HomeMy WebLinkAboutWQ0005135_Residual Annual Report 2019_20200225Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/25/2020
Received:*
Project Number* WQ0005135
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer Kendall.Williams@ncdenr.gov
Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Robert T. Branch
Email Address*
bbranch@branchrs.com
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0005135
ApplicantTermittee * von Drehle Corporation
Facility Name * von Drehle Corporation Class B
Phone Number*
336.312-9007
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Class B
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
vd_2019ar final.pdf 6.34MB
upload only 1 RDF document. NL@iple documents must be combined into one RDF file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/20/2020
2019 ANNUAL REPORT
VON DREHLE CORPORATION
CLASS B
CORDOVA, NORTH CAROLINA
PERMIT #WQ0005135
Prepared For:
Von Drehle Corporation
126 First Street
Cordova, North Carolina 28330
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
February 2020
BRANCH RESIDUALS & SOILS, LLC
8646 W. Market St. - Suite 111 • Greensboro, NC 27409
PHONE (336) 510-0340 • Fax (336) 510-0341
February 26, 2020
North Carolina Department of Environmental Quality
Division of Water Resource — Non -discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2019 LAND APPLICATION ANNUAL REPORT
Von Drehle Corporation
Cordova, North Carolina
Permit No. WQ0005135
Branch Residuals & Soils Project No. 2014-110
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Von Drehle Corporation. This data includes: 1) Certification Form, 2) Annual Residual
Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field
Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen and Vector Attraction
Reduction Forms, 8) Fecal and Salmonella Results, 9) Soils Lab Data, 10) 2019 Application Summary Table,
and 11) 2019 Application Condition Summaries.
Total production for 2019 was 59,495.35 wet tons for this facility. Disposal/applications were as follows:
• 11,186.31 wet tons being sent to the landfill,
• 22,860.19 wet tons sent for application in South Carolina under Belger farms permit
• 0.0 wet tons applied as Class A under separate permit, and
• 25,448.85 wet tons applied to the farms in North Carolina.
A total of 25,448.85 wet tons (9,228.29 dry tons) of residual by-product paper were land applied to the farms at
US and Hamlet (430 acres). Hamlet sites received 40 lbs/acre nitrogen topdressing in March 2019. The US-
1 site received 68 lbs/acres nitrogen in February 2019 from chicken litter for the millet crop. Millett was not
planted until September.
If any further information is required regarding this land application program, please do not hesitate to contact
me at (336) 312-9007.
Sincerely,
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Attachment
cc: Von Drehle Corporation
TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Form
II Annual Residual Sampling Summary Form
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction Forms
VIII Fecal and Salmonella Documentation and Results
IX Soil Analysis Reports
X 2019 Application Summary Table
XI 2019 Application Condition Summaries
CERTIFICATION FORM
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0005135 County: Richmond Year: 2019
Facility Name (as shown on permit): von Drehle Corporation
Land Application Operator: Belger Farms Phone: (803) 424-4731
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes Q No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals A lication Summary:
Total number of application fields in thepermit:
18
Total number of fields utilized for land application during the year:
18
Total amount of dry tons applied during the year for all application sites:
9,228.29
Total number of acres utilizes for land application during the year:
430.00
Part B - Annual Comuiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) Issued by the Division of Water Quality. ❑ Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations." /1-) 1--� r
Mr. Justin Dawkins, Cordova Plant Manager 1., 2 4 2 6 tl
Permittee ame and Title (type or print) Si ature of Perim ttee Date
0l•S--Zv
Signature of Preparer* Date
(if different from Permittee)
Signature of Land Applier
(if different from Permittee and Preparer)
Date
NONCOMPLIANCE ISSUES
Compliance for Part B Condition 7 — General Permit Requirements Crop Failure
The US-1 crop of Millet failed due to the late nature of the planting. Small Grain has been planted
at US-1 in January of 2020. Once this crop is harvested, an application will be made to US-1.
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0005135 Laboratory: 1)
Facility Name: von Drehle Corporation 2)
Residual Source WQ # or City of Rockingham 1UP #0015 3)
NPDES #: 4)
WWTP Name: Cordova Facility 5)
Residual Annlvsis Data
Microbac Labs
Parameter
(mg/kg)
Conc.
Limit
(mg/kg)a
Sample or Composite Date
1/8/2019
3/7/2019
5/6/2019
7/29/2019
9/9/2019
11/12/2019
Percent Solids (%)
NA
32.60
40.80
43.00
34.40
36.60
34.80
Arsenic
75
< 2.2
< 2.5
< 1.4
< 2.1
< 1.3
< 1.0
Cadmium
85
< 0.22
< 0.25
< 1.3
< 0.21
< 0.44
2.80
Copper
4,300
37.90
23.70
247.00
24.60
26.40
33.10
Chromium
NA
0.00
0.00
0.00
0.00
0.00
0.00
Lead
840
0.00
< 1.2
12.40
< 1.0
< 1.1
1.20
Mercury
57
0.02
< 0.015
0.02
0.01
< 0.61
0.02
Molybdenum
75
4.50
5.00
9.00
4.20
2.60
3.60
Nickel
420
2.80
1.40
18.60
1.20
1.60
1.40
Selenium
100
< 2.2
< 2.5
6.70
< 2.1
< 1.7
1.30
Zinc
7,500
73.10
65.80
597.00
97.90
53.10
135.00
Total Phosphorus
NA
15.00
50.00
2.20
29.00
3
72.00
TKN
NA
641.00
285.00
407.00
332.00
335
613.00
Ammonia -Nitrogen
NA
194.00
149.00
104.00
< 2.91
< 2.73
< 2.87
Nitrate and Nitrite
NA
< 2.282
< 4.34
< 14.52
< 16.11
< 19.05
< 3.09
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submittingose information, including the possibility of fines and imprisonment for knowing violations."
of PrenarK *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORMS
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual):
Permit #: W00005135 Cation Exchange Capacity (non 503 only):
Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
Acres Used: 23 Acres Permitted: 23 Site #: 3 Field #:
n/a
WcB
498.55
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-4 M B
mliMENNEEMENEEN
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
MIT, M,
Total
.
p•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including t ossibility of fines and imprisonment for knowing violations"
6& 2=7--
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual):
Permit #: WQ0005135 Cation Exchange Capacity (non 503 only):
Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
Acres Used: 9.1 Acres Permitted: 9.1 Site #: 3 Field #:
174.73
n/a
WcB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-4 MB
Total
Phos-
_phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
_phorusEENEENEENEENE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including a possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
18.9 Acres Permitted: 18.9 Site #: 3 Field #:
381.15
n/a
WcB
3A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-4 MB
Total
' •
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
_phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Q2� A 5-1 .2',
ignature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
37.2 Acres Permitted: 37.2 Site #: 3 Field #:
777.56
n/a
WcB
3B
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 20194 MB
Total
Phos-
phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
in
in
I
in
I
I
On-
VRW
TotalEmilio
Phos-
phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier
Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
13.2 Acres Permitted: 13.2 Site #:
261.99
n/a
WcB
Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 20194 MB
Total
Phos-
phorusEEEEEEEEEEEE
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
Phos-
phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual): 250.91
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
11.1 Acres Permitted: 11.1 Site #: 3 Field #:
n/a
WcB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-4 MB
Total
Phos-
phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
Phos-
phrusEEMENEEMENEEM.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
incittAing the possibility of fines and imprisonment for knowing violations"
-LO
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual):
Permit #: WQ0005135 Cation Exchange Capacity (non 503 only):
Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
Acres Used: 24.6 Acres Permitted: 24.6 Site #: 3 Field #:
484.69
n/a
WcB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-5 MB
6A
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
incluithe possibinlity of fines and imprisonment for knowing violations"
a,, Z
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
37.5 Acres Permitted: 37.5 Site #: 3 Field #:
679.09
n/a
WcB
6B
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 20194 MB 2019-5 MB
®
1 1
1 •
__-_---__-
Total
Phos-
phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
Phos-
�•
��
�.,
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includ" the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual): 480.76
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
19.1 Acres Permitted: 19.1 Site #: 4 Field #:
n/a
TbB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-2 MB
Total
' .E
. •
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inclu i g the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
37.1 Acres Permitted: 37.1 Site #: 4 Field #:
n/a
TbB
908.74
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-2 MB
•
Total
•E
• •
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
,•
,
••
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
incI d' g the ossibility of fines and imprisonment for knowing violations"
2— r-e a
Signature of Land Applier
Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
22.4 Acres Permitted: 22.4 Site #: 4 Field #:
554.17
n/a
TbA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-2 MB
•
Total
Phos-
_phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
• •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
i, -)--Za
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
50.8 Acres Permitted: 50.8 Site #: 4 Field #:
1,122.64
n/a
TbA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-1 MB 2019-2 MB
Total
' •
• •
ENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
WIT,
•
®
t
----------®
•
Total
Phos-
��
�:�
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including th ossibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
11.1 Acres Permitted: 11.1 Site #:
Field #:
280.20
n/a
TbA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
vd 2019-2 MB
Total
Phos-
phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
Phos-
_phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includi he possib*l' of tines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
18.9 Acres Permitted: 18.9 Site #: 4 Field #:
450.71
n/a
TbA
6A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-2 MB
' •
1
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
Phos-
phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includi he possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (712002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual):
Permit #: WQ0005135 Cation Exchange Capacity (non 503 only):
Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
Acres Used: 19.3 Acres Permitted: 19.3 Site #: 4 Field #:
461.87
n/a
TbA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-2 MB
6B
MIN
RUN --
Total
' •E
. •
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
Phos-
_phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includ"Jug the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual): 378.26
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
19.2 Acres Permitted: 19.2 Site #: 4 Field #:
n/a
TbA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-1 MB
Total
• •
—phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total00111111111111
Phos-
phorusEEMENEEMENEEM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
Author Darvl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
28.9 Acres Permitted: 28.9 Site #: 4 Field #:
558.62
n/a
TbA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-1 MB
Total
Phos-
__phorusEENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
Phos-
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includin he possibility of fines and imprisonment for knowing violations"
Signature of Land Applier
Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual):
WQ0005135 Cation Exchange Capacity (non 503 only):
von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series
28.6 Acres Permitted: 28.6 Site #: 4 Field #:
523.62
n/a
TbA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2019-1 MB
Total
Phos-
• •
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
10111111111111
OEM
Total
• .
1
•.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
1z - ?-0
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field summary
forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As —
Arsenic
Cd
— Cadmium
Cr —
Chromium
Cu
— Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se — Selenium
Zn —
Zinc
Nutrients (lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 498.55 Site #: I Acres Permitted:
Operator: von Drehle Corporation
Crop l Name: Rye
Predominat Soil Series
Crop 1 Max PAN: 80.00
WcB
Crop 2 Name
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
23.00
23.00
NA
#N/A
ol7
�'
CD 0
s
Specify
Totals
Per Acre
% Solids
As
Decimal
Volume
Applied per
Acre
DT. Ac
Residual Sources
(NPDES #. WQ#.
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry'
Wet'
Moist)
Prect p'
Past 24
Hrs.
Inches
a
K
r? �.
0 w_
°
<
w
* N
o
K
�'
w
CD
* o'
�
TKN
m g
z a
o o
?
W m k g
Nitrate
and
Nitrite
m &
PAN Applied
pp
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Jul-19
1,449.28
63.01
34.40
21.68
von Drehle Paper
INC
1.00
0.40
332
3
16
6.53
X
TOTALS:
63
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.09
0.01
0.00
1.07
0.04
0.00
0.18
0.05
0.09
4.24
1.26
6.53
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.42 2.22 NA 13.50 0.33 0.02 NA 2.60 0.45 38.34
0.33 2.21 NA 12.43 0.29 0.02 NA 2.55 0.35 34.10
36 34 NA 1.338 267 15 NA 374 89 2.498
80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate
FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 3 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 174.73 Site #: 2 Acres Permitted:
Operator: von Drehle Corporation
Crop 1 Name:
Predominat Soil Series
Crop 1 Max PAN: 80.00
WcB
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
9.10
9.10
NA
#N/A
oC7
W
� CD
� o
SDecify
Totals
Per Acre
u
/o Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #. WQ#.
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry.
Wet'
Moist)
Precip.
Past 24
Hrs.
Inches
o
� o
T.
c iv
* o•
o
w
N CD T
*
>
Fi w
*
* w
>
TKN
mg/kg
z a
3
o
C, ?
w
m g & g
Nitrate
and
Nitrite
m /k .
PAN Applied
(]bs/acre)
Must Select
Crop 1 of Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Jul-19
507.95
55.82
34.40
19.20
von Drehle Paper
INC
1.00
0.40
332
3
16
5.79
X
TOTALS:
56
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.08
0.01
0.00
0.94
0.04
0.00
0.16
0.05
1 0.08
3.76
1.11
5.79
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.27 0.06 NA 11.31 0.26 0.02 NA 1.62 0.46 29.82
0.19 0.05 NA 10.37 0.22 0.02 NA 1.57 0.38 26.06
36 34 NA 1.338 267 15 NA 374 89 2.498
80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit l st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
O� *Application Method: S - Surface, IN - Injection, INC - Incorporation
Z - _c� **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading R�tp
aDEIVR FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: 18.90
Owner: von Drehle Corporation Annual Dry Tons Applied: 381.15 Site #: 3A Acres Permitted: 18.90
Operator: von Drehle Corporation
Crop 1 Name: Rye
Predominat Soil Series
Crop 1 Max PAN: 80.00
WcB
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
NA
#N/A
l7
rD
o
Specify
Totals
Per Acre
u
/o Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste.
etc.)Wet.
Site
Cond.
(Dry'
Moist)
Precip.
Past 24
Hrs.
Inches
n
3 b
_
iv
* o
w
N
p"
=
w
;
TKN
mg/kg
z a
B
as o
g
mg/kg
Nitrate
and
Nitrite
,n ,
PAN Applied
pp
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet
Cu.Yd.
Report
Totals
in Gal.
Crop l
Crop 2
Crop 1
Crop 2
Jul-19
1 1,108.00
58.62
34.40
20.17
von Drehle Paper
INC
1.00
0.40
332
3
16
6.08
X
TOTALS:
59
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime Applied
Annuallbs/acre
0.08
0.01
0.00
0.99
0.04
0.00
0.17
0.05
0.08
3.95
1.17
6.08
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.47 0.06 NA 7.90 0.37 0.02 1 NA 0.97 0.51 21.14
0.39 0.05 NA 6.91 0.32 0.02 NA 0.92 0.42 17.19
36 1 34 1 NA 1.338 267 15 1 NA 374 89 2.498
80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit l st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loadingft
FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 777.56 Site #: 3B Acres Permitted:
Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN
37.20
37.20
NA
#N/A
C7
o
Specify
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT AC
Residual Sources
(NPDES #. WQ#.
Fert., Animal Waste.
etc.)
Site
Cond.
(D ry'
Wet'
Moist)
Precip.
Past 24
Hrs.
Inches
n
° iv
°
w
N
o'
°
�'
- W
�
TKN
m - g
z
0 o
g w
mg/kg
Nitrate
and
Nitrite
m dk
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Cro I
p
CCo 2
p
Crop l
p
Crop 2
p
Aug-19
2,260.35
60.76
34.40
20.90
von Drehle Paper
INC
1.00
0.40
332
3
16
6.30
X
TOTALS:
61
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.09
0.01
0.00
1.03
0.04
1 0.00
0.18
0.05
0.09
4.09
1 1.21
1 6.30
1 0.00
Date
lbs/ac
Current Cumulative Ibs/acre
0.51 0.06 NA 8.04 0.38 0.02 NA 0.99 0.52 22.71
0.42 0.05 NA 7.01 0.34 0.02 NA 0.94 0.44 18.62
36 34 NA 1 1.338 267 15 NA 374 89 2.498
r 80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate• Surface - 114 In•ection/Incor oration - 1 0
Signature of Land Applier
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.29
Date Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loadingft
FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 261.99 Site #: 4 Acres Permitted:
Operator: von Drehle Corporation
Crop 1 Name: Rye
Predominat Soil Series
Crop 1 Max PAN: 80.00
Wc13
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
13.20
13.20
NA
#N/A
o
CD
Specify
Totals
Per Acre
%Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #, WQ#.
Fert.. Animal Waste.
etc.)
Cond.
(Dry
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
�.
w
a o
w w
* N
°
3
w
TKN
m g/k g
z
o o
g
m g/k g
Nitrate
and
Nitrite
m
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wei Tons
Cu.Yd.
Report
Totals
in
in Gal.
1
Crop 2
Crop 1
Crop 2
Aug-19
761.60
57.70
34.40
19.85
von Drehle Paper
INC
1.00
0.40
332
3
16
5.98
X
TOTALS:
58
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.08
0.01
0.00
0.98
0.04
1 0.00
0.17
0.05
0.08
3.89
1.15
5.98
0.00
Date
Ibs/ac
Current Cumulative lbs/acre
0.42 0.96 NA 8.79 0.41 0.03 NA 1.26 1 0.53 34.53
0.34 0.95 NA 7.81 0.37 0.03 NA 1.21 0.45 30.65
36 34 NA 1.338 267 15 NA 374 89 2.498
80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2 r- Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Date Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 250.91 Site #: 5 Acres Permitted:
Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN
11.10
11.10
NA
#N/A
l7
CD
Specify
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT AC
Residual Sources
(NPDES #. WQ#,
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry
Wet.
Moist)
Precip.
Past 24
Hrs.
inches
K n
�.
° w
°
<
o
w
* N
o'
°
K
�'
m
* o'
o
TKN
mg/kg
z 3
�° o
g R.
w
m /k g
Nitrate
and
Nitrite
m ./k
PAN Applied
(lbs/acre)
Must Select
Crop I or Crop 2
Wei Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
p
[Cro 2
p
Crop 1
p
Crop 2
p
Aug-19
729.40
65.71
34.40
22.60
von Drehle Paper
INC
1.00
0.40
332
3
16
6.81
X
TOTALS:
66
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime A lied
Annuallbs/acre
0.09
0.01
0.00
1.11
0.05
0.00
0.19
0.05
0.09
4.43
1.31
6.81
0.00
Date
lbs/ac
Current Cumulative Ibs/acre
0.56 1.04 NA 10.78 0.42 0.02 NA 1.50 0.97 37.51
0.46 1.04 NA 9.67 0.37 0.02 NA 1.45 0.87 33.08
36 34 NA 1.338 267 15 1 NA 374 89 2.498
1 1 80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
(:��- Z **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 3 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 484.69 Site #: 6A Acres Permitted:
Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN
24.60
24.60
NA
#N/A
ol7
CD
Specify
Totals
Per Acre
a
/a Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #. WQ#.
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry
Moisi)
Precip.
Past 24
Hrs.
Inches
o
o
�.
o �_
* s'
M
<
2
w
» N
* ..
o'
>
K
5'
:e
w
*
o'
>
TKN
m lk g
z Y
B
o o
w
m Ac g
Nitrate
and
Nitrite
m
PAN Applied
pp
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Sep-19
1 1,324.29
53.83
36.60
19.70
von Drehle Paper
INC
1.00
0.40
335
3
19
6.10
X
TOTALS:
54
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
1PAN11PAN2
Lime Applied
Annuallbs/acre
0.05
0.02
0.00
1.04
0.04
0.02
1 0.10
0.06
0.07
2.09
0.13
6.10
0.00
Date
lbs/ac
Current Cumulative Ibs/acre
0.30 0.95 NA 7.53 0.36 0.04 NA 1.27 0.32 30.79
0.24 0.94 NA 6.49 0.32 0.02 NA 1.21 0.25 28.70
36 34 1 NA 1.338 267 15 NA 374 89 1 2.498
80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 679.09 Site #: 613 Acres Permitted:
Operator: von Drehle Corporation
Crop 1 Name: Rye
Predominat Soil Series
Crop 1 Max PAN: 80.00
WcB
Crop 2 Name
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
37.50
37.50
NA
#N/A
CJ
S ci
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #, WQ#,
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry.
Wet,
Moist)
Precip.
Past 24
Hrs.
Inches
o
K o
� �.
m
n o.
o
_:
w
N
« ?
_
5
w
w
TKN
m •n
z >
-;
�o o
m k
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
p
Totals
in Gal.
Crop 1[Crop
2
Crop I
Crop 2
Aug-19
1,738.66
46.36
34.40
15.95
von Drehle Paper
INC
1.00
0.40
332
3
16
4.81
X
Sep-19
221.30
5.90
36.60
2.16
von Drehle Paper
INC
1.00
0.40
335
3
19
0.67
X
TOTALS:
52
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN l
PAN 2
Lime Applied
Annuallbs/acre
0.07
0.01
0.00
0.90
0.04
0.00
1 0.15
0.05
0.07
3.35
0.94
5.47
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.30 0.94 NA 7.18 0.35 0.02 NA 1.23 0.32 30.57
0.22 0.94 NA 6.28 0.31 0.02 NA 1.19 0.24 27.22
36 34 NA 1.338 267 15 NA 374 89 2.498
80.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
.�- - S- - Z C.
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 19.10
Owner: von Drehle Corporation Annual Dry Tons Applied: 480.76 Site #: I Acres Permitted: 19.10
Operator: von Drehle Corporation Predominat Soil Series TbB Cation Exchange Capacity (non 503): NA
Crop 1 Name: Millett Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A
ol7
CD
s
Svecifv
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT AC
Residual Sources
(NPDES #. WQ#.
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry
t.
Moist )
Precip.
Past 24
Hrs.
Inches
�
3 v
�.
° w_
°
m W
* N
o
5
z C
"
'o
o
TKN
mg/kg
z Y
a0 o
g R.
mg/kg
Nitrate
and
Nitrite
m L/k
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop
Ticrop 2
Crop 1
Crop 2
Mar-19
1,178.33
61.69
40.80
25.17
von Drehle Paper
INC
1.00
0.40
285
149
4
10.46
X
TOTALS:
62
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.13
0.01
0.00
1.19
0.06
0.00
0.25
0.07
1 0.13
3.31
2.52
10.46
1 0.00
Date
Ibs/ac
Current Cumulative lbs/acre
0.64 0.22 NA 4.59 0.33 0.08 NA 1.20 1.04 21.30
0.51 0.21 NA 3.40 0.27 0.07 1 NA 1.13 0.92 1 17.99
36 1 34 NA 1.338 267 15 1 NA 374 89 2.498
1 100.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant LoadingDW
FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 908.74 Site #: 2 Acres Permitted:
Operator: von Drehle Corporation
Crop 1 Name:
Millett
Predominat Soil Series
Crop 1 Max PAN: 100.00
TbB
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
37.10
37.10
NA
#N/A
ol7
CD
S ci
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #, WQ#.
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry,
Moist )
Precip.
Past 24
Hrst..
Inches
b
K "S
�.
w
M
0
w -
N
o
9
z
g s
TKN
m k g
z Y
B
o0 o
w
m /k g
Nitrate
and
Nitrite
m
PAN Applied
(lbs/acre)
Must Select
Crop l or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop l
Crop 2
Crop 1
Crop 2
Mar-19
2,227.31
60.04
40.80
24.49
von Drehle Paper
INC
1.00
0.40
285
149
4
10.18
X
TOTALS:
60
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.12
0.01
0.00
1.16
0.06
1 0.00
0.24
0.07
0.12
3.22
2.45 1
10.18
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.49 0.17 NA 4.88 0.38 0.08 NA 0.94 1.03 20.80
0.37 0.15 NA 3.72 0.32 0.08 NA 0.87 0.90 17.58
36 34 NA 1.338 267 15 NA 374 89 2.498
LEE
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Ste- *Application Method: S - Surface, IN - Injection, INC - Incorporation
o **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate
DEM FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: 22.40
Owner: von Drehle Corporation Annual Dry Tons Applied: 554.17 Site #: 3 Acres Permitted: 22.40
Operator: von Drehle Corporation Predominat Soil Series TbA Cation Exchange Capacity (non 503): NA
Crop 1 Name: Milieu Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A
O
O CD
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT AcMoist)
Residual Sources
(NPDES #. WQ#,
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry
Wet.
Precip.
Past 24
Hrs.
Inches
v
s �.
w_
*
0
_:
NPO
o
3
w
TKN
m ,/k g
Z
a0 o
M w
mg/kg
Nitrate
and
Nitrite
m
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Mar-19
1,358.27
60.64
40.80
24.74
von Drehle Paper
INC
1.00
0.40
285
149
4
10.28
X
TOTALS:
61
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.12
0.01
0.00
1.17
0.06
0.00
1 0.25
0.07
0.12
3.26
2.47
10.28
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.25 0.07 NA 4.56 0.26 0.04 NA 0.77 0.39 13.98
0.13 0.05 NA 3.39 0.20 0.04 NA 0.70 0.27 10.72
36 34 NA 1.338 267 15 NA 1 374 89 2.498
1 100.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C�� *Application Method: S -Surface, IN -Injection, INC - Incorporation
Zd **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 1.122.64 Site #: 4 Acres Permitted:
Operator: von Drehle Corporation
Crop 1 Name: Millett
Predominat Soil Series _
Crop 1 Max PAN: 100.00
TbA
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
50.80
50.80
NA
#N/A
C7
o
Specify
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT AC
Residual Sources
(NPDES #, WQ#,
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry.
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
3 o
�.
a m
0
_:
* N
* o'
o
S*
z CD
w
* o'
o
TKN
m .n; g
Z a
-; B
�o o
?
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
pp
(Ibs/acre)
Must Select
Crop 1 or Crop 2
we�Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Feb-19
2,134.51
42.02
32.60
13.70
von Drehle Paper
INC
1.00
0.40
641
194
2
10.28
X
Mar-19
1,046.06
20.59
40.80
8.40
von Drehle Paper
INC
1.00
0.40
285
149
4
3.49
X
TOTALS:
63
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.10
0.01
0.00
1.44
0.02
0.00
1 0.21
0.10
0.10
3.11
1.25
13.77
1 0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.46 0.15 NA 6.08 0.40 0.07 NA 1.27 0.46 23.11
0.36 0.14 NA 4.64 0.38 0.07 NA 1.17 0.36 20.00
36 1 34 1 NA 1 1.338 1 267 15 NA 374 89 1 2.498
100.00
Prior Years Cumulative Ibs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2 i _ *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate
DENR FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 280.20 Site #: 5 Acres Permitted:
Operator: von Drehle Corporation
Crop I Name: Millett
Predominat Soil Series
Crop I Max PAN: 100.00
TbA
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
11.10
11.10
NA
#N/A
ol7
Specify
Totals
Per Acre
o
/o Solids
AS
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #, WQ#.
Fert., Animal Waste,
etc. )
Site
Cond.
(D
(Dry-
Wet.
Moist)
precip.
Past 24
Hrs.
Inches
n
3CD
?
w_
a
w w
* N
°
w
* o'
o
TKN
m g/k g
z
o o
m g/k g
Nitrate
and
Nitrite
m g/k
PAN Applied
(lbs/acre)
Must Select
Crop I or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Cro 1
p
Cro 2
p
Crop I
p
Crop 2
p
Mar-19
686.76
61.87
40.80
25.24
von Drehle Paper
INC
1.00
0.40
285
149
4
10.49
X
TOTALS:
62
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.13
0.01
0.00
1.20
1 0.06
0.00
1 0.25
0.07
1 0.13
3.32
2.52
10.49
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.40 0.98 NA 6.50 0.30 0.05 NA 1.50 0.63 22.68
0.27 0.97 NA 5.30 0.24 0.05 NA 1.43 0.51 19.36
36 34 NA 1.338 267 15 NA 374 89 2.498
loo.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
2 - 5 = zo
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 450.71 Site #: 6A Acres Permitted:
Operator: von Drehle Corporation
Crop 1 Name: Millett
Predominat Soil Series _
Crop l Max PAN: 100.00
TbA
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
18.90
18.90
NA
#N/A
El
K C7
o ?;
rD
Specify
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT Ac
Residual Sources
(NPDES #. WQ#.
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry'
Wet'
Moist)
Precip.
Past 24
Hrs.
inches
a
� -a
�
0 w
ca.a.
<
�
_:
w
* N
* F '
o
M
K
z �'
w
N
* w
TKN
mg/kg
Z 3
0 o
o
g
COM
mg/kg
Nitrate
and
Nitrite
m
PAN Applied
(Ibs/act'e)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Mar-19
1,104.69
58.45
40.80
23.85
von Drehle Paper
INC
1.00
0.40
285
149
4
9.91
X
TOTALS:
58
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.12
0.01
0.00
1.13
0.06
0.00
0.24
1 0.07
0.12
3.14
1 2.38
1 9.91
1 0.00
Date
Ibs/ac
Current Cumulative lbs/acre
0.71 1.10 NA 5.64 0.29 0.05 NA 1.43 1.06 21.03
0.59 1.09 NA 4.51 0.23 0.05 NA 1.36 0.94 17.89
36 34 NA 1 1.338 267 15 NA 374 89 2.498
1 100.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C " Z� - �?,, -
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate
DEW FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: 19.30
Owner: von Drehle Corporation Annual Dry Tons Applied: 461.87 Site #: 613 Acres Permitted: 19.30
Operator: von Drehle Corporation Predominat Soil Series TbA Cation Exchange Capacity (non 503): NA
Crop 1 Name: Millett Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A
� 0 �
CD
ci
Totals
Per Acre
a
/a Solids
As
Decimal
Volume
Applied per
Acre
DT/AC
Residual Sources
(NPDES #. WQ#,
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry.
Wet'
Moist)
Precip.
Past 24
Hrs.
inches
o
� o
�.
° m
°
w =
w
+ N
o'
w w
_
o'
=
TKN
I mg/kg
z >
o �
°
°
m w l g
Nitrate
and
Nitrite
ing/kg
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
WetTons
Cu.Yd.
Report
Totals
in Gal.
Crop
Ticrop 2
Crop l
Crop 2
Mar-19
1,132.03
58.65
40.80
23.93
von Drehle Paper
INC
1.00
0.40
285
149
4
9.94
X
TOTALS:
59
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.12
0.01
0.00
1.13
0.06
0.00
0.24
0.07
0.12
3.15
2.39
9.94
1 0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.75 1.10 NA 5.70 0.29 0.05 NA 1.49 1.06 22.77
0.63 1.09 NA 4.56 0.24 0.05 NA 1.42 0.94 19.62
36 34 NA 1 1.338 267 15 NA 374 89 2.498
100.00
Prior Years Cumulative Ibs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C, I? "I I � � 11 -
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 378.26 Site #• 7 Acres Permitted:
Operator: von Drehle Corporation Predominat Soil Series TbA Cation Exchange Capacity (non 503):
Crop 1 Name: Millett Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN
19.20
19.20
NA
#N/A
o
CD
o
Specify
To.
Per Acre
% Solids
As
Decimal
Volume
Applied per
Acre
DT AC
Residual Sources
(NPDES #. WQ#.
Fert.. Animal Waste.
etc.)
Cond.
(Dry.
Wet'
Moist)
Precip.
Past 24
Hrs.
Inches
K �
n.
m
* o•
w
N
w
w
*
* °=
=1
TKN
mgfkg
Z >
0CD Go o
CD
w
mg/kg
Nitrate
and
Nitrite
m ,
PAN Applied
(Ibs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Cr op 2
Crop 1
Crop 2
Feb-19
1 1,160.31
60.43
32.60
19.70
von Drehle Paper
INC
1.00
0.40
641
194
2
14.78
X
TOTALS:
60
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN ].PAN
2
Lime Applied
Annuallbs/acre
0.09
0.01
0.00
1.49
0.00
0.00 1
0.18
0.11
1 0.09
2.88
0.59
14.78
0.00
Date
Ibs/ac
Current Cumulative lbs/acre
0.43 1.01 NA 6.54 0.21 0.04 NA 1.28 0.94 19.85
0.34 1.00 NA 5.05 0.21 0.04 NA 1.17 0.85 16.97
36 34 NA 1.338 267 15 NA 374 89 2.498
1 100.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
- r -
Date
2 *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading
Rasp
aDENR FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 558.62 Site #: 8 Acres Permitted:
Operator: von Drehle Corporation
Crop 1 Name:
Millett
Predominat Soil Series
Crop 1 Max PAN: 100.00
TbA
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
28.90
28.90
NA
#N/A
o
Specify
Totals
Per Acre
o
/o Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #. WQ#.
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry,
Wet'
Moist)
Precip.
Past 24
Hrs.
inches
n
� v
� A.
° °_
°
m -
* N
o'
�
- w
* o'
o
TKN
m �
z >
a0 o
°
m �
Nitrate
andCD
Nitrite
mgtkg
PAN Applied
(Ibs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Jan-19
1,713.55
59.29
32.60
19.33
von Drehle Paper
INC
1.00
0.40
641
194
2
14.50
X
TOTALS:
59
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.09
0.01
0.00
1.47
1 0.00
0.00
0.17
0.11
0.09
2.83
0.58
1 14.50
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.45 1.02 NA 6.58 0.21 0.05 1 NA 1.64 0.92 21.96
0.36 1.01 NA 5.12 0.21 0.05 NA 1.53 0.83 19.13
36 34 NA 1.338 267 15 NA 374 89 2.498
1 100.00
Prior Years Cumulative Ibs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
- r- ZC.121
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized:
Owner: von Drehle Corporation Annual Dry Tons Applied: 523.62 Site #: 9 Acres Permitted:
Operator: von Drehle Corporation
Crop I Name:
Millett
Predominat Soil Series
Crop I Max PAN: 100.00
TbA
Crop 2 Name:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
28.60
28.60
NA
#N/A
3
o ?;
fD
Totals
Per Acre
o
/a Solids
As
Decimal
Volume
Applied per
Acre
DT AC
Residual Sources
(NPDES #, WQ#,
Fert.. Animal Waste.
etc.)
Site
Cond.
(Dry
Mois[ )
Precip.
Past 24
Hrs.
Inches
.o
3
�.
w
*
_:
w w
* N
3
� w
*
* o'
M
TKN
m k
z 3
.;
M o
g w
mg/kg
Nitrate
and
Nitrite
m /k
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop
T1Crop 2
Crop 1
Crop 2
Jan-19
1,606.20
56.16
32.60
18.31
von Drehle Paper
INC
1.00
0.40
641
194
2
13.73
X
TOTALS:
56
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.08
0.01
0.00
1.39
0.00
0.00
0.16
0.10
1 0.08
2.68
0.55
1 13.73
1 0.00
Date
I lbs/ac
Current Cumulative lbs/acre
0.54 1.04 NA 5.81 0.18 0.05 NA 1.41 0.95 21.47
0.46 1.03 NA 4.42 0.18 0.05 NA 1.30 0.86 18.79
36 34 1 NA 1 1.338 1 267 15 NA 374 89 1 2.498
1 100.00
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading
DEWR FORM FSF (12/2006)
RESIDUAL ANALYSIS LAB SHEETS
Facility:
von Drehle Corporation
Source:
von Drehle Paper
Location:
Cordova, North Carolina
Contractor:
Belger Farms
Type of Analysis:
Industrial
Report No:
vd 2019-1 MB
Date Sampled:
1/8/2019
Date Reported:
1/22/2019
Reporting Period:
Jan- Feb 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
32.60
Nitrogen (TKN)
0.064
641.000
Phosphorus
0.002
15.000
Potassium
0.109
1,090.000
Sulfate
0.000
Calcium
20.000
200,000.000
Magnesium
0.248
2,480.000
Sodium
0.109
1,090.000
Iron
---
Aluminum
---
1,850.000
Manganese
---
Copper
---
37.900
1,500
Zinc
---
73.100
2,800
Ammonia Nitrogen
0.019
194.000
Nitrate N / Nitrite N
---
2.2820
Cadmium
---
0.2200
39
Chromium
---
1,200
Nickel
---
2.8000
420
Lead
---
300
Arsenic
---
2.2000
41
Mercury
---
0.0170
17
Selenium
---
2.2000
100
pH
7.200
Calcium Carbonate Eq.
0.000
Organic Nitrogen
0.045
Molybdenum
---
4.5000
75
Chloride
---
Boron
Available P2O5
(�DMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0098
Von Drehle Corporation Project Name: Residuals Sample - 60 day
Mr. Chris Fowler Project / PO Number: N/A
126 First Street Received: 01/08/2019
Cordova, NC 28330 Reported: 01/22/2019
Analytical Testing Parameters
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Lab Sample ID: K9A0098-01
Method: Calculation
Plant Available Nitrogen
Method: EPA 300.0, Rev. 2.1 (1993)
Nitrate as N
Nitrite as N
Method: SM 2540 G-2011
% Solids
Method: SM 4500 NH3 C-2011
Ammonia as N
Method: SM 4500-Norg C-2011
Total Kjeldahl Nitrogen
Wet Chemistry
Method: Calculation
Sodium Adsorption Ratio, SAR
Method: EPA 9045 D
pH at 25 °C
Method: SM 4500 P F-2011
Phosphorus, Total (as P)
7471E
Method: 7471 B
Mercury
Result RL Units
231 mg/kg
Collected By: Wright
Collection Date: 01 /08/2019 11:45
Note Prepared Analyzed Analyst
01/21/19 1200 01/21/19 1201 JMO
<0.762
0.762
mg/kg dry wt.
dry
<1.52
1.52
mg/kg dry wt.
dry
32.6
1.00
%
194
3.07
mg/kg dry wt.
Y
dry
641
1.53
mg/kg dry wt.
dry
Result
RL
Units
Note
0.470
mg/kg
7.2
1.0
pH Units
H
is
0.77
mg/kg dry wt.
dry
Analyses Subcontracted to: Pace Analytical
Result
RL
Units
Note
0.017
0.0097
mg/kg dry wt.
01/09/19 1130 01/09/19 1516 DSK
01/09/19 1130 01/09/19 1516 DSK
01/09/19 1114 MT
01/10/19 1057 MT
01/09/19 0833 TAB
Prepared Analyzed Analyst
01/21/19 1155 01/21/19 1155 JMO
01/09/19 1101 DSK
01/10/19 1439 01/10/19 1154 DSK
Prepared Analyzed Analyst
01/15/19 0000 DS
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 5
VMICROBAC'
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0098
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Lab Sample ID: K9A0098-01
Collected By: Wright
Collection Date: 01/08/2019 11:45
SPLP Metals
Result
RL
Units
Note Prepared Analyzed
Analyst
Method: SW-846 6010E
Aluminum
1850
21.8
mg/kg dry wt.
01/15/19 0000
DS
Arsenic
<2.2
2.2
mg/kg dry wt.
01/15/19 0000
DS
Cadmium
<0.22
0.22
mg/kg dry wt.
01/15/19 0000
DS
Calcium
200000
1090
mg/kg dry wt.
01/15/19 0000
DS
Copper
37.9
1.1
mg/kg dry wt.
01/15/19 0000
DS
Magnesium
2480
21.8
mg/kg dry wt.
01/15/19 0000
DS
Molybdenum
4.5
1.1
mg/kg dry wt.
01/15/19 0000
DS
Nickel
2.8
1.1
mg/kg dry wt.
01/15/19 0000
DS
Potassium
<1090
1090
mg/kg dry wt.
01/15/19 0000
DS
Selenium
<2.2
2.2
mg/kg dry wt.
01/15/19 0000
DS
Sodium
<1090
1090
mg/kg dry wt.
01/15/19 0000
DS
Zinc
73.1
2.2
mg/kg dry wt.
01/15/19 0000
DS
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL: Minimum Detection Limit
RL: Reporting Limit
Y: This analyte is not on the laboratory's current scope of accreditation.
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
1 2l"Lx-e— �tiPiLdi �
Jeanne Overstreet
Client Relationship Specialist, Environmental
Reported: 01/22/2019 09:09
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 5
Fayetteville Division 2592 Hope Mills Road -- Fayetteville, NC 28306 (910) 864-1920 / 86
CHAIN OF CUSTODY RECORD
*K9A0098*
CLIENT NAME BADDRESS*
VonDrehle Corp.
126 First Street
Cordova, NC 28330
PO#
PROJECT/LOCATION:
Cordova - 60-day series
#OF
B
0
T
T
L
E
TYPE OF
ANALYSIS
PRESERVATION CODE
E
U
E
E
Q
N
a)C
U)
U
Q
�,
C
U
2
U
N
0
.J
in
I0
Z
_
O
N
CO
O
+
o
,M
Z
Z
o_
O
ZC
a
)—
Q
7E5
U)
r;!S
CODE: A = None
B = HNO3 (pH<2) + <4°C
C = H2SO4 (pH<2) + <4°C
D= NaOH + <4°C
E= ZN Acetate + <4°C
F = HCI
CONTACT PERSON:
Mr. Chris Fowler
PHONE:
910-410-9131
SAMPLER:
DATE 1 METHOD OF SHIPMENT:
Microbac
LAB ID #
SAMPLE
TYPE
DATE
TIME
COMP
GRAB
PH
D.O.
TEMP'C
CHLORINE
Residual from paper plant
1 /7 ,
X
2
A
A
A
A
A
A
A
A
A
Z
Relinquf;sW jb :
Date
Time
Received by: (Signature)
Date
Time
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
3
4
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
5
6
Comments or Special Hazards:
REVIEWED
I
Page 3 of 5
Microbac Laboratories,
Inc. - Fayetteville
�_
i i "(.) I °
y
SUBCONTRACT ORDER
SENDING LABORATORY: RECEIVING LABORATORY:
Microbac Laboratories, Inc. - Fayetteville Pace Analvtical
2592 Hope Mills Rd 9800 Kincey Ave., Suite 100
Fayetteville, NC 28306 Huntersville, NC 28078
Phone: 910.864.1920 Phone: -
Project Manager: Jeanne Overstreet
Proiect Info:
Project Type: ENV-DrinkingWaterNonRe Report TAT: 7
Project Location: North Carolina Due: 01/17/2019 17:00
Sample ID: K9A0098-01 Matrix: Solid Sampled: 01/08/2019 11:45
Analysis Method Analysis Due Expires
v
6010D
SW-846 6010B
Aluminum
Arsenic
5
mg/kg dry
mg/kg dry
0.5
mg/kg dry ftmj�
0.25
mg/kg dry
eampl
0.05
mg/kg dry
0.017
mg/kg dry
ftamm
Calcium
2.5
mglkg dry Cadmium ✓
0.05
mg/kg dry
5
mg/kg dry
0.1
mg/kg dry
fiiitil■ill■�
Copper
0.25
mg/kg dry 4foJEW
0.25
mg/kg dry
0.25
mg/kg dry dMidn
0.1
mg/kg dry
V✓
Lead
0
mg/kg dry thimM
5
mg/kg dry
0.25
mg/kg dry
0.0104
mg/kg dry
V
✓�+�
Magnesium o `I`
b
0.25
mg/kg dry HUMNION0=9
0.25
mg/kg dry
/
0.25
mg/kg dry Nickel ✓
0.25
mg/kg dry
0.72
mg/kg dry glillMopomMS
0.0157
mg/kg dry
0
mg/kg dry Potassium
500
mg/kg dry
v
Selenium
0.5
mg/kg dry amp""Ple
1.26
mg/kg dry
umfilff�
5
mg/kg dryer
0.25
mg/kg dry
Sodium
250
mg/kg dry 111molOW
0.25
mg/kg dry
smawlimme
0.05
mg/kg dryer
0.5
mg/kg dry
611111111ft
0.0036
mg/kg dry
0.25
mg/kg dry
0.1
mg/kg dry
0.25
mg/kg dry
�U&M1110rr
Zinc
0.5
mg/kg dryer
0.1
mg/kg dry
all metals this method
IN ?, A I K fJ I
Released By
Date
ncccivcu ny
Received By
Date
l"i
Page4of5
0
Microbac Laboratories,
Inc. - Fayetteville
SUBCONTRACT ORDER
K9A0098
SENDING LABORATORY: RECEIVING LABORATORY:
Microbac Laboratories, Inc. - Fayetteville Pace Analytical
2592 Hope Mills Rd 9800 Kincey Ave., Suite 100
Fayetteville, NC 28306 Huntersville, NC 28078
Phone: 910.864.1920 Phone: -
Project Manager: Jeanne Overstreet
Proiect Info:
Project Type: ENV-DrinkingWaterNonRe Report TAT: 7
Project Location: North Carolina Due: 01/17/2019 17:00
Sample ID: K9A0098-01 Matrix: Solid Sampled: 01/08/2019 11:45
Analysis Method Analysis Due Expires
6010D
SW-846 6010B
Vl
Aluminum
Arsenic
5 mg/kg dry 4hn1mgqft
U.4iU
mg/kg dry
0.5 mg/kg dry Qmj�
0.25
mg/kg dry
wompow"
0.05 mg/kg dry &EMAND
0.017
mg/kg dry
V
��
Calcium
2.5 mg/kg dry Cadmium ✓
0.05
mg/kg dry
5 mg/kg dry Iftift
0.1
mg/kg dry
f Weimm
Copper
0.25 mg/kg dry gJ@WM
0.25
mg/kg dry
0.25 mg/kg dry db6ft
0.1
mg/kg dry
V
Lead
0 mg/kg dryftn�
5
mg/kg dry
0.25 mg/kg dry
0.0104
mg/kg dry
V
Magnesium ` r
Mp�\I E WV1^
0.25 mg/kg dry
0.25
mg/kg dry
0.25 mg/kg dry Nickel ✓
0.25
mg/kg dry
0.72 mg/kg dry
0.0157
mg/kg dry
0 mg/kg dry Potassium
500
mg/kg dry
Selenium
0.5 mg/kg dry OWN""
1.26
mg/kg dry
Sodium
5 mg/kg dryer
0.25
mg/kg dry
�t
250 mg/kg dry qlomMft
0.25
mg/kg dry
0.05 mg/kg dry Nftdh�
0.5
mg/kg dry
0.0036 mg/kg dry 011111MEW
0.25
mg/kg dry/
0.1 mg/kg dry
0.25
mg/kg dry
V
Zinc
0.5 mg/kg dryer
0.1
mg/kg dry
all metals this method
i1-p- 1- e u. lr H
°7 q 7 1 /3
Released By
Date
by
Received By
Date -
Date
Page 5of5
Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
von Drehle Corporation
von Drehle Paper
Cordova, North Carolina
Belger Farms
Industrial
vd 2019-2 MB
3/7/2019
3/22/2019
March -April 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
40.80
Nitrogen (TKN)
0.029
285.000
Phosphorus
0.005
50.000
Potassium
0.123
1,230.000
Sulfate
0.000
Calcium
19.300
193,000.000
Magnesium
0.195
1,950.000
Sodium
0.123
1,230.000
Iron
---
Aluminum
---
1,850.000
Manganese
---
Copper
---
23.700
1,500
Zinc
---
65.800
2,800
Ammonia Nitrogen
0.015
149.000
Nitrate N / Nitrite N
---
4.3400
Cadmium
---
0.2500
39
Chromium
---
1,200
Nickel
---
1.4000
420
Lead
---
1.2000
300
Arsenic
---
2.5000
41
Mercury
---
0.0150
17
Selenium
---
2.5000
100
pH
7.500
Calcium Carbonate Eq.
0.000
Organic Nitrogen
0.014
Molybdenum
---
5.0000
75
Chloride
---
Boron
Available P2O5
&�MICROBAC-
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9C0100
Von Drehle Corporation Project Name: Residuals Sample - 60 day
Mr. Chris Fowler Project / PO Number: N/A
126 First Street Received: 03/07/2019
Cordova, NC 28330 Reported: 03/22/2019
Analytical Testing Parameters
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Lab Sample ID: K9C0100-01
Method: Calculation
Plant Available Nitrogen
Method: EPA 300.0, Rev. 2.1 (1993)
Nitrate as N
Nitrite as N
Method: SM 2540 G-2011
% Solids
Method: SM 4500 NH3 C-2011
Ammonia as N
Method: SM 4500-Norg C-2011
Total Kjeldahl Nitrogen
Wet Chemistry
Method: Calculation
Sodium Adsorption Ratio, SAR
Method: EPA 9045 D
pH at 25 °C
Method: SM 4500 P F-2011
Phosphorus, Total (as P)
SPLP Metals
Method: EPA 7471 B
Mercury
Method: SW-846 6010E
Result
RL
Units
118
mg/kg
3.12
0.610
mg/kg dry wt.
dry
<1.22
1.22
mg/kg dry wt.
dry
40.8
1,00
°f,
149
285
Result
5.41
7.5
Collected By: Brown
Collection Date: 03/07/2019 11:56
Note Prepared Analyzed Analyst
03/22/19 1430 03/22/19 1431 JMO
2.45 mg/kg dry wt. Y
dry
1.23 mg/kg dry wt.
dry
RL Units Not
mg/kg
1.0 pH Units H
50 0.61 mg/kg dry wt.
dry
Analyses Subcontracted to: Pace Analytical ( Huntersville)
Result RL Units Note
<0.015 0.015 mg/kg dry wt.
03/12/19 1102 03/12/19 1505 DSK
03/12/19 1102 03/12/19 1505 DSK
03/11/19 1322 MT
03/08/19 0913 MT
03/12/19 0839 DC
Prepared Analyzed Analyst
03/22/19 1423 03/22/19 1425 JMO
03/15/19 1433 CLB
03/15/19 1219 DSK
Prepared Analyzed Analyst
03/15/19 0000 KDF
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 3
(5)MICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9C0100
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Lab Sample ID: K9C0100-01
Collected By: Brown
Collection Date: 03/07/2019 11:56
SPLP Metals
Result
RL
Units
Note Prepared Analyzed
Analyst
Aluminum
1850
24.5
mg/kg dry wt.
03/15/19 0000
KDF
Arsenic
<2.5
2.5
mg/kg dry wt.
03/15/19 0000
KDF
Cadmium
<0.25
0.25
mg/kg dry wt.
03/15/19 0000
KDF
Calcium
193000
491
mg/kg dry wt.
03/15/19 0000
KDF
Copper
23.7
1.2
mg/kg dry wt.
03/15/19 0000
KDF
Lead
<1.2
1.2
mg/kg dry wt.
03/15/19 0000
KDF
Magnesium
1950
24.5
mg/kg dry wt.
03/15/19 0000
KDF
Molybdenum
5
1.2
mg/kg dry wt.
03/15/19 0000
KDF
Nickel
1.4
1.2
mg/kg dry wt.
03/15/19 0000
KDF
Potassium
<1230
1230
mg/kg dry wt.
03/15/19 0000
KDF
Selenium
<2.5
2.5
mg/kg dry wt.
03/15/19 0000
KDF
Sodium
<1230
12230
mg/kg dry wt.
03/15/19 0000
KDF
Zinc
65.8
2.5
mg/kg dry wt.
03/15/19 0000
KDF
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL: Minimum Detection Limit
RL: Reporting Limit
Y: This analyte is not on the laboratory's current scope of accreditation.
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
Report Comments
North Carolina DENR NPDES
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet
in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental
Reported: 03/22/2019 15:15
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 3
I,,.._,. _ Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 8F
CHAIN OF CUSTODY RECORD
*K9C0100*
CLIENT NAME BADDRESS:
VonDrehle Corp.
126 First Street
Cordova, NC 28330
PO#
PROJECT/LOCATION:
Cordova - 60-day series
#OF
B
O
T
T
L
E
s
TYPE OF
ANALYSIS
PRESERVATION CODE
E
�
E
N
V
E
c
�
Q
(q
U
`
Q
CL
U
E
2
U
.N
a�
c
J 1
.N
uJ
tD
�p
-
Y
U
Z
_
O
c
N
f=
=
rJ) )
�
p
Z
O
Z
Z
Z
z
a
0o
I—o
z
Y
a
to
-o
o
CODE: A = None
B = HNO3 H<2 + <4°C
(P )
C = H2SO4 (pH<2) + <4°c
D = NaOH + <4°C
E = ZN Acetate + <4°C
F = HCl
CONTACT PERSON:
Mr. Chris Fowler
PHONE:
910-410-9131
SAMPLER:
DATE 1 METHOD OF SHIPMENT:
Microbac
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
F H
D.O.
TEMP °C
RES.
CHLORINE
Residual from paper plant
X
2
A
A
A
A
A
A
A
A
A
1
A
A
A
A
A
A
A
A
A
inquished by:
�- i 1
Date
Timejec
ivad by: (Signature)
2
Date
Time
Relinquished by:
Date
Time
Rec ed by 'nature)
D
�/
3
4
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
5
6
Comments or Special Hazards:
REVIEWED
-4-A-
Page 3 of 3
Facility:
von Drehle Corporation
Source:
von Drehle Paper
Location:
Cordova, North Carolina
Contractor:
Belger Farms
Type of Analysis:
Industrial
Report No:
vd 2019-3 MB
Date Sampled:
5/6/2019
Date Reported:
5/14/2019
Reporting Period:
May -June 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
43.00
Nitrogen (TKN)
0.041
407.000
Phosphorus
0.000
2.200
Potassium
0.074
744.000
Sulfate
0.000
Calcium
1.240
12,400.000
Magnesium
0.242
2,420.000
Sodium
0.071
707.000
Iron
---
Aluminum
---
6,870.000
Manganese
---
Copper
---
247.000
1,500
Zinc
---
597.000
2,800
Ammonia Nitrogen
0.010
104.000
Nitrate N / Nitrite N
---
14.5200
Cadmium
---
1.3000
39
Chromium
---
1,200
Nickel
---
18.6000
420
Lead
---
12.4000
300
Arsenic
---
1.4000
41
Mercury
---
0.0170
17
Selenium
---
6.7000
100
pH
8.100
Calcium Carbonate Eq.
0.000
Organic Nitrogen
0.030
Molybdenum
---
9.0000
75
Chloride
---
Boron
Available P2O5
VMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9E0060
Von Drehle Corporation Project Name: Residuals Sample - 60 day
Mr. Chris Fowler Project / PO Number: N/A
126 First Street Received: 05/06/2019
Cordova, NC 28330 Reported: 05/14/2019
Analytical Testing Parameters
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Lab Sample ID: K9E0060-01
Calculation
Plant Available Nitrogen
EPA 300.0, Rev. 2.1 (1993)
Nitrate as N
Nitrite as N
SM 2540 G-2011
% Solids
SM 4500 NH3 C-2011
Ammonia as N
SM 4500-Norg C-2011
Total Kjeldahl Nitrogen
Wet Chemistry
Calculation
Sodium Adsorption Ratio, SAR
EPA 9045 D
pH at 25 °C
SM 4500 P F-2011
Phosphorus, Total (as P)
SPLP Metals
EPA 7471E
Mercury
SW-846 6010B
Collected By: Wright
Collection Date: 05/06/2019 11:46
Result
RL Units
Dilution
Note Prepared
Analyzed
Analyst
146
mg/kg
1
05/13/19 1128
05/13/19 1128
JMO
2.92
0.581 mg/kg dry wt.
1
05/07/19 1123
05/07/19 1650
DSK
dry
<11.6
11.6 mg/kg dry wt.
1
05/07/19 1123
05/07/19 1650
DSK
dry
43.0
1.00 %
1
05/06/19 1604
TMC
104
2.33 mg/kg dry wt.
1
y
05/10/19 0730
DSK
dry
407
1.16 mg/kg dry wt.
1
05/07/19 0850
MT
dry
Result
RL Units
Dilution
Note Prepared
Analyzed
Analyst
1.08
mg/kg
1
05/13/19 1128
05/13/19 1225
JMO
8.1
1.0 pH Units
1
H
05/10/19 1001
CLB
2.2 0.57 mg/kg dry wt. 1 05/09/19 1131 DSK
dry
Analyses Subcontracted to: Pace Analytical ( Huntersville)
Result RL Units Dilution Note Prepared Analyzed Analyst
0.017 0.015 mg/kg dry wt. 1 05/09/19 0000 TE
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 3
6)MICROBAC
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9E0060
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Collected By: Wright
Lab Sample ID: K9E0060-01
Collection Date: 05/06/2019 11:46
SPLP Metals
Result
RL Units
Dilution
Note Prepared Analyzed
Analyst
Aluminum
6870
14.1 mg/kg dry wt.
1
05/09/19 0000
TE
Arsenic
<1.4
1.4 mg/kg dry wt.
1
05/09/19 0000
TE
Cadmium
1.3
0.14 mg/kg dry wt.
1
05/09/19 0000
TE
Calcium
12400
14.1 mg/kg dry wt.
1
05/09/19 0000
TE
Copper
247
0.71 mg/kg dry wt.
1
05/09/19 0000
TE
Lead
12.4
0.71 mg/kg dry wt.
1
05/09/19 0000
TE
Magnesium
2420
14.1 mg/kg dry wt.
1
05/09/19 0000
TE
Molybdenum
9
0.25 mg/kg dry wt.
1
05/09/19 0000
TE
Nickel
18.6
0.25 mg/kg dry wt.
1
05/09/19 0000
TE
Potassium
744
500 mg/kg dry wt.
1
05/09/19 0000
TE
Selenium
6.7
0.5 mg/kg dry wt.
1
05/09/19 0000
TE
Sodium
<707
250 mg/kg dry wt.
1
05/09/19 0000
TE
Zinc
597
1.4 mg/kg dry wt.
1
05/09/19 0000
TE
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL: Minimum Detection Limit
RL: Reporting Limit
Y: This analyte is not on the laboratory's current scope of accreditation.
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
Report Comments
North Carolina DENR NPDES
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to �e�lL �LWi�dZ
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet
in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental
Reported: 05/14/2019 15:22
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 3
'K9E0060'
Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 (910) 864-1920 / 864-8774 fax
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CLIENT NAME A ADDRESS.
VonDrehle Corp.
126 First Street
Cordova, NC 28330
PO.
PNO.IECTILOCAMN:
Cordova - 60-dayseries
ROF
a
D
T
T
L
E
S
TYPE
OF
ANALYSIS
PRESERVATION CODE
E
N
U
E
C
E
TrQ
C
m
0
co
C
m
r;
CL
o
U
j
o
m
U
E
.N
c
m
te
N
J
E
.N
to
a
ae
U
Z
U
_
O
X
_c
N
<
N
Z
o
Z
M
=
Z
Z
a
o
a
F'
Z
Y
H
a
N
-6
o
~
CODE: A = None
B=HNO3(pH<2)+<4'C
C = H2SO4 (pH<z) + <4'C
D= NaOH +<4'C
E= ZN Acetate . <4'C
F=HCI
CONTACTPERSON:
Mr. Chris Fowler
PHONE:
910-410-9131
EANPLER:
OATEINETH00 OF SHIPMENT: MICrobac
LAB ID #
SAMPLE
TYPE
DATE
TIME
COMP
GRAB
PN
O.O.
TCEIMP •G
RES.
CHLORINE
2
Residual from paper plant
/0 r S
2
A
A
I A
I A
I A
A
I A
A
A
I
1
1
A
A
I A
I A
A
A
I A
I A
A
Otl.
nm.
Nc - Oby: tSlanaWn)
Oat•
�
T..
1
ten. 2
�j• •/
i�G3
N aLN.e by:
O.b
N.a.Ma by: tSlpmtun)
On•
nme
3
4
R•IiaNa..Eby:
O.t.
Tim
N-4d by: (Sigr—n)
Oat.
Tim.
5
6
Comments or Spedal Hazards
Page 3 of 3
Facility:
von Drehle Corporation
Source:
von Drehle Paper
Location:
Cordova, North Carolina
Contractor:
Belger Farms
Type of Analysis:
Industrial
Report No:
vd 2019-4 MB
Date Sampled:
7/29/2019
Date Reported:
8/9/2019
Reporting Period:
July- Aug 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
34.40
Nitrogen (TKN)
0.033
332.000
Phosphorus
0.003
29.000
Potassium
0.103
1,030.000
Sulfate
0.000
Calcium
1.710
17,100.000
Magnesium
0.191
1,910.000
Sodium
0.130
1,300.000
Iron
---
Aluminum
---
1,870.000
Manganese
---
Copper
---
24.600
1,500
Zinc
---
97.900
2,800
Ammonia Nitrogen
0.000
2.910
Nitrate N / Nitrite N
---
16.1100
Cadmium
---
0.2100
39
Chromium
---
1,200
Nickel
---
1.2000
420
Lead
---
1.0000
300
Arsenic
---
2.1000
41
Mercury
---
0.0120
17
Selenium
---
2.1000
100
pH
8.000
Calcium Carbonate Eq.
0.000
Organic Nitrogen
0.033
Molybdenum
---
4.2000
75
Chloride
---
Boron
Available P2O5
�DMICROBAC°
Microbac Laboratories, Inc. - Fayetteville
Revised Report: Amended - RURELIMINARY
REPORT. DATA SUBJECT TO CHANGE
Case Narrative.
K9G0397
Von Drehle Corporation
Project Name: Residuals Sample - 60 day
Mr. Chris Fowler
Project / PO Number: N/A
126 First Street
Received: 07/29/2019
Cordova, NC 28330
Reported: 08/09/2019
Case Narrative
Report amended on August 9, 2019 for work order K9G0397 that was originally reported on August 8, 2019: Missing sodium result and removed the units for
the SAR calculation.
Analytical Testing Parameters
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Collected By: Wright
Lab Sample ID: K9G0397-01
Collection Date: 07/29/2019 11:00
Result RL Units Dilution Note Prepared Analyzed Analyst
Calculation
Plant Available Nitrogen
102 mg/kg 1 08/08/19 1039 08/08/19 1050 JMO
EPA 300.0, Rev. 2.1 (1993)
Nitrate as N
1.91 0.708 mg/kg dry wt. 1 07/31/19 1019 07/31/19 1638 DSK
dry
Nitrite as N
<14.2 14.2 mg/kg dry wt. 1 07/31/19 1019 07/31/19 1638 DSK
dry
SM 2540 G-2011
% Solids 34.4 1.00 % 1 07/29/19 1415 DSK
SM 4500 NH3 C-2011
Ammonia as N <2.91 2.91 mg/kg dry wt. 1 Y 08/05/19 1011 MT
dry
SM 4500-Norg C-2011
Total Kjeldahl Nitrogen
332 1.45 mg/kg dry wt. 1
08/07/19 0904
08/07/19 1618
TBM
dry
Wet Chemistry
Result RL Units Dilution Note
Prepared
Analyzed
Analyst
Calculation
Sodium Adsorption Ratio, SAR
0.480 1
08/08/19 1039
08/08/19 1051
JMO
EPA 9045 D
pH at 25 °C
8.0 1.0 pH Units 1 H
08/07/19 1057
DSK
SM 4500 P F-2011
Phosphorus, Total (as P)
29 0.72 mg/kg dry wt. 1
07/31/19 1307
DSK
dry
Analyses Subcontracted to: Pace Analytical ( Huntersville)
SPLP Metals
Result RL Units Dilution Note
Prepared
Analyzed
Analyst
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 1 of 3
(tiMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
PRELIMINARY REPORT. DATA SUBJECT TO CHANGE
K9G0397
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid
Lab Sample ID: K9G0397-01
Collected By: Wright
Collection Date: 07/29/2019 11:00
SPLP Metals
Result
RL Units
Dilution
Note Prepared
Analyzed
Analyst
SW-846 6010E
Aluminum
1870
20.7 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Arsenic
<2.1
2.1 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Cadmium
<0.21
0.21 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Calcium
17100
207 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Copper
24.6
1 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Lead
<1.0
1 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Magnesium
1910
20.7 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Molybdenum
4.2
1 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Nickel
1.2
1 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Potassium
<1030
1030 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Selenium
<2.1
2.1 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
Sodium
<1030
1030 mg/kg dry wt.
1
08/08/19 0000
JB
Zinc
97.9
2.1 mg/kg dry wt.
1
08/08/19 0000
08/07/19 0000
JB
SPLP Metals
EPA 7471E
Mercury
Definitions
H:
MDL:
RL:
Y:
0.012
Result RL Units Dilution Note
0.0087 mg/kg dry wt. 1
Analyte was prepared and/or analyzed outside of the analytical method holding time
Minimum Detection Limit
Reporting Limit
This analyte is not on the laboratory's current scope of accreditation.
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
North Carolina DENR NPDES
Prepared Analyzed Analyst
08/07/19 0000 JB
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 2 of 3
*K9G0397*
Fayetteville Division 2592 Hope Mills Road •- Fayetteville, NC 28306 (910) 864-1920 / 864-F lffillilililitillif
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CLIENT NAME & ADDRESS:
VonDrehle Corp.
126 First Street
Cordova, NC 28330
PO #
PROJECT LOCATION:
I Cordova - 60-day series
# OF
B
0
T
T
L
E
S
TYPE OF
ANALYSIS
PRESERVATION CODE
E
E
U
C
E
Q
C
°'
N
�
a).2
Q`
�,
CL
C
0
U
E
'N
c
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m
to
E
'N
m
a°
-
Y
Z
=
c
N
E
�
Q
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O
Z
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o
Z
Z
Z
a
o
s
o-
I—
z
F
7-
to
O
tq
to
o
H
�
CODE: A = None
B = HNO3 (pH<2) + <4°C
C = H2SO4 (pH<2) + <4°C
D= NaOH + <4°C
E = ZN Acetate + <4°C
F = HCI
CONTACT PERSON:
Mr. Chris Fowler
PHONE:
910-410-9131
SAMPLER:
1 --
DATE I METHOD OF SHIPMENT:
Microbac
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
pH
D.O.
TEMP'C
CHLORINE
I`
Residual from paper plant
7 9 1 Y
j j. D 0
X
2
A
A
A
A
A
I A
I A
A
A
Rell b . 1'
Date
Time
R ed Signature)
Date
Time
1
Z 2J t�
13:/
2
- q-11
squished by:
Date
Time
Rece Vd by: (Signature)
Date
Time
3
4
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
5
6
Comments or Special Hazards:
REVIEWED
Page 3 of 3
Facility:
Source:
Location:
Contractor:
Type of Analysis:
von Drehle Corporation
von Drehle Paper
Cordova, North Carolina
Belger Farms
Industrial
Report No: vd 2019-5 MB
Date Sampled: 9/9/2019
Date Reported: 9/24/2019
Reporting Period: Sept -Oct 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
36.60
Nitrogen (TKN)
0.034
335.000
Phosphorus
0.000
3.200
Potassium
0.006
63.600
Sulfate
0.000
Calcium
19.100
191,000.000
Magnesium
0.235
2,350.000
Sodium
0.121
1,210.000
Iron
---
Aluminum
---
1,090.000
Manganese
---
Copper
---
26.400
1,500
Zinc
---
53.100
2,800
Ammonia Nitrogen
0.000
2.730
Nitrate N / Nitrite N
---
19.0500
Cadmium
---
0.4400
39
Chromium
---
1,200
Nickel
---
1.6000
420
Lead
---
1.1000
300
Arsenic
---
1.3000
41
Mercury
---
0.6100
17
Selenium
---
1.7000
100
pH
8.000
Calcium Carbonate Eq.
0.000
Organic Nitrogen
0.033
Molybdenum
---
2.6000
75
Chloride
---
Boron
Available P205
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K910109
Project Description
Residuals Sample - 60 day
For:
Mr. Chris Fowler
Von Drehle Corporation
126 First Street
Cordova, NC 28330
Client Relationship Specialist, Environmental
Jeanne Overstreet
Tuesday, September 24, 2019
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require
further assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil
samples are reported on a 'dry -weight' basis unless specified otherwise. Analytical results for water and wastes are reported on
a'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This
laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported
results are related only to the samples analyzed as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 1 of 7
Von Drehle Corporation
Mr. Chris Fowler
126 First Street
Cordova, NC 28330
Sample Summary Report
6)MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K910109
Project Name: Residuals Sample - 60 day
Project / PO Number: N/A
Received: 09/09/2019
Reported: 09/24/2019
Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received
Residual from Paper Plant, K910109-01 Solid Grab 09/09/19 13:30 09/09/19 14:59
Grab
Page 2 of 7
VMICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K910109
Analytical Testing Parameters
Client Sample ID: Residual from Paper Plant, Grab
Sample Matrix: Solid
Collected By: Wright
Lab Sample ID: K910109-01
Collection Date: 09/09/2019 13:30
Result
RL Units
Dilution
Note Prepared Analyzed
Analyst
Calculation
Plant Available Nitrogen 106
mg/kg
1
09/20/19 0858 09/20/19 0858
JMO
EPA 300.0, Rev. 2.1 (1993)
Nitrate as N 5.65
0.672 mg/kg dry wt.
1
09/10/19 1143 09/10/19 1601
DSK
dry
Nitrite as N <13.4
13.4 mg/kg dry wt.
1
09/10/19 1143 09/10/19 1601
DSK
dry
SM 2540 G-2011
% Solids
SM 4500 NH3 C-2011
Ammonia as N
SM 4500-Norg C-2011
Total Kjeldahl Nitrogen
Wet Chemistry
Calculation
Sodium Adsorption Ratio, SAR
EPA 9045 D
pH at 25 °C
SM 4500 P F-2011
Phosphorus, Total (as P)
SPLP Metals
EPA 601 OD
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
36.6 1.00 % 1
<2.73 2.73 mg/kg dry wt. 1 y
dry
335 1.36 mg/kg dry wt. 1
dry
Result RL Units Dilution Note
0.530 1
09/10/19 1143 CLS
09/13/19 0937 MT
09/10/19 1609 09/12/19 1111 TBM
Prepared Analyzed Analyst
09/20/19 0858 09/24/19 0848 JMO
8.0 1.0 pH Units
1 H
3.2 0.68 mg/kg dry wt.
1
dry
Analyses Subcontracted to: Pace Analytical (
Huntersville)
Result RL Units Dilution
Note Prepared
1090 4.4 mg/kg dry wt.
1
<1.3 1.3 mg/kg dry wt.
1
<0.44 0.44 mg/kg dry wt.
1
191000 4360 mg/kg dry wt.
1
26.4 0.87 mg/kg dry wt.
1
<1.1 1.1 mg/kg dry wt.
1
2350 218 mg/kg dry wt.
1
2.6 1.7 mg/kg dry wt.
1
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
09/18/19 1409 CLB
09/12/19 1459 DSK
Analyzed Analyst
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
Page 3 of 7
�gDMICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K910109
Client Sample ID:
Residual from Paper Plant, Grab
Sample Matrix:
Solid
Lab Sample ID:
K910109-01
SPLP Metals
Result
Nickel
1.6
Potassium
63.6
Selenium
<1.7
Sodium
1210
Zinc
53.1
EPA 7471 B
Mercury
<0.61
Collected By: Wright
Collection Date: 09/09/2019 13:30
RL Units
Dilution Note
0.87 mg/kg dry wt.
1
8.7 mg/kg dry wt.
1
1.7 mg/kg dry wt.
1
43.6 mg/kg dry wt.
1
0.87 mg/kg dry wt.
1
0.61 mg/kg dry wt. 1
Prepared Analyzed
Analyst
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/18/19 0000
DK
09/23/19 0000 ❑K
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 7
6)MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K910109
Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville
Spike Source %REC RPD
Result RL Units Level Result %REC Limits RPD Limit Notes
Batch K190078 - Wet Chem Solid - SM 2540 G-2011
Blank (K190078-BLK1)
Prepared & Analyzed: 09/10/2019
% Solids
<1.00
1.00
%
Duplicate (KI90078-DUP1)
Source: K910109-01
Prepared &Analyzed: 09/10/2019
% Solids
38.0
1.00
% 36.6
Batch K190113 - Wet Chem Solid
- SM 4500 NH3 C-2011
Blank (K190113-BLK1)
Prepared & Analyzed: 09/13/2019
Ammonia as N
<1.00
1.00
mg/kg
dry wt.
wet
Blank (K190113-BLK2)
Prepared & Analyzed: 09/13/2019
Ammonia as N
<1.00
1.00
mg/kg
dry wt.
wet
4 10
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 7
�VMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K910109
Definitions
H:
Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL:
Minimum Detection Limit
RL:
Reporting Limit
RPD:
Relative Percent Difference
Y:
This analyte is not on the laboratory's current scope of accreditation.
Cooler Receipt Log
Cooler ID:
Default Cooler Temp: 8.7°C
Cooler Inspection Checklist
Ice Present or not required?
Yes
Shipping containers sealed or not required?
Yes
Custody seals intact or not required?
Yes
Chain of Custody (COC) Present?
Yes
CDC includes customer information?
Yes
Relinquished and received signature on COC?
Yes
Sample collector identified on COC?
Yes
Sample type identified on COC?
Yes
Correct type of Containers Received
Yes
Correct number of containers listed on COC?
Yes
Containers Intact?
Yes
CDC includes requested analyses?
Yes
Enough sample volume for indicated tests received?
Yes
Sample labels match COC (Name, Date & Time?)
Yes
Samples arrived within hold time?
Yes
Correct preservatives on CDC or not required?
Yes
Chemical preservations checked or not required?
Yes
Preservation checks meet method requirements?
Yes
VOA vials have zero headspace, or not recd.?
Yes
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
Report Comments
North Carolina DENR NPDES
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted. �2lLlLX� L4iZdZe
The data and information on this, and other accompanying documents, represents {{//
only the sample(s) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet
in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental
Reported: 09/24/2019 09:01
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 7
Fayetteville Division 2592 Hope Mills Road �- Fayetteville, NC 28306 (910) 864-1920 / 864- *K910'109*
� ;Za �� ll��l��l�f Iil�lli�l�l��ll�l
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CLIENT NAME & ADDRESS:
VonDrehle Corp.
26 First Street
Cordova, NC 28330
PO#
I
PROJECT I LOCATION:
Cordova - 60-day series
#OF
B
T
T
L
E
S
TYPE OF
ANALYSIS
PRESERVATION CODE
=
E
U
E
c
E
C
U)
•U
a
`�
Q
�,
CL
o
V
Ef
.2
-FaO
c.i
t/)
c
.a
J
'(A
t��o
O
a
-
Y'
U
Z
(�
=
O
c
N
E
O
(J)
Q
-
p
Z
M
O
Z
m
Z
Z
Z
a
o
a.,
F—
z
Y
f—
a
Ul
O
°
o
CODE: A = None
B = HNO3 (pH<2) + c4°C
C = H2SO4 (pH<2) + <4°c
D= NaOH + <4°C
E= ZN Acetate + <4°C
F = HCI
PERSON:
CONTACTo
Mr. Chris Fowler
PHONE:
910-410-9131
SAMPLER:
�y
DATE! METHOD OF SHIPMENT:
Microbac
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
pH
D.O.
TEMPIC
ems'
CHLORINE
Residual from paper plant
49//
X
2
A
A
A
A
A
I A
I A
A
A
Q' r
1
A
A
A
A
A
A
A
A
A
Relnqut 1
Da/te
Tl�n/e, S 9Re
iv d b
S' "M 2
e q
Time
d by:
Data
Time
Received by: (Signature)
Date
Time
3
4
Relinquished by:
Date
me
Received by: (Signature)
Date
Tlme
5
6
Comments or Special Hazards:
REViL. 4V
--�A
Page 7 of 7
Facility:
von Drehle Corporation
Source:
von Drehle Paper
Location:
Cordova, North Carolina
Contractor:
Belger Farms
Type of Analysis:
Industrial
Report No:
vd 2019-6 MB
Date Sampled:
11/12/2019
Date Reported:
11/24/2019
Reporting Period:
Nov- Dec 2019
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
34.80
Nitrogen (TKN)
0.061
613.000
Phosphorus
0.007
72.000
Potassium
0.050
500.000
Sulfate
0.000
Calcium
17.500
175,000.000
Magnesium
0.176
1,760.000
Sodium
0.114
1,140.000
Iron
---
Aluminum
---
1,370.000
Manganese
---
Copper
---
33.100
1,500
Zinc
---
135.000
2,800
Ammonia Nitrogen
0.000
2.870
Nitrate N / Nitrite N
---
3.0900
Cadmium
---
2.8000
39
Chromium
---
1,200
Nickel
---
1.4000
420
Lead
---
1.2000
300
Arsenic
---
1.0000
41
Mercury
---
0.0200
17
Selenium
---
1.3000
100
pH
8.400
Calcium Carbonate Eq.
0.000
Organic Nitrogen
0.061
Molybdenum
---
3.6000
75
Chloride
---
Boron
Available P2O5
6)MICROBAC R
Microbac Laboratories, Inc. - Fayetteville
C
CERTIFICATE OF ANALYSIS
K9K0151
Project Description
Residuals Sample - 60 day
For:
Mr. Chris Fowler
Von Drehle Corporation
126 First Street
Cordova, NC 28330
Administration
Brittany Smith
Sunday, November 24, 2019
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further
assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are
reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported
on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be
reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the
samples analyzed as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 i 910.864.1920 p i www.microbac.com
Page 1 of 7
�VMICROBAC-
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9K0151
Von Drehle Corporation Project Name: Residuals Sample - 60 day
Mr. Chris Fowler Project / PO Number: N/A
126 First Street Received: 11 /12/2019
Cordova, NC 28330 Reported: 11/24/2019
Sample Summary Report
Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received
Residual from Paper Plant, K91<0151-01 Solid Grab 11/12/19 11:45 11/12/19 14:05
Grab
Page 2of7
MICROsAC
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9K0151
Analytical Testing Parameters
Client Sample ID: Residual from Paper Plant, Grab
Sample Matrix: Solid
Lab Sample ID: K91<0151-01
Result
Calculation
Plant Available Nitrogen
186
EPA 300.0, Rev. 2.1 (1993)
Nitrate as N
1.69
Nitrite as N
<1.40
SM 2540 G-2011
% Solids
34.8
SM 4500 NH3 C-2011
Ammonia as N
<2.87
SM 4500-Norg C-2011
Total Kjeldahl Nitrogen
613
Wet Chemistry
Result
Calculation
Sodium Adsorption Ratio, SAR
0.530
EPA 9045 D
pH at 25 °C
8.4
SM 4500 P F-2011
Phosphorus, Total (as P)
Mercury
SPLP Metals
SW-846 6010B
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Collected By: Wright
Collection Date: 11/12/2019 11:45
RL Units Dilution Note Prepared Analyzed Analyst
mg/kg 1 11/24/19 0040 11/24/19 0041 BNS
0.701 mg/kg dry 1
1.40 mg/kg dry 1
1.00 % 1
2.87 mg/kg dry 1 y
1.44 mg/kg dry 1
RL Units Dilution Note
NA 1
1.0 S.U. 1 H
11/15/19 0107 11/16/19 1000 JAW
11/15/19 0107 11/16/19 1000 JAW
11/18/19 1040 CLS
11/18/19 1000 MT
11/15/19 0857 CL8
Prepared Analyzed Analyst
11/24/19 0040 11/24/19 0041 BINS
11/18/19 1355 CLB
72
3.5 mg/kg dry 1
11/16/19 1019
JAW
Analyses Subcontracted
to: Pace Analytical ( Huntersville)
Result
RL Units Dilution Note
Prepared
Analyzed
Analyst
0.020 mg/kg
0.012 mg/kg dry wt. 1
11/15/19 1048
11/19/19 1457
TE
Result
RL Units Dilution Note
Prepared
Analyzed
Analyst
1370 mg/kg
10 mg/kg dry wt. 1
11/15/19 1127
11/17/19 2307
TE
<1
1 mg/kg dry wt. 1
11/15/19 1127
11/17/19 2307
TE
2.8 mg/kg
0.1 mg/kg dry wt. 1
11/15/19 1127
11/17/19 2307
TE
175000 mg/kg
10 mg/kg dry wt. 1
11/15/19 1127
11/17/19 2307
TE
33.1 mg/kg
0.5 mg/kg dry wt. 1
11/15/19 1127
11/17/19 2307
TE
1.2 mg/kg
0.5 mg/kg dry wt. 1
11/15/19 1127
11/17/19 2307
TE
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 3 of 7
�VMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9K0151
Client Sample ID:
Residual from Paper Plant, Grab
Sample Matrix:
Solid
Lab Sample ID:
K9K0151-01
SPLP Metals
Result
Magnesium
1760 mg/kg
Molybdenum
3.6 mg/kg
Nickel
1.4 mg/kg
Potassium
<500
Selenium
1.3 mg/kg
Sodium
1140 mg/kg
Zinc
135 mg/kg
Collected By: Wright
Collection Date: 11/12/2019 11A5
RL Units
Dilution
Note Prepared
Analyzed
Analyst
10 mg/kg dry wt.
1
11/15/19 1127
11/17/19 2307
TE
0.5 mg/kg dry wt.
1
11/15/19 1127
11/17/19 2307
TE
0.5 mg/kg dry wt.
1
11/15/19 1127
11/17/19 2307
TE
500 mg/kg dry wt.
1
11/15/19 1127
11/17/19 2307
TE
1 mg/kg dry wt.
1
11/15/19 1127
11/17/19 2307
TE
500 mg/kg dry wt.
1
11/15/19 1127
11/17/19 2307
TE
1 mg/kg dry wt.
1
11/15/19 1127
11/17/19 2307
TE
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 7
�VMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9K0151
Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville
Result RL
Batch KK91610 - Wet Chem Solid - SM 2540 G-2011
Blank (KK91610-BLK1)
% Solids <1.00 1.00
Duplicate (KK91610-DUP1) Source: K9K0151-01
% Solids 33.5 1.00
Batch KK91614 - Wet Chem Solid - SM 4500 NH3 C-2011
Blank (KK91614-BLK1)
Ammonia as N <1.00 1.00
Blank (KK91614-BLK2)
Ammonia as N <1.00 1.00
Spike Source %REC RPD
Units Level Result %REC Limits RPD Limit Notes
Prepared &Analyzed: 11/18/2019
Prepared &Analyzed: 11/18/2019
% 34.8 4 10
Prepared &Analyzed: 11/18/2019
mg/kg
wet
Prepared & Analyzed: 11 /18/2019
mg/kg
wet
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p 1 www.microbac.com Page 5 of 7
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9K0151
Definitions
%: Percent
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL: Minimum Detection Limit
mg/kg: Milligrams per Kilogram
NA: Not Applicable
RL: Reporting Limit
RPD: Relative Percent Difference
S.U.: Standard Units
Y: This analyte is not on the laboratory's current scope of accreditation.
Cooler Receipt Log
Cooler ID: Default Cooler Temp: 3.5°C
Cooler Inspection Checklist
Ice Present or not required?
Yes
Shipping containers sealed or not required?
Yes
Custody seals intact or not required?
Yes
Chain of Custody (COC) Present?
Yes
COC includes customer information?
Yes
Relinquished and received signature on COC?
Yes
Sample collector identified on COC?
Yes
Sample type identified on COC?
Yes
Correct type of Containers Received
Yes
Correct number of containers listed on COC?
Yes
Containers Intact?
Yes
COC includes requested analyses?
Yes
Enough sample volume for indicated tests received?
Yes
Sample labels match COC (Name, Date & Time?)
Yes
Samples arrived within hold time?
Yes
Correct preservatives on COC or not required?
Yes
Chemical preservations checked or not required?
Yes
Preservation checks meet method requirements?
Yes
VOA vials have zero headspace, or not recd.?
Yes
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
Report Comments
North Carolina DENR NPDES
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted. l
The data and information on this, and other accompanying documents, represents J\
only the sample(s) analyzed. This report is incomplete unless all pages indicated Brittany Smith
in the footnote are present and an authorized signature is included. Administration
Reported: 11/24/2019 01:06
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 6 of 7
*K9K0151*
Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 864-8 II IP, IIIIIIIIIIIIllP lul �I u�jl p�!
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CLIENT NAME &ADDRESS:
VonDrehle Corp.
126 First Street
Cordova, NC 28330
PO t#
PROJECT LOCATION:
Cordova - 60-day series
# OF
B
o
T
L
E
S
TYPE OF
ANALYSIS
PRESERVATION CODE
E
E
3
Q
C
N
U
U
'�
N
Q
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i?.
C
U
+=
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to
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m
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US
16
V
Z
=
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-
O
o
Z
=
Z
Z
a
o
n
Y
i—
n
to
o
c°n
ro
c
o
CODE: A = None
B = HNO3 (pH<2) + <4°C
C = H2SO4 (pH<2) + <4°C
o
D=NaOH+<4 C
E= ZN Acetate + <4°C
F = HCl
CONTACT PERSON:
Mr. Chris Fowler
PHONE:
910-410-9131
SAMPLER:
/
DATE 1 METHOD OF SHIPMENT:
Microbac
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
D.O.
TEMP'C
RES.
CHLORINE
Residual from paper plant
�t rZ I
[ (; ��
X
2
A
A
A
A
A
A
A
A
A
1
1
A
A
A
A
A
A
A
A
A
Rel'
Date ,
Time
OI
Re ei ed b (
Data
],,/,,
Time
Relinquished by:
Date
Time
Received by: (Signature)
Date
Time
3
4
Relinquished by:
to
Time
Received by: (Signature)
Date
Time
5
g
Comments or Special Hazards:
Page 7 of 7
TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT
*MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0355
Project Description
Residuals Sample -Annual
For:
Mr. Chris Fowler
Von Drehle Corporation
126 First Street
Cordova, NNCCy28330
Jeanne Overstreet
Client Relationship Specialist, Environmental
Monday, February 11, 2019
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require
further assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil
samples are reported on a 'dry -weight' basis unless specified otherwise. Analytical results for water and wastes are reported on
a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This
laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported
results are related only to the samples analyzed as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 1 of 8
�DMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0355
Von Drehle Corporation Project Name: Residuals Sample -Annual
Mr. Chris Fowler Project / PO Number: 2030767
126 First Street Received: 01/24/2019
Cordova, NC 28330 Reported: 02/11/2019
Sample Summary Report
Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received
Residual from paper plant K9A0355-01 Solid Grab 01/24/19 12:19 01/24/19 14:28
Page 2 of 8
�gDMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0355
Analytical Testing Parameters
Client Sample ID: Residual from paper plant
Sample Matrix: Solid Collected By: Wright
Lab Sample ID: K9A0355-01 Collection Date: 01/24/2019 12:19
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Result RL Units Note Prepared Analyzed Analyst
Method: 9045D
Corrosivity pH 8.49 UNITS 01/31/19 1440 AWE
Temperature At Determination (C) 19.3 UNITS 01/31/19 1440 AWE
8270 TC
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: 8270C
1,4-Dichlorobenzene
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
2,4,5-Trichlorophenol
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
2,4,6-Trichlorophenol
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
2,4-Dinitrotoluene
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
Hexachlorobenzene
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
Hexachlorobutadiene
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
Hexachloroethane
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
m-,p-Cresol
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
Nitrobenzene
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
o-Cresol
<100
100 ug/L
02/01/19 1205
02/05/19 1449
SCB
Pentachlorophenol
<500
500 ug/L
02/01/19 1205
02/05/19 1449
SCB
Pyridine
<500
500 ug/L
02/01/19 1205
02/05/19 1449
SCB
Surrogate: 2,4,6-Tribromophenol 111
Limit: 22-142 % Rec
02/01/19 1205
02/05/19 1449
SCB
Surrogate: 2-Fluorobiphenyl
97.6
Limit: 43-116 % Rec
02/01/19 1205
02/05/19 1449
SCB
Surrogate: 2-Fluorophenol
50.9
Limit: 19-119 % Rec
02/01/19 1205
02/05/19 1449
SCB
Surrogate: Nitrobenzene-d5
89.5
Limit: 35-114 % Rec
02/01/19 1205
02/05/19 1449
SCB
Surrogate: p-Terphenyl-d14
81.2
Limit: 10-130 % Rec
02/01/19 1205
02/05/19 1449
SCB
Surrogate: Phenol-d5
34.9
Limit: 10-94 % Rec
02/01/19 1205
02/05/19 1449
SCB
Ignitability of Solids
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: 1030
Bumrate - 1030
<2.20
2.20 mm/sec
02/06/19 1100
JDH
Mercury
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: 7470A
Mercury
<0.00200
0.00200 mg/L
02/04/19 1012
02/04/19 1542
KEH
Metals by 6010
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: 6010C
Arsenic, TCLP
<1.00
1.00 mg/L
02/04/19 0650
02/06/19 1214
KKB
Barium, TCLP
0.301
0.100 mg/L
02/04/19 0650
02/06/19 1214
KKB
Microbac
Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I
www.microbac.com
I Page 3 of 8
(�>MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0355
Client Sample ID: Residual from paper plant
Sample Matrix: Solid
Collected By: Wright
Lab Sample ID: K9A0355-01
Collection Date: 01/24/2019 12:19
Metals by 6010
Result
RL Units
Note
Prepared
Analyzed
Analyst
Cadmium, TCLP
<0.100
0.100 mg/L
02/04/19 0650
02/06/19 1214
KKB
Chromium, TCLP
<0.200
0.200 mg/L
02/04/19 0650
02/06/19 1214
KKB
Lead, TCLP
<1.00
1.00 mg/L
02/04/19 0650
02/06/19 1214
KKB
Selenium, TCLP
<0.800
0.800 mg/L
02/04/19 0650
02/06/19 1214
KKB
Silver, TCLP
<0.100
0.100 mg/L
02/04/19 0650
02/06/19 1214
KKB
Percent Solids
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: ASTM D2216-10
Percent Solids
41.1
1.00 weight %
02/05/19 0813
KMG
Reactivity, Cyanide
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: SW7.33
Reactivity, Cyanide
<9.93
9.93 mg/kg
02/04/19 1514
APH
Sulfide (Reacitivity)
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: SW7.34
Reactivity, Sulfide
<100
100 mg/kg
02/04/19 1400
EPT
TCLP HERBICIDES
Result
RL Units
Note
Prepared
Analyzed
Analyst
Method: 8151A
2,4-D
<20.0
20.0 ug/L
02/04/19 1708
02/06/19 1504
ECL
2,4,5-TP (Silvex)
<2.00
2.00 ug/L
02/04/19 1708
02/06/19 1504
ECL
Surrogate: 2,4-Dichlorophenylacetic acid
58.9
Limit: 20-144 % Rec
02/04/19 1708
02/06/19 1504
ECL
Volatile Organics
Result
RL. Units
Note
Prepared
Analyzed
Analyst
Method: 8260B
1,1-Dichloroethene
<50.0
50.0 ug/L
02/01/19 2247
EEA
1,2-Dichloroethane
<50.0
50.0 ug/L
02/01/19 2247
EEA
Benzene
<50.0
50.0 ug/L
02/01/19 2247
EEA
Carbon tetrachloride
<50.0
50.0 ug/L
02/01/19 2247
EEA
Chlorobenzene
<50.0
50.0 ug/L
02/01/19 2247
EEA
Chloroform
<50.0
50.0 ug/L
02/01/19 2247
EEA
Methyl Ethyl Ketone
<100
100 ug/L
02/01/19 2247
EEA
Tetrachloroethene
<50.0
50.0 ug/L
02/01/19 2247
EEA
Trichloroethene
<50.0
50.0 ug/L
02/01/19 2247
EEA
Vinyl chloride
<100
100 ug/L
02/01/19 2247
EEA
Surrogate: 1,2-Dichloroethane-d4
110
Limit: 80-120 % Rec
02/01/19 2247
EEA
Surrogate: 4-Bromofluorobenzene
91.1
Limit: 86-115 % Rec
02/01/19 2247
EEA
Surrogate: Dibromofluoromethane
101
Limit: 86-118 % Rec
02/01/19 2247
EEA
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I
www.microbac.com
Page 4 of 8
Microbac Laboratories, Inc. - Fayetteville
Client Sample ID: Residual from paper plant
Sample Matrix: Solid
Lab Sample ID: K9A0355-01
Volatile Organics
Surrogate: Toluene-d8
CERTIFICATE OF ANALYSIS
K9A0355
Result RL Units
94.6 Limit: 88-110 % Rec
Collected By: Wright
Collection Date: 01/24/2019 12:19
Note Prepared Analyzed Analyst
02/01/19 2247 EEA
Microbac Laboratories, In
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 8
6)MICROBAC'
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0355
Batch Quality Control Summary: Microbac Laboratories, Inc. - Ohio Valley
Spike Source %REC RPD
Reactivity, Cyanide Result RL Units Level Result %REC Limits RPD Limit Notes
Batch WG694692 - SW7.33 - SW7.33
BS (WG694692-01)
Reactivity, Cyanide ND 200
Sulfide (Reacitivity) Result RL
Batch WG694653 - SW7.34 - SW7.34
Prepared: Analyzed: 02/04/2019
mg/kg 11.8 .5-110 50 U
Spike Source %REC RPD
Units Level Result %REC Limits RPD Limit Notes
BLK (WG694653-01) Prepared: Analyzed: 02/04/2019
Reactivity, Sulfide ND 8.00 mg/kg -
BS (WG694653-02) Prepared: Analyzed: 02/04/2019
Reactivity, Sulfide 19.0 8.00 mg/kg 124 10-150 50
BS (WG694653-03) Prepared: Analyzed: 02/04/2019
Reactivity, Sulfide 1290 100 mg/kg 101 10-150 50
Definitions
MDL: Minimum Detection Limit
RL: Reporting Limit
RPD: Relative Percent Difference
U: Not detected at or above adjusted sample detection limit
Cooler Receipt Log
Cooler ID: Default Cooler
Cooler Inspection Checklist
Ice Present or not required?
Custody seals intact or not required?
COC includes customer information?
Sample collector identified on COC?
Correct type of Containers Received
Containers Intact?
Enough sample volume for indicated tests received?
Samples arrived within hold time?
Chemical preservations checked or not required?
VOA vials have zero headspace, or not recd.?
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
Temp: 4.1 °C
U
Yes
Shipping containers sealed or not required?
Yes
Yes
Chain of Custody (COC) Present?
Yes
No
Relinquished and received signature on COC?
No
No
Sample type identified on COC?
No
No
Correct number of containers listed on COC?
No
No
COC includes requested analyses?
No
No
Sample labels match COC (Name, Date & Time?)
No
No
Correct preservatives on COC or not required?
No
No
Preservation checks meet method requirements?
No
No
North Carolina DENR NPDES
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 8
�VMICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9A0355
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the samp/e(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
Jeanne Overstreet
Client Relationship Specialist, Environmental
Reported: 02/ 11 /2019 11:47
Microbac Laboratories, In
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 8
l c rm w;;5
Fayetteville Division 2592 Hope Mills Road -Fayetteville, NC 28306 (910) 864-1920 / 884 'K9A0355•
IR7W1IN@
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CL ENT NAME S ADDRESS
VonDrehle Corp.
126 First Street
Cordova, NC 28330
Fos
PROJECT:LOCATN)N
Cordova - Yearly
OF
a
O
T
r
L
E
S
TYPE OF ANALYSIS
PRESERVATION CODE
_
U
Q'
to
w
CC
J
�
m
x
=
a
J
F
<
X
UU
C
J
F
<
—12
0
c
J
I
p
w
c
J
F
CODE. A = <4•C ONLY
B = HNO3 (ph<2) + <4•C
c = H2SO4 (pI <z)+<a c
D = NaOH + <4•C
E = ZN Acetate + <4•C
F - Sodium Thlo.
CONTACT PERSON:
Mr. Chris Fowler
PHONE
910-410-9131
SAMPLER
DATE) METHOD OF SHIPMENT: Microbac
LAS ID >K
SAMPLE TYPE
DATE
TIME
COMP
ORAD
PH
D.O.
TEMP•C
ROBIN
�l
Residual from paper plant
)` I/�j
i L.! g
X
2
A
A
A
A
A
A
J
R. by0.1.
C
rim.
nawnl
D.H.
rim.
1
11y /✓
M.t�
z
I-JI 4-1
2
R.IInquM d!y
D.t.
Tina
19tV. try: ISlr..wnl
oat.
rim.
3
4
Rwi'A"hW/y
0-
rim
R-.—Gy: tSlpnawn)
D—
rim
5
6
R.rnR.i — by
Oat.
Tim.
R.e.rvM W: (sian.wn)
Da.
Tim.
7
8
Comments cr Speclal Hazards
Page 8 of 8
PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: von Drehle Corporation WQ Permit Number:
WWTP Name: Cordova Facility NPDES Number:
Monitoring Period: From 1/1/2019 To 2/28/2019
WQ0005135
NA
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) 0
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogens ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment[]
Thennophilic ❑
Beta Ray ❑
Gaimna Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑ 77777
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Y
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
..............
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
denses e-
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nioue
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
< 0.6
NA
< 0.9
GPams
0
imonthl
Grab
1E682
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization[]
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) R1
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC
Prep er Name and Title (type or print) Land Appli Name and Title (if applicable)(type or print)
;Z� 2- S,-ly ---z— Z-3 = a
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: von Drehle Corporation WQ Permit Number:
WWTP Name: Cordova Facility NPDES Number:
Monitoring Period: From 3/1/2019 To 4/30/2019
WQ0005135
NA
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) 0
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogens ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Ell
Heat Drying ❑
Heat Treatment❑
Thennophilic ❑
............
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
............
'
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑ —7777
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Y
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
...............
.........."`
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
Waue
Minimum
Geo. Mean
Maximurd
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
< 0.6
NA
0.7
Gras
0
imonthl
Grab
PA
E682
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) El
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
10 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC
Preparer e and Title (type or print) Land Ap r Name and Title (if applicable)(type or print)
2— C cp 2 --r, U
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135
WWTP Name: Cordova Facility
Monitoring Period: From 5/1/2019 To
NPDES Number: NA
6/30/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑T
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) CI
AIt.D (No Prior Test) ElProcess
to Further Reduce Pathogens El
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment[]
Thennophilic ❑
.............
..................
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
V
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
..............
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
Woue
Minimum
Geo. Mean
Maximu
Units
Fecal Colifonn
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
< 0.6
NA
< 0.9
Gr m's
0
imonthl
Grab
1E682
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) Rl
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC
Preparer Nape and ' le (type or print) Land Applier Name and Title (if applicable)(type or print)
a4-:� 2-s'-20 24Y=Z.
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 7/1/2019 To 8/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) 0
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogens ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment:- l
Thertnophilic ❑
Beta Ray LI
Gamma Ray ❑
Pasteurization LJ
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens Ll
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Li
Air Drying L]
Composting Ll
lAerobic Digestion Ll
Anaerobic Digestion Ll
..............
"' .. . .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
Frequency
of Analencesysis
Sample
Type
Analytical
Tech -
nioue
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
< 0.6
NA
< 0.6
Grams
0
imonthl
Grab
1E682
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
1Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Chris Fowler, Facility Manager
Preparer Name and Title (type or print)
01-� 111�--
Signature of Preparer*
Mr. Chris Fowler, Land Application ORC
Land Applier Name and Title (if applicable)(type or print)
zo 2-5 - U'
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T N 2/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135
WWTP Name: Cordova Facility NPDES Number: NA
Monitoring Period: From 9/1/2019 To 10/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) Q 7
Alt B (Alk Treatment) ElAlt.
C (Prior Testing)
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogens ❑
If applicable to alternative
performed (Class A only indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment[]
Thennophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
v
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.....` . `. `. ..
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number ot
Excee-
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
Waue
Minimum
Geo. Mean
aximu
Unitsences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
< 0.6
NA
< 0.6
GPams
0
imonthl
Grab
E682
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization[]
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying -Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) 21
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC
Preparer Name and Title (type or print) Land Appl' Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T N 2/20061
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: von Drehle Corporation
WWTP Name: Cordova Facility
WQ Permit Number: WQ0005135
NPDES Number: NA
Monitoring Period: From 10/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) El
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) t]
AIt.D (No Prior Test) ElProcess
to Further Reduce Pathogens ❑
If applicable to alternative
performed (Class A only indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment[]
Thermophilic ❑
Beta Ray ❑
Gamma Ray ElPasteurization
❑
Class B:
Alt. (1) Fecal Density 0I
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
V
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
. ..............
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analysis
Y
Sample
Type
na ytica
Tech -
waue
Minimu
Geo. Mean
aximu
Unitsences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
< 0.6
NA
0.8
Gras
0
imonthl
Grab
E
1682
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) O
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed Rl
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC
Pre/parer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
FECAL COLIFORM AND SALMONELLA DOCUMENTATION
Von Drehle Corporation
Cordova, NC
City of Rockingham IUP 0015
Jan-19
Biological Consulting Services
......
............. ..... :
.. value
a...............M.
Secondary:.:valuealmanella
......
..
...................................................................*....................
......................
.................. .. ...
.. ............
........ .... .......
........ ...
...........
.'....
.N:per:g#M
_
..,:XY
1901066
1/09/19
< 0.07
< 0.6
1901067
1/09/19
< 0.07
< 0.7
1901068
1/09/19
< 0.07
< 0.9
1901069
1/09/19
< 0.07
< 0.7
1901070
1/09/19
< 0.07
< 0.6
1901071
1/09/19
< 0.07
< 0.6
1901072
1/09/19
< 0.07
< 0.6
............... ................
Exceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Annual Pathogen
and Vector Attraction Reduction Form for Class A and Class B options.
inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
January 16, 2019
Robert Branch
Branch Residuals and Soils
8646 W. Market St. Suite 111
Greensboro NC 27409
336-510-0340
bbranch@branchrs.com
Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7
BCS ID: 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Cordova
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Imo , L ✓1 t it l� 11 �1 i
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2005 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
i�13��lVlRFc
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-1
Sample Date/Time: January 08, 2019 13:54
BCS Sample ID: 1901066 Sample Description: Biosolids
Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 41.5
Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes
Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-2
Sample Date/Time: January 08, 2019 13:57
BCS Sample ID: 1901067 Sample Description: Biosolids
Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 38.0
Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes
Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/]EC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
J��=NfRa
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-3
BCS Sample ID: 1901068
Date Received: January 09, 2019 10:05
Amount Analyzed: 30.00 g
Analysis Start: January 09, 2019 10:30
Analyst: Greta Pallack, B.A.
Sample Date/Time: January 08, 2019 14:00
Sample Description: Biosolids
Amount Submitted:100ml bottle % Solids: 30.4
Receipt Temperature: 5.4 deg C Preserved: Yes
Analysis Stop Date: January 12, 2019 11:40
Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
Cordova
Client Sample ID:
VD-4
BCS Sample ID:
1901069
Date Received:
January 09, 2019 10:05
Amount Analyzed: 30.00 g
Analysis Start:
January 09, 2019 10:30
Analyst:
Greta Pallack, B.A.
Sample Date/Time: January 08, 2019 14:03
Sample Description: Biosolids
Amount Submitted:100ml bottle % Solids: 40.1
Receipt Temperature: 5.4 deg C Preserved: Yes
Analysis Stop Date: January 12, 2019 11:40
Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
'a_IIaC'--NIRAA
r 1 11
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-5
Sample Date/Time: January 08, 2019 14:06
BCS Sample ID: 1901070 Sample Description: Biosolids
Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 41.3
Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes
Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-6
Sample Date/Time: January 08, 2019 14:08
BCS Sample ID: 1901071 Sample Description: Biosolids
Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 40.2
Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes
Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
41 ^ !
'^may <ccn coy o0
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-7 Sample Date/Time: January 08, 2019 14:12
BCS Sample ID: 1901072 Sample Description: Biosolids
Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 40.4
Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes
Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
._�
a�aG=iVIR/
At" T-W
Client: Branch Residuals and Soils
Project: Cordova
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924. ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
I certify that I have examined I am familiar with the information submitted herein. The results pertain only to
analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the
analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted
documents. The analysis was authorized commissioned by the client. The resulting data are representative of
the analysis conducted on the material/samples/articles provided by the client (or client's representative)
it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate
method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS
Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any
sample, batch, source, or the process they are derived from. Quality assurance controls were performed as
outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report
meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH
Environmental Laboratory Certification Program, as applicable unless otherwise noted.
Signature of Laboratory Director/Authorized Rep.
td�
Date: January 16, 2019
Page 7 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
-57
�aCl91ftA !?
�� 1:
DATA QUALIFIER CODES
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & laboratory practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greater than value given.
N Presumptive evidence for the presence of material. There is an indication that the analyte is present,
but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
LI Indicates that the compound was analyzed for but not detected. The specified component was not
detected. The reported value is the method detection limit.
V Analyte was detected in both sample and associated method blank. Data may not be accurate.
Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate.
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that
can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A BCS is not currently accredited for this analyte.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
WAN
CHAIN OF CUSTODY RECORD BCS? Laboratories
%ww.microbioservices.com 4609 NW 6th street, Building A
FL DOH Laboratory #E82924, EPA# FL01'147 Gainesville, FL 32609
I Tel. (3 ,2) 377-9272, Fax. (352) 377-5630
Client Name and Address: 1 A-C- �ti I:�y •; ,j� ` �; (`� �.� �, z'.�t��;�j Compliance Monitoring? F—]Yesr No
City/State/-Lip: .;'G• /(l. Lci{; �( /l'I ,�►! I�' ����r'�i - �i:: fc L ,mot bni ±, .? Project ID: V�U.t
Project Mianayer: /, 7 ,g i' Facility/Site: < IJ' C6;1& 1'
Telephone Number: Fax No.: Report To: 3'1,
Sampler Namt8: (11'rint) -1�: h >'�i? f�( Email: I h rGl a,-. ,;1 ���? �/ L-1�5 G• —
Sampler Signature: -- � �� %z invoice To: 5 -
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01/09/2019 10:05
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01/09/2019 10:05 -I— ;, } 01/091201910:05
�— Branch Residuals and Soils _ Branch Residuals and Soils
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I_ VD-1 1901067 1901068
Spr 1901066 01/09/2019 10:06 01/09/2019 10.05
01/09/2019 10:05
Method of Shipment: UPS/ Postal DI-11- FEDEX Other:
Reli g6iched b- : Date Time Received by: Date Time
Relinquished by: Date Time Received by BCS Laboratories: Date Time
INA I
Laboratory Comments:
CQ I
°C
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Custody Seal: Intact l/ Broken
N/
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Von Drehle Corporation
Cordova, NC
City of Rockingham IUP 0015
Mar-19
Biological Consulting Services
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3/11/19
< 0.07
< 0.6
1903150
3/11/19
< 0.07
< 0.6
1903151
3/11/19
0.07
0.700
1903152
3/11/19
< 0.07
< 0.6
1903153
3/11/19
< 0.07
< 0.6
1903154
3/11/19
0.07
0.700
1903155
3/11/19
< 0.07
< 0.6
Exceedances p
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Annual Pathogen
and Vector Attraction Reduction Form for Class A and Class B options.
inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
March 20, 2019
Robert Branch
Branch Residuals and Soils
8646 W. Market St. Suite 111
Greensboro NC 27409
336-510-0340
bbranch@branchrs.com
Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7
BCS ID: 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Cordova
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT !N FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
`. ;alaclHRA
Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
Cordova
Client Sample ID:
VD-1
BCS Sample ID:
1903149
Date Received: March 12, 2019 09:53
Amount Analyzed: 30.00 g
Analysis Start: March 12, 2019 11:00
Analyst: Greta Pallack, B.A.
Sample Date/Time: March 11, 2019 13:57
Sample Description: Biosolids
Amount Submitted:100ml bottle %Solids: 43.8
Receipt Temperature: 0.4 deg C Preserved: Yes
Analysis Stop Date: March 20, 2019 13:30
Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-2
BCS Sample ID:
Date Received:
Amount Analyzed
Analysis Start:
Analyst:
1903150
March 12, 2019 09:53
30.00 g
March 12, 2019 11:00
Greta Pallack, B.A.
Sample Date/Time: March 11, 2019 14:02
Sample Description: Biosolids
Amount Submitted:100ml bottle % Solids: 43.0
Receipt Temperature: 0.4 deg C Preserved: Yes
Analysis Stop Date: March 20, 2019 13:30
Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/]EC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AM
Aiwwl-
lacy
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-3
Sample Date/Time: March 11, 2019 14:07
BCS Sample ID: 1903151 Sample Description: Biosolids
Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 43.3
Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes
Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30
Analyst: Greta Pallack, B.A. Qualifier: None
Primary Value: 0.07 Salmonella MPN/mL sample analyzed
Secondary Value: 0.7 Salmonella MPN/4 dry grams
Analysis Notes: None
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-4
Sample Date/Time: March 11, 2019 14:12
BCS Sample ID: 1903152 Sample Description: Biosolids
Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 43.8
Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes
Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-5
Sample Date/Time: March 11, 2019 14:17
BCS Sample ID: 1903153 Sample Description: Biosolids
Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 44.0
Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes
Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-6
Sample Date/Time: March 11, 2019 14:22
BCS Sample ID: 1903154 Sample Description: Biosolids
Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 44.0
Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes
Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30
Analyst: Greta Pallack, B.A. Qualifier: None
Primary Value: 0.07 Salmonella MPN/mL sample analyzed
Secondary Value: 0.7 Salmonella MPN/4 dry grams
Analysis Notes: None
Page 4 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
�ISC-HfRA
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova
Client Sample ID: VD-7 Sample Date/Time: March 11, 2019 14:27
BCS Sample ID: 1903155 Sample Description: Biosolids
Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 44.0
Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes
Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
'�
��ac=lgRa
Client: Branch Residuals and Soils
Project: Cordova
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924. ISO/IEC 1 7025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
11ac-ls11RQGAAM
if
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I certify that I have examined I am familiar with the information submitted herein. The results pertain only to
analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the
analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted
documents. The analysis was authorized commissioned by the client. The resulting data are representative of
the analysis conducted on the material/samples/articles provided by the client (or client's representative)
it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate
method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS
Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any
sample, batch, source, or the process they are derived from. Quality assurance controls were performed as
outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report
meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH
Environmental Laboratory Certification Program, as applicable unless otherwise noted.
Signature of Laboratory Director/Authorized Rep.
Date: March 20, 2019
Page 7 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
laci�aAIIAB
DATA QUALIFIER CODES
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & laboratory practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greater than value given.
N Presumptive evidence for the presence of material. There is an indication that the analyte is present,
but the confirmation requirement was not met.
0 Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was not
detected. The reported value is the method detection limit.
V Analyte was detected in both sample and associated method blank. Data may not be accurate.
Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate.
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that
can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A BCS is not currently accredited for this analyte.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
aC'MRAAA6
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CHAIN OF CUSTODY RECORD
BCS Laboratories
www.microbioservices-com
4.609 NW 6th street, Building A
... ir�c.
FL DOH Laboratory #E82924, EPA# FL01147
FL
Gainesville; FL —
Tel. (352) 377-9272, Fax. (352) 377-5630
Client Name and Address:
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Compliance Monitoring? Yes❑
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Special Instructions: Laboratory Comments:
Method of Shipment: UPS Postal DHL FEDEX Other: Temp. @ recp't: i f `C
Relinqjished,6y� Date Time Received by: Date Time IR- Corrected f -IR
f / 7 Custody Seal: Intact I Broken
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Von Drehle Corporation
Cordova, NC
City of Rockingham IUP 0015
May-19
Biological Consulting Services
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5/15/19
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1905236
5/15/19
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1905237
5/15/19
< 0.07
< 0.8
1905238
5/15/19
< 0.07
< 0.7
1905239
5/15/19
< 0.07
< 0.7
1905240
5/15/19
< 0.07
<1 0.8
. . . . . . . . . . . . . . . . . . . . . . . .
Exceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Annual Pathogen
and Vector Attraction Reduction Form for Class A and Class B options.
3kinc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
May 21, 2019
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
bbranch@branchrs.com
Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7
BCS ID: 190S234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: N/A
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely,
J
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LAB0RATORIES
7�C=hfRA'A&B
\� +ccnco -cn
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD1
Sample Date/Time: May 15, 2019 14:07
BCS Sample ID: 1905234 Sample Description: Biosolids
Date Received: May 16, 2019 10:07 Amount Submitted:100 mL bottle % Solids: 30.5
Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes
Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.9 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD2
Sample Date/Time: May 15, 2019 14:09
BCS Sample ID: 1905235 Sample Description: Biosolids
Date Received: May 16, 2019 10:07 Amount Submitted:100 mL bottle % Solids: 40.4
Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes
Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISOAEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD3
BCS Sample ID:
Date Received:
Amount Analyzed
Analysis Start:
Analyst:
1905236
May 16, 2019 10:07
30.00 g
May 16, 2019 11:45
Wei -yea Hsu, M.S.
Sample Date/Time: May 15, 2019 14:12
Sample Description: Biosolids
Amount Submitted:100 mL bottle % Solids: 39.6
Receipt Temperature: 6.6 deg C Preserved: Yes
Analysis Stop Date: May 21, 2019 12:55
Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD4
BCS Sample ID: 1905237
Date Received:
Amount Analyzed:
Analysis Start:
Analyst:
May 16, 2019 10:07
30.00 g
May 16, 2019 11:45
Wei -yea Hsu, M.S.
Sample Date/Time: May 15, 2019 14:15
Sample Description: Biosolids
Amount Submitted:100 mL bottle % Solids: 32.5
Receipt Temperature: 6.6 deg C Preserved: Yes
Analysis Stop Date: May 21, 2019 12:55
Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 190S234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
;11^LEAA 1 102 � *J
,.o r .>
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD5
BCS Sample ID: 1905238
Date Received: May 16, 2019 10:07
Sample Date/Time: May 15, 2019 14:17
Sample Description: Biosolids
Amount Submitted:100 mL bottle % Solids: 35.7
Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes
Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD6
BCS Sample ID: 1905239
Date Received: May 16, 2019 10:07
Amount Analyzed: 30.00 g
Analysis Start: May 16, 2019 11:45
Analyst: Wei -yea Hsu, M.S.
Sample Date/Time: May 15, 2019 14:20
Sample Description: Biosolids
Amount Submitted:100 mL bottle % Solids: 36.4
Receipt Temperature: 6.6 deg C Preserved: Yes
Analysis Stop Date: May 21, 2019 12:55
Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
r yyqk
aCT
r
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD7
BCS Sample ID: 1905240
Date Received: May 16, 2019 10:07
Sample Date/Time: May 15, 2019 14:22
Sample Description: Biosolids
Amount Submitted:100 mL bottle % Solids: 34.4
Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes
Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
At"
.1,4•� ,,. eye.
Client: Branch Residuals and Soils
Project: N/A
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
. ,, e ?-
I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Signature of Laboratory Director/Authorized Rep.
Date: May 21, 2019
Page 7 of 8
Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/]EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
I alc-i R - rjj�',�
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X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
Value is between the laboratory method detection limit & laboratory practical quantitation
limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist forthe component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V
Analyte was detected in both sample and associated method blank. Data may not be accurate.
y The laboratory analysis was from an improperly preserved sample. The data may not be
accurate.
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analvsis notes.
Page 8 of 8
Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE
WRITTEN CONSENT OF BCS LABORATORIES
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CHAIN OF CUSTODY RECORD
www.microbioservices.com
FL DOH Laboratory #E82924, EPA# FLO1147
Client Name and Address:
City/State/Zip:
Project Manager:
Telephone Number: Fax No.:
Sampler Name: (Print)
Sampler Signature:
Preservative I Matrix
Project ID:
Facility/Site:
Report To:
Email:
Invoice To:
BCS Laboratories
4609 NW 6th street, Building A
Gainesville, FL 32609
Tel. (352) 377-9272, Fax. (352) 377-6630
Compliance Monitoring? Yes❑ No
Sample ID / Description
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Laoorarory Comments:
Method of
Shipment:
UPS
Postal DHL
FEDEY. Other: Temp. @ recp't:
66, -C
Reli�ishecJ by:
Date
Time
Received by:
Date Time IR-10
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Cordova, NC
City of Rockingham IUP 0015
Jul-19
Biological Consulting Services
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1907369
7/24/19
< 0.07
< 0.6
1907370
7/24/19
< 0.07
< 0.6
1907371
7/24/19
< 0.07
< 0.6
1907372
7/24/19
< 0.07
< 0.6
1907373
7/24/19
< 0.07
< 0.6
1907374
7/24/19
< 0.07
< 0.6
1907375
7/24/19
< 0.07
< 0.6
Exceedances
..............
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Annual Pathogen
and Vector Attraction Reduction Form for Class A and Class B options.
3inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLOR/DA, INC.
July 31, 2019
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
bbranch@branchrs.com
Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7
BCS ID: 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Cordova NC
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely, 1
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950. EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NC
Client Sample ID: VD1
Sample Date/Time: July 23, 2019 13:57
BCS Sample ID: 1907369 Sample Description: Biosolids
Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 46.4
Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes
Analysis Start: July 24, 2019 13:04 Analysis Stop Date: July 27, 2019 15:45
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NC
Client Sample ID: VD2
Sample Date/Time: July 23, 2019 13:59
BCS Sample ID: 1907370 Sample Description: Biosolids
Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 44.9
Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes
Analysis Start: July 24, 2019 13:09 Analysis Stop Date: July 27, 2019 15:45
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: _<0.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AAAB
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NC
Client Sample ID: VD3
Sample Date/Time: July 23, 2019 14:03
BCS Sample ID: 1907371 Sample Description: Biosolids
Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 43.2
Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes
Analysis Start: July 24, 2019 13:06 Analysis Stop Date: July 27, 2019 15:45
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NC
Client Sample ID: VD4
Sample Date/Time: July 23, 2019 14:07
BCS Sample ID: 1907372 Sample Description: Biosolids
Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 44.1
Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes
Analysis Start: July 24, 2019 13:09 Analysis Stop Date: July 27, 2019 15:45
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW. MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
Cordova NC
Client Sample ID:
VD5
BCS Sample ID:
1907373
Date Received:
July 24, 2019 9:54
Amount Analyzed:
30.00 g
Analysis Start:
July 24, 2019 13:12
Analyst:
Wei -yea Hsu, M.S.
Sample Date/Time: July 23, 2019 14:10
Sample Description: Biosolids
Amount Submitted:100 mL bottle % Solids: 42.9
Receipt Temperature: 7.8 deg C Preserved: Yes
Analysis Stop Date: July 27, 2019 15:45
Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NC
Client Sample ID: VD6
BCS Sample ID: 1907374
Date Received: July 24, 2019 9:54
Amount Analyzed: 30.00 g
Analysis Start: July 24, 2019 13:17
Sample Date/Time: July 23, 2019 14:15
Sample Description: Biosolids
Amount Submitted:100 mL bottle % Solids: 41.0
Receipt Temperature: 7.8 deg C Preserved: Yes
Analysis Stop Date: July 27, 2019 15:45
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
At"
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NC
Client Sample ID: VD7 Sample Date/Time: July 23, 2019 14:20
BCS Sample ID: 1907375 Sample Description: Biosolids
Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 40.5
Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes
Analysis Start: July 24, 2019 13:21 Analysis Stop Date: July 27, 2019 15:45
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
, C-QkA A&B
1�.
Client: Branch Residuals and Soils
Project: Cordova NC
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
�-, ► At"
I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Signature of Laboratory Director/Authorized Rep.
Date: July 31, 2019
Page 7 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/[EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
DATA QUALIFIER CODES
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greater than value given.
N Presumptive evidence forthe presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
0 Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:201 7 L2422 (ANAB), PA DEP# 68-03950, EPA# FL01 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
-=N1@A AM
CHAIN OF CUSTODY RECORD BCS Laboratories
~� www.microbloservices.com 4609 NW 6th street, Building A
'•`hrn ir1C.
FL DOH Laboratory #E82924, EPA# FL01147 Gainesville, FL 32609
C Tel. (352) 377-9272, Fax. (352) 377-5630
Client Name and Address: �j.2/-" 1"'s-I L � %s� � � j Compliance Monitoring? El Yes No
City/State/Zip: /-J3s yPckCB/,J J:A /c3 291 f � (� his 1 �C f �J� Project ID: ZuN- /l0
Project Manager: 86 Facility/Site:yu-1 Diaz Cu2JL, v a /,--I
Telephone Number: Fax No.: ReportTo:
Sampler Name: (Print) Email:c--
Sampler Signature: Invoice To:a-z y
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07/24/2019 9:54
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Von Drehle Corporation
Cordova, NC
City of Rockingham IUP 0015
Oct-19
Biological Consulting Services
.......................................
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10/02/19
< 0.07
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1910023
10/02/19
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1910024
10/02/19
< 0.07
< 0.6
1910025
10/02/19
< 0.07
< 0.6
1910026
10/02/19
< 0.07
< 0.6
1910027
10/02/19
< 0.07
< 0.7
1910028
10/02/19
< 0.07
< 0.6
Exceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Annual Pathogen
and Vector Attraction Reduction Form for Class A and Class B options.
Inc. BIOLOGICAL CONSULTING SERVICES
3 OF NORTH FLORIDA, INC.
October 08, 2019
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
bbranch@branchrs.com
Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7
BCS ID: 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Von Drehle
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (1SO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
4W
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Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD-1
Sample Date/Time: October 01, 2019 14:01
BCS Sample ID: 1910022 Sample Description: Biosolid
Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.7
Amount Analyzed: 30.06 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD-2
Sample Date/Time: October 01, 2019 14:06
BCS Sample ID: 1910023 Sample Description: Biosolid
Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 40.8
Amount Analyzed: 30.01 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: !90.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW. MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD-3
Sample Date/Time: October 01, 2019 14:09
BCS Sample ID: 1910024 Sample Description: Biosolid
Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.1
Amount Analyzed: 30.06 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD-4
Sample Date/Time: October 01, 2019 14:13
BCS Sample ID: 1910025 Sample Description: Biosolid
Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.4
Amount Analyzed: 30.01 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD-5
Sample Date/Time: October 01, 2019 14:17
BCS Sample ID: 1910026 Sample Description: Biosolid
Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.5
Amount Analyzed: 29.95 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD-6
Sample Date/Time: October 01, 2019 14:21
BCS Sample ID: 1910027 Sample Description: Biosolid
Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 40.1
Amount Analyzed: 29.91 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
— -- Page 4 of 8
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/]EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
I ^ U r,
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD-7 Sample Date/Time: October 01, 2019 14:25
BCS Sample ID: 1910028 Sample Description: Biosolid
Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 40.8
Amount Analyzed: 30.08 g Receipt Temperature: 4.4 deg C Preserved: Yes
Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: _<0.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Project: Von Drehle
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
n.ccnco <cn
I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
iCY��.�t'11��
Signature of Laboratory Director/Authorized Rep.
Date. October 08, 2019
Page 7 of 8
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/]EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950. EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
DATA QUALIFIER CODES
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist forthe component.
J3 The data are questionable because of improper laboratory orfield protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
U Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
- Page 8 of 8 —
Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
At"'"'
CHAIN OF CUSTODY RECORD
www.microbioservices.com
FL DOH Laboratory #E82924, EPA# FLO1147
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Client Name and Address: 71 I �'
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City/State/Zip:
Project Manager:
Telephone Number: Fax No.:
Sampler Name: (Print)
Sampler Signature: T$v�
BCS Laboratories
4609 NW 6th street, Building A
Gainesville, FL 32609
Tel. (352) 377-9272, Fax. (352) 377-5630
Compliance Monitoring? C�es[] No
Report To: (ta,e,(
Email: 4V%.r/�/�h 12s .
Quote #: -Ne)''
Project ID: Zc;,1q-/l0
Invoice To: �A)A,,�'-
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VD 5 VD-6
1910026 1910027
VD-3
1910025
10/02/2019 10:33
10/02/2019 10:33 10102/2019 10:33
t
1910024
Special Instructions:
1010212019 10:33
1 1
Laboratory Comments:
I
2 (0
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Method of
Shipment: UPS Postal
DHL
FEDEX
Other: Temp. @ recp't: 1
r
Relin ' hed �f
Da a
Time
Received by:
Dale
Time IR-
for IR
//
Presence of visable ice �5
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/ Y N
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Date
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Von Drehle Corporation
Cordova, NC
City of Rockingham IUP 0015
Dec-19
Biological Consulting Services
................................................
........
............................................
........................................
....................................
........................................
.........................
..................
............................ ..................
.......
.......
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.......
.......
1912179
12/12/19
< 0.07
< 0.6
1912180
12/12/19
0.07
0.800
1912181
12/12/19
< 0.07
< 0.7
1912182
12/12/19
< 0.07
< 0.6
1912183
12/12/19
< 0.07
< 0.6
1912184
12/12/19
< 0.07
< 0.7
1912185
12/12/19
< 0.07
< 0.6
Exceedances
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Annual Pathogen
and Vector Attraction Reduction Form for Class A and Class B options.
1
inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLOR/DA, INC.
December 19, 2019
Robert Branch
Branch Residuals and Soils
1735 Heckle Blvd. Suite 103-291
Rockhill SC 29732
336-312-9007
bbranch@branchrs.com
Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7
BCS ID: 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Von Drehle
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 191218S
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
OC7zmR�k A&B
l�� • ccn -
Client:
Branch Residuals and Soils
Analysis:
Salmonella
Project Name:
Von Drehle
Client Sample ID:
VD1
BCS Sample ID:
1912179
Date Received:
December 12, 2019 9:55
Amount Analyzed:
29.96 g
Analysis Start:
December 12, 2019 10:39
Sample Date/Time: December 11, 2019 14:14
Sample Description: Biosolid
Amount Su bm itted: 100 mL bottle % Solids: 45.0
Receipt Temperature: 3.9 deg C Preserved: Yes
Analysis Stop Date: December 17, 2019 9:28
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD2
BCS Sample ID:
Date Received:
1912180
Sample Date/Time: December 11, 2019 14:16
Sample Description: Biosolid
December 12, 2019 9:55 Amount Su bm itted: 100 mL bottle % Solids: 38.3
Amount Analyzed: 30.10 g Receipt Temperature:
Analysis Start: December 12, 2019 10:39 Analysis Stop Date:
Analyst: Wei -yea Hsu, M.S. Qualifier:
Primary Value: 0.07 Salmonella MPN/mL sample analyzed
Secondary Value: 0.8 Salmonella MPN/4 dry grams
Analysis Notes: None
3.9 deg C Preserved: Yes
December 18, 2019 9:50
None
Page 2 of 8
Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD3
Sample Date/Time: December 11, 2019 14:18
BCS Sample ID: 1912181 Sample Description: Biosolid
Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 40.0
Amount Analyzed: 30.09 g Receipt Temperature: 3.9 deg C Preserved: Yes
Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD4
Sample Date/Time: December 11, 2019 14:21
BCS Sample ID: 1912182 Sample Description: Biosolid
Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 44.7
Amount Analyzed: 30.08 g Receipt Temperature: 3.9 deg C Preserved: Yes
Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
A A0Ag
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD5
Sample Date/Time: December 11, 2019 14:23
BCS Sample ID: 1912183 Sample Description: Biosolid
Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 41.6
Amount Analyzed: 30.10 g Receipt Temperature: 3.9 deg C Preserved: Yes
Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD6
Sample Date/Time: December 11, 2019 14:25
BCS Sample ID: 1912184 Sample Description: Biosolid
Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 39.9
Amount Analyzed: 30.09 g Receipt Temperature: 3.9 deg C Preserved: Yes
Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAx. (352) 377-5630
WWW. MICROBIOSERVICES.COM
FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
_� - } TNI
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Von Drehle
Client Sample ID: VD7 Sample Date/Time: December 11, 2019 14:30
BCS Sample ID: 1912185 Sample Description: Biosolid
Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 43.7
Amount Analyzed: 30.10 g Receipt Temperature: 3.9 deg C Preserved: Yes
Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BC5 ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185
BCS LABORATORIES, INC. - GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Client: Branch Residuals and Soils
Project: Von Drehle
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
I certify that I have examined and I am familiar with the information submitted herein. The results pertain only
to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals
responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was
obtained from submitted documents. The analysis was authorized and commissioned by the client. The
resulting data are representative of the analysis conducted on the material/samples/articles provided by the
client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed
in accordance with the appropriate method , however due to the inherent limitations of the methods,
microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning
the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality
assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The
analysis and results presented in this report meet the requirements of the standards of The NELAC Institute
(TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless
otherwise noted.
Signature of Laboratory Director/Authorized Rep.
Date: December 19, 2019
Page 7 of 8
Final Report BCS ID 1912179, 1912190, 1912181, 1912182, 1912183, 1912184, 1912185
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
DATA QUALIFIER CODES
SYMBOL MEANING
B Results based on counts outside the acceptable range.
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit &the practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component.
J3 The data are questionable because of improper laboratory or field protocols.
L Off scale high. Actual value is known to be greaterthan value given.
N Presumptive evidence forthe presence of material. There is an indication that the analyte is
present, but the confirmation requirement was not met.
0 Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
L1 Indicates that the compound was analyzed for but not detected. The specified component was
not detected. The reported value is the method detection limit.
V Analyte was detected in both sample and the method blank. Data may not be accurate.
Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate
Z Too many colonies present (TNTC); the numeric value given represents the upper end of the
value that can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
** Not reported due to interference.
A Sampling container supplied by client. Sterility can not be confirmed by BCS.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. (352) 377-9272, FAX. (352) 377-5630
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
11G=iAf3i4'Ai&B
CHAIN OF CUSTODY RECORD
www.microbioservices.corn
Inc . FL DOH Laboratory #E82924, EPA# FL01147
Client
Name and Address:
City/State/Zip:
Project Manager:
15,-�
Telephone Number:
Fax No.:
Sampler Name: (Print)
Sampler Signature:
rti
0roc-fival M.friv
BCS Laboratories
4609 NW 6th street, Building A
Gainesville, FL 32609
Tel. (352) 377-9272, Fax. (352) 377-5630
Compliiaar Toniton g? CYes❑ No
Report To:n�r^r (Y� ✓` r ''
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Special Instructions:
Laboratory Comments:
I
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Method of Shipment: C UPS Postal DHL FEDEX Other:
Temp. @ recp't: 7 = •C
�',y IR-Y1;Corrected for IR
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SOIL ANALYSIS REPORTS
Page 1 of 4
Report Number: 19-193-0701
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Date Received: 07/12/2019
0
Waypoint
ANALYTICAL
'Every acre... Everyyear. "na
Date Of Analysis: 07/15/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 a Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle
Farm: US-1
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss on Ignition Water pH
Date Of Report: 07/24/2019 NC = North Carolina Fertility Index Value
Sample ID
Field ID
Lab
Number
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
%
Rate
Soil
Class
Ibs/A
M3
pprn Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
1
30965
2.9
L
102
18 M
NC = 15
14 VL
NC = 7
84 M
8124 VH
31
VL
8.1
0.0
41.5
MIN
2
30966
2.9
L
102
37 H
NC=31
13 VL
NC=7
113 M
18120 VH
42
VL
8.1
0.0
41.8
MIN
3
30967
3.3
M
110
28 M
NC=23
11 VL
NC=6
107 M
8100 VH
30
VL
8.1
0.0
41.6
MIN
4
30968
3.1
M
106
19 M
NC = 16
20 VL
NC = 10
97 M
8124 VH
29
VL
7.9
0.0
41.6
MIN
5
30969
5.2
H
148
8 L
NC=7
16 VL
NC=8
108 M
8079 VH
31
VL
8.2
0.0
41.5
MIN
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Exchangeable
Sodium
Percentage
%
K
%
Mg
%
Ca
%
Na
%
H
%
NO3N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
1
0.1
1.7
97.9
0.3
0.0
16 M
NC=33
10.7 VH
NC=267.5
5 VL
NC=31
14 VL
1.7 M
NC=85.0
0.6
H
0.020
2
0.1
2.3
97.1
0.4
0.0
21 H
NC=44
12.2 VH
NC=305.0
8 VL
NC:
22 VL
1.9 M
NC=95.0
0.6
H
0.140
3
0.1
2.1
97.4
0.3
0.0
16 M
NC=33
11.6 VH
NC=290.0
6 VLJ
NC=38
16 VL
1.9 M
NC=95.0
0.5
M
0.130
4
0.1
1.9
97.6
0.3
0.0
16 M
NC=33
11.1 VH
NC=277.5
6 VL
NC=38
14 VL
1.2 M
NC=60.0
0.7
H
0.140
5
0.1
2.2
97.3
0.3
0.0
20 M
NC=42
14.5 VH
NC=362.5
8 VL
NC=50
6 VL
1.2 M
NC=60.0
0.7
H
0.130
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by
Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Tennessee, Inc.
Oscar Ruiz
Page 2 of 4
Report Number: 19-193-0701
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Date Received: 07/12/2019
Date Of Report: 07/24/2019
Waypoi t0
ANALYTICAL
"Every acre... Every year.".
Farm: US-1
SOIL FERTILITY RECOMMENDATIONS
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
KZO
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
bu/acre
Tons/A
lb/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
1
Soybeans
50
0.0
0
72
150
16
12
0
6
0
0
2
Soybeans
50
0.0
0
30
150
0
0
0
6
0
0
3
Soybeans
50
0.0
0
52
150
0
12
0
6
0
0.5
4
Soybeans
50
0.0
0
70
150
10
12
0
6
0
0
5
Soybeans
50
0.0
0
98
150
0
10
0
6
0
0
Comments:
30965
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30966
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30967
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30968
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30969
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
Sample(s)
: 2,3,4,5 Crop: Soybeans
For soybeans on soils with a pH of 6.2 or less, apply limestone as recommended and plant seed treated with molybdenum. Apply 1-2 oz of sodium molybdate (0.4-0.8 oz
of elemental molybdenum) per acre as a seed treatment.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �•
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the f�
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Oscar Ruiz
Page 3 of 4
Report Number: 19-193-0701
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Date Received: 07/12/2019
Waypoi nt "0
ANALYTICAL
"Every acre... Every year. "n,,
Date Of Analysis: 07/15/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 a Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle
Farm: US-1
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Of Report: 07/24/2019 NC = North Carolina Fertility Index Value
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Rate
Soil
Class
IbslA
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
6A
30970
2.4
L
92
13 L
NC = 11
43 VL
NC = 22
98 M
8114 VH
34
VL
8.0
0.0
41.6
MIN
6B
30971
4.8
M
140
12 L
NC = 10
27 VL
NC = 14
118 M
8068 VH
40
VL
7.8
0.0
41.6
MIN
7
30972
4.1
M
126
15 M
NC = 12
19 VL
NC = 10
111 M
8084 VH
26
VL
8.0
0.0
41.5
MIN
8
30973
4.1
M
126
11 L
NC=9
24 VL
NC 12
119 M
8075 VH
32
VL
8.2
0.0
41.6
MIN
9
30975
5.3
HH
150
13 L
NC = 11
49 VL
NC = 25
120 M
�8068 VH
31
VL
8.0
0.0
41.6
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Exchangeable
Sodium
Percentage
%
K
%
Mg
1
Ca
%
Na
%
H
%
NO3N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
6A
0.3
2.0
97.5
0.4
0.0
17 M
NC=35
10.1 VH
NC=252.5
7 VL
NC=44
17 VL
0.8 L
NC=40.0
0.5
M
0.060
6B
0.2
2.4
97.0
0.4
0.0
22 H
NC=46
14.0 VH
NC=350.0
7 VL
NC=44
19 VL
2.1 M
NC=105.0
0.7
H
0.210
7
0.1
2.2
97.4
0.3
0.0
18 M
NC=37
13.5 VH
NC=337.5
5 VL
NC=31
11 VL
1.4 M
NC=70.0
0.7
H
0.110
8
0.1
2.4
97.1
0.3
0.0
19 M
NC=40
13.2 VH
NC=330.0
7 VL
NC=44
12 VL
1.6 M
NC=80.0
0.7
H
0.050
9
0.3
2.4
97.0
0.3
0.0
23 H
NC=48
15.4 VH
NC=385.0
7 VL
NC
12 VL
1.6 M
NC=80.0
0.8
H
0.150
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are relainnd a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Tennessee, Inc. by-.
Salts ms/cm x 640 = ppm.
Oscar Ruiz
Page 4 of 4
Report Number: 19-193-0701
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Date Received: 07/12/2019
Date Of Report: 07/24/2019
Waypoint,0
ANALYTICAL
"Every acre... Every year. ".
Farm: US-1
SOIL FERTILITY RECOMMENDATIONS
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
field Goal
Lime
N
P205
KZO
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
bulacre
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
6A
Soybeans
50
0.0
0
83
150
10
11
0
6
1.0
0.5
6B
Soybeans
50
0.0
0
86
150
0
0
0
6
0
0
7
Soybeans
50
0.0
0
78
150
0
11
0
6
0
0
8
Soybeans
50
0.0
0
89
150
0
10
0
6
0
0
9
Soybeans
50
0.0
0
83
150
0
0
0
6
0
0
'omments:
30970
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30971
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30972
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30973
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
30975
Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
If you
have questions, please call the lab.
Sample(s) : 6B,7,8,9 Crop: Soybeans
For soybeans on soils with a pH of 6.2 or less, apply limestone as recommended and plant seed treated with molybdenum. Apply 1-2 oz of sodium molybdate (0.4-0.8 oz
of elemental molybdenum) per acre as a seed treatment.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �•
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Oscar Ruiz
Page 1 of 4
Report Number: 19-305-0910
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
■
Waypoint
ANALYTICAL
"Every acre... Every year. "rM
SOIL ANALYSIS REPORT
Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/02/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 a Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle Cordova
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
NC = North Carolina Fertility Index Value
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
1
64132
2.5
L
94
10 L
NC=8
15 VL
NC=B
115 M
9424 VH
69
VL
8.2
0.0
98.4
I MIN
2
64133
2.3
L
90
4 L
NC=3
17 VL
NC=9
127 M
15873 VH
69
VL
8.3
0.0
130.8
MIN
3A
64134
3.1
M
106
2 VL
NC = 2
16 VL
NC = 8
126 M
11085 VH
41
VL
8.4
0.0
106.7
MIN
3B
64135
2.4
L
92
6 L
NC = 5
12 VL
NC = 6
127 M
6050 VH
80
VL
8.2
0.0
131.7
MIN
4
64136
4.1
MH
126
5 L
NC = 4
17 VL
NC = 9
129 M
17385 VH
73
VL
8.3
0.0
138.4
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
K
Mg
%
Ca
%
Na
%
H
%
NO3 N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
1
0.0
1.0
98.7
0.3
0.0
17 M
NC = 35
10.9 VH
NC = 272.5
5 VL
NC = 31
25 L
2.1 M
NC = 105.0
0.8
H
2
0.0
0.8
98.9
0.2
0.0
23 H
NC=48
13.6 VH
NC=340.0
5 VL
NC=31
20 VL
1.4 M
NC=70.0
0.8
H
3A
0.0
1.0
98.8
0.2
0.0
16 M
NC=33
10.8 VH
NC=270.0
5 VL
NC=31
17 VL
0.9 M
NC=45.0
0.6
H
3B
0.0
0.8
98.9
0.3
0.0
28 H
NC=58
12.6 VH
NC=315.0
5 VL
NC=31
18 VL
1.0 M
NC=50.0
0.9
H
4
0.0
0.8
98.9
0.2
0.0
31 H
NC=64
15.6 VH
NC=390.0
6 VL
NC=38
18 VL
1.2 M
NC=60.0
1.0
H
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. -Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a �.
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by:✓'�
Salts ms/cm x 640 = ppm. Analysis prepared by Waypoint Analytical Tennessee Inc
Oscar Ruiz
Page 2 of 4
Report Number: 19-305-0910 a ►�°
Account Number: 22972 Waypol nt w _ 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
Send To: Branch Residuals and Soils LLC ANALYTICAL www.waypointanalytical.com
Mr. Bob Branch "Every acre... Every year. ".M Grower: Von Drehle Cordova
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Comments:
64132 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you
have questions, please call the lab.
64133 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you
have questions, please call the lab.
64134 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you
have questions, please call the lab.
64135 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you
have questions, please call the lab.
64136 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you
have questions, please call the lab.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �.
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Oscar Ruiz
Page 3 of 4
Report Number: 19-305-0910
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Waypoi t.0
ANALYTICAL
"Every acre... Every year. "rM
SOIL ANALYSIS REPORT
Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/02/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 a Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle Cordova
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
NC = North Carolina Fertility Index Value
Sample ID
Field ID
Lab
Number
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
%
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
5
64137
3.1
M
106
4 L
NC = 3
23 VL
NC = 12
118 M
8416 VH
87 VL
8.2
0.0
93.5
I MIN
6A
64138
2.0
L
84
4 L
NC = 3
12 VL
NC = 6
97 M
9982 VH
67 VL
8.0
0.0
51.0
MIN
6B
64139
1.8
VLH
80
3 VL
INC = 2
13 VL
NC = 7
93 M
8301 VH
34 VL
8.3
0.0
42.5
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
K
%
Mg
"fie
Ca
"fie
Na
%
H
%
NOs N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
5
0.1
1.1
98.5
0.4
0.0
38 H
NC=79
10.4 VH
NC=260.0
5 VL
NC=31
18 VL
0.8 L
NC=40.0
1.3 H
6A
0.1
1.6
97.9
0.6
0.0
25 H
NC=52
6.7 H
NC=167.5
4 VL
NC=25
25 L
0.6 L
NC=30.0
0.7 H
6B
0.1
1.8
97.7
0.3
0.0
15 M
NC=31
6.3 H
NC=157.5
3 VL
NC=19
21 VL
0.5 L
NC=25.0
0.6 H
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble prepared Analysis re b : Wa by.
Salts ms/cm x 640 = ppm. Y P P Y ypoinlMalytical Tennessee Inc
Oscar Ruiz
Page 4 of 4
Report Number: 19-305-0910
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Comments:
Waypoi t(D
ANALYTICAL
"Every acre... Every year",.
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle Cordova
64137 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
have questions, please call the lab.
64138 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
have questions, please call the lab.
64139 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated.
have questions, please call the lab.
'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977
If you
If you
If you
Page 1 of 2
Report Number: 19-305-9155
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Waypoint(D
ANALYTICAL
"Every acre... Every year. "rM
SOIL ANALYSIS REPORT
Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/15/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle Cordova
Analytical Method(s):
NC = North Carolina Fertility Index Value
Sample ID
Field ID
Lab
Number
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
%
Rate
Soil
Class
Ibs/A
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
1
88700
2
88701
3A
88702
3B
88703
4
88704
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Cation
Exchange
Capacity
meg1100g
Exchangeable
Sodium
Percentage
%
K
%
Mg
%
Ca
%
Na
%
H
%
NO3 N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
1
5.40
2.82
2
5.10
3.18
3A
5.10
2.58
3B
5.40
4.24
4
7.90
3.01
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a 11-6501.-,
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, SolubleC.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysts prepared by: waypoint Analytical Tennessee, Inc.
Jimmy R. Ferguson
Page 2 of 2
Report Number: 19-305-9155
Account Number: 22972
Send To: Branch Residuals and Soils LLC
Mr. Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill SC 29732
Waypoint
ANALYTICAL
"Every acre... Every year. ".
SOIL ANALYSIS REPORT
Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/15/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
www.waypointanalytical.com
Grower: Von Drehle Cordova
Analytical Method(s):
NC = North Carolina Fertility Index Value
Sample ID
Field ID
Lab
Number
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
%
Rate
Soil
Class
Ibs/A
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
5
88705
6A
88706
6B
88707
Sample ID
Field ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Cation
Exchange
Capacity
meq/100g
Exchangeable
Sodium
Percentage
%
K
%
Mg
%
Ca
%
Na
%
H
%
NO3N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
5
5.90
4.72
6A
5.70
2.14
6B
5.90
2.39
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium)
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis
Salts ms/cm x 640 = ppm. alysis prepared by Waypoinl Analytical Tennessee Inca
Jimmy R. Ferguson
2019 APPLICATION SUMMARY TABLE
VON DREHLE CORPORATION
LAND APPLICATION PROGRAM
PERMIT NO. WQ0005135
2019 APPLICATION SUMMARY
......
............
e ...
... .....
........ ......
..............
..........................................
.......... ................
Vi'e ...................
....... ..................
...........
.............
..
........
...............
.....ad .
... .... ..
...... .........
....................
..................
...............................
'Tons...
... ...... .........
.............
...
.............
...... ... ..
.......
. ........
Dry 'Tons ..
... .........
............
.........
.......
.......... .
................
...........................
................
..... .........
......
.........................
..............
...........
-op.-
..
.......
...............
....
........ ......
3
1
23
Jul-19
1449.28
34.4
21.68
498.55
Rye
6.53
2
9.1
Jul-19
507.95
34.4
19.20
174.73
Rye
5.79
3A
18.9
Jul- 19
1108
34.4
20.17
381.15
Rye
6.08
3 B
37.2
Aug-19
2260.35
34.4
20.90
777.56
Rye
6.30
4
13.2
Aug-19
761.6
34.4
19.85
261.99
Rye
5.98
5
11.1
Aug- 19
729.4
34.4
22.60
250.91
Rye
6.81
6A
24.6
Sep-19
1324.29
36.6
19.70
484.69
Rye
6.10
6B
37.5
Aug-19
1738.66
34.4
15.95
598.10
Rye
5.47
Sep-19
221.3
36.6
2.16
81.00
Rye
4
1
19.1
Mar-19
1178.33
40.8
25.17
480.76
Milleft.
10.46
2
37.1
Mar-19
2227.31
40.8
24.49
908.74
Millett
10.18
3
22.4
Mar-19
1358.27
40.8
24.74
554.17
Millett
10.28
4
50.8
Feb-19
2134.51
32.6
13.70
695.85
Millett
13.77
Mar-19
1046.06
40.8
8.40
426.79
Millett.
5
11.1
Mar-19
686.76
40.8
25.24
280.20
Millett
10.49
6A
18.9
Mar-19
1104.69
40.8
23.85
450.71
Millett
9.91
6B
19.3
Mar-19
1132.03
40.8
23.93
461.87
Millett
9.94
7
19.2
Feb- 19
1160.31
32.6
19.70
378.26
Millett
14.78
8
28.9
Jan-19
1713.55
32.6
19.33
558.62
Millett.
14.50
9
28.6
Jan-19
1606.2
32.6
18.31
523.62
Millett 1
13.73
Total Acreage 430
von Drehle
[is
Wet Tons
Dry Tons
Permit
Limit
25,448.8]5
9,228.29
12,500
Branch Residuals Soils, LLC Confidential 1/31/2020 Page 1
2019 APPLICATION CONDITION SUMMARIES
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
Jan- Feb 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 50.8
Site/Tract: 4
Application Method: Incorporated
Field: 4
Percent Solids: 32.6
Residual Report No.: vd 2019-1 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
2/13/19
4
289.25
Warm,Cloud
Dry
0.33
2/14/19
4
142.38
Cool,Clear
Moist
0.00
2/15/19
4
168.83
Cool,Clear
Dry
0.00
2/18/19
4
193.10
Cool,Cloudy
Dry
0.13
2/19/19
4
239.67
Cool,Clear
Dry
0.00
2/20/19
4
22.32
Cool,Cloudy
Dry
0.21
2/21/19
4
194.52
Cool,Cloudy
Moist
0.05
2/25/19
4
288.98
Warm,Clear
Dry
0.00
2/26/19
4
298.82
Cool,Clear
Dry
0.00
2/27/19
4
296.64
Cool,Clear
Dry
0.00
Total Wet Tons
2,134.51
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
Jan- Feb 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 19.2
Site/Tract: 4
Application Method: Incorporated
Field: 7
Percent Solids: 32.6
Residual Report No.: vd 2019-1 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
2/4/19
7
71.10
Cool,Cloudy
Dry
0.01
2/5/19
7
216.15
Warm,Clear
Dry
0.00
2/6/19
7
244.77
Warm,Clear
Dry
0.00
2/7/19
7
101.19
Warm,Clear
Dry
0.00
2/8/19
7
120.52
Warm,Clear
Dry
0.00
2/11/19
7
166.00
Cool,Cloudy
Dry
0.01
2/12/19
7
240.58
Cool,Cloudy
Dry
0.07
Total Wet Tons
1,160.31
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
Jan- Feb 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 28.9
Site/Tract: 4
Application Method: Incorporated
Field: 8
Percent Solids: 32.6
Residual Report No.: vd 2019-1 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
1/22/19
8
209.55
Cold,Clear
Dry
0.00
1/28/19
8
411.10
Cool,Clear
Dry
0.00
1/29/19
8
211.54
Cool,Clear
Dry
0.00
1/30/19
8
217.87
Cool,Cloudy
Dry
0.20
1/31/19
8
260.82
Cool,Clear
Dry
0.00
2/1/19
8
118.27
Cool,Clear
Dry
0.00
2/4/19
8
284.40
Cool,Cloudy
Dry
0.01
Total Wet Tons
1,713.95
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
Jan- Feb 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 28.6
Site/Tract: 4
Application Method: Incorporated
Field: 9
Percent Solids: 32.6
Residual Report No.: vd 2019-1 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Feather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
1/14/19
9
335.93
Cool,Cloudy
Moist
0.14
1/15/19
9
330.24
Cool,Clear
Dry
0.00
1/16/19
9
158.57
Cool,Clear
Dry
0.00
1/17/19
9
189.53
Cool,Clear
Dry
0.00
1/18/19
9
143.74
Cool,Cloudy
Dry
0.17
1/21/19
9
239.23
Cool,Clear
Moist
0.00
1/22/19
9
94.00
Cold,Clear
Dry
0.00
1/23/19
9
114.96
Cool,Clear
Dry
0.00
Total Wet Tons
1,606.20
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
March -April 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 19.1
Site/Tract: 4
Application Method: Incorporated
Field: 1
Percent Solids: 40.8
Residual Report No.: vd 2019-2 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
3/29/19
1
140.28
Warm,Clear
Dry
0.00
4/1/19
1
431.16
Warm,Clear
Dry
0.00
4/11/19
1
255.90
Warm,Clear
Dry
0.00
4/15/19
1
350.99
Warm,Cloudy
Dry
0.07
4/16/19
1
0.00
Warm,Clear
Dry
0.00
4/17/19
1
0.00
Warm,Clear
Dry
0.00
Total Wet Tons
1,178.33
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
March -April 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 37.1
Site/Tract: 4
Application Method: Incorporated
Field: 2
Percent Solids: 40.8
Residual Report No.: vd 2019-2 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
3/11/19
2
427.04
Warm,Clear
Dry
0.00
3/12/19
2
204.54
Warm,Clear
Dry
0.00
4/3/19
2
352.28
Cool,Cloudy
Dry
0.14
4/4/19
2
329.93
Warm,Cloudy
Moist
0.01
4/5/19
2
142.02
Warm,Cloudy
Dry
0.10
4/8/19
2
294.82
Warm,Clear
Dry
0.00
4/9/19
2
141.56
Wann,Cloudy
Dry
0.43
4/10/19
2
237.42
Warm,Cloudy
Moist
0.10
4/11/19
2
97.70
Warm,Clear
Dry
0.00
Total Wet Tons
2,227.31
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
March -April 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 22.4
Site/Tract: 4
Application Method: Incorporated
Field: 3
Percent Solids: 40.8
Residual Report No.: vd 2019-2 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Feather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
3/5/19
3
333.59
Cool,Clear
Moist
0.00
3/6/19
3
367.40
Cool,Clear
Dry
0.00
3/7/19
3
411.36
Cool,Clear
Dry
0.00
3/8/19
3
145.44
Cool,Clear
Dry
0.00
3/11/19
3
100.48
Warm,Clear
Dry
0.00
Total Wet Tons
1,358.27
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
March -April 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 50.8
Site/Tract: 4
Application Method: Incorporated
Field: 4
Percent Solids: 40.8
Residual Report No.: vd 2019-2 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
3/1/19
4
277.69
Warm,Cloudy
Dry
0.26
3/13/19
4
175.75
Cool,Clear
Dry
0.00
3/14/19
4
135.34
Cool,Clear
Dry
0.00
3/15/19
4
117.97
Warm,Clear
Dry
0.00
3/18/19
4
267.49
Cool,Clear
Dry
0.00
3/19/19
4
71.82
Cool,Clear
Dry
0.00
Total Wet Tons
1 1,046.06
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
March -April 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 11.1
Site/Tract: 4
Application Method: Incorporated
Field: 5
Percent Solids: 40.8
Residual Report No.: vd 2019-2 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
3/21/19
5
220.46
Cool,Cloudy
Dry
0.32
3/22/19
5
102.35
Cool,Clear
Moist
0.00
3/25/19
5
246.95
Warm,Clear
Dry
0.00
3/26/19
5
0.00
Wann,Cloudy
Dry
0.40
4/16/19
5
117.00
Warm,Clear
Dry
0.00
Total Wet Tons
686.76
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
March -April 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 18.9
Site/Tract: 4
Application Method: Incorporated
Field: 6A
Percent Solids: 40.8
Residual Report No.: vd 2019-2 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
3/19/19
6A
167.58
Cool,Clear
Dry
0.00
3/20/19
6A
288.18
Cool,Clear
Dry
0.00
3/21/19
6A
0.00
Cool,Cloudy
Dry
0.32
4/15/19
6A
168.00
Warm,Cloudy
Dry
0.07
4/16/19
6A
287.91
Warm,Clear
Dry
0.00
4/17/19
6A
193.02
Warm,Clear
Dry
0.00
Total Wet Tons
1,104.69
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
March -April 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 19.3
Site/Tract: 4
Application Method: Incorporated
Field: 6B
Percent Solids: 40.8
Residual Report No.: vd 2019-2 MB
Crop: Millet
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
3/25/19
6B
235.47
Warm,Clear
Dry
0.00
3/26/19
6B
326.47
Warm,Cloudy
Dry
0.40
3/27/19
6B
236.51
Cool,Cloudy
Moist
0.10
3/28/19
6B
286.82
Cool,Clear
Dry
0.00
3/29/19
6B
46.76
Warm,Clear
Dry
0.00
3/30/19
6B
0.00
Warm,Clear
Dry
0.00
4/1/19
6B
0.00
Warm,Clear
Dry
0.00
4/8/19
6B
0.00
Warm,Clear
Dry
0.00
Total Wet Tons
1,132.03
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
July- Aug 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 23
Site/Tract: 3
Application Method: Incorporated
Field: 1
Percent Solids: 34.4
Residual Report No.: vd 2019-4 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
7/15/19
1
209.87
Hot,Clear
Dry
0.00
7/16/19
1
391.38
Hot,Clear
Dry
0.00
7/17/19
1
202.78
Hot,Clear
Dry
0.00
7/18/19
1
115.04
Hot,Cloudy
Dry
0.48
7/19/19
1
161.78
Hot,Clear
Moist
0.00
7/22/19
1
307.41
Hot,Clear
Moist
0.00
7/23/19
1
61.02
Hot,Clear
Dry
0.00
Total Wet Tons
1,449.28
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
July- Aug 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 9.1
Site/Tract: 3
Application Method: Incorporated
Field: 2
Percent Solids: 34.4
Residual Report No.: vd 2019-4 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Feather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
7/23/19
2
223.74
Hot,Clear
Dry
0.00
7/24/19
2
284.21
Hot,Cloudy
Dry
0.01
Total Wet Tons
1 507.95
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
July- Aug 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 18.9
Site/Tract: 3
Application Method: Incorporated
Field: 3A
Percent Solids: 34.4
Residual Report No.: vd 2019-4 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
7/25/19
3A
225.23
Warm,Clear
Moist
0.00
7/26/19
3A
174.69
Warm,Clear
Dry
0.00
7/29/19
3A
314.87
Hot,Clear
Dry
0.00
7/30/19
3A
346.79
Hot,Clear
Dry
0.00
8/1/19
3A
46.42
Hot,Clear
Dry
0.00
Total Wet Tons
1,108.00
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
July- Aug 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 37.2
Site/Tract: 3
Application Method: Incorporated
Field: 3B
Percent Solids: 34.4
Residual Report No.: vd 2019-4 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
8/1/19
3B
324.94
Hot,Clear
Dry
0.00
8/2/19
3B
276.87
Hot,Cloudy
Dry
0.16
8/5/19
3B
302.82
Hot,Cloudy
Dry
0.11
8/6/19
3B
200.14
Warm,Cloudy
Moist
0.45
8/7/19
3B
291.18
Hot,Cloudy
Moist
0.10
8/8/19
3B
234.82
Hot,Clear
Dry
0.00
8/9/19
3B
164.81
Hot,Clear
Dry
0.00
8/12/19
3B
301.01
Hot,Clear
Dry
0.00
8/13/19
3B
163.76
Hot,Clear
Dry
0.00
Total Wet Tons
2,260.35
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
July- Aug 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 13.2
Site/Tract: 3
Application Method: Incorporated
Field: 4
Percent Solids: 34.4
Residual Report No.: vd 2019-4 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
8/13/19
4
81.88
Hot,Clear
Dry
0.00
8/14/19
4
239.10
Hot,Cloudy
Dry
0.29
8/15/19
4
276.12
Hot,Cloudy
Moist
0.06
8/16/19
4
164.50
Hot,Clear
Moist
0.00
Total Wet Tons
761.60
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
July- Aug 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 11.1
Site/Tract: 3
Application Method: Incorporated
Field: 5
Percent Solids: 34.4
Residual Report No.: vd 2019-4 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Feather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
8/16/19
5
47.00
Hot,Clear
Moist
0.00
8/19/19
5
306.84
Hot,Cloudy
Dry
0.10
8/20/19
5
281.73
Hot,Clear
Dry
0.00
8/21/19
5
93.83
Hot,Cloudy
Dry
0.08
Total Wet Tons
729.40
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
July- Aug 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 37.5
Site/Tract: 3
Application Method: Incorporated
Field: 6B
Percent Solids: 34.4
Residual Report No.: vd 2019-4 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
8/21/19
6B
187.60
Hot,Cloudy
Dry
0.08
8/22/19
6B
189.34
Hot,Clear
Dry
0.00
8/23/19
6B
162.65
Hot,Cloudy
Dry
0.16
8/26/19
6B
277.87
Warm,Clear
Dry
0.00
8/27/19
6B
210.02
Warm,Clear
Dry
0.00
8/28/19
6B
264.99
Warm,Clear
Dry
0.00
8/29/19
6B
226.91
Hot,Clear
Dry
0.00
8/30/19
6B
219.28
Warm,Clear
Dry
0.00
Total Wet Tons
1,738.66
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
Sept -Oct 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 24.6
Site/Tract: 3
Application Method: Incorporated
Field: 6A
Percent Solids: 36.6
Residual Report No.: vd 2019-5 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
9/2/19
6A
110.65
Warm,Clear
Dry
0.00
9/3/19
6A
263.33
Hot,Clear
Dry
0.00
9/4/19
6A
227.47
Hot,Clear
Dry
0.00
9/5/19
6A
221.81
Hot,Cloudy
Dry
0.24
9/6/19
6A
250.26
Warm,Cloudy
Moist
0.00
9/9/19
6A
250.77
Hot,Clear
Dry
0.00
Total Wet Tons
1,324.29
von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
Sept -Oct 2019
von Drehle Paper
Farmer: Wayne Belger
Acres: 37.5
Site/Tract: 3
Application Method: Incorporated
Field: 6B
Percent Solids: 36.6
Residual Report No.: vd 2019-5 MB
Crop: Rye
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
9/2/19
6B
221.30
Warm,Clear
Dry
0.00
Total Wet Tons
221.30