WQ0019960_Residual Annual Report 2019_20200217

2019
City of Marion
WWTP
2019 Annual Report
Land Application Program
Permit No. WQOO1996O
RECEIVEDIh+CDECIDWR
FEB 1 7 2020
Non -Discharge
Pemlitting Unit
FFg ! 2020
AI DW° )

ANNUAL LAND APPLICATION CERTIFICATION FORM
< <WQ Permit#: WQ0019960 County: McDowell Year:
2019
Facility Name (as shown on permit):
Land Application Operator:
City of Marion
Phone: _ 336-957-7871
Land application of residuals as allowed by the permit occurred during the past calendar year?
21 Yes CQ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Fart A - Residuals Application Summarv:
Southern Soil Builders, Inc.
Total number of application fields in the permit: 8
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 145.89
Total number of acres utilizes for land application during the year: 44.6
A as L - A111uni %-umpAunce Statement: "
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes El No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T . 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 11 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a.deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and -belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing viola ons.
,� 2-1 �-2o2a
Pe •mittee Nam ) e and Title (type or printSi ature of Permit e /� Date
0- ��,1
�,�utu�� .,� Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1 102 (26) nFNR F(')RNA Af.P llolonnaN

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0019960
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Annlvcic Dntn
City of Marion
NC0031879
Corpening Creek
Laboratory:
1)
2)
3)
4)
5)
ETS
Conc.
Sample
or Composite
Date
Parameter
Limit
(mg/kg)
(mg/kg) a
3-5-19
Percent Solids (%)
NA
4.64
Arsenic
75
9.63
Cadmium
85
3.85
Copper
4,300
377
Chromium
NA
NA
Lead
840
52
Mercury
57
1.4
Molybdenum
75
31
Nickel
420
22.4
Selenium
100
9.63
Zinc
7,500
957
Total Phosphorus
NA
20900
TKN
NA
41400
Ammonia -Nitrogen
NA
1000
Nitrate and Nitrite
NA
22
e r__ _
•
.,. —1-11---f' aa, 1aU111LIU3 Ulu ..U111,,g wnccnLrauon umns ustea In tms corm are not applicable. Reference the individual permit. for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a. system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penaltie )or submitting false information, including the possibility of fines and imprisonment for knowing violations."
parer fi _Ij
2 - (o - --� -. ?e,-
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0019960
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
I
City of Marion
NC0031879
Corpening Creek
Laboratory:
1)
2)
3)
4)
5)
ETS
aampie or Composite Date
Parameter
3-5-19 (mg/kg)
Aluminum 25100
Calcium 15900
Magnesium 7230
Potassium 2760
Sodium 1020
pH 7.4
SAR 0.368
PAN 12642
66T ,+; _a _■,
--- ---.> > . F'11"��y Vl lAW, Wat Wis aocument was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1-102 (26)
2 -!a
Date

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility'Name: -City of Marion Total Dry Tons Applied (Annual): 38.98
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: John Fisher Owner: John Fisher Predominant Soil Series: HaC
Acres Used: 7 Acres Permitted: 7 Site #: F3
Field #: F3
Residual Analvsis Data (Nnavv Mptolr -A Ir-4-1 m_ ____I- -
Sample or
C0111-
posite
Date
? I2
3/25/20
L3j-
4
5
.. A ALur71/11V1
_6
uJ WW
7
111g/K
1 81
%o .aonas
use
Raw Percent
ft
9j
10
11
12
% Solids
4.64
Arsenic
9.63
Cadmium
3.85
Copper
377
Chromium
NA
Lead
52
Mercury
1.4
Molyb-
denum
Nickel
22.4
Selenium
9.63
Zinc
957
Total
Phos-
h01 IS
Annual
20900
Heavy Metal
Field
Loadin
s (Cal
1 t d
'
Total
DT/Ac./
1
2
3
g
4
cu a e
5
><n lbs/acre):
6
7
App.
Event
5.57
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molyb-
denum
0.107
0.043
4.199
######
0.579
0. 116
-
0.345
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0'.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0.00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Nickel
Selenium
Zinc
Total
0.249
0.107
10.659
0.000
0.0.00
0.000
0.000
0.000
0.000
0.000
7000
0.000
0.000
0.000
0.000
0.000
0.00.0
0.000
0.000
0.000
0.000
Phos-
232.784
0.000
0.000
0.000
0.000
0.000
0.000
•
' t e l l
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 lel
1 1�
I 1111
1 111
1 111
1 111
1 111
� ••
I 1111
1 111
1 011
1 111
1 111
I I Ile
1 111
1 Ill
1 111
1 111
1 •
I O 111
1 111
1 111
1 111
1 111
1 1 •
I1111
1 111
1 111
1 111
1 111
1�
I 1011
1 111
1 111
1 111
1 111
1�•
I 1111
1 111
1 ell
1 111
1 111
1 1
I 1111
1 111
1 111
1 111
1 111
1. •
1 1/1
1 111
1 111
1 ell
1 111
;,
"I certify, under penalty of law, that this document was prepared un superv�s>ton �n accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land pplier
09-4 u� d
Date
npNip rnonn nnci Clr f A I nnni,

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 30.19
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: John Fisher Owner: John Fisher
Predominant Soil Series: HaC
Acres Used: 6.7 Acres Permitted: 6.7 Site #: F4
Field #: F4
Residual Analysis Data (Heavy Metals and 'Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or l I 1 1 2 I s l I a I I a _
Com-
posite
Date
3/25/20
% Solids
4.64
Arsenic
9.63
Cadmium
3 85
Copper
377
chromium
Lead
Mercury
Molyb-
denurn
Nickel
Selenium
Zinc
Total
Phos-
NA
52
1.4
31
22.4
9.63
957
20900
Annual
Heavy
Metal Field Loadings
(Calculated in lbs/acre):
Total
DT/Ac./
1
2
3
4
5
6
7
8
9
10
11
12
App.
o
Event
4.51
Arsenic
.0.087
0..000
0.000
0.000
0.000
0.00.0
0.000
0.000
0,000
0.000
0.000
Cadmium
0.035 :
0.000
0,000
0.00.0
0.000
0.00.0
0.000
0.000
0.000
0.000
0.000
0.0.
00
0.087
Copper
3.398
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0,0' 0
0.03
Chromium
######
0.000
0.000
0.000
0.00.0
0.000
0.000
0.000
0.000
0.000
0.000
3.398
Lead
0.469
0.000 .
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
######
Mercury
0..013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.469
Molyb-
denum
0.279
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.013
Nickel
0.202
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.279
Selenium
0,.087
0..000
0.000
0.000
0.000
0.000
0.000
0.000
.0.000
0.000
0.0.00.
0.000
0.202
8.624
0..000
0.000
0.000
0.0000.000
0.000
0..000
0.000
0:000
0.0000.:087Zinc
0.000
q00
0.000
0:000
0.000
8.624Phos-
horus
188.351
0.000
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
] 88.351
"I certify, under penalty of law, that this document was
prepared under my direction or supervision
with a system designed to assure that qualified personnel
in
accordance
properly
I am aware that there are significant
gathered
and
evaluated
the
information
submitted.
penalties for submitting
imprisonment for knowing violations".
false information,
including
the possibility of fines and
i if?L_ ate(-) too
Signature of Land Applier
Date

ANNUAL METALS FIELD LOADING SUMMARY FORM*
'. Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 12.57
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: Brian Kay Owner: Brian Kay Predominant Soil Series: HaC
Acres Used: 17.2 Acres Permitted:. 17.2 Site #: R1 Field #: RI
Residual Analvsis Data (Henvv MPtale and Tn+nl D1,n....1.,....... _n__ n, c
Sample or
Com-
posite
Date
1
3/25/20
2
3
4
-----
5
-�r--
6
_ ..- ---
7
...b..�s,
8
io v�■au�
9
uao
10
i�ary rel-ceilt
11
}f ).
12
% Solids
4.64
Arsenic
9.63
Cadmium
3.85
Copper
377
Chromium
NA
Lead
52
Mercury
1.4
Molyb-
denum
Nickel
22.4
Selenium
9.63
Zinc
957
Total
Phos-
horus
Annual
20900
NPaVV MP+aI
F;ol.a
T
Total 1 2 3
4
DT/Ac./
5j-
[6�T
Ll
8 91101
11
12
App.°
Event 0.73
Arsenic 0.01.4 0.000 0.000 0.000
0.000
0.000
0.000 .
0.0.00 0:000
0.000
0.000
0.000
0.014
Cadmium 0.006 0:000 0.000. 0.000
0.000
0..000
0.000
0.000 0.000
0.000
0.000
0.000
0.006
Copper 0.551 0.000 0.:000 0:000
0.000
0.000
0:000
0.000 0.000
0.0 00
0.000
0.000
0.551
Chromium ###### 0.000 0.000 0.000
0.000
0.000
0.000
0..000 0.000
0.000
0.000
0.000
######
Lead 0.076 0:000 0.000 0.000
0.000
0.000
0.000
0.000 0.000
0.000
0.000
0.000
0.076
Mercury 0.002 0.000 0.00.0 0.000-
Molyb-
0.0.00
0.0007
0.000
0.000 0.000
0.000
0:000
0.000
0.002
denum 0.045 0.000 .0.000 0:000
0:000
0.000
0.000
0.0.00 0.000
0.000
0.000
' 0.000
0.045
Nickel 0.033 0_000 0.000 0. 000
0. 000
0:000
0.0.00
0.000 0.000
0.000
0;00"0
0.000
0.033
Selenium 0.014 0.000 0.000 0.000
0.000
0.0.00
0.000
0.000 0.000
0.000
0.000
0.000
0.014
Zinc 1.399 0.000 0.000 0.000
0.000
0.000
0.000
0.0000.000
0.000
0.0 00
0:000
1.399
Total
Phos- 30.556 0.000. 0.000 0.000
horus
0.000
0.000
0.000
0.000 0.000
0.:000
0.000
0.00"0
30.556
"I certify, under penalty of law, that this document was prepared under my direction
with a system designed to assure that qualified personnel
properly gathered and evaluated
or supervision
the
in accordance
information submitted.
I am aware -that there are significant penalties for submitting
false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Date
nFNR F(1RRA RAM cr:

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 64.14
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: Brian Kay. Owner: Brian Kay Predominant Soil Series: HaC
Acres Used: 13.7 Acres Permitted: 13.7 Site #: R2 Field #: R2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or 1 2 3 4 5 6 7 8 9 10 11 12
Com-
posite
Date 3/25/20
% Solids 4.64
Arsenic 9.63
Cadmium 3.85
Copper 377
Chromium NA
Lead 52
Mercury 1.4
Molyb- 31
denum
Nickel
22.4
Selenium
9.63
Zinc
957
Total
Phos-
20900
horus
Loadings (Calculated in lbs/acre):
Annual
Heavy Metal Field
Total
? 21
3 4 5
6
7
8
9
10
11
12
DT/Ac./
,
App.
°
Event
4.68
0.00'0 0.0.00 0.000 .
0.000 0.0.00 0.000 ,
0.00.0
0.000
0.0.00
0:000
0.000
0.000
0.0.00
0:000
0.000
0:000
0.0.00
0.000
0.000 "
0.000
0.090
0.036
Arsenic
0.090
0.000
Cadmium
0.036
0.000
Copper
3.530
0.000
0.000 0.000 0.:000
0.000
0000
.0.000
0.000
0.000
0.0.00
0.000
3.530
Chromium
######
0.000
0.000 0:000 0.000
0.000 0.000 0.000
60 00 0.000 0.000
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6 000
0.000
0.000
0.000
0.000
0.00.0
0.0 00
0.000
0.000
0.000
44####
0.487
0.013
Lead
0.487
0.000
Mercury
Molyb-
0.013
0�.000
denum
0.290
0.000
0.000 0.000 0.000
0.000 . 0.000 0.000
0.000
0.000
0.00.0
0.000
0.000
0.000
0.000
0.000 ;
0..000
0.000
0.000
0.000
0.000
0,000�
0.290
0.210
Nickel
0.210 0:000
Selenium
0..090 0.000
0.000 0:0.00 0.0"00
0.000
0.000
0.000
0.000 "
0:000
0.0.0:0
0.000
0.090
Zinc
8.961 0.006
0.000 0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
8.961
Total
Phos-
horus
1195.708 0:000
0.000 0.000 0.000
0.000
0.000
0.000
0.000
0.:000
0.0"00.
00.000195.708
"I certify,
under penalty of
law, that this document was prepared under my direction or supervision in accordance
with a system
designed to assure
that qualified personnel
properly gathered and evaluated the
information submitted.
I am aware
that there are significant
penalties for submitting
false information, including the possibility
of fines
and
imprisonment
for knowing
violations".
Signature of Land pplier Date
Mr=KID C:nDhl h/1M Cyr /Aninnn

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #• WQ0019960 Field #• F3 Acres Utilized: 7
Land Owner: John Fisher Annual Dry Tons Applied: 38.9878 Site #: F3 Acres Permitted: 7
Operator: John Fisher Predominant Soil Series: HaC Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I Max. PAN: 202 Crop 2 Name: Cron 2 Max. PAN:
_
°
Volume applied
Volume
Residual Sources
Soil
Precip_
D
<
o
K
z D
Nitrate
Name of Crop Type
P YP
° c
(enter one) Solids/
%
Applied per
PP P
(NPDES #, WQ#,
Cond.
Past 24
a
co _
,y _
x,
COw
TKN
_
o
and
PAN Applied
ReceivingResidua!
i °
Liquid
Solids
Acre
Fert., Animal
(Dn,
Hrs.
0 o'
a
-
°'
aq °
CD �.
J
Nitrite
( lbs/acre)
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc )
Wet
Moist)
inches
* =
0
mg/kg,
rng/kg
mg/kg
Crop 1
Crop 2
Crop I
Crop 2
4-2019
91000
4.64
2.515
WQ0019960
dry
0
s
0.5
0.3
41400
1000
22
63.598
NA
Fescue
9-2019
110500
4.64
3.054
WQ0019960
dry
0
s
0.5
0.3
41400
1000
22
77.226
NA
Fescue
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
0.000
0.000
0.000
0.000
0.000
6.060
0.000
0.000
0.000
Residuals Applications
totals
on FORM
FSF
supp ( attach
FORM
FSF supp
to this
form):
TOTALS:
01 201500
As
Cd Cu
Cr
Pb I
HR
Mo
Ni
Se
Zn
P
140.8241
0.000
Lime
Applied
Annuallbs/acre
0.107
0.043 4.199
#######
0.579
0.016
0.345
0.240
0.107
10.659
232.784
...
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.246
0.1
0.143
34
5.689
9.888
1338
1.763
#######
NA
0.881
1.460
267
0.035
0.051
15
0.294
0.639
NA
0.375
0.624
374
0.242
0.349
89
16.731
27.390
2498
J.
12-19
2000
Current Cumulative lbs/ac
0.353
Permitted C. P. L. R.****
36
Permit PAN Limit Ist/2nd Crop
...... .... .... -.... .
202
I Cer-iiiy, unuer penaity of iaw, tnat tnis document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
d 1& 8 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
}

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F4 Acres Utilized: 6.7
Land Owner: John Fisher Annual Dry Tons Applied: 30.1841 Site #: F4 Acres Permitted: 6.7
Operator: John Fisher Predominant Soil Series: HaC Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I .Max. PAN: 202 Cron 2 Name:, Crnn I. Vfny PAN -
o �
Q
4-2019
9-2019
Volume applied
(enter one) Solids/
Li uid
9
Cu. Yds Gallons
78000
78000
%.
Solids
4.64
4.64
Volume
Applied per
Acre
(Dry Tons/Ac)
2.253
2.253
0.000
0.000
Residual Sources
NPDES # W #
( Q
Fert., Animal
Waste, etc)
WQ0019960
WQ0019960
Soil
Cond.
p
( ry'
Wet,
Moist)
dry
dry
Preci P
past 24
Hrs.
inches
0
0
a
K a
5 o-
o m
s
s
<
o
x �;
� "
N
o•
7
0.5
0.5
n
� �,
* N
°*
o
0.3
0.3
TKN
mg/kg
41400
41400
Z a
_.
Mo o
g °
�'
mg/kg
1000
1000
Nitrate
and
Nitrite
mg/kg
22
22
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
PP
Crop i
56.953
56.953
0.000
6.000
Crop 2
NA
NA
0.000
0.000
Crop 1
Crop 2
Fescue'
Fescue
0.0.00
0.000
0-000
0.000
0.000
0.000
0.000
0.000
0.000 .
0.000
0:000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000-
0.000
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM
FSF supp to this form):
0.000
0.000
TOTALS:
Annual
0 156000 ,::;::.''::'.:;;..
Ibs/acre
As Cd Cu Cr Pb Hg Mo Ni Se Zn P 1. 1137007 0.066
0.087 0.035 3.398 ####### 0.469 0:013 0.279 0.202 0.087 8.624 188.351 <':`.:'' <:: <`<` ':
0.254 0.849 9.081 2.109 1.29 0.049 0.353 0.553 0.264 21.788
0.341 0.884 12.479 ####### 1.759 0.062 0.632 0.755 0.351 30.412
36 34 1338 NA 267 15 NA 374 89 2498
....
........:.. ;::... ..,:202
Lime Applied
Date Ibs/ac
Prior Years Cumulative lbs/ac
0
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
... kll,, 4A11UG1 !lG11aRLy ul law, tnat uus uocument was prepares under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
ignature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
.PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #• WQ0019960 Field #• R1 Acres Utilized: 17.2
Land Owner: Brian Kay Annual Dry Tons Applied: 12.5767 Site #• R1 Acres Permitted: 17.2
Operator: Brian Kay Predominant Soil Series: Hac Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
Volume applied V I Soil
o Y
0 o
Q
(enter one) Solids/
Liquid
9
Cu. Yds Gallons
%
Solids
o ume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert. Animal
'
Waste, etc)
Cond.
D
( ry'
Wet,
Moist)
Prec�p.
Past 24
Hrs.
inches
o>
a a
�•
o
C. o•
-
o
?'
_
N
_�
O
o
�.
�,
o
TKN
mg/kg
Z
0 o
2
P,
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
9-2019
65000
4.64
0.731
WQ0019960
dry
0
s
0.5
0.3
41400
1000
22
18.488
0.000
NA
0.000
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
6.006
0.000
0 000
0 000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS: 0 bs000 <.<;:.:: ` As Cd Cu Cr Pb Hg I Mo Ni Se Zn P _18.488 6.00o Lime Applied
Annual lbs/acre 0.014 0.006 0.551 ####### 0.076 0.002 0.045 0.033 0.614 1:390 30.556 _`. : ''.`.;; Date Ibs/ac
Prior Years Cumulative lbs/ac 0.137 0.073 9.706 1.475 1.469 0.057 1.285 0.602 0.178 24.591 12-19 2000
Current Cumulative lbs/ac 0.151 0.079 10.257 ####### 1.545 0.059 1.330 0.635 0.192 25.990
Permitted C. P. L. R. * * * *. 36 34 1338 NA 267 ' 15 NA 374 89 2498
Pe rmit PAN Limit lstl2nd Crop
02
qualified personnel properly gathered I certify,under penalty of law, that this document was prepared under m direction or �� p �' ' P P y supervision in accordance with a system designed to assure that
9 p p p y g d and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
d l .l 620 Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #• WQ0019960 Field #• R2 Acres Utilized: 13.7
Land Owner: Brian Kay Annual Dry Tons Applied: 64.1413 Site #: R2 Acres Permitted: 13.7
Operator: Brian Kay Predominant Soil Series: HaC Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
_
Volume applied
Volume
Residual Sources
0
a-
(enter one) Solids/
%
Applied
PP P er
(NPDES #, WQ#,
QLiquid
Solids
Acre
Fert., Animal
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
5-2019
45500
4.64
0.643
WQ0019960
9-2019
253500
4.64
3.580
WQ0019960
10-2019
32500
4.64
0.459
WQ0019960
3011
Precip.
Cond.
Past 24
0
cD
o
w
m 0
(Dry,
Hrs.
o w
* N
CD
Wet,
Moist)
inches'
dry
0
s
0.5
0.3
dry
0
s
0.5
0.3
dry
0
s
0.5
0.3
TKN
mg/kg
41400
41400
41400
Z Y
P;: 3
a o
QQ
g �=
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Crop 1
Crop 2
1000
22
16.248
NA
1000
22
90.523
NA
1000
22
11.605
1 NA
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Name of Crop Type
Receiving Residual
Application
Crop 1 Crop 2
Fescue
Fescue
Fescue
0.000_ 0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS: 01 331500 As Cd Cu Cr I Pb Hg I Mo Ni Se Zn P i l 8J 761 0.000 Lime Applied
Annual Ibs/acre 0.090 0.036 3.530 ##Ow 0.487 0.013 0.290 0.210 0.090 8.961 195.708 Date Ibs/ac
Prior Years Cumulative Ibs/ac 0.069 0.05 7.23 0.065 0.899 0.328 0.749 0.392 0.089 16.659 0
Current Cumulative lbs/ac 0.159 0.086 10.760 ####### 1.386 0.341 1.039 0.602 0.179 25.620
Permitted C. P. L. R. * * * * 36 34 NA 1338 267 15 NA 374 89 2498
PeCrop:;.:: < ...;...:..:...
:.
rmit PAN L_:.::.:.:.:::::::.:.:.:.................:
tmrt 1 st/2nd
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Signature of Land Applier Date
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate

3
xavr •
Environmental Testing Solutions, Inc.
Project name: Marion WWTP
Collection date:
Date received:
5-Mar-19
5-Mar-19
Certificate of Analysis
PO Bok 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number' 1903Q5.563
Sample identification: CC Sludge - Grab
Sample number:
164485
Parameter
Method
Result
RL
Units
Date
AnalYSt
Fbo'tnotes
Analyzed
Total Solids
SM 2540 G
4.64
0.10
%
7-Mar-19
MLR
-1
Mercury
7471B
1.4
0.4
mg/kg
is-Mar-19
TLT
1
Aluminum
6010 D
25100
482
mg/kg
20-Mar-19
LMC
1
Arsenic
6010 D
<9.63
9.63
mg/kg
15-Mar-19
LMC
1
Cadmium
6010 D
<3.85
3.85
mg/kg
15-Mar-19
LMC
Calcium
6010 D
15900
1070
mg/kg
22-Mar-19
LMC
1
Copper
6010 D
377
3.85
mg/kg
15-Mar-19
LMC
1
Lead
6010 D
52.0
9.6
mg/kg
15-Mar-19
LMC
1
Magnesium
6010 D
7230
96.3
mg/kg
15-Mar-19
LMC
t 1
Molybdenum
6010 D
31.0
9.63
mg/kg
15-Mar-19
LMC
1
Nickel
6010 D
22.4
3.,85
mg/kg
20-Mar-19
LMC
1
Potassium
6010 D
2760
19.3
mg/kg
15-Mar-19
LMC
; 1
Selenium
6010 D
<9.63
9.63
mg/kg
15-Mar-19
L1VIC
1
Sodium
6010 D
1020
19.3
mg/kg
15-Mar-19
LMC
1
Zinc
6010 D
957
9.30
mg/kg
. 20-Mar-19
LMC
1
Nitrate + Nitrite as N
300.0
<22.0
22.0
mg/kg
14-Mar-19
JM,M
1
Total Phosphorus
6010C
20900
535
mg/kg
2-Apr-19
LMC
.1
Total Kjeldahl Nitrogen
351.2
41400
716
mg/kg
15-Mar-19
LEW
1
Total Nitrogen
Calculation
41400
716
mg/kg
15-Mar-19
LEW
1
Ammonia Nitrogen
SM 4500 NH3 D
1000
210
mg/kg
7-Mar-19
KEK
pH
SW846 9040 C
7.4
0.1
S.U.
5-Mar-19
MS
2
Percent Solids
SM 2540 G
4.8
0.10
%
5-Mar-19
MS
N-PAV
Calculation
12620
5-Apr-19
KE,K
Sodium Absorption Rate
Calculation
13.4
5-Apr 19
KEK
SA R
SL7
Footnotes: l Z p
,Z
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analzyed outside holding time.
.opt4�
Date reviewed: NC Certifcation Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
NC Drinking Water Certification Number: 37786

SAR
Sodium Absorption Ratio
Na : Sodium (Mg/L) * Equivalent weight: 23
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Na M /L Ca M /L Mg(Mg/L)
48.96 1 763.2 1 347.04
Mg. (MEN
1
2,128696
1 38.16
28.92
Milli Equivalent = Mg/L / Equivalent weight The amour
amount of E
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power i
Permitting
SAR = 0.367563 (From Mg/L entered above)
SAR= 0.367788 (From ME entered below)
Na ME
Ca (ME)
M ME
2.13
1 38.16
1 28.92

PAN
Mineralization
as decimal
Total dry
tons/year
Acres
Applied on
Rate
0.3
TKN
41400
NH3
1000
NO3
22
NO2
0
% Solids
0.048
PAN Surface
12642 mg/kg 25.284 lbs/dry ton
0 Ibs total PAN
#DIV/0! llbs PAN/acre
PAN Injection
13142 mg/kg 26.284 lbs/dry ton
0 lbs total PAN
#DIV/0! lbs PAN/acre
Dry Tons/1000 gal.
0.20016
1st year PAN
Surface lbs.
0
1st year PAN
Injected lbs.
0
lbs./acre
Surface
#DIV/0!
lbs./acre
Injected
#DIV/0!
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
1000 X 8.34 X %solids X sp. gravity
2000
"=dry tons/1000gal."

��•• �'iiz. �t.�
a� l.. 1.�..:.
.0 Environmental Testing Solutions, Inc,
Project name: Marion WWTP
Collection date: 18-Mar-19
Date received: 18-Mar-19
Certificate ®f Analysis
Sample identification: _CC Sludge #1- Grab
PO' Box 7565
'Aslieville, NC 28802
Phone; [phone]
F.ax: [phone]
Project number: 1903A.506
Sample number: 16059
Parameter Method Result RL Units Date Analyit Footnotes
Analyzed
°/aTS SM 2540 G 4.9 0.10 % 18-Mar-19 MS
MuliTle Tube Fermentation Procedure SM.9221-E . <882 882 MPN is-Mar=19
Sample identification: CC Sludge #2 -Grab Sample number: 166160
Parameter Method Result RL Units Date Analyst,; Footnotes
Analyzed
%TS SM 2540 G 4.8 0.10 % 18-Mar-19 MS '
Mulitple Tube Fermentation Procedure SM 9221-E <864 864 MPN 18-Mar-19 KEK
Sample identification: CC Sludge #3 Grab Sample number: 166761
Parameter Method Result RL Units Date Analyst . Footnotes
Analyzed y':'
%TS SM 2540 G 4.7 0.10 % 18-Mar-19 IvIS•
Mulitple Tube Fermentation Procedure SM 9221-E <846 846 MPN 18-Mar-19 KEK
Sample identification: CC Sludge 04 Grab Sample number: 16042
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
°/aTS SM 2540 G 5.0 0.10 % 18•mar-19 MS.
Mulitple Tube Fermentation Procedure SM 9221'-E <900 900 MPN is.mar-19 KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
Date reviewed: NC Certification Number: 600
Data reviewed by: _ Kelley E. Keenan SC Certification Numb.. 99053
Signature: & NC Drinking Water Certification Numbers 37786
This reportshould not be —reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, nc:
The results in this report relate only to the samples submitted for analysis.

° "' J [W,PO
s'
Box 7565
Asheville NC 28802
Phone: [phone]
Fax: [phone]
i Envlronmentat Testing Solutions, Inc.
Certificate of Analysis
Project name: Marion WWTP
Project number: 190325.502
Collection date: 25-Mar-19
Date received: 25-Mar-19
Sample identification: CC Sludge #5 - Grab
Sample number: 166917
Parameter
Method
Result
RL
Units
Date Analyst Footnotes
Analyzed
%TS
SM 2540 G
5.0
0.10
%
25-Mar-19 MS
Mulitple Tube Fermentation Procedure
SM 9221-E
<900
900
MPN
25-Mar-19 KEK
Sample identification: CC Sludge #6 - Grab
Sample number: 166918
Parameter
Method
Result
RL
Units
Date Analyst Footnotes
Analyzed
%TS
SM 2540 G
5.0
0.10
%
25-Mar-19 MS
Mulitple Tube Fermentation Procedure
SM 9221-E
<900
900
MPN
25-Mar-19 KEK
Sample identification: CC Sludge #7 Grab
Sample number: 166919
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%TS SM 2540 G 5.0 0.10 % 25-Mar-19 MS
Mulitple Tube Fermentation Procedure SM 9221-E <900 - 900 MPN 25-Mar-19 KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
Date reviewed: 01 NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
Signature: VA__ NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc
The results in this report relate only to the samples submitted for analysis.

Environmental Testing Solutions, Inc.
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: (828) 350=9364
Fax: [phone]
Project name: City of Marion Project number:
Collection date: 5-Mar-19
Date received: 5-Mar-19
Sample identification: CC Sludge - Grab Sample number:
190305.564
166486
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Arsenic - TCLP
6010 C
<0.25
0.25
mg/L
18-Mar-19
LMC
1
Barium - TCLP
6010 C
<2.50
2.50
mg/L
18-Mar-19
LMC'
1
Cadmium -TCLP
6010 C
<0.05
0.05
mg/L
18-Mar-19
LMC
1
Chromium - TCLP
6010 C
<0.25
0.25
mg/L
18-Mar-19
LMC
1
Lead - TCLP
6010 C
<0.25
0.25
mg/L
I8-Mar-19
LMC
1
Selenium - TCLP
6010 C
<0.25
0.25
mg/L
18-Mar-19
LMC
1
Silver - TCLP
6010 C
<0.10
0.10
mg/L
18-Mar-19
LMC
1
Mercury - TCLP
7470A
<0.0020
0.0020
mg/L
20-Mar-19
TLT
1
Full Scan TCLP Organics
See attached sheets
1,2
Reactive Cyanide
335.4
<0.049
0.049
mg/kg
18-Mar-19
ECHEM
2
Reactive Sulfide
SM 4500 S D
4.04
0.1
mg/kg
21-Mar-19
ECHEM
2
Ignitability
SW 846 1010
>210
210
OF
20-Mar-19
ECHEM
2
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analzyed by Rogers & Callcott Environmental.
2. Sample analyzed by Enviro Chemists, Inc.
Date reviewed: 03z 7a
Data reviewed by: .Kelley E. Keenan
Signature:
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc:
The results in this report relate only to the samples submitted for analysis.

Rogers & callcott
ENVIRONMENTAL
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Dear Client:
Laboratory Report
Project:
Work Order:
Received:
Marion W WTP
9030366
03/06/2019 14:40
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on March 06, 2019, Rogers and Callcott maintains a formal QA/Q.0 program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the TNI standard The analyses met the QA/QC confidence
interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. ,
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by
mistake, please notify Rogers and Callcott immediately,
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at amy.ashley@rogersandeallcott,com or
(864)-335-4962 if you have any questions about this report.
Report Approved By:
0/?, �' %'WY
Amy Ashley
Project Manager
This report ma), not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.
PO Box 5655 1 Greenville, SC 29606 1 426 Pairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandeallcott.com
an employee -owned company
Page 1 of 19

tl-
Rogers &Callcott
AEI rl ENVIRONMENTAL
Certificate of Analysis
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Sample Number Sample Description
9030366-01 Marion WWTP Sludge - Grab
South Carolina Greenville Laboratory Identification 23105
South Carolina Columbia Laboratory Identification 40572
North Carolina Laboratory Certification Number27
North Carolina Drinking Water Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
Georgia Drinking Water Lab ID 880
Project: Marion WWTP
Work Order: 9030366
Received: 03/06/2019 14:40
Matrix Sampled Type
Sludge 03/05/19 08:17 Grab
PO Box 5655 1 Greenville, SC 29606 1 426 Fnirforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax B64.232.614o rogersandcallcott.com
an employee -owned company
0312212019 09:39 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 2 of 19

Rogers &Callcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Marion WWTP
351 Depot St. Work Order: 9030366
Asheville, NC 28801-4310 Reported: 03/22/19 09:39
Sample Data
Sample Number 9030366-01
Sample Description Marion WWTP Sludge - Grab collected on 03/05/19 08:17
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
TCLP Metals
Mercury
ND
0.0020
mg/L
10.0
03/20/19 11:09
EPA 7470A
TLT
B9C0800
Arsenic
ND
0.25
mg/L
5.00
03/18/19 17:44
EPA 6010D
LMC
B9C0624
Barium
ND
2.50
mg/L
5.00
03/18/19 17:44
EPA 6010D
LMC
B9C0624
Cadmium
ND
0.05
mg/L
5.00
03/18/19 17:44
EPA 6010D
LMC
B9C0624
Chromium
ND
0.25
mg/L
5.00
03/18/19 17:44
EPA6010D
LMC
B9C0624
Lead
ND
0.25
mg/L
5.00
03/18/19 17:44
EPA6010D
LMC
B9C0624
Selenium
ND
0.25
mg/L
5.00
03/18/19 17:44
EPA 6010D
LMC
B9C0624
Silver
ND
0.10
mg/L
5.00
03/18/19 17:44
EPA6010D
LMC
B9C0624
TCLP Volatile Organics
Benzene
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
2-Butanone (MEK)
ND
0.200
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
Carbon tetrachloride
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
S JAR
B9C0600
Chlorobenzene
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600 '
Chloroform
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
1,2-Dichloroethane
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
1,4-Dichlorobenzene
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
1,1-Dichloroethene
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
S JAR
B9C0600
Tetrachloroethene
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
Trichloroethene
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
Vinyl chloride
ND
0.100
mg/L
50.0
03/13/19 20:16
EPA 8260B
JAR
B9C0600
Surrogates
%REC
%REC Limits
Flag
1,2-Dichloroethane-D4
97
70-130
Toluene-D8
104
70-130
4-Bromo luorobenzene
121
70-130
TCLP Semi -Volatile Organics
2-Methylphenol (o-Cresol)
ND
0.100
mg/L
50.0
03/18/19 12;08
EPA 8270D
RJM
B9C0546
3/4-Methylphenol(m,p-Cresol)
ND
0,100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
total Cresol
ND
0.200
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
2,4-Dinitrotoluene
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
Hexachlorobenzene
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
Hexachlorobutadiene
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
Hexachloroethane
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
Nitrobenzene
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
139C0546
PO Box 5655 1 Greenville, SC 29606 1 426
Fairforest Way
I Greenville,
SC 29607 1
main 864.232.1556 1 fix 864.232.6140
rogersandcallcott.com
an employee -owned company
0312212019 09:39 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 3 Of 1 J

*t.Rogers &Callc®tt
ta ENVIRONMENTAL
Environmental Testing Solutions Project: Marion WWTP
351 Depot St. Work Order: 9030366
Asheville, NC 28801-4310 Reported: 03/22/19 09:39
Sample Number 9030366-01
Sample Description Marion W WTP Sludge - Grab collected on 03/05/19 08:17
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
TCLP Semi -Volatile Organics
Pentachlorophenol
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
Pyridine
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
2,4,5-Trichlorophenol
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
2,4,6-Trichlorophenol
ND
0.100
mg/L
50.0
03/18/19 12:08
EPA 8270D
RJM
B9C0546
Surrogates
%REC
%REC Limits
Flag
Nitrobenzene-D5
46
15-314
2-Fluorobiphenyl
45
32-118
2-Fluorophenol
38
20-110
Phenol-D5
41
8-424
2,4,6-Tribromophenol
59
39-130
Terphenyl-D14
98
26-173
TCLP Pesticides
Gamma-BHC (Lindane)
ND
0.00050
mg/L
10.0
03/19/19 13:22
EPA 8081B
RICH
B9C0686
Chlordane
ND
0.0050
mg/L
10.0
03/19/19 13:22
EPA8091B
RICH
B9C0686
Endrin
ND
0.00050
mg/L
10.0
03/19/19 13:22
EPA8081B
RICH
B9C0686
Heptachlor
ND
0.00050
mg/L
10.0
03/19/19 13:22
EPA8081B
RICH
B9C0686
Heptachlor epoxide
ND
0.00050
mg/L
10.0
03/19/19 13:22
EPA8081B
RKH
B9C0686
Toxaphene
ND
0.0050
mg/L
10.0
03/19/19 13:22
EPA8081B
RICH
B9C0686
Methoxychlor
ND
0.00050
mg/L
10.0
03/19/19 13:22
EPA8081B
RICH
B9C0686
Surrogates
%REC
%REC Limits
Flag
2,4,5,6-Tetrachloro-m-xylene
100
60-130
Decachlorobiphenyl
98
30-150
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way i Greenville, SC 29607 1 main 864.232,1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
0312212019 09:39 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 4 Of 19

Environmental Testing Solutions, Inc. Date of Report: Mar 21, 2019
Post Office Box 7565 Customer PO #:
Asheville NC 28802 Customer ID: 08100.055
Attention: Kelley Keenan (ETS) Report #: 2019-03789
Project ID: Marion WWTP
Lab ID Sample ID: Marion WWTP
p Collect Date/Time Matrix Sampled by
19-09573 Site: Sludge 3/5/201'9 8:17 AM Solid/Sludge Client
Test Method Results Date Analyzed
Cyanide
EPA 335.4
<0.049 mg/kg
03/18/2019
Sulfide
SM 4500 S D
4.04 mg/kg
03/21/2019
Flash Point
SW 846 method 1010
>210 OF
03/20/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.003 mg/L
03/18/2019
2,4-D (TCLP)
SW848 Method 8151A
<0.003 mg/L
03/18/2019
Comment:
Reviewed by:
Report #:: 2019-03789 Page 1 of 1

X
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature.
Dissolved Oxygen Level
8.06
. 7, 96
7.71
7.52
7.37
7.26
6.96
6.75
6.57
6.36
6.18
6.01
5.85
5.65
5.47
5.27
Cor ening Creek
WQ 0019960
3/19/2019
10
3/19/19 0804
TH
3/19/19 0928
TH
1000
0.8
25
25
Slope: 0.2
Intercept: 8.1
Correlation Coefficient: 1.0
nilliliters
/o Dry Solids
iegrees Celsius
iegrees Celsius
Oxygen Uptake Rate: 11.37 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.42 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 1.111 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically,

Oxygen Uptake Rate Chart v--0-1894X+8.2945.
9
8
c
7
6
on
to 5
a
x
O
a
> 4
o
H
3
2
1
0
1 2 3 4 5 6 7 8 9
10 11 12 13 14 15 16
Time (minutes)
-31111�--A9

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15'
Facility Name: Cor enin Creek
Bicsolids Permit Number: WQ 0019960
Date: 3/20/201
Digester Temperature: 1
Sampling Date/Time: 3/20/19 0613
Sampled By: TH
Analysis Date/Time: 3/20/19 0739
Analyzed By: TH
Sample Volume: 100(
Total Solids: 0 E
Beginning Temperature: 2E
End Temperature: _ 25
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
0.2
7.9
1.0
'milliliters
% Dry Solids
degrees Celsius
degrees Celsius
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate: 11.mg Oxygen/ /
Average Temperature; .71 mg Oxygen/ghr
25 degrees Celsius
Temperature Correction Factor:
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:
1.34 mg Uygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and, the Spreadsheet execute automatic
ally.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Method: SM 2710 13-2011
Date: 3/20/2019
Time Sampled: 0613
Sampled By: TH
Time Started Aeration: 0619
Time Stopped Aeration: 0737
Time Analyzed: 0739
Analyzed By:TH
Total Time of Test: < 2 hrs, ( 1 hour 41 mins
Total time of test includes the time sample was aerated.

E
tto
0
W
0
4
V1
0.
in.
3
2
i
Oxygen Uptake Rate Chart Y = -0.2277x + 8.1245
' a y 10 11 12 13 14 15 16 I
Time (minutes)
r

11 s
CITY OF MARION
CORPENING CREEK WASTE TMTMENT PLANT LABORATORY
tsl Solids. Itn Solid and:3®rrt160,11d Samples.
—Dried
at 103"106°C
n-dRrd MGthbde--# 2640 0-2011
N.DATE:
4LYST. f� /2yv
TIME.)N: U
TEMP IN: 103 -C
TIME.OUT:
Time Weighed
TEMP OUT:/Dx °C
// 15-0
B
APCE .. DA San1A A. Dis
ID COLLECT Vci. WT.
C. q A.- B.
Dish + D +;Res'=
C.- B C - B
!Residue
MO
Wet I9mPle Driod ResidueightWei
-M(3
ht ToML.
Solids
MGMG
MG
Weight ordried res{due *.dish, my;
weight of dish,
Weight of. Wet sample + dish, mg
Total S011de a �
Oggcum-
! ��
o

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Corpenin Creek
Biosolids Permit Number WQ 0019960
Date: 3/21/2019
Digester Temperature: 12
Sampling Date/Time: 3/21
Sampled By: TH
Analysis Date/Time: 3/21
Analyzed By: TH
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9
AT 82 . Dry Solids
25 degrees Celsius
25 degrees Celsius
Slope: 0.3
Intercept: 8.0
Correlation Coefficient: 1,0
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate: 15.1.86 mg Oxygen/ /
Average Temperature: mg Oxygen/ghr
25 degrees Celsius
Temperature Correction Factor:
0,783526166
Temperature Corrected Specific Oxygen Uptake Rate:
1.46 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically.
Y

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Method: SM 2710 B-2011
Date: 3/21/2019
Time Sampled: 0552
Sampled By: TH
Time Started Aeration: 0600
Time Stopped Aeration: 0715
Time Analyzed: 0719
Analyzed By:TH
Total Time of Test: < 2 hrs. ( 1 hour 42 mins
Total time of test includes the time sample was aerated.

E
X
0
-0
q
0
V1
ca
w
3
2
n
31--vlly
Oxygen Uptake Rate Chart y = -0.2547x + 8.212
O y 1u 11 12 13 14 15 16
Time (minutes)

CITY OF MARION
CORPENINQ: CREEK`WA STE TREATMENT PLANT LABORATORY
9otida: In'9alld end 3emtsolld 3amples�.Drled::ai
103.106°C
anti �Asthoda-.�. Z64p 0=�011
;;
>ATE: j—Z % (°
'
(ST:� /��
TIME IN: 66
TEMP IN: /Q3 oC
TIME OUT:. /0 5-
Tlme•Weighed:
TEMP'OUT: /0� °C
B ,c
COLLECT s ple Dish Dlsh�+
D e :+ A -B
.Res : ue: � -
...C' B �C B�
RN
M VVetsa V19.
MO MO
Dried:�esidue We At
8
MO
due' Tote
welt Solids
j /08
MQ.
MG
S
.x
75,, 5
57q�
% T wegnt of dried re'sldue +:dish, mg; T
B we(yht of dish,
C weOt Of.wst:eamPle + dish, mg
Total Solids a LAZALXILO

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Corpening Cr
Biosolids Permit Number: WQ 0019960
Date: 3/221
Digester Temperature:
Sampling Date/Time: 3/22/19 063
Sampled By: TH
Analysis Date/Time: 3/22/19 080
Analyzed By: TH
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
1000 milliliters
0.84 % Dry Solids
25 degrees Celsius
25 degrees Celsius
0.3
7.2
1.0
J
A
Oxygen Uptake Rate: 15.38 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.83 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.78352616E
Temperature Corrected Specific Oxygen Uptake Rate:
1.43 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N,C.
Method: SM 2710 B-2011
Date: 3/22/2019
Time Sampled: 0634
Sampled By: TH
Time Started Aeration: 0641
Time Stopped Aeration: 0805
Time Analyzed: 0808
Analyzed By:TH
Total Time of Test: < 2 hrs, ( 1 hour 49 mins
Total time of test includes the time sample was aerated.

Oxygen Uptake Rate Chart
Y =-0.2563x -r- 7.4693
,i 15 16
.3/zz/,f

CITY OF MARION.
CORP.JINGEr * i '
, :CREE,K'WASTE TREATMENT PLANT LABORATORy i
103"706°C
2540 .0-2011
R.
N.DATE:
YST.
TIMaIN:
TIMEDUT:
TEMP 0-3
TEM 0
-C
-C
.11mlif-Wilghed:
�$WP—LE
ID
COLLECT
--Ta—Mple
vol.
ML.
B
Dls7_1r18h
WT,
c
'+ .
-is
Wet MWO
A A -8
. Dish: -
... :+ * - Rft Us
DrWd.R"Idue W61911J:
C.. 8
X100
C-13
% Iota
-ROB due
mo
----
MG
Welght
'MG
Solids
. . ........
. . ....... . .... .. ........
I
3
3, ILI
--------
#,I
t5l
If.
le
q �
6L
f6g, 0
-------
A*T-Welght 0fdnetreeldug -r.uien, mg;
T.-Wolght of dish,
wei0ht Of wet sample * dish, rrig
fib Total'sollft a C - S100
i

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14.
15
Specific Oxygen Uptake Rate
. SOUR
Facility Name: Corpening Creek
Biosolids Permit Number: WQ 6019960
Date: 3/26/2019
Digester Temperature: 13
Sampling Date/Time: 3/26/2019 0620
Sampled By:
Analysis Date/Time:
Analyzed By'
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
-z64 07V�
I
1000 milliliters
0.86 % Dry Solids
25 degrees Celsius
25 degrees Celsius
Slope: 0.3
Intercept: 7.8
Correlation Coefficient: 1.0
i
Oxygen Uptake Rate: 15.22 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate;
Average Temperature: 1,77 mg Oxygen/g/hr
Temperature Correction Factor: 25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:
1.39 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute 'automaticall . .
I y

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C,
Method: SM 2710 B-2011
I
Date: 3/26/2019
Time Sampled: 0620
Sampled. By: TH
Time Started Aeration: 0625
Time Stopped Aeration: 0742 !
Time Analyzed: 0744 j
Analyzed By:TH
Total Time of Test: < 2 hrs. ( 1 hour 39 mns. )
Total time of test includes the time sample was aerated.

9
8
7
6
E
c
m 5
an
X
X
'a
d
4
O
3
2 -
1 2 3 4
S/20 9
Oxygen Uptake Rate Chart
y = -0.2537x + 8.0372
5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

IV p
CITY: OYMARION
CORPENING-CREEK ,WASTE TREATMENT PLANT LAIBORATORy
*Soflds: 1wealld and -:'S9ml50IId-Sample- - —Drl',.0 d ai-10t.-.106o'd
ndardMothods-4 264O.G4'011
4PATE: 2-6
kL..y 8 . T.; TIME-IM Z—
TIME OUT,
TIM8--Wi-196d;
B (3(
7
PiPLE �AT C
A A-B
�1PIe Dish
ID COLLECT Vol. WT. .,.Dieh+ Dial
Wet#MPIO Dded;R,
IVIL. ma
U
k z(? 50' A
62, 5�52-
qq, 6�g-2
5,5
� of
-T ;�t�';dish,
rGsIdue +-dish, mg;
weight Of-w9t BRMPIO + dish, mg
Total solids = L6zB)-x=
C-;B '
Sm
IN: ( 6 3 PC
OUT:/ e-I oc
fA-8) X I Do
C-B
eaidue Total
Velghf solids
MG

r
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10'
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature;
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Corpening Creek
WQ 0019960
3/27/2018
13
3/27/19 0614
TH
3/27/19 0743
TH
1000
0.88
25
25 c
0.3
7.8
1.0
nilliliters
io Dry Solids
legrees Celsius
legrees Celsius
Oxygen Uptake Rate; 15.25 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.73 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate;
1.36 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execut automatically.

0
D.
7
3
2
Col
Oxygen Uptake Rate Chart y =-0.2542x + 8.0835
1 2 3 4 5 -6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Method: SM 2710 B-2011
Date: 3/27/2019
Time Sampled: 0614
Sampled By: TH
Time Started Aeration: 0620
Time Stopped Aeration: 0738
Time Analyzed: 0743
Analyzed By:TH
Total Time of Test: < 2 hrs. ( 1 hour 44 mi'ps
Total time'of test includes the time sample was aerated.

I
CITY OF AfARION
T 4®I $oltcia: Cop-PENINGI C
tn:8011dl"d;g®mtsolltl sam los-
9XI �'AS.T>� r TMENT PLAN LABO
A � Z p 1)66d at 103� o TOItY
C�1011 10fi C
TIME
7'lMSObT; 1p gs--- TEM�+ IN: 1�03 'C
PLfTIme-Wstghed; TEMt,-CUT;. 'C
3 A . Sam B C
ID COLLECT I
p e.
Vol, Dieh Dlsh'+ Da AA '
ML, MO Wet;eample Dried. Residue ""due . Residue
If nk fWt3. M0 Weight VN Total
f1itG I Sollds ":a:
s16d
eYg,F3 ,�r
y 73
�f l • 00�L Z
`{ z Zt
R 1 Wefgfrt of dried MOIdus - dish, Mb;
j weight of dish,
1 Vml ht of wet sample + dish, mg -„
i
Total Solids
I '
t ,
I

m 4
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: CorpeniE3/2q812
Biosolids Permit Number: WQ 001
Date;
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9
01
E
000 milliliters
0.9 % Dry Solids
25 degrees Celsius
25 degrees Celsius
Slope: 0.3
Intercept: 7.9
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 15.06 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
Average Temperature: 1.67 mg Oxygen/g/hr
Temperature Correction Factor: 25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:
1.31 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute; automatically,
y

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Method: SM 2710 B-2011
Date: 3/28/2019
Time Sampled: 0631
Sampled By: TH
Time Started Aeration: 0637
Time Stopped Aeration: 0752
Time Analyzed: 0755
Analyzed By:TH
Total Time of Test: < 2 hrs. ( 1 hour 39 mins
Total time of test includes the time sample was aerated.

Dissolved Oxygen (mg/1)
O N W Ln
0) V 00 if
N
I
N
1
I
W
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I
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CITY OP IVIARION
CORPENING .CREEK WASTE TREATMENT PLANT LAIJORATORY
tal Solids: In Soldd and 9emisoll4 62.mplas—D1lod at 703-106°C
ndRM Methods--# 2540 Qs2011
TIME, IN: C) 6 TEMP -IN: C63 �p
TIMEO.UT: j D0 TEMP OUT: /03 0c }:
Time Welgheid:�///
4PLE ° A . A q .:g. lA-B
lb COLLECT Sample D s Dlah + C ' B . B
Vol, WT. D eh,+ Residue Residue
ML. Wet sample Drl�diResidue Wel�ht. Wei ht Tod
k ... MG M0. -Me MG MO Solids
G953 �
I
weight of driedxesidue +:d— (ep�
Weight of dish,
weight of wet sample + dish, mg
Total soil" =

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SL015586
Client:
Brian Kay
Advisor: Zach Key
Predictive
980 ArI s Lane
Y
Southern Soil Builders,
iY
(J€'� r cx7:*), n'��
,
Soil Mehlich-3 Extraction
Report
Tryon, NC 28782'
Inc.
958 Hoots Rd
, 3
y
Sampled County: McDowell
Roaring River, NC 28669
Links to Helpful Information
Sampled:11/07/2019
Received: 11/12/2019 completed: 12/03/2019
Farm:
Client ID' 504558
Advisor ID: 231531
Sample ID: R1
Recommendations: Lime -
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.1
120-200 0
80
0 0 0
0
0 0
Note: 12
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH P-1 K-I
Ca% Mg% S-1
Mn71
Mn-All Mn-AI2 Zn-I
Zn-AI
cu-I Na ESP SS-1 NO3-N
0.60 0.91 7.9
74 2.1 5.3 114 29
54 18 51
98
76 244
244
221 0.1 1
Sample ID: R2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 0
80
0 0 0
0
0 0
Note: 12
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC
BS% Ac pH P-1 K-I
Ca% Mg% S-1
Mn-1
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.56 0.86 10.0
88 1.2 6.3 160 31
62 25 51
103
75 245
245
244 0.1 1
North Carolina
4�'+i,�,lR(t,;A Y:fit:'�a i'4t."€l ti„SbX;SIt3vkS4�3i�;
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SLO15586
Brian Kay
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of.
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
Mg%
%CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-AI2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-1
manganese index
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
M-O
mineral -organic soil class
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
N
nitrogen
ncaqr.gov/agronomi/pubs_htm.
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr..qov/agronomi/obpart4.htmVf#sfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaargoy/agronom%/uyrst.htm

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SI-015585
Client:
John Fisher
Advisor: Zach Key
l "
Predictive
400 Dairy Rd.
Southern Soil Builders,
y
Soil, Report Mehlich-3
Extraction
Maggie Valley, NC 28751
Inc.
958 Hoots Rd
Sampled County: McDowell
Roaring River, NC 28669
Links to Helpful Information
Client ID: 478472
Advisor ID: 231531
Sampled: 11/07/2019
Received: 11/12/2019 Completed: 12/03/2019
Farm:
Sample ID: F3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.9
120-200 0
10
0 0 0
0
0 0
Note: 12
2- 0.0
Test Results [units - WIV in g/cm 3 ; CEC and Na in meq/100 cm3; NO3-N in mg/dM3]:
Soil Class: Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.81 0.93 7.9
75 2.0 5.5 139 75
47 23 60
293
193 261
261
297 0.1 1
Sample ID: F4
Recommendations: Lime
— --
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu B
Information
Lime History:
I -Fescue/OGrass/Tim, M 0.0
120-200 0
100
0 0 0
0
0 0
Note: 12
2- 0.0
Test Results [units - WN in g/cm3 ; CEC and Na in meq/100 cm3; NO3-N in mg/drn 3
Soil Class: Mineral
HM% WIV CEC
BS% Ac pH P-1 K-1
Ca% . Mg% S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.56 0.92 7.8
85 1.2 6.1 63 21
58 25 39
159
111 184
184
351 0.1 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture ,

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SLO15585
John Fisher
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report
Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg°°
%CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
M-0
N
mineral -organic soil class
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
nitrogen
sodium
nca.qr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.html nd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume .
0 o
The first seven values [soil class, HM /°, WN, CEC, BS /°, Ac and pH] describe the soil and its degree of acidity. The -
Zn-AI
zinc availability index
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm

V4 W ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Marion
WWTP Name: Corpening Creek
Monitoring Period: From 1/1/2019 To
WQ Permit Number:
NPDES Number:
12/31 /2019
WQ0019960
NCO031879
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Performed:
Class A:
Alt. A (time/temp) C1
Alt B (Alk Treatment)®
Alt. C (Prior Testing)E]
A t.D (No Prior Test) 11
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 11
Heat Drying D
1 Heat Treatment ❑
Thermophilic (�
Beta Ray 11
Gamma Ray k
Pasteurization CI
Class B:
Alt. (1) Fecal Density 21
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 11
Air Drying C
Composting El
jAerobic Digestion LJ
Anaerobic s on171
obi Di e ti
g
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
y
Number o
Exceg
Bencee-
Frequency
of Analysis
Sample
Type
na ytica
Tech-
ni ie
MinimumGeo.
Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
846
883.95
900
MPN
0
7
grab
sm9221
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
vector Attraction 1eduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.I (VS reduction) D
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench)
Alt. 4 (Spec. Oz uptake) 21
Alt. 5 (14-Day Aerobic) Q
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying- Stable) C
jAlt. 8 (Drying- Unstable) Cl
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) Q
No vector attraction reduction alternatives were performed . ® .
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Prepay r Name and Title (type or print)
Z-!D -ZD ZJ
4g�e Preparer* Date
Dennis Key Southern Soil Builders, Inc.
Land Applier Name and
�Title (if applicable)(type or print)
jQ
/ Zr Y PAN-� dy(;
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)