WQ0037094_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Residual Annual Report
what is the submittal r Additional Information
type? * r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:
Project Number* WQ0037094
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Rob Willcox
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0037094
Applicant\Permittee * Howard Fertilizer Company, Inc.
Facility Name * Howard Fertilizer Company DCAR
Phone Number*
3363399128
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Howard Fertilizer 2019 Annual Report
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
Howard Fertilizer - 2019 ANNUAL REPORT
21.61 MB
WQ0037094. pdf
Upload only 1 RDF docurrent. Miltiple docurrents rust be corrbined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/17/2020

2019 ANNUAL REPORT
HOWARD FERTILIZER COMPANY, INC.
DISTRIBUTION OF CLASS A MUNICIPAL
WASTEWATER TREATMENT PLANT RESIDUALS
NON -DISCHARGE PERMIT #WQ0037094
Prepared For:
Howard Fertilizer Company, Inc.
8306 South Orange Avenue
Orlando, Florida 32809
Compiled By:
Willcox & Mahe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
February 2020

willcoX&'l abe
SOIL SOLUTIONS
February 14, 2020
N.C. Department of Environmental Quality
Division of Water Resources — Non -Discharge Branch
512 N. Salisbury Street, 0 Floor, Office # 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Branch
Reference: 2019 ANNUAL REPORT
Howard Fertilizer Company, Inc.
Non -Discharge Permit No. WQ0037094
WMSS Project No. 15-07, Phase: 06
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit for Howard Fertilizer Company,
Inc. (Howard Fertilizer) on behalf of Howard Fertilizer. WMSS compiled this report using
data provided by Howard Fertilizer. This data includes: 1) Class A Annual Distribution of
Marketing / Surface Disposal Certification and Summary Form, 2) Annual Residual
Sampling Summary Form, 3) Annual Pathogen and Vector Attraction Reduction Form
(503), and 4) Analytical Data.
Howard Fertilizer distributed 1,167.85 Total Dry Tons of blended fertilizer and South Cross
Bayou WRF pellets in North Carolina under Permit No. WQ0037094 during the 2019
calendar year.
If there is any further information required or questions regarding this distribution program
please do not hesitate to contact Mr. Michael Brooks, Corporate Compliance Officer (407)
466-2960 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Rob Willcox, L.S.S.
Soil Scientist
Enclosure(s)
cc: Howard Fertilizer Company, Inc.
Shared\WMSS Projects\2015\15-07 Howard Fertilizer\Phase 06 - 2019 Annual Report\2019 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, INC 27358 / Rob 336.339.9128 or
Martin 336.312.1396 / www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Class A Distribution and Marketing / Surface Disposal
Certification Summary Form
Form DMSDF
II Annual Residual Sampling Summary Form
Form RSSF
III Annual Pathogen and Vector Attraction Reduction Form
(503 Rules)
Form PVRF 503
IV Lab Sheets
Analytical Data

Class A Distribution and Marketing / Surface Disposal Certification
Summary Form
FORM DMSDF

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: W00037094 FACILITY NAME: _ Howard Fertilizer Company, Inc. / South Cross Bayou WRF Pelletizing Facility
PHONE:[phone] COUNTY: Statewide OPERATOR: N/A
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
p Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar vear? Yes p No ❑ —► If No skip parts A, B, C and certify form below
Part A*:
Part B*•
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons
Recipient Information
Amendment/
Bulkina Aeent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
South Cross Bayou WRF Pelletizing Facility
1,167.85
Class A Residuals utilized
1,167.85
Fertilizer
February
(Fertilizer)
(Pellets)
(Blended Product)
for Distribution during 2018
March
April
May
June
Jul
August
September
October
November
December
Total from FORM DMSDF (sir)
0
0
0
0
Totals: Annual (dry tons):
0
0
1,167.85
1-167.85
Amendments) used: I
Bulking Agent(s) used:
if more space is required_ attach admtionai information sheets (FURM DMSDF (supp)): Total Number of Form DMSDF (Supp)l
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit p yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"1 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are
significant penalties for information, including the possibility of fines and imprisonment for knowing violations."
N/A N/A
Signature of ermittee ateZd Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

Annual Residual Sampling Summary Form
FORM RSSF

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0037094 Laboratory:
Facility Name: Howard Fertilizer Company, Inc. (Permittee)
Residual Source WQ # or N/A - Florida Permit
NPDES #:
WWTP Name: South Cross Bayou WRF Pelletizing Facility
Residual Analvsis Data
1) Pace Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Com osite Date
1/3/19
1/3/19
1/3/19
4/2/19
4/2/ 19
4/2/19
7/2/19
7/2/19
712/19
10/2/19
10/2119
10/2/19
Percent Solids (%)
NA
93.3
93.3
93.3
92.9
92.9
92.9
92.0
92.0
92.0
93.2
93.2
93.2
Arsenic
75
4.6
4.6
4.6
3.7
3.7
3.7
5.9
5.9
5.9
10.0
10.0
10.0
Cadmium
85
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.2
1.5
1.5
1.5
Copper
4,300
569
569
569
499
499
499
595
595
595
580
580
580
Chromium
NA
38.7
38.7
38.7
1 39.6
39.6
39.6
34.1
1 34.1
34.1
1 41.6
41.6
41.6
Lead
840
18.9
18.9
18.9
16.6
16.6
16.6
14.9
1 14.9
14.9
17.8
17.8
17.8
Mercury
57
0.24
1 0.24
0.24
0.42
0.42
1 0.42
0.24
0.24
0.24
0.46
0.46
0.46
Molybdenum
75
13.1
13.1
13.1
11.8
11.8
11.8
10.6
10.6
10.6
12.1
12.1
12.1
Nickel
420
22.0
22.0
22.0
21.4
21.4
21.4
25.3
25.3
25.3
41.4
41.4
41.4
Selenium
100
2.6
2.6
2.6
4.9
4.9
4.9
4.2
4.2
4.2
4.7
4.7
4.7
Zinc
7,500
668
668
668
700
700
700
708
708
708
756
1 756
756
Total Phosphorus
NA
34,000
34,000
34,000
30,700
30,700
30,700
35,300
35,300
35,300 1
33,900
33,900
33,900
TKN
NA
40,100
40,100
40,100
45,000
45,000
45,000
50,800
50,800
50,800
48,700
48,700
48,700
Ammonia -Nitrogen
NA
1,160
1,160
1,160
1,920
1,920
1,920
1,940
1,940
1,940
1,910
1,910
1,910
Nitrate and Nitrite
NA
1 6.1 1
6A
6.1 1
5.0
5.0
5.0
7.0
7.0
7.0
6.9
6.9
6.9
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false info mati including the possibility of fines and imprisonment for knowing violations"
* Permitte (Howard Fertilizer).:'.-_�
Signature of Preparer * Datte
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 IO2 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: W00037094 Laboratory:
Facility Name: Howard Fertilizer Company, Inc. (Permittee)
Residual Source N/A - Florida Permit
NPDES # or WQ#:
W WTP Name: South Cross Bayou WRF Pelletizing Facility
Residual Aualvsis Data
1) Pace Analytical
2)
3)
4)
5)
Sam le or Composite Date
Parameter
(mg/kg)
1/3/19
113/19
1/3/19
4/2/19
4/2/19
4/2/19
7/2/19
7/2/19
7/2/19
10/2/19
10/2/19
10/2/19
Aluminum
28,300
28,300
28,300
28,300
28,300
28,300
28,300
28,300
28,300
28.300
28,300
28.300
Calcium
35,200
35,200
35,200
32,400
32,400
32,400
31,100
31.100
31.100
33,600
33,600
33,600
Magnesium
6.160
6,160
6,160
6.270
6,270
6,270
6,140
6,140
6,140
6,320
6,320
6,320
pH
6.9
6.9
6.9
6.9
6.9
6.9
6.8
6.8
6.8
7.0
7.0
7.0
Potassium
2,610
2,610
1 2,610
2,620
1 2,620
2,620
1 2,510
2,510
1 2,510
2,710
1 2,710
2,710
Sodium
1,430
1,430
1.430
1,430
1,430
1,430
1,240
1,240
1,240
1,330
1,330
1,330
SAR
1.78
1.78
1.78
1.83
1.83
1.83
1.61
1.61
1.61
1.68
1.68
1.68
PAN
12,268.1
12,268.1
12,268.1
13,889.0
13,889.0
13,889.0
15,635.0
15,635.0
15,635.0
14,998.9
14,998.9
14,998.9
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting (false information, including the possibility of fines and imprisonment for knowing violations."
* Pennitte (Howard Fertilizer)
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

Annual Pathogen and Vector Attraction Reduction Form - (503 Rules)
FORM PVRF 503

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
FacilityName: Howard Fertilzer Company, Inc. (Permittec) WQ Permit Number: W00037094
WWTP Name: South Cress Bayou WRF Pelletizing Facility NPDES Number:
Monitoring Period: From 1/12019 To 3/312019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 El
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Corn st ❑ Heat Drying 0 Heat Treatment ❑ Thermo hilic ❑
Beta Ra ❑ Gamma Ray❑ Pasteurization ❑
Class B: Alternative 1 ❑ Altemmive 2 ❑
If applicable to alternative pe formed (Class B only) indicate "Process to Significaotl Reduce Pathogens":
Lime Stabilization ❑ Air D in ❑ Com sting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative perffformed
(Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
l umxro
Excee-
Frequency
of Mal
Analysis
Sample
Type
" rein
Tech.
Minim
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weiehn
Salmonella bacteria
(in lieu of kcal
WHOM)
3 MPN per 4 grams
I total solid (dry
weight
Vector Attraction Reduction (40 CFR 50333) - Please indicate option performed:
AI61 (VS reduction) ❑
AIL 2 (40-day bench) ❑
JAIL 3 (30day bench) ❑
AIL 4 (Spec. Os uptake) ❑
AIL 5 (14-Day Aerobic) ❑
AIL 6 (Alk. Stabilization ❑
jAlt 7 (Drying - Stable) ❑
AIL 8 (Drying - Unstable) El
AIL 9 (Injection) ❑
JAIL 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met"
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met" (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
militant pen,,Iryes for false cgrtificati9n including fine and imprisonment"
Ie- Pe Et�13 /oward��'Yly�CtCrnC2
* Permute (Howard FertiliurY N/A
P,_r� r N viand pe or prinQ Land Applier Name and Title (if applicable)(type or print)
2 /7 N/A
Signs ure of- reparery Plate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (1212006)

ANNUAL PATHOGEN AND VECTORATTRACTION REDUCTION FORM (503 Rules)
FacilityName; Howard Fertilzer Company, Inc.(Permidee) WQ Permit Number: W00037094
W WTP Name: South Cross Bayou WRF Pelletizing Facility NPDES Number:
Monitoring Period: From 4/1/2019 To 6/30/2019
Pathogen Redaction (40 CFR 503.32) - Please indicate level achieved and alternative nerformed:
Class A:
Altemative 1 ❑ Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑ Alternative 5 O
Alternative 6 ❑
If a licable to alternative erformed (Class A only) indicate `Process to Further Reduce Pathogens":
Coat st ❑ Heat D in Q Heat Treatment ❑ 1 Thermo hilic ❑
Beta Rav ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alternative I ❑ Altemative 2 ❑
If applicable to alternative performed (Class B only) indicate `Process to Significantly Reduce Patbogens":
Lime Stabilization ❑ Air Dryin"❑ Com ostin ❑ Aerobic Dilicstion ❑
Anaerobic Digestion ❑
If applicable to
alternative performed (Class A or Class. B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
�
Pathogen Density
°1" fO
Frequency
of Anal sis
y
Sample
Type
" y'
Teeh-
Minimu
Geo. Mean
axim
Units
Fecal COliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight
Salmonella bacteria
(in lieu offecal
celdburn)
3 MPN per 4 grems
total solid (dry
weigh[
vector Attraction Keduction (40 CFK50333) -Please indicate option Derformed:
AltI (VS reduction) ❑
Alt 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt.4 (Spec. Or uptake) ❑
Alt 5 (14-Day Aerobic) ❑
JAR. 6 (Alk. Stabilization ❑
JAR 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) El
AIL 9 (Injection) ❑
jAlt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were perfbrmcd ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
s gnificant penalties for false certifiFation including fine and imprisonment"
l Pcrmtje (HoTvsfd Fcrfillrsr �L N/A
Prepmer Namc and Tit (type r print) .5 Land Applier Name and Title (if applicable)or print)
N/A
*Preparer is defined in 40 CFR Pad 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503(122006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
FacilityName: Howard Fertilzer Company, Inc. Mcninince) WQ Permit Number: W00037094
W WTP Name: South Crass Bayou WRF Pelletizing Facility T POES Number:
Monitoring Period: From 7/12019 To 9/302019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Altemative 1 ❑
Altemative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 EI
I Altemative 6 ❑
It ap licable to slternafive erformed (Class A only) indicate "Process to Further Reduce Pathogens":
Com ost ❑ HeatD in O Heat Treatment❑ Themto hilic ❑
Beta Ray❑ Gamma Ray❑ Pasteurization ❑
Class B: Alternative 1 ❑ Altemative 2 ❑
If applicable to alternative pe formed (Class B only) indicate `Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air D -n Com slip ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative pmWerformed
(Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in SludgeExcee-
Pathogen Density
u o
Frequency
of Anal sis
y
Sample
Type
` m y"
'fcch-
inim
Gen. Mean
maximu
Units
Fecal Coliform
ox lOwthe
fith power
per gram of
tow solids
MPN
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifarm)
3 MPN per 4 grams
total solid (dry
eight
Vector Attraction Reduction (40 CFR 50333) - Plane indicate option performed:
AILI (VS reduction) ❑
JAIL.2 (40-day bench) ❑
JAR. 3 (30-clay bench) ❑
Alt.4 (Spec- Or uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
JAIL 6 (Alk. Stabilization ❑
lAlt 7 (Drying - Stable) ❑ JAIt
8 (Drying - Unstable) W
Alt. 9 (Injection) ❑
JAIL 10 (Incorporation) ❑
jNo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met"
❑ 'rl certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met" (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
ifigant p& ies for jfej se ccertri-fiiccaattiion including fine and imprisonment"
V ` Permitte(Howard Fertiliurp 1r J N/A
Preparer nd Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1� � N/A
Signature o 'renarer' Date Sienature of land Amilier (if aoolicable) Date
-Preparcr is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T A 102 (26)
DENR FORM PVRF 503 (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION RE➢UCTION FORM (503 Rules)
FacilityName: Howard Fertilzer Company. Inc.(Permittee) WQ Permit Number: W00037094
W WTP Name: South Cross Bayou WRF Pelletizing Facility NPDES Number -
Monitoring PeriZ7 From 10/1/2019 TO 12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Altemative 1 ❑
Alternative 2 ❑
T Altemative 3 ❑
Alternative 4 ❑
Altemative 5 W
I Alternative 6 ❑
Ifa licable to alternative erformed (Class A only) indicate `Process to Further Reduce Palhoune:
Copt st ❑ HkD 'n 21 Heat Treatment❑ Thermo hilic ❑
Bcla Ray❑ Gamma Ray❑ Pasleuriyation ❑
Class B: I Alternative 1 ❑ Alternative 2 ❑
Ifapplicable to alternative performed (Class B only) indicate "Process to SiFmficandWE duce Pathogens":
Lime Stabilization ❑ Air D in Com Ostin ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
Ifapplicable to
alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
8
Pathogen Density
um o
Fxcee-
Frequency
of Anal si
y s
Sample
Type
yn`
Tmh-
9inimu
Gen. Mean
4laximu
Units
Fecal Coliforrl
2 x 10 to the
5th power
per gram of
total solids
tvlPN
CFU
1000 mpn per gram
of total solid (dry
weight
Salmonella bacteria
(in lieu of fecal
culifonn
3 MPN per grams
m solid (dry
wei= t
vector Attraction Keduchon NU CFK 503.33) - Please indicate option performed:
Alt.1 (VS reduction) ❑
jAlt 2 (40-day bench) ❑
jAlt. 3 (30-day bench) ❑
JAIL 4 (Spec. Or uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
IAIL 6 (Alk Stabilization ❑
jAlt7 (Drying -Stable) ❑
Alt 8 (Drying - Unstable) El
Alt. 9 (Injection) ❑
JAIL 10 (Incorporation) ❑
jNo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why von have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
sign(ti Ga(It pe #jig for ffa(e u .ificati l including fine and imprisonment."
�1 * Peermitte(QIIo-�Fd(Fertilizer) N/A
Pre r Name and Title (type or�hu) Land Applier Name and Title (if applicable)(type or print)
•Prepaner is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

Lab Sheets
ANALYTICAL DATA

HOWARD FERTILIZER
CLASS A
BIOSOLIDS ANALYSIS
Residual Type: Wastewater Treatment Plant(Pinellas)
Date Sampled: January 3, 2019
South Cross Bayou WRIT (1st Quarter 2019) Permit No. W00037094
Mineralization Rate 0.30 93.30 % Solids
6.9 pH
Parameter % Mg/Kg Dry Weight I Pounds/Dry Ton
(% x 10,000) (MOKa x 0.0021
:n(1KN)
4.010
40,100.000
80.200
orus
3.400
34,000.000
68.000
Wall
0.261
2,610.000
5.220
njected)*
1.285
12,848.100
25.696
urface)*
1.227
12,268.100
24.536
:liaNitrogen
0.116
1,160.000
2.320
n
3.520
35,200.000
70.400
n Carbonate Eq.
---
---
_-
dum
-
6,160.000
12.320
t
--
1,430.000
2.860
N / Nitrite N
---
6.100
0.012
le---
---
---
.um
---
28,300.000
56.600
---
4.600
0.009
lm
---
1.200
0.002
um
---
38.700
0.077
---
569.000
1.138
---
18.900
0.038
y
---
0.240
0.000
lenum
---
13.100
0.026
---
22.000
0.044
on
---
2.600
0.005
---
668.000
1.336
Pace Analytical 35439786
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
1.78
Ceiling Cancan,
(M"9)
75
85
4,300
840
57
75
420
100
7,500

aceAnalAcal
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January 14, 2019
William Reyes
Synagro
RE: Project: Pinellas County Pelletizer
Pace Project No.: 35439786
Dear William Reyes:
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 03, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cameron Meynardie
[e-mail]
[phone]
Project Manager
Enclosures
cc: Robert Ervin, Synagro
*460R)J500
I
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Project: Pinellas County Pelletlzer
Pace Project No.: 35439786
Ormond Beach Certification Os
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification* E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Pace Analytical Services, LLC
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Oldsmar. FL 34677
[phone]
CERTIFICATIONS
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate M 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification* FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TNO2974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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Oldsmar, FL 34677
[phone]
SAMPLE SUMMARY
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
Lab ID Sample ID Matrix Date Collected Date Received
35439786001 Pellet Solid 01/0311911:00 01103/1912:15
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
35439786001 Pellet EPA 8082
AER
9
PASI-O
EPA6010
JWP, LEC
18
PAS[-0
EPA 7471
AMS
1
PASI-O
ASTM D2974-87
NMP
1
PASI-O
SM 254OG
SA1
1
PASI-O
SM 254OG
SA1
1
PASI-O
EPA 9045
AGS
1
PASI-O
ASTM D5057
JDW
1
PASI-O
TKN-NH3 Calculation
AEM
1
PASI-O
EPA 350.1
CLL
1
PASI-O
EPA 351.2
JMD
1
PASI-O
EPA 353.2
AMP
2
PASI-O
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pellelizer
Pace Project No.: 35439786
Sample: Pellet
Lab ID:
35439786001
Collected:
0110311911:00
Received: 01/03/19 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8082 GCS PCB
Analytical
Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)
0.34 U
mg/kg
0.56
0.34
5
01/0411913:12
01/0511922:55
12674-11-2
J(M1),
J(R1),
P1
PCB-1221(Areclor 1221)
0.26 U
mg/kg
0.56
0.26
5
01104/1913:12
01105/1922:55
11104-28-2
P1
PCB-1232 (Aroclor 1232)
0.28 U
mg/kg
0.56
0.28
5
01/04/19 13:12
01/05/19 22:55
11141-16-5
P1
PCB-1242 (Aroclor 1242)
0.30 U
mg/kg
0.56
0.30
5
01/0411913:12
01/05/19 22:55
53469-21-9
P1
PCB-1248 (Aroclor 1248)
0.35 U
mg/kg
0.56
0.35
5
01/04119 13:12
01/05/19 22:55
12672-29.6
P1
PCB-1254 (Aroclor 1254)
0.22 U
mg/kg
0.56
022
5
01/04/19 13:12
01/05/19 22:55
11097-69-1
P1
PCB-1260 (Aroclor 1260)
0.34 U
mg/kg
0.56
0.34
5
01/04119 13:12
01/05119 22:55
11096-82-5
P1
Surrogates
Tetrachloro-m-xylene(S)
94
%
59-129
5
01/0411913:12
0110511922:55
877-09-8
Decachlorobiphenyl(S)
27
%
26-172
5
0110411913:12
01/05/19 22:55
2051-24-3
6010 MET ICP
Analytical
Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
4.6
mg/kg
3.5
1.7
1
0110411915:42
01/05/19 17:53
7440-38-2
Boron
60.3
mglkg
17.3
8.7
1
01/04/19 15:42
01/05/19 17:53
7440-42-8
Cadmium
1.2
mglkg
0.35
0.17
1
01/04/19 15:42
01/05/19 17:53
7440-43-9
Calcium
35200
mgtkg
865
433
5
01/04/19 15:42
01/07119 15:23
7440-70-2
Chromium
38.7
mg/kg
1.7
0,87
1
01/0411915:42
0110511917:53
7440-47-3
Copper
569
mg/kg
8.7
4.3
5
01/04/19 15:42
01/0711915:23
7440-50-8
Iron
8780
mglkg
13.8
6.9
1
01/04/19 15:42
01/05/19 17:53
7439-89-6
Lead
18.9
mg/kg
3.5
1.7
1
01/04/19 15,42
01/05119 17:53
7439-92-1
Magnesium
6160
mglkg
173
86.5
1
01/04/19 15:42
01/0511917:53
7439-95-4
Manganese
216
mglkg
1.7
0.87
1
01/04/19 15:42
01/05/19 17:53
7439-96-5
Molybdenum
13.1
mglkg
3.5
1.7
1
01/04/19 15:42
01/06/1917:53
7439-98-7
Nickel
22.0
mglkg
1.7
0.87
1
01/04/19 15:42
01/05119 17:53
7440-02-0
Phosphorus
34000
mg/kg
17300
8650
50
01/0411915:42
01/08/1909:54
7723-14-0
Potassium
2610
mglkg
346
173
1
01104/1915:42
01/05/19 17:53
7440-09-7
Selenium
2.6 U
mg/kg
5.2
2.6
1
01/0411915:42
01/05/19 17:53
7782-49-2
Sodium
1430
mg/kg
346
173
1
01/04/19 15:42
0110511917:53
7440-23-5
Sulfur
10800
mglkg
346
173
1
01/04/19 15:42
01105/1917:53
Zinc
668
mglkg
6,9
3.5
1
01/04/19 15:42
01/0511917:53
7440-66-6
7471 Mercury
Analytical
Method: EPA 7471 Preparation Method: EPA
7471
Mercury
0.24
mg/kg
0.062
0.031
1
01/0411914:46
01/07/1916:34
7439-97-6
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
5.3
%
0.10
0.10
1
01104/1909:44
J(D6)
2540G Total Solids
Analytical
Method: SM 2540G
Total Solids
93.3
%
0.0010
0.0010
1
01104/1908:18
2540G Total Volatile Solids
Analytical
Method: SM 2540G
Total Volatile Solids
71.1
%
0.0010
0.0010
1
01/04/19 08:18
Date: 01/14/2019 04:42 PM
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
sample: Pellet
Lab ID: 35439786001 Collected: 01/03M9 11:00 Received: 01103/1912:15 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units PQL MOIL DF Prepared
Analyzed
CAS No. Qual
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
6.9 Sid. Units 0.10 0.10 1
01/04/19 15:55
Q
Specific Gravity/Bulk Density
Analytical Method: ASTM D5057
Specific Gravity
0.570 1
01/08/1916:37
N2
Total Organic Nitrogen Soil
Analytical Method: TKN-NH3 Calculation
Total Organic Nitrogen
38900 mg/kg 21.1 21.1 1
01/11/19 12:49.
350.1 Ammonia
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1
Nitrogen, Ammonia
1160 mg/kg 45.1 15.0 50 01/0411906:00
0110411908:37
7664-41-7
361.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2
Nitrogen, Keldahl, Total
40100 mg/kg 2690 1340 30 01/07/19 09:30
01/09/19 13:54
7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Preparation Method: EPA 353.2.
Nitrogen, NO2 plus NO3
3.7 mg/kg 0.53 0.26 1 01/04/19 14:46
01/04/19 16:36
Nitrogen, Nitrate
2.4 mg/kg 0.53 0.26 1 01/04119 14:46
01/04/19 16:36
14797-55-8
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04:42 PM without the written consent of Pace Analocal Services, LLC.
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Pace Analytical Services, LLC
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I [phone]
QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
QC Batch: 505727 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 35439786001
METHOD BLANK 2731138 Matrix: Solid
Associated Lab Samples: 35439786001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury mglkg 0.0043 U 0.0086 0.0043 0110711915:58
LABORATORY CONTROL SAMPLE: 2731139
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/kg 0.049 0.048 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2731140
2731141
MS
MSD
35439719001 Spike
Spike
MS
MSD MS MSD %Rec Max
Parameter Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD RPD Qual
Mercury mglkg 0.41 0.42
0.41
0.82
0.67 98 66 80-120 19 20 J(M1)
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pinellas County Pellelizer
Pace Project No.: 35439786
QC Batch: 505767
QC Batch Method: EPA 3050
Associated Lab Samples: 35439786001
Analysis Method:
Analysis Description:
'
EPA6010
6010 MET Solid
METHOD BLANK: 2731292
Matrix: Solid
Associated Lab Samples: 35439786001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Arsenic
mg/kg
0.25 U
0.51
0.25
01/0511916:44
Boron
mg/kg
1.3 U
2.5
1.3
01/0711914:08
Cadmium
mglkg
0.025 U
0.051
0.025
0110711914:08
Calcium
mg/kg
12.7 U
25.4
12.7
01/07/1914:08
Chromium
mg/kg
0.13 U
0.25
0.13
0110711914,08
Copper
mg/kg
0.13 U
0.25
0.13
01/07/1914:08
Iron
mg/kg
1.3 1
2.0
1.0
01107/1914:08
Lead
mg/kg
025 U
0.51
0.25
01107/1914:08
Magnesium
mg/kg
12.7 U
25.4
12.7
01107/1914:08
Manganese
mg/kg
0.13 U
0.25
0.13
01/07/1914:08
Molybdenum
mg/kg
0.25 U
0.51
0,25
01/07/1914:08
Nickel
mg/kg
0.13 U
0.25
0.13
01/07/1914:08
Phosphorus
mg/kg
25.4 U
50.8
25.4
01/07/1914:08
Potassium
mg/kg
25.4 U
50.8
25.4
01/07/1914:08
Selenium
mg/kg
0.38 U.
0.76
0.38
01/07/1914:08
Sodium
mg/kg
26.4 U
50.8
25.4
0110711914:08
Sulfur
mg/kg
25.4 U
50.8
25.4
01/0711914:08
Zinc
mg/kg
0.51 U
1.0
0.51
01107/1914:08
LABORATORY CONTROL SAMPLE:
Parameter
2731293
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
13.8
12.8
92
80-120
Boron
mglkg
69.2
63.1
91
80-120
Cadmium
mg/kg
1A
1.3
94
80-120
Calcium
mg/kg
692
683
99
80-120
Chromium
mg/kg
13.8
13.7
99
80-120
Copper
mglkg
13.8
13.8
100
80-120
Iron
mglkg
138
135
97
80-120
Lead
mglkg
13.8
13.1
95
80-120
Magnesium
mglkg
692
671
97
80-120
Manganese
mglkg
13.8
13.7
99
80-120
Molybdenum
mg/kg
13.8
13.3
96
80-120
Nickel
mglkg
13.8
13.4
97
80-120
Phosphorus
mg/kg
13.8
27.7 U
98
80-120
Potassium
mg/kg
692
636
92
80-120
Selenium
mg/kg
13.8
11.2
81
80-120
Sodium
mg/kg
692
656
95
80-120
Sulfur
mg/kg
138
118
86
80-120
Zinc
mg/kg
69.2
64.6
93
80-120
Pace Analytical Services, LLC
110 South Sayview Blvd.
Oldsmar, FL 34677
[phone]
Qualifiers
Qualifiers
Results presented on this page are In the units Indlcated by the •Units" Column except where an alternate unit la presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE 2731294
2731295
MS
MSD
35438990001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Dual
Arsenic
mg/kg
14.7
26.7
35.6
34.9
43.2
76
80
75-125
21
20 J(Rl)
Boron
mg/kg
4.9 1
133
179
78.2
120
55.
64
75-125
42
20 J(M1),
J(Rl)
Cadmium
mg/kg
0.20
2.7
3.5
2.4
3.2
81
85
75-125
31
20 J(Rl)
Calcium
mg/kg
8980
1330
1790
10300
11100
102
119
75-125
7
20
Chromium
mg/kg
23.6
26.7
35.6
53.6
65.2
112
116
75-125
20
20
Copper
mg/kg
79.1
26.7
35.6
109
119
111
112
75-125
9
20 L
Iron
mg/kg
43800
267
356
39200
43500
-1690
-72
75-125
10
20 J(Ml),
L
Lead
mglkg
11.0
26.7
35.6
33.7
42.8
85
89
75-125
24
20 J(R1)
Magnesium
mpg
8260
1330
1790
10900
11900
198
204
75.125
9
20 J(M1),
L
Manganese
mglkg
1050
26.7
35.6
993
1050
-230
-3
75-125
6
20 J(M1),
L
Molybdenum
mglkg
0.72 1
26.7
35.6
20.3
28.8
73
78
75-125
35
20 J(M1),
J(Rl)
Nickel
mg/kg
16.2
26.7
35.6
39.9
49.8
89
94
75-125
22
20 J(Rl)
Phosphorus
mg/kg
429
26.7
35.6
535 1
715 U
397
397
75-125
20 M6
Potassium
mg/kg
768
1330
1790
2110
2640
101
105
75-125
22
20 J(Rl)
Selenium
mglkg
9.8 U
26.7
35.6
14.9
22.5
56
63
75-125
40
20 J(M1),
J(Rl)
Sodium
mglkg
756
1330
1790
2060
2540
98
100
75-125
21
20 J(Rl)
Sulfur
mglkg
2780
267
356
3150
3260
139
132
75-125
3
20 J(Ml)
Zinc
mglkg
75.5
133
179
186
235
83
89
75-125
23
20 J(Rl)
Results presenter) on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04:42 PM without the written consent of Pace Analytical Services, L-C.
Page 9 of 21

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QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
QC Batch: 505630 Analysis Method: EPA 8082
QC Batch Method: EPA 3546 Analysis Description: 8082 PCB Solid MW
Associated Lab Samples: 35439786001
METHOD BLANK: 2730675
Matrix:
Solid
Associated Lab Samples: 35439786001
Blank
Reporting
Parameter
Units
Result
Limit
MOIL
Analyzed
PCB-1016 (Aroclor 1016)
mg/kg
0.010 U
0.017
0.010
0110511922:15
PCB-1221 (Aroclor 1221)
mg/kg
0.0080 U
0.017
0.0080
0110511922:15
PCB-1232 (Aroclor 1232)
mg/kg
0.0085 U
0.017
0.0085
01/05/19 22:15
PCB-1242 (Aroclor 1242)
mg/kg
0.0092 U
0,017
0.0092
01/05/19 22:15
PCB-1248 (Aroclor 1248)
mg/kg
0.011 U
0.017
0.011
01/05/19 22:15
PCB-1254 (Aroclor 1254)
mg/kg
0.0068 U
0.017
0.0068
01/05/19 22:15
PCB-1260 (Aroclor 1260)
mg/kg
0.010 U
0.017
0.010
01/05M9 22:15
Decachlorobiphenyl (S)
%
84
26-172
01/05/19 22:15
Tetrachloro-m-xylene (S)
%
83
59-129
01/05/19 22:15
LABORATORY CONTROL SAMPLE:
2730676
Spike
LCS LCS
% Rae
Parameter
Units
Cone.
Result % Rae
Limits
PCB-1016 (Aroclor 1016)
mg/kg
0.063
0.074 89
50-141
PCB-1260 (Aroclor 1260)
mg/kg
0.083
0.062 75
54-145
Decachlombiphenyl (S)
%
80
26-172
Tetrachloro-m-xylene (S)
%
77
59-129
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar , FL 34677
[phone]
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2730677
2730678
MS
MSD
35439786001
Spike
Spike
MS
MSD
MS
MSD
% Rise
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rae
% Rae
Limits
RPD RPD Qual
PCB-1016 (Aroclor 1016)
mg/kg
0.34 U
0.58
0.55
1.7
0.64
299
118
50-141
91 40 D3,
J(M7),
J(R1)
PCB-1260 (Aroclor 1260)
mg/kg
0.34 U
0.58
0.55
0.40 1
0.34 U
69
59
54-145
40 D3
Decachlorobiphenyl(S)
%
11
39
26-172
J(S5)
Tetrachloro-m-xylene (S)
%
247
72
59-129
J(SO)
Results presented on this page are In the units indicated by the "Units^ column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04:42 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

aceAnalytical e
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QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
QC Batch: 505646 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 35439786001
SAMPLE DUPLICATE: 2730801
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2730802
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2730803
Parameter
Percent Moisture
35439786001 Dup
Units Result Result
% 5.3 5.8
92409944048 Dup
Units Result Result
e/ 7.7 7.7
92409944082 Dup
Units Result Result
% 14.7 16.3
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar. FL 34677
[phone]
Max
RPD RPD Qualifiers
9 5 J(D6)
Max
RPD RPD Qualifiers
0 5
Max
RPD RPD Qualifiers
10 5 J(D6)
Results presented on this page are In the units Indlealed by the "units" column except where an alternate unit Is presented to the right of Me result.
REPORT OF LABORATORY ANALYSIS
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aceAnalydcal
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QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
QC Batch: 505610 Analysis Method: SM 2540G
QC Batch Method: SM 2540G Analysis Description: 2540E Total Solids
Associated Lab Samples: 35439786001
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
SAMPLE DUPLICATE: 2730574
35439834001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 3.8 3.7 2 5
SAMPLE DUPLICATE: 2730575
35439836001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 2.9 3.0 3 5
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/1412019 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 21

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project:
Pinellas County Pelletizer
Pace Project No.:
35439786
QC Batch:
505612 Analysis Method: SM 254OG
QC Batch Method:
SM 2540G Analysis Description: 254OG Total Volatile Solids
Associated Lab Samples:
35439786001
METHOD BLANK: 2730576
Associated Lab Samples: 35439786001
Parameter Units
Total Volatile Solids %
SAMPLE DUPLICATE: 2730577
Parameter
Total Volatile Solids
SAMPLE DUPLICATE. 2730578
Parameter
Total Volatile Solids
Matrix: Solid
Blank Reporting
Result Limit MDL Analyzed Qualifiers
0.0010 U 0.0010 0.0010 01/0411908:07
35439834001 Dup
Units Result Result
% 61.9 62.4
35439836001 Dup
Units Result Result
% 67.4 67.0
Max
RPD RPD Qualifiers
1 5
Max
RPD RPD Qualifiers
0 5
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04:42 PM without the written consent of Pace Analytical Services, I.L.C. Page 13 of 21

aceAnalytical e
� www.pacelabscdm
QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar. FL 34677
[phone]
QC Batch: 506399 Analysis Method: ASTM D5057
QC Batch Method: ASTM D5057 Analysis Description: Spec.GravitylBulk Density,ASTM D5057
Associated Lab Samples: 35439786001
SAMPLE DUPLICATE: 2734026
Parameter
Specific Gravity
35439786001 Dup
Units Result Result
0.570 0.580
Max
RPD RPD Qualifiers
2 N2
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04A2 PM without the written consent of Pace Analytical Services, LLC, Page 14 of 21

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletlzer
Pace Project No.: 35439786
QC Batch; 505588
Analysis Method:
EPA 350.1
QC Batch Method: EPA 350.1
Analysis Description:
350.1 Ammonia
Associated Lab Samples: 35439786001
METHOD BLANK: 2730504
Matrix: Solid
Associated Lab Samples: 35439786001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Nitrogen, Ammonia
mglkg
0.28 U 0.85 0.28
01/04/19 07:59
LABORATORY CONTROL SAMPLE:
2730505
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/kg
10.2 10.1
99
80-120
MATRIX SPIKE SAMPLE:
2730507
35439793001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mglkg
0.62 U 22.8
22.4
98
80-120
SAMPLE DUPLICATE: 2730506
35439793001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Ammonia
mglkg
0.62 U 0.63
U
20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 21

ace Analytical
eww.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
QC Batch: 505998
Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2
Analysis Description: 351.2 TKN
Associated Lab Samples: 35439786001
METHOD BLANK: 2732428
Matrix: Solid
Associated Lab Samples: 35439786001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
10.4 U 20,8
10.4
01/09/19 12:51
LABORATORY CONTROL SAMPLE:
2732429
Spike LCS
LCS
% Rec
Parameter
Units
Conic. Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
1030 1010
98
90-110
MATRIX SPIKE SAMPLE:
2732431
35438705001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
653 3770
4610
105
90-110
MATRIX SPIKE SAMPLE:
2732433
35439719001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
58200 16100
74000
99
90-110
SAMPLE DUPLICATE: 2732430
35438705001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
653 595
9
20
SAMPLE DUPLICATE: 2732432
35439719001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
58200 53600
8
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04:42 PM without the written consent of Pace Analytical Services, L-C. Page 16 of 21

(�IaceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
QC Batch: 505763
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 35439786001
METHOD BLANK: 2731264
Matrix: Solid
Associated Lab Samples: 35439786001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Nitrogen, Nitrate
mg/kg
0.25 U 0.50 0.25
01/0411916:27
Nitrogen, NO2 plus NO3
mg/kg
0.25 U 0.50 0.25
01/04/19 16:27
LABORATORY CONTROL SAMPLE:
2731265
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/kg
20 21.2 106
90-110
MATRIX SPIKE SAMPLE:
2731267
35439719001 Spike MS
Ms
% Rec
Parameter
Units
Result Conc. Result
%Rec
Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/kg.
1.5 1 84.6 52.4
60
80-120 J(M1)
SAMPLE DUPLICATE: 2731266
35439719001 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Nitrogen, Nitrate
mg/kg
1.5 1 1.7 1
20
Nitrogen, NO2 plus NO3
mg/kg
1.5 1 1.7 1
20
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2019 04:42 PM without the written consent of Pace Analytical Services, U.C. Page 17 of 21

Pace Analytical Services, LLC
aceAnalytical a "° sewn Bayvie
Oldsmar, FLL 346774677
w ..pacalabs.wm [phone]
QUALIFIERS
Project: Pinellas County Pelletizer
Pace Project No.: 35439786
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
MDL -Adjusted Method Detection Limit.
PQL- Practical Quanlitation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte In a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitmsodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
U Compound was analyzed for but not detected.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory
control limits.
J(Mi) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS)
recovery.
J(R1) Estimated Value. RPO value was outside control limits.
J(SO) Estimated Value. Surrogate recovery outside laboratory control limits.
J(S5) Estimated Value. Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
L Off -scale high. Actual value is known to be greater than value given.
Me Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELACITNI accreditation for this parameter.
P1 Routine initial sample volume or weight was not used for extraction, resulting in elevated reporting limits.
Q Sample held beyond the accepted holding time. Analysis initiated morethan 15 minutes after sample collection.
REPORT OF LABORATORY ANALYSIS
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Date: 01/1412019 04:42 PM without the written consent of Pace Analytical Services, U.C. Page 18 of 21

JceAnalytical'
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar , FL 34677
[phone]
Project:
Pace Project No.:
Pinellas County Pelletizer
35439786
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
35439786001
Pellet
EPA 3546
505630
EPA 8082
505806
35439786001
Pellet
EPA3050
505767
EPA6010
505836
35439786001
Pellet
EPA 7471
505727
EPA7471
505807
35439786001
Pellet
ASTM D2974-87
505646
35439786001
Pellet
SM 2540G
505610
35439786001
Pellet
SM 254OG
505612
35439786001
Pellet
EPA9045
505791
35439786001
Pellet
ASTM D5057
506399
35439786001
Pellet
TKN-NH3 Calculation
507416
35439786001
Pellet
EPA 350.1
505588
EPA 350.1
505616
35439786001
Pellet
EPA 351.2
505998
EPA 351.2
506621
35439786001
Pellet
EPA 353.2
505763
EPA 353.2
505790
Date: 01/14/2019 04:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analylical Services, LLC.
Page 19 of 21

SYNAGRO
5900 74di Sfma Nnnh
Sr. I' mnhm. R. 33709
Phone [phone]
Fax [phone]
CHAIN OF CUSTODY RECORD
No
MAILING ADDRESS:
SYNAGRO o
P.O. Box 3227
Pinellas Park- FL 337RO b
PROJECT I PROJECT NAME
Pinellas County
LABORATORY:
PARAMETERS
# 29-0750
Pelletizer
FR L '�
SAMPLERS (Signature)
2M
(Print)'
1
y
g'
C
tl
�2e y W.Qy JyRScp Jg ^m
�WA+J/
SAMPLE NUMBER DATE TIME
ay
o ¢ a
, z o' o o
'�� o° ytY a'� y� g` yo° 3 SAMPLE
u o 3 in y
,'—.. r ¢ LL o
G� 20 ae x a• ae ae a,. :, x LOCATION
Pel1e
i
`h-)/I
nz.
✓
Gi.
4
✓
;!r
J`
✓
,j'
G;-, j,.: .
WO#:35439785
II I I I III III it I I II I III
35139786
PARAMETERS
2W¢� Wy4,`S d boy �� oa g` vg rya ya. @y g� C
SAMPLE NUMBER DATE TIME °¢? o A g a o'r g ,�c� °W `4W r'W �° .�°'' eo`� 0 SAMPLE REMARKS
¢¢F ar ¢¢ a¢F d' dt :r x y¢` a yo ¢u ¢r" LOCATION
O t(:
�(�
✓
�: nrs ` 1� ..
Wi Wcfw R k-) r ;
%ItylIZ
for Re

�- aceMaly[i/'
acumen ame
Sample Condition Upon Receipt
P P p
WCUMent ReViSed:
May 30, 2a19
cumen o.:
F-FL-C-007 rev. 13
ssmng u only:
1 Pace Florida Oualiry Office
Sample
Condition Upon Receipt
Form (SCUR)
Project #
Iio#
: 35439785
Date
and Initials erson:
Project Manager:
Pm: CEM
Gue Gatie: Ol/14/19 Examining eo ten :
Client:
CLIENT:
37-SYNAGRO
Label:
Delivvee r:
pH:
Thermometer Used: T-202
Date: 1-5•- (9
Time: [Z-i S Initials: t�ry� %-•�
State of Origin: FL
Cooler#1 Temp.'C �• (Visual)
❑ For WV projects, all containers verified to 0 •C
0.O (Correction Factor) �f ���///•••
l�(Actual) Samples on Ice, waling process has begun
Cooler#2 TempJC
(Visual)
(Correction Factor)(Actual)
Samples an Ice, cooling process has begun
Cooler#3 Temp.'C
(Visual)
(Correction Factor) (Actual)
❑ Samples on ice, cooling process has begun
Cooler#4 Temp.'C
(Visual)
(Correction Factor) (Actual
❑ Samples on ice, cooling process has begun
Cooler#5 Temp.'C
(Visual)
(Correction Factor) _(Actual)
❑ Samples on ice, waling process has begun
Cooler#6 Temp.'C
(Visual)
(Correction Factor) (Actual)
❑ Samples on ice, cooling process has begun
Courier: ❑ Fed Ex ❑ UPS ❑ USPS Alient ❑ Commercial ❑ Pace ❑ Other
Shipping Method: ❑ First Overnight ❑ Priority Overnight O Standard Overnight ❑ Ground ❑ International Priority
❑ Other
Billing: ❑ Recipient
Tracking #
❑ Sender ❑ Third Party ❑ Credit Card ❑ Unknown
Custody Seal on Cooler/Box Present: 01'es 240 Seats Intact: ❑ Yes ❑ No Ice: Wel Blue Dry None
Packing Material: ❑Bubble Wrap Bubble Sags []None ❑Other
Samples shorted to lab of Yes, complete) Shorted Dale: Shorted Time: City:
Chain of Custody Present
es
❑ No ON/A
Chain of Custody Filled Out
es
❑ No 13NIA
Relinquished Signature & Sampler Name COC
es
❑ No ONIA
Samples Arrived within Hold Time
Arfes
❑ No DN/A
Rush TAT requested on COC
OYes
o ON/A
Sufficient Volume
4efes
❑ No ON/A
Correct Containers Used
es
❑ No OWA
Containers Intact
es
❑ No ONIA
Sample Labels match CDC (sample IDS & dateltime of
collection)
XeYes
❑ No ON/A
All containers needing acid base preservation have been
checked. OYea
All Containers needing preservation are round to be in
compliance with EPA recommendation: OYes
Excepdons: VOA, Coliform, TOC, 0&G, Carbamales
❑ No AIA
❑ No /A
Preservation Informadon:
Preservative:
Lot q/Trace #:
Date: Time:
ls:
Inilia :Headspace
in VOA Vials? ( s6mm):
OYes
❑ No AIA
Trip Blank Present:
OYes
❑ No 9W
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution (use back for additional
Deterrime:
Project Manager Review: Dale: a 21 of 21

HOWARD FERTILIZER
CLASS A
BIOSOLH)S ANALYSIS
Residual Type: Wastewater Treatment Plant(Pinellas)
Date Sampled: April 2, 2019
South Cross Bayou WRF (2nd Ouarter 2019) Permit No. W00037094
Mineralization Rate 0.30 92.90 % Solids
6.9 pH
Parameter % Mg/Kg Dry Weight I Pounds/Dry Ton
(% x 10,000) (Me/Ke x 0.0021
Carbonate
N / Nitrite N
1,920.000
5.000
28,300.000
3.700
1100
39.600
499.000
16.600
0.420
11.800
21.400
4.900
700.005
Pace Analytical 35458289
61.400
5.240
29.698
27.778
3.840
64.800
12.540
0.010
0.033
0.001
0.024
0.043
0.010
1.400
"Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
1.83
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

aC6Ana1j&a1
nwwpaWabs.00m
April 11, 2019
William Reyes
Synagro
RE: Project: Pinellas County Pelletizer
Pace Project No.: 35458289
Dear William Reyes:
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 02, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cameron Meynardie
[e-mail]
[phone]
Project Manager
Enclosures
cc: Robert Ervin, Synagro
iw�e PCCRpOj��
y(l
eORASO
REPORT OF LABORATORY ANALYSIS
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Project: Pinellas County Pellelizer
Pace Project No.: 35458289
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Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
CERTIFICATIONS
Montana Certification #: Carl 0074
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Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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Project: Pinellas County Pelletizer
Pace Project No.: 35458289
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
35458289001 Pellet Solid 04102/1915:30 04/02/1916:45
REPORT OF LABORATORY ANALYSIS
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Oldsmar, FL 34677
[phone]
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Project: Pinellas County Pelletizer
Pace Project No.: 35458289
Lab ID Sample ID
35458289001 Pellet
Pace. Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA6010
LEC, SC1
18
PASI-O
EPA 7471
AMS
1
PASI-O
ASTM D2974-87
CLT
1
PASI-O
SM 2540G
SA7
1
PASI-O
SM 2540G
SA1
1
PASI-O
EPA 9045
JDW
1
PASI-O
ASTM D5057
JDW
1
PASI-O
TKN-NH3 Calculation
JMD
1
PASI-O
EPA 350.1
MAJ
1
PASI-O
EPA 351.2
JMD
1
PASI-O
EPA 353.2
AMP
2
PASI-O
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
Sample: Pellet Lab ID: 35458289001 Collected: 04102119 15:30 Received: 04/02/19 16:45 Matrix: Solid
Results reported on a "dry weight"basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units PQL MOIL DF Prepared Analyzed CAS No. Qua[
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA3050
Arsenic
3.7 mg/kg 1.0
0.52
1
04106/1906:58
04/07/19 18:43
7440-38-2
Baron
60.0 mg/kg 5.2
2.6
1
04106/19 06:58
04/07/19 18:43
7440-42-8
Cadmium
1.2 mg/kg 0.10
0.052
1
04/06/19 06:58
04107/19 18:43
7440-43-9
Calcium
32400 mg/kg 520
260
10
04/06/19 06:58
04/08/19 15:13
7440-70-2
Chromium
39.6 mg/kg 0.52
0.26
1
04/06/19 06:58
04/07/19 18:43
7440-47-3
Copper
499 mg/kg 5.2
2.6
10
04/06/19 06:58
04108/19 15:13
7440-50-8
Iron
7860 mg/kg 41.6
20.8
10
04/06/19 06:58
04108/19 15:13
7439-89-6
Lead
16.6 mg/kg 1.0
0.52
1
04106/19 06:58
04/07/19 18:43
7439-92-1
Magnesium
6270 mg/kg 52.0
26.0
1
04106/1906:58
04/0711918:43
7439-95-4
Manganese
202 mg/kg 5.2
2.6
10
04/06/19 06:58
04/08/19 15:13
7439-96-5
Molybdenum
11.8 mg/kg 1.0
0.52
1
04/06/19 06:58
04/0711918:43
7439-98-7
Nickel
21.4 mg/kg 0.52
0.26
1
04/06/19 06:58
04/07/19 18:43
7440-02-0
Phosphorus
30700 mg/kg 10400
5200
100
04/06/19 06:58
04/08/19 15:16
7723-14-0
Potassium
2620 mg/kg 104
52.0
1
04/06/19 06:58
04/07/19 18:43
7440-09-7
Selenium
4.9 mg/kg 1.6
0.78
1
04/O6/19 06:58
04/07/19 18:43
7782-49-2
Sodium
1430 mg/kg 104
52.0
1
04/06/19 06:58
04/07/19 18:43
7440-23-5
Sulfur
11700 mg/kg 1040
520
10
04/06/19 06:58
04/08119 15:13
Zinc
700 mg/kg 20.8
10.4
10
04106/19 06:58
04/08/19 15:13
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.42 mg/kg 0.075
0.037
1
04/04/19 11:23
04/04/19 21:01
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
6.2 % 0.10
0.10
1
04/08/19 08:35
254OG Total Solids
Analytical Method: SM 254OG
Total Solids
92.9 % 0.0010
0.0010
1
04/03/19 07:48
254OG Total Volatile Solids
Analytical Method: SM 2540G
Total Volatile Solids
71.4 % 0.0010
0.0010
1
04/03/19 07:48
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
6.9 Std. Units 0.10
0.10
1
04/09/19 12:39
Q
Specific Gravity/Bulk Density
Analytical Method: ASTM D5057
Specific Gravity
0.610
1
04/10/19 14:49
N2
Total Organic Nitrogen Soil
Analytical Method: TKN-NH3 Calculation
Total Organic Nitrogen
43100 mg/kg 21.3
21.3
1
04/10/19 16:03
350.1 Ammonia
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1
Nitrogen, Ammonia
1920 mg/kg 9.0
3.0
10
04/04/1911:20
04/0411916:08
7664-41-7
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Sample: Pellet
Lab ID: 35458289001 Collected: 04/02119 15,30 Received: 0410211916:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters
Results Units PQL MDL DF Prepared Analyzed CAS No. Qua[
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA351.2 Preparation Method: EPA 351.2
Nitrogen, Kjeldahl, Total
45000 mg/kg 943 472 10 04/09/19 10:38 04/10/19 13:15 7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Preparation Method: EPA 353.2
Nitrogen, NO2 plus NO3
3.1 mg/kg 0.53 0.27 1 04/03/19 13:30 04/03/19 14:32
Nitrogen, Nitrate
1.9 mg/kg 0.53 0.27 1 04/03119 13:30 04/03/19 14:32 14797-55-8
Date: 04/11/2019 10:48 AM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pellellzer
Pace Project No.: 35458289
QC Batch: 528349
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 35458289001
METHOD BLANK: 2859721
Matrix: Solid
Associated Lab Samples: 35458289001
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Mercury mg/kg
0.0045 U 0.0090 0.0045 04/04119 20:00
LABORATORY CONTROL SAMPLE: 2859722
Spike LCS LCS
% Rec
Parameter Units
Conc. Result %Rac
Limits Qualifiers
Mercury mglkg
0.083 0.086 104
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2859723 2859724
MS MSD
35457920004
Spike Spike MS MSD
MS MSD
%Rec Max
Parameter Units Result
Conc. Cone. Result Result
% Rec % Rec
Limits RPD RPD Qual
Mercury mg/kg 0.062 U
1.3 1.1 0.81 0.74
64 64
80-120 10 20 J(M1)
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Dale: 04/11/2019 10:48 AM without the written consent of Pace Analytical Services, L-C.
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QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
QC Batch: 528981 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid
Associated Lab Samples: 35458289001
Pace Analytical Services, LLC
110 South Baywew Blvd.
Oldsmar, FL 34677
[phone]
METHOD BLANK: 2863815
Associated Lab Samples: 35458289001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed Qualifiers
Arsenic
mg/kg
0.28 U
0.57
0.28
04107/1918:00
Boron
mglkg
1.4 U
2.8
1.4
04/0711918:00
Cadmium
mg/kg
0.028 U
0.057
0.028
04/0711918:00
Calcium
mg/kg
14.2 U
28.4
14.2
04/07/1918:00
Chromium
mg/kg
0.14 U
0.28
0.14
04/07/1918:00
Copper
mg/kg
0.14 U
0.28
0.14
04/07/1918:00
Iron
mg/kg
1.1 U
2.3
1.1
04107/1918:00
Lead
mg/kg
0.28 U
0.57
0.28
0410711918:00
Magnesium
mg/kg
14.2 U
28.4
14.2
04/0711918:00
Manganese
mg/kg
0.14 U
0.28
0.14
04/07/19 18:00
Molybdenum
mg/kg
0.28 U
0.57
0.28
04107/1918:00
Nickel
mg/kg
0.14 U
0.28
0.14
04/0711918:00
Phosphorus
mg/kg
28.4 U
56.8
28.4
04107/1918:00
Potassium
mg/kg
28.4 U
56.8
28.4
04107/1918:00
Selenium
mg/kg
0.43 U
0.85
0.43
04/07/1918:00
Sodium
mg/kg
28.4 U
56.8
28.4
04/0711918:00
Sulfur
mg/kg
28.4 U
56.8
28.4
04/0711918:00
Zinc
mg/kg
0.57 U
1.1
0.57
04/07/1918:00
LABORATORY CONTROL SAMPLE:
2863816
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
15.1
14.9
98
80-120
Boron
mg/kg
75.6
71.3
94
80-120
Cadmium
mg/kg
1.6
1.6
104
80-120
Calcium
mg/kg
756
797
105
80-120
Chromium
mg/kg
15.1
16.0
106
80-120
Copper
mg/kg
15.1
14.9
99
80-120
Iron
mg/kg
151
161
106
80-120
Lead
mg/kg
15.1
15.7
104
80-120
Magnesium
mg/kg
756
739
98
80-120
Manganese
mg/kg
15.1
15.9
105
80-120
Molybdenum
mg/kg
15.1
15.7
104
80-120
Nickel
mg/kg
15.1
16.1
106
80-120
Phosphorus
ni
15.1
30.2 U
104
80-120
Potassium
mg/kg
756
742
98
80-120
Selenium
mg/kg
15.1
14.4
95
80-120
Sodium
mg/kg
756
784
104
80-120
Sulfur
mg/kg
151
139
92
80-120
Zinc
mg/kg
75.6
78.6
104
80-120
Results presented on this page are In the units Indicated by the "Units' column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2863817
MS
35457507001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2863818
MS
Result
MSD
Result
MS
% Rec
MSD
% Rao
%Rec
Limits
Max
RPD RPD Qual
Arsenic
mg/kg
10.7
12.8
12.3
14.7
15.8
31
42
75-125
7
20 J(M1)
Boron
mg/kg
1.3 U
64
61.5
45.4
42.4
69
67
75-125
7
20 J(M1)
Cadmium
mg/kg
0.062
1.3
1.2
1.1
0.99
78
76
75-125
6
20
Calcium
mg/kg
1660
640
615
1240
1180
-65
-78
75-125
5
20 J(Mt)
Chromium
mg/kg
8.7
12.8
12.3
18.6
17.3
77
71
75-125
7
20 J(M1)
Copper
mg/kg
29.8
12.8
12.3
29.8
31.5
0
14
75-125
6
20 J(M1)
Iron
mg/kg
10600
128
123
7380
8430
-2480
-1740
75-125
13
20 J(M1),
L
Lead
mg/kg
31.2
12.8
12.3
34.2
35.8
24
38
75-125
5
20 J(MI)
Magnesium
mg/kg
154
640
615
630
580
74
69
75-125
8
20 J(M1)
Manganese
mg/kg
75.3
12.8
12.3
77.4
72.3
16
-25
75-125
7
20 J(M1),
L
Molybdenum
mg/kg
1.0
12.8
12.3
10.5
9.8
74
72
75-125
7
20 J(M1)
Nickel
mg/kg
5.3
12.8
12.3
15.1
14.9
76
77
75-125
2
20
Phosphorus
mg/kg
1310
12.8
12.3
1250
734
482
4680
75-125
52
20 J(M1),
J(R1),
L
Potassium
mg/kg
150
640
615
618
571
73
69
75-125
8
20 J(M1)
Selenium
mg/kg
0.39 U
12.8
12.3
8.8
8.5
69
69
75-125
4
20 J(M1)
Sodium
mg/kg
93.0
640
615
607
554
80
75
75-125
9
20
Sulfur
mg/kg
130
128
123
168
227
30
79
75-125
30
20 J(M1),
J(R1)
Zinc
mg/kg
6.6
64
61.5
56.1
52.1
77
74
75-125
7
20 J(M1)
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 36458289
QC Batch: 529137
Analysis Method:
ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description:
Dry Weight/Percent Moisture
Associated Lab Samples: 35458289001
SAMPLE DUPLICATE: 2864624
35457507001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
7.7
8.1 6
10
SAMPLE DUPLICATE: 2864625
35458132002
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
1.1
0.92 15
10 J(D6)
SAMPLE DUPLICATE: 2864626
35458304004
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
15.7
15.8 0
10
SAMPLE DUPLICATE: 2864627
35458748002
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
6.6
73 11
10 J(D6)
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pinellas County Pellefter
Pace Project No.: 35458289
QC Batch: 527978 Analysis Method: SM 2540G
QC Batch Method: SM 2540G Analysis Description: 254OG Total Solids
Associated Lab Samples: 35458289001
Pace Analytical Services, LLC
110 South Bayvlew Blvd.
Oldsmar, FL 34677
[phone]
SAMPLE DUPLICATE: 2857646
35458004001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 3.1 3A 1 5
SAMPLE DUPLICATE: 2857647
35457985001 Cup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 2.8 2.8 1 5
Results presented on (his page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
QC Batch: 527979
Analysis Method: SM 254OG
QC Batch Method: SM 254OG
Analysis Description: 254OG Total Volatile Solids
Associated Lab Samples: 35458289001
METHOD BLANK: 2857648
Matrix:
Solid
Associated Lab Samples: 35458289001
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed
Qualifiers
Total Volatile Solids
%
0.0010 U
0.0010 0.0010
04/03/19 07,38
SAMPLE DUPLICATE: 2857649
35458004001
Dup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Total Volatile Solids
%
67.0
66.5 1
5
SAMPLE DUPLICATE: 2857650
36457985001
Dup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Total Volatile Solids
%
67.5
672 0
5
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to Me right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pinellas County Pellefizer
Pace Project No.: 35458289
Pace Analytical Services, LLC
110 South Bayview, Blvd.
Oldsmar, FL 34677
[phone]
UU Batch: 529526 Analysis Method: ASTM D5057
QC Batch Method: ASTM D5057 Analysis Description: Spec.Gravity/Bulk Density,ASTM D5057
Associated Lab Samples: 35458289001
SAMPLE DUPLICATE: 2866740
Parameter
Specific Gravity
35458289001 Dup
Units Result Result
0.610 0.610
Max
RPD RPD Qualifiers
0 N2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the night of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
QC Batch: 528399
Analysis Method:
EPA350.1
QC Batch Method: EPA 350.1
Analysis Description:
350.1 Ammonia
Associated Lab Samples: 35458289001
METHOD BLANK: 2859962
Matrix: Solid
Associated Lab Samples: 35458289001
Blank Reporting
Parameter
Units
Result Limit
MOIL
Analyzed
Qualifiers
Nitrogen, Ammonia
mg/kg
0.28 U 0.85 0.28
04/04/19 16:09
LABORATORY CONTROL SAMPLE:
2859963
Spike LCS
LCS
% Rao
Parameter
Units
Conc. Result
% Rao
Limits Qualifiers
Nitrogen, Ammonia
mg/kg
10.2 10.6
105
80-120
MATRIX SPIKE SAMPLE:
2859965
35456866001 Spike
MS
MS
% Rao
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/kg
12300 44.8
11100
-2600
80-120 M6
SAMPLE DUPLICATE: 2859964
35456866001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Ammonia
mg/kg
12300 12200 0
20
Results presented on this page are in the units indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
QC Batch: 529312
Analysis Method: EPA 351.2
QC Batch Method: EPA 361.2
Analysis Description: 351.2 TKN
Associated Lab Samples: 35458289001
METHOD BLANK: 2865177
Matrix: Solid
Associated Lab Samples: 35458289001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
10.9 U 21.8
10.9
04/10/19 13:07
LABORATORY CONTROL SAMPLE:
2865178
Spike LCS
LCS
% Rec
Parameter
Units
Conic. Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
821 765
93
90-110
MATRIX SPIKE SAMPLE:
2865180
35458276002 Spike
MS
MS
% Rec
Parameter
Units
Result Conic.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
43900 14500
47500
25
90-110 J(Mi)
MATRIX SPIKE SAMPLE:
2865182
35459256001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mglkg
667 6620
6650
90
90-110
SAMPLE DUPLICATE: 2865179
35458276002 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
43900 40500
8
20
SAMPLE DUPLICATE: 2865181
35459256001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Kjeldahl, Total
mglkg
667 430
43
20 J(D6)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pinellas County Pellelizer
Pace Project No.: 36458289
QC Batch: 528092 Analysis Method: EPA 353.2
QC Balch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 35458289001
METHOD BLANK: 2858100
Associated Lab Samples: 35458289001
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
LABORATORY CONTROL SAMPLE:
2858101
Parameter
Units
Nitrogen, NO2 plus NO3
mglkg
Matrix: Solid
Blank Reporting
Result Limit
0.25 U 0.50
0.25 U 0.50
Spike LCS
Conc. Result
20 20.9
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
MDL Analyzed Qualifiers
0.25 04/03/1914:26
0.25 041031191426
LCS % Rec
% Rec Limits Qualifiers
104 90-110
MATRIX SPIKE SAMPLE:
2858103
35458276002
Spike
MS MS
%Rec
Parameter
Units
Result
Conc.
Result %Rec
Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/kg
4,9
78
81.2
98 60-120
SAMPLE DUPLICATE: 2858102
35458276002
Dup
Max
Parameter
Units
Result
Result
RPD RPD
Qualifiers
Nitrogen, Nitrate
mg/kg
2.3
3.6
44
20 J(D6)
Nitrogen, NO2 plus NO3
mglkg
4.9
3.6
30
20 J(D6)
Results presented on this page are In the units Indicated by the "Unite column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: Pinellas County Pelletizer
Pace Project No.: 35458289
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
MDL-Adjusted Method Detection Limit.
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
PQL - Practical Quantitation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazme decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
U Compound was analyzed for but not detected.
J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory
control limits.
J(M1) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS)
recovery.
J(R1) Estimated Value. RPD value was outside control limits.
L Off -scale high. Actual value is known to be greater than value given.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditation/certifications may apply. A
complete list of accreditations/certifications is available upon request.
Q Sample held beyond the accepted holding time. Analysis initiated more than 15 minutes after sample collection.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project:
Pace Project No.:
Pinellas County Pelletizer
35458289
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
35458289001
Pellet
EPA 3050
528981
EPA 6010
529029
35458289001
Pellet
EPA 7471
528349
EPA 7471
528513
35458289001
Pellet
ASTM D2974-87
529137
35458289001
Pellet
SM 2540G
527978
35458289001
Pellet
SM 2540G
527979
35458289001
Pellet
EPA 9045
529528
35458289001
Pellet
ASTM D5057
529526
35458289001
Pellet
TKN-NH3 Calculation
530054
35458289001
Pellet
EPA 350.1
528399
EPA 350.1
528551
35458289001
Pellet
EPA 351.2
529312
EPA 351.2
529837
35458289001
Pellet
EPA 353.2
528092
EPA 353.2
528186
Date: 04/11/2019 10:48 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 20

SYNAGRO Phone [phone]
191107+a, Slmel North Fax [phone]
CHAIN OF CUSTODY RECORD
N
MAILING ADDRESS: `o
SYNAGRO w
•�_^ ,• r.v. aox szu a
° " ` Pinellas Park, FL 33780 a
PROJECT PROJECT NAME Pinellas County LABORATORY: PARAMETERS
# 29-0750 Pelletizer PO -
SAMPLERS (Signature) (print) a, aey a WZ7
)SAMPLE NUMBER DATE TIME �� e: fO o w° �.¢' apAMPLE
OCATION
.2-li i53D to bL l
WO#:35458289
IIII I IIII IIIIIII III III
35458289
PARAMETERS
2�ey 2
SAMPLE NUMBER DATE TIME� SAMPLE REMARKS
¢ ep ¢ ¢ LOCATION
Pe e °I z- 9 IT3o
IEEE[
Rellnquishad By!
with Shipment - Pink Copy for Flla
by:
n.- 11 c srouevoa

ocumen time:
Document Havised:
ace Abe/yriCd/.
Sample Condition Upon Receipt Form
May 30. 2018
cameo o.:
ssu' ' on
_. •d�
F-FL-0007 rev. 13
Pace Fladda Duality Office
Sample
Condition Upon Receipt Form (SCUR)
Project #
WQ#
: 35458288
Date and Initials of person:
Project Manager:
Client'
PM: CEM
CLIENT:
Due Dale: 04/11/19
37-SYNAGRO
Examining o tents: mu'1-
Label: ? !'3
Deliver:.
pH: I • A
Thermometer Used:
T-203
Date: G[ �' (�1
Time: I (L6- �-z Initials: L. Z"
State of Origin:
FL
❑ For VW iprojects, all wnlainem verified to i °C
Cooler#1 Temp.'C a—' (Visual) 0.0.
(Correction Factor) ""{=i (Actual)
/ Samples an ice, cooling process has begun
Cooler#2 Temp.'C
(Visual)
(Correction Factor)
(Actual)
❑ Samples on ice, cooling process has begun
Cooler#3 Temp.'C
(Visual)
(Correction Factor)
(Actual)
❑ Samples an ice, cooling process has begun
Cooler#4 Temp.'C
(Visual)
(Correction Factor)
(Actual)
❑ Samples on ice, cooling process has begun
Cooler #5 Temp.'C
(Visual)
(Correction Factor)
(Actual)
❑ Samples an Ice, cooling process has begun
Cooler#6 Temp.'C
(Visual)
(Correction Factor)
(Actual)
❑ Samples on ice, cooling process has begun
Courier: ❑ Fed Ex ❑ UPS 0 USPS Client ❑ Commercial ❑ Pace ❑ Other
Shipping Method: ❑ First Overnight ❑ Priority Overnight ❑ Standard Overnight ❑ Ground ❑ International Priority
Billing:
Tracking #
❑ Other
❑ Recipient ❑ Sender ❑ Third Parry ❑ Credit Card ❑ Unknown
Custody Seal on Cooler/Box Present: /❑Yes (QND Seals Intact: El Yes ❑ No Ice:
Packing Material: ❑Bubble Wrap YJ Bubble Baggs ❑None ❑Other
Samples shorted to lab (if Yes, complete) Shorted Date: Shorted Time:
f:nmmen}¢•
Dry None
Oty:
Chain of Custody Present
❑Yes
❑ No OWA
Chain of Custody Filled Out
0s
❑ No ON/A
Relinquished Signature & Sampler Name COG
\B
❑Yes
❑ No OWA
Samples Arrived within Hold Time
11yes
❑ No ONIA
Rush TAT requested an COC
[]Yes
b No ONIA
Sufficient Volume
Yes
❑ No ON/A
Correct Containers Used
4 Yes
❑ No ON/A
Containers Intact
i 1)es
❑ No ON(A
Sample Labels match CDC (sample IN & date/fime of
N
collection)
es
El No ON/A
All containers needing acidibase preservation have been
Preservafion Infonnafion:
checked.
Oyes
❑ NGNON/A
Preservative:
All Containers needing preservation are found to be in
Lot #/!race #:
compliance with EPA recommendation:
OYes
❑ No �N/A
Date: Time.
Exceptions: VOA, Coliform, TOO, O&G, Carbamates
\
Inifials:
Headspace in VOA Vials? (>Smm):
❑Yes
O No N/A
Trip Blank Present:
OYss
❑ No ON/A
Client Notificationl Resolution:
Person Contacted:
Comments! Resolution (use back for additional comments):
Project Manager Review: Date: Page 20 of 20

HOWARD FERTILIZER
CLASS A
BIOSOLIDS ANALYSIS
Residual Type: Wastewater Treatment Plant (Pinellas)
Date Sampled: July 2, 2019
South Cross Raven WRF Ord Ouarter 20191
Mineralization Rate 0.30 92.00 % Solids
6.8 pH
Permit No. W00037094
Parameter
I %
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
5.080
50,800.000
101.600
Phosphorus
3.530
35,300.000
70.600
Potassium
0.251
2,510.000
5.020
PAN (injected)*
1.661
16,605.000
33.210
PAN (surface)*
1.564
15,635.000
31.270
Ammonia Nitrogen
0.194
1,940.000
3.880
Calcium
3.110
31,100.000
62.200
Calcium Carbonate Eq.
--
--
Magnesium
---
6,140.000
12.280
Sodium
---
1,240.000
2.480
Sulfur
---
___
___
Nitrate N / Nitrite N
---
7.000
0.014
Barium
---
---
-_-
Chloride
---
---
___
Iron
---
---
_--
Aluminum
---
28,300.000
56.600
Arsenic
5.900
0.012
Cadmium
---
1.200
0.002
Chromium
34.100
0.068
Copper
---
595.000
1.190
Lead
---
14.900
0.030
Mercury
---
0.240
0.000
Molybdenum
---
10.600
0.021
Nickel
---
25.300
0.051
Selenium
4.200
0.008
Zinc
---
708.000
1.416
Pace Analvtical 35479123
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia Nt) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are. listed as detection limits
for calculation purposes.
SAR
1.61
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

aceAnalytical
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July 12, 2019
William Reyes
Synagro
RE: Project: Pelletizer
Pace Project No.: 35479123
Dear William Reyes:
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 02, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
olh--e-
Cameron Meynardie
[e-mail]
[phone]
Project Manager
Enclosures
cc: Robert Ervin, Synagro
*`e140R)X100
I
REPORT OF LABORATORY ANALYSIS
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CERTIFICATIONS
Pace Analytical Services, LLC
110 South Sayvlew Blvd.
Oldsmar , FL 34677
[phone]
Project: Pelletizer
Pace Project No.: 35479123
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Missouri Certification #: 236
Alaska DEC- CSIUSTILUST
Montana Certification #: Cert 0074
Alabama Certification #: 41320
Nebraska Certification: NE-OS-28-14
Arizona Certificatlon#AZ0819
New Hampshire Certification #. 2958
Colorado Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
Connecticut Certification #: PH-0216
New York Certification #: 11608
Delaware Certification: FL NELAC Reciprocity
North Carolina Environmental Certificate #: 667
Florida Certification #: E83079
North Carolina Certification #: 12710
Georgia Certification #: 955
North Dakota Certification #: R-216
Guam Certification: FL NELAC Reciprocity
Oklahoma Certification #: D9947
Hawaii Certification: FL NELAC Reciprocity
Pennsylvania Certification M 68-00547
Illinois Certification #: 200068
Puerto Rico Certification #: FLO1264
Indiana Certification: FL NELAC Reciprocity
South Carolina Certification: #96042001
Kansas Certification #: E-10383
Tennessee Certification #: TN02974
Kentucky Certification #: 90050
Texas Certification: FL NELAC Reciprocity
Louisiana Certification #: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Virginia Environmental Certification #: 460165
Maryland Certification: #346
West Virginia Certification #: 9962C
Michigan Certification #: 9911
Wisconsin Certification #: 399079670
Mississippi Certification: FL NELAC Reciprocity
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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I
Project: Pelletizer
Pace Project No.: 35479123
Lab ID Sample ID
35479123001 Pellet
SAMPLE SUMMARY
Matrix Date Collected Date Received
Solid 07102/1915:00 0710211915:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wdtten consent or Pace Analytical Services, LLC.
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
110 South Bayview, Blvd.
Oldsmar, FL 34877
[phone]
Project:
Pace Project No.:
Pellefizer
35479123
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
35479123001
Pellet
EPA6010
LEC
18
PASI-O
EPA 7471
CS2
1
PASI-O
ASTM D2974-87
CLT
1
PASI-O
SM 2540G
MRS
1
PASI-O
SM 254OG
MRS
1
PASI-O
EPA 9045
AGS
1
PASI-O
ASTM D5057
JDW
1
PASI-O
TKN-NH3 Calculation
JMD
1
PASI-O
EPA350.1
MAJ
1
PASI-O
EPA3512
JMD
1
PASI-O
EPA 353.2
KAW
2
PASI-O
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project Pelletizer
Pace Project No.: 35479123
Sample: Pellet Lab ID: 35479123001 Collected: 07102119 15:00 Received: 07/02/19 15:33 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
6010 MET ICP
Arsenic
Boron
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Phosphorus
Potassium
Selenium
Sodium
Sulfur
Zinc
7471 Mercury
Mercury
Percent Moisture
Percent Moisture
254OG Total Solids
Total Solids
254OG Total Volatile Solids
Total Volatile Solids
9045 pH Soil
pH at 25 Degrees C
Specific Gravity/Bulk Density
Specific Gravity
Total Organic Nitrogen Soil
Total Organic Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
Date: 07/1212019 04:00 PM
Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 6010 Preparation Method: EPA 3050
5.9
mg/kg
0.65
0.33
1
07/08/19 17:46
07/10/19 20:02
7440-38-2
63.7
mg/kg
3.3
1.6
1
07/08/19 17:46
07/10119 20:02
7440-42-8
1.2
mg/kg
0.065
0.033
1
07/08/19 17:46
07/10/19 20:02
7440-43-9
31100
mg/kg
327
164
10
07/08/19 17:46
07/10/19 20:06
7440-70-2
34.1
mg/kg
0.33
0.16
1
07/0811917:46
0711011920:02
7440-47-3
595
mg/kg
32.7
16.4
100
07/08/19 17:46
07111/1912:14
7440-50-8
7490
mglkg
26.2
13.1
10
07/08/19 17:46
07/10/19 20:06
7439-89-6
14.9
mg/kg
0.65
0.33
1
07/08/19 17:46
07/10/19 20:02
7439-92-1
6140
mpg
32.7
16.4
1
07/08/19 17:46
07/10119 20:02
7439-95-4
185
mg/kg
3.3
1.6.
10
07/08/19 17:46
07/10/19 20:06
7439-96-5
10.6
mg/kg
0.65
0.33
1
07/08/19 17:46
07/10/19 20:02
7439-98-7
25.3
mg/kg
0.33
0.16
1
07/08119 17:46
07/10/19 20:02
7440-02-0
35300
mg/kg
32700
16400
500
07/0811917:46
0711111912:17
7723-14-0
2510
mg/kg
65.4
32.7
1
07/0811917:46
07/10/19 20:02
7440-09-7
4.2
mg/kg
0.98
0.49
1
07/08/19 17:46
07/10/19 20:02
7782-49-2
1240
mg/kg
65.4
32.7
1
07/08/19 17:46
07/10119 20:02
7440-23-5
11000
mglkg
654
327
10
07/08/19 17:46
07/10/19 20:06
708
mg/kg
13-1
8.5
10
07108/19 17:46
07/10/19 20:06
7440-66-6
Analytical Method: EPA
7471 Preparation Method: EPA 7471
0.24
mg/kg
0.0099
0.0049
1
07/09/1915:54
07/10/1914:08
7439-97-6 J(M1)
Analytical Method: ASTM
D2974-87
6.1
%
0.10
0.10
1
07/08/19 08:58
Analytical Method: SM 254OG
92.0
%
0.0010
0.0010
1
07/08/19 17:46
Analytical Method: SM 254OG
70.0
%
0.0010.
0.0010
1
07/08(1917:46
Analytical Method: EPA 9045
6.8 Sid. Units 0.10 0.10 1
07/10/19 13:45 Q
Analytical Method: ASTM D5057
0.620 1
07/11/1914:21 N2
Analytical Method: TKN-NH3 Calculation
48900 mg/kg 21.3 21.3 1
07/12/19 08:54
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1
1940 mg/kg 9.0 3.0 10 07/09/1912:20
07109/1914:44 7664-41-7 M6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
vAthout the written consent of Pace Analytical Services, I.I.C.
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(�Iaceilnalyfical'
m ..pacslabsxom
ANALYTICAL RESULTS
Project: Pelletizer
Pace Project No.: 35479123
Pace Analytical Services, LLC
110 South Baymew Blvd.
Oldsmar, FL 34677
[phone]
Sample: Pellet Lab ID: 35479123001 Collected: 07102119 15:00 Received: 07102119 15:33 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
. Parameters Results Units PQL MDL DF Prepared Analyzed CAS No, Qual
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Date: 07/12/2019 04:00 PM
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2
50800 mg/kg 876 438 10 07/07/1911:23 07/09/1916:00 7727-37-9
Analytical Method: EPA 353.2 Preparation Method: EPA 353.2
4.2 mglkg 0.53 0.27 1 07/03119 09:34 07/03/19 13:23
2.8 mglkg 0.53 027 1 07/03/19 09:34 07/03119 13:23 14797-55-8
REPORT OF LABORATORY ANALYSIS
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Without the written consent of Pace Analytical Services, LLC.
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ace Analytical
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QUALITY CONTROL DATA
Pace Analytical Services; LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pelletizer
Pace Project No.: 35479123
QC Batch: 552534
Analysis Method:
EPA 7471
QC Batch Method: EPA 7471
Analysis Description:
7471 Mercury
Associated Lab Samples: 35479123001
METHOD BLANK: 2995974
Matrix: Solid
Associated Lab Samples: 35479123001
Blank Reporting
Parameter Units
Result Limit
MDL Analyzed Qualifiers
Mercury mg/kg
0.0059 1 0.0099 0.0049 07/10/19 13:57
LABORATORY CONTROL SAMPLE: 2995975
Spike LCS
LCS %Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/kg
0.087 0.081
94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2995976 2995977
MS MSD
35479123001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg 0.24
0.1 0.083 0.33
0.28 93 48 80-120 17 20 J(M1)
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2019 04:00 PM without the written consent of Pace Analytical Services, L-C.
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laceAnalyticals
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QUALITY CONTROL DATA
Project: Pelletizer
Pace Project No.: 35479123
QC Batch: 552263 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid
Associated Lab Samples: 35479123001
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
METHOD BLANK: 2994130
Associated Lab Samples: 35479123001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed Qualifiers
Arsenic
mg/kg
0.31 U
0.61
0.31
07/10/1919:49
Boron
mg/kg
1.5 U
3.1
1.5
07/10/1919:49
Cadmium
mg/kg
0.031 U
0.061
0.031
07/1011919:49
Calcium
mg/kg
15.3 U
30.6
15.3
07110/1919:49
Chromium
mg/kg
0.15 U
0.31
0.15
07/10/1919:49
Copper
mg/kg
0.15 U
0.31
0.15
07/09/1917:28
Iron
mg/kg
1.2 U
2.4
1.2
07/1011919:49
Lead
mg/kg
0.31 U
0.61
0.31
07/1011919:49
Magnesium
mg/kg
15.3 U
30.6
15.3
07/10/1919:49
Manganese
mg/kg
0.15 U
0.31
0.15
07/10/1919:49
Molybdenum
mg/kg
0.31 U
0.61
0.31
07/10/1919:49
Nickel
mg/kg
0.15 U
0.31
0.15
07/1011919:49
Phosphorus
mg/kg
30.6 U
61.2
30.6
0711011919:49
Potassium
mg/kg
30.6 U
61.2
30.6
07/10/1919:49
Selenium
mg/kg
0.46 U
0.92
0.46
07/10/1919:49
Sodium
mg/kg
30.6 U
61.2
30.6
07/1011919:49
Sulfur
mg/kg
30-6 U
61.2
30.6
07/1011919:49
Zinc
mg/kg
0.61 U
1.2
0.61
07/10/1919:49
LABORATORY CONTROL SAMPLE:
2994131
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
15.5
12.9
83
80-120
Boron
mg/kg
77.5
63.1
81
80-120
Cadmium
mg/kg
1.6
1.4
90
80-120
Calcium
mg/kg
775
701
90
80-120
Chromium
mg/kg
15.5
14.2
91
80-120
Copper
mg/kg
15.5
14.7
95
80-120
Iron
mg/kg
155
142
92
80-120
Lead
mg/kg
15.5
14.1
91
80-120
Magnesium
mg/kg
775
642
83
80-120
Manganese
mg/kg
15.5
14.2
91
80-120
Molybdenum
mg/kg
15.5
14.0
90
80-120
Nickel
mg/kg
15.6
14.1
91
80-120
Phosphorus
ni
15.5
31.0 U
83
M120
Potassium
mg/kg
775
659
85
80-120
Selenium
mg/kg
15.5
13.2
85
80-120
Sodium
mglkg
775
688
89
80-120
Sulfur
mg/kg
155
133
85
80-120
Zinc
ni
77.5
70.3
91
80-120
Results presented an this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pelletizer
Pace Project No.: 35479123
Pace Analytical Services, LLC
110 South Bayvlew Blvd.
Oldsmar, FL 34677
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2994132
2994133
MS
MSD
35479160004
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mg/kg
1.6
17.3
17.1
14.2
14.4
72
74
75-125
1
20 J(M1)
Boron
mglkg
1.8 U
86.6
85.5
59.8
61.3
68
71
75-125
2
20 J(M1)
Cadmium
mg/kg
0.060 1
1.7
1.7
1.2
1.2
64
69
75-125
6
20 J(M1)
Calcium
mglkg
233000
866
855
196000
225000
4310
-965
75-125
14
20 J(M1),
L
Chromium
mg/kg
23.0
17.3
17.1
51.9
43.2
167
118
75-125
18
20 J(M1)
Copper
mg/kg
1.6
17.3
17.1
15.8
16.2
82
85
75-125
2
20
Iron
mg/kg
7140
173
171
10800
8800
2120
976
75-125
20
20 J(M1),
L
Lead
mglkg
3.7
17.3
17.1
17.0
16.2
77
73
75-125
5
20 J(MI)
Magnesium
mg/kg
990
866
855
2050
1920
122
109
75-125
6
20
Manganese
mglkg
22.0
17.3
17.1
48.5
43.0
153
122
75-125
12
20 J(M1)
Molybdenum
mglkg
0.35 U
17.3
17.1
11.4
11.8
65
69
75-125
4
20 J(M1)
Nickel
mg/kg
3.2
17.3
17.1
18.3
17.0
87
81
75-125
7
20
Phosphorus
mglkg
59.0 1
17.3
17.1
93.7
81..4
200
131
75-125
14
20 J(M1)
Potassium
mg/kg
149
866
855
1090
1060
109
107
75-125
3
20
Selenium
mg/kg
0.53 U
17.3
17.1
9.9
11.0
54
62
75-125
11
20 J(M1)
Sodium
mg/kg
120
866
855
881
888
88
90
75-125
1
20
Sulfur
mg/kg
201
173
171
285
295
48
55
75-125
4
20 J(M1)
Zinc
ni
1.9
86.6
85.5
60.2
60.4
67
68
75-125
0
20 J(Mt)
Results presentetl on this page are In the units indicated by the 'units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 9 of 20

11�2ceAnaljftalo
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL34677
[phone]
Project: Pelletizer
Pace Project No.: 35479123
QC Batch: 552068
Analysis Method:
ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 35479123001
SAMPLE DUPLICATE: 2993351
35476902001
Dup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Percent Moisture
%
94.5
94.6 0
10
SAMPLE DUPLICATE: 2993352
35478902001
Dup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Percent Moisture
%
17.6
17.5 0
10
SAMPLE DUPLICATE: 2993353
35478902010
Dup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Percent Moisture
%
16.4
16.4 0
10
SAMPLE DUPLICATE: 2993354
35479794001
Dup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Percent Moisture
%
17.0
17.0 0
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pelletizer
Pace Project No.: 35479123
QC Batch: 551983 Analysis Method: SM 254OG
QC Batch Method: SM 254OG Analysis Description: 254OG Total Solids
Associated Lab Samples: 35479123001
SAMPLE DUPLICATE: 2993091
Parameter
Total Solids
SAMPLE DUPLICATE: 2994198
Parameter
Total Solids
35479666001 Dup
Units Result Result
% 2.8 2.8
10481709002 Dup
Units Result Result
% 76.4 75.4
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Max
RPD RPD Qualifiers
1 5
Max
RPD RPD Qualifiers
1 5
Results presented on this page are In the units Indicated by the "Bnas" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical e
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Project Pelletizer
Pace Project No.: 35479123
QC Batch: 551984
OC Batch Method: SM 254OG
Associated Lab Samples: 35479123001
METHOD BLANK: 2993093
Associated Lab Samples: 35479123001
Parameter
Total Volatile Solids
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar. FL 34677
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 254OG
Analysis Description: 2540E Total Volatile Solids
Matrix: Solid
Blank Reporting
Units Result Limit MDL Analyzed Qualifiers
% 0.0010 U 0.0010 0.0010 07/0811917:55
SAMPLE DUPLICATE: 2993094
35479666001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Tatal Volatile Solids % 65.6 65.6 0 5
SAMPLE DUPLICATE: 2994200
10481709002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Volatile Solids % 11.4 11.4 1 5
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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ace Analytical
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QUALITY CONTROL DATA
Project: Pelletizer
Pace Project No.: 35479123
Pace Analytical Services, LLC
110 South Bayvlew Blvd.
Oldsmar, FL 34677
1813)881-9401
QC Batch: 552858 Analysis Method: ASTM D5057
QC Batch Method: ASTM D5057 Analysis Description: Spec.GravitylBulk Density,ASTM D5057
Associated Lab Samples: 35479123001
SAMPLE DUPLICATE: 2998242
Parameter
Specific Gravity
35477980003 DUp
Units Result Result
1.01 1.01
Max
RPD RPD Qualifiers
0 N2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
aceAnalytical ® 110 South Bayvlew Blvd.
Oldsmar, FL 34677
ww,vpacelabs.cam
[phone]
QUALITY CONTROL DATA
Project Pelletlzer
Pace Project No.: 35479123
QC Batch: 552412 Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1 Analysis Description: 350.1 Ammonia
Associated Lab Samples: 35479123001
METHOD BLANK: 2995448 Matrix: Solid
Associated Lab Samples: 35479123001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Ammonia mglkg 0.28 U 0.85 0.28 07/09/19 14:40
LABORATORY CONTROL SAMPLE: 2995449
Spike LCS LCS %Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 10.1 10.6 105 80-120
MATRIX SPIKE SAMPLE:
2995451
35479123001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/kg
1940
10.8
1950
66
80-120 M6
SAMPLE DUPLICATE: 2995450
35479123001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Nitrogen, Ammonia
mg/kg
1940
1950
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview, Blvd,
Oldsmar, FL 34677
[phone]
Project: Pellefizer
Pace Project No.: 35479123
QC Batch: 551822
Analysis Method:
EPA 351.2
QC Batch Method: EPA351.2
Analysis Description:
351.2 TKN
Associated Lab Samples: 35479123001
METHOD BLANK: 2992288
Matrix: Solid
Associated Lab Samples: 35479123001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Nitrogen, Kjeldahl, Total
mglkg
42.7 U 85.5 42.7
07/09/19 15:56
LABORATORY CONTROL SAMPLE: 2992289
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
%Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
2890 2810
97
90-110
MATRIX SPIKE SAMPLE: 2992291
35479402001 Spike
MS
MS
%Rec
Parameter
Units
Result Conic.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
82100 16500
93500
69
90-110 M6
SAMPLE DUPLICATE: 2992290
35479402001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
82100 81300 1
20
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit la presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pelletizer
Pace Project No.: 35479123
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
QC Batch: 551201
Analysis Method: EPA 353 9
QC Batch Method: EPA 363.2
Analysis Description: 353.2 Nitrate
+ Nitrite
Associated Lab Samples: 35479123001
METHOD BLANK: 2989093
Matrix: Solid
Associated Lab Samples: 35479123001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
0.25 U 0.50
0.25 07/03/19 13:15
Nitrogen, NO2 plus NO3
mg/kg
0.25 U 0.50
0.25 07/03/19 13:15
LABORATORY CONTROL SAMPLE:
2989094
Spike LCS LCS
% Rec
Parameter
Units
Cone. Result %Rec
Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/kg
20 20.8 104
90-110
MATRIX SPIKE SAMPLE:
2989096
35478071001 Spike MS
MS % Rec
Parameter
Units
Result Cone. Result
% Rec Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/kg
734 2890 3650 101 80-120
SAMPLE DUPLICATE: 2989095
35478071001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Nitrogen, Nitrate
mg/kg
266 868
106 20 J(D6)
Nitrogen, NO2 plus NO3
mg/kg
734 868
17 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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01/
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QUALIFIERS
Project: Pelletizer
Pace Project No.: 35479123
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
140 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
PQL- Practical Quantitation Limit.
RL- Reporting Limit- The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
U Compound was analyzed for but not detected.
J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory
control limits.
J(Mi) Estimated Value. Matrix spike recovery exceeded QC limits. Balch accepted based on laboratory control sample (LCS)
recovery.
L Off -scale high. Actual value is known to be greater than value given.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELACITNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
Q Sample held beyond the accepted holding time. Analysis initiated more than 15 minutes after sample collection.
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project:
Pace Project No.:
Pelletizer
35479123
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
35479123001
Pellet
EPA 3050
552263
EPA6010
552324
35479123001
Pellet
EPA 7471
552534
EPA 7471
552732
35479123001
Pellet
ASTM D2974-87
552068
36479123001
Pellet
SM 2540G
551983
36479123001
Pellet
SM 2540G
551984
35479123001
Pellet
EPA 9045
552876
35479123001
Pellet
ASTM D5057
552858
35479123001
Pellet
TKN-NH3 Calculation
553455
35479123001
Pellet
EPA 350.1
552412
EPA 350.1
552505
35479123001
Pellet
EPA 351.2
551822
EPA 351.2
552479
35479123001
Pellet
EPA 353.2
551201
EPA 353.2
551309
Date: 07/12/2019 04:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 20

SYNAGRO
5900 74d1 Suety Nuyyh
Sy. Pon , hun„ IL 13709
Phone [phone]
Fax [phone]
CHAIN OF CUSTODY RECORD
No
2
N
MAILING ADDRESS: '6
SYNAGRO m
P.O. Box 3227 w
Pinellas Park. FL 33780 p
PROJECT I PROJECT NAME
Pinellas County I LABORATORY:
PARAMETERS
# 29-0750
Pelletizer
SAMPLERS (Signature
(Pr' 1)`w
SAMPLE NUMBER DATE TIME
a y
o ¢ a o
o w ao
6
0 3 m m
a o g
a° :s
LOCATIONm
-2-t°I
16-00
u7
✓(,L
1
'�
i`nv p n
PARAMETERS
4-0
A
`yd'
SAMPLE NUMBER DATE TIME sc g is g pQ' c SAMPLE REMARKS
.9 Q x 4� Q�c �F Q� �, gy�yC p eo �e �r LOCATIIION
Relinquished By(S&Xalum) DWeM""' WO## : 35479123
Reeelmaby. nalum,
%(afro Is33?4
(Ptlnl) INN)
II�II�III�IIII�I�IIIII
35479123
Relinqukhetl S' lu J
DataTma
ftmwW br L.W.1t,ry It, (S19.1 m)
oatR ma
Remarks
IPylnll ^. 1
(Print)

ocumenName:
Llocument Havised:
aCeAoa/N/ca!
Sample Condition Upon Receipt Form
May 30, 2018
cumen o.:
F-FL-C-007 rev. 13
ssumg on ;
Pace Florida Quality Office
Sample•
• •n Upon Receipt
Project # WO#
: 35479123
Date and Initials ofp�r� 11
Project Manager: PM: CEM
Oue Date: 07/12/19
Examining contents: !! i / 9
Client: CLIENT:
37-SYNAGRO
Label: J
Deliver:
pH: IV /
Thermometer Used: T-203
Date: �b/I� Time:
Initials: MV6-
State of Origin: FL
❑ For WV projects, all containers verified to s6 •C
Cooler#1 Temp1C � • K (Visual) 0.0
(Correction Factor i
) (Actual)
11
Samamples on ice, cooling process has begun
Cooler#2 Tdmp.•C (Visual)
(Correction Factor) -(Actual)
❑ ples on ice, cooling process has begun
Cooler#3 Temp.-C (Visual)
(Correction Factor) (Actual)
)
Samples on ice, coolie
❑ Samp g process has begun
Cooler#4 Temp.'C (Visual)
(Correction Factor) (Actual)
❑ Samples an Ice, cooling process has begun
Cooler#6 Temp.'C (Visual)
(Correction Factor) Actual)
❑ Samples on ice, cooling process has begun
Cooler #6 Temp.'C (Visual)
(Correction Factor) (Actual)
❑ Samples on ice, coaling process has begun
�&Client
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Commercial ❑ Pace
❑ Other
Shipping Method: ❑ First Overnight ❑ Priority' Overnight ' 0 Standard Overnight ❑ Ground ❑ International Priority
❑ Other
Billing: ❑ Recipient
Tracking #
❑ Sender ❑ Third Party O Credit Card ❑ Unknown
Custody Seal on Cadler/Box Present: —❑Yes No
Packing Material: ❑Bubble Wrap �9ubble Bags ❑None
Samples shorted to lab (If Yes, complete)\ Shorted Date:
Seals Intact: ❑ Yes ❑ No
[I Other
P ,..e 4.
Ice: \Wet')Blue Dry None
Shorted Time, City:
Chain of Custody Present
AYes
❑ No ONIA
Chain of Custody Filled Out
�EfYes
0 No ON/A
Relinquished Signature & Sampler Name COG
,Z�ft/es
❑ No ON/A
Samples Arrived within Hold Time
; C1Yes
Cl No ON/A
Rush TAT requested an CDC
Oyes
ErNo ON/A
Sufficient Volume
idYes
❑ No ONIA
Correct Containers Used
DYes
❑ No ONIA
Containers Intact
Oyes
❑ No ON/A
Sample Labels match CDC (sample IDs & datenime or
collection)
,•OYes
❑ No ON/A
All containers needing acidibase preservation have been
�
Preservation Information:
checked.
Oyes
❑ N0,C]NIA
Preservative:
All Containers needing preservation are round to be in
/
Lot #/Trace#:
compliance with EPA recommendation:
Dyes
❑N0,61A
Date: Time:
Exceptions: VOA, Coliform, TOG, O&G, Carbamates
Initials:
Headspace in VOA Vials? (>6mm):
OYes
❑ No pNIA
Trip Blank Present:
OYes
❑ No AIA
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution (use back for additional
Project Manager Review:
20 of 20

HOWARD FERTILIZER
CLASS A
BIOSOLIDS ANALYSIS
Residual Type: Wastewater Treatment Plant (Pinellas)
Date Sampled: October 2, 2019
South Cross Bayou WRIT (4th Quarter 2019) Permit No. W00037094
Mineralization Rate 0.30 93.20 % Solids
7.0 pH
Parameter % Mg/Kg Dry Weight I Pounds/DryTon
(% x 10.000) (Ma/Ka x 0.002)
Carbonate
N / Nitrite N
2,710.000
15,953.900
14,998.900
1,910.000
33,600.000
6,320.000
1,330.000
6.900
28,300A00
10.000
1.500
41.600
580.000
12.100
41.400
4.700
756.000
Pace Analytical 35501902
67.800
5.420
31.908
29.998
3.820
67.200
12.640
0.014
56.600
0.083
1.160
0.036
0.001
0.024
0.083
0.009
1.512
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N +Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
1.68
Ceiling Concert.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

aceAnalytical
ww xpacolabxwm
October 14. 2019
William Reyes
Synagro
RE: Project: Pinellas County Pelletizer
Pace Project No.: 35501902
Dear William Reyes:
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, Fl- 34677
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 02, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
0114-1—
Cameron Meynardie
[e-mail]
813-855-1844
Project Manager
Enclosures
cc: Robert Ervin, Synagro
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Page 1 of 20

aceAnalytical e
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CERTIFICATIONS
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Missouri Certification #: 236
Alaska DEC- CS/UST/LUST
Montana Certification #: Cart 0074
Alabama Certification #: 41320
Nebraska Certification: NE-OS-28-14
Arizona Certification# AZO819
New Hampshire Certification #: 2958
Colorado Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
Connecticut Certification #: PH-0216
New York Certification #: 11608
Delaware Certification: FL NELAC Reciprocity
North Carolina Environmental Certificate #: 667
Florida Certification #: E83079
North Carolina Certification #. 12710
Georgia Certification #: 955
North Dakota Certification #: R-216
Guam Certification: FL NELAC Reciprocity
Oklahoma Certification #: D9947
Hawaii Certification: FL NELAC Reciprocity
Pennsylvania Certification #: 68-00547
Illinois Certification #: 200068
Puerto Rico Certification #: FL01264
Indiana Certification: FL NELAC Reciprocity
South Carolina Certification: #96042001
Kansas Certification #: E-10383
Tennessee Certification #: TNO2974
Kentucky Certification #: 90060
Texas Certification: FL NELAC Reciprocity
Louisiana Certification #: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Louisiana Environmental Certificate M 05007
Virginia Environmental Certification #: 460165
Maryland Certification: #346
West Virginia Certification M 9962C
Michigan Certification #: 9911
Wisconsin Certification #: 399079670
Mississippi Certification: FL NELAC Reciprocity
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical
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SAMPLE SUMMARY
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
Lab ID Sample ID Matrix Date Collected Date Received
35601902001 Pellet Solid 10/0211915:20 10/0211916:20
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 20

aceAnalytical
w .pacslsbsx=
I
SAMPLE ANALYTE COUNT
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
(013)BB1-9401
Lab ID Sample ID Method
Analysts
Analyses
Reported
Laboratory
35501902001 Pellet EPA6010
ATC, CS2,
18
PASI-O
LEC
EPA 7471
NMP
1
PASI-O
ASTM D2974-87
CLT
1
PASI-O
SM 2540G
MRS
1
PASI-O
SM 254OG
MRS
1
PASI-O
EPA 9045
AGS
1
PASI-O
ASTM D5057
JDW
1
PASI-O
TKN-NH3 Calculation
AEM
1
PASI-O
EPA 350.1
MAJ
1
PASI-O
EPA 351.2
JMD
1
PASI-O
EPA 353.2
MH1
2
PASI-O
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 20

aceAnalytical e
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
110 South 6ayview Blvd.
Oldsmar. FL 34677
[phone]
Project: Pinellas County Pellellzer
Pace Project No.: 35501902
Sample: Pellet
Lab ID: 35501902001 Collected:
10/02/19 15:20
Received: 10/02/19 16:20 Matrix: Solid
Results reported on a "dryweight"basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units PQL
MDL
OF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method: EPA 3050
Arsenic
10 mg/kg 1.1
0.54
1
10/0811916:23
10/09/1915:10
7440-38-2
Boron
57.3 mg/kg 5.4
2.7
1
10108/1916:23
10109/1915:10
7440-42-8
Cadmium
1.5 mg/kg 0.11
0,054
1
10/08/19 16:23
10/09/19 15:10
7440-43-9
Calcium
33600 mglkg 1080
542
20
10/0811916:23
10/11/1910:24
7440-70-2
Chromium
41.6 mg/kg 0.54
0.27
1
10/08/19 16:23
10/09/1915;10
7440-47-3
Copper
580 mg/kg 10.8
5.4
20
1010811916:23
10/11/1910:24
7440-50-8
Iron
9590 mg/kg 86.7
43.4
20
10/08/19 16:23
10/11/19 10:24
7439-89-6
Lead
17.8 mpg 1.1
0.54
1
10/08/19 16:23
10/09/19 15:10
7439-92-1
Magnesium
6320 mg/kg 54.2
27.1
1
10/0811916:23
10/09/1915:10
7439-954
Manganese
251 mg/kg 10.8
5.4
20
10/08/19 16:23
10111/19 10:24
7439-96-5
Molybdenum
12.1 mglkg 1.1
0.54
1
10/08/19 16:23
10/09/19 15:10
7439-98-7
Nickel
41.4 mg/kg 0.54
0,27
1
10108/1916:23
10/09/1915:10
7440-02-0
Phosphorus
33900 mg/kg 10800
5420
100
10/08/19 16:23
10111/19 15:56
7723-14-0
Potassium
2710 mg/kg 108
54.2
1
10/08/19 16:23
10/09/19 15:10
7440-09-7
Selenium
4.7 mg/kg 1.6
0,81
1
10/08/19 16:23
10/09/1915:10
778249-2
Sodium
1330 mg/kg 108
54.2
1
10108/1916:23
10109/1915:10
7440-235
Sulfur
11400 mg/kg 2170
1080
20
10/08/19 16:23
10/11/1910:24
Zinc
756 mglkg 43.4
21.7
20
10108/1916:23
10111/1910:24
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA
7471
Mercury
0.46 mg/kg 0.067
0.034
1
10/03/19 08:51
10/03/19 13:22
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
7.8 % 0.10
0.10
1
10/10/19 15:33
254OG Total Solids
Analytical Method: SM 254OG
Total Solids
93.2 % 0.0010
0.0010
1
10/03/19 16:11
254OG Total Volatile Solids
Analytical Method: SM 254OG
Total Volatile Solids
84.9 % 0.0010
0.0010
1
10/03/19 16:02
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.0 Sid. Units 0.10
0.10
1
10/11/19 14:14
Q
Specific Gravity/Bulk Density
Analytical Method: ASTM D5057
Specific Gravity
0.630
1
10/1111915:37
N2
Total Organic Nitrogen Soil
Analytical Method: TKN-NH3 Calculation
Total Organic Nitrogen
46800 mg/kg 21.7
21.7
1
10/11/19 18:00
350.1 Ammonia
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1
Nitrogen, Ammonia
Isla mg/kg 9.2
3.1
10
10107/1911:54
10/08/1911:09
766441-7 M6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Dale: 10/14/2019 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20

(�IaceAnalytcal'
a ,Pacelab&Wrn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
110 South Bayview Blvd,
Oldsmar, FL34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
Sample: Pellet Lab ID: 35501902001 Collected: 1010211915,20 Received: 10/02/1916:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qua[
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Preparation Method: EPA 351.2
Nitrogen, Kjeldahl, Total 48700 mg/kg 4010 2000 50 10/1011912:15 10/11/1916:25 7727-37-9
353.2 Nitrogen, N021NO3 Analytical Method: EPA 353.2 Preparation Method: EPA 353.2
Nitrogen, NO2 plus NO3 4.0 mg/kg 0.55 0.27 1 10/05/19 12:00 10/05/19 19:38
Nitrogen, Nitrate 2.9 mg/kg 0.55 0.27 1 10105/1912:00 10/05/1919:38 14797-55-8
Date: 10/14/2019 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 20

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QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
QC Batch: 575291 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 35501902001
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
METHOD BLANK: 3126635
Matrix: Solid
Associated Lab Samples: 35501902001
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed Qualifiers
Mercury
mg/kg
0.0049 U 0.0099
0.0049 1010311912:50
LABORATORY CONTROL SAMPLE:
3126636
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Mercury
mg/kg
0,098 0.094
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3126637 3126638
MS MSD
35601967001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg 0.0063 1 0.11 0.11 0.11 0.10 95 87 80-120 7 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2019 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 20

7ace Analytical
nwwparelabsxom
QUALITY CONTROL DATA
Project: Pinellas County Pellelizer
Pace Project No.: 35601902
QC Batch: 576670 Analysis Method: EPA 6010
QC Balch Method: EPA3050 Analysis Description: 6010 MET Solid
Associated Lab Samples: 35501902001
METHOD BLANK 3133955
Associated Lab Samples: 35501902001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Arsenic
mg/kg
0.30 U
0.60
0.30
10/09/1914:29
Boron
mglkg
1.5 U
3.0
1.5
10/09/1914:29
Cadmium
mg/kg
0.030 U
0.060
0.030
10/09/1914:29
Calcium
mg/kg
15.1 U
30.2
15.1
10/0911914:29
Chromium
mg/kg
0.15 U
0.30
0.15
10/0911914:29
Copper
mg/kg
0,15 U
0.30
0.15
10/09/1914:29
Iron
mg/kg
1.2 U
2.4
12
10/09/1914:29
Lead
mg/kg
0.30 U
0.60
0.30
1010911914:29
Magnesium
mg/kg
15.1 U
30.2
15.1
10/0911914:29
Manganese
mglkg
0.15 U
0.30
0.15
10/09/19 14:29
Molybdenum
mg/kg
0.30 U
0.60
0.30
10I09/1914:29
Nickel
mg/kg
0.15 U
0.30
0.15
10109/1914:29
Phosphorus -
mg/kg
30.2 U
60.5
30.2
10/0911914:29
Potassium
mglkg
30.2 U
60.5
30.2
1010911914:29
Selenium
mg/kg
0.45 U
0.91
0.45
10/0911914:29
Sodium
mg/kg
30.2 U
60.5
30.2
10/09/1914:29
Sulfur
mg/kg
302 U
60.5
30.2
10/09/1914:29
Zinc
mg/kg
0.60 U
1.2
0.60
10109/1914:29
LABORATORY CONTROL SAMPLE:
Parameter
3133956
Units
Spike
Conc.
LCS
Result
LCS
%Rec
% Rao
Limits
Arsenic
mg/kg
15.1
13.8
92
80-120
Boron
mg/kg
75.4
68.1
90
80-120
Cadmium
mg/kg
1.5
1.5
99
80-120
Calcium
mg/kg
754
770
102
80-120
Chromium
mg/kg
15.1
15.4
102
80-120
Copper
mg/kg
15.1
14.6
96
80-120
Iron
mg/kg
151
155
103
80-120
Lead
mg/kg
15.1
15.2
100
80-120
Magnesium
mg/kg
754
723
96
80-120
Manganese
mg/kg
15.1
15.2
100
80-120
Molybdenum
mg/kg
15.1
15.3
101
80-120
Nickel
mg/kg
15-1
15.2
100
80-120
Phosphorus
mglkg
15.1
30.2 U
95
80-120
Potassium
mglkg
754
735
98
80-120
Selenium
mg/kg
15.1
12.6
84
80-120
Sodium
mglkg
754
755
100
80-120
Sulfur
mg/kg
151
132
88
80-120
Zinc
mg/kg
75.4
75.1
100
80-120
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar , FL 34677
[phone]
Qualifiers
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column eacept where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2019 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 20

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project:
Pace Project No.:
Pinellas County Pelletizer
35501902
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3133957
3133958
MS
MSD
35501630001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mglkg
0.57 U
28.6
28.1
25.0
24.7
87
88
75-125
1
20
Boron
mg/kg
2.9 U
143
140
102
102
71
73
75-125
0
20 J(M1)
Cadmium
mg/kg
0.057 U
2.9
2.8
2.8
2.7
97
97
75-125
2
20
Calcium
mg/kg
151
1430
1400
1580
1590
99
103
75-125
1
20
Chromium
mglkg
0.79
28.6
28.1
29.1
29.0
99
101
75-125
0
20
Copper
mg/kg
12.2
28.6
28.1
41.0
40.8
100
102
75-125
0
20
Iron
mg/kg
67.2
286
281
378
383
108
113
75-125
1
20
Lead
mg/kg
0.57 U
28.6
28.1
28.3
28.1
99
100
75-125
1
20
Magnesium
mg/kg
28.7 U
1430
1400
1410
1390
96
98
75-125
1
20
Manganese
mg/kg
8.5
28.6
28.1
39.2
41.0
107
116
75-125
5
20
Molybdenum
mglkg
0.57 U
28.6
28.1
28.0
27.5
97
97
75-125
2
20
Nickel
mg/kg
0.29 U
28.6
28.1
28.5
28.3
99
101
75-125
0
20
Phosphorus
mglkg
529
28.6
28.1
651
643
425
406
75-125
1
20 J(M1),
L
Potassium
mg/kg
427
1430
1400
1960
1950
107
109
75-125
0
20
Selenium
mg/kg
0.86 U
28.6
28.1
24.7
23.9
84
83
75-125
3
20
Sodium
mg/kg
2070
1430
1400
3810
3750
121
120
75-125
2
20
Sulfur
mg/kg
2280
286
281
2830
2650
191
132
75-125
6
20 J(M1)
Zinc
mg/kg
2.9
143
140
145
142
99
99
75-125
2
20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/14/2019 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 20

aceAnal)&al
umwpacelabs.com
Project: Pinellas County Pellefizer
Pace Project No.: 36501902
QC Balch: 577378
QC Batch Method: ASTM 02974-87
Associated Lab Samples: 35501902001
SAMPLE DUPLICATE: 3138154
Parameter
Percent Moisture
SAMPLE DUPLICATE: 3138155
Parameter
Percent Moisture
Pace Analytical services, LLC
110 South Baywew Blvd.
Oldsmar, FL 34677
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
35502064001 Dup Max
Units Result Result RPD RPD Qualifiers
% 19.4 21.1 8 10
35502350004 Dup Max
Units Result Result RPD RPD Qualifiers
% 8.7 7.6 13 10 J(D6)
SAMPLE DUPLICATE: 3138156
35502522001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 84.5 84.5 0 10
SAMPLE DUPLICATE: 3138157
35503593004 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 20.2 17.0 17 10 J(D6)
Results presented an this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
� www.pacelabs.crom
QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
QC Balch: 575400 Analysis Method: SM 2540G
QC Balch Method: SM 2540G Analysis Description: 2540G Total Solids
Associated Lab Samples: 35501902001
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar , FL 34677
[phone]
SAMPLE DUPLICATE: 3127201
35501936001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 3.33.3 1 5
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/14/2019 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 20

(�IaceAnalXical'
i .pacefabsxona
QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
QC Balch: 575402 Analysis Method: SM 254OG
QC Batch Method: SM 2540G Analysis Description: 254OG Total Volatile Solids
Associated Lab Samples: 35501902001
METHOD BLANK: 3127210 Matrix: Solid
Associated Lab Samples: 35501902001
Blank Reporting
Parameter Units Result Limit
Total Volatile Solids % 0.0010 U 0.0010
SAMPLE DUPLICATE: 3127211
35501936001 Dup
Parameter Units Result Result
Total Volatile Solids % 65.4 65.1
Pace Analytical Services, LLC
110 South Bayview Blvd,
Oldsmar, FL 34M
[phone]
MDL Analyzed Qualifiers
0.0010 10103/1916:14
Max
RPD RPD Qualifiers
1 5
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/14/2019 04:50 PM without the written consent of Pace Analyltcal Services, LLC.
Page 12 of 20

aceAnalj6cal
mm..pacefabs. com
QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
013)881-9401
UC; Batch: 5775e7 Analysis Method: ASTM 05057
QC Batch Method: ASTM D5057 Analysis Description: Spec-Gravity/Bulk Density,ASTM D5057
Associated Lab Samples: 35501902001
SAMPLE DUPLICATE: 3140076
Parameter
Specific Gravity
35501653001 Dup
Units Result Result
1,00 1.00
Max
RPD RPD Qualifiers
0 N2
Results presented on this page are in the units Indicated by the "Units" column except Where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/14/2019 04:50 PM without the written consent of Pace Analytical Services, L-C. Page 13 of 20

IceAnalytical"
wn,ypacefabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
QC Batch: 576156
Analysis Method:
EPA 350.1
QC Batch Method: EPA350.1
Analysis Description:
350.1 Ammonia
Associated Lab Samples: 35501902001
METHOD BLANK: 3131769
Matrix: Solid
Associated Lab Samples: 35501902001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Nitrogen, Ammonia
mglkg
0.28 U 0.85 0.28
10/08/19 10:51
LABORATORY CONTROL SAMPLE:
3131770
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/kg
10.1 10.6
104
80-120
MATRIX SPIKE SAMPLE:
3132099
35501902001 Spike
MS
MS
%Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/kg
1910 11.1
2040
1180
80-120 M6
SAMPLE DUPLICATE: 3132098
35501902001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrogen, Ammonia
mglkg
1910 1940 1
20
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Dale: 10/14/2019 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20

ace Analytical
n .pacelabaoom
QUALITY CONTROL DATA
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
QC Balch: 577070 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 3512 TKN
Associated Lab Samples: 35501902001
METHOD BLANK: 3136393
Associated Lab Samples: 35501902001
Parameter Units
Nitrogen, Kjeldahl, Total mglkg
Matrix: Solid
Blank Reporting
Result Limit
39.6 U 79.2
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
MDL Analyzed Qualifiers
39.6 10/11/19 15:09
LABORATORY CONTROL SAMPLE:
3136394
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg.
1770 1710
96
90-110
MATRIX SPIKE SAMPLE:
3136396
35501839001 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
67900 15100
79800
79
90-110 i(MI)
MATRIX SPIKE SAMPLE:
3136398
35503176002 Spike
MS
MS
eta Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
11400 1940
12900
80
90-110 J(Mt)
SAMPLE DUPLICATE: 3136395
Parameter
Nitrogen, Kjeldahl, Total
SAMPLE DUPLICATE: 3136397
Parameter
Nitrogen, Kjeldahl, Total
35501839001 Dup
Units Result Result
mglkg 67900 59700
35503176002 Dup
Units Result Result
mglkg 11400 11600
Max
RPD RPD Qualifiers
13 20
Max
RPD RPD Qualifiers
2 20
Results presented on this page are in the units indicated by the" Bn[W column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
t .pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
QC Batch: 576007
Analysis Method: EPA3532
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate
+ Nitrite
Associated Lab Samples: 35501902001
METHOD BLANK: 3131193
Matrix: Solid
Associated Lab Samples: 35501902001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Nitrogen, Nitrate
mg/kg
0.25 U 0.50
025 10/05/1919:32
Nitrogen, NO2 plus NO3
mg/kg
0.25 U 0.50
0.25 10/05/19 19:32
LABORATORY CONTROL SAMPLE: 3131194
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Quallfiers
Nitrogen, NO2 plus NO3
mg/kg
19.8 20.8 105
90-110
MATRIX SPIKE SAMPLE: 3131196
35501839001 Spike MS
MS
%Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/kg
1.0 U 80.6 35.9 44
80-120 J(M1)
SAMPLE DUPLICATE: 3131195
35501839001 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Nitrogen, Nitrate
mgft
1.0 U 1.0 U
20
Nitrogen, NO2 plus NO3
mg/kg
1.0 U 1.0 U
20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This repod shall not be reproduced, except in full.
Date: 10/14/2019 04:50 PM without the written consent of Para Analytical Services, LLC. Page 16 of 20

000711
,�aoeAnajfyficalo
m ..pacelabs.mm
QUALIFIERS
Project: Pinellas County Pelletizer
Pace Project No.: 35501902
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL34677
[phone]
PQL- Practical Quantitation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-O Pace Analytical Servloes- Ormond Beach
ANALYTE QUALIFIERS
I The reported value is between the laboratory method detection limit and the laboratory practical quanlitation limit.
U Compound was analyzed for but not detected.
J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory
control limits.
J(M1) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS)
recovery.
L Off -scale high. Actual value is known to be greater than value given.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELACITNI accreditation for this parameter but other accreditation/certifications may apply. A
complete list of accreditations/certifications is available upon request.
O Sample held beyond the accepted holding time. Analysis initiated more than 15 minutes after sample collection.
REPORT OF LABORATORY ANALYSIS
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11�aceAnalytical e
i a .pacelabs.cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
110 South Bayview Blvd.
Oldsmar, FL 34677
[phone]
Project:
Pace Project No.:
Pinellas County Pelletizer
35501902
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
35501902001
Pellet
EPA 3050
576670
EPA6010
576724
35501902001
Pellet
EPA7471
575291
EPA 7471
575356
35501902001
Pellet
ASTM D2974-87
577378
35501902001
Pellet
SM 2540G
575400
35601902001
Pellet
SM 2540G
575402
35501902001
Pellet
EPA9045
577570
35501902001
Pellet
ASTM D5057
577587
35601902001
Pellet
TKN-NH3 Calculation
577821
35501902001
Pellet
EPA350.1
576156
EPA 350.1
576246
35501902001
Pellet
EPA 351.2
577070
EPA 351.2
577611
35501902001
Pellet
EPA 353.2
576007
EPA 353.2
576026
Date: 10/14/2019 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, -I-C.
Page 18 of 20

SYNAGRO Phone [phone]
59M 74,1, N,,,,I, Fax [phone]
S,. Nw.1mx, FL 33709
CHAIN OF CUSTODY RECORD
-, ,
0
WO#:35501902
a
PROJECT
PROJECT NAME
Pinellas CountY
LABORATORY:
IIIIIIIIIIIIIIIIIIIIII
PP501902
# 29-0750
Pelletizer
Po -c s
355
SAMPLERS (Signature)
/� t j p _
(Print) (]
aw 2we
y
� obG� �(�✓ i n1 W� de
q=' YQ� ? Fo
SAMPLENUMBER
w
DATE TIME
oiJ�
w �P o4 .`a" �-Q aJ c'=w 3F
s E a o0 Al SAMPLE
w w o
2' a ao yJ
w LOCATION
P� l e
to a-
! tS
�Z
✓
��.
!
✓
✓
✓
✓
N/•,�..1 �3;.�
PARAMETERS
0
w >
O rCi01,
z w°9 Pg we ea' w4u �tv $= m SAMPLE
SAMPLE NUMBER DATE TIME c
=p. g � � �` � a� $F s
d' d` d' d` d'
�i e-�
D;Z-1
�S-d
I
✓d`
✓
✓d'
Fina.,� bin
It, N. 6 •;-o

ocumen ame:
u0cument Kevised:
aceAna/N/ aP
Sample Condition Upon Receipt Form
May 30, 2018
issuing u on :
F-FL-C-007 rev. 13
Pace Florida Quality Office
LIN 35501902
Project #
Due Dale: 10/11/19
Date and Initials of person:l
Project Manager: PM:
CEM
Examining contentg:
CLIENT:
37—sYNRGRO
Label: i / iz 1 I
Client:
Deliver;
pH.
Thermometer Used: T-203
Date: I Time:
f YYY
1 Lac- Initial,
State of Origin: FL
❑ For VJV projects, all containers venfied to C
Cooler #1 Temp.'C. ( ! L(Vlsual)
-0.1 (Correction Factor) 7 -3 (Actual)
p X Samles on ice, cooling process has begun
Cooler#2 Temp.'C (Visual)
(Correction Factor) (Actual)
❑ Samples on ice, cooling process has begun
Cooler#3 Temp.'C (Visual)
(Correction Factor) _(Actual)
❑ Samples an ice, wolfing process has begun
Cooler#4 Tomp.'C (Visual)
(Correction Factor) (Actual)
❑ Samples an ice, cooling process has begun
Cooler#6 Temp.'C (Visual)
(Correction Factor) (Actual)
❑ Samples on ice, cooling process has begun
Cooler#6 Temp.'C (Visual)
(Correction Factor) (Actual )
❑ Samples an ice, cooling process has begun
Courier: ❑ Fed Ex ❑ UPS
r�{/'
❑ USPS 0 Client ❑ Commercial ❑ Pace ❑Other
Shipping Method: ❑ First Overnight ❑ Priority Owimight ❑ Standard Overnight ❑ Ground ❑ International Priority
❑ Other
Billing: ❑ Recipient ❑ Sender ❑ Third Party
Tracking #
Custody Seal an Cooler/Box Present: ❑Yes ❑No
Packing Material: ❑Bubble Wrap Bubble Bags ❑None
Samples shorted to lab (If Yes, compete) Shorted Date:
❑ Credit Card ❑ Unknown
Seals intact: ❑ Yes ❑No
❑ Other
Ice: ( Wet Pl'ue Dry None
Shorted Time: Oty:
Chain of Custody Present
OYes
❑ No ON/A
Chain of Custody Filled Out
0les
❑ No ON1A
Relinquished Signature & Sampler Name COG
OYes
❑ No ON/A
Samples Arrived within Hold Time
,,.. OYes
❑ No ONlA
Rush TAT requested on CDC
OYes
.O"No ON/A
Sufficient Volume
­OYes
❑ No ElN1A
Coned Containers Used
IOYes
❑ No ON/A
Containers Intact
.OYes
❑ No ON/A
Sample Labels match COG (sample IDs & detelume of
collection)
OYes
❑ No ON/A
All containers needing acid/base preservation have been
checked. OYes
All Containers needing preservation are found to be in
compliance with EPA recommendation: OYes
Exceptions: VOA, Conform, TOG, 0&G, Carbamates
✓
❑ No ON/A
❑ No ON/A
f
Preservation Information:
Preservative:
Lot #?race #:
Dale: Time:
Initials:
Headspace In VOA Vials? ( >6mm):
OYes
❑ No,ON/A
Trip Blank Present:
OYes
❑ No .ON/A
Client Notlflcalionl Resolution:
Person Contacted:
Comments/ Resolution (use back for additional
Project Manager Review: _ Date: Page 20 of 20

CERTIFICATION
"I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: January 2019
Name: William Re s — Pl�nt/I/�anage Synagro
Signature:.L/L/ L Date:1-Feb-2018
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
"I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: February 2019
Name: William Rgyesl—Plant an er Synagro
Signature: �.� Date: 1-M rch-2018
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: March 2019 f%\J
Name: William Reyes— Plant a age' r Synagro
Signature: Gti a Date:1-April-2018
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
"I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements In §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: April 2019
Name: William eye — PI nt an ger Synagro
Signature: Date:1-Mav-2019
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
"I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: May 2019
Name: William Reyes— lant Me age Synagro
Signature:��/L_ Date: 1-June-2019
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
1 certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: June 2019
Name: William Reyes - Plant M age Synagro
Signature. 4 ) 1- Date:1-July-2019
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: July 2019
Name: William
/Reyes
��— Plant a ager Synagro
Signature: 4)4: - Date:1-August-2019
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. 1 am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: August 2019
Name: William
Reyes
Q—Plant f(� —��/cam ager Synagro
Signature: ^' �J l \ Date: 1-September-2019
The Class A pathogen requirements were met through §503.32(a)(7)_ The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
" I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: September 2019
Name: William Reyes — Plant Man er ^ Synagro
Signature: Aso Date:1-October-2019
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
"I certify, under penalty of law. that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment."
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: October 2019
Name: William Reyes— Plant M Synagro
Signature: �ageZV� Date:1-November-2019
61
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

0 CERTIFICATION
I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment"
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: November2019
Name: William Reyes — Plant Ma ger Synagro
Signature: Date: 1-December-2019
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
® biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90

CERTIFICATION
"I certify, under penalty of law, that the information that will be used to determine compliance with the
Class A pathogen requirements in §503.32(a) and the vector attraction reduction requirement in
§503.33(b)(8) was prepared under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate this information. I am aware that there
are significant penalties for false certification including the possibility of fine and imprisonment"
Project(s): South Cross Bayou WRF Pelletizing Facility
Reporting Period: December2019
Name: William Rees — Plant M� Synagro
Signature: 4,� Date:2-January-2020
The Class A pathogen requirements were met through §503.32(a)(7). The Process to Further Reduce
Pathogens was Heat Drying (Appendix B, B.2.). The biosolids were dried by direct or indirect contact with
hot gases to reduce the moisture content to 10% or lower. The temperature of the biosolids particles
exceeded 80 degrees Celsius. Fecal coliform testing was performed and the density of fecal coliform in
the biosolids was <1000 MPN per gram of total solids (dry weight basis).
The vector attraction reduction requirement was met through §503.33(b)(8). The percent solids of the
biosolids that contains unstabilized solids generated in a primary wastewater treatment process shall be
>90% based on the moisture content and total solids prior to mixing with other materials.
NTYPE 29: CA5 PR PELL PT VAR 90
, w,

Summing
UJENVIRON61E341TALTECHNOLOGIF.S, INC
atr,71y0cai l.abomton'5
June 25.2019
William Reyes
Synagro
5900 744L Street North
St. Petersburg, FL 33789
TEL: [phone]
FAX: [phone]
RE: Revised:
Dear William Reyes:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX [phone]
Wehsite: hunApivtv.setrek.cam
Order No.: 19060616
Summit Environmental Technologies, Inc. received 1 sample(s) on 6/11/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Brian J. Fackelman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 884735, California 07256CA, Colorado, ConnecticutPH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-0H-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
40971 [,New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 63I. North Dakota R-201, Olio DW, Ohio VAP CL0O52,
Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 9201600 [,Texas T104704466-11-5, Utah OH009232011-
1, Virginia VELAP 9456, Washington C891
Page 1 of 29

UM
,°� Summit Environmental Technologies, St.. Case Narrative
3310 10 Win St.
ENV:nCNNETAL TECHN 01-MrS, INC Cuyahoga Falls, Ohio 44223 WO#: 19060616
A nvlytJca7 Laboratories TEL: [phone] FAX: [phone]
Website: hamllivrow.settek.co,c Date: 6/25/2019
CLIENT: Synagro
Project: Revised:
WorkOrder Narrative:
19060616: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19060616-001 A F1ashPt_S(1010): Z = Method deviation, due to sample matrix could not stir to 250
RPM as required by the method
Revised: Report revised 06/25/19 to include Aluminum per client request.
Revision vl
Page 2 of 29

Summing
EiiFNVIHONh1FNTAL TECHNOLOGIES, INC
AoalyVcal Laboratorlss
CLIENT: Synagro
Project: Revised:
Summit Environmental Technologies, Inc,
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http:/Avwm.seuekcom
Workorder
Sample Summary
WOH: 19060616
25-Jun-19
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
19060616-001 Final Bin Pellets 6/10/2019 2:20:00 PM 6/11/2019 10:20:00 AM Solid
Page 3 of 29

'•, _„�-;-s �: � Summi(Enviromnen(ol Technologies, lne.
DATES REPORT
;�Ay 33/0 Win S(.
g ENVlaottaIeN7ALTect:tloLorie5, w(:. Cuyahoga Falls, Ohio 44223
._,_•� .^-nriyl/cc! TEL: [phone]I1 FAR [phone] WO#; 19060616
Website: han:/Avmrv.settek.com 25-Jun-19
Client: Synagro
Project: Revised:
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
19060616-OOIA Final Bin Pellets 6/10/20192:20:00 PM Solid Flashpoint Determination(1010)
6/17/201912: 14:46 PM
Metals Analysis (6010B)
6/25/2019 9: 10:00 AM
6/25/2019 4:37:57 PM
pH(SW9045D)
6/14/2019 1:10,00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
6/12/2019 3,57:00 PM
Reactive Sulfide (9034y7.3.4.2
6/12/2019 3:57:00 PM
TCLP Herbicides Analysis (SW1311/86/12120193:00:00 PM
6/121201911:00:00 AM
6/15/201912:33:00 AM
solid
TCLP Mercury Analysis (SW1311/74-o6/12/2019 3:00:00 PM
6/14/20191:40:OOPM
6/14/20195:39:00 PM
TCLP Metals Analysis (SW 1311/60ID 6/12/2019 3:00:00 PM
6/13/2019 920:00 AM
6/13/2019 7:3220 PM
TCLP Pesticides Analysis (SW 1311/8(6/12/20193:00:00 PM 6/17/2019 10:10:00 AM 6/17/2019 9:52:00 PM
TCLP Semi-Volatiles Analysis 6/12120193:00:00 PM 6/17/20193:00:00 PM 6119/20194:53:00 PM
(S W 1311/8270)
TCLP Semi-Volatiles Analysis 6/12/2019 3:0O:OOPM 6/17)2019 3:0O:OO PM 6/18/2019 2;02:00 PM
(SW1311/8270)
TCLP Volatiles Analysis by SW8260B 6/12/2019 3:00:00 PM 6/13/2019 5:52,00 PM
Revision vl
Page 4 of 29

Summit Environmental Technologies, Inc.
WO#:
19060616
MMSUM,T
M
3310 Win St.
ENVIR01,I1.104TALT[CHNOLOCIFS, INC
Cuyahoga Falls, Ohia 44223
Date Reported:
6/25/2019
hnnlyacal Laborotmles
TEL: [phone] FAX.-. [phone]
Company:
Synagro
Website: huy.11winv.senekcon
Address:
5900 744L Street North
St. Petersburg FL 33789
Received:
6/11/2019'
Project#:
Revised:
Flashpoint Determination (1010)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001
6/10/2019 Flashpoinl (140°F)
>140 °F
Solid
EPA 1010
1
6/17/2019
TAH
TCLP Metals Analysis (SW1311/6010C)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001
6/10/2019 TCLP Arsenic(As)
0.250 0.0280 mg/L
Solid
EPA 6010 C
1
5.00
6/1312019
KMO
Final Bin Pellets
001
6/10/2019 TCLP Barium(Ba)
2.50 0.291 mg/L
Solid
EPA 6010 C
1
100
6/13/2019
KMO
Final Bin Pellets
001
6110/2019 TCLP Cadmium(Cd)
0,125 0.00198 mg/L
Solid
EPA 6010 C
1
1.00
6/13/2019
KMO
Final Bin Pellets
001
6/10/2019 TCLP Chromium(Cr)
0.250 0.00524 mg/L
Solid
EPA 6010 C
1
5.00
6/1312019
KMO
Final Bin Pellets
001
6/10/2019 TCLP Lead(Pb)
0.500 ND mg/L
Solid
EPA 6010 C
1
5.00
6/13/2019
KMO
Final Bin Pellets
001
6/10/2019 TCLP Selenium(Se)
1.00 0.118 mg/L
Solid
EPA 6010 C
1
1.00
6/13/2019
KMO
Final Bin Pellets
001
6/10/2019 TCLP Silver(Ag)
0.500 ND mg/L
Solid
EPA 6010 C
1
5.00
6/1312019
KMO
Metals Analysis (6010B)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001
6/10/2019 Aluminum(AI)
a47 28300 mg/Kg
Solid
EPA 6010 B
100
6/25/2019
KMO
TCLP Mercury Analysis (SW1311/7470)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001
6/10/2019 TCLP Mercury
3.000200 0.00130 mg/L
Solid
EPA 7470 A
1
0.200
6114/2019
DNS
TCLP Pesticides Analysis (SW1311/8081)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001
6/10/2019 Chlordane, total
0.000500 ND mg/L
Solid
EPA 8081 B
10
0.0300
6/17/2019
MES
Flnal Bin Pellets
001
6/10/2019 Toxaphene
0.00160 ND mg/L
Solid
EPA 8081 B
10
0.500
6/17/2019
MES
Final Bin Pellets
001
6110/2019 Endrin
.0000500 ND mg/L
Solid
EPA 8081 B
10
0.0200
6/17/2019
MES
Final Bin Pellets
001
6/10/2019 Lindane
.0000500 ND mg/L
Solid
EPA 8081 B
10
0.400
6/17/2019
MES
Final Bin Pellets
001
6/1012019 Heptachlor
.0000500 ND mglL
Solid
EPA 8081 B
10
0.00800
6/17/2019
MES
Final Bin Pellets
001
6/10/2019 Heptachlor epoxide
.0000500 ND mg/L
Solid
EPA 8081 B
10
0.00800
6/17/2019
MES
Final Bin Pellets
001
6/10/2019 Methoxychlor
.0000500 ND mg/L
Solid
EPA 8081 B
10
10.0
6/17/2019
MES
Final Bin Pellets
001
6/10/2019 Surr: TCMX
10-119 68.2 %Rec
Solid
EPA 8081 B
10
6/17/2019
MES
Final Bin Pellets
001
6/10/2019 Sun: DCB
10-119 96-5 %Rec
Solid
EPA 8081 B
10
6/17/2019
MES
Page 5 of 29

SU��,�
Summit Environmental Technologies, Inc.
3310 Win Sr.
WO#:
19060616
EiiENVIRON&IIINTAL
TECHNOLDGIFS, INC
Cuyahoga Falls, Ohio 44223
Date Reported:
6/25/2019
Analyocal Laboratories
TEL: [phone] Fit& [phone]
Company:
Synagro
Wehsite: haaa/,v,m.seuekcom
Address:
5900 744L Street North
St. Petersburg FL 33789
Received:
6/I1/2019
Project#:
Revised:
TCLP Herbicides Analysis (SW1311/815l)-solid
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units
Matrix
Method DF RegLvl Run Analyst
Final Bin Pellets
Final Bin Pellets
Final Bin Pellets
001
001
001
6110/2019 2,4-D 0.000886 ND mg/L Solid
6/10/2019 2,4,5-TP 0.000226 ND mg/L Solid
6110/2019 Sum DCAA 20-140 84.4 %Rec Solid
TCLP Volatiles Analysis by SW8260B
EPA 8151 A
EPA 8151 A
EPA 8151 A
1
1
1
10.0
1.00
6/15/2019
6/15/2019
6/15/2019
MES
MES
MES
Client ID#
Lab ID# Collected Analyte
Rep Lord: Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001
6/10/2019 V-Dichloroethene
0.0165
ND mg/L
Solid
EPA 8260 B
50
0.700
6/13/2019
CTB
Final Bin Pellets
001
6/10/2019 1,2-Dichloroelhane
0.00950
ND mg/L
Solid
EPA 8260 B
50
0.500
6/13/2019
CTB
Final Bin Pellets
001
6/1012019 MEK
0.120
0.372 mg/L
Solid
EPA 8260 B
50
200
6/13P2019
CTB
Final Bin Pellets
001
6/10/2019 Benzene
0.0125
ND mg/L
Solid
EPA 8260 B
50
0.500
6/13P1019
CTB
Final Bin Pellets
001
6/1012019 Carbon tetrachloride
0.0160
ND mg/L
Solid
EPA 8260 B
50
0.500
6/13/2019
CTB
Final Bin Pellets
001
6/10/2019 Chlurobenzene
0.0115
ND mg/L
Solid
EPA 8260 B
50
100
6/1312019
CTB
Final Bin Pellets
001
6/10/2019 Chloroform
0.0135
ND mg/L
Solid
EPA 8260 B
50
6.00
6/13/2019
CTB
Final Bin Pellets
001
6/10/2019 Tetrachloroethene
0.0125
ND mg/L
Solid
EPA 8260 B
50
0.700
6/13/2019
CTB
Final Bin Pellets.
001
6/10/2019 Trichloroethene
0.0140
ND mg/L
Solid
EPA 8260 B
50
0.500
6/13/2019
CTB
Final Bin Pellets
001
6/10/2019 Vinyl chloride
0.0175
ND mg/L
Solid
EPA 8260 B
50
0.200
6/13/2019
CTB
Final Bin Pellets
001
6110/2019 Sun: 4-
70-130
94.9 %Rae
Solid
EPA 8260 B
50
6/13/2019
CTB
Bromofluombenzene
Final Bin Pellets
001
6/1012019 Sur:
70-130
99.8 %Rec
Solid
EPA 8260 B
50
6/13/2019
CTB
Dibromofluoromethane
Final Bin Pellets
001
6/10/2019 Sur: Toluene-d8
70-130
102 %Rec
Solid
EPA 8260 B
50
6/13/2019
CTB
Page 6 of 29

SU
Sunmrit Enurronmenla/Technologies,
WO#:
19060616
M'NI
331010 Win St.
St..
ENVIaON14FUTAL TECHN01.0r1rS, INC
Cuyahoga Falls. Ohio 44223
Date Reported:
625/2019
A nalyttcal Laboratorlcs
TEL: [phone] FAX. [phone]
Company:
Synagro
Websile: hay.-1Avmv.seltek.cont
Address:
5900 744L Street North
St. Petersburg FL 33789
Received:
6/11/2019
Project#:
Revised:
TCLP Semi-Volatiles Analysis (SW1311/8270)
Client ID#
Lab ID# Collected Analyte
Rep Lint Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001
6/10/2019 1,4-Dichlorobenzene
0.00267
ND mg/L
Solid
EPA 8270 C
1
7.50
6/19/2019
BJH
Final Bin Pellets
001
6/1012019 2,4,5-Tnchlorophenol
0.00267
NO mg/L
Solid
EPA 8270 C
1
400
6/19/2019
BJH
Final Bin Pellets
001
6/1012019 2,4,6-Tdchlorophenol
0.00267
NO mg/L
Solid
EPA 8270 C
1
2.00
6/19/2019
BJH
Final Bin Pellets
001
6/10/2019 2,4-Dinilrotoluene
0.00267
NO mg/L
Solid
EPA 8270 C
1
0.130
6/19/2019
BJH
Final Bin Pellets
001
6110/2019 Cresols, Total
0.00667
2.59 mg/L
Solid
EPA 8270 C
1
200
6119/2019
BJH
Final Bin Pellets
001
6110/2019 Hexachloro-1,3-
0,00267
NO mg/L
Solid
EPA 8270. C
1
0.500
6/19/2019
BJH
butadiene
Final Bin Pellets
001
6/10/2019 Hexachlorobenzene
0.00267
NO mg/L
Solid
EPA 8270 C
1
0.130
6/19/2019
BJH
Final Bin Pellets
001
6/10/2019 Hexachlomethane
0.00267
NO mg/L
Solid
EPA 8270 C
1
3.00
6/1912019
BJH
Final Bin Pellets
001
6/10/2019 Nitrobenzene
0.00267
NO mg/L
Solid
EPA 8270 C
1
2.00
6/192019
BJH
Final Bin Pellets
001
6/10/2019 Pentachlorophenol
0,00800
NO mg/L
Solid
EPA 8270 C
1
100
6/1912019
BJH
Final Bin Pellets
001
6/10/2019 Pyridine
0.00267
NO mg/L
Solid
EPA 8270 C
1
5.00
6/19/2019
BJH
Final Bin Pellets
001
6/10/2019 Sun: 2-Fluorophenol 10-109
50.7 %Rec
Solid
EPA 8270 C
1
6/IW019
BJH
Final Bin Pellets
001
6/102019 Sum Phenol-d6
10-109
59.6 %Rec
Solid
EPA 8270 C
1
6/192019
BJH
Final Bin Pellets
001
6/10/2019 Sum Nitrobenzene-
19-120
53.8 %Rec
Solid
EPA 8270 C
1
6/19/2019
BJH
d5
Final Bin Pellets
001
6/1012019 Sum 2,4;6-
10-120
75A %Rec
Solid
EPA 8270 C
1
6/192019
BJH
Tribromophenol
Final Bin Pellets
001
61102019 Surr: 2-
22-117
52.2 %Rec
Solid
EPA 8270 C
1
6/19/2019
BJH
Fluorobiphenyl
Final Bin Pellets
001
6/10/2019 Sum p-Terphenyl-
34-116
52.2 %Rec
Solid
EPA 8270 C
1
61192019
BJH
d14
Reactive Cyanide (9014/7.3.3,2)-Solid
Client ID#
Lab ID# Collected Analyte
Rep Lint Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001 6/10/2019 Cyanide, Reactive
0.294 0.161 mglKg
Reactive Sulfide (9034)/7.3.4.2
Solid
EPA 9014
1
6/1212019
MS
Client ID#
Lab ID# Collected Analyte
Rep Lint Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001 6/10/2019 Sulfide, Reactive
25.0 NO mg1Kg
pH (SW9045D)
Solid
EPA 9034
1
6/12/2019
MS
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Final Bin Pellets
001 6110/2019 pH
7.1 s.u.@20.1
Solid
EPA 9045 D
1
6/14/2019
CXS
Page 7 of 29

summ,lliff_
33f 0 Win St.
Summit Environmental Technologies. Inc.rn
QC SUMMARY REPORT
ENVInONNfEN1'ALTECHNOLOG]rS, INC
Cuyahoga Falls. Ohio 44223
Analyllcal Laboratorle<-
TEL: [phone] FAX: [phone]
WO#: 19060616
Websue: humllrvirmsetrekcorn
25-7un-19
Client:
Synagro
Project:
Revised:
BatchlD: 37878
Sample ID: MB-37878
SampType:
MBLK
TeslCode: TCLP-svoc-H Units: mg/L
Prep Date: 6/1212019
RunNo: 99600
:lienf ID: PBS
Batch ID:
37878
TestNo: SW8151A SW8161A
Analysis Date: 6/1412019
SegNo: 2163213
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-0 ND 0.000100 0 0
2,4,5-TP ND 0.0000500 0 0
Su.. DCAA 4.43 5.000 88.7 20 140
Sample ID: LCS-37878
SampType:
LCS
TestCode: TCLP-svoc-H Units: mg1L
Prep Date: 6/1212019
RunNo: 99600
;lient ID: LCSS
Batch ID:
37878
TestNo: SW8151A SW8151A
Analysis Date: 6/1412019
SegNo: 2163315
\nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HlghLimil RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.00542 0.000100 0.00500 0 108 43.8 130
2,4,5-TP 0,00477 0.0000500 0.00500 0 95.3 51.5 ill
Surr: DCAA 5.29 5.000 106 342 150
Sample ID: LCSD-37878
SampType:
LCSD
TeslCode: TCLP-svoc-H Units: mg/L
Prep Date: 6/1212019
RunNo: 99600
client ID: LCSS02
Batch ID:
37878
TestNo: SW8151A SW8151A
Analysis Date: 6/1412019
SegNo: 2163356
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl3mit High -unit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.00504 0.000100 0.00500 0 101 43.8 130 0.00542 7.38 30
2,4,5-TP 0.00466 0.0000500 0.00500 0 91.2 51.5 130 0.00477 4.42 30
Sum DCAA 4.65 - 5.000 93.0 34.2 150 0
QualiOers: B Analyte detected in the associated Method Blank E Value above quantization range H Holding times for preparation or ana13
J Analyte detected below quntitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit Page 8 of 29

97�H Summit Environmenlol Teclmologies, Inc. QC SUMMARY REPORT
S �.IMMIT
33/0 Win St.
EN:'I,I ON 1'ENTALTECHNOLQGIFS, INC Cityahoga Falls, Ohio 44223
Analyl+cal Laboratories TEL: (330)2S3-82// FAX..[phone] W0#: 19060616
Website: hay.-Mvinv.setrekcom 25-Jun-19
Client: Synagro
Project: Revised: Batchll): 37885
Sample ID: LCS•99516
SampType: LCS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 99516
Client ID: LCSS
Batch ID: 37885
TestNo: SW8260 SW1311M
Analysis Date: 611312019
SegNo: 2159553
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDUmit Qual
1,1-Dichloroethene
0.0218
0.00500
0.0200
0
109
70
131
1,2-Dichloroethane
0.0206
0.00500
0.0200
0
103
70
137
MEK
0.139
0.100
0.100
0
139
55.1
163
Benzene
0,0203
0.00500
0.0200
0
101
70
132
Carbon tetrachloride
0.0202
0.00500
0.0200
0
101
63.7
139
Chlorobenzene
0.0199
0.0500
0.0200
0
99.3
70
139
Chloroform
0.0202
0.00500
0.0200
0
101
70
130
Tetrachloroethene
0.0210
0.00500
0.0200
0
105
56.2
187
Trichloroethene
0.0202
0.00500
0.0200
0
101
64.1
138
Vinyl chloride
0.0212
0.00200
0.0200
0
106
22.1
147
Sum: 4-Bromofluorobenzene
50.2
50.00
100
70
130
Surr. Dibromofluoromethane
50.5
50.00
101
70
130
Surr: Toluene-d8
50.2
50.00
100
70
130
J
Sample ID: MS-37885
SampType:
MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 6/13/2019
RunNo: 99516
Client ID: PBS
Batch ID:
37885
TestNo: SW8260 SW7311M
Analysis Date: 611312019
SegNo: 2159558
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND 0.0500
1,2-Dichloroethane
ND 0.0500
MEK
ND 1.00
Benzene
ND 0.0500
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal)
I
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds Revision vl
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit Page 9 of 29

M'N
Summit Environmental Technologies, Inc.SUM
3310 Win St.
QC CTTRAR`REPORT
ENVInQNarENTA-TECtiNCLOGIr.S, INC
Cuyahoga Falls, Ohio 44223
_ _ v
AruOyf/cal L2Uoratodes
TEL: [phone] FAX- [phone]
WO#: 19060616
Website: htto:!/www.seftekcom
25-Jun-19
Client:
Synagro
Project:
Revised:
6atchlD: 37885
Sample ID: MB-37885
SampType:
MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 611312019
RunNo: 99516
Client ID: PBS
Batch ID:
37885
TestNo: SW8260 SW1311M
Analysis Date: 6/13/2019
SegNo: 2159558
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride NO
0.0500
Chlorobenzene NO
0.500
Chloroform NO
0.0500
Tetrachloroethene ND
0.0500
Trichloroethene ND
0.0500
Vinyl chloride ND
0.0200
Surr: 4-Bromotuorobenzene 496
500.0 99.1 70
130
Surf: Dibromofluoromethane 519
500.0 104 70
130
Surf: Toluene-d8 514
500.0 103 70
130
Qualifiers: B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anall
3 Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds Revision vl
PL Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit Page 10 of 29

uraml3310
Win St. Summit Environmental Technologies, Inc.
QC SUMMARY REPORT
_
ENVMONRIENTAL TECHMOLOOMS, INC
Analytical Laboratories
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX..- [phone]
WO#: 19060b1fi
Website: huxlAvrtnv.settekcan
25-✓uu-19
Client:
Synagro
Project:
Revised:
BatchlD: 37889
Sample ID: MB-37889
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 611312019
RunNo: 99505
:lient ID: PBS
Batch ID: 37889
TestNo: SW6010C SW3010A
Analysis Date: 611312019
SegNo: 2159328
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCSa7889
SampType:
LCS
TestCode: Mtl-TCLP4(6 Units: mg/L
Prep Date: 6/13/2019
RunNo: 99505
CI[ent ID: LCSS
Batch ID:
37889
TestNo: SW6010C SW3010A
Analysis Date: 6/1312019
SegNo: 2159329
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HlghLimit RPD Ref Val
%RPD RPDLimit Qua[
I ULr arsenic(As)
2.00
0.500
2.000
0
99.9
80
120
TCLP Barium(Ba)
2.08
5.00
2.000
0
104
80
120 3
TCLP Cadmium(Cd)
1.88
0.100
2.000
0
94.0
80
120
TCLP Chromium(Cr)
2.14
0.200
2.000
0
107
80
120
TCLP Lead(Pb)
2.14
0.500
2.000
0
107
80
120
TCLP Selenium(Se)
2.04
0.0500
2.000
0
102
80
120
TCLP S[Iver(Ag)
2.27
0.500
2.000
0
114
80
120
Qualifiers: B Analyte detected in the associated Method Blank
1 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
B Value above quantitation range H Holding times for preparation oranall
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Revision vl
Page 1 I of 29

5u '�
Summit EnvironmentalTechnol10 Technologies, St. .
3310 Win St.
QC SUMMARY REPORT
ENVInONMENTALTECHNOLOOIF9,INC
Analytical Laboratories
Cuyahoga Falls, Ohio44223
TELr [phone] FAX. [phone]
Wok: 19060616
Website: hna:/Anny.settekcain
25-✓un-19
Client:
Synagro
Project:
Revised:
BatchID: 37889
Sample ID: 19060567-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mglL
Prep Date: 6113/2019
RunNo: 99505
client ID: BatchQC
Batch ID: 37889
TestNo: SW6010C SW3010A
Analysis Date: 6/1312019
SegNo: 2160088
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
I OLr
Arsenic(As)
2.19
0.500
2.000
0
110
70
130
TCLP
Barium(Ba)
3.07
5.00
2.000
1.086
99.1
70
130 J
TCLP
Cadmium(Ccl)
1.94
0.100
2.000
0
96.9
70
130
TCLP
Chromium(Cr)
2.08
0.200
2.000
0
104
70
130
TCLP
Lead(Pb)
1.96
0.500
2.000
0
98.0
70
130
TCLP
Selenium(Se)
2.32
0.0500
2.000
0.04507
114
70
130
TCLP
Silver(A,q)
2.35
0.500
2.000
0
118
70
130
Sample ID: 19060567-001AMSD
SampType: MSD
TestCode: Mtl.TCLP-7(6 Units: mg/L
Prep Dale: 6/13/2019
RunNo: 99505
Client ID: Batch=
Batch ID: 37889
TestNo: SW6010C SW3010A
Analysis Date: 6/13/2019
SegNo: 2160089
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowUmft HighLimit RPD Ref Val
%RPD RPDLimit Qual
I (;LP Arsenlc(As)
2.19
0.500
2.000 0
109
70
130
2.190 0.144
20
TCLP Barium(Ba)
3.06
5.00
2.000 1.086
98.9
70
130
3.068 0.121
20 J
TCLP Cadmium(Cd)
1.93
0.100
2.000 0
96.4
70
130
1.939 0.526
20
TCLP Chromium(Cr)
2.08
0,200
2.000 0
104
70
130
2.079 0.0549
20
TCLP Lead(Pb)
1.97
0.500
2.000 0
98.6
70
130
1.961 0.592
20
TCLP Selenlum(Se)
2.35
0,0500
2.000 0.04507
115
70
130
2.324 0.962
20
TCLP Silver(Ag)
2.34
0.500
2.000 0
117
70
130
2.353 0.386
20
Qualifren: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anti
1
Analyte detected below quantitation limits
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
Revision V 1
PL
Permit Limit
R
RPD outside accepted recovery
limits
RL
Reporting Detection Limit
Page 12 of 29

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win S7.
SUMM111-
ENVtADPIRl,rriTA'-TECH14OLOCIPS, Cuyahoga Falls, Ohio 44223
4naiyr1c3l LabOfL'.O' TEL: [phone] FAX., [phone] WO#: 19060616
Website: htro:/Avrotv.settekeorn 25-✓un-79
Client: Synagro
Project: Revised: BatchID: 37923
Sample ID: MB-37923
SampType:
MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 611412019
RunNo: 99584
Client ID: PBS
Batch ID:
37923
TestNo: SW7470A SW7470A
Analysis Date: 6114/2019
SegNo: 2161771
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
ULr Memury NU u.u020u
Sample ID: LCS-37923
SampType:
LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 6/14/2019
RunNo: 99584
:lient ID: LCSS
Batch ID:
37923
TestNo: SW7470A SW7470A
Analysis Date: 6114/2019
SegNo: 2161772
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
ULr Iviercury U.UU4U1 u.uu2uu 0.00400 0 100 80 120
Sample ID: MB2-37923
SampType:
MBLK
TestCode: HIS _TCLP(74 Units: PPM
Prep Date: 6/14/2019
RUnNO: 99584
;lient ID: PBS
Balch ID:
37923
TestNo: SW7470A SW7470A
Analysis Date: 611412019
SegNo: 2162401
\nalyle
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
tar Memury ND 0.00200
Sample ID: 19060468-OOIAMS
SampType:
MS
TestCode: HIS TCLP(74 Units: PPM
Prep Date: 6/14/2019
RunNo: 99584
-lient ID: BatchQC
Batch ID:
37923
TestNo: SW7470A SW7470A
Analysis Dale: 611412019
SegNo: 2162405
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLlmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
I �Lr Mercury U.UU441 0.00200
0.00400 0 110 75
125
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantimtion range
H
Holding times for preparation or anall
3 Analyte detected below quantization limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND Not Detected
Q RSD is greater than RSDlimit
P
Second column confirmation exceeds Revision vl
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit Page 13 Of 29

SUMMIT3310 WSummit EnvironmentalTechnal10Win St. St.Inc. QC SUMMARY REPORT
ENVIRONMENTAL TECH NOLOGIF.S, INC Cuyahoga Falls, Ohio 44223 WOM 19060616
A nalylical Laboratories TEL: [phone] FAX [phone]
Website: htto:/dvww.seltekcom 25-Jun-19
Client: Synagro
Project: Revised: Batchll): 37923
Sample ID: 19060468-001AMS
SampType:
MS
TestGode: HG_TCLP(74 Units: PPM
Prep Dale: 6/14/2019
RunNo: 99584
Client ID: BafchOC
Batch ID:
37923
TestNo: SW7470A SW7470A
Analysis Date: 6/14/2019
SegNo: 2162405
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDUmit Qua]
Sample ID: 19060468-001AMSD
SampType:
MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 6114/2019
RunNo: 99584
Client ID: BatchQC
Batch ID:
37923
TeslNo: SW7470A SW7470A
Analysis Dale: 6114/2019
SegNo: 2162406
Analyte
Result
POL SPK value SPK Ref Val
%REC L=Umit HighLimit RPD Ref Val
%RPD RPDUmlt Qua[
-CLP Mercury 0.00431 0.00200 0.00400 0 108 75 125 0.00441 2.29 20
Qualifiers; B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anall
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confinnation exceeds Revision vl
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 14 of 29

S umm'al Summit Environmental Technologies, Inc, QC SUMMARY REPORT
3310 Win St.
ENVInnNMENTAL TEdHNQI.nnIFS, INC Cuyahoga Falls, Ohio 44223
A,nniyrical Laboratories TEL: [phone] FAX. [phone] WO#: 19060616
Webstte: hrro:/Avrv,P.senekcam 25-Jun-19
Client: Synagro
Project: Revised: BatchID: 37938
Sample ID: mb-37938
SampType:
MBLK
TestCode: TCLPSvoc-C Units: mglL
Prep Date: 611712019
RunNo: 99647
client ID: PBS
Batch ID:
37938
TestNo: SW8081A SW3510C
Analysis Date: 611712019
SegNo: 2164473
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Hight-imit RPD Ref Val
%RPD RPDL[mit Qua[
Chlordane, total
ND
0.00260
Toxaphene
ND
0.00500
Endrin
ND
0.000500 d
Lindane
ND
0.000500 d
Heptachlor
ND
0.000500 d
Heptachlor epoxide
ND
0.000500 d
Methoxychlor
ND
0.000500 d
Surr: TCMX
9.17
20.00 45.9 10 119
Surr: DCB
13.7
20.00 68.3 10 119
Sample ID: Ics-37938
SampType:
LCS
TestCode: TCLPSVOC- Units: mglL
Prep Date: 611712019
RunNo: 99647
Client ID: LCSS
Batch ID:
37938
TestNo: SW8081A SW3510C
Analysis Date: 611712019
SegNo: 2164474
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighL[mit RPD Ref Val
%RPD RPDLimit Qual
Enddn
0.00759
0.000500
0.0100 0 75.9
20
216
Lindane
0.00615
0.000500
0.0100 0 61.5
20
197
Heptachlor
0.00484
0.000500
0.0100 0 48.4
20
200
m
Heptachlor epoxide
0.00634
0.000500
0.0100 0 63.4
20
200
Methoxychlor
0.00747
0.000500
0.0100 0 74.7
20
227
Surf: TCMX
927
20.00 46.4
20
143
Surr: DCB
14.9
20.00 74.5
20
151
Qualifiers:
B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anti
I
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
O RSD is greater than RSDlimit
P
Second column confinnation exceeds
Revision V 1
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 15 of 29

'` _`7,,�*`
-
SUMMIT
Summil Environmental Technologies, Inc.
3310 Win S1.
QC SUMMARYREPORT
ENVIFIMMENTALTECHNOLOGIFS, INC
Cuyahoga Falls, Ohio 44223
t-
s..^'
Analyrical OL•oraro?/es
TEL: [phone] FAX [phone]
tVQp; 1906061fi
Website: hno:/Aurvru.sellekcom
25-Jun-19
Client:
Synagro
Project:
Revised:
BatchlD: 37938
Sample ID: 19060616.001ams
SampType:
MS
TeslCode: TCLP-SVOC- Units: mg1L
Prep Date: 6/17/2019
RunNo:
99647
Cllent ID: Final Bin Pellets
Balch ID:
37938
TestNo: SW8081A SW3510C
Analysis Date: 6/1712019
SegNo:
2164475
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD
RPDLimit Qual
Enddn
0.00881
0.00500
0.0100
0
88.1
10
224
Lindane
0,00727
0.00500
0.0100
0
72.7
10
192
Heptachlor
0.00240
0.00500
0.0100
0
24.0
10
197 J
Heptachlor epoxide
0.00740
0.00500
0.0100
0
74.0
10
208
Methmrychlor
0.00994
0.00500
0.0100
0
99.4
10
251
Sum: TCMX
9.75
20.00
48.8
10
157
Sun: DCB
14.5
20.00
72.5
10
194
Sample ID: 19060616-001amsd
SampType:
MSD
TestCode: TCLPSVOC- Units: mg/L
Prep Date: 611712019
RunNo: 99647
Client ID: Final Bin Pellets
Batch ID:
37938
TestNo: SW8081A SW3510C
Analysis Date: 6117/2019
SegNo: 2164476
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imil HighLimit RPD Ref Val
%RPD RPDLimit Qual
Enddn
0.0160
0.00500
0.0100
0
160
10
224
0.00881
58.2
30
R
Lindane
0.0117
0.00500
0.0100
0
117
10
192
0.00727
46.9
30
R
Heptachlor
0.00431
0.00500
0.0100
0
43.1
10
197
0.00240
57.1
30
JR
Heptachlor epoxide
0.0129
0.00500
0.0100
0
129
10
208
0.00740
54.4
30
R
Methmrychlor
0.0161
0.00500
0.0100
0
161
10
251
0.00994
47.6
30
R
Surr: TCMX
16.9
20.00
84.5
10
157
0
Surr. DCB
23.6
20.00
118
10
194
0
Qualifiers: B Analyte detected in the associated Method Blank
I Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or analx
M Manual Integration used to determine area response MC Value is below Minimum Compound
lJ RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 16 of 29

Rol
UMM'�
Summit Environmental Technologies, St..
3310 Win St
QC GUITAR` REPORT
A
�G 11.. SUMMARY lYll�'1t1L1 i REPORT
ENVInONarENTALTEC8NaLOOIES.l0IC
Cuyahoga Falls, Ohio 44223
WO#: 19060616
.�_s_
Anafyt;ca! LeeoraroNe<_
TEL: [phone] FAX [phone]
Website: htto:OAPtvwsettekcom
25Jun-19
Client:
Synagro
Project:
Revised:
BatchID: 37947
Sample ID: MB-37947
SampType:
MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 6/1712019
RunNo: 99670
Client ID: PBS
Batch ID:
37947
TestNo: SW8270C SW3510C
Analysis Date: 6/18/2019
SegNo: 2165011
Analyte
Result
PQL SPKvalue SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Tdchlorophenol
ND
01100
2,4-Dinitrotoluene
ND
0.0200
o-Cresol
ND
0.100
mfp-Cresol(s)
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachlomethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0.100
Pyridine
ND
0.100
Sum: 2-Fluorophenol
0.469
1.000
46.9
10
109
Sum: Phenol-d6
0.617
1.000
61.7
10
109
Sum: Nitrobenzene-d5
0.507
1.000
50.7
19
120
Sum: 2,4,6-Tdbromophenol
0.609
1.000
60.9
10
120
Sum: 2-Fluorobiphenyl
0.552
1.000
55.2
22
117
Sum: p-Terpheny1-d14
0.579
1.000
57.9
34
its
Qoalifiers: B Analyte detected in the associated Method Blank
E
Value above quantimtion range
H
Holding times for preparation or anall
I Analyte detected below quantization limits
M
Manual Integration used to determine
area response
MC
Value is below Minimum Compound
ND Not Detected
Q
RSD is greater than RSDlimit
P
Second column confirmation exceeds Revision v1
PL Permit Limit
R
RPD outside accepted recovery
limits
RL
Reporting Detection Limit Page 17 Of 29

S U M M 1'i Summi(Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIAONa9ENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratorles TEL: [phone] FAX.- [phone] WO#: 19060G16
Websile: hito.-Mvmrv.settekcom 25-Jun-19
Client: Synagro
Project: Revised: 6atchlD: 37947
Sample ID: LCS-37947
SampType:
LCS
TeslCode! SVOC-BNA_T Units: mg/L
Prep Date: 6/17/2019
RunNo: 99670
Client ID: LCSS
Batch ID:
37947
TestNo: SW8270C SW3510C
Analysis Date: 6/18/2019
SegNo: 2165012
Analyte
Result
PQL SPK value SPK Ref Val
%REG Lowl-Imit Highl-imit RPD Ref Val
%RPD RPDLImlt Qual
1,4-Dichlorobenzene
0.319
0.0400
0.8000 0
39.9
36.4
130
2,4,5-Trichlorophenol
0.508
0.100
0.8000 0
63.5
31.7
132
2,4,6-Trichlomphenol
0.504
0.100
0.8000 0
63.0
31.1
133
2,4-Dinitrotoluene
0.541
0.0200
0.8000 0
67.6
43.3
130
o-Cresol
0.447
0.100
0.8000 0
55.9
32.9
130
m/p-Cresols)
0.491
0.100
0.8000 0
61.4
30.4
130
Cresols, Total
0.939
2.00
1.600 0
58.7
31.7
130
Hexachloro-1,3-butadiene
0,288
0.00800
0.8000 0
36.0
31.4
130
Hexachlorobenzene
0.412
0.0200
0.8000 0
51.5
43.1
130
Hexachloroethane
0.295
0.0400
0.8000 0
36.9
36.5
130
Nitrobenzene
0.389
0.0400
0,8000 0
48.6
39.5
130
Pentachlorophenol
0.389
0.100
0.8000 0
48.6
34
130
Pyridine
0.402
0.100
0.8000 0
50.2
10
130
in
Sun: 2-Fluorophenol
0.485
1.000
48.5
17.1
130
Surr: Phenol-d6
0.562
1.000
56.2
10
130
Surr. Nitrobenzene-d5
0.490
1.000
49.0
32.6
130
Surc 2,4,6-Tdbromophenol
0.682
1.000
68.2
4.43
130
Surf: 2-Fluorobiphenyl
0.472
1.000
47.2
41.8
130
Surr. p-Terphenyl-d14
0.692
1.000
69.2
36.4
130
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quamitation range
H Holding times for preparation or anall
1 Analyte detected below quantitation limits
M Manual Integration used to determine area
response
MC Value is below Minimum Compound
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
Revision v1
PL Permit Limit
R RPD outside accepted recovery
limits
RL Reporting Detection Limit
Page 18 Of 29

pqprm
5u�'�_ Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 19060616
«sy 4nnfyrical Labcrarorles TEL: [phone] FAX-[phone]
Website: htto:/Avivivsenek.com 25-Jun-19
Client: Synagro
Project: Revised: BatchID: 37947
Sample ID: 19060670-001AMS
SampType:
MS
TestCode: SVOC-BNA T Units: mg1L
Prep Dale: 6/17/2019
RunNo: 99670
Client ID: BatchQC
Batch ID:
37947
TestNo: SW8270C SW3510C
Analysis Date: 8/18/2019
SegNo: 2165738
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLlmit RPD Ref Val
%RPD RPDUmit Qual
1,4-Dichlorobenzene
0.380
0.0800
0.8000 0
47.5
33.8
126
W
2,4,5-Trichlorophenol
0.559
0.200
0.8000 0
69.8
28.7
144
W
2,4,6-Trichlorophenol
0.576
0.200
0.8000 0
72.0
12.8
153
W
2,4-Dinitrotoluene
0.586
0.0400
0.8000 0
73.2
20.4
155
W
o-Cresol
0.502
0.200
0.8000 0
62.8
10
148
W
m1p-Cresol(s)
0.549
0.200
0.8000 0
68.6
10
148
W
Cresols, Total
1.05
4.00
1.600 0
65.7
10
148
JW
Hexachlom-1,3-butadiene
0.396
0.0160
0.8000 0
49.6
29
126
W
Hexachlorobenzene
0,476
0.0400
0.8000 0
59.5
33.7
134
W
Hexachloroethane
0.360
0.0800
0.8000 0
45.0
32.8
132
W
Nitrobenzene
OA58
0.0800
0.8000 0
57.3
20
158
W
Pentachlorophenol
0.717
0.200
0.8000 0
89.7
10
176
W
Pyridine
0.398
0.200
0.8000 0
49.8
10
130
mW
Surr. 2-Fluorophenol
0.566
1.000
56.6
3.39
130
W
Sum Phenol-d6
0.676
1.000
67.6
5
130
W
Sur. Nitrobenzene-d5
0.558
1.000
55.8
14.5
154
W
Surr: 2,4,6-Tribromophenol
0.762
1.000
76.2
19.5
130
W
Sun: 2-Fluorobiphenyl
0.552
1.000
55.2
34.4
130
W
Surr: p-Terphenyl-d14
0.603
1.000
60.3
8.86
156
W
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or anal]
3 Analyte detected below quantitation limits
M Manual Integration used to determine
area
response
MC Value is below Minimum Compound
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
Revision V 1
PL Permit Limit
R RPD outside accepted recovery
limits
RL Reporting Detection Limit
Page 19 of 29

SVMM17` Summit r w EnonnenalTechnologes,lnc. 3310 Win St. QC SUMMARY REPORT
ENVInONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 ILJAnalytical Laboratories TEL. (330J 253-8211 FAX [phone] WO#: 19060616
Website: h1pr1AyiPw.settekco n 25-✓un-19
Client: Synagro
Project: Revised: BatchID: 37947
Sample ID: 19060670-001AMSD
SampType:
MSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 6/17/2019
RunNo: 99670
Client ID: Batch=
Batch ID:
37947
TestNo: SW8270C SW3510C
Analysis Date: 6/18/2019
SegNo: 2165739
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowt-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.295
0.0800
0.8000
0
36.8
33.8
126
0.3800
25.3
30
W
2,4,5-Trichlorophenol
0.521
0.200
0.8000
0
65.2
28.7
144
0.5588
6.96
30
W
2,4,6-Trichlorophenol
0.538
0.200
0.8000
0
67.2
12.8
153
0.5764
6.97
30
W
2,4-Dinitrotoluene
0.554
0.0400
0.8000
0
69.3
20.4
155
0.5856
5.47
30
W
o-Cresol
0.460
0.200
0.8000
0
57.4
10
148
0.5020
8.82
30
W
m/p-Cresol(s)
0,523
0.200
0.8000
0
65.4
10
148
0.5492
4.93
30
W
Cresols, Total
0.982
4.00
1.600
0
61.4
10
148
1.051
6.77
30
JW
Hexachloro-1,3-butadiene
0.317
0.0160
0.8000
0
39.6
29
126
0.3964
22.3
30
W
Hexachlorobenzene
0.416
0.0400
0.8000
0
52.0
33.7
134
0.4760
13.5
30
W
Hexachloroethane
0.277
0.0800
0.8000
0
34.6
32.8
132
0.3604
26.1
30
W
Nitrobenzene
0.368
0.0800
0.8000
0
46.1
20
158
0.4584
21.8
30
W
Pentachlorophenol
0.686
0.200
0.8000
0
85.7
10
176
0.7172
4.51
30
W
Pyridine
0.378
0.200
0.8000
0
47.3
10
130
0.3984
5.15
30
mW
Sum: 2-Flucrophenol
OA96
1.000
49.6
3.39
130
0
W
Sum: Phenol -dB
0.644
1.000
64.4
10
130
0
W
Sum: Nitrobenzene-d5
0.471
1.000
47.1
14.5
154
0
W
Sum: 2,4,6-Tribromophenol
0.781
1.000
78.1
19.5
130
0
W
Sum;2-Fluombiphenyl
0.460
1.000
46.0
34.4
130
0
W
Sum: p-Terphenyl-d14
0.575
1.000
57.5
8.86
156
0
W
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal]
1 Analyte detected below quantitalion limits
M Manual integration used to determine area response
MC
Value is below Minimum Compound
ND Not Detected
O RSD is greater than RSDlimit
P
Second column confirmation exceeds Revision V 1
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit Page 20 of 29

summi
33/0 Win Sr. Summit Environmental Technologies, Inc,
QC SUMMARY REPORT
ENVInONN%UITALTECHNOLOGMS, INC
Cuyahoga Falls, Ohio 44223
WO#: 19060616
-
0naryifc2l Loorator es
TEL: [phone] FAX.. [phone]
Website: h1m.,1Avwm.seuekcom
25-Jua-19
Client:
Synagro
Project:
Revised:
BatchlD: 38075
iample ID: MB-38075
SampType:
MBLK
TestCode: MTL4CP_S(6 Units: mg/Kg
Prep Date: 6/2512019
RunNo: 99986
'Ilent ID: PBS
Balch ID:
38075
TestNo: SW6010 SW3050B
Analysis Date: 6125/2019
SegNo: 2176639
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Aluminum(AI) ND 25.0
iample ID: LCS-38075
SampType:
LCS
TestCode: MTL-ICP_S(6 Units: mg/Kg
Prep Dale: 612512019
RunNo: 99986
:lient ID: LCSS
Batch ID:
38075
TestNo: SW6010 SW3050B
Analysis Date: 612512019
SegNo: 2176640
\nalyte
Result
PQL SPK value SPK Ref Val
%REC LowUmit HIghLlmit RPD Ref Val
%RPD RPDLimit Qual
Aluminum(AI) too 25.0 100.0 0 100 80 120
Qualifiers: B Analyte detected in the associated Method Blank
1 Analyte detected below quentitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal}
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 21 Of 29

dn=ppm
SummitSummrl
Environmental Technologies,3310 4y10in Sr. Inc.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGIES, INC
Cuyahoga Falls, Ohio 44223
WO#: 19060616
Ant+lyrical Laboratories TEL: [phone] FAX. [phone]
Website: la lhvimv.seuekcom
25-Jun-19
Client:
Synagro
Project:
Revised:
Batchll): R99484
Sample ID: 19060625-004AMS
SampType: MS
TestCode: Cyanlde,Rea Units: mg/Kg
Prep Date:
RunNo: 99484
:Iient ID: BatchQC
Batch ID: R99484
TestNo: SW9014
Analysis Date: 6/12/2019
SegNo: 2158775
\nalyte
Result
PQL SPK value SPK Rat Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.73 0.495 10.00 0.1523 95.8 81.6 122
iample ID: 19060625-004AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 99484
:lient ID: BatchQC
Balch ID: R99484
TestNo: SW9014
Analysis Date: 611212019
SegNo: 2158776
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 9.69 0.490 10.00 0.1523 95.4 81.6 122 9.728 0.364 5
Qualifiers: B Analyte detected in the associated Method Blank
I Analyte detected below quantitation limits
ND Nat Detected
PL Permit Limit
E Value above quandtation range H Holding times for preparation at anti
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 22 Of 29

F=ZroouS
uM illit
Summit Environmental Technologies, Inc,
3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTALTECHNQLD(Ur:S, INC
Cuyahoga Falls. Ohio 44223
gnalyr/cal Laboraforles
TEL: [phone] FAX: [phone]
WO#: 19060616
Websile: law.11 viviv.senekconi
25-Jun-19
Client:
Synagro
Project:
Revised:
BatchID: R99484
iample ID: M13LK
SampType:
MBLK
TestCode: Cyanide,Rea Units: mgIL
Prep Date:
RunNo: 99484
:lient ID: PBW
Batch ID:
R99484
TestNo: SW9014
Analysis Date: 6112/2019
SegNo: 2158760
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.495
iample ID: LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mglL
Prep Date:
RunNo: 99484
;lient ID: LCSW
Batch ID: R99484
TestNo: SW9014
Analysis Date: 611212019
SegNo: 2158761
lnalyte
Result
PQL SPK value SPK Ref Val
%REC LmLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.16 0.481 10.00 0 91.6 85 115
Sample ID: RLC
SampType:
RLC
TestCode: Cyanide,Rea Units: mglt.
Prep Date:
RunNo: 99484
Client ID: BatchOC
Batch ID:
R99484
TestNo: SW9014
Analysis Date: 611212019
SegNo: 2168763
Analyte
Result
PQL SPK value SPK Ref Val
%REC LOWLimit HighLimit RPD Ref Val
%RPD RPDLimit Dual
Cyanide, Reactive 0.411 0.495 0.5000 0 82.1 50 150 J
Qualifiers: B Analyte detected in the associated Method Blank
I Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 23 of29

SvMM'It
Summit Environmental Technologies. Inc.
3310 Win St.
QC SUMMARY REPORT
j
ENVMONMENTALTeCNNOLDGI69, INC
Gryahoga Falls, Ohio 44223
WO#: 1906061G
._ .
Analytical Ltoles
TEL: [phone] FAX: [phone]
Website: hrlo://wrvtv.seuek.corn
25-✓un-19
Client:
Synagro
Project:
Revised:
BatchID: R99485
iample ID: 19060625-004AMS
SampType:
MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 99485
;lien( ID: BatchQC
Batch ID:
R99485
TestNo: SW9034
Analysis Dale: 6112/2019
SegNo: 2158805
lnalyle
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4630 25.0 4800 0 96.5 80 120
iample ID: 19060625-004AMSD
SampType:
MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 99485
;lien( ID: BatchQC
Batch ID:
R99485
TestNo: SW9034
Analysis Date: 611212019
SegNo: 2158806
>nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimil HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfde, Reactive 4660 25.0 4800 0 97.1 80 120 4630 0,646 30
Qualifiers: B Analyte detected in the associated Method Blank
1 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
8 Value above quanlimtion range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 24 of 29

SUMMIT
Summit Environmental Technologies. St..
33l0 Win�.
QC SUMMARY REPORT
ENVInrINMENTALTECHN4t01IFS, INC
Cuyahoga Falls, Ohio 44223
WO#: 19060616
4nalyl/cal Laboratarlss
TEL: [phone] FAX.- [phone]
Website: hun.-Annu.senekcnrn
25-Jun-19
Client:
Synagro
Project:
Revised:
BatchID: R99485
iample ID: MB-R99485
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 99485
;lien[ ID: PBW
Batch ID: R99485
TeslNo: SW9034
Analysis Date: 6112/2019
SegNo: 2158793
\nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimil HighLlmit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
iample ID: LCS-R99485
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 99485
;lient ID: LCSW
Batch ID: R99485
TeslNo: SW9034
Analysis Date: 611212019
SegNo: 2158794
\nalyte
Result
POL SPK value SPK Ref Val
%REC Lowl-imil Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4720 25.0 4800 0 98.3 85 115
Qualifiers: B Analyte detected in the associated Method Blank
1 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E. Value above quantitation range H Holding times for preparation or anal}
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision v1
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 25 of 29

TSUMM11
Sanuuit Environmental Technologies, WinInc. QC SUMMARY REPORT
33/O Win St. 1. SUMMARY REPORT
111
EN%°:F1OPln'ENTALTECHPJOLOG165, INC Cuyahoga Falls. Ohio 44223
An -r, 1ir;' I oe oratortvs TEL: [phone] FAX: [phone] CVO#: 19060616
Website: hum://wwtesettek.com 25-✓un-19
Client: Synagro
Project: Revised: BatchID: R99565
Sample ID: LCS-R99565
SampType:
LCS
TestCode: pH_NPW(450 Units: s.u.@21.2°C
Prep Dale:
RunNo: 99565
Client ID: LCSW
Batch ID:
R99565
TestNo: SW9045D
Analysis Date: 6114/2019
SegNo: 2160845
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowUmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 19060440-OOl DDUP
SampType:
DUP
TestCode: pH_NPW(450 Units: s.u.@21.4°C
Prep Date:
RunNo: 99565
Client ID: BatchQC
Batch ID:
R99565
TestNo: SW9045D
Analysis Date: 6114/2019
SegNo: 2160847
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 3.0 3.0 1.0 5
Sample ID: LCS-1199565
SampType:
LCS
TestCode: pH_NPW(450 Units: s.u.@21.5°C
Prep Date:
RunNo: 99565
Client ID: LCSW
Batch ID:
R99565
TestNo: SW9045D
Analysis Date: 6114/2019
SegNo: 2160956
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
R RPD outside accepted recovery limits RL Reporting Detection Limit Page 26 of 29

ummi3310
Win StStSUMMARYSvmmit Environmental Technologies,Inc.
QC SUMMARY REPORT
ENVIAONNsENTAL TECNNOLOnIFS, INC
Cuyahoga Falls, Ohio 44223
Anaiydcal Laborarorins
TEL: [phone] FAX.[phone]
WO#: 19060616
Wehsite: hno://rvrvrv.seitekcorn
25-1un-19
Client:
Synagro
Project:
Revised:
BatchID: R99605
Sample ID: LCS-RS9605
SampType:
LCS
TestCode: FlashPt S(10 Units: °F
Prep Date:
RunNo: 99605
Client ID: LCSS
Batch ID:
R99605
TestNo: SW7010
Analysis Date: 6/17/2019
SegNo: 2163459
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimi( Qual
Flashpoint(140'F) 138 135.4 0 102 98 102
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantization range H Holding times for preparation or anal)
J Analyte detected below quantization limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V I
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit Page 27 of 29

SUMMIT 3310 Win Summit Technologies,
n Qualifiers and Acronyms
ENVIFIONrdEraTALTECHNOI.GGI[S,IMC Cuyahoga Falls, Ohio 442: WO#: 19060616
AnalyUcal Laberator7c? TEL: [phone] FAX: [phone] Date: 6252019
Website: hl(p:// vinp,senekco
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CC V recovery failed low (-) or high (+)_
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+),
QMR The MS/MSD RPD was outside of accepted recovery Inuits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quamitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
1CB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 28 of 29

ULTWOnn, o
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12
O
5
i
E
q
V
0
.wni.,,,x u•L��ne plmrl:JmnneN�': YIS W)F*.,,,kr l' 1nolfllll:
c. Tcmp! u -'ll a, YES o : mellnl
.__._,.�..._.........1 .....le...., ..—ack.mm

Ilazardous Waste Detrrnduatlon: Complete the 1`01101ving to demonstrate that the residuals are 11011-
htzardous under RCRA: (Note - this item does ain have to be contPietcd for facilities that are Ices than 0.5
MGD in design flow thm treat 100",10 non-munielp:d. domestic wastewater only)
a. Are the residuals kted in 40 CFR §261.31-§261.33: ❑ yes ❑ no.
If yes. list the numbetls):
b. Specify whether or not the residuals exhibii env of the characteristics defined by 40 CFR §261,21-
26l.24: ❑ Yes ❑ no.
Fill in like following tables with the results of the lute<t nuicity characteristic leaching procedure
(TCLP) analysis as well as those for croons ivity, igailability, and reactivity:
1.nh0mtory: _ and Dale ofanulysis:
Passed corrosiviq test: ❑ yes ❑ no. p11: s.u. (2 < pH 12.5)
Passed ignitability test: ❑ yes ❑ no. Fiashpoint: _ "F (> 14W)
Passed reactivity test ❑ yes ❑no. HCN•`_ ntglkg (<250) R H:S: - mgJkg (<500)
TCLP Parameter
Limit
Result
TCLP Parameter
Limit
Result
Arsenic
3.0
HcxachloroM:nzene
0.13
Barium
100.0
1lexacldom-1,3-Butadiene
0.5
Benz0nc
0.5
Hexachloroctlionc
10
Cadmium
I'll
Lead
5.0
_--
Carbon Tetmchlonde
0.5
Linden
o.4
Chlordane
0,03
Mercury
0.2
Chlombcoun0
L00.f1
Methoxychlor
1010
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobeuicnc
2.0
in -Cresol
200.0
Pentachlomphcnol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5,0
2A-D
10.0
Tetrachloractlrylene
0.7
1.4-Dielrlorolienrcnc
7.5
--
Toxaphcnc
0.5
--'
1.2-Dichloroah.me
0.5
Trichiomethylene
0.5
1.1-Dichlotoethylenc
0.7
2.4,5-Trichlomphenol
400.0
2,44)inirrotoluene
0.13
2.4.6-Trichlorophenol
2.0
&tdrin
0.02
2,4,5-TP(Silvex)
IA
Heptachlor and its
Hydroxide
000$
Vinyl Chloride
0.2

� � � Summit Environmental Technologies, Inc.
3310 Win Sr.
ENVIRONh1EWAL TECH NOLOGIF9. ➢4C. Cuyahoga Falls. Ohio 44223 Sample Log -In Check List
Pnalydcal Lahwalorfo's TEL: [phone] FAX., [phone]
Wehsile: hnor//rvrvntsenekcmr
Client Name: SYN-FL-33709 Work Order Number. 19060616 RcptNo: 1
Logged by: Jesseca E. Westfall 6/11/2019 10:20:00 AM
`�:e
By: Jesseca E. Westfall 6I12/2019 11:49:41 AM
111yy1
y�Completed
Reviewed By: Brian J. Fackelman 6112/2019 1:00:16 PM
.�y
Ghain of Gustodv
1. Is Chain of Custody complete? Yes 0 No ❑ Not Present ❑
2, How was the sample delivered? UPS
LOq In
3, Coolers are present? Yes ❑ No ❑� NA ❑
4,
Shipping container/cooler in good condition?
Yes
®
No ❑
Custody seals intact on shipping container/cooler
Yes
❑
No ❑
Not Present W
No. Seal Date:
Signed By:
5,
Was an attempt made to cool the samples?
Yes
❑
No R
NA ❑
6.
Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑
No W
NA ❑
Not required
7.
Sample(s) in proper container(s)?
Yes
©
No ❑
6,
Sufficient sample volume for indicated test(s)?
Yes
©
No ❑
g.
Are samples (except VOA and ONG) properly preserved?
Yes
No ❑
10.
Was preservative added to bottles?
Yes
❑
No 0
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials
12. Were any sample containers received broken?
Yes
No ❑
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly Identified on Chain of Custody?
Yes
©
No ❑
15. Is it clear what analyses were requested?
Yes
0
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order
Yes
❑
No ❑ NA
Person Notified: Date i_
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Samples were received at ambient temperature in a box.. TCLP does not require receipt within 0-6°C. Sample received broken,
sample was salvaged and client approved analysis.
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
I Seal No
Seal Date
Si ned B
box
ambient
Page 29 of 29