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HomeMy WebLinkAboutNCS000508_COMPLIANCE_20161221-- STORMWATER-DIVISION-CODING-SHEET— PERMIT NO. DOC TYPE ❑ FINAL PERMIT ❑ MONITORING INFO ❑ APPLICATION ®'COMPLIANCE ❑ OTHER DOC DATE ❑b"I YYYYM M DD RE5EARCII & AIV YTkAt Report of Analysis LAbORATOR6E5, INC. a 12/912016 n f CS ()O� For: Pilot Environmental�,* PO Box 128 W '24,�-9Hg4Y`5� Kernersville, NC 27285 RECEIVED 1cc iw NC a34 '� = z: Attn: BJ Lineback DEC 212016 Nca37701 CENTRAL FILES � �RECt0 �co $ DWR SECTION ,�'���,�1> ClientSample ID: SDO 004 - Lab Sample ID: 27735-01 Site: Pilot. Environmental Collection Date: 11/29/2016 16:00 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Ammonia Nitrogen SM 4500 NH3 D-1997 0.163 mg/L 0.1 MZ 121512016 BOD-5 SM 5210 B-2001 3.89 mg/L 2 SR 12/1/2016 1320 COD EPA 410.4 16 mg/L 5 BR 12/5/2016 Hydrocarbon O&G EPA 1664 Revision S/Silica <5 mg/L 5 ON 12/l/2016 Gel MBAS SM 5540 C-2000 <0.1 mg/L 0.1 AW 1113012016 Nitrate + Nitrite SM 4500 NO3 E-2000 0.677 mg/L 0.05 DW 11/30/2016 1440 Total Phosphorous SM 4500 P E-1999 0.452 mg/L 0.05 SK 12/6/2016 Total Suspended Solids (TSS) SM 2540.0-1997 13.4 mg/L 5 AW 12/1/2016 Client Sample ID: SDO 024 Lab Sample ID: 27735-02 Site: Pilot Environmental Collection Date: 11/29/2016 15:12 Parameter , Method .Result Units Rep Limit Analyst Analysis DatelTime Ammonia Nitrogen SM 4500 NH3 D-1997 0.119 mg/L 0.1 MZ 12/5/2016 BOD-5 SM 5210 B-2001 17.0 mg/L 2 BR 12/1/2016 1320 COD EPA 410.4 67 mg/L 5 BR 12/5/2016 Hydrocarbon O&G EPA 1664 Revision B/Silica <5 mg/L 5 ON 12/1/2016 Gel MBAS SM 5540 C-2000 0.116 mg/L 0.1 AW 11/30/2016 Nitrate + Nitrite SM 4500 NO3 E-2000 0.279 mg/L 0.05 DW 11/30/2016 1450 P.O. Box 473 1p6Short Street Kernersville; North Carolina 27284 Tel: 336-996-2841 Fax: 336-996-0326 vnvw.randalabs.com .Page 1 ral .ca_basi� vtd RESEARCh & ANAlyTlCAI Report of Analysis LAbORATORBES, INC. 12/9/2016 Client Sample ID: SDO 024 Lab Sample ID: 27735-02 Site: Pilot Environmental Collection Date: 1129/2016 15:12 Parameter Method, Result Units Rep Limit Anal s Analysis Date/Time Total Phosphorous SM4500 P E-1999 0.898 mg/L 0.05 SK 12/62016 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 AW 12/1/2016 Client Sample ID: SDQ033 Lab Sample ID: 27735.03 Site: Pilot Environmental Collection Date: 11/29/2016 16:30 Parameter Method Result Units Rep Limit Analyst Analysis Datefrime Ammonia Nitrogen SM 4500 NH3 D-1997 0.115 mg/L 0.1 MZ 121512016 BOD-5 SM 5210 B-2001 14.7 mg/L 2 BR 12/l/2016 1320 COD EPA 410A 20 mg/L 5 SR 12/5/2016 Hydrocarbon 08G EPA 1664 Revision B/Silica <5 mg/L 5 DN 12/12016 Gel MBAS SM 5540 C-2000 0.271 mg/L 0:1 AW 11/30/2016 Nitrate + Nitrite SM 4500 NO3 E-2000 1.90 mg/L 0.05 DW 11/30/2016 1450 Total Phosphorous SM 4500 P E-1999 0.406 mg/L 0.05 SK 12/6/2016 Total Suspended Solids.(TSS) SM 2540.0-1997 18.6 mg/L 5 AW 12/1/2016 NA = not Onclyzed P.O. Box 473 106 Shod Street Kemersville, North Carolina 27284 Tel: 336-996-2841 Fax: 336.996-0326' www.randolabs.com Page 2 ral coo basic yid Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 12/01/16 Performing Test Research & Analytical Laboratories; Inc. Comments: Stormwater Effluent A Pilot Environmental Project f O r in Responsible Charge RAL #27735-01 MabilLr,ftory Supervisor MAIL ORIGINAL TO: Div. Of WatertQuallSciences Branch N.C. DENR 1621 Mail Service Center Raleigh; NC 27699-1621 North Carolina Ceriodanhnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results. CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t # Young Produced Tabular t % Reduction Adult (L).ive. (D)ead %Mortali ty Ef(luentoh TREATMENT 2 ORGANISMS # Young. Produced Adult (L) We (D) cad PH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 Control CV control organisms brood L Ind sample B t e a n r d t Ist sample Ist sample 2nd sample Control D.O. "1'reatmeni 2. 1.C50/Acute Toxicity Test. ,(Mortality expressed as %. combining repli=cs) PASS FAIL Check One 11 / 30 16 Collection (Startl Date Sample 1 1129/16 Sample2 Snmplc Typc/Dumdon Sample I Sample 2 Grab Comp. Duration X Spec.Cond.(µmhos) Chlorine(mg/1) Sample temp. at receipt 0 % 6.25 % 72.5 % 25 % 50 % 100 % °/a I % % % o % 0 % 1 0 % 0 % o % u % % % % % LC50 = >low. % Method of Determination .....................-.................. 95°h Confidence Limits Moving Average �S Probit ........................... % % Spearman Karber Other ............ X ........... Organism Tested Ceriodaphnia dubia Duration (firs) 24 Copy DWQ rorrn AT.1 (3187) rev. I1/95 K S c -nn N _ C pfp/t y 3 3.0 Concentration Mortality Noic: Plcsu Complete 71tis Section Also StwVod Stantemd 6.94 6.99 1 Cantral 8.6 8.4 6.73 6.81 High 6.3 1 6.1 PH Conc. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 12101/16 Laboratory Performing Test Research & Analytical Laboratories, Inc. Comments: StotmwaterEAluent X A Pilot Environmental Project Sign a c Qpc orin csponsiblc Charge RAL 9 27735.02 -- X �/ Sigufibureb1`Lab4jtarySupervisor Environmental Sciences E MAIL ORIGINAL TO: Div. Of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North. Carolina Ceriodanhnia ChronicPass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 ;< Young Produced Adult (L) ive (D) ead Effluent%% TREATMO472 ORGANISM N Young Produced Adult (L) ive (D) ead Control PH Treatment 2 D.O. Control 'rreunnent 2 1st sample F1 t c o n r d t 1 st sample M (Mortality expressed as %, combining replicates) MEN 2nd sam le s t e a n d t 2nd t Com fete This For Either Test 'D rest Stan ate Il 30 16 Collection (Start) Date Sample 1 11/29/16 Sur 2 Samnle'1'ym(Duration _ N G y Sample 1 C c w Snmple2 rt n Hardness (mg0)op Spcc.Cnd.(µmhos)Chloriadmg/1)Sarnple temp. at receipt Graff Comp. Duration X 0 %O 6.25 .% 12.5 % 25 % 50 % 100 °% % % % % 0 % 0. % 0 % 0 % 0. % 0 % % % % % LC50 = >100% % Method of Determination .............:.........-................ 95%Confidence Limits Movie Aver e S Average Q Pro6it . ....................... % Spearman Karber Other ... X Drganism'rested Ceriodaphniadubia Duration (Ins) 24 7opy DWQ forte Al'-1(3/87) rev. 11195 Concentrudon Mortality Nalc', plcax Cnmplele This Seition Nso Start/end Ston/cvd 6.94 6.99 Control 6.6 8.4 6.99 7.04 Higb 6.2 6.0 pli Conc. ' D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 12/01/16 Performing Test, Research & Analytical Laboratories, Inc. Comments: StormwaterEftluent A Pilot Environmental Project f �e r i esponsible Charge RAL 9 27735-03 f abo ry Supervisor ' ;5 Branch ORIGINAL TO- DEnvironmental Q;lry N.C. DENR. 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodoohnia Chronic PUSs/Fail Reproduction Toxicity Test Chronic Testlt=lts COMI'ROLORGAMSMS 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t Tabular t d Young Produced % Reduction Adult (L) ive (D) ead I I I I I I I I I I I I ( 04 Mortalit Ef7lumtYo TREATMENT 2 ORGANISMS 4 Young Produced Adult (L) ive (D) ead Control PH Treatment 2 I St sample 1st sam le a S t e t < Ind sam le y t C a n St sample Ist sample 2nd Control D.O. Treatment 2 LC50/Acute Toxicitv, Test (Mortality expressed as %, combining replicates) FAIL I I Check One I 11 30 16 Collection (Start) Date Sample 1 11/29/16- Sampla2 Sample'IMEIDuration Sample I Sample 2 Grab Comp. Utaation X Spec.Cond.(µmhos) Chlor(ne(mgd) Sample temp, at receipt 0 % 6.25 % 12.5 0/0 25 �0 50 °/% 100 % % % 0 % 0 % 0 % 0 % 0. % 0 % % % % % LC50 = >100% . % Method of Determination ...... -..........' ft s................ -T 95%Confidencelimits Moving Average Probit "/r :.....:................: °� Spearman Kerber Other X' Organism Tested Ceriodaphnia dubia Dunuon (um) 24 Copy DWQ j0rm AT -I (3187) rev. 11/95 Concentration Mortality 3.0 T Nutc: Please Complete This Seaticn Alsu Start/cnd Stanlcad .6.94 1 6.99 1 Conacl 1 .6 8.4 6,16: 7.00 Hid, 7.5 1 7.3 PH Cone. D.O. Effluent Toxicitv Renort Form - Chronic Pass/Fail and Acute LC50 Date 12/01/16 Performing Test Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent APilot Environmental Project _ �O r! sponsible Charge RAL 8 27735-04 f nbo ory Supervisor Environmental Sciences f MAIL ORIGINAL TO: Div. Of Water Quality N.C. DENR 1621 Mail Service Centet Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Renroduction'Foxicitv'fest CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t Tabular t # Young Produced %Reduction Adult (L) ive (D) cad % Mortal ity Emuept% TREATMENT 2 ORGANISMS # Young Produced Adult (L) ive (D)cad pH Control Treatment 2 Control D.O. Treatment.2 1 2 3 4 5 6 7 8 9 10 11 12 Control CV control,organivns prodacin 3rd brood I st sample 5 t e a n r d t •1st sample (Morality expressed as %, combining replicates) Istsam le s t c a n d 1 Ist sample 2nd sample FH 1 C a n r d t 2nd sample FON FAIL I I Check One I 11 /1 30 / 16 ;ollection (Stan) Date Sample.1 11/29/16 Sample Sam IIc Ty rAffatian Sample I Sample 2- Grab Comp.. Duration X Spec.Cond,(pmhos) 1 190 Chlorine(mg1l) Sample temp. at reccipt 0 % 6.25 % '12:5 of 25 % 50 % 100 % % % % % 0 % 0 % 1 0 % 0 % 0 % 0 % % % V. I % LC50= >I00% % Method of Determination ....._........- ......................... 95%Confidence Limits Making Average � � Prpbit % Spearman Karba Q Other .,X Irganism'restcd Ccriodaphniadubia Daraoon(hts) 24 opy D WQ.to= AT.1 (3/87) rev. 11/95 3.0 Concentration Mortality No¢: Nlcase Campletc This Sccdon Also StaNend StwVmd 6.94 6.99 Cannot 1 8.6 8.4 7.11 7.15 yid 7.1 1 6.9 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 12/01/16. Piedmont Triad Airport Authority NPDES4NC-S000508 Pipe4 IS #02 County Guilford Performing Test Research k Analytical Laboratories, Inc. Comments: Stormwater Effluent APilot Environmental Project 2f Opp esponsible Charge RAL #? 27735-05 f Ubohdary Supervisor MAIL ORIGINAL TO: oi'v' N.C. North Carolina Ceriodvnhnia Chronic Pass/Fail Reproduction Toxicitv'rest. CONTROL ORGANISMS 1 2. 3 4 5 6 7 8 9 10 11 12 N Young Produced Adult (L) ivvee'(D) cad Effluent% I I. 1'REA'rMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 II 12 N Young Produced Adult (L)ive (D) cad PH l • Control Treatment 2 Control Treatment 2 l st sample s I C a n r d L 1st sample M (Mortality expressed as %, combining replicates) I st sample s t C a n r d t I st 2nd sample s t C s n d 1 1621 11 30 16 Collection (Start) Dnle. Sample ) 1 29/16 Samplc 2 Samnle Tvne/Dmation Sample I Sample 2 Grab Comp. I Duration X e N 6 o � o O C. Hardness (mI 1 49 )1i Sp. C", 190 110 Chlodne(mgd) ® 0.03 Sample temp. at receipt 3.0 0 °l0 6.25 °l 12.5 */0 25 A0 50 % 100 % % :° % % 0 % 0 % 1 0 % 0 % 0 % 0 % % % % % LC50= >I00% % Method of Determination 95°fo Confidence Limits- Moving Average � Probit %- % Spearman Kmber Other X Organism Tested Ceriodaphnia dubia Dun ion (Is) 24 Copy DWQ farm AT.I (3187) rev. 11195. Concentration T Mortality Note:.Plc°sc Campleta This Sectlan Alin Startlend Stan/end 6.94 699 1 Cannot 8.6 8.4 7.03 7.08 Hiah 6.4 1 6.1 pll Conc D.O. Effluent Toxicitv Report Form - Chronic Pass/Fail and Acute LOO Date 12/01/16 Facility Piedmont Triad Airport Authority NPUESNNC� S000508 Pipcq IS 405 County Guilford Laboratory Performing Test Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent X A Pilot Environmental Project Sigtlaturyrof Oip risible Charge RAL k27735-06 X Sign re Labo ory Supervisor MAIL ORIGINAL TO:Environmental Div. Of Water Quality ranch North Carolina Ceriodaahnio. Chronic Pass/Fail Reproduction Toxicity Tcst Chronic Tat Results CONTROL ORGANISMS. 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t Tabular t N Young Produced %Reduction Adult (L) ive (U) cad %Mortali ty Eltlucnt% Treatment 2 Treatment 2 TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV N Young Produced ° 0 FCh.k control organisms Adult (L) ive (U) ead producing 3rd broad Istsample Istsample 2ndSample 11 % 30 11 Control lCollection (Start) Date pH Sample ) I U29/16 Sample 2 Treatment 2 M FR Sample TypHDuration I C I C rc 17 9 Grab Comp: Duration a.a n a n a n c o"" r d r d r d sample I X G n t. t t I P = � c Ist sample Ist sample 2nd sample Sample 2 R n Control Hardness rnhos(mgA)rm p,G,[1] FE P] SpeaGand.(µmhos)Treatment 2 Chlorine(mg/I)LC50/Acute Toxicitv'rest Sample temp. at receipt (Mortality expressed as %, combining replicates) 0 % 6.25 % 12.5 c/ 25 50 % ' 100 % % / ,% % 0 °h 0 % 1 0 % 0 % 0 % 0 % °h % % % LC50= Method of Determination ..... ...>100%-,,,,.......°/. 95%Confiden..._ce Limits Moving Average 1°robit III` ........................... %- ! Spearman Barber Other .........._X........... Organism'rested Ceriodaphniadubia Durarion(hn) 24 Copy UWQ form AT -I (3197) rev. I1/95 Concentration Mortality Nate: Pleme Compktc This Smian Also Starvend Start end 6.94, 6.99 Control 8.6 8A 6.96 1 7.00 Hid 7.3 1 7.1 PH Cone. U.O. Effluent Toxicity Report Form- Chronic Pass/Fail and Acute LC50 Date 12/01116 Piedmont Triad Airport Authority NPDES#NC S000508 Pipe# 1S #06.. County Guilford Performing Test Research & Analytical Laboratories, Inc. Corrlments: Stormwater Effluent A Pilot Environmental Pro eft f Opt. rim sponsible Charge RAL #27735-07 �LabO ory Supervisor MAIL ORIGINAL TO: Quality North Carolina Ceriodaahnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10fl 12 Calculated t Tabular t # Young Produced o h Reduction Adult (L)ive (D)cad °/aMortality Avg. Rcrod. Control Control EfllueoN/o Treatment 2 Treatment 2 TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV PASS FAIL # Young Produced ° O /o control organisms Adult (L) ive (D) end Producin 3rd brood Check One Complete This For ither Li -'lost Start Date l stsample Ist sample 2nd sam le I1 30 16 Control Collection (Start) Date pH Sample l 11/29/16 Sample 2 Treatment 2 FT1 Sample Typc/Dtuation s s s e t e e m a n a n a n Grab Comp, Duration j r d r d r d Sample I X t r t P P3 P3 E Ist simple IStsample 2nd sample Sampie 2 e a rt Control Hardness (hos) 49 ®. D.O. SpecCand(µmhos) 190 137 Treatment 2 Chlorine(mg/p 0.04 LC50/Acute Toxicitv'rest Sample temp. at receipt 3.0. (Mortality expressed as %, combining replicates) 0 % 6.25 % 12.5 % 25 '/0 50 % 100 '% % I % % % 0 % 0 °% 1 0 % 0 % 0 % 0 % % I % I % I % LC50 = >100% % Method of Determination 95%Confden.c.cL. *i..m...i.t.s................. Moving Average Probii ........... %. ..................... % Spearman Kerber O Other ................. .,, Organism Tested Ceriodaphnia dubia Duration (ors) 24 Copy DWQ form AT.1 (3187) rev. 11/95 Concentration T Mortality New Please Complete 71ds. Section Also Stanfend Suattend 6.94 6.99 1 Camrol 1 8.6 8.4 6.97 7.01 High 7.0 1 6.8 PH Conc. D.O. Effluent Toxicitv Report Form - Chronic Pass/Fail and Acute'LC50 Date 12/01/16 Performing Test. Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent _elect A Pilot Environmental Pr..L_...._.-.__._........ fOpc orin.ResponsiblcCharge RAI,N'27735-08 f Labo tory Supervisor Environmental Sciences Branch MAIL ORIGINAL TO: N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnio Chronic PasslFail Reproduction Toxicity Test Chrpnic Test Rcsallt CONTROL ORGANISMS 1 2 3 4 5 6, 7 8 9 10 11 12 Calculated t -- — — Tabular t N Young Produced % Reduction Adult {I) ive. (D) cad % Morality Avg. Reprod. rod. Control Control Eftlucnt% Treatment 2 Treatment 2 TREKI MENf 2 ORGANISMS 1 2 3 4 5 6" 7 8 9 10 11 12 Control CV N Young Produced o 0 PASS FAIL /o control organisms Adult (L) ive (D) ead produca�3rd brood LEEEEI. Control PH 'Treatment 2 Ist sample Control D.O. Treatment 7 LC50/Acute Toxicity Test (Mortality expressed as %, wrabining replicates) l st sample s t c a n r d I Ind sample 5 t C a n r d t 2nd sample 11 / 30 16 Collection (Start) Date Sample 1 11/29/16 Sample 2. Sample Typ- =tion---� I GrablComp.l Duration I Sample 1 x Sample 2 O 0 Spec.Cond.(µtnbos) 190 Chlorine(mg/l) 10-0 Sample imp. at receipt o- 0 % 6.25 % 112.5 %1 25 %1 50 % 100 °! % % % °h D %1 0 % 1 0 %1 0 %1 0 %1 0 % % I % I % % LC50= ?I00% % 'Method of Determination. ..'n'c'r....Lim......._its................._. 95%ConfidencMoving Average. Probit ...........................°h" ........................% Spearman Kerber Other ............X............ organism Tested Ceriodaphnia dubia Dmuuon (irs) 24 ;opy DWQ fonn AT-] (3187) tcv. I IM 3.0 Conccnaadon' T Mortality Note: please Complete This Section Also Stert( n_d Sarveod 6.94 6.99 Control 8.6 8.4 7.13 7.17 High 7.3 1 7.0 PH Cone. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute.LC50 Date 12/01/16 Performing Test Research & Analytical Laboratories,Inc. Comments: Storrawater Effluent A Pilot Environmental'Pro•ect le Charge RAL # 27735-09 Supervisor MAIL ORIGINAL TO: North Carolina Cerindnphm6, Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS # Young Produced Adult (L) ive (D) cad Effluent0A TRFA•IMENT2 ORGANISMS # Young. Produced Adult (L) ive (D) cad U Control Treatment 2 it Service Center NC 27699-1621 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t Tabular t _ % Reduction %MortwiIy Avg. Rc rod. Control Control Treatment 2 Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 Control Cv PASS FAIL % control organisms producin 3rg dbrood Check One lstsample Isern le 2ndsample . S S 6 t e t < t e a n a n a n d r d d t t t I st sample I st sample 2nd sample Control D.O. "Treatment 2- LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates) ,Smnple1 1129116 Sample Sample TJpe/Durafion Grab Comp. Duration N z c � c o :Sample 1 X' S Snmple2 ; n v _ Hardness,(mgA) Spec.Cond.(pmhos) Chlorine(mg1l)- Sample temp. at receipt• 190 106 0.03 0 % 6.25 % 12.5 % 25 % 50 '/O 100 % % % % '% 0 % 1 0 % 1 0 % 0 % 0 % 0 % % % % LC50.= >100% % Method of Determination ........._...._................_...... 95%Confidence Limits- Moving Average e � Probit .............%' ...._..-..............% Spearman Karba. Q Other ............ X...... Organism Tested Ceriodaphnia dubia Daradon (Ins) 24 Copy D WQ form ATd (387) rev. I M5 Conaastration Mortality Note: Pleax ComplMe Tld5 Section Also Sturt/end StarVend 6,94 6.99, .Conuol 8.6 1 8.4 6.98 1 7.02 1 High 7.4 7.2 PH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 12/01/16 'rind Airport Authority NPDESNNC S000508 Pipc4 IS 411 County Guilford Test Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent A Pilot Environmental Project �_Rmonsibic Charge RAL 427735-10 _ y Supervisor MAIL ORIGINAL TO:Environmental Div. Of Water Quality ty s rant North Carolina Ceriodaphniu Chronic Pass/Pail Reproduction Toxicity Tcst Chronic'res Results COMI'ROL ORGANISMS I, 2 3 4 5 6 7 8 9 10 I l 12 Calculated t Tabular t # Young Produced H_ %/*,Reduction Adult (L) ive (D) cad % Mortality Avg. Re rod. Control Control EfOuent°A Treatment 2 Treatment 2 TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 II 12 Control CV N Young Produced ° 0. PASS FAIL control organisms Adult (L) ive (ll) ead producing 3rd ood Check Onc +H I st sample Ist sam Ie 2nd sample 11 / 30 / 16 Control Collection (Startl Data pH Sample 1 11/29/16 Sample 2 Treatment 2 Sanple TvnelDuretion t e t c t c ..Grab Comp. Duration V n a n a n a n r d r d r d Sample 1 i at sample Istsample 2nd sample Samplc2. Control Hardness (mgAmhos9 D,D.O.1E EHSpeaCond.(µmhos) 190 253 Treatment 2 Chlorine(mg/1) 0.04 L.C50/Acute Toxicity Test Sample temp. at receipt ® 3.0 (Mortality eVressed as %, combining replicates) 0 % 6.25 % 12.5 % 25 % 50 % 100 % °h % % % LC50= >100% % Method of Determination ..__._._............._....._..... 95% ConfidcnceLimits Moving Average Probit ...........°/r °h Spearman Karber Other .............X............ Drganism Tcsted Ceriodaphnia dubia Dumrinn (hrs) 24 =opy DWQ to. AT.1 (3187) rev. 11195 Concentration Mortality Nnre: Pleare Complem Thi3 Section AISo Start/end Sta /end 6.94 1 6.99 1 Conuni 1 8.6 8A 6.99 7.03 kligh 7.4 7.1 pH. Cone. D.O. RESEARCH & ANA yTICAI I.A oRATdRks, INC. AM"cat / Procam consultations Phen ..vas, ena-tow. CHAIN OF CUSTODY RECORD Rarer/R'astewater Mtsa Company Job No. Pilot Environmental, Inc. (PTAA PO 12157) Street Address Project g - d PO Box 128 PTIA NPDES Compliance (N2Y7P2E1T-) gp -ff City, State, Zip Sampler Name (Please Print)It Kernersville, NC 27285 B.J. Lineback336.708.4655 't s < ° � m ° q �' � p x a z z Contact Phone Sampler Sigaatu q BJ. Lineback 336.310.4527 U c z m 0 9 $ 9 8, t 6 Si $ 0 i e& C 0 e $ 0 o: 0 a �� C> 0 v e 4 8 sample Number Date Time d E a 1° to Temp °C Rp, CL Chtori mov Sample Metric Sample Location / LD. P O Z (Lab Use Only) e rj a a a a .a ,� .a Q 1 j 3 Il tloot� ✓ w soo ooa 6 1 2 1 z 'O o a o w u ^ a U ✓ w -5De46A— 6 1 2 1 2 p T c. 2 W F ui w e owrpz CS zm w p a0 'x o ✓ w —SD&466A— 6 1 2 1 2 15a ✓ w soo024 6 1 2 1 2 ✓ w —3B@9z'Cr 6 1 2 1 2 = n °o Z Z O a a � d tmD gym, r+ m a te; (D 0 z / W enn 2; —esaes,v� 6 1 2 1 2 ✓ w-39 6 1 2 1 2 u> () ✓ w SDO 033 6 1 2 1 2 Co 1 gQ ✓ w Is #01 1 1ca } N a d W Z ~ •U O U - m Y Q FO— y $ U �o ( ✓ w IS #02 1 1 ✓ w IS #05 1 1 It . 47✓ w IS #06 1 1 ✓ w IS #07 1 1 ; 5 u o t v <au ✓ w 13 #SA 1 1 Iq ( ✓ w Is#10 1 1 N ✓ w I5 #11 1 1 a Re' Wished ete/f Received By /i /ta g30 lklfiquhhedB batifrime Recelve y Routine (quart and Deicing Event (4 b/w Oct -Apr) Analytical Monitoring. Please p results to httos•//Profect5mbake ro mm/PMA/UsU//Lab%MResults/Ali tams asoz Moveh 1p 6 s` �J3o-re /0i1ro4. EK ke sample Temperature at receipt °C RESEARCh & ANA1yTICAt LAbORATORIES, INC. Analytical/Process Consultatons December 1, 2016 Pilot Environmental, Inc. P.O. Box 128 Kernersville, NC 27285 Attention: B.J. Lineback 1. EPA Method 8015 Parameter Ethylene Glycol Propylene Glycol Sample Number: Sample Collected Date: Sample Collected Time (Hrs): Project Name: PTIA NPDES Compliance (N2Y7P2E1T-) Quantitation Limit (me/L) 10.0 10.0 SDO 004 SDO 024 SDO 33 Results Results Results (me/L) m L (ma/L) BQL BQL BQL BQL BQL BQL 27735-01 27735-02 27735-03 11 /29/ 16 11 /29/ 16 11 /29/ 16 1600 1512 1630 mg/L = milligrams per Liter = parts per million (ppm) BQL - Below Quantitation Limit RESEARC{l1 & AutyflCAL UbORATORks, INC. CHAIN OF CUSTODY RECORD Analvtlml / Process Consultations Water Wastewater Mist Company Job No. Pilot Environmental, Inc. (PTAA PO 12157) Street Address Project PO Box 128 PTIA NPDES Compliance (N2Y7P2E1T-) City, State, 21p Sampler Name (Please Print) C Kernersville, NC 27285 B.J. Llneback336.708.4655 1 x N y a z Q x 'p z 5 0 Contact Phone Sampler Signatar o> B.J. Lineback 336.310.4527� tj ✓ I" V 5 g 6 9 oa V n' o: s p` "'t Sample Number Date Time d 6 a Temp Rea. Chlorin w Semple Maui: Sample Location / I.D. P O (Leb One Only) (5 V °C CI. r z a .. .a a .7 .. .i Y 2—I 3 It/MGt(noa ✓ w SD0004 6 1 2 1 2 O o a o v- y V, p > ✓ w —sa966A— 6 1 2 1 2 m 0 _ F vi LL c ✓ w "091^" 6 1 2 1 2 1,512 ✓ w SDO 024 6 1 2 1 2 0 ,du Z O ✓ w —49@946— 6 1 2 1 2 s N m p ra o 0 a m v? z r a ✓ W `99 027. 6 1 2 1 2 `o V r 0 ✓ W —Sao Bd0 6 1 2 1 2 ❑ Z Z 0 a ✓ W SDO 033 6 1 2 112. 50 ✓ w IS #01 1 1 o v F X at ,q F\ L 0$ 4 o a" n e s d i p ✓ W IS #02 1 1 ✓ w IS #OS 1 1 ✓ w IS #06 1 1 ✓ W IS #07 1 1 ✓ W l5 #BA 1 1 1711 ✓ W IS#10 1 1 W u N m n ✓ W IS #11 1 1 Bn atshed ate r* Received By Re / !te 830 Re' go[sbed B atdTime Receivery Routine (quart and Deicing Event (4 b/w Oct -Apr) Analytical Monitoring. Please pperresults to r ects.mbaker r m PTI sts R ults Alllte s n ke I Sample Temperature at receipt °C 4 �TI DIEM Mt.TmM enVUWMML AIRPWT fRp O e v.r I Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report NPDES Permit: NCS000508 Page 2 of 3 3 > k h + ;ne ac 9uldanceoncom, completing thts� =n r ,c a - Quantitative Data to be;collected $ investigator 336.708.4655 "-_"` `•, oftion ti x`* s p a �IFIr //aortal ncdenrarp web/< •a • r / " duungRoutine (P) and De1cinj$ s ff-° x - s,� a ,,, oo Event (E) Sampling F Y:- Date ftfnpdesstorrnwoter/ 'g�, { N 4 ou £y} a� , ,.+s.-. .t., `NPD.ES.r„ .seVoD.�Oenod„m>, of yTer (A, RSDOonly) 2 I 7 I 2 1ca c �m v > mti a i o 4 =%o �;+.1=r�� nary nee .E, ` n q. t r °' ,r 01 s> y2r {/� * Ni Ti. i •p V X �.+«'f0 +.t i /' t�S.0 O fE !S&RSDO) {E= ISortty) (E !Sooty)_ N 7� Turbidt rD O , P iditV ,' c .� " Y �° . Structure :- CIA R+,S r_-[ Ci ' 500: � Time Flow ..Q=ei 0. =—,0_ 4 IyO;t `.rts i `Ii ?t0 + { �. ly Zl NTU) ' (S mg%L)' (6 - 9) Structure; , ::3COndlnon: v u ,O ' u a vlr, LL wA , O.. o . =(SU 004 54° ✓ �/ J QAor �/ / j / '/ IV �( N 3 04 = yRCP'_ o e R A i d15� fi•"I i6A riPrapswale 024 6 RCP �l� ✓ 1P.�+f l � 7-Tf P.a� n za' 026 36 CMP a (5 3® N z D 027 54 RCP$ 3' IV o z _ e 030 4 MPe' 3% f .�J A: �r s 92t�RCP^�) �. �� ,t „'oit`d t'2 033 � ��P�J� I5: rLa%ation F•Timex'wCondition`Flow„,, `,' .<t+...-Eiosion(tributiiry;/.bank'stability)' ' �:€<^ ,t ^.'H #_ Turbidi • '6D.O. * #Ol Bn sh Creekr,>,{0 F -._x �: E 0.r� - #02 Bnish Cre�eyk>!,�; ��j� '�`sa �/'--.. { �. a5� $. 36 In -Stream Deicine=Event laboratory Analysts: 40; Btush Cree y - a . GY ! 8 v �.8 'rk„l O Acut Townty . #06 BrushC�eekx' Y z_ .51 i UT to s .. s'!zA Horsepe 4r 0UTto P 7 a-t Horse en t httas•//arolectz°mtiakercnm com/Prik - " #11 Horsepen 7 Y x �J A/U[s/Field%20Refults/Ailltem'sosox€ x r T7. Xf By this signature, I certify that this report is accurate and complete to the best of my knowledge: r APT/. ntrxonr ,rzuo rraterwm—m &emit Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report. NPDES Permit NCSOOOS08 y. - Page 1 of 3 s me ac Investigator' %r_`gurdonce oh completing this r* a 01 c "+ x erg„ T $ Quaiihtatrve Data to be collected 336.M8.46SS a»� pornonoftfiisjorm vrsrt y i ax *^ � c r- during Routinex(P) and DetcingI II ¢httnl/oortolncdenrorg/tveb/e + o,o . 'ia N t}'F "b$.a 2 Y i "�'t Event (E) SampLng Date o� N�vt E Ir/nudes stvrimvater/$f * /$�a. F i=L.C'cr Y .; ��^Y •OAV�1 C ), "':�L[. .O 'x t ,,.. a X. •M�p.G-�`s'?✓zc.' Peritid� EventTrer2 �.�_.0 Fe "tSYt k 5 3'.i' %Bv'a J�lY Y'r'a'.< `'T. �NPDES. ZSeason ... 2 � 7 '' ` � L � N � '�' #; m v >_ a, >�•, jj,rr+ f L-�fH-iSanty)g (E ISoniY) ( a wstructure' ��<�,� � c u i.. «; tea E '. '',P H Turbrdr tY D O h kx-x, �gf vs a' dad .,e." o-.� .`xiro-5 s t :.tin nv�1` , q+'���6 _ �f�iondtttony,Flow a'tr �, -�O �s�0"w'` Ott -,V 9fo ).- y)50 1 d.7 j....'Sie..9 _: 0 ..._ha±e LLK VI v.A LL'C ! Y 001 60 'RCP 002, 18 REPI ,' � m r i 005 42 RCP , i /Y /NJ t 007 60 RCP 5, `7 z Psi i 008 48 CMPr 1 V e_Leaf )i Pos"t campleted.vgn�ed(orm to A rol[cts:mbakerrom.com/Pflj x 27 009 . a * F ,2 ,ifW+ , Jjc)& ✓ ,�. Llra{ 1 N 1h�3 ✓ 9 �trstslFteld9fd0Aeiults/Aliltemsasox; 010 grasssheetf 011� grasssheetf 1t ay 012 grass sheetf - - . �'ta ,/ 013 grasssheetf v Inilll1 014 gr_assswale ' n y ,1N3 Id Y r prap swale 016 grass swa" o ?� it-/ 10117 151RCP � E Jl.t fQ M 018 a5f RCP:, z •8 019 31 RCP 3 m `o p/ et 020 � h%t ' 54u',rRCP�;.i 9 O 1023 •24 ' RCP ( s' z 025 13%;Mpll �028 48 � tRCPJ*d 029, 24 RCP '11{j 3 .7 031 36rRCP?G 3 032 ' '42` RCP, 03642 - a RCP E , / Y r r✓ t n.l ' 038 ; ' RCP ✓Le r xa 040 30 S RCP= '062 24 , By, this signature, I certify that this report is accurate and complete to the best of my knowledge- _ z National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page I of 4 Greensboro. Piedmont Triad International Airport Enter Your "City, S"h" or zip code Go metric en espanol 0 Precipitation D Temperature(°F) Pressure Wind Heat (in.) a Time Wind Vis. Weather Sky Relative Chill Index t test) (mph) (mi.) Cond. 6 hour Humidity (OF) (OF) altimeter sea Air Dwpt level 1 fir 3 fir 6 hr e Max. Min. (in) (mb) 29 16:54 SW 10.00 Overcast BKNO14 66 64 93% NA NA 29.90 1011.7 14 OVCO22 29 15:54 SW 10.00 Overcast BKN018 66 63 90% NA NA 29.87 1010.9 0.14 16 OVC030 29 14:54 SW 10.00 Overcast BKNO17 67 64 91% NA NA 29.85 1010.3 16 13KN042 OVC150 29 13:54 SW 10.00 Overcast BKNO08 66 65 96% NA NA 29.85 1010.2 0.14 206 OVCO21 25 29 12:54 S 16 2.00 Light 13KNO08 65 64 67 63 97% NA NA 29.84 1009.7 0.06 0.08 Rain OVC016 Fop/Mist 29 11:54 S 20 9.00 Light BKNO20 66 63 90% NA NA 29.86 1010.4 0.01 G 32 Rain OVC050 29 10:54 S 20 8.00 Light 13KNO17 65 63 93% NA NA 29.88 1011.1 0.01 G 26 Rain OVCO24 29 09:54 S 22 10.00 Overcast OVC018 65 61 87% NA NA 29.88 1011.1 G 33 and Breezy 29 08:54 S20 10.00 Light OVC018 64 61 90% NA NA 29.86 1010.7 G 30 Rain 29 07:54 S 21 10.00 Overcast OVC019 64 60 87% NA NA 29.86 1010.6 G 30 and Breezv 29 06:54 S 16 10.00 Overcast OVC019 63 59 63 56 87% NA NA 29.86 1010.6 0.0i G 30 29 05:54 S 20 10.00 Light OVC019 62 58 86% NA NA 29.86 1010.6 G 29 Rain 29 04:54 S 13 10.00 Overcast OVCO21 60 57 90% NA NA 29.85 1010.2 G 28 29 03:54 S 12 5.00 Light SCT021 57 56 96% NA NA 29.86 1010.7 0.07 0.08 Rain BKNO27 Fog/Mist OVC036 29 02:54 S 12 3.00 Light BKN029 57 55 93% NA NA 29.91 1012.3 0.01 Rain 13KN036 Fog/Mist OVC060 29 01:54 S 15 10.00 Overcast 13KNO44 58 53 84% NA NA 29.90 1012.0 OVC085 29 00:54 S 15 10.00 Overcast 13KNO45 57 52 57 51 83% NA NA 29.90 1012.3 OVC200 28 23:54 S 15 10.00 Overcast 56 51 84% NA NA 29.94 1013.4 http://wl.weather.gov/data/obhistory/KGSO.Iltmi 1 1 /29/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 2 of SCt050 BKN 130 OVC200 28 22:54 S 20 10.00 Overcast 13KN070 56 50 81% NA NA 29.94 1013,6 G25 OVC200 28 21:54 S 16 10.00 Overcast BKN065 56 49 77% NA NA 29.98 1015.0 G25 OVC200 28 20:54 S 22 10.00 Overcast BKN060 54 46 75% NA NA 29.98 1015.2 G 25 and OVC200 Breezy 28 19:54 SE 7 10.00 Overcast BKN065 52 42 69% NA NA 30.00 1016.1 13KN 130 OVC200 28 18:54 SE 5 10.00 Overcast 13KNO55 51 41 55 51 69% NA NA 30.02 1016.7 BKN 130 OVC200 28 17:54 S 7 10.00 Overcast SCt050 51 40 66% NA NA 30.02 1016.8 BKN 130 OVC200 28 16:54 SE5 10.00 Overcast EEW050 53 39 59% NA NA 30.02 1016.6 SCT 130 OVC200 28 15:54 Sr 5 10.00 Overcast 13KN048 55 38 53% NA NA 30.04 1017.4 BKN 130 OVC190 28 14:54 S 10 10.00 Mostiv BKN039 54 37 53% NA NA 30.05 1017.8 Cloudy 13KN130 BKN 190 28 13:54 S 9 10.00 Overcast I3KN036 55 32 42% NA NA 30.07 1018.2 OVC050 28 12:54 S 13 10.00 Overcast SCt038 54 31 54 34 42% NA NA 30.10 1019.2 BKNO55 BKN 150 OVC250 28 11:54 SW 7 10.00 Overcast EEW035 50 32 50% 47 NA 30.14 1020.8 BKN140 13KN 190 OVC250 28 10:54 S 6 10.00 Overcast FEW 100 46 34 63% 43 NA 30.16 1021.6 BKN 140 OVC230 28 09:54 SW 6 10.00 Overcast 13KN150 43 34 71% 39 NA 30.18 1022.3 OVC250 28 08:54 S 5 10.00 Overcast OVC150 40 33 77% 36 NA 30.18 1022.2 28 07:54 S 6 10.00 Mostiv BKN200 36 32 86% 31 NA 30.18 1022.2 Cloudy 28 06:54 SW 5 10.00 Mostiv 13KN250 35 29 39 34 78% 31 NA 30.16 1021.7 Cloudy 28 05:54 S 3 10.00 Mostiv IIKN250 35 30 82% NA NA 30.16 1021.5 Cloudy 28 0454 Calm 10.00 Mostiv BKN250 38 31 76% NA NA 30.16 1021.5 Cloudy 28 03:54 Calm 10.00 Mostly IIKN250 37 30 76% NA NA 30.16 1021.4 Cloudy http://wl.weather.gov/data/obhistory/KGSO.html 1 1 /29/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 3 of 28 0254 S 5 10.00 Fair CLR 36 30 79% 32 NA 30.16 1021.4 28 01:54 S 5 10.00 Fair CLR 38 31 76% 34 NA 30.18 1022.0 28 00:54 SW 3 10.00 Overcast OVC250 39 30 42 37 70% NA NA 30.19 1022.4 27 23:54 SW 5 10.00 Overcast OVC250 38 30 730,0 34 NA 30.18 1022.3 27 22:54 Calm 10.00 Overcast OVC230 40 30 68% NA NA 30.19 1022.6 27 21:54 SW 3 10.00 Overcast OVC250 39 29 67% NA NA 30.20 1023.0 27 20:54 Calm 10.00 Mostly 13KN250 38 28 68% NA NA 30.20 1022.8 Cloudy 27 19:54 Calm 10.00 Partly SCT250 42 28 58% NA NA 30.18 1022.5 Cloudy 27 18:54 SW 3 10.00 A Few FEW250 42 27 54 42 55% NA NA 30.18 1022.6 Clouds 27 17:54 Calm 10.00 Partly SCT250 47 26 44% NA NA 30.19 1022.5 Cloudy 27 16:54 W 3 10.00 Partly SCT250 50 25 38% NA NA 30.18 1022.3 Cloudy 27 15:54 W 3 10.00 A 17ecv FEW250 53 24 32% NA NA 30.18 1022.2 Clouds 27 I4:54 SW 3 10.00 Fair CLR 53 26 35% NA NA 30.19 1022.5 27 13:54 Vrb16 10.00 Fair CLR 52 27 38% NA NA 30.20 1023.0 27 12:54 W 5 10.00 Fair CLR 51 27 51 29 39% NA NA 3022 1023.6 27 11:54 Calm 10.00 Fair CLR 50 28 43% NA NA 30.25 1024.6 27 10:54 Vrbl 5 10.00 Fair CLR 47 29 50% 45 NA 30.29 1026.0 27 09:54 Calm 10.00 A Fcw FEW250 43 29 58% NA NA 30.29 1026.1 Clouds 27 09:54 NE 6 10.00 Partly SCT250 41 30 65% 37 NA 30.29 1026.0 Cloudy 27 07:54 N 3 10.00 Mostly 13KN250 33 28 82% NA NA 30.28 1025.7 Cloudy 27 06:54 Calm 10.00 Partly SCT250 31 27 37 29 85% NA NA 30.26 1025.3 Cloudy 27 05:54 Calm 10.00 Fair CLR 31 27 85% NA NA 30.26 1025.1 27 04:54 Calm 10.00 Fair CLR 32 27 82% NA NA 30.25 1024.7 27 03:54 N 5 10.00 Fair CLR 34 27 76% 29 NA 30.24 1024.2 27 02:54 N 5 10.00 Fair CLR 34 27 76% 29 NA 30.24 1024.2 27 01:54 Calm 10.00 Fair CLR 32 26 79% NA NA 30.25 1024.5 27 00:54 N 5 10.00 Fair CLR 36 27 44 35 70% 32 NA 30.25 10245 26 23:54 Calm 10.00 Fair CLR 35 27 72% NA NA 30.25 10243 26 22:54 N 3 10.00 Fair CLR 38 27 65% NA NA 30.25 1024.6 26 21:54 N 3 10.00 Fair CLR 40 27 60% NA NA 30.26 1024.7 26 20:54 N 6 10.00 Fair Cl,R 42 27 55% 38 NA 30.25 10243 26 19:54 N 5 10.00 Fair CLR 43 27 53% 40 NA 3024 1024.1 26 18:54 N 3 10.00 Fair CLR 44 27 56 44 51% NA NA 30.22 1023.6 26 17:54 N 3 10.00 Fair CLR 47 27 46% NA NA 30.22 1023.4 D Time Wind Vis. Weather Sky Max. Min. Relative Wind Heat altimeter sea a (est) (mph) (mi.) Cond. Air Dwpt Humidity Chill Index (in) level 1 hr 3 hr 6 hr t 6 hour (°F) (°F) (mh) e Temperature (°F) Pressure http://wl.weather.gov/data/obhistory/KGSO.litmi 11 /29/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 4 of 4 Precipitation (in.) National Weather Service Back to previous page Last Modified: Febuary. 7 2012 Southern Region Headquarters Privacv Poliev Fort Worth, Texas Disclaimer http://wl.weather.gov/data/obhistory/KGSO.litml 1 1 /29/2016 OP � JUL 13 Z016 To: North Carolina Department of'Ehvironmental Quality Division of Energy Mineral and Land Resources TRpLFILES ioriginol Attn: Central Files p VR SECTION a 1 copy) 1617 Mail Service Center Raleigh, NC 27699-1617 Discharge Monitoring Report Facility Name: Piedmont Triad International Airport Permit: NCS000508 County: Guilford Phone: (3361665-5600 Person Collecting Sample: B.J. Lineback, Pilot Environmental, Inc. (336) 708-4997 Certified Laboratory(s): Research and Analytical Laboratories, Inc. Lab #: 34 Lab #: Date of Sample Collection: June 24, 2016 Schedule (NPDES 2): Season 6 (year) Period 4 (quarter) Event (deicing) Tier Two (month) ADF Applied (if applicable) 0 gallons on June 24, 2016 0 gallons on June 23, 2016 0 gallons on June 22, 2016 Total Event Precipitation: 0.09 inches on June 24, 2016 0.39 inches on June 23, 2016 0.00 inches on June 22, 2016 Routine, Deicing Event, and/or Tier Two Analytical Monitoring Results Attached I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. 5- g 7/11/201.6 Signature: A///"''��" Date: https://p,oje,..mbake,ro, .[ IP11AAi1..IAttochmenIS135/DMF.do(e M Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report NPDES Permit: NCS000508 Pagel of 3 PIEDMONT TRIAD INTER NJLUDN t AIRPORT .. me ac)orguidonceon completing this - _ � . QUantltatiVe:Data to_be collected investigator: 336.708.4655 portion ojthisjorm, visit c during Routine (P) and Deicing - // -- �•//oortalncdenroro/weh/ 0 o _. +9_ - w — - -Event (E}Sampling Dater - '^ o '0 `'"- m °c o o In d d. -- c _o v IS (P-RSDO only) (P-RSDO Doty) - (E-OW) (E - IS only) (E - IS only) NPDES Season Period Event Tier ' c N •� _'a E .ace U,W.N. r U `o �` �`o m-. o N m = a „'a pH Turbidity D.O.. 1 - (50 NTUj (5 mg/L) .. - Structure SDO DOI 002 Structure 60 " RCP 18 " RCP Time 7 J ! $ ( �y Condition ✓ Flow [� u -a O a u ? u3i �° O w Og(69) ! I°i6vam��aervtm� lTllRi31)fn t E t t tj. f ,.. 003 OO5 18 " CMP 42 "RCP { a 0 q3� /� ✓ I I / N N N I I t i " 007 008 009 60 " RCP 48 " CMP 24 " RCP —7 f 5 �j�q ✓ ✓ / ( f _ C�e.t i _ c )E^� f I /`� —1 t t A' � Ad --�t�N ( ( 1 /J n/ I� _ cocompleted signed/oral too h[[Ds //Droterts mbakermro.com/PTt - 010 grass sheetfl —�2 R5 �( _/ N �_ 1 �_ _-__ A/Lc c/F r)dX20Resu1[s/AIlltems osDx 011 grass sheetf N 012 013 grass sheetf grass sheetf 55 014 grass Swale —43 ✓ _ _ ( m 015 riprap Swale , - 016 017 grass Swale 15 " RCP �Q� ✓ tj &L I $ $ 018 019 15 " RCP 36 " RCP _ o / �P�� !—'- I ( /J - Al 020 023 54 " RCP 24 " RCP �/ �_`� ...- — �l ; ti! I ( ! r A A l " RCP 025 36 .10 028 48 " RCP 0s 1 g U 10 029 24 " RCP r 031 36 "RCP ✓ — ---I � 032 036 038 42 " RCP 42 " RCP 48 " RCP [15 (����� ✓ I / /� i L I — i�! 1—� --) / I " i 040 30 "RCP RTs� Y� ✓ — �062 24 " CMP I I A Fx' By this signature, I certify that this report is accurate and complete to the best of my knowledge: _0- Ae co wsTru�:'le..�. eF,e, SDO .--r access.VV- APT/ PIEDMONT TRUDWWRNALDNM AIRPORT Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report NPDES Permit: NC5000508 Page 2 of 3 Lineback forguidance on completing this c Quantitative Data to be collected Investigator:336.708.4655 portion ofthisform,visit N during Routine (P) and Deicin g — Date:" �1 /n. —(� (- �e WD —httportal.ncdencorg/w/ eb �' = '� Event (E) Sampling (E/Hades-stormwater/ `^ -o N v u' e ? ' O 10�„ rs a o - NPDES Season Period Event Tier P-RSI)Oon P-RSIMon ( tNJ [ t3') 2 \ \ _ m o V m (E - !S&RSDO). (E - IS Daly) (E- lS only) c N y .o. c c a 'W N �. .Ln c r -'Structure pH Turbidity D.O.. SDO Structure Time Condition Flow ? - LL LL 0 0 (6 - 9) (50 NTU) (5 mg/L) u° O u v' m 004 54 " RCP (J 7 ✓ �1 rI I r T I (�'IN ( 7,a� Q c c 006 46 " RCP j/os11 16A riprapswale r00 % I 1cy: I I ( — ,E 024 36 " RCPAl 026 36 " CM P m 027 54 "RCP cr (J m 030 24"MP ' �� '�oO ✓ , I ( " ( f N 4 �.1a 033 42"RCP //�^, �(Sy� j ✓ ( 1 Iv ( l I i �I N N q �. 3.S 1 o t1 �c zt° G1eq✓ 15 Location Time Y ( _ -) Flow H Turbidity D.O. #01 Brush Creek lit #02 Brush Creek A ro -3'3 r r k05 Brush Creek ' r ^ a ' y s 'R } Tx r,, F er s c .-$.3"'1 M s 3 , . _ ,- =if�Y '.. 'ice*; tt06 Brush Creek ' In Stream Delclne Event Laborat tp Ahalysls UT toAE.IifET`rOXlCI1y!..,l gg' tt07 Horsepen _� t�j UT to itBA Horsepen s. .. Post completed signed form to: UTto s/�r,oiects.mbokerromPI T #10Horsepen A/sts/held%IOResuls/Am t7 'v t 'T—•� 'L-- 5 #11 Horsepen ice' & rs, .w•n .; e , .' s a' t> T° a Creek 1{. " ' .at r-t..r-: t -;5-.f ni t - r +� By this signature, I certify that this report is accurate and complete to the best of my knowledge: /�?c9-000stj� RESEARCh & ANA1yTICA1 LABORATORIES, INC. For: Pilot Environmental PO Box 128 Kernersville, NC 27285 Attn: BJ Lineback Report of Analysis 7/7/2016 .y NC 1134 Z. NC 937701 Client Sample ID: SDO 004 Lab Sample ID: 20922-01 Site: Pilot Environmental Collection Date: 6/24/2016 11:25 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Ammonia Nitrogen SM 4500 NH3 D-1997 <0.1 mg/L 0.1 JB 6/29/2016 BOD-5 SM 5210 B-2001 2.49 mg/L 2 KN 6/24/2016 1545 COD EPA 410A 14 mg/L 5 KN 6/29/2016 Hydrocarbon O&G EPA 1664 Revision B/Silica <5 mg/L 5 DN 6/27/2016 Gel MBAS SM 5540 C-2000 <0.1 mg/L 0.1 AW 6/2412016 Nitrate + Nitrite SM 4500 NO3 E-2000 0.965 mg/L 0.05 DW 6/24/2016 1420 Total Phosphorous SM 4500 P E-1999 0.056 mg/L 0.05 LP 7/6/2016 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 JB 6/27/2016 Client Sample ID: SDO 024 Lab Sample 10: 20922-02 Site: Pilot Environmental Collection Date: 6/24/2016 10:36 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Ammonia Nitrogen SM 4500 NH3 D-1997 <0.1 mg/L 0.1 JB 6/29/2016 BOD-5 SM 5210 B-2001 7.16 mg/L 2 KN 6/24/2016 1545 COD EPA 410.4 60 mg/L 5 KN 6/29/2016 Hydrocarbon 0&G EPA 1664 Revision B/Silica <5 mg/L 5 DN 6/27/2016 Gel WAS SM 5540 C-2000 0.388 mg/L 0.1 AW 6/24/2016 Nitrate + Nitrite SM 4500 NO3 E-2000 0.695 mg/L 0.05 DW 6/24/2016 1420 P.O. Box 473 106 Shod Street Kernersville, North Carolina 27284 Tel: 336-996-2841 Fax 336-996-0326 v ,randalabs.com Page 1 rat cea b2sic vld RESEARCh & ANA1YTiCA1 LA ORAY®RIES, INC. Report of Analysis 7/7/2016 Client Sample ID: SDO 024 Lab Sample ID: 20922-02 Site: Pilot Environmental Collection Date: 6/24/2016 10:36 Parameter Method Result Units Rep Limit Analyst Analysis Date(Time Total Phosphorous SM 4500 P E-1999 0.236 mg/L 0.05 LP 7/6/2016 Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 JB 6/27/2016 Client Sample ID: Site: SOO 030 Pilot Environmental Lab Sample 10: Collection Date: 20922-03 6/24/2016 11:00 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Ammonia Nitrogen SM 4500 NH3 D-1997 <0.1 mg/L 0.1 JB 6/29/2016 BOD-5 SM 5210 B-2001 <2 mg/L 2 KN 6/24/2016 1545 COD EPA 410.4 10 mg/L 5 KN 6/29/2016 Hydrocarbon O&G EPA 1664 Revision S/Silica <5 mg/L 5 ON 6/27/2016 Gel MBAS SM 5540 C-2000 <0.1 mg/L 0.1 AW 6/24/2016 Nitrate + Nitrite SM 4500 NO3 E-2000 1,17 mg/L 0.05 DW 6/24/2016 1430 Total Phosphorous SM 4500 P E-1999 <0.05 mg/L 0.05 LP 7/6/2016 Total Suspended Solids CTSS) SM 2540 D-1997 <5 mg/L 5 JB 6/2712016 Client Sample ID: S00 033 Lab Sample ID: 20922-04 Site: Pilot Environmental Collection Date: 6/24/2016 11:56 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Ammonia Nitrogen SM 4500 NH3 D-1997 <0.1 mg/L 0.1 JB 6/29/2016 BOD-5 SM 5210 B-2001 5.02 mg/L 2 KN 6/24/2016 1545 COD EPA 410.4 14 mg/L 5 KN 6/29/2016 Hydrocarbon O&G EPA 1664 Revision B/Silica <5 rng/L 5 ON 6/27/2016 Gel MBAS SM 5540 C-2000 <0.1 rng/L 0.1 AW 6/2412016 Nitrate + Nitrite SM 4500 NO3 E-2000 0.542 mg/L 0.05 DW 6/24/2016 1430 Total Phosphorous SM 4500 P E-1999 0.115 mg/L 0.05 LP 7/6/2016 P.O. Box 473 706 Short Street Kernersville, North Carolina 27264 Tel: 336-996-2841 Fax. 336-996.0326 vrmi.randalabs.com Page 2 IJI LOd 1xisic v1d RESEARCh & ANA1yTICA1 LAbORATORIES, INC. Client Sample ID: SDO 033 Report of Analysis Lab Sample ID: 20922-04 7/7/2016 Site: Pilot Environmental Collection Date: 6/24/2016 11:56 Parameter Method Result Units Rep Limit Analyst Analysis Date/Time Total Suspended Solids (rSS) SM 2540 D-1997 5.6 mg/L 5 JB 6/2712016 NA = not analvzed ......__._ '- .. ...._ .._. ........ ................ P.O. Box 473 106 Short Street Kernersville. North Carolina 27284 Tel: 336-996-284i Fax: 336-996-0326 www.randalabs.com Page 3 ral coa basic vld RESEARCH & ANA[yTICA[ LAbORATOR1ESt INC. Astalytlwl / Pro gu, Conaultallona Phone (336)996-2861 CHAIN OF CUSTODY RECORD Water/Wastewater Mist ompany Pilot Environmental, Inc. o No. 9 O> p z s _ x m V "� -� x S $ X V '19 a. '^ 9 7 V a; O � V o _ V ^ V .a ° 9 V -� @ 0 = treat Address PO Box 128 Project PTIA NPDES Compliance (N2Y6P4E-T-) City, State, Tap - Kernersville, NC 27285 Sampler Name (Please Print) B.J. Lineback 1336.708.4655 Contact B.J. Lineback Phone 336.330.4527 Sampler Signature Sample Number Date ` Time IIaS 6' U a V ✓ Temp 'C Res. CL Chlorin emo rN Sample Matrix or w Sample Location / LD. son ooa (Lab Uee Ody) 2 t� este7��Uo z 1 z = ✓ w dry.-5B�006 5 2 1 2 �s°„ 0 °' w - DO46& 5 2 1 2 )036 ✓ w 5DO 024 5 2 1 2 w — S 2 1121 z�� C N O m ✓ w SD() in 5 2 1121 � y � m p w a z z 6 ✓ w SDO 030 5 2 1 2 1- a M= F ,y z z 6 Ib ✓ w SDO 033 5 2 1121 R 1' hed De a. we aib�3a Received B Re Routine (quarterly) - AnaWcal Monitoring. results to https•//orolects mbakermm mm/PTI rlts6/Lab%ZCResults/Allltems asox R nquished y D te/I'ime Receiv try - _ On Ira Sample Temperature at receipt °C National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont "rr... Page I of 4 weather.gov Greensboro, Piedmont Triad International Airport' p , Enter Your "City, ST' or zip code u Go metric an espariol p Temperature ff) Wind Heat Pressure Precipitation (in.) a Time Wind Vis. Relative t (edt) (mph) (mi.) Weather Sky Cond. 6 hour Humidity Chill Index altimeter sea Air Dwpt (.F) (.F) (in) level 1 hr 3 hr 6 hr e Max. Min. (mb) 24 07:54 Calm 10.00 Overcast FEW007 70 68 70 68 93% NA NA 30.00 1014.9 OVC250 24 06:54 Calm 10.00 Overcast FEW007 69 67 93% NA NA 29.99 1014.3 OVC200 24 0554 SW 10.00 Overcast SCT007 68 67 96% NA NA 29.99 1014.2 3 OVC250 24 04:54 SW 10.00 Mostly FEW009 69 68 96% NA NA 29.96 1013.3 8 Cloudy SCT100 BKN250 24 0354 W 5 10.00 Overcast OVC007 69 68 96% NA NA 29.98 1013.8 24 0254 S 13 10.00 Overcast FEW003 69 68 96% NA NA 29.95 1012.8 SCT048 OVC090 24 01:54 S 9 10.00 Overcast SCT080 69 67 84 68 93% NA NA 30.00 1014.7 0.05 0.< OVC100 24 00:54 S 10 10.00 Thunderstorm SCT006 69 68 96% NA NA 30.04 1015.9 0.04 G 18 Light Rain BKN090CB OVC120 23 23:54 S 5 6.00 Thunderstorm BKN040CB 69 68 96% NA NA 30.06 1016.7 0.34 Light Rain OVC080 Fog/Mist 23 22:54 NE 5.00 Thunderstorm BKN011CB 71 67 87% NA NA 30.09 1017.8 14 G Light Rain BKN060 25 Fog/Mist 23 21:54 E 15 10.00 Mostly SCT065 74 65 74% NA NA 30.01 1015.1 Cloudy BKNO90 BKN120 23 2054 SE 7 10.00 Overcast SCT060 82 70 67% NA 86 29.95 1013.0 BKN100 OVC250 23 19:54 SE 9 10.00 Mostly SCT060TCU 84 71 93 84 65% NA 89 29.92 1012.0 Cloudy BKN150 BKN250 23 18:54 SW 10.00 Mostly SCT060TCU 92 68 46% NA 96 29.91 1011.4 8 Cloudy BKN120 BKN250 23 17:54 SW 10.00 Mostly FEW050 92 69 47% NA 97 29.90 1011.2 9 Cloudy SCT100 BKN250 23 16:54 SW 10.00 Overcast FEW048 91 70 50% NA 97 29.93 1012.1 0.01 0.01 9 SCT070TCU BKN200 OVC250 23 15:54 Vrbl 10.00 Overcast SCT065CB 91 69 49% NA 96 29.95 1012.8 7 BKNO95 OVC250 0.01 http://wi.weather.gov/data/obhistory/KGSO.html 6/24/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 2 of 4 23 1454 W 7 10.00 Light Rain BKN065TCU 88 69 54% NA 93 29.97 1013.4 BKN100 OVC250 23 1354 W 10.00 Overcast SCT045 90 69 90 77 50% NA 95 29.99 1014.1 10 OVC250 23 12:54 SW 10.00 Overcast FEW035 88 70 55% NA 93 29.99 1014.3 8 SCT180 OVC250 23 11:54 SW 10.00 Overcast FEW100 87 69 55% NA 91 30.01 1014.8 7 SCT180 OVC250 23 1054 Vrbl 10.00 Overcast FEW100 86 70 59% NA 91 30.03 1015.6 5 OVC250 23 09:54 W 8 10.00 Overcast FEW030 84 70 63% NA 88 30.06 1016.6 SCT100 SCT180 OVC250 23 08:54 W 8 10.00 Overcast OVC250 82 71 69% NA 86 30.03 1015.6 23 07:54 W 9.00 Overcast OVC250 77 72 77 75 85% NA 78 30.01 1014.9 10 23 06:54 SW 9.00 Overcast FEW200 76 71 85% NA 77 29.99 1014.4 10 OVC250 23 05:54 SW 9.00 Mostly FEW200 75 71 88% NA NA 29.99 1014.1 9 Cloudy BKN250 23 04:54 SW 10.00 Partly Cloudy SCT250 76 71 85% NA 77 29.98 1014.0 9 23 03:54 SW 10.00 Partly Cloudy SCT250 77 71 82% NA 79 30.00 1014.6 3 23 02:54 SW 10.00 Partly Cloudy SCT250 77 72 85% NA 78 29.99 1014.1 3 23 01:54 SW 10.00 Mostly BKN250 77 72 86 77 85% NA 78 30.00 1014.7 5 Cloudy 23 00:54 Calm 10.00 Mostly FEW070 78 72 82% NA 80 30.02 1015.1 Cloudy SCT110 BKN250 22 23:54 S 5 10.00 Partly Cloudy SCT065 81 72 74% NA 85 30.04 1015.9 SCT150 22 22:54 Calm 10.00 Mostly FEW075 83 72 70% NA 88 30.05 1016.2 Cloudy BKN150 22 21:54 S 3 10.00 Mostly FEW080 82 70 67% NA 86 30.04 1015.8 Cloudy SCT160 BKN200 22 20:54 Calm 10.00 Mostly SCT180 84 69 61 % NA 88 30.04 1015.8 Cloudy BKN250 22 19:54 W 6 10.00 Mostly SCT180 86 70 94 86 59% NA 91 30.02 1015.2 Cloudy BKN250 22 18:54 W 6 10.00 Mostly FEW040 88 65 46% NA 90 30.01 1015.0 Cloudy SCT150 BKN180 BKN250 22 17:54 NW 10.00 Mostly FEW040 91 65 42% NA 93 30.00 1014.6 12 Cloudy SCT150 BKN250 22 16:54 W 3 10.00 Mostly FEW040 91 65 42% NA 93 30.01 1014.9 Cloudy SCT060 BKN250 22 15:54 10.00 91 65 42% NA 93 30.02 1015.2 http://wI.weather.gov/data/obhistory/KCiSO.html 6/24/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 3 of 4 NW Mostly FEW050 10 Cloudy BKNO60 BKN220 22 14:54 NW 10.00 Mostly FEW055 92 64 40% NA 94 30.03 1015.5 10 G Cloudy BKN065 20 BKN250 22 1354 NW 10.00 Mostly FEW048 90 65 92 73 44% NA 92 30.04 1015.8 12 Cloudy BKNO60 BKN250 22 1254 NW 10.00 Mostly BKN048 88 66 48% NA 90 30.05 1016.4 8 G Cloudy BKN250 16 22 11:54 W 10.00 Mostly SCT055 87 65 48% NA 89 30.05 1016.3 10 Cloudy BKN250 22 1054 W 7 10.00 Mostly FEW045 84 65 53% NA 86 30.04 1015.9 Cloudy BKN250 22 09:54 NW 10.00 Mostly BKN250 82 66 58% NA 84 30.03 1015.6 8 Cloudy 22 08:54 W 5 10.00 Mostly BKN250 78 67 69% NA 80 30.04 1015.9 Cloudy 22 07:54 W 5 10.00 Mostly BKN250 73 68 73 69 84% NA NA 30.02 1015.4 Cloudy 22 06:54 SW 8.00 Partly Cloudy SCT250 70 67 90% NA NA 30.00 1014.7 5 22 05:54 S 3 10.00 A Few Clouds FEW250 70 67 90% NA NA 29.98 1014.1 22 04:54 SW 10.00 Fair CLR 71 67 87% NA NA 29.99 1014.2 5 22 03:54 W6 10.00 Fair CLR 73 67 81% NA NA 29.98 1014.0 22 0254 W 8 10.00 Fair CLR 72 67 84% NA NA 29.97 1013.6 22 01:54 SW 10.00 A Few Clouds FEW250 72 67 83 71 84% NA NA 29.97 1013.7 7 22 00:54 SW 10.00 Partly Cloudy FEW100 73 67 81% NA NA 29.98 1014.0 5 SCT250 21 23:54 SW 10.00 Mostly FEW055 75 67 76% NA NA 29.98 1013.9 6 Cloudy SCT100 BKN250 21 22:54 SW 10.00 Mostly FEWO50 76 67 74% NA 77 30.00 1014.7 7 Cloudy BKN100 BKN250 21 21:54 W 5 10.00 Overcast FEW050 78 65 64% NA 80 30.00 1014.5 BKN100 OVC180 21 2054 W 5 10.00 Overcast FEW045 82 60 47% NA 82 29.98 1014.0 BKN070 OVC200 21 1954 SW 10.00 Overcast FEW050 83 59 92 83 44% NA 83 29.97 1013.7 7 SCT100 OVC250 21 1854 SW 10.00 Overcast FEWO60 85 59 42% NA 85 29.96 1013.4 9 BKN100 OVC250 21 17:54 SW 10.00 Overcast BKN075 87 60 40% NA 87 29.96 1013.3 9 OVC250 21 16:54 SW 10.00 Overcast BKN065 89 58 35% NA 88 29.97 1013.4 16 G OVC250 22 hitp://wl.weather.gov/data/obhistory/KGSO.htmi 6/24/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 4 of 4 21 15:54 SW 10.00 Mostly 16 G Cloudy 23 21 1454 SW 10.00 Mostly 14 G Cloudy 18 21 13:54 W 10.00 Mostly 10 Cloudy 21 12:54 W 8 10.00 Overcast 21 11:54 SW 10.00 Overcast 9 21 10:54 SW 10.00 Overcast 7 21 09:54 SW 10.00 Overcast 8 21 0854 SW 10.00 Overcast 8 D a Time Wind Vis. Weather t (edt) (mph) (mi.) e National Weather Service Southern Region Headquarters Fort Worth, Texas Disclaimer FEW060 91 59 34% NA 90 29.96 1013.3 BKN250 FEW055 91 60 35% NA 90 30.00 1014.4 SCT095 BKN250 FEW060 86 63 88 71 46% NA 87 30.04 1016.0 SCT110 SKN200 BKN250 FEW060 86 63 46% NA 87 30.06 1016.7 SCT110 BKN200 OVC250 FEW110 85 63 48% NA 86 30.08 1017.2 OVC250 FEW150 81 64 57% NA 83 30.07 1017.0 OVC250 FEW150 78 63 60% NA 80 30.07 1017.1 OVC250 FEW045 75 62 64% NA NA 30.07 1017.2 OVC250 Max. Min. Air Dwpt Relative Wind Heat meter altimeter sea level 1 hr 3 hr 6 hr Sky Card. 6 hour Humidity Chill Index (in.) (mb) ( F ) F Temperature (°F) Pressure Precipitation (in.) Back Last Modifed: Febuory, 7 2012 to previous page Privacy Policy http://wi.weather.gov/data/obhistory/KGSO.html 6/24/2016 hC6-aDD52' Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Performing Test Research & Analytical Laboratories, Inc. Comments: Storm eater Effluent A Pilot Environmental Project f/Opgr in Responsible Charge RAL k 14194-01 EaboraWry Supervisor MAIL ORIGINAL TO: Div. Of WatearlQual tyes B N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina CeriodaDhnia Chronic Pass/Pail Reoroduction'roxicitv,rest CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D)cad Effluent% TREATMENT 2 ORGANISMS N Young Produced Adult (L) ive (D) ead pH M Control Treatment 2 Control Treatment 2 Calculated t Tabular t Reduction 1 2 3 4 5 6 7 8 9 10 11 12 Control CV %a control organisms produci�od (Mortality expressed as %, combining replicates) l st sample 5 I e a n r d t Ist 2nd sample f I e a n d I 2nd 2 PASS FAIL I I Check One I 01 / 23 / 16 Collection (Startl Date Sample 1 01122/16 Sample 2 Sample Type/Duration Sample I Sample 2 Grab Comp. Duration X Hardness (mgA) Spee.Cond.(pmhos) Chlorine(mgll) Sample temp, at receipt 0 % 6.25 % 12.5 % 25 % 50 % 100 0 % 0 % 1 0 % 0 %1 5 %1 5 % % % % LC50 = >I00% % Method of Determination .. *'................................. 95%Confidence Limits Moving Average Pmbit ........................... %- ........................ % Spearman Karber O Other ............_'X Organism Tested Ceriodaphnia dubia Damtlon (hrs) 24 Copy D WQ form AT-1 (3187) rev. 11,95 _N C o' Q, 9 0 tl 0.02 1.9 Concen ation Monolity Nata Plcas'c Complete This Sttrion Also SturVcnd StarVend 6.94 6.87 Control 8.6 7.9 6.86 6.79 High 7.7 1 TO nH Cone. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 LaboratoryPerformin Pest Research & Analvtical Laboratories, Inc. Comments.: StormWater Effluent g' cot X A Pilot Environmental Project Si am o 0pµr�!Of m onsible Charge RAL M 14194-02 X 'yFb//i/ Sign a "borat Supervisor, g MAIL ORIGINAL TO: Div. Of Quality Branch N.C. DENR 1621 Mail Service Center Ralei{;h, NC 27699-1621 North Carolina Ceriodanhnia Chronic Pass/Fail Reproduction Toxicit 'test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 II 12 k Young Produced Adult (L) ive (D) ead Effluent% TREATMENT 2 ORGANISMS 4 Young Produced Adult (L) ive (D) cad Control pH Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 IA sample s t c u n d t Istsample F1 t c u n r d 2nd sample s c a n d t Istsample Istsample 2nd Control D.O. Treatment 2 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicatcs) Com fete This For Either'I'cst Test Stan Date 01 / 23 / 16 Collection (Start) Date Sample 1 01/22/16 Sample 2 SMI)Ie Iype/Dumtion — o Grab Comp. Duration a O T A x 0 % 6.25 % 12.5 °" 25 % 50 % 100 % 0 % 0 % 1 0 % 0 % 10 % 5 % I % % % LC50= >100% % Method of Determination ........... L'i'.... _............... 95%Confidence Limits 's.Moving Average Probit ....%" ........................% Spearman Karbn Other .............X ....................... Organism Tested Ceriodaphnia dubia Dumu°a (hrs) 24 Copy DWQ form AT.] (3187) rev. 11195 Mor[ality Note: Rleau Complete 7 his amian Alsa StarUrnd Start/rnd 6.94 6.87 Convol 8,6 7.9 7.14 7.01 Hilt 8.1 7.9 pit Canc. U.O. LC50= >100% % Method of Determination ........... L'i'.... _............... 95%Confidence Limits 's.Moving Average Probit ....%" ........................% Spearman Karbn Other .............X ....................... Organism Tested Ceriodaphnia dubia Dumu°a (hrs) 24 Copy DWQ form AT.] (3187) rev. 11195 Mor[ality Note: Rleau Complete 7 his amian Alsa StarUrnd Start/rnd 6.94 6.87 Convol 8,6 7.9 7.14 7.01 Hilt 8.1 7.9 pit Canc. U.O. Organism Tested Ceriodaphnia dubia Dumu°a (hrs) 24 Copy DWQ form AT.] (3187) rev. 11195 Mor[ality Note: Rleau Complete 7 his amian Alsa StarUrnd Start/rnd 6.94 6.87 Convol 8,6 7.9 7.14 7.01 Hilt 8.1 7.9 pit Canc. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 .... performing Test Research 8t Analytical Laboratories, Inc. Comments: Stormwater Effluent A Pilot Environmental Project f p i esponsible Charge RAL # 14194-03 Laborlitory Supervisor MAIL ORIGINAL TO: Div.. Of Water QitSciencesBranch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaahnia Chronic PmVFail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) ead Effluent% TRFATMFNf 2 ORGANISMS # Young Produced Adult (L) ive (D) cad pH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 M a t e a n r d t I sl sample s I c a n r d I 2nd Sample a t e a n d t Ist sample Ist sample 2nd sample Control D.O. "Treatment 2 LC501Acute Toxicity Test (Mortality expressed as %, combining replicates) Complete This For Either Test Test Start Date 01 / 23 / 16 Collection (Start) Date Sample 01/22/16 Sample Sample Twc[Duration a Grab Comp, Duration 0 % 6.25 % 12.5 % 25 % 50 % 100 % % 0 % 0 % 1 0 % 0 % 0 % 0 % % LC50 = >100% %Method of Determination ......................................... 95% Confidence Limits Moving Average Probit ...........................%- ........................%% Spearman Karber Other ..........._X............ Organism Tested Ceriodaphnia dubia Duration(hrs) 24 Copy DWQ form AT-1 (3187) rev. 11195 Concentration LC50 = >100% %Method of Determination ......................................... 95% Confidence Limits Moving Average Probit ...........................%- ........................%% Spearman Karber Other ..........._X............ Organism Tested Ceriodaphnia dubia Duration(hrs) 24 Copy DWQ form AT-1 (3187) rev. 11195 Concentration Organism Tested Ceriodaphnia dubia Duration(hrs) 24 Copy DWQ form AT-1 (3187) rev. 11195 Concentration Morality Note: F'leas< Complcm'fhis Section Also $tartJrnd Start/end 6.94 6.87 Cantnd 8.6 7.9 7.20 7.09 gh 8.1 8.0 pH Conc. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Dale 01/24/16 Perforrning,rest Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent I A Pilot Environmental Project f 9peµµor " Re nsible Charge RAL S 14194-04 Fl-aborato 'upervisor MAIL ORIGINAL TO: Div. Of Water QlSciences rant N.C. DL"NR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaoknia Chronic Pass/Fail Renroduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 II 12 # Young Produced Adult (L) ive (D) ead Enluent% TREATMENT 2 ORGANISMS g Young Produced Adult (L) ive (D) cad Control pH Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 I St sam le s t a a n r d t I St sample ISt sample 2nd Control D.O. Treatment 2 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates) Com lete This Far Either Test 'Pan Dat est Ste of 1 23 / 16 Collection (Start) Date sample 1 01/22/16 Sample 2 Sample Tyne/Duration _ N F c Sample 1 S Sample 2 c Hardness (mg/I)J93 Spec.Cond.(µ nitu)TChlorine(mg4)Sample temp. at receipt Cimb Comp. Duration X 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % 0 % 0 % 0 % 0 % 0 % 0 % % % LC50 a >I00% % Method of Determination ......................................... S 6 95%Confidence Limits Moving Average Pmbil ........................ % Spemman Karber Other ............_X Organism Tested Ceriodaphnia dubia Duration (hrs) 24 Copy UWQ fops A'i-1 (3/87) mv. I1/95 Concentration Mortality Note'. Pleve Complde'ITis Sccsion Also SlarUcmd SlarUcnd 6.94 6.87 Canuol 8.6 7.9 7.18 7.I0 Fligh 8.0 7.8 pH Conc. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Laboratory Performing Test Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent X A Pilot Environmental Project Signal /OpQ in R onsible Charge RAL H 14194-05 X ! —K// Suture Laboratory Supervisor MAIL ORIGINAL TO: Div' Of Water Quality s Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Pail Rcproduction'I'oxicity "Pest CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad Effluent% I TREATMENT 2 ORGANISM: # Young Produced Adult (L) ive (D) ead Control ptl Treatment 2 1 2 3 4 5 6 7 8 9 10 I I 12 I st sample s I C a n r d t I St sample I St sample 2nd sample Control D.O. Treatment 2 FE LC50/Acute Toxicity Test (Morality expressed as %%, combining replicates) 01 / 23 / 16 Collection (Start) Date Sample 1 0122/16 Sample 2 Sample TyTe/Duratinn Sample I Sample 2 Club Comp. Duration X N S � [1 v v. c ? N o — _ Hardness (mgA) 48 M Spec.Cond.(µmhos) 193 119 Chlorine(mg/1) ® 0.03 Sample temp, at receipt 1.9 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % 0 %1 0 % 1 0 %1 0 %1 0 %1 0 % LC50= >100% % Method of Determination 95°/%ConfidenceLimits Moving Average Proba ........................%% Spearman Karber Q Other ...........X Organism Tested Ceriodaphnia dubia Duration (his) 24 Copy D WQ form AT-1 (3/87) rev. 11/95 ::oncttmtration Mortality Note: Please Complcte'fhis Section Also Start/end StarUend 6.94 6.87 Conuol 8.6 7.9 7.01 7.00 tlfgh 86 1 8.4 pH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Performing Test Research & Analytical Laboratories, Inc. Comments: Slortnw ester Effluent A Pilot Environmental Project 4OTttt Re nsible Charge RAL # 14194-06 L•a�iy Supervisor MAILORIGINAL TO: EnvironmentaliOtQ;Sciences tone N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity "test Chronic Tat Results CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 II 12 Calculated t Tabular t # Young Produced Reduction Adult (L) ive (D) ead] %Mortality Avg. Re rod. Control Control Efflumt% Treatment 2 Treatment 2 TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV PASS PAIL # Young Produced %control organi Adult (L) ive (D) cad ��ms ��s ��ddbbd producing 337° Check One pH Control Treatment 2 2nd sample s I C a n r d I Ist Sample Ist sample 2nd sample Control [1] E] P] U.O. Treatment Z LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates) 01 / 23 16 Collection (Start] Uate Semple 01/22116 Sample2_ Sample Type/Duration Grab Camp. Duration =' n R T O Sample I X R O Sample 2 0' 0 0 _ Hardness Spec.Cond.(pmhos) Chlarina(mg/1) Semple temp. (mg/I) at receipt 46 193 IIS 0.04 1.9 0 % 6.25 % 12.5 % 25 % 50 % 100 % % 0 % 0 % 1 0 % 0 % 10 % 15 % LC50@ >I00% % Method of Determination 'e'ri.........snit.................. B Average '. 95%Confidence Limits Moving Aver c Q Prabit O °h. ........................ % Spearman Karber Other ............ X............. Organism Tested Ccriodaphnia dubia Dumdoo (his) 24 Copy DWQ futm AT.1 (3187) rev. 11195 Concentration Mortality Nom; Please Complete This Section Also Start/end Stwu`md 6.94 6,87 Control 1 8.6 7.9 6.89 6.88 High 8.2 1 8.1 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Performing Test Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent A Pilot Environmental Protect f O rptgr in onsible Charge RAL 414194-07 f Laabo ry Supervisor MAIL ORIGINAL TO: North Carolina Cerindanhnia Chronic Pass/Pail Reproduction Toxicity Test CONTROL ORGANISMS 9 Young Produced Adult (L) ive (D) ead Effluent% TREATMENT 2 ORGANISMS # Young Produced Adult (L) ive (D) ead PH Control Treatment 2 Div. Of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 1 2. 3 4 5 6 7 8 9 10 11 12 H 11 11 11 11 1 11 11 1 2 3 4 5 6 7 8 9 10 11 12 Ist sample Ist sample 2nd sample Control U.O. Treatment 2 LC50/Acute Toxicitv'fest (Mortality expressed as %. combining replicates) Cora leieThis For Either Test 'rest Stan Date 01 / 23 / 16 Collection (Stan) Uatc Sample) 0122/16 Sample2 Samnle'ryne/Duration � N Grab Comp. Duration Sample I X Samplc 2 y f. Hardness (mg/1) 48 Spec.Condtjumhos) 193 114 Chlorinc(mgA) 0.03 Sample tlmlm p. at receipt 1.9 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % % 0 % 0 % 1 0 % 0 % 0 % 0 % % % % LC50= >I00% % Method of Determination 95% Confidence Limits Moving Average Probit ........................... %- ........................ % Spearman Karber Other X Organism Tested Ceriodaphniadubia Dumnon(hrs) 24 Copy D WQ form AT-1 (3/87) rev. 11195 Concentration Mortality Note: Please Complc¢ This Section Alsa StarVend Starlend 6.87 Control 8.6 7.9 �6981� 6.90 High 8.5 8.2 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Piedmont Triad Airport Authority NPDES#NC S000509 Pipe# IS #06 County Guilford Performing Test Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent A Pilot Environmental Project fop onsible Charge RAL # 14194-08 t1t Laboratory Supervisor MAILORIGE% AL TO: Environmental Sciences Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaahnia Chronic Pass/Fail Rcnroduction Toxicitv'fest CONTROL ORGANISMS # Young Produced (Adult (L) ive (D) cad l EfPuento/o TREATMENT 2 ORGANISMS # Young Produced Adult (L) ive (D) ead PH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t Tabular t % Reduction %Mortality 1 2 3 4 5 6 7 8 9 10 11 12 Control CV %1 contmlorganisms producig 3rd br lJood IStsample s t c a n r d t I sl sample s' l e a n r d I 2nd sample s t C n n d t FAIL [yT44. SUM malt This For Either Test 'rest Start Date 01 / 23 / 16 Collection (Start) Samplcl 01221162116 Snmple2 Sample Tvne/Dwation Grab lComml Duration sample I ( X 1 St sample 1st sample 2nd sample ( Sample 2 I f ControlHardness (mg/I; D.O.EH FE PA Spcc.Cond.(pmhos) Treatment 2 Chlorine(mgfi) LC50/Acute Toxicity Test Sample temp. at receipt (Mortality expressed as %, combining replicates) 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % % •/ 0 % 0 % 1 0 % 0 % 0 % 0 % % % % LC50= >I00% % Method of Determination 95% Confidence Limits Moving Average Probit ...........................%' ........................ % Spearman Karba Other ............_X. Organism Tested Ceriodaphnia dubia Duration (hts) 24 Copy DWQ t'onn AT-1 (3187) mv. 11195 N Z e a c — c' v+ v: 48 ' ..' � 193 1 113 1 1.9 Concentration Mortality Nam: Please Complete This Section Alsa Starvend Start/end 6.94 6.87 Connol 8.6 7.9 6.89 6.80 High 7.8 1 T6 pit Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Laboratory Performing Test Supervisor Research r&. Analytical Laboratories, Inc. Charge Date 01/24/16 IS #07 Comments: Storrawater Effluent A Pilot Environmental Project RAL # 14194-09 MAILORIGINAL TO: Ditv.lronmentOf W ter Quality l Sciences Branch N.C. DENR 1621 Mail Service Center Raleiph, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity'1'est CONrROL ORGANISMS 1 2 3 4 5 6 7 8 .9 _-- 10 II 12 # Young Produced FT1411 Adult (L) ive (U) ead Effluent% TRFA rMENT 2 ORGANISMS 4 Young Produced Adult (L) ive (D) cad PH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 I A sample I st sample 2nd sample 4 5 5 t C C t C a n a a a n r d r d r d I t 1 st sample I st sample 2nd sample Control P] D.O. 'I'rcatmcnt 2 EEL LC50/Acute'l'oxicity Test (Mortality expressed as %, combining replicates) omplete This For Either Test I Test Start Date 01 / 23 / 19 Sample lSta01/22J16c Sample Samplc *1 ygdDuration Sample 1 Sample 2 1 Grab lComo.l Duration Hardness (mg/1) Spec.Cond.(µmhos) Chlorine(mg(l) Sample temp. at receipt 0 % 6.25 % 12.5 % 25 a5o % 100 % 0 % 0 % 1 0 % 0 % 0 % 0 % LC50= >100% % Method of Determination ......................................... 95%Confidence Limits Moving Average 8 Probit ...........................%- ........................% Spearman Karber Other ..........._X............. Organism Tested Ceriodaphnia dubia Duration(hrs) 24 Copy DWQ form AT-1 (3187) rev. 11/95 Concentration Mortality 6 w a: o' 1.9 T Note; Please Completc'I'his Section Alsp Star/end Start/end 6.94 1 6.87 1 Control. 1 8.6 F 7.9 6.96 16.91 High 1 8.0 1 7.9 pH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Piedmont Triad Airport Authority NPDES#NC S000508 Pipe# 1S #08 County Guilford Performing Test Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent A Pilot Environmental Project Snz in Re ponsible Charge RAL # 14194-10 f Lab�omttiryry Supervisor MAIL ORIGINAL TO: Div' Of Wate Quality Sciences s Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaahnia Chronic Povas/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 II 12 # Young Produced F:FFFI'' ''1 11 Adult (L) ive (D) ead Effluent% I TREATMENT 2 ORGANISM # Young Produced Adult (L) ive (D) cad Control pH 'treatment 2 D.O. Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 (Mortality expressed as %, combining replicates) 2nd sam le s 1 c a n r d I Complete This For Either Test Test Start Date 01 / 23 / 16 Collection (Stan) Date Sample 1 01/22/16 Sample 2 Sample Tyne/Duration _ N Grab Comp, Duration", Sample I x C T C E O Sample 2 y 6 ,. n Hardness (mg/I) 48 Spee.Cond.(µmhps) 193 159 Chlorine(mg/1) 0.03 Sample temp. at receipt 1,9 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % % 0 % 0 % 1 0 % 0 % 1 0 0 % % LCSO— >I00% % Method of Determination ..'ne*e....Limmi.... i.................... 95%Confidets Moving Average Prohit ...........................%- ........................% Spearman Karbet Other .............X Organistrilested Ccriodaphniadubia Durcaon(hrs) 24 Copy DWQ form AT-1 (3/87) r , 11195 Concentration Mortality N°tc: Ple°sc C°mPlac'I'his Section Also Start end _ StanIcnd 6,94 6.87 1 Control 1 8.6 7.9 7.05 7.01 High 8.3 1 8.0 PH Cone, D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Facility Piedmont Triad Airport Authority NPDES#NC S000508 Pipe# IS #010 County Guilford Laboratory Performing Test Research 8. Analytical Laboratories, Inc. Comments: Stormwater Effluent X A Pilot Environmental Project Signatur f.Op to Re ible Charge RAL # 14194-11 X /) P5 Si�e of aborat upervisor MAIL ORIGINAL TO: EnvironmentalitQualiSciences Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnio Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS I 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) ead Effluent% TREATMENT 2 ORGANISMS # Young Produced Adult (L) ive (D) cad PH ►• Control Treatment 2 Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 Cum fete This For Either Test •rest Start Date Ist sample 1st sample 2nd sample 01 1 23 16 CpStart) Date Sample 01/22/16 Sample Smote 3'vpc[Dmation s S s _ N 1 C t C t C T a n n n Grab a n Comp. Duration (! c r r d r d r d Sam p le 1 X G �` — N G 3 p 1st sample 1st sample 2nd sample Sample 2 Hardness (mhos) 19 (` " FR 1E Ell SpecCond.(µmhos) 193 237 Chlorine(mg/1) 0.02 Sample temp. at receipt . 1.9 (Mortality expressed as %, combining replicates) 0 011 6.25 % 12.5 % 25 % 50 % 100 % % % % % 0 % 0 % 1 0 % 0 % 0 % 0 % % % % % LC50 = >I00% % od Methof Determination ......................................... 95%Confidence Limits Moving Average �8 Probit ... /° ........................ % Spearman Karber Other X Organism Tested Ceriodaphnia dubia Dumtion(tus) 24 Copy DWQ form AT-1 (3/87) my, 11/95 Concentration Mortality Note: Please Complete This $Ccppn Also Start/end _ Startlend 6.94 6.87 Convol 8.6 7.9 6.98 6.91 High 8.6 1 8.5 pH Cone. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/24/16 Performing rest Research & Analytical Laboratories, Inc. Comments: Stormwater Effluent A Pilot Environmental Project fr9pc r in onsible Charge RAI, # 14194-12 F,((L''abor ry Supervisor MAIL ORIGINAL TO: Environmental. OQuality Brant N.C. OENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodanimia Chronic Pass/Fail Reproduction Toxicity lest Chronic Test Results CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t # Young Produced o 'Tabular t /o Reduction Adult (L) ive (U) cad %Mortality Effluent% TRFAI MENT 2 ORGANISMS # Young Produced Adult (L) ive (D) cad PH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 Control CV control organisms producing 3rd Istsam Ic s t e a n r d I 1st sample s t e a n r d I 2nd sample s e a n d t PASS FAIL Check One 01 / 23 / 16 Collection (Stan) Date Sample 1 01/22/16 Sample 2 Samnlc Tvpe/Duration I Grab I Comp.1 Dumtion I Sample I I K 1 St sample Ist sample 2nd sample I Samplc 2 Control Hardness (mg/I; U.O. Spec.Cond.(Pmhos) Treatment 2. CNorine(mp/1) LC50/Acute'roxicity Test Sample temp. at receipt (Mortality expressed m %, combining replicates) 0 % 6.25 % 12.5 % 25 % 50 % 100 0 % 0 % 1 0 % 0 % 0 % 0 % % % LC50 = >100% % Method of Detrnnination ......................................... 95%Confidence Limits Moving Average Probit ........................... %- _...................... % Spearman Karba Other ,........... X Organism'rested Ceriodaphniadubia Duradon(hm) 24 Copy DWQ form A'LI (3187) rev, 11195 N p n N J A c = c a K a o rt n 1.9 Concentration Mortality No[s Please Complete This SC[[I00 AI30 Start/cnd Start/end 6.94 6.87 Control 8.6 7.9 7.15 7,10 High 7.6 1 7.6 all Cona U,O. RESEARCII & ANA YTICAI. UoRATOR1ESr INC. Analytical / Process Consultations CHAIN OF CUSTODY RECORD Phone (336) 990-2841 - Water/Wastewater Misc. Company Pilot Environmental, Inc. Job No. PTAA Purchase Order E< z - m .7 S T St i a y m 6 9' �' !j ti o 0 a. `t h m O s i✓ c! `I 9 o 0 o: , S 7 0 e: , m z O A , z S 11 Street Address PO Box 128 Project PTIA NPDES Compliance (NMP-EH-) City, State, Zip - Kernersville, NC 27285 Sampler Name (Please Print) B.J. Lineback 336.708.4655 C Contact BJ.Lineback Phone 336.310.4527 Sampler Signature o w Sam le NnmDer Date Time d 6 (j a I° Ttmp °C gq, CL CWoria mov or Sa Matrix r Sample Location / LD. O CSO Z (Lob Use Only) Requested as 0 L5 a ✓ w SD0004 1 1 o v O r en o L N S ✓ w SL�'SBt3.886-- 1 1 A5 ✓ w g_�L- WG 16A. I y q�1-O t3pS ✓ w SDO024 1 1 NS ✓ w rn o Q z F o Z u > _ o0 ✓ w 1 1 111214 -OSS B ✓ w SDO030 1 1 t35$ ✓ w SDO033 1 11 1a -Q 30 '� w IS #01 1 1 ,� m w 47o a ✓ w IS #02 1 1 I e100 ✓ w IS #05 1 1 ✓ w IS #06 1 1 H t t4 o d o m m 0 u O t N a? •-t=_ w u N n 15 ✓ w IS #07 1 1 d ✓ w Is #08 1 1 -( / 5D ✓ w Is #010 1 1 - a l•r•f5 ✓ w Is#011 1 1 'nquished B Da ime Received By Remarks Deicing Event (4 b/w OR -Apr) Analytical Monitoring. Please post results to F rr sects mbakercom mm/MA/lists/LobYO 1Resu111MItems asox Re o ed By AuMme Received By On Ice Sample Temperature at receipt 1.4 °C .APT/ PIEDMONT 7nW INTER WIIWIAL AINPW Storinwater Discharge Outfall (SDO) Qualitative Monitoring Report NPDES Permit: NCS000sog Page 1 of 2 �i a ne at lnvesh ator. g 336.708.4655 ' Date @NPDES sSeason''Penod`- Event-:�"Tier�_�''^'^ I��.. 2 6 I 2 fo"rgurdonceohcomplenrigthLs r u cT 4 ��*� x ? portion ofthisform vLsu', n z f. r c h�(R,/�norral.ncdenrarp%web/—.,.�-«rN'€�-"_---'- oo ,, �i odes srormuaier/ t� o� y' o o v >'`=w <°e N\-1Fi _ \ x �� " ter v WVW0, �� � �,r« c. E;y`..o s wsb',. �`s u _:O a�.': u LL i n.r °= O °w` ..,60 v Qx: i " ° + ° uanhtattve Data to be collected s =z during Routine (P)land Deidiig a� r )*� sA Event(E) Sampling `(PRSDOonty)(PRSDOonty) .�. lE !S&RSDO f E=1S ort1 E'IS onl = "` :Structure` ..r .JyS•C SDO Structure _ Tlme Condnlon ;Flow pH zrTurbldlty-= 0O ..a, a(6' 004 006 54"RCP 46 " RCP (S��I �� 1 a) t'j c a 16A riprap Swale 1153 ( AL ��e1F :w 024 026 027 030 033 36 "RCP 36 " CMP 54 " RCP 24 " MP 42 "RCP T A I t A) AJ (a.-73 m s6' z m 'n / 3'Iaa / tj 3a 5 ) 3 / 3S6 ( / l 1&K K tJ t l N t l t Al A I t !li IS Location „ Tune ; 'Flow :v H t " Turbldlt #01 Brush Creek /'l3 [[ . 83 _ . � (0. 37 — g 3 #02 Brush Creek "� /5 y 15 J L, t�/ (� •q Z of #05 Brush Creek k7L) f7. 3 .8 rl • col<cv8 #06 Brush Creek t�7"`�j' l ln-S earn efcing�Fven[ boratory Arlaly s: 7.01 10, 5f 7C . ICJ UT to #07 Horsepen �_ as `( Ac to rcr (/ (� .5 , 0 ( UT to #08 Horsepen UT to #10 Horsepen 1a a- ` ) Y .7-5 g, 3 f q T 8 l Post completed slgnedform to: httos://oroleminbakercora.corn/pn A/Lists/HeldWOResults/NRtems.osox & . 77 35 Horsepen #11 Creek (�J.L -t (�) g� ? S • 4 J g By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page I of 4 Enter Your "City, ST or zip code Go metric en espanol D Temperature (°F) Pressure Precipitation (in.) Time Wind Weather Sky 6 hour Relative Wind Heat Index sea t t lest) (mph) (mi. (mi.) Cond. Air Dwpl HumidityChill ("F) ("F) altimeter 1 hr 3 hr 6 hr e Max. Min. (in) (mb) 23 0954 NW 10.00 Overcast OVC033 28 19 69% 18 NA 29.59 1002.9 12 23 08:54 N 9 10.00 Overcast SCT033 28 19 69% 19 NA 29.58 1002.5 OVC043 23 07:54 N 9 G 9.00 Overcast OVC043 26 19 75% 17 NA 29.57 1002.2 18 23 06:54 N 9 G 9.00 Light OVC042 25 20 25 23 81% 16 NA 29.57 1002.1 0.01 17 Snow 23 05:54 N 12 2.00 Light FEW012 24 21 88% 13 NA 29.55 1001.6 0.01 G 17 Snow OVCO26 Fog/Mist 23 0454 N 9 G 2.50 Light FEW010 23 20 88% 13 NA 29.55 1001.4 16 Snow OVC033 Fog/Mist 23 03:54 N 12 1.50 Light FEW011 23 20 88% 11 NA 29.54 1001.1 G 16 Snow BKNO18 Fog/Mist OVC031 23 02:54 N 12 3.00 Light OVC012 23 20 88% 11 NA 29.54 1001.3 G 20 Freezing Drizzle Fog/Mist 23 01:54 NE 10.00 Light OVC014 23 19 85% 11 NA 29.56 1001.7 14 G Freezing 20 Drizzle 23 00:54 NE 9.00 Light OVC014 23 18 23 22 81% 11 NA 29.56 1002.0 0.1' 14 G Freezing 30 Drizzle 22 23:54 NE 9.00 Light OVC014 23 18 81% 10 NA 29.59 1002.9 15 G Snow 31 22 22:54 NE 9.00 Light BKNO14 22 19 89% 8 NA 29.63 1004.1 16 G Snow OVC038 24 22 21:54 NE 6.00 Light BKNO16 22 19 89% 8 NA 29.64 1004.5 0.11 18 G Freezing BKN029 26 Drizzle OVC038 Fog/Mist 22 20:54 NE 0.50 Light OVC012 22 20 92% 7 NA 29.69 1006.2 0.02 20 G Freezing 25 Drizzle Fog/Mist 22 19:54 N 8 0.50 Light OVC009 23 21 92% 14 NA 29.74 1007.9 0.09 Freezing http://wl.weather.gov/data/obhistory/KGSO.htmi 1 /23/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont "rr... Page 2 of 4 Rain Fog/Mist 22 18:54 N 13 0.50 Light OVC009 23 21 24 23 92% 11 NA 29.72 1007.3 0.19 0.33 Freezing Rain Fog/Mist 22 17:54 NE 1.00 Light OVC009 23 21 92% 8 NA 29.69 1006.4 0.03 20 G Freezing 25 Rain Fog/Mist 22 1654 NE 7.00 Overcast OVC009 23 20 88% 7 NA 29.73 1007.6 23 G and 31 Breezy 22 1554 NE 1.50 Light OVC012 24 21 88% 11 NA 29.77 1009.0 0.01 0.11 17 G Freezing 28 Rain Fog/Mist 22 14:54 NE 1.00 Light SCT012 23 20 88% 9 NA 29.82 1010.7 0.03 18 Snow OVC018 Fog/Mist 22 1354 NE 1.00 Fog/Mist SCT010 23 21 92% 11 NA 29.88 1012.9 0.07 14 G OVCO23 22 22 12:54 NE 1.50 Fog/Mist BKN023 23 20 24 23 88% 10 NA 29.95 1015.0 0.09 0.34 16 G BKN031 26 OVC055 22 11:54 NE 1.25 Fog/Mist SCT009 23 20 88% 11 NA 30.03 1017.9 0.09 14 G OVCO29 22 22 10:54 NEB 0.75 Light SCT009 23 21 92% 14 NA 30.10 1020.1 0.04 Snow OVCO25 Fog/Mist 22 09:54 NE 0.75 Light SCT010 24 21 88% 13 NA 30.12 1020.7 0.04 0.12 12 Snow BKNO14 Fog/Mist OVCO23 22 0854 NE 1.50 Overcast FEW007 24 22 91% 16 NA 30.10 1020.2 0.03 OVC014 22 0754 NE 4.00 Light BKNO09 24 21 88% 11 NA 30.08 1019.6 0.05 17 Freezing OVC060 Rain 22 0654 E 16 0.75 Light VV012 24 22 31 24 91% 11 NA 30.13 1021.3 0.04 0.08 Snow Fog/Mist 22 0554 E 15 1.00 Light VV013 25 22 88% 13 NA 30.18 1022.6 0.03 G 21 Snow Fag/Mist 22 0454 E 13 3.00 Overcast BKN034 28 18 66% 17 NA 30.20 1023.2 0.01 OVC045 22 03:54 E 9 9.00 Light BKN050 30 16 56% 22 NA 30.20 1023.2 Snow OVC070 22 02:54 E 10 10.00 Overcast OVC090 31 17 56% 22 NA 30.18 1022.6 22 01:54 E 8 10.00 Overcast BKN110 31 18 59% 24 NA 30.18 1022.6 OVC200 22 00:54 E6 10.00 Overcast SCT110 31 19 34 29 61% 25 NA 30.20 1023.3 BKN140 OVC200 http://wl.weather.gov/data/obhistory/KCiSO.htmi 1 /23/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro. Piedmont Tr... Page 3 of 4 21 23:54 E 6 10.00 Mostly BKN150 29 19 66% 23 NA 30.21 1023.5 Cloudy BKN200 21 22:54 NE 3 10.00 Mostly SCT150 31 18 59% NA NA 30.21 1023.7 Cloudy BKN250 21 21:54 Calm 10.00 A Few FEW200 31 18 59% NA NA 30.23 1024.3 Clouds 21 2054 E 3 10.00 A Few FEW200 32 17 54% NA NA 30.22 1024.2 Clouds 21 19:54 E 3 10.00 Partly FEW180 34 18 52% NA NA 30.23 1024.4 Cloudy SCT210 21 18:54 E 5 10.00 Partly SCT210 34 18 42 34 52% 29 NA 30.22 1024.0 Cloudy 21 1754 E 5 10.00 Partly SCT230 37 17 44% 33 NA 30.23 1024.3 Cloudy 21 16:54 Calm 10.00 Mostly FEW180 39 17 41% NA NA 30.21 1023.8 Cloudy BKN250 21 15:54 NE 6 10.00 Partly SCT250 41 17 38% 37 NA 30.20 1023.4 Cloudy 21 14:54 NE 6 10.00 Partly SCT250 41 18 39% 37 NA 30.19 1023.0 Cloudy 21 1354 N 6 10.00 A Few FEW190 40 18 41% 36 NA 30.21 1023.7 Clouds 21 12:54 NE 9 10.00 A Few FEW190 40 20 40 29 45% 34 NA 30.24 1024.5 Clouds 21 11:54 Vrbl5 10.00 Partly FEW190 39 21 48% 35 NA 30.27 1025.5 Cloudy SCT250 21 1054 N 8 10.00 Mostly FEW190 36 22 57% 30 NA 30.27 1025.6 Cloudy BKN250 21 09:54 N 9 10.00 Mostly FEW080 34 22 61% 27 NA 30.26 1025.6 Cloudy SCT190 BKN250 21 0854 N 3 10.00 Mostly FEW090 32 23 69% NA NA 30.25 1025.0 Cloudy BKN200 21 0754 NE 3 10.00 Mostly BKN200 30 23 75% NA NA 30.23 1024.5 Cloudy 21 0654 N 7 10.00 Mostly BKN250 30 23 31 23 75% 23 NA 30.21 1023.8 Cloudy 21 0554 NW 5 10.00 Partly SCT250 29 23 78% 24 NA 30.19 1023.2 Cloudy 21 04:54 NW 8 10.00 A Few FEW250 29 24 82% 21 NA 30.18 1022.8 Clouds 21 03:54 Calm 6.00 Fog/Mist BKN250 26 24 92% NA NA 30.14 1021.5 21 02:54 W 3 6.00 Fog/Mist BKN250 25 23 92% NA NA 30A5 1021.6 21 01:54 W 7 7.00 Mostly BKN040 26 24 92% 18 NA 30.14 1021.3 Cloudy 21 0054 SW 6 8.00 Mostly BKN040 27 24 30 24 89% 20 NA 30.13 1021.0 Cloudy 20 2354 NW 3 10.00 Fair CLR 28 25 88% NA NA 30.13 1021.0 20 2254 SW 5 10.00 Mostly BKN046 29 26 89% 24 NA 30.13 1021.0 Cloudy 20 21:54 W 5 10.00 Overcast OVC050 30 26 85% 25 NA 30.15 1021.7 20 20:54 SW 6 10.00 Overcast OVC055 30 26 85% 24 NA 30.14 1021.5 http://wi.weather.gov/data/obhistory/KGSO.html 1 /23/2016 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 4 of 4 20 19:54 W 6 10.00 Overcast OVC060 30 26 85% 24 NA 30.16 1022.2 20 18:54 SW 7 10.00 Overcast SCT015 29 26 36 29 89% 22 NA 30A5 1022.0 0.01 BKN035 OVC080 20 17:54 SW 8 7.00 Overcast BKN022 29 26 89% 21 NA 30.15 1021.9 OVC039 20 16:54 W 10 1.50 Light BKNO17 29 27 92% 20 NA 30.15 1021.8 0.01 Snow OVC032 Fog/Mist 20 1554 W 8 7.00 Light BKN037 33 18 54% 26 NA 30.14 1021.7 Snow OVC047 20 14:54 SW 10.00 Overcast BKN035 35 11 37% 27 NA 30.15 1022.0 1013 OVC060 18 20 13:54 SW 10.00 Overcast BKNO50 35 8 32% 27 NA 30.17 1022.6 12 OVC080 20 12:54 SW 10.00 Mostly FEW055 36 8 36 21 31% 28 NA 30.20 1023.5 12 Cloudy SCT095 BKN250 20 11:54 SW 10.00 Overcast SCT055 32 6 33% 24 NA 30.26 1025.7 10 BKN110 OVC250 20 10:54 SW 7 10.00 Overcast FEW065 30 5 34% 23 NA 30.31 1027.3 SCT080 OVC250 D a Time Wind Sky Air Max. Min. Dw t p Relative Wind Heal altimeter (in.) sea level 1 hr 3 hr 6 hr t last) (mph) (mi.) (mi. Weather Cond. 6 hour Humidity Chill Index (mb) ('F) ('F) e Temperature (OF) Pressure Precipitation (in.) National Weather Service Last Modified: Febuary, 7 2012 Southern Region Headquarters Back to previous page Privacy Policy Fort Worth, Texas Disclaimer http://wl.weather.gov/data/obhistory/KGSO.html 1 /23/2016 a RESEARCh & ANA[YTICA1 LABORATORIES, INC. AnotyOccil/Process ConsuOatlons March 10, 2014 ECS Carolinas, LLP 4811 Koger Blvd. Greensboro, NC 27407 Attention: Brad Luckey Project Name: PTI Y4E4 Project Number: 16399D L Miscellaneous OF-004 OF-006 OF-026 OF-027 OF-033 Parameters Unit Results Results Results Results Results BOD-5 mg/L 22.3 11.4 62.0 7,500 121 COD mg/L 47.0 38.0 104 13,100 128 NH-3-N mg/L 1.52 2.18 11.6 0.241 <0.10 RAL Sample Number: 779911 779912 779913 779914 779915 Date Collected: 03/04/14 03/04/14 03/04/14 03/04/14 03/04/14 Time Collected: 1127 1059 1232 1246 1208 mg1L = milligrams per Liter - parts per million < - Less than or below detection limit RESEARCh & ANA[yTICA[ LABORATORIES, INC. Ano"cal/Process ConsuRatlons March 10, 2014 ECS Carolinas, LLP 4811 Koger Blvd. Greensboro, NC 27407 Attention: Brad Luckey Chemical Analysis for Selected Parameters for Samples Identified as PTI Y4E4 (An ECS Carolinas, LLP Project N16399D, collected 04 March 2014) a D ANP�' L EPA Method 8015 Quaotitation OF-004 OF-006 OF-026 OF-027 OF-033 Limit Results Results Results Results Results Parameter (ma/L) (me/L) (ma/L) (me/L) (me/L) (ms/L) Ethylene Glycol 10.0 BQL BQL BQL 89.6 BQL Propylene Glycol 10.0 18.7 BQL BQL 46,800 57.9 Sample Number: 779911 779912 779913 779914 779915 Sample Collected Date: 03/04/14 03/04/14 03/04/14 03/04/14 03/04/14 Sample Collected Time (Hrs): 1127 1058 1232 1246 1208 mg/L = milligsms per Liter = parts per million (ppm) BQL = Below Quantitation Limp Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project 4 PTI Y4E4 f ppntOr n Responsible Charge RAL 4 779903 Final Effluent LabVatgry Supervisor Environmental 9ciences Branch MAIL ORIGINAL TO: Div. Of water Quality N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodophnio Chronic Pass/Fail Reproduction 'toxicity Test Ichronic Test Resul6 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Calculated I 4 Young Produced Tabular I %Reduction Adult (L) Ive (D) cad %Mortality Control Ef lumP/ Treatment 2 TRFATMENi2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Cannot CV 4 Young Produced 0 control organisms Adult (L) ive (D) cad producin 3rd brood PH Control Treatment 2 1 st Sam le 9 I C a n r d t Istsam le 5 I C a n I d t 2nd sam le 5 5 t C a n r d t 1st sample Ist sample 2nd sample Central [1] IE EL D.O. 'treatment 2 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates) Sample 1 03/04/14 Samnle'1'vne/Dumtion Grab Comp. Duration Sample I X Sample 2 Sample FAIL Check One Hardness (mg/1)g SpecCond.(pmhas)Chlorinc(mg/1)Sample temp. at receipt 0 �0 6.25 % 12.5 % 25 % 50 % 100 % % 0 % 0 % 1 0 % 0 % 0 % 0 LC50= >100% % Method of Determination ......................................... 95%Confidence Limits Moving Average Probit . %' ........................% Spearman Karbe Other ..........._X Organism Tested Ceriodaphniadubia Dumtion(h.) 24 Copy DWQ Form AT-1 (3187) rev. I1/95 _N Concentration Mortality Nole Pleau Complete This Section Also Start/end Start/end 6.96 7.01 Control R5 8.3 6.80 1 6.80 High &0 8.0 pH Cone. D.O. Effluent Toxicity Report Farm - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI Y4E4 FOptpr Jn Responsible Charge RAL # 779904 Final Effluent Fabdfatdly Supervisor vfto Sciences Branch ORIGINAL TO: Diow Quality N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodanhnia Chronic Pass/Fail Renroduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad Effluent% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad PH Control Treatment 2 Istsam le s t C a n r d t 2nd sam le s C d L - - 03 / 05 14 Collection (Start) D•atc Sample ) 03/04/14 Sample 2 Sample Tvne/Duration Grab I ComD.I Duration Sample I I X l st sample Ist sample 2nd sample I Sample 2l Control t H(mg0) D.O.LE El Spcc.Cand.(Cand.(µmhos) Treatment 2 Chlorine(mg/1) LC50/Acute Toxicity Tes[ Sample temp. at receipt (Mortality expressed as %, combining replicates) 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % % 0 % 0 % 1 0 % 0 % 0 % 0 % % I % % LC50= >100% % Method of Determination ......................................... 8 8 95%Confidence Limits Moving Average � Prohit ........................... %' ........................ % Spearman Karher Other ..............X Organism Tested Ceriodaphnia dubia Dump.. (his) 24 Copy DWQ form AT.1 (3/87) rev. 11195 �onccntration Nortallty Note: Ple¢se Complete This Secnan Alsu Start/end Siart/end 6.96 7.01 Cantral 8.5 8.3 6.60 6.70 Hid 8A 8.3 PH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Performing Test Research & Analytical Laboratories, Inc. IS-5 4 PTI Y4E4 Date 03/12/14 MAIL ORIGINAL TO: Evironmental Div. Of Water Qual ty s Bran` N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnia Chronic Pus/Fail Renroduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 4 Young Produced Adult (L) ive (D) ead Etllumr% TREATMENT 2 ORGANISMS 4 Young Produced Adult (L) ive (D) cad pH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 4+-H 1st Sam le Ist Sam M le 2nd sour le s $ s t e e o a n Ist sample 1st sample 2nd sample Control D.O. 'I'rea[ment 2 LC50/Acute Toxicity Tes[ (Mortality expressed as %, combining replicates) Guilford Com fete "This For Either Test Test Start Date 03 / 05 / 14 Collection (Start) Date Sample) 03/04/14 Sample2 Sample Type/Duration N Grab Comp. Duration e C ` p J X Sample 1 e O Sample o v .7 Hardness (mp/I) 48 Spec.Cond.(µmhos) 195 231 Chlorine(mg/1) 0.03 Sample temp. at receipt 3.1 0 % 6.25 % 12.5 % 25 % 50 % 100 % 0 % 0 % 1 0 % 0 % 0 % 0 LC50= >100% % Method of Determination 95% Confidence Limils Moving Average Probit ........................... %- ........................ % Spcarmen Karba Other ..........._X Organism'rested Ceriodaphnia dubia Dar°uon(hn) 24 Copy D WQ form AT-1 (3/87) rev. 11/95 Concentration Mortality T Note: Please Complete This Section Also SuuVend Start/cad 6.96 7.01 Canuol 8.5 8.3 6.56 6.60 High 8.2 8.0 PH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI Y4E4 fo rain _Responsible Charge RAL # 779906 Final Effluenthab m ry Supervisor MAIL ORIGINAL TO: Div. Of Wte Quality Sciences Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaahnio Chronic Pw JFail Reproduction Toxicity Test Chronic Test Results CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Calculated [ # Young Produced Tabular [ %Reduction Adult (L) ive (D) ead °/a Mortali Enluent% I TREATMENT 2 ORGANISM # Young Produced Adult (L) ive (D) cad Control pit 'treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 Control Cv 6Cb FAI wntroto33rrrgrnirrs��msproducmm��ddbb odk One l St sample 5 t c a n r d I 2nd sample 5 t e a n d t I st sample ISt sample 2nd sample Control D.O. Treatment 2 LE LC50/Acute Toxicity Test (Mortality apressed as %, combining replicates) Date / 14 Sample 1 03/04/14 Sample 2 Sample TYnc/Duration Gmb Comp. Duration =, E N C Sample 1 Sample2 F f. n Hardness (mgA) 48 195 701 Spec.Cond.(µmbos) Chlorinc(mg/l) '� 0.02 Sample temp. at receipt 3.1 0 % 6.25 % 12.5 % 25 %1 50 % 100 % % % % % 0 % 0 % 1 0 % 0 % 0 %1 0 LC50= >100% % Method of Determination 95%Confidence...-........Li....mits......_................ Moving Avem8 c Probit ........................... ........................ % Spearman Karber Other ..........._X Organism Tested Ceriodaphnin dubia Duration(hm) 24 Copy DWQ farm AT4 (3/87) rev. 11195 Concentration Mortality Notc: Plea¢ Complete This Smtion Also Start/end S[aNend 6.96 7.01 Control 8.5 6.3 6.64 6.60 High 8.3 8.3 pH Cone. U.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project 4 PTI Y4E4 ,�f pe//ptto In Responsible Charge RAL N 779907 .t /{( Final Effluent f a[ Supervisor MAILORIGINAL TO: Environmental Sciences Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Tes[ CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 p Young Produced Adult (L) the (D) ead 47 H Effluent% TREATMENT 2 ORGANISMS # Young Produced Adult (L) rve (D) ead pit Control Treatment 2 NNEEMEMENWE I st Sam le s t c a n r d t 2nd sample 5 c n n d t Ist sample 1st sample 2nd sample Control D.O. Treatment 2 LC50/Acute Toxicity Tes[ (Mortality expressed as %, combining replicates) Complete This For Either Test Test Start Date 03 / 05 / 14 Collection (Start) Date Sample 1 03/04/14 Samplc 2 Sample l'ype/Duration Grab Comp. Dmetion Sample 1— G _ y � O N c N Somplc 2 a' c = 'o Hardness (mgn) I 48 ,,7. `7` Spec.Cond.(µmhos) 195 835 CWorine(mgn) JMJ 0.01 Sample temp. at receipt 3.1 0 % 6.25 % 12.5 % 25 % 50 % 100 % % -71 0 % 0 % 1 0 % 0 % 0 % 0 % % LC50 = >I00% % Method of Determination ......................................... 95%Confidence Limits Moving Average I'robit ........................... % ........................ % Spearman Karber Other ..........._X Organism'1'ested Ceriodaphnia dubia Dumlion(hm) 24 s.opy �,vq.arm n.., the c7 rev. , uvn Concentration Mortality Nom: Please Campldc'rhis Section Also Start/end StarUend 6.96 1 7.01 1 Conuol 58.5TJ 8.3 6.67 1 6.50 Hid 8.5 1 8.3 pH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI Y4E4 rr 0tos Re ponsible Charge RAL # 779908 /� Final Effluent P'LaboKtoYSupervisor ronmental MAIL ORIGINAL TO: Div. Water Quality Sciences Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaahnia Chronic Pass/Fail Reproduction Toxicitv'l es t Chronic Test Results CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 Il 12 Calculated t # Young Produced Tabular t % Reduction Adult (L) ive (D) cad %Mortality Effluent% I Treatment 2 Treatment 2 'REATMENf 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV Young Produced 0 PASS FAIL control orgmisms \dull (L) ive (D) ead produoin&3rd brood Check Onc Ist Sample I sam le 2nd sample 03 / 05 / 14 Control Collection (Start) Date pH Sample1 03/04/14 sample2 Treatment 2 Sample TvtrclDwation 5 _ N a n a n a n Grub Comp. Duration — 'n o' c' d ; d r d Sample 1 I st sample Ist sample 2nd sample Sample2 6' a ' E Control Hardness (mg/1) 48 D.O. SpecChlori(pmhos) 195 160 Treatment 2 Chlorine(mg/I) 0.02 LC50/Acute Toxicitv Test Sample temp. at receipt ® 3.1 7 (Mortality expressed as %, wmbining replicates) 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % % 0 % 0 % 1 0 % 0 % 0 % 0 % % % % LC50= >100% % Method of Determination ................................... 95%Confidence.. Li...mits Moving Average Probit ...........................%- ........................% Spearman Kerber Other ..........._x Organism Tested Cedodaphniadubia D=aim(hm) 24 Copy DW Q fmm AT -I (3187) rcv. 11195 Concentration Mortality Nme: Please Complem This Secdon Alsa Stanfend Stanlmd 6.96 7.01 Control 8.5 8.3 6.74 1 6.80 1 Higl 8.5 8.4 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 ECS Carolinas NPDES#NC S000508 Pipe# IS-10 County Guilford Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI Y4E4 f Ope or jgjltee nsible Charge RAL # 779909 .1 �. Final Effluent J?LaborfifbrYSUperViS0T MAIL ORIGINAL TO: Div.. Of Wate QhSciencesBranch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodanhnia Chronic Pass/Fail Reproduction Toxicitv'I'es[ CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad Effluent% TREATMENT 2 ORGANISMS # Young Produced Adult (L) rve (D) ead pH Control 'treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 M S s t e a n r d t l st sample s t c a n r d I 2nd sam le a t c a n d t 1 St sample I st Sample 2nd sample Control D.O. Treatment 2 LC50/Acute Toxiciry Test (Mortality expressed as %, combining replicates) omplete This Far Either "lest I Test Start Date 03 / 05 / 14 (Start/ Date Ce Sample 1 Sam le 1 03/04/14 Sam le 2 p Sample TypefDuration Grab Comp. Duration _ N o r o' Sample 1 c O Z Sample 2,� _ '� — o Hardness (mg/1) t®p. at receipt3.1 P48Spcc.Cond.(pmhos)Chlorine(mg/1)Sample 0 % 6.25 % 12.5 % 25 `/° 50 % 100 % % % 0 % 0 % 1 0 % 0 % 0 % 0 % % LC50= >100% % Method of Determination ......................................... 95% Confidence Limits Moving Average Probi[ ...........................%- ........................ % Spearman Karbm Other ..........._X............. Organism Tested Ceriodaphniadubia Duration(hrs) 24 C°py DWQ form AT. (3/87) rev. 11195 :oncenbmion Mortality Natc: Please Complete This Section Als° Start/end Start/end 6.96 7.01 Convpl 8.5 1 8.3 6.75 6.88 High 8.3 8.0 pH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 ECS Carolinas NPDES#NC S000508 Pipe# - Is-]] County Guilford Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI Y4E4 fop t own a Charge PAL # 779910 I Final Effluent ftabomtoYy Supervisor MAIL ORIGINAL TO:Envronmental Div.'Of WaterQuality s Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7r 8 9 10 11 12 # Young Produced Adult (L)the (D)cad14 -11 11 11 11 11 11 11 1 11 Effluent% TREATMENT 2 ORGANISMS # Young Produced Adult (L) Ive (D) cad pH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 1st sam le I st sam le 2nd sam le 5 S t c t e t e f l st s�ammple� F Isaample2nd sample ControlI I I D.O. Treatment 2 LC50/Acute Toxicity Te (Mortality upresscd as %, combining replicates) Comnlete This For Either Test Test Start Date 03 / 05 / 14 Collection (Start) Date Sample 03/04/14 Sample2 Sample Tyne/Duration _ N Groh Camp. llumtion � c o r o Sample I 00 Sample 0' _ _ Hardness (mgA) 48 M Spec.Cond.(µmhos) 195 272 Chlorine(mgd) 0.04 Sample temp. at receipt � 3.1 0 % 6.25 % 12.5 % 25 % 50 % 100 0 % 0 % 1 0 %1 0 %1 0 %1 0 % % % % LC50= >100% % Method of Determination 95% Confidence Limits Moving Average Probit ...........................%" ........................% Spearman Karher Other ............_X Organism Tested Ceriodaphniadubia Duration(hrs) 24 Copy DWQ to. AT-1 (3/87) rev. 1 IN5 Concentration Mortality T Note:' Please Complcm Phis Sccuon Alsc Start/cnd Stan/cnd 6.96 7.01 Control 8.5 8.3 6.86 6.90 High 8.4 8.3 nH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Laboratory Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project X Project # PTI Y4E4 Signature �OF e or nsible Charge RAL # 779911 Si (f/�,6 es Final EffluentSignatV rof'.aborat.rySuper-visor MAIL ORIGINAL TO: Environmental Quality Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Tes[ CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) ead , H41 I I I I I I I Effluent% TREATMENT 2 ORGANISMS # Young Produced Adult (L) ive (D) cad PH me Control Treatment 2 Control Treatment 2 1 st sample M (Mortality expressed as %, combining replicates) 1 st sample PH 2nd 1 Complete This For Either Test Test Start Date 03 / 05 / 14 Collect;.. (Start) Date Sample) 03/04/14 Sample $=RIC Tyoe/Durntion Grab Camp. Duration — E ° Sample 1 X G u 4 C Sample 2 y f Hardness (mgn) 48 Spec.Cond.(pmhos) 195 1180 Chlorine(mg4) = 0.01 Sample temp. at rcccipt = 3.1 0 % 6.25 % 12.5 % 25 % 50 % 100 % 0 % 0 % 1 0 % 0 % 0 % 0 LC50= >100% % Method of Determination ......................................... 6 8 95%Confidence Limits Moving Averae Probit ........................... %" ........................ % Spearman Karber Other ..........._X Organism Tested Ceriodaphnia dubia Dvreden (h.) 24 Copy DWQ form Kr-1 (3/87) rev. 11/95 Concentration Mortality Notc: Plc..• Complctc This Sccdov Also Start/end Start/end 6.96 7.01 Control 8.5 8.3 6.68 6.74 Higb K2 8.1 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Laboratory Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project X Project 4 PTI Y4E4 Signatur ope�ato Re onsible Charge RAI, N 779912 X // '�f'' 71 Final Effluent Sign re�rato Supervisor MAIL ORIGINAL TO: DivtOf Water Quality s Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 s 9 10 11 12 Young Produced Adult (L) rve (D) cad Effluent% TREATMENT 2 ORGANISMS 9 Young Produced Adult (L) rve (D) cad pH ► 6 Control Treatment 2 Control Treatment 2 1 st sample F I (Mortality expressed m %, combining replicates) 1st sample F 2nd t Complete This For Either Test Test Start Date 03 / 05 / 14 Collection (Start) Date sample 1 03/04/14 Sample 2 Satanic Tvae/Dunuion N 4 Sample 1 v w y Sample2 Hardness (mgn) Spec.Cond.(µrnhos)126 Chlorine(mg/1)0.02Sample J815 temp. at receipt 3.1 0 % 6.25 % 12.5 % 25 % 50 % 100 0 % 0 % 1 0 % 0 %1 0 % 0 % % % % LC50= >100% % Method of Dncnnination 95%Confidence Limits Moving Average Probit ...........................%- ........................ % Spearman Kerber Other ..........._X Organism Tested Ceriodaphniadubia Duration(hrs) 24 Copy DWQ form AT-1 (3187) rev. I I/95 Concentration Mortality Nate: Please Complae TNs Section Also Starprnd Starueod 6.96 7.01 Control 6.5 8.3 6.54 6.60 High 8.5 9.3 pH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # P I I Y4E4 f 9pej}ttoyjn R onsible Charge RAL # 779913 �6/26/� Final Effluent fLaboraW Supervisor MAIL ORIGINAL TO:Envronmental Div.Of Water Quality s Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaahnia Chronic Pass/]'all Reproduction Toxlcity'rest CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) Ive (D) cad Effluent% TREATMENT 2 ORGANISMS # Young Produced Adult (L) ive (D) cad pH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 1st sam le 1st sample 2nd sam le 5 5 5 L C I C I C a a a n a n I itr it r it I t I Ist sample Ist sample 2nd sample Control FEI 1E U.O. Treatment 2 FE- LC50/Acute Toxiciry Test (Mortality expressed as %, combining replicates) Complete This For Either Test Test Start Date 03 / 05 14 Collection (Start) Date Sample) 03/04/14 sample Samnlc TwcfDurution ^ Z 5 d Sample 1 Sample Hardness (mg/1)071 Spec.Cond.(µmhos) Chlorine(mgA) Sample t®p. at receipt Grab Camp. Uuradon X 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % % 0 % 0 % 0 % 0 % 0 %� 100 % % % % LC50= 70 % Method of Determination 95% Confidence Limits Moving Average Probit ........................... %" ........................ % Spearman Kmber Other ............_'X Organism Tested Ceriodaphnia dubia Dumuom(his) 24 Copy U WQ form AT -I (3/87) rcv. 11/95 Cancrntration Mprtallty Note: Plcasc Completa This Sccdon Also Start/md �S-w—U�md- 6.96 7.01 Cannol gl 5 1 8.3 b.bl 6.70 High 8.0 8.0 pit Conc. D.O. Effluent Toxicity Report Farm - Chronic Pass/Fail and Acute LC50 Dale 03/12/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Pro ect # PTI Y4E4 perato, * Respo9sible Charge RAL # 779914 er / U 7 Final Effluent PLaborldolf Supervisor MAIL ORIGINAL TO: DiEnvironmental ' o W` to Quality Bra" N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaahnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad Effluent% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 to 11 12 # Young Produced Adult (L) ive (D) ead 1st sam le 1st sam le 2nd sample PH Control � � Sample 1 03/04/14 'Treatment 2 Samnle Type/Duratinn s s s t c t c t c Grab Comp. a n a n a n r d r d r d Sample 1 X t t Ist sample 1st Sample 2nd sample Semple 2 6 Control Treatment 2 (Mortality expressed as %, combining replicates) 03 / 05 / 14 Sample Duration c y w 5 .O Hardness (mg/I) 48 Spcc.Cund.(pmhos) 195 246 Chlorine(mgn) ® 0.0' Sample temp. at receipt ® 3.1 0 % 6.25 % 12.5 % 25 % 50 % 100 % 0 % 0 % 1 0 % 0 % 0 % 0 % % % % �0 LC50= >I00% % Method of Determination 95% Confidence Limits Moving Average Probit ........................... %. ........................ % Spearman Karber Other ..........._X Organism Tested Ceriodaphnia dubia Duration(hn) 24 -oov DWO form AT-1 (3/87) ¢v. I1/95 Coneennation Mortality Note: Please Complete This Sation Also StarUmd Sumtlend 6,96 7.01 1 Control 8.5 8.3 6.21 1 6.40 8.3 8.3 pit Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 03/12/14 Laboratory Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project X Project # PTI Y4E4 Signp C�y or' esponsible Charge RAL # 779915 at X ,�/�j (" Final Effluent Sib ature f Ubdeiitory Supervisor 7� �/'� Environments Sciences Branch MAIL ORIGINAL AL TO. Div. Of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity'I'est CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) Ive (D) ead EfOuctt°/ TREATMENT 2 ORGANISMS # Young Produced Adult (L) ive (D) cad pH Control Treatment 2 Istsam le s t c a n r d t I st Sample s t c ° n r d t 2nd sample s c a o d t Ist sample Ist sample 2nd sample Control D.O. Treatment 2 LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates) 03 D 05 / 14 Collection (Stahl Date Sample 03/04/14 Sample2 Sample Type/Dumdon Grab Comp. Duration N o � o Sample 1 Sample 2 'e' O B ,_� e= Hardness Spec.Coud.(µmhos) Chlorinc(mg/1) Sample tarp. (mg/1) at rcuipt 48 195 161 0.03 3.1 0 % 6.25 % 12.5 % 25 % 50 % 100 % % % % % 0 % 0 % 1 0 % 0 % 0 %° 0 % LC50 = >100% % Method of Determination ...............inii-.................. 6 95%Confidence Limi[s Moving Avaa a Probit %' ........................ % Spearman Karba Other ............ X Drganism Tested Ceriodaphniadubia Damdon(hrs) 24 2opy D WQ forth AT-1 (3/87) rev. 11195 Concentration Mortality Nom: Plcose Compldc This Section Also Staniend Start/end 6.96 7.01 Canuol 8.5 8.3 6.73 16.88 }lid 7.8 79 pH Conc. D.O. National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page I of weather.gov v Qm's ensboro, Piedmont Triad International Air oil Y .� ,m,Tho. Enter Your "City, ST" or zip code F-------j Go metric an espanol D Temperature (OF) Pressure Precipitation (in.) a Time Wind Vis. Weather Sky 6 hour Relative Wind Chill Heat Index sea t (est) (mph) (mi.) Cord. Air Dw t p Humidity (F) ('F) altimeter level 1 hr 3 hr 6 hr e Max. Min. (�n) (mo) 04 07:54 NE 9 10.00 Mostly SCT220 17 10 74% 6 NA 30.32 1027.9 Cloudy BKN250 04 0654 NE 8 10.00 Mostly BKN250 14 9 20 13 80% 3 NA 30.29 1027.2 Cloudy 04 05:54 NE 6 10.00 A Few FEW250 14 10 84% 5 NA 30.28 1026.7 Clouds 04 0454 NE 6 10.00 A Few FEW250 15 10 80% 6 NA 30.27 1026.3 Clouds 04 03:54 NE 7 10.00 Fair CLR 14 9 80% 4 NA 30.25 1025.4 04 02:54 NE 10.00 Fair CLR 18 10 71% 6 NA 30.25 1025.4 10 04 01:54 NE 10.00 Fair CLR 19 10 68% 6 NA 30.26 1025.7 12 04 0054 NE 10.00 Fair CLR 20 12 25 20 71% 7 NA 30.25 1025.4 13 03 23:54 NE 10.00 Fair CLR 21 13 71% 10 NA 30.25 1025.4 10 03 22:54 NE 10.00 Fair CLR 22 16 78% 9 NA 30.24 1024.9 14 03 21:54 NE 9 10.00 A Few FEW200 22 16 78% 12 NA 30.26 1025.3 Clouds 03 2054 NE 10.00 Fair CLR 23 17 78% 11 NA 30.23 1024.4 12 03 19:54 NE 10.00 Overcast SCTO16 24 18 77% 11 NA 30.19 1023.1 15 G OVC085 23 03 18:54 NE 10.00 Overcast BKNO05 25 20 31 24 81% 13 NA 30.18 1022.3 0.04 0.11 13 G OVC016 20 03 17:54 NE 0.25 Snow VV007 24 22 91% 11 NA 30.13 1020.7 0.03 15 Freezing Fog 03 16:54 NE 2.50 Light BKNO08 25 21 85% 11 NA 30.10 1019.6 20 G Snow BKN021 24 Fog/Mist OVC055 03 15:54 NE 4.00 Light BKN008 27 23 85% 13 NA 30.07 1018.5 0.01 0.04 20 G Snow OVC014 26 Fog/Mist 03 14:54 NE 4.00 Light BKN010 28 24 85% 15 NA 30.06 1018.1 0.02 18 G Freezing BKN016 26 Rain OVCO24 Fog/Mist http://wl.weather.gov/data/obhistory/KCiSO.htmi 3/4/2014 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 2 of 4 03 13:54 NE 2.00 Light BKNO08 29 25 85% 17 NA 30.01 1016.6 0.01 18 G Freezing OVC019 29 Rain Fog/Mist 03 12:54 NE 2.50 Light BKNO09 31 27 54 31 85% 16 NA 30.00 1015.9 29 G Freezing OVC014 39 Rain Fog/Mist and Windy 03 11:54 NE 5.00 Light BKNO08 34 31 89% 23 NA 29.98 1015.3 20 G Snow OVC019 28 Fog/Mist 03 10:54 NE 10.00 Light BKNO09 36 32 86% 25 NA 29.97 1014.8 0.01 20 G Rain OVC014 28 03 09:54 NE 4.00 Light BKNO08 38 35 89% 30 NA 29.93 1013.6 0.12 0.30 14 Rain OVC019 Fog/Mist 03 08:54 NE 2.50 Rain OVC008 40 37 89% 32 NA 29.91 1012.7 0.16 15 G Fog/Mist 22 03 07:54 NE 3.00 Light OVC006 43 40 89% 36 NA 29.86 1010.9 0.02 14 Rain Fog/Mist 03 06:54 NE 10.00 Overcast OVC060 55 45 60 55 69% NA NA 29.83 1009.6 16 03 0554 S 6 10.00 Overcast SCT070 56 44 65% NA NA 29.82 1009.0 BKN100 OVC170 03 04:54 S6 10.00 Overcast OVC180 55 44 67% NA NA 29.80 1008.5 03 03:54 SW 6 10.00 Fair CLR 55 44 67% NA NA 29.80 1008.6 03 02:54 SW 7 10.00 Overcast OVC200 57 44 62% NA NA 29.82 1009.3 03 01:54 SW 8 10.00 Overcast OVC200 59 44 58% NA NA 29.84 1009.7 03 00:54 SW 9 10.00 Overcast OVC250 60 44 65 59 56% NA NA 29.86 1010.4 02 2354 SW 9 10.00 Mostly BKN250 61 44 54% NA NA 29.88 1011.1 Cloudy 02 22:54 S 10 7.00 Mostly BKN250 60 44 56% NA NA 29.89 1011.7 Cloudy 02 21:54 S 7 6.00 Overcast OVC250 60 43 53% NA NA 29.91 1012.4 with Haze 02 20:54 SW 6 6.00 A Few FEW075 61 43 52% NA NA 29.93 1013.3 Clouds with Haze 02 19:54 SW 8 10.00 Partly SCT150 62 42 48% NA NA 29.94 1013.8 Cloudy 02 1854 S 12 10.00 Mostly FEW150 65 42 70 65 43% NA NA 29.93 1013.3 Cloudy BKN250 02 17:54 SW 10.00 Mostly FEW150 66 41 40% NA NA 29.93 1013.4 10 Cloudy BKN250 02 1654 S 15 10.00 Mostly FEW150 69 40 35% NA NA 29.95 1014.0 G 24 Cloudy BKN250 02 15:54 SW 10.00 Mostly FEW150 70 39 32% NA NA 29.98 1014.8 0.31 http://wI.weather.gov/data/obhistory/KGSO.html 3/4/2014 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 3 of 4 14 G Cloudy BKN250 22 02 14:54 SW 10.00 Mostly SCT160 69 39 33% NA NA 29.99 1015.5 16 G Cloudy BKN230 26 02 13:54 SW 10.00 Mostly BKN200 68 39 35% NA NA 30.01 1016.0 17 G Cloudy 26 02 12:54 S 14 10.00 Partly SCT250 67 39 67 32 36% NA NA 30.03 1016.7 G 22 Cloudy 02 11:54 SW 10.00 Partly SCT250 64 38 38% NA NA 30.09 1018.6 18 G Cloudy 23 02 10:54 SW 10.00 Mostly BKN250 60 36 41% NA NA 30.12 1019.8 13 Cloudy 02 09:54 SW 9 10.00 Mostly BKN250 57 37 47% NA NA 30.13 1020.1 Cloudy 02 08:54 S 9 9.00 Mostly BKN250 48 36 63% 44 NA 30.14 1020.8 Cloudy 02 07:54 SW 7 5.00 Mostly BKN250 38 32 79% 33 NA 30.18 1022.3 Cloudy with Haze 02 06:54 S7 6.00 Fog/Mist BKN250 32 28 39 32 85% 25 NA 30A7 1022.1 02 05:54 Calm 8.00 Fair CLR 35 30 82% NA NA 30.18 1022.4 02 0454 W 7 9.00 Fair CLR 36 29 76% 30 NA 30.16 1021.6 02 03:54 SW 6 9.00 Fair CLR 33 28 82% 27 NA 30.16 1021.5 02 02:54 SW 3 9.00 Fair CLR 34 27 76% NA NA 30.17 1021.9 02 01:54 Calm 9.00 Fair CLR 37 28 70% NA NA 30.19 1022.6 02 00:54 Calm 10.00 Fair CLR 37 28 48 36 70% NA NA 30.21 1023.5 01 23:54 Calm 10.00 Fair CLR 40 28 63% NA NA 30.21 1023.4 01 22:54 SW 3 10.00 Fair CLR 39 27 62% NA NA 30.22 1023.8 01 21:54 SW 3 10.00 Fair CLR 41 27 57% NA NA 30.23 1024.1 01 20:54 Calm 10.00 Fair CLR 44 27 51% NA NA 30.22 1023.8 01 19:54 S 6 10.00 Fair CLR 45 26 48% 42 NA 30.21 1023.5 01 1854 Calm 10.00 Fair CLR 49 26 53 44 41% NA NA 30.21 1023.4 01 17:54 S 3 10.00 A Few FEW070 50 25 38% NA NA 30.20 1022.9 Clouds 01 1654 Vrbl 3 10.00 A Few FEW080 52 25 35% NA NA 30.20 1022.9 Clouds 01 15:54 Calm 10.00 Mostly BKN080 51 23 33% NA NA 30.20 1022.9 Cloudy 01 14:54 SW 9 10.00 Mostly SCT070 50 21 32% 46 NA 30.22 1023.7 Cloudy BKN110 01 13:54 W 6 10.00 Mostly BKN075 48 19 32% 45 NA 30.25 1024.7 Cloudy BKN120 01 12:54 Vrbl3 10.00 Mostly BKN065 44 16 44 28 32% NA NA 30.28 1025.7 Cloudy BKN120 01 11:54 Calm 10.00 Overcast SKN070 40 15 36% NA NA 30.31 1027.0 OVC120 01 10:54 Calm 10.00 Mostly BKN080 36 15 42% NA NA 30.32 1027.5 Cloudy BKN130 http://w l.weather.gov/data/obhistory/KGSO.htm] 3/4/2014 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 4 of 4 01 09:54 N 3 10.00 Mostly BKN085 33 14 45% NA NA 30.33 1027.9 Cloudy BKN120 01 08:54 Calm 10.00 Mostly BKN095 31 14 49% NA NA 30.34 1028.1 . Cloudy D a Time Wind Vis. Max. Min. Wind Sky Air Dwpt Relative sea Heat altimeter level ( in 1 hr 3 hr 6 hr t (est) (mph) (mi.) Weather Cond. 6hour Humidity (Fit Index .) (mb) e Temperature ff) Pressure Precipitation (in.) National Weather Service Lasl Motlifietl: Fe7 2012 Back to previous page I Southern Region Headquarters Privac Privacy Policy Fort Worth, Texas Credits Disclaimer http://wI.weather.gov/data/obhistory/KGSO.html 3/4/2014 RESEA Ch & ANA1ygicl Ub®woRks, INC. Ana"cal/Process Consultatlons January 31, 2014 ECS Carolinas, LLP 4811 Koger Blvd. Greensboro, NC 27407 Attention: Brad Luckey /-hc S-o v d 5-Dr Project Name : PTI Project Number: Y4Q3E3 L Miscellaneous OF4104 OF-026 OF-027 OF-033 Parameters Unit Results Results Results Results BOD-5 mg/L Q00 • + + TSS mg/L 9.0 20.0 12.5 6.00 NH-3-N mg/L 0.125 0.203 <0.10 <0.10 COD mg/L <5.00 50 128 20.0 MBAS mg/L <0.1 <0.1 <0.1 <0.1 NO2+NO3 mg/L 1.20 1.26 1.08 1.95 Phosphorus,Total mg/L <0.050 0.050 0.053 0.076 Oil & Grease (TPH) mg/L <5.0 <5.0 <5.0 <5.0 RAL Sample Number: 777235 777236 777237 777238 Date Collected: 01l22/14 01/22/14 01/22/14 OMM14 Time Collected: 1100 1225 1237 1155 mg/L = milligams per liter- parts per million < = Less than or below detection limit * - BOD results not available due to laboratory QA/QC problems. RISFARCh & ANAdyricAl Ubommis, Oyc. Analy W/Process Consultanons January 31,2014 ECS Carolinas, LLP 4811 Koger Blvd. Greensboro, NC 27407 Attention: Bred Luckey Chemical Analysis for Selected Parameters for Samples Identified as PTI (An ECS Carolinas, LLP Project O 4Q3E3 collected 22 January 2014) L EPA Method 8015 Quantitation OF-004 OF-026 OF-027 OF-033 Limit Results Results Results Results Parameter m L (me/L) (me/L1 (me/L) lare/L) Ethylene Glycol 10.0 BQL BQL BQL BQL Propylene Glycol 10.0 BQL BQL 100 17.4 Sample Number: 777235 777236 777237 777238 Sample Collected Date: O1/22/14 01/22/14 01/27J14 Ol/27J14 Sample Collected Time (Hrs): 1100 1215 1237 1155 mg1L - milligrams per Liter = parts per million (ppm) BQL = Below Quantitation Limit J Client: Address: Address: Quote #: R(Eszmch & AMAYrgchlt LA(DRA-ToRiEsp Nwc. Analytical / Process Consultations Phone [336) 996-2841 I; `z !,A; ERIINNI,, ON.- 1. rM7 Project ID, Contact: -furnaround.: Phone: Job NLImber: Fax: P.O. I\Iumbei,:----,— Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 'rigid International Airport NPDES#NC S000508 Pipe# OF-004 County Guilford Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI-Y4Q3E3 Responsible Charge RAL # 777239 7 Final Effluent / Supervisor MAIL ORIGINAL TO: Di�ronmental Of Water Quality s rant N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity Teri CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad E®ueot% I TREATMENT 2 ORGANISM.' # Young Produced Adult (L) ive (D) cad Control pH Treatment 2 Control Treatment 2 I St Sample s t c a a r d t Iri Sample FR (Mortality expressed as %, combining replicates) 2nd sarrle s t e a n d t 2nd Complete This For Either Test Teri Start Date Ol / 23 / 14 Collection fStartl Date Sample 01/22/14 Sample2 Sample Twe/Dmatioo N Grab Comp. Duration Sample I Sample 2 'o' O Hardness (mgn) 48 Spec.Cond.(µmhus) 195 321 Chlorine(mg/1) 0.03 Sample temp. at receipt 3.1 0 % 5 % 1 10 % 20 % 40 % 70 % 100 % % % % 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % . LC50= >100% % Method of Determination ........_...._......................... �B 95%CpnSdenceLimits Moving Average � Probit % Spearman Karber Q Other X_..._.... Organism Tested Ceriodaphnia dubia Duration (la) 24 Copy DWQ form AT-1 (3/87) rev. 11195 Concentration Mortality Nose: Plensc Campine This Scctiov Also Start/end Start/cod 6.98 7.04 Control 9.5 8.4 6.80 6.95 Hid 8.4 8.4 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 Test Research & Analytical Laboratories, Inc. Continents: An ECS Carolinas, LLP Project Project # PTl-Y4Q3E3 f Responsible Charge RAL # 777240 Final Effluent Supervisor MAIL ORIGINAL TO: North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad EBlumt% TREATNENf20RGAMSMS # Young Produced Adult (L) ive (D) ead pH Control Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 1st sam le Ist sam le 2nd soar le s s s t e t e e a n a n a n I d r d r d 01 / 23 / 14 Collection (Start) Date Sanple I 01=4 Sample 2 SampleTwe/Duration Grab Camp. Sample 1 I X I st sample Iri sample 2nd sample Sample2 Control D.O. M M Treatmrnt 2 LC50/Acute Toxicity Teril (Mortality expressed as %a combining replicates) — v � Duman � g a O n o w ey _ = ey O. 9 a Hardness (rn /) 48 Spec.Cood(µmhps) 195 42( Chlorin on A) 0.0: Sampletemp.atreccipt 3.1 0 % 5 % 1 10 % 20 % 40 % 70 % 100 % % % 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % LC50 = >I00°/s % Method of Determination 95%Confidence Limits Moving Average Probit ...........__........... % % Spearman Karber Othm X Organism Tested Ceriodaphnia dubia Dmatloo (h s) 24 Copy DWQ form AT-1 (3/871 rcv. 11195 Couceohffiion Mortality T Note: Phase Complete This Sccuon Also Stan/md StwVmd 6.98 17.04 1 Cpnbol 1 8 6.68 17.17 High 1 7.5 1 8.4 pH Corr. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 Piedmont Triad International Airport NPDES#NC S000508 Pipe# OF-027 County Guilford Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI-Y4Q3M pelt -' sponsible Charge RAL # 777241 Final Effluent f o to Supervisor MAIL ORIGINAL TO: Div. `Of Water Quality ences Branc N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad , 4- H i Efrlumr% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Young Produced Adult (L) ive (D) ead Complete this For Either "test I Test Start Date 1st sample M 2nd sample 01 / 23 / 14 Control �IpIpB I�L� Sample 0122/]4 Sample Treatment 2 Sample TvndDmatipn s s s N a n a n e o Grab Comp. Duration = c d r d r d K i t t t S®pie 1 l st sample Ist sample 2nd sample Sample2 z Control timdnesso) D.O.141 Ell Spec.Caad.(µmbmhos19) 195 239 Treatment 2 CWocinc(mSA) 0.03 LC50/Acute Toxicity Test Sample temp. at receipt 3.1 (Mortality expressed as %, combining replicates) 0 % 5 % 1 10 % 20 % 40 % 70 % 100 % 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % LC50= >100% % Method of Determination ......................_............._. 95% Confidence Limits Moving Avaegc Prabit ................%" ....% Spearman Kmbm Other X Organism Testcd Ceriodaphnia dubia Duration (hos) 24 Copy DWQ form AT-1 (3/87), v, 11/95 Concentration Mortality T Nom: Please Complete This Sxtian Alm SmNend Start/end 6.96 T 7.0,1Control 81 5 F 8,4 1.6.29 16.80 High 1 7.7 1 8.0 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI-Y4Q3E3 f pey�to : orisible Charge RAL # 777242 Final Effluent ?Labmtimr3rSupervfsor nK MAIL ORIGINAL TO:Envirortmental Div. Of Water Quality s Branc N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGAMSMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad EHlumr% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad Ist Sam It Ist sample 2nd sam It Control pH Treatment 2 5 5 S I e t c t e v n a v a n 1st sample 1st sample 2nd sample Control D.O. Treatment 2 R1 LC50/Acute Toxicity Test (Mortality expresscd as %, combining replicates) 01 A 23 / 14 'ollection (Start) Date Saruple 1 01=4 Sample 2 Sample Type/Duration Grab Comp. Duration = ^ N ii Sample I X p y Sample2 e o i v O 2 ' a° Hardam (mg/1) 48 195 720 Spec.Cmd.(µmhps) Chlorine(mf/1) BM 0.01 K0.11 3.1 Sample temp. al rcceipt 0 % 5 % 1 10 % 20 % 40 % 70 % 100 % '% % 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % % LC50= >I00% % Method ofDeterrnination .__-..-..._..i................ am6 95%ConSdence.Limts._Moving Average Probit ........ % Spearman Karba Odra ............ X Organism Tested Ceriodaphniadubia D=don(hn) 24 Copy DWQ Tmm AT -I (3/87) rcv. 11/95 Concentration Mortality T Nate: Phase Complete This 5ecdov Also Start/end Start/end �— 6.98 7.04 Control RI 5 I 8.4 6.6I 1 16.73I Hid 1 1.4 1 8.2 pH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Performing Test Research & Analytical Laboratories, Inc. MAIL ORIGINAL TO: Di ester N C. DENR, 1621 Mail Sen Raleigh; NC 2 North Carolina Ceriodanhnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 .11 12 q Young Produced Adult. (L) the (D) ead E®uent%% . tREATMINT 2 ORGANISMS 1 2 3 4. 5 6 .7 8 9 10 11 12' 0 Young Produced Adult (L)ive (D)ead 1st sam le .1st sam le 2nd sample Control pH Treatment 2 r 9 9 t e t C t C a n a n a n r d d r d t t t Ist sample lstsample 2nd sample Control D.O. Treatment LC50/Acute ToxicityTest (Mortality expressed as %, combining replicates) Date 01/30/14 Calculated t Tabular t % Reduction Sampled 01W14 Sample Twe/Durauon Gmh Comp. Duration Sample.I X Sample 2 Sample 2 Check One Hardness (mg/1) 48.. Sped.Caad.(µtnhp"s) 195 �77 Chlorine(mg✓1) 0.03' Sample temp. m receipt 3:1 0 %/0 5 % 1 10 % 20 % 40 %1 70 % 100 % % % 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % '% % % LC50= __>100% _ % Method ofDelamination M% Confidence Limits Moving Average Probit ......_ % ...... % Spenrmen Karba Other .._........ X Organism Tested Ceriodaphniadubia Darnoan(bn) 24 Caov DWO fans AT-1 (3187) rev. 11195 14 ;oncentmtion dertauty Note: Pleau Complac This Secdoa Also Sta end stawmd 6.98 7.04 1 Control 8.5 1 8.4 6.79 1 7.00 High 8.3 8.4 PH Conc. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI-Y4Q3E3 eor jry Responsible Charge RAL # 777244 ,(/ �� Final Effluent /Laboratoig Supervisor MAIL ORIGINAL TO: Di Of Water ronmentalSciences s Branc N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad Effluent% TREATMENT2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) ead pH Control Treatment 2 F 5 t e a a r d t 1st Semple Ist sample 2nd sample Control D.O. Treatment 2 IE LC50/Acute Toxicity Test (Mortality expressed as %, combining replicates) 01 / 23 SampleI 0IaVI4 S®ple2 Sample Type/Dumtian Grab Comp. Dmaticn = � N ii Sanple 1 X p '0` y O w S®ple2 0' o u a Hardness (mgl0 Spcc.Cond.(µmhos) Chlorine(mr/I) Sample temp. at rcocipt 48 S 107 19S 0.02 0 % 5 % 1 10 %° 20 % 40 % 70 % 100 % % % 0 % 0 % 0 % 0 % 0 % 0 / 0 % % % LC50 = >100% % Method ofDeterrnination _..__............_................... � 95%ConSdenee Limits Moving Average Probit Y % Spearman Karber Other , X Organism Tested Ceriodaphnia dubia 13=t an (hrs) 24 Copy DWQ form AT-1 (3/87) mv. 11/95 Concentration Mortality Note: Pleau Complem This Section Alsa Start/end Start/end 6.98 7.04 1 Control 8.5 8.4 6.67 6.98 High 8.5 8.4 pH Cone. _ D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project B PTI-Y4Q3E3 0 to m o le Charge RAL 4 777245 OTTZFinal Effluent fUboratory Sdpervisor Envlronmen Sciences Brdnc MAIL ORIGINAL TO: Diy. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnio Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Calculated t 4 Young Produced Tabular t %Reduction Adult (L) ive (D)eadi H-H 11 11 11 11 11 11 11 11 %Mortality Effluent./ I TREATMENT 2 ORGANISM B Young Produced Adult (L) ive (D) ead Control pH Treatment 2 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 0 PASS FAI %control argalusms producing �od 3rd broodChcck One Ist sample 1st sample 2nd sample Control D.O. Treatment 2 LC50/Acute Toxicity Tes[ (Mortality expressed as %a, combining replicates) Ol / 23 / 14 Collection (Stall Date Sample 0=14 Sample Sample TwelDure tion Grab Comp. Duration _ E _ c —i Sample 1 X p X N Sample 2 ii' o _ ,Z _ SpecCmd.(µmhos) 195 1 133 CWorme(mgA) OAI Sample temp. a receipt ,t�. 3.1 0 % 5 % 1 10 % 20 % 40 % 70 % 100 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % LC50= >100% % Method of Determination ....._.-_._._ .................... 8 g 95%Confidence Limits Moving Average Probit ....../ ......... % Spearman Karber Other ............ X Organism Tested Ceriodaphniadubia Dumdon(hrs) 24 Copy DWQ form AT-1 (3187) rev. 11195 Cooccutration Mortality Norc: Plcase Camplcic This Secdov Also Stantend Start/end 6.98 7.04 Control 8.5 8.4 6.69 6.99 High 8.2 8.4 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Dale 01/30/14 Piedmont Triad ]ntemational Airport NPDES#NC S000508 Pipe# IS-6 County Guilford Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project # PTI-Y4Q3E3 fO pyrpI ' Re nsible Charge RAL # 777246 i/ e ! Final Effluent Last Supervisor MAIL ORIGINAL TO: D Of Water Qualironmental ty s Branch N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnio Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 ]0 Il 12 Calculated t # Young Produced Tabular t %Reduction Adult (L) rve (D)cad %Mortality Avg. Reprod. Control Control E®ua°h� Treatment 2 Treatment 2 TREAThiFNf2ORGANISMS 1 2 3 4 5 6 7 8 9 10 ll 12 ComtrplCV # Young Produced PASS FAIL % control organisms Adult (L) ive (D) cod pmdu._. cing 3rd brood Chh dk Onc Complete This For Either Test Test Start Date . 1st sam le lst sam le 2nd sam le 01 / 23 / 14 Control Collection (Start] Dale pH Sample] 0122/14 Sample2 Treatment 2 Sample TvpelDuration 9 5 5 C t C C Z N a n a v a v Grob Camp. Duration r d r d r d T t t t Sample 1 X Istsample Istsample 2nd sample Sample Control Hardness (mg/I) D.O. 1E SpcaCond(µmhos) I95 125 Treatment 2 Chlorinc(mg/1) 0.02 LC50/Acme TomciTcst Sample temp. m receipt 3.1 (Mortality expressed as %, combining replicates) 0 % 5 % 1 10 % 20 % 40 % 70 % 100 % % % % p % 0 % 1 0 % 0 % 0 LC50= >100% % Method of Determination ......................................... 9S%ComSdence Limits Mos4n Averse 8 g Probit .._._.._.._..__.. %- ............... % Spearman Karbm Other X Organism Tested Ceriodaphnia dubia D.don (h.) 24 Copy DWQ farm AT-1 (3/87) rev. 11195 Copcentration Mortality Note: Pleme Complete Thiz Secvon Also StarVend StmVend 6.98 7.04 Cannot 8.5 8.4 6.68 7.06 High 8.4 8.4 pH Cove. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project N PTI-Y4Q3E3 f (3p r}�yRe onsible Charge RAL 9 777247 raj ���i/ Final Effluent �orko' Supervisor 7nWoMmental Sciences BranchAriTL OntVTVAL TO: N.C. DENR 1621 Mai] Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Tes[ CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 p Young Produced I H Adult (L) the (D) cad , H Efllumt% TREATMENT 2 ORGANISMS N Young Produced Adult (L) ive (D) cad pH M Control Treatment 2 Control Treatment 2 Ist sam le 1st sam le 2nd sample Co01 / 23 / 14 llection lStartl Date Sample 0122/14 Sample2 SompleTwrJDmation s s N a e a v a e Gab Comp. Duration = ii r d r d r d t t t Sample 1 I st sample lst sample 2nd sample Smaple2 =O HardChloess (mg/1) 48 Spec.Cond.(µmhos) 195 221 Sample temre p. at ceipt 3.1 (Mortality expressed a %, combining replicates) 0 % 5 % 10 % 20 % 40 % 70 % 100 % 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % LC50= >100% % Method ofDetennination ...........'L'i'......................_ R R 95%ConSdcnce Limits Moving Average Probit %- % Spearman Kmber Other X Organism Tested Ceriodaphniadubia Duration(hm) 24 Copy DWQ form AT-1 (3187) rev. 11195 Concea atica Mortality Nate: Please Complete This Secaov Alzo Start/end Starr/and 6.98 7.04 1 Cvvtrvl 8.5 8.4 6.60 1 7.10 Hid 7.8 8.1 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 12/31/13 Performing Test Research & Analytical Laboratories, Inc. I Comments: An ECS Carolinas, LLP Project Project # PTI-Y4Q3E3 f O o onsihle Charge RAL # 777248 Final Effluent Rlab�� Supervisor MAIL ORIGINAL TO: Environmental ter Quality BranD N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaohnia Chronic Pus/Fail Reproduction Toxicity Ten CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) cad EfllucaM TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D) end In sam le 1st Sam le 2nd sam le Control pH Treatment 2 S 5 5 t C t c t C a v a e e n 01 / 23 / 14 Collection (Stan) Date Sample) 0IWI4 Sample2 Semple TvadDuration l GrablComp.l Duration I - - - Sample 1 X In sample In sample 2nd sample Soon Control D.O. Treatment 2 FEI LC50/Acute Toxicity Ten (Mortality expressed as %, combining replicates) Hmdoess (mg/I) 48 SpecCond.(pmhos) 195 14' Chlorine(mg/1) 0.01 Sample t®p.mreaip[ _..,. 3.1 0 % 5 % 1 10 % 20 % 40 % 70 % 100 % % `/O 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % LC50 = >100% % Method of Determination ............- ........................... g Average 95%ConSdence Limits Moving Av a Probit %. ........................ % Spearman Karber Other ..... X Organism Tested Ceriodaphnia dubia Duration Ch.) 24 Copy DWQ form AT -I (3/87) rev. 11195 Concentration Mortality T Note: Please Complete This Section Also Start/end Stan/end 6.98 7.04 Covtrol 8.5 8.4 6.99 7.201 Higb 1 7.5 1 8 4 pH Cone. D.O. Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date 01/30/14 Performing Test Research & Analytical Laboratories, Inc. Comments: An ECS Carolinas, LLP Project Project#{ PT1-Y4Q3E3 f opyratc, in esponsible Charge RAL # 777249 .%� Final Effluent f 17alrorgory, Supervisor Envirorkmeni@ 9clences Branch MAIL ORIGINAL TO: Div. Of water Quality N.C. DENR 1621 Mail Service Center Raleigji, NC 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced I 'L7kHiiii-m Adult a) ive (D) ead Effluent% TRPATMINT 2 ORGANISMS # Young Produced Adult (L) ive (D) cad pH IM Control Treatment 2 Control Treatment 2 1st sam le Ist Sample 2nd sample 01 / 23 14 Collection !Start) Dale Sample! 0122114 S®ple2 Smple Twe/Dmation s s s t e t e t e .- a n a n a n Gmb Comp. Duration = I ii d r d r d c T a t t t Sample 1 1 X p E. y 1st sample 1st sample 2nd sample Sample 2 I a 9°3 Hardness ton gA) 48 Spee.Cand.(pmhos) 195 127' Chlorine(mg) OA2 Sample temp. at receipt (Mortality expressed as %, combining replicates) 0 % 5 % 1 10 % 20 % 40 % 70 % ]00 % 0 % a % 0 % 0 % 0 % 0 % o % % % % LC50= >100% % Method of Determination 95%Confidence _......._........_....-.._......... Moving Limits Average � Probi[ ............. %" ................ % Spearman Karber Otber X Drganism Tested Ceriodaphnia dubia Donation (has) 24 Copy DWQ fmm AT -I (3197) rev. 11/95 Concentration Mortality Note: Please Complete Tbis 8ecoov Also Start/md Starttmd 6.98 7.04 1 Contra) 8.5 8A 6.98 7.21 High 7.8 8.3 pH Cone. D.O. Date 01/30/14 Effluent Tolocity Report Form - Chronic Pass/Fail and Acute LC50 Performing Test Research & Analytical Laboratories, Inc. Continents: An ECS Carolinas, LLP Project Project # PTI,Y,IQ3E3 dOp to ; R onsible Charge RAL# 777250 ' Final Effluent ,PLaboratory Supervisor MAIL ORIGINAL TO: Div o wale lSciences ual ri 5 N.C. DENR 1621 Mail Service Center Raleigh, NC 27699-1621 North Carolina Ceriodaphnia _Chronic_Pass/Fail Reproduction Toxicity Test CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 # Young Produced Adult (L) ive (D)cadi H411 11 11 11 '1 11 11 11 11 EfOucat% I TREATMINT 2 ORGANISM # Young Produced Adult (L) ive (D) cad Control pH Treatment 2 Ist Sam le s r c v v d t Ist Sample s i e e n r d t 2nd sample s I e a n r d I I st sample Ist sample 2nd sample Control D.O. Treatment 2 LC50/Acute Toxiciry Test (Mortality expressed as %, cambining replicates) 01 / 23 / 14 Collection (Start) Date sample 01W14 Sample2 Sample Twe(Dmation Grab Comp. tnation - N n c T o Sample 1 X EEE M a O PO Sample 2 0 0 0 Hardness SpecCond.(µmhos) Chlorine(mg/1) Sample temp. (mg0) at receipt 48 195 17fi 0.03 0 % 5 % 10 % 20 % 40 % 70 100 % % % 0 % 0 % 1 0 % 0 % 0 % 0 % 0 % % % LC50= >100% % Method of Determination .- ..................................... 8 6 95%Confidence Limits Morin Average Probit ............... %- ....... % Spearman Karber (hhcr _.......... X Organism Tested Ceriodaplmiadubia Dumdvn tan) 24 Copy DWQ farm AT-1 (3/97) rev, 11195 :oncmtradon Mortality Note: Pleasc Complete This Sectiav Also Startlend StarVend 6.98 7.04 1 Control 8,5 9.4 6.89 7.21 High 8,2 8.3 pH Conc. D.O. ANAtyTiCAi • TESri kc. CHARM OF CUSTODY RECORLD) 05228 Aa Ss-.Consultetions -2841 Phone -(3 96-- el 4-b(z) Project;ID 00 Date: ReporiTo: )L6 �"(je J­xt' _b L,�t_-L C - Client: Address: Contact, Phone: l 114#--10` Turnaround: 5ND Job Number: Address: Fax: P.O. Nurnber:------ Invoice Ta: Quote #: 41 - cf NC_ TI0UI-4 �O L144 ORIGINAL SC •Othe Client: Address: &ez,\f*p Address: Quote #: PPoj' Vi ` Contact: Phone: Fax: CHAN OF WSWODY RECORD 0,5227 Date'. Turnaround: Job Number: P.O. Number: MOUCIA 'v 6,-Dc—I13cy pp4,-L;7-M ORIGINAL 3;3z�p.j Deport TIJ: I nvolce, Tw IRESEARch & ANA1YTICA[ UbORATORIES ANC. w at - Analytical/Process Consultations _ February 7, 2014 Engineering Consulting Services 4811 Koger Blvd Greensboro, NC 27407 Attention Brad Luckey Dear Mr. Luckey, On 22 January 2014 Engineering Consulting Services (ECS) submitted samples from PTI for BOD testing. Due to laboratory QA/QC,,problems no data is available for those samples. It appears that due to laboratory contamination all oxygen was depleted from all samples and dilutions, therefore, BOD concentrations were unable to be calculated. Samples were not able to be re -tested due to the 48 hour holding time requirement for BOD testing. RAL apologizes for any inconvenience this may have caused ECS and will do everything possible to avoid this from happening in the future. Sincerely, Sidney L. Champion Director of Laboratory Services SLC/sy P.O. Box 473. 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2B41 • Fax 336-996-0326 www,randalabs.com National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page I of 3 weather.gov `M1TI,��r' [Greensboro oti Piedmont Triad International Airportp r Enter Your "City, ST or zip code F IGo metric en espanol 0 Temperature (OF) Pressure Precipitation (in.) a Time Wind Vis. Weather Sky 6 hour Relative Wind Chill Heat Index sea t lest) (mph) (mi.) Cord. Air Dwpt Humidity (°F) (°F) altimeter (in) level 1 hr 3 hr 6 hr a Max. Min. (mb) 22 06:54 NW 9 10.00 Partly FEW150 18 7 23 18 62% 7 NA 29.93 1014.4 Cloudy SCT200 22 05:54 NW 5 10.00 Mostly BKN200 19 12 74% 12 NA 29.90 1013.5 Cloudy 22 04:54 Calm 10.00 Mostly BKN200 20 12 71% NA NA 29.89 1013.0 Cloudy 22 03:54 IN 10.00 Fair CLR 20 12 71% 13 NA 29.89 1012.8 22 02:54 IN 10.00 Fair CLR 21 13 71% 12 NA 29.86 1011.8 22 01:54 -. N 6 10.00 Fair CLR 22 15 75% 14 NA 29.84 1011.1 22 00:54 N 5 10.00 A Few FEW025 23 17 33 23 78% 17 NA 29.83 1010.6 0.02 Clouds 21 23:54. N 5 10.00 Partly FEW044 25 19 78% 19 NA 29.81 1010.0 Cloudy SCT075 21 22:54 N 7 2.00 Light OVC037 27 22 81% 19 NA 29.82 1010.2 Snow g 21 21:54 N 10 8.00 Light OVC035 28 22 78% 19 NA 29.79 1009.2 0.02 G 18 Snow 21 20:54 N 12 8.00 Light FEW010 30 21 69% 20 NA 29.76 1008.3 • G 22 Snow OVC037 21 19:54 N 12 3.00 Light FEW004 32 29 88% 23 NA 29.72 1006.9 0.02 Snow SCT010 Fog/Mist OVC055 21 18:54 N 8 1.00 Light OVC004 33 31 47 33 92% 26 NA 29.69 1006.0 0.06 0.15 Snow Fog/Mist 21 17:54 N 7 2.00 Light OVC006 34 32 92% 28 NA 29.64 1004.2 0.04 Snow Fog/Mist 21 16:54 N 8 7.00 Light FEW017 38 34 86% 32 NA 29.61 1003.1 0.05 Rain BKN031 OVC041 21 15:54 N 8 10.00 Light BKN035 43 31 63% 38 NA 29.58 1001.9 Rain OVC046 21 14:54 N 6 10.00 Mostly FEW060 45 29 54% 42 NA 29.54 1000.6 Cloudy BKN080 BKN100 21 13:54 NE 7 10.00 Mostly BKN080 46 28 50% 42 NA 29.54 1000.6 Cloudy BKN100 21 12:54 NE 9 10.00 Mostly SCT070 45 27 45 33 49% 40 NA 29.56 1001.1 Cloudy BKN100 21 11:54 N 6 10.00 Partly SCT100 45 27 49% 42 NA 29.60 1002.5 http://wI.weather.gov/data/obhistory/KGSO.htm] 1 /22/2014 National Weather Service : Observed Weather for past 3 Days : Greensboro, Piedmont Tr... Page 2 of 3 Cloudy 21 10:54 N 8 10.00 Partly SCT095 41 27 57% 36 NA 29.64 1003.8 Cloudy 21 09:54 NE 10.00 Partly FEW065 38 26 62% 30 NA 29.65 1004.3 12 Cloudy SCT100 21 08:54 NE 10.00 Overcast FEW065 34 25 70% 25 NA 29.66 1004.7 13 SCT080 BKN090 BKN140 OVC250 21 07:54 NE 8 10.00 Mostly FEW140 34 25 70% 27 NA 29.68 1005.3 Cloudy SCT170 BKN250 21 06:54 N 6 10.00 Mostly BKN250 33 23 37 31 66% 27 NA 29.70 1005.8 Cloudy 21 05:54 N 7 10.00 Mostly BKN250 34 24 67% 28 NA 29.70 1005.7 Cloudy 21 04:54 Calm 10.00 Partly SCT250 31 22 69% NA NA 29.71 1006.0 Cloudy 21 03:54 NE 3 10.00 Fair CLR 33 23 66% NA NA 29.73 1006.7 21 02:54 Calm 10.00 Fair CLR 34 24 67% NA NA 29.74 1007.1 21 01:54 Calm 10.00 Fair CLR 33 24 70% NA NA 29.75 1007.6 21 00:54 Calm 10.00 Fair CLR 36 24 53 34 62% NA NA 29.77 1008.1 20 23:54 Calm 10.00 Fair CLR 38 24 57% NA NA 29.80 1009.0 20 22:54 Calm 10.00 Fair CLR 39 24 55% NA NA 29.82 1009.7 20 21:54 Calm 10.00 Fair CLR 40 24 53% NA NA 29.83 1010.4 20 20:54 Calm 10.00 Fair CLR 45 22 40% NA NA 29.84 1010.5 20 19:54 W 5 10.00 Fair CLR 48 22 36% 46 NA 29.83 1010.4 20 18:54 SW 6 10.00 A Few FEW250 52 22 62 50 31% NA NA 29.82 1009.9 Clouds 20 17:54 SW 7 10.00 Partly SCT250 54 22 29% NA NA 29.80 1009.3 Cloudy 20 16:54 SW 10.00 A Few FEW250 59 21 23% NA NA 29.79 1008.6 13 Clouds 20 15:54 SW 10.00 A Few FEW250 62 21 21 % NA NA 29.78 1008.2 15 Clouds 20 14:54 W 10 10.00 A Few FEW250 61 22 22% NA NA 29.77 1008.0 Clouds 20 13:54 SW 10.00 A Few FEW250 60 21 22% NA NA 29.77 1008.2 15 Clouds 20 12:54 SW 10.00 Partly SCT250 59 19 59 28 21% NA NA 29.79 1008.8 15 G Cloudy 21 20 11:54 SW 10.00 Mostly BKN250 54 19 25% NA NA 29.82 1009.9 10 Cloudy 20 10:54 SW9 10.00 Mostly BKN250 50 22 33% 46 NA 29.85 1010.9 Cloudy 20 09:54 SW 8 10.00 Mostly BKN250 43 24 47% 38 NA 29.86 1011.4 Cloudy 20 08:54 W 8 10.00 Partly SCT250 37 25 62% 31 NA 29.86 1011.4 Cloudy 20 07:54 SW 9 10.00 A Few FEW250 30 23 75% 22 NA 29.85 1011.1 http://wI.weather.gov/data/obhistory/KGSO.htmi 1 /22/2014 National Weather Service : Observed Weather for past 3,Days : Greensboro, Piedmont Tr... Page 3 of 3 Clouds 20 06:54 SW 8 10.00 A Few FEW250 29 22 36 29 75% 21 NA 29.85 1011.3 Clouds 20 05:54 SW 7 10.00 A Few FEW250 31 23 72% 24 NA 29.86 1011.4 Clouds 20 04:54 SW 7 10.00 A Few FEW250 31 23 72% 24 NA 29.85 1011.2 Clouds 20 03:54 SW6 10.00 Fair CLR 32 23 69% 26 NA 29.86 1011.3 20 02.54 SW6 10.00 Fair CLR 31 22 69% 25 NA 29.86 1011.5 20 01:54 SW6 10.00 Fair CLR 33 22 64% 27 NA 29.86 1011.3 20 00:54 SW6 10.00 Fair CLR 34 21 42 31 59% 29 NA 29.87 1011.9 19 23:54 SW6 10.00 Fair CLR 35 21 57% 30 NA 29.89 1012.6 19 22:54 SW 3 10.00 Fair CLR 35 20 54% NA NA 29.92 1013.4 19 21:54 SW6 10.00 Fair CLR 34 21 59% 29 NA 29.92 1013.5 19 20:54 SW 5 10.00 Fair CLR 38 20 48% 34 NA 29.91 1013.4 19 19:54 W 9 10.00 Fair CLR 40 20 45% 34 NA 29.93 1014.0 19 18:54 W 9 10.00 Fair CLR 42 21 51 41 43% 37 NA 29.93 1014.1 19 17:54 W 10 10.00 Fair CLR 44 21 40% 39 NA 29.93 1014.1 19 16:54 W 14 10.00 Fair CLR 48 21 34% 42 NA 29.92 1013.4 19 15:54 W 16 10.00 A Few FEW055 50 22 33% 44 NA 29.91 1013.0 G 23 Clouds 19 14:54 W 15 10.00 A Few FEW055 50 23 35% 45 NA 29.89 1012.4 G 21 Clouds 19 13:54 W 18 10.00 Partly SCT055 50 23 35% 44 NA 29.89 1012.5 G 25 Cloudy 19 12:54 W 16 10.00 A Few FEW065 49 23 49 27 36% 43 NA 29.90 1012.6 Clouds 19 11:54 W 10 10.00 A Few FEW060 47 21 36% 42 NA 29.92 1013.7 Clouds 19 10:54 SW 8 10.00 Fair CLR 43 16 34% 38 NA 29.93 1014A - 19 09:54 SW 10.00 A Few FEW250 38 14 37% 30 NA 29.93 1014.2 13 Clouds 19 08:54 W 7 10.00 A Few FEW250 34 15 46% 28 NA 29.92 1013.8 Clouds 19 07:54 SW6 10.00 Partly SCT250 27 14 58% 20 NA 29.90 1013.2 Cloudy D a Time Wind vis. Sky Air Dwpt Max. Min. Relative Wind Heat altimeter (in.) sea level 1 hr 3 hr 6 hr t (est) (mph) (mi.) Weather Cond. 6 hour Humidity Chill Index (mb) (`F) ("F) e Temperature (OF) Pressure Precipitation (in.) National Weather Service -r, - -�-__-,--«-„��..-,..--�.�-�., l3acktoprevtouslpa e Last Modified: Febuary, 7 2012 Southern Region Headquarters - --��-�+�-� � r•9,• Privacy Policy Fort Worth, Texas Credits Disclaimer http://wI.weather.gov/data/obhistory/KGSO.html 1 /22/2014