month to date snowfall 1.0 0.4 Since 1 July snowfall 2.4 5.9 Snow Depth 0.00 in Sea Level Pressure Sea Level Pressure 29.82 in Wind Wind Speed 4 mph (South) Max Wind Speed 32 mph Max Gust Speed 47 mph Visibility 8 miles Events Fog , Rain , Thunderstorm T = Trace of Precipitation, MM = Missing Value Source: NWS Daily Summary Daily Weather History Graph F 90 80 70 60 50 40 30 20 midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 in Hg Barometric Pressure 29.9 29.8 29.7 midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 mph midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 360.0 270.0 180.0 90.0 0.0 midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 Vm ,w report rI,;S ad i ,..4i.''f adsS Search for Another Location ,irport or City: KRDU Submit 0 32 27 21 16 10 4 -1 -7 hPa 1013 1009 1006 kmrh Trip Planner Search our weather history database for the weather conditions in past years. The results will help you decide how hot, cold, wet, or windy it https://www.wunderground. comlhistory/airport/KRDU1201613 / 14IDailyHistory. html?req_... 3 /24/2016 f I . Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 3 of 5 miqht be! Date: March 14 Submit report this ad =iiy adrs Astronomy Mar. 14, 2016 Rise Set Actual Time 7:26 AM EDT 7:22 PM EDT Civil Twilight 7:01 AM EDT 7:47 PM EDT Nautical Twilight 6:31 AM EDT 8:17 PM EDT Astronomical Twilight 6:01 AM EDT 8:47 PM EDT Moon 11:34 AM EDT (3/14) 12:47 AM EDT (3/14) Length of Visible Light 12h 46m Length of Day 11h 55m Waxing Crescent, 38%of the Moon is Illuminated Mar 14 Mar 15 Mar 23 Mar 31 Apr 7 Waxing Crescent First Quarter Full Last Quarter New report I:ins ad i vhy a, ls. Hourly Weather History & Observations Time [EDT] Temp. Heat Index Dew Point Humidity Pressure Visibility Wind Wind Gust Precip Events Conditions Dir Speed Speed 12:AM AM 64.4 °F 62.6 °F 94% 29.88 in 10.0 mi South 5.8 mph N/A Thunderstorm Thunderstorm M A AM 63.0 °F 62.1 OF 97 % 29.87 in 10.0 mi Calm Calm 0.00 in Thunderstorm Thunderstorm 1:09 64.4 °F 62.6 °F 94% 29.90 in 3.0 mi Variable 6.9 mph 18.4 mph 0.02 in Rain , Thunderstorms AM Thunderstorm and Rain 1:15 AM 64.4 °F 62.6 IF 94% 29.90 in 1.5 mi WNW 6.9 mph 18.4 mph 0.04 in Thunderstorm Heavy Thunderstorms and Rain 1:35 AM 64.4 IF 62.6 OF 94% 29.90 in 1.5 mi SW 4.6 mph 0.27 in Rain , Light Thunderstorms Thunderstorm and Rain M AM AM 64.4 IF 62.6 OF 94% 29.89 in 10.0 mi Calm Calm 0.27 in Overcast 1:51 AM 64.0 OF 62.1 OF 93 % 29.88 in 10.0 mi Calm Calm 0.27 in Overcast 2:51 AM 64.0 OF 63.0 OF 96% 29.86 in 10.0 mi South 4.6 mph 0.00 in Overcast https://www.wunderground.com/histoiy/airport/KRDU/2016/3/ 14/DailyHistory.html?req_... 3/24/2016 @ 1 - Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 4 of 5 Time Heat Dew Wind Wind Gust (EDT) Temp. Index Poirrt Humidity Pressure Visibility Dir Speed Speed Precip Events Conditions 3:51 AM 64.0 OF 62.1 IF 93 % 29.85 in 10.0 mi Calm Calm N/A Mostly Cloudy 4:51 AM 63.0 OF 62.1 IF 97 % 29.86 in 10.0 mi Calm Calm N/A Mostly Cloudy 5:06 AM 62.6 OF 62.6 IF 100% 29.87 in 5.0 mi Calm Calm N/A Overcast 5:19 62.6 OF 62.6 °F 100% 29.86 in 5.0 mi Calm Calm N/A Overcast AM 5:51 AM 63.0 IF 62.1 IF 97% 29.85 in 5.0 mi Calm Calm N/A Overcast 6,51 64.0 IF 63.0 OF 96% 29.87 in 7.0 mi Calm Calm N/A Overcast AM M AM AM 64.0 °F 63.0 IF 96% 29.88 in 5.0 mi Calm Calm N/A Fog Patches of Fog 8.26 AM 64.4 °F 64.4 OF 100% 29.89 in 7.0 mi Calm Calm N/A Overcast 8.51 AM 66.0 °F 64.0 OF 93% 29.89 in 7.0 mi SW 4.6 mph N/A Mostly Cloudy 9:51 AM 66.9 OF 64.9 °F 93% 29.88 in 9.0 mi Calm Calm N/A Mostly Cloudy I AMm 70.0 OF 64.0 OF 81% 29.88 in 10.0 mi SW 4.6 mph N/A Mostly Cloudy 11:51 73.0 IF 63.0 OF 71% 29.87 in 10.0 mi Variable 4.6 mph N/A Scattered AM Clouds 12:51 PM 75.0 OF 63.0 IF 66% 29.87 in 10.0 mi Calm Calm N/A Mostly Cloudy 1:51 PM 77.0 OF 61.0 IF 58% 29.83 in 10.0 mi SW 6.9 mph N/A Mostly Cloudy 2:51 PM 78.1 OF 57.9 OF 50% 29.79 in 10.0 mi Calm Calm N/A Mostly Cloudy PM M PM 80.1 OF 80.6 OF 57.9 OF 47% 29.77 in 10.0 mi WSW 6.9 mph N/A Mostly Cloudy PM M PM 75.0 OF - 60.1 OF 60% 29.76 in 10.0 mi Variable 3.5 mph 0.00 in Mostly Cloudy 5:51 PM 75.9 °F - 57.9 OF 54 % 29.74 in 10.0 mi SSE 10.4 mph N/A Mostly Cloudy 6:51 0 PM 71.1 F 63.0 F 75 /0 29.75 in 10.0 mi ENE 8.1 mph - N/A Mostly Cloudy 7:51 68.0 IF 62.1 °F 81 % 29.72 in 10.0 mi East 13.8 mph - N/A Overcast PM 8:15 66.2 OF 62.6 °F 88% 29.72 in 9.0 mi ENE 12.7 mph - 0.02 in Rain , Thunderstorms PM Thunderstorm and Rain 8:26 Rain , Heavy PM 64.4 IF 60.8 IF 88% 29.79 in 2.0 mi SW 32.2 mph 47.2 mph 0.02 in Thunderstorm Thunderstorms and Rain 8:30 Rain, Heavy PM 57.2 IF 57.2 OF 100% 29.77 in 2.0 mi WSW 19.6 mph 47.2 mph 0.24 in Thunderstorm Thunderstorms and Rain 8:39 Rain, Heavy PM 59.0 OF 59.0 IF 100% 29.75 in 2.0 mi NW 8.1 mph 19.6 mph 0.80 in Thunderstorm Thunderstorms and Rain https: //www.wunderground. com/historylairportlKRDU1201613 / 14IDailyHistory.html?req_... 3 /24/2016 Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 5 of 5 Time (EDT) Temp. Heat Index Dew Point Humidity Pressure Visibility Wired Wind Gust Precip Events Conditions Dir Speed Speed 8:45 60.8 OF 59.0 OF 94% 29.76 in 4.0 mi WSW 3.5 mph 0.84 in Rain , Thunderstorms PM Thunderstorm and Rain 8:51 PM 60.1 OF 59.0 OF 96% 29.75 in 10.0 mi Variable 3.5 mph 0.84 in Rain , Light Thunderstorms Thunderstorm and Rain 9:01 PM 62.6 IF 59.0 IF 88% 29.76 in 10.0 mi West 4.6 mph 0.00 in Rain Light Rain 9:51 PM 61.0 OF 59.0 OF 93 % 29.77 in 10.0 mi NE 8.1 mph 0.00 in Overcast 10:04 60.8 IF 57.2 °F 88% 29.76 in 10.0 mi ENE 5.8 mph 0.00 in Rain , Thunderstorms PM Thunderstorm and Rain 10,15 PM 60.8 OF 59.0 OF 94% 29.78 in 4.0 mi Variable 5.8 mph 0.06 in Rain , Heavy Thunderstorms Thunderstorm and Rain 10:25 PM 60.8 OF 59.0 IF 94% 29.79 in 3.0 mi NE 9.2 mph - 0.33 in Rain , Heavy Thunderstorms Thunderstorm and Rain 10:43 PM 62.6 OF 60.8 OF 94% 29.77 in 9.0 mi East 11.5 mph 20.7 mph 0.70 in Rain Light Rain 10:51 PM 62.1 OF 60.1 IF 93 % 29.76 in 10.0 mi ENE 4.6 mph - 0.70 in Rain Light Rain 11:06 PM 62.6 OF 60.8 IF 94% 29.77 in 1.0 mi ENE 4.6 mph 0.00 in Rain , Heavy Thunderstorms Thunderstorm and Rain 11:1PM PM 62.6 OF 60.8 OF 94% 29.76 in 10.0 mi ENE 6.9 mph 0.06 in Mostly Cloudy 11:5 PM PM 11 62.1 OF 59.0 OF 90% 29.75 in 10.0 mi SW 4.6 mph 0.06 in Mostly Cloudy https://www.wunderground. com/history/airportlKRDU1201613114IDailyHistory.html?rec_... 3/24/2016 OUTFALL 001 SAMPLE RESULTS -'01 `%NELAB. NATIONWIDE. Collected date/time: 03/14/16 23:20 L823562 Gravimetric Analysis by Method 2540 D-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time ..1 Suspended Solids 46.8 2.50 1 03/17/201610:50 WG356.�1 Wet Chemistry by Method 351.2 E Result Qualifier RDL Dilution Analysis Batch Analyte mg/I 11 11 1111111— mg/I 11 date / time ., Cn Kjeldahl Nitrogen, TKN 3.00 0.250 1 03/23/20116 08:43„ a �bSl'17 Wet Chemistry by Method 353.2 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time C C Nitrate -Nitrite 0.671 0.100 1 03/21/201617:36 W(,857120 �GI !Net Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch AnalIyte mg/I mg/I date / time AI Phosphorusjotal 0.457 0.100 1 03/17/201617:57 WG357029 SC Wet Cnell-listry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time COD 61.0 10.0 1 03/18/201612:57 WG&570141 Wet Chemistry by Method 450OH : B-2011 Result Qualifier Dilution Analysis Batch Analyte su date / time pH 6.75 1 03/16/201613:02 r.856819 Sample Narrative: 4500H+ B-2011 L823562-01 WG856819: 6.75 at 13.9c Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time BOD 17.9 3.33 1 03/21/2016 09:00 G856835 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Cargill, Inc. L823562 03/23/1615:37 5 of 17 �,. �L, ,.. ; Cr w, s-w� n 5 «tl -4 _m'^ M C .,au..., °t `.. Yell Ln c r IM Rt > to x.: Gt. 0 ut. 3 1 s n'rc $r , i x 't-Liter HOPE w/no preserv. BOO: x ILiter i CAPE wtno preserv. pH. 9 x 12 ml HDPE w/no preserv. '. NitratetNMIte 1 x 500ml HDPE wt5ml Sulfuric Acid preserv. COD: (Corribine /NitrateINItrite Bottle) KN: (Combine wihtitrateMitrite Bottle) Total Phosphorous, iCombine w/Nitratel itrite Bottle) 3 8 0 c t' 6 yvk+lk ��A i, 71. i n. 01 u ([°o c, °e to co x ao w /oq% QiN1,611" DEMLR — Storm water Permitting Program Attn: Storm water Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE. Cargill, Incorporated, Raleigh, NC — Storm water Discharge Permit NCS000282 Year 5, Period 2 - Analytical Monitoring Results March 14, 2016 In accordance with the Cargill, Raleigh facility's Storm water Discharge Permit NCS000282, Part III, Section E, Cargill is submitting Discharge Monitoring Reports for the Year Five, Period Two monitoring period. The monitoring was completed on September 8"' 2014 during characteristic storm event. SDO01 Characteristic Benchmark Lub Results Tier 3/14/2016 COD 120 mg/L 61 1 3/14/2016 BOD 30 mg/L 17.9 1 3/14/2016 Total Phosphorus 2 mg/L 0.457 1 3/14/2016 TKN 20 mg/L 3 1 SDO02 Characteristic Benchmark Lab Results Tier COD 120 mg/L BOD 30 mg/L Total Phosphorus 20 mg/L TSS 100 mg/L If there are any questions regarding this submittal please feel free to contact me at (919) 899-6604. Sincerely, Michael Klauke Plant Superintendent Cargill, Incorporated Raleigh, NC 1400 S. Blount Street Raleigh, NC27603-2506 ciirdllf DEMLR — Storm water Permitting Program Attn: Storm water Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 April 12, 2016 ';CEIVE® MAY 10 ZU16 CENTRAL FILES DWR SECTION RE: Cargill, Incorporated, Raleigh, NC — Storm water Discharge Permit NCS000282 Year 5, Period 2 - Analytical Monitoring Results In accordance with the Cargill, Raleigh facility's Storm water Discharge Permit NCS000282, Part III, Section E, Cargill is submitting Discharge Monitoring Reports for the Year Five, Period Two monitoring period. The monitoring was completed on September 8t` 2014 during characteristic storm event. L3 SDO01 Characteristic Benchmark lab Results Tier 4/12/2016 COD 120 mg/L 83.3 1 4/12/2016 BOD 30 mg/L 22.7 1 4/12/2016 Total Phosphorus 2 mg/L 0.611 1 4/12/2016 TKN 20 mg/L 4.11 1 SDOO2 Characteristic Benchmark Cab Results 7Tier COD 120 mg/L BOD 30 mg/L Total Phosphorus 20 mg/L TSS 100 mg/L If there are any questions regarding this submittal please feel free to contact me at (919) 899-6604. Sincerely, Michael Klauke Kdoo 3111 Plant Superintendent Cargill, Incorporated Raleigh, NC 1400 S. Blount Street Raleigh, NC 27603-2506 Ln U) O fD e m - C O < p m IDz O O ems-* rD rn Z - m v m m c v ( m r+ z X. fl m art (I rn m �+ (p y O C e r a) N u c rt O n S r+ O ^ •y; n N rt = O v O ... Q V ^_ 'yh k O' O" O CD v S 't O N S v O c v(Di W rl• � .. 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Q O O r M m -{ ,+ v w r cn Z -G ° o m m G) O < + -p -� Z i �-SO m v 0 _h Z to D ^• a C m < M 70 rn ;° n rr (D S n m m °0i M v � (D- m (n m 4�- s y. Z v M O V 4�J 3 ° m D M m NO C 07 O w O v � � &|� � e � � ._] � ■ .■ / m 2 g A \ C>=COL r m 0)■ o § ` m fu / CL ¢ m 2 n - ƒ 2 § § 2 eD 0 2 -h < m $ k v FD � - -�E2 ƒ eo a CL & R tu c \2 � § ■ M�2� TE�tu � g ■ / a § J W tu CL n -1 t 2 2 § & ( - Emm ° 0 e cr n§ 2 •� E rCL 22ƒ§ (D 2 m 0 7 § « B CL ? r e / 2 ) $c CL g 0 o .§R _ ( C r CL" 2 0—a _ _ o M= r+ E 0 k o o J fu \ �. s 7 0 § § 2 2 0 § C § 2 aw.�_ tog § k E E k � Tier 1 Checklist 6 4 Sampling Event Number SD000282 Sample Date 4/12/2016 Sampler Antwoine Howard Outfall Number RNC-SD001 or RNC SDO02 Contract Laboratory ESC Lab Sciences Results Parameter (Units) Value Benchmark Values Benchmark Exceedance? BOD 22.7 30 mg/L NO COD 83.3 120 mg/L NO pH 6.36 Standard (6-9) NO Nitrate -Nitrite 0.48 10 mg/L NO Phosphorus,Total 0.61 2 mg/L NO Kjeldahl Nitrogen, TKN 4.11 20 ing/L NO Suspended Solids(TSS) 29.3 100 mg/L NO Tier I Checklist Stormwater inspection conducted within 2 weeks? Yes List of possible Causes leaves, product on ground from unloading/operations Potential Solutions housekeeping Actions Taken (include dates of implementation) inform Area supervisor Keep a record of all Tier 1 actions with facility SWPPP Tier 2 Checklist n addition to repeating the steps for Tier 1, monthly sampling is required for all parameters at every outfall where an exceedance was recorded until 3 consecutive sampling events results are below benchmarks. Sampling Event Number SD000282 Sample Date 4/12/2016 Sampler Antwoine Howard Outfall Number RNC-SD001 or RNC SD002 Contract Laboratory ESC Lab Sciences Results RNC SDOO1 Parameter (Units) Value Benchmark Values Benchmark FxrPPdanrP7 BOD 22.7 30 mg/L NO COD 83.3 120 mg/L NO pH 6.4 Standard (6-9) NO Nitrate -Nitrite 0.48 10 mg/L NO Phosphorus,Total 0.61 2 mg/L NO Kjeldahl Nitrogen, TKN 4.11 20 mg/L NO Suspended Solids(TSS) 29.3 100 mg/L NO Results RNC SD002 Parameter (Units) Value Benchmark Values Benchmark Exceedance? BOD 0 30 mg/L NO TSS 0 100 mg/L NO Total Kjeldahl Nitrogen 0 20 mg/L NO Nitrate -Nitrite 0 10 mg/L NO Total Phosphorus 0 2 mg/L NO COD 0 120 mg/L NO pH 0 Standard NO * Keep a record of all Tier 1 actions with facility SWPPP Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 1 of 6 rep,c)rt. this ad Raleigh, NC Raleigh -Durham International Weather History for KRDU - April, 2016 12 m View Tuesday, April 12, 2016 Daily Weekly Monthly Custom Temperature Mean Temperature Max Temperature Min Temperature Degree Days Heating Degree Days Month to date heating degree days Since Duly heating degree days Cooling Degree Days Month to date cooling degree days Year to date cooling degree days Growing Degree Days Moisture Dew Point O 10:33 AM EDT on April 20, 2016 (GMT -0400) Actual Average Record 60 ° F 64 °F 55 °F 5 116 2493 0 8 46 10 (Base 501 57 ° F 59 ° F 72 ° F 47 ° F 7 98 3094 1 12 24 94 ° F (1930) 26 ° F (1973) https://www.wunderground.com/history/airport/KRDU/2016/04/ 12/DailyHistory.html?req... 4/20/2016 Weather History for Raleigh -Durham Airport, NC I Weather Underground Actual Average Average Humidity 84 Maximum Humidity 100 Minimum Humidity 67 Precipitation Precipitation 0.85 in 0.10 in Month to date precipitation 1.20 1.25 Year to date precipitation 11.65 12.09 Snow Snow 0.00 in 0.00 in Month to date snowfall 0.0 0.1 Since 1 July snowfall 1.4 6.1 Snow Depth 0.00 in Sea Level Pressure Sea Level Pressure 30.11 in Wind Record 1.65 in (1959) T in (1918) Page 2 of 6 Wind Speed 9 mph (SW) Max Wind Speed 18 mph Max Gust Speed 28 mph Visibility 6 miles Events Fog , Rain T = Trace of Precipitation, MM = Missing Value Source: NWS Daily Summary Daily Weather History Graph https://www. wunderground. com/history/airport/KRDU/2016/04/ 12/DailyHistory.html?req... 4/20/2016 Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 3 of 6 F Temperahrre Dew Point Normal Highll.ow 75 _. .. ..... ..... �_ .. , 70 _... 65 _. 60 .,. -.v _ _- 50 '._. 40 midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 in Hg Earomelric Pressure 30.3 30.2 30.1 30.0 midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 nnh p 30.0 25.0 20.0 15.0 10.0 5.0 0.0 midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 C 24 21 16 1 4 hpa 1026 1023 1019 1016 kmrh 48 40 32 24 16 8 0 Search for Another Location Airport or City: KRDU Submit Trip Planner Search our weather history database for the weather conditions in past years. The results will help you decide how hot, cold, wet, or windy it might be! Date: April 12 Submit Astronomy Apr. 12, 2016 Rise Set Actual Time 6:45 AM EDT 7:46 PM EDT https://www.wunderground. com/history/airport/KRDU/2016/04/12/DailyHistory.html?req... 4/20/2016 Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 4 of 6 Apr.12, 2016 Rise Set Civil Twilight 6:19 AM EDT 8:12 PM EDT Nautical Twilight 5:48 AM EDT 8:44 PM EDT Astronomical Twilight 5:15 AM EDT 9:16 PM EDT Moon 11:12 AM EDT (4/12) 12:37 AM EDT (4/12) Length of Visible Light __ --------- _------------- _ -------- 13h 53m Length of Day 13h O1m Waxing Crescent, 34% of the Moon is Illuminated Apr 12 Apr 14 Apr 22 Apr 29 May 6 Waxing Crescent First Quarter Full Last Quarter New report this ad ,,:hy f ds? I lourly Weather I listory & Observations Time Dew Wind Wind Gust (EDT) Temp. Point Humidity Pressure Visibility Dir Speed Speed Precip Events Conditions 12:51 AM 62.1 OF 52.0 OF 70% 30.12 in 10.0 mi SSW 15.0 mph 21.9 mph N/A Overcast 1:51 AM 62.1 OF 52.0 OF 70% 30.09 in 10.0 mi SSW 13.8 mph - 0.00 in Rain Light Rain 2:51 AM 60.1 OF 54.0 OF 80% 30.09 in 5.0 mi SSW 9.2 mph 17.3 mph 0.00 in Rain Light Rain 3:51 AM 59.0 IF 55.0 IF 87% 30.10 in 5.0 mi SSW 10.4 mph - 0.02 in Rain Light Rain 4:51 AM 57.9 IF 55.9 IF 93% 30.09 in 3.0 mi SSW 6.9 mph - 0.08 in Rain Rain 5:25 AM 57.2 °F 55.4 OF 94% 30.10 in 3.0 mi SW 6.9 mph - 0.05 in Rain Light Rain 5:51 AM 57.9 OF 55.9 OF 93% 30.10 in 3.0 mi SSW 11.5 mph - 0.09 in Rain Rain 6:14 AM 57.2 OF 55.4 OF 94% 30.10 in 3.0 mi SSW 9.2 mph - 0.05 in Rain Light Rain 6:36 AM 57.2 IF 55.4 IF 94% 30.10 in 3.0 mi SSW 11.5 mph - 0.09 in Rain Light Rain 6:51 AM 57.9 OF 55.9 OF 93% 30.10 in 6.0 mi SSW 12.7 mph - 0.10 in Rain Light Rain 7:51 AM 59.0 OF 55.9 °F 90% 30.09 in 3.0 mi SSW 9.2 mph 21.9 mph 0.05 in Rain Light Rain https://www.wunderground. com/history/airport/KRDU/2016/04/ 12/DailyHistory.html?req... 4/20/2016 Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 5 of 6 Time (EDT) Temp. Dew Point Humidity Pressure Visibility Wind Dir Wind Gust Precip Events Conditions Speed Speed 8:51 AM 59.0 IF 57.0 IF 93% 30.09 in 6.0 mi SW 12.7 mph 0.02 in Rain Light Rain 9:51 AM 60.1 IF 57.9 IF 93% 30.09 in 6.0 mi SW 15.0 mph - 0.04 in Rain Light Rain 10:51 AM 60.1 IF 57.9 IF 93% 30.10 in 4.0 mi WSW 8.1 mph 0.03 in Rain Light Rain 11:51 AM 61.0 IF 59.0 IF 93% 30.09 in 6.0 mi WSW 9.2 mph - 0.05 in Rain Light Rain 12:51 PM 62.1 IF 60.1 IF 93% 30.09 in 7.0 mi SW 11.5 mph - 0.02 in Rain Light Rain 1:51 PM 62.1 OF 60.1 OF 93% 30.08 in 4.0 mi SW 9.2 mph - 0.04 in Rain Light Rain 2:51 PM 62.1 IF 60.1 OF 93% 30.07 in 6.0 mi WSW 8.1 mph - 0.05 in Rain Light Rain 3:11 PM 62.6 IF 60.8 IF 94% 30.08 in 5.0 mi WSW 5.8 mph - 0.02 in Rain Light Rain J.51 PM 62.1 IF 60.1 IF 93% 30.07 in 3.0 mi WSW 6.9 mph - 0.08 in Rain Light Rain 4:10 PM 60.8 OF 59.0 OF 94% 30.07 in 1.5 mi West 4.6 mph - 0.05 in Rain Rain 4:36 PM 60.8 OF 60.8 °F 100% 30.07 in 4.0 mi Calm Calm - 0.17 in Rain Light Rain 4:51 PM 62.1 OF 57.9 IF 86% 30.06 in 6.0 mi WSW 3.5 mph - 0.18 in Rain Light Rain 5:51 PM 62.1 IF 60.1 IF 93% 30.08 in 10.0 mi SW 4.6 mph - 0.00 in Mostly Cloudy 6:51 PM 63.0 IF 60.1 IF 90% 30.09 in 10.0 mi WSW 4.6 mph - N/A Mostly Cloudy 7:51 60.1 OF 57.9 IF 93% 30.10 in 10.0 mi Calm Calm - N/A Scattered PM Clouds 8:51 57.0 IF 55.9 OF 96% 30.12 in 10.0 mi ENE 3.5 mph N/A Fog Patches of PM Fog 9:51 57.0 OF 55.9 OF 96% 30.17 in 7.0 mi NE 4.6 mph - N/A Fog Patches of PM Fog 10:26 PM 57.2 OF 57.2 OF 100% 30.18 in 10.0 mi NE 12.7 mph 18.4 mph N/A Fog Patches of Fog 10:39 PM 57.2 °F 55.4 OF 94% 30.19 in 10.0 mi NE 13.8 mph 19.6 mph N/A Mostly Cloudy 10:51 PM 55.9 OF 55.0 IF 97% 30.19 in 10.0 mi NE 11.5 mph - N/A Mostly Cloudy 11:24 55.4 °F 48.2 OF 77% 30.22 in 10.0 mi NNE 11.5 mph - N/A Mostly PM Cloudy https://www.wLinderground. com/history/airportlKRDU/2016/04/ 12/DailyHistory.html?req... 4/20/2016 Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 6 of 6 Time Temp. Dew Humidity Pressure Visibility Wind Wind Gust Precip Events Conditions (EDT] Point Dir Speed Speed 11:51 55.0 °F 48.0 °F 77% 30.21 in 10.0 mi NE 9.2 mph - N/A Mostly PM Cloudy 11 report: This ad https://www.wunderground. com/history/airport/KRDU/2016/04/ 12/DailyHistory.html?req... 4/20/2016 OUTFALL #1 SAMPLE RESULTS - 01 ONE LAB. NATIC)N IDE. Collected date/time: 04/12/16 07:10 1829172 Gravimetric Analysis by Method 2540 D-2011 - Result Qualifier RDL Dilution Analysis Batch Analyte mg/I Suspended Solids 29.3 mg/I 2.50 1 date / time 04/16/2016 04:11 WG 86 2, 9 L Wet Chemistry by Method 351.2 3 Ss Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date /time Kjeldahl Nitrogen, TKN 4.11 . _....... 0.250 ..1 04/99/201610:58 1 6 4 ,.., _..... e _ Fn Wet Chemistry by Method 353.2 Result Analyte mg/I �... Qualifier a.... RDL mg/I Dilution Analysis date / time Batch C Nitrate-Nitrite 0.482 0.100 1 11 04/14/2016 21:17 WG; 8,144 29 Wet Chemistry by Method 355.4 F, Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time E 1 l Phosphorus,Total 0.611 m J6 ", , _ 0.100 1 .__--_ . . _.. 04/18/201611:49 ­ WG8.4820 �.. _ a�.., BSc Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time COD 83.3 10.0 1 04/13/2016 22:58 Wet Chemistry by Method 4500H— B-2011 Result Qualifier Dilution Analysis Batch Analyte su date / time pH 6.36 1 04/14/2016 08:43 wG-8164 5 Sample Narrative: 4500H+ B-2011 L829172-01 WG864335: 6.36 at 22.5c Wet Chemistry by Method 5210 B-2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time BOD 22.7 10.0 1 04/18/ i � .w 2016 09:24 :�, 8c 53 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Cargill, Inc. L829172 04/19/16 14:20 5 of 18 ciirdill, Ivit�Y 2 � 2016 DEMLR — Storm water Permitting Program Attn: Storm water Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Cargill, Incorporated, Raleigh, NC — Storin water Discharge Permit NCS000282 Year 5, Period 2 - Analytical Monitoring Results May 3, 2016 In accordance with the Cargill, Raleigh facility's Storm water Discharge Permit NCS000282, Part III, Section E, Cargill is submitting Discharge Monitoring Reports for the Year Five, Period Two monitoring period. The monitoring was completed on September 8th 2014 during characteristic storm event. SDO01 Characteristic Benchmark Lab Results Tier 5/3/2016 COD 120 mg/L 18.3 1 5/3/2016 BOD 30 mg/L 3.40 1 5/3/2016 Total Phosphorus 2 mg/L .182 1 5/3/2016 TKN 20 mg/L 1.50 1 SDO02 Characteristic Benchmark Lab Results Tier COD 120 mg/L BOD 30 mg/L Total Phosphorus 20 mg/L TSS 100 mg/L If there are any questions regarding this submittal please feel free to contact me at (919) 899-6604 Sincerely, Michael Klauke Plant Superintendent Cargill, Incorporated Raleigh, NC 1400 S. Blount Street Raleigh, NC 27603-2506 q 0 � � e o o a)� E 2 g E ° = / m z v g v E n % a)2 d(D M Cr) — E _ k 2 U ° 2 c o o § @ ( � \ / m 2 7 ° ( E .. 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BOD 3.4 30 mg/L NO COD 18.3 120 mg/L NO pH 6.63 Standard (6-9) NO Nitrate -Nitrite 0.43 10 mg/L NO Phosphorus,Total 0.18 2 mg/L NO Kjeldahl Nitrogen, TKN 1.5 20 rng/L NO Suspended Solids(TSS) 29.8 100 mg/L NO Tier I Checklist Stormwater inspection conducted within 2 weeks? Yes List of possible Causes leaves, product on ground from unloading/operations Potential Solutions housekeeping Actions Taken (include dates of implementation) inform Area supervisor Keep a record of all Tier 1 actions with facility SWPPP Tier 2 Checklist n addition to repeating the s eos for Tier 1, monthlv samp inR is reauired for all parameters at every outfall where an exceedance was recorded until 3 consecutive sampling events results are below benchmarks. Sampling Event Number SD000282 Sample Date 5/3/2016 Sampler Antwoine Howard Outfall Number RNC-SD001 or RNC SD002 Contract Laboratory ESC Lab Sciences Results RNC SDOO1 Parameter (Units) Value Benchmark Values Benchmark Exceedance? BOD 3.4 30 mg/L NO COD 18.3 120 mg/L NO pH 6.6 Standard (6-9) NO Nitrate -Nitrite 0.43 10 mg/L NO Phosphorus,Total 0.18 2 mg/L NO Kjeldahl Nitrogen, TKN 1.5 20 mg/L NO Suspended Solids(TSS) 29.8 100 mg/L NO Results RNC SD002 Parameter (Units) Value Benchmark Values Benchmark Exceedance? BOD 0 30 mg/L NO TSS 0 100 mg/L NO Total Kjeldahl Nitrogen 0 20 mg/L NO Nitrate -Nitrite 0 10 mg/L NO Total Phosphorus 0 2 mg/L NO COD 0 120 mg/L NO IpH 0 Standard NO * Keep a record of all Tier 1 actions with facility SWPPP Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 1 of 5 r epor; 6his ad Raleigh, NC A Raleigh -Durham International Weather History for KRDU - May, 2016 May 3 2016 O 9:33 AM EDT on May 13, 2016 (GMT -0400) View Tuesday, May 3, 2016 Daily Weekly Monthly Custom Actual Average Record Temperature Mean Temperature 71 IF 65 OF Max Temperature 79 IF 77 OF Min Temperature 63 IF 53 OF Degree Days Heating Degree Days 0 3 Month to date heating degree days 0 10 Since 1 July heating degree days 2557 3199 Cooling Degree Days 6 3 Month to date cooling degree days 21 9 Year to date cooling degree days 116 70 Growing Degree Days 22 (Base 50) Moisture Dew Point 64 IF Average Humidity 76 Maximum Humidity 93 Minimum Humidity 58 93 IF (19591 37 IF [1978) https://www.wunderground. comlhistory/airport/KRDU/2016/5/3IDailyHistory.html?req_ci... 5/ 13 /2016 Weather History for Raleigh -Durham Airport, NC ( Weather Underground Actual Precipitation Precipitation 0.44 in Month to date precipitation 0.71 Year to date precipitation 14.14 Snow Snow Tin Month to date snowfall T Since 1 July snowfall 1.4 Snow Depth 0.00 in Sea Level Pressure Sea Level Pressure 29.81 in Wind Wind Speed 5 mph (SW) Max Wind Speed 15 mph Max Gust Speed 20 mph Visibility 9 miles Events Rain , Hail , Thunderstorm Average 0.09 in 0.26 14.02 0.00 in 0.0 6.1 T = Trace of Precipitation, MM = Missing Value Source: NWS Daily Summary Daily Weather History Graph r 80 75 70 65 60 55 50 45 midnight 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 in Hy Barometric Pressure 29.9 29.8 29.7 midnight1 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 h mp 20.0 15.0 10.0 5.0 00 midnightl 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 11 360.0 270.0 180.0 90.0 0.0 c 27 24 21 18 16 13 10 7 hPa 1013 1009 1006 kmrh 32 24 16 8 0 midnight1 2 3 4 5 6 7 8 9 10 11 noon 1 2 3 4 5 6 7 8 9 10 1ikn,et Page 2 of 5 Record 1.95 in (1972) 0.00 in () https://www.wunderground.comlhistorylairport/KRDU/2016/5/3IDailyHistory.html?req_ci... 5/ 13/2016 'Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 3 of 5 repo? lhi<.. ail I why ads"? Search for Another Location Airport or City KRDU Submit Trip Planner Search our weather history database for the weather conditions in past years. The results will help you decide how hot, cold, wet, or windy it might be! Date: May 3 Submit roper' this ad 'why ads'? Astronomy May. 03, 2016 Rise Set Actual Time 6:20 AM EDT 8:04 PM EDT Civil Twilight 5:52 AM EDT 8:31 PM EDT Nautical Twilight 5:19 AM EDT 9:05 PM EDT Astronomical Twilight 4:43 AM EDT 9:40 PM EDT Moon 4:17 AM EDT (5/3) 4:35 PM EDT (5/3) Length of Visible Light 14h 39m Length of Day 13h 44m Waning Crescent, 14% of the Moon is Illuminated May 3 May 6 May 13 May 21 May 29 Waning Crescent New First Quarter Full Last Quarter report ort this ad , ••'fey ad? Hourly Weather History & Observations Time Dew Wind (EDT) Temp. Humidity Point Pressure Visibility Dir 12:51 66.9 OF 64.0 OF 90% 29.88 in 10.0 mi WSW AM 1:04 66.2 OF 64.4 °F 94% 29.89 in 10.0 mi SW AM Wind Gust Precip Events Speed Speed 6.9 mph - N/A 9.2 mph - N/A Conditions Mostly Cloudy Mostly Cloudy https://www.wunderground.com/history/airport/KRDU/2016/5/3/DailyHistory.html?req_ci... 5/ 13/2016 , Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 4 of 5 Time Dew Wind Wind Gust (EDT) Temp. Point Humidity Pressure Visibility Dir Speed Precip Speed Events Conditions 1:41 66.2 OF 64.4 OF 94% 29.90 in 10.0 mi WSW 9.2 mph N/A Overcast AM 1:51 66.9 OF 64.9 OF 93% 29.88 in 10.0 mi WSW 8.1 mph 0.00 in Rain Light Rain AM 2:12 66.2 OF 64.4 OF 94% 29.89 in 10.0 mi WSW 6.9 mph 0.00 in Rain Light Rain AM 2:51 66.9 OF 64.9 OF 93% 29.87 in 10.0 mi WNW 3.5 mph - 0.04 in Rain Light Rain AM 3:24 66.2 IF 64.4 IF 94% 29.87 in 10.0 mi Calm Calm - 0.03 in Overcast AM 3:51 66.0 IF 64.0 OF 93% 29.86 in 5.0 mi Calm Calm - 0.03 in Rain Rain AM 4:51 64.9 OF 63.0 OF 93% 29.86 in 9.0 mi Calm Calm - 0.11 in Rain Light Rain AM 5:51 64.0 OF 63.0 OF 96% 29.85 in 7.0 mi Calm Calm - 0.03 in Rain Light Rain AM 6:51 64.0 OF 63.0 OF 96% 29.83 in 5.0 mi Calm Calm - 0.03 in Rain Light Rain AM 7:51 64.9 OF 63.0 OF 93% 29.84 in 6.0 mi SSE 4.6 mph - 0.02 in Rain Light Rain AM 8:51 66.0 IF 64.0 OF 93% 29.85 in 7.0 mi SSW 5.8 mph - 0.03 in Rain Light Rain AM 9:25 66.2 OF 64.4 OF 94% 29.86 in 10.0 mi SW 5.8 mph - 0.00 in Overcast AM 9:51 66.0 OF 64.9 °F 96% 29.85 in 8.0 mi WSW 5.8 mph - 0.01 in Rain Light Rain AM 10:51 68.0 OF 64.9 IF 90% 29.83 in 10.0 mi SW 8.1 mph - 0.00 in Overcast AM 11:51 69.1 OF 64.9 IF 87% 29.83 in 10.0 mi WSW 10.4 mph - N/A Overcast AM 12:38 71.6 °F 66.2 OF 83% 29.82 in 10.0 mi WSW 11.5 mph - N/A Overcast PM 12.51 PM 73.0 IF 66.0 IF 79% 29.81 in 10.0 mi SW 9.2 mph N/A Mostly Cloudy 1:51 73.0 OF 64.0 OF 73% 29.78 in 10.0 mi WSW 5.8 mph - N/A Mostly Cloudy PM 2:51 73.9 °F 64.0 IF 71% 29.78 in 10.0 mi West 5.8 mph N/A Mostly Cloudy PM 3:51 78.1 °F 63.0 OF 60% 29.74 in 10.0 mi West 5.8 mph N/A Mostly Cloudy PM 4:51 75.9 OF 63.0 OF 64% 29.73 in 10.0 mi SSW 9.2 mph 0.00 in Rain Light Rain PM 5:26 Rain Light PM 69.8 OF 64.4 °F 83% 29.74 in 5.0 mi SSW 10.4 mph , 0.00 in Thunderstorms Thunderstorm and Rain https://www.wunderground. com/history/airport/KRDU/2016/5/3IDailyHistory.html?req_ci... 5/ 13/2016 Weather History for Raleigh -Durham Airport, NC I Weather Underground Page 5 of 5 Time Temp. Dew Humidity Pressure Visibility Wind Wind Gust Precip Events Conditions (EDT) Point Dir Speed Speed Light 68.0 °F 63.0 IF 84% 29.73 in 5.0 mi Variable 3.5 mph 0.03 in Rain Thunderstorms PM Thunderstorm and Rain 6:03 68.0 IF 64.4 °F 88% 29.74 in 5.0 mi WSW 6.9 mph 0.02 in Rain , Hail , Thunderstorms PM Thunderstorm with Hail Light 6:0 68.0 IF 64.4 IF 88% 29.74 in 7.0 mi SW 8.1 mph 0.02 in Rain , Thunderstorms PM Thunderstorm and Rain 6:31 66.2 IF 62.6 OF 88% 29.73 in 10.0 mi South 6.9 mph 0.02 in Mostly Cloudy PM 6:51 66.0 OF 63.0 OF 90% 29.72 in 10.0 mi South 5.8 mph 0.02 in Mostly Cloudy PM 7:51 66.0 OF 64.0 OF 93% 29.72 in 10.0 mi Calm Calm N/A Mostly Cloudy PM 8:51 64.9 OF 63.0 OF 93% 29.75 in 10.0 mi Calm Calm N/A Mostly Cloudy PM Rain Light PM7 64.9 OF 63.0 OF 93% 29.75 in 7.0 mi North 3.5 mph 0.01 in Thunderstorms Thunderstorm and Rain 10:39 64.4 OF 62.6 OF 949/u 29.75 in 10.0 mi WSW 4.6 mph 0.02 in Ovorcast PM 10:51 64.0 IF 63.0 OF 96% 29.76 in 10.0 mi Calm Calm 0.02 in Mostly Cloudy PM 11:51 64.0 OF 63.0 OF 96% 29.76 in 5.0 mi WSW 8.1 mph 0.02 in Rain Light Rain PM 11 report this gib https://www.wunderground. comlhistorylairportlKRDU120161513IDailyHistory.html?req_ci... 5/ 13/2016 OUT'FALL''#1 SAMPLE RESULTS -'01 rNELAS,NATIOhWIDE Collected date/time: 05/03/16 06:30 L833144 Gravimetric Analysis by Method 2540 D-2011 t t Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Suspended Solids 29.8 2.50 1 05/10/2016 04:22 WG871108 Wet Chemistry by Method 351.2 3Ss Result Qualifier RDL Dilution Analysis Batch AnalyAnalyte mg/I te _"I'll .___, .. —. w ..... mg/I w.. .. ._'., .. ..._ .. date /time a /time1 ., . �.. _ ._.. � ''I'll . C n 1 hl Nitrogen, TKN 1.50 0.250 1 05/06/201614:53 W blu329 Wet Chemistry by Method 353.2 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / timeC Nitrate -Nitrite 11 0.431 I'll 1 0.100 1 05/11/2016011 008 i'G,8 7 1 1 212 �GI Wet Chemistry by Method 365.4 Result Qualifier RDL Dilution Analysis Batch c} Analyte mg/I mg/I date / time Phosphorus Total 0.182 0.100 1 05/11/201616:07 G870667 �5c Wet Chemistry by Method 410.4 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time COD 18.3 10.0 1 05/10/201611:54 WG870 17 Wet Chemistry by Method 4500H+ B-2011 Result Qualifier Dilution Analysis Batch Analyte su date / time pH 6.63 1 05/05/2016 1408 WG86983 : Sample Narrative: 4500H+ B-2011 L833144-01 WG869834: 6.63 at 10.2c Wet Chemistry by Method 5210 B--2011 Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time BOD 3.40 J- 1.02 1 05/09/2016 09:31 W 86 849 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Cargill, Inc. L833144 05/12/1617:16 5 of 18 t3 I' 1 ", c ELo ca w tnCL ''" s i cur tub . nojogdsotjd 1e3o allAIINIalla"AI IM wing oo) :aoo � pye au F { 4 fir w dd "� 1ii 4 tiL 8 €1 is�?Y � � Cl k E n 44 W cc � �