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HomeMy WebLinkAboutWQ0005135_Residual Annual Report 2019_20200225Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application r Annual Report what is the submittal r Residual Annual Report type?* r Additional Information r Other Annual Report 2019 Year* Date Paper Copy 2/25/2020 Received:* Project Number* WQ0005135 Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues. .......................................................................................................................................................................................................................................................................................................................................................................... Name * Robert T. Branch Email Address* bbranch@branchrs.com Project Information Submittal Type* r New Permit Application r Renewal r Annual Report r Other Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted? r Yes r Nor N/A Permit Number* WQ0005135 ApplicantTermittee * von Drehle Corporation Facility Name * von Drehle Corporation Class B Phone Number* 336.312-9007 r Modification (Major or Minor) r Additional Information r Residual Annual Report r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Class B Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) vd_2019ar final.pdf 6.34MB upload only 1 RDF document. NL@iple documents must be combined into one RDF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required, be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been received. The paper copy shall include the following: o Application Form o All relevant attachments {talcs, soils report, specs, etc.] o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) Mailine address: Division of Water Resources ! Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W - = Raleigh, NC 27699-1617 S12 N.5alisburySt. For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560. * rJ By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/20/2020 2019 ANNUAL REPORT VON DREHLE CORPORATION CLASS B CORDOVA, NORTH CAROLINA PERMIT #WQ0005135 Prepared For: Von Drehle Corporation 126 First Street Cordova, North Carolina 28330 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill, SC 29732 February 2020 BRANCH RESIDUALS & SOILS, LLC 8646 W. Market St. - Suite 111 • Greensboro, NC 27409 PHONE (336) 510-0340 • Fax (336) 510-0341 February 26, 2020 North Carolina Department of Environmental Quality Division of Water Resource — Non -discharge Permitting Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2019 LAND APPLICATION ANNUAL REPORT Von Drehle Corporation Cordova, North Carolina Permit No. WQ0005135 Branch Residuals & Soils Project No. 2014-110 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of the Von Drehle Corporation. This data includes: 1) Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen and Vector Attraction Reduction Forms, 8) Fecal and Salmonella Results, 9) Soils Lab Data, 10) 2019 Application Summary Table, and 11) 2019 Application Condition Summaries. Total production for 2019 was 59,495.35 wet tons for this facility. Disposal/applications were as follows: • 11,186.31 wet tons being sent to the landfill, • 22,860.19 wet tons sent for application in South Carolina under Belger farms permit • 0.0 wet tons applied as Class A under separate permit, and • 25,448.85 wet tons applied to the farms in North Carolina. A total of 25,448.85 wet tons (9,228.29 dry tons) of residual by-product paper were land applied to the farms at US and Hamlet (430 acres). Hamlet sites received 40 lbs/acre nitrogen topdressing in March 2019. The US- 1 site received 68 lbs/acres nitrogen in February 2019 from chicken litter for the millet crop. Millett was not planted until September. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sincerely, Robert T. Branch, L.S.S. Land Application/Residuals Operator #15676 RTB Attachment cc: Von Drehle Corporation TABLE OF CONTENTS SECTION NO. TITLE I Certification Form II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary Forms V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Forms VIII Fecal and Salmonella Documentation and Results IX Soil Analysis Reports X 2019 Application Summary Table XI 2019 Application Condition Summaries CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0005135 County: Richmond Year: 2019 Facility Name (as shown on permit): von Drehle Corporation Land Application Operator: Belger Farms Phone: (803) 424-4731 Land application of residuals as allowed by the permit occurred during the past calendar year? ❑ Yes Q No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals A lication Summary: Total number of application fields in thepermit: 18 Total number of fields utilized for land application during the year: 18 Total amount of dry tons applied during the year for all application sites: 9,228.29 Total number of acres utilizes for land application during the year: 430.00 Part B - Annual Comuiance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) Issued by the Division of Water Quality. ❑ Yes 0 No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /1-) 1--� r Mr. Justin Dawkins, Cordova Plant Manager 1., 2 4 2 6 tl Permittee ame and Title (type or print) Si ature of Perim ttee Date 0l•S--Zv Signature of Preparer* Date (if different from Permittee) Signature of Land Applier (if different from Permittee and Preparer) Date NONCOMPLIANCE ISSUES Compliance for Part B Condition 7 — General Permit Requirements Crop Failure The US-1 crop of Millet failed due to the late nature of the planting. Small Grain has been planted at US-1 in January of 2020. Once this crop is harvested, an application will be made to US-1. ANNUAL RESIDUAL SAMPLING SUMMARY FORM ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0005135 Laboratory: 1) Facility Name: von Drehle Corporation 2) Residual Source WQ # or City of Rockingham 1UP #0015 3) NPDES #: 4) WWTP Name: Cordova Facility 5) Residual Annlvsis Data Microbac Labs Parameter (mg/kg) Conc. Limit (mg/kg)a Sample or Composite Date 1/8/2019 3/7/2019 5/6/2019 7/29/2019 9/9/2019 11/12/2019 Percent Solids (%) NA 32.60 40.80 43.00 34.40 36.60 34.80 Arsenic 75 < 2.2 < 2.5 < 1.4 < 2.1 < 1.3 < 1.0 Cadmium 85 < 0.22 < 0.25 < 1.3 < 0.21 < 0.44 2.80 Copper 4,300 37.90 23.70 247.00 24.60 26.40 33.10 Chromium NA 0.00 0.00 0.00 0.00 0.00 0.00 Lead 840 0.00 < 1.2 12.40 < 1.0 < 1.1 1.20 Mercury 57 0.02 < 0.015 0.02 0.01 < 0.61 0.02 Molybdenum 75 4.50 5.00 9.00 4.20 2.60 3.60 Nickel 420 2.80 1.40 18.60 1.20 1.60 1.40 Selenium 100 < 2.2 < 2.5 6.70 < 2.1 < 1.7 1.30 Zinc 7,500 73.10 65.80 597.00 97.90 53.10 135.00 Total Phosphorus NA 15.00 50.00 2.20 29.00 3 72.00 TKN NA 641.00 285.00 407.00 332.00 335 613.00 Ammonia -Nitrogen NA 194.00 149.00 104.00 < 2.91 < 2.73 < 2.87 Nitrate and Nitrite NA < 2.282 < 4.34 < 14.52 < 16.11 < 19.05 < 3.09 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submittingose information, including the possibility of fines and imprisonment for knowing violations." of PrenarK * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORMS ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): Permit #: W00005135 Cation Exchange Capacity (non 503 only): Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series Acres Used: 23 Acres Permitted: 23 Site #: 3 Field #: n/a WcB 498.55 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-4 M B mliMENNEEMENEEN Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): MIT, M, Total . p• "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including t ossibility of fines and imprisonment for knowing violations" 6& 2=7-- Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series Acres Used: 9.1 Acres Permitted: 9.1 Site #: 3 Field #: 174.73 n/a WcB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-4 MB Total Phos- _phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- _phorusEENEENEENEENE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including a possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 18.9 Acres Permitted: 18.9 Site #: 3 Field #: 381.15 n/a WcB 3A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-4 MB Total ' • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- _phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Q2� A 5-1 .2', ignature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 37.2 Acres Permitted: 37.2 Site #: 3 Field #: 777.56 n/a WcB 3B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 20194 MB Total Phos- phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): in in I in I I On- VRW TotalEmilio Phos- phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 13.2 Acres Permitted: 13.2 Site #: 261.99 n/a WcB Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 20194 MB Total Phos- phorusEEEEEEEEEEEE Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total Phos- phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): 250.91 WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 11.1 Acres Permitted: 11.1 Site #: 3 Field #: n/a WcB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-4 MB Total Phos- phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total Phos- phrusEEMENEEMENEEM. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incittAing the possibility of fines and imprisonment for knowing violations" -LO Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series Acres Used: 24.6 Acres Permitted: 24.6 Site #: 3 Field #: 484.69 n/a WcB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-5 MB 6A Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incluithe possibinlity of fines and imprisonment for knowing violations" a,, Z Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 37.5 Acres Permitted: 37.5 Site #: 3 Field #: 679.09 n/a WcB 6B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 20194 MB 2019-5 MB ® 1 1 1 • __-_---__- Total Phos- phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total Phos- �• �� �., .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includ" the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): 480.76 WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 19.1 Acres Permitted: 19.1 Site #: 4 Field #: n/a TbB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-2 MB Total ' .E . • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inclu i g the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 37.1 Acres Permitted: 37.1 Site #: 4 Field #: n/a TbB 908.74 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-2 MB • Total •E • • Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total ,• , •• "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, incI d' g the ossibility of fines and imprisonment for knowing violations" 2— r-e a Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 22.4 Acres Permitted: 22.4 Site #: 4 Field #: 554.17 n/a TbA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-2 MB • Total Phos- _phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- • • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" i, -)--Za Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 50.8 Acres Permitted: 50.8 Site #: 4 Field #: 1,122.64 n/a TbA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-1 MB 2019-2 MB Total ' • • • ENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): WIT, • ® t ----------® • Total Phos- �� �:� .• "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including th ossibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 11.1 Acres Permitted: 11.1 Site #: Field #: 280.20 n/a TbA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft vd 2019-2 MB Total Phos- phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total Phos- _phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includi he possib*l' of tines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 18.9 Acres Permitted: 18.9 Site #: 4 Field #: 450.71 n/a TbA 6A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-2 MB ' • 1 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total Phos- phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includi he possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series Acres Used: 19.3 Acres Permitted: 19.3 Site #: 4 Field #: 461.87 n/a TbA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-2 MB 6B MIN RUN -- Total ' •E . • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- _phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includ"Jug the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): 378.26 WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 19.2 Acres Permitted: 19.2 Site #: 4 Field #: n/a TbA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-1 MB Total • • —phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total00111111111111 Phos- phorusEEMENEEMENEEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Darvl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 28.9 Acres Permitted: 28.9 Site #: 4 Field #: 558.62 n/a TbA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-1 MB Total Phos- __phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total Phos- .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includin he possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 28.6 Acres Permitted: 28.6 Site #: 4 Field #: 523.62 n/a TbA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2019-1 MB Total Phos- • • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 10111111111111 OEM Total • . 1 •. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" 1z - ?-0 Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 498.55 Site #: I Acres Permitted: Operator: von Drehle Corporation Crop l Name: Rye Predominat Soil Series Crop 1 Max PAN: 80.00 WcB Crop 2 Name Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 23.00 23.00 NA #N/A ol7 �' CD 0 s Specify Totals Per Acre % Solids As Decimal Volume Applied per Acre DT. Ac Residual Sources (NPDES #. WQ#. Fert.. Animal Waste. etc.) Site Cond. (Dry' Wet' Moist) Prect p' Past 24 Hrs. Inches a K r? �. 0 w_ ° < w * N o K �' w CD * o' � TKN m g z a o o ? W m k g Nitrate and Nitrite m & PAN Applied pp (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Jul-19 1,449.28 63.01 34.40 21.68 von Drehle Paper INC 1.00 0.40 332 3 16 6.53 X TOTALS: 63 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.09 0.01 0.00 1.07 0.04 0.00 0.18 0.05 0.09 4.24 1.26 6.53 0.00 Date lbs/ac Current Cumulative lbs/acre 0.42 2.22 NA 13.50 0.33 0.02 NA 2.60 0.45 38.34 0.33 2.21 NA 12.43 0.29 0.02 NA 2.55 0.35 34.10 36 34 NA 1.338 267 15 NA 374 89 2.498 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 3 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 174.73 Site #: 2 Acres Permitted: Operator: von Drehle Corporation Crop 1 Name: Predominat Soil Series Crop 1 Max PAN: 80.00 WcB Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 9.10 9.10 NA #N/A oC7 W � CD � o SDecify Totals Per Acre u /o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #. WQ#. Fert.. Animal Waste. etc.) Site Cond. (Dry. Wet' Moist) Precip. Past 24 Hrs. Inches o � o T. c iv * o• o w N CD T * > Fi w * * w > TKN mg/kg z a 3 o C, ? w m g & g Nitrate and Nitrite m /k . PAN Applied (]bs/acre) Must Select Crop 1 of Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Jul-19 507.95 55.82 34.40 19.20 von Drehle Paper INC 1.00 0.40 332 3 16 5.79 X TOTALS: 56 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.08 0.01 0.00 0.94 0.04 0.00 0.16 0.05 1 0.08 3.76 1.11 5.79 0.00 Date lbs/ac Current Cumulative lbs/acre 0.27 0.06 NA 11.31 0.26 0.02 NA 1.62 0.46 29.82 0.19 0.05 NA 10.37 0.22 0.02 NA 1.57 0.38 26.06 36 34 NA 1.338 267 15 NA 374 89 2.498 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." O� *Application Method: S - Surface, IN - Injection, INC - Incorporation Z - _c� **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading R�tp aDEIVR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: 18.90 Owner: von Drehle Corporation Annual Dry Tons Applied: 381.15 Site #: 3A Acres Permitted: 18.90 Operator: von Drehle Corporation Crop 1 Name: Rye Predominat Soil Series Crop 1 Max PAN: 80.00 WcB Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN NA #N/A l7 rD o Specify Totals Per Acre u /o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste. etc.)Wet. Site Cond. (Dry' Moist) Precip. Past 24 Hrs. Inches n 3 b _ iv * o w N p" = w ; TKN mg/kg z a B as o g mg/kg Nitrate and Nitrite ,n , PAN Applied pp (lbs/acre) Must Select Crop 1 or Crop 2 Wet Cu.Yd. Report Totals in Gal. Crop l Crop 2 Crop 1 Crop 2 Jul-19 1 1,108.00 58.62 34.40 20.17 von Drehle Paper INC 1.00 0.40 332 3 16 6.08 X TOTALS: 59 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN I PAN 2 Lime Applied Annuallbs/acre 0.08 0.01 0.00 0.99 0.04 0.00 0.17 0.05 0.08 3.95 1.17 6.08 0.00 Date lbs/ac Current Cumulative lbs/acre 0.47 0.06 NA 7.90 0.37 0.02 1 NA 0.97 0.51 21.14 0.39 0.05 NA 6.91 0.32 0.02 NA 0.92 0.42 17.19 36 1 34 1 NA 1.338 267 15 1 NA 374 89 2.498 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loadingft FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 777.56 Site #: 3B Acres Permitted: Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): Crop 1 Name: Rye Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN 37.20 37.20 NA #N/A C7 o Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT AC Residual Sources (NPDES #. WQ#. Fert., Animal Waste. etc.) Site Cond. (D ry' Wet' Moist) Precip. Past 24 Hrs. Inches n ° iv ° w N o' ° �' - W � TKN m - g z 0 o g w mg/kg Nitrate and Nitrite m dk PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Cro I p CCo 2 p Crop l p Crop 2 p Aug-19 2,260.35 60.76 34.40 20.90 von Drehle Paper INC 1.00 0.40 332 3 16 6.30 X TOTALS: 61 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.09 0.01 0.00 1.03 0.04 1 0.00 0.18 0.05 0.09 4.09 1 1.21 1 6.30 1 0.00 Date lbs/ac Current Cumulative Ibs/acre 0.51 0.06 NA 8.04 0.38 0.02 NA 0.99 0.52 22.71 0.42 0.05 NA 7.01 0.34 0.02 NA 0.94 0.44 18.62 36 34 NA 1 1.338 267 15 NA 374 89 2.498 r 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate• Surface - 114 In•ection/Incor oration - 1 0 Signature of Land Applier ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.29 Date Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loadingft FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 261.99 Site #: 4 Acres Permitted: Operator: von Drehle Corporation Crop 1 Name: Rye Predominat Soil Series Crop 1 Max PAN: 80.00 Wc13 Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 13.20 13.20 NA #N/A o CD Specify Totals Per Acre %Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#. Fert.. Animal Waste. etc.) Cond. (Dry Wet, Moist) Precip. Past 24 Hrs. inches �. w a o w w * N ° 3 w TKN m g/k g z o o g m g/k g Nitrate and Nitrite m PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wei Tons Cu.Yd. Report Totals in in Gal. 1 Crop 2 Crop 1 Crop 2 Aug-19 761.60 57.70 34.40 19.85 von Drehle Paper INC 1.00 0.40 332 3 16 5.98 X TOTALS: 58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.08 0.01 0.00 0.98 0.04 1 0.00 0.17 0.05 0.08 3.89 1.15 5.98 0.00 Date Ibs/ac Current Cumulative lbs/acre 0.42 0.96 NA 8.79 0.41 0.03 NA 1.26 1 0.53 34.53 0.34 0.95 NA 7.81 0.37 0.03 NA 1.21 0.45 30.65 36 34 NA 1.338 267 15 NA 374 89 2.498 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2 r- Z **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Date Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 250.91 Site #: 5 Acres Permitted: Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): Crop 1 Name: Rye Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN 11.10 11.10 NA #N/A l7 CD Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT AC Residual Sources (NPDES #. WQ#, Fert.. Animal Waste. etc.) Site Cond. (Dry Wet. Moist) Precip. Past 24 Hrs. inches K n �. ° w ° < o w * N o' ° K �' m * o' o TKN mg/kg z 3 �° o g R. w m /k g Nitrate and Nitrite m ./k PAN Applied (lbs/acre) Must Select Crop I or Crop 2 Wei Tons Cu.Yd. Report Totals in Gal. Crop 1 p [Cro 2 p Crop 1 p Crop 2 p Aug-19 729.40 65.71 34.40 22.60 von Drehle Paper INC 1.00 0.40 332 3 16 6.81 X TOTALS: 66 As Cd Cr Cu Pb H Mo Ni Se Zn P PAN I PAN 2 Lime A lied Annuallbs/acre 0.09 0.01 0.00 1.11 0.05 0.00 0.19 0.05 0.09 4.43 1.31 6.81 0.00 Date lbs/ac Current Cumulative Ibs/acre 0.56 1.04 NA 10.78 0.42 0.02 NA 1.50 0.97 37.51 0.46 1.04 NA 9.67 0.37 0.02 NA 1.45 0.87 33.08 36 34 NA 1.338 267 15 1 NA 374 89 2.498 1 1 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation (:��- Z **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 3 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 484.69 Site #: 6A Acres Permitted: Operator: von Drehle Corporation Predominat Soil Series WcB Cation Exchange Capacity (non 503): Crop 1 Name: Rye Crop 1 Max PAN: 80.00 Crop 2 Name: #N/A Crop 2 Max. PAN 24.60 24.60 NA #N/A ol7 CD Specify Totals Per Acre a /a Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #. WQ#. Fert.. Animal Waste. etc.) Site Cond. (Dry Moisi) Precip. Past 24 Hrs. Inches o o �. o �_ * s' M < 2 w » N * .. o' > K 5' :e w * o' > TKN m lk g z Y B o o w m Ac g Nitrate and Nitrite m PAN Applied pp (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Sep-19 1 1,324.29 53.83 36.60 19.70 von Drehle Paper INC 1.00 0.40 335 3 19 6.10 X TOTALS: 54 As Cd Cr Cu Pb Hg Mo Ni Se Zn P 1PAN11PAN2 Lime Applied Annuallbs/acre 0.05 0.02 0.00 1.04 0.04 0.02 1 0.10 0.06 0.07 2.09 0.13 6.10 0.00 Date lbs/ac Current Cumulative Ibs/acre 0.30 0.95 NA 7.53 0.36 0.04 NA 1.27 0.32 30.79 0.24 0.94 NA 6.49 0.32 0.02 NA 1.21 0.25 28.70 36 34 1 NA 1.338 267 15 NA 374 89 1 2.498 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 3 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 679.09 Site #: 613 Acres Permitted: Operator: von Drehle Corporation Crop 1 Name: Rye Predominat Soil Series Crop 1 Max PAN: 80.00 WcB Crop 2 Name Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 37.50 37.50 NA #N/A CJ S ci Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#, Fert.. Animal Waste. etc.) Site Cond. (Dry. Wet, Moist) Precip. Past 24 Hrs. Inches o K o � �. m n o. o _: w N « ? _ 5 w w TKN m •n z > -; �o o m k Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report p Totals in Gal. Crop 1[Crop 2 Crop I Crop 2 Aug-19 1,738.66 46.36 34.40 15.95 von Drehle Paper INC 1.00 0.40 332 3 16 4.81 X Sep-19 221.30 5.90 36.60 2.16 von Drehle Paper INC 1.00 0.40 335 3 19 0.67 X TOTALS: 52 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN l PAN 2 Lime Applied Annuallbs/acre 0.07 0.01 0.00 0.90 0.04 0.00 1 0.15 0.05 0.07 3.35 0.94 5.47 0.00 Date lbs/ac Current Cumulative lbs/acre 0.30 0.94 NA 7.18 0.35 0.02 NA 1.23 0.32 30.57 0.22 0.94 NA 6.28 0.31 0.02 NA 1.19 0.24 27.22 36 34 NA 1.338 267 15 NA 374 89 2.498 80.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier .�- - S- - Z C. Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: 19.10 Owner: von Drehle Corporation Annual Dry Tons Applied: 480.76 Site #: I Acres Permitted: 19.10 Operator: von Drehle Corporation Predominat Soil Series TbB Cation Exchange Capacity (non 503): NA Crop 1 Name: Millett Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A ol7 CD s Svecifv Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT AC Residual Sources (NPDES #. WQ#. Fert.. Animal Waste. etc.) Site Cond. (Dry t. Moist ) Precip. Past 24 Hrs. Inches � 3 v �. ° w_ ° m W * N o 5 z C " 'o o TKN mg/kg z Y a0 o g R. mg/kg Nitrate and Nitrite m L/k PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop Ticrop 2 Crop 1 Crop 2 Mar-19 1,178.33 61.69 40.80 25.17 von Drehle Paper INC 1.00 0.40 285 149 4 10.46 X TOTALS: 62 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.13 0.01 0.00 1.19 0.06 0.00 0.25 0.07 1 0.13 3.31 2.52 10.46 1 0.00 Date Ibs/ac Current Cumulative lbs/acre 0.64 0.22 NA 4.59 0.33 0.08 NA 1.20 1.04 21.30 0.51 0.21 NA 3.40 0.27 0.07 1 NA 1.13 0.92 1 17.99 36 1 34 NA 1.338 267 15 1 NA 374 89 2.498 1 100.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant LoadingDW FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 908.74 Site #: 2 Acres Permitted: Operator: von Drehle Corporation Crop 1 Name: Millett Predominat Soil Series Crop 1 Max PAN: 100.00 TbB Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 37.10 37.10 NA #N/A ol7 CD S ci Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#. Fert.. Animal Waste. etc.) Site Cond. (Dry, Moist ) Precip. Past 24 Hrst.. Inches b K "S �. w M 0 w - N o 9 z g s TKN m k g z Y B o0 o w m /k g Nitrate and Nitrite m PAN Applied (lbs/acre) Must Select Crop l or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop l Crop 2 Crop 1 Crop 2 Mar-19 2,227.31 60.04 40.80 24.49 von Drehle Paper INC 1.00 0.40 285 149 4 10.18 X TOTALS: 60 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 1.16 0.06 1 0.00 0.24 0.07 0.12 3.22 2.45 1 10.18 0.00 Date lbs/ac Current Cumulative lbs/acre 0.49 0.17 NA 4.88 0.38 0.08 NA 0.94 1.03 20.80 0.37 0.15 NA 3.72 0.32 0.08 NA 0.87 0.90 17.58 36 34 NA 1.338 267 15 NA 374 89 2.498 LEE Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Ste- *Application Method: S - Surface, IN - Injection, INC - Incorporation o **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate DEM FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: 22.40 Owner: von Drehle Corporation Annual Dry Tons Applied: 554.17 Site #: 3 Acres Permitted: 22.40 Operator: von Drehle Corporation Predominat Soil Series TbA Cation Exchange Capacity (non 503): NA Crop 1 Name: Milieu Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A O O CD Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT AcMoist) Residual Sources (NPDES #. WQ#, Fert.. Animal Waste. etc.) Site Cond. (Dry Wet. Precip. Past 24 Hrs. Inches v s �. w_ * 0 _: NPO o 3 w TKN m ,/k g Z a0 o M w mg/kg Nitrate and Nitrite m PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Mar-19 1,358.27 60.64 40.80 24.74 von Drehle Paper INC 1.00 0.40 285 149 4 10.28 X TOTALS: 61 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 1.17 0.06 0.00 1 0.25 0.07 0.12 3.26 2.47 10.28 0.00 Date lbs/ac Current Cumulative lbs/acre 0.25 0.07 NA 4.56 0.26 0.04 NA 0.77 0.39 13.98 0.13 0.05 NA 3.39 0.20 0.04 NA 0.70 0.27 10.72 36 34 NA 1.338 267 15 NA 1 374 89 2.498 1 100.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." C�� *Application Method: S -Surface, IN -Injection, INC - Incorporation Zd **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 1.122.64 Site #: 4 Acres Permitted: Operator: von Drehle Corporation Crop 1 Name: Millett Predominat Soil Series _ Crop 1 Max PAN: 100.00 TbA Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 50.80 50.80 NA #N/A C7 o Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT AC Residual Sources (NPDES #, WQ#, Fert.. Animal Waste. etc.) Site Cond. (Dry. Wet, Moist) Precip. Past 24 Hrs. inches 3 o �. a m 0 _: * N * o' o S* z CD w * o' o TKN m .n; g Z a -; B �o o ? mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (Ibs/acre) Must Select Crop 1 or Crop 2 we�Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Feb-19 2,134.51 42.02 32.60 13.70 von Drehle Paper INC 1.00 0.40 641 194 2 10.28 X Mar-19 1,046.06 20.59 40.80 8.40 von Drehle Paper INC 1.00 0.40 285 149 4 3.49 X TOTALS: 63 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.10 0.01 0.00 1.44 0.02 0.00 1 0.21 0.10 0.10 3.11 1.25 13.77 1 0.00 Date lbs/ac Current Cumulative lbs/acre 0.46 0.15 NA 6.08 0.40 0.07 NA 1.27 0.46 23.11 0.36 0.14 NA 4.64 0.38 0.07 NA 1.17 0.36 20.00 36 1 34 1 NA 1 1.338 1 267 15 NA 374 89 1 2.498 100.00 Prior Years Cumulative Ibs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 2 i _ *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 280.20 Site #: 5 Acres Permitted: Operator: von Drehle Corporation Crop I Name: Millett Predominat Soil Series Crop I Max PAN: 100.00 TbA Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 11.10 11.10 NA #N/A ol7 Specify Totals Per Acre o /o Solids AS Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #, WQ#. Fert., Animal Waste, etc. ) Site Cond. (D (Dry- Wet. Moist) precip. Past 24 Hrs. Inches n 3CD ? w_ a w w * N ° w * o' o TKN m g/k g z o o m g/k g Nitrate and Nitrite m g/k PAN Applied (lbs/acre) Must Select Crop I or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Cro 1 p Cro 2 p Crop I p Crop 2 p Mar-19 686.76 61.87 40.80 25.24 von Drehle Paper INC 1.00 0.40 285 149 4 10.49 X TOTALS: 62 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.13 0.01 0.00 1.20 1 0.06 0.00 1 0.25 0.07 1 0.13 3.32 2.52 10.49 0.00 Date lbs/ac Current Cumulative lbs/acre 0.40 0.98 NA 6.50 0.30 0.05 NA 1.50 0.63 22.68 0.27 0.97 NA 5.30 0.24 0.05 NA 1.43 0.51 19.36 36 34 NA 1.338 267 15 NA 374 89 2.498 loo.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 2 - 5 = zo Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 450.71 Site #: 6A Acres Permitted: Operator: von Drehle Corporation Crop 1 Name: Millett Predominat Soil Series _ Crop l Max PAN: 100.00 TbA Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 18.90 18.90 NA #N/A El K C7 o ?; rD Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT Ac Residual Sources (NPDES #. WQ#. Fert.. Animal Waste. etc.) Site Cond. (Dry' Wet' Moist) Precip. Past 24 Hrs. inches a � -a � 0 w ca.a. < � _: w * N * F ' o M K z �' w N * w TKN mg/kg Z 3 0 o o g COM mg/kg Nitrate and Nitrite m PAN Applied (Ibs/act'e) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Mar-19 1,104.69 58.45 40.80 23.85 von Drehle Paper INC 1.00 0.40 285 149 4 9.91 X TOTALS: 58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 1.13 0.06 0.00 0.24 1 0.07 0.12 3.14 1 2.38 1 9.91 1 0.00 Date Ibs/ac Current Cumulative lbs/acre 0.71 1.10 NA 5.64 0.29 0.05 NA 1.43 1.06 21.03 0.59 1.09 NA 4.51 0.23 0.05 NA 1.36 0.94 17.89 36 34 NA 1 1.338 267 15 NA 374 89 2.498 1 100.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." C " Z� - �?,, - Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate DEW FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: 19.30 Owner: von Drehle Corporation Annual Dry Tons Applied: 461.87 Site #: 613 Acres Permitted: 19.30 Operator: von Drehle Corporation Predominat Soil Series TbA Cation Exchange Capacity (non 503): NA Crop 1 Name: Millett Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A � 0 � CD ci Totals Per Acre a /a Solids As Decimal Volume Applied per Acre DT/AC Residual Sources (NPDES #. WQ#, Fert.. Animal Waste. etc.) Site Cond. (Dry. Wet' Moist) Precip. Past 24 Hrs. inches o � o �. ° m ° w = w + N o' w w _ o' = TKN I mg/kg z > o � ° ° m w l g Nitrate and Nitrite ing/kg PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 WetTons Cu.Yd. Report Totals in Gal. Crop Ticrop 2 Crop l Crop 2 Mar-19 1,132.03 58.65 40.80 23.93 von Drehle Paper INC 1.00 0.40 285 149 4 9.94 X TOTALS: 59 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.12 0.01 0.00 1.13 0.06 0.00 0.24 0.07 0.12 3.15 2.39 9.94 1 0.00 Date lbs/ac Current Cumulative lbs/acre 0.75 1.10 NA 5.70 0.29 0.05 NA 1.49 1.06 22.77 0.63 1.09 NA 4.56 0.24 0.05 NA 1.42 0.94 19.62 36 34 NA 1 1.338 267 15 NA 374 89 2.498 100.00 Prior Years Cumulative Ibs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." C, I? "I I � � 11 - Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading -Rate FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 378.26 Site #• 7 Acres Permitted: Operator: von Drehle Corporation Predominat Soil Series TbA Cation Exchange Capacity (non 503): Crop 1 Name: Millett Crop 1 Max PAN: 100.00 Crop 2 Name: #N/A Crop 2 Max. PAN 19.20 19.20 NA #N/A o CD o Specify To. Per Acre % Solids As Decimal Volume Applied per Acre DT AC Residual Sources (NPDES #. WQ#. Fert.. Animal Waste. etc.) Cond. (Dry. Wet' Moist) Precip. Past 24 Hrs. Inches K � n. m * o• w N w w * * °= =1 TKN mgfkg Z > 0CD Go o CD w mg/kg Nitrate and Nitrite m , PAN Applied (Ibs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Cr op 2 Crop 1 Crop 2 Feb-19 1 1,160.31 60.43 32.60 19.70 von Drehle Paper INC 1.00 0.40 641 194 2 14.78 X TOTALS: 60 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN ].PAN 2 Lime Applied Annuallbs/acre 0.09 0.01 0.00 1.49 0.00 0.00 1 0.18 0.11 1 0.09 2.88 0.59 14.78 0.00 Date Ibs/ac Current Cumulative lbs/acre 0.43 1.01 NA 6.54 0.21 0.04 NA 1.28 0.94 19.85 0.34 1.00 NA 5.05 0.21 0.04 NA 1.17 0.85 16.97 36 34 NA 1.338 267 15 NA 374 89 2.498 1 100.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier - r - Date 2 *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rasp aDENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: W00005135 Field #: 4 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 558.62 Site #: 8 Acres Permitted: Operator: von Drehle Corporation Crop 1 Name: Millett Predominat Soil Series Crop 1 Max PAN: 100.00 TbA Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 28.90 28.90 NA #N/A o Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #. WQ#. Fert.. Animal Waste. etc.) Site Cond. (Dry, Wet' Moist) Precip. Past 24 Hrs. inches n � v � A. ° °_ ° m - * N o' � - w * o' o TKN m � z > a0 o ° m � Nitrate andCD Nitrite mgtkg PAN Applied (Ibs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 Jan-19 1,713.55 59.29 32.60 19.33 von Drehle Paper INC 1.00 0.40 641 194 2 14.50 X TOTALS: 59 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.09 0.01 0.00 1.47 1 0.00 0.00 0.17 0.11 0.09 2.83 0.58 1 14.50 0.00 Date lbs/ac Current Cumulative lbs/acre 0.45 1.02 NA 6.58 0.21 0.05 1 NA 1.64 0.92 21.96 0.36 1.01 NA 5.12 0.21 0.05 NA 1.53 0.83 19.13 36 34 NA 1.338 267 15 NA 374 89 2.498 1 100.00 Prior Years Cumulative Ibs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier - r- ZC.121 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: von Drehle Corporation WQ Permit #: WQ0005135 Field #: 4 Acres Utilized: Owner: von Drehle Corporation Annual Dry Tons Applied: 523.62 Site #: 9 Acres Permitted: Operator: von Drehle Corporation Crop I Name: Millett Predominat Soil Series Crop I Max PAN: 100.00 TbA Crop 2 Name: Cation Exchange Capacity (non 503): #N/A Crop 2 Max. PAN 28.60 28.60 NA #N/A 3 o ?; fD Totals Per Acre o /a Solids As Decimal Volume Applied per Acre DT AC Residual Sources (NPDES #, WQ#, Fert.. Animal Waste. etc.) Site Cond. (Dry Mois[ ) Precip. Past 24 Hrs. Inches .o 3 �. w * _: w w * N 3 � w * * o' M TKN m k z 3 .; M o g w mg/kg Nitrate and Nitrite m /k PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Wet Tons Cu.Yd. Report Totals in Gal. Crop T1Crop 2 Crop 1 Crop 2 Jan-19 1,606.20 56.16 32.60 18.31 von Drehle Paper INC 1.00 0.40 641 194 2 13.73 X TOTALS: 56 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.08 0.01 0.00 1.39 0.00 0.00 0.16 0.10 1 0.08 2.68 0.55 1 13.73 1 0.00 Date I lbs/ac Current Cumulative lbs/acre 0.54 1.04 NA 5.81 0.18 0.05 NA 1.41 0.95 21.47 0.46 1.03 NA 4.42 0.18 0.05 NA 1.30 0.86 18.79 36 34 1 NA 1 1.338 1 267 15 NA 374 89 1 2.498 1 100.00 Prior Years Cumulative lbs/acre Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading DEWR FORM FSF (12/2006) RESIDUAL ANALYSIS LAB SHEETS Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2019-1 MB Date Sampled: 1/8/2019 Date Reported: 1/22/2019 Reporting Period: Jan- Feb 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids 32.60 Nitrogen (TKN) 0.064 641.000 Phosphorus 0.002 15.000 Potassium 0.109 1,090.000 Sulfate 0.000 Calcium 20.000 200,000.000 Magnesium 0.248 2,480.000 Sodium 0.109 1,090.000 Iron --- Aluminum --- 1,850.000 Manganese --- Copper --- 37.900 1,500 Zinc --- 73.100 2,800 Ammonia Nitrogen 0.019 194.000 Nitrate N / Nitrite N --- 2.2820 Cadmium --- 0.2200 39 Chromium --- 1,200 Nickel --- 2.8000 420 Lead --- 300 Arsenic --- 2.2000 41 Mercury --- 0.0170 17 Selenium --- 2.2000 100 pH 7.200 Calcium Carbonate Eq. 0.000 Organic Nitrogen 0.045 Molybdenum --- 4.5000 75 Chloride --- Boron Available P2O5 (�DMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0098 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 01/08/2019 Cordova, NC 28330 Reported: 01/22/2019 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Lab Sample ID: K9A0098-01 Method: Calculation Plant Available Nitrogen Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N Method: SM 2540 G-2011 % Solids Method: SM 4500 NH3 C-2011 Ammonia as N Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Method: Calculation Sodium Adsorption Ratio, SAR Method: EPA 9045 D pH at 25 °C Method: SM 4500 P F-2011 Phosphorus, Total (as P) 7471E Method: 7471 B Mercury Result RL Units 231 mg/kg Collected By: Wright Collection Date: 01 /08/2019 11:45 Note Prepared Analyzed Analyst 01/21/19 1200 01/21/19 1201 JMO <0.762 0.762 mg/kg dry wt. dry <1.52 1.52 mg/kg dry wt. dry 32.6 1.00 % 194 3.07 mg/kg dry wt. Y dry 641 1.53 mg/kg dry wt. dry Result RL Units Note 0.470 mg/kg 7.2 1.0 pH Units H is 0.77 mg/kg dry wt. dry Analyses Subcontracted to: Pace Analytical Result RL Units Note 0.017 0.0097 mg/kg dry wt. 01/09/19 1130 01/09/19 1516 DSK 01/09/19 1130 01/09/19 1516 DSK 01/09/19 1114 MT 01/10/19 1057 MT 01/09/19 0833 TAB Prepared Analyzed Analyst 01/21/19 1155 01/21/19 1155 JMO 01/09/19 1101 DSK 01/10/19 1439 01/10/19 1154 DSK Prepared Analyzed Analyst 01/15/19 0000 DS Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 5 VMICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0098 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Lab Sample ID: K9A0098-01 Collected By: Wright Collection Date: 01/08/2019 11:45 SPLP Metals Result RL Units Note Prepared Analyzed Analyst Method: SW-846 6010E Aluminum 1850 21.8 mg/kg dry wt. 01/15/19 0000 DS Arsenic <2.2 2.2 mg/kg dry wt. 01/15/19 0000 DS Cadmium <0.22 0.22 mg/kg dry wt. 01/15/19 0000 DS Calcium 200000 1090 mg/kg dry wt. 01/15/19 0000 DS Copper 37.9 1.1 mg/kg dry wt. 01/15/19 0000 DS Magnesium 2480 21.8 mg/kg dry wt. 01/15/19 0000 DS Molybdenum 4.5 1.1 mg/kg dry wt. 01/15/19 0000 DS Nickel 2.8 1.1 mg/kg dry wt. 01/15/19 0000 DS Potassium <1090 1090 mg/kg dry wt. 01/15/19 0000 DS Selenium <2.2 2.2 mg/kg dry wt. 01/15/19 0000 DS Sodium <1090 1090 mg/kg dry wt. 01/15/19 0000 DS Zinc 73.1 2.2 mg/kg dry wt. 01/15/19 0000 DS Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. Reviewed and Approved By: 1 2l"Lx-e— �tiPiLdi � Jeanne Overstreet Client Relationship Specialist, Environmental Reported: 01/22/2019 09:09 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 5 Fayetteville Division 2592 Hope Mills Road -- Fayetteville, NC 28306 (910) 864-1920 / 86 CHAIN OF CUSTODY RECORD *K9A0098* CLIENT NAME BADDRESS* VonDrehle Corp. 126 First Street Cordova, NC 28330 PO# PROJECT/LOCATION: Cordova - 60-day series #OF B 0 T T L E TYPE OF ANALYSIS PRESERVATION CODE E U E E Q N a)C U) U Q �, C U 2 U N 0 .J in I0 Z _ O N CO O + o ,M Z Z o_ O ZC a )— Q 7E5 U) r;!S CODE: A = None B = HNO3 (pH<2) + <4°C C = H2SO4 (pH<2) + <4°C D= NaOH + <4°C E= ZN Acetate + <4°C F = HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER: DATE 1 METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB PH D.O. TEMP'C CHLORINE Residual from paper plant 1 /7 , X 2 A A A A A A A A A Z Relinquf;sW jb : Date Time Received by: (Signature) Date Time Relinquished by: Date Time Received by: (Signature) Date Time 3 4 Relinquished by: Date Time Received by: (Signature) Date Time 5 6 Comments or Special Hazards: REVIEWED I Page 3 of 5 Microbac Laboratories, Inc. - Fayetteville �_ i i "(.) I ° y SUBCONTRACT ORDER SENDING LABORATORY: RECEIVING LABORATORY: Microbac Laboratories, Inc. - Fayetteville Pace Analvtical 2592 Hope Mills Rd 9800 Kincey Ave., Suite 100 Fayetteville, NC 28306 Huntersville, NC 28078 Phone: 910.864.1920 Phone: - Project Manager: Jeanne Overstreet Proiect Info: Project Type: ENV-DrinkingWaterNonRe Report TAT: 7 Project Location: North Carolina Due: 01/17/2019 17:00 Sample ID: K9A0098-01 Matrix: Solid Sampled: 01/08/2019 11:45 Analysis Method Analysis Due Expires v 6010D SW-846 6010B Aluminum Arsenic 5 mg/kg dry mg/kg dry 0.5 mg/kg dry ftmj� 0.25 mg/kg dry eampl 0.05 mg/kg dry 0.017 mg/kg dry ftamm Calcium 2.5 mglkg dry Cadmium ✓ 0.05 mg/kg dry 5 mg/kg dry 0.1 mg/kg dry fiiitil■ill■� Copper 0.25 mg/kg dry 4foJEW 0.25 mg/kg dry 0.25 mg/kg dry dMidn 0.1 mg/kg dry V✓ Lead 0 mg/kg dry thimM 5 mg/kg dry 0.25 mg/kg dry 0.0104 mg/kg dry V ✓�+� Magnesium o `I` b 0.25 mg/kg dry HUMNION0=9 0.25 mg/kg dry / 0.25 mg/kg dry Nickel ✓ 0.25 mg/kg dry 0.72 mg/kg dry glillMopomMS 0.0157 mg/kg dry 0 mg/kg dry Potassium 500 mg/kg dry v Selenium 0.5 mg/kg dry amp""Ple 1.26 mg/kg dry umfilff� 5 mg/kg dryer 0.25 mg/kg dry Sodium 250 mg/kg dry 111molOW 0.25 mg/kg dry smawlimme 0.05 mg/kg dryer 0.5 mg/kg dry 611111111ft 0.0036 mg/kg dry 0.25 mg/kg dry 0.1 mg/kg dry 0.25 mg/kg dry �U&M1110rr Zinc 0.5 mg/kg dryer 0.1 mg/kg dry all metals this method IN ?, A I K fJ I Released By Date ncccivcu ny Received By Date l"i Page4of5 0 Microbac Laboratories, Inc. - Fayetteville SUBCONTRACT ORDER K9A0098 SENDING LABORATORY: RECEIVING LABORATORY: Microbac Laboratories, Inc. - Fayetteville Pace Analytical 2592 Hope Mills Rd 9800 Kincey Ave., Suite 100 Fayetteville, NC 28306 Huntersville, NC 28078 Phone: 910.864.1920 Phone: - Project Manager: Jeanne Overstreet Proiect Info: Project Type: ENV-DrinkingWaterNonRe Report TAT: 7 Project Location: North Carolina Due: 01/17/2019 17:00 Sample ID: K9A0098-01 Matrix: Solid Sampled: 01/08/2019 11:45 Analysis Method Analysis Due Expires 6010D SW-846 6010B Vl Aluminum Arsenic 5 mg/kg dry 4hn1mgqft U.4iU mg/kg dry 0.5 mg/kg dry Qmj� 0.25 mg/kg dry wompow" 0.05 mg/kg dry &EMAND 0.017 mg/kg dry V �� Calcium 2.5 mg/kg dry Cadmium ✓ 0.05 mg/kg dry 5 mg/kg dry Iftift 0.1 mg/kg dry f Weimm Copper 0.25 mg/kg dry gJ@WM 0.25 mg/kg dry 0.25 mg/kg dry db6ft 0.1 mg/kg dry V Lead 0 mg/kg dryftn� 5 mg/kg dry 0.25 mg/kg dry 0.0104 mg/kg dry V Magnesium ` r Mp�\I E WV1^ 0.25 mg/kg dry 0.25 mg/kg dry 0.25 mg/kg dry Nickel ✓ 0.25 mg/kg dry 0.72 mg/kg dry 0.0157 mg/kg dry 0 mg/kg dry Potassium 500 mg/kg dry Selenium 0.5 mg/kg dry OWN"" 1.26 mg/kg dry Sodium 5 mg/kg dryer 0.25 mg/kg dry �t 250 mg/kg dry qlomMft 0.25 mg/kg dry 0.05 mg/kg dry Nftdh� 0.5 mg/kg dry 0.0036 mg/kg dry 011111MEW 0.25 mg/kg dry/ 0.1 mg/kg dry 0.25 mg/kg dry V Zinc 0.5 mg/kg dryer 0.1 mg/kg dry all metals this method i1-p- 1- e u. lr H °7 q 7 1 /3 Released By Date by Received By Date - Date Page 5of5 Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: von Drehle Corporation von Drehle Paper Cordova, North Carolina Belger Farms Industrial vd 2019-2 MB 3/7/2019 3/22/2019 March -April 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids 40.80 Nitrogen (TKN) 0.029 285.000 Phosphorus 0.005 50.000 Potassium 0.123 1,230.000 Sulfate 0.000 Calcium 19.300 193,000.000 Magnesium 0.195 1,950.000 Sodium 0.123 1,230.000 Iron --- Aluminum --- 1,850.000 Manganese --- Copper --- 23.700 1,500 Zinc --- 65.800 2,800 Ammonia Nitrogen 0.015 149.000 Nitrate N / Nitrite N --- 4.3400 Cadmium --- 0.2500 39 Chromium --- 1,200 Nickel --- 1.4000 420 Lead --- 1.2000 300 Arsenic --- 2.5000 41 Mercury --- 0.0150 17 Selenium --- 2.5000 100 pH 7.500 Calcium Carbonate Eq. 0.000 Organic Nitrogen 0.014 Molybdenum --- 5.0000 75 Chloride --- Boron Available P2O5 &�MICROBAC- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9C0100 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 03/07/2019 Cordova, NC 28330 Reported: 03/22/2019 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Lab Sample ID: K9C0100-01 Method: Calculation Plant Available Nitrogen Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N Method: SM 2540 G-2011 % Solids Method: SM 4500 NH3 C-2011 Ammonia as N Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Method: Calculation Sodium Adsorption Ratio, SAR Method: EPA 9045 D pH at 25 °C Method: SM 4500 P F-2011 Phosphorus, Total (as P) SPLP Metals Method: EPA 7471 B Mercury Method: SW-846 6010E Result RL Units 118 mg/kg 3.12 0.610 mg/kg dry wt. dry <1.22 1.22 mg/kg dry wt. dry 40.8 1,00 °f, 149 285 Result 5.41 7.5 Collected By: Brown Collection Date: 03/07/2019 11:56 Note Prepared Analyzed Analyst 03/22/19 1430 03/22/19 1431 JMO 2.45 mg/kg dry wt. Y dry 1.23 mg/kg dry wt. dry RL Units Not mg/kg 1.0 pH Units H 50 0.61 mg/kg dry wt. dry Analyses Subcontracted to: Pace Analytical ( Huntersville) Result RL Units Note <0.015 0.015 mg/kg dry wt. 03/12/19 1102 03/12/19 1505 DSK 03/12/19 1102 03/12/19 1505 DSK 03/11/19 1322 MT 03/08/19 0913 MT 03/12/19 0839 DC Prepared Analyzed Analyst 03/22/19 1423 03/22/19 1425 JMO 03/15/19 1433 CLB 03/15/19 1219 DSK Prepared Analyzed Analyst 03/15/19 0000 KDF Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 3 (5)MICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9C0100 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Lab Sample ID: K9C0100-01 Collected By: Brown Collection Date: 03/07/2019 11:56 SPLP Metals Result RL Units Note Prepared Analyzed Analyst Aluminum 1850 24.5 mg/kg dry wt. 03/15/19 0000 KDF Arsenic <2.5 2.5 mg/kg dry wt. 03/15/19 0000 KDF Cadmium <0.25 0.25 mg/kg dry wt. 03/15/19 0000 KDF Calcium 193000 491 mg/kg dry wt. 03/15/19 0000 KDF Copper 23.7 1.2 mg/kg dry wt. 03/15/19 0000 KDF Lead <1.2 1.2 mg/kg dry wt. 03/15/19 0000 KDF Magnesium 1950 24.5 mg/kg dry wt. 03/15/19 0000 KDF Molybdenum 5 1.2 mg/kg dry wt. 03/15/19 0000 KDF Nickel 1.4 1.2 mg/kg dry wt. 03/15/19 0000 KDF Potassium <1230 1230 mg/kg dry wt. 03/15/19 0000 KDF Selenium <2.5 2.5 mg/kg dry wt. 03/15/19 0000 KDF Sodium <1230 12230 mg/kg dry wt. 03/15/19 0000 KDF Zinc 65.8 2.5 mg/kg dry wt. 03/15/19 0000 KDF Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments North Carolina DENR NPDES Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental Reported: 03/22/2019 15:15 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 3 I,,.._,. _ Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 8F CHAIN OF CUSTODY RECORD *K9C0100* CLIENT NAME BADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 PO# PROJECT/LOCATION: Cordova - 60-day series #OF B O T T L E s TYPE OF ANALYSIS PRESERVATION CODE E � E N V E c � Q (q U ` Q CL U E 2 U .N a� c J 1 .N uJ tD �p - Y U Z _ O c N f= = rJ) ) � p Z O Z Z Z z a 0o I—o z Y a to -o o CODE: A = None B = HNO3 H<2 + <4°C (P ) C = H2SO4 (pH<2) + <4°c D = NaOH + <4°C E = ZN Acetate + <4°C F = HCl CONTACT PERSON: Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER: DATE 1 METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB F H D.O. TEMP °C RES. CHLORINE Residual from paper plant X 2 A A A A A A A A A 1 A A A A A A A A A inquished by: �- i 1 Date Timejec ivad by: (Signature) 2 Date Time Relinquished by: Date Time Rec ed by 'nature) D �/ 3 4 Relinquished by: Date Time Received by: (Signature) Date Time 5 6 Comments or Special Hazards: REVIEWED -4-A- Page 3 of 3 Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2019-3 MB Date Sampled: 5/6/2019 Date Reported: 5/14/2019 Reporting Period: May -June 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids 43.00 Nitrogen (TKN) 0.041 407.000 Phosphorus 0.000 2.200 Potassium 0.074 744.000 Sulfate 0.000 Calcium 1.240 12,400.000 Magnesium 0.242 2,420.000 Sodium 0.071 707.000 Iron --- Aluminum --- 6,870.000 Manganese --- Copper --- 247.000 1,500 Zinc --- 597.000 2,800 Ammonia Nitrogen 0.010 104.000 Nitrate N / Nitrite N --- 14.5200 Cadmium --- 1.3000 39 Chromium --- 1,200 Nickel --- 18.6000 420 Lead --- 12.4000 300 Arsenic --- 1.4000 41 Mercury --- 0.0170 17 Selenium --- 6.7000 100 pH 8.100 Calcium Carbonate Eq. 0.000 Organic Nitrogen 0.030 Molybdenum --- 9.0000 75 Chloride --- Boron Available P2O5 VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9E0060 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 05/06/2019 Cordova, NC 28330 Reported: 05/14/2019 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Lab Sample ID: K9E0060-01 Calculation Plant Available Nitrogen EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N SM 2540 G-2011 % Solids SM 4500 NH3 C-2011 Ammonia as N SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Calculation Sodium Adsorption Ratio, SAR EPA 9045 D pH at 25 °C SM 4500 P F-2011 Phosphorus, Total (as P) SPLP Metals EPA 7471E Mercury SW-846 6010B Collected By: Wright Collection Date: 05/06/2019 11:46 Result RL Units Dilution Note Prepared Analyzed Analyst 146 mg/kg 1 05/13/19 1128 05/13/19 1128 JMO 2.92 0.581 mg/kg dry wt. 1 05/07/19 1123 05/07/19 1650 DSK dry <11.6 11.6 mg/kg dry wt. 1 05/07/19 1123 05/07/19 1650 DSK dry 43.0 1.00 % 1 05/06/19 1604 TMC 104 2.33 mg/kg dry wt. 1 y 05/10/19 0730 DSK dry 407 1.16 mg/kg dry wt. 1 05/07/19 0850 MT dry Result RL Units Dilution Note Prepared Analyzed Analyst 1.08 mg/kg 1 05/13/19 1128 05/13/19 1225 JMO 8.1 1.0 pH Units 1 H 05/10/19 1001 CLB 2.2 0.57 mg/kg dry wt. 1 05/09/19 1131 DSK dry Analyses Subcontracted to: Pace Analytical ( Huntersville) Result RL Units Dilution Note Prepared Analyzed Analyst 0.017 0.015 mg/kg dry wt. 1 05/09/19 0000 TE Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 3 6)MICROBAC­ Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9E0060 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K9E0060-01 Collection Date: 05/06/2019 11:46 SPLP Metals Result RL Units Dilution Note Prepared Analyzed Analyst Aluminum 6870 14.1 mg/kg dry wt. 1 05/09/19 0000 TE Arsenic <1.4 1.4 mg/kg dry wt. 1 05/09/19 0000 TE Cadmium 1.3 0.14 mg/kg dry wt. 1 05/09/19 0000 TE Calcium 12400 14.1 mg/kg dry wt. 1 05/09/19 0000 TE Copper 247 0.71 mg/kg dry wt. 1 05/09/19 0000 TE Lead 12.4 0.71 mg/kg dry wt. 1 05/09/19 0000 TE Magnesium 2420 14.1 mg/kg dry wt. 1 05/09/19 0000 TE Molybdenum 9 0.25 mg/kg dry wt. 1 05/09/19 0000 TE Nickel 18.6 0.25 mg/kg dry wt. 1 05/09/19 0000 TE Potassium 744 500 mg/kg dry wt. 1 05/09/19 0000 TE Selenium 6.7 0.5 mg/kg dry wt. 1 05/09/19 0000 TE Sodium <707 250 mg/kg dry wt. 1 05/09/19 0000 TE Zinc 597 1.4 mg/kg dry wt. 1 05/09/19 0000 TE Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments North Carolina DENR NPDES Reviewed and Approved By: Samples were received in proper condition and the reported results conform to �e�lL �LWi�dZ applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental Reported: 05/14/2019 15:22 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 3 'K9E0060' Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 (910) 864-1920 / 864-8774 fax CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENT NAME A ADDRESS. VonDrehle Corp. 126 First Street Cordova, NC 28330 PO. PNO.IECTILOCAMN: Cordova - 60-dayseries ROF a D T T L E S TYPE OF ANALYSIS PRESERVATION CODE E N U E C E TrQ C m 0 co C m r; CL o U j o m U E .N c m te N J E .N to a ae U Z U _ O X _c N < N Z o Z M = Z Z a o a F' Z Y H a N -6 o ~ CODE: A = None B=HNO3(pH<2)+<4'C C = H2SO4 (pH<z) + <4'C D= NaOH +<4'C E= ZN Acetate . <4'C F=HCI CONTACTPERSON: Mr. Chris Fowler PHONE: 910-410-9131 EANPLER: OATEINETH00 OF SHIPMENT: MICrobac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB PN O.O. TCEIMP •G RES. CHLORINE 2 Residual from paper plant /0 r S 2 A A I A I A I A A I A A A I 1 1 A A I A I A A A I A I A A Otl. nm. Nc - Oby: tSlanaWn) Oat• � T.. 1 ten. 2 �j• •/ i�G3 N aLN.e by: O.b N.a.Ma by: tSlpmtun) On• nme 3 4 R•IiaNa..Eby: O.t. Tim N-4d by: (Sigr—n) Oat. Tim. 5 6 Comments or Spedal Hazards Page 3 of 3 Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2019-4 MB Date Sampled: 7/29/2019 Date Reported: 8/9/2019 Reporting Period: July- Aug 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids 34.40 Nitrogen (TKN) 0.033 332.000 Phosphorus 0.003 29.000 Potassium 0.103 1,030.000 Sulfate 0.000 Calcium 1.710 17,100.000 Magnesium 0.191 1,910.000 Sodium 0.130 1,300.000 Iron --- Aluminum --- 1,870.000 Manganese --- Copper --- 24.600 1,500 Zinc --- 97.900 2,800 Ammonia Nitrogen 0.000 2.910 Nitrate N / Nitrite N --- 16.1100 Cadmium --- 0.2100 39 Chromium --- 1,200 Nickel --- 1.2000 420 Lead --- 1.0000 300 Arsenic --- 2.1000 41 Mercury --- 0.0120 17 Selenium --- 2.1000 100 pH 8.000 Calcium Carbonate Eq. 0.000 Organic Nitrogen 0.033 Molybdenum --- 4.2000 75 Chloride --- Boron Available P2O5 �DMICROBAC° Microbac Laboratories, Inc. - Fayetteville Revised Report: Amended - RURELIMINARY REPORT. DATA SUBJECT TO CHANGE Case Narrative. K9G0397 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 07/29/2019 Cordova, NC 28330 Reported: 08/09/2019 Case Narrative Report amended on August 9, 2019 for work order K9G0397 that was originally reported on August 8, 2019: Missing sodium result and removed the units for the SAR calculation. Analytical Testing Parameters Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K9G0397-01 Collection Date: 07/29/2019 11:00 Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Plant Available Nitrogen 102 mg/kg 1 08/08/19 1039 08/08/19 1050 JMO EPA 300.0, Rev. 2.1 (1993) Nitrate as N 1.91 0.708 mg/kg dry wt. 1 07/31/19 1019 07/31/19 1638 DSK dry Nitrite as N <14.2 14.2 mg/kg dry wt. 1 07/31/19 1019 07/31/19 1638 DSK dry SM 2540 G-2011 % Solids 34.4 1.00 % 1 07/29/19 1415 DSK SM 4500 NH3 C-2011 Ammonia as N <2.91 2.91 mg/kg dry wt. 1 Y 08/05/19 1011 MT dry SM 4500-Norg C-2011 Total Kjeldahl Nitrogen 332 1.45 mg/kg dry wt. 1 08/07/19 0904 08/07/19 1618 TBM dry Wet Chemistry Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Sodium Adsorption Ratio, SAR 0.480 1 08/08/19 1039 08/08/19 1051 JMO EPA 9045 D pH at 25 °C 8.0 1.0 pH Units 1 H 08/07/19 1057 DSK SM 4500 P F-2011 Phosphorus, Total (as P) 29 0.72 mg/kg dry wt. 1 07/31/19 1307 DSK dry Analyses Subcontracted to: Pace Analytical ( Huntersville) SPLP Metals Result RL Units Dilution Note Prepared Analyzed Analyst Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 3 (tiMICROBAC" Microbac Laboratories, Inc. - Fayetteville PRELIMINARY REPORT. DATA SUBJECT TO CHANGE K9G0397 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Lab Sample ID: K9G0397-01 Collected By: Wright Collection Date: 07/29/2019 11:00 SPLP Metals Result RL Units Dilution Note Prepared Analyzed Analyst SW-846 6010E Aluminum 1870 20.7 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Arsenic <2.1 2.1 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Cadmium <0.21 0.21 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Calcium 17100 207 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Copper 24.6 1 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Lead <1.0 1 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Magnesium 1910 20.7 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Molybdenum 4.2 1 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Nickel 1.2 1 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Potassium <1030 1030 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Selenium <2.1 2.1 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB Sodium <1030 1030 mg/kg dry wt. 1 08/08/19 0000 JB Zinc 97.9 2.1 mg/kg dry wt. 1 08/08/19 0000 08/07/19 0000 JB SPLP Metals EPA 7471E Mercury Definitions H: MDL: RL: Y: 0.012 Result RL Units Dilution Note 0.0087 mg/kg dry wt. 1 Analyte was prepared and/or analyzed outside of the analytical method holding time Minimum Detection Limit Reporting Limit This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Prepared Analyzed Analyst 08/07/19 0000 JB Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 2 of 3 *K9G0397* Fayetteville Division 2592 Hope Mills Road •- Fayetteville, NC 28306 (910) 864-1920 / 864-F lffillilililitillif CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENT NAME & ADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 PO # PROJECT LOCATION: I Cordova - 60-day series # OF B 0 T T L E S TYPE OF ANALYSIS PRESERVATION CODE E E U C E Q C °' N � a).2 Q` �, CL C 0 U E 'N c � m to E 'N m a° - Y Z = c N E � Q N O Z + o Z Z Z a o s o- I— z F 7- to O tq to o H � CODE: A = None B = HNO3 (pH<2) + <4°C C = H2SO4 (pH<2) + <4°C D= NaOH + <4°C E = ZN Acetate + <4°C F = HCI CONTACT PERSON: Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER: 1 -- DATE I METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB pH D.O. TEMP'C CHLORINE I` Residual from paper plant 7 9 1 Y j j. D 0 X 2 A A A A A I A I A A A Rell b . 1' Date Time R ed Signature) Date Time 1 Z 2J t� 13:/ 2 - q-11 squished by: Date Time Rece Vd by: (Signature) Date Time 3 4 Relinquished by: Date Time Received by: (Signature) Date Time 5 6 Comments or Special Hazards: REVIEWED Page 3 of 3 Facility: Source: Location: Contractor: Type of Analysis: von Drehle Corporation von Drehle Paper Cordova, North Carolina Belger Farms Industrial Report No: vd 2019-5 MB Date Sampled: 9/9/2019 Date Reported: 9/24/2019 Reporting Period: Sept -Oct 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids 36.60 Nitrogen (TKN) 0.034 335.000 Phosphorus 0.000 3.200 Potassium 0.006 63.600 Sulfate 0.000 Calcium 19.100 191,000.000 Magnesium 0.235 2,350.000 Sodium 0.121 1,210.000 Iron --- Aluminum --- 1,090.000 Manganese --- Copper --- 26.400 1,500 Zinc --- 53.100 2,800 Ammonia Nitrogen 0.000 2.730 Nitrate N / Nitrite N --- 19.0500 Cadmium --- 0.4400 39 Chromium --- 1,200 Nickel --- 1.6000 420 Lead --- 1.1000 300 Arsenic --- 1.3000 41 Mercury --- 0.6100 17 Selenium --- 1.7000 100 pH 8.000 Calcium Carbonate Eq. 0.000 Organic Nitrogen 0.033 Molybdenum --- 2.6000 75 Chloride --- Boron Available P205 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K910109 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Client Relationship Specialist, Environmental Jeanne Overstreet Tuesday, September 24, 2019 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil samples are reported on a 'dry -weight' basis unless specified otherwise. Analytical results for water and wastes are reported on a'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 7 Von Drehle Corporation Mr. Chris Fowler 126 First Street Cordova, NC 28330 Sample Summary Report 6)MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K910109 Project Name: Residuals Sample - 60 day Project / PO Number: N/A Received: 09/09/2019 Reported: 09/24/2019 Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, K910109-01 Solid Grab 09/09/19 13:30 09/09/19 14:59 Grab Page 2 of 7 VMICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K910109 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K910109-01 Collection Date: 09/09/2019 13:30 Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Plant Available Nitrogen 106 mg/kg 1 09/20/19 0858 09/20/19 0858 JMO EPA 300.0, Rev. 2.1 (1993) Nitrate as N 5.65 0.672 mg/kg dry wt. 1 09/10/19 1143 09/10/19 1601 DSK dry Nitrite as N <13.4 13.4 mg/kg dry wt. 1 09/10/19 1143 09/10/19 1601 DSK dry SM 2540 G-2011 % Solids SM 4500 NH3 C-2011 Ammonia as N SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Calculation Sodium Adsorption Ratio, SAR EPA 9045 D pH at 25 °C SM 4500 P F-2011 Phosphorus, Total (as P) SPLP Metals EPA 601 OD Aluminum Arsenic Cadmium Calcium Copper Lead Magnesium Molybdenum 36.6 1.00 % 1 <2.73 2.73 mg/kg dry wt. 1 y dry 335 1.36 mg/kg dry wt. 1 dry Result RL Units Dilution Note 0.530 1 09/10/19 1143 CLS 09/13/19 0937 MT 09/10/19 1609 09/12/19 1111 TBM Prepared Analyzed Analyst 09/20/19 0858 09/24/19 0848 JMO 8.0 1.0 pH Units 1 H 3.2 0.68 mg/kg dry wt. 1 dry Analyses Subcontracted to: Pace Analytical ( Huntersville) Result RL Units Dilution Note Prepared 1090 4.4 mg/kg dry wt. 1 <1.3 1.3 mg/kg dry wt. 1 <0.44 0.44 mg/kg dry wt. 1 191000 4360 mg/kg dry wt. 1 26.4 0.87 mg/kg dry wt. 1 <1.1 1.1 mg/kg dry wt. 1 2350 218 mg/kg dry wt. 1 2.6 1.7 mg/kg dry wt. 1 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com 09/18/19 1409 CLB 09/12/19 1459 DSK Analyzed Analyst 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK Page 3 of 7 �gDMICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K910109 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Lab Sample ID: K910109-01 SPLP Metals Result Nickel 1.6 Potassium 63.6 Selenium <1.7 Sodium 1210 Zinc 53.1 EPA 7471 B Mercury <0.61 Collected By: Wright Collection Date: 09/09/2019 13:30 RL Units Dilution Note 0.87 mg/kg dry wt. 1 8.7 mg/kg dry wt. 1 1.7 mg/kg dry wt. 1 43.6 mg/kg dry wt. 1 0.87 mg/kg dry wt. 1 0.61 mg/kg dry wt. 1 Prepared Analyzed Analyst 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/18/19 0000 DK 09/23/19 0000 ❑K Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 7 6)MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K910109 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD Result RL Units Level Result %REC Limits RPD Limit Notes Batch K190078 - Wet Chem Solid - SM 2540 G-2011 Blank (K190078-BLK1) Prepared & Analyzed: 09/10/2019 % Solids <1.00 1.00 % Duplicate (KI90078-DUP1) Source: K910109-01 Prepared &Analyzed: 09/10/2019 % Solids 38.0 1.00 % 36.6 Batch K190113 - Wet Chem Solid - SM 4500 NH3 C-2011 Blank (K190113-BLK1) Prepared & Analyzed: 09/13/2019 Ammonia as N <1.00 1.00 mg/kg dry wt. wet Blank (K190113-BLK2) Prepared & Analyzed: 09/13/2019 Ammonia as N <1.00 1.00 mg/kg dry wt. wet 4 10 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 7 �VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K910109 Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit RPD: Relative Percent Difference Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 8.7°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes CDC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes CDC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on CDC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments North Carolina DENR NPDES Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. �2lLlLX� L4iZdZe The data and information on this, and other accompanying documents, represents {{// only the sample(s) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental Reported: 09/24/2019 09:01 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 7 Fayetteville Division 2592 Hope Mills Road �- Fayetteville, NC 28306 (910) 864-1920 / 864- *K910'109* � ;Za �� ll��l��l�f Iil�lli�l�l��ll�l CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENT NAME & ADDRESS: VonDrehle Corp. 26 First Street Cordova, NC 28330 PO# I PROJECT I LOCATION: Cordova - 60-day series #OF B T T L E S TYPE OF ANALYSIS PRESERVATION CODE = E U E c E C U) •U a `� Q �, CL o V Ef .2 -FaO c.i t/) c .a J '(A t��o O a - Y' U Z (� = O c N E O (J) Q - p Z M O Z m Z Z Z a o a., F— z Y f— a Ul O ° o CODE: A = None B = HNO3 (pH<2) + c4°C C = H2SO4 (pH<2) + <4°c D= NaOH + <4°C E= ZN Acetate + <4°C F = HCI PERSON: CONTACTo Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER: �y DATE! METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB pH D.O. TEMPIC ems' CHLORINE Residual from paper plant 49// X 2 A A A A A I A I A A A Q' r 1 A A A A A A A A A Relnqut 1 Da/te Tl�n/e, S 9Re iv d b S' "M 2 e q Time d by: Data Time Received by: (Signature) Date Time 3 4 Relinquished by: Date me Received by: (Signature) Date Tlme 5 6 Comments or Special Hazards: REViL. 4V --�A Page 7 of 7 Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2019-6 MB Date Sampled: 11/12/2019 Date Reported: 11/24/2019 Reporting Period: Nov- Dec 2019 Parameter % PPM Dry Weight EPA Monthly Limits Solids 34.80 Nitrogen (TKN) 0.061 613.000 Phosphorus 0.007 72.000 Potassium 0.050 500.000 Sulfate 0.000 Calcium 17.500 175,000.000 Magnesium 0.176 1,760.000 Sodium 0.114 1,140.000 Iron --- Aluminum --- 1,370.000 Manganese --- Copper --- 33.100 1,500 Zinc --- 135.000 2,800 Ammonia Nitrogen 0.000 2.870 Nitrate N / Nitrite N --- 3.0900 Cadmium --- 2.8000 39 Chromium --- 1,200 Nickel --- 1.4000 420 Lead --- 1.2000 300 Arsenic --- 1.0000 41 Mercury --- 0.0200 17 Selenium --- 1.3000 100 pH 8.400 Calcium Carbonate Eq. 0.000 Organic Nitrogen 0.061 Molybdenum --- 3.6000 75 Chloride --- Boron Available P2O5 6)MICROBAC R Microbac Laboratories, Inc. - Fayetteville C CERTIFICATE OF ANALYSIS K9K0151 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Sunday, November 24, 2019 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 i 910.864.1920 p i www.microbac.com Page 1 of 7 �VMICROBAC- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9K0151 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 11 /12/2019 Cordova, NC 28330 Reported: 11/24/2019 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, K91<0151-01 Solid Grab 11/12/19 11:45 11/12/19 14:05 Grab Page 2of7 MICROsAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9K0151 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Lab Sample ID: K91<0151-01 Result Calculation Plant Available Nitrogen 186 EPA 300.0, Rev. 2.1 (1993) Nitrate as N 1.69 Nitrite as N <1.40 SM 2540 G-2011 % Solids 34.8 SM 4500 NH3 C-2011 Ammonia as N <2.87 SM 4500-Norg C-2011 Total Kjeldahl Nitrogen 613 Wet Chemistry Result Calculation Sodium Adsorption Ratio, SAR 0.530 EPA 9045 D pH at 25 °C 8.4 SM 4500 P F-2011 Phosphorus, Total (as P) Mercury SPLP Metals SW-846 6010B Aluminum Arsenic Cadmium Calcium Copper Lead Collected By: Wright Collection Date: 11/12/2019 11:45 RL Units Dilution Note Prepared Analyzed Analyst mg/kg 1 11/24/19 0040 11/24/19 0041 BNS 0.701 mg/kg dry 1 1.40 mg/kg dry 1 1.00 % 1 2.87 mg/kg dry 1 y 1.44 mg/kg dry 1 RL Units Dilution Note NA 1 1.0 S.U. 1 H 11/15/19 0107 11/16/19 1000 JAW 11/15/19 0107 11/16/19 1000 JAW 11/18/19 1040 CLS 11/18/19 1000 MT 11/15/19 0857 CL8 Prepared Analyzed Analyst 11/24/19 0040 11/24/19 0041 BINS 11/18/19 1355 CLB 72 3.5 mg/kg dry 1 11/16/19 1019 JAW Analyses Subcontracted to: Pace Analytical ( Huntersville) Result RL Units Dilution Note Prepared Analyzed Analyst 0.020 mg/kg 0.012 mg/kg dry wt. 1 11/15/19 1048 11/19/19 1457 TE Result RL Units Dilution Note Prepared Analyzed Analyst 1370 mg/kg 10 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE <1 1 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 2.8 mg/kg 0.1 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 175000 mg/kg 10 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 33.1 mg/kg 0.5 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 1.2 mg/kg 0.5 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 7 �VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9K0151 Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Lab Sample ID: K9K0151-01 SPLP Metals Result Magnesium 1760 mg/kg Molybdenum 3.6 mg/kg Nickel 1.4 mg/kg Potassium <500 Selenium 1.3 mg/kg Sodium 1140 mg/kg Zinc 135 mg/kg Collected By: Wright Collection Date: 11/12/2019 11A5 RL Units Dilution Note Prepared Analyzed Analyst 10 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 0.5 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 0.5 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 500 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 1 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 500 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE 1 mg/kg dry wt. 1 11/15/19 1127 11/17/19 2307 TE Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 7 �VMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9K0151 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Result RL Batch KK91610 - Wet Chem Solid - SM 2540 G-2011 Blank (KK91610-BLK1) % Solids <1.00 1.00 Duplicate (KK91610-DUP1) Source: K9K0151-01 % Solids 33.5 1.00 Batch KK91614 - Wet Chem Solid - SM 4500 NH3 C-2011 Blank (KK91614-BLK1) Ammonia as N <1.00 1.00 Blank (KK91614-BLK2) Ammonia as N <1.00 1.00 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes Prepared &Analyzed: 11/18/2019 Prepared &Analyzed: 11/18/2019 % 34.8 4 10 Prepared &Analyzed: 11/18/2019 mg/kg wet Prepared & Analyzed: 11 /18/2019 mg/kg wet Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p 1 www.microbac.com Page 5 of 7 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9K0151 Definitions %: Percent H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram NA: Not Applicable RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 3.5°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments North Carolina DENR NPDES Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. l The data and information on this, and other accompanying documents, represents J\ only the sample(s) analyzed. This report is incomplete unless all pages indicated Brittany Smith in the footnote are present and an authorized signature is included. Administration Reported: 11/24/2019 01:06 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 7 *K9K0151* Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 / 864-8 II IP, IIIIIIIIIIIIllP lul �I u�jl p�! CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENT NAME &ADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 PO t# PROJECT LOCATION: Cordova - 60-day series # OF B o T L E S TYPE OF ANALYSIS PRESERVATION CODE E E 3 Q C N U U '� N Q �, i?. C U += ,� O U E to c m O J E U) US 16 V Z = O N E O w � Q - O o Z = Z Z a o n Y i— n to o c°n ro c o CODE: A = None B = HNO3 (pH<2) + <4°C C = H2SO4 (pH<2) + <4°C o D=NaOH+<4 C E= ZN Acetate + <4°C F = HCl CONTACT PERSON: Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER: / DATE 1 METHOD OF SHIPMENT: Microbac LAB ID # SAMPLE TYPE DATE TIME COMP GRAB PH D.O. TEMP'C RES. CHLORINE Residual from paper plant �t rZ I [ (; �� X 2 A A A A A A A A A 1 1 A A A A A A A A A Rel' Date , Time OI Re ei ed b ( Data ],,/,, Time Relinquished by: Date Time Received by: (Signature) Date Time 3 4 Relinquished by: to Time Received by: (Signature) Date Time 5 g Comments or Special Hazards: Page 7 of 7 TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT *MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0355 Project Description Residuals Sample -Annual For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NNCCy28330 Jeanne Overstreet Client Relationship Specialist, Environmental Monday, February 11, 2019 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil samples are reported on a 'dry -weight' basis unless specified otherwise. Analytical results for water and wastes are reported on a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 8 �DMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0355 Von Drehle Corporation Project Name: Residuals Sample -Annual Mr. Chris Fowler Project / PO Number: 2030767 126 First Street Received: 01/24/2019 Cordova, NC 28330 Reported: 02/11/2019 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from paper plant K9A0355-01 Solid Grab 01/24/19 12:19 01/24/19 14:28 Page 2 of 8 �gDMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0355 Analytical Testing Parameters Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K9A0355-01 Collection Date: 01/24/2019 12:19 Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Result RL Units Note Prepared Analyzed Analyst Method: 9045D Corrosivity pH 8.49 UNITS 01/31/19 1440 AWE Temperature At Determination (C) 19.3 UNITS 01/31/19 1440 AWE 8270 TC Result RL Units Note Prepared Analyzed Analyst Method: 8270C 1,4-Dichlorobenzene <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB 2,4,5-Trichlorophenol <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB 2,4,6-Trichlorophenol <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB 2,4-Dinitrotoluene <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB Hexachlorobenzene <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB Hexachlorobutadiene <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB Hexachloroethane <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB m-,p-Cresol <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB Nitrobenzene <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB o-Cresol <100 100 ug/L 02/01/19 1205 02/05/19 1449 SCB Pentachlorophenol <500 500 ug/L 02/01/19 1205 02/05/19 1449 SCB Pyridine <500 500 ug/L 02/01/19 1205 02/05/19 1449 SCB Surrogate: 2,4,6-Tribromophenol 111 Limit: 22-142 % Rec 02/01/19 1205 02/05/19 1449 SCB Surrogate: 2-Fluorobiphenyl 97.6 Limit: 43-116 % Rec 02/01/19 1205 02/05/19 1449 SCB Surrogate: 2-Fluorophenol 50.9 Limit: 19-119 % Rec 02/01/19 1205 02/05/19 1449 SCB Surrogate: Nitrobenzene-d5 89.5 Limit: 35-114 % Rec 02/01/19 1205 02/05/19 1449 SCB Surrogate: p-Terphenyl-d14 81.2 Limit: 10-130 % Rec 02/01/19 1205 02/05/19 1449 SCB Surrogate: Phenol-d5 34.9 Limit: 10-94 % Rec 02/01/19 1205 02/05/19 1449 SCB Ignitability of Solids Result RL Units Note Prepared Analyzed Analyst Method: 1030 Bumrate - 1030 <2.20 2.20 mm/sec 02/06/19 1100 JDH Mercury Result RL Units Note Prepared Analyzed Analyst Method: 7470A Mercury <0.00200 0.00200 mg/L 02/04/19 1012 02/04/19 1542 KEH Metals by 6010 Result RL Units Note Prepared Analyzed Analyst Method: 6010C Arsenic, TCLP <1.00 1.00 mg/L 02/04/19 0650 02/06/19 1214 KKB Barium, TCLP 0.301 0.100 mg/L 02/04/19 0650 02/06/19 1214 KKB Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com I Page 3 of 8 (�>MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0355 Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K9A0355-01 Collection Date: 01/24/2019 12:19 Metals by 6010 Result RL Units Note Prepared Analyzed Analyst Cadmium, TCLP <0.100 0.100 mg/L 02/04/19 0650 02/06/19 1214 KKB Chromium, TCLP <0.200 0.200 mg/L 02/04/19 0650 02/06/19 1214 KKB Lead, TCLP <1.00 1.00 mg/L 02/04/19 0650 02/06/19 1214 KKB Selenium, TCLP <0.800 0.800 mg/L 02/04/19 0650 02/06/19 1214 KKB Silver, TCLP <0.100 0.100 mg/L 02/04/19 0650 02/06/19 1214 KKB Percent Solids Result RL Units Note Prepared Analyzed Analyst Method: ASTM D2216-10 Percent Solids 41.1 1.00 weight % 02/05/19 0813 KMG Reactivity, Cyanide Result RL Units Note Prepared Analyzed Analyst Method: SW7.33 Reactivity, Cyanide <9.93 9.93 mg/kg 02/04/19 1514 APH Sulfide (Reacitivity) Result RL Units Note Prepared Analyzed Analyst Method: SW7.34 Reactivity, Sulfide <100 100 mg/kg 02/04/19 1400 EPT TCLP HERBICIDES Result RL Units Note Prepared Analyzed Analyst Method: 8151A 2,4-D <20.0 20.0 ug/L 02/04/19 1708 02/06/19 1504 ECL 2,4,5-TP (Silvex) <2.00 2.00 ug/L 02/04/19 1708 02/06/19 1504 ECL Surrogate: 2,4-Dichlorophenylacetic acid 58.9 Limit: 20-144 % Rec 02/04/19 1708 02/06/19 1504 ECL Volatile Organics Result RL. Units Note Prepared Analyzed Analyst Method: 8260B 1,1-Dichloroethene <50.0 50.0 ug/L 02/01/19 2247 EEA 1,2-Dichloroethane <50.0 50.0 ug/L 02/01/19 2247 EEA Benzene <50.0 50.0 ug/L 02/01/19 2247 EEA Carbon tetrachloride <50.0 50.0 ug/L 02/01/19 2247 EEA Chlorobenzene <50.0 50.0 ug/L 02/01/19 2247 EEA Chloroform <50.0 50.0 ug/L 02/01/19 2247 EEA Methyl Ethyl Ketone <100 100 ug/L 02/01/19 2247 EEA Tetrachloroethene <50.0 50.0 ug/L 02/01/19 2247 EEA Trichloroethene <50.0 50.0 ug/L 02/01/19 2247 EEA Vinyl chloride <100 100 ug/L 02/01/19 2247 EEA Surrogate: 1,2-Dichloroethane-d4 110 Limit: 80-120 % Rec 02/01/19 2247 EEA Surrogate: 4-Bromofluorobenzene 91.1 Limit: 86-115 % Rec 02/01/19 2247 EEA Surrogate: Dibromofluoromethane 101 Limit: 86-118 % Rec 02/01/19 2247 EEA Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 8 Microbac Laboratories, Inc. - Fayetteville Client Sample ID: Residual from paper plant Sample Matrix: Solid Lab Sample ID: K9A0355-01 Volatile Organics Surrogate: Toluene-d8 CERTIFICATE OF ANALYSIS K9A0355 Result RL Units 94.6 Limit: 88-110 % Rec Collected By: Wright Collection Date: 01/24/2019 12:19 Note Prepared Analyzed Analyst 02/01/19 2247 EEA Microbac Laboratories, In 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 8 6)MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0355 Batch Quality Control Summary: Microbac Laboratories, Inc. - Ohio Valley Spike Source %REC RPD Reactivity, Cyanide Result RL Units Level Result %REC Limits RPD Limit Notes Batch WG694692 - SW7.33 - SW7.33 BS (WG694692-01) Reactivity, Cyanide ND 200 Sulfide (Reacitivity) Result RL Batch WG694653 - SW7.34 - SW7.34 Prepared: Analyzed: 02/04/2019 mg/kg 11.8 .5-110 50 U Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes BLK (WG694653-01) Prepared: Analyzed: 02/04/2019 Reactivity, Sulfide ND 8.00 mg/kg - BS (WG694653-02) Prepared: Analyzed: 02/04/2019 Reactivity, Sulfide 19.0 8.00 mg/kg 124 10-150 50 BS (WG694653-03) Prepared: Analyzed: 02/04/2019 Reactivity, Sulfide 1290 100 mg/kg 101 10-150 50 Definitions MDL: Minimum Detection Limit RL: Reporting Limit RPD: Relative Percent Difference U: Not detected at or above adjusted sample detection limit Cooler Receipt Log Cooler ID: Default Cooler Cooler Inspection Checklist Ice Present or not required? Custody seals intact or not required? COC includes customer information? Sample collector identified on COC? Correct type of Containers Received Containers Intact? Enough sample volume for indicated tests received? Samples arrived within hold time? Chemical preservations checked or not required? VOA vials have zero headspace, or not recd.? Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Temp: 4.1 °C U Yes Shipping containers sealed or not required? Yes Yes Chain of Custody (COC) Present? Yes No Relinquished and received signature on COC? No No Sample type identified on COC? No No Correct number of containers listed on COC? No No COC includes requested analyses? No No Sample labels match COC (Name, Date & Time?) No No Correct preservatives on COC or not required? No No Preservation checks meet method requirements? No No North Carolina DENR NPDES Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 8 �VMICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9A0355 Report Comments Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the samp/e(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. Reviewed and Approved By: Jeanne Overstreet Client Relationship Specialist, Environmental Reported: 02/ 11 /2019 11:47 Microbac Laboratories, In 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 8 l c rm w;;5 Fayetteville Division 2592 Hope Mills Road -Fayetteville, NC 28306 (910) 864-1920 / 884 'K9A0355• IR7W1IN@ CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CL ENT NAME S ADDRESS VonDrehle Corp. 126 First Street Cordova, NC 28330 Fos PROJECT:LOCATN)N Cordova - Yearly OF a O T r L E S TYPE OF ANALYSIS PRESERVATION CODE _ U Q' to w CC J � m x = a J F < X UU C J F < —12 0 c J I p w c J F CODE. A = <4•C ONLY B = HNO3 (ph<2) + <4•C c = H2SO4 (pI <z)+<a c D = NaOH + <4•C E = ZN Acetate + <4•C F - Sodium Thlo. CONTACT PERSON: Mr. Chris Fowler PHONE 910-410-9131 SAMPLER DATE) METHOD OF SHIPMENT: Microbac LAS ID >K SAMPLE TYPE DATE TIME COMP ORAD PH D.O. TEMP•C ROBIN �l Residual from paper plant )` I/�j i L.! g X 2 A A A A A A J R. by0.1. C rim. nawnl D.H. rim. 1 11y /✓ M.t� z I-JI 4-1 2 R.IInquM d!y D.t. Tina 19tV. try: ISlr..wnl oat. rim. 3 4 Rwi'A"hW/y 0- rim R-.—Gy: tSlpnawn) D— rim 5 6 R.rnR.i — by Oat. Tim. R.e.rvM W: (sian.wn) Da. Tim. 7 8 Comments cr Speclal Hazards Page 8 of 8 PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WWTP Name: Cordova Facility NPDES Number: Monitoring Period: From 1/1/2019 To 2/28/2019 WQ0005135 NA Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) 0 Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment[] Thennophilic ❑ Beta Ray ❑ Gaimna Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ 77777 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Y Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ .............. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot denses e- Frequency of Analysis Sample Type Analytical Tech - nioue MinimumGeo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.9 GPams 0 imonthl Grab 1E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) R1 No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Prep er Name and Title (type or print) Land Appli Name and Title (if applicable)(type or print) ;Z� 2- S,-ly ---z— Z-3 = a Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WWTP Name: Cordova Facility NPDES Number: Monitoring Period: From 3/1/2019 To 4/30/2019 WQ0005135 NA Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) 0 Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Ell Heat Drying ❑ Heat Treatment❑ Thennophilic ❑ ............ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ ............ ' Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ —7777 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Y Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ ............... .........."` If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type na ytica Tech - Waue Minimum Geo. Mean Maximurd Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) < 0.6 NA 0.7 Gras 0 imonthl Grab PA E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 10 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer e and Title (type or print) Land Ap r Name and Title (if applicable)(type or print) 2— C cp 2 --r, U Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility Monitoring Period: From 5/1/2019 To NPDES Number: NA 6/30/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑T Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) CI AIt.D (No Prior Test) ElProcess to Further Reduce Pathogens El If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment[] Thennophilic ❑ ............. .................. Beta Ray 01 Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": V Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ .............. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dences Frequency of Analysis Sample Type Analytical Tech - Woue Minimum Geo. Mean Maximu Units Fecal Colifonn 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.9 Gr m's 0 imonthl Grab 1E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) Rl No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Nape and ' le (type or print) Land Applier Name and Title (if applicable)(type or print) a4-:� 2-s'-20 24Y=Z. Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 7/1/2019 To 8/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) 0 A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment:- l Thertnophilic ❑ Beta Ray LI Gamma Ray ❑ Pasteurization LJ Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens Ll If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Li Air Drying L] Composting Ll lAerobic Digestion Ll Anaerobic Digestion Ll .............. "' .. . . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- Frequency of Analencesysis Sample Type Analytical Tech - nioue Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.6 Grams 0 imonthl Grab 1E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ 1Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Preparer Name and Title (type or print) 01-� 111�-- Signature of Preparer* Mr. Chris Fowler, Land Application ORC Land Applier Name and Title (if applicable)(type or print) zo 2-5 - U' Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T N 2/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 9/1/2019 To 10/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) Q 7 Alt B (Alk Treatment) ElAlt. C (Prior Testing) Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment[] Thennophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": v Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ .....` . `. `. .. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ot Excee- Frequency of Analysis Y Sample Type Analytical Tech - Waue Minimum Geo. Mean aximu Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) < 0.6 NA < 0.6 GPams 0 imonthl Grab E682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 21 No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Appl' Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T N 2/20061 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WWTP Name: Cordova Facility WQ Permit Number: WQ0005135 NPDES Number: NA Monitoring Period: From 10/1/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) El Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) t] AIt.D (No Prior Test) ElProcess to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment[] Thermophilic ❑ Beta Ray ❑ Gamma Ray ElPasteurization ❑ Class B: Alt. (1) Fecal Density 0I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": V Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ . .............. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number o Excee- Frequency of Analysis Y Sample Type na ytica Tech - waue Minimu Geo. Mean aximu Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) < 0.6 NA 0.8 Gras 0 imonthl Grab E 1682 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) O Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Rl CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Pre/parer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) FECAL COLIFORM AND SALMONELLA DOCUMENTATION Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Jan-19 Biological Consulting Services ...... ............. ..... : .. value a...............M. Secondary:.:valuealmanella ...... .. ...................................................................*.................... ...................... .................. .. ... .. ............ ........ .... ....... ........ ... ........... .'.... .N:per:g#M _ ..,:XY 1901066 1/09/19 < 0.07 < 0.6 1901067 1/09/19 < 0.07 < 0.7 1901068 1/09/19 < 0.07 < 0.9 1901069 1/09/19 < 0.07 < 0.7 1901070 1/09/19 < 0.07 < 0.6 1901071 1/09/19 < 0.07 < 0.6 1901072 1/09/19 < 0.07 < 0.6 ............... ................ Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. January 16, 2019 Robert Branch Branch Residuals and Soils 8646 W. Market St. Suite 111 Greensboro NC 27409 336-510-0340 bbranch@branchrs.com Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7 BCS ID: 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Cordova Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Imo , L ✓1 t it l� 11 �1 i Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2005 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES i�13��lVlRFc Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-1 Sample Date/Time: January 08, 2019 13:54 BCS Sample ID: 1901066 Sample Description: Biosolids Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 41.5 Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-2 Sample Date/Time: January 08, 2019 13:57 BCS Sample ID: 1901067 Sample Description: Biosolids Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 38.0 Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/]EC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES J��=NfRa Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-3 BCS Sample ID: 1901068 Date Received: January 09, 2019 10:05 Amount Analyzed: 30.00 g Analysis Start: January 09, 2019 10:30 Analyst: Greta Pallack, B.A. Sample Date/Time: January 08, 2019 14:00 Sample Description: Biosolids Amount Submitted:100ml bottle % Solids: 30.4 Receipt Temperature: 5.4 deg C Preserved: Yes Analysis Stop Date: January 12, 2019 11:40 Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-4 BCS Sample ID: 1901069 Date Received: January 09, 2019 10:05 Amount Analyzed: 30.00 g Analysis Start: January 09, 2019 10:30 Analyst: Greta Pallack, B.A. Sample Date/Time: January 08, 2019 14:03 Sample Description: Biosolids Amount Submitted:100ml bottle % Solids: 40.1 Receipt Temperature: 5.4 deg C Preserved: Yes Analysis Stop Date: January 12, 2019 11:40 Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 'a_IIaC'--NIRAA r 1 11 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-5 Sample Date/Time: January 08, 2019 14:06 BCS Sample ID: 1901070 Sample Description: Biosolids Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 41.3 Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-6 Sample Date/Time: January 08, 2019 14:08 BCS Sample ID: 1901071 Sample Description: Biosolids Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 40.2 Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 41 ^ ! '^may <ccn coy o0 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-7 Sample Date/Time: January 08, 2019 14:12 BCS Sample ID: 1901072 Sample Description: Biosolids Date Received: January 09, 2019 10:05 Amount Submitted:100ml bottle % Solids: 40.4 Amount Analyzed: 30.00 g Receipt Temperature: 5.4 deg C Preserved: Yes Analysis Start: January 09, 2019 10:30 Analysis Stop Date: January 12, 2019 11:40 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ._� a�aG=iVIR/ At" T-W Client: Branch Residuals and Soils Project: Cordova Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924. ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined I am familiar with the information submitted herein. The results pertain only to analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted documents. The analysis was authorized commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. td� Date: January 16, 2019 Page 7 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES -57 �aCl91ftA !? �� 1: DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & laboratory practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence for the presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. LI Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and associated method blank. Data may not be accurate. Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate. Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A BCS is not currently accredited for this analyte. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 1901066, 1901067, 1901068, 1901069, 1901070, 1901071, 1901072 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES WAN CHAIN OF CUSTODY RECORD BCS? Laboratories %ww.microbioservices.com 4609 NW 6th street, Building A FL DOH Laboratory #E82924, EPA# FL01'147 Gainesville, FL 32609 I Tel. (3 ,2) 377-9272, Fax. (352) 377-5630 Client Name and Address: 1 A-C- �ti I:�y •; ,j� ` �; (`� �.� �, z'.�t��;�j Compliance Monitoring? F—]Yesr No City/State/-Lip: .;'G• /(l. Lci{; �( /l'I ,�►! I�' ����r'�i - �i:: fc L ,mot bni ±, .? Project ID: V�U.t Project Mianayer: /, 7 ,g i' Facility/Site: < IJ' C6;1& 1' Telephone Number: Fax No.: Report To: 3'1, Sampler Namt8: (11'rint) -1�: h >'�i? f�( Email: I h rGl a,-. ,;1 ���? �/ L-1�5 G• — Sampler Signature: -- � �� %z invoice To: 5 - F Prest:rvative Matrix— I Analysis a a C o L N � o U Y U ri n D C. Q M_ cc -0 O Ti ` IC rn C. L; U ' G ii U U U- .Car11�118If: / DC:aCPIjItIQtI r _ -- E Z N U U U U n C h Y'• ' " Li (O A V0-5 •y 'J` ci 4, � :U n• c tLJ N U O CtJ v 2 0 = E u CL U rt �I N m ul 7_ c' trn I w n Ire N _{ U r C c a ir, C C' 11 G t'3 �- E O Ci U lJ 1 7 :L ri C O a a m U UI U1 U L w F- :- tL tl (') 2 Branch Residuals and Soils 1 VD4 _ (i� 1 ^� 1901069 J ` 01/09/2019 10:05 C is Q L IL Branch Residuals and Soil VD-6 1901071 01/09/2019 10:05 Branch Residuals and Soils Branch Residuals and Soil VD-5 VD-7 1901070 I 1901072 01/09/2019 10:05 -I— ;, } 01/091201910:05 �— Branch Residuals and Soils _ Branch Residuals and Soils Branch Residuals and Soils VD-2 VD-3 I_ VD-1 1901067 1901068 Spr 1901066 01/09/2019 10:06 01/09/2019 10.05 01/09/2019 10:05 Method of Shipment: UPS/ Postal DI-11- FEDEX Other: Reli g6iched b- : Date Time Received by: Date Time Relinquished by: Date Time Received by BCS Laboratories: Date Time INA I Laboratory Comments: CQ I °C Temp. @ recp't: �• Corrected for IR Custody Seal: Intact l/ Broken N/ Presence of visable ice Presence of ice pack$ ✓__ / Y l� Hold Time J..:�. G...r•. JIF :�' [e..le•r.s lam. Llt•..�•G'e.v an xr.U�G:. [•-1••'y.".`t: Yn�Y•:�k Yrl Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Mar-19 Biological Consulting Services Cali:# i Da...rnzed....P....a '' '... ..... .: '`ii r.'::atiieSalmoll .. n....e'° . ....i..i..l.m......o... .. ...............l...l....a........ .. €.r....l..VPN 'YIP .......:. 1903149 3/11/19 < 0.07 < 0.6 1903150 3/11/19 < 0.07 < 0.6 1903151 3/11/19 0.07 0.700 1903152 3/11/19 < 0.07 < 0.6 1903153 3/11/19 < 0.07 < 0.6 1903154 3/11/19 0.07 0.700 1903155 3/11/19 < 0.07 < 0.6 Exceedances p All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. March 20, 2019 Robert Branch Branch Residuals and Soils 8646 W. Market St. Suite 111 Greensboro NC 27409 336-510-0340 bbranch@branchrs.com Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7 BCS ID: 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Cordova Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT !N FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES `. ;alaclHRA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-1 BCS Sample ID: 1903149 Date Received: March 12, 2019 09:53 Amount Analyzed: 30.00 g Analysis Start: March 12, 2019 11:00 Analyst: Greta Pallack, B.A. Sample Date/Time: March 11, 2019 13:57 Sample Description: Biosolids Amount Submitted:100ml bottle %Solids: 43.8 Receipt Temperature: 0.4 deg C Preserved: Yes Analysis Stop Date: March 20, 2019 13:30 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-2 BCS Sample ID: Date Received: Amount Analyzed Analysis Start: Analyst: 1903150 March 12, 2019 09:53 30.00 g March 12, 2019 11:00 Greta Pallack, B.A. Sample Date/Time: March 11, 2019 14:02 Sample Description: Biosolids Amount Submitted:100ml bottle % Solids: 43.0 Receipt Temperature: 0.4 deg C Preserved: Yes Analysis Stop Date: March 20, 2019 13:30 Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/]EC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AM Aiwwl- lacy Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-3 Sample Date/Time: March 11, 2019 14:07 BCS Sample ID: 1903151 Sample Description: Biosolids Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 43.3 Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30 Analyst: Greta Pallack, B.A. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-4 Sample Date/Time: March 11, 2019 14:12 BCS Sample ID: 1903152 Sample Description: Biosolids Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 43.8 Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-5 Sample Date/Time: March 11, 2019 14:17 BCS Sample ID: 1903153 Sample Description: Biosolids Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 44.0 Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-6 Sample Date/Time: March 11, 2019 14:22 BCS Sample ID: 1903154 Sample Description: Biosolids Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 44.0 Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30 Analyst: Greta Pallack, B.A. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None Page 4 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �ISC-HfRA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova Client Sample ID: VD-7 Sample Date/Time: March 11, 2019 14:27 BCS Sample ID: 1903155 Sample Description: Biosolids Date Received: March 12, 2019 09:53 Amount Submitted:100ml bottle % Solids: 44.0 Amount Analyzed: 30.00 g Receipt Temperature: 0.4 deg C Preserved: Yes Analysis Start: March 12, 2019 11:00 Analysis Stop Date: March 20, 2019 13:30 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES '� ��ac=lgRa Client: Branch Residuals and Soils Project: Cordova Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924. ISO/IEC 1 7025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11ac-ls11RQGAAM if ��w' sccnco-i. I certify that I have examined I am familiar with the information submitted herein. The results pertain only to analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted documents. The analysis was authorized commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: March 20, 2019 Page 7 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES laci�aAIIAB DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & laboratory practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence for the presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and associated method blank. Data may not be accurate. Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate. Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A BCS is not currently accredited for this analyte. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 1903149, 1903150, 1903151, 1903152, 1903153, 1903154, 1903155 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES aC'MRAAA6 \��F Acc, co.-r.o CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices-com 4.609 NW 6th street, Building A ... ir�c. FL DOH Laboratory #E82924, EPA# FL01147 FL Gainesville; FL — Tel. (352) 377-9272, Fax. (352) 377-5630 Client Name and Address: 1 (7 7•-�'� )r = ��• --ts ' �t r I ; Compliance Monitoring? Yes❑ 140 City/State/Zip: Project ID: Project Manager: h .-I _( Facility/Site: V o,, T�i��i,Jt Ji (� r-• t ra t>k4,'1 Telephone Number: Fax No.: Report To: i; Sampler Name: (Print) f>i; JJ /�� a��- Email: J� 1�r�•:-,r r.�� �' _�,z <; r.•�, f: ;. i Sampler Signature: �(��— Invoice To: Preservative Matrix I_ Analysis N 2 •> m U -- ci C a N O d Y W N 2 '\ N fl. CL C CO U U CL N .. M O rq 'D�i, .. ,� 2 'j a U O` E i= m a a n c c, U �' 9 a? io °' �i ', � I G�y7 m a Z 'C o 3 U a � Z � > O 5 N m U CU o .= v F- c N E W 0 U __ w 0 8 d — = N Ip N G N 6! n '> a t9 3 m .Vjl a W N N rl yr 0 U .O U of •p U L C c, U N C Ql E N 3 ;: Q �- rn a) caEo U T 0 1 0 c o d Y c 4 L d tD c7 q _ O 0 C o L iv ° E ~ d Z m ° ° a " m E F- L ° m ° o ° 0 Q Q w w Z`CL c o m U N a �o M w a z o rc Sample ID ! Description a r� z o in U ui u� r = cn �r - ���%/.i� f . °i Branch Residuals and Soils VD-1 1903149 03/12/2019 9:53 Branch Residuals and Soils Branch Residuals and Soils VD-4 1903152 03/12/2019 9:53 Branch Residuals and Soils ` ,n o (n m in h La CD L/ I� " I Z• �'Z ` 4 I J r 'J j iL VD-2 1903150 03/12/2019 9:53 Branch Residuals and Soils VD-5 1903153 03/12/2019 9:53 Branch Residuals and Soils z u r. o: t o u I) C. z 2 , A Z' G� ' f, VD-3 VD 6 m 1903151 03/12/2019 9:53 1903154 03/12/2019 9:53 Special Instructions: Laboratory Comments: Method of Shipment: UPS Postal DHL FEDEX Other: Temp. @ recp't: i f `C Relinqjished,6y� Date Time Received by: Date Time IR- Corrected f -IR f / 7 Custody Seal: Intact I Broken /G --� -11/vi 7 ��� Presence of visable ice Relinquished by: Date Time Received b B 'S Labo Loris ate Time Presence of ice pac s (1'J N �' I/1 AA ')!' �' c/L�IHoId Time_ .a..-aea w.wuoe eov e.snws wn r .rdv.•n..wvto:s cocmosirsn�w+• Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 May-19 Biological Consulting Services .......... — ... ............. ..... .I......... A... .......................... . on ar:y;4�1�fi-ta.lj4 a .: ............... .. ........... ....... ... . N... ........ ....... 00... ........ ..i. PN4::0............................... 0�* ..... ...9. )Qu: 1905234 5/15/19 < 0.07 < 0.9 1905235 5/15/19 < 0.07 < 0.6 1905236 5/15/19 < 0.07 < 0.7 1905237 5/15/19 < 0.07 < 0.8 1905238 5/15/19 < 0.07 < 0.7 1905239 5/15/19 < 0.07 < 0.7 1905240 5/15/19 < 0.07 <1 0.8 . . . . . . . . . . . . . . . . . . . . . . . . Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. 3kinc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. May 21, 2019 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 190S234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: N/A Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, J Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LAB0RATORIES 7�C=hfRA'A&B \� +ccnco -cn Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD1 Sample Date/Time: May 15, 2019 14:07 BCS Sample ID: 1905234 Sample Description: Biosolids Date Received: May 16, 2019 10:07 Amount Submitted:100 mL bottle % Solids: 30.5 Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD2 Sample Date/Time: May 15, 2019 14:09 BCS Sample ID: 1905235 Sample Description: Biosolids Date Received: May 16, 2019 10:07 Amount Submitted:100 mL bottle % Solids: 40.4 Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISOAEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD3 BCS Sample ID: Date Received: Amount Analyzed Analysis Start: Analyst: 1905236 May 16, 2019 10:07 30.00 g May 16, 2019 11:45 Wei -yea Hsu, M.S. Sample Date/Time: May 15, 2019 14:12 Sample Description: Biosolids Amount Submitted:100 mL bottle % Solids: 39.6 Receipt Temperature: 6.6 deg C Preserved: Yes Analysis Stop Date: May 21, 2019 12:55 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD4 BCS Sample ID: 1905237 Date Received: Amount Analyzed: Analysis Start: Analyst: May 16, 2019 10:07 30.00 g May 16, 2019 11:45 Wei -yea Hsu, M.S. Sample Date/Time: May 15, 2019 14:15 Sample Description: Biosolids Amount Submitted:100 mL bottle % Solids: 32.5 Receipt Temperature: 6.6 deg C Preserved: Yes Analysis Stop Date: May 21, 2019 12:55 Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 190S234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ;11^LEAA 1 102 � *J ,.o r .> Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD5 BCS Sample ID: 1905238 Date Received: May 16, 2019 10:07 Sample Date/Time: May 15, 2019 14:17 Sample Description: Biosolids Amount Submitted:100 mL bottle % Solids: 35.7 Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD6 BCS Sample ID: 1905239 Date Received: May 16, 2019 10:07 Amount Analyzed: 30.00 g Analysis Start: May 16, 2019 11:45 Analyst: Wei -yea Hsu, M.S. Sample Date/Time: May 15, 2019 14:20 Sample Description: Biosolids Amount Submitted:100 mL bottle % Solids: 36.4 Receipt Temperature: 6.6 deg C Preserved: Yes Analysis Stop Date: May 21, 2019 12:55 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES r yyqk aCT r Client: Branch Residuals and Soils Analysis: Salmonella Project Name: N/A Client Sample ID: VD7 BCS Sample ID: 1905240 Date Received: May 16, 2019 10:07 Sample Date/Time: May 15, 2019 14:22 Sample Description: Biosolids Amount Submitted:100 mL bottle % Solids: 34.4 Amount Analyzed: 30.00 g Receipt Temperature: 6.6 deg C Preserved: Yes Analysis Start: May 16, 2019 11:45 Analysis Stop Date: May 21, 2019 12:55 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES At" .1,4•� ,,. eye. Client: Branch Residuals and Soils Project: N/A Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES . ,, e ?- I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: May 21, 2019 Page 7 of 8 Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/]EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I alc-i R - rjj�',� �� X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). Value is between the laboratory method detection limit & laboratory practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and associated method blank. Data may not be accurate. y The laboratory analysis was from an improperly preserved sample. The data may not be accurate. Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analvsis notes. Page 8 of 8 Final Report BCS ID 1905234, 1905235, 1905236, 1905237, 1905238, 1905239, 1905240 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �^ A ^ti ��,,.o,..,, CHAIN OF CUSTODY RECORD www.microbioservices.com FL DOH Laboratory #E82924, EPA# FLO1147 Client Name and Address: City/State/Zip: Project Manager: Telephone Number: Fax No.: Sampler Name: (Print) Sampler Signature: Preservative I Matrix Project ID: Facility/Site: Report To: Email: Invoice To: BCS Laboratories 4609 NW 6th street, Building A Gainesville, FL 32609 Tel. (352) 377-9272, Fax. (352) 377-6630 Compliance Monitoring? Yes❑ No Sample ID / Description � O O N CD N n y C C O o ZC^ m o U LL y LL C O U S a C v ° c) Q O Z Y n w a o 1E c > mVy C6 U v 0, 1 w nU to •2 c C N �N W O N o Z ¢ Q w D ti �+ E O N O—O0 U O ui w E 4 mu w > U`. O _ ca cc p O FL a m O a O c0 Ql -J a) z llCDnF-` j OO .a d U. - FQFv=- i Branch Residuals and Soils :. •j Vol �; 11 7 ;' , .• 05/161201910:07 c �� �- a n N �r - m o Branch Residuals and Soils ��N�, C Q �;' O o o VD2 9> O N °r' � O Ln r r i0 t0 N r 1905236 y T N> m v> N �J t1 ?'' 05/16/2019 10:07 r 0 Z d r •`Z Branch Residuals and Soils c N r Uo 1 VD3 - m` M c Branch Residuals and Soils 1905236 m m VD7 — 05/16/201910:07 1905240 _ Special Instructions: 05/16/2019 10:07 _ Laoorarory Comments: Method of Shipment: UPS Postal DHL FEDEY. Other: Temp. @ recp't: 66, -C Reli�ishecJ by: Date Time Received by: Date Time IR-10 Corrected for IR - he -AC, � -„ r- Custody Seal: Intact Broken Zvi%/Z/C I -J /J -/i' i ,J Presence of visable ice Y Relinquished by: Date Time ReC/�/1's b Laboratories: Dale Time Presence of ice packs Time N 51� •�9 A 07 (Hold � :� L ...•u+av re �.walec. ccs narnr mt�:ca:.,�. Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Jul-19 Biological Consulting Services .... -D t ..... .. mar Y.: P-A V ..... .. ....... ........ ............... ........................ ............... ................ ..... ........ ................ ............ 1907369 7/24/19 < 0.07 < 0.6 1907370 7/24/19 < 0.07 < 0.6 1907371 7/24/19 < 0.07 < 0.6 1907372 7/24/19 < 0.07 < 0.6 1907373 7/24/19 < 0.07 < 0.6 1907374 7/24/19 < 0.07 < 0.6 1907375 7/24/19 < 0.07 < 0.6 Exceedances .............. All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. 3inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, INC. July 31, 2019 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, 1 Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950. EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD1 Sample Date/Time: July 23, 2019 13:57 BCS Sample ID: 1907369 Sample Description: Biosolids Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 46.4 Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes Analysis Start: July 24, 2019 13:04 Analysis Stop Date: July 27, 2019 15:45 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD2 Sample Date/Time: July 23, 2019 13:59 BCS Sample ID: 1907370 Sample Description: Biosolids Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 44.9 Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes Analysis Start: July 24, 2019 13:09 Analysis Stop Date: July 27, 2019 15:45 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: _<0.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AAAB Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD3 Sample Date/Time: July 23, 2019 14:03 BCS Sample ID: 1907371 Sample Description: Biosolids Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 43.2 Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes Analysis Start: July 24, 2019 13:06 Analysis Stop Date: July 27, 2019 15:45 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD4 Sample Date/Time: July 23, 2019 14:07 BCS Sample ID: 1907372 Sample Description: Biosolids Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 44.1 Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes Analysis Start: July 24, 2019 13:09 Analysis Stop Date: July 27, 2019 15:45 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW. MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD5 BCS Sample ID: 1907373 Date Received: July 24, 2019 9:54 Amount Analyzed: 30.00 g Analysis Start: July 24, 2019 13:12 Analyst: Wei -yea Hsu, M.S. Sample Date/Time: July 23, 2019 14:10 Sample Description: Biosolids Amount Submitted:100 mL bottle % Solids: 42.9 Receipt Temperature: 7.8 deg C Preserved: Yes Analysis Stop Date: July 27, 2019 15:45 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD6 BCS Sample ID: 1907374 Date Received: July 24, 2019 9:54 Amount Analyzed: 30.00 g Analysis Start: July 24, 2019 13:17 Sample Date/Time: July 23, 2019 14:15 Sample Description: Biosolids Amount Submitted:100 mL bottle % Solids: 41.0 Receipt Temperature: 7.8 deg C Preserved: Yes Analysis Stop Date: July 27, 2019 15:45 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES At" Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD7 Sample Date/Time: July 23, 2019 14:20 BCS Sample ID: 1907375 Sample Description: Biosolids Date Received: July 24, 2019 9:54 Amount Submitted:100 mL bottle % Solids: 40.5 Amount Analyzed: 30.00 g Receipt Temperature: 7.8 deg C Preserved: Yes Analysis Start: July 24, 2019 13:21 Analysis Stop Date: July 27, 2019 15:45 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES , C-QkA A&B 1�. Client: Branch Residuals and Soils Project: Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �-, ► At" I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: July 31, 2019 Page 7 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/[EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 1907369, 1907370, 1907371, 1907372, 1907373, 1907374, 1907375 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:201 7 L2422 (ANAB), PA DEP# 68-03950, EPA# FL01 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES -=N1@A AM CHAIN OF CUSTODY RECORD BCS Laboratories ~� www.microbloservices.com 4609 NW 6th street, Building A '•`hrn ir1C. FL DOH Laboratory #E82924, EPA# FL01147 Gainesville, FL 32609 C Tel. (352) 377-9272, Fax. (352) 377-5630 Client Name and Address: �j.2/-" 1"'s-I L � %s� � � j Compliance Monitoring? El Yes No City/State/Zip: /-J3s yPckCB/,J J:A /c3 291 f � (� his 1 �C f �J� Project ID: ZuN- /l0 Project Manager: 86 Facility/Site:yu-1 Diaz Cu2JL, v a /,--I Telephone Number: Fax No.: ReportTo: Sampler Name: (Print) Email:c-- Sampler Signature: Invoice To:a-z y Sample ID / Description VI) l ns Preservatirei Matrix C'C O o W 41 'L L C •lo 'D m C O i 47 O U m Y to C E E U ro O C LL v O U d C H p —0p E o o m E H Z CD O L: 15 - I I I Z. 2- H. Branch Residuals and SoilF Vol 1907369 07/24/2019 9:54 Branch Residuals and Soils VD2 1907370 07/2412019 9:64 Method of Shipment: Date Time Received by: -�/? 411t? 2 <-�- /C—JJ/� L-- V V Date Time Received by 7 U U N C W y O rn 0 C) 0 ` � > O C1 7 p U Q C 0 v _v w U7 O 0 C O in o t O 7 5 Q 0- Branch Residuals and Soils VD3 1907371 07/24/2019 9:54 Postal DHL FEDEX Other: 77/ 10 16 10 Cl LO > o `o v € v "CL O O U co in p _ p U °� u C O f9 to f0 w U w W Fes— >W uu- Branch Residuals and Soils VD4 1907372 07/24/2019 9:64 _dboratory Comments: U �fl-zt-' I\ N o C ID ~ C" M cm C Branch Residuals and ' 00 VD5 1907373 07/2412019 9:54 Temp. @ recp't: Ia.0 () °C Time IR- (O Corrected fo—rIEL Custody Seal: Intact Broken Presence of visable lee -d..- Time N Presence of ice packs Y �Hold Time •o. nx w. u� cs .wf �. iwmuapreNRT(ECSGaCmm �trs..�sr Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Oct-19 Biological Consulting Services ....................................... We ji ij�ji . . . . . . . . . i i 61 lh*`::::::::: ...................... .......... S 0- "a"flair:: ...... ................. ................... ......... .................. ........................ ...... ...... 'A N:p Wjr, 1910022 10/02/19 < 0.07 < 0.6 1910023 10/02/19 < 0.07 < 0.6 1910024 10/02/19 < 0.07 < 0.6 1910025 10/02/19 < 0.07 < 0.6 1910026 10/02/19 < 0.07 < 0.6 1910027 10/02/19 < 0.07 < 0.7 1910028 10/02/19 < 0.07 < 0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. Inc. BIOLOGICAL CONSULTING SERVICES 3 OF NORTH FLORIDA, INC. October 08, 2019 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7 BCS ID: 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Analysis Method Salmonella EPA 1682; BCS SOP M-4 (1SO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 4W �Ici��►AA w Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-1 Sample Date/Time: October 01, 2019 14:01 BCS Sample ID: 1910022 Sample Description: Biosolid Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.7 Amount Analyzed: 30.06 g Receipt Temperature: 4.4 deg C Preserved: Yes Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-2 Sample Date/Time: October 01, 2019 14:06 BCS Sample ID: 1910023 Sample Description: Biosolid Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 40.8 Amount Analyzed: 30.01 g Receipt Temperature: 4.4 deg C Preserved: Yes Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: !90.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-3 Sample Date/Time: October 01, 2019 14:09 BCS Sample ID: 1910024 Sample Description: Biosolid Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.1 Amount Analyzed: 30.06 g Receipt Temperature: 4.4 deg C Preserved: Yes Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-4 Sample Date/Time: October 01, 2019 14:13 BCS Sample ID: 1910025 Sample Description: Biosolid Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.4 Amount Analyzed: 30.01 g Receipt Temperature: 4.4 deg C Preserved: Yes Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-5 Sample Date/Time: October 01, 2019 14:17 BCS Sample ID: 1910026 Sample Description: Biosolid Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 41.5 Amount Analyzed: 29.95 g Receipt Temperature: 4.4 deg C Preserved: Yes Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-6 Sample Date/Time: October 01, 2019 14:21 BCS Sample ID: 1910027 Sample Description: Biosolid Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 40.1 Amount Analyzed: 29.91 g Receipt Temperature: 4.4 deg C Preserved: Yes Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units — -- Page 4 of 8 Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/]EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I ^ U r, Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD-7 Sample Date/Time: October 01, 2019 14:25 BCS Sample ID: 1910028 Sample Description: Biosolid Date Received: October 02, 2019 10:33 Amount Submitted:100 mL bottle % Solids: 40.8 Amount Analyzed: 30.08 g Receipt Temperature: 4.4 deg C Preserved: Yes Analysis Start: October 02, 2019 11:05 Analysis Stop Date: October 08, 2019 10:57 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: _<0.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Project: Von Drehle Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES n.ccnco <cn I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. iCY��.�t'11�� Signature of Laboratory Director/Authorized Rep. Date. October 08, 2019 Page 7 of 8 Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/]EC 17025:2017 L2422 (ANAB), PA DEP# 68-03950. EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit & the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. - Page 8 of 8 — Final Report BCS ID 1910022, 1910023, 1910024, 1910025, 1910026, 1910027, 1910028 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES At"'"' CHAIN OF CUSTODY RECORD www.microbioservices.com FL DOH Laboratory #E82924, EPA# FLO1147 t--) Client Name and Address: 71 I �' I r C City/State/Zip: Project Manager: Telephone Number: Fax No.: Sampler Name: (Print) Sampler Signature: T$v� BCS Laboratories 4609 NW 6th street, Building A Gainesville, FL 32609 Tel. (352) 377-9272, Fax. (352) 377-5630 Compliance Monitoring? C�es[] No Report To: (ta,e,( Email: 4V%.r/�/�h 12s . Quote #: -Ne)'' Project ID: Zc;,1q-/l0 Invoice To: �A)A,,�'- Preservative Matrix Analysis -0 n n o - E m m U N 2 a Y U C \ 0 G 0 r v m C v o coi m n d U . °? lD a) -0 •U w vi m w 7 E o L) € m > U 4l ? aoi Q. E a !„p N a)_ y c U d m t5 3 7 N U o y o O f0 F 3 m E o (a o E L o 'Mn � a, m m' a E M Eh.S a m in � c le ID Description O F z 0 ii = az 9 _ o 0� i- n U3 C w0 uj w w u- = o cn 3) 0 0 6 w cn wSam D-1 1D 111 2.iz I l Branch Residuals and Soils 10022 10/02/2019 10:33 Branch Residuals and Soils VD-2 1910023 10102/201910:33 (A, 0 ti a M m N p O o V ( V� �?► f �� z. z� y� i m _ Branch Residuals and Soils Branch Residuals and Soils Branch Residuals and Soils m` Branch Residuals and Sods VD-4 VD 5 VD-6 1910026 1910027 VD-3 1910025 10/02/2019 10:33 10/02/2019 10:33 10102/2019 10:33 t 1910024 Special Instructions: 1010212019 10:33 1 1 Laboratory Comments: I 2 (0 'C Method of Shipment: UPS Postal DHL FEDEX Other: Temp. @ recp't: 1 r Relin ' hed �f Da a Time Received by: Dale Time IR- for IR // Presence of visable ice �5 //Co��rrected / Y N Relinquished by: Date Time Rece d y BCS Laboratories: �%�n pat Time` Hold Time �� f �`-� (�I7/7 /033 / �5 Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Dec-19 Biological Consulting Services ................................................ ........ ............................................ ........................................ .................................... ........................................ ......................... .................. ............................ .................. ....... ....... ............pe......... ....... ....... 1912179 12/12/19 < 0.07 < 0.6 1912180 12/12/19 0.07 0.800 1912181 12/12/19 < 0.07 < 0.7 1912182 12/12/19 < 0.07 < 0.6 1912183 12/12/19 < 0.07 < 0.6 1912184 12/12/19 < 0.07 < 0.7 1912185 12/12/19 < 0.07 < 0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. 1 inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLOR/DA, INC. December 19, 2019 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1, VD2, VD3, VD4, VD5, VD6, VD7 BCS ID: 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 191218S BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES OC7zmR�k A&B l�� • ccn - Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD1 BCS Sample ID: 1912179 Date Received: December 12, 2019 9:55 Amount Analyzed: 29.96 g Analysis Start: December 12, 2019 10:39 Sample Date/Time: December 11, 2019 14:14 Sample Description: Biosolid Amount Su bm itted: 100 mL bottle % Solids: 45.0 Receipt Temperature: 3.9 deg C Preserved: Yes Analysis Stop Date: December 17, 2019 9:28 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD2 BCS Sample ID: Date Received: 1912180 Sample Date/Time: December 11, 2019 14:16 Sample Description: Biosolid December 12, 2019 9:55 Amount Su bm itted: 100 mL bottle % Solids: 38.3 Amount Analyzed: 30.10 g Receipt Temperature: Analysis Start: December 12, 2019 10:39 Analysis Stop Date: Analyst: Wei -yea Hsu, M.S. Qualifier: Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.8 Salmonella MPN/4 dry grams Analysis Notes: None 3.9 deg C Preserved: Yes December 18, 2019 9:50 None Page 2 of 8 Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD3 Sample Date/Time: December 11, 2019 14:18 BCS Sample ID: 1912181 Sample Description: Biosolid Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 40.0 Amount Analyzed: 30.09 g Receipt Temperature: 3.9 deg C Preserved: Yes Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD4 Sample Date/Time: December 11, 2019 14:21 BCS Sample ID: 1912182 Sample Description: Biosolid Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 44.7 Amount Analyzed: 30.08 g Receipt Temperature: 3.9 deg C Preserved: Yes Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 1 7025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A A0Ag Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD5 Sample Date/Time: December 11, 2019 14:23 BCS Sample ID: 1912183 Sample Description: Biosolid Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 41.6 Amount Analyzed: 30.10 g Receipt Temperature: 3.9 deg C Preserved: Yes Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 150.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD6 Sample Date/Time: December 11, 2019 14:25 BCS Sample ID: 1912184 Sample Description: Biosolid Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 39.9 Amount Analyzed: 30.09 g Receipt Temperature: 3.9 deg C Preserved: Yes Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES _� - } TNI Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Client Sample ID: VD7 Sample Date/Time: December 11, 2019 14:30 BCS Sample ID: 1912185 Sample Description: Biosolid Date Received: December 12, 2019 9:55 Amount Submitted:100 mL bottle % Solids: 43.7 Amount Analyzed: 30.10 g Receipt Temperature: 3.9 deg C Preserved: Yes Analysis Start: December 12, 2019 10:39 Analysis Stop Date: December 17, 2019 9:28 Analyst: Wei -yea Hsu, M.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BC5 ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB). PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Project: Von Drehle Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISOAEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: December 19, 2019 Page 7 of 8 Final Report BCS ID 1912179, 1912190, 1912181, 1912182, 1912183, 1912184, 1912185 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. 0 Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. L1 Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 1912179, 1912180, 1912181, 1912182, 1912183, 1912184, 1912185 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2017 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 11G=iAf3i4'Ai&B CHAIN OF CUSTODY RECORD www.microbioservices.corn Inc . FL DOH Laboratory #E82924, EPA# FL01147 Client Name and Address: City/State/Zip: Project Manager: 15,-� Telephone Number: Fax No.: Sampler Name: (Print) Sampler Signature: rti 0roc-fival M.friv BCS Laboratories 4609 NW 6th street, Building A Gainesville, FL 32609 Tel. (352) 377-9272, Fax. (352) 377-5630 Compliiaar Toniton g? CYes❑ No Report To:n�r^r (Y� ✓` r '' Email: Quote #: Project ID: l/�t\,/V 04?ate r" Invoice To: V;u,4-,"( Annlvale U � CL O O y 2 7 GI a)y (� .Qd w U j U O Q c UU f0 U f0 O M U a =i . Om Q o. f0 c U N m N O m O = m CL aii in_ T =3 `p y p > OL � n Q 3 M (n (n O O f0 N O_ v •D 3 En C w 7 O U O O O d y U 75 E oo' m o d m E a� o co = o .o t w o. OU a� m v 0ffi E m E �, s z t v=i Sample ID /Description z `� a 9 z 9 o 3 00 `n w U ui w 9 w LL = I°- in 3 0 0 0� in `/ l� I .l%I/� Cf G , Branch Residuals and Soils VD1 Branch Residuals and Soils 1912179 12/12/2019 9:55 Branch Residuals and Soils 1912182 12/12/2019 9:55 Branch Residuals and Soils h 0 m y •� \J (J j z, ,�/ D C i VD2 1912180 VD5 1912183 ,� on m Cc a p N o `(� S 9 Z• 7 12/12/2019 9:55 12/12/2019 9:55 y ( a cu '- a y Branch Residuals and Soils l VD3 I 1 I I I I I I I Branch Residuals and Soils r u m ` m • �•, 1 1912181 12/12/2019 9:55 VD6 1912IN L+' 12/12/2019 9:55 Special Instructions: Laboratory Comments: I ` � 1 0 C G� Method of Shipment: C UPS Postal DHL FEDEX Other: Temp. @ recp't: 7 = •C �',y IR-Y1;Corrected for IR ed b9- Date Time Received by: Date ime 7/i /�� I21111l Y,'/�7 � ft . • � t t ,1J1 L '" Presence of visable ice Y Cl V I� Relinquished by: Date Time Received by BCS Laboratories: Time , a 4 Hold Time SOIL ANALYSIS REPORTS Page 1 of 4 Report Number: 19-193-0701 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 07/12/2019 0 Waypoint ANALYTICAL 'Every acre... Everyyear. "na Date Of Analysis: 07/15/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Farm: US-1 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss on Ignition Water pH Date Of Report: 07/24/2019 NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A M3 pprn Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 1 30965 2.9 L 102 18 M NC = 15 14 VL NC = 7 84 M 8124 VH 31 VL 8.1 0.0 41.5 MIN 2 30966 2.9 L 102 37 H NC=31 13 VL NC=7 113 M 18120 VH 42 VL 8.1 0.0 41.8 MIN 3 30967 3.3 M 110 28 M NC=23 11 VL NC=6 107 M 8100 VH 30 VL 8.1 0.0 41.6 MIN 4 30968 3.1 M 106 19 M NC = 16 20 VL NC = 10 97 M 8124 VH 29 VL 7.9 0.0 41.6 MIN 5 30969 5.2 H 148 8 L NC=7 16 VL NC=8 108 M 8079 VH 31 VL 8.2 0.0 41.5 MIN Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Exchangeable Sodium Percentage % K % Mg % Ca % Na % H % NO3N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 1 0.1 1.7 97.9 0.3 0.0 16 M NC=33 10.7 VH NC=267.5 5 VL NC=31 14 VL 1.7 M NC=85.0 0.6 H 0.020 2 0.1 2.3 97.1 0.4 0.0 21 H NC=44 12.2 VH NC=305.0 8 VL NC: 22 VL 1.9 M NC=95.0 0.6 H 0.140 3 0.1 2.1 97.4 0.3 0.0 16 M NC=33 11.6 VH NC=290.0 6 VLJ NC=38 16 VL 1.9 M NC=95.0 0.5 M 0.130 4 0.1 1.9 97.6 0.3 0.0 16 M NC=33 11.1 VH NC=277.5 6 VL NC=38 14 VL 1.2 M NC=60.0 0.7 H 0.140 5 0.1 2.2 97.3 0.3 0.0 20 M NC=42 14.5 VH NC=362.5 8 VL NC=50 6 VL 1.2 M NC=60.0 0.7 H 0.130 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Tennessee, Inc. Oscar Ruiz Page 2 of 4 Report Number: 19-193-0701 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 07/12/2019 Date Of Report: 07/24/2019 Waypoi t0 ANALYTICAL "Every acre... Every year.". Farm: US-1 SOIL FERTILITY RECOMMENDATIONS 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 KZO Mg S Zn Mn Fe Cu B Field ID bu/acre Tons/A lb/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 1 Soybeans 50 0.0 0 72 150 16 12 0 6 0 0 2 Soybeans 50 0.0 0 30 150 0 0 0 6 0 0 3 Soybeans 50 0.0 0 52 150 0 12 0 6 0 0.5 4 Soybeans 50 0.0 0 70 150 10 12 0 6 0 0 5 Soybeans 50 0.0 0 98 150 0 10 0 6 0 0 Comments: 30965 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30966 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30967 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30968 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30969 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. Sample(s) : 2,3,4,5 Crop: Soybeans For soybeans on soils with a pH of 6.2 or less, apply limestone as recommended and plant seed treated with molybdenum. Apply 1-2 oz of sodium molybdate (0.4-0.8 oz of elemental molybdenum) per acre as a seed treatment. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �• Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the f� work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Oscar Ruiz Page 3 of 4 Report Number: 19-193-0701 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 07/12/2019 Waypoi nt "0 ANALYTICAL "Every acre... Every year. "n,, Date Of Analysis: 07/15/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Farm: US-1 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Of Report: 07/24/2019 NC = North Carolina Fertility Index Value OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number % Rate Soil Class IbslA M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 6A 30970 2.4 L 92 13 L NC = 11 43 VL NC = 22 98 M 8114 VH 34 VL 8.0 0.0 41.6 MIN 6B 30971 4.8 M 140 12 L NC = 10 27 VL NC = 14 118 M 8068 VH 40 VL 7.8 0.0 41.6 MIN 7 30972 4.1 M 126 15 M NC = 12 19 VL NC = 10 111 M 8084 VH 26 VL 8.0 0.0 41.5 MIN 8 30973 4.1 M 126 11 L NC=9 24 VL NC 12 119 M 8075 VH 32 VL 8.2 0.0 41.6 MIN 9 30975 5.3 HH 150 13 L NC = 11 49 VL NC = 25 120 M �8068 VH 31 VL 8.0 0.0 41.6 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Exchangeable Sodium Percentage % K % Mg 1 Ca % Na % H % NO3N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 6A 0.3 2.0 97.5 0.4 0.0 17 M NC=35 10.1 VH NC=252.5 7 VL NC=44 17 VL 0.8 L NC=40.0 0.5 M 0.060 6B 0.2 2.4 97.0 0.4 0.0 22 H NC=46 14.0 VH NC=350.0 7 VL NC=44 19 VL 2.1 M NC=105.0 0.7 H 0.210 7 0.1 2.2 97.4 0.3 0.0 18 M NC=37 13.5 VH NC=337.5 5 VL NC=31 11 VL 1.4 M NC=70.0 0.7 H 0.110 8 0.1 2.4 97.1 0.3 0.0 19 M NC=40 13.2 VH NC=330.0 7 VL NC=44 12 VL 1.6 M NC=80.0 0.7 H 0.050 9 0.3 2.4 97.0 0.3 0.0 23 H NC=48 15.4 VH NC=385.0 7 VL NC 12 VL 1.6 M NC=80.0 0.8 H 0.150 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are relainnd a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Tennessee, Inc. by-. Salts ms/cm x 640 = ppm. Oscar Ruiz Page 4 of 4 Report Number: 19-193-0701 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Date Received: 07/12/2019 Date Of Report: 07/24/2019 Waypoint,0 ANALYTICAL "Every acre... Every year. ". Farm: US-1 SOIL FERTILITY RECOMMENDATIONS 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop field Goal Lime N P205 KZO Mg S Zn Mn Fe Cu B Field ID bulacre Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 6A Soybeans 50 0.0 0 83 150 10 11 0 6 1.0 0.5 6B Soybeans 50 0.0 0 86 150 0 0 0 6 0 0 7 Soybeans 50 0.0 0 78 150 0 11 0 6 0 0 8 Soybeans 50 0.0 0 89 150 0 10 0 6 0 0 9 Soybeans 50 0.0 0 83 150 0 0 0 6 0 0 'omments: 30970 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30971 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30972 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30973 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 30975 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. Sample(s) : 6B,7,8,9 Crop: Soybeans For soybeans on soils with a pH of 6.2 or less, apply limestone as recommended and plant seed treated with molybdenum. Apply 1-2 oz of sodium molybdate (0.4-0.8 oz of elemental molybdenum) per acre as a seed treatment. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �• Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Oscar Ruiz Page 1 of 4 Report Number: 19-305-0910 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 ■ Waypoint ANALYTICAL "Every acre... Every year. "rM SOIL ANALYSIS REPORT Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/02/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Cordova Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NC = North Carolina Fertility Index Value OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number % Rate Soil Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 1 64132 2.5 L 94 10 L NC=8 15 VL NC=B 115 M 9424 VH 69 VL 8.2 0.0 98.4 I MIN 2 64133 2.3 L 90 4 L NC=3 17 VL NC=9 127 M 15873 VH 69 VL 8.3 0.0 130.8 MIN 3A 64134 3.1 M 106 2 VL NC = 2 16 VL NC = 8 126 M 11085 VH 41 VL 8.4 0.0 106.7 MIN 3B 64135 2.4 L 92 6 L NC = 5 12 VL NC = 6 127 M 6050 VH 80 VL 8.2 0.0 131.7 MIN 4 64136 4.1 MH 126 5 L NC = 4 17 VL NC = 9 129 M 17385 VH 73 VL 8.3 0.0 138.4 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts K Mg % Ca % Na % H % NO3 N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 1 0.0 1.0 98.7 0.3 0.0 17 M NC = 35 10.9 VH NC = 272.5 5 VL NC = 31 25 L 2.1 M NC = 105.0 0.8 H 2 0.0 0.8 98.9 0.2 0.0 23 H NC=48 13.6 VH NC=340.0 5 VL NC=31 20 VL 1.4 M NC=70.0 0.8 H 3A 0.0 1.0 98.8 0.2 0.0 16 M NC=33 10.8 VH NC=270.0 5 VL NC=31 17 VL 0.9 M NC=45.0 0.6 H 3B 0.0 0.8 98.9 0.3 0.0 28 H NC=58 12.6 VH NC=315.0 5 VL NC=31 18 VL 1.0 M NC=50.0 0.9 H 4 0.0 0.8 98.9 0.2 0.0 31 H NC=64 15.6 VH NC=390.0 6 VL NC=38 18 VL 1.2 M NC=60.0 1.0 H Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. -Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a �. (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by:✓'� Salts ms/cm x 640 = ppm. Analysis prepared by Waypoint Analytical Tennessee Inc Oscar Ruiz Page 2 of 4 Report Number: 19-305-0910 a ►�° Account Number: 22972 Waypol nt w _ 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 Send To: Branch Residuals and Soils LLC ANALYTICAL www.waypointanalytical.com Mr. Bob Branch "Every acre... Every year. ".M Grower: Von Drehle Cordova 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Comments: 64132 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 64133 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 64134 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 64135 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. 64136 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. If you have questions, please call the lab. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �. Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Oscar Ruiz Page 3 of 4 Report Number: 19-305-0910 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Waypoi t.0 ANALYTICAL "Every acre... Every year. "rM SOIL ANALYSIS REPORT Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/02/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 a Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Cordova Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 5 64137 3.1 M 106 4 L NC = 3 23 VL NC = 12 118 M 8416 VH 87 VL 8.2 0.0 93.5 I MIN 6A 64138 2.0 L 84 4 L NC = 3 12 VL NC = 6 97 M 9982 VH 67 VL 8.0 0.0 51.0 MIN 6B 64139 1.8 VLH 80 3 VL INC = 2 13 VL NC = 7 93 M 8301 VH 34 VL 8.3 0.0 42.5 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts K % Mg "fie Ca "fie Na % H % NOs N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 5 0.1 1.1 98.5 0.4 0.0 38 H NC=79 10.4 VH NC=260.0 5 VL NC=31 18 VL 0.8 L NC=40.0 1.3 H 6A 0.1 1.6 97.9 0.6 0.0 25 H NC=52 6.7 H NC=167.5 4 VL NC=25 25 L 0.6 L NC=30.0 0.7 H 6B 0.1 1.8 97.7 0.3 0.0 15 M NC=31 6.3 H NC=157.5 3 VL NC=19 21 VL 0.5 L NC=25.0 0.6 H Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble prepared Analysis re b : Wa by. Salts ms/cm x 640 = ppm. Y P P Y ypoinlMalytical Tennessee Inc Oscar Ruiz Page 4 of 4 Report Number: 19-305-0910 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Comments: Waypoi t(D ANALYTICAL "Every acre... Every year",. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Cordova 64137 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. have questions, please call the lab. 64138 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. have questions, please call the lab. 64139 Due to the magnesium and/or calcium carbonate levels in the soil, the calculated CEC and cation saturation percentages may not be accurately estimated. have questions, please call the lab. 'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977 If you If you If you Page 1 of 2 Report Number: 19-305-9155 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Waypoint(D ANALYTICAL "Every acre... Every year. "rM SOIL ANALYSIS REPORT Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/15/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Cordova Analytical Method(s): NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 1 88700 2 88701 3A 88702 3B 88703 4 88704 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Cation Exchange Capacity meg1100g Exchangeable Sodium Percentage % K % Mg % Ca % Na % H % NO3 N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 1 5.40 2.82 2 5.10 3.18 3A 5.10 2.58 3B 5.40 4.24 4 7.90 3.01 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a 11-6501.-, soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, SolubleC.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysts prepared by: waypoint Analytical Tennessee, Inc. Jimmy R. Ferguson Page 2 of 2 Report Number: 19-305-9155 Account Number: 22972 Send To: Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Waypoint ANALYTICAL "Every acre... Every year. ". SOIL ANALYSIS REPORT Date Received: 11/01/2019 Date Of Analysis: 11/04/2019 Date Of Report: 11/15/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Grower: Von Drehle Cordova Analytical Method(s): NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 % Rate Soil Class Ibs/A ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 5 88705 6A 88706 6B 88707 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Cation Exchange Capacity meq/100g Exchangeable Sodium Percentage % K % Mg % Ca % Na % H % NO3N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 5 5.90 4.72 6A 5.70 2.14 6B 5.90 2.39 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium) H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis Salts ms/cm x 640 = ppm. alysis prepared by Waypoinl Analytical Tennessee Inca Jimmy R. Ferguson 2019 APPLICATION SUMMARY TABLE VON DREHLE CORPORATION LAND APPLICATION PROGRAM PERMIT NO. WQ0005135 2019 APPLICATION SUMMARY ...... ............ e ... ... ..... ........ ...... .............. .......................................... .......... ................ Vi'e ................... ....... .................. ........... ............. .. ........ ............... .....ad . ... .... .. ...... ......... .................... .................. ............................... 'Tons... ... ...... ......... ............. ... ............. ...... ... .. ....... . ........ Dry 'Tons .. ... ......... ............ ......... ....... .......... . ................ ........................... ................ ..... ......... ...... ......................... .............. ........... -op.- .. ....... ............... .... ........ ...... 3 1 23 Jul-19 1449.28 34.4 21.68 498.55 Rye 6.53 2 9.1 Jul-19 507.95 34.4 19.20 174.73 Rye 5.79 3A 18.9 Jul- 19 1108 34.4 20.17 381.15 Rye 6.08 3 B 37.2 Aug-19 2260.35 34.4 20.90 777.56 Rye 6.30 4 13.2 Aug-19 761.6 34.4 19.85 261.99 Rye 5.98 5 11.1 Aug- 19 729.4 34.4 22.60 250.91 Rye 6.81 6A 24.6 Sep-19 1324.29 36.6 19.70 484.69 Rye 6.10 6B 37.5 Aug-19 1738.66 34.4 15.95 598.10 Rye 5.47 Sep-19 221.3 36.6 2.16 81.00 Rye 4 1 19.1 Mar-19 1178.33 40.8 25.17 480.76 Milleft. 10.46 2 37.1 Mar-19 2227.31 40.8 24.49 908.74 Millett 10.18 3 22.4 Mar-19 1358.27 40.8 24.74 554.17 Millett 10.28 4 50.8 Feb-19 2134.51 32.6 13.70 695.85 Millett 13.77 Mar-19 1046.06 40.8 8.40 426.79 Millett. 5 11.1 Mar-19 686.76 40.8 25.24 280.20 Millett 10.49 6A 18.9 Mar-19 1104.69 40.8 23.85 450.71 Millett 9.91 6B 19.3 Mar-19 1132.03 40.8 23.93 461.87 Millett 9.94 7 19.2 Feb- 19 1160.31 32.6 19.70 378.26 Millett 14.78 8 28.9 Jan-19 1713.55 32.6 19.33 558.62 Millett. 14.50 9 28.6 Jan-19 1606.2 32.6 18.31 523.62 Millett 1 13.73 Total Acreage 430 von Drehle [is Wet Tons Dry Tons Permit Limit 25,448.8]5 9,228.29 12,500 Branch Residuals Soils, LLC Confidential 1/31/2020 Page 1 2019 APPLICATION CONDITION SUMMARIES von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan- Feb 2019 von Drehle Paper Farmer: Wayne Belger Acres: 50.8 Site/Tract: 4 Application Method: Incorporated Field: 4 Percent Solids: 32.6 Residual Report No.: vd 2019-1 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 2/13/19 4 289.25 Warm,Cloud Dry 0.33 2/14/19 4 142.38 Cool,Clear Moist 0.00 2/15/19 4 168.83 Cool,Clear Dry 0.00 2/18/19 4 193.10 Cool,Cloudy Dry 0.13 2/19/19 4 239.67 Cool,Clear Dry 0.00 2/20/19 4 22.32 Cool,Cloudy Dry 0.21 2/21/19 4 194.52 Cool,Cloudy Moist 0.05 2/25/19 4 288.98 Warm,Clear Dry 0.00 2/26/19 4 298.82 Cool,Clear Dry 0.00 2/27/19 4 296.64 Cool,Clear Dry 0.00 Total Wet Tons 2,134.51 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan- Feb 2019 von Drehle Paper Farmer: Wayne Belger Acres: 19.2 Site/Tract: 4 Application Method: Incorporated Field: 7 Percent Solids: 32.6 Residual Report No.: vd 2019-1 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 2/4/19 7 71.10 Cool,Cloudy Dry 0.01 2/5/19 7 216.15 Warm,Clear Dry 0.00 2/6/19 7 244.77 Warm,Clear Dry 0.00 2/7/19 7 101.19 Warm,Clear Dry 0.00 2/8/19 7 120.52 Warm,Clear Dry 0.00 2/11/19 7 166.00 Cool,Cloudy Dry 0.01 2/12/19 7 240.58 Cool,Cloudy Dry 0.07 Total Wet Tons 1,160.31 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan- Feb 2019 von Drehle Paper Farmer: Wayne Belger Acres: 28.9 Site/Tract: 4 Application Method: Incorporated Field: 8 Percent Solids: 32.6 Residual Report No.: vd 2019-1 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 1/22/19 8 209.55 Cold,Clear Dry 0.00 1/28/19 8 411.10 Cool,Clear Dry 0.00 1/29/19 8 211.54 Cool,Clear Dry 0.00 1/30/19 8 217.87 Cool,Cloudy Dry 0.20 1/31/19 8 260.82 Cool,Clear Dry 0.00 2/1/19 8 118.27 Cool,Clear Dry 0.00 2/4/19 8 284.40 Cool,Cloudy Dry 0.01 Total Wet Tons 1,713.95 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan- Feb 2019 von Drehle Paper Farmer: Wayne Belger Acres: 28.6 Site/Tract: 4 Application Method: Incorporated Field: 9 Percent Solids: 32.6 Residual Report No.: vd 2019-1 MB Crop: Millet Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 1/14/19 9 335.93 Cool,Cloudy Moist 0.14 1/15/19 9 330.24 Cool,Clear Dry 0.00 1/16/19 9 158.57 Cool,Clear Dry 0.00 1/17/19 9 189.53 Cool,Clear Dry 0.00 1/18/19 9 143.74 Cool,Cloudy Dry 0.17 1/21/19 9 239.23 Cool,Clear Moist 0.00 1/22/19 9 94.00 Cold,Clear Dry 0.00 1/23/19 9 114.96 Cool,Clear Dry 0.00 Total Wet Tons 1,606.20 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 March -April 2019 von Drehle Paper Farmer: Wayne Belger Acres: 19.1 Site/Tract: 4 Application Method: Incorporated Field: 1 Percent Solids: 40.8 Residual Report No.: vd 2019-2 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/29/19 1 140.28 Warm,Clear Dry 0.00 4/1/19 1 431.16 Warm,Clear Dry 0.00 4/11/19 1 255.90 Warm,Clear Dry 0.00 4/15/19 1 350.99 Warm,Cloudy Dry 0.07 4/16/19 1 0.00 Warm,Clear Dry 0.00 4/17/19 1 0.00 Warm,Clear Dry 0.00 Total Wet Tons 1,178.33 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 March -April 2019 von Drehle Paper Farmer: Wayne Belger Acres: 37.1 Site/Tract: 4 Application Method: Incorporated Field: 2 Percent Solids: 40.8 Residual Report No.: vd 2019-2 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/11/19 2 427.04 Warm,Clear Dry 0.00 3/12/19 2 204.54 Warm,Clear Dry 0.00 4/3/19 2 352.28 Cool,Cloudy Dry 0.14 4/4/19 2 329.93 Warm,Cloudy Moist 0.01 4/5/19 2 142.02 Warm,Cloudy Dry 0.10 4/8/19 2 294.82 Warm,Clear Dry 0.00 4/9/19 2 141.56 Wann,Cloudy Dry 0.43 4/10/19 2 237.42 Warm,Cloudy Moist 0.10 4/11/19 2 97.70 Warm,Clear Dry 0.00 Total Wet Tons 2,227.31 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 March -April 2019 von Drehle Paper Farmer: Wayne Belger Acres: 22.4 Site/Tract: 4 Application Method: Incorporated Field: 3 Percent Solids: 40.8 Residual Report No.: vd 2019-2 MB Crop: Millet Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/5/19 3 333.59 Cool,Clear Moist 0.00 3/6/19 3 367.40 Cool,Clear Dry 0.00 3/7/19 3 411.36 Cool,Clear Dry 0.00 3/8/19 3 145.44 Cool,Clear Dry 0.00 3/11/19 3 100.48 Warm,Clear Dry 0.00 Total Wet Tons 1,358.27 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 March -April 2019 von Drehle Paper Farmer: Wayne Belger Acres: 50.8 Site/Tract: 4 Application Method: Incorporated Field: 4 Percent Solids: 40.8 Residual Report No.: vd 2019-2 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/1/19 4 277.69 Warm,Cloudy Dry 0.26 3/13/19 4 175.75 Cool,Clear Dry 0.00 3/14/19 4 135.34 Cool,Clear Dry 0.00 3/15/19 4 117.97 Warm,Clear Dry 0.00 3/18/19 4 267.49 Cool,Clear Dry 0.00 3/19/19 4 71.82 Cool,Clear Dry 0.00 Total Wet Tons 1 1,046.06 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 March -April 2019 von Drehle Paper Farmer: Wayne Belger Acres: 11.1 Site/Tract: 4 Application Method: Incorporated Field: 5 Percent Solids: 40.8 Residual Report No.: vd 2019-2 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/21/19 5 220.46 Cool,Cloudy Dry 0.32 3/22/19 5 102.35 Cool,Clear Moist 0.00 3/25/19 5 246.95 Warm,Clear Dry 0.00 3/26/19 5 0.00 Wann,Cloudy Dry 0.40 4/16/19 5 117.00 Warm,Clear Dry 0.00 Total Wet Tons 686.76 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 March -April 2019 von Drehle Paper Farmer: Wayne Belger Acres: 18.9 Site/Tract: 4 Application Method: Incorporated Field: 6A Percent Solids: 40.8 Residual Report No.: vd 2019-2 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/19/19 6A 167.58 Cool,Clear Dry 0.00 3/20/19 6A 288.18 Cool,Clear Dry 0.00 3/21/19 6A 0.00 Cool,Cloudy Dry 0.32 4/15/19 6A 168.00 Warm,Cloudy Dry 0.07 4/16/19 6A 287.91 Warm,Clear Dry 0.00 4/17/19 6A 193.02 Warm,Clear Dry 0.00 Total Wet Tons 1,104.69 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 March -April 2019 von Drehle Paper Farmer: Wayne Belger Acres: 19.3 Site/Tract: 4 Application Method: Incorporated Field: 6B Percent Solids: 40.8 Residual Report No.: vd 2019-2 MB Crop: Millet Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/25/19 6B 235.47 Warm,Clear Dry 0.00 3/26/19 6B 326.47 Warm,Cloudy Dry 0.40 3/27/19 6B 236.51 Cool,Cloudy Moist 0.10 3/28/19 6B 286.82 Cool,Clear Dry 0.00 3/29/19 6B 46.76 Warm,Clear Dry 0.00 3/30/19 6B 0.00 Warm,Clear Dry 0.00 4/1/19 6B 0.00 Warm,Clear Dry 0.00 4/8/19 6B 0.00 Warm,Clear Dry 0.00 Total Wet Tons 1,132.03 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 July- Aug 2019 von Drehle Paper Farmer: Wayne Belger Acres: 23 Site/Tract: 3 Application Method: Incorporated Field: 1 Percent Solids: 34.4 Residual Report No.: vd 2019-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/15/19 1 209.87 Hot,Clear Dry 0.00 7/16/19 1 391.38 Hot,Clear Dry 0.00 7/17/19 1 202.78 Hot,Clear Dry 0.00 7/18/19 1 115.04 Hot,Cloudy Dry 0.48 7/19/19 1 161.78 Hot,Clear Moist 0.00 7/22/19 1 307.41 Hot,Clear Moist 0.00 7/23/19 1 61.02 Hot,Clear Dry 0.00 Total Wet Tons 1,449.28 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 July- Aug 2019 von Drehle Paper Farmer: Wayne Belger Acres: 9.1 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 34.4 Residual Report No.: vd 2019-4 MB Crop: Rye Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/23/19 2 223.74 Hot,Clear Dry 0.00 7/24/19 2 284.21 Hot,Cloudy Dry 0.01 Total Wet Tons 1 507.95 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 July- Aug 2019 von Drehle Paper Farmer: Wayne Belger Acres: 18.9 Site/Tract: 3 Application Method: Incorporated Field: 3A Percent Solids: 34.4 Residual Report No.: vd 2019-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/25/19 3A 225.23 Warm,Clear Moist 0.00 7/26/19 3A 174.69 Warm,Clear Dry 0.00 7/29/19 3A 314.87 Hot,Clear Dry 0.00 7/30/19 3A 346.79 Hot,Clear Dry 0.00 8/1/19 3A 46.42 Hot,Clear Dry 0.00 Total Wet Tons 1,108.00 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 July- Aug 2019 von Drehle Paper Farmer: Wayne Belger Acres: 37.2 Site/Tract: 3 Application Method: Incorporated Field: 3B Percent Solids: 34.4 Residual Report No.: vd 2019-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/1/19 3B 324.94 Hot,Clear Dry 0.00 8/2/19 3B 276.87 Hot,Cloudy Dry 0.16 8/5/19 3B 302.82 Hot,Cloudy Dry 0.11 8/6/19 3B 200.14 Warm,Cloudy Moist 0.45 8/7/19 3B 291.18 Hot,Cloudy Moist 0.10 8/8/19 3B 234.82 Hot,Clear Dry 0.00 8/9/19 3B 164.81 Hot,Clear Dry 0.00 8/12/19 3B 301.01 Hot,Clear Dry 0.00 8/13/19 3B 163.76 Hot,Clear Dry 0.00 Total Wet Tons 2,260.35 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 July- Aug 2019 von Drehle Paper Farmer: Wayne Belger Acres: 13.2 Site/Tract: 3 Application Method: Incorporated Field: 4 Percent Solids: 34.4 Residual Report No.: vd 2019-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/13/19 4 81.88 Hot,Clear Dry 0.00 8/14/19 4 239.10 Hot,Cloudy Dry 0.29 8/15/19 4 276.12 Hot,Cloudy Moist 0.06 8/16/19 4 164.50 Hot,Clear Moist 0.00 Total Wet Tons 761.60 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 July- Aug 2019 von Drehle Paper Farmer: Wayne Belger Acres: 11.1 Site/Tract: 3 Application Method: Incorporated Field: 5 Percent Solids: 34.4 Residual Report No.: vd 2019-4 MB Crop: Rye Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/16/19 5 47.00 Hot,Clear Moist 0.00 8/19/19 5 306.84 Hot,Cloudy Dry 0.10 8/20/19 5 281.73 Hot,Clear Dry 0.00 8/21/19 5 93.83 Hot,Cloudy Dry 0.08 Total Wet Tons 729.40 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 July- Aug 2019 von Drehle Paper Farmer: Wayne Belger Acres: 37.5 Site/Tract: 3 Application Method: Incorporated Field: 6B Percent Solids: 34.4 Residual Report No.: vd 2019-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/21/19 6B 187.60 Hot,Cloudy Dry 0.08 8/22/19 6B 189.34 Hot,Clear Dry 0.00 8/23/19 6B 162.65 Hot,Cloudy Dry 0.16 8/26/19 6B 277.87 Warm,Clear Dry 0.00 8/27/19 6B 210.02 Warm,Clear Dry 0.00 8/28/19 6B 264.99 Warm,Clear Dry 0.00 8/29/19 6B 226.91 Hot,Clear Dry 0.00 8/30/19 6B 219.28 Warm,Clear Dry 0.00 Total Wet Tons 1,738.66 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Sept -Oct 2019 von Drehle Paper Farmer: Wayne Belger Acres: 24.6 Site/Tract: 3 Application Method: Incorporated Field: 6A Percent Solids: 36.6 Residual Report No.: vd 2019-5 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 9/2/19 6A 110.65 Warm,Clear Dry 0.00 9/3/19 6A 263.33 Hot,Clear Dry 0.00 9/4/19 6A 227.47 Hot,Clear Dry 0.00 9/5/19 6A 221.81 Hot,Cloudy Dry 0.24 9/6/19 6A 250.26 Warm,Cloudy Moist 0.00 9/9/19 6A 250.77 Hot,Clear Dry 0.00 Total Wet Tons 1,324.29 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Sept -Oct 2019 von Drehle Paper Farmer: Wayne Belger Acres: 37.5 Site/Tract: 3 Application Method: Incorporated Field: 6B Percent Solids: 36.6 Residual Report No.: vd 2019-5 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 9/2/19 6B 221.30 Warm,Clear Dry 0.00 Total Wet Tons 221.30