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HomeMy WebLinkAboutNCG060095_Monitoring Report_20200116')r w�r td BErn Nn Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: littp://port tl.ncdenr.org/web/wghWS/su/npdessw#tab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: 406,s MMI—"T-Q. g x +- Date of Inspection: 1 a - Q 3 - Q01� Time of Inspection: 3 t 3s Total Event Precipitation (inches): I.1-1 . n Was this a Representative Storm Event? (See information below) es ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. ..............-................................ ............................................ By this signatu3;4 certify that this report is accurate and complete to the best of my knowledge: (Signature o/Permittee or Desf6ee) 1. Dut€ A-D"Griptiem: 3 w lzoop- Ra, «, t� �+e r •� Omf-&�. _L Structure (pipe, ditch, etc.) _ pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: sA•r++7 t� i-S.t�..6., �'1��,,.. VV k ` 1 6 C061. J 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: el.a.ar 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): vier.,,` Page 1 of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: _ U2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is nob solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 isnosolids and 5 is extremely muddy: 0j 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes EO 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No c¢ 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-20120613 �NCDNR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: littu://L)ortal.ncclenr.org/web/wq/ws/ku/npdessw#tab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: _Goulston Technologies, Inc County: Union Phone No. 704-296-6427 Inspector: rn --ma" Date of Inspection: _ 10 3 Time of Inspection: 3! 35 e►ry. Total Event Precipitation (inches): I . `) Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). ......... ..................... ...... ........................... .......... ........ .................................. ..... ................ ............... _._............ A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. ........... ................ ..... .............................................................................................................................-........................................ .............................. ......._.................... ...... ................_....................................... ... ............ .................... ... ....... ............. ..._... ...... ...... ......................... ..... ................. By this si nature, I certify that this report is accurate and complete to the best of my knowledge: � 2-Y � Z ,... _ _ -�7— (Signature of Permittee or 6esignee) 1. <: -,-f 1n/ R00 R tea �n S c I-►z �� -� dale, .era Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: WH '- A 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): non .e- Page 1 of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: P2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: b 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: D 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 10 8. Is there an oil sheen in the stormwater discharge? Yesio� 9. Is there evidence of erosion or deposition at the outfall? Yes Ko� 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-20120613 ( n �� ij I [ C �� - -)I Surfmc, Moolificotion Tochnolocgios January 13, 2020 Attention: Lily Kay North Carolina Department of Environmental Quality Division of Energy, Mineral & Land Resources Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Dear Lily, RECEIVED JAN 16 RECD DENR-DEMLk Land Quality Section Mooresville Regional Office Results from the roof run off stormwater sampling requested during our October 22, 2019 Compliance Evaluation Inspection are attached. The pH for both samples was 6.9. Please feel free to contact me at vmckinney@goulston.com or 704-296-6427 if there are any questions or if additional information is needed. Regards, ��..(", \ Veronica McKinney Human Resources Ma ager 700 N. Johnson St. I Monroe, NC 28110, USA P.O. Box 5025 1 Monroe, NC 28111-5025, USA PHONE 704-289-6464 1 FAx 704-296-6400 1 www.gouiston.com 1�;a'ce A nalXical / www.pacelabs.com January 07, 2020 John McTaggart Goulston Technologies 700 N. Johnson Street Monroe, NC 28110 RE: Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Dear John McTaggart: Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 26, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, I-foo5ka Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ms. Sally Duncan, Goulston Technologies Veronica McKinney, Goulston Technologies John McTaggart pCCRF\�\\ �lgeORAtQQy/ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 12 �paceAnalytical' www.pacelabs.com Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification It: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Paco Analytical Services, LLC. Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 12 �PaceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: RAIN WATER ROOF DISCHARGE 92458747 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92458747001 RAIN WATER ROOF DISCHARGE A EPA 1664B HH 1 PASI-C SM 254OD-2011 CJL 1 PASI-A SM 5220D-2011 LEF 1 PASI-A 92458747002 RAIN WATER ROOF DISCHARGE B EPA 1664E HH 1 PASI-C SM 2540D-2011 CJL 1 PASI-A SM 5220D-2011 LEF 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 aceAnalytical www.pacelabs.com i ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Sample: RAINWATER ROOF Lab ID: 92458747001 Collected: 12/23/19 15:35 Received: 12/26/19 11:45 Matrix: Water DISCHARGE A Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 01/06/20 13:30 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids ND mg/L 2.5 1 12/27/19 15:52 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/31/19 12:01 12/31/19 15:48 Sample: RAINWATER ROOF Lab ID: 92458747002 Collected: 12/23/19 15:35 Received: 12/26/19 11:45 Matrix: Water DISCHARGE B Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 01/06/20 13:35 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids ND mg/L 2.5 1 12/27/19 15:53 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/31/19 12:01 12/31/19 15:49 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 UU Batch: 517897 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92458747001, 92458747002 METHOD BLANK: 2772436 Matrix: Water Associated Lab Samples: 92458747001, 92458747002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 01/06/20 13:24 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2772437 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 37.6 94 78-114 MATRIX SPIKE SAMPLE: 2772438 92458866001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 5.3 40 44.9 99 78-114 Results presented on this page are in the units indicated by the "Units" column except whore an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 ,�;aceAnalytical www.pacelabs.com i I QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 QC Batch: 517022 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92458747001, 92458747002 METHOD BLANK: 2769232 Matrix: Water Associated Lab Samples: 92458747001, 92458747002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/27/19 15:49 LABORATORY CONTROL SAMPLE: 2769233 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 254 102 90-110 SAMPLE DUPLICATE: 2769234 92458634003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 830 1070 25 SAMPLE DUPLICATE: 2769235 92458746001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 69.0 70.0 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 Oro .---!;aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 517274 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92458747001, 92458747002 METHOD BLANK: 2770044 Matrix: Water Associated Lab Samples: 92458747001, 92458747002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 12/31/19 15:42 LABORATORY CONTROL SAMPLE: 2770045 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 744 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2770046 2770047 MS MSD 92458595001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 138 100 100 234 238 96 101 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2770048 2770049 MS MSD 2626933001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 28.2 100 100 138 122 109 94 90-110 12 R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 aceAnalytical www.pacelabs.com QUALIFIERS Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS R1 RPD value was outside control limits. Date: 01/07/2020 03:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 8 of 12 �PakeAnaljdical www.pacelabs.com i i QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92458747001 RAIN WATER ROOF DISCHARGE EPA 1664B 517897 A 92458747002 RAIN WATER ROOF DISCHARGE EPA 1664B 517897 B 92458747001 RAIN WATER ROOF DISCHARGE SM 2540D-2011 517022 A 92458747002 RAIN WATER ROOF DISCHARGE SM 2540D-2011 517022 B 92458747001 RAIN WATER ROOF DISCHARGE SM 5220D-2011 517274 SM 5220D-2011 517467 A 92458747002 RAIN WATER ROOF DISCHARGE SM 5220D-2011 517274 SM 5220D-2011 517467 B Date: 01/07/2020 03:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 12 2aceAnalytieal Document Name: Document Revised: February 7, 2018 d i Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: 1 F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood I•)untersville-Q Raleigh❑ Mechanicsville❑ y � Client Name: O V 7 Project is.: ��jj hat;- %.S(t)� Courier: ❑Fed Ex ❑UPS QUSPS ❑Client Il ll l I Il I'll" l 111 ❑ Commercial QPace ❑Other: �92455747 Custody Seal Present? ❑Yes QNo Seals Intact? ❑Yes „QNo Date/InitialsPerson ExaminingContents: Hacking Material: ❑Bubble Wrap /�r[]8ubble Bags []'None ❑ Other Biological Tissue Fyozen? Thermometer,,` (❑Yes ❑No .QN/A `p.IR Gun ID: 92T058 Type of Ice: []Wet ❑Blue ❑None Cooler Temp (°C): _ r� Correction Factor: Add/Subtract ('Cl O.00C 3 Temp should be above freezing to VC Cooler Temp Corrected ('C): [)Samples out of temp criteria. Samples on ice, cooling process USDA Regulated Soil _(Ja1N/A, water sample) has begun Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, nYes 17Nn uiuuumg ndvidn dna F'ueri0 niCO)r LJYeS LJNO Comments/Discrepancy: I Chair, of Custody Present? f�JYes ONO N; A 1. Samples Arrived within Hold Time? QYes ONO ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes o ❑N/A 3. -i Rush Turn Around Time Requested? ❑Yes (26 [:]N/A 4. I Sufficient Volume?LDyeS (-'f,n- .. (_f N/A S. - 6. _ Correct Containers Used? i Yes ; jNo ❑N/A -Pace Containers Used? 0%s �No ❑N/A Containers Intact? 0e,s ONO ❑N/A 7. r Dissolved analysis: Samples Field Filtered? _ []Yes []No~ ❑N/A B. T Sample Labels Match COO -includes Date/Time/ID/Analysia_ Matrix: Headspace in VOA Vials (>5-6mm)? ,•❑Q yes Oyes ❑No [lr•:o []N/A 6 g. 10. Trip Blank Present? Oyes ONO ' ❑Q N/gi Trip Blank Custody Seals Present? ❑Yes ❑No , 7 COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted. Project Manager SCURF Review: f stf r Project Manager SRF Review: Date/Time: Field DataRequlred? []Yes ONO Date: Date: i;V Page 10 of 12 Document Name: Document Revised: February 7, 2018 �AceAflalyfidal-" Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: f-CAR•CS-033-Rev.06 Pace Carolinas Quality Office *Checi( mark top half of box if pH and/or dechiorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project f: 5 7 7 PM: TIH Due Date: 01/07/20 CLIENT: 92-Goulsten U Q 2 ¢ Z C Z U A O 1O �j Z d ? V Q Z \ i� ? q Z a 'D 'O Z Z ry ry a Z y ti a a c Z v y zn N a 2 Z Q Z n _v 2 A z M O o. ccc > > > c S 2 _ U � O?^ O - � > 2�i � 'a v`v^ c= u U D u u 0) 2 DQ E J T Z c, Zu 7 73 a a a d a a a ..i a J ° G E E ¢ E ¢ ¢ E ¢ J o a^ O > ¢ > O > O > _ w 4 y` a w u v J �o J E Q c to •° ¢ A N rl o ^ .N-1 N h N ut N V u=. rl v ,-1 c N o ,.'I a E 2 E v E �f E y v y E N r1 E ul N E N N of O E E 1 _ a to a Co n. Co a m G. Go u co3 l7 l7 a l7 a l7 a .7 a t7 a l7 a t7 c>> W 0 0 o> O >$0. 1Ffl N M v Y z I(1- \N 3 4 —1- — N I 5 NNN 6 _ -•• -4- N NNN I \N \�N\ 7\�\N 8 N\ I 9 N \�\N I 10 2,\ N — 11 12 7 -- H Ad'ustment Log for Preserved Samples Sample tU Type of Preservative pH upon receipt Dote preservation adjusted Time preservation adjusted Amount of Preservative added tot JI I _I _.._, _..,._.,.. ..,,.... ,,,,,.�N„����� ,a�„N,��, o —vy ww ue5eni to ine r4onn Carolina UUMM Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 11 of 12 Iro< 0 z .) C; -Y- o 0 0 V 1 2 (NIA) OLIIJC)1(10 JL311ppa�j U 0 L, z u U U 0 U) .2 t-W — LL 0- (0 0 CO E 0 21 u uj 0-1 0 0 0 U) TI a) E N /A iga.L SISAIL'Uvt JOL110 fJ >, NOUN z w IOH D 0 I 'ONH 0 0 0 F 5.: . 'I I z Q� "OS'H 0 1 < a E ;-, 11 0 Z Palua—clun 0 SM3NIV1N0O JC) # U) f- < No11o:31103 -L\i c11,1.zj1 2111WIVS -r Uw 0 C) w 0 cl 3 Idl ws U (I;lj 01 3000 XI&LVI"'i 0- S 6 0 r)f 0) 05z- -(00 -0 0 LS 0 Z- Lu w a I— U) 2 U) E 40 Ul -1 I.I. 0 I- 2i z 0 t — C3 o uj -j w w fL (L z z 0 0 . Ul E w w z ti z it2 o of a. LU -i rL CY LU 0 L) z t 0 0 ge 12 of 12