HomeMy WebLinkAboutWQ0001800_Residual Annual Report 2019_20200225Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/25/2020
Received:*
Project Number* WQ0001800
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer Kendall.Williams@ncdenr.gov
Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
Ifinnerty@synagro.com
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0001800
Applicant\Permittee * Synagro
Facility Name * Town of Yadkinville
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Yadkinville 2019 Annual Report
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
YADKIWILLE NC 2019 Annual Report FINAL.pdf 42.95MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/21/2020
435 `Williams Court, Suite 100
Baltimore, 1\,M 21220
wwwsynagro.corn
FEBRUARY 21, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0001800
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the Town of Yadldnville, NC.
If you have any questions or need additional information, please do not hesitate to contact Perry
Williams at (336) 679-8732 or Alex Fox at (336) 703-8681.
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Perry Williams — Town of Yadldnville
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD
TOWN OF YADKINVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001800
2019 ANNUAL REPORT
Residuals Land Application Program
1. Certification Form and Annual ®perations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms &Metal Field
Loading Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNectorRttraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00001800 County Yadkin Year 2019
Facility Name (as shown on permit) Town of Yadkinville WWTP & WTP NPDES No. NC0020338, NCO079260
Land Application Operator Svnagro Phone# (336) 9984150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summary:
Total number of application fields in the permit: 19
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 67.13
Total number of acres utilized for land application during the year: 44.1
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
143 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C —Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
7 -
Perry Williams, Director of Public Works
Permittee Name and Title (type or print) SiOaature of Pe Ott I Date
SignatureofPreparer* Date Signatu o andAppli Date
(if different from Permittee) (if different from 7ermittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
i
YADKINVILLE, NC WWTP LIQUID
DRY METRIC
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT TONS
June 2019 3101000,00 G 22,76 D 20465
November 2019 4277800400 G 31,42 D 28049
YEARLY TOTAL 7377800400 G 54.18 D 49,14
YADKINVILLE, NC WTP LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
May 2019 751600M G 5.30 D 4.80
June 2019 591500,00 G 4417 D 178
November 2019 49,700.00 G 3648 D 3.16
Y EARL Y I O I AL 184, 800.00 G 12.95v i i .74
1 /30/2020
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: 1NQ0001800
Facility Name: YADKINVILLE, NC
NPDES# : NCO020338
or WQ# (residual only)
WWTP Name: YADKINVILLE WWTP
Residuals Analysis Data
Product Type LIQ
Date Sampled (grab) or 02/27/19
Date Composited
Percent Solids 1. 76
PARAMETERS (mg/kg dry weight)
Arsenic <5
Cadmium <1
Mercury 0.513
Chromium 58 . 4
Copper 964
Lead 28.5
Molybdenum 5. 74
Nickel 5509
Selenium <5
Zinc 2320
Total Phosphorus 25200
TKN 72800
Ammonia -Nitrogen 17200
Nitrate and Nitrite <4 . 82
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supE�rvision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated fihe information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATU
OF PREPARER)
DENR FORM RSSF (5/2003) Prini:ed: Wednesday - FebruaN 5, 2020 at 12:45:22 for: 2056 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name
NPDES#
or WQ# (residual only)
WWTP Name
Residual Analysis Data
Product Type
Date Sampled
Date Composited
Percent Soilds
WQ0001800
YADKINVILLE, NC
NC0020338
YADKINVILLE WWTP
LIQ
02/27/19
PARAMETERS (mg/kg dry weight)'
Aluminium
31400
Calcium
15100
Magnesium
3140
pH
7.50
Potasium
2810
Sodium
2850
PAN
25285
SAR
0.7291
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in aca�rdiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware thiat there are significant penalties for
subrrAting false information, including the possibility of fines and imprisonment for knowing violations."
(SIGNATURE
PREPARER)
n
NR -Data Not Reported or Data Not Required Report Run Date:- 2/5/2020 3:42:27 PM
i
Waypoint.
ANALYTICAL
3/7/2019
Synagro Central LLC/ Yadkinville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-060-0216
Project Description: Yadkinville WV TP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax 804-271-6446
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/1/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 (CFR 136 Method Update Rule May 2012) and NELAC winless otheRvise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability
in
any claim relating to analyses performed
shall be limited to, at laboratory's option, repeating the
analysis in question
at
laboratory's expense, or the refund of the
charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Page 1 of 6
"0
• j '
� l �
Report Number:
Client Project Description:
Lab No Client Sample ID
19-060-0216
Yadkinville WW7'P
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypo i nta n a l yti ca I. co m
Matrix Date Collected Date Received Method
65085 Yadkinville WWTP Solids 02/27/2019 10:00 03/Ol/2019
65085 Yadkinville WWTP Solids 02/27/2019 10:00 03/01/2019
65085 Yadkinville WWTP Solids 02/27/2019 10:00 03/01/2019
65085 Yadkinville WWTP Solids 02/27/2019 10:00 03/01/2019
65085 Yadkinville WWTP Solids 02/27/2019 10:00 03/01/2019
65085 Yadkinville WWTP Solids 02/27/2019 10:00 03/01/2019
65085 Yadkinville WWTP Solids 02/27/2019 10;00 03/01/2019
65085 Yadkinville WWTP Solids 02/27/2019 10:00 03/01/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Lab ID
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-2540G
WTN
Page 2 of 6
Reps.. Number: 19-060-0216
Account Number: 46507
Send To: Synagro Central LLC/ Yadkinville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Wa of ntr�,
Yp
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Niain 804-743-9401 °Fax 804-271-6446
www.waypointanalytical.com
ProJecfi :Yadkinville WWTP
REPORT OFANALYSAS Date Sampled: 2/27/2019 10:00:00
Lab Number : 65085 Date Received: 03/01/2019 00:00
Sample Id :Yadkinville WWTP Date Reported: 03/07/2019
Total Solids *
Moisture *
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
17600
72800
25200
2810
10000
15100
3140
2850
22900
31400
3430
964
f►.[cyzi]
17200
55600
<4.82
100.0
100.0
250
50.0
50.0
50.0
250
50.0
250
50.0
50.0
5.00
2.50
12.5
100
CJ R
CLP
BKN
BKN
BKN
BKN
BKN
BKN
BKN
KKM
KKM
BKN
BKN
ZBD
03/06/2019 15:50
03/06/2019 15:50
03/06/2019 14:00
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/07/2019 00:25
03/04/2019 15:15
03/04/2019 15:15
03/06/2019 12:45
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H -Beyond Holding Time
Our reports
and
letters are
for
the exclusive and confidential use
of our clients, and may not be reproduced in whole or part,
nor may
any reference be made
to fhe work,
the
results, or
the
company in any advertising, news
release, or other public announcements without obtaining
our prior
written authorization.
SM-2540G
S M-2540 G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
Pauric McGroary
Agronomist
Paae 3 c�F 6
Red., _Number: 19-060-0216
Account Number: 46507
ANALYTICAL
Send To: Synagro Central LLC/ Yadkinville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
7621 Whitepine Road, Richmond, vA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypointanalytical.com
Project :Yadkinville WWTP
REPORT OFANALYS/S Date Sampled: 2/27/2019 10:00:00
Lab Number : 65085 Date Received: 03/01/2019 00:00
Sample Id :Yadkinville WWTP Date Reported: 03/07/2019
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Molybdenum
Comments:
<1.00
1.00
BKN
03/07/2019
00:25
58.4
2.50
BKN
03/07/2019
00:25
55.9
2.50
BKN
03/07/2019
00:25
28.5
3.00
BKN
03/07/2019
00:25
<5.00
5.00
BKN
03/07/2019
00:25
0.513
0.0153
TJS
03/06/201914:32
<5.00
5.00
BKN
03/07/2019
00:25
7.5
JSL
03/07/201910:50
5.74
2.50
BKN
03/07/2019
00:25
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H -Beyond Holding Time
Our reports
and
letters are
for
the exclusive and confidential use
of our clients, and may not be reproduced in whole or part,
nor may
any reference be made
to fhe work,
the
results, or
the
company in any advertising, news
release, or other public announcements without obtaining
our prior
written authorization.
6010D
6010D
6010D
9045D
6010D
Pauric McGroary
Agronomist
�xo
- �- � ,
\�_ �_
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9403 °Fax 804-271-6446
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46507
Customer Name: Synagro Central LLC/ Yadkinville
Report Number: 19-060-0216
Shipping Method
Fed Ex 0 US Postal � Lab � Other
UPS 0 Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes 0 No
Number of coolers received 1
Custody seals intact on shipping container/cooler? � Yes 0 No Not Required
Custody seals intact on sample bottles? � Yes 0 No Not Required
Chain of Custody (COC) present? Yes � No
COC agrees with sample label(s)? Yes � No
COC properly completed Yes 0 No
Samples in proper containers? Yes � No
Sample containers intact? ®Yes � No
Sufficient sample volume for indicated test(s)? ®Yes � No
All samples received within holding time? ®Yes 0 No
Cooler temperature in compliance? ®Yes � No
Cooler/Samples arrived at the laboratory on ice. ®Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No N/A
Water -VOA vials free of headspace � Yes � No N/A
Trip Blanks received with VOAs � Yes � No N/A
Soil VOA method 5035 —compliance criteria met 0 Yes � No N/A
� High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes No
Comments:
Signature: Brandi Watson Date &Time
03/01/2019 14:25:00
Page 5 of 6
Iv
rn
0
M
SAMPLING LOG # A P
�L 76�
Ric 111111111I11111111111111111111111111111111111111111111ll11111103 06 RECORD
Il.�l�a5�
2196
GusTOM>=R: ��YB����� ° eoti
�7 Svnaciro Central LLCI Yadkmville 14:24:32
FL YadkinvilleVWVTP
PROJECT MANAGER: sampling procedures
....,,mot on of these samples.
SAMPLE I.I.
L®CATI®N
T'IPP.E CONTAINERS
Relinquished by Sampler: Date Time
Relinquished by: I . a e Time
1 i� �I
Relinquished by:
Time
Recieved by:
rtecleved by:
aH1VIYLlIIiCa
LATE TIME
z/Z� ICl�ct, du,.
METIi®CI
PRESER`JED
j
REMARKS:
METI-lOL3
SKIPPED
Cad(zy—
SPECIAL INSTRUCTIONS:
For. (STATE)monitoring purposes. PO#:
SAMPLE ANALYSIS REQUEST
1'C' SLR SL2 NH4�N N�73 N Organic Cd Cr Ni Pb As gig S® N CaCo3 Volatile
P equly. Solids Mo Cl NO2-N
eOW
SLR; Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLi plus Sulfur, GalciumI Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
• •� • 1'`�
eLIQUID
Na mg/I = (Na mg/kg x %Solids) = 100 = (2850 x 1.7600) _ 100 = 50.16
Ca mg/I = (Ca mglkg x %Solids) _ 100 = (15100 x 1.7600) + 100 = 265.76
Mg mg/I = (mg mg/kg x %Solids) + 100 = (3140 x 1.7600) _ 100 = 55.264
Na meq = Na mgll = Molec.Wgt.Na = 50.16 = 23 = 2.18087
Ca meq = Ca mgll + Molec.Wgf.Ca = 265.76 _ 20 = 13.288
Mg meq = Mg mg/I = Molec.Wgt.Mg = 55.264 = 12 = 4.60533
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.18087 + SgrRoot[0.5(13.288+4.60533)] = 0.72912
Printed: 2/5/2020
Page 1 10:38
ANNUAL RESIDUALS SAMPLING SIJMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
Facility Name: YADKINVILLE, NC
NPDES# : WQ0001800
or WQ# (residual only)
WWTP Name: YADKINVILLE WTP
Residuals Analysis Data
Product Type WPL
Date Sampled (grab) or 02/27/19
Date Composited
Percent Solids 1. 68
PARAMETERS (mg/kg dry weight)
Arsenic 8 . 7 2
Cadmium <1
Mercury 0. 0476
Chromium 32. 8
Copper 73.3
Lead 16.9
Molybdenum <2.5
Nickel 12.3
Selenium <5
Zinc 213
Total Phosphorus 2210
TKN 26500
Ammonia -Nitrogen 6470
Nitrate and Nitrite <4 a 89
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance wifih a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
11
(SIGNATJOfj�E OF PREPARER)
Date d/lU
DENR FORM RSSF (5/2003) Printed: Wednesday -February 5 2020 at 12:45:28 for: 2056 02
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name
NPDES#
or WQ# (residual only)
WWTP Name
Residual Analysis Data
Product Type
Date Sampled
Date Composited
Percent Soilds
YADKINVILLE, NC
WQ0001800
YADKINVILLE WTP
WPL
02/27/19
PARAMETERS (mg/kg dry weight)'
Aluminium
182000
Calcium
1720
Magnesium
822
pH
6.80
Potasium
769
Sodium
607
PAN
11252
SAR
0.3892
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accardiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
subm{ I g false information, including the possibility of fines and imprisonment for knowing violations." /
X � Date 02 �� oZ�
(SIGNATURE PREPARER)
NR -Data Not Reported or Data Not Required Report Run Date:- 2/5/2020 3:45:16 PM
•
Waypoint;
ANALYTICAL
3/8/2019
Synagro Central LLC/ Yadkinville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-060-0215
Project Description: Yadkinville WTP
762I Whitepine Road, Richmond, CIA 23237
Main 804-743-9401 0 Fax 804-271-6446
www,waypointanalocal.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/1/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CrR 136 Method Update Rule iviay 2012) and ivELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's Liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
uC-
k
Page 1 of 6
�� y •�:
i � �
7621 Whitepine Road, Richmond, VA 23237
Main 504-743-9401 ° Fax �04-271-6446
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-060-0215
Client Project Description: Yadkinville WTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
SM-4500-NH3C
WTN
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
9045D
WTN
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
4500NO3F-2011
WTN
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
6010D
WTN
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
SW-7471B
WTN
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
SM-4500-NH3C-TKN
WTN
65084
Yadkinville
WTP
Solids
02/27/2019
09:00
03/01/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
Rep. _Number: 19-060-0215
Account Number: 46507
Send To: Synagro Central LLC/Yadkinville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Wa oini�.,�
�p
ANALYTICAIL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypointanalytical.com
Project :Yadkinville WTP
REPORT OFANALYS/S Date sampled: 2/27/2019 09:00:00
Lab Number : 65084 Date Received: 03/01/2019 00:00
Sample Id :Yadkinville WTP Date Reported: 03/08/2019
Total Solids * 1.68 16800 100.0 CJR 03/06/2019 15:50 SM-2540G
Moisture * 98.30 100.0 CJR 03/06/2019 15:50 SM-2540G
Total Kjeldahl Nitrogen 2.65 26500 250 CLP 03/06/2019 14:00 SM-4500-NH3C-TKN
Phosphorus 0.22 2210 50.0 BKN 03/07/2019 00:20 6010D
Potassium 0.08 769 50.0 BKN 03/07/2019 00:20 6010D
Sulfur 0.64 6440 50.0 BKN 03/07/2019 00:20 6010D
Calcium 0.17 1720 250 BKN 03/07/2019 00:20 6010D
Magnesium 0.08 822 50.0 BKN 03/07/2019 00:20 6010D
Sodium 0.06 607 250 BKN 03/07/2019 00:20 6010D
Iron 24300 50.0 BKN 03/07/2019 00:20 6010D
Aluminum 182000 250 BKN 03/08/201913:08 6010D
Manganese 7850 25.0 BKN 03/08/201913:08 6010D
Copper 73.3 2.50 BKN 03/07/2019 00:20 6010D
Zinc 213 12.5 BKN 03/07/2019 00:20 6010D
Ammonia Nitrogen 0.65 6470 100 ZBD 03/04/2019 15:15 SM-4500-NH3C
Organic N 2.00 20030 250 03/04/2019 15:15 CALCULATION
Nitrate+Nitrite-N <4.89 4.89 ZBD 03/06/201912:44 4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H -Beyond Holding Time �G��6 �� V���
Our reports and letters are for the exclusive and confidential use of ourclients, and may not be reproduced in whole or part, normayany reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news re/ease, or other public announcements without obtaining our prior written authorization. AgrorlomlSt
Paae 3 of 6
Ret. .Number: 19-060-0215
Account Number: 46507
Send To: Synagro Central LLC/ Yadkinville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
�O1
Val
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project :Yadkinville WTP
REPORT OFANALYS/S Date Sampled: 2/27/2019 09:00:00
Lab Number : 65084 Date Received: 03/01/2019 00:00
Sample Id :Yadkinville WTP Date Reported: 03/08/2019
Cadmium <1.00 1.00 BKN 03/07/2019 00:20 6010D
Chromium 32.8 2.50 BKN 03/07/2019 00:20 6010D
Nickel 12.3 2.50 BKN 03/07/2019 00:20 6010D
Lead 16.9 3.00 BKN 03/07/2019 00:20 6010D
Arsenic 8.72 5.00 BKN 03/07/2019 00:20 6010D
Mercury 0.0476 0.0145 TJS 03/06/2019 14:31 SW-7471 B
Selenium <5.00 5.00 BKN 03/07/2019 00:20 6010D
pH * 6.8 JSL 03/07/2019 10:50 9045D
Molybdenum <2.50 2.50 BKN 03/07/2019 00:20 6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank Fi -Beyond Holding Time ��LL �� ����
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric MCGCOary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. AgronOmlSt
O
'`� �=
� � �
762! Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypointanalytica l.com
Cooler Receipt Form
Customer Number: 46507
Customer Name: Synagro Central LLC/ Yadkinville
Report Number: 19-060-0215
Shipping Method
0 Fed Ex � US Postal � Lab � Other : ��
UPS � Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes � No
Number of coolers received 1
Custody seals intact on shipping container/cooler? � Yes 0 No Not Required
Custody seals intact on sample bottles? � Yes 0 No Not Required
Chain of Custody (COC) present? Yes � No
COC agrees with sample label(s)? Yes 0 No
COC properly completed ®Yes � No
Samples in proper containers? Yes 0 No
Sample containers intact? Yes 0 No
Sufficient sample volume for indicated test(s)? ®Yes � No
All samples received within holding time? ®Yes � No
Cooler temperature in compliance? Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No N/A
Water -VOA vials free of headspace � Yes � No N/A
Trip Blanks received with VOAs � Yes 0 No N/A
Soil VOA method 5035 —compliance criteria met � Yes 0 No N/A
High concentration container (48 hr) (� Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) (— Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes No
Comments:
Signature: Brandi Watson Date &Time
Page 5 of 6
03/01 /2019 14:23:51
SAMPLING LOG #
PROJECT MANAGER:
�. r33L -�
Y.ar IL V�
Relinquished by Sampler:
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS:
ffiFor.
iiiiiiiiiii
LOCATE®N
A �C �. EAa! II�II'III�IIIIIIIIIIII IIIII�IIII IIIIIIIIII�IIIIIIIIIIIIIIIIII IIII 0 01 20195 p p
� L
7621 WhltE Yadkinville WTP 14;22:Y1 F i{�itUSToov
Richmond, & ANAILYS a
m 804/74344U1 rHn, ciu,/cr
I attest that the proper field sampling procedures
were used during the collection of these samples.
Tav%W
Date
Date
� e
Date
monitoring purposes.
T°IP.E
Time
2 3a
Time
Time
CCNTAINEFIS
Recleved by:
by;
py:
a7HtY1 f"LIl\11JI
®ATE TIME
SlL�: Total Solids (Moisture), Total Kjeldalll Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, CaleiumI Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
MET7.1 � C2
I�RESERVED
REMARKS:
METl�4®
Si IIPPELD
�C_ C)
LIQUID
Na mg/I = (Na mg/kg x %Solids) _ 100 = (607 x 1.6800) + 100 = 10.1976
Ca mg/I = (Ca mg/kg x %Solids) = 100 = (1720 x 1.6800) + 100 = 28.896
Mg mg/I = (mg mg/kg x %Solids) _ 100 = (822 x 1.6800) _ 100 = 13.8096
Na meq = Na mg/I _ Molec.Wgt.Na = 10.1976 _ 23 = 0.443374
Ca meq = Ca mg/I = Molec.Wgt.Ca = 28.896 _ 20 = 1.4448
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 13.8096 = 12 = 1.1508
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.443374 _ SgrRoot[0.5(1.4448+1.1508)] = 0.389194
Printed: 2/5/2020
Page 1 10:38
FACILITY NAME: YADKINVILLE,NC
OWNER: TOWN OF YADKINVILLE
SITE #: NC YK 00029 FIELD# : YK 00029 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : CLIFFORD
PERMIT #: W00001800
OPERATOR: TOWN OF YADKINVILLE
ANNUAL DRY TONS APPLIED : 12.95
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.50 ACRES PERMITTED: 11.50
rage: 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TK1V
Nitrogen
and
m
(pp )
crop
p
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/8/19
142400,00 (G)
1252,174
F1.68
0.088
YWPL
DRY
0-<1/2"
SUR
0.5
0.40
265500. p
6,470.00 p
4.89 p
11252
FESCUE HAY
5/9/19
32,400.00 (G)
2817,391
11.68
0.197
YWPL
DRY
0-<1/2"
SUR
0.5
0.40
26,500. p
6,470.00 p
4.89 p
11252
I FESCUE HAY
5/10/19
282800,00 (G)
2504,3481
1.68
0.175
YWPL
DRY
0-<1/2"
SUR
0.5
0.40
26,500. p
6,470.00 p
4.89 p
1.1252
FESCUE HAY
May-19
75,600*00 (G)
69571913
6/27/19
10,500.00 (G)
913,043
1.68
0.064
yWPL
DRY
0-<1/2"
SUR
0.5
0.40
26,500. p
6,470.00 p
4.89 p
11252
I FESCUE HAY
6/28/19
492000,00 (G)
4260,8701
1.68
0.299
YWPL
DRY
0-<1/2"
SUR
0.5
0.40
26,500. p
6,470.00 p
4.89 p
11252
FESCUE HAY
Jun49
59,500.00 (G)
5,173.913
11/6/19
49,700.00 (G)
4321.7391
1.68
0.303
YWPL
DRY
1 0-<1/2"
SUR
0.5
0.40
26,500. p
6,470.00 p
4.89 p
11212
FESCUE HAY
Nov49
491700.00 (G)
4,321.739
I
1
I
(
FACILITY NAME: YADKINViLLE,NC
OWNER: TOWN OF YADKINVILLE
SITE #: NC YK 00029 FIELD# : YK 00029 0001
RESIDUAL SOURCE(S): See list at bottom of report
OTNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : CLIFFORD
PERMIT #: WQ0001800
OPERATOR: TOWN OF YADISINMLE
ANNUAL DRY TONS APPLIED : 12.95
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.50 ACRES PERMITTED: 11.50
Page: 2
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past24
Method
zation
zation
TEN
Nitrogen
and
(ppm)
Crop
MONTH
Total
per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac:
TOTALS:
16,069.57
GI�IO
As � Cd I Cr I Cu I Pb Hg I Mo I Ni I Se I Zn I P I PAN
Annual lbs/acre
0.020
0.002
0.074
0.165
0.038
<.001
0.006
0.028
0.011
0.480
4.98
25
Cumulative lbs/acre
0.026
0.022
0.167
0.446
0.201
<.001
0.017
0.083
0.016
1.302
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
1
375.0
89.0
2500.0
YWPL = YADKINVILLE, NC WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered azid
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for 1mowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p =ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR -Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
aerator:
Acres Used:
Yadkinville, NC
WQ0001800
Town of Yadkinville
Total Dry Tons Applied (Annual): 12.95
Cation Exchange Capacity (non 503 only):
Owner: Town of Yadkinville Predominant Soil Series:
Clifford
11.5 Acres Permitted: 11.5 Site #: NC YK 00029 Field #: YK 00029 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/27/19
2
3
4
5
6
7
8
9
10
11
12
Solids
1.68
Arsenic
8.72
Cadmium
1
Copper
73.3
Chromi
32.8
Lead
16.9
Mercury
0.0476
Molyb-
denum
2.5
Nickel
12.3
Selenium
5
Zmc
2i3
Total
Phos-
nhorus
2210
inual Heaw Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
H
DT/Ac./
�
APP•
Event
1.13
Arsenic
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.165
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.165
Chromi
0.074
0.000
0.000
0.000
0.000
0.000
0.000'
0.000
0.000
0.000
0.000
0.000
0.074
Lead
0.038
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
demon
Nickel
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Selenium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Zinc
0.480
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.480
Total
Phos-
4.977
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.977
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
�prisonme�it�for knowing violations".
Signature of Land Applier
� � ��
Date
DENR FORM MFLSF (12/2006)
FACII.,ITYNAME: YADKINVILLE, NC
OWNER: KENNETH GRAY HOBSON
SITE #: NC YK 00033 FIELD# : YK 00033 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SO]L SERIES: CLIFFORD
PERMIT #: W00001800
OPERATOR: JAMES HOBSON
ANNUAL DRY TONS APPLIED : 15.47
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.60 ACRES PERMITTED: 7.60
Page : 1
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli.
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TI<N
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
615119
6,200.00 (G)
8150789
1.76
0.060
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
FESCUE HAY
6/26/19
1052400,00 (0)
138684421
136
1.018
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
FESCUE HAY
6/27/19
12,400.00 (G)
1631,579
L76
0.120
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
FESCUE HAY
Jun-19
1241000.00 (G)
16,31&789
11/10/19
24,800.00 (G)
3263,158
1.76
0.239
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
I FESCUE HAY
11/11/19
372200.00 (G)
4894,737
136
0.359
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
FESCUE HAY
11/15/19
24,800.00 (G)
3263,158
1.76
0.239
YL
MOIST
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
FESCUE HAY
Nov-19
869800.00 (G)
11,421.053
1 nral liauons /Ac: 27,736.84
Total Wet Tons/Au:
Total Cubic Yds/Ac: 0.00
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
0.020
0.004
0.238
1925
0.116
0.002
0.023
0.228
0.020
9.445
102.60
103
Cumulative lbs/acre
0.020
0.004
0.238
1925
0.116
0.002
0.023
0.228
0.020
9.445
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crap
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
734,8
7
1339.0
267.9
15.0
375.0
89.0
2500.0
i
YL = YADKINVILLE, NC WWTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify under penalty of law,. that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANN-UAL METALS FIELD LOADING SiIMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
aerator:
Acres Used:
Yadkinville, NC
WQ0001800
3ames Hobson
7.6
Total Dry Tons Applied (Annual): 15.47
Cation Exchange Capacity (non 503 only):
Owner: Kenneth Gray Hobson Predoiriinant Soil Series:
Clifford
Acres Permitted: 7.6 Site #: NC YK 00033 Field #: YK 00033 0001
Residual Analysis Data (Heald Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/27/19
2
3
4
5
6
7
8
9
10
11
12
%Solids
1.76
Arsenic
5
Cadmium
1
Copper
964
Chromi
5 8.4
Lead
28.5
Mercury
0.513
Molyb-
denum
5.74
Nickel
55.9
Selenium
5
Znlc
2320
Total
Phos-
nhorus
25200
nnual Heaw Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
H
DT/Ac./
�
�
°�
APP•
Event
2.04
Arsenic
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
3.923
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.923
Chromi
0.238
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.238
Lead
0.116
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.116
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
denum
Nickel
0.228
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.228
Selenimn
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Zinc
9.442
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.442
Total
Phos-
102.564
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
102.564
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
�prisonlnent for knowing violations".
Signature of Land Applier
7/ /J�
Date
DENR FORM MFLSF (12/2006)
FACILITY NAME: YADKINVILLE,NC
OWNER: KENNETH GRAY HOBSON
SITE #: NC YK 00033 FIELD# : YK 00033 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : CLIFFORD
PERMIT #: W00001800
OPERATOR: KENNETH GRAY HOBSON
ANNUAL DRY TONS APPLIED : 21.39
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40
rage: 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
6/3/19
62,000.00 (G)
9687,500
1.76
0.711
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
FESCUE HAY
6/4/19
862800.00 (G)
13562,500
1.76
0.995
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
I FESCUE HAY
615119
37,200.00 (G)
5812,500
1.76
0.427
YL
DRY
0-<1/2"
SUR
0.5
0.30
7:2,800. p
17,200.00 p
4.82 p
25285
FESCUE HAY
Jun49
186,000.00 (G)
299062.500
11/7/19
437400,00 (G)
6781,250
1.76
0.498
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
I FESCUE HAY
11/10/19
182600,00 (G)
2906,250
1.76
0.213
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
I FESCUE HAY
11/11/19
18,600.00 (G)
2906.250
1.76
0.213
YL
DRY
0-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
I FESCUE HAY
11/15/19
242800,00 (G)
3875,000
1.76
0.284
yL
MOIST
0-<1/2"
SUR
0.5
0.30
725800, p
17,200.00 p
4.82 p
25285
FESCUE HAY
Nov-19
1051400.00 (G)
169468.750
FACILITY NAME: YADKINVILLE, NC
OWNER: KENNETH GRAY HOBSON
SITE #: NC YK 00033 FIELD# : YK 00033 0002
RESIDUAL SOURCE(S): See list at bottom of report
ViNUAL LAND APPLICATION FIEELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: WQ0001800
OPERATOR: JAMES HOBSON
ANNUAL DRY TONS APPLIED : 21.39
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40
1-age: 2
Lime Applied ***
Date Lbs/Ac
T
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner"
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
Solids
Per
Residual
Dry, Wet,
Past24
Method
zation
zation
TKN
Nitrogen
and
(pp m )
Crop
p
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
otal Gallons/Ac: 451531 a25
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
0.033
0.007
0.390
6.443
0.190
0.003
0.038
0.374
0.033
15.505 168.42
169
Cumulative lbs/acre
0.033
0.007
0.390
6.443
0.190
0.003
0.038
0.374
0.033
15.505
Pernut PAN Limit (lbs/acre) 1st Crop/2nd Crop
202
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
f 1339.0
267.9
15.0
375.0
89.0
2500.0
YL = YADKINVILLE, NC WWTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that quaed personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SiJMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkinville, NC Total Dry Tons Applied (Annual): 21.39
Permit #: WQ0001800
Aerator: Kenneth Gray Hobson Owner:
Acres Used: 6.4 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Kenneth Gray Hobson. Predominant Soil Series:
6.4 Site #: NC YK 00033
Clifford
Field #: YK 00033 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/27/19
2
3
4
5
6
7
8
9
10
11
12
Solids
1.76
Arsenic
5
Cadmium
1
Copper
964
Chromi
5 8.4
Lead
28.5
Mercury
0.513
Molyb-
denum
5.74
Nickel
55.9
Selenium
5
Z1nC
23211
Total
Phos-
chorus
25200
anual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
°may.
App
Event
3.34
Arsenic
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
6.441
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.441
Chromiui
0.390
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.390
Lead
0.190
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.190
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.038
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
denum
Nickel
0.374
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.374
Selenium
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Zinc
15.502
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
15.502
Total
Phos-
168.386
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
168.386
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonmen�fo� knowingons".
Signature of Land Applier
����/z�
Date
DENR FORM MFLSF (12/2006)
FACILITY NAVE: YADKINVILLE , NC
OWNER: JAMESKHOBSON
SITE #: NC YK 00033 FIELD# : YK 00033 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: WQ0001800
OPERATOR: JAMES K HOBSON
ANNUAL DRY TONS APPLIED : 5.46
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.50 ACRES PERMITTED: 8.50
rage: 1
Lune Applied ***
Date Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp )m
Crop
p
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
11/7/19
12,400.00 (G)
1458,824
1.76
0.107
YL
DRY
0-<1/2"
SUR
0.5
0.30
721800.p
17,200.00 p
4.82 p
25285
WHEAT
11/8/19
62,000.00 (G)
7294,118
1.76
0.535
YL
MOIST
0-<1/2"
SUR
0.5
0.30
720800.p
17,200.00 p
4.82 p
25285
WHEAT
Nov-19
74,400.00 (G)
8,752.942
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Ac:
TOTALS
8,752.94
Annuallbs/aore 0.006 0.001 0.075 1.239 0.037 <.001 0.007 0.072 0.006 2.981 32.38 32
Cumulative lbs/acre 0.006 0.001 0.075 1.239 0.037 <.001 0.007 0.072 0.006 2.981
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 50
�i
FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0
i
YL = YADKINVILLE, NC WWTP LIQUID
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 50
�i
FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0
i
YL = YADKINVILLE, NC WWTP LIQUID
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
YL = YADKINVILLE, NC WWTP LIQUID
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % =percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SiTMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Yadkuiville, NC Total Dry Tons Applied (Annual): 5.46
permit #: WQ0001800 Cation Exchange Capacity (non 503 only):
aerator: James K Hobson Owner: James K Hobson Predominant Soil Series:
Acres Used:
Clifford
8.5 Acres Permitted: 8.5 Site #: NC YK 00033 Field #: YK 00033 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/27/19
2
3
4
5
6
7
8
9
10
11
12
%Solids
1.76
Arsenic
5
Cadmium
1
Copper
964
Chromi
58.4
Lead
28.5
Mercury
0.513
Molyb-
denum
5.74
Nickel
55.9
Selenium
5
zlllC
232U
Total
Phos-
chorus
25200
.�nual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
D T /Ac./
App.
Event
0.64
Arsenic
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Cadmium
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Copper
1.238
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.238
Chromi
0.075
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.075
Lead
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
denum
Nickel
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Selenium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
zinc
2.979
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.979
Total
Phos-
32.357
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
32.357
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
�rison�►e�pt for knowing violations".
Signature of Land Applier
�C� �v
Date
DENR FORM MFLSF (12/2006)
FACILITY NAME : YADKINVILLE , NC
OWNER: GENEVA & ROGER DAVIS
SITE #: NC YK 00035 FIELD# : YK 00035 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : CLIFFORD
PERMIT #: W00001800
OPERATOR: GENEVA & ROGER DAVIS
ANNUAL DRY TONS APPLIED : 11.83
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 10.10 ACRES PERMITTED: 10.10
rage: 1
Lime Applied ***
Date Lbs/Ac
DATE or
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp )m
Crop
p
Total
Per Acre
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
11/18/19
31,000.00 (G)
3069,307
1.76
0.225
YL
MOIST
0-<1/2"
SUR
0.5
0.30
72,800. p
172200,00 p
4.82 p
25285
FESCUE PASTURE
11/20/19
68,200.00 (G)
6752.475
L76
0.496
YL
MOIST
110-<1/2"
SUR
0.5
0.30
72,800. p
17,200.00 p
4.82 p
25285
FESCUE PASTURE
11/21/19
62,000.00 (G)
61380614
1.76
0.451
YL
DRY
110=<1/2"
SUR
0.5
0.30
72,800. p
172200000 p
4.82 p
25285
FESCUE PASTURE
Nov49
161,200.00 (G)
15,960.396
Total Gallons/Ac:
Total Wet Tons/Ac:
15,960.40
a vLcu �uviv •�u. V.VV
TOTALS:
As
Cu
Cr
Cu
Pb
rig
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
0.012
0.002
0.137
2.258
0.067
0.001
0.013
0.131
0.012
5.435
59.04
59
Cumulative lbs/acre
0.012
0.002
0.137
2.258
0.067
0.001
0.013
0.131
0.012
5.435
Permit PAN Limit pbs/acre) 1st Crop/2nd Crop
151
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
'
1339.0
267.9
15.0
375.0
89.0
2500.0
YL=YADKINVILLE, NC WWTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **'k See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Yadkinville, NC
WQ0001800
Aerator: Geneva &Roger Davis Owner:
Acres Used: 10.1 Acres Permitted:
Total Dry Tons Applied (Annual): 11.83
Cation Exchange Capacity (non 503 only):
Geneva &Roger Davis Predominant Soil Series
10.1
Clifford
Site #: NC YK 00035 Field #: YK 00035 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use m�/k�, %Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/27/19
2
3
4
5
6
7
8
9
10
11
12
%Solids
1.76
Arsenic
5
Cadmium
1
Copper
964
Chromi
5 8.4
Lead
28.5
Mercury
0.513
Molyb-
denum
5.74
Nickel
55.9
Selenium
5
Zinc
2320
Total
Phos-
nhorus
25200
lnual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
o
App•
r+
Event
1.17
"
Arsenic
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
2.260
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.260
Chromi
0.137
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.137
Lead
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
denum
Nickel
0.131
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.131
Selenium
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Zinc
5.438
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.438
Total
Phos-
59.069
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
59.069
hoius
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonme t or knowing vio�latio�ns".
��I .
Signature of Land Applies
- � �J
Date
DENR FORM MFLSF (12/2006)
9-1summill
�1GF s1 I' �7trYa:l�rlE�
March 14, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Yadkinville WWTP
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http:11www.settek.com
Dear Erik Bruce: Order No.: 19030127
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/1/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon 0112O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466A 1-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 31
' ' =nISZ IF=5 JN{7
�LIENT: Synagro
Project: Yadkinville WWTP
WorkOrder Narrative:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: hgp://www.settek.com
WO 1: 19030127
Date: 3/14/2019
190301270 This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies,. Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
19030127-001A 434790a Prep Comments for MtlPrep_TCLP(3010A), Sample 19030127-OOlA:
Sample was filtered after digestion.
Original
Page 2 of 31
S I
U M I'T
+, y lttrvtirdt_ �r�.L TEMIN'M n ,1-. , ;r C
Arratyrs'c �' 1'_aborason.66t
SummitEnvironmental Technologies, In
3310 Win 5
Cuyahoga Falls, Ohio 442z'
TEL: (330) 253-8211 FAX: (330) 253-446
Wehsite: htW.v11Www.settekco.
These commonly used Qualifiers and Acronyms may or may not be present m this report.
Quaers
WO 1: 19030127
Date: 3/14/2019
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+),
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
)CS Quality Control Sample CRQL Contract Required Quantitation Limit
31 Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reexiraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 31
Summit Environmental Technologies, Inc.
3310 Win St,
Cuyahoga Falls, Ohio 44223
TEL; (330) 253-8211 FAX.• (330) 253-4489
Website: hgp://www.settek.com
Warkoi deir
mple Summery
WO#: 19030127
14-MaY-19
CLIENT: Synagro
Project: Yadkinville WWTP
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
19030127-001 Yadkinville VJWTP 2/27/2019 3/1/2019 10:15:00 AM Sludge
F•
FF - Summit Environmental Technologies, Inc.
'X 3310 Win St.
Cuyahoga Falls, Ohio 44223
rn ^PfJ r' i 131��Jr��� 2 TEL: (330) 253-8211 FAX(330) 2534489
Website: hgp://www.settelc.com
Client: Synagro
Project: Yadkinville WWTP
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
19030127-OOlA Yadlcinville WWTP 2/27/2019 Sludge Ignitability of Solids (SW-846: 1030) 3/5/2019 12:00:00 PM
pH (SW9045D) 3/5/2019 2:33:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid 3/5/2019 5:16:00 PM
Reactive Sulfide (9034)/7.3.4.2 3/5/2019 5:16:00 PM
SVOC SW-846: 8151 HerbicidesJU3/4/2019 6:00:00 PM 3/7/2019 3:00:00 PM 3/12/2019 10:00:00 PM
TCLP Mercury Analysis (SW1311/7473/4/2019 6:00:00 PM 3/6/201912:40:00 PM 3/6/2019 4:49:00 PM
TCLP Metals Analysis (SW1311/6010:3/4/2019 6:00:00 PM 3/6/2019 8:10:00 AM 3/6/2019 5:41:33 PM
TCLP Pesticides Analysis (SW1311/8(3/4/2019 6:00:00 PM 3/11/2019 5:20:00 PM 3/12/2019 9:45:00 PM
TCLP Semi-Volatiles Analysis 3/4/2019 6:00:00 PM 3/11/2019 12:15:00 PM 3/12/2019 6:11:00 PM
(SW1311/8270)
TCLP Volatiles Analysis 3/5/2019 2:05:00 PM
Original
Paae 5 of �;1
Sununit Envirownental Technologies, Inc.
sump*mk 3310 Win A
E';ti�lf? �N�1�tiTp.L x _�?t�6-�i <;" - Cuyahoga Falls, Ohio 44223
- Anaty0cal TEL: (330) 253-8211 FAX: (330) 253-4489
CLIENT:
Matrix:
Lab ID:
Project:
Synagro
SLUDGE
19030127-001A
Yadkinville WWTP
Client Sample ID Yadkinville WWTP
Analytical Report
(base report)
WO#: 19030127
Websate: http://www.settekcona Date Reported: 3/14/2019
Tag Number:
Collection Date: 2/27/2017
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury ND 0.00500 mg/L 1 3/6/2019 4:49:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As) ND 0.500 mg/L 1 3/6/2019 5:41-133 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 3/6/2019 5:41:33 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 3/6/2019 5:41-133 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 3/6/2019 5:41:33 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 3/6/2019 5:41:33 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 3/6/2019 5:41:33 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 3/6/2019 5:41:33 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270 Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.0800 mg/L 2 3/12/2019 6:11:00 PM
2,4,5-Trichlorophenol ND 0.200 mg/L 2 3/12/2019 6:11:00 PM
2,4,6-Trichlorophenol ND 0.200 mg/L 2 3/12/2019 6:11:00 PM
2,4-Dinitrotoluene ND 0.0400 mg/L 2 3/12/2019 6:11:00 PM
Cresols, Total ND 4.00 mg/L 2 3/12/2019 6:11:00 PM
HexachloroA,3-butadiene ND 0.0160 mg/L 2 3/12/2019 6:11:00 PM
Hexachlorobenzene ND 0.0400 mg/L 2 3/12/2019 6:111-00 PM
Hexachloroethane ND 0.0800 mg/L 2 3/12/2019 6:11:00 PM
Nitrobenzene ND 0.0800 mg/L 2 3/12/2019 6:11:00 PM
Pentachlorophenol ND 0.200 mg/L 2 3/12/2019 6:11:00 PM
Pyridine ND 0.200 mg/L 2 3/12/2019 6:11:00 PM
Surr: 2-Fluorophenol 71.5 10 - 109 %Rec 2 3/12/2019 6:11:00 PM
Surr: Phenol-d6 71.7 10 - 109 %Rec 2 3/12/2019 6:11:00 PM
Surr: Nitrobenzene-d5 93.7 19 - 120 %Rec 2 3/12/2019 6:11:00 PM
Surr: 2,4,6-Tribromophenol 94.2 10 - 120 %Rec 2 3/12/2019 6:11:00 PM
Surr: 2-Fluorobiphenyl 92.6 22 - 117 %Rec 2 3/12/2019 6:11:00 PM
Surr: p-Terphenyl-d14 117 34 - 130 %Rec 2 3/12/2019 6:11:00 PM
Qualifiers:
* Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 6 of 31
Suininit Environmental Technologies, Inc.
3310Win st. Analytical Report
' 04 Li -J L base re
r �'.'li?10WK1 ,•1TAL TIEC!JfWol ; ':5, yNr' Cuyahoga Falls, Ohio 44223 report)
Arr'.:T6gr'sRl' L.a'borasoin;;oll TEL (330) 253-8211 FAX.• (330) 253-4489 WO#: 19030127
website: hgp://wwiv.settek.com Date Reported: 3/14/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 2/27/2019
Lab ID: 19030127-OOIA
Project: Yadkinville WWTP
Client Sample ID Yadkinville WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW351OC Analyst: SFG
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND 0,250 mg/L 10 3/12/2019 9:45:00 PM
Toxaphene ND 0.500 mg/L 10 3/12/2019 9:45:00 PM
Endrin ND 0,0250 mg/L 10 3/12/2019 9:45:00 PM
gamma-BHC ND 0.0250 mg/L 10 3/12/2019 9:45:00 PM
Heptachlor ND 0,0250 mg/L 10 3/12/2019 9:45:00 PM
Heptachlor epoxide ND 0,0250 mg/L 10 3/12/2019 9:45:00 PM
Methoxychlor ND 0,0250 d mg/L 10 3/12/2019 9:45:00 PM
Surr: TCMX 100 10 - 119 %Rec 10 3/12/2019 9:45:00 PM
Surr: DCB 106 10 - 119 %Rec 10 3/12/2019 9-145:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: SFG
SVOC SW-846: 8151 HERBICIDES-TCLP
214-D ND 1,00 mg/L 1 3/12/2019 10:00:00 PM
21415-TP ND 0.500 d mg/L 1 3/12/2019 10:00-100 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260 Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 3/5120192:05:00 PM
1,2-Dichloroethane ND 0,250 mg/L 50 3/5/2019 2:05:00 PM
MEK ND 1,25 mg/L 50 3/5/2019 2:05:00 PM
Benzene ND 0,250 mg/L 50 3/5/2019 2:05:00 PM
Carbon tetrachloride ND 0,250 mg/L 50 3/5/2019 2:05:00 PM
Chlorobenzene ND 0,250 mg/L 50 3/5/2019 2:05-100 PM
Chloroform ND 0,250 mg/L 50 3/5/2019 2-105-100 PM
Tetrachloroethene ND 0.250 mg/L 50 3/5/2019 2:05:00 PM
Trichloroethene ND 0,250 mg/L 50 3/5/2019 2:05:00 PM
Vinyl chloride ND 0,100 mg/L 50 3/5/2019 2:05:00 PM
Surr: 4-Bromofluorobenzene 92.9 70 - 130 %Rec 50 3/5/2019 2-105:00 PM
Surr: Dibrom ofluorom ethane 89.7 70 - 130 %Rec 50 3/5/2019 2:05:00 PM
Surr: Toluene-d8 104 70 - 130 %Rec 50 3/5/2019 2:05:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 31
LIENT:
Matrix:
Lab ID:
Project:
Ri$eiliot4rdeid"I'i'! I::rll[iti1 S 'a
Synagro
SLUDGE
19030127-001A
Yadkinville WWTP
Client Sample ID Yadkinville W WTP
Su7777nit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 253-4489
Analytical Report
(base report)
WO#: 19030127
Websate: http://www.settek.co»a Date Reported: 3/14/2019
Tag Number:
Collection Date: 2/27/2019
Analyses Result RL Qual Units DF Date Analyzed
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7112)-SOLID
Cyanide, Reactive
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability
RCI-SOLID-W/ IGNITABILITY1030
PH (SW9045D)
D
H
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
non-flammable
7.6
SW9014 Analyst: MS
0.485 mg/Kg 1 3/5/2019 5:16:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
SW1030 Analyst: AJT
1 3/5/2019 12:00:00 PM
SW9045D Analyst: DHC
s.u.n19.6C 1 3/5/2019 2:33:00 PM
SW9034 Analyst: MS
25.0 mg/Kg 1 3/5/2019 5:16:00 PM
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8of31
Summit Environmental Technologies, Inc. Accr editafion Frrogrnm
w low 3310 Win St,
ail►_r tdrlKt.�re.� r c:t. r Rtit -, ,:.s Cuyahoga Falls, Ohio 44223 AIr11a ytes Report
t
Alrnt' iVezil tabn.rato,F'tjpt TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 19030127
Website: http:/1www.settek.com 14-Mar49
Client: Synagro State: NC
Project: Yadkinville WWTP Program Name: NC WW SCM
Sample ID Matrix Test Name Analyte Status
1903012MOIA Sludge Ignitability of Solids (SW-846: 1030) Ignitability A
Sludge pH (SW9045D) Hydrogen Ion (pH) A
Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U
Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Sludge SVOC SW-846: 8151 Herbicides-TCLP 2A5-TP A
Sludge SVOC SW-846: 8151 Herbicides-TCLP 2,4-1) A
Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A
Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis (SW1311/6010) Barium A
Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis (SW1311/6010) Chromium A
Sludge TCLP Metals Analysis (SW1311/6010) Lead A
Sludge TCLP Metals Analysis (SW1311/6010) Selenium A
Sludge TCLP Metals Analysis (SW1311/6010) Silver A .
Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A
Sludge TCLP Pesticides Analysis (SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A
NC_WW SCM
A Accredited NC WW SCM U Unavailable
Original # 1
Page 9 of 31
l
4
r. _ — �' -� Summit Environmental Technologies, Inc. Acell effitaflon Program
3310 Win St,
r":I(:. h1Pe7e •li�.L FEit«:t11 i�4 3 Cuyahoga Falls, Ohio 44223 `������� ���®��
tabaraxonk TEL: (330) 253-8211 FAX: (330) 2534489 WO#: 19030127
Wehsite: hyp://www.settek.com 14-Mar49
Client: Synagro State: NC
Project: Yadkinville WWTP Program Name. NC_WW SCM
Sample ID Matrix Test Name Analyte Status
19030127-001A Sludge TCLP Volatiles Analysis lj1 Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tefrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
NC WW SCM A Accredited NC WW SCM U Unavailable
Page 10 of 31
Original # 1
--- -- - -` L Summit Environmental Technologies, Inc. QC SUMMARY RE-eORT
J �JY 3310 Win St.
1,++ +idf t_ d i +L 7 12 :arn; Cuyahoga Falls, Ohio 44223 WO#: 19030127
TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: hge:llwww.settek.corn 14-Mar-19
Client: Synagro
Project: Yadldnville WWTP
BatchID0 36252
Sample ID 19030086-001AMS SampType: MS TestCode: MTL-TCLP-7( Units: mg/L Prep Date: 3/6/2019 RunNo: 95376
Client ID: Batch= Batch ID: 36252 TestNo: SW6010D SW3010A Analysis Date: 3/6/2019 SegNo: 1987166
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
TCLP
Arsenic(As)
2.31
0.500
2.000
0
115
70 130
TCLP
Barium(Ba)
ND
5.00
2.000
0.2767
99A
70 130
TCLP
Cadmium(Cd)
1.97
0.100
2.000
0
98.4
70 130
TCLP
Chromium(Cr)
2.11
0.200
2.000
0
105
70 130
TCLP
Lead(Pb)
2.06
0.500
2.000
0
103
70 130
TCLP
Selenium(Se)
2.39
0.0500
2.000
0,02516
118
70 130
TCLP
Silver(Ag)
2.37
0.500
2.000
0
118
70 130
Sample ID 19030086-001AMSD SampType: MSD
Client ID: BatchQC Batch ID: 36252
Analyte
Result
TestCode: MTL-TCLP-7( Units: mglL Prep Date: 3/6/2019
TestNo: SW6010D SW3010A Analysis Date: 3/6/2019
PQL SPK value SPK Ref Val °1°REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
RunNo: 95376
SegNo: 1987167
%RPD RPDLimit 02ua1
TCLP
Arsenic(As)
2.35
0.500
2.000
0
117
70
130
2.310 1.68
20
TCLP
Barium(Ba)
ND
5.00
2.000
0.2767
101
70
130
0 0
20
TCLP
Cadmium(Cd)
1.99
0.100
2.000
0
99.7
70
130
1.967 1.30
20
TCLP
Chromium(Cr)
2.15
0.200
2.000
0
107
70
130
2.109 1.77
20
TCLP
Lead(Pb)
2.08
0.500
2.000
0
104
70
130
2.061 0.952
20
TCLP
Selenium(Se)
2.42
0.0500
2.000
0,02516
120
70
130
2.392 1.33
20
TCLP
Silver(Ag)
2040
0.500
2.000
0
120
70
130
2.368 1.48
20
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte
detected in the
associated Method
Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte
detected below
quantitation limits
M
Manual Integration used to detennine
Original
Page 11 of 3'I
Summit Environmental Technologies, Inc.
. L g 3310 Win St. iQC SUMMARY Rf ORT
'fir FPaIrMTAL a4tIl A0.rro,, + C 1 Cuyahoga Falls, Ohio44223 C�• _ > vrhf.i` La-barjlto to_ TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 19030127
Website: httl2:llwww.settelc.com 14-Mar-19
Client: Synagro
Project: Yadldnville WWTP
BatchIDa 36252
Sample ID MB-36252 SampType: MBLK TestCode: MTL-TCLP-7( Units: mg/L Prep Date: 3/6/2019 RunNo: 95376
Client ID: PBS Batch ID: 36252 TestNo: SW6010D SW3010A Analysis Date: 3/6/2019 SegNo: 1998092
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Arsenic(As) ND 0.500
TCLP Barium(Ba) ND 5.00
TCLP Cadmium(Cd) ND 0.100
TCLP Chromium(Cr) ND 0.200
TCLP Lead(Pb) ND 0.500
TCLP Selenium(Se) ND 0.0500
TCLP Silver(Ag) ND 0.500
Sample ID LCS-36252 SampType: LCS TestCode: MTL-TCLP-7( Units: mg/L Prep Date: 3/6/2019 RunNo: 95376
Client ID: LCSS Batch ID: 36252 TestNo: SW6010D SW3010A Analysis Date: 3/6/2019 SegNo: 1998093
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Arsenic(As) 2.09 0.500 2.000 0 104 80 120
TCLP Barium(Ba) ND 5.00 2.000 0 105 80 120
TCLP Cadmiuni 1.87 0.100 2.000 0 93.6 80 120
TCLP Chromiuni 2.12 0.200 2.000 0 106 80 120
TCLP Lead(Pb) 2.15 0.500 2.000 0 108 80 120
TCLP Selenium(Se) 2.08 0.0500 2.000 0 104 80 120
TCLP Silver(Ag) 2.24 0.500 2.000 0 112 80 120
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 12 of 31
_ - - ILLJ
Summit Environmental Technologies, Inc. SUMMARY
T n FibJOT
u I _ ^3310 Win St. QC lJ AR Y i\Ll K
11ud�!J{7_�di L 'r J'+arn��; _ Cuyahoga Falls, Ohio44223
TEL: (330) 253-8211 FAX.• (330) 2534489
WO#: 19030127
Website: httl2:llwww.settelc.com 14-Mar-19
Client: Synagro
Project: Yadldnville WWTP
SatchID6 36264
Sample ID MB-36264 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 3/6/2019 RunNo: 95406
Client ID: PBS Batch ID: 36264 TestNo: SW7470A SW7470A Analysis Date: 3/6/2019 SegNo: 1986470
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[
TCLP Mercury
ND 0.00200
Sample ID LCS-36264 SampType: LCS TestCode: HG_1CLP(74 Units. PPM Prep Date: 3/6/2019 1-1 95406
Client ID: LCSS Batch ID: 36264 TestNo: SW7470A SW7470A Analysis Date: 3/6/2019 SegNo: 1986471
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua]
TCLP Mercury
0.00409 0.00200 0.00400
Sample ID 19030086-001AMS SampType: MS
Client ID: BatchQC Batch ID: 36264
Analyte
TCLP Mercury
Result
0 102 80 120
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
0.00445 0.00200 0.00400
Sample ID 19030086-001AMSD SampType: MSD
Client ID: Batch= Batch ID: 36264
Analyte
TCLP Mercury
Result
Prep Date: 3/6/2019
Analysis Date: 3/6/2019
%REC LowLimit HighLimit RPD Ref Val
0 111 75 125
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
Prep Date: 3/6/2019
Analysis Date: 3/6/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 95406
SegNo: 1986475
%RPD RPDLimit Qual
RunNo: 95406
SegNo: 1986476
%RPD RPDLimit Qual
0.00443 0.00200 0.00400 0 111 75 125 0.00445 0.450 20
Qualifiers: * Value exceeds Maxhnum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 13 of 31
Summit Environmental Technologies, Inc.
i. J
J L� �f 3310 Win St. QC SUMMARY RJPORT
Cuyahoga Falls, Ohio 44223 WO#: 19030127
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: hO.*11www.settek.com 14-Mar49
Client: Synagro
Project: Yadldnville WWTP
Sample ID 19030086-001AMSD SampType: MSD
Client ID: Batch= Batch ID: 36264
Analyte
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
BatchID0 36264
Prep
Date:
3/6/2019
RunNo:
95406
Analysis
Date:
3/6/2019
SegNo:
1986476
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank 1J Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 14 of 31
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY Ri eORT
J L_1
E�: Orl O W MENT,RL rz „ 1 U r ;; Cuyahoga Falls, Ohio 44223
+'''��=' 'vfjon: �L abara� dnol TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 19030127
Website: hQ:Ilwww.settek.corn 14-Mar49
Client: Synagro
Project: Yadkinville WWTP
BatchID0 36316
Sample ID MB-36316 SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: 3/7/2019 RunNo: 95654
Client ID: PBS Batch ID: 36316 TestNo: SW8151A SW8151A Analysis Date: 3/12/2019 SegNo: 1996428
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D ND 1.00 d
21415-TP ND 0.500 d
Surr: 2,4-Dichlorophenylacetic acid 373 500.0 74.6 20 140
Sample ID LCS-36316 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 3/7/2019 RunNo: 95654
Client ID: LCSS Batch ID: 36316 TestNo: SW8151A SW8151A Analysis Date: 3/12/2019 SegNo: 1996429
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
274-D
ND
1.00 0.500
0 73.6
43.8
130
Sample ID 19030122-001AMS SampType: MS
Client ID: Batch= Batch ID: 36316
Analyte
Result
TestCode: TCLPSVOC- Units: mg/L
TestNo: SW8151A SW8151A
PQL SPK value SPK Ref Val
Prep Date: 3/7/2019
Analysis Date: 3/12/2019
%REC LowLimit HighLimit RPD Ref Val
m
RunNo: 95654
SegNo: 1996430
%RPD RPDLimit Qual
214-D ND 1.00 0.500 0 73.7 37 105 m
27475-TP ND 0.500 0.500 0 70A 38 106 m
Sum 2,4-Dichlorophenylacetic acid 713 500.0 143 20 140 Sm
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit, ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 15 of 311
-- Summit Environmental Technologies, Inc.
JLi I� QC SUMMARY REPORT
f m if II- L 3310 win St.
�C ^a''Ililr rYdh1rdT�r.L T�4tirLR, v ,,7 Cuyahoga Falls, Ohio 44223
WO#: 19030127
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http:/hvww.settek.com 14-Mar49
Client: Synagro
Project: Yadldnville WWTP
Sample ID 19030122-001AMSD SampType: MSD
Client ID: BatchQC Batch ID: 36316
Analyte
Result
BatchII)0 36316
TestCode: TCLP-SVOC- Units: mg/L Prep Date: 3/7/2019
TestNo: SW8151A SW8151A Analysis Date: 3/12/2019
PQL SPK value SPK Ref Val °i°REC LowLimit HighLimit RPD Ref Val
RunNo: 95654
SegNo: 1996431
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 67.2 37 105 0 0 30 m
21415-TP ND 0.500 0.500 0 64.6 38 106 0 0 30 m
Surr: 2,4-Dichlorophenylacetic acid 875 500.0 175 20 140 0 30 Sm
Qualifiers: * Value exceeds Maximum Contaaninant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 16 of 31
' Summit Environmental Technologies, Inc.
1 Ii I 1 1 3310Win St,
ij is l��l i•.1"I L _I�, er�.r; Cuyahoga Falls, Ohio44223
t�3�'; Its ��' i ur dntar TEL: (330) 253-8211 FAX: (330) 253-4489
Website: hQ:11www.settek.com
Client: Synagro
Project: Yadkinville WWTP
QC SUMMARY R LPORT
EatchID0 36331a
WO#: 19030127
14-Mar-19
Sample ID LCS-36331 SampType: LCS TestCode: TCLP-SVOC_ Units: mg/L Prep Date: 3/11/2019 RunNo: 95613
Client ID: LCSS Batch ID: 36331a TestNo: SW8270 Analysis Date: W12/2019 SegNo: 1996811
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene
0.491
0.0400
0.8000
0
61.4
19.1
126
2,4,5-Trichlorophenol
0.633
0.100
0.8000
0
79.2
11.7
151
2,4,6-Trichlorophenol
0.719
0.100
0.8000
0
89.9
12A
150
2,4-Dinitrotoluene
0.741
0.0200
0.8000
0
92.7
20.6
140
o-Cresol
0.623
0.100
0.8000
0
77.9
13.8
137
Cresols, Total
ND
2.00
1.600
0
77.2
10
129
Hexachloro-1,3-butadiene
0.378
0,00800
0.8000
0
47.2
14.7
137
Hexachlorobenzene
0.672
0.0200
0.8000
0
84.0
12
139
Hexachloroethane
0.386
0.0400
0.8000
0
48.2
14.8
132
Nitrobenzene
0.676
0.0400
0.8000
0
84.6
15.6
138
Pentachlorophenol
0.721
0.100
0.8000
0
90.2
10
156
Pyridine
0.366
0.100
0.8000
0
45.7
1
130
Surr: 2-Fluorophenol
0.609
1.000
60.9
10
147
Surr: Phenokd6
0.587
1.000
58.7
10
140
Surr: Nitrobenzene-d5
0.763
1.000
76.3
10
169
Surr: 2,4,6-Tribromophenol
0.795
1.000
79.5
10
185
Surr:2-Fluorobiphenyl
0.664
1.000
66A
10
169
Surr: p-Terphenykd14
1.02
1.000
102
10
179
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 17 of 31
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: htW.//www.settelc.com
Client: Synagro
Project: Yadldnville WWTP
Sample ID MB-36331 SampType: MBLK TestCode: TCLPSVOC_ Units: mg/L
Client ID: PBS Batch ID: 36331a TestNo: SW8270
Analyte Result PQL SPK value SPK Ref Val
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0,100
2,4,6-Trichlorophenol
ND
0,100
2,4-Dinitrotoluene
ND
0.0200
o-Cresol
ND
0.100
Cresols, Total
ND
2,00
Hexachloro-1,3-butadiene
ND
0,00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0,100
Pyridine
ND
0.100
Sum 2-Fluorophenol
0,496
Sum Pbenokd6
0.503
Sum Nitrobenzene-d5
0.621
Sum 2,4,6-Tribromophenol
0.623
Sum. 2-Fluorobiphenyl
0.567
Sum p-Terphenyl-d14
0,728
QC SUMMARY RiPORT
WO#: 19030127
14-MaY-19
SatchIDa 36331a
Prep Date: 3/11/2019
Analysis Date: 3/12/2019
%REC LowLimit HighLimit RPD Ref Val
1.000
49.6
10
109
1.000
50.3
10
109
1.000
62.1
19
120
1.000
62.3
10
120
1.000
56.7
22
117
1.000
72.8
34
116
RunNo: 95613
SegNo: 1998657
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Pen -nit Limit
R
RPD outside accepted recovery limits
Original
Page 18 of 31
Summit Environmental Technologies, Inc. QC SUMMARY
7�tT RLeO T
l.. V 1V11�'ll-�it 1 it
- 3310 Win St.
1 n l :•;'� L �, a P �; , ; Cuyahoga Falls, Ohio 44223
••+.�I'v Or.�,1' L _wLib�n raidata�PS � TEL: (330) 253-8211 FAX: (330) 253-4489
WO#: 19030127
Website: ha://www.settefc.com 14-Mar49
Client: Synagro
Project: Yadkinville WWTP
BatchID4 36332
Sample ID MB-36332 SampType: MBLK TestCode: TCLP SVOC•• Units: mg/L Prep Date: W11/2019 RunNo: 95664
Client ID: PBS Batch ID: 36332 TestNo: SW8081 SW3510C Analysis Date: 3/12/2019 SegNo: 1996798
Analyte
Result
PQL SPK value SPK Ref Val
Chlordane, total
ND
0.0250
Toxaphene
ND
0.0500
Endrin
ND
0,00250
gamma-BHC
ND
0,00250
Heptachlor
ND
0.00250
Heptachlor epoxide
ND
0,00250
Methoxychlor
ND
0,00250
Surr: TCMX
12.1
Surr: DCB
15A
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
d
d
20.00 60.3 10 119 m
20.00 77.1 10 119
Sample ID LCS-36332 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 3/11/2019
Client ID: LCSS Batch ID: 36332 TestNo: SW8081 SW3510C Analysis Date: 3/12/2019
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 95664
SegNo: 1996799
%RPD RPDLimit Qual
Endrin 0.0130 0.00250 0.0250 0 52.0 20 157
gamma-BHC 0.0112 0,00250 0.0250 0 44.7 22 137
Heptachlor 0.0105 0,00250 0,0250 0 42.2 24 121
Heptachlor epoxide 0.0117 0,00250 0.0250 0 46.9 27 152
Methoxychlor 0.0131 0,00250 0.0250 0 52A 10 199
Surr: TCMX 12.8 20.00 64.0 10 119
Surr: DCB 16.7 20.00 83.5 10 119
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 19 of 31
Summit Environmental Technologies, Inc, QC SUMMARY RhORT
W'5 p„,�V,� �lI__; _� i 3310 Win St.
�, +4,r11''Ydh1Cri�TL iL� I"nir,:;,, Cuyahoga Falls, Ohio 44223
40 a1' r _;J,' ' Syr uYot0r'd WO#: 19030127
IF aw TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: htt42:llwww.settelc.com 14-Mar49
Client: Synagro
Project: Yadlunville WWTP
BatchID0 36332
Sample ID 19030122-001AMS SampType: MS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 3/11/2019 RunNo: 95664
Client ID: BatchQC Batch ID: 36332 TestNo: SW8081 SW3510C Analysis Date: 3/12/2019 SegNo: 1996800
Analyte
Result
PQL SPK value SPK Ref Val
°'°REC LowLimit HighLimit RPD Ref Val
Endrin
ND
0.0250
.0.0250
0
71.1
20
157
gamma-BHC
ND
0.0250
0.0250
0
60.3
22
137
Heptachlor
ND
0.0250
0.0250
0
59.6
24
121
Heptachlor epoxide
ND
0.0250
0.0250
0
67.8
27
152
Methoxychlor
ND
0.0250
0.0250
0
77.8
10
199
Surr: TCMX
18.9
20.00
94.4
10
119
Surr: DCB
21.7
20.00
109
10
119
%RPD RPDLimit Qual
Sample ID 19030122-001AMSD SampType: MSD TestCode: TCLPSVOC- Units: mg/L Prep Date: 3/11/2019 RunNo: 95664
Client ID: Batch= Batch ID: 36332 TestNo: SW8081 SW3510C Analysis Date: 3/12/2019 SegNo: 1996801
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
ND
0.0250
0.0250
0
56.7
20
157
0
0
30
gamma-BHC
ND
0.0250
0.0250
0
53.1
22
137
0
0
30
Heptachlor
ND
0.0250
0.0250
0
50.2
24
121
0
0
30
Heptachlor epoxide
ND
0.0250
0.0250
0
56.6
27
152
0
0
30
Methoxychlor
ND
0.0250
0.0250
0
59.1
10
199
0
0
30
Surr: TCMX
16.5
20.00
82.3
10
119
0
Surr: DCB
17.5
20.00
87.7
10
119
0
Qualifiers: y` Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 20 of 31
IL Summit Environmental Technologies, Inc. QC SUMMARY RORT
L J 3310 Win St. �:P
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 19030127
Website: hgg.*11www.settek.com 14-Mar49
Client: Synagro
Project: Yadkinville WWTP
Sample ID LCS-R95317 SampType: LCS TestCode: Ignitability_S Units:
Client ID: LCSS Batch ID: R95317 TestNo: SW1030
Analyte Result PQL SPK value SPK Ref Val
Ignitability
7.60
Sample ID
19021576-001ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R95317
Analyte
Ignitability
Result
Sample ID 19030122-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R95317
Analyte
Ignitability
Result
non-flammable
Sample ID 19030124-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R95317
An
Ignitability
non-flammable
7.240
TestCode: Ignitability_S Units:
TestNo: SW1030
BatchID0 R95317
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
0 105 70 130
PQL SPK value SPK Ref Val
TestCode:lgnitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
TestCode: lgnitability_:i Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
i
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
If
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPDIII
Ref Val
RunNo: 95317
SegNo: 19835511
%RPD RPDLimit Qual
RunNo: 95317
SegNo: 1983553
%RPD RPDLimit Qual
0 20
RunNo: 95317
SegNo: 1983555
%RPD RPDLimit Qual
0 20
RunNo: 95317
SegNo: 1983557
%RPD RPDLimit Qual
0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 21 of 31
Summit Environmental Technologies, Inc.
F-
QC SUMMARY R.LPORT
� L
— i '._.1,k.1 s,}a'i.__ . LJ^ 3310 Win St.
Cuyahoga Falls, Ohio44223 WO#: 19030127
I I � , 'f r;J moTEL: (330) 253-8211 FAX.• (330) 253-4489
Website: htt42:llwww.settek.com 14-Mar49
Client: Synagro
Project: Yadkinville WWTP BatchID: R95317
Ignitability non-flammable 0 0 20
Sample ID 19030127-001ADUP SampType: DUP TestCode: Ignitabi1ity_5 Units: Prep Date: RunNo: 95317
Client ID: Yadkinville WWTP Batch ID: R95317 TestNo: SW1030 Analysis Date: 3/5/2019 SegNo: 1983561
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quautitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 311
4 - i �, L Summit Environmental Technologies, Inc. Q!� SUMMARY 3310WinSt. 1�.. �7V it it
",�k� Nr.,(hlpsi ENJTP1 GIRi v, ,I I'T Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX:* (330) 253-4489 WO#: 19030fl27
Website: hgp://www.settek.com 14-Mar49
�llneIIA Synagro
Project: Yadkinville WWTP
Sample ID
MB-95319
SampType:
MBLK
Client ID:
PBS
Batch ID:
R95319
Analyte Result
TestCode: tclp-voc-mstr Units: mg/L
TestNo: SW8260
PQL SPK value SPK Ref Val
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0,00500
MEK
ND
0.0250
Benzene
ND
0,00500
Carbon tetrachloride
ND
0500500
Chlorobenzene
ND
0,00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0000500
Trichloroethene
ND
0,00500
Vinyl chloride
ND
0,00200
Surr: 4-Bromof] uorobenzene
46.8
Surr: Dibromofluoromethane
43.4
Surr: Toluene-d8
52.3
Prep Date:
Analysis Date: 3/5/2019
°'°REC LowLimit HighLimit RPD Ref VaI
50.00
93.6
70 130
50.00
86.9
70 130
50.00
105
70 130
RunNo: 95319
SegNo: 1983592
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
13 Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual 1litegration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
I- - L Summit Environmental Technologies, Inc.
I _al 3310 Win St.
?,C' i'A M 'U J. y _ya err„yr ,'; Cuyahoga Falls, Ohio44223
+'Zna(vrlt'a)' L1borgy'v not TEL: (330) 253-8211 FAX: (330) 2534489
Website: h=://www.settek.com
Client: Synagro
Project: Yadkinville WWTP
QC SUMMARY REPORT
WO#: 19030127
14-ItIar-19
Sample ID LCS-95319 SampType: LCS TestCode: tclp-voc-mstr Units: mg/L Prep Date: RunNo: 95319
Client ID: LCSS Batch ID: R95319 TestNo: SW8260 Analysis Date: 3/5/2019 SegNo: 1984745
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Highl_imit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene 0.0206 0.00500 0.0200 0 103 79.4 131
1,2-Dichloroethane 0.0202 0,00500 0.0200 0 101 73.6 137
MEK 0.111 0.0250 0.100 0 111 55.1 163
Benzene 0.0210 0,00500 0.0200 0 105 73.1 132
Carbon tetrachloride 0.0193 0,00500 0.0200 0 96.4 63.7 139
Chlorobenzene 0.0213 0.00500 0.0200 0 106 72.3 139
Chloroform 0.0198 0400500 0.0200 0 99.0 79.3 129
Tetrachloroethene 0.0235 0400500 0.0200 0 117 56.2 187
Trichloroethene 0.0220 0,00500 0.0200 0 110 64.1 138
Vinyl chloride 0.0191 0000200 0.0200 0 95.7 22.1 147
Surr:4-Bromofluorobenzene 48.5 50.00 96.9 80A 126
Surr: Dibromofluorom ethane 50.1 50.00 100 70.3 125
Surr: Toluene-d8 53.6 50.00 107 82 117
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDhmit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Client: Synagro
Project: Yadkinville WWTP
Summit Environmental Technologies, Inc.
L3310 Win St. QC SUMMARY REPORT
_i.
Cuyahoga Falls, Ohio44223 WO#: 19030127
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: htt42:Ilwww.settelc.com 14-Mar49
BatchID0 R95327
Sample ID LCS-R95327 SampType: LCS TestCode: pH_Oil(9045 Units: s.u.@19.31C Prep Date: RunNo: 95327
Client ID: LCSW Batch ID: R95327 TestNo: SW9045D Analysis Date: 3/5/2019 SegNo: 1983688
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0 100 90 110
Sample ID 19030186-001ADUP SampType: DUP TestCode: pH_Oil(9045 Units: s.u.@20.3C Prep Date: RunNo: 95327
Client ID: BatchQC Batch ID: R95327 TestNo: SW9045D Analysis Date: 3/5/2019 SegNo: 1983690
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua]
pH
6.0
i
6.0 0.5 10
Sample ID CHECK 7 SampType: LCS TestCode: PH_OIL(9045 Units: s.u.@19.2C Prep Date: RunNo: 95327
Client ID: LCSW Batch ID: R95327 TestNo: SW9045D Analysis Date: 3/5/2019 SegNo: 1983707
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0 101 90 110
Qualifiers: * Value exceeds Maximiun Contaminant Level. B Analyte detected in the associated Method Blanlc E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 25 of 31
-- - Summit Environmental Technologies, Inc.
�L3310 Win St.
�J� QC SUMMARY RLPORT
li � •�'1'• : p i
r-;4,'w+lROAMNTAL. a cF',r lca9 C. ;i . Cuyahoga FalZs, Ohio 44223
i
.�?Nydo—f' Lab rd'worle TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 19030127
Website: hO.F11www.settek.com 14-Mar49
Client: Synagro
Project: Yadlinville WWTP
Sample ID
19030127-001AMS
SampType:
MS
Client ID:
Yadkinville WWTP
Batch ID:
R95449
Analyte
Sulfide, Reactive
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
4640 25.0 4800
Sample ID
19030127-001AMSD
SampType:
MSD
Client ID:
Yadkinville WWTP
Batch ID:
R95449
Analyte
Sulfide, Reactive
Result
BatchID: R95449
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
0 96.7 80 120
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
4550 25.0 4800
PreDate:
Analysis Date: 3/6/2019
p
%REC LowLimit HighLimit RPD Ref Val
RunNo: 95449
SegNo: 1987979
%RPD RPDLimit Qual
RunNo: 95449
SegNo: 1987980
%RPD RPDLimit Qual
0
94.8 80 120 4640 1.96 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 26 of 31
- Summit Environmental Technologies, Inc,
It I i F I QC SUMMARY X%JUI '�'
= i 3310 Win St.
l ' E„'oil J;,,� diVI_,iL.L TLC ° 'aal_a Cuyahoga Falls, Ohio44223 WO#: 19030127
V;1Vrc;rn4' La; bari9aritL7 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: httl2://www.settelc.com 14-Mrar49
Client: Synagro
Project: Yadkinville WWTP
Sample ID MB-R95449
Client ID: PBW
Analyte
Sulfide, Reactive
Sample ID LCS-R95449
Client ID: LCSW
Analyte
Sulfide, Reactive
SampType: MBLK
Batch ID: R95449
Result
TestCode: Sulfide,Keact Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
ND 25.0
SampType: LCS
Batch ID: R95449
Result
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
4470 25.0 4800
Prep Date:
Analysis Date: 3/5/2019
°ioREC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
0 93.1 85 115
RunNo: 95449
SegNo: 1987967
%RPD RPDLimit Qual
RunNoI 95449
SegNo: 1987968
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 27 of 31
-- — - - Summit Environmental Technologies, Ina QC SUMMARY REPORT
-- J �L V3310 Win St.
'1,rJ�W,il{ Cuyahoga Falls, Ohio 44223
f r 9i';i r,+Laas' L ai�LrYaJ'ub&m TEL: (330) 253-8211 FAX.• (330) 253-4489
WO#: 19030127
Website: hg2.*11www.settek.com 14-Mar-19
Client: Synagro
Project: Yadkinville WWTP
BatchIDa R95453
Sample ID 19030127-001AMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 95453
Client ID: Yadkinville WWTP Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988039
Analyte Result PQL SPK value SPK Ref Val °'°REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
9.23 0.485 10.00 0.1837 90.4 81.6 122
Sample ID 19030127-001AMSD SampType: MSD
Client ID: Yadkinville WWTP Batch ID: R95453
Analyte
Cyanide, Reactive
Result
TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 95453
TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988040
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
8.74 0.459 10.00 0.1837 85.6 81.6 122 9.226 5.42 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quanutation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 28 of 31
Summit Environmental Technologies, Inc.
-- - QC SUMMARY R.LPORT
- L J 3310 Win St.
I 1 h 9 � j, l . _. I r tq IL Cuyahoga Falls, Ohio 44223 WO#: 19030127
TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: http://Www.settek.com 14-Mar49
Client: Synagro
Project: Yadkinville WWTP
BatchID4 R95453
Sample ID Blank SampType: MBLK TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 95453
Client ID: PBW Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988024
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
Sample ID LCS SampType: LCS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 95453
Client ID: LCSW Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988025
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
9.55 0.490 10.00
0 95.5 85 115
Sample ID RLCheck SampType: RLC TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 95453
Client ID: BatchQC Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988027
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
0.506 0.495 0.5000
0 101 50 150
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank B Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 29 of 31
ul� 3
P AL Fes
Paae 30 of 31
S
Summit Environmental Technologies, Inc.
UMMIT 3310 Win St,
FEN1 lirr+t N NTAL TECHtt.CJI- „t ,'a;,^ Cuyahoga Falls, Ohio44223 3 a m p a Lon gmOn Chis c k Ust
— . Arfa'joicai L s +;rasonoF TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http:Ilwww.settek.coni
Client Name: SYWNC-27028 Work Order Number: 19030127 RcptNo: 1
Logged by: Christopher Livengood 3/1/2019 10:15:00 AM _
Completed By: Jesseca E. Westfall 3/512019 10:12:48 AM 7,L
Reviewed By: Jennifer Woolf 3/5/2019 11:24:21 AM
Chain of Custody
1. Is Chain of Custody complete? Yes. ❑� No ❑ Not Present ❑
2, How was the sample delivered? UPS
Loeb In
3, Coolers are present? Yes❑ No ❑ NA ❑
4, Shipping container/cooler in good condition? Yes � No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes � No ❑ NA ❑
g, Were all samples received at a temperature of >0° C to 6.0°C Yes ❑� No ❑ NA ❑
7, Sample(s) in proper container(s)? Yes � No ❑
$. Sufficient sample volume for indicated test(s)? Yes ❑� No ❑
g. Are samples (except VOA and ONG) properly preserved? Yes❑ No ❑
10. Was preservative added to bottles? Yes ❑ No ® NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials
12. Were any sample containers received broken? Yes ❑ No ❑�
13. Does paperwork match bottle labels? Yes � No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes � No ❑
15. Is it clear what analyses were requested? Yes � No ❑
16. Were all holding times able to be met? Yes ❑� No ❑
(If no, notify customer for authorization.)
Special Handlin_g (if applicable)
17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA 0
Person Notified: � --� Date
By Whom: � Via: ❑ eMail ❑Phone ❑Fax ❑ In Person
Regarding:
Client Instructions:
18, Additional remarks:
COC not received at time of sample receipt. Received pink copy via email 3/5/19
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Si ned B
1
5.2
Good
Not Present
Page 31 of 31
_ Summit Environmental Technologies, Inc.
f 3310 Win St.
��.'Jlii� f•1F1 ,1T�.L 71 C491YCi! - Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 2534489
Website: http://www.settek.com
March 14, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 99M450
RE: Yadkinville WTP
Dear Erik Bruce:
Order No.: 19030122
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/1/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E$7688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
)H0092320114, Virginia VELAP 9456, Washington C891
Page 1 of 31
VIIrt'�MIAIci•JTB,L TECHIN0l 0GI-:3, TNCa
JMM
l�
�LIENT: Synagro
Project: Yadkmville WTP
WorkOrder Narrative:
S
ummit Environmental Technologies, Inc.
3310 Win A
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 2534489
Wehsite: http•/hvww.settek.conz
WO#: 19030122
Date: 3/14/2019
19030122a This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the. accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
19030122Jaw 434787: Prep Comments for MtlPrep_TCLP(3010A), Sample 19030122-OOlA:
Sample was filtered after digestion.
Analytical Sequence QC Notes:
19030122-OOlAMS TCLP-SVOC-Herb_NPW(8151): Surrogate spike recovery possibly indicates
matrix interference. The method is in control as indicated by the laboratory control sample (LCS).
19030122-001AMSD TCLP-SVOC-Herb_NPW(8151): Surrogate spike recovery possibly indicates
matrix interference. The method is in control as indicated by the laboratory control sample (LCS).
1903012MMAMS TCLP-SVOC-CPest(8081B): High RPD due to suspected sample inhomogeheity.
1903012M01AMSD TCLP-SVOC-CPest(8081B): High RPD due to suspected sample inhomogeneity.
Original
Sunzntit Environmental Technologies, be
3310 Win S
Cuyahoga Falls, Ohio 442�
TEL: (330) 253-8211 FAX.• (330) 253-44b
Website: htm://wwwsettek.co.
�' These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
WO#: 19030122
Date: 3/14/2019
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit..
r The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
Ii/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QIa1R The MS/MSD R?'D was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit.
MB MethodBlank LOD Level ofDetection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quaniitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum ContaminationLimit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial CalibrationBlank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 31
y%
p AIN A, M�� A
_lik��lr(_5 JP
W pe�W1•,lArAL j�y�i.7j. 'vr�� ��tiil ?il'.i ,
CLIETVT: Synagro
Project, Yadkinville WTP
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.• (330) 253-4489
Website; http://www.settek.com
Lab SampleID Client Sample ID Tag No
19030122-OOl Yadkinville WTP
Date Collected
2/27/2019 9:05:00 AM
WO#: 19030122
Date Received
3/1/2019 10:15:00 AM
14 Mar 19
Matrix
Solid
Page 4 of 31
Summit Environmental Technologies, Inc. '~
i. 1 3310 Win St.
elo��_+rl�.iir.aeL rrP Cuyahoga Falls, Ohio44223
z a it td�ar Lr-barnforiE TEL: (330) 2534211 FAX: (330) 253-4489
Website: httn:11www.settek.com
DATES R 1OII T
WO#: 19030122
14-Ndar-19'
CIlienta Synagro
roject: Yadkinville WTP
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
19030122-001A Yadkinville WTP 2/27/2019 9:05:00 AM Solid Ignitability of Solids (SW-846: 1030) 3/5/2019 12:00:00 PM
pH (SW9045D) 3/5/2019 2:30:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid 3/5/2019 5:16:00 PM
Reactive Sulfide (9034)/7.3.4.2 3/5/2019 5:16:00 PM
SVOC SW-846: 8151 Herbicides-TCL3/4/2019 6:00:00 PM 3/7/2019 3:00:00 PM 3/12/2019 8:41:00 PM
TCLP Mercury Analysis (SW1311/7473/4/2019 6:00:00 PM 3/6/2019 12:40:00 PM 3/6/2019 4:43:00 PM
TCLP Metals Analysis (SW1311/6010'3/4/2019 6:00:00 PM 3/6/2019 8:10:00 AM 3/6/2019 5:21:25 PM
TCLP Pesticides Analysis (SW1311/8(3/4/2019 6:00:00 PM 3/11/2019 5:20:00 PM 3/12/2019 8:26:00 PM
TCLP Semi-Volatiles Analysis 3/4/2019 6:00:00 PM 3/11/2019 12:15:00 PM 3/12/2019 4:27:00 PM
(SW1311/8270)
TCLP Volatiles Analysis 3/5/2019 3:07:00 PM
®riginal
Paae5of�=1
Summit Environmental Technologies, Inc.
Summoir 3310 Win St.
Pd4'I!OWNI�NT"u.L TECRb'01 C!M7ASjTwr1rh Cuyahoga Falls, Ohio 44223
.Ana;{ t,'Cal L2barafovo! TEL: (330) 253-8211 FAX.• (330) 2534489
b:report)
• 'I I
Webszte:://www.settek.com Date Reported: 3/14/2019
'LIENT: Synagro Tag Number:
Matrix• SOLID Collection Date: 2/27/2019 9:05:00 AM
Lab ID: 19030122-001A
Project: Yadkinville WTP
Client Sample ID Yadkinville WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND 0.00200
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW131116010)
SW7470A SW7470A Analyst: DNS
mg/L 1 3!6/2019 4:43:00 PM
SW6010D SW3010A Analyst: KMO
TCLP
Arsenic(As)
ND
0.500
mg/L
1
3/6/2019
5:21:25
PM
TCLP
Barium(Ba)
ND
5.00
mg/L
1
3/6/2019
5:21:25
PM
TCLP
Cadmium(Col)
ND
0.100
mg/L
1
3/6/2019
5:21:25
PM
TCLP
Chromium(Cr)
ND
0.200
mg/L
1
3/6/2019
5:21:25
PM
TCLP
Lead(Pb)
ND
0.500
mg/L
1
3/6/2019
5:21:25
PM
TCLP
Selenium(Se)
ND
0.0500
mg/L
1
3/6/2019
5:21:25
PM
TCLP
Silver(Ag)
ND
0.500
mg/L
1
3/6/2019
5:21:25
PM
'CLP METALS, VOC, BNA, PEST; HERB -SOLID SW8270, Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.0800 mg/L 2 3/12/2019 4:27:00 PM
2,4,5-Trichlorophenol ND 0.200 mg/L 2 3/12/2019 4:27:00 PM
2,4,6-Trichlorophenol ND 0.200 mg/L 2 3/12/2019 4:27:00 PM
2,4-Dinitrotoluene ND 0.0400 mg/L 2 3/12/2019 4:27:00 PM
Cresols, Total ND 4.00 mg/L 2 3/12/2019 4:27:00 PM
Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 3/12/2019 4:27:00 PM
Hexachlorobenzene ND 0.0400 mg/L 2 3/12/2019 4:27:00 PM
Hexachloroethane ND 0.0800 mg/L 2 3/12/2019 4:27:00 PM
Nitrobenzene ND 0.0800 mg/L 2 3/12/2019 4:27:00 PM
Pentachlorophenol ND 0.200 mg/L 2 3/12/2019 4:27:00 PM
Pyridine ND 0.200 mg/L 2 3/12/2019 4:27:00 PM
Surr: 2-Fluorophenol 53.2 10 - 109 %Rec 2 3/12/2019 4:27:00 PM
Surr: PhenolA6 56.3 10 - 109 %Rec 2 3/12/2019 4:27:00 PM
Surr: Nitrobenzene-d5 68A 19 - 120 %Rec 2 3/12/2019 4:27:00 PM
Surr: 2,4,6-Tribromophenol 66.6 10 - 120 %Rec 2 3/12/2019 4:27:00 PM
Surr: 2-171uorobiphenyl 66.1 22 - 117 %Rec 2 3/12/2019 4:27:00 PM
Surr: p-Terphenyl-d14 88.6 34 - 116 %Rec 2 3/12/2019 4:27:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 6 ®f 31
- - Sununit Environmental Technologies, Inc.
I,t,Lt " ' � V, A ' ` a i l 3310 Win St.
HOWN1_t•JTAL 3Zrr11t'+Qi.')1 ,,,17'� Cuyahoga Falls, Ohio 44223
-- -F Ajta-Vroloal L gbnyafano TEL: (330) 253-8211 FAX: (330) 253-4489
Wb' l // 1
CLIENT: Synagro
Matrix: SOLID
Lab ID: 19030122-001A
Project: Yadkinville WTP
Client Sample ID Yadkinville WTP
Analytical Report
(base report)
WO#: 19030122
e stte. 1ttp. www.sette c.cona Date Reported: 3/14/2019
Tag Number:
Collection Date: 2/27/2019 9:05:00 AM
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.250
Toxaphene
ND
0.500
Endrin
ND
0.0250
gamma-BHC
ND
0.0250
Heptachlor
ND
0.0250
Heptachlor epoxide
ND
0.0250
Methoxychlor
ND
0.0250
Surr: TCMX
94.5
10 - 119
Surr: DCB
99A
10 - 119
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
2,4,5-TP
ND
1.00
ND 0.500
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
fJ
mg/L
mg/L
mg/L
mg/L
m g/L
m g/L
mglL
%Rec
%Rec
SW8081 SW3510C Analyst: SFG
SW8151A
m g/L
d mg/L
SW8260
10
3/12/2019
8:26:00
PM
10
3/12/2019
8-126:00
PM
10
3/12/2019
8:261-00
PM
10
3/12/2019
8:26:00
PM
10
3/12/2019
8:26:00
PM
10
3/12/2019
8:26:00
PM
10
3/12/2019
8:26:00
PM
10
3/12/2019
8:26:00
PM
10
3/12/2019
8:26-100
PM
SW8151A Analyst: SFG
1
3/12/2019
8:41:00
PM
1
3/12l2019
8:41:00
PM
Analyst: CTB
1,1-Dichloroethene ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
1,2-Dichloroethane ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
MEK ND 1.25 mg/L 50 3/5/2019 3:07:00 PM
Benzene ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
Carbon tetrachloride ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
Chlorobenzene ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
Chloroform ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
Tetrachloroethene ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
Trichloroethene ND 0.250 mg/L 50 3/5/2019 3:07:00 PM
Vinyl chloride ND 0.100 mg/L 50 3/5/2019 3:07-100 PM
Sum- 4-Bromofluorobenzene 92.9 70 - 130 %Rec 50 3/5/2019 3-107-100 PM
Surr: Dibrom ofluorom ethane 87.7 70 - 130 %Rec 50 3/5/2019 3-107:00 PM
Surr: Toluene-d8 101 70 - 130 %Rec 50 3/5/2019 3:07:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 31
LIENT: Synagro
Matrix. SOLID
Lab ID: 19030122-001A
Project: Yadkinville WTP
Client Sample ID Yadkinville WTP
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability
RCI-SOLID-W/ IGNITABILITY1030
PH (SW9045D)
pu
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
Sunanait Environmental Technologies, Inc.
3310 Yf/rin A
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 253-4489
ND
flammable
non-
7.1
ND
Analytical Report
(base report)
WO#: 19030122
Webstte. http.//ivwlvsettekcona Date Reported: 3/14/2019
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
Tag Number:
Collection Date: 2/27/2019 9:05:00 AM
Si/1/9014 Analyst: MS
0.472 mg/Kg 1 3/5/2019 5:16:00 PM
SW1030 Analyst: AJT
1 3/5/2019 12:00:00 PM
SW9045D Analyst: DHC
s.L�.�19.4C 1 3/5/2019230:00PM
SW9034 Analyst: MS
25.0 mg/Kg 1 3/5/2019 5:16:00 PM
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 31
_ _ Summit Environrarental Technologies, Inc. ������' Il��t�®� ����� ��
.. _ 3310 Win St. AL��� ��� �(� ��°�
��'."Iltr'�tJP+1_�dT�L 6.` ai�C�l- � �;' Cuyahoga Falls, Ohio 44223
tl�^,i!-_,., sec';
- — .���il�'d4�t' i���Yrat�t'deg TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 19030122
Website: http://www.settekcom I4-Mar-19
Client: Synagro State: NC
Project: Yadkinville WTP Program Name: NC WW SCM
Sample ID Matrix Test Name Analyte Status
19030122-OOlA Solid Ignitability of Solids (SW-846: 1030) Ignitability A
Solid pH (SW9045D) Hydrogen Ion (pH) A
Solid Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U
Solid Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Solid SVOC SW-846: 8151 Herbicides-TCLP 2,4,5-TP A
Solid SVOC SW-846: 8151 Herbicides-TCLP 2,4-D A
Solid TCLP Mercury Analysis (SW1311/7470) Mercury A
Solid TCLP Metals Analysis (SW1311/6010) Arsenic A
Solid. TCLP Metals Analysis (SW1311/6010) Barium A
Solid TCLP Metals Analysis (SW131Z/6010) Cadmium A
Solid TCLP Metals Analysis (SW1311/6010) Chromium A
Solid TCLP Metals Analysis (SW1311/6010) Lead A
Solid TCLP Metals Analysis (SW1311/6010) - Selenium A
Solid TCLP Metals Analysis (SW1311/60I0) Silver A
Solid TCLP Pesticides Analysis (SW1311/8081) Chlordane,. total A
Solid TCLP Pesticides Analysis (SW1311/8081) Endrin A
Solid TCLP Pesticides Analysis (SW1311/8081) gamma-BHC A
Solid TCLP Pesticides Analysis (SW13ll/8081) Heptachlor A
Solid TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A
Solid TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A
Solid TCLP Pesticides Analysis (SW1311/8081) Toxaphene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Nitrobenzene A
Solid TCLP Semi-Volatiles Analysis (SW1311/8270) Pentachlorophenol A
Solid. TCLP Semi-Volatiles Analysis (SW1311/8270) Pyridine A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original # 1
t _ Summit Environmental Technologies, Inc.�rogirn
3310 Win St. Al Ill O tes Report
_w"v"1�_" P.1h1rt.Si.L t'i0t + :-�, r, Cuyahoga Falls, Ohio44223
- ARa(yrilcal "W.?baralarw TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 19030122
Website: hg2:11www.settek.com 14-Mar49
Client: Synagro State: NC
Project: Yadkinville WTP Program Name: NC WW SCM
Sample ID Matrix Test Name Analyte Status
1903012M01A Solid TCLP Volatiles Analysis 1,1-Dichloroethene A
Solid TCLP Volatiles Analysis 1,2-Dichloroethane A
Solid TCLP Volatiles Analysis 2-Butanone A
Solid TCLP Volatiles Analysis Benzene A
Solid TCLP Volatiles Analysis Carbon tetrachloride A
Solid TCLP Volatiles Analysis Chlorobenzene A
Solid TCLP Volatiles Analysis Chloroform A
Solid TCLP Volatiles Analysis Tetrachloroethene A
Solid TCLP Volatiles Analysis Trichloroethene A
Solid TCLP Volatiles Analysis Vinyl chloride A
NC WW SCM A Accredited NC WW SCM U Unavailable
Page 10 of 31
Original # 1
-1 r- - -. -- Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY Rt'ORT
L
ClI C" P, - Cuyahoga Falls, Ohio 44223 „
_ TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 19030122
Website: hW.&11www.settek.com 14111,Mar49
Client: Synagro
Project: Yadldnville WTP
)BatchID: 36252
Sample ID 19030086-001AMS SampType: MS TestCode: MTL-TCLP-7( Units: mg/L Prep Date: 3/6/2019 RunNo: 95376
Client ID: BatchQC Batch ID: 36252 TestNo: SW6010D SW3010A Analysis Date: 3/6/2019 SegNo: 1987166
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP
Arsenic(As)
2.31
0.500
2.000
0
115
70
130
TCLP
Barium(Ba)
ND
5.00
2.000
0.2767
99.1
70
130
TCLP
Cadmium(Cd)
1.97
0.100
2.000
0
98A
70
130
TCLP
Chromium(Cr)
2.11
0.200
2.000
0
105
70
130
TCLP
Lead(Pb)
2.06
0.500
2.000
0
103
70
130
TCLP
Selenium(Se)
2.39
0.0500
2.000
0,02516
118
70
130
TCLP
Silver(Ag)
2.37
0.500
2.000
0
118
70
130
Sample ID 19030086-001AMSD SampType: MSD
Client ID: BatchQC Batch ID: 36252
Analyte
Result
TestCode: MTL-TCLP-7( Units: mg/L Prep Date: 3/6/2019
TestNo: SW6010D SW3010A Analysis Date: 3/6/2019
PQL SPK value SPK Ref Val `%REC LowLimit HighLimit RPD Ref Val
RunNo: 95376
SegNo: 1987167
%RPD RPDLimit Qual
TCLP
Arsenic(As)
2.35
0.500
2.000
0
117
70
130
2.310 1.68
20
TCLP
Barium(Ba)
ND
5.00
2.000
0.2767
101
70
130
0 0
20
TCLP
Cadmium(Cd)
1.99
0.100
2.000
0
99.7
70
130
1.967 1.30
20
TCLP
Chromium(Cr)
2.15
0.200
2.000
0
107
70
130
2.109 1.77
20
TCLP
Lead(Pb)
2.08
0.500
2.000
0
104
70
130
2.061 0.952
20
TCLP
Selenium(Se)
2.42
0.0500
2.000
0.02516
120
70
130
2.392 1.33
20
TCLP
Silver(Ag)
2.40
0.500
2.000
0
120
70
130
2.368 1.48
20
Qualifiers: *
Value exceeds Maximum Contamiriant Level.
B
Analyte
detected in the
associated Method
Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte
detected below
quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Pen -nit
Limit
R
RPD outside accepted recovery limits
Original
Page 11 of 3'1
Summit Environmental Technologies, Inc.
1 1 1 J L�Jr 3310 Win St, QC SUMMARY R 1,PORT
p
Cuyahoga FallsOhio 44223
TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 19030122
Website: htto:llwww.settek.com 14-Mar49
Client: Synagro
Project: Yadlcinville WTP
�atchIDa 36252
Sample ID MB-36252 SampType: MBLK TestCode: MTL-TCLP-'( Units: mg/L Prep Date: 3/6/2019 RunNo: 95376
Client ID: PBS Batch ID: 36252 TestNo: SW6010D SW3010A Analysis Date: 3/6/2019 SegNo: 1998092
Analyte
Result
PQL SPK value SPK Ref Val
TCLP Arsenic(As) ND 0.500
TCLP Barium(Ba) ND 5.00
TCLP Cadmium(Cd) ND 0.100
TCLP Chromium(Cr) ND 0.200
TCLP Lead(Pb) ND 0.500
TCLP Selenium(Se) ND 0.0500
TCLP Silver(Ag) ND 0.500
Sample ID LCS-36252
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 36252
Result
TestCode: MTL-TCLP-7'( Units: mg/L
TestNo: SW6010D SW3010A
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
Prep Date: 3/6/2019
Analysis Date: 3/6/2019
`%REC LowLimit HighLimit RPD Ref Val
TCLP Arsenic(As) 2.09 0.500 2.000 0 104 80 120
TCLP Barium(Ba) ND 5.00 2.000 0 105 80 120
TCLP Cadmium(Cd) 1.87 0.100 2.000 0 93.6 80 120
TCLP Chromium(Cr) 2.12 0.200 2.000 0 106 80 120
TCLP Lead(Pb) 2.15 0.500 2.000 0 108 80 120
TCLP Selenium(Se) 2.08 0.0500 2.000 0 104 80 120
TCLP Silver(Ag) 2.24 0.500 2.000 0 112 80 120
%RPD RPDLimit Qual
RunNo: 95376
SegNo: 1998093
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding tunes for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 12 of 30I
�- Summit Environmental Technologies, Inc. QC SUMMARYRmOORT
— ri- ,r I I �I L 3310 Win St.
Cuyahoga Falls, Ohio44223
=:+;i��r,��r' �' F.B,_+��Pbx� WO#: 19030122
.jfTEL: (330) 253-8211 FAX: (330) 253-4489
Website: hgp://www.settek.com 14-Mar49
Client: Synagro
Project, Yadkinville WTP BatchID: 36264
TCLP Mercury ND 0.00200
TCLP Mercury 0.00409 0.00200 0.00400 0 102 80 120
TCLP Mercury 0.00445 0.00200 0.00400 0 111 75 125
Sample ID 19030086-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM
Analyte
Result PQL SPK value SPK Ref Val
Prep Date: 3/6/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 95406
%RPD RPDLimit Oual
TCLP Mercury 0.00443 0.00200 0.00400 0 111 75 125 0.00445 0.450 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 13 of 31
r — -- Summit Environmental Technologies, wUMMARY
4 IL QSPORT
11 oil.
- 3310 Win St. d SUMMARY
Cuyahoga Falls, Ohio44223
Ajr+ t'yNc rd' Laboari �Yonell TEL: (330) 2531-8211 FAX* (330) 2534489 WO#: 19030122
Website: hyg.ii www.settekcom 14-Mar~19
Client: Synagro
Project: Yadkinville WTP
Sample ID
19030086-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
36264
Analyte
Result
TestCode: HG_TCLP(74 units: PPM
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
Prep Date: 3/6/2019
Analysis Date: 3/6/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 95406
SegNo: 1986476
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 14 of 31
-_ _- Summit Environmental Technologies, Inc.
iL
3310 Win St, QC SUMMARY RLP®RT
+': r� +L err Cuyahoga Falls, Ohio 44223 i� 1
0 LL m I 1J ^'.+p�+ o' ! _vjJbr tjyoraL� r TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 19030122
Website: http://www.settelzcom 14-Mar49
Client: Synagro
Project: Yadkinville WTP
�atchID: 36316
Sample ID MB-36316 SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: 3/7/2019 RunNo: 95654
Client ID: PBS Batch ID: 36316 TestNo: SW8151A SW8151A Analysis Date: 3/12/2019 SegNo: 1996428
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D ND 1.00 d
21415-TP ND 0.500 d
Sum 2,4-Dichlorophenylacetic acid 373 500.0 74.6 20 140
Sample ID LCS-36316 SampType: LCS TestCode: TCLPSVOC- Units: mg/L Prep Date: 3/7/2019 RunNo: 95654
Client ID: LCSS Batch ID: 36316 TestNo: SW8151A SW8151A Analysis Date: 311212019 SegNo: 1996429
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 19,
214-D
ND
1.00 0.500
0 73.6
43.8
130
21415-TP
ND
0.500 0.500
0 67.2
51.5
111
Surr: 2,4-Dichlorophenylacetic acid
468
500.0
93.5
34.2
150
Sample ID 19030122-001AMS SampType: MS
Client ID: Yadkinville WTP Batch ID: 36316
Analyte
Result
TestCode:
TCLPSVOC-
Units:
mg/L
TestNo:
SW8151A
SW8151A
PQL SPK value SPK Ref Val
Prep Date: 3/7/2019
Analysis Date: 3/12/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 95654
SegNo: 1996430
On
RPDLimit Qual
214-D ND 1.00 0.500 0 73.7 37 105 m
2,4,5-TP ND 0.500 0.500 0 70A 38 106 m
Sum 2,4-Dichlorophenylacetic acid 713 500.0 143 20 140 Sm
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 15 of 301
Summit Environmental Technologies, Inc.
_ J L� 'f 3310 Win St. L QC SUMMARY R-eORT
l
4I; IDiJVJd1� L �� �Cv, 101 G , - Cuyahoga Falls, Ohio 44223
d �g'rIcfa L-clbexradorJ& TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 19030122
�,�
Website: hW.'11www.settek.com 14-Mar~19
Client: Synagro
Project: Yadkinville WTP
]BatchID: 36316
Sample ID 19030122-001AMSD SampType: MSD TestCode: TCLPSVOC- Units: mg/L Prep Date: 3/7/2019 RunNo: 95654
Client ID: Yadkinville WTP Batch ID: 36316 TestNo: SW8151A SW8151A Analysis Date: 3/12/2019 SegNo: 1996431
Analyte
Result
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
274-D
ND
1.00 0.500
0 67.2
37
105
0 0
30
m
21415-TP
ND
0.500 0.500
0 64.6
38
106
0 0
30
m
Surr: 2,4-Dichlorophenylacetic acid
875
500.0
175
20
140
0
30
Sm
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manua1111tegration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 16 of 301
- - L Summit Environmental Technologies, Inc.
� 3310 Win St.
JI 1;,, ud 1 ; T° L E C! i, CAI C r Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: htt12:11Www.settek.com
Client: Synagro
Project: Yadlcinville WTP
QC SUMMARY R-L-eORT
WO#: 19030122
14-NZaY-I9
BatchID: 36331a
Sample ID LCS-36331 Samp I ype: LCS TestCode: TCLPSVOC_ Units: mg/L Prep Date: 3/11/2019
Client ID: LCSS Batch ID: 36331a TestNo: SW8270 Analysis Date: 3/12/2019
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 95613
SegNo: 1996811
%RPD RPDLimit Qual
124-Dichlorobenzene
0.491
0.0400
0.8000
0
61.4
19.1
126
2,4,5-Trichlorophenol
0.633
0.100
0.8000
0
79.2
11.7
151
2,4,6-Trichlorophenol
0.719
0.100
0.8000
0
89.9
12A
150
2,4-Dinitrotoluene
0.741
0.0200
0.8000
0
92.7
20.6
140
o-Cresol
0.623
0.100
0.8000
0
77.9
13.8
137
Cresols, Total
ND
2.00
1.600
0
77.2
10
129
Hexachloro-1,3-butadiene
0.378
0,00800
0.8000
0
47.2
14.7
137
Hexachlorobenzene
0.672
0.0200
0.8000
0
84.0
12
139
Hexachloroethane
0.386
0.0400
0.8000
0
48.2
14.8
132
Nitrobenzene
0.676
0.0400
0.8000
0
84.6
15.6
138
Pentachlorophenol
0.721
0.100
0.8000
0
90.2
10
156
Pyridine
0.366
0.100
0.8000
0
45.7
1
130
Surr: 2111Fluorophenol
0.609
1.000
60.9
10
147
Surr: Phenokc[6
0.587
1.000
58.7
10
140
Surr. Nitrobenzene-d5
0.763
1.000
76.3
10
169
Surr: 2,4,6-Tribromophenol
0.795
1.000
79.5
10
185
Surr:2-Fluorobiphenyl
0.664
1.000
66A
10
169
Surr: p-Terphenyl-d14
1.02
1.000
102
10
179
Qualifiers: * Value exceeds
Maximum Contaminant Level.
B
Analyte detected
in the
associated Method
Blank
E
Value above quantitation range
H Holding times
for preparation or
analysis exceeded
J
Analyte detected
below
quantitation
limits
M
Manual hitegration used to determine
MC Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 17 of 301
-- L:
1 �^
FFI
- - 3.i K/ �' LAF7�JLei 9ria
Client: Synagro
Project: Yadlunville WTP
Summit Environmental Technologies, Inc.
3310 Win St,
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: htW:Ilwww.settelc.com
QC SUMMARY P%i)RT
WO#: 19030122
14-Mar-19
BatchTD: 36331a
Sample ID 1V1B-36331 SampType: MBLK TeStCode: TCLP SVOG_ Units: mg/L Prep Date: 3/11/2019
Client ID: PBS Batch ID: 36331a TestNo: SW8270 Analysis Date: 311212019
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 95613
SegNo: 1998657
%RPD RPDLimit Qual
1,4-Dichlorobenzene ND 0.0400
2,4,5-Trichlorophenol ND 0.100
2,4,6-Trichlorophenol ND 0.100
2,4-Dinitrotoluene ND 0.0200
o-Cresol ND 0.100
Cresols, Total ND 2.00
Hexachloro-1,3-butadiene ND 0,00800
Hexachlorobenzene ND 0.0200
Hexachloroethane ND 0.0400
Nitrobenzene ND 0.0400
Pentachlorophenol ND 0.100
Pyridine ND 0.100
Surr: 2-Fluorophenol 0.496 1.000 49.6 10 109
Sum Phenol-d6 0.503 1.000 50.3 10 109
Sum, Nitrobenzene-d5 0.621 1.000 62A 19 120
Sum 2,4,6-Tribromophenol 0.623 1.000 62.3 10 120
Surr:2-Fluorobiphenyl 0.567 1.000 56.7 22 117
Sum p-Terphenyl-d14 0.728 1.000 72.8 34 116
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 18 of 31
Summit Environmental Technologies, Inc. �! +SUMMARY 77 JORT
3310 Win St. 1. 1J V l�ll�.ir�.i` i itLl
I +01111 •;r+l 0e r:.,. -. Cuyahoga Falls, Ohio 44223 WO#:. 19030122
TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: hZ.*11www.settek.com 14-Mar49
Client: Synagro
Project: Yadkinville WTP
BatchIDa 36332
Sample ID MB-36332 SampType: MBLK TestCode: TCLPSVOC- Units: mg/L Prep Date: 3/11/2019 RunNo: 95664
Client ID: PBS Batch ID: 36332 TestNo: SW8081 SW3510C Analysis Date: 311212019 SegNo: 1996798
Analyte Result PQL SPK value SPK Ref Val
Chlordane, total
ND
0.0250
Toxaphene
ND
0.0500
Endrin
ND
0,00250
gamma-BHC
ND
0,00250
Heptachlor
ND
0.00250
Heptachlor epoxide
ND
0,00250
Methoxychlor
ND
0,00250
Surr: TCMX
12.1
Surr: DCB
15A
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
d
d
20.00 60.3 10 119 m
20.00 77.1 10 119
Sample ID LCS-36332 SampType: LCS TestCode: TCLPSVOC- Units: mg/L Prep Date: 3/11/2019 RunNo: 95664
Client ID: LCSS Batch ID: 36332 TestNo: SW8081 SW3510C Analysis Date: 3/12/2019 SegNo: 1996799
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
Endrin
0.0130
0.00250
0.0250
0
52.0
20
157
gamma-BHC
0.0112
0,00250
0.0250
0
44.7
22
137
Heptachlor
0.0105
0.00250
0.0250
0
42.2
24
121
Heptachlor epoxide
0.0117
0,00250
0.0250
0
46.9
27
152
Methoxychlor
0.0131
0,00250
0.0250
0
52A
10
199
Surr: TCMX
12.8
20.00
64.0
10
119
Surr: DCB
16.7
20.00
83.5
10
119
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit, ND Not Detected 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Pen -nit Limit R RPD outside accepted recovery limits
Page 19 of 31
i oil Summit Environmental Technolo ies, Inc.
- 'I1 , _. �_�! I� �L�� 3310 Win St, QC SUMMARY R i eORT
I-r, Cuyahoga Falls, Ohio 44223
- TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 19030122
Website: httl2://www.settek.corn 14-Mar49
Client: Synagro
Project: Yadkinville WTP
Sample ID 19030122-001AMS SampType: MS
Client ID: Yadkinville WTP Batch ID: 36332
Analyte
Result
BatchID0 36332
TestCode: TCLP SVOC- Units: mg/L Prep Date: 3/11/2019 RunNo: 95664
TestNo: SW8081 SW3510C Analysis Date: 3/12/2019 SegNo: 1996800
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
Endrin
ND
0.0250
0.0250
0
71.1
20
157
gamma-BHC
ND
0.0250
0.0250
0
60.3
22
137
Heptachlor
ND
0.0250
0.0250
0
59.6
24
121
Heptachlor epoxide
ND
0.0250
0.0250
0
67.8
27
152
Methoxychlor
ND
0.0250
0.0250
0
77.8
10
199
Surr: TCMX
18.9
20.00
94.4
10
119
Surr: DCB
21.7
20.00
109
10
119
Sample ID
19030122-001AMSD
SampType:
MSD
Client ID:
Yadkinville WTP
Batch ID:
36332
Analyte
Result
TestCode: TCLP-SVOC•• Units: mg/L
TestNo: SW8081 SW3510C
PQL SPK value SPK Ref Val
Prep Date: 3/11/2019
Analysis Date: 3/12/2019
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
m
RunNo: 95664
SegNo: 1996801
%RPD RPDLimit Qual
Endrin
ND
0.0250
0.0250
0
56.7
20
157
0
0
30
gamma-BHC
ND
0.0250
0.0250
0
53.1
22
137
0
0
30
Heptachlor
ND
0.0250
0.0250
0
50.2
24
121
0
0
30
Heptachlor epoxide
ND
0.0250
0.0250
0
56.6
27
152
0
0
30
Methoxychlor
ND
0.0250
0.0250
0
59.1
10
199
0
0
30
Surr: TCMX
16.5
20.00
82.3
10
119
0
Surr: DCB
17.5
20.00
87.7
10
119
0
Qualifiers: *
Value exceeds Maxnmm� Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 20 of 31
- Summit Environmental Technologies, Inc. (�! SUMMARY 77nJ
?ORT ��I J� 3310WinSt. �Cl. SUMMARY [�
�I, �r�rtr•]T�I r,;;� �el�r, ;L,. Cuyahoga Falls, Ohio 44223
WO#: 19030122
TEL: (330) 253-8211 FfIX.• (330) 253-4489
Website: htW:Ilwww.settek.com. 14-MaY-19
Client. Synagro
Project: Yadkinville WTP BatchII): R95317
Ignitability 7.60 7.240 0 105 70 130
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSA is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 21 of 31
_ H -- — - L Summit Environmental Technologies, Inc. �y r�
- ` � �i 3310 Win St. QC SUMMARY R-LPOR Jl
177 11EN41101COIJPal L;x'�UI . U:Cj ,,4I01 Cb a'� ' , '�l'�l Cuyahoga Falls, Ohio 44223
al
44,r,+j� ytknfi Lsbijr&'arwd . TEL: (330) 253-8211 FAX: (330) 253-4489
WO#: 19030122
Website: http://www.settek.com 14-Mar49
Client: Synagro
Project: Yadkinville WTP BatchID: R95317
Sample ID
19030124-001ADUP
SampType:
DUP
Client ID:
Batch=
Batch ID:
R95317
Analyte
Result
Sample ID
19030125-001ADUP
SampType:
DUP
Client ID:
Batch=
Batch ID:
R95317
Analyte
Result
TestCode:
Ignitability_S Units:
Prep
Date:
RUnNo:
95317
TestNo:
SW1030
Analysis
Date: 3/5/2019
SegNo:
1983557
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 95317
SegNo: 1983559
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID
19030127-001ADUP
SampType:
DUP
Client ID:
Batch=
Batch ID:
R95317
Analyte
Result
TestCode: Ignitability_S Units:
TestNo: SW1030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
RunNo: 95317
SegNo: 1983561
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected ni the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to deterul e
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 22 of 31
Summit Environmental Technologies, Inc.
3310 Win St,
QC SUMMARY REPORT
1 +e n 9 Vd i •1`r: L„ I o ram: Cuyahoga Falls, Ohio 44223 WO#: 19030122
TEL: (330) 253-8211 FIX: (330) 253-4489
Website: hQ:Ilwww.settelc.com I4-Mar49
Client: Synagro
Project: Yadkinville WTP
Sample ID MB-95319 SampType: MBLK
Client ID: PBS Batch ID: R95319
Analyte Result
TestCode: tclp-voc-mstr Units: mg/L
TestNo: SW8260
PQL SPK value SPK Ref Val
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0,00500
MEK
ND
0.0250
Benzene
ND
0,00500
Carbon tetrachloride
ND
0,00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0,00500
Trichloroethene
ND
0,00500
Vinyl chloride
ND
0,00200
Surr: 4-Bromofluorobenzene
46.8
Surr: Dibromofluoromethane
43A
Surr: Toluene-d8
52.3
Batchll)a R95319
Prep Date:
Analysis Date: W5/2019
%REC LowLimit HighLimit RPD Ref Val
50.00
93.6
70 130
50.00
86.9
70 130
50.00
105
70 130
RunNo: 95319
SegNo: 1983592
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blanlc E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 23 of 31
-Y Summit Environmental Technologies, Inc.
3310 Win St,
s,I rJVol arsr u ZIa; �';�r i; Cuyahoga Falls, Ohio44223
TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: hO.*11www.settek.com
Client: Synagro
Project: Yadkinville WTP
QC SUMMARY REPORT
WO#: 19030122
14-1�1ar-19
Sample ID LCS-95319 SampType: LCS TestCode: tclp-voc-mstr Units: mg/L Prep Date. RunNo: 95319
Client ID: LOSS Batch ID: R95319 TestNo: SW8260 Analysis Date: 3/5/2019 SegNo: 1984745
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene
0.0206
0.00500
0.0200
0
103
79.4
131
1,2-Dichloroethane
0.0202
0,00500
0.0200
0
101
73.6
137
MEK
0.111
0.0250
0.100
0
111
55.1
163
Benzene
0.0210
0400500
0.0200
0
105
73.1
132
Carbon tetrachloride
0.0193
0000500
0.0200
0
96A
63.7
139
Chlorobenzene
0.0213
0000500
0.0200
0
106
7203
139
Chloroform
0.0198
0,00500
0.0200
0
99.0
79.3
129
Tetrachloroethene
0.0235
0.00500
0.0200
0
117
56.2
187
Trichloroethene
0.0220
0,00500
0.0200
0
110
64.1
138
Vinyl chloride
0.0191
0,00200
0.0200
0
95.7
22.1
147
Surr:4-Bromofluorobenzene
48.5
50.00
96.9
80A
126
Surr: Dibromofluoromethane
50.1
50.00
100
70.3
125
Surr: Toluene-d8
53.6
50.00
107
82
117
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Summit Environmental Technologies, Inc. QC SUMMARY
7� PORT
LI l� <J Y 1�L JL
_J 3310 Win St.
IJ
A 1 s r s' I 114, 1 _ , li r. L : CA e Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX: (330) 2534489 WO#: 19030122
r Iv'-t �Ipi R1 i - - • Y
Website: http://www.settelc.com 14-Mar49
Client: Synagro
Project. Yadkinville WTP
SatchID: R95327
Sample ID LCS-R95327 SampType: LCS TestCode: pH_Oil(9045 Units: s.u.@19.3C Prep Date:
Client ID: LCSW Batch ID: R95327 TestNo: SW9045D Analysis Date: 3/5/2019
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
pH
7.0
7.0
0 100 90 110
RunNo: 95327
SegNo: 1983688
%RPD RPDLimit Qual
Sample ID 19030186-001ADUP SampType: DUP TestCode: pH_Oil(9045 Units: s.u.@20.3C Prep Date: RunNo: 95327
Client ID: BatchQC Batch ID: R95327 TestNo: SW9045D Analysis Date: 3/5/2019 SegNo: 1983690
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
6.0
0
0
6.0 0.5 10
Sample ID CHECK 7 SampType: LCS TestCode: PH_OIL(9045 Units: s.u.@19.2C Prep Date: RunNo: 95327
Client ID: LCSW Batch ID: R95327 TestNo: SW9045D Analysis Date: 3/5/2019 SegNo: 1983707
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
0 101
90 110
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blanlc E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual wtegration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 25 of 31
Summit Environmental Technologies, Inc.
- L r 3310 Win St. QC SUMMARY REPORT
41sir+i9f I :•1`i�L ' e9 r Cuyahoga Falls, Ohio 44223
A.i7a!'y0c: P La orrAlvill TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 19030122
Website: http:llwww.settek.com 14-Mar49
Client: Synagro
Project: Yadkinville WTP
Sample ID
19030127-001AMS
SampType:
MS
Client ID:
BatchQC
Batch ID:
R95449
Analyte
Sulfide, Reactive
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
4640 25.0 4800
Sample ID
19030127-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R95449
Analyte
Sulfide, Reactive
Result
BatchID0 R95449
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
0 96.7 80 120
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
PQL SPK value SPK Ref Val
4550 25.0 4800
Prep Date:
Analysis Date:
RunNo: 95449
SegNo: 1987979
%RPD RPDLimit Qual
RunNo: 95449
3/5/2019 SegNo: 1987980
°�oREC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
0 94.8 80 120 4640 1.96 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual filtegration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Original
Page 26 of 31
— Summit Environmental Technologies, Inc.
L� 3310 Win St, QC SUMMARY RLPORT
Wall,' 111' �+J{�i spJT �u Ir+l r, ;;`. �� Cuyahoga Falls, Ohio 44223
WO#: 19030122
ANyU .:n+' LabaraldmG- TEL: (330) 253-8211 FAX.• (330) 253-4489
Website: http://www.settelc.com 14-Mar49
Client: Synagro
Project: Yadldnville WTP
Sample ID MB-R95449 SampType: MBLK TestCode: Sulfide,React Units: mg/L
Client ID: PBW Batch ID: R95449 TestNo: SW9034
Analyte Result PQL SPK value SPK Ref Val %REC
Sulfide, Reactive
Sample ID LCS-R95449
Client ID: LCSW
Analyte
Sulfide. Reactive
SampType: LCS
Batch ID: R95449
Result
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
4470 25.0 4800
BatchID0 R95449
Prep Date:
Analysis Date: 3/5/2019
LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 3/5/2019
%REC LowLimit HighLimit RPD Ref Val
0 93.1 85 115
RunNo: 95449
SegNo: 1987967
%RPD RPDLimit Qual
RunNo: 95449
SegNo: 1987968
%RPD RPDLimit Qual
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
.Analyte detected in the associated Method Blanlc
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below qumA at on limits
M
Manual Integration used to determnie
MC
Value is below Minimum Compound Limit,
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confha nation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 27 of 31
C
Summit Environmental Technologies, Inc. QC SUMMARY R.LPORT
I _ ^ 3310 Win St,
I; 9�dt °'r• r l �z n.,� Cuyahoga Falls, Ohio 44223
rPlrp� :u' i i� ldrli �a_ TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 19030122
kf`ebsite: http://www.settek.com 14-MaP49
Client: Synagro
Project: Yadldnville WTP
BatchID0 R95453
Sample ID 19030127-001AMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 95453
Client ID: BatchQC Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988039
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
9.23 0.485 10.00 0.1837 90.4 81.6 122
Sample ID
19030127-001AMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R95453
Analyte
Cyanide, Reactive
Result
TestCode: Cyanide,Rea Units: mg/Kg
TestNo: SW9014
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 3/5/2019
9%REC LowLimit HighLimit RPD Ref Val
RunNo: 95453
SegNo: 1988040
%RPD RPDLimit Qual
8.74 0.459 10.00 0.1837 85.6 81.6 122 9.226 5.42 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected ui the associated Method Blank I✓ Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery lhnits
Original
Page 28 of 311
r - Summit Environmental Technologies, Inc. �t
- + r I i ' I L'I j 3310 Win St. QC SUMMARY REPORT
1 __. L�
� 1C+iJl 4 �1 i''iL 'a �71 106 r; ; Cuyahoga Falls, Ohio 44223 WO#: 19030122
TEL: (330) 253-8211 FAX: (330) 253-4489
Website: htW:11www.settek.com 14-Mar49
Client, Synagro
Project. Yadkinville WTP
SatchID0 R95453
Sample ID Blank SampType: MBLK TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 95453
Client ID: PBW Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988024
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
Sample ID LCS SampType: LCS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 95453
Client ID: LCSW Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988025
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
9.55 0.490 10.00
0 95.5 85 115
Sample ID RLCheck SampType: RLC TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 95453
Client ID: BatchQC Batch ID: R95453 TestNo: SW9014 Analysis Date: 3/5/2019 SegNo: 1988027
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
0.506 0.495 0.5000
0 101 50 150
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Original
Page 29 0f 311
-. _- - .. -
IPaae 30 of 31
:� � � Sunsznit Environmental Technologies, Inc.
3310 Win St.
het'��I(?�IdP.i��JT�LT��9PPtitt3lt�ti��=a,rtt' CuyalzogaFalls,Ohio44223 ��(❑��jQ(� �O�oQ� �'�(���� �0��
- - .�.rP�Ptri',�r:��' �' ��rfir,�d�t'dtt TEL: (330) 253-8211 FAX.• (330) 253-4489
I�ebsite: http://www.settekcom
Client Name: SYN-NC-27028 Work Order Number: 19030122 RcptNo: 1
Logged by: Christopher Livengood
Completed By: Jesseca E. Westfall
Reviewed By: Jennifer Woolf
3/1/2019 10:15:00 AM ����� a
P, r!,f�*
315/2019 10:11:41 AM 44��"-�����
3/5/2019 10:51:57 AM �{}� ���
_Chain of Custody
1, Is Chain of Custody complete? Yes � No ❑ Not Present ❑
2, How was the sample delivered? UP5
Log In
3, Coolers are present? Yes ❑� No ❑ NA ❑
4, Shipping container/cooler in good condition? Yes 0 No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑�
No. Seal Date: Signed By:
5, Was an attempt made to cool the samples? Yes ❑� No ❑ NA ❑
g. Were all samples received at a temperature of >0° C to 6.0°C Yes � No ❑ NA ❑
7, Sample(s) in proper container(s)? Yes � No ❑
$, Sufficient sample volume for indicated test(s)? Yes � No ❑
g, Are samples (except VOA and ONG) properly preserved? Yes❑ No ❑
1 Q, Was preservative added to boftles? Yes ❑ No❑ i�lA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials 0
12, Were any sample containers received broken? Yes ❑ No
13_ Does paperwork match bottle labels? Yes � No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes❑ No ❑
15. Is it clear what analyses were requested? Yes 0 No ❑
16. Were all holding times able to be met? Yes ❑� No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA
Person Notified:
By Whom:
Regarding:
Client Instructions:
18, Additional remarks:
Date
�I Via: ❑ eMail ❑Phone ❑Fax ❑ In Person
-- -_ ___
COC not received at time of sample receipt. Received pink copy via email 3/5/19
Cooler Information
Cooler No
Temp °G
Condition
Seal Intact
Seal No
Seal Date
Signed B
1
5.2
Good
Not Present
Page 31 of 31
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of YadkinVIRC
WWTPName: Yadkinville WWTP
Monitoring Period: From 01/01/ 2019 To 12/31/19
WQ Permit Number: WQ 00001800
NPDES Number: NC0006190
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (timeRemp) Alt, 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
10
Beta Ray
Compost
Class B:
Alt. (1) Fecal Density X
rying
Gamma Ray
Heat D
Pasteurization
Alt. (2) Process to Signiftcantly Reduce Pathogens
Thhilic
eimop
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Au Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf annlicahle to alternative. nerfnrmed (f acc A nr C'lass Rl emm�lete the fnllnwina mnnitnrina data^
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2xl0tothe 6s'
M I'N
12921
21221
52980
MPN/g
0
Annual
Grab
Sm9221C
Coliform
power per gram
E
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction) X
Option/Alt.
5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
(40-day bench)
Option/Alt. 2
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
(30-day bench)
Option/Alt. 3
Option/Alt. 7
(Drying — Stable)
(Spec.
Option/Alt. 4
02 uptake)
Option/Alt. 8
(Drying —Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector atraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A IN 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation whyyou have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been rnet. I am aware that there are significant penalties for false certification m g fine andimprisonment.". )
Grant Trivette Plant Manager , /
Preper3P Name and } rtle (type orprint) Land A lie Name and Title (if applicable) (type or print)
Signature ofPreparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Analytical Results STA.TESVILLE
ANALYTICAL
Town of Yadkinville
PO Box 816
Yadkinville, NC 27055
Receive Date: 01/24/2019
Reported: 01/25/2019
For:
Comments: Geometric Mean 21,221 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190124A5-01 Fecal Coliforms 1 52980 MPN/g SM92210E-200$ 01/24/2019 WC
190124-15-01 Percent Solids 1 1451 % SM254OB-2011 01/24/2019 WC
190124-15-02 Fecal Coliforms 2 21277 MPN/g SM92210E-2006 01/24/2019 WC
190124-15-02 Percent Solids 2 1041 % SM25408-2011 01/24/2019 WC
190124-15-03 Fecal Coliforms 3 12921 MPN/g SM92210E-2006 01/24/2019 WC
4nn40A 45
n-._�..... Solids
n A �n Q// SM254OB-2011 A nAlnnAf C
1 Vu 146+- 10.03 Perce It Solids 3 1 • 1 0 JO l� 1/G'+14U 1:7 WV
190124-15-04 Fecal Coliforms 4 30120 MPN/g SM92210E-2006 01/24/2019 WC
190124-15-04 Percent Solids 4 1,66 % SM2540B-2011 01/24/2019 WC
190124-15-05 Fecal Coliforms 5 18405 MPN/g SM92210E-2006 01/24/2019 WC
190124-15-05 Percent Solids 5 1.63 % SM2540B-2011 01/24/2019 WC
190124-15-06 Fecal Coliforms 6 15132 MPN/a SMMlCE-2006 01/24/2019 WC
190124-15-06 Percent Solids 6 1,52 % SM254OB-2011 01/24/2019 WC
190124-15-07 Fecal Coliforms 7 15862 MPN/g SM92210E-2006 01/24/2019 WC
190124-15-07 Percent Solids 7 1,45 % SM25408-2011 01/24/2019 WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 •Statesville, NC 28687 •704/872/4697
Page 1 of 4
vetmjL- 96 TOTA =$� �6.1�' i
S -2W
GalCulaied EW.
Q v e,�
DI \L�;/
r
USA %imi t iAL ANE)-FINAL AVERAGES OF YOUR % VOLATILE FRACTION TO CALCULATE THE
PERCENT REDUCTION (ME. THE VAN tCLEECK: FORMULA)
l ae K i xtction: If" :%. vol. Vic. - Final %. Vol, frac. X 100 = % u n
tnffi* % VOL `irac. - ((rirflal % vial. €rac x Final 9b vol. €rac.)
minus t LP 7 x 1.00 -L64J I f6
* D0 Mul 0at1on inside [( )) before you subtract on bottom of equaWn.
s
r ` J
�•�Z.ZU
{r T
Agricultural Lime Application Log
Year: 2019
Project:
Yadkinville WWTP
New
(state -county -site -field)
Soil 1Lime
pH
Requirement
(from soil analysis)
Tons/Acre
Applied(CCE Eq.)
Date Applied
YK-33-1
5.9
O.OT/Ac.
YK-33-1
6.9
0.OT/Ac.
YK-33-3
6.3
0.0 T/AC
YK-35-2
5.8
5.OT/Ac.
.75tons/ac
YK-2M
6.6
O.OT/Ac.
*Lime will
be applied
when
conditions
improve.
NCDA&CS Av )mic Division
Phone: (919) 733-2655
Website: wwv igr.gov/agronomi/
Report No. '20-SL004618
lot
Client: City of Yadkinville Advisor: Alex Fox
? %`��1� . " Predictive 213 Van Buren St
,r'x�" ¢' Synagro
It 1 y:=ll Yadkinville, NC 27055 284 Boger Rd
�` r! .`�'�I S o i I Report Mehlich-3 Extraction Mocksville, NC 27028
Sampled County: Yadkin
ieyZ
III Y°.
-__� Links to Helpful Information
Client ID: 476642 Advisor ID: 501947
Sampled: 09/11/2019 Received: 09/12/2019 completed: 09/21/2019 Farm: NC-YK-29
Sample ID: 01 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 110 40 0 0 pH$ 0 0 0 Note: 12 Note:
2 - 0.0
Test Results [units - WN in g1cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P4 K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.27 0.99 7.0 92 0.6 6.6 13 48 55 34 38 663 406 182 1 182 98 0.1 1
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
to Steve Troxler, Commissioner of Agriculture
i jn.l^.glir'I'.�,�y;lupi(u11'ia514.�1u
NCDA&CS Agronomic Division Phone: (919) 733=2655 Website: www.neagr.gov/agronomi/
Report No. FY20-SL004618
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report
Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. M and P-I values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-AI2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
M-O
manganese index
soil class
mineral -organic
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm,
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft, If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncapr.gov/agronomi/obpart4.htrntsfind information that
P-I
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS4
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-I
zinc index
remaining 16 [P-I, M, Ca%, Mg%, Mrid, Mn-All, Mn-AI2, Znd, Zn-Al, Cud, S.-I, SS -I, Na, ESP, SSd, NO3-1\1 (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.goy/agronomi/uyrst.htm
Page 1 of 1
Report Number: 19-326-0587
Account Number: 46431
Send To: Synagro Central LLC
Marshal Puryear
284 Boger Rd
Mocksville NC 27028
Alaypoint
ANALYTICAL
"Every acre... Every dear. "rM
SOIL ANALYSIS REPORT
Date Received: 11/22/2019 Date Of Analysis: 11/25/2019 Date Of Report: 11/25/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax 804-271-6446
www.waypointanalytical.com
Grower: James Hobson
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
NC =North Carolina Fertility Index Value
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Rate
Soil
Class
Ibs/A
M3
pp m Rate
pp m Rate
pp m Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
p H
Buffer
Index
H
meq/100g
meg1100g
41K-33-3
16364
3A
M
105
37 M
NC = 31
70 M
NC = 36
140 H
572 M
10 VL
6.3
0.5
4.7
MIN
Percent
Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample
Field ID ID
K
Mg
%
Fca
Na
%
H
%
NO3 N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
4K-33-3
3.8
24.8
60.9
0.9
10.6
18 M
NC=37
7.0 H
NC=175.0
18 M
NC=113
148 VH
1.6 H
NC=80.0
0.3 VL
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/10og
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
This report applies to sample(s) tested. Samples are retained a
maximum of thirty days after testing.
Analysis prepared by: WaypointAnalytical Virginia, Inc.
Pauric McGroary
NCDA&CS Ag �mic Division Phone: (919) 733-2655
Website: www
gr.gov/agronomi/
Report No.
'20-SL004632
-r, a r• ,.
a Uj
Client:
James Hobson
Advisor:
Alex Fox
Predictive
3541 Apperson Rd
Synagro
�_s u�CF44 'a'`4
East Bend, NC 27018
284 Boger Rd
lu 1.'—'.FIxill:
y" Soil
Report
Mehlich-3
Extraction
Mocksville, NC 27028
Sampled County: Yadkin
Links to Helpful Information
i
Client ID: 493738
Advisor
ID: 501947
Sampled: 09/10/2019 Received: 09/12/2019 Completed: 09/21/2019
Farm: NC-YK-33
Sample ID: 01
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M
0.0
120-200 0
70
0 0 0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN
in g/cm3; CEC and Na in meq/100
cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH Pool
K-1
Ca% Mg%
S-I
Mn-I
Mn-All Mn-AI2 Zn-1
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
0.46 0.95 8.0
82 1 A 5.9 77
34
61 19
44
147
105 355
355
217
0.1 1
Sample ID: 02
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, M
0.0
120-200 0
70
0 0 pH$
0
0
0
Note: 12 Note:
2 -
0.0
Test Results [units - WN
in g/cm3; CEC and Na in meq/100
cm3; NO3-N
in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH P4
K-I
Ca% Mg%
S-I
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I
Na ESP
SS -I NO3-N
0.46 1.06 10.7
94 0.6 6.9 148
34
64 29
42
219
135 890
890
248
0.1 1
.11 '' a
11.111;KS i !rtl".r, I' Ia1;u:I r.,4iCh)fi�itilla�ii
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of A.priculture
NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/
James Hobson
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For noAill or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients, In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Report No. FY20-SL004632
Page 2 of 2
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K2O potash
Mg % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn-availability index for crop 1
Mn-A
Mn-I
12 Mn-availability index for crop 2
manganese index
M-O mineral -organic soil class
N nitrogen
Na sodium
NOs-N
O RG
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmf ff,9f nd information that P-1
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P2O5
S-I
Test Results � SS -I
WN
Zn-AI
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I
remaining 16 [P-I, K-I, Ca %, Mg%, Mn-I, Mn-A11, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, Sod, Na, ESP, SS -I, NU3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index
Page 1 of 1
Report No: 19-326-0585
Account No: 46507
Advisor: Synagro Central LLC/ Yadkinville
Mary Brewer
284 Boger Road
Mocksville NC 27028
Naypolnt.h,
ANALYTICAL
Client: Roger Davis
Yadkinville WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804443-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Farm:4K-35
Date Received: 11/22/2019
Date of Report: 12/02/2019
Lab No Field ID Sample ID Soil Class HM% W/V pH AC P-1 K I S-I Mn-1 Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N
16360 2 MIN 5.8 1.0 9 27 52 250 123 123 25 5.2 80 44 33 0.9 0
ICrop Recommendations; Rec Uom Lime (M/acre) N P205 K2 S Mn Mn-Al Zn Cu B Mg Last Crop I
1- Pasture lb/acre 0.5 50 86 120 0 0 170 0 0 0.5 0
COmmenfi:
Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
ni.,.+ti r��„r.,� nt„���,,,, .,f+nra+o� n�r+„ �orf�f��+�,,,, tns� anaivcic a�� fortili+�� rannmmanriatinnc shown nn this ran�rt ara nerfnrmed in accordance within NCDA guidelines. Analysis prepared bv: Wavpoint Analytical Virginia, Inc.