NCS000330_Monitoring Report Lab Results_20200220

4#X-AT1
b'jW�o NOpU�' o�
February 14, 2020 ®� ��� .8.ox 5030
�� R 10--roe,
Ashcraft Avenue
/
W ® NC 28111-5030
CV Attn: Central Files � done: [phone]
W O'�ax: [phone]
N.C. Division of Water Quality fy OcO *,mail: [e-mail]
1617 Mail Service Center o
Raleigh, NC 27699-1617
Central Files: Period 2 Sampling/Tier 2 Monthly Monitoring Status
Attached, please find stormwater monitoring data for ATI Specialty Materials — Monroe Plant
Permit No NCS000330. The originals and one copy are included. The monitoring data is for
the following monitoring schedule:
Monitoring Events
Sample Number
Start
End
Year 2 - Period 2 1
2
1 January 1 St, 2020
June 30th , 2020
Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
"I certify, under penalty of law, that this document and all attachments were prepared
under my direction or supervision in accordance with a system designed to assure that
qualified personnel prvperlygather and evaluate the in1brrnation submitted. Based on my
inquiry of'the person or persons who manage the system, or those persons directly
responsible forgathering the information, the information submitted is, to the best of'my
knowled#Ie and belief, true, accurate, and complete. I am aware that there arc, significant
penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations. "
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
Tyler Mercer
EHS Manager

aceAnalytical
www.pacelabs.com
February 04, 2020
Tyler Mercer
ATI Specialty Materials
2020 Ashcraft Avenue
Monroe, NC 28110
RE: Project: Jan Tier 2 SW02
Pace Project No.: 92462251
Dear Tyler Mercer:
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 24, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Danielle Barrack, Allvac
Mr. Tommy Long, Allvac
Mike McManus, ATI Specialty Metals
Scott Ryan, Allvac
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Project: Jan Tier 2 SW02
Pace Project No.: 92462251
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Jan Tier 2 SW02
92462251
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92462251001
Jan Tier 2 SW02
EPA 1664B
HH
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
SM 2540D-2011
CJL
1
PASI-A
SM 5210B-2011
JP1
1
PASI-A
SM 5220D-2011
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Jan Tier 2 SW02 Lab ID: 92462251001 Collected: 01/24/20 04:51 Received: 01/24/20 08:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Cadmium
Chromium
Lead
Nickel
Zinc
2540D Total Suspended Solids
Total Suspended Solids
5210B BOD, 5 day
BOD, 5 day
5220D COD
Chemical Oxygen Demand
Date: 02/04/2020 05:32 PM
Analytical Method: EPA 1664E
ND mg/L
5.0
1
01/30/2015:55
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
ND ug/L
1.0
1 01/30/20 00:41
02/01/20 12:52
7440-43-9
50.7 ug/L
5.0
1 01/30/20 00:41
02/01/20 12:52
7440-47-3
ND ug/L
5.0
1 01/30/20 00:41
02/01/20 12:52
7439-92-1
166 ug/L
5.0
1 01/30/20 00:41
02/01/20 12:52
7440-02-0
162 ug/L
10.0
1 01/30/20 00:41
02/01/20 12:52
7440-66-6
Analytical Method: SM 2540D-2011
7.1 mg/L
2.5
1
01/29/2017:32
Analytical Method: SM 521OB-2011
2.4 mg/L
2.0
1 01/25/20 06:07
01/30/20 02:47
B3, L1
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
25.5 mg/L
25.0
1 01/30/2016:20
01/30/2023:33
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
QC Batch: 522368
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description:
1664 SGT-HEM, TPH
Associated Lab Samples: 92462251001
METHOD BLANK: 2793943
Matrix: Water
Associated Lab Samples: 92462251001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 5.0
01/30/20 15:46
LABORATORY CONTROL SAMPLE: 2793944
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 18.2
91 64-132
MATRIX SPIKE SAMPLE: 2793945
92462220001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 20
16.1 75 64-132
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
QC Batch: 522196 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92462251001
METHOD BLANK: 2793100
Matrix:
Water
Associated Lab Samples: 92462251001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Cadmium
ug/L
ND
1.0
02/02/20 00:16
Chromium
ug/L
ND
5.0
02/02/20 00:16
Lead
ug/L
ND
5.0
02/02/20 22:37
Nickel
ug/L
ND
5.0
02/02/20 00:16
Zinc
ug/L
ND
10.0
02/02/20 22:37
LABORATORY CONTROL SAMPLE:
2793101
Parameter
Units
Cadmium
ug/L
Chromium
ug/L
Lead
ug/L
Nickel
ug/L
Zinc
ug/L
Qualifiers
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
500
466
93
85-115
500
446
89
85-115
500
494
99
85-115
500
465
93
85-115
500
482
96
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2793102
2793103
MS
MSD
92461767001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
505
508
101
102
70-130
1
Chromium
ug/L
ND
500
500
477
478
95
95
70-130
0
Lead
ug/L
ND
500
500
488
489
97
97
70-130
0
Nickel
ug/L
ND
500
500
487
490
97
97
70-130
1
Zinc
ug/L
148
500
500
621
483
95
67
70-130
25 M1,131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2793104
2793105
MS
MSD
92462200003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
509
510
102
102
70-130
0
Chromium
ug/L
34.5
500
500
554
525
104
98
70-130
5
Lead
ug/L
ND
500
500
516
513
103
103
70-130
1
Nickel
ug/L
125
500
500
656
599
106
95
70-130
9
Zinc
ug/L
223
500
500
722
707
100
97
70-130
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/04/2020 05:32 PM without the written consent of Pace Analytical Services, -LC.
Page 6 of 14

aceAnalytical
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QUALITY CONTROL DATA
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
U ; Batch: 522170 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92462251001
METHOD BLANK: 2792927
Associated Lab Samples: 92462251001
Parameter Units
Total Suspended Solids mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 01/29/2017:31
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 2792928 2792929
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Total Suspended Solids mg/L 250 248 234 99 94 90-110 6 25
SAMPLE DUPLICATE: 2792930
92462422002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 29.0 31.0 7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/04/2020 05:32 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
QC Batch: 521379 Analysis Method: SM 521OB-2011
QC Batch Method: SM 521 OB-2011 Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92462251001
METHOD BLANK: 2789465
Associated Lab Samples: 92462251001
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 01/30/20 01:18 B3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2789466
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 248 125 84.6-115 B3,L1
SAMPLE DUPLICATE: 2789468
92462056001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L 266 265 0 B3
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/04/2020 05:32 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
QC Batch: 522315
Analysis Method:
SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description:
5220D COD
Associated Lab Samples: 92462251001
METHOD BLANK: 2793592
Matrix: Water
Associated Lab Samples: 92462251001
Blank Reporting
Parameter Units
Result Limit
Analyzed
Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0 01/30/20 23:29
LABORATORY CONTROL SAMPLE: 2793593
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits
Qualifiers
Chemical Oxygen Demand mg/L
750 739
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2793594
2793595
MS MSD
2628213001
Spike Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone. Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L ND
100 100 120
120 109
109
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2793596 2793597
MS MSD
2628200003
Spike Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Chemical Oxygen Demand mg/L 3450
100 100 3520
3570 70
116
90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/04/2020 05:32 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
WIN itrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Jan Tier 2 SW02
Pace Project No.: 92462251
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92462251001
Jan
Tier 2 SW02
EPA 1664B
522368
92462251001
Jan
Tier 2 SW02
EPA 200.7 Rev 4.4 1994
522196
EPA 200.7 Rev 4.4 1994
522216
92462251001
Jan
Tier 2 SW02
SM 2540D-2011
522170
92462251001
Jan
Tier 2 SW02
SM 521 OB-2011
521379
SM 521 OB-2011
521415
92462251001
Jan
Tier 2 SW02
SM 5220D-2011
522315
SM 5220D-2011
522443
Date: 02/04/2020 05:32 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 11 of 14

Document Name:
Document Revised: February 7, 2018
/__�
Sample Condition Upon Recetpt(SCUR)
Page 1 of 2
Document No.:
ry
Issuing Authority:
i1G'tfAnaf leaf
) __
F-CAR-CS-033-Rev.06
— Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[]
Greenwood ❑
fluntersville
EI Raleigh[] Mechanicsville[]
140* Client Marne:
Project I
Courier: [Fed Ex [ ]UPS ❑USNS
❑C.lient
{ 1 fINLLL
1�Commercial
(Pace
❑Other;
1188111111 lilt ( ttttll tttlllttt UUUUUUtt tt UU ti
Custody Seal Present? Oyes (�No
Seals intact? []Yes
QNo
Date/initials Person Examining Contents:
F
PacE<fng Material: ❑Bubble Wrap
❑Bubble Bags (INone
[7] Other
Biological Tissue.Froxen?
Thermometer:
❑IR GUn ID; Type of ice: ❑Wet QBlue
Cooler Temp ('C): ) c � Correction Factor: Add/Subtract ('Q O.00C
Cooler Temp Corrected ('C):
USDA Regulated Soil (0' N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or, SC (check maps)?
(—iYes FIN.
DNone Uyes [INO ON/A
Temp should be above freezing to VC
®samples out of temp criteria. Samples an ice, cooling pror.ess
has begun
Did samples originate from a foreign source (internationally,
Comments/Discrepancy;
Chain of Custody Present?
(QY s
FIN r
❑N/A
_
1.
Samples Arrived within Hold Time?
[QYes
❑No
❑N/A
2.
Short (fold Time Analysis (<72 hr.)?
Dyes
❑No
ON/A
3,
Rush Turn Around Time Requested?
❑Yes
Q(i .
❑N/A
4.
Sufficient Volume? _
(QYes
_I ]Nu
_
QN/A
S.
Correct Containers Used?
-Pace Containers Used?
oYe
QVes'
ONO
(QNo
[JN/A
[IN/A
6.
Containers Intact?
(QYes
❑Nn
QN/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]No
EIN/A
8. _A
9.
Sample labels Match COC? ,; Yes QNo ON/A
s
-Includes Date/Time/lo/Analysis Matrix:
- 1-leadspace in VOA Vials (>1-6mm)? __
[JYes
(QNo
QNJA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
❑Yes
QNo
[]No
QN/n
QNN/A
11.
COMMENTS/SAMPLE OISCREPANCV
Field Data Required? ❑Yes ONO
_ _ Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION I
Person contacted: A T_ — Date/lime:
Project Manager SCURF Review: Date: a
Date:
Project Manager SRF Review: (%�
j g .....z �� \
Page 12 of 14

Document Name:
Document Revised: February 7, 2018
)aceAr�alytica!`
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
_
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
"Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coiiform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box Is to list number of bottle
Project #WO#:92462251
PM: MWB Due Date: 02/04/20
CLIENT: 92-Allvae NC
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot t1
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will besent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
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