NCGNE0452_COMPLETE FILE - HISTORICAL_20130806

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
NCGNE N 5 a
DOC TYPE
Z HISTORICAL FILE
DOC DATE
❑ !�/�LL�O�C�
YYYYMMDD

��1 : •' Division of Water Quality / Surface Water Protection
N�®E,,�yppI®
9�lIt National Pollutant Discharge Elimination System
PERMIT NAME/OWNERSHIP CHANGE FORM
4 xv �xOxix[ x1"D NMWA� RES ux i9
FOR AGENCY USE ONLY
Date Received
Year
I Month
Day
I. Please enter the permit number for which the change is requested.
NPDESPermit (or) Certificate of Coverage
N C 1 S 1 b I I I I I I I N I C 10 1 N E 0 4 5 2
II. Permit status prior to requested change.
a. Permit issued to (company name):
b. Person legally responsible for permit:
First MI Last
Title
Ferinil Bolder Mailing Address
City Stale Zip
Phone Fax
c. Facility name (discharge): Merck Manufacturing Division (Old Name)
d. Facility address: 4633 Merck Road
Address
Wilson NC 27893
City State Zip
e. Facility contact person: Sandy West [phone]
First / MI / Last Phone
111. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ❑ Change in ownership of the facility
❑ Name change of the facility or owner
ff other please explain:
b. Permit issued to (company name):
e. Person legally responsible for permit:
First MI Last
Title
Permit Bolder Mailing Address
City
Slate Zip
( )
Phone
E-mail Address
d. Facility name (discharge):
Merck Sharp
& Dohnte Corp (New Name)
e. Facility address:
4633 Merck Road
Address
Wilson
NC 27893
City
State Zip
f. Facility contact person:
Sandy
West
First
MI Last
[phone]
sandy west a,merck.com
I'hone
E-mail Address
Revised 2012Ap23

NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
IV. Permit contact information (if different from the person legally responsible for the permit)
Permit contact:
First MI Last
Title
Mailing Address
City State Zip
I'hone E-mail Address
V. Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
X Yes
❑ No (please explain)
VI Required Items: THIS APPLICATION WILL 13E RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
.....................................................................................................................
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. Por a name change request, the signed
Applicant's Certification is sufficient.
PERM ITTEE CERTIFICATION (Permit holder prior to ownership change):
1, , attest that this application for a name/ownership change has been reviewed and is accurate and
complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as incomplete.
Signature Date
APPLICANT CERTIFICATION
I, Sandy West, attest that this application for a name/ownership change has been reviewed and is accurate
and complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as incomplete.
/o -2U- 2-ol Z-
Signature Date
PLEASE SF,ND THE COMPLETE APPLICATION PACKAGE TO:
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Revised 712008

Merck Sharp & Dohme Corp
4633 Merck Road
Wilson, NC 27893
Certified Mail (7012 0470 0001 6459 4758)
October 23, 2012
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Company Name Change Notification
Merck Manufacturing Division, located at 4633 Merck Rd, Wilson North Carolina has changed its name to
Merck Sharp & Dohme Corp. Our business and the utilization of the facility has not changed. Attached is
an updated Permit Name/Ownership Change Form. Please update your database systems to ensure future
communications are timely and accurate.
Thank you to Bethany Georgoulias for her support and guidance. If you have any questions or need
additional information, please contact me at 252-246-6254.
Since � ®e7 %�
Sandy West
CC: 22.8

On-Site'Inspection Report
LABORATORY NAME: Merck Sharpe and Dohme Corporation
NPDES PERMIT#: NCG060000 � C/O
ADDRESS: 4633 Merck Road
Wilson, NC 27893
CERTIFICATE #: 5441 (� I
DATE OF INSPECTION: February 10, 2011
S
TYPE OF INSPECTION: Field Maintenance
AUDITOR(S): Jeffrey R. Adams
LOCAL PERSON(S) CONTACTED: Sandy West and Mike Fry
I. INTRODUCTION:
This laboratory was inspected to verify its compliance with the requirements of 15A NCAC 2H .0800 for the
analysis of environmental samples.
GENERAL COMMENTS:
The laboratory was neat and equipment was well maintained. Records were well organized. The laboratory
appears to be doing a good job in implementing the North Carolina Wastewater/Groundwater Laboratory
Certification policies.
The laboratory was given a packet containing the Technical Assistance Documents and quality control
requirements for all field parameters during the inspection.
III. FINDINGS, REQUIREMENTS, COMMENTS AND RECOMMENDATIONS:
pH — Standard Methods, 18th Edition, 4500 H+ B
Comment: The temperature sensor correction is not posted on the meter. The Technical Assistance for
Field Analysis of pH document states: The temperature correction (even if it is zero) must be posted on the
meter as well as in hard copy format (to be retained for 5 years). This finding was addressed and corrected
during the inspection. No further response is necessary for this finding.
IV. PAPER TRAIL INVESTIGATION:
The paper trail consisted of comparing laboratory benchsheets and contract lab reports to Self Monitoring
Reports submitted to the City of Wilson. Data were reviewed for Merck Sharpe and Dohme Corporation
(NCG permit #NCG060000) for February and August, 2010. This laboratory is only required to sample twice
a year. No transcription errors were detected. It appears the laboratory is doing a good job of accurately
transcribing data.
V. CONCLUSIONS:
The finding noted during this inspection was adequately addressed during the inspection and prior to the
completion of this report. The inspector would like to thank the staff for its assistance during the inspection
and data review process. No response is required..
Report prepared by: ' Jeffrey R. Adams Date: January 28, 2011
Report reviewed by: Tonja Springer Date:February 22, 2011

il&
NODE R
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
March 31. 2011
RECE EED
5441
Mr. Sandy West APR - 6 2011
Merck Sharp and Dohme Corporation
4633 Merck Road NCDENR
Wilson, NC 27893 Raleigh Regional Office
Subject: North Carolina Wastewater/Groundwater Laboratory Certification (NC WW/GW LC)
Maintenance Inspection
Dear Mr. West:
Enclosed is a report for the inspection performed on February 10, 2011 by Mr. Jeff Adams. I apologize
for the delay in getting this report to you. Since the finding(s) cited during the inspection were all
corrected prior to the completion of the enclosed report, a response is not required. The staff is
commended for taking the initiative in correcting the findings in such a timely manner. For certification
maintenance, your laboratory must continue to carry out the requirements set forth in 15A NCAC 2H
.0800.
Copies of the checklists completed during the inspection may be requested from this office. Thank you
for your cooperation during the inspection. If Vou wish to obtain an electronic copV of this report by
email or if you have questions or need additional information, please contact us at 919-733-3908.
Sincerely, '.
Dana Satterwhite
Certification Unit Supervisor
Laboratory Section
Enclosure
cc: Jeff Adams
Raleigh Regional Office
DENR Dw0 Laboratory Section NC Wastewater/Groundwater Laboratory Certification Branch
1623 Mail Service Center, Raleigh, North Carolina 27699-1623
Location: 4405 Reedy Creek Road. Raleigh, North Carolina 27607-6445
Phone: [phone] FAX: [phone]
Internet: w Awglab,org
None
rthCarolina
Naturallrff
An Equal Opponunilyl Affirmative Action Employer Customer Service: 1-877-623-6748 www.nawaterquality.org

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
w® 1
December 28, 2007
Sandy West
Merck Manufacturing Division
4633 Merck Road
Wilson, NC 27896
Coleco H. Sullins, Director
Division of Water Quality
<<a EVE
=— 1�
��f I DEC 3 1 2007
DENR RALEIGH REGIONAL OFFICE
Subject: No Exposure Certification NCGNE0452
Merck Manufacturing Division
4633 Merck Road, Wilson
Wilson County
Dear Mr. West:
The Division has reviewed your submittal of the No -Exposure Certification for Exclusion from NPDES
Stormwater Permitting form, which we received on September 5, 2007. Based on your submittal and signed
certification of no exposure at the above referenced facility, the Division is granting your certification as
provided for under 40 CFR 126.22(g), which is incorporated by reference in North Carolina regulations, and
hereby rescinding your current Certificate of Coverage NCG060106.
Please note that by our acceptance of your no exposure certification, you are obligated to maintain no
exposure conditions at your facility. If conditions change such that your facility can no longer qualify for a no -
exposure exclusion, you are obligated to immediately obtain NPDES permit coverage for your stormwater
discharge. Otherwise, the discharge becomes subject to enforcement as an un-permitted discharge. Your
conditional no -exposure exclusion expires in five years (December 31, 2012). At that time you must re -certify
with the Division, or obtain NPDES permit coverage for any stormwater discharges from your facility.
Your certification of no exposure does not affect your facility's legal requirements to obtain environmental
permits that may be required under other federal, state, or local regulations or ordinances.
If you have any questions or need further information, please contact Sarah Young at [phone], ext.
502, or at [e-mail].
cc: Raleigh Regional Office
Stormwater Permitting Unit Files
NCG060106 Permit file
Sincerely,
.
for Coleen H.
Sullins
Central Files —w/attachments
Fran McPherson -Budget Office
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [phone]
Ef
Customer Service
1-877-623-6748

Division of Water Quality / Surface Water Protection
w�
NCDENRNational Pollutant Discharge Elimination System
..� NO EXPOSURE CERTIFICATION for Exclusion
NCGNE0000
NO EXPOSURE CERTIFICATION
r
Mk AGENCY USE ONLY
Dale Received
Year Mon�h
Day
O
Ce"ificam or Coverage
National Pollutant Discharge Elimination System application for exclusion from a Stormwater Permit
based on NO EXPOSURE:
Submission of this No Exposure Certification constitutes notice that your facility does not require permit
authorization for its stormwater discharges associated with industrial activity in the State of North
Carolina because it qualifies for a no exposure exclusion. A condition of no exposure at an industrial
facility means all industrial materials and activities are protected by a storm resistant shelter (with some
exceptions) to prevent exposure to rain, snow, snowmelt, and/or runoff.
Industrial materials or activities include, but are not limited to: material handling equipment or activities,
industrial machinery, raw materials, intermediate products, by-products, final products, or waste
products. Material handling activities include the storage, loading and unloading, transportation, 1
conveyance of any raw material, intermediate product, final product or waste product. A storm r
shelter is not required for the following industrial materials and activities: drums, barrels, tanks,
V
similar containers that are tightly sealed, provided those containers are not deteriorated and do 1 ak. rr
"Sealed" means banded or otherwise secured and with locked or non -operational taps or valves; j c
adequately maintained vehicles used in material handling; and final products, other than produc Q( t
would be mobilized in stormwater discharges (e.g., A
g., rock salt).
0
A No Exposure Certification must be provided for each facility qualifying for the no exposure ex tp 18 n.
In addition, the exclusion from NPDES permitting is available on a facility -wide basis only —not ; V
individual outfalls. If any industrial activities or materials are, or will be, exposed to precipitation, th, ems_
facility is not eligible for the no exposure exclusion. By signing and submitting this No Exposure
Certification form, you certify that a condition of no exposure exists at this facility or site and are
obligated to comply with the terms and conditions of 40 CFR 122.26(g).
You are required to reapply for the No Exposure Exclusion once every five (5) years
For questions, please contact the DINO Regional Office for your area. (See page 5)
(Please print or type)
1) Mailing address of owner/operator
Name % 1 ✓ - /✓iT/
Street Address �/G33 rs7oL�.r d f�,.�/
City �{1�L SU,y State_ ZIP Code 2 7` (:,
Telephone No. 2S2- 2 y6 -6 L-q Fax: 2jS-2` 7_6/4; - 6 337
2) Location of facility producing discharge:
Facility Name Lsl-z1fE /fS ��O✓G
Facility Contact
Street Address
City
County
Telephone No.
Page 1 of 5
State ZIP Code
Fax:
SWU-NE-060607 Last revised 06/06/07

w
I
: ' t NCGNE0000 No Exposure Certification
3) Physical location information:
Please provide a narrative description of how to get to
distance and directign from a roag>vay intersection). ,
(A copy of a map with the f9cility, clearly located on it should be included with the
4) Is the facility located on Native American Lands? ❑ Yes VNO
5) Is this a Federal facility? ❑ Yes �No
6) Latitude Longitude (deg, min, sec)
7) This NPDES Permit Application applies to which of the following:
road numbers, and
application.)
❑ New or Proposed Facility Date operation is to begin
V Existing Date operation began /51J'7
8) Was this facility or site ever covered under an NPDES Stormwater Permit? 04es ❑ No
If yes, what is the NPDES Permit Number?
9) Standard Industrial Classification:
Provide the 4 digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility
SIC Code: L Q
10) Prov] a brief description of the ttyypes of industrial activities an1products produced t this facility:
//A��I,i h ri /f/ilzrii/'A T ✓vl d- r lA ii Y
11) Does this facility have any Non -Discharge permits (ex: recycle permits)?
O No
6Y%es
If yes, list the permit numbers for all current Non -Discharge permits for this facility: tiG� %�5 %i8 35 �TSA J
Exposure Checklists (12. - 14.)
12) Are any of the following materials or activities exposed to precipitation, now or in the foreseeable
future? (Please check either "Yes" or "No.") If you answer "Yes" to any of these items, you are not
eligible for the no exposure exclusion.
a. Using, storing, or cleaning industrial machinery or equipment, and areas where
residuals from using, storing or cleaning industrial machinery or equipment remain
and are exposed to stormwater
b. Materials or residuals on the ground or in stormwater inlets from spills/leaks
c. Materials or products from past industrial activity
d. Material handling equipment (except adequately maintained vehicles)
e. Materials or products during loading/unloading or transporting activities
I. Materials or products stored outdoors (except final products intended for outside
use [e.g.. new cars] where exposure to stormwater does not result in the discharge
of pollutants)
Page 2 of 5
SWU-NE-060607
❑ Yes O"No
❑ Yes OINo
❑ Yes VNo
O Yes eNo
O Yes SKNo
❑ Yes ¢'No
Last revised 06/06/07

' NCGNE0000 No Exposure Certification
g. Materials contained in open, deteriorated or leaking storage drums, barrels, tanks, ❑ Yes FSNo
and similar containers
h. Materials or products handled/stored on roads or railways owned or maintained by ❑ Yes 92"No
the discharger
i. Waste material (except waste in covered, non -leaking containers [e.g., dumpsters]) ❑ Yes t(No
j. Application or disposal of process wastewater (unless otherwise permitted) ❑ Yes VNo
k. Particulate matter or visible deposits of residuals from roof stacks and/or vents not ❑ Yes HYNo
otherwise regulated (i.e., under an air quality control permit) and evident in the
stormwater outflow
L Empty containers that previously contained materials that are not properly stored ❑ Yes 2/No
(i.e., not closed and stored upside down to prevent precipitation accumulation)
m. For any exterior ASTs, as well as drums, barrels, tanks, and similar containers ❑ Yes "o
stored outside, has the facility had any releases in the past three (3) years?
13) Above Ground Storage Tanks (ASTs): If you answer "No" to any of the following items, you are not
eligible for the no exposure exclusion.
a. Are exterior ASTs or piping free of rust, damaged or weathered coating, pits, or Ed Yes ❑ No
deterioration, or evidence of leaks?
b. Is secondary containment provided for all exterior ASTs? If so, is it free of any 9/Yes ❑ No
cracks, holes, or evidence of leaks, and are drain valves maintained locked shut?
14) Secondary Containment: If you answer "No" to any of the following items, you are not eligible for the
no exposure exclusion.
a. Is secondary containment provided for single above ground storage containers
(including drums, barrels, etc.) with a capacity of more than 660-gallons?
b. Is secondary containment provided for above ground storage containers stored
in close proximity to each other with a combined capacity of more than 1,320-
gallons?
c. Are release valves on all secondary containment structures locked?
13Yes ❑ No
ta'Yes ❑ No
c'(es ❑ No
Page 3 of 5
SWU-NE-060607 Last revised 06/06/07

NCGNE0000 No Exposure Certification
15) Hazardous Waste:
a. Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility?
cKyes ❑ No
b. Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste
❑ Yes 0"No
generated per month) of hazardous waste?
c. Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste
PI(es ❑ No
generated per month) of hazardous waste?
If you answered yes to questions b. or c., please provide the following information:
Type(s)ofwaste: L,.fg '' 0 ef.2xyzaSit/ c T zrett1 /E
How is material stored: ,O[ inr t l tlTitJtLti7�C / r ff 7c%0 .
44'&'
Where is material stored: TS.O /J,9 C%/PeuSis
How many disposal shipments per year:
Name of transport! disposal vendor:
Vendor address: %d t Zs >' r:i 06 J74- 3a0 , r�mjdlyF 6-C 2` &7_
16) Certification:
I certify under penalty of law that I have read and understand the eligibility requirements for claiming a condition of "no
exposure" and obtaining an exclusion from NPDES stormwater permitting.
I certify under penalty of law that there are no discharges of stonmwater contaminated by exposure to industrial activities
or materials from the industrial facility or site identified in this document (except as allowed under 40 CFR 122.26(g)(2)).
I understand that I am obligated to submit a no exposure certification form once every five (5) years to the North Carolina
Division of Water Quality and, if requested, to the operator of the local municipal separate storm sewer system (1434) into
which the facility discharges (where applicable). I understand that I must allow the North Carolina Division of Water
Quality, or MS4 operator where the discharge is into the local MS4, to perform inspections to confirm the condition of no
exposure and to make such inspection reports publicly available upon request.
In the event that the site no longer qualifies for a No Exposure Exclusion, I understand that I must obtain coverage under
an NPDES permit prior to any point source discharge of stormwater from the facility. Additionally, I certify under penalty
of law that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based
on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is to the best of my knowledge and belief true, accurate and complete. I am aware
that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for
knowing violations.
I certify that I am familiar with the information contained in this application and that to the best of my knowledge and
belief such information is true, complete, and accurate.
Printed Name of Person Signing:
Title:////�s✓�il/f'IV
of
a7
(D fe Sig d)
Please note: This application for the No Exposure Exclusion is subject to approval by the
NCDENR Regional Office prior to issuance. The Regional Office may inspect your facility for
compliance with no exposure conditions prior to that approval. The Regional Office may also
inspect your facility at any time in the future for compliance with the No Exposure Exclusion.
Page 4 of 5
SWU-NE-060607 Last revised 06/06/07

NCGNE0000 No Exposure Certification
North Carolina General Statute 143-215.6 B(i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other
document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false
statement of a material fad in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly
renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the
[Environmental Management] Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine
not to exceed ten thousand dollars ($10,000).
There is currently no fee for a No Exposure Exclusion.
Final Checklist
This application should include the following items:
❑ This completed application and all supporting documentation.
❑ A map with the location of the facility clearly marked.
KAMI�the entire packa
Stormwater Permitting Unit
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Note
The submission of this docum�nt does not guarantee the issuance of a No Exposure Exclusion.
For questions, please contact the D WQ Reqional Office for vour area. I
DWQ Reqional Office Contact Information:
Asheville Office ...
Fayetteville Office
Mooresville Office
Raleigh Office .....
Washington Office
Wilmington Office
Winston-Salem ...
Central Office .....
... [phone]
... [phone]
... [phone]
... [phone]
...[phone]
... [phone]
... [phone]
....[phone]
Page 5 of 5
SWU-NE-060607 Last revised 06/06/07

35,752778N 78.001667W - Google Maps http://maps.google.com/maps?q=35.752778N+78.0016...
356 45 i 0166 7(,F° of �,c� EGG-606 33F
k.1 Y l? `Jq c
2 of
ICI(- G- cq Z 5�
mer(tZ_
16)) 70 eve% �
wdsw, tq(L 2-7S-%
10/8/2007 5:26 PM

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
� —f
August 23, 2002
ETHAN ALLEN PRIEST
MERCK MFG DIVISION
4633 MERCK ROAD
WILSON, NC 27893
Alan W. Klimek, P.E., Director
Division of Water Quality
Subject: NPDES Stormwater Permit Renewal
Merck Mfg Division
COC Number NCG060106
Wilson County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG060000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983,
The following information is included with your permit package:
A new Certificate of Coverage
A copy of General Stormwater Permit NCG060000
A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Aisha Lau of the Central Office Stormwater
and General Permits Unit at [phone], ext. 578
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
ern
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1- 800-623-7748

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
j
December 27, 2001
1'I'l IAN Al-1-EN PR[ES'I'
NIERCK MPG DIVISION
4633 MERCK RD
WILSON. NC 27893
Gregory J. Thorpe, Ph.D.
Acting Director
Division of Water Quality
Subject: NPDES Slormwaler Permit Renewal
MERCK AIFG DIVISION
COC Number NCC;060106
Wilson County
Dour Pcinlitice:
Your I:iciIity is currently covered for skn'nnomer(Iischarge under General Permit NCG060000. This permil expires
on August 31, 2002. 'file Division staff is currently in the process of rewriting this permit and is scheduled to have
file permil ICissuul by late summer of 2002. Oncc the permil is reissued. yam' facility would be eligible for
continue(] arvCage under the reissued permit.
In order to assure your continued covcmgc under the general permil, you must apply m the Division of Wlllel-
Quality (DWQ) for renewal of your permit coverage. Tu make this rcncw;d pmcuss c;tsiu', we arc inlinnling you in
advance Ihat your perttlil will be expiring. Enclosed you will find a General Permit Coverage Renewal
Application Furor. The application must be completed and retn'ned by March 4, 2002 in order to assure continued
covenlge under the general permit.
Failure to request re11CWa1 within this little period m;ry result in a civil assessment of least $250.00. Larger
penalties may he assessed (]cpcncling on the dclinqucncy Mahe rcqucsl. Discharge of stornlwatcr from your futility
Without covcruge under a valid sturnlwater NPDES permil would constitute a violation of NCGS 143-215.1 and
could resull in assessments of civil ponallics Of to $10,000 perchry.
Please note that recent federal le gislalion has extended the "no CvposwC a.sclusinn" to ell opet;uurs of indusu'i:II
facilities in any of the I I categories of "storm water discharges assneiated with industrial activity," (avccpt
cons l tic lion :tctivitics). 11'you ICCI your' I,IciIity c;m cerlily a cundiIloll of "no c.cpusure". i.e. the IaciIfV industrial
materials and uper;ilions arc not expnsc(] 10 stormw;acl, you can apply for the nu Cvposure exclusion. Per additional
information contact the Central Of ficc Stormwalcr StalT memhcr listed below or check file Slunnwalcr S Gcnend
Permits Unit Web Site at htq,://h2o.errsl;UCnc.us/su/sulrmwalur.hlml
If the subject stnrmwuter discharge to waters of the state has been Iernaimlted. please complete the enclosed
Rescission Request Form. Mailing instruclions Zile listed on the hottonl of the form. You will he notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact .lot AIII iston of the Raleigh
Regional Office ❑I 919-571-4700 or Aishu Lau of the CCtltral Office SWIIIIw:Ilet' Unit at [phone], ext. 57S
Sincerely.
Bradley Bernell, Supervisor
SIOI'nlwttl Cland GCHCr;d Purinils Unit
cc: Central Piles
K;dci�_h Rcaiunal Office
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1- 800-623-7748

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. James L Burson
Merck MFG Division
Rt 2 Box 558
Wilson, NC 27893
Dear Mr. Burson:
October 22, 19913A
.14V%
'QO
Subject: General Permit No. NCG060000
Merck Manufacturing Division
COC NCG060106
Wilson County
In accordance with your application for discharge permit received on September 28, 1992, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state -. NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Environmental Management. The Division of Environmental Management may require modification or
revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Bill Mills at telephone number 919/733-
5083.
Sincerely,
A. Preston Howard, Jr., P. E.
cc: rRaleigh Regional Office)
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10%post-consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE NO. NCG060106
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Merck Manufacturing Division
is hereby authorized to discharge stormwater from a facility located at
Merck Manufacturing Division
Merck Road
Wilson
Wilson County
to receiving waters designated as an unnamed tributary to Bloomery Swamp in the Neuse River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I,11, Ill
and IV of General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective October 22, 1993.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day October 22, 1993.
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

nb)o°on,N
PLOP-4EO, GG,[�� SVPv Pf SiOx. v,P4irv,�-99) 78°00'
m f ,7W--° E frl4 MI TO U.S. 30,y
ROAD CLASSIFICATION
hard or
Primary highway, improvedght surface
hard surface._.-...-..'--_ improved surface.......
Secondary highway,
hard surface._- -..- Unimproved road......._-----
�iInterstate Route � U. S. Route State Route
BAILEY, N. C.
SID4 SPRING HOPE 15' GUADRANGLE
N3545—`N7800/7.5
1978 MODELING FILE
PHOTOREVISED 1961
DMA 5355 1 SE —SERIES V842 10
L9
3
730 ODO
FEET
35°45 -29
78000'
dy Mapped, edited, and published by
Control by USGS, NOS/NOAA, and North Ca
f\
Topography by photogrammetric methods fr•
photographs taken 1974. Field checked 1
Projection and 10,000-foot grid ticks: Nort
system (Lambert conformal conic)
3000-meter Universal Transverse Mercator
e zone 18, Shown in blue. 1927 North Am,
Fine red dashed lines indicate selected fer
'I generally visible on aerial photographs. Ti

J
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
s 1
� Y
December 28, 2007
Sandy West
Merck Manufacturing Division
4633 Merck Road
Wilson, NC 27896
Subject: No Exposure Certification NCGNE0452
Merck Manufacturing Division
4633 Merck Road, Wilson
Wilson County
Dear Mr. West:
Coleen H. Sullins, Director
Division of Water Quality
The Division has reviewed your submittal of the No -Exposure Certification for Exclusion from NPDES
Stormwater Permitting form, which we received on September 5, 2007. Based on your submittal and signed
certification of no exposure at the above referenced facility, the Division is granting your certification as
provided for under 40 CFR 126.22(g), which is incorporated by reference in North Carolina regulations, and
hereby rescinding your current Certificate of Coverage NCG060106.
Please note that by our acceptance of your no exposure certification, you are obligated to maintain no
exposure conditions at your facility. If conditions change such that your facility can no longer qualify for a no -
exposure exclusion, you are obligated to immediately obtain NPDES permit coverage for your stormwater
discharge. Otherwise, the discharge becomes subject to enforcement as an un-permitted discharge. Your
conditional no -exposure exclusion expires in five years (December 31, 2012). At that time you must re -certify
with the Division, or obtain NPDES permit coverage for any stormwater discharges from your facility.
Your certification of no exposure does not affect your facility's legal requirements to obtain environmental
permits that may be required under other federal, state, or local regulations or ordinances.
If you have any questions or need further information, please contact Sarah Young at [phone], ext.
502, or at [e-mail].
cc: Raleigh Regional Office
Stormwater Permitting Unit Files
NCG060106 Permit file
Sincerely,
A� 47/
for Coleen H. Sullins
Central Files — w/attachments
Fran McPherson -Budget Office
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [phone]
NT ENR
Customer Service
1-877-623-6748

ncgne0452, 0359, and 0427
Subject: ncgne0452, 0359, and 0427
From: Mitch Hayes <[e-mail]>
Date: Wed, 17 Oct 2007 09:54:50 -0400
To: Sarah Young <sarah.young cr ncmail.net>
Sarah,
The following facilities: Alliance One International, Inc. NCGNE0427 in Wilson, NC;
Merck Manufacturing Division NCGNE0452 in Wilson NC; and Estes Express Lines
NCGNE0359 in Wilson, NC all meet the conditions for the Non -Exposure Stormwater
Permit. The RRO has no objections in issuing the permits. If you have any questions,
please contact me via email or phone [phone].
Thanks,
Mitch Hayes
Mitch Hayes <mitch.hayes((bncmail.net>
Environmental Specialist
Environment & Natural Resources
NC Division of Water Quality
I of 1 12/11/2007 2:00 PM

AfflU_5XA
GM
NCDENR
��.x �„ax. oa.,...�x. o<
Exvinoxncxr �xo Nuu,k nescwces
NC(swglDDivision of Water Quality / Surface Water Pron
National Pollutant Discharge Elimination System
NO EXPOSURE CERTIFICATION for Exclusion
NCGNE0000
NO EXPOSURE CERTIFICATION
4111111110
AGIitfCY USG ONLI'
Dale Rcccivcd
Ycar Month
Dav
O
�e�ihea,e erc��e��Ee
FN
National Pollutant Discharge Elimination System application for exclusion from a Stormwater Permit
based on NO EXPOSURE:
Submission of this No Exposure Certification constitutes notice that your facility does not require permit
authorization for its stormwater discharges associated with industrial activity in the State of North
Carolina because it qualifies for a no exposure exclusion. A condition of no exposure at an industrial
facility means all industrial materials and activities are protected by a storm resistant shelter (with some
exceptions) to prevent exposure to rain, snow, snowmelt, and/or runoff.
Industrial materials or activities include, but are not limited to: material handling equipment or activities,
industrial machinery, raw materials, intermediate products, by-products, final products, or waste
products. Material handling activities include the storage, loading and unloading, transportation,
conveyance of any raw material, intermediate product, final product or waste product. A storm re
shelter is not required for the following industrial materials and activities: drums, barrels, tanks,
similar containers that are tightly sealed, provided those containers are not deteriorated and dot I ak.
"Sealed" means banded or otherwise secured and with locked or non -operational taps or valves;
adequately maintained vehicles used in material handling; and final products, other than produc pj t
would be mobilized in stormwater ( discharges e. n
g g., rock salt).
A No Exposure Certification must be provided for each facility qualifying for the no exposure exillp n. oV
In addition, the exclusion from NPDES permitting is available on a facility -wide basis only —not
individual outfalls. If any industrial activities or materials are, or will be, exposed to precipitation, thy_
facility is not eligible for the no exposure exclusion. By signing and submitting this No Exposure
Certification form, you certify that a condition of no exposure exists at this facility or site and are
obligated to comply with the terms and conditions of 40 CFR 122.26(g).
You are required to reapply for the No Exposure Exclusion once every five (5) years.
For questions, please contact the DWQ Regional Office for your area. (See page 5)
(Please print or type)
1) Mailing address of owner/operator
iff-7u%
Street Address 1/6r &3 i17ot
City AJ/L.147A/
Telephone No. 2S2- 2 96 -
2) Location of facility producing discharge:
Facility Name
Facility Contact
Street Address
City
County
Telephone No.
State Ne_ ZIP Code �[ L /Y-4�41
Fax: 25-2 24G - to 337
�Sf!!NE fiS �/6e✓L-�
Page 1 of 5
State ZIP Code
Fax:
SWU-NE-060607 Last revised 06/06/07

" A5

n
I
r
NCGNE0000 No Exposure Certification
3) Physical location information:
Please provide a narrative description of how to get to
distance and directign from a roar>vay intersection).
(A copy of a map with the facility clearly located on it should be included with the
4) Is the facility located on Native American Lands? ❑ Yes V<O
5) Is this a Federal facility? ❑ Yes V<O
6) Latitude
Longitude
(deg, min, sec)
7) This NPDES Permit Application applies to which of the following:
❑ New or Proposed Facility Date operation is to begin
VExisting Date operation began /9k3
road numbers, and
application.)
8) Was this facility or site ever covered under an NPDES Storm/water Permit? plies ❑ No
If yes, what is the NPDES Permit NumbeG66 YT
9) Standard Industrial Classification:
Provide the 4 digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility
SIC Code:2_ Q I
10) Provi a brief description of the�t�yypes of industrial activities an products producedG at this facility:
�//AA!l1,f�Tlc.AL /l7itya/`.re �rrx./frG �' iJce / /IGiG i i Y
11) Does this facility have any Non -Discharge permits (ex: recycle permits)?
❑ No
&4es 1
If yes, list the permit numbers for all current Non -Discharge permits for this facility: V6,0 7f6,? 19g,3S r!TS/J J
Exposure Checklists (12. - 14.)
12) Are any of the following materials or activities exposed to precipitation, now or in the foreseeable
future? (Please check either "Yes" or "No.") If you answer "Yes" to any of these items, you are not
eligible for the no exposure exclusion.
a. Using, storing, or cleaning industrial machinery or equipment, and areas where
residuals from using, storing or cleaning industrial machinery or equipment remain
and are exposed to stormwater
b. Materials or residuals on the ground or in stormwater inlets from spills/leaks
c. Materials or products from past industrial activity
d. Material handling equipment (except adequately maintained vehicles)
e. Materials or products during loading/unloading or transporting activities
f. Materials or products stored outdoors (except final products intended for outside
use [e.g., new cars] where exposure to stormwater does not result in the discharge
of pollutants)
❑ Yes EKNo
❑ Yes A
❑ Yes VNo
❑ Yes VNo
❑ Yes VNo
❑ Yes LAI0
Page 2 of 5
5 W U-NE-060607 Last revised 06/06/07

f

NCGNE0000 No Exposure Certification
No
g. Materials contained in open, deteriorated or leaking storage drums, barrels, tanks,
❑ Yes
and similar containers
h. Materials or products handled/stored on roads or railways owned or maintained by
❑ Yes
93'No
the discharger
i. Waste material (except waste in covered, non -leaking containers [e.g., dumpsters))
❑ Yes
f/No
j. Application or disposal of process wastewater (unless otherwise permitted)
❑ Yes
VNo
k. Particulate matter or visible deposits of residuals from roof stacks and/or vents not
❑ Yes
vl0
otherwise regulated (i.e., under an air quality control permit) and evident in the
stormwater outflow
I. Empty containers that previously contained materials that are not properly stored
❑ Yes
B/No
(i.e., not closed and stored upside down to prevent precipitation accumulation)
m. For any exterior ASTs, as well as drums, barrels, tanks, and similar containers
❑ Yes
Ri 40
stored outside, has the facility had any releases in the past three (3) years?
13) Above Ground Storage Tanks (ASTs): If you answer "No" to any of the following items, you are not
eligible for the no exposure exclusion.
a. Are exterior ASTs or piping free of rust, damaged or weathered coating, pits, or 6311yes ❑ No
deterioration, or evidence of leaks?
b. Is secondary containment provided for all exterior ASTs? If so, is it free of any a Yes ❑ No
cracks, holes, or evidence of leaks, and are drain valves maintained locked shut?
14) Secondary Containment: If you answer "No" to any of the following items, you are not eligible for the
no exposure exclusion.
a. Is secondary containment provided for single above ground storage containers
(including drums, barrels, etc.) with a capacity of more than 660-gallons?
b. Is secondary containment provided for above ground storage containers stored
in close proximity to each other with a combined capacity of more than 1,320-
gallons?
c. Are release valves on all secondary containment structures locked?
9/yes ❑ No
VYes ❑ No
U Yes ❑ No
Page 3 of 5
SWU-NE-060607 Last revised 06/06/07

NCGNE0000 No Exposure Certification
15) Hazardous Waste:
a. Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility? /Yes ❑ No
b. Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste ❑ Yes R/No
generated per month) of hazardous waste?
c. Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste P'1'es ❑ No
generated per month) of hazardous waste?
If you answered yes to questions b. or c., please provide the following information:
Type(s) of waste
How is material stored: ,O, am's Dart?rt7t[NY S eAl AP- 7,T.4 Lc/A7GE�duiG�
Where is material stored: 7so GJrPiCL !/eUSG'
How many disposal shipments per year:
Name of transport / disposal vendor: Cr�A.Y i¢G(Sd/LS
Vendor address: Zod -mxm, L.s1ae,$00/4, .376r Sao %im61A (S-G 2`iLZ 3
16) Certification:
I certify under penalty of law that I have read and understand the eligibility requirements for claiming a condition of "no
exposure" and obtaining an exclusion from NPDES stormwater permitting.
I certify under penalty of law that there are no discharges of stormwater contaminated by exposure to industrial activities
or materials from the industrial facility or site identified in this document (except as allowed under 40 CFR 122.26(g)(2)).
I understand that I am obligated to submit a no exposure certification form once every five (5) years to the North Carolina
Division of Water Quality and, if requested, to the operator of the local municipal separate storm sewer system (MS4) into
which the facility discharges (where applicable). I understand that I must allow the North Carolina Division of Water
Quality, or MS4 operator where the discharge is into the local MS4, to perform inspections to confirm the condition of no
exposure and to make such inspection reports publicly available upon request.
In the event that the site no longer qualifies for a No Exposure Exclusion, I understand that I must obtain coverage under
an NPDES permit prior to any point source discharge of stormwater from the facility. Additionally, I certify under penalty
of law that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based
on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is to the best of my knowledge and belief true, accurate and complete. I am aware
that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for
knowing violations.
I certify that I am familiar with the information contained in this application and that to the best of my knowledge and
belief such information is true, complete, and accurate.
Printed Name of Person Signing:
Title: `f�' 1J1J1&,VZM&7V
of
(D to Sig dJ
Please note: This application for the No Exposure Exclusion is subject to approval by the
NCDENR Regional Office prior to issuance. The Regional Office may inspect your facility for
compliance with no exposure conditions prior to that approval. The Regional Office may also
inspect your facility at any time in the future for compliance with the No Exposure Exclusion.
Page 4 of 5
SWU-NE-060607 Last revised 06/06/07

NCGNE0000 No Exposure Certification
North Carolina General Statute 143-215.6 B(i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other
document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false
statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly
renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the
[Environmental Management] Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine
not to exceed ten thousand dollars ($10,000).
There is currently no fee for a No Exposure Exclusion.
Final Checklist
This application should include the following items:
❑ This completed application and all supporting documentation.
❑ A map with the location of the facility clearly marked.
atl the entire oacka
Stormwater Permitting Unit
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Note
The submission of this document does not guarantee the issuance of a No Exposure Exclusion.
For questions, please contact the DWQ Regional Office for your area.
DWQ Regional Office Contact Information:
Asheville Office ......
[phone]
Fayetteville Office ...
[phone]
Mooresville Office ...
[phone]
Raleigh Office ........
[phone]
Washington Office ...(252)
946-6481
Wilmington Office ...
[phone]
Winston-Salem ......
[phone]
Central Office .........(919)
733-5083
Page 5 of 5
SWU-NE-060607 Last revised 06/06/07