WQ0018525_Residual Annual Report 2019_20200226

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/26/2020
Received:*
Project Number* WQ0018525
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Martin Mabe
Email Address*
[e-mail]
Project Information
.........................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0018525
Applicant\Permittee * Steven M. Barnes
Phone Number*
336-312-1396
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Facility Name * Barnes Environmental Waste and Hauling, Inc.
Please provide comments/notes on your current submittal below.
One hard copy is being mailed to NCDEQ today per the regulations by UPS.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
Barnes Environmental 2019 Annual Report
20.05MB
WQ0018525. pdf
Upload only 1 RJF docurrent. Nlaltiple docurrents must be corrbined into one RJF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/25/2020

2019 ANNUAL REPORT
LAND APPLICATION PROGRAM
BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
PERMIT #WQ0018525
WMSS Project No. 15-02 Ph: 01
Prepared for:
Barnes Environmental Waste and Hauling, Inc.
Post Office Box 654
Newport, North Carolina 28570
Compiled by:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
February 2020

Willcox&mate
SOIL SOLUTIONS
February 25, 2020
NCDEQ-DWR Non -Discharge Compliance Unit
512 North Salisbury Street
9th Floor, Office# 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Compliance Unit
Reference: 2019 ANNUAL REPORT FOR W00018525
Barnes Environmental Waste and Hauling, Inc.
WMSS, Inc. Project No. 15-02 Ph: 01
Non -Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Barnes Environmental
Waste and Hauling, Inc. (Bames Environmental Waste). WMSS compiled this report using
data gathered during the compliance year by Barnes Environmental Waste.
If there is any further information required or questions regarding this land application
program please do not hesitate to contact Mr. Steve Barnes, with Barnes Environmental
Waste 252-241-5014 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosure(s)
cc Barnes Environmental Waste
WMSS Projects\2015\15.02 Barnes Ernironmental\2019 Annual Report\2019 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC /7231 B Summerfield Road /Summerfield, NC 27358 / Rob336.339.9128 or
Martin 336.312.1396 /www.willcoxmabesoll.com

TABLE OF CONTENTS
SECTION NO. TITLE
Certification Form
II Residuals Analyses & Pathogen and Vector Attraction
III Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

+\L�v,tiil 1JC11\LH 1L11.K11V1\l.L`1\111•ll.?111V1\V%JAMYl
WQPermittt: WQ0018525 County: Carteret Year: 2019
Facility Name (as shown on permit): Barnes Environmental Waste and Hauling, Inc.
Land Application Operator: Steven M. Barnes Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
O Yes ❑ No - If No, sldp Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Annlvenfinn fi"mm.vm-
Total number of application fields in thepermit;
6
Total number of fields utilized for land application during the yearl
5
Total amount of dry tons applied during the year for all a lication sites: 1
29.49
Total number of acres utilized for land application during the yearl
T _a
24.7
v.. +• - ea..uun, a,vntnusuce Otatement•
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality, 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective.
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable. to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities),
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Steven M. Barnes, President
Permittee Name and Title (type or print)
r
.�%,211Q020
Signature of Permittbeee Date
ignature of Preparer* Date Signature of Land Applier
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DEN FORM ACF (12/2006)

RESIDUAL ANALYSES REPORTS AND
PATHOGEN AND VECTOR ATTRACTION REDUCTION

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Artad, M loan to the cortaspondng labcmlary.r*W&
Please note Out your pamill me, conWn adddonal ,onunclem to be anwSed Nan mete required to be summmzed an We rams.
Permit Number
WOOOt8525
Facility Name
Bames Envronmental
NPDES #
I See Below
W AF P Name
I See Below
RESIDUAL ANALYSIS DATA
Laboratory III Envimnmenl l.lnc
21 Environmental Chemists, Inc
3
NPOES#
W00004059 WQ0013676
VI-15-17
VI-0&18
WOOD03044 i VWS-13
DEH - Local
V142.18
W00019331
WOOD24756
VJvylP Name
AIIanOc Station I Beacons Reach
CC Sass
Hamplon Suites
li Duneseape ElghVIJ2 Marina
IOngsbridge It
McGinnis PolM
NCAWarium
The Grove
Composted l Grab
01/17/19 011US119
04/16/19
D3/19fl9
01129 S 12/23119
01102/19
1 01/15/19
0117119
04125119
Pere+nl sow.
0.88 1.69
240
129
1.230-34
099
1 1.91
0.71 1
0.73
0M
Arsenic
250
3.30
8.63
2-50
2.50
6.10
2.50
3.90
2.50
3.70
Cadmium
0.50
1.10.
8.63
0.50
0.72
1.00
2.50
0.82
6.20
0.62
Copper
639.00
1,811.00
69200
1.009.00
62&00
1,037.00
405.00
2,016.00
206.00
88.00
Lead
17.00
23.00
8.63
4,80
13.00
23,00
39.00
37.00
24.00
520
Meraay
0.17
023
0:96
0.13
0.16
1.30
0.38
0.28
OAO
0.15
Molybdenum
5.00
6.00
8,63
5.00
5.00
6.00
8.00
5.00
5.00
5.00
Nickel
11.00
17.00
8.63
8.00
8.00
8.00
12.00
11.00
11.00
6,00
Selenium
5.00
5.00
8.63
5.00
5.00
5A0
5.00
5.00
5.00
5.00
Zinc
1,116.00
1.345.00
583.00
474.00
837.00
2.125.00
6,620.00
1.198.00
393.00
556.00
TnN
47.780.00
41,460.OD
76,700.00
61.980.00
75.870.00
44,540.00
51,310.00
91.770.00
77.680.00
56.120.00
AmmoniaNibo9en
287.fi0
87720
4,480.00
2,505.00
258.70
41.94
610.50
1,354.00
-86.92
1,400.00
Kdmte4litrogen
6.99
3.H6
195,00
6.94
5.92
1,957.00
1,806.00
115.eD
57.95
6.00
Total Phosphorus 1
28.130.00
16.590.00 1
23.300.00
9.692-00
1 15.890.00
1 17240.00
26,920.00
1 60210.00
51,350.00
114,950.00
RESIDUAL ANALYSIS DATA
NPOES0
WQ0D1a420
W00002128
V1-16-13
W00000224
WGODD-a437
W00000]65
W00013027 VI-09-17
W000011R1
W00p18992
WhTP Name
Ocean Club
Pebble Beech
Pine Knoll Toynos
Potnt Emerald Villas
Queerie Court
Sands We
I Sea Isle PlantationI Sea Spray
Sound Of The Sea
SoulhwindS Caldos
Compo lbxJlGrsb
01102f19
I VIWVI9
1 OW05119
1 01110/19
1 04/15/19
1 01129/19
07102119 03107fl9
'01107119
04a5f79
Perry ISapds
0.63
0.59
1 1.69
1 1117
1 121
1 2.92
029 2.44
1.65
1.15
PARAMETERS (m9/k9.
dryweight)
Arsenic
330
250
3.30
250
16AO
2.50
2.50
2.60
260
250
Cadmium
0.74
0.99
IAA
120
16.40
0.85
14O
0.78
120
0.56
Copper
312.00
202-00
751.00
S15.00
134.00
301.00
135.00
870.OD
758.00
757A0
Lead
11.00
1200
17.00
93.00
16.40
10.00
35.00
8.50
49.00
12.00
Mercury
0.12.
0.32
021
0.43
1.63
023
OAS
0.16
0.06
025
molybdenum
5.00
5.00
5.00
5.00
16.40
5.00
5.00
5.00
500
5.00
Nickel
.8A0
10.00
12-00
12.00
16.40
11.00
10.00
12.00
11.00
9.00
Selenium
5.00
5.00
5.00
5.00
16.40
5.00
5.00
5.00
5.00
5.00
Zinc
1,524.00
1.065.00
2415.00
2,817.00
1.110.00
1.087.00
731.00
843.00
1,67200
1,028.00
TM
$3,780.00
65,370.00
23,330.00
63,130.00
80.200.00
85,600.00
46.440.00
89.920.00
49,950.00
56,200.00
ANm7e
360.60
205.70
75550
8.12.00
178390
,1Z330.00
89.62
1.984110
95&00
1,2598000
tnea-N-Ni8f,
13.87
7.73
3.99
728.70
218.00
5
8on
.3
5.98
25
Total Phosphorus
38,91D.00
15,950.00
1 13,900.00
14,950.00
14,500.00
1 17,890.0D
14,760.00
20,910.00
1T:;bu.00
15.500.00
(SIGNATURE OF PREPARER) DATE
I certify; under penally of law, that this document was prepared under my direction or supervision in aaordance WM a system designed
to assurelhal qualified personnel_pmpedy gathered and evaluated lheinformation sutimided. 1 amawarerethat thereare signito:am
penaJflw for subm0ling false Infonna8an, including the possibifdyoffines and imprisaumenitar knnv7mg vtoletiads.
Page 1

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Anadi Nis form 1. the eoimspmwei, labo2loryapelysh.
Please noio Nat Yaw pemut MY =Wl eddua2tpvamelers to beanalwed Nan Nose mgvfmG tv De nmmadmd on Nis corm.
Penult Number
1 Wo0018525
Facility Name
Sames Envimnmental
NPDES#
See Below
wwrp Nam,
I See Below
RESIDUALANALYSIS DATA
Laboratory 1 Envimnment 1, In4
2 Eilvimnmental Chemists. Ine:
3
NPDES#
VF12-17
VI-20-1S
VYNrrP Name
Summer Winds
Whaler lnn
Compnsrted/G2D1
01/17/19
1 02121119
Percent Solids
1 1.62
0.60
PARAMETERS (malkc div wei ht
Arsenic
2.50
250
Cadmium
0.67
0.62
Copper
53200
570.00
Lead
15.00
11.00
Mermry
DAG
0.15
Molybdenum
5.00
6.00
Nickel
11.00
6.00
Selenium
5.00
$,00
Zinc
1,954.00
901.00
TI(N
132,100.00
23,890.00
Anunvn Nilmgan
986.20
125,60
h8f2te'Ni m m
891
124.60
Tolal Phasptmms
36,260.00
12,940.00
x ✓J M _LJy-L----- rir b
(SIGNATURE OF PREPARER) DATE '
I"do. under penahy of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that quafi6ed personnel pmpedy gathered and evaluated the information submitted. I am award that them am significant
penalties for submitting false information, inducing the possltTdy of fines and Imprisonment far knowing violations.
Page 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2019
Permit No. W00018525
Atlantic Station 0.88 % Solids
1201.nH !taken frnm lime ctahilizatinn event!
Parameter
%
Mg/Kg Dry Weight
(% x 10,0001
Pounds/Dry Ton
x 0.002)
Nitrogen (TKN)
0.723
47,780.000
__(Mg/Kg
95.560
Phosphorus
0.263
28,130.000
56.260
Potassium
0.449
3,844.000
7.688
PAN (injected)*
0.254
2,544.890
5.090
PAN surface)*
0.228
2,281.390
4.563
Ammonia Nitrogen
0.053
287.600
0.575
Calcium
3.558
36,702.000
73.404
Calcium Carbonate E .
---
--
Magnesium
---
2,605.000
5.210
Sodium
---
14,320.000
28.640
Sulfur
---
---
Nitrate N / Nitrite N
---
6.990
0.014
Barium
---
---
—
Chloride
--
---
---
Iron
---
Aluminum
---
3,067.00
6.134
Arsenic
--
2.50
0.005
Cadmium
---
0.50
0.001
Chromium
—
13,000
---
Copper
---
639.00
1.278
Lead
---
17.00
0.034
Mercury
---
0.17
0.000
Molybdenum
--
5,00
0.010
Nickel
--
11.00
0.022
Selenium
—
5.00
0.010
Zinc
—
1,116,00
2.232
Environment 1, Incorporated 108A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) +Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
1.82
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

ATLANTIC STATION (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Code
Aluminum, (dry wt, basis), mg/kg
3067
01/29/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
01/29/19
MTM
3113E-04
Calcium (dry wt. basis), mg/kg
36702
01129119
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
<0,5
01/30/19
MTM
3113B-04
Copper (dry wt, basis), mg/kg
639
01/29/19
LFJ
EPA200.7
Chromium, T,(dry wt. basis),mg/kg
13
01/29/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
17
01/31/19
MTM
3113B-04
Magnesium (dry wt. basis), mgllig
2605
01/29/19
LFJ
EPA200.1
Mercury (dry wt. basis), mg/kg
0.17
02/07/19
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
11
01/29/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
3844
01/29/19
LFJ
EPA200.7
Selenium (dry wt, basis), mg/kg
<5.0
01/31/19
MTM
3113B-04
Sodium (dry wt. basis), mg/kg
14320
01/29/19
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1116
01/29/19
LFJ
EPA200.7
Total Solids, %
0.88
01/23/19
IMS
2540G-11
TEN (dry wt.), mg/kg
c 47780
0U25J19
DTL
351.2 112-93
Ammonia Nitrogen (dry wt ),mg/kg
c 287.6
01i24f19
CLO
:3_=4.1 R2-93
Phosphorus, T. (dry -.}it.), mgIg
Nttmte-Nitrite (dry wt.), mg/kg
,c,
Plant Available Nitrogen, mg/kg
Y91•i8
01128J7-9
SEJ
Molybdenum (dry wL basis), mg/kg <5.0 01129/19.JLFJ EPA200.7
e vv-..rtified data
ID#: 108 A
DATE COLLECTED: 01/17/19
DATE REPORTED : 02/15/19
REVIEWED BY:
DWa does not offer coo. -aqueous certification for this analytical procedure.
sw

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 8, 2019
Permit No. W 00018525
Beacons Reach 1.69 %Solids
6.3 pH
Parameter
%
Mg/K Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
4.146
41,460.000
82.920
Phosphorus
1.659
16,590.000
33.180
Potassium
0.241
2,406.000
4.812
PAN (injected)*
1.306
13,055.920
26.112
PAN (surface)*
1.262
12,617.320
25.235
Ammonia Nitrogen
0.088
877.200
1.754
Calcium
3.710
37,098.000
74.196
Calcium Carbonate E .
---
___
Magnesium
-
3,113.000
6.226
Sodium
-
8,414.000
16.828
Sulfur
-
Nitrate N / Nitrite N
---
3.880
0.008
Barium
---
-__
Chloride
---
---
---
Iron
---
Aluminum
---
3,172.00
6.344
Arsenic
3.30
0.007
Cadmium
---
1.100
0.002
Chromium
---
14.000
Copper
---
1,811.00
3.622
Lead
---
23.00
0.046
Mercury
---
0.23
0.000
Molybdenum
---
6.00
0.012
Nickel
---
17.00
0.034
Selenium
---
5.00
0.010
Zinc
---
1,345.00
2.690
Environment 1 H 554A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = %PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = %° PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
1.46
Ceiling Concen.
(M /K )
75
85
4,300
840
57
75
420
100
7,500

C MWOMEcPfl� Flo �IMWTPOO(ld
BEACON'S REACH I/POND (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting)
6.3
01/08/19
EDS
4500HB-11
Aluminum, (dry wt. basis), mg/kg
3172
01/17/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
3.3
01/22/19
MTM
3113M4
Calcium (dry wt. basis), mg/kg
37098
01/17/19
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.1
01/17/19
MTM
311311-04
Copper (dry wt. basis), mg/kg
1811
01/17/19
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mglkg
14
01/17/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
23
OV18119
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
3113
01/17/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.23
01/18/19
MTM
FPA747119
Nickel (dry wt. basis), mg/kg
17
01/17/19
LFJ
EPA200.7
Potassium (dry wt, basis), mg/kg
2406
01/17/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
01/28/19
MTM
3113B-04
Sodium (dry wt. basis), mg/kg
8414
01/17/19
LFJ
EPA200.7
Zinc (dry wt, basis), mg/kg
1345
011I7/19
LFJ
EPA200.7
Total Solids, %
1.69
01/09/19
ICDS
2540GI1
TKN (dry wt.), mg/kg
c 41460
01/18/19
TLH
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 877.2
01/14/19
TLH
350.1 112-93
Phosphorus, T. (dry wt.), mg/kg
c 16590
01/18/19
BLD
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 3.88
01/15/19
DTL
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
6
01/17/19
LFJ
EPA200.7
ID#: 554 A
DATE COLLECTED: 01/08/19
DATE REPORTED : 01/30/19
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 16, 2019
Permit No. W00018525
CC Sass 2.40 % Solids
6.94 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
7.670
76,700.000
153.400
Phosphorus
2.330
23,300.000
46.600
Potassium
0.862
8,620.000
17.240
PAN injected)*
2.634
26,341.000
52.682
PAN (surface)*
2.410
24,101.000
48.202
Ammonia Nitrogen
0.448
4,480.000
8.960
Calcium
1.530
15,300,000
30.600
Calcium Carbonate E .
---
---
Magnesium
---
5,960,000
11.920
Sodium
---
10,400.000
20.800
Sulfur
___
___
_
Nitrate N / Nitrite N
---
195.000
0.390
Barium
---
---
--
SAR
Chloride
___
-_
2.79
Iron
---
---
---
Ceiling Concen.
Aluminum
---
2,050.00
4.100
(Mg/Kg)
Arsenic
---
8.63
0.017
75
Cadmium
---
8.63
0.017
85
Chromium
57.900
0.116
--
Copper
---
692.00
1.384
4,300
Lead
---
8.63
0.017
840
Mercury
0.958
0.002
57
Molybdenum
---
8.63
0.017
75
Nickel
---
8.63
0.017
420
Selenium
---
8.63
0.017
100
Zinc
--
583.00
1.166
7,500
Envimuttem # 2019-06102
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

Fortin Contract Services
Date of Report: May 06, 2019
Post Office Box 4188
Customer PO #:
Emerald Isle NC 28694
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2019-06102
Project ID: CCSASS Sludge
Lab ID Sample ID:
Collect Daterl Ime Matrix Sampled by
19-15376 Site: Annual Sludge
4116/2019
9:45 AM Solid/Sludge Kevin Stanley
Test
Method
Results Date
Analyzed
pH
SW 646 Method 00450
6.94 units
04/24/2019
Sludge Residuals
Aluminum
EPA200.7
2050mg/kg
04/2212019
Arsenic
EPA200.7
<8,63mglkg
04/23/2019
Cadmium
EPA200.7
<8.63mglkg
04/23/2019
Calcium
EPA200.7
15300mg/kg
04122/2019
Chromium
EPA200.7
57.9mg/kg
04122/2019
Copper
EPA200.7
692mglkg
04/2212019
Lead
EPA200.7
<8.63mg/kg
04/25/2019
Magnesium
EPA200.7
6960mg/kg
04/22/2019
Molybdenum
EPA200,7
<8.63mg/kg
04/23/2019
Nickel
EPA 200,7
<8.63 mg/kg
04/23/2019
Potassium
EPA200.7
8620mg/kg
04122/2019
Selenium ..
. EPA 20/1.7
.__,... .. &,. i
W23JLD49
Sodium
EPA200.7
10400mglkg
04iM019
Zinc
EPA200.7
583mg/kg
0412212019
Nitrate+Nitrite-Nitrogen
EPA363.2
195mg/kg
051022019
Total Solids (%)
SM 2540 B
2.40 %
04/17/2019
Ammonia Nitrogen
SM 4500 NH3 C
4480 mg/kg
04/29/2019
Total Kjeldahl Nitrogen (TKN)
SM 45000rg B
76700 mg/kg
04/2912019
Total Phosphorus
SM 4500 P F
23300 mg/kg
04/30/2019
Mercury
SW0467471B
<0.958mglkg
04/22/2019
Comment: Sludge residuals, except pH, reported on a dry
weight basis. pH reported on an as received basis,
Reviewed by: R()jA DL
OWfm
E-MAILED MAY 07 201R
Report N:: 2010-06102
Page 1 of 1

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 19, 2019
Permit No. WQ0018525
Hampton Suites 1.29 %Solids
Parameter
%
I Mg(l g Dry Weight
(% x 10,000)
I Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
6.198
61,980.000
123.965
Phosphorus
0.969
9,692.000
19.384
Potassium
0.407
4,067.000
8.134
PAN (injected)*
2.035
20,354.440
40.709
PAN surface)*
1.910
19,101.940
38.204
Ammonia Nitrogen
0.251
2,505.000
5.010
Calcium
3.174
31,744.000
63,488
Calcium Carbonate E .
--
---
---
Magnesium
2,134.000
4.268
Sodium
29,635.000
59.270
Sulfur
---
---
—
Nitrate N / Nitrite N
---
6.940
0.014
Barium
---
Chloride
---
--
Iron
---
--
--
Aluminum
---
1113.000
2.226
Arsenic
---
2.50
0.005
Cadmium
---
0.50
0.001
Chromium
---
4.000
---
Copper
—
1,009.00
2.018
Lead
--
4.80
0.010
Mercury
---
0.13
0.000
Molybdenum
--
5.00
0.010
Nickel
--
8.00
0.016
Selenium
---
5.00
0.010
Zinc
---
474.00
0.948
Environment 1, Incorporated 551 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SA R
4.93
Ceiling Concen.
(M/K)
75
85
4,300
840
57
75
420
100
7,500

En1Y/,ummuC°�611 � t hc� po @T@I(Pd
HAMPTON INN (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Code
PH (not to be used for reporting)
6.9
03/19/19
TCW
4500HB-11
Aluminum, (dry wt. basis), mg/kg
1113
04/04/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
04/04/19
MTM
311313-04
Calcium (dry wt. basis), mg/kg
31744
04/04/19
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
<0.5
04/08/19
MTM
3113B.04
Copper (dry wt. basis), mg/kg
1009
04/04119
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
4
04/04/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
4.8
04/05/19
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
2134
04/04/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.13
04/08/19
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
8
04/04/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/lig
4067
04/04/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
04/03/19
MTM
3113B-04
Sodium (dry wt. basis), mg/kg
29635
04/18/19
AKS
3111B.11
Zinc (dry wt. basis), mg/kg
474
04/04/19
LFJ
EPA200.7
Total Solids, %
1.29
03/19/19
ICDS
254OG-11
TKN (dry wt.), mg/kg
c 61980
03/26/19
CLO
351.2 112-93
Ammonia Nitrogen (dry wQ,mg/kg
c 2505
04/01/19
CLO
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 9692
03/26/19
DTL
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 6.94
04/02/19
DTL
353.2 R2.93
Molybdenum (dry wt, basis), mg/kg
<5.0
04/04/19
LFJ
EPA200.7
ID#: 551 A
DATE COLLECTED: 03/19/19
DATE REPORTED : 04/22/19
REVIEWED BY:
c Wnoertified data. DWA doe. not offer non-aguecue cortification for thie analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 29, 2019
Permit No. WQ0018525
_Dunescape 1.23 %Solids
7.6 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Too
(Mg/Kg x 0.002)
Nitrogen (TKN)
7.587
75,870.000
151.740
Phosphorus
1.589
15,890.000
31.780
Potassium
0.278
2,777.000
5.554
PAN (injected)*
2.295
22,948.010
45.896
PAN (surface)*
2.282
22,818.660
45.637
Ammonia Nitrogen
0.026
258.700
0.517
Calcium
4.370
43,704.000
87.408
Calcium Carbonate E .
—
---
Magnesium
--
6,774.000
13.548
Sodium
- -
7,414.000
14.828
Sulfur
---
___
_
Nitrate N / Nitrite N
---
5.920
0.012
Barium
---
---
---
SAR
Chloride
---
---
0.96
Iron
---
---
---
Ceiling Concert.
Aluminum
---
2,518.00
5.036
(Mg/Kg)
Arsenic
---
2.50
0.005
75
Cadmium
---
0.72
0.001
85
Chromium
---
10.000
---
--
Copper
---
623.00
1.246
4,300
Lead
---
13.00
0.026
840
Mercury
---
0.16
0.000
57
Molybdenum
5.00
0.010
75
Nickel
8.00
0,016
420
Selenium
---
5.00
0.010
100
Zinc
---
837.00
1.674
7,500
Environment 14 556 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Emwou ow(W Flo hmmormho
DVNESCAPE (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Code
PH (not to be used for reporting)
7.6
01/29/19
TCW
4500HB-11
Aluminum, (dry wt. basis), mglkg
2518
02/11/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/19/19
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
43704
02/11/19
LFJ
EPA200.7
Cadmium (dry Wt, basis), mg/kg
0.72
02/15/19
MTM
311311-04
Copper (dry wt. basis), mg/kg
623
02/11/19
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
10
02/11/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
13
02/14/19
MTM
311311-04
Magnesium (dry wt. basis), mg/kg
6774
02/11/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.16
02/07/19
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
8
02/11/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
4086
02/11/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
O2/20/19
MTM
3113B-04
Sodium (dry wt. basis), mg/kg
7414
02/22/19
AILS
3111B-11
Zinc (dry wt. basis), mg/kg
837
02/11/19
LFJ
EPA200.7
Total Solids, %
1.23
01/30/19
IOS
2540G-11
TIN (dry wt.), mg/kg
c 75870
02/07/19
DTL\
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg1k9
c 258.7
02/04/19
BLD
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 15890
02/07/19
DTL
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 5.92
02/01/19
BLD
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
<5.0
02/11/19
LFJ
EPA200.7
ID#: 556 A
DATE COLLECTED: 01/29/19
DATE REPORTED : 02/26/19
REVIEWED BY:
c Uncertified data. DWR does not offer non-aquecuo certification for thle analytical pronedura.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 23, 2019
Eight 1/2 Marina
N / Nitrite N
Permit No. WQ0018525
0.34 % Solids
12.16 pH (taken from
%
Mg/Kg Dry
(% x 10,0
2.438
44
0.244
li
0.349
3
0.934
S
0.929
5
0.010
41.940
58,647.000
17,128,000
1,957.000
5,384.00
5.10
1.00
22.000
1,037.00
23.00
1.30
6.00
8.00
5.00
2,125.00
Environment 1 M 196A
Ton
102E
89.080
34.480
7.106
0.084
117.294
7,884
34.256
3.914
10.768
0.010
0.002
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) +Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
0.046
0.003
0.012
0.016
0.010
4.250
SAR
1.08
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

cad
ID#: 196 A
EIGHT & ONE-HALF MARINA(FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES DATE COLLECTED: 12/23/19
P.O. BOX 4188 DATE REPORTED : O1/22/20
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg4cg
Arsenic (dry wt. basis), mg4cg
Calcium (dry wt, basis), mg/kg
Cadmium (dry wt, basis), mg/kg
Copper (dry wt. basis), mg4cg
Chromium, T,(dry wt. basis),mg4cg
Lead (dry weight basis), mg4cg
Magnesium (dry wt. basis), mg4cg
Mercury (dry wt. basis), mg4cg
Nickel (dry wt. basis), mg/lig
Potassium (dry wt. basis), mg/kg
Selenium (dry wt, basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt, basis), mg/kg
Total Solids, %
TKN (dry wt,), mg/kg
Ammonia Nitrogen (dry wQ,mg1kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg4cg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg4cg
Sludge Analysis Method
Sample Date Analyst Code
5384 01/09/20 LFJ EPA200.7
5.1 01/08/20 MTM 3113B-04
58647 01/08/20 LFJ EPA200.7
1.0 01/08/20 MTM 3113B-04
1037 01/08/20 LFJ EPA200,7
22 01/08/20 LFJ EPA200.7
23 01/07/20 MTM 311313-04
3942 01/08/20 LFJ EPA200.7
1.3 01/16/20 MTM EPA7471B
8 01/08/20 LFJ EPA200.7
3553 01/08/20 LFJ EPA200.7
<5A 01/09/20 MTM 3113B-04
17128 01/08/20 LFJ EPA200.7
2125 01/08/20 LFJ EPA200.7
0.34 12/30/19 KDS 2540G-11
c 44540 12/27/19 AKS 351.2 112-93
c 41.94 12/26/19 AKS 350.1 R2-93
c 17240 12/27/19 TLH 365.4.74
c 1957 12/26/19 DTL 353.2 R2-93
19777 12/27/19 SEJ
6 01/09/20 LFJ EPA200.7
REVIEWED BY _A-0
Us
o Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2019
Permit No. W00018525
Kinesbridee II 0.99 % Solids
6.10 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
5.131
51,310.000
102.620
Phosphorus
2.692
26,920.000
53.840
Potassium
0.213
2,129.000
4.258
PAN injected)*
1..763
17,626.350
35.253
PAN (surface)*
1.732
17,321.100
34.642
Ammonia Nitrogen
0.061
610.500
1.221
Calcium
2.996
29,963.000
59.926
Calcium Carbonate E .
---
---
Magnesium
---
1,627.000
3.254
Sodium
---
7,054.000
14.108
Sulfur
___
___
Nitrate N / Nitrite N
---
1,806.000
3.612
Barium
---
---
Chloride
---
___
Iron
---
---
__-
Aluminum
---
11484.000
22.968
Arsenic
--
2.50
0.005
Cadmium
---
2.60
0.005
Chromium
---
27.000
Copper
---
405.00
0.810
Lead
---
39.00
0.078
Mercury
---
0.38
0.001
Molybdenum,
---
8.00
0.016
Nickel
---
12,00
0.024
Selenium
---
5.00
0.010
Zinc
---
6,620.00
13.240
Environment I, Incorporated 216
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
1.07
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

iJC�.S Aa�"�V LJ� ��V o41IVO1J WV'��
XINGSBRIDGE (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE [NC 28594
PARAMETERS
PH, units
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt, basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TEN (dry wt.), mg/kg
Ammonia Nitrogen (dry wtJ,mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
Wa¢epygear lD, .aa
PHONE [phone]
FAX [phone]
ID#: 216
DATE COLLECTED: 01/02/19
DATE REPORTED : 01/28/19
REVIEWED BY:
6.1
01/04/19
HMM 4500H13-11
11484
01/15/19
LFJ
EPA200.7
<2.5
01/22/19
MTM
3113B-04
29963
01/15/19
LFJ
EPA200.7
2,6
01/17110
MTM
3113B-04
405
01/15/19
LFJ
EPA200.7
27
01115/19
LFJ
EPA200.7
39
01/18/19
MTM
311313-04'
1627
01/15/19
LFJ
EPA200.7
0.38
01/18119
MTM
EPA7471B
12
01/15/19
LFJ
EPA200.7
2129
01/15/19
LFJ
EPA200.7
<5.0
01/15/19
MTM
3113E-04
7054
01/15/19
LFJ
EPA200.7
6620
01/15/19
LFJ
EPA200.7
0.99
01/03/19
JMS
2540G11
c 51310
01/16/19
CLO
351.2 R2.93
c 610;5.
,OL1L39
DTL..330.1
R2-93....:.
c 26910
01/16/10
DTL 1
365.4-74
c 1806
01/11/19
CLO
353.2 R2-93
8
01/15/19
LFJ
EPA200.7
w
a Uncertified data. DWa dose not offer non -aqueous certification [or thia analytical procedure,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 15, 2019
McGinnis Point 1.91 % Solids
7.3 pH
Parameter
%
Mg/K;
Nitrogen (TKN)
9.177
Phosphorus
6.021
Potassium
0.155
PAN (injected)*
2.859
PAN surface)*
2.792
Ammonia Nitrogen
0.135
Calcium
4.080
Calcium Carbonate E .
--
Magnesium
---
Sodium
---
Sulfur
Nitrate N / Nitrite N
---
Barium
---
Chloride
--
Iron
--
Aluminum
---
Arsenic
---
Cadmium
---
Chromium
---
Copper
---
Lead
---
Mercury
Molybdenum
---
Nickel
—
Selenium
Zinc
---
Permit
Permit No. W00018525
x 10,0u0) (Mg/Kg x
91,770.000
60,210.000
1,553.000
28,594.600
27,917.600
1,354.000
40,795.000
3,934.000
9,803.000
115.800
5,806.00
3.90
0.82
26.000
2,016.00
37.00
0.28
5.00
11.00
5.00
1,198.00
Environment I N
Ton
)02)
183.540
120.420
3.106
57.189
55.835
2.708
81.590
7.868
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = %% PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N)+Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or<detection limits are listed as detection limits
for calculation purposes.
0.232
11.612
0.008
0.002
4.032
0.074
0,001
0.010
0.022
0.010
2.396
SAR
1.71
Ceiling Concen.
(M /K )
75
85
4,300
840
57
75
420
100
7,500

EIMFpNUmm Flo hCuppTOW
MCGINNIS POINT (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basts),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mgflcg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TRN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
n
Sludge Analysis Method
Sample Date Analyst Code
7.3 01/15/19 TCW 4500HB-11
5806 01/29/19 LFJ EPA200.7
3.9 01/29/19 MTM 3113B-04
40795 01/29/19 LFJ EPA200.7
0.82 01/30/19 MTM 3113B-04
2016 01/29/19 LFJ EPA200.7
26 01/29/19 LFJ EPA200.7
37 01/31/19 MTM 311311-04
3934 01/29/19 LFJ EPA200.7
0.28 02/07/19 MTM EPA7471B
11 01/29/19 LFJ EPA200.7
1553 01129/19 LFJ EPA200.7
<5.0 01/31/19 MTM 3113E-04
9803 01/29/19 LFJ EPA200.7
1198 01/29/19 LFJ EPA200.7
1.91 01/15/19 IKDS 2540G-11
c 91770 01/25/19 DTL 351.2 R2-93
c 1354 01/24/19 CLO 350.1 R2-93
c 60210 01/25/19 CLO 365.4-74
c 115.8 01/22/19 DTL 353.2 112.93
<5.0 01/29/19 LFJ EPA200.7
ID#: 555 A
DATE COLLECTED: 01/15/19
DATE REPORTED : 02/15/19
REVIEWED BY: 10"
c Uncertified data. DWR does not offer non.aqueoua certification for Chia analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2019
Permit No. WQ0018525
NC Aquarium at Pine 0.71 % Solids
Knoll Shores 12.33 pH (taken from lime stabilizati
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
trogen (TKN)
7.768
77,680.000
tos horus
5.135
51,350.000
tassium
0.632
6,324.000
iN (injected)*
2.342
23,416.794
IN (surface)*
2.337
23,373.334
nmonia Nitrogen
0.009
86.920
dcium
3.301
33,013.000
dcium Carbonate E .
---
---
a esum
---
8,967.000
dium
---
142,383.000
Ifur
--
—_
trate N / Nitrite N
--
51.950
rium
doride
___
,n
uminum
---
569.00
senic
---
2.50
dmium
---
6.20
tromium
---
11.000
,pper
---
206.00
ad
24.00
:rcu
---
0,40
Al bdenum
---
5.00
ckel
---
11.00
lenium
---
5.00
tc
---
393.00
Environment 19 444 A
Ton
)02)
155.360
102.700
46.747
0.174
66.026
17.934
284.766
0.104
1.138
0.005
0.012
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or<detection limits are listed as detection limits
for calculation purposes.
0.048
0.001
0.0I0
0.022
0.010
0.786
SAR
I�.O6
Ceiling Concen.
M )
75
85
4,300
840
57
75
420
100
7,500

Egow0 [MEW 1, hmpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
NC AQUARIUM AT PINE KNOLL SHORES
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt, basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
569 01/29/19 LFJ EPA200.7
<2.5 01/29/19 MTM 3113B-04
33013 01/29/19 LFJ EPA200.7
6.2 01/30/19 MTM 3113B-04
206 01/29/19 LFJ EPA200.7
11 01/29/19 LFJ EPA200.7
24 01/31/19 MTM 3113B-04
8967 01/29/19 LFJ EPA200.7
0.40 02/07/19 MTM EPA7471B
11 01/29/19 LFJ EPA200.7
6324 01/29/19 LFJ EPA200.7
<5.0 01/31/19 MTM 3113B-04
142383 01/29/19 LFJ EPA200.7
393 01/29/19 LFJ EPA200.7
0.71 01/23/19 KDS 254OG-11
c 77680 01/25/19 DTL 351.2 R2-93
c 86.92 01/24/19 CLO 350.1 R2-93
c 51350 01/25/19 CLO 365.4-74
c 51.95 01/22/19 DTL 353.2 112-93
23373 01/28/19 SEJ
<5.0 01/29/19 LFJ EPA200.7
wastewater ID, iv
PHONE [phone]
FAX [phone]
ID#: 444 A
DATE COLLECTED: 01/17/19
DATE REPORTED : 02/15/19
REVIEWED BY: ,
c Uncertified data. DWR doe. not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 25, 2019
The Grove W WTP 0.73 % Solids
7 pH
Parameter
%
Mg/KJ
(ova
Nitrogen (TKN)
5.612
Phosphorus
1.495
Potassium
0.752
PAN (injected)*
1.782
PAN surface)*
1.712
Ammonia Nitrogen
0.140
Calcium
2.612
Calcium Carbonate E .
---
Magnesium
---
Sodium
—
Sulfur
---
Nitrate N / Nitrite N
---
Barium
Chloride
---
Iron
Aluminum
---
Arsenic
---
Cadmium
---
Chromium
---
Copper
---
Lead
Mercury
Molybdenum
Nickel
Selenium
7.ine
Permit No. W Q0024756
14,950.000
7,519.000
17,822.000
17,122.000
1,400.000
26,117.000
3,625.000
14,810.000
6,000
1630.000
3.70
0.62
11.000
88.00
5.20
0.15
5.00
Environment 1 # 549 A
Ton
)02)_
112.240
29.900
15.038
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) +Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
2.800
52.234
7.250
29.620
0.012
3.260
0.007
0.001
0.010
0.000
0.010
0.012
0.010
1.112
SAR
1.94
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

THE GROVE WWTP (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt, basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt, basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mglkg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
IMN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.0 04/25/19 JMH 4500HB-11
1630 05/02/19 LFJ EPA200.7
3.7 05/07/19 MTM 3113B-04
26117 05/02/19 LFJ EPA200.7
0.62 05/02/19 MTM 3113B-04
88 05102/19 LFJ EPA200.7
11 05/02/19 LFJ EPA200.7
5.2 05/09/19 MTM 3113B-04
3625 05/02/19 LFJ EPA200.7
0,15 05/10/19 MTM EPA7471B
6 05/02/19 LFJ EPA200.7
7519 05/02/19 LrJ EPA200.7
<5.0 05/09/19 MTM 3113B-04
14810 05/15/19 LFJ EPA200.7
556 05/02/19 LFJ EPA200.7
0.73 04/29/19 JTH 2540G-11
c 56120 05/03/19 TLH 351.2 112-93
c 1400 04/30/19 BLD 350.1 112-93
c 14950 05/03/19 BLD 365.4-74
c 6,00 04/30/19 DTL 353.2 112-93
<5.0 05/02/19 LFJ EPA200.7
ID#% 549 A
DATE COLLECTED% 04/25/19
DATE REPORTED : 05/15/19
REVIE11ED BY
a Onoartlfied data. DWs does not offer non -aqueous certi Eication for Chia analytical Procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2019
Permit No. W00018525
Ocean Club 0.53 %Solids
12.19 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(M x 0.002)
Nitrogen (TKN)
6.378
63,780.000
127.560
Phosphorus
3.891
38,910.000
77.820
Potassium
0.766
7,660.000
15.320
PAN (injected)*
1.940
19,400.290
38.801
PAN surface)*
1.922
19,21.9.990
38.440
Ammonia Nitrogen
0.036
360.600
0.721
Calcium
4.350
43,498.000
86.996
Calcium Carbonate E .
--
---
---
Magnesium
---
4,924.000
9.848
Sodium
---
23,930.000
47.860
Sulfur
---
---
Nitrate N / Nitrite N
---
13.870
0.028
Barium
---
--
--
SAR
Chloride
---
---
---
2.11
Iron
---
---
--
CeilingConcen.
Aluminum
---
1,846.00
3.692
(M /K )
Arsenic
---
3.30
0.007
75
Cadmium
---
0.74
0.001
85
Chromium
---
9.000
--
---
Copper
---
312.00
0.624
4,300
Lead
---
11.00
0.022
840
Mercury
---
0.12
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
8.00
0.016
420
Selenium
---
5.00
0.010
100
Zinc
---
1,524.00
3.048
7.500
Environment I # 404 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

OCEAN CLUB (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES
P.O. BOX 4188
EMERALD ISLE ,NC 28594
Sludge
_PARAMETERS Sample
Analysis Method
Date Analyst Cade
FAX [phone]
ID#: 404 A
DATE COLLECTED: 01/02/19
DATE REPORTED : 01/28/19
REVIEWED BY:
Aluminum, (dry wt. basis), mg/kg
1846
01/15/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mglkg
3.3
01/22/19
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
43498
01/15/19
ZFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg'
0.74
01/17/19
MTM
3113B-04
Copper (dry wt. basis), mg/kg
312
01/15/19
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
9
01/15/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
11
Ol/18/19
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
4924
01115/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.12
01/18/19
MTM
EPA7471B
Nickel (dry wt, basis), mg/kg
8
01/15/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
7660
01/15/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
01/15/19
MTM
311311-04
Sodium (dry wt. basis), mg/kg
23930
01/15/19
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1524
01/15/19
LFJ
EPA200.7
Total Solids, %
0.53
01/03/19
JMS
2540G11
TKN (dry wt.), mg/kg
c 63780
01/16/19
CLO
351.2 112-93
Ammonia Nitrogen (dry wt.),mg/kg
c 360.6
01/11/19
DTL
350.1 R2.93
Phosphorus, T. (dry wt.), mg/kg
c 38910
01/16/19
DTL,--365.4-74
.. -
Nitrate -Nitrite (dry wt.), mg/kg
c 13.87
01/11/19
CLO
353.2 R2-93
Plant Available Nitrogen, mglkg
19220
01/16/19
SEJ
Molybdenum (dry wt. basis), mg/kg
<5.0
01/15/19
LFJ
EPA200.7
M
c Uncerti Lied date. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 29, 2019
Pebble Beach
0.59 % Solids
Permit No. W00018525
7.6 PH
Parameter
%
Mg/Kg Dry Weight
I % x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
6.537
65,370.000
130.740
Phosphorus
1.595
15,950.000
31.900
Potassium
0.490
4,903.000
9.806
PAN (injected)*
1.976
2,464.097
4,928
PAN (surface)*
1.966
2,435,542
4.871
Ammonia Nitrogen
0.021
205.700
0.411
Calcium
2.953
29,528.000
59.056
Calcium Carbonate E .
---
---
---
Magnesium
---
14,888.000
29.776
Sodium
---
10,402.000
20.804
Sulfur
---
--
Nitrate N / Nitrite N
---
7.730
0.015
Barium
---
---
__
Chloride
---
Iron
--
--
---
Aluminum
---
2,525.000
5.050
Arsenic
---
2.50
0.005
Cadmium
---
0.99
0.002
Chromium
---
8.000
Copper
---
202.00
0.404
Lead
---
12.00
0.024
Mercury
---
0.32
0.001
Molybdenum
---
5.00
0.010
Nickel
--
10.00
0.020
Selenium
---
5.00
0.010
Zinc---
1,065.00
2.130
Environment 1 It 287A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
0,94
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

rated
PEBBLE BEACH (HYDROTECH)
ATTNt DON O'KARA
RYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.6
OV29/19
TCW
4500HB-11
2525
02/11/19
LFJ
EPA200.7
<2.5
02(19/19
MTM
3113B-04
29528
02/11/19
LFJ
EPA200.7
0.99
02/15/19
MTM
3113B-04
202
02/11/19
LFJ
EPA200.7
8
02/11/19
LFJ
EPA200.7
12
02/14/19
MTM
3113B-04
14889
02/11/19
LFJ
EPA200.7
0.32
02/07/19
MTM
EPA7471B
10
02/11/19
LFJ
EPA200.7
4903
02/11/19
LFJ
EPA200.7
<5.0
02/20/19
MTM
3113B-04
10402
02/21/19
AKS
3111B-11
1065
02/11/19
LFJ
EPA200.7
0.59
01/30/19
KDS
2540G-11
c 65370
02/07/19
DTL\
351.2 R2-93
c 205.7
02/04/19
BLD
350.1 R2-93
c 15950
02/07/19
DTL
365.4-74
c 7.73
02/01/19
BLD
353.2 R2-93
19660
02/09/19
SEJ
<5.0
02/11/19
LFJ
EPA200.7
ID#t 287 A
DATE COLLECTED1 01/29/19
DATE REPORTED r 02/25/19
/�Jtn t �
REVIElp AB / V
0 Vneertified data. DaR does not offer non -aqua... ... tifi..tion for this analytionl .....dure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 5, 2019
Permit No. WQ0018525
Pine Knoll Townes 1.89 % Solids
74 nN
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
M x 0.002)
Nitrogen (TKN)
2.333
23,330.000
46.660
Phosphorus
1.390
13,900.000
27.800
Potassium
0.087
871.000
1.742
PAN (injected)*
0.744
7,439.230
14.878
PAN (surface)*
0.713
7,127.630
14.255
Ammonia Nitrogen
0.062
623.200
1.246
Calcium
3.592
35,922.000
71.844
Calcium Carbonate E .
---
--
Magnesium
---
2,457.000
4.914
Sodium
---
5,864.000
11.728
Sulfur
Nitrate N / Nitrite N
---
3.990
0.008
Barium
---
___
---
Chloride
___
I ___
--
Iron
---
---
---
Aluminum
---
4,265.00
8.530
Arsenic
--
3.30
0.007
Cadmium
---
1.40
0.003
Chromium
---
16.000
Copper
--
751.00
1.502
Lead
---
17.00
0.034
Mercury
---
011
0.000
Molybdenum
---
5.00
0.010
ickel
---
12.00
0.024
Selenium
---
5.00
0.010
Zinc
---
2,415.05
4.830
f
Environment I N 558 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
1.11
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100

ERAmMUM Flo hmpufflUd
PINE KNOLL TOWNES (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/icg
Copper (dry wt. basis), mg/kg
Chromium, T,(dry wt. basts),mglkg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt, basis), mg/kg
Total Solids, %
TICN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/Icg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.5 02/05/19 KDS 4500H13-11
4265 02/14/19 LFJ EPA200.7
3.3 02/19/19 MTM 3113B-04
35922 02/14/19 LFJ EPA200.7
1.4 02/15119 MTM 3113B-04
751 02/14/19 LFJ EPA200.7
16 02/14/19 LFJ EPA200.7
17 02/14/19 MTM 3113B-04
2457 02/21/19 LFJ EPA200.7
0,21 02/26/19 MTM EPA7471B
12 02/14/19 LFJ EPA200.7
871 02/14/19 LFJ EPA200.7
<5.0 02/20/19 MTM 311313-04
5864 02/22/19 AILS 3111B-11
2415 02114/19 LFJ EPA200.7
1.89 02/11/19 JMH 2540G11
c 23330 02/15/19 TLH 351.2 R2-93
c 623.2 02/08/19 BLD 350.1 112-93
c 13900 02/22/19 TLH 365.4-74
c 3.99 02/12/19 DTL 353.2 112-93
<5.0 02/21/19 LFJ EPA200.7
Dr£nking Water ID, 31715
ID#: 558 A
DATE COLLECTED: 02/05/19
DATE REPORTED : 02/26/19
REVIEWED BY:
c uncertified data. DWR does not offer n01-e4ueoue certi Cfoation Car this analytical Procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 10, 2019
Permit No. WQ0018525
Point Emerald Villas 1.07 %Solids
6.7 pH
Parameter
%
Mg/K Dry Weight
x 10,000)(Mg/Kg
Pounds/Dry Ton
(Mg/Kgx 0.002)
Nitrogen (TIW)
5.254
63,130.000
126.260
Phosphorus
1.482
14,950.000
29,900
Potassium
0.273
1,981.000
3.962
PAN injected)*
1.673
16,728.500
33.457
PAN (surface)*
1.656
16,558.000
33.116
Ammonia Nitrogen
0.034
755.500
1.511
Calcium
4.028
22,629.000
45.258
Calcium Carbonate E .
---
---
-__
Magnesium
---
1,617.000
3.234
Sodium
---
14,838.000
29.676
Sulfur
---
---
Nitrate N / Nitrite N
--
728.700
1.457
Barium
--
---
---
Chloride
---
---
---
Iron
---
---
--
Aluminum
---
6,643.00
13.286
Arsenic
--
2.50
0.005
Cadmium
--
1.20
0.002
Chromium
---
23.000
Copper
---
515.00
1.030
Lead
---
93.00
0.186
Mercury
--
0.43
0.001
Mol bdenum
5.00
0.010
Nickel
---
12.00
0.024
Selenium
5.00
0.010
Zinc
---
2,817.00
5.634
Environment 1 # 348 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N =% PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
2.65
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100

i�v�r (nment 1, nc
mhd.
ID#: 348 A
DNE [phone]
FAX [phone]
POINT EMERALD VILLAS (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES DATE COLLECTED: 01/10/19
P.O. BOX 4188 DATE REPORTED : 01/30/19
EMERALD ISLE ,NC 28594
REVIEWED BYz
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH, Units 6.7 01/18/19 JTH 450OBB-11
Aluminum, (dry wt, basis), mg/kg 6643 01/17/19 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 01/22/19 MTM 311313-04
Calcium (dry wt. basis), mg/kg 22629 01/17/19 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 1.2 01117/19 MTM 3113B-04
Copper (dry wt. basis), mg/kg- 515 ,01/17119 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 23 01/17/19 LFJ EPA200.7
Lead (dry weight basis), mg/kg 93 01/18/19 MTM 311313-04
Magnesium (dry wt. basis), mg/kg 1617 01/17/19 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.43 01/18/19 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 12 01/17/19 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 1981 01117/19 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 01/28/19 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 14838 01/17/19 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 2817 01/17/19 LFJ EPA200.7
Total Solids, % 1.07 01/14/19 KDS 2540G-11
TKN (dry wQ, mg/kg c 63130 01/23/19 BLD 351.2 112-93
Ammonia Nitrogen (dry wt.),mg/kg c 755.5 01/24/19 CLO 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 14950 01/23/19 DTL 365.4-74
Nitrate -Nitrite (dry wt.), mg/kg c 728.7 01/15/19 DTL 353.2 R2.93
Molybdenum (dry wt, basis), mg/kg <5.0 01/17/I9 LFJ EPA200.7
W
e uncertified data. DWR dcea nut offer non -aqueous certification for thin analytical procedure,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 16, 2019
Oueens Court 1.31 % Solids
7.21 pH
Parameter
%
Mg/K I
(% x
Nitrogen (TKN)
8.020
Phosphorus
1.450
Potassium
0.659
PAN (injected)*
2.996
PAN (surface)*
2.590
Ammonia Nitrogen
0.812
Calcium
1.090
Calcium Carbonate E .
--
Magnesium
Sodium
Sulfur
---
Nitrate N / Nitrite N
---
Barium
__.
Chloride
---
Iron
---
Aluminum
---
Arsenic
---
Cadmium
---
Chromium
---
Co er
---
Lead
---
Mercury
...
Molybdenum
---
Nickel
Selenium
---
Zinc
Permit No. W00018525
)ry Weight
10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
80,200.000
160.400
14,500.000
29.000
6,590.000
13.180
29,962.000
59.924
25,902.000
51.804
8,120.000
16.240
10,900.000
21.800
2,890.000
5.780
218.000
1,900.00
16.40
16.40
16.400
134.00
16.40
1.68
16.40
16.40
16.40
1,110.00
Envirwhem #
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
0.436
3.800
0.033
0.033
0.268
0.033
0.003
0.033
2.220
SAR
3.84
Ceiling Concen.
(M/K)
75
85
4,300
840
57
75
420
100
7,500

Environmental Chemists, Inc.
4
mo
6602 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 > 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 < 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Fortin Contract Services Date of Report: May 06, 2019
Post Office Box 4188 Customer PO #:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2019-06096
Project ID: Queens Court
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
19-15363 Site: Annual Sludge 4/1.612019 9:00 AM Solid/Sludge Kevin Stanley
Test Method Results Rate Analyzed
pH
Sludge Residuals
SW 846 Method 90450
7.21 units 04/24/2019
Aluminum
EPA200.7
1900mg/kg
04/22/2019
Arsenic
EPA 200.7
<16.4 mg/kg
04/23/2019
Cadmium
EPA200.7
<16.4mgtkg
04/2312019
Calcium
EPA200.7
10900mg/kg
0412212019
Chromium
EPA200.7
<16.4mg/kg
04/23/2019
Copper
EPA200.7
134mg1kg
04/22/2019
Lead
EPA200.7
<16.4mg/kg
04/25/2019
Magnesium
EPA200.7
2890mg/kg
04/2212019
Molybdenum
EPA200.7
<16.4mg/kg
04/23/2019
Nickel
EPA200.7
<16.4mg/kg
0412312019
Potassium
EPA200.7
6590mg/kg
04/22/2019
ttlrm,,::
E.fA299.7
<16.4.mg/kg
04/23/2019
Sodium
EPA200.7
15300mg/kg
04/22/2019
Zinc
EPA 200,7
1110 mglkg
04/22/2019
Nitrate+Nitrite-Nitrogen
EPA363.2
218mglkg
05/02/2019
Total Solids (%)
SM 2640 B
1.31 %
04117/2019
Ammonia Nitrogen
SM4600NH3 C
8120mg/kg
04/29/2019
Total Kjeldahl Nitrogen (TKN)
SM46000rgB
80200mg/kg
04/29/2019
Total Phosphorus
SM 4600 P F
14500 mg/kg
04/30/2019
Mercury
SW0467471B
<1.68mg/kg
04/22/2019
Comment: Sludge residuals, except pH, reported on a dry weight basis.
pH reported on an as received
basis.
Reviewed by:
a91OX-
E-MAILED MAY 07 2019
V
Report #:: 2019-06096 Page 1 of 1

BARNES ENVIRONriIENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 29, 2019
Permit No. WQ0018525
Sands Villas 2.92 %Solids
6.7 nH
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(MgtKg x 0.002)
Nitrogen (TKN)
8.560
85,600.000
171.200
Phosphorus
1.789
17,890.000
35.780
Potassium
0.275
2,748.000
5.496
PAN (injected)*
2.694
26,938.690
53.877
PAN (surface)*
2.605
26,047.190
52.094
Ammonia Nitrogen
0.178
1,783.000
3.566
Calcium
3.712
37,120.000
74.240
Calcium Carbonate Eq.
---
---
---
Magnesium
--
3,105.000
6210
Sodium
---
3,635.000
7.270
Sulfur
—
---
---
Nitrate N / Nitrite N
10.590
0.021
Barium
---
--
—
SAR
Chloride
---
---
---
0.83
Iron
---
---
--
Ceiling Concen.
Aluminum
---
3,450.00
6.900
M /K )
Arsenic
---
2.50
0.005
75
Cadmium
---
0.85
0.002
85
Chromium
---
17.000
---
---
Copper
--- 1
301.00
0.602
4,300
Lead
---
10.00
0.020
840
Mercury
---
0.23
0.000
57
Molybdenum
---
5.00
0.010
75
Nickel
---
11.00
0.022
420
Selenium
---
5.00
0.010
100
Zinc
---
1,087.00
2.174
7,500
Environment IN 559
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5 )(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.

EIMATmom % how
SANDS VILLA (HYDROTECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
od
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Code
PH (not to be used for reporting)
6.7
01/29/19
TCW
45001]B-11
Aluminum, (dry wt. basis), mg/kg
3450
02/11/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/19/19
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
37120
02/11/19
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.85
02/15/19
MTM
311311-04
Copper (dry wt. basis), mg/kg
301
02/11/19
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
17
02/11/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
10
02/14/19
MTM
3113B-04
Magnesium (dry wt, basis), mg/kg
3105
02/11/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.23
02/07/19
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
11
02/11/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
2748
02/11/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
02/20/19
MTM
3113E-04
Sodium (dry wt. basis), mg/kg
3635
02/22/19
AKS
3111B•11
Zinc (dry wt. basis), mg/kg
1087
02/11/19
LFJ
EPA200.7
Total Solids, %
2.92
01/30/19
KDS
2540G-11
TKN (dry wt.), mg/kg
c 85600
02/07/19
DTL\
351.2 112-93
Ammonia Nitrogen (dry wQ,mg/kg
c 1783
02/04/19
BLD
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 17890
02/07/19
DTL
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 10.59
02/04/19
TLH
353.2 R2.93
Molybdenum (dry wt. basis), mg/kg
<5.0
02/11/19
LFJ
EPA200.7
ID#: 559
DATE COLLECTED: 01/29/19
DATE REPORTED : 02/26/19
REVIEWED BY: .�
a Dnoerti Lied data. DWR doe. not offer non-aquaouo certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2019
Permit No. WQ0018525
Sea Isle Plantation 0.29 % Solids
12.04 pH (taken from lime stabilization event)
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.917
46,440.000
92.880
Phosphorus
0.675
14,760.000
29.520
Potassium
0.452
7,426.000
14.852
PAN (injected)*
0.813
8,134.148
16.268
PAN (surface)*
0.810
8,095.328
16.191
Ammonia Nitrogen
0.008
69.620
0.139
Calcium
4.831
25,298.000
50.596
n Carbonate E .
---
---
-_
3ium
---
2,771.000
5.542
L
---
51,101.000
102.202
N / Nitrite N
---
2,330.000
4.660
um
---
2,573.00
5.146
---
2.50
0.005
im
---
1.10
0.002
um
---
14.000
---
---
135.00
0.270
---
35.00
0.070
--
0.19
0.000
lenum
---
5.00
0.010
---
10.00
0.020
In
5.00
0.010
---
731.00
1.462
Environment I # 96A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
4.37
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

PHONE [phone]
%yam a� FAX [phone]
ID#: 96 A
1'7LE .PLANTATION
Mtl �F.ORTIN
"TOH'Y4b :CDNTRACT SERVICES DATE COLLECTED- 01/02/19
'P:6. 808 4188 DATE REPORTED i 01/28/19
!.vv¢RALD ISLE ,NC 28594
.. REVIEWED BY:
Sludge Analysis Method
PARA-1,15TERS Sample Date Analyst Code
Alunokman (dry wL basis), mg/kg 2573 01/15/19 LF7 EPA200.7
U'PRA'• My vtt- bass), m,lkg <2.5 01/22/19 MTM 3113B-04
:.'Qx tfkrc'vt basss), mg/kg 25298 01/15/19 LFJ EPA200.7
:.r,'. . c pi bass), mg/kg 1.1 01/17/19 MTM 3113B-04
faww vi-- bxsL), mg/kg 135 ' 011,5119 L LFJ EPA200.7
3;!L s' srt hasis),mg/kg 14 01/13/19 LFJ EPA200.7
may �mm 1 bases), mg/kg 35 01/18119 MTM 3113B-04
(dis Art..ba9is), mg/kg 2771 Ol/15/I9 LFJ EPA200.7
: F, tdrg pit .basis), mg/kg 0.19 01/18/19 MTM EPA7471B
(dry wt. basis), mglkg 10 01/15/19 LFJ EPA200.7
Pa (dry wt. basis), mg/kg 7426 01/15/19 LFJ EPA200.7
Sdmium (dry wt. basis), mg/kg <5.0 01/15/19 MTM 3113B-04
Sodium (dry wt basis), mg/kg 51101 01/15/19 LFJ EPA200.7
Z� (dry wt basis), mglkg 731 01/15/19 LFJ EPA200,7
Tagat saits, % 0.29 01/03119 JMS 2540G11
Zi `i (dry L), fmVkg c 46440 Ob111/19 BLD 351.2 112.93
Awnvum-b ?warm (dry wt.),mgVkg - c 69M 01J1ll19 DTL 350.1 R2-93
�• , T (dry w.),mg c 1#i60 Q]111419 11,H 3654-74
-Mbaft-'S�iCz (dre srt.),`mgP6g c,2330 0plM9 'CLO 3531 R2-93 '
Plant _Available-Mrogea, .; 16276-01114119 SEJ
MohiAeamn (dry wt. basis), mg/kg <5.0 01/15/19 LFJ EPA200.7
Or
e. 2_eartified data. nWR does not offer non-agneona certification for this analytical prooedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 7, 2019
Sea Spray 2.44 % Solids
7.1 pH
Parameter
%
Mg/Kg I
(% x
Nitrogen (TKN)
2.885
Phosphorus
0.416
Potassium
0.100
PAN (injected)*
0.889
PAN (surface)*
0.873
Ammonia Nitrogen
0.032
Calcium
3.890
Calcium Carbonate E .
---
Magnesium
---
Sodium
--
Sulfur
Nitrate N / Nitrite N
---
Barium
Chloride
Iron
--
Aluminum
---
Arsenic
---
Cadmium
---
Chromium
---
Copper
Lead
---
Mercury
---
Molybdenum
Nickel
Selenium
---
Zinc
---
40,839.000
2,840.000
2,993.000
10.830
2.50
0.78
8.000
870.00
8.50
0.18
5.00
12.00
5.00
843.00
Environment I #
Permit No. WQ0018525
Ton
302)
179.840
41.820
3.910
17.778
17.460
3.968
81.678
5.680
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N+Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
0.022
5.690
0.005
0.002
1.740
0.017
0.000
0.010
0.024
0.010
1.686
SAR
0.60
Ceiling Concert.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

EnwU r MEW Flo bw
SEA SPRAY (HYDROTECH)
DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
(Ed
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
PH (not to be used For reporting)
7.1
03/07/19
ICDS
4500HB-11
Aluminum, (dry wt. basis), mg/kg
2845
03/20/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
03/21/19
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
40839
03/20/19
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.78
03/27/19
MTM
3113E-04
Copper (dry wt. basis), mg/kg
870
03/20/19
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
8
03/20/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
8.5
03/20/19
MTM
3113B-04
Magnesium (dry wt, basis), mg/kg
2840
03/20/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.18
03/19/19
MTM
EPA7471B
Nickel (dry wt, basis), mg/lcg
12
03/20/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
1955
03/20/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
03/26/19
MTM
3113E-04
Sodium (dry wt. basis), mg/kg
2993
03/27/19
AKS
3111E-11
Zinc (dry wt. basis), mg/kg
843
03/20/19
LFJ
EPA200.7
Total Solids, %
2.44
03/11/19
KDS
2540G31
TEN (dry wt.), mg/kg
c 89920
03/13/19
DTL
351.2 R2-93
Ammonia Nitrogen (dry wt,),mg/kg
c 1994
03/12/19
CLO
350.1 R2-93
Phosphorus, T. (dry wt.), mg/lig
c 20910
03/13/19
CLO
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 10.83
03/13/19
TLH
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
<5.0
03/20/19
LFJ
EPA200,7
ID#: 560
DATE COLLECTED: 03/07/19
DATE REPORTED : 03/29/19
REVIEWED BY:
0 Uncertified data. DWR doe. not offer non -aqueous oartitication for thin analytical procedure,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 7, 2019
Permit No. W00018525
Sound Of The Sea 1.65 % Solids
A nit
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
x 0.002)
Nitrogen (TKN)
2.885
49,950.000
_(ME/Kg
99.900
Phosphorus
0.416
17,560.000
35.120
Potassium
0.100
2,032.000
4.064
PAN (injected)*
0.888
8,884.160
17.768
PAN (surface)*
0.873
8,725.160
17.450
Ammonia Nitrogen
0.032
2,958.000
5.916
Calcium
3.890
19,948.000
39.896
Calcium Carbonate E .
---
--
Magnesium
---
5,305.000
10.610
Sodium
-
6,496.000
12.992
Sulfur
Nitrate N /Nitrite N
---
5.960
0.012
Barium
___
___
Chloride
—
___
---
Iron
Aluminum
--
3,451.00
6.902
Arsenic
--
2.50
0.005
Cadmium
--
1.20
0.002
Chromium
---
10.000
---
Copper
---
758.00
1.516
Lead
---
49.00
0.098
Mercury
---
0.06
0.000
Molybdenum
---
5.00
0.010
Nickel
---
11.00
0.022
Selenium
---
5.00
0.010
Zinc
---
1,672.00
3.344
Environment 1 # 561
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
1.35
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100

EWFOM t�ii W %
Md
SOUND OF THE SEA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/lig
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.7 01/08/19 IDS 4500HB-11
3451 01/15/19 LFJ EPA200.7
<2.5 01/22/19 MTM 311313-04
19948 01/15/19 LFJ EPA200.7
1.2 01/17/19 MTM 3113B-04
758 01/15/19 LFJ EPA200.7
10 01/15/19 LFJ EPA200.7
49 01/18/19 MTM 3113B-04
5305 01/15/19 LFJ EPA200.7
0.06 01/18/19 MTM EPA7471B
11 01/15/19 LFJ EPA200.7
2032 01/15/19 LFJ EPA200.7
<5.0 01/15/19 MTM 3113B-04
6496 01/15/19 LFJ EPA200.7
1672 01/15/19 LFJ EPA200.7
1.65 01/09/19 KDS 2540G-11
c 49950 01/18/19 TLH 351.2 R2-93
c 2958 01/24/19 CLO 350.1 112-93
c 17560 01/18/19 BLD 365.4-74
c 5.96 01/15/19 DTL 353.2 R2-93
5 01/15/19 LFJ EPA200.7
ID#: 561
DATE COLLECTED: 01/07/19
DATE REPORTED : 01/28/19
REVIEWED BY:
c Vncartified data. DWR doe. not oflat son -aqueous certification for thin analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 25, 2019
Permit No. WQ0018525
Southvvinds Condominiums 1.15 % Solids
7.1 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
5.620
56,200.000
112.400
Phosphorus
1.550
15,500.000
31.000
Potassium
0.427
4,265.000
8.530
PAN injected)*
1.775
17,747.880
35.496
PAN (surface)*
1.712
17,118.380
34.237
Ammonia Nitrogen
0.126
1,259.000
2.518
Calcium
3.991
39,914.000
79.828
Calcium Carbonate E .
---
---
---
Magnesium
---
3,147.000
6.294
Sodium
---
6,570.000
13.140
Sulfur
Nitrate N / Nitrite N
---
6.580
0.013
Barium
---
--
--
SAR
Chloride
---
--
0.91
Iron
---
--
--
Ceiling Concen.
Aluminum
---
3042.000
6.084
M )
Arsenic
---
2.50
0.005
75
Cadmium
---
0.56
0.001
85
Chromium
---
11.000
---
—
Copper
---
757.00
1.514
4,300
Lead
---
12.00
0.024
840
Mercury
---
0.25
0.001
57
Molybdenum
---
5.00
0.010
75
Nickel
—
9.00
0.018
420
Selenium
---
5.00
0.010
100
Zinc
---
1,028.00
2.056
7,500
Environment 14 562 B
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = %* PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

EROW'UnIM ui]&M Flo hCorrmmUd
SOUTHWINDS (HYDROTECH)
DON OIMARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Code
PH (not to be used for reporting)
_ 7.1
04/25/19
JMH
4500IIB-11
Aluminum, (dry wt. basis), mg/ki;
3042
05/02/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
05/07/19
MTM
311311.04
Calcium (dry wt. basis), mg/kg
39914
05/02/19
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0,56
05/02/19
MTM
311311-04
Copper (dry wt. basis), mglkg
757
05/02/19
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mgHcg
11
05/02/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
12
05/08/19
MTM
3113E-04
Magnesium (dry wt. basis), mg/kg
3147
05/02/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.25
05/10/19
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
9
05/02/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
4265
05/02/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/lig
<5.0
05/09/19
MTM
3113E-04
Sodium (dry wt. basis), mg/kg
6570
05/15/19
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1028
05/02/19
LFJ
EPA200.7
Total Solids, %s
1,15
04/29/19
JTH
2540G.11
TRN (dry wt.), mg/kg
c 56200
05/03/19
TLH
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 1259
04130/19
BLD
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 15500
05/03/19
BLD
365.4.74
Nitrate -Nitrite (dry wt.), mg/kg
c 6.58
04/30/19
DTL
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
<5.D
05/02/19
LFJ
EPA200.7
ID#: 562 B
DATE COLLECTED: 04/25/19
DATE REPORTED : 05/15/19
REVIEWED BY:
o Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 17, 2019
Summer Winds 1.62 %Solids
7.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Nitrogen (TKN)
13.210
132,100.000
Phosphorus
3.626
36,260.000
Potassium
0.392
3.916.000
N / Nitrite N
986.200
48,513.000
5,550.000
28,107.000
8.910
691.00
2.50
0.67
8.000
532.00
15.00
0.16
5.00
11.00
Permit No. WQ0018525
Pounds/Dry Ton
_LMg/Kg x 0.002)
264.200
72.520
7.832
80.659
79.672
1.972
97.026
11.100
56.214
0.018
Environment 1 # 119A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
5.382
0.005
0.001
1.064
0.030
0.000
0.010
0.022
0.010
3.908
SAR
4.09
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Environment 1,
SUMMERWINDS HOA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH
P.O. BOX 4602
EMERALD ISLE ,NC 28594
Nd
Sludge
Analysis
Method
PARAMETERS
Sample
Date Analyst
Code
PH (not to be used for reporting)
7.4
01/17/19
TCW
4500HB-11
Aluminum, (dry wt. basis), mg/kg
2691
01/29/19
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
01/29/19
MTM
3113E-04
Calcium (dry wt. basis), mg/kg
48513
01/29/19
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
0.67
01/30/19
MTM
3113E-04
Copper (dry wt. basis), mg/kg
532
01/29/19
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
8
01/29/19
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
15
01/31/19
MTM
3113E-04
Magnesium (dry wt. basis), mg/kg
5550
01/29/19
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.16
02/07/19
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
11
01/29/19
LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
3916
01/29/19
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
01/31/19
MTM
3113E-04
Sodium (dry wt. basis), mg/kg
28107
01/29/19
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
1954
01/29/19
LFJ
EPA200.7
Total Solids, %
1.62
01/23/19
IMS
2540G-11
TKN (dry wt.), mg/kg
c 132100
01/25/19
DTL
351.2 R2-93
Ammonia Nitrogen (dry wW,mg/kg
c 986.2
01/24/19
CLO
350.1 R2-93
Phosphorus, T. (dry wt.), mg/Itg
c 36260
01/25/19
CLO
365.4-74
Nitrate -Nitrite (dry wQj mg/kg
c 8.91
01122/19
DTL
353.2 R2-93
Molybdenum (dry wt. basis), mg/kg
<5.0
01/29/19
LFJ
EPA200.7
ID#: 119 A
DATE COLLECTED: 01/17/19
DATE REPORTED : 02/15/19
I
REVIEWED EY:
c Uncertified data. DWR does not offer non -aqueous certi ESeatlan for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 21, 2019
Whaler Inn
0.60 % Solids
i.A pn
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Nitrogen (TKN)
1.601
23,890.003
Phosphorus
0.397
12,940.000
Potassium
0.399
3,748.000
PAN (injected)*
0.513
5,131.800
PAN (surface)*
0.499
4,986.800
Ammonia Nitrogen
0.029
125.600
Calcium
5.591
49,404.000
Calcium Carbonate E .
---
--
Magnesium
---
2,908,000
Sodium
---
90,132.000
Sulfur
---
---
Nitrate N / Nitrite N
---
124.600
Barium
---
---
Chloride
---
---
Iron
---
---
Aluminum
---
2,197.00
Arsenic
---
2.50
Cadmium
---
0.62
Chromium
---
8.000
Copper
---
570.00
Lead
---
11.00
Mercury
---
0.15
Molybdenum
---
5.00
Nickel
---
6.00
Selenium
---
5.00
Zinc
--
901.00
Permit No. WQ0018525
x
47.790
25.880
7.496
10.264
9.974
0.251
98.808
— 180.264
0.249
Environment 1 A 70A
*Determination of Pant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
4.394
0.005
0.001
1.140
0.022
0.000
0.010
0.012
0.010
1.802
SAR
8.24
Ceiling Concen.
(M )
75
85
4,300
840
57
75
420
100
7,500

EIMU oo[iow % h orryor Ood
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
THE WHALER INN
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD.
MAYSVILLE ,NC 28555
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt, basis), mg/lig
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TEN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7.2 02/21/19 KDS 4500HB-11
2197 03/20/19 LFJ EPA200.7
<2.5 03/07/19 MTM 311313-04
49404 03/20/19 LFJ EPA200.7
0.62 03/11/19 MTM 3113B-04
570 03/20/19 LFJ EPA200.7
8 03/20/19 LFJ EPA200.7
11 03/06/19 MTM 3113B-04
2908 03/20/19 LFJ EPA200.7
0.15 02/26/19 MTM EPA7471B
6 03/20/19 LFJ EPA200.7
3748 03/20/19 LFJ EPA200.7
<5.0 03/08/19 MTM 3113B-04
90132 03/27/19 AILS 3111B-11
901 03/20/19 LFJ EPA200.7
0.60 02/21/19 JTH 254OG-11
c 23890 02/28/19 TLH 351.2 112-93
c 125.6 02/28/19 DTL 350.1 R2-93
c 12940 02/28/19 BLD 365.4-74
c 124.6 02/27/19 DTL 353.2 112-93
7317 03/04/19 SEJ
<5.0 03/20/19 LFJ EPA200.7
FAX [phone]
ID#: 70 A
DATE COLLECTED: 02/21/19
DATE REPORTED : 03/28/19
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

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PATHOGEN AND VECTOR ATTRACTION REDUCTION MONITORING

Al\1\VAL 1 A 111V VL' 1\ Al\L Y i•.a., 1 V1m n 1 11(al, i iuiN 1tL' mul. i i"ri r uitivl tuA i ituies)
Facility Name: Barnes Environmental Waste and Hauling, Inc. WQ Permit Number: W00018525
WWTP Name: SEE ATTACHED LIST NPDES Number: SEE ATTACHED
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
I Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Patho en s ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermo 9rilic ❑
Beta Ra ❑
Y
Ganima Ra ❑
e '
Past uuzatior r ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
Com �osfiug ❑
lAcTobic Digestion ❑:•r}}:
Anaerobic g
•A
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>:.•i:..
•data:. •
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able to alternat' p rve performed (Class or B) complete the following
monitoring
Parameter
Allowable Level
in
in Sludge
Pathogen Density
NUM er o
Excee.
Frequency
of Anal sis
Y
Sample
Type
na rca
Tech -
ninue
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Geo. Mean
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Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
IMPN
CFU
1000 mpn per gram
of total solid (dry
wei ht
Salmonella bacteria
(in lieu offecal I
coliform
3 MPN per 4 grams
total solid (dry
weight)
vector Attraction itednCtron WA 1NUAU ULT .111)71- Please indicate alternative nerformede
Alt. I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt, 5 (14-Day Aerobic) ❑
JAIL 6 (Alk, Stabilization❑
JAR 7 (Drying - Stable) ❑
Alt. 8 (Drying. -Unstable) ❑
Alt. 9 (Injection) ❑
JAR. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
C RTijHCATIO N STA'iUdENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met"
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please. note
if you check this statement attach an explanation why you have not met one or both of the
finis uerer•mnauon nas ueen made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I ant aware that there are
significant penalties for false certification including fine and imprisonment."
Steven M. Barnes, President
Prepar7, ame and Title(typeor print) Land Applier Name and Title (if applicable)(type or print)
/ / 26,4V
Signature of Prepar•er* T Date Signature of Land Applier• (if applicable) Date.
*Prepater is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: P.O.#
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name:
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name:
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ^ / rp�py} Lt,A P.O.#
Batch Size (gallons): ry .6 O Q Lbs. or Gallons Used: / / D D Material Used For Stabilization: Llme
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER SIOSOLIDS
Facility Name: ejgwl; k P.O.#
Batch Size (gallons): 4 nob Lbs. or Gallons Used: .9k st Material Used For Stabilization: lime
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ;'1nf>. �2i�D i W nS P.O.#
Batch Size (gallons): `? S V V Lbs. or Gallons Used: ) Tc� Material Used For Stabilization: Urne
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 7]T &- ,eec.)j e f ias P.O.#
Batch Size (gallons): ( 7 ,� 6 Lbs. or Gallons Used: )7b Material Used For Stabilization: Lime
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: t1911,0po S t&d f plT P.O.#ry
Batch Size (gallons): �1 00() Los. or Gallons Used: 16S w" Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: P.0) .#
Batch Size (gallons): A3 6 ha Lbs. or Gallons Used: Mob Material Used For Stabilization: Lime
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ,�JC�- Tq An, P.O.#
Batch Size (gallons): -� i a 06 Lbs. or Gallons Used: /on Material Used For Stabilization: Lime
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: (,7&eA ,7e1Zx61
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 6 up4 64- l V1e , ]Qo P.O.#
Batch Size (gallons): Lbs. or Gallons Used: ,qmcia Material Used For Stabilization: 1-ime
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: (36" yam, t4/ vGZS P.O.#
Batch Size (gallons): 12DO 0 Lbs, or Gallons Used:;_ ram U Material Used For Stabilization: lime
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WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: /,17 P roAnpri.ji-41dC P.O.#
+p Batch Size (gallons): rj b ® Lbs. or Gallons Used: 7226 b Material Used For Stabilization: Lime
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M
(fJ
O
M
O
N
CO
N
I-
N
Co
N
(l]
N
7
N
M
N
N
N
T
N
0
N
0
O
I`
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V
M
N
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O
F

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 14 J�6je.- �—/L/Aj P.O.#
Batch Size (gallons): /0 ,] n 6 Lbs. or Gallons Used: r "TIO,,5M Material Used For Stabilization: Lime
a
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2019 APPLICATION SUMMARY

BARNES ENVIRONMENTAL WASTE
Permit # WQ 0018525
RESIDUALS APPLICATION
II 2019 APPLICATION SUMMARY II
Will Turner
2019
1
6.20
94,500
9.92
31.48
20.88
Site WT
2019
2
5.00
80,500
5.44
42.81
0.00
2019
3
8.00
119,000
5.67
27.05
1 0.00
2019
5
2.60
73,500
3.39
34.57
18.70
2019
6
2.90
105,000
5.07
27.42 130.19
Totals
Total Gallons 472,500
W WTP - Metric Tons 26.75

FIELD LOADING RATE REPORTS

ANNUAL LAND APPLICATION FIELD SLWMARY FORM
Facility Name: Itarnatnvironmemviyymc3Haulinn Permit: W00018525 Annual Dry Tons Applied: 992
Owner. Will Turner Operator. Steve Barnes Cation Exchange Capacity( non 503): 2.2
Site & WT Field 0. 1 Acres Utilized: 6.20 Acres Permitted: 6.20
Application Method*: S Volatilization Rate**: OS Mineralization Rate: 30 %
Predominant Soil Series: GOA
:.:.::.:
ti:: ...t:
..Date:.
:iit:iiii'::::i.'.•.•:::t
tt tat
..fi.$75:.
t:>;4'e "tit
.... ce..
:::e'.::::
:; ::::-.:::.:.__..::...,....::
..�`n9.:F
::......:::.::
:_4ckC:
..s•::::
t>4:i'�`011)1'bi:;[::.C'01Id,
:::...:i
.::-:::::.:;
::ra
:.:-:.::.c•>:::>..::.••;...:.:.:.:»:>:r<.:..:....::..::::..:::::.:..
--
_:.::...................
.,.....
. .
:;:�::e
;....:..;
c:;f,'Y[Et:
.:..:.::
-:4:dE:i
.:::::::...:.:.:::::
:'-pi�:::
p::Q�ii
ciit'f0:>
>:; ':.::.:
r:.hlrpCy
-• �:::::
�::
-.:s
::. , . , .,
., ..: ..
-
•
• • •
2019
7,000
1,129
0.88
0.04
Adande Station
G1D
0.000
0.000
0.053
0.001
0.000
0.000
0.001
0.000
0.092
0,10
0.10
2.33
Com
Rye
,196
0.02
0.00
2019
17.500
Z823
1.69
010
Bm=5 R=6
G/D-
0.001
0.000
0:720
0.009
0.000
0.002
0.0071
0.002
0:535
2.01
3.01
6.60
Cam
Rye
16.49
0.35
0.00
2019
14,000
2,258
2.40
023
CC secs
G/D
0.004
0.004
0313
0.004
0.000
0.004
0.004
0.004
0264
8.17
2.72
10.53
Com
Rye
34.67
2.02
0.09
2019
3,500
565
129
0.03
1Lv PtouSuim
G/D
0.000
0.000
0.061
0.000
0.000
0.000
0.000
0.000
0.029
L16
0.59
Rye
3.76
0.15
0.00
2019
1 7,000
1.129
1.91
1 0,09
McGinnis Point
G/D
0.00t
0.000
0.363
0.007
0.0001
0.001
0.002
0.001
0.215
5.02
10.83
Rye
16.50
0.24
0.02
2019
3,500
565
053
1 0.01
0cmClab
G/D
0.000
0.000
0.008
0.000
0.0001
0.000
0.000
0.000
0.0381
0.48
0.97
Corn
1.59
0.01
0.00
2019
3,500
7,000
1.89
0.55
ne Knod
,
G/D
0.004
0.002
0.929
0.019
0.0001
0.006
0.013
0.006
1665
1 7.86
1534
Com
25.74
0,69
0.00
2019
7,000
1,129
131
0.06
Que Coun
0/1)
0.002
0.002
0.017
0.002
0.000
0-002
0.002
0,002
0.I37
1.60
1.60
1.79
Com
Rye
9.89
1.00
0.03
2019
7,000
1.129
2M
0.14
Surds Vfflss
G/D
0,001
0-000
0.083
0.003
0.000
1 0:001
0.003
0.001
0.299
7.16
4.92
Rye
2354
0.49
0:00
2019
3,500
565
0.29
0.01
So l:tePlwmlian
GO
0.000
0.000
0.002
0.000
0.0001
0.000
0.000
0.000
0.010
0.11
0.20
Rye
0-63
000
0,03
2019
7,000
1,L9
2.44
0.11
Sm Spry
0/0
0.001
0.000
0200
0.007
0.0001
0.001
0.003
0.001
0.194
2.01
4.80
Com
20:66
0.46
0.110
2019
10,500
1.694
1.62
0_11
Summc Winds
G/D
0.001
0.000
0.122
0.003
0.000.
0.001
0.003
0,001
0,447
9.11
830
Com
30.23
0.23
0.00
2019
3,500
565
0.60
0.01
WAalerinn
G/D 10.000
D.000
0.016
0,000
0.0001
0.0001
0.000
0:000
0.0251
0.14
0.37
Com
0.67
0.00
0:00
Total
94,500
Annual lbs/acre 0.014 0.009 2.785 0.051 0.001 0.019 0.038 0.019 4.950 31.48 20.88 67.56
Current Cumulative Ibs/sere 0.07 0.05 19.861 0.34 0.01 0.1t 0.19 1 0.10 25.11 148 50 Permit PAN Limt Ist/2nd Crop
Prior Y=m Cumulative lbs/aere 0.06 0.04 17.08 0.29 0.00 0.09 0_IS 0.09 20.16
Pcrmitt CP1.R.*** 36 34 1338 1 267 IS N/A 374 89 2498
"1 certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personuel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false.information, including the possibility of fines and imprisonment for knowing violations."
.q
Lime
AD
Date I
Lbs/A
X � %)/'::_IJG'r'"^�•^� i /..:1����i2.li 'Application Method: S-Surface, IN -Injection, INC- Incorporation
(Signature of Land Applier) Daze *'Volatilization Rate:. Surface- 05, Injection/Incorporation -1.0
***C.P.L.R:. Cumulative.Pollutant Loading Rate
WMSS, PLLC
DENR FORM FSF(V2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: B:rcnas Eariroamanml wage & R.araa Permit#: WOOO18525. Annual Dry Tons Applied: 5.44
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity ( non 503): 6.8
Site ff: WI• Field X: 2 Acres Utilized: 5:00 Acres Permitted: 5.00
Application Method*: S Volatilization Rate**: 0_5 Mineralization Rate: 30 % Predominant Soil Series: GoA
:��^:i:i:i;�;i?t:�':0i:::�:
tittli'..uf
_ti-
iiti '.::::
- :€
s• .0 : sit
`[y-:�
s. _ :.'
::' - :':
- ::':
C*iR::.:.: tit
at_ .: ::afar
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:it€y::t?t:its<i
=itt:ti3i0ii�:
.:.Mc-
• •.: •: -„
:.::::::;
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7� :::� ::Y::+
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<.: � :.>:.r:y:
:.::.:
.-.::._
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::
-
i : •: .::
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7<::i[t
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itti: '"o-:
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�f�ci
.:..: . _
j5'I{lit
......:.:
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Pf:Eb`4`Iti
iici
St:�So-:
s ""
-�:`�El;i
... .......
?.1klY2i
SEzs31.Fz?[
.Cf'9
_
2019
24,500
4,900
0.88
OA8
Adanec Slarian
G/D
0.001
0.000
0.230
0.006
0.000
0.002
0.004
0.002
0.401
0.82
10.12
Caastat
17.18.
0.10
0.00
2.019
7,000
1,4t10
140
0.14
CC Sass
G/D
0.002
0.002
0.194
0.002
0.000
0.002
0.002
0.002
0.163
6.75
6.53
cmw
21.49
1.26
0.05
2019
3.500
700
129
0.04
[L-Fnaasailes
G/D
0.000
0.000
0.076
0.000
0.000
0.000
0.001
0.000
0.036
1.44
0.73
cossw
4.67
0.19
0.00
2019
7,000
1,400
1.23
0.07
DanacaPc
G/D
0.000
0.000
0.089
0.002
0,000
0.001
0.001
0.001
0.120
328
2.29
coastal
10.90
0.04
0.00
2019
3,500
700
0.34
0-o1
Fig', 12 Mamu
G/D
moo
omit
0.021
0.000
0.000
0.000
OA00
0.0o0
0.042
0.18
0.34
coast!
0.88
0.00.
0.04
2019
3,500
700
1.31
0.04
Queens Caud
G/D
0.001
0.001
0.010
0.001
0.000
0.001
0.001
0.001
0.085
1.98
1.11
coastal
1
6.13
0.62
0.02
2019
10,500
2,100
2.92
026
Sands Villas
G/D
0.0011
0.000
0.1541
0.005
0.000
0.003
0.006
0.003
0.556
1332
9.I5
Coastal
43.78
0.91.
0.01
20I9
10,500
2,100
2,44
021
San Spay
G/D
0.001
0.000
0.3721
0.004
0.006
0.002
0,005
0.002
0.360
3.73
9.94
Coastal
38.43
0.85
0.00
2019
IM00
2,100
1.62
0.14
S-o`ymds
G/D
0.001
0-000
0.151
0,004
0.000
0.001
0.003
0.001
0.554
11.30
10.29
Caaral
37.48
0.28
0-00
Total
80,500
Annuallbs/acre 0.008 0.005 1.297 0.025 0.001 0.013 0.023 0.013 2.318 42.81 0.00 49.48
COrrent Cumulativelbs/acre 1.85 0.03 75.13 25.03 OA6 0.29 -0.97 0.63 89.61 299 50 Permit PAN Limt lst/2nd Crop
Prior Years Cumulative lbslacre 1.84 0.08 73.83 25.00- 0.45 0.27 0.94 0.61 8730
Permitt CP.LR.*** 36 34 1338 267 1 .15 1 N/A 374 89 2498
*1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, Including the possibility of fines and imprisonment -for knowing violations,"
n
LimeA
Date
Lbs/A
-
UY
(SignamreofLandApplier) Date
*Application Method: 5 - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, InjectionMcorpotapon -1.0
***C:P.L.R.: Cumulative Pollutant Loading Rate
WMSS; PLLC
DENR FORM FSF (712002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Barnes Environmental Waste& iraurine Permit#: W00018525
Owner. Will Turner
Operator. Steve Barnes
Site#. WT Field It. 3
Application Method*: S
Acres Utilized. 8.00
Volatilization Rate-: 0.5
Annual Dry Tons Applied: 5.67
Cation Ezclsaage, Capacity ( non 503): 8.2
Acres Permitted: 8.00
Mineralization Rate: 30 % Predominant Soil Series: rnA
_
-
11.
;in.....Al�t4
:L�Aitt2
>a:::;1.
tCpo
2019
10,500
1,313
0.88
0.05
Adanlic Station
rA:)
0.000
0.000
0.062
0.002
0.000
0.000
0.001
0.000
0.108
0.22
2.71
Costa
4.60
0-03
OM
2019
14,000
1750
1.69
0.12
1- Ruch
G/D
0.001
0.000
0.447
0.006
0.000
0.001
OM4
0.001
0.332
3.11
4.09
coastal
10.23
022
0.00
2019
3,500
438
1.25
0.02
lfampmnSuha
G/D
0.000
0.000
0.047
0,000
0.000
0.000
0.000
0.000
0.022
0,90
0.46
Coastal
2,92
M2
0.00
2019
10,500
1,313
123
0.07
DonaseaPe
G/D
0-000
'0.000
0.084
0.002
0.000
0.001
0.001
0.001
0.113
3.07
2.14
cmaai
10.22
0.03
0,00
2019
21,000
1 2.625
0.73
0.08
The Grove
O/D
0.001
0.000
0.014
0.001
OMO
0.00t
0.001
0.0011
0.089
2.74
2.39
Count
8.97
022
0.00
2019
3,500
438
0.53
0.01
ocean dub
G/D
0.000
0.000
0.006
0,000
0.000
0.000
0.000
0.000
0.029
0.37
0.75
Coastal
1.23
0.01
0.00
2019
14,000
1,750
0.59
0.04
Pebblebeach
G/D
0.000
1 0.000
1 0.0171
0.001
0.0001
0.000
0.001
0-000
0.092
021
137
.C.]
5.63
0.02
0.00
20I9
3,500
438
0.29
0.01
Sealsk Planastian
GA)
0.000
oxcol
not
I 0.000
0.000
0.000
0.000
0.000
0.008
0.09
0.16
Coosa
0.49
0.00
0.02
2019
14,000
1;750
1.65
0.12
smmdor'the Su
G/D
0.001
0.0001
0.183
10.012
0.000
0.001
0.003
0.001
0.463
2.10
4.23
Coasal
12.03
0.71
0.00
2019
21,000
Z625
1,62
0.18
Summer Winds
G/D
0.001
0.000
0.189
T0,005
0.000
0.002
0.004
0.002
0.693
14.13
12.86
Costal
46.85
0.35
0.00
2019
3.500
438
0.60
0.01
wblsr Om
G/D
0.000
0.000
0.012
0.000
0.000
0.000
0.000
0.000
0.020
0.11
0,52
0.00
0.00
Total
119,000
Annualibs/acre (1.004 0.001 1.062 0.029 6.000 0.007 0.015 0.007 1.907 27.05 D. 33A4
Curreat Cumulstivelbs/acre O.19 039 60.67 0.94 0.01 0.7.3 0.61 0.20 63.25 299 50 PermitPAN LimtlsM2nd.Crop
Prior Years Cumulative lbs/acre 0.18 039 59.61 0.91 0.01 0.22 0.60 0.19 61.34
PermiK C.P.L.R**` 36 34 1338 267 15 MA 374 89 2498-
"I certify, under penalty oflaw, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted- I am aware that there are
significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations."
Lime
Date
L6s/A
7
X ��"`"-J "�`/��/"��''�� *Application Method: S-Surface,.IN-Injection, INC -Incorporation
ignature of Land Applies) Date **Volatilization Rate: Surface- 0.5, Injection/Incorpotation- 1.0
***C,P.LR:: Cumulative Pollutant Loading Rate
WMSS, PLLC DENR FORM FSF (712002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: B.."Envlronmenralwaste&Haarina Permit#:W000I8525 Annual Dry Tons Applied: 3.39
Owner. Will Turner Operator. Steve Barnes Cation Exchange Capacity ( non 503): 5.9
Site M WT Field #: 5 Acres Utilized: 2.60 Acres Permitted: 2.60
Application Method*: S Volatilization Rate--: 0.5 Mineralization Rate: 30 %
Predominant Soil Series! GnA
...
-
.... ..:...
.:Crd 2
ti:7 �Ys.1{l`1FJ3i
2019
7,000
2,692
2.40
0.27
CC Sass
G/D
0.005
0.005
0.373
0,005
0.001
0.005
0.005
0.005
0.3I4
6.50
650
1256
Coastal
Rye
41.33
2.41
0.11
2019
7,000
2,692
129
0.14
Hampton Suites
G/D
0.001
0.000
0.292
0.001
0.000
0.001
0.002
0.001
0.137
5.53
2.81
coastal
17.95
0.73
0.00
2019
7,000
2,692
1.23
0.14
Duneseape
G/D
0.001
0.000
0-172
0.004
0.000
0.001
0.002
0.001
0,231
6.30
4.39
coastal
20.95
0.07
0.00
2019
2019
3,500
3,500
1,346
1,346
0.99
0.71
0.06
0.04
Kingsbridge It
NU quanum a[
Pint rnnllSho=
G/D
G/D
0.000
0.000
0.000
0.000
0.045
0.016
0.004
0.002
0.000
0.000
0.001
0.000
0.001
0.001
0.001
0.000
0.736
0.031
1.93
1.86
2.99
1 4.09
Coastal
Coastai
5.70
6.19
0.07
0.01
0.20
0.00
2019
2019
10,500
3,500
4,038
1,346
0.53
1.07
0.09
0.06
OoeanClub
omt u
villas
G/D
G/D
0.001
0.000
0.000
0.000
1 0.056
0.062
0.002
0.011
0.000
0.000
0.001
0.001
0.001
0.001
0.001
0.001
0.272
0.338
2.29
1.99
1.14
6.95
1.80
Coastal
coastal
Rye
11.39
7.58
0-06
1 0.09
1 0.00
0.09
2019
7,000
2,692
1.31
0.15
Queens Cam
G/D
0.005
0.005
0.039
0.005
0.000.
0.005
0.005
0.005
0.327
3.81
3.81
4.27
Coastal
Rye
23.59
2-39
0.06
2019
10,500
4,038
0.29
0.05
Sea Isk Plantation
G/D
0.000
0.000
0.013
0.003
0.000
0.000
0.001
0.000
0.071
0.79
1.44
Coastal
4.54
0.01
0.23
2019
7,000
2;692
1.65
0:19 15ouridofThestal
G/D
0.001
0.000
0.281
0.0,18
0.000
0.002
0.004
0.0021
0.619
3.23
6.51
Coastal
1851
1.10
0.00
2019
3,500
1,346
1.62
0.09
Stoare"Winds I
G/D.
0.000
0.000
0.097
0.003
0.000
0.001
0.002
0.001 1
0.355
7.25
6.59
Coastal
Rye
24.03
0.18
0.00
2019
3,50D
1,346
0.60
0.03
whaler inn
G/D
0.000
0.000
0.039
0.001
0-0001
0.000
0.000
0.0001
0.061
0.34 1
0.87
Coastat
1.61
0.01
Total
73,500
it
Annuallbs/acre 0.0140.012 1.485 0.059 0.001 0.019 0.027 0.0I8 3.494 34.57 I8.70 5526
Current Cumulative Ibs/acre 0.066 0.043 15.291 0.359 D.007 0.101 0214 0.097 20.812 299 50 Permit PAN Unit Ist/2nd Crop
Prior Years Cumulative Ibs/acre 0.052 0.032 13.806 0.300 0.006 O.OS2 0.187 0.078 17.319
Permitt C.P.L.R*** 136 34 1335 267 15 N/A 374 89- 2498
"I certify, under penalty of law, that this document ivas prepared under my directiortor supervision in accordance with asystem
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including.the possibility of finesand imprisonment for !mowing violations."
n
Lim
JApp.
Date
X &, � �''�G`'--�- '-;) /-l/�,y�..� !1 *Application Method: S - Surface, IN - Injection, INC - Incorporation
(Signature of land Applier) Date "Volatilization Rate: Surface - 0.5, Jnjectionnitcorporation -1.0
***C:P.L.R.: Cumulative Pollutant Loading Rate
WMSS, PLLC
DENR FORM FSF (7/2002) Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Barnes E.o*..vumw.,.&Prai Permit#: W00018525 Annual Dry Tans Applied: 5.07
Will Turner Operator. Steve Barnes Cation Exchange Capacity (non 503): 6.7
Site& WT Field 4- 6 Acres Utilized: 790 Acres Permitted: 2.90
Application Method": S Volatilization Rate--: 0.5 Mineralization Rate: 30
Predominant Soil Series: GoA
:: �. _.�
.::..»>...:.:.:..:...
siDxfe:�:
�.::rs•.a:::
$tEt
4' 9..:.:..
:[:iltre �;'si`#S`.:t
....
7..
1;-#:-:
-..,-......
t$c2e
:: ,� ".aE t:
. dt!.:.....
:s:iS4urce...
j:'Sittii
4'lond:
"tO:t:r':i0it?>:<�>iFii:2:Y�::-......:
.........:..::..
_..
it$tt77f:
:.::..:.
slacj
•.:
................
�.:.:..::
�::' � �:::::>i:::i:_
...
....::
4: �:::t: �::i::::::::::�
.... .:.
.........:.:::
:_ t::::>:::
:
...:.:.:..:
.......:..:::.:::s.::...>:.:.�
:>,ka::::::Glft;
t;t0"ict
atR6:.
x:F# •::
;a1io::•
a:Dz::::'xi
...
Mt
...
2019
3500
1207
0.88
0.04
Adanic Station
G/D
0.000
0.000
0.057
0.002
0.000
0.000
0.001
0.00o
0.099
0.20
2.49
c=w
423
1 0.03
0.00
2019
7.000
2,414
1.69
0.17
B.onm Rh
CdD
0,001
0.000
0.616
0.008
0.000
0.002
0.006
0.002
0.458
4,29
5.64
coanat
14.11
0.30
0.00
2019
7,000
2,414
.2AO
024
CCS.
G/D
0.004
0.004
0.334
0.004
0.000
0.004
0.004
0.004
0282
11.64
1126
Con i
Rye
37.06
2.16
0.09
2019
7,000
2.414
1.29
0.13
Hamp:an Soites
G/D
0.001
0.000
0162
OA01
0.000
0.001
0.002
0.001
0.123
2AB
2.49 .
2.52
Coasut
Rye
16.10
0.65
0.00
2019
14,000
1 4.828
1.23
1 025
Duooesyc
G/D
1 0:001
0.000
0309
0.006
0.000
0.002
0.004
0.002
0:415
5.65
5.65
7.87
Consul
Rye
3757
0.13
0,00
2019
35DO
1207
0.99
0.05
RinssbddswR
G/D
0.000
0.000
0.040
0.004
0.000
0.001
0.001
0.0001
0.660
1-73
2.68
tb,r.t
5.11.
0.06
0.18
2019
7,000
2414
1.91
0.19
McGinnis Point
G/D
0.001
1 0.000
0.775
0.014
0.000
0.002
'0004
0.002
0.461
f0.73
2115
consul
3529
052
0.04
2019
3500
1207
0.53
0.03
On. Curb
G/D
0.000
0.000
1 0.017
0.001
0.000
0.000
0.000
0,000
0.081
1.03
2.08
CmmW
3.40
0.02
0.00
2019
35,000
12,069
0.59
0.30
Pebbi.Beach
G/D
0.0011
0.001
0.120
0.007
0.000
0.003
0.006
0.003
0.632
1.3L
0.14
9.47
Comm
Rye
38.82
0.12
0.00
2019
3500
1207
1.31
0.07
Qooem Chun
G/D
0-OD2
0.002
0.019
002
0.000
0.002
0.002.
0.002
0.146
3.42
L91
Rye
1058
L07
0.03
2019
7.000
2.414
1.65
0.17
SoundOM.Sea
G/D
0.Wl
0.000
0252
0.016
O.00D
0.002
0.004
0.002
0.555
2.90
5.83
Rye
16.59
0.99
"0
2019
7.000
2,414
1.15
0.12
hwinds Condomi
G/D
0.001
0.000
0.175
0.003
0.000 1
0.001
0.002
0.001
.0,138
3.96
3.59
kw
13.01
0.29
0.00
Total
105,000
Annual lhs/acre 0.0I4 0.009 2.974 (068 0.001 0.021 0.037 0,021 4.150 27.42 30.19 78.49 _
Current Cumulative lbs/acre 0.078 .0.048 19.452 0.466 0.008 0.122 0.287 0.136 29.104 299 50 Permit PAN Lint Isd2nd Crop
Prior Years Cumulative lbs/acre 0.063 .0.039 16.478 0398 0.007 0.101 0."1 0.115 24.955
Perini C.P.L.IL*"" 36 34 1338 267 15 N/A 374 89 2498
"I certify, under penalty oflaw, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted Iam aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
n
Lime Ace.
Date ILWA,
X -,/. i / Z117 /..2112,Lz0 4Applicadon Method:S-Surface, IN - Injection, INC -lnroryoridon
(Signature of Land Applier) Date **Volatilization Rate: Surface-05, Injection&curpora ion- 1.0
*"C.P.L,R.: Cumulative.Pollmant Lending Rate
WMSS,.PLLC DENR FORM FSF (712002) Mod-

FIELD APPLICATION SUMMARIES

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG _
SEP
OCT
NOV
DEC
TOTALS
Corn
Rye
BARNES ENVIRONMENTAL WASTE
2019 FIELD APPLICATION SUMMARY FORM
Permi[ W00018525
FIELD WT-01 6.2 ACRES TOTAL GALLONS 84,000
arina
Plant can
Condos
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
tl
ttt
o0o
tl
o000000o
III
o
3,500
7,000
10,500
0
0
0
0
0
0
0
0
0
0
0
0
0
0
3,500
1 10,500
1 3,500
1 0
1 0
1 0
1 3,500
1 0
1 0
0
1 0
1 0
0
0
0
7,000
0
The
Grove
Ocean
Club
Ocean
Condos
Ocean
Terrace
Pebble
Beach
Peppertme
Resort
Pi
Knoll
Poin[
Emerald
Queens
Court
Sands
Villa
Sea Island
Plantation
Sea
Spray
Sound of
The Sea
Southwinds
Condos
Summer
Winds
Whaler lnn
3,500
7,000
3,500
3,500
3,500
10,500
3,500
3,500
7,000
0
3,500
0
0
0
0
3,500
0
7,000
7,000
3,500
7,000
0
0
10,500
3,500
0
3,500
0
0
0
0
3,500
0
3,500
0
0
7,000
0
0
10,500
3,500
0
0
0
0
0
0
0
0
3,500
7,000
3,500
0
0
0
0
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2019 FIELD APPLICATION SUMMARY FORM
Permit W00018525
FIELD WT-02 5.0 ACRES TOTAL GALLONS 80,500
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----
-----------
tt
o
Ott
o0o
tt
ttt
tt
o0000000
�. t t
o
t t t
o0o
t t
t t t
o0000000
-----------------
00000000000000000
----------------
Point
Enteral
Ilia
----------------
----------------
----------------
----------------
----------------
----------------
----------------
000
o00o
tt
t tt
o
tt
oo
t tt
o
0000000o
t t
t t t
o
t t t
oo
t t t
o
----------------
0000000000000000

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2019 FIELD APPLICATION SUMMARY FORM
Permit W00018525
FIELD WT-03 8.0 ACRES TOTAL GALLONS 115,500
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
111
III
---------------
-----------------
-----------------
-----------------
1 11
111
0000
11
I II
o00000000
� I II
,111
0000
11
I II
o00000000
-----------------
00000000000000000
The
Grove
Ocean
Club
Ocean
Condos
Ocean
Terrace
Pebble
Beach
Pepperlree
Resort
Pine
Knoll
Point
Emerald
Queens
Court
Sands
Villa
Sealsland
Plantation
Sea
Spray
Sound of
The Sea
South Winds
Condos
Summer
Winds
Whaler Inn
3,500
3,500
14,000
3,500
7,000
3,500
3,500
21,000
21,000
21,000
3,500
0
0
14,000
0
0
0
0
0
3,500
0
14,000
0
21,000
3,500
21,000
3,500
0
0
14,000
0
0
0
0
0
3,500
0
14,000
0
21,000
3,500
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2019 FIELD APPLICATION SUMMARY FORM
Permit W00018525
FIELD WT-05 2.6 ACRES TOTAL GALLONS 66,500
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
00
111
000
111
111
00000
11
00
11
00
11
000
111
111
00000
11
00
11
00
11
0000
000000000
The
Grove
Ocean
Club
Ocean
Condos
Ocean
Terrace
Pebble
Beach
Peppenree
Resort
Pine
Knoll
Poin[
Emerald
Queens
Court
Sands
Villa
Sea Island
Plantation
Peat
S m
Sound of
The Sea
Southwinds
Condos
Summer
Winds
Whaler Inn
3,500
3,500
7,000
3,500
7,000
3,500
3,500
3,500
3,500
3,500
3,500
0
10,500
0
0
0
0
0
3,500
7,000
0
10,500
0
7,000
0
3,500
3,500
0
7,000
0
0
0
0
0
3,500
3,500
0
10,500
0
7,000
0
0
3,500
0
3,500
0
0
0
0
0
0
3,500
0
0
0
0
0
3,500
0

JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS
Coastal
Rye
BARNES ENVIRONMENTAL WASTE
2019 FIELD APPLICATION SUMMARY FORM
Permit W00018525
FIELD WT-06 2.9 ACRES TOTAL GALLONS 98,000
Beacons
Reach
Cedar
1039M
-----------------
-----------------
--NO
i i
---------
-----------------
-----------------
-----------------
-----------------
-----------------
-----------------
tt
ttt
ttt
o0o
ttt
, ttt
o000o
tt
o
ttt
o
3,500
7,000
0
0
0
0
3,500
7,000
0
0
0
0
0
3,500
0
7,000
0
0
0
7,000
0
0
0
3,500
7,000
0
0
0
0
0
0
0
0
0
----------------
----------------
----------------
----------------
----------------
----------------
o
tt
oo
ttt
o0o
tt
o0o
ttt
o0
0
3,500
0
0
31,500
0
1 0
1 0
1 0
1 0
1 0
1 0
1 0
0
1 0
0
0
0
0
0
3,500
0
0
0 1
3,500
0
1 0
0
1 7,000
1 7,000
0
0

SOIL ANALYSIS REPORTS

All residual sources land applied by Barnes Environmental Waste and Hauling, Inc. (Barnes
Environmental) during the 2019 calendar year were lime stabilized to meet Pathogen and Vector
Attraction Reduction monitoring. Therefore lime additions are continually applied to the fields
throughout the year through land application.
The Sodium Adsorption Ratio (SAR) calculation for NC Aquarium at Pine Knoll Shores for 2019
was 15.06. Barnes Environmental contracted with Willcox & Mabe Soil Solutions, PLLC (WMSS)
to address this prior to land application occurring in 2019. With an anticipated total application of
only 3,500 gallons and considering that the biosolids were going to utilize alkaline stabilization to
meet Pathogen and Vector Attraction Reduction, WMSS did not anticipate any potential long term
effects of performing the land application. Land application was scheduled for October of 2019. It
should be noted that an additional 7,000 gallons of alkaline stabilized residuals were also land
applied to the same field within the same month of October from Kingsbridge II and Sea Island
Plantation. There was no crop loss after application or any visible symptoms of crop stunting. We
will continue to monitoring the crop/field in the future and make any necessary crop/soil
amendments if something occurs from this application.
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
Agronomist

Page 1 of 1
Report No: 20-052-0796
Account No: 08361
Advisor: Willcox & Mabe Soil Solutions, PLLC
7231 B. Summerfield Rd
Summerfield NC 27358
0
Waypoint..
ANALYTICAL
Client: Steve Barnes
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Farm:
Date Received: 02/21/2020
Date of Report: 02/24/2020
Lab No Field ID
Sample ID
Soil Class
HM% WN pH
Ac
P-1
K-1
S-1
Mn-1
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
03226
WT-01
MIN
0.6
5.7
0.5
200
12
21
100
75
75
125
2.4
81
61
15
1.6 0
Crop Recommendations:
1-Corn
Rec Uom
lb/acre
Lime (Nacre)
0.5
N
160
P2 05
0
KO
119
S
20
Mn
0
Mn-AI
81
Zn
0
Cu
0
B
1.5
Mg
0
Last Crop
03227
WT-02
MIN
0.8
6.4
0.5
239
8
29
31
95
95
370
5.9
91
83
7
1.0 0.1
Crop Recommendations:
1-Corn
Rec Uom
lb/acre
Lime (Nacre)
0.0
N
160
Pz 05
0
K20
129
S
20
Mn
0
Mn-AI
29
Zn
0
Cu
0
B
1.2
Mg
0
Last Crop
03228
WT-03
MIN
1.3
7.4
0.0
197
6
33
31
323
323
1125
10.8
101
95
5
0.7 0.1
Crop Recommendations:
1-Com
Rec Uom
lb/acre
Lime (Nacre)
0.0
N
160
P205
0
K20
134
S
20
Mn
10
Mn-AI
14
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03229
WT-05
MIN
0.6
7.7
0.0
275
6
31
31
543
543
520
8.3
100
94
5
0.5 0
Crop Recommendations:
1- Corn
Rec Uom
lb/acre
Lime (Nacre)
0.0
N
160
Pz 05
0
K20
134
S
20
Mn
10
Mn-AI
10
Zn
0
Cu
0
B
1.2
Mg
0
Last Crop
03230
WT-06
MIN
0.7
7.6
0.0
272
6
33
31
693
693
870
8.5
101
93
7
0.8 0.1
Crop Recommendations:
1-Corn
Rec Uom
lb/acre
Lime (Nacre)
0.0
N
160
P205
0
K20
134
S
20
Mn
10
Mn-AI
11
Zn
0
Cu
0
B
1.2
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/toocm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines. Analysis prepared by Waypoint Analytical Virginia, Inc.