WQ0011413_Residual Annual Report 2019_20200225

2/26/2020 Monitor I Laserfiche Forms
Initial Review
I I ki I 1110 F-11 N NATAIATA
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application
what is the submittal
type? *
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2019
Date Paper Copy Received: * 2/25/2020
Project Number* WQ0011413
Email Notifications
Does this need review by the hydrogeologist? *
Yes No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]
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Submitted Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff
Name* Nainesh Patel
Email Address*
[e-mail]
Project Information
Submittal Type* New Permit Application
Renewal
Annual Report
Other
Permit Type* Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
Yes No N/A
Permit Number* W00011413
Applicant\Permittee* NC Department of Public Safety
Facility Name* Odom Correctional Institution
electronic submittal, confirmation of receipt, and other issues.
Phone Number*
919-324-1283
Modification (Major or Minor)
Additional Information
Residual Annual Report
High -Rate Infiltration
Reclaimed Water
Residuals
Other
Please provide comments/notes on your current submittal below.
A hard copy as required by the permit has been submitted to the DEQ.
Please attach all information required or requested for this submittal to be review here.
Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2019 Residual Biosolids Land App Rpt.pdf 3.58MB
Upload only 1 PDF document. Multiple documents must be combined into one PDF file.
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For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contact the reviewer or Tessa Monday. If a paper application is required,
be advised, applications accepted for pre -review until both the paper and electronic copies have been
received. The paper copy shall include the following:
❑ Application Form
❑ All relevant attachments (calcs, soils report, specs, etc.)
❑ ene full-size engineering plan set
❑ One 11x17° engineering plan set
❑ One extra set of specifications
❑ Fee (if required)
Mal I i ng address:
I-------------------------------------------
--By- LJ.S. Postal Service
Division of Water Resources
-------------------------------------------
Non_Discharge Branch
1617 Mail Service Center
-------------------------------------------
RaleiRh, INC 27699-1617
Division of Water Resources
------------------------------------------
Non-Discharue Branch
Att: Nathaniel Thomburg, 9"Floor, Office #942W
512 N.5a1isbury51.
Ra le ijzh. INC 276D4-1170
For questions or problems contact Tessa Monday at [e-mail] or 919.707.3660.
By checking this box I acknowledge that I understand the application will not be
accepted for pre -review until the paper copy (if required) and fee (if required) have been
received by the Non -Discharge Branch. I also confirm that the uploaded document is a
single PDF with all parts of the application in correct order (as specified by the
application).
Signature
Submission Date 2/25/2020
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�- NCDEQ
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699
Subject: 2019 Annual Biosolids Land Application Certification
North Carolina Department of Public Safety — Odom Correctional Institution
Permit 4WQ0011413
Northampton County, N.C.
Dear Madam or Sir,
Enclosed for your review is the 2019 Annual Report for the monitoring and reporting of the Biosolids
Land Application Program for the NCDPS Odom Correctional Institution as required by 40 CFR-503
Regulations.
We were compliant this past year with the Land Application Program at Odom C.I. I notified Rick
Trone, Environmental Specialist II, with NCDEQ prior to each application event to meet our 24-hour
notice requirements and for his professional input should he have desired to share it. All applications
occurred on clear days with zero rainfall in the past 24 hours.
On Friday, December 61h, 2019, the site was visited by Mr. Gary Kreiser, NCDEQ Soil Analyst, in
regards to checking the soil conditions facility wide, with particular focus upon tract B. This was
important for renewing our land application permit. He also wanted to check tract A since it was in the
flood plain and a recent DOT project had placed a public access road through the tract. He found that
tract A should remain unused except during the dry season of the year and that we were underutilizing
Zone 3 of tract B. The soil in all areas was acceptable. Based upon his findings, I expect a renewal with
some seasonal limitations upon tract A and I or whoever takes over this next year should redirect
Odom's applications to include more upon Zone 3 since its soil was the best of all the zones in tract B.
Should you have any further question or comments, please contact me.
Sincerely,
Geoffrey S. Pittard
Odom C.I. Land App ORC LA#1003310
Maintenance / Construction Technician IV
Caledonia Correctional Institute, NCDPS
2787 Caledonia Dr.
Tillery, NC 27887
P: [phone] Xt. 731 or Xt. 740
Fax: [phone]

NCDPS- Odom Correctional Institution
Northampton County, NC
Residuals Land Application Program
2019 Annual Report
Table of Contents
1. ACF — Annual Land Application Certification Form, Annual Operations Summary, Facility and
Operator -in -Responsible Charge (ORC) Contact Information
2. RSSF —Annual Residual Sampling Form, Residual Analysis
3. MFLSF — Annual Metals Loading Summary Form (by Zone)
4. FSF —Annual Land Application Field Summary Form (by Zone)
5. PVRT —Annual Pathogen and Vector Attraction Reduction Form (503 Rule), SOURS Test
6. Soil Analysis
7. TCLP Analysis
8. Copies of Lab Results

pCF

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0011413 County:
Facility Name (as shown on permit):
Land Application Operator:
Northampton
Year: 2019
North Carolina Department of Public Safety — Odom Correctional Ins.
Geoffrey S Pittard Phone: [phone]
Land�lication of residuals as allowed by the permit occurred during the past calendar year?
Yes No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Sum
Total number of a22lication fields in thepermit: 1 3
Total number of fields utilized for land application during the year: 1 1
Total amount of dry tons applied during the year for all application sites: 2.61
Total number of acres utilizes for land application during the year: 1 -13.8
Part B - Annual Com iance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources., Yes No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soi 1 pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources. -
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
JEFFREY T. QRtA►.►T ojZ
of �tv��rNG
Permittee Name and Title (type or print) Signatu ermittee Date
Sigr►a(of Preparer*
Date
of Land Applier
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

NCDPS- Odom Correctional Institution
Residuals Land Application Program
2019 Annual Report
FacFac ility:
Odom Correctional Institution
485 Odom Prison Rd.
Jackson, NC 27845
[phone]
Permit Number:
WQ0011413
Responsible Official:
Nainesh Patel
Civil/Environmental Engineering Manager
NC Department of Public Safety
Central Engineering
2020 Yonkers Road
4216 Mail Service Center
Raleigh, NC 27699-4216
Phone: [phone]
Fax: [phone]
E-Mail: [e-mail]
ORC:
Geoffrey S Pittard
Maintenance / Construction Technician IV
Caledonia Correctional Institute, NCDPS
2787 Caledonia Dr.
Tillery, NC 27887
P: [phone] Xt. 731 or Xt. 740
Fax: [phone]
Geotkeu [e-mail]
ncdps.gov
LA License #1003310
Land Application Report Prepared By:
Geoffrey S Pittard

North Carolina Department of Public Safety
Odom Correctional Institution
Residual Solids Land Application (503)
Northampton County
Permit #WQ0011413
2019
Total Gallons of Biosolids Applied
Month Loads Gallons
January
0
0 -
February
0
0
March
0
0
April
0
0
May
0
0
June
13
26000
July
0
0
August
0
0
September
4
8000
October
0
0 _
November
0
0
December
0
0
Total: 34000 Gal
Solids Percent: 2.09 Percent
Conversion: 0.00417 DT/Gal
Total solids: 2.96 Dry Tons

North Carolina Department of Public Safety
Odom Correctional Institution
Residual Solids Land Application
(503)
Northampton County
Permit #WQ0011413
Date Tract Zone Lot
Loads
06/17/19 B 1 1
3
06/27/19 B 1 2
5
06/27/19 B 1 3
3
09/04/19 B 1 1
2
09/04/19 B 1 2
1
09/04/19 B 1 3
1
Total Zone 1 Loads:
15 -
Total Zone 2 Loads: 0
Total Zone 3 Loads: 0
Gallons/Load: 2000
DT/load: 0.1742 _
Total Loads: 15

��5r

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0411413 Laboratory:
Facility Name: Odom Correctional Institute
Residual Source WQ # or
NPDES #:
WWTP Name:
12ucirina1 Analveie data
NCO027642
1) Statesville Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
}a
Sample or Com osite Date
5/07/19
Percent Solids (%)
NA
2.09
Arsenic
75
4.11
Cadmium
85
2.73
Copper
4,300
378
Chromium
NA
19.1
Lead
Mercury
840
57
16.94
0.066
Molybdenum
75
7.99
Nickel
420
14.6
Selenium
100
<.24
Zinc
7,500
1377
Total Phosphorus
NA
16270
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
a Rnr e„rfacP disnnsal 6nilitiec
NA 55786
NA 5626.8
NA 248.8
the ceiling concentration limits listed
in this form are not applicable.
Reference the individual permit formetals limits.
"I certify, under penalty of law, that this documegt was prepared ,under my direction or supervision in accordance with a system, designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Sigjflta"re of Preparer *
z
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0011413 Laboratory: 1) Statesville Analytical
Facility Name: Odom Correctional Institution 2)
Residual Source
NPDES # or WQ#:
WWTP Name:
�noirl■■nl Analvvie ill*S•
NCO027642
3)
4)
5)
Parameter
-
•
Aluminum
; 1
_�---------_
--_--------
i i'•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure�that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signaturero"reparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
2� a
Date

1"1 �L� F

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
,_Facility Name: Odom Correctional Institution
Total Dry Tons Applied (Annual):-. 2.61
ermit #: WQ0011413
Cation Exchange Capacity (non 503 only):
Operator: Geoffrey S Pittard Owner:
NC DPS Predominant Soil Series:
Acres Used: 13.8 Acres Permitted:
41.4 Site #: Tract - B Field #: Zone 1
Residual Analysis Data {Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #
Sample or
Com-
posite
Date 6/17/19 6/27/19 6/27/19 9/4/19 9/4/19
9/4/19
% Solids 2.09 2.09 2.09 2.09 1 2.09
2.09
Arsenic 4.11 4.11 4.11 4.11 4.11
4.11
Cadmium 2.73 2.73 2.73 2.73 2.73
2.73 -
Copper 378 378 378 378 378
378
Chromium 19.1 19.1 19.1 19.1 19.1
1.9.1
Lead 16.94 16.94 16.94 16.94 16.94
16.94
Mercury 0.066 0.066 0.066 0.066 0.066
0.066
Molyb-
7.99 7.99 7.99 7.99 7.99
denum
7.99 -
Nickel 14.6 14.6 14.6 14.6 14.6
14.6
Selenium 0 0 0 0 0
0
Zinc 1377 1377 1377 1377 1377
1377
Total
Phos- 16270 16270 16270 16270 16270
16270
horus I
I I I -
Annual Heavv Metal Field Loa din s Calculated in lbs/acre :
Total
DT/Ac./
c
App.
�.
Event 0.52 0.87 0.52 0.35 0.17
0.17
y
Arsenic 0.004 0.007 0.004 0.003 1 0.001
0.001 0.000 1 0.000 0.000 1 0.000 1 0.000 0.000
0.021
Cadmium 0.003 0.005 0.003 0.002 0.001
0.001 0.000 0.000 0.000 0.000 0.000 0.000
0.014
Copper 0.395 0.658 0.395 0.263 0.132
0.132 0.000 0.000 0.000 0.000 0.000 0.000
1.975
Chromium 0.020 0.033 0.020 0.013 0.007
0.007 0.000 0.000 0.000 0.000 0.000 0.000
0.100
Lead 0.018 0.030 0.018 0.012 1 0.006
0.006 0.000 0.000 0.000 0.000 0.000 0.000
0.089
Mercury 0.000 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000 0.000 0.000
0.000
Molyb- 0.008 0.014 0.008 0.006 0.003
denum
0.003 0.000 0.000 0.000 0.000 0.000 0.000
0.042
Nickel 0.015 0.025 0.015 0.010 1 0.005
0.005 0.000 0.000 0.000 0.000 -0.000 0.000 1
0.076
Selenium 0.000 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000 1 0.000 0.000
0.000
Zinc 1.439 2.399 1.439 0.959 0.480
0.480 0.000 0.000 0.000 0.000 0.000 0.000
7.196
Total
Phos- 17.005 28.342 17.005 11.337 5.668
5.668 0.000 0.000 0.000 0.000 0.000 0.000
85.027
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
m aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sigma r Land Applier
ate
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD 6%6G SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
/ 'acility Name:
Odom Correctional Institution Total Dry Tons Applied (Annual): 0.00
?ermit #:
WQ0011413 Cation Exchange Capacity (non 503 only):
Operator:
Geoffrey S Pittard Owner: NC DPS Predominant Soil Series:
Acres Used:
13.8 Acres Permitted: 41.4 Site #: Tract - B Field #: Zone 2
Residual Analysis Data Heave Metals and Total Phosphorus use m % Solids use Raw Percent #
Sample or
,
Com-
posite
Date
% Solids
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molyb-
denum
Nickel
Selenium
Zinc
Total
Phos-
phorus
♦ _ _7 77__
r&uuuai
Heavy
Total
DT/Ac./
App.
Event
Arsenic
0.000
Cadmium
0.000
Copper
0.000
Chromium
0.000
Lead
0.000
Mercury
0.000
Molyb-
0.000
denum
Nickel
0.000
Selenium
0.000
Zinc
0.000
1vietai ricid Loadings tualculatea in lbs/acre):
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos- 0.000 0.000
y
0
w
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
-ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
_ am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations". -
Sao
Signatu a of Land Applier Date
Page 1

ANNUAL METALS FIELAAgG SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
to'- ,icility Name:
t'ermit #:
Operator:
Acres Used:
Odom Correctional Institution Total Dry Tons Applied (Annual): 0.00
WQ0011413
Geoffrey S Pittard Owner:
13.8 Acres Permitted:
Cation Exchange Capacity (non 503 only):
NC DPS Predominant Soil Series:
41.4 Site #: Tract - B Field #:
Zone 3
Residual Analysis Data [Hear• Metals and Total Phosphorus use m k , % Solids use Raw Percent #y:
Sample or
Com-
posite
Date
% Solids
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molyb-
denum
Nickel
Selenium
Zinc
Total
Phos-
phorus _
Annual Heavv Metal Field Loadinac WnlenlatiM in the/arrel-
Total
DT/Ac./
rt
App •
Event
y
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
1 0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
Copper
0.000
j 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
ChromiLffil
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000,
0.000
0.000
0.000
0.000
0.000
enum d
enum
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Nickel
0.000
0.000
0.000
0.000
t 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
horus
LG, aiy, uuuer hei1auy ui law, tnai ims aocument was prepared under my direction or supervision in accordance
•ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
Y am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signs �r�of Land Applier
Page 1
ate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Odom Correctional WQ Permit #: WQ0011413 Field #: Zone 1 Acres Utilized:
Land Owner: NC DPS Annual Dry Tons Applied: 2.6146 Site #: Tract -- B Acres Permitted:
Operator: Geoffrey S Pittard
Crop 1 Name: Pine
Predominant Soil Series: CrB, Le
Crop 1 Max. PAN: 75 Crop 2 Name:
Cation Exchange Capacity (non 503):
N/A
Crop 2 Max. PAN:
13.8
41.4
N/A
N/A
.,
A
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
A hed per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Cond
D
W
Moist)
Precip.
Past 24
Hrs.
inches
b
�?
�.
a w
* o
�
o
?»
_
*
Z
w -,
*
0
TKN
mg/kg
z
o 6
o0 0
w•
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/17/19
6000
2.09
0.038
NCO027642
Dry
0
S
0.5
0.3
55786
5626.8
248.8
1.372
NA
Pine
6/17/19
10000
2.09
0.063
NCO027642
Dry
0
S
0.5
0.3
55786
5626.8
248.8
2.287
NA
Pine
6/17/19
6000
2.09
0.038
NCO027642
Dry
0
S
0.5
0.3
55786
5626.8
248.8
1.372
NA
Pine
9/4/19
4000
2.09
0.025
NCO027642
Dry
0
S
0.5
0.3
55786
5626.8
1 248.8
0.915
NA
Pine
9/4/19
2000
2.09
0.013
NCO027642
Dry
0
S
0.5
0.3
55786
5626.8
248.8
0.457
NA
Pine
9/4/19
2000
2.09
0.013
NCO027642
Dry
0
S
0.5
0.3
55786
5626.8
248.8
0.457
NA
Pine
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
0
3000o
As
Cd
Cu
Cr
Pb
H r
Mo
Ni
Se
Zn
P
6.862
0.000
Lime Applied
Annuallbs/acre
0.021
0.01800848
0.039
36
0.014
0.01076
0.025
34
1.975
1.84743
3.823
1338
0.100
0.0585
0.158
N/A 1
0.089
0.11132
0.200
267
0.000
0.00333
0.004
15 1
0.042
0.07691
0.119
N/A
0.076
0.10884
0.185
374
0.000
0.02933
0.029
89
7.196
4.84704
12.043
2498
85.027
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
75 N/A
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICAfffig' ELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Odom Correctional
Land Owner: NC DPS
Operator: Geoffrey S Pittard
Crop 1 Name: Pine
WQ Permit #: WQ0011413 Field #: Zone 2 Acres Utilized:
Annual Dry Tons Applied: 0.0000 Site #: Tract - B Acres Permitted:
Predominant Soil Series: CrB, Le Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 75 Crop 2 Name: N/A Crop 2 Max. PAN:
13.8
41.4
N/A
N/A
'~
0 �
°
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
( ry'
Wet
Moist
Precip.
Past 24
Hrs.
inches
Y
K 'a
F �?
n
.� o'
o
w ?'
=
70 =
?� �
rn s✓
N
?:
TKN
mg/kg
Z Y
p E5
o El
no o
g w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
0.000
0.000
NA
Pine
0.000
0.000
NA
Pine
0.000
0.000
NA
Pine
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals
on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
0
o
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
0.000
0.0oo
Lime A lied
Annuallbs/acre
0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000
0.018 0.01219 2.05324 0.0856 0.11922 0.00318 0.074 0.13478 0.029 5.45501
0.018 1 0.012 2.053 0.086 0.119 0.003 0.074 0.135 0.029 5.455
36 1 34 1 1338 N/A 1 267 1 15 1 N/A 1 374 89 2498
75 N/A
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and,imprisonment for knowing violations." I 1 .
ignature of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
lead **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
Page 1

ANNUAL LAND APPLICAT IM' 'ELD SUMMARY FORM �1
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Odom Correctional WQ Permit #: WQ0011413 Field #: Zone 3 Acres Utilized: 13.8
Land Owner: NC DPS Annual Dry Tons Applied: 0.0000 Site #: Tract - B Acres Permitted: 41.4
Operator: Geoffrey S Pittard
Crop 1 Name:
Volume applied
Y (enter one) Solids/
a> �
Q Liquid
Cu. Yds I Gallons
Pine
Volume
% Applied per
Solids I Acre
(Dry Tons/Ac)
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Predominant Soil Series: CrB, Le Cation Exchange Capacity (non 503): N/A
Crop 1 Max. PAN: 75 Crop 2 Name: N/A Crop 2 Max. PAN: N/A
Residual Sources
Soil
Precip.
a
o
Z >
(NPDES #, WQ#,
Cond.
Past 24
b
TICN
o
Fert., Animal
D
Wet,
Hrs.
o"
ory a;
rn `r
*
D ...
Co
Waste, etc
Moist)
inches
o
*
0
mg/kg
mg/kg
Nitrate
and
Nitrite
mg/kg
Residuals Applications totals
on FORM FSF supp ( attach
FORM FSF supp to this form):
TOTALS: 01-01
As
Cd
Cu
I Cr
Pb
Hg
Mo
Ni
I Se
Zn P
Annuallbs/acre
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 0.000
Prior Years Cumulative lbs/ac
0.018
0.01063
1.81576
0.05668
0.10871
0.00274
0.074
0.10877
0.029
4.73575
Current Cumulative Ibs/ac
0.018
1 0.011
1.816
0.057
0.109
0.003
0.074
0.109
0.029
4.736
Permitted C. P. L. R.****
36
1 34
1338
N/A
1 267 1
15
N/A
374
89
2498
Permit PAN Limit lst/2nd Crop
Name of Crop Type
PAN Applied
Receiving Residual
( Ibs/acre)
Application
Crop 1 Crop 2
Crop 1
Crop 2
0.000 NA
Pine
0.000 NA
Pine
0.000 NA
Pine
0.000 NA
Pine
0.000 NA
Pine
0.000 NA
Pine
0.000 NA
Pine
0.000 NA
Pine
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
o.000 o.000
Lime
Applied
Date
lbs/ac
75
N/A
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing; violations."
Rc2o
Signature of Land Applier Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Odom Correctional
WWTP Name: Odom Wastewater Treatment Facility
If a
WQ Permit Number:.,
NPDES Number:
Monitoring Period: 1/1/2019 To 12/31/2019
Pathogen Reduction (- Please indicate level achieved and alternative performed:
Class A: Alternative 2 ❑ Alternative 3 ❑
Alternative 5 ( i Alj __ternative 6 ❑
ble to alternative performed (C g
(3 Heat Drying ❑
Beta
From
40 CFR 503.32
Alternative 1 ❑
Alternative 4 ❑
Gamma
lass A only) indicate "Process to Further Reduce Pathogens":
Heat Treatment ❑ Thermophilic
Pasteurization ❑
WQ0011413
NC0027642
Class B: Alternative I ❑ Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying© Conn postin=, ❑ Aerobic Digestion
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density um ler of Frequency Sample na ytica
Parameter in Sludge Excee- of Analysis s elicesType Tech-
g �7 inimun Geo. Mean Maximo Units Y T e
ninni-
2 x 10 to the MPN 7210 8745 10177 MPN 0 7/OPS G SM9221C
6th power E-2006
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
Coliform I wei ,ht
Vector Attraction Reduction (40 CFR 503.33 - Please indicate option performed:
Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) © Alt. 3 (3-daybench) ❑ Alt. 4 (Spec. OZ uptake) Lk
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) © Alt. 8 (Drying - Unstable) El
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
[I/ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer N, e and Title (type or print)
zz
2
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
�atSignature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Odom Correctional
WQ0011413
04/16/19
24.1
4/16/2019 1100
Pittard
4/16/2019 1110
Pittard
2
22.7
22.2
0.21
7.0
0.97
Yo Dry Solids
9egrees Celsius
Degrees Celsius
Oxygen Uptake Rate: 12.84 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.64 mg Oxygen/hr/g
Average Temperature: 22 degrees Celsius
Temperature Correction Factor: 0.91
Temperature Corrected Specific Oxygen Uptake Rate: 0.58 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

8
7
6
IM
E 5
c
d
rn
x 4
O
V
m
> 3
0
N
D
2
1
0
1
Oxygen Uptake Rate Chart
2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

I- ) I' J I &

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY19-SLO30055
Client: Geoffrey Pittard Advisor:
Predictive Odom Correctional Institution
x 485 Odom Prison Rd
w Soil Report Mehlich-3 Extraction Jackson, NC 27845
51 Links to Helpful Information Sampled County: Northampton
Client ID: 228704 Advisor ID:
Sampled: Received: 04/16/2019 Completed: 04/26/2019 Farm:
Sample ID. 2151 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Pine, M 0.0 100-150 0 20 0 0 0 0 Note: 11
2- 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drr?]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.51 0.87 6.9 65 2.4 5.0 63 30 47 15 35 524 1476 1476 86 0.1 1
Sample ID: 2252 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Pine, M 0.0 100-150 50 0 0 0 0 0 Note: 11
2- 0.0
Test Results [units - WN in g/crr?; CEC and Na in meq/100 cm3; NO3-N in mg/drrt3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N
0.36 0.79 5.1 52 2.4 4.7 12 47 32 15 54 963 866 866 48 0.1 2
Sample ID: 2351 Recommendations: Lime Nutrients (lb/acre) _ More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Pine, M 0.0 100-150 0 30 0 0 0 0 Note: 11
2- 0.0
Test Results [units - WN in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mg/drrh: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-Al Cu-I Na ESP SS-1 NO3-N
0.56 0.90 6.6 66 2.2 5.2 57 24 51 14 34 500 666 666 77 0.1 2
North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
I'Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Y 9 9 9 9 q Y•
- Steve Troxler, Commissioner of Agriculture
TAixto irusr Foal C(a ftwor.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY19-SL030055
Geoffrey Pittard Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime ' Ac
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS%
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca%
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I
ESP
Fertilizer HM%
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg%
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to Mote: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagrgov/agronomi/o42art4.h(M nd information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.noI/agronomi/uvrsthtm
exchangeable acidity
boron
• CEC occupied by basic cations
• CEC occupied by calcium
cation exchange capacity
copper index
exchangeable sodium percent
percent humic matter
potassium index
potash
% CEC occupied by magnesium
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

r C �P

Analytical Results
NCDOC-Odom Correctional Institution
485 Odom Prison Rd.
Jackson, NC 27845
Receive Date: 05/07/2019
Reported: 02/ 18/2020
For: Digester
Comments:
Sample Number Parameter Sample ID Result
190507-43-01 TCLP
Respectfully submitted,
Dena Myers
NC Cert #440,
igCDW Cert #37755,
EPA #NC00909
Digester See Attached
STATESVILLF
ANALYTICAL
Unit Method Analyzed Analyst
as Noted 05/08/2019 PACE
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 37

Condition of Receipt
Sample Number 190507-43-01 Temp on Arrival: 2.5
Parameter Schedule: TCLP
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 37

O
iD
0
x
N
N
00
N
rf
r+
m
m
z
N
00
rn
00
V
Ciien,:
MIEBVII.LBANALiPTiCAL
Addn
M Court Shin • P.O. Box 228
5tOSWEIe. NC 38W
—
-
- ---
-
(704) 872�1697 -
p.
Contact Per6on
Phone #
P FAX�t
O
Own of
Pas
f Requisitioned by:
D.re�
Custody Record
comer
&nVI& K*
Time Sampled
lab ID K (Grab Only
Date SAMPled
(amboww
P+maOeE�re�e�edfary f
ww
p•WOjE r
4
src
Relinquished
Time :��pm Data
Sampled by: A
Received
Time \4p `. G7 a r�) pm Date f .�L
Traneported by.
Relinquished
,
Time am, pm DaWNEJ� Jj1
Holding times met:
Received by: t/"[ -
#1:
Time �y am, pm Date �/��4
Compliance work
Composite t3amaling __ _ ---
Time begin am, pm Date _!J
Non-compikme work:
i
Time end am, pm Date —JJ
Lab
Corr: Samples TnumpMed On Ice: ` -
Coml oslte. SemRHx
M
Time begin am, pm Date
Time end am, pm Date —J—J—
ir�nals:

/ ceA►aaalydcal e
wew�peOeia6eopn
May 23, 2019
Crystal Little
Statesville Analytical, Inc.
122 Court Street
PO Box 228
Statesville, NC 28687
RE: Project: TCLP
Pace Project No.: 92428480
Raps Analytical Services, LLC
'4MKinceyAve. Suite 100
Hun1mv lo, NC 24M
p04)e7eaioei
Dear Crystal Little:
Enclosed are the analytical results for sample(s) received by the laboratory on May 08, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Aw4,—
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
r �
REPORT OF LA130RATORYANALYSIS
This report shall not be reproduced, except in rull,
1 without the written consent of pace AnalylloW Seruiees, uLG.
Page 1 of'34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 4 of 37

esayaaaleAcoae
r
Project: TCLP
Pace Project No.: 92428M
Pennsylvania Certftatlon IDs
1638 Roseytown Rd Suites 2,31t4. Greensburg, PA 15601
ANAS DOD-ELAP Red Accreditation #: L2417
Alabama Certification M. 415W
Arkom Certification #: AZO734
Arkansas Certification
California Certification # 04222CA
Colorado Certification #: PA01547
Connecticut Certification #: PH-0694
Delaware Certification
EPA Region 4 DW Red
Florlda/TNI Certification #: E87683
Georgia Certification #: C040
Florida: CertE871149 SEKS WET
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
Kansas/TNI Certification #: E-10358
Kentucky Certification #: KY90133
KY WW Permit, #, KY0098221
KY WW Permit* KY0000221
Louisiana DHH/TNI Certification #: LAI80012
Louisiana DEQMNI Certification P. 4086
Maine Certification #: 2017020
Maryland Certification M. 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification #: 9991
CERTIFICATIONS
Missouri Certification #. 235
Montana Certification #: CerU1082
Nebraska Certification P. NE-08-29-14
Nevada Certification #. PA01457201 B-1
New HampshirarrNij Certification #: 297617
New JerseyfTNI Certification #: PA051
New Mexico Certification fk PA01457
New York' TNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #r R-190
Ohio EPA RadApproval: #41249
OmgcWTNI Certification #: PA200002-010
Peansyivanfa/TNI Certification #: 65-00282
Puerto Rico Certification #: PAi01457
Rhode Island Certification #: 65.00282
South Dakota Certification
Tennessee Certification #: 02867
Texas/TNI Certification #: 7104704188-17-3
UtahrrNI Certification #i PA014572017 8
USDA Sol[ Permit #: P330-17-00091
Vermont DepL of Health: ID# VT-0282
Virgin (siand/PADEP Certification
VirginialVELAP Certification #: 9526
Washington Certification # C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 9964C
Wisconsin Approve List for Red
Wyoming Certification #: 8TMS-L
Charlotte Certlfiesdon IDs
9800 Kincey Ave. Ste 100. Huntaraville, NC 21078
South Carolina Certification #s 99006001
Louisiana/NELAP Cartiftatlah # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 6342
virginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville. Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Caroline Wastewater Certification #: 40
Flodda/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 VirglniaIVELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
TtiisreWeliall not be reproduced. except in full.
wlMeut the written consent of Pace Analytical Services, LU.C.
Pace Analytical Services, LLC
NO Kincey Ave. 'Suite 100
Huntelsville, NC 28078
[phone]
Page 2 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 5 of 37

ceAnalyiical e
sww.peceliskoom
Project: TCLP
Pace Project No.: 92428480
Lab ID Sample ID
92429460001 19050743-01
92428480002 19050745-01- PCB
Paw Analytical Sarviees, LLC
9b0o Kincey Ave. 'Suite f00
Huntersvllle, NO 2408
[phone]
SAMPLE ANALYTE COUNT
Anatytes
Method
Analysis
Reported
Laboratory
EPA 8081 B
SEM
9
PASI-C
EPA 8082A
RES
8
PASI-C
EPA6010D
DS
7
PAST -A
EPA7470A
JMW1
1
PASI•A
EPA8270E
Bpi
18
PASI-C
EPA 8280D
SAS
14
PASI-C
ASTM 02974-87
KDF
1
PASI-C
EPA f01'0A
SMK
f
PASI-A
EPA9045D
SMK
1
PASI-A
EPA 9095E
SMK
1
PASI-A
EPA 9014
PAS
1
PASI-PA
SM 450082F-00
PAS
1
PASI-PA
EPA 8082A
SEM
8
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 34
PO Box 228 a Statesville, NC 28687 9 704/872/4697
Page 6 of 37

ANALYTICAL RESULTS
Project. TCLP
Pace Project No.: 92428480
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hurnersvllle, NC28078
(704)87t3-9092
Sample: INS074341 Lob 10: 92438480001 Collected: 05M7119 09:30 Received: 0510811913:50 Matrix: Solid
Rasults rapo►ted on ashy welght' basis and are adjusted lbrpam cant moisd^ sample she and any dilutions.
Parameters Results Unite Report Limes DF Prepared Analyzed CAS No. Qual
8081 TCLP Pesticides RVE
gamma-BHC (Lindans)
Chlordane (Technical)
Enddn
Heptachlor
Heptachlor epoxide
Medioxychlor
Toxaphehe
Surrogates
Decachlorobiphanyl (S)
Tetrachlororrl-xylene (S)
8082 TCLP PCBs RVE
PCB-1016 (Amclor 1016)
PCB-1221 (Amdor1221)
PCB-1232 (Arodor 1232)
PCB-1242 (Arodor 1242)
PCB-1248 (Arottor 1248)
PCB-1254 (Arodor 1254)
PCB-1260 (Arodor 1260)
Surrogates
Docachlorobiphenyl (8)
Analytical Method: EPA 8081 B Preparation Method: EPA 351 OC
Leachate Method/Date:.EPA 131l; 0511419 16:31 Initial
pH: 5.28; Final pH: 5
ND
u9/1-
0.50
1
05/17/19 09:18 05/17/19 18:07 58489-9
ND
ug/L
3.0
1
OW17119 09:18 05/17,110 18:07 57-74-9
ND
4L
0.50
1
OW17/19 0918 06/17119 18:07 72-21 -8
ND
ug/L
0.50
1
05/17/19 0916 05M7/19 18:07 76-44-8
ND
ug/L
0.50
1
05/17/19 09:18 05/17/19 18:07 1024-57-3
ND
ug/L
1000
1.
05/17/19 09:18 05117119 18:07 72-43.5
ND
ug/L
3.0
1
05/17/19 09:18 05/17/19 18:07 8001-35-2
42 % 10-139 1 05/17119 09:18 05/17/19 18:07 2051-24-3
29 % 10-110 1 D5117/19 09:18 05/17/19 18:07 877-09-8
Ang"cal Method: EPA 8082A Preparation Method: EPA 3610C
Leachate Mathod/Date: EPA 1311; 05/14/19 %31 Initial pH: 5.28; Final pH: 5
ND
ug/L
1000
1
06/16119 13:66 06/16119 22:30 12674-11-2
ND
ug/L
1000
1
05/16/1913:55 05/16/19 22:30 11104-28-2
ND
ug/L
1000
1
06/16/19 13:55 06/16119 22:30 11141-16-6
ND
ug/L
1000
1
05/16/19 13:55 05/16119 22:30 53469-21-9
'ND
ug/L
1000
1
05/16M913:55 05/1611922:30 12672-29-6
ND
ug/L
1000
1
06/1611913:55 05116/1922:30 11097-69-1
ND
ug/L
1000
1
05M611913:55 OSM6/19 22:30 11096-82-5
81
%
10-132
1
05116/1913:65 05/16119 22:30 2051-24-3
6010 MET ICP, TCLP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 05/16/19 23:31 Initial pH: 7.39; Final pH: 4.5
Arsenic
ND m91L 0.050 1 05/17/19 22:62 05/19/19 01:14 7440-38-2
Barium
0.92 mg/L 0.26 1 05/17/19 22:52 05/19/19 01:14 7440-39-3
Cadmium
Nb mg/L 010050 1 05/17/19 22:52 0511911901:14 7440-43-9
Chromium
ND mg/L 0.050 1 05M7/19 22:52 05/19/19 01:14 7440-47-3
Lead
ND mg/L 0.025 1 05/17/19 22:52 05/19/19 01:14 7439-92-1
Selenium
ND mg/L 0.10 1 05/17/19 22:52 05/19119 01:14 7782-49-2
Silver
ND mg/L 0.025 1 05117119 22:52 05/19/19 01:14 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 05/16/19 23:31 Initial pH: 7,39; Final pH: 4.5
Mercury
ND mg/L 0.000,20 1 05/20119 08:34 05/20/19 15:31 7439-97-6
8270E MSSV TCLP $ep Funnel
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
1,4-Dlchlombenzene
ND ug/L 50.0 1 05116/1920:10 05/2111916:04 106-46-7
2,4-Dlnitrotoluene
ND ug/L 50:0 1 05/16119 20:10 05/21/19 16.04 121-14-2
Hexachloro-11,3-butediene
ND ug1L 50.0 1 05/16/19 20:10 05/21/19 16.04 87-08-3
Hexachlorobenzene
ND ug/L 50.0 1 05/1611920:10 05121/1916:04 118-74-1
Hexachioroathane
ND ug/L 50.0 1 05/16/19 20:10 06/21119 16:04 67-72-1
2-McMylphanoi(o-Creson
No ug/l. 50:0 1 05116/1920:10 0512111916:04 95-48-7
W-Methylphencl(m&p Cresol)
ND ug/L 50:0 1 05/16/19 20:10 05/21/19 16:04 15831-10-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 05/23/2019 04:56 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 34
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 7 of 37

r=,
ceAnalyhcal a
wMep"OW&COM
ANALYTICAL RESULTS
Project: TCLP
Pace Project No.: 92428480
Pace Analytical Services, LLC
QWDKinceyAve. Suite100
HuntergWl e, NO 2W
Sample: 190507-43-01 Lab ID: 9242848MI Collected: 05/07/19,09:3D Received: 05/08/1913:50 Maw: Solid
Results reported on a 'dry waight' holds and are adjusted for percent moisture, sample al" and any dilutions.
Parameters Results Units Report Limit OF Prepared Analvzed CAS Nn.
8270E MSSV TCLP Sep Funnel
Nitrobenzene
Pentachiorophanol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Ruorobiphenyl(S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
8260D MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichioroetharie
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Didiloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
1010 Flashpoint,Closed Cup
Flashpoint
9045 pH Soil
pH at 25 Degrees C
9D95 Paint Filter Liquid Test
Free Liquids
733C S Reactive Cyanide
Cyanide, Reactive
Date: 05/23/2019 04:56 PM
Analytical Method: EPA 8270E Preparation Method.: EPA 3510C
NO
ug/L
5010
1
05116/1920.1.0 05121M916:04 9845-3
NO
ug/L
100
1
051161192010 D5/21l19 16:04 87-e6-5
ND
ug/L
50,0
1
05/16MO20:10 05/2111916:04 110486-1
ND
ug/L
50:0
1
05116/1920:10 05121/1916:04 95-95.4
ND
ug/L
50.0
1
05/16/19 20:10 05/21ti9 16:04 88.06-2
47
%
12-102
1
05/16/19 20:10 05/21119 16:04 4165-60-0
43
%
13-107
1
05/16/1920:10 05/2111916:04 321-60-8
70
%
21-132
1
05/16/10 20:10 05121/1916.04 1718-51-0
16
%
10-110
1
06116/19 20:10 0612111916.04 13127-88-3
25
%
10-110
1
05116/1920:10 06MI/1918:04 367-12-4
56
%
27-108
1
05116119 20:10 05/21/19 16.04 118-79-6
Analytical Method: EPA 8260D
NO
ug/L
100
20
05/22/1918:39 71.43-2
NO
ug/L
200
20
05/2211.918:39 78-93-3
NO
ug/L
100
20
05/22/1918:39 56-23-5
NO
ug/L
100
20
0512211918:39 108-9D-7
NO
ug/L
100
20
05W0918:39 61-66-3
NO
ug/L
100
20
05/221491839 10646-7
NO
ug/L
100
20
05/22/1918.39 107-06-2
NO
ug/L
100
20
05/2211918:39 15-35-4
NO
ug/L
100
20
05/2211918:39 127-18-4
NO
ug/L
100
20
05/22/1918:39 79-01-6
NO
uglL
100
20
06=1918:39 75-01-4
113
%n
70-130
20
05/22/1.918:39 17060.07.0
103
%
67-13$
20
OW211018,39 2037 26-5_
102
%
70-130
20
05/2211018:39 460-00-4
Analytical Method: ASTM D2974-87
97.4 %
0.10
1
05/09/1916:58
Analytical Method: EPA 1010A
>200 deg F
70.0
1
05/2011015:45
Analytical Method: F-PiA9045D
7.2 Std. Units
0.10
1
05M3119 15:13
Analytical Method: EPA 9095B
Fail
1.0
1
05/13119 18:18
Analytical Method: EPA 9014 Preparation Method: SW=846 7.3.32
NO mg/kg
39.1
1 05/16/19 22:38 05/17119 01:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Qua]
H3
Page 5 of 34
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 8 of 37

Pace Analytical Services. LLC
9800 Kh=yAve. Suite 100
HurdervAle. NC 28078
[phone]
ANALYTICAL RESULTS
Project: TCL:P
Pace Project No.: 92428M
Sample: 190507-43-01 L:ab 1D: 92428480001 Collected: 05/07119 09:30 Received: 05/08/1913:50 Matrix: Solid
Results reported on a "dry weight" bash and are aaijusted for percent mo/atum, sample size and any dludons.
Parameters Results Unite Report Limit OF Prepared Analyzed CAS No. Qual
7US Resctit"Suttlde Analg0eat Method: SM S2F-W Preparation Me4+od: SVW-846 7.3A.2
Sulfide, Reactive ND m9*9 391 1 05116119 22:38 06/16/19 22:49
Sample: 190507.43.01- PCB Lab ID: 924Z8480002 Collected: 05/07/19 09:30 Received: 05/08/19 13:50 Matrix: Non Aqueous
Liquid
Results reported on a "dry weight' basis and are arqusted for percent moisture, sample size and any dihrtMns.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[
am GCS PCB
PCB-1016 (Arodor 1016)
PCB-1221 (Arodor 1221)
PCB-1232. (Arodor 1232)
PCB-1242 (Arodor 1242)
PCB-1240 (Arodor 1248)
PCB-1264 (Arodor 1254)
PCB-1260 (Arodor 1260)
Surrogates
Decachlorobiphenyt (S)
Date: 05/23/2019 04:56 PM
Analytical McOrod: EPA W82A Preparation Method: EPA 3580
NO
mg/kg
lk
1
05121/1907:43 05/2111916:03 12674-11-2
ND
mglkg
1.0
1
05/21/1907:43 05/2111916:03 11104-28-2
ND
mg/kg
1.0
1
05/21/19 07:43 06/21/1916:03 11141-16-5
NO
m9ft
1.0
1
06/21M907:43 0512IM916:03 53469-21-9
NO
mg/kg
1.0
1
06/21/19 07.43 05121/1016.03 12672-29-6
NO
mglltg
1:0
1
05/21/19 07:43 05/21/19 16:03 11097-69-1
NO
m9ft
1.0
1
05/21119 07:43 05121/4916:03 11096-82.5
31
%
49-130
1
05W/19 07:43 06/21119 16:03 2051-24-3 S2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services. LLC.
Page 6 of 34
PO Box 228 a Statesville, NC 28687 e 704/872/4697
Page 9 of 37

_ aceAwlly bl
wwrpaealabsrom
QUALITY CONTROL DATA
Project: TCLP
Pace Project No.: 92428480
Pace Anslytiesl Strikes, LLC
MW Kincey Ave. Suite i0a
Huntersvi9e, NC 2eQ78
(704)8759092
QC Batch: 476096
Analysis Method: EPA 7470A
QC Batch Method; EPA7470A
Analysis Description: 7470 MercuryTCLP
Associated Lab Samples: 92428480001
METHOD BLANK: 2578524
Matrix: {Water
Associated Lab Samples: 92428480001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Merry mg/L
ND 0.00020 05/2aJ191,5:D1
LABORATORY CONTROL SAMPLE: 2579773
Spike LCS LCS % Roe
Parameter Units
Cone. Result % Roe Limits Qualifiers
Mercury mg/L
0.0025 0.0023 92 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2579774 2579776
MS MSD
92428492001
Spike Spike MS MSD MS MSD % Rae
Parameter Units Result
Cone, Cone, Result Result %Rec %Rec Limits RPD Qual
Mercury mg/L ND
0.0025 0.0026 0.0022 0.0022 87 86 75-125 0
Results presented on this papa are In the units indicated by the R111hs' column except where an altemate unit Is presented to the right of dis result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05123/2019 04:56 PM without the written consent of Pace Analytical Services, LLC, Page 7 of 34
PO Box 228 a Statesville, NC 28687 is 704/872/4697
Page 10 of 37

wdwpomt-
Project: TCUP
Pace Project No.: 92428M
0C Batch: 476094
QC Batch Method: EPA 3010A
Associated lab Samples: 92428480001
METHOD BLANK 2578524
Associated Lab Samples: 92428480001
Parameter
units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mglt-
Lead
mg/L
Selenium
mg/L
Silver
mg1L
LABORATORY CONTROL SAMPLE: 2579770
QUALITY CONTROL DATA
Analysis Method:
EPA 6010D
Analysis Description:
6010 MET TCLP
Matrix: Water
Blank Reporting
Result Limit
Analyzed
NO
0.050
05119119 00:31
NO
0.25
05/19/19 00:31
NO
0.0060
05/19/19 00:31
NO
0.050
05/19119 D0:31
NO
0.025
05/19/19 00:31
ND
0.10
05/19/19 00:31
ND
0.025
05119M19 00.31
qualifiers
Pace Analyfiwl Services, LLC
98W KirweyAve. Suite 100
Huntersville. NC 20078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Arsenic
mg/L
2.5
2.2
89
80-120
Barium
mg/L
2.5
2.3
92
80-120
Cadmium
mg/L
2.6
2.3
90
M120
Chromium
hog/L
2:5
2.2
90
80-120
Lead
mg/L
2.5
2.2
87
80-120
Selenium
mg/L
2.5
2.4
96
80-12D
Silver
mg/L
1.2
1.2
94
80-120
MATRIX SPIKE 8: MATRIX SPIKE DUPLICATE: 2579771
2579772
MS
MSD
92425492002
Splke
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Cone.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Quai
Arsenic
mg/L
NO
2.5
2.5
2.2
2.2
89
89
75-125
0
Barium
mg/L
0.32
2.5
2.5
2.6
2.6
90
91
75-125
1
Cadmium
mg/L
NO
2.5
2.5
2.2
2.2
89
89
75-125
1
Chromium
mg/L
NO
2.5
2.5
2.2
2.3
89
89
75-125
0
Lead :
mg/L
ND
2.5
2.5
2.2
2.2
87
87
75-125
0
Selenium
mg/L
NO
2.5
2.5
2A
2A
94
96
75-125
2
Silver'
n1911
ND
11
1.2
1.2
1.2
93
94'
75.125
1
Reauib pmswrk d on this page am In the unhaIndesled by the'[Mu' cohnM except whore an aMmete unit Is pres6nbd to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full.
Date: 05/23/2019 045B PM without the written consent of Pace Analytical Services. LLC.
Page 8 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 11 of 37

QUALITY CONTROL DATA
Project: TCLP
Pace Project No.: 92428480
QC Batch: 476885
Analysis Method:
EPA 8260D
QC Batch Method: EPA 8260D
Analysis Desarip0on: 8260D MSV TCLP
Associated Lab Samples: 9242M0001
METHOD BLANK: 2582807
Matrix: Water
Associated Lab Samples: 92428480001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1-Dichloroethene
ug/L
NO
5.0
06=1915:28
1,2-Dichloroethane
ug/L
NO
5.0
05/22/1915:28
1,4-Dichiorobenzene
ug/L
NO
5.0
05/22/1915.28
2-Butanone (MEK)
ug/L
NO
10.0
05/22/1915:26
Benzene
ug/L
NO
5.0
05/2211915:28
Carbon tetrachloride
ug/L
NO
5.0
0512211916-28
Chlorobenzene
ug/L
NO
6.0
05122f1915:28
Chloroform
ug/L
NO
6.0
06=1916:28
Tetrachioroethene
ug/L
NO
5.0
05=191528
Trichloroethene
ug/L
NO
5.0
05/22J1915 28
Vinyl chloride
ug/L
NO
5.0
OW2119 15:28
1,2-Dichloroethane-d4 (S)
%
109
70-130
05/22f1915:28
4-BromaNuorobenzene (S)
%
97
70-130
05/22/19 15,28
Toluene -dB (S)
%
102
67-135
06=19 15:28
Qualifiers
LABORATORY CONTROL SAMPLE:
2582806
Spike
LOS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1, 1 -Dichloroethene
ug/L
5o
52.8
106
70-130
1.2-Dichloroethane
ug/L
50
47.8
96
70-130
1,4-Dichlorobenzene
ug/L
50
50.4
101
70-130
2-Butanone (MEK)
ug/L
100
99.3
99
64-135
Benzene
ug/L
50
50.9
102
70-130
Carbon tetrachloride
ug/L
50
51.5
103
70-130
Chlorobenzene
ug/L
50
50.4
101
7Q-130
Chloroform
ug/L
50
51.0
102
70-130
Tetrachloroethene
ug/L
50
51.3
103
69-130
Trichloroethene
ug/L
50
49.9
100
70-130
Vinyl chloride
ug/L
5o
55.7
111
70-131
1,2-Dichlaroethene-d4 (S)
%
100
70-130
4-eromofluorobenzens (S)
%
98
70-130
Toluene-d8 (S)
%
100
67-135
Pace Analytical Servkea, LLC
9800 Kincey Ave. Suite 100
HuntowAle, NO 24070
Q04)87540"
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2582808 2582809
MS MSO
92428876002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
10-Dichioroethene ug/L NO 400 400 484 504 121 126 70-154: 4
Results prosanted on this papesre In Ms un(tr Indleafad by go'UMb" cWumn except %td" On ONW699 WO.is pr"wftd to the rh;M girths result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/23/2019 04:56 PM without the written consent of Pace Analytical Services, Li<C. Page 9 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 12 of 37

�J`II ►al
QUALITY CONTROL DATA
Project TCLP
Pace Project No.: 92428480
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
2592808
2582809
MS
MSD
92428876002
Spike
Spike
MS
Parameiwr
Units
Result
Conc.
Colic.
Result
12-131chlbroethane
ug/L
NO
400
460
430
1,4-Dichtorobenzene
upt
NO
400
400
429
243utamne (MEK)
ug/L
NO
800
800
960
Benzene
ug/L
ND
400
400
448
Carbon tetrachloride
ug/L
ND
400
400
444
Chlorobenzene
ugfL
NO
400
400
428
Chloroform
U91L
NO
400
400
447
Tetrachloroethene
uglL
NO
400
400
428
Trlchloroethene
ug/L
NO
400
40D
424
Vinyl chloride
ug/L
NO
400
400
523
1,2-Dichloroethane-d4 (S)
%
4-Bromoflucrobenzene (5)
%
Toluene-d8 (S)
%
Pace Analytical Services, LLC
9t100 Kincey Ave. Suite 1D0
Huntersville, NC 28078
[phone]
MSD
Result
MS
% Rec
MSD
% Rec
% Rao
Limits
RPD
459
107
116
70-137
7
443
107
111
70-133
3
1010
109
115
60-139
5
466
112
116
70-151
4
469
111
117
70-143
6
442
107
110
70-138
3
492
112
123
70-139
10
432
107
108
59-143
1
454
106
113
70-147
7
532
131
133
70-156
2
105
103
70430
101
99
70-130
100
98
67-135
Results presorted on this page are In the units Indicated by the'Iiritte' oelumn except wines an alternate unit Is presented to the right of the mulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/23/2019 04:56 PM without the written consent of Pace Analytical Services. LLC.
Qual
Page 10 of 34
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 13 of 37

.4111
WAWica!'
QUALITY CONTROL DATA
Project: TCLP
Pace Project No.: 92428480
QC Batch: 475707 Analysis Method: EPA 8081B
QC Batch Method: EPA 3510C Analysis Description: 8081 TCLP Pesticides RV
Associated Lab Samples: 92428480001
METHOD BLANK: 2575604
Associated Lab Samples: 92428480001
Parameter
Units
Chlordane (Technical)
ug/L
Endrin
ug/L
gamma-BHC (Lindane)
ug/L
Heptachlor
uglL
Heptachlor epoxide
ug/L
Methoxychlor
u9/L
Toxaphene
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
LABORATORY CONTROL SAMPLE: 2577952
Parameter
Units
Endrin
ug/L
gamma-BHC (Lindane)
ug/L
Heptachlor
ug/L
Heptachlor epoxide
ug/L
Methoxychlor
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
MATRIX SPIKE SAMPLE:
2577953
Parameter
Units
Endrin
ug/L
gamma-BHC (Lindane)
ug/L
Heptachlor
ug/L
Heptachlor epoxide
ug/L
Methoxychlor
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
wee Ano"cat StM IeW LLC
9800 Kincey Ave. Suite 100
Huntersvtlle, Nc 28p78 f
(704)8754M2
Matibc water
Blank
Reporting
Result
Limit
Analyzed
Qualifiers
NO
3.0
06116/1919:44
NO
0.50
06116/1919:44
NO
0.50
05/1611919:44
NO
0.50
05/1611919 44
NO
0.50
05/161191a."
NO
1000
05/18/19 19t44
NO
3.0
05/16M919:44
99
10-138
06/16/1919:44
96
10-110
05/1611919:44
Spike
LOS
LCS %'Rao
Conc.
Result % Rec Limits Qualifiers
1.2
1A
108
20-134
1.2
1.2
96
20-118
1.2
1.1
89
20-342
1.2
1.3
101
22-133
3.8
3.7J
98
44-160
96
10-138
85
10410
92428789001 Spike
Result
Conc.
NO
1.2
NO
1.2
NO
1.2
NO
1.2
NO
3.8
MS
MS
Result
% Rec
1.1
85
1.1
91
1.6
119
1.0
62
3.1J
82
68
77
% Rec
Limits Qualifiers
21-133
24-110
16-128
50-150
50-160
10-138
10-110
SAMPLE DUPLICATE: 2577954
92428789002 Dup
Parameter Units Result Result 1RPD Qualifiers
Chlordane (Technical) ug/L NO NO
Endrin ug/L NO ND
Resues presented on this page sm to the units l"cated by Me'Unw column except whom an axernate unitis presented to the right of the mautt
REPORT OF LABORATORY ANALYSIS
This report shall nat be reproduced, except in fill.
Date: 05/2312019 04.56 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 34
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 14 of 37

e
l'L'At��IJ/fical
Project: TCLP
Pace Project No.: 92428M
SAMPLE DUPLICATE: 2677954
Parameter
gamma-BHC (Lihdane)
Heptachfor
Haptachfor epoxide
Methoxychlor
Toxaphene
DecachloroblPhimIA (S)
Tetraohbro-m-*ene (S)
QUALITY CONTROL DATA
92428789002
Dup
Urtb
Result
Result
uglL
ND
ND
ug1L
ND
ND
Ug/L
ND
ND
UWL
ND
ND
ug(L
ND
ND
46
0
0
%
0
0
RPD Qualffiers
D3,S4
S4
Pace Ang"cal Services, LLC
9800 leincey Ave. Suite 100
Huntersville, NO 28078
(704)8754W92
Re.utb pnowded on thk pe0. aft In &a uaPoe Indteeted by the'Uplte' adunm except.rhee.n aasmeb unft is prsseued to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full.
Date: 05/2312019 04:56 PM without the written consent of Pace Ans"eai Services, LLC.
Page 12 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 15 of 37

/_
ceAnalyiical
/ wwrapar�e.wm
QUALITY CONTROL DATA
Project: TCLP
Pace Project No.: 92428480
Pace Ans"cai Services, LLC
9800 Kincey Ave. suite 100
HuntBrgvtlle, NC 2W.78
(7a4�ers.el�a
QC Batch: 476468
Analysis Method:
EPA 8082A
QC Batch Method:. EPA 3680
Analysis Description:
8082 GCS PCB Oil
Associated Lab Samples: 92428480002
METHOD BLANK: 2581047
Matrix: Non Aqueous Liquid
Associated Lab Samples: 92428480002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
PCB-1016 (Arodor 1016)
mglkg
NO
1.0
06121M919:13
PCB-1221 (Aroclor 1221)
mglkg
NO
1.0
05121/19 19:13
PCB-1232 (Aroclor 1232)
mglkg
NO
1:0
06/21/19 19:13
PCB-1242 (Aroclor 1242)
mg/kg
NO
1.0
05121/19 19:13
PCB-1248 (Aroclor 1248)
mglkg
NO
1.0
05121/1919:13
PCB-1254 (Aroclor 1254)
mglkg
ND
1.0
05/21/191913
PCB-1260 (Arocior 1260)
mg/kg
ND
1.0
05/21/191913
Decachlorobiphenyl (S)
%
51 49-130
05/21/1912:13
LABORATORY CONTROL SAMPLE: 2581048
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
PCB-1016 (Aroclor 1016)
mg/kg
10 11.8
Its
50-148
PCB-1260 (Aroclor 1260)
mg/kg
10 6.8
88
63-149
Decachlorobiphenyl (S)
%
52
49-130
MATRIX SPIKE SAMPLE: 2581049
92429664001 Spike
MS
MS % Rec
Parameter
Units
Result Conc.
Result
% Rec Limits Qualifiers
PCB-1016 (Aroclor 1016)
mg/kg
ND 10
12.2
122 56-143
PCB-1260 (Aroolor 1260)
mglkg
1.3 10
11.7
104 10-156
Decachloroblphenyl (S)
%
106 49-130
SAMPLE DUPLICATE: 2581o50
92429664003 Dup
Parameter
Units
Result Result
RPO
Qualifiers
PCB-1016 (Aroclor 1016)
mg/kg
NO —
NO
PCB-1221 (Arodor 1221)
mg/kg
ND
ND
PCB-1232 (Aroclor 1232)
mglkg
NO
NO
PCB-1242 (Arodor 1242)
mg/kg
NO
ND
PCB-1248 (Aroclor 1248)
mg/kg
NO
ND
PCB-1254 (Aroclor 1254)
mglkg
ND
ND
PCB-1260 (Aroclor 1260)
mg/kg
1.6
1.6
3
Decachlorobiphenyl (S)
%
93
91
Results Presented on this PMP are In ere units 1"catad by are Nntts' opturnn exeeptwhere an akemaw unit is prwentadto-the ftm of" result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/23/2019 04:66 PM without the written consent of Pace Anaiyucat Services, IAC. Page 13 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 16 of 37

eww.pacela6attom
Project:
'TCLP
Pace Project No.:
92428480
QC Batch: y
475711
QC Batch Method:
EPA 3510C
Associated Lab Samples: 92428480001
QUALITY CONTROL DATA
Analysis Method: EPA 8082A
Analysis Description: 8082 TCLP PCB RV
METHOD BLANK: 2576604
Matrix: Water
Associated. Lab Samples: 024284MMI
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
NO
1000
05116/19 23:21'
PCB-1221 (Aroclor 1221)
ug/L
ND
1000
05/16/19 23:21
PCB-1232 (Aroclor 1232)
ug/L
ND
1000
05/16/19 23:21
PCB-1242 (Aroclor 1242)
ug/L
NO
1000
05116119 23.21
PCB-1248 (Aroolor 1.248)
u41L
NO
1000
05/16119 23:21
PCB-1264 (Aroclor 1254)
ug1L
ND
1000
06/16/19 23:21
PCB4260 (Aroclor 1260)
u01L
NO
1000
O5/16/19 ft21
Decachlorobiphehyl(S)
%
80
1OA32
05/1611923:21
LABORATORY CONTROL SAMPLE: 2517966
Pace Analytical Services, LLC
11800 KlnceyAve. 'Suite 100
Hunt6nsville, NC 20078
(704)8754=2
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
PCB-1016 (Aroclor 1016)
u91L
25
NO
81
38-113
PCB-1260 (Aroclor 1260)
ug/L
25
NO
66
35-120
Decachloroblphenyl (S)
%
96
10-132
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2677967
2577966
MS
MSD
92426480M1
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Unit$ Resylt
Cone.
Cone.
Result
Result
% Rec % Rec
Limits RPD
PCB-1016 (Aroclor 1016)
ugll. NO
25
25
NO
NO
66 77
19-142
PCB-1260 (Aroclor 1266)
ug/L ND
25
25
NO
NO
47 49
19-142
Decaohlorobiphanyl (S)
%
71 66
10-132
Results Presented on this peps are In the units indicated by the' links' column except wham an attemateunit Is preaented to the NpM of thO result.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except In full,
Date: 05123/2019 04:56 PM without the written consent of Pace Analytical Ser-Aces, LLC.
Qual
Page 14 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 17 of 37

F..
e•
/ acAffl6l l
/ www.peaeleds a m
r
Project: TCLP
Pace Project No.: 92428480
QC Batch: 475849
QC Batch Method: EPA 3510C
Associated Lab Samples: 92428480001
METHOD BLANK: 2575604
Associated Lab Samples: 92428480001
QUALITY CONTROL DATA
Analysis Method: EPA 8270E
Analysis Description: 8270E TCLP MSSV
Matrk- Water
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,4-Dichlorobenzene
ug/L
ND
50.0
05/16/1917:27
2,4,5-Trichlorophenol
ug/L
ND
50.0
05116/1917:27
2,4,6-Tric:htorophenol
ug/L
ND
50.0
0511611917:27
2,4-Dinitrotoluens
ug/L
ND
50.0
05/1611917:27
2-Methytphenol(o-Cresol)
ug/L
NO
50.0
0511611917.17
3&4-Methylphenol(m&p Cresol)
ug/L
NO
50:0:
05/16119 17:27
Hexachloro-1,3-butadiene
ug/L
NO
50.0
06116/1917:27
Hexachlorobenzene
ug/L
NO
50.0
05/1611917:27
Hexachloroethane
ug/L
NO
50.0
05116/19 17:27
Nitrobenzene
ug/L
ND
50.0
05116/1917:27
Pentachlorophenol
ug/L
NO
1D0
05116/1917:27
Pyridine
ug/L
ND
50,0
0511611917:27
2,4,6-Tribromophenol (8)
%
97
27-108
05116/19 1727
2-Fluorobiphenyl (S)
%
83
13-107
05116/1917*27
2-Fluorophenol (S)
%
41
10-110
05/16/1917:27
Nitrobenzene-0 (S)
%
81
12.102
0511611917:27
Phenold6 (S)
%
26
10-110
05/16/1917:27
Terphenyl-04 (S)
%
104
21-132
05116/1917:27
LABORATORY CONTROL SAMPLE: 2578590
Qualifiers
flee Ansly6oel S•rvico., Lt C
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rep
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
500
368
74
1D-110
2,4,5-Trichlorophenol
ug/L
500
467
93
39-108
2,4,6-Trichlorophenol
ug/L
600
459
92
40-104
2,4-Dinitrotoluene
ug/L
500
461
92
42-109
2-Methylphenol(o-Cresol)
ug/L
Sao
338
68
31-110
3&4-Methylphenol(m&p Cresol)
ug/L
500
288
58
30-110
Hexachloro-1,3-butadiene
ug/L
500
373
75
10-110
Hexachlorobenzene
ug/L
500
480
96
39-121
Hexachlomethane
ug/L
500
335
67
10-110
Nitrobenzene
u9/L
$00
400
80
32-101
Pentachlorophenol
ug/L
1000
805
80
18-108
Pyridine
ug/L
500
237
47
10-11D
2,4,6-Tribromophenol(S)
%
103
27-108
2-Fluorobiphenyl (S)
%
93
13-107
2-Fluorophenoi(S)
%
45
10-110
Nitrobenzene-d5 (S)
%
85
12-102
Phenol-d6 (S)
%
29
10-110
Terphenyl-04 (S)
%
95
21-132
Results presented on this peas ore in the unite Indicant by the'Units" column eX9W White en aMerrd" unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 05/23/2019 04:56 PM without &* written consent of Pace Analytical Services, U.C.
Page 15 of 34
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 18 of 37

f
ceAnal��cal.
Project:
TCLP
Pace Project No.:
92428M
QC Eudch:
474373
QC Batch McLthod:
ASTM D2974-07
Associated Lab Samples; 92428480001
SAMPLE DUPLICATE: 2571899
Parameter Units
Percent Moisture - — %
QUALITY CONTROL DATA
Analysis Method. ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92428408001 Dup
Result Result RPD Qualifiers
20.7 19.9 4
SAMPLE DUPLICATE: 2571900
92428480001 Dup
Parameter Unts Resuft Result RPD Qualifiers
Percent Moisture % 97.4 97A 0
Pace Analytical Services, LLC
9800 Wncey Ave. Suite 1A0
Huntersvilie. NC 28078
p04j875-9092
Results preawned on this page wo In do uNts Indlested by the' UrIW eotunm exeaptwhere an altarhab unit is prebmibd to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/23/2019 04:56 PM without the written consent of Pace Analytical Services. LLC.
Page 16 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 19 of 37

aceA►aalyiica!
axtxpewNbatmm
QUALITY CONTROL DATA
Project: TCLP
Pate Project No.: 92428M
QC Batch: 476285 Analysis Method: EPA 1010A
QC Batch Method: EPA 1010A Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92428480001
SAMPLE DUPLICATE: 2580307
92428380001 Dup
Parameter Units Result Result RPO Qualifiers
Flashpoint deg F >200 >200
°ace Analytical Services, LLC
t1800 Kincey Ave. 'Suite f 00
Huntersville, NC 24078
(704)87&9092
Results Pmsenbd on this pow am in the unite "Cates by the'Units" cOumn except where an atlemats unit to presented to the right of the reau8.
REPORT OF LABORATORY ANALYSIS
This report shall not bb reproduced, except in full.
Date: 05/23/2019 04;56 PM without the written Consent of Pace Analytical.Serviees, LI:C.
Page 17 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 20 of 37

Pace Analytical Services, LLC
9800 KinceyAve. Suite 1.00
Hurdersville. NC 28078
(704)875-9D92
Projects TCLP
Pace Project No.: 92428M
QC Batch: 474806
QC Batch Method: EPA 9045D
Associated Lab Samples: 92428480001
SAMPLE DUPLICATE: 2574056
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description; 9045 pH
92428020001 Dup
Parameter Urfds Result Result iRPD Qualifiers
pH at 25 Degrees C Bid. Units 7.7 7.8 1 H3
SAMPLE DUPLICATE: 2674057
924282190D1 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C SW. Units 6.1 6.2 1 H7
Results pnsenled on this papa an In the uNte Indleated by the'UWW aoknm except when an ekemato unit Is prof 0 lad to the right of the reaulL
REPORT OF LABORATORY ANALYSIS
This report emit not be reproduced. except in full.
Date: 0512312019 04:56 PM without the wHttan consent of Pace Ans"cal Service, LLC,
Page 18 of 34
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 21 of 37

IrW
I,AwAnaocale
wwwomewWom
i
Project: TCLP
Pace Project No.: 92428480
QC Batch: 474804
QC Batch Method: EPA9095B
Associated Lab Samples: 9242848DO01
SAMPLE DUPLICATE: 2574063
Parameter
Free Liquids
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 24078
1704)875-9092
QUALITY CONTROL DATA
Analysis Method: EPAS095B
Analysis DescrIption: 9095 PAINT FILTER LIQUID TEST
92428000001 Dup
Units Result Result RPD Qualifiers
Pass Pass
Results presented on this pays ere In the uMts indicated by Via VnW column except no -so sh ehemals Wills pressftd to tl1i rlyht of the result
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Date: 05/23/2019 04:56 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 34
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 22 of 37

fi`a/'V IUI ,
_ rwlapot>�As.vas
Project TCLP
Pace Project No.: 92428400
QC Batch: 342750
QC Batch Method: SV4-846 7.3.3.2
Associated Lab Samples: 92426480001
METHOD BLANK: 1668235
Assooletad Lab Samples: 92428480001
Parameter Units
Cyanide, Reactive mg"
LABORATORY CONTROL SAMPLE:
1668236
Parameter
Units
Cyanide, Reactive
m9*9
SAMPLE DUPLICATE: 1655237
Parameter
Units
Cyanide, Reactive
Pave Analytical Services, LLC
9800 Kinoey Ave. Su'de 100
Hunteraviile, NC 28078
(704)875-9D92
QUALITY CONTROL DATA
Analysis Method: EPA 9014
Analysis Description: 733C Reactive Cyanide
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.99 05117119 00:60
Spike LCS LCS %Rec
Conc. Result % Rec Limits Qualifiers
99.2 ND 0 0-8
30294119001 Dup
Result Result
1.3 U ND
RPD Qualifiers
Results pressnud an this pegs au In the units Indicated by the'UnW column except whom an alternate unit Is presented to the right of tM result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Data: 05/23/2019 04:56 PM without the written consent of Pace Analytieai Services, LLC. Page 20 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 23 of 37

8C2A**jl e
Project: TCLP
Pace Project No: 92428M
QC Batch: 342751
QC Batch Method: SW-846 7.3.4.2
Associated Lab Samples: 92428MOol
METHOD BLANK: 1668238
Associated Lab Samples: 92428480001
Parameter
Sulfide, Reactive
Units
mg/kg
LABORATORY CONTROL SAMPLE: 1668239
Parameter Units
Sulfide, Reactive mg*g
SAMPLE DUPLICATE: 1660240
Parameter Units
Sulfide, Reactive mglkg
QUALITY CONTROL DATA
Analysis Method: SM 4500S2F-00
Analysis Description: 734S Reactive Sulfide
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 9.9 05116/19 22:49
Qualifiers
Pace Anattrdeal Services, LLC
9800 KinoeyAm. Suds /oo
Huntaryville, NC 20078
U04075402
Spike LCS LCS % Rec
Conc. Result % Rea Limits Qualifiers
199 39.7 20 0-52
30294119001 Oup
Result Result RPD Qualifiers
12.5 U ND
Results presented on this pegs are In the units indicated by the'Units" column except when, an a9emate unit In presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 05/23/2019 04.56 PM without the written consent of Pace Analytical Services, L4.C. Page 21 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 24 of 37

WCeA*"
W-Pno"01110
QUALIFIERS
Project TCLP
Pace Project No.: 92428480
DEFINITIONS
DF - Dilution Factor, I reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllls, NC 24078
[phone]
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOL -Adjusted Method Detection UmiL
POL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest twncentrallm value that meets project requirements for quantitative data with known precision and
bias for a specific one" in a specific matrix.
S - Surrogate
1,2-01phenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unroundeddata are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP- Sample Duplicate
RPD - Relative Percent'Ditference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyt ether.
A separate Wei preserved to a pH of 4-5 Is recommended in SW846 Chapter 4 for the analysis of Acroleln and Acrylonitrtie by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anaiyte Is a cornbined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
RASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-anarybis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
Date: 06t23/2019 0056 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 34
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 25 of 37

�2aceAWicalo
f wwgpeos�sean
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: TCLP
Pace Project No.: 92428480
Lab ID
Sample ID
92428480001
190507-43-01 `
924284B0002
190507.43-01- PCB
92428460001
190507.43-01
92428480001
190507-43.01
9242M0001
190507-43-01
92428480"1
190507-43-01
924284B0001
190507.0-01
92428480001
190507.43-01
92428480001
190507-43-01
92428480001
19050743-01
92428480001
190507-43-01
92428480001
190507.43-01
92428"0001
1"507-43.01
Date: 05/23/2019 04:56 PM
Pace Analytical Services, LLC
91i00 Kincey Ave. Suite 100
Hurteravllle, NC 24078
[phone]
QC Batch Method
QC Batch
AnaWlW IYlathod
Anal
800h
EPA 3510C
475T07
EPA 8081 B
4759M
EPA 3580
476468
EPA 8082A
476626
EPA 351 OC
475711
EPA W82A
475939
EPA 3010A
476094
EPA 8010D
476130
EPA 7470A
476096
EPA 74701A
476266
EPA 351 OC
475649
EPA 8270E
476290
EPA 8260D
476885
ASTM D2974-87
474373
EPA 1010A
476285
EPA 9045D
474806
EPA 9095B
474804
SW-846 7.3.3.2
342750
EPA 9014
342939
SW-846 7.3.4.2
342751
SM 450062F-00
342937
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 23 of 34
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 26 of 37

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�,,• ANALYTICAL REPORT
waonalCanre dutng&tmaxalon May 20, 2019
Ss
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1097608 rqn
Samples Received: 05M0/2019
FSr
Project Number: 92428480
Description: TCLP 6QC
Site: 001
Report To: Tyriek Hooks rGI
9800 Kincey Avenue, Suite 100 'AI
Huntersville, NC 2:8078
17-1
9SC
Entire Report Reviewed By: �- W La--'v�.
Nancy McLain
Project Manager
Resufts telate ordytd,the hems tested or calibrated and are repotted astounded valves. Tills test report shall not be
reproduced; except in full,vathoutwritten appreal of the laboratory: Where applicable, sampling conducted by Pace National
Is performed per guidance provided laitic rato7standard operating protedure3: 060302, 060303, and 060304.
ACCOUNT: PROJECT: SDG: DATEMME: PAGE-.
PaceAna"cal- Huntersville,NC 92428480 ..-... L1097608 0512CV1916:56 toff©
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 28 of 37

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
c p; %"otter Par;?
{
F r,—
Tc: Table of Contents
2
j
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
190507-43-01 L1097608-01
5
Qc: Quality Control Summary
6
Fn]
Chlorinated Acid Herbicides (GC) by Method 8151A
6
FSr
Gk Glossary of Terms
7
Al: Accreditations & Locations
$
s
QC
Sc: Sample Chain of Custody
9
r q,
Page 26 of 34
ACCOUNT: PROJECT: SDG: DAITEITIME: PAGE:
Pees Ana"wl - HUntePaWlie. NC 92428490 L10976W 05126t12 *56 2 of 10
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 29 of 37

190507-43-01 L1097608-01 Waste
Method
Preparation by Method 1311
Chlorinated Acid Herbicides (GC) by Method 8151A
ACCOUNT:
Pace Analytical - Huntersville. NEE
SAMPLE SUMMARY ONE LAS. NATIONMC>E.
Collected by
Batch Dilution Preparation
date/time
WG1281786 1 05115/1917.24
WG1282168 1 05/ A9 08:46
PROJGCT: SbG:
92428490 L1097608
Collected daWlilme Received dete/time
05/07119 0930
D5l10/19 08-43
Analysis
Analyst Location
datehime
05A5A917:24
CGD Mt. Juliet, TN
05119719 09:24
KLM Mt. Juliet, TN
Page 27 of 34
bATEJTIME PAGE
05/2011016:56 9 of 10
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 30 of 37

CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, In the proper containers, with the l
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOO) values reported for environmental samples FTC]
have been corrected for the dilution factor used in the analysis. All Method and Batch Ouality Control
are within established criteria except where addressed In this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been Identified by the laboratory, and no information or data have been ■
knowingly withheld that would affect the quality of the data.
Fri
/1 e
Nancy McLain Al
Project Manager
9Sc
Page 28 of 34
ACCOUNT: PRolmr.. Soo: DATUrIME: PAGE:
Pace Ana"tai- HuntemAlfe. NG 92428490 L1097608 0512011016.56 401`10
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 31 of 37

190507-43-01
SAMPLE RESULTS - 01
ONE LAB.NATIONWtM.
Collected date/time: 05/07/19 09:10
L1097605
Preparation by Method 1311
Result
ggdner Prep Batchi?
Analyte
date i time
TCLP Extraction -
571512019 5:24:55 PM WG7291786
TC
Fluid 1
51IM019 Sr2455 P9 WG128TM'
Initial pH 7.23
SAW0195:24:55 PM W61281786
Final pH 4.82
MOM 5:24:55 PM WG1281786
S3
Chlorinated Acid Herbicides (GC) by Method 8151A
rc n]
Result
OualiOet RDL Limit Dilution
Analysis
Batch
Anal e m ll
m A m A
date Itime
2,4,5-TP(Silvex) ND
0.00200 1 1
05f19l201909:24
NfG1 76$
2,4'0 ND
0.00200 10 1
05A9l201909:24
W612fl2768
6(�C
(S)7,4-DichlorophenylAcetic AC7tl 81.6
14.0-158
05119120190924
WG1282768
ACCOUNT:
Pace Analytical - tiuntennrlile, NC
F11
CAI
9Sc
Page 29 of 34
PROJECT: SDG: DATEtrime PAGE:
9742WO L1097608 05I20AS 16:56 5 Qf 10
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 32 of 37

WG1282768
QUADTY CONTROL SUMMARY
ONE LAB. NATIONWIDE
Chfo60a1od Acid Harbisides (GC),pY Method 9161A -
- L1097609.01.
f Method Blank (MB)
(MB)a341NWt 03119n908:56
M8 Result MB OuaMler MB MDL
MB RDL
m9fi Froll
- ...
m9fiTc
2.4- U (1409667
0.00200
2,4;5-'IP M e# U 0.000687
0.11=1
3S5
75.8
14.0.199
Acl/dd2.4-WiamphenidAceitc
4Cn
Laboratory COtItrol Sample (LCS)
SSr
(LCS)R3412968-2 0611911909:10
Spike Amount LCS Result LCS Rec
Res. Umlts LCS Qualifter
Analyle .. mpA %
%
..
. .. - ..
._ ......
. .1.
...
■
2,40 • .. .79 _ ....
0.0500 0.0506 101
50.01120
.
24.SPD(S" 0.0500 6.0mg 109
50.0425
1 GI
Ac(SI Z,40Uchhuophw44AceBc 88.4
M.0.758
aAi
1-1097608-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
95c
(OS) L109%084t OF,d19A909:24 • (MS) R3413968-3 05ASA9 0938
• (MSD) R34129684 05A9A909:51
Spate Amount Original Result MS Result
MSO Result MS Rec. MSD Rep. Dilution
Rep. Limits MS OuaROer MSD OualiAer RPD
RPD Limits
Anelyte mg4 mg0 m9p
mgR % %
% %
%
2,4OA500 ND 0.0534
0.0515 107 103 1
50.0.1I0 161
20
2,4,5-'DP(Sllve4 0.0500 ND 0.0567
0.0546 it} 109 1
50.0-M 3,77
20
(S)1,4,DkhIgropher84Aee8c
Acid
8E8 92..4
14.0-158
..•. .. Page 30 of 34
ACCOUNT: PROJECT: Sm OATS711A PAGE
Pape Anelye[el -Hunts We. NC 92428480 L-m7608 0600A916:56 6 of 10
PO Box 228 • Statesville, NC 28687 9 704/872/4697
Page 33 of 37

GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This Is not
intended as a comprehensive explanation, and If you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected At the Reportlpg Umft (or MDL where appticable).
RDL
Reported Detection Limit
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Croup.
Surrogate (Surrogate Standard) - Analyses added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detectedin all environmental media.
O
Not detected At the Reportingg Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses And Methods will have multiple anaVias
reported.
If the sample matrlx contains an Interfering material, the sampre preparation volume of weight values differ from the
Dilution
standard, or if concentratlons.of anafytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. if a Value differarrt than f is used in this field, the
result reported has already beeh corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non spilcedsampple in the prep batch used to determine the Relative percent (]ifjeteriM (RMI iroM a x rlity r fntrol
sample, The OriglAal.5ample may -not be Included within the reported SD6.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible Implications of the Qualifier In the Case Narrative if applicable.
The actual Analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result In this column may state "ND' (Not Detected) or't3DL"
Result
(Below Detectable Levels). The Information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection limit) that defines thelowestvalue that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma,
g
A brief discussion about the included sample results. Including a disctisslon of eny.non-cohformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present. there will
be a section In the Case Narrative to discuss the meaning of any data qualifiers used In the report.
Quality Control
This section of the reportIncludes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material,
This is the document created in the field when your samples were initially collected, This is used to verify the time and
Sample Chain of
dateof collection, the person collecting the samples, and the analyses thatthe iabo. ty is requested to.perform.'Thls
Custody (Sc)
cha[n of custody also documents all persons (excluding commercial shlppers) that have toil Control or putseaslon.afthe
samples from the time of C008Ct10h until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis for
section
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, Including the dates and
times of preparation And/or analysis.
Qualifier
Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG
ACCOUNT:
Pace Anatytical - Huntersvllle, NC
Paige St of 34
PROJECT: 5013: DATE/TIME: PAGE
92429480 L1097608 05/2011916:56 70fto
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 34 of 37

ACCREDITATIONS & LOCATIONS
ONE LAB. NATIONWIDE.
Pace.Hatlaretlsldeo* awironmental laboratory accredReMcettli ed m support yaw work nationwide from one locatlon. One phone call, one palntef contact, one laboratory. No ~lab Is as
accesitble at prepared m daaNeyour needs throughout the cbua0y. Ouf Lapadly_andcapabl8ly f�atr our single locaDon laboratory 1s amparable W 1fie cdlacth/e Fatah of the network
r I
lahoraWrieS In atk Intktstty. The mostsigM8eant benefit to mitaft kra6ofide3lptllS tke design of our Latkfratdry campus. Ttre model is torMudve to accekaated PtodutlMty decreasing
turnaround tlme, and preverttlag cresscantaminattan. thus ptotettitgsample kdegrity.Our focus on premium qualityand prompt service allows us to be YOUR lA8 OF CHOOIICE
;
j
• Notall cerkRcagonsiheld by the laboratory are applicable to the resitOs repotted In the attached report.
'Accreditation Is only appllcableto the test methods specffied an each scope oraccreddation held by Pace National
Tc
State Accreditations
3
Nodama._ 40660 - --_-- Nebraska
NEOS-1"5
S]
Alaska 774ti6 Nevada
TN-03-2002-34
Ancona A20612 NewNampshlre .:..
_ - 2975
88-0464 _.--_—_— ---__---- New J,mee-NE_LAP�..__ - _--------
TN002
_Arkansas ._ .. ... ___.... _
California 2932 New Mexico
n!a
Colorado TN00003 New York
11742
Conneeacut PH-0197 North Carolina
EnV375
Fri
Fronde E97497 North Carolina'
OW21704
Georgia North Caroline''
41
923 Georgia' Norm Dakota
923
R-410
QC
Idaho TN00D03 Ohio-VAP
CL0069'
Illinois 200009 Oldahoma
9915
7GI
Indiana C-TN-01 Oregon .
TN2O=
Iowa 364 Pennsylvenle
66-02979
Konsas E-10277
Rhode Island
LA000356
Kentucky" 90010
South Carolina
94004
Kentucky' 16
South Dakota
Na .
Louisiana Au30792
Tennessee"
n
..._.._...
T06
104704245.1B-15
SC
Louisiana ..... ...;NppD20 ............. ........-..... _
ne
to,
LA9W'32
Maryland $24
Utah
TN"M
Massachusetts A4TN003
Vermont
VTZ006
. Michigan .. .. 9958 ..
Vlrvnla
460132..
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missoud 340
Wisconsin
9980939MO
Montana CERT0086
Wyoming
AAA
Third Party Federal Accreditations
QLA-,LSO T7625 1461:01
AIHA-LAP,LLC EMLAP
100789
A21A- ISO 110251461:02
DOD
1461M
Canada 1161.01
USDA
P33045.00234
EPA-Crypto TN00003
' Drinking Water 'Underground Storage Tanks 'Aquatic Toxicity ' Chemical/Mlcroblological s Mold
`Wastewater rda Accreditation not applicable
Our Locations
Pace National _has -sixbrfour dlerd suppod centers that providesampfe pickup andlarthe delivery of sampling supplies. R you would like ass6Uncefrom.one of our suppod offices, please contact
our main office. Pace NetWBIlperformsall testing at our bentral Laboratory.
WA
MT NO
v LD 90 I ♦ v n SY
..�F
�y
ll�
" T V61V 1
CA\ co i{ INO T
t €CS i �....,r."`P KY ilk, r'I
r
All
♦ ---. Ms�vGA
LA
TX
-.. \
V ..
-_ ems``'`{ ♦ S�.....a-�,..,�-�':., �`"�
...w7� HL
Page 32 of 34
ACCOUNT: PROJECT: SDG: DATEMME PAGE.
Pace Analydral - Huntersville- NC 924M90 1-1007608 175'720A916:56 a of io
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 35 of 37

s
Chain of Custody
J247
Workorder. 924284M Workorder Nwee: TCLP
ne r imrrerc a Resulb Requested By: 812=19
TWiek Hooka sedneiyrar� Ta Anrtyals ..-
Pepe Anelytloal C 3aft a
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P.Q.
Suite 100
Hunters,Alk%NC 28078
Pace National
Ph—(704)0759M
12065 Lebanon Rd
Email: ty ,,m
Mt Juliet, TN 37222
615-758-5858
State of Sa M 06 In: NC
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FMT-ALLL-002rev.0024Ma'ch21109 Page J34 1
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 36 of 37

Pace Anflylical National Center for Testing & Innovation
Cooler Receip' Form
(Client! 14G % ol-7
SL7t�a:
i"ooler Rettiverl/Or, On: 5 / If / 19 Temperature:
'j
Receiml By: Jeremy Webb
Signature:
ReWpt check Ust NP
Yes
No
COC Seal Present J intact?
COC Stgned J Accurate?
BotOes arrive intact?
Correct bottles used?
Sufficient volume sent?
VOA Zero heads ace?
e-,*NatlM CohVd Chetket!?:'
Page 34 of 34
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 37 of 37

LA CS

Analytical Results r - STATE. sic LF
ANANCDOC-Odom Correctional Institution
485 Odom Prison Rd.
Jackson, NC 27845
Receive Date: 05/07/2019
Reported: 02/18/2020
For:
Comments: GM 8745 MPN/g -
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190507-42-01
Fecal Coliforms
1
9957
MPN/g
SM92210E-2006
05/08/2019
WC
190507-42-01
Percent Solids
1
2.31
%
SM2540-2011
05/08/2019
WC
190507-42-02
Fecal Coliforms
2
10000
MPN/g
SM92210E-2006
05/08/2019
WC
190507-42-02
Percent Solids
2
2.30
%
SM2540s-2011
05/08/2019
WC
190507-42-03
Fecal Coliforms
3
10177
MPN/g
SM92210E-2006
05/08/2019
WC
190507-42-03
Percent Solids
3
2.26
%
SM2540e-2011
05/08/2019
WC
190507-42-04
Fecal Coliforms
4
8394
MPN/g
SM92210E-20W
05/08/2019
WC
190507-42-04
Percent Solids
4
2.74
%
SM254OB-2011
05/08/2019
WC
190507-42-05
Fecal Coliforms
5
7904
MPN/g
SM92210E-2006
05/08/2019
WC
190507-42-05
Percent Solids
5
2.91
%
SM25409-2011
05/08/2019
WC
190507-42-06
Fecal Coliforms
6
8070
MPN/g
SM92210E-2006
05/08/2019
WC
190507-42-06
Percent Solids
6
2.85
%
SM2540B-2011
05/08/2019
WC
190507-42-07
Fecal Coliforms
7
7210
MPN/g
SM92210E-2006
05/08/2019
WC
190507-42-07
Percent Solids
7
3.19
%
SM254os-2011
05/08/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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STATESVILLEANAGY7TCAL '
t22 Court Street - 'HO. Box =
Statesville, NC 2W7
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Time end am, pm Date _l—1
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_ Compliance work:
Non-compliance work:
Lab Comments: Samples Transp ned On,lce:f— —
Initials. ��/

Analytical Results
NCDOC-Odom Correctional Institution
485 Odom Prison Rd.
Jackson, NC 27845
STATESVILLE
ANALYTICAL
Receive Date:
Reported:
For:
Comments:
Sample Number
05/07/2019
02/18/2020
Digester
Parameter
Sample ID
Result
Unit
Method
-
Analyzed
Analyst
190507-41-01
Aluminum
Digester
8370
mg/kg
EPA 200.7 rev4.4 1994
05/20/2019
MD
190507-41-01
Ammonia Nitrogen
Digester
5626.79
mg/kg
SM450ONH3BE-1997
05/13/2019
MD
190507-41-01
Arsenic - Solid
Digester
4.11
mg/kg
SM3113 B-2004
05/20/2019
MD
190507-41-01
Calcium
Digester
17800
mg/kg
EPA200.7
05/20/2019
MD
19050741-01
Chromium
Digester
19.1
mg/kg
EPA200.7
05/14/2019
MD
190507-41-01
Copper
Digester
378
mg/kg
EPA200.7
05/14/2019
MD
190507-41-01
Lead -Solid
Digester
16.94
mg/kg
SM3113B
05/10/2019
MD
190507-41-01
Magnesium
Digester
4460
mg/kg
EPA200.7
05/20/2019
MD
190507-41-01
Mercury Solid
Digester
0.066
mg/kg
SM3112B-2011
05/21/2019
MD
190507-41-01
Molybdenum
Digester
7.99
mg/kg
EPA200.7
05/16/2019
MD
190507-41-01
Nickel
Digester
14.6
mg/kg
EPA200.7
05/14/2019
MD
190507-41-01
Nitrate/Nitrite -
Digester
248.804
mg/kg
SM45DOF/A
05/28/2019
CL
Solids
190507-41-01
PAN
Digester
483.3
mg/L
Calculation
05/29/2019
CL
190507-41-01
Percent Solids
Digester
2.09
%
SM25406.2011
05/08/2019
WC
190507-41-01
pH
Digester
7.19
Std. Units
SM4500HB-2011
05/07/2019
MD
190507-41-01
Potassium
Digester
2320
mg/kg
EPA200.7
05/1.5/2019
Meritech
190507-41-01
SAR
Digester
1.81
%
Calculation
05/29/2019
CL
190507-41-01
Selenium
Digester
<0.24
mg/kg
EPA200.7
05/20/2019
MD
190507-41-01
Sodium - Solid
Digester
7224.88
mg/kg
SM3111 B
05/20/2019
MD
190507-41-01
T. Phosphorus Solid
Digester
16270
mg/kg
SM450OPE-2011
05/08/2019
CL
190507-41-01
TKN
Digester
55785.6
mg/kg
SM450ONorgB-2011
05/10/2019
CL
190507-41-01
Zinc
Digester
1377
mg/kg
EPA200.7
05/14/2019
MD
PO Box 228 - Statesville, NC 28687 - ' 04/872/4697
Page 1 of 5

Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190507-41-01 Cadmium - Solid Digester 2.73 mg/kg sM3111&1999 05/20/2019 MD
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

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STATESYIT,GE,ihIALYTiCAL
Address:
122.Cairt'&radt : P.O. Box 229
SntesvilJeq WC :28b87
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(704) M 407
Contact Person: H Ube K,
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Phone # �1 C' �„ Rb, .. W* FAX#
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Sample ID#
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Grab Orly)
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Time begin am; pm Date _/_J_
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Time end am, pm Date —/
1.a6 Comments: SemplesTrensported On ICA:
Composite Sampling #2:
Time begin • am, pm Date _ _/
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Inleal

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No.165
Contact: C. Little
Client: Statesville Analytical
1Z2 Court St
Statesville, NC 28677
Report Date: 5/17/2019
Date Sample Rcvd: 5/0/2019
Meritech Work Order # 05081943 Sample: 190507.41.01 Grab 5/7/2019
Parameter results Analysis Date Reporting Limit Method'
%. Total Solids 2.48 % 5/10/2019 0 100 % SM 2540B
Potassium, total 2320 mg/kg 5/15/2019 1.00 mg/lcg EPA 200.7
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

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FORM SLUIR-'i Slurry and Sludge Application Field Record
For Recording Slurry Applicaton Events on Different Fields
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