SW8900419_MONITORING INFO_20100922

NOTIFICATION OF DISCHARGE REPORT
CHLORIDE SYSTEMS, A PHILLIPS GROUP BRAND
272 WEST STAG PARK SERVICE ROAD
BURGAW, NORTH CAROLINA
SEPTEMBER 8, 2010
CATLIN PROJECT NUMBER: 210016.17
ynC rETVEI7
SEP 222010
BY:
CATLIN
Engineers and Scientists
NC CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585
NC CORPORATE LICENSURE NO. FOR GEOLOGY SERVICES C-118

-,"Z"CATLIN
Engineers and Scientists
September 22, 2010
North Carolina Department of Environment and
Natural Resources
Division of Water Quality, Aquifer Protection Section
Attn: Mr. Charles Stehman
127 Cardinal drive Extension
Washington, North Carolina 27405
Re: Notification of Discharge Report For
CHLORIDE Systems, a PHILIPS Group Brand
Burgaw, North Carolina 28425
CATLIN Project No. 200016.17
Dear Mr. Stehman:
Post Office Box 10279
Wilmington. North Carolina 28404-0279
Telephone: [phone]
Fax: [phone]
www.catlinusa.com
On behalf of Chloride Systems, enclosed is one copy of the finalized "Notification of
Discharge Report for CHLORIDE Systems, a PHILIPS Group Brand" dated September
8, 2010 for your review files. Based on laboratory analysis, detected contaminant
concentrations were mitigated to below compliant levels for established 2L GWQS and
2B Surface Water Standards. Therefore, CATLIN recommends that the CHLORIDE
Site be considered for "No Further Action" by the NCDENR Division Water Quality -
Surface Protection, and Aquifer Protection Sections. A copy of this report has been
submitted to the NCDENR Wilmington Regional Office Surface Water Protection
Section as well.
If you should have any questions or concerns, please contact CATLIN Engineers and
Scientists at your convenience.
Sincere7)
Thom . Landis, P.G.
Project Manager
Enclosure
cc: Mr. Terry Hollingsworth - CHLORIDE Systems (Letters only)
Mr. Dick McLaughlin - CHLORIDE Systems (w/2 enclosures)
Mr. Rick Shiver - (w11 enclosure)
200017- Chloride Pond NCDENR Stehman Itr Sept 2010.doc

CATLIN
Engineers and Scientists
September 22, 2010
Post Office Box 10279
Wilmington. North Carolina 28404-0279
North Carolina Department of Environment and
Natural Resources
Division of Water Quality, Surface Water Protection Section
Attn: Mr. Rick Shiver
127 Cardinal drive Extension
Washington, North Carolina 27405
Re: Notification of Discharge Report For
CHLORIDE Systems, a PHILIPS Group Brand
Burgaw, North Carolina 28425
CATLIN Project No. 200016.17
Dear Mr. Shiver:
Telephone: [phone]
Fax: [phone]
www.catlinusa.com
On behalf of Chloride Systems, enclosed is one copy of the finalized "Notification of
Discharge Report for CHLORIDE Systems, a PHILIPS Group Brand" dated September
8, 2010 for your review/files. Based on laboratory analysis, detected contaminant
concentrations were mitigated to below compliant levels for established 2L GWQS and
2B Surface Water Standards. Therefore, CATLIN recommends that the CHLORIDE
Site be considered for "No Further Action" by the NCDENR Division Water Quality -
Surface Water Protection, and Aquifer Protection Sections. A copy of this report has
been submitted to the NCDENR Wilmington Regional Office, Aquifer Protection Section
as well.
If you should have any questions or concerns, please contact CATLIN Engineers and
Scientists at your convenience.
Sincerely,
Tho s andis, P.G. R'CLIV�
Project Manager SEP 2 2 2010
Enclosure
$Y:
cc: Mr. Terry Hollingsworth — CHLORIDE Systems (Letters only)
Mr. Dick McLaughlin — CHLORIDE Systems (w12 enclosures)
Mr. Charles Stehman - (w11 enclosure)
200017- Chloride Pond NCDENR Shiver Itr Sept 2010.doc

NOTIFICATION OF DISCHARGE REPORT
• .I
CHLORIDE SYSTEMS, A PHILIPS GROUP BRAND
BURGAW, NORTH CAROLINA
SEPTEMBER 8, 2010
PREPARED FOR:
CHLORIDE SYSTEMS, A PHILIPS BRAND COMPANY
272 WEST STAG PARK SERVICE ROAD
BURGAW, NORTH CAROLINA 28425
CATLIN PROJECT NO. 200016.17
PREPARED BY:
CATLIN ENGINEERS AND SCIENTISTS
P. O. BOX 10279
WILMINGTON, NORTH CAROLINA 28404-0279
[phone]
CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585

TABLE OF CONTENTS
PAGE
1.0
PURPOSE AND INTRODUCTION 2
1.1 DATE AND TIME OF DISCOVERY 2
1.2 PHONE NUMBER OF PERSON TO BE CONTACTED CONCERNING THE
RELEASE 2
1.3 RESPONSIBLE PARTY'S NAME, ADDRESS, LOCATION, PHONE NUMBER,
AND DIRECTIONS TO SITE 2
2.0
NATURE OF RELEASE: TYPE OF SUBSTANCE RELEASED, QUANTITY RELEASED
AND SOURCE OF RELEASE; 3
2.1 DOCUMENT THE PRESENCE OF FREE PRODUCT (IF KNOWN) 4
2.2 STATE HOW THE RELEASE WAS DISCOVERED (E.G. ODORS, SAMPLE
RESULTS, STAINING, ETC.) 4
2.3 DOCUMENT THE ACTION TAKEN TO STOP THE RELEASE 4
3.0
DOCUMENT THE NUMBER OF WATER SUPPLY WELLS WITHIN 1,500 FEET OF
THE RELEASE 6
4.0
ANY OTHER RELEVANT INFORMATION PERTAINING TO THE RELEASE OR
SUSPECTED RELEASE. 6
5.0
LATITUDE AND LONGITUDE OF RELEASE WITH A PRECISION LEVEL WITHIN 1
MINUTE. 7
6.0
EVALUATIONS AND CONCLUSIONS 7
TABLES
TABLE 1 SUMMARY OF SURFACE WATER LABORATORY RESULTS - EPA Method 8260
FIGURES
FIGURE 1 SITE LOCATION MAP
FIGURE 2 SITE LOCATION MAP WITH POTABLE WATER WELLS
FIGURE 2 SITE MAP
APPENDICES
APPENDIX A MSDS SHEETS
APPENDIX B LABORATORY REPORTS
Chloride; 200016 discharge notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17 1 September 2010

' NOTIFICATION OF DISCHARGE REPORT
' FOR
CHLORIDE SYSTEMS a PHILIPS GROUP BRAND
BURGAW, NORTH CAROLINA
' CATLIN PROJECT NO. 200016.17
I
SEPTEMBER S, 2010
' 1.0 PURPOSE AND INTRODUCTION
This purpose of this report is to provide formal notification and documentation
' regarding a one time release in accordance with UST Section Guidelines for the
Investigation and Remediation of Contamination From Non -UST Petroleum
Releases and NCDENR Memorandum: Initial Response and Abatement Action for
' Non -UST Petroleum Releases: a summary of current policy and Guidance, dated
February 8, 2010.
'
1.1 DATE AND TIME OF DISCOVERY
The initial date a discharge was discovered on Friday, August 06, 2010 at
'
approximately 4:00 pm. It was subsequently determined that the actual
discharge occurred on the afternoon of Friday, July 30, 2010.
'
1.2 PHONE NUMBER OF PERSON TO BE CONTACTED CONCERNING
THE RELEASE
'
Terry Hollingsworth- Plant Manager PH: 910.259.1126
Dick McLaughlin- Manager Human Resources PH: 910.259.1021
1 1.3 RESPONSIBLE PARTY, S NAME, ADDRESS, LOCATION, PHONE
NUMBER, AND DIRECTIONS TO SITE
(Refer to Figure 1)
' Chloride Systems, a Philips Brand Company
272 West Stag Park Service Road
Burgaw, North Carolina 28425
' From Wilmington: Traveling North on Market Street Turn LEFT onto
g g 2.0 mi
GORDON RD.
tjt' ► , 2. Merge onto 1-40 W toward BENSON.
21.4 mi
Chloride; 200016_discharge_notif.doc CATLIN Engineers and Scientists
CA TLIN Project No. 200016.17 2 September 2010

Take the NC-53 exit, EXIT 398, toward
3' BURGAW/JACKSONVILLE.
i41, © 4. Turn LEFT onto NC-53.
4v 5. Turn LEFT onto STAG PARK RD.
dR , 6. Turn SLIGHT RIGHT onto W STAG PARK SERVICE RD.
0.5 mi
[811FAM,
0.2 mi
7. CHLORIDE, 272 W STAG PARK SERVICE RD is on the RIGHT.
1
2.0 NATURE OF RELEASE: TYPE OF SUBSTANCE RELEASED, QUANTITY
' RELEASED AND SOURCE OF RELEASE;
(Refer to Figure 3)
' One time inadvertent surface spill on impervious surface (asphalt/concrete
loading dock area) while rinsing containers for recycle;
' Reclaimed screen wash solution; a byproduct of the silk screen cleaning
process. The screen wash solution is a mixture silk screen ink (9700 Series
All Purpose Screen Ink - NAZDAR SHAWNEE, mfg.) and ink wash solvent
' (XTEND PRESS WASH 105 — SERICOL INC., mfg.) created while cleaning
a silk screen tablet. MSDS Sheets are included in Appendix A
' A total of (4) empty Screen Wash waste containers (5 gallon) were found in
the recycle bin. These containers were used to hold the spent solution,
t along with rags and were reported to be were partially (1/3 to1/2) full before
they were emptied. Therefore, the total quantity of spent solution released
is estimated to have been 15-20 gallons at most. These and other waste
' products are normally properly disposed by CHLORIDE's waste
management contractor (ECOFLO).
' A temporary employee — assigned to final rinse previously cleaned and air
dried empty (5) gallon containers in preparation of recycle, inadvertently and
inappropriately emptied the contents of 4-5 (5) gallon similar looking
containers of spent Screen Wash solution which were partially (1/3 to1/2)
full. The Screen Wash solution was inadvertently poured onto the pavement
and then a hose was used to rinse out the (5) gallon containers. The running
' water from the hose - diluted and flowed the Screen Wash solution in a + 10
foot swath down across approximately 100 feet of pavement; where it
dispersed along the asphalt/ concrete surface and generally evaporated.
' Chloride; 200016discharge_notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17 3 September 2010

' (Temperatures in the 90+ range) However, apparently not all of the solution
( A g AA Y
evaporated — as it appears some of the diluted solution and water used to
' clean the pavement made its way to the sump pump (previously installed as
part of flood control measures) located in the low point of the loading dock
area. Enough water accumulated in the loading dock sump to activate the
' pump which in turn caused a slug of water to be pumped via hard piping to
the surface of the stormwater retention pond.
' 2.1 DOCUMENT THE PRESENCE OF FREE PRODUCT (IF KNOWN)
' Subsequent to the initial release, a CHLORIDE employee reported an odor
from the area of the stormwater detention pond - located directly behind the
loading dock. (Pond dimensions approx. 20 x 250 feet; depth 3 ft).
' CHLORIDE management followed up on the report and noticed the pond did
have a slight odor — but was observed to be full of bull frogs, small fish and
other aquatic life.
' Visual inspection of the pond revealed extensive algae cover over much of
the pond surface. A slight sheen was noted in the areas of algae cover
' however upon further inspection it was determined that the majority if not all
of this sheen was likely naturally occurring. When broken the sheen would
not congeal back together as is typical of petroleum sheens. In addition,
' when a sorbent pad was placed on the shield little to no product could be
observed on the sorbent pad.
I
2.2 STATE HOW THE RELEASE WAS DISCOVERED (E.G. ODORS,
SAMPLE RESULTS, STAINING, ETC.)
' The original discharge at the staging/loading dock area was discovered by
visual observation of staining caused by the spent dye on the pavement
where the diluted solution ran down the concrete loading area to the sump
' low point drain in the loading dock. As outlined in Section 2.1 the potential
for impact to the retention pond was initially discovered by odor. Impact to
the pond surface water was subsequently confirmed by collection of surface
' water sample collection and laboratory analysis.
2.3 DOCUMENT THE ACTION TAKEN TO STOP THE RELEASE
' Once CHLORIDE management discovered the release on Friday, August 6,
9 Y g
2010, they initiated measures to clean any residual solution which had not
1 already evaporated. The initial response was to scrub and pressure wash
the stained area of pavement. CATLIN Engineers and Scientists (CATLIN)
' was then contacted as to what occurred and for regulatory guidance to
mitigate the incident.
' • Based on the ensuing conversation between CHLORIDE and CATLIN
and the fact that the pond had been potentially impacted, CATLIN
recommended sampling the retention pond. Due to a lack of rainfall
' Chloride; 200016_discharge_notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17 4 September 2010

in the area over the summer months the pond water elevation was low
enough that no water was discharging from the stormwater discharge
point in the pond into the adjacent ditch. As part of flood proofing
measures installed after Hurricane Floyd (2000) the detention pond
was equipped with a shear gate valve which allows the pond to be
totally closed from discharge so stormwater can be stored and
pumped from the pond during flooding events. Therefore, CHLORIDE
was advised and implemented lock out of the closed shear gate valve
and pump to keep any discharge of the pond from occurring until the
water could be sampled and analyzed.
• CATLIN made a site visit on Monday, August 9, 2010 and
recommended as a precautionary measure that sorbent boom and
vacuuming be used to collect the areas of algae where a slight sheen
was observed. Approximately 30 gallons of algae and surface water
were collected and were containerized in a 55 gallon drum along with
the used boom for disposal by CHLORIDE's waste disposal contractor
ECOFLO. In addition, the sump reservoir at the loading dock was
vacuumed and cleaned with Simple Green to eliminate any residual
solution which may have been present.
• A surface water sample (SW-1) was collected by CATLIN on
Tuesday, August 10, 2010 for analysis per EPA Method 8260.
Review of the laboratory results indicated exceedances of three 8260
list compounds which have established 2L GWQS. Additionally, four
8260 list compounds were detected at levels above established 2B
Surface Water Standards. Laboratory results are summarized on
Table 1 and laboratory reports are included in Appendix B.
• On August 19, 2010, once initial abatement was complete and the
laboratory data received and reviewed, CATLIN officially provided
Notification of Discharge via telephone to Rick Shiver with the
NCDENR- WiRo DWQ on behalf of CHLORIDE. CATLIN agreed that
written notification would be provided and no water would be
discharged from the pond until levels were below the established
applicable standards and NCDENR approval was granted. Since 2L
GWQS exceedances were also detected CATLIN was also directed to
submit this documentation to the NCDENR-WiRo Aquifer protection
section as well.
• In the interim to further mitigate the confirmed impact, aeration of the
pond was planned to volatize the contaminates out of solution. A
base line surface water sample (SW-1 resample) was collected on
Friday, August 20, 2010 to more accurately determine contaminant
concentrations for design parameters of the aeration system. Review
of the laboratory results indicated the exceedances of the three 8260
list compounds which have established 2L GWQS and four 8260 list
compounds which were detected at levels above established 2B
Chloride; 200016_discharge_notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17 5 September 2010

1
' Surface Water Standards had been reduced to compliant
concentrations with the exception of Acetone (2600 ug/L) which
remained non compliant for the established 2B Surface Water
Standard (2000 ug/L). The reduction in contaminant concentrations
can be attributable to continued evaporation of the volatile
' compounds and an increase in water volume in the pond due to
substantial storm events. Laboratory results are summarized on Table
1 and laboratory reports are included in Appendix B.
' Over the weekend heavy rains completely filled the and and loading
� vY P Y P 9
' dock area to the point that water was within 1/2 inch of entering the
back of the facility. On Monday, August 23, 2010 CATLIN collected a
third surface water sample (SW-3) for accelerated laboratory analysis
' to confirm if concentrations were reduced enough to discharge the
pond water before another rain event caused the facility to begin
flooding. Initial screening results from the lab indicated that all
' contaminant concentrations were below established 2L GWQS and
2B Surface Water Standards. The final lab report confirmed the
preliminary laboratory screening results. Laboratory results are
' summarized on Table 1 and laboratory reports are included in
Appendix B. In order to avoid flooding the facility CATLIN, contacted
the NCDENR on Tuesday, August 24, 2010 in order to request
' permission to discharge the stormwater from the pond. Based on the
final sample results the NCDENR granted permission via telephone
to discharge the water which had been retained in the permitted
' detention pond.
3.0 DOCUMENT THE NUMBER OF WATER SUPPLY WELLS WITHIN 1,500 FEET
' OF THE RELEASE
(Refer to Figure 2)
' According to the Pender County Department of Environmental Heath potable well
inventory records have only recently been established for new structures as they are
completed. However the department indicated that public water supply is not
' available in the area. Based on the structures indentified within a 1500 foot radius
it is estimated that at least nine potable water supply wells are located within 1500
feet of the site.
' 4.0 ANY OTHER RELEVANT INFORMATION PERTAINING TO THE RELEASE OR
SUSPECTED RELEASE.
' With successful mitigation of the release the detention pond has been put back into
normal operation . Although a one time occurrence, procedures and protocols for
' waste stream management at the facility have been reviewed by CHLORIDE
management to prevent a similar scenario from occurring. In addition, the
necessity of following established, proper procedures and protocols for waste
' stream management have been reiterated to employees of the facility involved with
waste management.
Chloride; 200016_discharge_notif.doc
CATLIN Project No. 200016.17
CATLIN Engineers and Scientists
September 2010

5.0 LATITUDE AND LONGITUDE OF RELEASE WITH A PRECISION LEVEL WITHIN
1 MINUTE.
Latitude 34.563
Longitude-77.899
6.0 EVALUATIONS AND CONCLUSIONS
Since the release occurred on non pervious surface no soil impacts are believed to
have occurred. Based on laboratory analysis, detected contaminant concentrations
were mitigated to below compliant levels for established 2L GWQS and 2B Surface
Water Standards Therefore, CATLIN recommends that the CHLORIDE Site be
considered for "No Further Action" by the NCDENR Division of Solid Waste, and
Aquifer Protection Sections.
Chloride; 200016_discharge notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016. 17 7 September 2010

I

TABLE
Chloride; 200016discharge_notif.doc
CATLIN Project No. 200016.17
CATLIN Engineers and Scientists
September 2010

Page i of 1
TABLE 1
SUMMARY OF SURFACE WATER LABORATORY RESULTS
Analytical Method: EPA Method 8260
Incident Name: CHLORIDE Pond
m
a)
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Contaminant of Concern
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Sample Location
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2L GWOS {µg/L)
6000
4000
70
600
70
5
NE
NE
6
70
600
400
400
500
Varies
CHLORIDE Pond
SW-1
8/10/2010
5550
4.19
18.8
0.590 J
46.9
BOL
44.1
4.01 J
2.66
206
10.8
2040
559
61.63
BQL
CHLORIDE Pond
SW-1 Resample
8/20/2010
2600
11.1 J
0.840 J
BQL
1.09
0.27
1.64 1
4.82 1
BOL
5.05
1.33
39.3
51.2
232
BQL
CHLORIDE Pond
SW-3
8/23/2010
495
BQL
BQL
BQL
BQL
BQL
0.540 J
BQL
BQL
BQL
BQL
0.460 J
13.7
0.3
BOL
15A NCAC 2B Surface
Water - Freshwater Aquatic
2000
160,000
3.9'
97
320
590 HH
320'
26,000
330
80'
11
390
630
800
Varies
Life u L
CHLORIDE Pond
SW-1
8/10/2010
5550
4.19
18.8
0.590 J
46.9
BOL
44.1
4.01 J
2.66
206
10.8
2040
559
61.63
BQL
CHLORIDE Pond
SW-1 Resample
8/20/2010
2600
11.1 J
0.840 J
BQL
1.09
0.27
1.64
4.82
BQL
5.05
1.33
39.3
51.2
2.32
BQL
CHLORIDE Pond
SW-3 1
8/23/2010
495
BQL
BQL
BQL
BQL
BQL
0.540 J
BQL
BQL
BQL
BQL
0.460 J
13.7
0.3
BQL
' BQL = Below Quantitation Limits
J = Detected below the cluantitation Limts
ug/L = parts per billion
' 2L GWOS = NCAC T15A:02L Groundwater Quality Standards
(HH) = Human Health; Standard Based on consumption of fish -see 2B .0224
= as provided by NCDENR; Division of Water Quality -Classification and Standards Unit
' sec - Butylbenzene (CAS # 135-98-8): human health standard = No data available; freshwater aquatic life standard = No data is available for this chemical; 3.9 ug/L LID can be used (this is based on the use
of n-butylbenzene data as a surrogate)
4-Isopropyltoluene (CAS # 99-87-6): human health standard = No data available; freshwater aquatic life standard = 320 ug/L LD
' n-Propylbenzene (CAS # 103-65-1): human health standard = 3200 ug/L; freshwater aquatic life standard = 80 ug/L LID
Exceedance of 2L GWOS
Exceedance of 15 NCAC 2B Surface Water std.
1
' Client; CHLORIDE Pond 8260W.xls CATLIN Engineers and Scientists
CATLIN Project No. 200-016.17 September 2010

I

1
11
FIGURES
Chloride; 200016_discharge_notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17 September 2010

1
1
1

1
1

1
7

APPENDICES
1
0
1
1
L'
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' Chloride; 200016 discharge notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17 September 2010

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Chloride; 200016_discharge_notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17 September 2010

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"ALCOHOL" FOAM CO2 DAY CHEMICAL 'AATCR F=
a)NUSUAL ?T= Ora EXPLOSION 11AZAak0s: KEEN CONTAINDRN VTQHTLY CLp5ZD.
ISOLaTS FROM HEAT, 3PARKS, )IONO OF" ELtIMES. CLOSED CONTAINERS MAY
ItUIPTURE ±1Mr-W VSPOSED TO 7EXTF..EMe HEAT. WhTER MAY 6E USED TO COOL
ONRUVrURZO CONTAINER9.
DURING 7-tjMFtaENCY CONDITIONS, nvGnXX80SUR13 TO DECOMPOSITION FIIODUCT3
MAY CONSTITUTE A HEALTH NIALARD. SYMPTOMS MAY NOT HE TwEDTATELY
APPARENT. ObTAXN MEDICAL AITY)NT100.
SPECIAL FTRE$'IGnTING PROCEDURES: ::ATZR MAY SO UNSUITABLE FOR US£ O-W
13Uaib %N* LIQUIDS. FULL PROTP-CTLVE tQVIVMENT 15 fLZCoMnb-.NoxD TO PROTECT
fZRE GTIGHTERS r 20;7 :MY HAZARDOUS DFCCMPOSITION PRODUCTS.
WATER SPRAY MAY BE INHZ?Z*CTzvY. IF WATER MOST 3E USED, FOG NOZZLES ARE
li=CblLY ARYFERABLE - WATMIX MAY OE UyaO TO COOL CLOSED CoNT'AINZN3 TO
PREVENT PRESSURZ BUILD-UP AND COSSrSLK AUTO -IGNITION OR EXPLOSION WHRU
bx809 a TO FXTREMM FRZAT.
38CTION V --- eo=RG _NCY ARID FIRST -AID
e
-PROCEDURES ...rY --
5-'-....�___ +a•CJ�W�.Ar�e� --..ASS--r --
y ... -
PRIMARY ROUTES OF ENTRY AR9 DERMAL AND INHALATION.
3WALLOWIAC: "lvZX EMERGENCY M IMOICAL ATTENTION- ' mTz PRODUCT IS 3LICUTLY
—
TOXIC 9Y INC ZSTZON AND AX ACPIRATIO14 RAZARD, TP VICTIM iD 0140WUV OR
-J-NCQNSCIQUS, PLACM ON THE LEFT SIDE wITR THE READ DOWN AND ❑O NOT r: TUM
1LNYTHING BY MOUTH. IF VICTIM IS CONSCIOUS, ALERT FIND NOT .SPONTANEOUSLY
VOMITINC, TnEW VOMTT'TNG 9%ROULD Slit INCUCED FOR I-NCE STIONS OF LARGK AMOUNTS
(MORE THAN 5 O"CrS IN AN ADULT) PPZTH;RAB7,Y WITH SYRUP Or TPLCAC CINDER
a
DIAI;CTION FROM A PHYSICIAN OR P0I3ON CL"NTYI%. IF POSS'IAT-e- DO tWOT LEAVE
VICTIM OVATTEINDEA.
SKIN CONTACT: REMOVE`, CONTAMINATED CLOT( lN5. WASH THOROUGHLY WIT" MILD
SOAP AND WARM WATSA. CONSULT A PHYSICIAN IP HERE ZS ANY PERSISTING
'IRRxTr�Tzot� .
INHALATIONS IF RESPIRATORY SYMPTOMS OR OTHER SYMPTOMS OF EX$OSUAZ DEVELOP,
MOVE VICTIM AWhY Z.ROM 9OURC0 OF EXV0dVhM i%ND INTO FRESH AIR. IF 5IMPTOMS
pZRsXST, SEMN IYR4EDIATO bWDXC4. .4TTXNTZON. IF VICTIM TS NOT BREATHING,
ARTIFICIAL RnSPIRATION SHOULD BE ADMTNISTMrAZD. xF SREATR;ING DIFZZCULTSES
❑zvr.Lop, OwYGEN SHOULD ma v.DmxuisTrRzo BY 4UALIFi$p PL'it+,�owwEL. 39EK
1MMEIDTATF, MEDICAL ATTENTION.
.YES CONTACT: MOVE VICTIM AWAY FROM EXPOSORS TO VAWORS AND INTO FRESH AIR.
IT IRRITATION OR REDNESS ❑ZVELOFS, SEEK MEDICAL ATTENTION- FOR DlkKCT
CONTACT, 11=3 nYELZD3 APART PaNtl FLUSH TRA AFFECTED L'YE fS) WxxH CLEAn wArrtt
SOLt AT LG1►T 1-5 ximuTE5. 9£LK MEDICAL oTTCNT3019,
SP9CIAL NOTES T4 ATTZN0jN* ?HYSICSAN: T:HERF. I3 NO 3PL*CI£'IC AXTTCOTZ-
TRSATME" OT OVICRBXPOSURR SHOUL13 aX TiIRPLI lTdD AT CONTROL GS 714P. SYMPTOMS
AND THE CLINICAL CONDITION.
SECTION vY SIGNS AND SYMPTOMS Ob' OVER—EXPOSURET
I

al dA"d INV S833NI M N1103-01 _wail wr90:00 01-90-sny PRA14IRN
ul U4/ „M 111',U 14: JJ FAA S(11'tUi
@ 003eat
PAGOGN XPW-105
ACUTE F_F'F':SGT:3:
1
::yii1LLOATN(3� 7HI3 MATERIAL, 111t�!s A LOW DEGHXX Or T=TCYTY. 11432:JITXON OY
MxCXsrruZ QUAWTITTnS MAY "Q9Z tk1k1TaTIOM Or THO DIGESTIV13 •rR..CT AND SIGNS
CT lV$RVQUS 'iYSTI:M ❑EPRZSSIQN (E.G.. IIAOWSINeSS, DIZZINESS, LOSS aF
CC0nDINATICN AND rATZGUE) . ASPIRATION HAZARD - ONE Old MORS COUPCNENTS ON
'axis HATERIAL CZW B\ITEA i_{3)ucs L:UAINr; :'WALLOWING OR VOMITING nND CAUZZ Lawc
ZNIFLAMMATTON AND DlUMAQ$.
: 'KTN ABSORPTION: CONTACT MAY RESULT IN :THIN ABSOI PTiON 2uT SYMPTOMS OP
TOXICITY 14AM NOT X4TTCrr^TSD b7 THIS :SOUTZ ALONlS 13D)CY,1t 17gRMAI. Cull ITLQnB
'
07 U50. 2ZRSONS W'IT9 PRL-RXIET$NG rKIN 0I60auimgS MAY aS MORH 303C=PTIBL9
TO THE EFFECTS OF THIS MATERIAL.
TNIThThM10Wti THIS N'xT%RTAL 11AS A 'LOW DLO }; ow -roX'IGITY GY INHALATION.
BRI,ATBINC nGH c,ONCENTRATIONS Of VAPORS OR MISTS MAY CAUSE I14RITATION OF
T113 NOSH AND THROAT AND c;jCN8 OF NOPLVOUS SYSTEM t?L'1"flffi9SION. PROLONGED OR
RZEMATEU EXPOSURE TO VAkIORS OR M12TS MAY CAUSE LIVER AND KIDNEY DA14lptGE AND
DLOOD M13OUDZRS (ANFtAT A) . RE3PIRATORV SYMPTOMS ASSOCZATUD WTTH PAE-
IiXISTZNC LUNG DISORDERS IZ.C., A&TfiMA- 'Lx:t9 CCNOITION3) MAY MM AGC-PAVATCD
3Y EXPOSURE TO THIS MAT£RTAL-
SXIN CONTACT: ONE CR MORE C❑UPQNENTS CAP THIS MATERIAL MAY CAUSE SEIN
IRRITATION. FROLUNG&O OR RZ-.BAT1rSL7 CONTACT MAY CAUSE REDNESS, SURNTNG AND
DMYINO AND C,ZACX=N3 OF THE SKIN AND BXIN OA1dAG85.
zXZ codT.ACT: ObM Oh MC RE; COrIPONENT3 02- THIS MATERIAL Y3 AN LLYIS IRRITANT.
DIRECT CONTACT WITH THE LIQUID OR EXPOSURE TO VAPORS OR MISTS MAY CAUSS
STZNGING, TEARING. REDNESS AND SWELLING.
COIAMITTFWS KNOWN TO BE ACCA&VAT20 BY OVZRZXPOSMAM. BL:S-ZXISTING KIDNEY,
L:VKR, -, 7Lovo DISORDERS rVAY 34 nC;CRAVATE0 BY EXPOSURE TO THIS MATBRI.AL,
CHRONIC ZryZCT3.- ONE COCSPONXWT r.,AUSg❑ TAZ TOLLAWINC ESLTECTS IN 771SORaT01iY
AN:LivrA1,3 - ANEMIA, LIVBEt AHNGRI`JALx tixL g, XTONEY DHmAam.
ADDITIONAL KNOWN HLkLTH HAZARDS: REPO;,TS HAVE ASSOCIATE'n rF=Qw=v OR
REPEATED OCCUPATIONAL OVEREXPOSURE TO SOLVENTS WITA PERMANENT BRAIN AND
NEF.VOUS SYST2H nnxa ;9. IDITENTIONAL MIS0813 13V DEL2B£RATZLY CONCENTRATXWO
AND INIU=N6 THE GONTRNTS MAY BE HARMFUI. OF r2%TAL-
- _--
SECTION VII -- REAC'TIVITY DATA
'
THIS LOIRTURS 25 STAbLs AND nAZARDOUS YoLyX4naaTLON wTLL w= OCCUpt.
INCOMPATIBILITY (MATERIALS TO ,A,VOTO) : STRONG ACIDS OR BASES, OXIDI2ING
aC33NTS, 3ELECTSD ANINFS, 4INC, ALUMINUM, AND ALicALXtS.
HALA.ADOU3 =r_0M"JTTZ0W PRODUCTS. TtICRMAL DECOMPOSITION IN THE PRESENCE OF
'%XA MAY YY1wLC CARRON MONOXIDS AND/OR C.A BON RIOXIDE.
CCrtQ=1rXQmS TO AVOID: ZXTR AZ T meAsAwuR85, 5PARKS, OVEN ?LATHES OR ANY
OTHER IGNITION SOURCES,
LECTION `rxxx -- �rVXL . OR LEAK P1?OCEDURES
STgVg TO UZ TACKN Zr NATZATAL TS SPILLED OR AMy=ASZoe UZTNG NoN-
SPARKING 'LTDCL5, PtAC't LZAhINQ CONTAI14eRS IN A 91E:LL VEPNILATF_-0 AREA.
ELXH'XXX'9Z AL';j BOURCESS OF 11CAT, 3PA"S, OR !!GNTTTQN. NOTITY PROPER
AUTHORiTIEZ IF PUBLIC WATERS OR -XW2RS ARE CCWTAMIPIATED.
WEAR APPROPRIATE PROTLCTIVR CLOTHING AND RZSPIRATORY PRCTECTION
u,OUIPMENT 'AiIEI.1 LATZRINQ TXZ OVILL AATA. SHUT OFF LEAK IF IT CAN BE
DONE SAFELY, VENTILATE THE AREA. DIKE AND Pt MP OFF LARGO S12ZLLS
3
I

I i nerd ,1V S�33050 WIVO-01 _lufli j lar90:80 01-60-Inn p"AIQzeJ
u,1r UC/ LUf1J IMU l4; 34 11Al surico
1
( 004/a
'
mS[)S# XPW-105
fNTO UALVAGIJ OA :,'VOMCI4 CONTAINERS. TAAM UP RGG,TOUL OR :1MNLL JPTLLS
W IT4 A9SORRENT KATF,RTAL JUCH AS CLAY OR VEi:Rm1CCSLIT3. nccn ] UV ALL
ti:AIVTAM�trRTLO 5OYL ANn DT-5imiv. OS Vm .3AP19C MANNEfi Ai T111:1 v?k0OUC:T.
NASTE DISPOSAL METHOD: AS A HAZARDOU3 !4ASTL, THIS MATCAXA,L MUST 73E
U1320590 Off' IN ACCORDANCE: WTTS ALL FEDF-AAL, STATIS, AND LOCAL
�ALyx�lxulcres_ INQUIRE OV YOUR LOCAL ZNVIAON41r24TAL A4P-WCZ"£S FOR T" 2XACT
1,613AL IiP_jZ[]2flvylg(GT T 'EEC YOUR ARIA.
IIEMR 70 3EG7E'71QN3 TV, V, VI, WEI AND IX DE TRX9 DOCUMnNT 5HL00ri17 ATTEMIPTING
I;1,EANC7P.
—_—_.----------._
---------__---'-- ------
--
BECTTCN TX SAFE HPONDLING AND USE INFORMATION
------- ---------.y------_TyOL,r,e�=��t���.11�'d�==���L'Ih4��
R3SPIRATORY PROTECTION: VXERZ CCNCENTRATIONS IN AIR MAY EXC9ED 'CHIC
'
fJIMIT3 GIVEN LN :SECTION IT AND nNO.INOMAtN I, WCRR PRAG'I'TC% OR OTHER
MEANS OF EXPOSURE REDUCTION ARE NOT ADEQUATE, ?1IOSH/MSHA APPROVED
RESPTRATO145 MAT bE N4CE3SARY TO l?KL-,,vANT CV?TIG�GPC750RC.
VENTILATION REQCJIaMIENTS: LOCAL 9XAAUST RECOMMON DED WREN APPROPRIATZ TO
CONTROL EXPOSEJRE To MIST OR ,1CROSO►,S. CL'N]i6AL EXHAUST is WOVXALLY AmEODATT
TO MINIMTZId EXPCSURS TO VAPORS.
i'AOTECTIVS GLOVES: RUBBER OR NEOPRENE TO MINIMIZE .SHIN CONTACT.
EYE PROTECTION: 3AnTY GOGGLES OR TULL FACE SHIZLO.
HyisIENIC SAFETY PRACTICERc WASH ISANDS 30VORE MATTNO, USING TOaACCO
PRODUCTS, 92 USTDIG TH.$ ASHROCM. TODALCCO AND PAGE .SHOULD Zr CUNSUDMD IN
3L9IGNAT7;D PAZA3 ONLY.
ADDITIONAL SAFETY EQUIPMCNT: IMPERMEABIA APRONS ANO >30OTS. SAFETY SHOWER
AND EYE BATH SHOULD 22 MAOE AVAIIABLX.
--_------..--------
SECTIOAI X SPECIAL. PRCCF.0t7P85
-------.--_ —. r -ter.----_
TRANSPDXTATI01v, STOKAGE AND KA1r DUNG: AVOTP CONDITIONS LISTED IN SECTION
VII. AVn:C0 WROLONGED 2TORAGE XT ' V-MPERATUIiF,'8 FN ZXCE88 Or 100 P.
OTHER I'REC:AUTIONS: NONE.
------T --
OECTIDN XI DISCLAIMER
GRATCOLP two, W'RM3 No WNR?JL1STY, EXPIi£98IID OR LMPLVMD, c%z To THZ ACCURACY
OR RKLIABILITY OF INFORMATION CONTAXPIED AERSIN, Z:XCEPT THAT SUCH
It rOAMATION I.+, TO T= BE5T or SL°RICOL' S XwcwLGDCS Aran b]CI.IMT, ACCVRATZ
AG OS THE DATE :CNSDTCAT%O ON THIS DOCW-MNT. TtNAL 0ETERMINATT021 qs
SUITABILITY OF ANY M&TER= IS THI SOLE RES?0NS1BTLmTY OT THE USER. .ALL
MXTZRIALS MAY MSBENT UNKNOWN HEALTH 11ALARD5 AND S NOUI,D 13E USED WITH
cAUTIoN, ALTHOUCH CERTAIV 1{i ZAADS ARIr 02sc xaED Rr2.ZzW, Wx cAiTWOT
GUARANTS:M 1THftT TBESE ARE' THE ONLY 1'IA7ARDS THAT EXIST.
SECTION XI1: ?URCHA5XX' S ❑BLIMATIC Z
SERSc4L, INC. URCP 3 THE COSTO:EER XVCEZVING IRIS N&TERTAL SAFETY Dr4TA SH='r
TO STUOX TV ChRYiULLY TO oxcOs+1E AWARE or H, ZARDSI, IF ANY, OF THD PRODUCTS
INVOLVED. IN THE INTEREST OF SAnTY. YOU SHOULD (1) NOTIFY YOURuY
mmrLOYEES, AGXWTO, AND CONT%IACTOR3 OF TMZ INFORMATION? ON THIS SkIEBT, (2)
170UNIUR A COPY To TACH OF YOUR COSTWERS OCR THIS PRCCUCT, I1 0 131 REQUEST
YOU"A CV57(MVERS TO I11YORM THEIR ZMYLOYZES, CUSTOMRS, AND AGENTS, AS WELL.
-----------------
SIJC'i'20N1 xIII REGULATORY T'NFQ[iMAxiOin
�..,
4

z( ;iepd ()MY S833N{9N3 N003-01 -ua13 'U►.10:60 01-60-9ny PaAIiuq
' vv, v ll cuv, }tr,u l:l: a1l Ml sorico 1 .4005/0
lv160EJ� ;Cs?W-7U5
TOXIC :!"SOTANCES CONTROL ACT ',T£CA) .;'V.VfUZ i Tl;% jN%;LZrDIFNT$ OLD '1'H28
PRODUCT ARE LISTF,D ON THE TSCA .INWKNTORY.
,ruz:'. VR,3MTJCT CONTArNs A TOXIC CWk!polC.aL OR CS UNTCALZ UVBJ 7GT TO TIE bNNOAL
m rCRTING RCQUIREMENTS 07 JECTION 311 air TITtZ -rig OF TIi`E 3UPERrONO
,"VHNDKE'ivTS AND REAUTTIOR1ZATION AC'r op 1096 HNv 40 CFR PART 372.
OONTHTt�TS: L,2, �-TPtTa�7'riYLaEN��;vf, CA58 40-d9-e
100 'ay WOMCHT.
CUMEiNZ, CA50 10-82-6,
1.Sl: 3Y WZJCAT.
A*e'LZNZ, CAJ* 1330-20-7
3.51k BY WICRT.
THIS NOTIr'rCA'TION MUST NOT BE DE,TAC94D FROM THE blkTmAlAL 3A.BETY DATA SKEL''T
(MSDS) AN❑ ANY COPYING AND REDISTRIBUTION OF THE MSDS SRALL INCLUDE
COPYING "0 REDISTRZOUTION OT 'T"U NOTICE !AT"TAChXg) TO GOPSLr5 OF THE MSMS
SUMS2004OTLY RSDTSTRTnUT=0-
3TATZ OF C&LIZ-OANIA 3ArZ UAINXING WATZK AND TOXIC ENFORCENE1V'L' ACT Or
1906 (PROPOSITION SS): THIS ?R0DUCT DOES NOT CONTAIN CHEMICALS KNOWN TO
itli STATE OF Cp.LxroRrJTA TO CAOSZ CANCER, OR RL"sROOUCTLVE TOXICITY.
STAT13 OL* CALTt-OANTA 'SOUTH COAST AIR CUALITY �,+nU=&NZWT DISTRICT RULM 103:
Lj"O-:OChFMTCALLT Mr.AGTIVIL BY ❑EFYNXTION,
1
0
6

ZO AREd ONY S833NIDN3 NlIiVO-al -wolf WERO:60 01-60•-EMY PQhlaOaa
MATERIAL SAFETY DATA SHEET PAGE: 1 OF 6
E OF LAST CHANGE: 05/23/05 DATE PRINTED ........... : 10/13/05
ACTURER'S NAME:
UUAR SHAWNEE EMERGENCY TELEPHONE #: [phone]
(U.S. and Canada)
8501 HEDGE LANE TERRACE EMERGENCY TELEPHONE #: [phone]
W,AMEE (OULsida U.S. and Canada, collect calls are acceptad)
66227 USA INFORMATION TELEPHONE #: [phone]
SECTION 1 -- CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
......---.-•-•----------
CODE: 97NL
IDE NAME...: 9700 SERIES ALL PURPOSE SCREEN INK . H M I S C 0 D E S -
fUC7 CLASS: SCREEN INK
SERIES...:
HEALTH 2*
FLAMMABILITY 2
REACTIVITY 0
PPE X
WT
VOC
VOC
X VOC
Off
VOC
VOC
x VOC
Item Description--•••••
9719 FIRE RED
19-7-2-2-U-L'TRA
lb/gal
8.3
g/L
575
lb/gal
4.8
volumes
64
------Item Description• •---••
9721 PEACOCK BLUE
lb/gal
8.6
g/L
569
lb/gal
4.7
volUtde
53
BLUE
8.5
585
4.9
65
9724 BLACK
8.3
588
4.9
65
9727 MIXING/OVERPRINT CLEAR
8.1
617
5.1
68
9748 FLATTING PASTE
8.9
672
5.6
74
9758 TINTING WHITE
4760 ORANGE
10.5
8.5
545
562
4.5
4-7
60
fit
9759 TINTING BLACK
9761 YELLOW
8.3
8.3
595
573
5.0
4.8
66
63
762 WARM RED
8.3
589
4.9
65
9763 RUBINE RED
8.3
585
4.9
65
764 RHODAMINE RED
8.7
$75
4.8
64
9755 PURPLE
8.5
580
4.8
64
9766 VIOLET
8.3
591
4.9
65
9767 REFLEX BLUE
8.4
577
4.8
64
,9760PROCESS BLUE
775 SUPER OPAQUE WRITE
8.8
11.2
570
518
4.8
4.3
63
57
9769 GREEN
9780 YELLOW TONER
9.2
8.3
563
584
4.7
4.9
62
65
781 ORANGE TONER
8.5
574
4.8
64
9782 CARMINE TONER
8-2
587
4.9
65
9783 MAGENTA TONER
8.3
583
4.9
65
9784 MAROON TONER
8.3
599
5.0
66
9785 GREEN TONER
8.5
583
4.9
65
9786 BLUE TONER (65)
8.4
576
4.8
64
7 BLUE TONER (RS)
8.3
576
4.8
64
9788 VIOLET TONER
8.2
596
5.O
66
F71
789 RED TONER
8.4
583
4.9
65
97PB12 TRANS MEDIUM YELLOW
8-2
592
4.9
66
818 TRANS RED
8.2
621
5.2
69
97PB60 STOP SIGN RED
8.2
589
4.9
65
TTB HALFTONE BLUE
8.2
708
5.9
78
97HTBK HALFTONE BLACK
8.3
685
5.7
76
97HTEX HALFTONE EXT BASE
8.3
696
5.8
77
97HTR HALFTONE RED
8.4
692
5.8
76
7HTY HALFTONE YELLOW
8.4
700
5.8
77
97LF 1D PRIMROSE YELLOW
8.6
569
43
63
7LF 11 LEMON YELLOW
8.6
556
4.6
62
97LF 12 MEDIUM YELLOW
8.5
556
4.6
62
7LF 13 EMERALD GREEN
8.8
573
4.8
64
97LF 18 SCARLET RED
6.3
574
4.8
64
97LF 20 BRILLIANT ORANGE
8.4
570
4.8
63
.0
0
.0
0
------------------------
SECTION
--- ..••...COMPOSITION,......------•INFORMATION•-----•---•-ON-------.......
2
............................
INGREOiEN75
.-----------------
....
-••------•....................................•--•-----------------•--..........-----------------•--------------•-------------------
CHEMICAL NAME:
PERCENT
OCCUPATIONAL EXPOSURE LIMITS
VAPOR
C ON NAME.
BY
.......ACGIH
....... .......OSHA........
PRESSURE
CIINUMBER
WEIGHT
TLV PEL
IN mmHg
NOTES
----------•---•------------•
* 2.BUTOXYETHANOL:
----------
38.64
20 Ppm 25 ppm
0.6
@ 20C
E LENE GLYCOL MONOBUTYL ETHER:
Skin
C #: 111.76.2
R N MIXTURES:
13.34
NOT NOT
41 @
20C
CAS #= NOT AVAILABLE
ESTABLISHED ESTABLISHED
R L BENZYL PHTHALATE;
-
2
NOT NOT
0,16
@ 150C
(
1)
P TICIZER:
ESTABLISHED ESTABLISHED
I
#: 85.68-7
f�IUM DIOXIDE:
#: 13463-67-7
SILICA, AMORPHOUS:
#: 112926-00-8
BUTOXYETHANOL ACETATE:
LENE GLYCOL BUTYL ETHER ACETATE:
;V-..1 112.07.2
ENTS;
JURE;
:AS #: NOT AVAILABLE
0.36
0.23
0-15
0-11
10 mg/m3
10 mg/m3
20 ppm
10 mg/0
Total dust
10 mg/m3
6 mg/m3
NOT 1.0 @ 20C
ESTABLISHED
15 mg/0
Total dust
N/A
N/A ( 2)
( 3)
N/A
( 4)
1

a EO RXed M S833MN3 NIiIVO—ol —wo)d we80:60 01-60—anV PRAIenRd
1
IDUCT CODE: 97NL
HOUS FUMED SILICA:
: 112945-52-5
CARBON BLACK: 0-d
PIGMENT BLACK;
#: 1333-86.4
UBJECT TO REPORTING REQUIREMENT OF SECTI N 313 OF TITLE
III OF SARA (4-0 CFR PART 372).
NAZDAR SHAWNEE PAGE: 2 OF 6
.............................
NOT 20 mppcf
ESTABLISHED
3.500 mg/m3 35.00 mg/m3
N/A 1 ( �....
y
N/A
) Supplier recommended exposure limit of 5.0 mg/m3.
) When referencing 'TSCA, use Silica CAS# 7631.86.9. CAS# 112926-00.8 was created to help further categorize the family of
Silica. It has not yet been listed on TSCA.
3) NIOSH has set a Recommended Exposure Limit (REL) of 5 pp+m.
This chemical is included an the list of Hazardous Air Pollutants (HAPs) from Title III of the Clean Air Act Amendments of
1990 (Glycol Ethers Category).
See Section 8 Exposure Controls. Personal Protection - Exposure Guidelines for more information on exposure limits.
5) When referencing TSCA, use Silica CAS# 7631.86.9. CAS# 112945.52.5 was created to help further categorize the family of
Silica. It has not yet been listed on TSCA.
The recommended ppermissible exposure limits (PEL) indicated above reflect the levels adopted by OSHA in 1989. Although, some
of the 1989 lavzls have since been vacated, the Nazdar Company recommends that the lower exposure levels be observed as
reasonable worker protection.
1 NOTE: Due to the broad spectrum of colors each MSDS may represent, ranges of some ingredients listed in Section 2 may exceed
those specified in the Canadian Controlled Product Regulations. If specific concentration information is needed to comply
with this regulation contact Nazdar's Regulatory Compliance Department at 913-422-1735.
.................. ..................................
...IFICATION.---....--........---------------------------------.........------.
SECTION -- HA2AROS
AEl-RAI-L"HE"-A*L-rH"E"'FF'E'C'T'S ---------------------------­ * ----------------------------------------------------------------
------------......------------------------------ ---------------
THE FOLLOWING INFORMATION HAS BEEN DEVELOPED BASED UPON USING THE PRODUCT AS INTENDED By THE MANUFACTURER. The potential
health effects of this product are based on the hazards of its components. The use of this product in combination with other
products may product synergistic (additive) health effects. Ccutionary labeling and matarial safety data sheets of all
`aerials used with this product should be reviewed before use -
EYES
Eye contact with liquid, vapors or mists may cause moderate to severe irritation, including burning, tearing, redness or
swelling.
SKIN
Skin contact may cause irritation. Symptoms may include dryness, chapping and redness. Penetrates the skin readily. Toxic
I Iand may be harmful if absorbed through the skin.
LATION
Repeated and prolonged overexposure by inhalation may cause respiratory tract irritation. Symptoms may include central
nervous system disorders such as headaches, dizziness, weakness and fatigue.
[ STION
Ingestion may cause gastrointestinal tract irritation. Symptoms may Include headaches, nausea and vomiting. Contains
material that may be moderately toxic if ingested.
�NIC EFFECTS/TARGET ORGANS
Reports have associated repeated and prolonged vccupa'tivhul overexposure to solvents with permanent brain and nervous system
damage. Intentional misuse by deliberately concentrating and inhaling the contents may be harmful or fatal,
AL STUDIES
2-eutoxyethanol has caused reproductive and blood disorders resulting in kidney, liver and lung damage In lab animals. Butyl
benzyl phthalate produced limited evidence of damage to the liver. kidney and male reproductive system and harm to the fetus
In lab anirmals after overexposure- The relevance of -these findings to humans is uncertain. 2•Butoxyethanol acetate has
'caused reproductive and blood disorders resulting in kidney, liver and lung damage in lab animals. For animal studies,
reference TSCA Section 4 Test Rule Result$ or contact the manufacturer for further details.
iEDICAL CONDITIONS AGGRAVATED BY EXPOSURE
Pregnant women and parsons with pre-existing health disorders should consult their physician before using this product.
Repeated and prolonged overexposure and/or individual sensitivity may increase the potential for and degree of adverse health
effects. See Section 3 -Hazards Identification" for effects of certain hazardous ingredients.
tQv — s OF EXP05URE
imary exposure routes: Inhalation -Dermal (Contact/Absorption)•Ingestion
1 ........... ...I ....
......... I...........
SECTIO4 -- FIRST AID MEASURES ..............,.........
........................... ..................•-----•------------------------------------------------I......I.....--• ..............
1

70 AN ONY S833NIDN3 NI11VO-A1 -mojj wqo: 60 01-60-BnV PAM AOAN
DUCT r=ODE: 97NL NAZDAR SHAWNEE PAGE: 3 OF 6
EYES
f
...............••................
..------.......-----------. ...............
•--------------- . - -------••-----------..-
�fter initial flushing, remove any contact lenses and continue flushing for at least 15 minutes, If irritation persists have
,/es examined and tested by medical personnel.
SKIN
In case of contact, Immediately wash skin with a mild soap and plenty of water for at least 15 minutes. while removing
contaminated clothing and shoes. Coal water is initially suggested to prevent the pores of the skin from opening. This will
minimize both the area and time of skin contact. Lukewarm water may then be used to ensure all contaminants are removed.
Skin should be monitored for reddening or chemical burns. Mild soap is suggested to help prevent abrading the skin or rubbing
the chemicals into pares during cleansing. Get medical attention if irritation persists or significant contact has occurred.
Thoroughly wash (or discard) clothing and shoes before reuse.
HALATION
Remove to fresh air. If not breathing, give artificial respiration or give oxygen by trained personnel
medical attention 'if breathing difficulty is experienced.
)�ESTION
If swallowed.
an unconscious
Seek immediate
do NOT induce vomiting. Call a physician or poison control center immediately. Never give anything by mouth to
person.
rR COMMENTS
No Data Availabla
ME. •--.. .....-•----•---•----•.................................
SECTION S -• FIRE FIGHTING MEASURES
F H POINT ----------------------------
........--------------.......------------------------------------------
.......
....................
143 Degrees - 145 Degrees Fahrenheit (PMCC)
0[ FLAMMABILITY CLASSIFICATION (NFPA)
Class IIIA Combustible Liquid
LEL - LOWER EXPLOSIVE LIMIT / UEL - UPPER EXPLOSIVE LIMIT
Elr1. 1X volume in air / No Data Available
UISHING MEDIA
aam-CO2-Dry Chemical -Water Spray
F1AND EXPLOSION HAZARDS
Isolate from heat, electrical c-quipment, sparks. and oPrn flame. Keep containers tightly closed- Vapors may be heavier than
air and can travel to a source of ignition then flash back. Closed containers may explode when exposed to extreme heat,
F FIGHTING EQUIPMENT
Full protective equipment including self-contained breathing apparatus (SCBA) is recommended to protect firefighters.
S IAL FIRE FIGHTING PROCEDURES
Water may be ineffective but may be used to cool containers. Fumes released on burning may be toxic and dangerous.
SECTION........................S..MEASURES--------------......,................... I-----------.._.-. ---
RELEASE MANAGEMENT MEASURES
Remove all sources of ignition (flames, hot surfaces and electrical, static or frictional sparks). Avoid contact or breathing
vapors. Ventilate area. Contain release and remove with inert absorbent. Use non -sparking tools to place material in
appropriate container for disposal. Isolate the hazard area and deny entry to unnecessary and unprotected personnel. The
National Response Center (800-424-8802) and local authorities should be contacted for any reportable spill/release.
........................SECTION.... ...HAND.... AND STORAGE .. ............
-HOLING AND STORAGE METHODS
Use in a well ventilated area. Follow all MSDS/label precautions even after container is emptied; container may retain
product residues. Store in closed containers in cool. dry, well ventilated area away 'Prom sources of ignition. Keep
containers closed when not in use. Smoke in designated areas only. Avoid prolonged or repeated overexposure to this product.
Keep out of reach of children. Follow label directions carefully. Do not take internally. Harmful or fatal if swallowed.
--•----------- .......... ............ .--------------------------------------- ............. ...........................
SECTION 8 __ EXPOSURE CONTROLS, PERSONAL PROTECTION
lF"- TORY PROTECTION
concentrations of hazardous ingredients exceed exposure limits listed in Section 2 an appropriate NIOSH (National Institute
for Occupational Safety and Health) approved respirator with an organic vapor cartridge should be used, If material is
handled under mist. spray or dust 'Forming conditions. a P100 (99.97% efficiency) filter should be used in addition to the
organic vapor cartridge. Protection provided by air -purifying respirators is limited_ If no exposure limits are listed in
Section 2, follow general safety guidelines in 29 CFR 1910.134 Respiratory Protection or other applicable respiratory
1

90 Aced W S833NION3 NI11Y3-e1 -woad weea:60 01-60-DnV pAAtnnq
1
ODUCT CODE: 97NL NAZDAR SHAWNEE PAGE: 4 OF 5
standard, ............. .... ------
PROTECTION
Use neoprene, nitrile or other gloves resistant to chemicals listed in Section 2. Contact a reputable safety supply company
for appropriate gloves. Solvent resistant aprons arfi recommended. Prevent prolonged skin contact with contaminated clothing.
PROTECTTON
Use ANSI (American National Standards Institute) approved safety glasses, faceshield or splashroof goggles to prevent eye
contact. Contact a reputable safety supply company for appropriate eye protection. The availability of an aye wash is highly
recommended.
�OSURE GUIDELINES
See Section 2 -Composition. Information on Ingredients" for occupational exposure 'iimits. Excessive concentrations of
nuisance dusts or particulates not otherwise classified (PNOC) or regulated (PNOR) may reduce visibility dnd cause unpleasant
deposits in the eyes, ears, and nasal passages. The TLV and PEL has been established for all non -toxic "nuisance dusts- that
are not otherwise classified and refers to both organic and inorganic dusts. Exposure or generation of these dusts is not
anticipated during normal printing operations. The use of dry pigments and powders, grinding or sanding of printed products
may generate quantities of these particulates. Refer to Section 2 Composition, Information on Ingredients for exposure
limits.
�IENIC PRACTICES
Wash with soap and water before eating, smoking or using toilet facilities. Separately wash or discard clothing and footwear
before reuse. NEVER try to remove product from the skin by using solvent or thinner. Such action is likely to increase the
possibility of undesirable effects. Remove contaminated clothing to prevent prolonged skin contact.
INEERING CONTROLS
Use applicable engineering controls. work practices and personal protective equipment to ensure all concentrations are kept
below the exposure limits listed in Section Z. Adequate controls should be implemented to ensure employee safety from fine
mists which may he produc3d under some printing conditions.
�ER PROTECTION
No Data Available
.SECTION 9 -- PHYSICAL AND CHEMICAL PROPERTIES
`............................................................................. ........................... ...............
q� ( ARANCE :
® viscous liquid
ODOR
Characteristic
P'SI CAL STATE : '
Liquid
Not applicable
V R PRESSURE
See Section 2 for individual ingredients.
vR DENSITY
�
Heavier than air
80 LING POINT
Greater than 300 degrees Fahrenheit
F ING POINT
Not available
SlILITY IN WATER
Not tested
EVAPORATION RATE
rOlawor than ether
SITY
-.-'reater than water
RJENT VOLATILE 8Y VOLUME: SEE SECTION ONE
d HT PER GALLON: SEE SECTION ONE
1

% 30 aced CNV SMNIM N1100-0i
I
-woij ulnwaa 01-60-9mv psnlaaea
RODUCT CODE: 97NL NAZOAR SHAWNEE
0c; SEE
OCHEMICALLY REACTIVE
No
Percent volatile = Percent VOC
PAGE: 5 OF
I ..........................
SECTION 10 -- STABILITY AND REACTIVITY
-------------------------------- ............ ------------------------------------------ .................... ....... I.— ......... ................................................ — ----------- ------------------------------------------
CHEMICAL STABILITY
5table
NDITIONS TO AVOID
Avoid excessive hat. ignition sources, sparks and open flame.
COMPATIBILITY WITH OTHER MATERIALS
Strong acids/bases, oxidizing/reducing agents and reactive chemicals.
HAZARDOUS DECOMPOSITION PRODUCTS
May produce hazardous fumes when heated to decomposition e.g. carbon knomoxide, carbon dioxide and other noxious gases.
ARDOUS POLYMERIZATION
Not anticipated during normal printing and storage conditions.
........................... ................................ I ------------ .......................... .............
-- TOXICOLOGICAL
�---------------I..........SECTION.-11......
................. I .INFOWATIO4..... ­ ....... ............ ......................................
EXPERIMENTAL TOXICITY DATA
Refer to Section 3 Hazards Identification for additional toxicological data. Experimental toxicity data on 2-butoxyethamol
has given the following results: Oral LDSO Rat; 1746 mg/kg: Intraperitone4l LD50 Rat; 55D mg/kg. Experimental toxicity data
an 2-butoxyethanal acetate has given the following results: Oral L050 Rat: 2400 mg/kg: Dermal L050 Rabbit; 1500 mg/kg.
........................ .......... I ........•
............................... ------------------
SECTION 12 -- ECOLOGICAL INFORMATION
JX-I,G-I,T,Y --­------------------------- * ............................
Because this product may be 4 mixture of chemirals, some of which may be ecologically toxic, it is strongly suggested that -it
not be disposed of into the anviroment, i.e. soil. water courses. lakes, landfills, sewers. etc.
IRONMENTAL FATE
No Data Available
­-------------- .......................... .................. ......................... ...............................
SECTION 13 -- DISPOSAL CONSIDERATIONS
.................................. I ............................................................ ..................
DISPOSAL METHODS
This product, as supplied, is considared non-lazerdous, for disposal purposes by the U.S. Environmental Protection Agency
Resource Conservation and Recovery Act (RCRA). If combined with other products, the user should determine if hazardous waste
codes are re-quired. It is the responsibility of the user to determine if local, county, state, or provincial regulations "lay
also apply to the disposal of this product and/or the container.
........................... ......................... ......... I ............................................. ......... I -------
SECTION 14 -- TRANSPORT INFORMATION
ISPORT-INFORMIATION, ......................... I ------------­------ I ----------------- ­­ ............................ -------------
Not regulated. The product(s) described by this Material Safety Data Sheet do not meet the definition of nor are they
classified as a hazardous material/dangerous good as defined by the United States Department of Transportation (DOT), the
International Civil Aviation arganization (ICAO), the international Maritime Organization (IMO) or the Canadian Transportation
of Dangerous Goods Act (TI10), Questions concerning transportation requirements should be directed to Nazddr's Regulatory
Compliance Department 913-422-1735.
............................................. ................................. ................................. -------------­--
SECTIONREGULATORY INFORMATION
....................................................................... ­­ ............ ­ ..................... -----------
SARA TITLE 111 313 INFORMATION
J3 See Section 2 'Composition. Information on Ingredients" for applicable chemicals.
C SUBSTANCES CONTROL ACT STATUS
, 11 ingredients in section 2 are 'listed an the U.S. Environmental Protection Agency's Toxic 5ubstances Control Act (TSCA)
.nventory and the Canadian Domestic Substance List-
11R REGULATORY INFORMATION
OCCUPATIONAL SAFETY and HEALTH ADMINISTRATION (OSHA) - MSDS is compliant with Occupational Safety and Health Administration
Hazard Communication Standard - 29 CFR 1910,1200. AMERICAN NATIONAL STANDARDS INSTITUTE - This MSOS follows the ANSI
1

10 geed QNV SUB IDN3 Nlliv:-ol -moat we90:aD 01-60-eny panla�aN
ODUCV COCE: 97NL NAZOAR SRAWNEE PAGE: 6 OF 6
Z4U0.I-t998 ramdt. I140RULKE HAZARDOUS MATERIAL INFORMATION SYSTEM (UHM S) - This product has been classified in accordance,.
0th the hazard criteria of the Controlled Products Regulations (CPR) and the MSDS contains all the information required by
the CPR.
WHI415 CLASSIFICATION (CANADA):
83 Combustible Liquids; 01A Material causing immediate and serious toxic effects, very toxic material; D28 _ Materials
causing other toxic effects. toxic material:
SECTION L6 OTHER [NFORNATiON
�SCLOSORE
The information and recommendations contained herein are based upon data believed to be correct. However, no guarantee or
warranty of any kind express or implied is made with respect to the information contained herein. The data in this MSDS
relates only to the specific material designated herein and does not apply to use in combination with any other material or
process.
DEFINITIONS
ACGIH: American Conference of Governmental Industrial Hygienists
AIHA: American Industrial Hygiene Association
CEILING: (TLV-Ceiling and PEL Ceiling Limit) The ceiling exposure limit or concentration not to be exceeded for even brief
times.
DOT: Department of Transportation
HMIS: The Hazardous Materials Identification System (HHiS) developed by the National Paint and Coatings Association (NPCA) to
provide information on the acute health hazards, reactivity and flammability of products encountered in the workplace at room
temperatures.
HMIS codes assigned for this product are only suggested ratings based on anticipated normal screen printing applications. The
,,employer has the ultimate responsibility for assigning these ratings and should fully evaluate the MSDS. Mork practices and
environmental conditions prior to assigning the appropriate ratings.
.1MIS rating involves data interpretations that may vary from ecynpdny to company.
HMES Personal Protection Index of 'X-Ask your supervisor` is given an this HSDS due to varying work conditions which may
dictate different levels of protection. Please review this MSDS before determining appropriate protective equipment and
beginning work.
IARC: International Agency for Research on Cancer
NFPA. National Fire Protection Association
NTP: National Toxicology Program
ST1L: Short -Term Exposure Limit: ACGIH terrminology for the short-term exposure limit or maximum concentration for a continuous
exposure period of 15 minutes.
TLV: 'rhreshold Limit Value, A term ACGIH uses to express the airborne concentration of a material to which most workers can
'be exposed during a normal daily and weekly work schedule without adverse effects.
TWA: Time -Weighted Average
VOC: Volatile Organic Compound
1

m ® © ® ® = = = ® ® ® ® m m m m S

1
APPENDIX B
LABORATORY REPORTS
I
k�
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Chloride; 200016 discharge notif.doc CATLIN Engineers and Scientists
CATLIN Project No. 200016.17September 2010
I

SGS North America, Inc.
Pom Landis
Richard Catlin & Associates
P.O. Box 10279
Wilmington, NC 2.8404-0279
I
0
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1
Report Number- G128-2579
Client Project: Chloride Pond
Dear Tom Landis,
0�3 lie/0
'J 14 P V 67
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable, The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. Any samples
submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Barbara Hager at
[phone], We will be happy to answer any questions or concerns which you may have,
Thank you for using SGS North America, Inc, for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America, Inc.
Z_ --- Id
Project Manager Date
Barbara Hager
SGS Ncrih America Inc. Environmental Division 550D Business Dr., Wlialington, NC 28405 t t910135D•1903 f 19101350-1557 www,us.sgs.com
Mamoor al the SGS Group
N.C. Certification 9481 Page 1 of 7

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SGS North America, Inc.
List of Reporting Abbreviations
And Data Qualifiers
13 = Compound also detected in batch blank
13QL = Below Quantification Limit (RL or MDL)
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = L-stimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL/CL = Reporting Limit / Control Limit
RPD = Relative Percent Difference
UJ = Target analytes with recoveries that are 10% < %R < LCL; /I of MEs are allowable
and compounds are not detected in the sample.
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block; see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
N.C. Certification 4481
M134.021808.4
Page 2 of 7

SGS North America,
Inc.
'
Results for Volatiles
by GCMS 8260
Client Sample ID: SW-3 Chloride Pond
Analyzed By.
DVO
Client Project ID: Chloride Pond
Date Collected: 8/23/2010 15:30
Lab Sample ID: G128-2579-18
Date Received: 8/24/2010
Lab Project ID: G128-2579
Matrix: Water
Sample Amount. 5 mL
Result
Quantitation
MDL
Dilution
Date
1
Compound
UGIL
Limit UGIL
UGIL
Factor
Analyzed
Acetone
495 100
8.72
4
8/25/2010
Benzene
Bromobenzene
BQL
BQL
1.00
1.00
0.0650
0.0560
1
1
8125/2010
8/25/2010
Bromochicromethane
BQL
1.00
0.101
1
8/25/2010
Bromodichloromethane
BQL
1.00
0.0760
1
8125/2010
8romoform
BQL
1.00
0.120
1
8/25/2010
Bromomethane
BQL
1.00
0.133
1
812512010
2-Butanone
BQL
25.0
0.544
1
8/25/2010
n-Butylbenzene
BQL
1.00
0.109
1
8/25/2010
sec -Butyl benzene
BQL
1.00
0.0840
1
8/2512010
tert-Butylbenzene
8QL
1.00
0.0500
1
8/25/2010
Carbon disulfide
BQL
1.00
0.0690
1
8/25/2010
1
Carbon tetrachloride
BQL
1.00
0.0870
1
8/2512010
Chlorobenzene
BQL
1.00
0.0820
1
8/25/2010
Chloroethane
BQL
1.00
0,106
1
8/25/2010
8QL
1.00
0.0790
1
8/25/2010
'Chloroform
Chloromethane
BQL
1.00
0.146
1
8/2512010
2-Chlorotolueno
SOL
1.00
0,0990
1
8/25/2010
4-Chlorotoluene
BQL
1.00
0.0800
1
8/25/2010
Dibromochloromethane
BQL
1.00
0.0900
1
8125/2010
1,2-Dibromo-3-chloropropane
BQL
5.00
1.21
1
8/25/2010
Dibromomethane
SQL
1.00
0.113
1
8/25/2010
1,2-Dibromoethane (EDB)
BQL
1.00
0.124
1
8/25/2010
1,2-Dichlorobenzene
BQL
1.00
0.127
1
8/25/2010
1,3-Dichlorobenzene
BQL
1.00
0.0810
1
8/2512010
1,4-Dichlorobenzene
BQL
1.00
0.0790
1
8/25/2010
trans-l.4-Dichloro-2-butene
8QL
5.00
0.630
1
8/25/2010
1,1-Dichloroethene
BQL
1.00
0.0740
1
812512010
1,1-Dichloroethene
BQL
1.00
0.0890
1
8/25/2010
1,2-Dichloroethane
BQL
1.00
0.0790
1
8/2512010
cis- 1,2-Dichloroethene
BQL
1.00
0.0650
1
8/25/2010
trans-1,2-dichloroethene
BQL
1.00
0.0890
1
8/2512010
1,2-Dichloropropane
8QL
1.00
0.0940
1
8/25/2010
1,3-Dichloropropane
BQL
1.00
0.127
1
8/25/2010
2,2-Dichlorapropane
BQL.
1.00
0.0590
1
8/25/2010
1,1-Dichloropropene
BQL
1.00
0.0720
1
8/25/2010
cis- 1.3-Di ch loropropene
BQL
1.00
0.0760
1
8/25/2010
trans-1,3-Dichloropropene
BQL
1.00
0.0760
1
8/2512010
Dichlorodifluoromethane
BQL
5.00
0.0940
1
8/25/2010
Diisopropyl ether (RIPE)
BQL
1.00
0.0730
1
8/25/2010
Ethylbenzene
BQL
1.00
0.0770
1
8/25/2010
Hexachlorobutadiene
BQL
1.00
0.228
1
8/25/2010
2-Hexanone
BQL
5.00
0.720
1
8125/2010
lodomethane
BQL
1.00
0.0420
1
8/25/2010
lsopropylbenzene
BQL
1.00
0,0710
1
8/25/2010
Page 1 of 2
N.C. Certification #481
Page 3 of 7
Flag
GCMS
MO

SGS North America, Inc.
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Results for Voiatiles
by GCMS 8260
Client Sample ID: SW-3 Chloride Fond Analyzed By: DVO
Client Project ID: Chloride Pond Date Collected: 8/23/2010 15,30
Lab Sample ID: G128-2579-18 Date Received: 8/24/2010
Lab Project ID: G128-2579 Matrix: Water
Sample Amount 5 mL
Result
Quantitation
MDL
Dilution
Date
Compound
UG/L
Limit UGIL
UG1L
Factor
Analyzed
Flag
4-Isopropyltoluene
0.540
1.00
0.0480
1
8/25/2010
J
Methylene chloride
BQL
5.00
0.0980
1
8/25/2010
4-Methyl-2-pentanone
BQL
5.00
0.550
1
8/25/2010
Methyl-tert-butyl ether (MTBE)
BQL
1.00
0.0670
1
8/25/2010
Naphthalene
BQL
1.00
0.133
1
8/25/2010
n-Propyl benzene
BQL
1.00
0.0800
1
8/25/2010
Styrene
BQL
1.00
0.0850
1
8/2512010
1,1,1,2-Tetrachloroethane
BQL
1.00
0.0900
1
8/2512010
1,1,2,2-Tetrachloroethane
BQL
1.00
0,115
1
8/25/2010
Tetrachloroethene
BQL
1,00
0.0690
1
8/25/2010
Toluene
BQL
1.00
0.0760
1
8/25/2010
1,2.3-Trichlorobenzene
BQL
1.00
0.190
1
8/25/2010
1,2,4-Trichlorobenzene
8QL
1.00
0.119
1
8/25/2010
Trichloroethane
BQL
1.00
0.0540
1
8125/2010
1,1,1-Trichloroethane
BQL
1.00
0,0540
1
8/25/2010
1,1,2-Trichloroethane
BQL
1.00
0.182
1
8/2512010
Trichlorofluoromethane
BQL
1.00
0,111
1
8/25/2010
1,2,3-Trichloropropane
BQL
1.00
0.120
1
8125/2010
1,2,4-Trimethylbenzene
0.460
1.00
0.0650
1
8125/2010
J
1,3,5-Trimethylbenzene
13.7
1.00
0.0740
1
8/25/2010
Vinyl chloride
BQL
1,00
0.149
1
8/2512010
m-,p-Xylene
BQL
2.00
0.0980
1
8/25/2010
o-Xylene
0.300
1.00
0.0650
1
8/25/2010
J
Spike
Spike
Percent
Added
Result
Recovered
1,2-Dichloroethane-d4
30
29.1
97
Toluene-d8
30
30
100
4-Bromofluorobenzene
30
30.3
101
' Comments:
Flags:
BQL =Below QuLLantitativn Limits.
Analyst: 6�/
1
Reviewed By: CC
Pago 2 of 2 c$ so
N.C. Certificalion #481 Page 4 of 7

1 SGS North America, Inc.
Results for Volatiles
by GCMS 8260
Client Sample ID: Trip Blanks (Not on COC) Analyzed By: DVO
1 Client Project ID: Chloride Pond Date Collected: 1/011900 0:00
Lab Sample ID: G128-2579-2A Date Received: 8/24/2010
Lab Project ID: G128-2579 Matrix: Water
Sample Amount: 5 mL
Compound
Result
UGIL
Quantitation
Limit UGIL
MDL
UGIL
Dilution
Factor
Date
Analyzed
Acetone
BQL
25.0
2.18
1
8/25/2010
Benzene
BQL
1.00
0.0650
1
8125/2010
Bromobenzene
BQL
1.00
0.0560
1
8/25/2010
Bromochloromethane
BQL
1.00
0.101
1
8/25/2010
Bromodichloromethane
BQL
1.00
0.0760
1
8/25/2010
Bromoform
BQL
1.00
0.120
1
8/2512010
Bromomethane
BQL
1.00
0.133
1
8125/2010
2-Butanone
BQL
25.0
0,544
1
8125/2010
n-Butylbenzene
BQL
1.00
0,109
1
8/25/2010
sec-Butylbenzene
BQL
1.00
0.0840
1
8125/2010
tert-Butylbenzene
BQL
1.00
0.0500
1
8/25/2010
Carbon disulfide
BQL
1.00
0.0690
1
8/25/2010
Carbon tetrachloride
BQL
1.00
0.0870
1
8/25/2010
Chlorobenzene
BQL
1.00
0.0820
1
8/25/2010
Chloroethane
BQL
1.00
0.106
1
8/25/2010
BQL
1.00
0.0790
1
8/25/2010
'Chloroform
Chloromethane
BQL
1.00
0.146
1
8/25/2010
2-Chlorotoluene
BQL
1.00
0.0990
1
8/25/2010
4-Chlorotoluene
BQL
1.00
0.0800
1
8/25/2010
Dibromochloromethane
BQL
1.00
0.0900
1
8/25/2010
1,2-Dibromo-3-chloropropane
BQL
5.00
1.21
1
8/25/2010
Dibromomethane
BQL
1.00
0,113
1
8/2512010
1,2-Dibromoethane (EDS)
1,2-Dichlorobenzene
BQL
BQL
1.00
1.00
0.124
0.127
1
1
8/25/2010
8/25/2010
1,3-Dichlorobenzene
BQL
1.00
0,0810
1
8/25/2010
1,4-Dichlorobenzene
BQL
1.00
0.0790
1
8/25/2010
trans-1,4-Dichloro-2-butene
BQL
5.00
0.630
1
6/2512010
1,1-01chloroethane
BQL
1.00
0.0740
1
8125/2010
1,1-Dichloroethene
BQL
1.00
0.0890
1
8/25/2010
1,2-Dichloroethane
BQL
1.00
0.0790
1
8/25/2010
cis-1,2-Dichloroethene
BQL
1.00
0.0650
1
8/25/2010
trans- 12-dichloroethene
BQL
1.00
0.0890
1
8/25/2010
1,2-Dichloropropane
BQL
1.00
0.0940
1
8/25/2010
1,3-Dichloropropane
BQL
1.00
0.127
1
8/25/2010
2,2-Dichloropropane
BQL
1.00
0.0590
1
8/25/2010
1,1-Dichloropropene
BQL
1.00
0.0720
1
8/25/2010
cis- 1,3-Dichloropropene
BQL
1.00
0.0760
1
8/25/2010
trans-1,3-0lchloropropene
BQL
1.00
0.0760
1
8125/2010
Dichlorodifluoromethane
BQL
5.00
0.0940
1
8/25/2010
Diisopropyl ether (DIPE)
BQL
1.00
0.0730
1
8/25/2010
Ethylbenzene
BQL
1.00
0.0770
1
8/25/2010
Hexachlorobutadiene
BQL
1.00
0.226
1
8/25/2010
2-Hexanone
BQL
5.00
0,720
1
8125/2010
lodomethane
BQL
1.00
0.0420
1
8/25/2010
Isopropylbenzene
BQL
1.00
0.0710
1
8/25/2010
Page 1 of 2
N.C. Certification #481
Page 5 of 7
Flag
GCMS
0200

'
SGS North America, Inc.
Results for Volatiles
by GCMS 8260
Client Sample ID: Trip Blanks (Not on COG)
Analyzed By: DVO
Client Project ID: Chloride Pond
Date Collected: 1/0/1900
0:00
Lab Sample ID: G128-2579-2A
Date Received: 8/24/2010
Lab Project ID: G128-2579
Matrix: Water
1
Sample Amount: 5
mL
Result
Quantltatlon
MOL
Dilution
Date
1
Compound
UG/L
Limit UGIL
UGIL
Factor
Analyzed
4-lsopropyltoluene
BQL
1.00
0.0480
1
8125/2010
Methylene chloride
4-Methyl-2-pentanone
0.860 5.00
BQL 5.00
0.0980
0.550
1
1
8/25/2010
8125/2010
Methyl -tort -butyl ether (MTBE)
BQL
1.00
0.0670
1
8/25/2010
Naphthalene
BQL
1.00
0.133
1
8/25/2010
n-Propyl benzene
BQL
1.00
0.0800
1
8/25/2010
Styrene
BQL
1.00
0.0850
1
8125/2010
1,1,1,2-Tetrachloroethane
BQL
1.00
0,0900
1
8/25/2010
1,1,2,2-Tetrachloroethane
BQL
1.00
0.115
1
8/25/2010
Tetrachloroethene
BOL
1.00
0,0690
1
8/2512010
Toluene
BQL
1.00
0.0760
1
8/25/2010
1,2,3-Trichlorobenzene
BQL
1.00
0.190
1
8/25/2010
1,2,4-Trichlorobenzene
BQL
1.00
0.119
1
8/25/2010
Trichloroethene
80L
1.00
0,0540
1
8/25/2010
1. 1,1 -Trichloroethane
BQL
1.00
0.0540
1
8/25/2010
1,1,2-Trichloroethane
BQL
1.00
0.182
1
8/25/2010
Trichlorofluoromethane
BQL
1.00
0.111
1
8/25/2010
1,2,3-Trichloropropane
BQL
1.00
0,120
1
8/2512010
1,2,4-Trimethylbenzene
SQL
1.00
0.0650
1
8/25/2010
1,3,5-Trimethylbenzene
BOL
1.00
0.0740
1
8/25/2010
Vinyl chloride
BQL
1.00
0.149
1
8/25/2010
m-,p-Xylene
BQL
2.00
0.0980
1
8125/2010
o-Xylene
BQL
1.00
0.0650
1
8125/2010
Spike
Spike
Percent
Added
Result
Recovered
1,2-Dichloroethane-d4
30
29.8
99
Toluene-d8
30
30.1
100
4-Bromofluorobenzene
30
30
100
1
Comments:
Flags:
BQL =Below Quantitation Limits.
Analyst: VD
I
Reviewed By: W
Flag
J
GCMS
Page 2 of 2 6260
N.C. Certification M81 Page 6 of 7

V
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CHAIN OF CUSTODY RECORD AiaSka I.Iarr1anc
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INVOICE QUOTE #: �' `
2 Y /,Lzlj P.O. NUMBER: IU O S t —3
LAB NO.
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DATE
TIME
MATRIX
t)
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Date
Time
Rec ed f3y:
Special Detiverahie Requirements-
Chain of Custody Seal: (Circle)
INTACT BROKEN ABSE14T
Relinquished By. (3)
Date
Time
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Special lnsuuciions:
Relinquished By: (4)
Date
Time
Received By:
FRB uesied Tumaro d T e:
fY RUSM
7� Date Nee
CI STD
D 200 W. Potter Dave Anchorage, AK 99518 Tel: [phone] Fax: [phone]
0 5500 Business Drive Wilmington, NC 28405 Tel: [phone] Fax: [phone]
z
0
3
CD
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v
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1'.c:e-FieZ ac cr lzp

SGS North America, Inc.
Jlru �Zilr �l
Tom Landis
Richard Catlin & Associates
P.O. Box 10279
Wilmington, NC 28404-0279
1
1
0
L
I
K
I
Report Numbec G128-2572
Client Project: Chloride Pond
Dear Tom Landis,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. Any samples
submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Barbara Hager at
[phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America, Inc. for your analytical services. We took forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America, Inc.
Project Manager
Barbara Hager
Date
, '2Q 10
5G5 North Amenca Inc. Environmental Division 5500 Business Dr„ Wilmington, NC 28405 t [phone] t [phone] www.us.sgs,cum
M4mbv of the SGS Gra99
N.C. Certification #481 Page 1 of 5

0
0
s
SGS North America, Inc.
List of Reporting Abbreviations
A nd Data Qua] i f iers
B = Compound also detected in batch blank
BQL = Below Quantification Limit (RL or MDL)
DF = Dilution factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL/CL = Reporting Limit / Control Limit
RPD = Relative Percent Difference
UJ = Target analytes with recoveries that are 10% < %R < LCL; 4 of Mrs are allowable
and compounds are not detected in the sample.
mg/kg = milligram per kilogram, ppm, parts per million
uglkg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Ree = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples arc digested with a hot block; see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
N.C. Certification 4481
M134.021808.4
Page 2 of 5

SGS North America, Inc.
N
I
1
1
1
I
0
Results for Volatiies
by GCMS 8260
Client Sample ID: SW-1 Analyzed By: DVO
Client Project 1D: Chloride Por.d Date Collected: 8/10/2010 15:15
Lab Sample ID: G128-2572-1 B Date Received: 8/1 1/2010
Lab Project ID: G128-2572 Matrix: Water
Sample Amount: 5 mL
Result
Quantitation
MDL
Dilution
Date
Compound
UGIL
Limit UGIL
UG/L
Factor
Analyzed
Acetone
5550
1250
109
50
8/13/2010
Benzene
BQL
1.00
0.0650
1
8/13/2010
Bromobenzene
BQL
1.00
0.0560
1
8/13/2010
Bromochloromethane
SOL
1.00
0.101
1
8/13/2010
Bromodichloromethane
BQL
1.00
0.0760
1
8/1312010
Bromoform
BQL
1,00
0.120
1
8/13/2010
Bromomethane
BQL
1.00
0.133
1
8/13/2010
2-Butanone
4.19
25.0
0.544
1
8/13/2010
n-Butylbenzene
BQL
1.00
0.109
1
8/13/2010
sec-Butylbenzene
18.8
1.00
0.0840
1
8/13/2010
tert-Butylbenzene
BQL
1.00
0.0500
1
8/13/2010
Carbon disuifide
BQL
1.00
0.0690
1
8/13/2010
Carbon tetrachloride
BQL
1,00
0.0870
1
8/13/2010
Chlorobenzene
BQL
1.00
0.0820
1
8/13/2010
Chloroethane
BQL
1.00
0,106
1
8/13/2010
Chloroform
BQL
1.00
0.0790
1
8/13/2010
Chloromethane
BQL
1.00
0.146
1
8/13/2010
2-Chlorotoluene
BQL
1.00
0,0990
1
8/13/2010
4-Chlorotoluene
BQL
1.00
0,0800
1
8/13/2010
Dibromochloromethane
BQL
1.00
0.0900
1
8/13/2010
1,2-Dibromo-3-chloropropane
BQL
5.00
1,21
1
8/13/2010
Dibromomethane
BQL
1.00
0.113
1
8/13/2010
1,2-Dibromoethane (EDB)
BQL
1.00
0.124
1
8/13/2010
1,2-Dichlorobenzene
BQL
1.00
0.127
1
8/13/2010
1,3-Dichlorobenzene
BQL
1.00
0,0810
1
8/13/2010
1,4-Dichlorobenzene
BQL
1.00
0.0790
1
8/13/2010
trans-1,4-Dichloro-2-butene
BQL
5.00
0.630
1
8/13/2010
1,1-Dichloroethane
BQL
1,00
0.0740
1
8/13/2010
1,1-Dichloroethene
BQL
1.00
0.0890
1
8/13/2010
1,2-Dichloroethane
BQL
1.00
0,0790
1
8/13/2010
cis- 1,2-Dichloroethene
BQL
1.00
0.0650
1
8/13/2010
trans-1,2-dichloroethene
BQL
1.00
0,0890
1
8/13/2010
1,2-Dichloropropane
BQL
1.00
0.0940
1
8/13/2010
1,3-Dichloropropane
BQL
1.00
0.127
1
8/13/2010
2,2-Dichloropropane
BQL
1.00
0.0590
1
8/13/2010
1,1-Dichloropropene
BQL
1.00
0.0720
1
8/13/2010
cis-1,3-Dichloropropene
BQL
1.00
0.0760
1
8/13/2010
trans- 1,3-Dichloropropene
BQL
1,00
0.0760
1
8/13/2010
Dichlorodifluoromethane
BQL
5.00
0.0940
1
8/13/2010
Diisopropyl ether (D)PE)
BQL
1.00
0.0730
1
8/13/2010
Ethylbenzene
0.590
1.00
0.0770
1
8113/2010
Hexachlorobutadiene
BQL
1.00
0,228
1
8/13/2010
2-Hexanone
BQL
5.00
0.720
1
8/13/2010
lodomethane
BQL
1.00
0.0420
1
8/13/2010
lsopropylbenzene
46.9
1.00
0,0710
1
8/13/2010
Flag
J
J
CCMs,Kis
Page 1 of 2 0200
N.C. Certification #481 Page 3 of 5

'
SGS North America, Inc.
1
Results
for Volatiles
by GCMS 0260
Client Sample ID: SW-1
Analyzed By: DVO
Client Project ID: Chloride Pond
Date Collected: 8/10/2010 15:15
Lab Sample ID: G128-2572-1B
Date Received: 8/11/2010
Lab Project 1D: G128-2572
Matrix: Water
Sample Amount: 5 mL
Compound
Result
UG1L
Quantitation
Limit UGIL
MDL
UGIL
Dilution
Factor
Date
Analyzed Flag
4-Isopropyitoluene
44.1
1.00
0.0480
1
8/13/2010
Methylene chloride
BQL
5.00
0.0980
1
8113/2010
4-Methyl-2-pentanone
4.01
5.00
0.550
1
8/13/2010 J
Methyl-tert-butyl ether (MTBE)
BQL
1.00
0.0670
1
8/13/2010
Naphthalene
2.66
1.00
0,133
1
8/13/2010
n-Propyl benzene
206
50.0
4.00
50
8/13/2010
Styrene
BQL
1.00
0.0850
1
8/13/2010
1. 1, 1,2-Tetrachloroethane
BQL
1.00
0,0900
1
8/13/2010
1,1,2.2-Tetrachloroethane
BQL
1.00
0.115
1
8/13/2010
Tetrachloroethene
BQL
1.OD
0.0690
1
8/13/2010
Toluene
10.8
1.00
0,0760
1
811312D10
1,2,3-Trichlorobenzene
BQL
1.00
0.190
1
8/13/2010
1,2,4-Trichlorobenzene
BQL
1.00
0.119
1
8113/2010
Trichloroethene
BQL
1.00
0.0540
1
8/13/2010
1, 1, 1 -Trichloroethane
BQL
1.00
0.0540
1
8/13/2010
1,1,2-Trichloroethane
BQL
1.00
0,182
1
8/13/2010
Trichlorofluoromethane
BQL
1.00
0.111
1
8/13/2010
1,2,3-Trichloropropane
BQL
1.00
0.120
1
8/13/2010
1,2,4-Trimethylbenzene
2040
50.0
3.25
50
8/13/2010
1,3,5-Trimethylbenzene
559
50.0
3.70
50
8/13/2010
Vinyl chloride
BQL
1.00
0.149
1
8/13/2010
m-,p-Xylene
6.03
2.00
0,0980
1
8/13/2010
o-Xylene
55.6
1.00
0.0650
1
8/13/2010
1
Spike
Spike
Percent
Added
Result
Recovered
1,2-Dichloroethane-d4
30
30.3
101
Toluene-d8
30
30
100
4-Bromofluorobenzene
30
29.8
100
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Analyst:
Reviewed By:
1
Page 2 cf 2
GCM8280
azeo
N.C. Certification 4481
Page 4 of 5

I&
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www.ussos.com 095674
CLIENT:
SGS Reference;
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LAB NO.
SAMPLE IDENTIFICATION
DATE
TIME
N9AYt31X
1515
?�
3
�0tl5
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TiiimeeReceived
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Shipping Ticket NoT
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TemperaturdC: `7 • 3
RDate
Time
Re ded By:
Special Deliverable Requirements:
Chain of Custody Seak (Circle)
INTACT BROKEN ABSEN
RDate
Time
Received By:
Special Instructions;
RelinquisheBy:
Date
Time
Received By:
Requested Tumaround Time-,
[:]RUSH I STD
Date Needed
O 200 W. Potter Drive Anchorage, AK 99518 Tel: [phone] Fax: [phone]
5500 Business Drive Wilmington, Ne 28405 Tel: [phone] Fax: [phone]
Y,n�:E - Rel2 re', La_
Pick - ne;a�e1 :y C.,en:

SGS North America, Inc
1z'1 goro
Tom Landis
1 Richard Catlin & Associates
P.O. Box 10279
Wilmington, NC 28404-0279
Report Nufnbec G1211-2577
Client Project; Chloride Pond
1 Oear Tom Landis,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
1 Environmental Laboralory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. Any samples
submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Barbara Hager at
[phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America, Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America, Inc.
61 PZAa5- - o
Project Manager e
Barbara Mager 6
1
1
SGS *01 Amtxica Inc Environmental Division 5500 Business Dr , Wilmington, NC 22405 t [phone] f (910) 350-*51 www us-sgs com
fAcmber of the SGS Group
N.C. Certification #481 Page 1 of 7

SGS North America, Inc.
List of Reporting Abbreviations
And Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantification Limit (RL or MDL)
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
F = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitalion Limit
RL/CL = 1Zeporting Limit / Control Limit
RPD = Relative Percent Difference
UJ = 'Fargct analytes with recoveries that are 10% < %R < LCL; # of Ml s are allowable
and compounds are not detected in the sample.
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block; see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
M134.021808.4
N.C. Certification #481 Page 2 of 7

SGS North America, Inc.
0
1
0
1
0
1
1
1
Results for Volatiles
by GCMS 8260
Client Sample ID: SW-1 Resample
Client Project ID: Chloride Pond
Lab Sample 1D: G128-2577-1A
Lab Project ID: G128-2577
Analyzed By: DVO
Date Collected: 8/20/2010 10:50
Date Received: 8/20/2010
Matrix: Water
Sample Amount: 5 mL
Result
Quantitation
MDL
Dilution
Date
Compound
UGIL
Limit UG/L
UG1L
Factor
Analyzed
Acetone
2660
500
43.6
20
8/25/2010
Benzene
BQL
1.00
0.0650
1
8/2512010
Bromobenzene
SOL
1.00
0.0560
1
812512010
Bromochloromethane
BQL
1.00
0.101
1
8/25/2010
Bromodichloromethane
BOL
1.00
0.0760
1
8/25/2010
Bromoform
SOL
1.00
0.120
1
8/25/2010
Bromomethane
SOL
1.00
0.133
1
8/25/2010
2-Butanone
11.1
25.0
0.544
1
8/25/2010
n-Butylbenzene
BOL
1.00
0.109
1
8/25/2010
sec -Butyl benzene
0,840
1.00
0.0840
1
8/25/2010
tert-Butylbenzene
BQL
1.00
0.0500
1
8/25/2010
Carbon disulfide
BQL
1.00
0.0690
1
8/25/2010
Carbon tetrachloride
BQL
1.00
0.0870
1
8/25/2010
Chlorobenzene
SOL
1.00
0.0820
1
8/25/2010
Chloroethane
BQL
1.00
0,106
1
8/25/2010
Chloroform
BOL
1.00
0.0790
1
8/25/2010
Chloromethane
BQL
1.00
0.146
1
8/25/2010
2-Chlorotoluene
BQL
1.00
0.0990
1
8/25/2010
4-Chlorotoluene
BQL
1.00
0.0800
1
8/25/2010
Dibromochloromethane
BQL
1.00
0.0900
1
8/25/2010
1,2-Dibromo-3-chloropropane
BQL
5.00
1.21
1
8125/2010
Dibromomethane
BQL
1.00
0.113
1
8/25/2010
1,2-Dibromoethane (EDB)
BQL
1.00
0,124
1
8/25/2010
1,2-Dichlorobenzene
BQL
1.00
0.127
1
8/25/2010
1,3-Dichlorobenzene
BQL
1.00
0.0810
1
8/25/2010
1,4-Dichlorobenzene
BQL
1.00
0.0790
1
8125/2010
trans-1,4-Dichloro-2-butene
SOL
5.00
0.630
1
8125/2010
1,1-Dichloroethane
SOL
1.00
0.0740
1
8/25/2010
1,1-Dichloroethene
BQL
1.00
0.0890
1
8/25/2010
1,2-Dichloroethane
BQL
1.00
0.0790
1
8/25/2010
cis-1,2-Dichloroethene
BQL
1.00
0.0650
1
8/25/2010
trans-1 ,2-dichloroethene
BQL
1.00
0.0890
1
8/25/2010
1,2-Dichloropropane
BQL
1.00
0,0940
1
8/25/2010
1,3-Dichloropropane
BQL
1.00
0.127
1
8/25/2010
2,2-Dichloropropane
SOL
1.00
0.0590
1
8/25/2010
1,1-Dichloropropene
BQL
1.00
0.0720
1
8/25/2010
cis-1,3-Dichloropropene
BQL
1.00
0.0760
1
8/25/2010
trans-1,3-Dichloropropene
SOL
1.00
0.0760
1
8/25/2010
Dichlorodifluoromelhans
BQL
5.00
0.0940
1
8/25/2010
Diisopropyl ether (DIPS)
BQL
1.00
0.0730
1
8/25/2010
Bthyibenzene
BQL
1.00
0,0770
1
8125/2010
Hexachlorobutadiene
BQL
1.00
0.228
1
8125/2010
2-Hexanone
SOL
5.00
0.720
1
8/25/2010
ladomethane
BQL
1.00
0,0420
1
8/25/2010
Isopropylbenzene
1.09
1.00
0.0710
1
8/2512010
Page 1 or 2
N,C. Certification #481
Page 3 of 7
Flag
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GCMS
8250

SGS North America, Inc.
I
r
1
1
Client Sample ID: SW-1 Resample
Client Project 10: Chloride Fond
Lab Sample 10: G128-2577-1A
Lab Project ID: G128-2577
Compound
4-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone
Methyl-tert-butyl ether (MTBB)
Naphthalene
n-Propyl benzene
Styrene
1,1,1,2-Tetrachloroethane
1.1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichiorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1,1,1-Trichloroelhane
1,1,2-Tric hloroetha ne
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-, p-Xylene
o-Xylene
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
1 Comments:
Flags:
BQL =Below Quantitation Limits.
Analyst• f V
I
Results for Volatiles
by GCMS 8260
Analyzed By: DVO
Date Collected: 8/20/2010 10:50
Date Received: 8/20)2010
Matrix; Water
Sample Amount: 5 mL
Result
Quantitation
MDL
Dilution
Date
UG/L
Limit UG/L
UG1L
Factor
Analyzed
1.64
1.00
0.0480
1
8/25/2010
D.270
5.00
0.0980
1
812512010
4.82
5.00
0.550
1
8/25/2010
BQL
1.00
0.0670
1
8/25/2010
BQL
1.00
0.133
1
8/25/2010
5.05
1 A0
0.0800
1
8125/2010
BQL
1,00
0.0850
1
8/25/2010
BQL
1.00
0.0900
1
8125/2010
BQL
1.00
0.115
1
8/25/2010
BQL
1.00
0.0690
1
8/25/2010
1.33
1.00
0.0760
1
8/25/2010
BQL
1.00
0.190
1
8/2512010
BQL
1.00
0.119
1
8/25/2010
BQL
1.00
0.0540
1
8125/2010
BQL
1.00
0.0540
1
8125/2010
BQL
1.00
0.182
1
8/2512010
BQL
1.00
0,111
1
8/25/2010
BQL
1.00
0.120
1
8/25/2010
39.3
1,00
0.0650
1
8/25/2010
51.2
20.0
1,48
20
8/2512010
BQL
1.00
0.149
1
8/25/2010
BQL
2.00
0.0980
1
8/25/2010
2.32
1.00
0.0650
1
8/25/2010
Spike
Spike
Percent
Added
Result
Recovered
30
30
100
30
30.1
100
30
30.4
101
Reviewed By: W
Flag
J
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Page 2 of 2
N.C. Car ification #481 Page 4 of 7
GCMS
8200

SGS North America, Inc.
I
1
0
1
1
0
1
1
a
1
Results for Volatiles
by GCM5 8260
Client Sample ID: Trip Blank (not on COC) Analyzed By: DVO
Client Project ID: Chloride Pond Date Collected: 6/20/2010 0:00
Lab Sample ID: G128-2577-2A Date Received: 8/20/2010
Lab Project ID: G128-2577 Matrix: Water
Sample Amount: 5 mL
Result
Quantitatlon
MDL
Dilution
Date
Compound
UGIL
Limit UGIL
UGIL
Factor
Analyzed
Acetone
BQL
25.0
2,18
1
8/25/2010
Benzene
BQL
1,00
0.0650
1
8/25/2010
Bromobenzene
BQL
1.00
0.0560
1
8/25/2010
Bromochloromethane
BQL
1.00
0.101
1
8/25/2010
Bromodichloromethane
BQL
1.00
0.0760
1
8125/2010
Bromoform
BQL
1.00
0.120
1
8/25/2010
Bromomethane
BQL
1.00
0.133
1
8/2512010
2-Butanone
BQL
25.0
0.544
1
8/25/2010
n-Butylbenzene
BQL
1.00
0.109
1
8/25/2010
sec-Butylbenzene
BQL
1.00
0.0840
1
8/25/2010
tent-Butylbenzene
BQL
1.00
0.0500
1
8/25/2010
Carbon disulfide
BQL
1,00
0.0690
1
8125/2010
Carbon tetrachloride
BQL
1.00
0.0870
1
8/25/2010
Chlorobenzene
BQL
1,00
0.0820
1
8/25/2010
Chloroethane
BQL
1,00
0,106
1
8/25/2010
Chloroform
BQL
1.00
0,0790
1
B12512010
Chloromethane
BQL
1.00
0,146
1
8/25/2010
2-Chlorotoluene
BQL
1.00
0,0990
1
8/2512010
4-Chlorotoluene
BQL
1.00
0.0800
1
8/25/2010
❑ibromochloromethane
BQL
1.00
0,0900
1
B125/2010
1,2-Dibromo-3-chloropropane
BQL
5.00
1.21
1
B125/2010
Dibromomethane
BQL
1.00
0.113
1
8/25/2010
1,2-Dibromoethane (EDB)
8QL
1.00
0,124
1
8/25/2010
1,2-Dichlorobenzene
BQL
1.00
0.127
1
8/25/2010
1,3-Dichlorobenzene
BQL
1.00
0.0810
1
8/25/2010
1,4-Dichlorobe nzene
BQL
1.00
0,0790
1
8/2512010
trans-1 ,4-Dichloro-2-butene
8QL
5.00
0.630
1
8/25/2010
1,1-Dichloroethane
BQL
1.00
0.0740
1
8/2512010
1,1-Dichloroethene
BQL
1.00
0.0890
1
8/25/2010
1,2-Dichloroethene
BQL
1.00
0.0790
1
8/25/2010
cis- 1,2-Dichloroethene
BQL
1,00
0.0650
1
8/25/2010
trans- l ,2-dichloroethene
BQL
1.00
0.0890
1
8/25/2010
1,2-Dichloropropane
BQL
1.00
0.0940
1
8/25/2010
1,3-Dichloropropane
BQL
1.00
0.127
1
8125/2010
2,2-Dichloropropane
BQL
1.00
0.0590
1
8125/2010
1,1-Dichloropropene
BQL
1.00
0.0720
1
8/25/2010
cis-1,3-Dichloropropene
BQL
1.00
0.0760
1
8/2512010
trans-1,3-Dichloropropene
BQL
1.00
0.0760
1
8/25/2010
Dichlorodifluoromethane
BQL
5.00
0.0940
1
8/25/2010
Diisopropyl ether (DIPE)
BQL
1.00
0.0730
1
8/25/2010
Ethylbenzene
BQL
1.00
0.0770
1
8/25/2010
Hexachlorobutadiene
BQL
1.00
0.228
1
8/25/2010
2-Hexanone
BQL
5.00
0.720
1
8/25/2010
lodomethane
BQL
1.00
0,0420
1
8/25/2010
Isopropylbenzene
BQL
1.00
0.0710
1
8125/2010
Page 1 of 2
N.C. Ceriificafion #4B1
Page 5 of 7
Flag
GCM5
6260

'
SGS North America Inc.
Results for Volatiies
by GCMS 8260
Client Sample ID: Trip Blank (not on COC)
Client Project ID: Chloride Pond
Analyzed By: DVO
Date Collected: 8/2012010 0:00
Lab Sample ID: G128-2577-2A
Date Received: 8/20/2010
Lab Project 1D: G128-2577
Matrix: Water
1
Sample Amount: 5
mL
Result
Quantitation
MDL
Dilution
Cate
Compound
UG/L
Limit UGIL
UGIL
Factor
Analyzed
4-Isopropyltoluene
BQL
1,00
0.0480
1
8/25/2010
Methylene chloride
4-Methyl-2-pentanone
1.01 5.00
8QL 5.00
0.0980
0,550
1
1
8/25/2010
8/25/2010
Methyl -tent -butyl ether (MTBE)
BQL
1,00
0.0670
1
8/25/2010
Naphthalene
BOL
1.00
0.133
1
812512010
n-Propyl benzene
8QL
1.00
0.0800
1
8125/2010
Styrene
BQL
1.00
0.0850
1
8/25/2010
1,1,1,2-Tetrachloroethane
BQL
1.00
0.0900
1
8/25/2010
11,22-Tetrachloroethane
Tetra chloroethe n e
BQL
BQL
1.00
1.00
0,115
0.0690
1
1
8125/2010
8/25/2010
Toluene
BQL
1.00
0.0760
1
8/25/2010
1,2,3-Trichlorobenzene
BQL
1.00
0.190
1
8/25/2010
1,2,4-Trichlorobenzene
8QL
1.00
0,119
1
8/25/2010
Trichloroethene
BQL
1.00
0.0540
1
8/25/2010
1,1,1-Trichloroethane
BQL
1.00
0.0540
1
8/25/2010
1,1,2-Trichloroethane
BQL
1.00
0,182
1
8/2512D10
Trichlorofiuoromethane
BQL
1,00
0.111
1
8/2512010
1,2,3-Trichloropropane
BQL
1.00
0.120
1
8/2512010
12,4-Trime1hylbenzene
BQL
1.00
0.D650
1
8/25/2010
1,3,5-Trimethylbenzene
BQL
1.00
0.0740
1
8/25/2010
Vinyl chloride
BQL
1.00
0.149
1
8/25/2010
m-,p-Xylene
BQL
2.00
0.0980
1
8/25/2010
o-Xylene
SOL
1.0D
0.0650
1
8/25/2010
Spike
Spike
Percent
Added
Result
Recovered
1,2-Dichloroethane-d4
30
29.6
99
Toluene-d8
30
29.8
99
4-Bromofluorobenzene
30
29.7
99
Comments:
Flags:
BQL = Below Quantitation Limits.
Analyst: Oy0
1
1
Reviewed By: 6
Flag
J
Page 2 of 2 Cans
area
N.C. Certification #481 Page 6 of 7

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