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Home My WebLink AboutNCG170140_COMPLETE FILE - HISTORICAL_20140731ill t, (A" 141t,o STORMWATER DIVISION CODING SHEET RESCISSIONS. PERMIT NO. f V w U I DOC TYPE 0"COMPLETE FILE - HISTORICAL DATE OF RESCISSION ❑ �vi`� U I YYYYMMDD Compliance Inspection Report Permit: NCG170140 Effective: 08/O1/09 Expiration: 07/31/14 Owner: Guilford Mills Inc SOC: Effective: Expiration: Facility: Guilford Mills Incorporated -Wake County: Wake 200 Dickens Rd Region: Raleigh Fuquay Varina NC 27526 Contact Person: Paul Bruesch Title: Phone: 336-317-0244 Directions to Facility: System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 09/13/2013 Entry Time: 01:00 PM Exit Time: 01:30 PM Primary Inspector: David R Parnell Phone: 919-791-4260 Secondary Inspector(s): Reason for Inspection: Routine Inspection Type: Technical Assistance Permit Inspection Type: Textile Mill Products Stormwater Discharge COC Facility Status: ❑ Compliant 0 Not Compliant Question Areas: ■Storm Water (See attachment summary) Page:1 Permit: NCG170140 Owner -Facility: Guilford Mills Inc Inspection Date: 09/13/2013 Inspection Type: Technical Assistance Reason for Visit: Routine Inspection Summary: Facility is closed. Rescind the permit. No production or production materials are exposed. Page:2 w i I m t Wca-- �� Division of Water Quality / Surface Water Protection NCNCDENR National Pollutant Discharge Flimination System M 0Nmnu NC]gi�CC] RESCISSION REQUEST FORM Cxrw°x"[xr FOR AGENCY USE ONLY DataReceived Year Month I Day Please fill out and return this form if you no longer need to maintain your NPDES stormwater permit. 1) Enter the permit number to which this request applies: Individual Permit (or) Certificate of Coverage N C S 1 7 0 0 0 0 N C G 1 7 0 1 4 0 2) Owner/Facility Information: • Final correspondence will be mailed to the address noted below Owner/Facility Name Guilford Mills, Inc./ former Fuquay Facility Contact Street Address City County Telephone No. Paul R. Bruesch _ 1754 NC Hwy 903 Kenansville Duplin (336) _ 855-879i State NC_ ZIP Code 28349 _ E-mail Address pbruesch@gfd.com Fax: (509) _ 691-3042 3) Reason for rescission request (This is required information. Attach separate sheet if necessary): ® Facility closed or is closing on December 2008 . All industrial activities have ceased such that no discharges of stormwater are contaminated by exposure to industrial activities or materials. ❑ Facility sold to on, If the facility will continue operations under the new owner it may be more appropriate to request an ownership change to reissue to permit to the new owner. ❑ Other: 4) Certification: I, as an authorized representative hereby request rescission of coverage under the NPDES Stormwater Permit for the subject facility. I am fa 'liar wit ormation contained in this request and to the best of my knowledge and belief such information isirde, comple and ccurate. Signature ll� 'Y- Date Auglicr A. III P Corporate Fnvirnmental Manager Print or type name of person signing above Title Please return this completed rescission request form to: 1617 Mail Service Center, Ralegh, North Carolina 27699-1617 Location: 512 N. Salisbury St Ralegh, North Carolina 27604 Phone: 919807-63001 FAX: 919-807-64921 Customer Service: internal: w .nawaterquality.org An Equal Opportunity 1 Atfrmehve Action Employer SW NPDES Permit Coverage Rescission Stormwater Permitting Unit AUIS P, 2a13 NorthiCarolina Naturally 'tO�- W ATF'q _ r April 1, 2008 Mr. Paul Bruesch Guilford Mills, Inc. 200 Dickens Rd Fuquay Varina, NC 27526 zMA ILL E-9 SUBJECT: Compliance Evaluation Inspection Guilford Mills Inc. Permit Number- NCG170140 County — Wake Dear Mr. Bruesch: Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Coleen H. Sullins, Director Division of Water Quality On March 5, 2008, Autumn Hoban, of the Division of Water Quality (DWQ), Raleigh Regional Office, performed a stormwater compliance evaluation inspection of the plant. Mr. Bob Messer assisted me with the inspection and his cooperation was helpful and appreciated. Inspection findings are listed below. Indus;try ;Siie�Descriptionn,,, Guilford Mills Inc. prior to 2005 manufactured yarn. In 2005, it was reported that the plant shut down the manufacturing process. The stormwater runoff and process wastewater generated at such facilities is regulated by General Permit NCG170000. DWQ has therefore issued Guilford Mills certificate of coverage, NCG170140, which became effective on August 1, 2004 and expires on July 31, 2009. The facility has nine stormwater outfalls and a pond on site. Process water is discharged through the sanitary sewer system to the Fuquay Varina WWTP. The facility has two tanks on -site that hold 3,000 gallons of finish oil that have secondary containment and lock out as required. Other bulk oil storage was reported to have been removed last year, tanks emptied, and locked out upon the shut down of the manufacturing process. Waste oil and 55 gallon drums are stored under cover, with containment, and are locked in fenced area. The waste oil is removed from the site by Noble Oil, The facility was in compliance with permit requirements with one exception. It is required that the Stormwater Pollution Prevention Plan be updated annually and the plant should provide an updated plan that reflects the current operations of the plant upon future inspections. The pond on site overflows to an unnamed tributary of Basal Creek. The pond overflow was sampled during the inspection and the results are attached. pH, Conductivity and Dissolved Oxygen were in normal range. 3400 Barrett Drive One Raleigh, North Carolina 27609 NorthCaiolina Phone:919-791-0200 Fax:919-788-7159 Natu"ally FwArF �O 9Q Michael F. Easley, Governor �O G ,•.. + v e s William G. Ross Jr., Secretary y .,North Ca Molina Department of Environment and Natural Resources >_ ...... -{ Coleen H. Sullins, DirgctoF O '< ^-••^•••^^^•�•••"' Division of Water Qualihf It is our goal to insure the quality of the surface waters of this State. Please review the attached report. If you or your staff has any questions, do not hesitate to contact Autumn Hoban at919-791-4200. Sincerely, / Autumn Hoban Enclosures cc: Central files RRO/DWQ Stormwater Compliance Files Stormwater Permitting Unit 3400 Barrett Dive One Raleigh, North Carolina 27609 NorthCaiolina Phone: 919-791-4200 Fax: 919-788-7159 Naturally Permit: NCG170140 SOC: County: Wake Region: Raleigh Compliance Inspection Report Effective: 08/01/04 Expiration: 07/31/09 Owner: Guilford Mills Inc Effective: Expiration: Facility: Guilford Mills Incorporated -Wake 200 Dickens Rd Contact Person: Paul R Bruesch Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related Permits: Fuquay Varina NC 27526 Title: Phone: 336-316-4319 Certification: Phone: Inspection Date: 03/05/2008 Entry Time: 0'1/:0�0 PM Exit Time: 03:00 PM �/ / ,71 '7 Prima Inspector: Autumn Hoban / U " s c�16j 7 '7 7 Primary P t� �— Phone: Secondary Inspector(s): Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Textile Mill Products Stormwater Discharge COC Facility Status: ■ Compliant ❑ Not Compliant Question Areas: 0 Storm Water (See attachment summary) Page: 1 Permit: NCG170140 Owner -Facility: Guilford Mills Inc �, f Inspection Date: 03/05I2008 Inspection Type: Compliance Evaluation Reason for Visit: Routine Inspection Summary: The facility should update the Stormwater Pollution Prevention Plan to reflect the current operations of the plant. Page:2 46 Permit NCG170140 Inspection Date: 03/05/2008 Owner - Facility: Guilford Mills Inc Inspection Type: Compliance Evaluation Reason for Visit: Routine Stormwater Pollution Prevention Plan Does the site have a Stormwater Pollution Prevention Plan? # Does the Plan include a General Location (USGS) map? # Does the Plan include a "Narrative Description of Practices'? # Does the Plan include a detailed site map including outfall locations and drainage areas? # Does the Plan include a list of significant spills occurring during the past 3 years? # Has the facility evaluated feasible alternatives to current practices? # Does the facility provide all necessary secondary containment? # Does the Plan include a BMP summary? # Does the Plan include a Spill Prevention and Response Plan (SPRP)? # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? # Does the facility provide and document Employee Training? # Does the Plan include a list of Responsible Party(s)? # Is the Plan reviewed and updated annually? # Does the Plan include a Stormwater Facility Inspection Program? Has the Stormwater Pollution Prevention Plan been implemented? Comment: The Plan has not been updated since 2000. In 2005, manufacturing ended at the plant, changing operations significantly. The plan is required to be updated annually and be reflective of the current operations. There are two tanks on -site that hold 3,000 gallons of finish oil. These tanks contain secondary containment as required. Other tanks on the site were reported cleaned out and are no longer in use. Waste oil and 55 gallon drums are stored with secondary containment, under cover, and in a locked, fenced area at the facility and are picked up by Noble Oil. Qualitative Monitoring Has the facility conducted its Qualitative Monitoring semi-annually? Comment: Analytical Monitoring Has the facility conducted its Analytical monitoring? # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? Comment: No vehicle maintenance was reported on -site. Yes No NA NE m❑❑❑ m ❑ ❑ ❑ ❑❑■❑ ■ ❑ ❑ ❑ ■❑❑Ell ■ ❑ ❑ ❑ IN ❑ ❑ ❑ IN ❑ ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ ❑■❑❑ ■ ❑ ❑ ❑ ■❑❑❑ Yes No NA NE ■ ❑ ❑ ❑ Yes No NA NE Permit: NCG170140 Owner - Facility: Guilford Mills Inc Inspection Date: 03/05/2008 Inspection Type: Compliance Evaluation Reason for Visit: Routine Permit and Outfalls # Is a copy of the Permit and the Certificate of Coverage available at the site? # Were all outfalls observed during the inspection? # If the facility has representative outfall status, is it properly documented by the Division? # Has the facility evaluated all illicit (non stormwater) discharges? Comment: All stormwater outfalls were observed during the inspection. The SW flows to a pond onsite and to a UT of Basal Creek. The pond on -site was sampled during the inspection. Results are attached. The process water on -site and the cooling tower blowdown are not discharged, they are sent to the Fuquay Varina Wastewaster Treatment Plant. / ", Yes No NA NE ■ ❑ ❑ ❑ ■ Cl ❑ ❑ ■ ❑ ❑ ❑ ■ ❑ ❑ ❑ Page: 4 County. WAKE River Basin _ pF Vr A Report To RROSP _ �� E Collector: A HOBAN ` Region: RROi4�» `ivc:u?'" Sample Matrix: SURFACEWATER;,Iji `: I�y11v , Loc. Type: RIVER/STREAM --....- Emergency Yes/No •-- ._. - _.-^lir:r:� �C ��(,E � COC Yes/No : i\1 ,:n ..._,.._:., r-_.__._ VisitlD Sample ID: AB26762 PO Number# 8W1133 Date Received: 02/18/2008 Time Received: 09:10 Labworks LogmlO CGREEN Dale Reported: 3/3/08 Report Generated: 03/03/2008 Loc. Descr.: GUILFORD POND Location ID: NCG170140 Collect Date: 02/15/2008 Collect Time:. 15:00 Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to wvvw.dwglab.org under Staff Access A -Value reported is the average of two or more determinations B1-Countable membranes with <20 colonies; Estimated B2- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated B4-Filters have counts of both >60 or 80 and < 20: Estimated BS-Too many colonies were present; too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination, Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated N 1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB N3-Estimated concentration is < PQL and >MDL NE -No established PQL P-Elevated PQL due to matrix interference and/or sample dilution Q1-Holding time exceeded prior to receipt at lab. Q2- Holding time exceeded following receipt by lab PQL- Practical Quantitalion Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected XI- Sample not analyzed for this compound I Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 10 NC (DWQQ Laboratory Section Results Sample ID - AB26762 Location ID: NCG170140 Collect Dale'. 02116/2008 _ Loc. Descr.: GUILFORD POND Collect Time:: 16:00 Visit ID vvt: i POL Result Qualifier Units Sample tempemtufe at receipt by lab 3.6 •C DSAUNDERS JGOODwIN Method Reference V18108 2118108 Grasse and Oil In liquid 10 10 U mg/L MIBRAHIMI CGREEN Method Reference EPA1664A 225108 228108 NH3 as N In liquid 0.02 0.26 mglL as N MAJAYI CGREEN Method Reference Lac10-107-06 1-J 222108 228/08 Total l9eldahl N as N In liquid 0.2 0.76 J2 mg/L as N GBELK CGREEN Method Reference Lachatl07-06-2-H 226/08 2/29/08 NO2+NO3 as N In liquid 0.02 0.10 mg/L as N MAJAYI CGREEN Method Reference Lacl0-107-04-1-c 2121108 228108 Phosphorus_tofal as P In liquid 0.02 0.04 mglL as P MAJAYI CGREEN Method Reference Lac10-115-01-1EF 2/20108 226108 7440-22A Ag by ICPMS 5.0 5.0 U,J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222708 229108 ra UY1, r- Ju 1/0 J6 ugfL DSTANLEY ESTAFFORD Method Reference EPA 200.7 221/08 229/08 7440-38-2 As by ICPMS 5.0 5.0 U,J6 u9/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 2/22/08 229108 7440-38-3 Ba by ICP 10 14 J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 221r08 2129108 744041-7 Be by ICP 5.0 5.0 U/J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200,7 W 1108 229108 wvy." uJu J.b J6 mgfl- DSTANLEY ESTAFFORD Method Reference EPA 200 7 _ 2MM8 229/08 7440-43-9 Cd by ICPMS 1.0 1.0 U,J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 2122/08 2/29/OB 7440-08-0 Cobalt by ICPMS 50 50 U/J6 ugf- DSTANLEY ESTAFFORD Method Reference EPA200.8 221108 2/29108 7440-47-3 Cr by ICPMS 10 10 U,J6 u9/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222/08 2/29/08 7440-50-8 Cu by ICPMS 2.0 2.0 U,J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 2/22/08 272910E Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 10 NC D WQ Laboratory Section Resufts Sample ID aL326762 Location ID: NCG170140 Collect Date: 02/15/2008 Loc. Descr.: GUILFORD POND Collect Time:'. 15:00 Visit ID f UAJ * Analyte Name PQL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA 2003 2121108 229M8 7439-97-6 Hg 245.1 0.2 0.20 U/J6 ug/L JJURGEVICH ESTAFFORD Method Reference EPA 245.1 2/20/08 2/29/08 7440-09-7 Kby ICP 0.10 22 J6 mg/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 2/21/08 2/29M 7439-93-2 LI ICP 25 25 U J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 220108 229/08 7439-95,1 Mg by ICP 0.10 1.1 J6 ni DSTANLEY ESTAFFORD Method Reference EPA 200.7 221/08 W9108 7439-96-5 Mn by ICPMS 10 16 J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 221/08 2R9m 7440-234 Na by ICP 0.10 4.1 J6 mg/L DSTANLEY ESTAFFORD Method Reference EPA 2007 221/08 229m 7440-02-0 NI by ICPMS 10 10 U, J6 ugf- PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222108 229/08 7439-92-1 Pb by ICPMS 10 10 U,J6 U91L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222108 2129/08 778249-2 Se by ICPMS 5.0 5.0 U, J6 ug[L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222108 229/08 7440-62-2 V by ICP 25 25 U/J6 ugfL DSTANLEY ESTAFFORD Method Reference EPA 200.7 221108 229to8 7440-66-6 Zn by ICPMS 10 21 J6 ug(L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222I08 2f29/08 VUL Volatile Organic In liquid _TITLE_ ug/L ATERRY RKELLING Method Reference EPA50301624/8260 M11108 2/20108 75-78-1 Dlchlorodl0uoromethane 1.0 Not detected ugfL ATERRY RKELLING Method Reference EPA5030/624M260 2/1 SIM Moles 74-87-3 Chlommethane 0.50 Not detected ugfL ATERRY RKELLING Method Reference EPA503016248260 2/18/08 mom 75-01-4 Vinyl Chloride 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18108 2/20/08 74-83-9 Bromomethane 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2118108 220IOa 75-00-3 Chloroethane 0.50 Not detected ugfL ATERRY WELLING Method Reference EPA5030/62418260 2111908 2120/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 3 of 10 NC Q)rWQ Laboratory Section 12esuCts Sample ID AB26762 Location ID_ NCGI70140 Collect Date: 02/15/2008 Loc. Descr.: GUILFORD POND Collect Time:: 15:00 Visit ID i,Aa « Anaiyre Name PQL Result Qualifier Units Analyst/Uafe Approved By (Date Method Reference EPA5030162418260 2118/08 M0108 75-35-4 1,1-0Ichloroethene 0.25 Not detected ugll ATERRY RKELLING Method Reference EPA5030/62418260 2/18108 2/20/08 75-09-2 Methylene Chloride 10 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2119/08 2/20/08 156-60-5 trans-1,2-0Idiloroethene 0.25 Not detected ug/L ATERRY RKELLING ' Method Reference EPA503W62418260 N18108 220MB 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected u91L ATERRY RKELLING Method Reference EPA503W62418260 y18108 226/08 75-34-3 11,1-0ichloroethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA503016241B260 211 SIN 220/08 156-59-4 cls-1,2-Dlchloroethene 0.25 Not detected uglL ATERRY RKELLING Method Reference EPA5030162418260 2/18108 220/08 74-97-5 Bromochloromethene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118108 212OMS 67-66-3 Chloroform 0.25 Not detected uglL ATERRY RKELLING Method Reference EPA50301624M260 2118108 22W08 590-20-7 2,2-0khloropropane 0.25 Not detected uglL ATERRY RKELLING Method Reference EP ,503W62418260 2/18108 W0108 107-06-2 1,2-0khloroethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18= 220/08 71-55-6 1,1,1-Tdchlofoethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118108 W20/08 563-58-6 1,1-01chloropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18N8 mom 56-23-5 Carbon Tetrachlodde 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 2120108 71-43-2 Benzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624M260 V18108 212W0B 74-95-3 Dlbrcmometharle 1.0 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118MB 2/2WDB 78-87-5 1,2-0khlorepropane 0.25 Not detected ugrL ATERRY RKELLING Method Reference EPA5030162418260 2/18/08 220/08 79-01-6 Tdchloroethene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624M260 2118108 2(20108 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 t919) 733-3908 Page 4 of 10 NC ID(WQ Laboratory Section 12esuCts Sample ID AB26762 Location ID: NCG170140 Collect Date: 02/15/2008 Loc. Descr.: GUILFORD POND Collect Time:: 15:00 - Visit ID U.r u Analyte Name PDL Result Qualifier Units AnalysUDate Approved By /Date Method Reference EPA5030162418260 2AW8 220/08 10061-01-5 cls-1,3-DIchbropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 Vlatoit 220/O8 10061-02-6 trans-11,3-DIcNaropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18/OB 2/20/08 79-00-5 1,1,2-TrIchlooethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18/08 moloa too-ao-s lmuerle 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18/08 2220/08 142-28-9 1,3-0Idlbropropane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/I8/08 V20/06 124-46-1 Dlbromochlmmethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162448260 2/18/08 220/08 106-934 (EDB)1,2-DIbromcethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18/08 2/20/08 127-18A Tetrachloroethene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2118108 2/ =8 108-90-7 Chlorobenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162419260 2/18/08 220/08 10041-4 Ethylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 2/20MB 75-25-2 Bromotoml 1.0 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162448260 2/18N8 WOM 108-38-3 m,p-Xylene 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2219108 220108 100-42-5 Styrene 0,25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2//8/08 Maras 79-34-5 1.1,2,2-Tebachloroethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118108 moms 630-20-6 1,1,1,2-Tebachloroethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030t624/8260 2218108 220/08 95-47-6 c-Xylene 0.25 Not detected ug2 ATERRY RKELLING Method Reference EPA50301624/9260 2/18/O8 220108 96-18-0 1,2,3-Trlchloropropane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118/08 mlU Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 5 of 10 NC 1D WQ Laboratory Section Results Sample ID A626762 Location ID: NCG170140 Collect Date: 02/152008 - Loc. Descr.: GUILFORD POND Collect Time:: 15:00 Visit ID Analyte name POL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA5030/624M260 2118/08 woo 108-86-1 Bromobeorane 0.25 Not detected ug(L ATERRY RKELLING Method Reference EPA5030r62418260 7 HVDB 2/20/)8 103-65-1 n-Propylbervene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624111260 2/18108 220108 95-49-8 2-CNorotoluene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 211 W9 220/08 10643-4 4-Chloretoluene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 7118MB 2/20MB 108-67-8 1,3,5-Tdmethylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2//8108 220MB 98-06-6 ten-Butylbenzens 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118408 2n0M8 95-63-6 1,2,4-Tdmethyltlenrene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 220/08 135-98-8 seo-Butylbenzene 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA50301624/8260 2/18/08 2/20M 543-73-1 m401chlorobenzene(1,3) 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030a12418260 2/18N8 2n0108 106-46-7 p-Dlchlorobenzene(1,4) 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162m8260 2119108 M0108 95-50-1 0-01chlofobenzene(1,2) 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA50301624/8260 211&UB 2120/08 99-87-6 p4sopfopylloluerle 0.25 Not detected u g/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 2120/08 104-51-8 n-Btdylbenzene 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA50301624/8260 2/1B4)8 2120/08 96-12-8 1,2-0Ibrort10-3-CHoropropane 2.0 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18ID8 L20/08 120-82-1 1,2,4-TrIchI obenrene 0.50 Not detected ugfL ATERRY RKELLING Method Reference EPA50301624/8260 2/18M8 212WOB 91-20-3 Naphthalene 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPAW30/62418260 2118108 2/20/08 87-68-3 Rexachlorohutadlene 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18r08 2/20/08 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 6 of 10 Location ID: NCG170140 NC DWQ Laboratory Section 12esufts Sample ID 4826M Collect Date: 02/75/2008 - Loc. Descr.: GUILFORD POND Collect Time:: 15:00 ' Visit ID .....r•=....... rtJE Result Qualifier Units Method Reference EPA5030/62418260 2/18/08 V20I08 2-Chloro" vinyl ether - X1 ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2/18108 2/20108 VOC'S BY GC/MS Not detailed ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2118108 V20108 - SemNolatlle Organics (BNAs) In Ilquld _TITLE_ ug/L JSTYLES RKELLING Method Ref efence EPA62518270/3510 2 1/08 2126/08 62-53-3 Anlllne 10 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/827013510 2/21/08 2126108 108-95-2 Phenol 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270n510 2/21108 2n6/08 111-0a-4 Bis(2-chlofoethyl)ether 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 2n1/08 2/26I08 95-57-8 Chlorophenol, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 2/21/08 2n6N8 541-73-1 Dlchlorobenzene, 1,3 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221/08 2126108 10646-7 Dichlorobenzene, 1,4 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62548270n510 D24108 V26I08 100-51-6 Benzyl alcohol 20 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 2121108 226108 95-50-1 Dichlorobenzene, 1,2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270f3510 2121108 2/26108 95-48-7 Methylphenol, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 212mil 2126108 108-60-1 Bis(2chl0rolsopropylethsr 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 2/26108 106�4-5 Methylphenoi, 4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 226108 621-64-7 Ntlitrosodk+ propylamine 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 2/21108 V26108 67-72-1 Hemchloroethane 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221108 2/26108 96-95-3 Nitrobenzene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 2/26108 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 7 of 10 9VC (UWQ Laboratory Section Results Sample 10 AB26762- Location ID: NCG170140 Collect Date: 02/75/2008 ' Loc. Descr.: GUILFORD POND Collect Time:: 15:00 Visit ID - I nnatyre name PQL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA62518270/3510 221/08 226/08 88-75-5 NIbWhenol, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625I827013510 221MB 226/08 105-67-9 Dlrnethylphenoi, 2,4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 - 221108 W6/08 65-85-0 Berizolc add 50 Not detected ugf- JSTYLES RKELLING Method Reference EPA625/8270(3510 2121108 226/08 111-91-1 Bls(2oltiOoethoay)methane 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625M270/3510 2121I08 2/26108 120-83-2 Dichlorophenol, 2,4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 226I08 120-82-1 Tdchlorobenzane, 1,$4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221108 1/26/08 91-20-3 Naphthalene(SV) 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270f3510 2121/08 2261N 10647-8 Chloroantllne, 4- 20 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/138 M15109 87-68-3 Helatillorobutadlene(SV) 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 226/08 59-50-7 Chloro-3-methyl phenol, 4- 20 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270f3510 221108 226/08 91-57-6 Metirylnaphthalene, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221108 Mwa 7747-4 Helachlorocydopentadlene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221N8 226/O8 88-06-2 Tdchlorophenol, 2,4,6- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/9510 221/08 2261OB 95-95-4 Tdchlorophenol, 2,4,5- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/9270/3510 2I21108 226/08 91-58-7 Chloronaphthalene, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/ 510 221/OS 226/08 88-744 Nltroaniline, 2- 50 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 2/26/08 131-11-3 Dlmethyl phthalate 10 Not defected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 2/21/08 212WB 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 8 of 10 NC D WQ Laboratory Section Xesufts Sample ID AB26762 -- Location ID: NCG170140 Collect Dale: 02/15/2008 Loc. Descr.: GUILFORD POND Collect Time:: 15:00 Visit ID CAS # Analyte Name _ POL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA625/8270r3510 221108 2/26/08 606-20-2 Dinitrotcluene, 2,6- 10 Not detected U91L JSTYLES RKELLING Method Reference EPA62518270/3510 2/24/08 226/08 99-09-2 Nltroanlllne, 3- 50 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/927013510 221/08 MU08 83-32-9 Acenaphthene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 2nlMB 228/08 51-28-5 Dlnitrophenol, 2,4 50 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 22ri/OB 100-02-7 Nltrophenol, 4- 50 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221108 226/08 132-64-9 Dibenrcturan 10 Not detected ug/L JSTYLES RKELLING Method Reference EPAfi25/827013510 221/08 226/Oe 121-14-2 Dlnitrotoluene, 2,4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221108 ME1108 84-66-2 Dlethyl phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 2/26108 7005-72-3 Chlorophenyl phenyl ether, 4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 226/OB 86-73-7 Fluorene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827W5/0 221108 MWIE; 100-01-6 Nltrwrilline, 4- 50 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/827013510 2/21/08 2126MB 534-52-1 Dlnitro-2-rnethyl phenol, 4,6- 50 Not detected J2 ug2 JSTYLES RKELLING Method Reference EPA625/927013510 221/08 226/08 86-30-6 N-nitrosodiphenylamine 10 Not detected ug/L JSTYLES RKELLING Method Reference - EPA625/8270r 510 221108 226/08 104-55-3 Bromophenyl phenyl ether, 4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221108 2726/08 118-74-1 Hexachlorobenzene 10 Not detected ugf- JSTYLES RKELLING Method Reference EPA6251827013510 221/08 226/08 87-86-5 Pentachlorophenol 50 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA6251827Of3510 2121/08 226M 85-01-8 Phenanthrerle 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221108 226108 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 1919) 733-3908 Page 9 of 10 Location ID: NCG170140 NC DWQ Laboratory Section 12esufts Loc. Descr.: GUILFORD POND Visit ID Sample ID AB26762 Collect Date: 02/15/2008 Collect Time:: 15:00 y Anatyte Name POL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA6251827013510 22i/08 2/26108 84-74-2 D14I, yl phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 WWII 226M8 206-44-0 Fluoranthene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270t3510 221/08 226/08 129-00-0 Pyrerle 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/82702510 221/OB 2/26108 85-68-7 Butylbenzyl phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 2121/08 Me= 91-94-1 Dlchloroben2Jdlne, 3,3- 20 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA62518270r3510 221/OB 2/26108 56-55-3 Be=(a)anthracene 10 Not detected uglL JSTYLES RKELLING Method Reference EPA625/8270r3510 Wl= mma 218-01-8 'Chrysene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270l510 221MB 2126= 117-81-7 Bis(2-ethylhexyl)phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221/08 Whine 117-84-0 Dltloctyl phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221108 2/26/08 205-99-2 BenZo(b)IIu0ranthene 10 Not detected ug/L -JSTYLES RKELLING Method Reference EPA6251827013510 221/08 2/26/08 207-08-9 Benno(k)1Iwran1hene 10 Not detected - ugfL JSTYLES RKELLING Method Reference EPA6251827013510 2121108 2/26M8 50-32-8 Berizo(a)pyrene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221108 226/08 193-39-5 hfdeno(1,2,3cd)pyrene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 2/211O8 212WOB 53-70-3 Dlbe=(a,h)anthracene 10 Not detected ug/L JSTYLES RKELLING. Method Reference EPA6251827013510 201108 2261O8 19l-24-2 Ben2:o(g,h,l)perylene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221108 2/26/06 No BN/As detected by GUMS. Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221108 2Q6108 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 10 of 10 COUNTY: RIVER BASIN i-a') e REPORT TO: SHIPPED BY: COLLECTOR(S) Estimated BOD Range: Sad: Chlorinated:_ DIVISION OF WATER QUALITY - LAB FORM W❑ PRIORISAMPLE TYPE TY ❑ AMBIENT ❑ QASTREAM 0 EFFLUENT ❑ COMPLIANCE ❑ CHAIN OF CUSTODY ❑ LAKE ❑ INFLUENT EMERGENCY _ ESTUARY L�ViUNI� 1 ^� ElStation Location: (r /�L7 1-7 C, (L f D Remarks: L'J LC Station q �/ (j /'1 1 - UI Date Begin (yy/mm/dd BOD 310 D mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 #/100 mis Coliform: MF Total 31504 #1100 mis Coliform: Tube Fecal 31615 #/100 ruts Coliform: Fecal Strep 31673 #/100 MIS Residue: Total 500 mg/L Volatile 505 mg/L Fixed 510 mg/L Residue: Suspended 530 mg/L Volatile 535 mg/L Fixed 540 mg/L H 403 units Acidity to pH 4.5 436 mg/L Acidity to pit 8.3 435 mg/L Alkalinity to PH 8.3 415 mg/L Alkalinity to pH 4.5 410 mg/L TOC 680 mg/L Turbidity 82079 NTU Coliforrn Total Tube 31508 #1100 mis COMMENTS: D`te End /mm1 Time Bpon Time Eit Depth -DM, DB, DBM Value Type - A, H,LI 5.<: Chloride 940 mg/L ->< NH3 as N 610 mg/L Chi a: 70953 .- 80 83 Color: pH T Cyanide 720 Fluoride 951 Grease and Oils 556 Hardness Total 900 Specific Cond. 95 MBAS 38260 Phenols 32730 Sulfate 945 Sulfide 745 Bomn: Total 1022 Tannin & Lienin 32: 11 , - X TKN as N 625 NO2 plus NO3 as N 6 P: Total as P 665 C.U. PO4 as P 70507 C.U. P: Dissolved as P 666 c.u. k K- Potassium m8/L Cd-Cadmium 1027 mg/L Cr- Chromium:Total I mg/L Cu-Copper 1042 m Ni- Nickel 1067 mg/I, Pb- Lead 1051 pmhos/cm2 Zn- Zinc 1092 mg/L V- Vanadium pg/L Ag- Silver 1077 ntgtL "-' Ak Aluminum 1105 mg/L `. Be- Beryllium 1012 #g/L Ca -Calcium 916 AWL - Co -Cobalt 1037 1032 _ µg/L Z Fe- Iron 1045 Pooint % (2) Conductance (94O Water T1em; rC (10) D.O. (30000)pH (400) 8.3 Alkalinity (I 5i'' t57 depth m Salinity ppt (480) Pmcipit-In/day (45) Cloud Cover % (32) Wind Dir-Deg (31 Sum Flow Scv /i,!) Alkalinity (431) 4.5 Acidity bidity Severity (13 Wind Vela Lab Number: Date Receivede Time Received : Received By: Data Released Date Reported posite-T, S, B Sample Type C GNXX Li -Lithium 1132 Mg- Magnesium 927 mg/L Mn- Manganese 1055 µg/L Na-Sodium 929 mg/L As- Arsenic:Total 1002 µg/L Se -Selenium 1147 µg/L Hg- Mercury 71900 µg/L Ba-Barium µg/L Organochlorine Pesticides I I Acid Herbicides I Base/Neutral&Acid Extractable Organics TPH Diesel Range Purgeable Organics (VOA bottle req d) TPH Gasoline Ranee LAB USE ONLY remperature m arrival (eC Acidity (82242) jAir Tempt (20) m Sm Depth-fl (64) IStrm Width-R (4) NC DENR/DWQ Laboratory Report to: _ FRO Sample Anomaly Report (SAR) LRb,Number. AB26762 Sample ID: 8W1133 Station Location: NCG170140 County: Wake Region: Neuse ample Type: Stream Priority: Complaint Collector: A. Haban Jate collected: 2/15/08 Date received: 2/I8/08 Date analyzed: Affected Parameter(s): K, Cd, Cr, Cu, Ni, Pb Zn V Ag AI Be Ca Co Fe Li Mg Mn Na As Se Hg Ba Analytical Area (check one): ❑WCH ®METALS ❑NUT []MICRO The following anomalies occurred (check all that apply): []Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ®Sample not chemically preserved properly ®pH out of range (record pH): 6.5 ✓ El Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): Comments: Corrective Action: ❑VOA ❑SVGA . ❑PEST (]Quality Control ❑Instrument failure— no reportable results ❑Analyst error — no reportable results ❑Surrogates ❑None added El Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards ❑Blank contamination ❑QC data reported outside of controls (i.e. QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume []Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used: J6 ' ❑Other (explain): Notification Required'? ❑ Yes ❑ No Person Contacted: Date: Form completed by: S. Goss Lead Chemist Review (initial): ❑BIOCHEM 9?METALS Date: 2/ 18/08 ❑PEST ❑VOA Branch Head Review (initial QA/QC Review (in' QA`. Fwms\Lab mtor,SAR a t/Qg ❑SVGA Logged into database by (initial): �S 1 M3101 A, County: WAKE River Basin Report To RROSP Collector. A HOBAN Region. RRO Sample Matrix: SURFACEWATER Loc. Type: RIVER/STREAM Emergency Yes/No COC Yes/No Vlsi(ID Sample ID. AB26763 , PO Number if 8Wl134 r Date Received. 02/18/2008 r Time Received: 09:10 Labworks LoginlD CGREEN Date Reported: 2/25/08 Report Generated: 02/25/2008 Loc. Descr.: GUILFORD POND -TRIP BLANK Location ID: NCG170160 Collect Date: OT/15/2008 Collect Time:: 15:00 Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations B7-Countable membranes with <20 colonies; Estimated B2- Counts from all filters were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated B4-Filters have counts of both >60 or 80 and c 20; Estimated 85-Too many colonies were present; too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination; Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample, Estimated NI -The component has been tentatively identified based on mass spectral library search and has an estimated value L 13 N3-Estimaled concentration is < PQL and >MDL NE -No established PQL P-Elevated POL due to matrix interference and/or sample dilution Qt-Holding time exceeded prior to receipt at lab. 02- Holding time exceeded following receipt by lab PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected Xt- Sample not analyzed for this compound Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 5 Location ID: NCG170140 NC 1D'WQ Laboratory Section Resufts Loc. Descr. GUILFORD POND -TRIP BLANK Visit ID aampte to Collect Date: Collect Time:: AOLb/ oa 02/15/2008 15:00 t.raa x Analyle Name POL Result Qualifier Units Anal sUDate Ap proved pproved By /Date Method Reference 2/18/08 2/18/08 Volatile Organics In llquid _TITLE_ ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18108 222M8 75-78-1 DIdllorodlellorotnetharre 1.0 Not detected ug(L ATERRY RKELLING Method Reference EPA50301624/8260 2/1=8 2722/08 74-87-3 Chlorometharia 0.50 Not detected ugfL ATERRY RKELLING Method Reference EPA5030/624B260 2JIB= V22MB 75-014 Mnyl Chloride 0.50 Not detected ugfL ATERRY RKELLING Method Reference EPA503WG24/8260 2118/08 222/08 74-83-9 Bromomethane 0.50 Not detected ug(L. ATERRY RKELLING Method Reference EPAS030152418260 2/19108 2122J08 75-00-3 Chloroetharle 0.50 Not detected ugfl- ATERRY RKELLING Method Reference EPA503WG24/8260 211 MS 2122/08 75-69-4 Tdchlorofluoromethane 0.50 Not detected ug(L ATERRY RKELLING Method Reference EPA50301624/8260 2/18/08 222/08 75-35-4 1,1-01chloroetherre 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624M260 2/18/08 222/08 75-09-2 Methylene Chloride 10 Not detected ugfL ATERRY RKELLING Method Reference EPA5030/62418260 2/18108 2/22/08 156-60-5 trans-1,2-0Icfllaroetlrene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPAS030/62418260 2/18108 2122/08 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected ugf- ATERRY RKELLING Method Reference EPAS0301624M260 2/IM8 2t22108 75-34-3 1,1-0khloroetharre 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPAS030162418260 2/18I08 =ffill 156-59A cls-1,2-Dichlorcethene 0.25 Not detected UWL ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 2/22108 74-97-5 Bromochlofofnetharet 0.25 Not detected ug(L ATERRY RKELLING Method Reference EPA503016248260 2/18N8 2122M 67-66-3 Chloroform 0.25 Not deWiced ug/L ATERRY RKELLING _ Method Reference EPA503N624M260 2/1810B W2108 590-20-7 2,2-Dlchloropropane 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA5030/62418260 2118MB V22108 107-06-2 1,2-0Ichloroethane 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA5030162418260 2118109 2122/136 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 5 Location ID: NCG170140 NC (DWQ Ga6oratory Section Xesufts Loc. Descr.: GUILFORD POND -TRIP BLANK Visit ID aampie iu Horn/" Collect Date'. 02/15/2008 Collect Time:: 15:00 11.o Anaryle Name POL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA50301624/8260 2/18108 212208 563-58-6 1,1-Dichl0ropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2118M 2/22108 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 2/22108 71-43-2 Benzenes 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118108 i22108 74-95-3 Dibromomethane 1.0 Not detected ug/L ATERRY RKELLING Method Refefeore EPA5030162418260 211=9 2/22108 78-87-5 1,2-Dlctbropropane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 21181fi8 22MB 79-01-6 Tdclloroethene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 vil3fa8 22M 75-27-4 Bromodbhloromethane 0.25 0.14 N3 ug/L ATERRY RKELLING Method Reference EPA5030/62418260 211808 22MB 10061-01-5 ds-1,3-0Icloropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA 30/624M260 2/18108 222/08 10061-02-6 trans-1,3-0Icloropropene 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA50301624/8260 V18108 222/08 79-00-5 1,1,2-TrIchloroetharle 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118108 222108 108-88-3 Toluene 025 Not detected uglL ATERRY RKELLING Method Reference EPA5030/62418260 WWII 222= 142-28-9 1,3-0Idhioropropane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18108 2/22108 12448-1 Dlbromoehloromelhane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2119108 222/08 106-93-4 (EDB)1,2-0Ituomoethane 0.25 Not detected ug/L ATERRY. RKELLING Method Reference EPA5030/62418260 2118108 222/08 127-18-4 Tetracllofoethene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118108 222/08 108-90-7 Chlorobenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/6248260 2/18/08 222/08 10OAl-4 Ethylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2118108 2/22/09 Laboratory Section>> 1623 Mail Service Center, Raleigh, INC 27699-1623 (919) 733-3908 Page 3 of 5 Location ID: NCG170140 NC CDWQ Laboratory Section Results Loc. Descr.: GUILFORD POND -TRIP BLANK Visit ID .,, a,7re Result - Qualifier aampie lu Collect Date: Collect Time:: AOLb/b3 02/15/2008 15:00 Method Referenw EPA5030162418260 Warm MWEI 108-38-3 m,p.Xylene 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18/08 222/08 100-42-5 Styrene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 =08 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030P62418260 21IMB 222/08 630-20-6 1,1,1,2-Te/rachloroethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624M260 2118/08 M2108 95-47-6 oXylene 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA503N62418260 2/IB/OB 22VO8 96-18-4 1,2,3-Tdchloropropane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2/18108 222/OB 98-82-8 Isopropylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18/08 2/27108 108-86-1 Bromobenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/19/08 2/22108 103-65-1 n-Propyltlenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624M260 2/18/08 V22/08 9549-8 2-Chloroboluene 0.25 NW detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18108 2/22M8 106-43-4 4-Chlorotoluene 0.25 Not detected ug2 ATERRY RKELLING Method Reference EPA50301624/8260 2118/08 222/08 108-67-8 1,3,5-Tdmethylberizene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118108 2/22/OB 98-06-6 tart-Blrtylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 21I8/08 M2/O8 95-63-6 1,2,4-Tdmethylbenzene 0,25 Not detected u9A_ - ATERRY RKELLING Method Reference EPA503016248260 2/18/08 2/22/08 135-98-8 seo-Butylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624eI260 2/18/08 222/08 543-73-1 m-Dichlorobervene(1,3) 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA503016248260 2118108 2/22/08 106-46-7 p-0khlorobenzene(1A) 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPAK30162418260 2118I08 2/22N8 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 4 of 5 Location ID: NCG170140 NC QDWQ Laboratory Section 12esufts Loc. Descr.: GUILFORD POND -TRIP BLANK Visit ID Anaiyte Name Result aampte lu Collect Date. Collect Time:: Abn t,1oa 02/15/2008 15:00 Method Reference EPA503Ut62418260 2118/08 W2108 99-87-6 pasopmpyltoluene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA503062418260 2/18108 V22108 104-51-8 n-Butylbenzene 0,25 Not detected ug/l. ATERRY RKELLING Method Reference EPA503Od62418260 2118108 2/22/08 96-12-8 1,2-Dibmmo-3Chloropropane 2.0 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2118108 2a2/Ofl 120-82-1 1,2,4-Tdchlorohenzene 0.50 Not detected ug(L ATERRY RKELLING Method Reference EPA5030162418260 2118108 WV08 91-20-3 Naphthalene 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 211 Mitt 2a2108 87 68 3 Heachlorobutadlene 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162419260 2/18/08 2/22/08 87-61-6 1,2,3-Tdchleroberizerle 1.0 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 7/18/08 2a2M 2-Chloroethyl vinyl ether - X1 ugtL ATERRY RKELLING Method Reference EPA5030/624/8260 2/19108 2a2/08 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 5 of 5 COUNTY: RIVER BASIN: REPORT TO: t •y SHIPPED BY: COLLECPOR(S) : � % n J Estimated HOD Range: Seed: Chlorinated: DIVISION OF WATER QUALITY - LAB FORM ElSAMPLE TYPE P_ OR'rY rc-�� El AMBIENT QA 11<1-STREAM EFFLUENT COMPLIANCE ❑CHAIN OF CUSTODY �� ,LAKE INFLUENT EMERGENCY / ❑ ESTUARY Fv?] !+ Station Location: �V c G I U, �. (� — �f � r to t �7 4:YY 1 Remarks: , - ( ` 'tZ' t^j is )i'U (. f t Station # - Date Begin (yy/mm/d a-UnrIVIEN IS : Lab Number: Date Received: Time Received: Received By Data Released Date Reported d) r Date End OT/mMdd) 4'Yme _ 'o ,Time End Depth - DM, DR, DBM Value Type - A, H, L Composite-T, S, B Sample Type G C GNXX Chloride 940 mg/L NH3 as N 610 nrg/L Li- Lithium 1132 ug/L Chl a: 70953 µg/L TKN as N 625 mg/L Mg- Magnesium 927 mg/L NO2 plus NO3 as N 630 mg/L Mn- Manganese I055 µg/L P: Total as P 665 mg/L Na- Sodium 929 mg/L Color: Tme 80 C.U. 1`64 as P 70507 mg/L As- Arsenic:Towl 1002 pg/L Color: H) 83 C.U. P: Dissolved as P 666 m Color: H 7.6 82/L Sc- Selenium 11 0 µg/L C.U.cuK- Potassium Cyanide 720 m mg/L Hg- Mercury 7190 pg/L Y>/L Cd- Cadmium 1027 pg/L Ba- Barium pg/L Fluoride 951 mg/L Cr- Chmmium:Tosl 1034 pg/L Organochospho Pesticides Formaldehyde 71880 mg/L Cu- Copper 1042 pg/L Organophsphorus Pesticides Grease and Oils 556 mg/L Ni- Nickel 1067 Hardness Total 900 P/L mg/L Pb- Lead 1051 µg/L Acid Herbicides Specific Cond. 95 pmhcs/em2 Zn- Zinc 1092 µg/L MBAS 38260 mg/L V- Vanadium pg/LWDiesel ral&Acid Extractable Organics Phrnols 32730 pg/L Ag- Silver 1077 µg/Ll Range / Sulfate 945 mg/L Al- Aluminum 1105 '>^' Sulfide 745 mg/L Be- Beryllium 1012Bomn: Total 1022 µB/LOrganics (VOA bottle req'd) µg/L - Ca- Calcium 916 mg/Lline RangeTannin & Lignin 32240 µg/L Co- Cobalt 1037 µg/L Gasoline Range Hexavalrnt Chrormum 1032 µg/L Fe- Iron 1045 ,wa..,._ Point %(2) Conductance(94) Water Temp-C(10) D.O. (3000) [� depth in Salinity ppt 480) Precipit-In/day (45) Cloud Cover % (32) G.0 (400) , 8.3 Alkalinity (822, 4�. id Dir-Deg (3gStrm Flow Sev (135 Alkalinity (431) 14.5 Acidity Severity LAB USE Y npera[ttre arrival (°C): j SUM Depth-R (64) IShm Width-R (4) Point %(2) Conductance(94) Water Temp-C(10) D.O. (3000) [� depth in Salinity ppt 480) Precipit-In/day (45) Cloud Cover % (32) G.0 (400) , 8.3 Alkalinity (822, 4�. id Dir-Deg (3gStrm Flow Sev (135 Alkalinity (431) 14.5 Acidity Severity LAB USE Y npera[ttre arrival (°C): j SUM Depth-R (64) IShm Width-R (4) County WAKE River Basin Report To RROSP Collector: A HOBAN Region: RRO Sample Matrix SURFACEWATER Loc. Type: RIVER/STREAM Emergency Yes/No CDC Yes/No OF Vf A7r /� REVISED ¢ qRi Lli r�J'^T VisrtlO Loc. Descr.: GUILFORD POND MAR - 7 2008 Sample ID. AB26762 PO Number# 8W1133 Date Received 02/18/2008 Time Received. 09:10 Labworks LoginlD CGREEN Date Reported 3/3/08 Report Generated' 03/03/2008 II Location ID: NCG170140 I Collect Date: 02/1512008 I Collect Time:: 15:00 Sample Depth SampleQualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwqlab.org under Staff Access A -Value reported is the average of two or more determinations Bt-Countable membranes with 120 colonies; Estimated B2- Counts from all fliers were zero. B3- Countable membranes with more than 60 or 80 colonies; Estimated B4-Filters have counts of both >60 or 80 and < 20; Estimated B5-Too many colonies were present, too numerous to count (TNTC) J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination, Estimated J6-The lab analysis was from an unpreserved or improperly chemically preserved sample, Estimated N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB N3-Estimated concentration is < PQL and >MDL NE -No established PQL P-Elevated POL due to matrix interference and/or sample dilution Q1-Holding time exceeded prior to receipt at lab. Q2- Holding time exceeded following receipt by lab PQL- Practical Ouantitalion Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected X1- Sample not analyzed for this compound Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 10 NC D WQ Laboratory Section Resufts Sample ID A826762 Location ID: NCG170140 Collect Date: 02/15/2008 Loc. Descr.: GUILFORD POND Collect Time:: 15:00 , Visit ID GAO u Analyte Name POE Result Qualifier Units Analyst/Date Approved By /Date Sample temperature at receipt by lab 3.6 °C DSAUNDERS JGOODWIN Method Reference 2/18/08 2A W08 Grease and Oil In liquid 10 10 U mg/L MIBRAHIMI CGREEN Method Reference EPA1664A 225/08 228/08 NUI NH3 as N In liquid 0.02 0.26 mg/L as N MAJAYI CGREEN Method Reference LacIO-107-06-1-J 222108 212W08 Total Ige1dahl N as N In liquid 0.2 0.76 J2 mgfL as N GBELK CGREEN Method Reference Latlwt107-06-2-1-1 226108 229/08 NO2+NO3 as N In liquid 0.02 0./0 mg/L as N MAJAYI CGREEN Method Reference Lacl O-107-04-1-c 221/08 228/08 Phosphorus total as P In liquid 0.02 0.04 mg/L as P MAJAYI CGREEN Method Reference LaclD-115-01-1 EF 220108 226MB 7440-22-0 Ag by ICPMS 5.0 5.0 U. J6 Ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222108 WIM08 7429-90-5 AI by ICP 50 170 J6 U91L DSTANLEY ESTAFFORD Method Reference EPA 2007 221/O8 229/08 7440-38-2 As by ICPMS 5.0 5.0 U,J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 2122108 2/29M 7440-38-3 Be by ICP 10 14 J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 221/38 229M 7440A 1-7 Be by ICP 5.0 5.0 U/J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 221/O8 2/29108 7440-70-2 Ca by ICP 0.10 3.5 J6 mglL DSTANLEY ESTAFFORD Method Reference EPA 200.7 221/08 229/O8 744043-9 Cd by ICPMS 1.0 1.0 U, J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222/08 229/Od 7440-48-4 Cobalt by ICPMS 50 50 U/J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 221/08 229/0a 7440-47-3 Cr by ICPMS 10 10 U,J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222/08 2/29/06 7440-50-8 Cu by ICPMS 2.0 2.0 U, J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 2/22/08 229/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 10 Location ID: NCG170140 NC D WQ Laboratory Section Results Sample ID Collect Date: AB26762 02/75/2008 Loc. Descr.: GUILFORD POND Collect Time:: 15:00 r, Visit ID 1 11 « stnatyce name PUL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA 2003 221N8 229108 7439-97-6 Hg 245.1 0.2 0.20 U/J6 ug/L JJURGEVICH ESTAFFORD Method Reference EPA 245.1 220108 229108 744M9-7 Kby ICP 0.10 2.2 J6 M91L DSTANLEY ESTAFFORD Method Reference EPA 200.7 221/OS M9108 7439-93-2 U ICP 25 25 UJ6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200 7 220/08 229108 7439-95A Mg by ICP 0.10 1.1 J6 mg/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 221MR 2/29/08 7439-96-5 Mn by ICPMS 10 16 J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.8 221MS 229/08 7440-234 Na by ICP 0.10 4.1 J6 mg/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 221/08 229108 7440-02-0 NI by ICPMS 10 10 U, J6 U91L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222/08 229108 7439-92-1 Pb by ICPMS 10 10 U, J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222/08 229/08 778249-2 Be by ICPMS 5.0 5.0 U. J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 222/08 229/08 7440-62-2 V by ICP 25 25 U/J6 ug/L DSTANLEY ESTAFFORD Method Reference EPA 200.7 221108 229108 7440-66-6 Zn by ICPMS 10 21 J6 ug/L PGAUTHIER ESTAFFORD Method Reference EPA 200.8 Volatile Organics In liquid Method Reference EPA503W624/8260 222/08 229/OB _TITLE_ ug/L ATERRY RKELLING Dims 2201W 75-78-1 DlMlorodiiucromethane 1.0 Not detected ug/L ATERRY RKELLING Method Reference EPA5030I624/8260 2/18108 Z120/08 74-87-3 Chloromethane 0.50 Not detected ug/L ATERRY RKELLING method Reference EPA503W62418260 2/18/08 220M 75-01-4 Vinyl Chloride 0.50 Not detected tg/L ATERRY RKELLING Method Reference EPA50301624/8260 2/19/08 220100 74-83-9 Bromomethane 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA503W62418260 211 W08 220MB 75-00-3 Chloroethane 0.50 Not detected U91L ATERRY RKELLING Method Reference EPA5030062418269 2/18/O8 220/08 Laboratory Sectiori 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 3 of 10 WC T)WWQ Laboratory Section ResultsCollect ID A626762 Location ID: NCG170140 Collect Dale: 02/16/2008 Loc. Descr.: GUILFORD POND r Collect Time:: 15:00 Visit ID i,..o « nnatyle Name PQL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA5030162418260 211 a108 220108 75-35-4 1,1-Dichlorcethene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/19M 220/08 75-09-2 Methylene Chloride 10 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18108 2/20108 156-60-5 trans-1,2-0IdBoroeftne 0.25 Not detected ugfL ATERRY RKELLING I Method Reference EPA503W624/8260 2I18I08 220108 1634-04-4 Methyl Ten -Butyl Ether 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 211 W08 220/08 75-34-3 1,1-0Ictlloroethane 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA5030162418260 2/1 a= 220108 156-59-4 cls-1,2-Dlchloroethene 0.25 Not -detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18/08 220108 . 74-97-5 Bromochloromethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118/08 W0108 67-66-3 Chloroform 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA5030162418260 2118/O8 220/08 590-20-7 2,2-0Ichloropropam 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118108 220/08 107-06-2 1,2-0Irhloroethane 0.25 Not detected ugA- ATERRY RKELLING Method Reference EPA503W62418260 211 Mill M0108 71-55-6 1,1,1-Tnchloroehame 0.25 Not detected uglL ATERRY RKELLING Method Reference EPA5030162418260 2118/08 Warne 563-58-6 M-Dihloropropene 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPAS030/62418260 2/18I08 220/08 56-23-5 Carbon Tetrachlorlde 0.25 Not detected u9fL ATERRY RKELLING Method Reference EPAS030/62418260 211 aft 220/08 71A3-2 Benzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPAS030/62408260 2/18/08 220108 74-95-3 Dibromomethane 1.0 Not detected ug1L ATERRY RKELLING Method Reference EPA50301624M260 2/18/O8 220108 78-87-5 1,2-Dlchloropropane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624M260 W8108 2 offie 79-01-6 Tdchloroetherre 0.25 Not defected ugf- ATERRY RKELLING Method Reference EPA5030/624M260 2118108 220/08 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 4 of 10 NC DWQ Laboratory Section 12esurts Sample ID AB26762 Location ID: NCG170140 ,- Collect Date: 02/152008 Lot. Descr.: GUILFORD POND Collect lime:'. 15:00 Visit ID �Aa w Analyte Name PQL Result Qualifier Units Analyst/Date Approved By /Date Method Reference EPA5030/624/8260 2118108 2120/00 10061-01-5 cl -1,3-Dlchloropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18108 220108 10061-02-6 trans-1,3-0Idlloropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18f08 220108 79-00-5 1,1,2-Tdchloroethane 0,25 Not detected ug/L ATERRY RKELLING Method Reference EPA60301624/8260 2/18N8 220/08 108-88-3 Toluene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18108 220/08 142-28-9 1,3-0Ichloropropene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 Visors 220/08 124-48-1 Dibromochlorcmethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2118rbe 220/08 106-934 (EDB)1,2-DIbromoethane 0.25 Not detected ugfL ATERRY RKELLING Method Reference EPA5030/624/8260 2118108 220108 127-184 Tebacincroethene 0.25 - Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2118/08 220/08 108-90-7 Chlorobenzene 0,25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18108 2120/08 100-414 Ethylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 211810E 220108 75-25-2 Bromoform 1.0 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2/18108 220108 108-38-3 m,p-Xylene 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2118108 2120/08 100-42-5 Styrene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2/18p8 220/08 79-34-5 1,1,2,2-Tetrachloroethane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 211=8 2/20/08 630-20-6 1, 1,1,2-TetracNoroethane 0.25 Not detected -- ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118/08 2/20/08 95.47-6 o-Xylene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2/18108 2/2U/08 96-18-4 1,2,3-Tdchloropropane 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18108 220/08 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 5 of 10 NC DWQ Laboratory Section 12esufts Sample ID A626762 Location ID: NCG170140 Collect Date: 02/15/2008 Loc. Descr.: GUILFORD POND Collett Time:: 75:00 L Visit ID CAS # Analyte Name POL Result Qualifier Units Analyst(Date Approved By /Date Method Reference EPA5030/62418260 Via= 2/20M 108-86-1 Bromobenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62418260 2J18108 2/20108 403-65-1 n-Propylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2/18/08 2noroe 9549-8 2Chlorctoluene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118/08 M0108 10643-4 4CNorotoluene 0.25 Not detected ug(- ATERRY RKELLING Method Reference EPA503W62418260 2I18108 2120108 108-67-8 1,35-Tdmettybertzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2J18108 220N8 98-06-6 tert-Butylbenzene 0,25 Not detected uglL ATERRY RKELLING Method Reference EPA503W62418260 7J18108 220108 95-63-6 1,2,4-Tdnrethylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2/18108 2120/08 135-98-8 s Butylbenzene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA503016241R260 2/18N8 220108 543-73-1 m-0trhlorobenzerle(1,3) 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2118N8 WWII 10646-7 p-Dichbrobenzene(1,4) 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030162418260 2118/08 220/08 95-50-1 0-DIc111000benzene(1,2) 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA5030;62418260 2118/08 220MB 99-87-6 p4sopropy8oluene 0.25 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2118/08 220/08 104-51-8 n-BtdylbeMWe 0.25 Not detected uglL ATERRY RKELLING Method Reference EPA50301624/8260 2A8108 220/08 96-12-8 1,2-DIbmrno- - loropropane 2.0 Not detected ug/L ATERRY . RKELLING Method Reference EPA503W62418260 2/18/OB 220108 120-82-1 1,24-TrIchlorobenzene 0.50 Not detected uglL ATERRY RKELLING Method Reference EPA50301624/8260 2118/O8 220108 91-20-3 Naphthalene 0.50 Not detected uglL ATERRY RKELLING Method Reference EPA503W624/8260 2118/08 Maine 87-68-3 Hexachlorohutadiere 0.50 Not detected ug/L ATERRY RKELLING Method Reference EPA50301624/8260 2118/08 220MB Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 6 of 10 NC DWQ Laboratory Section ResultsSample ID AB26762 Location ID: NCG170140 Collect Date: 02/152008 Loc. Descr.: GUILFORD POND Collect Time:'. 15:00 Visit ID SEM POL Result Qualifier Units Method Reference EPA5030162418260 2118/08 2W08 2CNoroethyl Any! ether - X7 ug/L ATERRY RKELLING Method Reference EPA5030/624/8260 2118/08 220I08 VOCS BY GCJMS Not detected ug/L ATERRY RKELLING Method Reference EPA5030/62419260 Semlvoladle Organics (BNAs) In liquid Method Reference EPA625/8270EI510 2/18/08 220I08 _TITLE_ ugfL JSTYLES RKELLING 221/08 226/08 62-53-3 Anlllne 10 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/827013510 2 Iw 226/08 108-95-2 Phenol 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 2126108 111-44-4 Bls(2-chlorcethyl)ether 10 Not detected ugfl- JSTYLES RKELLING Method Reference EPA625/82702510 2121/08 2126/08 95-57-8 Chlorophenol, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 2261M 541-73-1 Dichlorobenehtne, 1.3 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 226/08 106-46-7 Dichlorobenzene, 1,4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 W6108 100-51-6 Benzyl alcohol 20 Not detected ugfL JSTYLES RKELLING Method Reference EPA625/827013510 221/08 226I08 95-50-1 Dichlonobenzene, 1,2- 10 Not detected u9tL JSTYLES RKELLING Method Reference EPA625/8270/3510 221/08 226/08 95-48-7 Methylphanol, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 22l/08 226/08 108-60-1 Bis(2chlorolsopropyl)ether 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221108 226/08 106-44-5 Methylphenol, 4- 10 Not detected ugfL JSTYLES RKELLING Method Reference EPA625B270n5I0 22l/08 V26I08 621-64-7 NKtitrosodl-0-propylamine 10 Not detected uWL JSTYLES RKELLING Method Reference EPA625/8270r 510 221/08 2/26108 67-72-1 Hemchloroethane 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270f3510 22l= 2116/08 98-95-3 Nitrobenzene 10 Not detected ugf- JSTYLES RKELLING Methotl Reference EPA6251827013510 221/08 2126M Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 7 of 10 NC (DWWQ Laboratory Section 12esufts Sample ID A826762 Lccation ID: NCG170140 Collect Date: 02/15/2008 Loc. Descr.: GUILFORD_POND Collect Time: 15:00 0 Visit ID Method Reference EPA62543270/3510 221108 226/08 88-75-5 Nitrophenol, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270n510 221/08 2/26108 10b-b/-9 Dlmethylphenol, 2,4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 2/21I08 226ro8 65-85-0 Benzoic acid 50 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221/08 2/26/08 111-91-1 Bls(2-hlomethoMmethane 10 Not detected ugfL JSTYLES RKELLING Method Reference EPA6251827013510 221108 226/08 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625182702510 221/08 226/08 120-82-1 Tdchlorobenzene, 1,2,4- 10 Not detected ugfL JSTYLES RKELLING Method Reference EPA6251827013510 2121/08 226/08 91-20-3 Naphthalene(SV) 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 2nl= 2/26108 106-47-8 Chlorcanlllne, 4- 20 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/82702510 221108 22N08 87-68-3 Helotlllorobutadlerle(SV) 10 Not detected ugfL JSTYLES RKELLING Method Reference EPA6251927013510 221108 226/08 59-50-7 Chloro-3-rrlethyl phenol, 4- 20 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 2/21/08 W6108 91-576 Methylnaphthalene, 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625M270/3510 221/08 2/26108 77-47-4 Helachlorocyclopentadiene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/82706510 221/08 226108 88-06-2 Tdchloruphenol, 2,4,6- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625182700510 221= 2126M 95-95A Trlchlorophenol, 2,4,5- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270f3510 221/08 2f26/08 91-58-7 Chloronaphthaleri 2- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 2/2WW 88-74-4 Niuoaniline, 2- 50 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 226M8 131-11-3 Dlmethyl phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 22 V08 226108 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 8 of 10 Sample ID A626762 NC 1�rWQ Ga6oratory Section Results Location ID: NCG170140 Collect Date: 02/15/2008 Loc. Descc: GUILFORD POND Collect Time:: 15:00 �. Visit ID Analyte name Result Qualifier Method Reference EPA625/8270f3510 221108 226/08 606-20-2 Dlnitrotoluene, 2,6- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 226/08 99-09-2 Nltr0anlllne, 3- 50 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 226ro8 83-32-9 Acenaphthene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 226/08 51-28-5 Dlnibophenol, 2,4- 50 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270/3510 221I08 226/08 100-02-7 Nitrophenol, 4- 50 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270r3510 2121108 226108 132-64-9 Dlbenzofuran 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 226/08 121-14-2 Dlnitrctoluene, 2,4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 2/21/08 226/O8 84-66-2 Dlethyl phthatate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 M&08 7005-72-3 Chlorophenyl phenyl ether, 4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221108 MU08 86-73-7 Fluo2ne 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62SM27013510 221/08 226/OB 100-01-6 Nltroanlllne, 4- 50 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 226108 534-52-1 01nitro-2-methyl phenol, 4,6- 50 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 2/2&08 86-30-6 N-nttrosodlphenylamine 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270r3510 221/08 226/08 101-55-3 Bromophenyl phenyl ether, 4- 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270r3510 221N8 2126108 118-74-1 Hefachlorobenzene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625M270r3510 221108 226/08 87-86-5 Pentachlorophenol 50 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/8270r3510 22IM8 226/08 85-01-8 Phenanthrene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270r3510 221108 226/08 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 9 of 10 NCG770140 Sample ID AB26762 NC �`f'�Q Laboratory Section 12esuCts Location ID: Collect Date: 02/15/2008 Loc. Descr.: GUILFORD POND Collect Time:: 15:00 Visit ID 1-. n vmaryce name PQL Result Qualifier Units Analyst/Date Aooroved Rv /Date Method Reference EPA62518270r3510 221108 _ 2/28108 84 74 2 DI-Ibutyl phthalate. 10 Not detected ugfL JSTYLES RKELLING Method Reference EPA625182702510 221/08 226/08 206-44-0 Fluoranthene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270n510 221/08 2/26/08 129-00-0 Pyrene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/82700510 221108 226/08 85-68-7 ButylbeW phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625M27013510 221/08 226/08 91-94-1 DIchlorobenzldlne, 3,3' 20 Not detected J2 ug/L JSTYLES RKELLING Method Reference EPA625/8270n510 221M8 226/08 56-55-3 Benzo(a)anthracene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 2126108 218-01-9 Chrysene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827013510 221/08 226MB 117-81-7 Bls(2-ethylhexyl)ph1halate 10 Not detected LVL JSTYLES RKELLING Method Reference EPA62518270f3510 221MB 226/08 117-84-0 DI-n-octyl phthalate 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270l3510 221/08 W6108 205-99-2 Benzo(b)fluonmthene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA62518270/3510 221108 226MB 207-08-9 Benzo(k)0ttoranthene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/827013510 221/08 226/08 50-32-8 Ben (a)pyrene 10 Not detected u g/L JSTYLES RKELLING Method Reference EPA625182702510 221/08 226M8 193 39 5 Indeno(1,2,3-cd)pyrene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA6251827D/3510 221108 226M8 53-70-3 Dibenzn(a,h)anthracene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625182702510 221108 2261o8 191-24-2 Be=(g,h,l)perylene 10 Not detected ug/L JSTYLES RKELLING Method Reference EPA625/8270n510 221108 W6108 No RN/As defected by GCJMS. Not detected ugf- JSTYLES RKELLING Method Reference EPA625182702510 221108 226108 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 10 of 10 COUNTY: RIVER BASIN: AICIIASC REPORT TO: SHIPPED BY: COLLECTOR(S) :'" -, ; r.7 /j Estimated BOD Range: Seed: Chlorinated: DIVISION OF WATER QUALITY - LAB FORM W❑ SAMPLE TYPE PRIORI rt�- ❑ AMBIENT ❑ QA IX i STREAM ❑ EFFLUENT ❑ COMPLIANCE ❑ CHAIN OF CUSTODY f❑LAKE ❑ INFLUENT ❑ EMERGENCY ❑ ESTUARY Station Location: Station # Date Begin (yY/mm/dd BOD 310 a,) r~ mg/L COD High 340 1 mg/L COD Low 335 mg/L Colifmm: MF Fecal 31616 #/100 mis Coliform: MF Total 31504 #1100 mis Coliform: Tube Fecal 31615 #/100 mis Coliform: Fecal Strep 31673 #/100 mls Residue: Total 500 mg/L Volatile 505 M9tL Fixed 510 mg/L Residue: Suspended 530 mg/L Volatile 535 mg/L Fixed 540 mg/L H 403 units Acidity to pH 4.5 436 mg/L Acidity to pH 8.3 435 mg/L Alkalinity to pH 8.3 415 mg/L Alkalinity to pH 4.5 410 mg/L TOC 680 mg/L Turbidity 82079 N1U Coliform Total Tube 31508 #/100 mis LUMMEN7N: Remarks Date End (YY/mm/dd) Time Bqgin Time End Depth - DM, DB, DBM Value Type- A, H, L i Chloride 940 mg/L >< NH3 as N 610 mg/L Chi a: 70,953 g/L \ ' TKN N 62 P . as 5 mg/L X NO2 plus NO3 as N 630 mg/L P: Total as P 665 rng/L Color: True 80 C.U. PO4 as P 70507 mg/L Color: (pH ) 83 C.U. P: Dissolved as P 666 mg/L Color: pH 7.6 82 C.U. 7< K- Potassium mg/L Cyanide 720 mg/L < Cd- Cadmium 1027 PY/1- Fluoride 951 mg/L Cr- Chromium:Total 1034 pg/L Formaldehyde 71880 mg/L Cu- Copper 1042 µg/L, Grease and Oils 556 mg/L Ni- Nickel 1067 pPJL Hardness Total 900 mg/L Pb- Lead 1051 µg/L Specific Cond. 95 µmhos/cm2 Zn- Zinc 1092 µg/L, MBAS 38260 mg/L ': V- Vanadium pg/L Phenols 32730 µg/L Ag- Silver 1077 µg/I, Sulfate 945 mg/L %'' AI- Aluminum 1105 pg/L Sulfide 745 mg/L <— Be- Beryllium 1012 µg/L Boron: Total 1022 pg/L Ca- Calcium 916 mg/L Tannin & Lignin 32240 µg/L " Co- Cobalt 1037 µ8/1 Hexavalrnt Chrorrdum 1032 µg/L i Fe- Iron 1045 ue/I. Point % (2) Conductance (94) Water Temp-C (10) D.O. (30�0/)) C 7 0, depth m Salinity plat (480) Precipit-Wday (45) Cloud Cover% (32) (400) 8.3 Alkalinity (8224 id Dir-Deg (31 Strm Flow Sev (135 Alkalinity(431) 14.5Acidity Lab Number: Date Receivedl Time Received: Received By : Data Released Date Reported posite-T, S, B Sample Type C �^ GNXX Li- Lithium 1132 t� ug/L Mg- Magnesium 927 mg/L Mn- Manganese 1055 pg/L Na- Sodium 929 mg/L As- Arsenic:Total 1002 µg/L Se- Selenium 1147 µg/L Hg- Mercury 71900 ua/L Organophosphoms Pesticides Acid Herbicides Base/Neumd&Acid Extractable Organics TPH Diesel Range Purgeable Organics (VOA bottle req'd) TPH Gasoline Range TPH/BTEX Gasoline Range Phytoplankton LAB USE ONLY remperature m arrival (eC): Acidity (82242) Air Temper (20) m Strm Depth-fi (64) IStrm Width-ft (4) NC DENRIDWQ Laboratory Report to: _ _RRO Sample Anomaly Report (SAR) LaVumber: AB26762 Sample ID: 8WI133 'Station Location: NCG170140 County: Wake Region: Neuse 'ample Type: Stream Priority: Complaint Collector: A. }Iaban Jate collected: 2/15/08 Date received: 2/18/08 Date analyzed: Affected Parameter(s): K, Cd, Cr, Cu, Ni, Pb, Zn, V, Ag, AI, Be Ca Co Fe Li MR Mn Na As Se Hg Ba Analytical Area (check one): ❑WCH ®METALS ❑NUT ❑MICRO The following anomalies occurred (check all that apply): ❑Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑M islabeled as to tests, preservatives, etc. []Holding time expired ❑Prior to receipt in lab ❑After receipt in lab []Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ®Sample not chemically preserved properly ®pH out of range (record pH): 6.5 ✓ ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): Comments: Corrective Action: ❑VOA ❑SVOA ❑PEST ❑Quality Control []Instrument failure— no reportable results ❑Analyst error— no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Intemal standards ❑Blank contamination ❑QC data reported outside of controls (i.e. QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used: J6 ' ❑Other (explain): Notification Required'? ❑ Yes ❑ No Person Contacted: Date: Form completed by: S. Goss Lead Chemist Review (initial): ❑BIOCHEM O) METALS Date: 2/18/08 ❑PEST ❑VOA_ Branch dead Review (initial : QA/QC Review (ia 'al): QA\FDO s\LaWrnory'SAR a/fit/Qg ❑SVGA Logged into database by (initial): CS 10/D/01dtx Report to: _RROSP NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) 112*Nu+nber: Station Location: AB26762 6' '(�f-4 Sample Type: SURFACE H2O Date collected: 2/15/2008 Affected Parameter(s): TKN Sample ID: tjc& 1701 LJO County: WAKE Region: RRO Priority: ROUTINE Collector: Date received: 2/18/2008 Date analyzed: Analytical Area (check one): ❑ WCH ❑METALS ENUT []MICRO The following anomalies occurred (check all that apply): ❑Samples ❑Improper container used []VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference []Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): A. HOBAN _ 2(zL V ❑VOA ❑WARD ❑PEST ❑SVOA []Quality Control ❑Instrument failure — no reportable results []Analyst error— no reportable results ❑Surrogates ❑None added []Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards []Blank contamination EQC data reported outside of controls (e.g., QCS. LCS) []Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration []Elevated detection limits due to: ❑Insufficient sample volume Comments: LFB OUTSIDE QUALIFICATION LIMIT OF 90% TO 110%. RESULTS REPORTED WITH A J2 QUALIFIER. Corrective Action: is I, ccla,�r•1 ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until:. ®Sample reported with qualification. Data qualification code used:J2 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: OWENDOLYN Lead Chemist Review (initial): ®BIOCHEM MO ❑METALS ❑PEST ❑ VOA Branch Head Review (initial): QA/QC Review (initial): Date: 2/27/2008 ❑SVGA Logged into database by (initial): IA\F..,s eb.,.,or \SA 10 Wilb, PM Work Order # 002528 Type PM Priority 3 PM # 000203*4 Status Completed Start Date 9/18/2007 Printed 2/15/2008 Rating 27 Department BAM Reported By DENISE BAKER (DBAK 11:13 AM 911812007 jp roject # Material Account 100-5400-6515-4000 Equipment # SW/DRAINS Department Location REP 53 Required 12/17/2007 Phone Number Labor Account 100-5400-6515-4000 Area Equipment Description PLANT/GROU STORMWATER DRAINS Interval Quarter Month Weekpay Freauencv Last Done 1 180 2/6/2008 PM Description STORMWATER POLLUTION PREVENTION Meter Work Description STORMWATER POLLUTION PREVENTION INSPECT ALL THE OUTFALLS AT THE FUQUAY PLANT DURING DRY WEATHER AND DURING A RAINFALL EVENT.THE ASSOCIATE PERFORMING THESE INSPECTIONS WILL BE TRAINED BY THE CORPORATE ENVIRONMENTAL MANAGER TO OBSERVE THE OUTFALLS FOR COLOR,ODOR, SOLIDS,FOAM,OUTFALL STAINING AND VISIBLE SHEENS.THE ASSOCIATE WILL ALSO INSPECT ALL STORMWATER STRUCTURES AND CONVEYANCES TO MAKE SURE THEY ARE IN WORKING ORDER A RECORD OF THIS INSPECTION AND ANY SUBSEQUENT MAINTENANCE ACTIVITIES , PERFORMED WILL BE MAINTAINED WITH THE STORMWATER POLLUTION PREVENTION PLAN (SPPP) LOCATED IN THE PLANT MANAGERS OFFICE. THESE RECORDS TO BE MAINTAINED FOR 5 YEARS. A FORM FOR RECORDING INFORMATION FROM THE INSPECTION IS AVAILABLE IN THE SPPP.DOCUMENT THE DATE AND TIME OF INSPECTION AND A NARRATIVE DESCRIPTION OF THE PLANT'S STORMWATER SYSTEM, DOCUMENTATION OF THIS VISUAL MONITORING WILL BE MAINTAINED WITH THE INSPECTION REPORT. IF ANY PROBLEMS ARE NOTED DURING THE INSPECTIONS, NOTIFY THE PLANT MANAGER. Task Task Description 1 INSPECTION OF STORMWATER DRAINS Task CP Craft Procedures Start Foreman Shift Persons Hrs/Person Pick Tickets Completed 1 1 NA 09/18/07 1 1 2.00 02/06/08 Employee Task Date Shift Craft Secured Date Time Restored Date Time Hours Completed By Date 2/6/2008 Approved By DENISE BAKER (DBAK 1:13 AM 9/18/2007 NO INFO Work Performed Page 1 of 1 PM Work Order # 001999 Type PM Priority 3 Rating 27 groject # Material Account 100-5400-6515-4000 PM # 000204*1 Status Completed Start Date 6/14/2007 Printed 2/15/2008 Department BAM Reported By DENISE BAKER (DBAK 07:30 AM 5/30/2007 Required 6/14/2007 Phone Number Labor Account 100-5400-6515-4000 Equipment # Department Location Area Equipment Description Meter SW/DRAINS REP 53 PLANT/GROU STORMWATER DRAINS Interval Quarter Month Week pay Frequency Last Done 1 365 2/6/2008 PM Description STORMWATER POLLUTION PREVENTION TRAINING Work Description STORMWATER POLLUTION PREVENTION TRAINING REVIEW STORMWATER POLLUTION PREVENTION PLAN WITH ALL MAINTENANCE PERSONNEL. Task Task Description 1 REVIEW STORMWATER POLLUTION PLAN Task CP Craft Procedures Start Foreman Shift Persons Hrs/Person Pick Tickets Completed 1 1 MECH 06/14/07 1 1 1.00 02/06/08 Employee Task Date Shift Craft Hours Secured Date Time Restored Date Time Completed By Date 2/6/2008 Approved By DENISE BAKER (DBAK 7:30 AM 5/30/2007 Work Performed NO INFO Page 1 of 1 . PM # 000204 Revision 1 2/15/2008 WO Type PM Priority 3 Department BAM Approved By FQVDMB 8/1/2006 E ii e t # Department Location Area Equipment Description SW/DR INS REP 53 PLANT/GROUN STORMWATER DRAINS Interval Quarter Month Week Day Frequency Completed Due Date . 0 365 2/6/2008 6/13/2008 Labor Account Code 100-5400-6515-4000 Material Account Code 100-5400-6515-4000 Test ID Type Equipment # Test Description Status Procedures Procedure Description Procedure Purpose PM Description STORMWATER POLLUTION PREVENTION TRAINING Work Description STORMWATER POLLUTION PREVENTION TRAINING REVIEW STORMWATER POLLUTION PREVENTION PLAN WITH ALL MAINTENANCE PERSONNEL. Task Task Description 1 REVIEW STORMWATER POLLUTION PLAN Task Craft Procedures Foreman Shift Persons Hours Total Hrs Total Cost 1 MECH 1 1 1.00 1,00 16.97 Part Number Description Quantity Unit Cost Item Cost Total Hrs 1.00 Total Labor 16.97 Total Parts 0.00 Total Cost 16.97 Page 1 of 1 GP Ma Te Work Order History By Machine - Excluding PMs Work Work Performed Start Comp- Problem Description Department Downti Est Hours Est Cost Comments = DRY User CMC Date 03/28/05 Component = Condition = Comments = WET 086164 User BAM Date 10/19/05 06/2210 10/19/0 STORMWATER POLLUTION BAM 28595 5 5 PREVENTION TRAINING 6 1.00 16.97 Component = Condition = Comments = NO INFO 086376 User BAM Date 10/19/05 06/29/0 10/19/0 STORMWATER POLLUTION BAM 2696:0 2.00 5 5 PREVENTION 6 0.00 Component = Condition = Comments = NO INFO 087481 User CMC Date 02/23/05 02/22/0 02/23/0 STORMWATER POLLUTION BAM 2254:3 2.00 0-00 5 5 PREVENTION 6 Component DRAIN Comments =CMC TRAINED 088808 TRAINING HELD ON 08/28/06 09/28/0 09/29/0 STORMWATER POLLUTION BAM 0.00 0.00 6 6 PREVENTION. TRAINING ROD MASHBURN STACY FERGUSON RANDY GAY ELCIE NASH ROB PRINCE JIM STEVENSON CALVIN MCCOY - STEVE WEAVER DONNIE WIGGINS EDDIE POOLE _ CHARLES GILES EDDIE DENNIS ETTRICK SPEED DENISE BAKER TERRYJONES KEITH MANGUS ROSS STEENSTRA BOBBURNS 089125 DRY INSPECTION COMPLETE 0812810 09101/0 STORMWATER POLLUTION BAM 0.00 0.00 6 6 PREVENTION WET INSPECTION COMPLETE 31 records processed 2/15/2008 1:39:01 Phl Actual 'Actual Cost r 0.00 0.00 000 0.00 4.00 0.00 0.60 10A8 2.00 33-94 Equipment # _ "SW/DRAINS" and Status = "COMP" and Type <> "EQP" and Type <> "OTHR" Guilford Mills Fuquay GP Ma Te Work Order History By Machine - Excluding Pbls Work Work Performed Start Comp. Problem Description Department Downti Est Hours Est Cost 001307 SVV/DRAINS 02/05/0 04/08/0 STORMWATER POLLUTION BAM 2.00 0.00 7 7 PREVENTION Stormwater pollution Dry weather 2/28/2007 1. Unspeced all outfalls 2. Cut 4 small saplings 3. All outfalls appear to be - Wet weather 4/8/2007 1. Inspected all outfalls 2. All look good 001999 NO INFO O6/14/0 02106/0 STORMWATER POLLUTION 7 8 PREVENTION TRAINING 002528 NO INFO 09/18/0 02/06/0 STORMWATER POLLUTION 7 8 PREVENTION 035401 User THJ Date 10/09/96 10/09/9 12/1119 STORMWATER POLLUTION 6 6 PREVENTION Component = DRAIN/LINE Comments = User THJ Date 12/09/96 Component = DRAIN/LINE Comments = NO PROBLEM 038632 User THJ Date 02/14/97 02114/9 03/10/9 STORMWATER POLLUTION 7 7 PREVENTION Component = DRAIN/LINE Comments =RAIN FALL User THJ Date 03/07/97 Component = DRAIN/LINE Comments =DRY WEATHER 043535 User THJ Date 07/31/97 07131/9 07/31/9 STORMWATER POLLUTION 7 7 PREVENTION Component = DRAIN/LINE Comments =SYSTEM DRAIN BY THE POND, I SEE FROM THE CHIP HOLDING THE RIP -RAP, BUT STILL THE 048531 User THJ Date 02/16/98 02/16/9 02/19/9 STORMWATER POLLUTION 8 8 PREVENTION Component = DRAIN Comments = NO User THJ Date 02/27/98 Component = DRAIN Comments = DRY 053278 User THJ Date 08/27/98 08/14/9 08/27/9 STORMWATER POLLUTION 8 8 PREVENTION Component = DRAIN Comments =ALL NO VISIBLE SEENS DURING 056470 User THJ Date 02/12/99 02/10/9 02/12/9 STORMWATER POLLUTION Equipment # _ "SW/DRAINS" and Status = "COMP" and Type <> "EQP" and Type <> "OTHR" Guilford Mills Fuquay 211512008 1:39:01 Phl Actual 4cmal�Cost 2.00 F 33.94 r BAM 1.00 16.97 0,00 0.00 BAM 2.00 0.00 0.00 0.00 REP 1503:1 250 0.00 4.00 0-00 5 REP 79230 2.50 0.00 2.00 0.00 REP 3208 2.50 0.00 2,50 0,00 REP 64718 2.50 0.00 2,50 0.00 REP 360,51 2,50 0.00 2.00 0,00 REP 56:40 2.00 0.00 2.00 0,00 GP Ma Te Work Order History By Machine - Excluding PMs Work Work Performed Start Comp. Problem Description Department Downti Est Hours Est Cost 9 9 PREVENTION Component = DRAIN Comments = ONE WORK WAREHOUSE #1 DOWN 058596 User THJ Date 06/16/99 06/19/9 06/18/9 STOMWATER POLLUTION REP 4852 9 9 PREVENTION TRAINING 1.00 16,97 Component =EQUIPMENT Comments =TRAINING FOR 059427 User THJ Date 08/17/99 08117/9 08/17/9 STORMWATER POLLUTION REP 15256 2,00 9 9 PREVENTION 0,00 Component = DRAIN Comments = 062128 User THJ Date 02/21/00 02121/0 03103/0 STORMWATER POLLUTION REP 547:18 0 0 PREVENTION 2.00 0.00 Component = DRAIN Comments = DRY User THJ Date 02/28/00 Component = DRAIN Comments =WET 063968 User THJ Date 08/16/00 08116/0 08/16/0 STOMWATER POLLUTION REP 1508:2 0,00 0 0 PREVENTION TRAINING 7 0.00 = Component EQUIPMENT Comments = 065011 User THJ Date 08/31/00 0813010 09/05/0 STORMWATER POLLUTION REP 14355 2.00 0.00 - 0 0 PREVENTION Component = DRAIN Comments = DRY WET INSPECTION, NO SHEENS 067299 User THJ Date 03/02/01 03/02/0 03/16/0 STORMWATER POLLUTION REP 383:52 2.00 1 1 PREVENTION 0.00 Component = DRAIN Comments = User THJ Date 03/15/01 Component = DRAIN Comments = BOTH DRY AND 068498 User THJ Date 06/19/01 06/19/0 06/20/0 STOMWATER POLLUTION REP 175:20 1.00 16.97 1 1 PREVENTION TRAINING Component =WATER Comments =COVERED 069512 User THJ Date 09/17/01 0911710 09/2010 STORMWATER POLLUTION REP 19851 2.00 0.00 1 1 PREVENTION Component = DRAIN Comments = NO VISUAL User THJ Date 09/20/01 Component = DRAIN _ Comments ALL SYSTEMS 071604 User THJ Date 03/15/02 03/15/0 03115/0 STORMWATER POLLUTION REP 120:56 2,00 0.00 2 2 PREVENTION Component =DRAIN Equipment # = "SW/DRAINS" and Status = "COMP" and Type <> "EQP" and Type <> "OTHR" Guilford Mills Fuquay 2/15/2008 1:39:01 PM Actual 'Actual Cost A 46.00 780,62 2,00 000 2-00 000 6.00 101.82 3.00 0.00 2.00 0.00 2,00 33.94 2.00 0.00 2.00 0.00 GP Ma Te Work Order History By Machine - Excluding PMs 2/15/2008 1:39:01 P61 Work Work Performed Start Comp. Problem Description Department Downti Est Hours Est Cost Actual ? Cost Comments = 'Actual M User THJ Date 03118/02 Component =DRAIN r Comments = 072642 User THJ Date 06/18/02 06/17/0 06125/0 STOMWATER POLLUTION THJ 319:33 1.00 2 2 PREVENTION TRAINING 16.97 2.00 33.94 Component = DRAIN Comments =COVERED 073573 User THJ Date 09/16/02 09/16/0 09116/0 STORMWATER POLLUTION THJ 2042:3 2.00 0,00 2 2 PREVENTION 3 1.00 0.00 Component =DRAIN Comments =WET 075937 User BAM Date 03/20/03 03/20/0 03/26/0 STORMWATER POLLUTION BAM 33531 2.00 0.00 2.00 0.00 3 3 PREVENTION Component INSPECTION Comments = 1. DIRT IN 2. CHIPS IN STORMWATER " 3. OUT FALLS COLOR IS 077108 User BAM Date 06/24/03 06/2410 06/27/0 STORMWATER POLLUTION BAM 1180:5 1.00 16.97 2,00 33.94 3 3 PREVENTION TRAINING 3 Component =INSPECTION Comments =ALL PREVENTION TRAINING TRAINING User REP Date 06/25/03 Component = Condition = Comments =ALL TRAINING ALONG WITH 078555 User BAM Date 10/06/03 10106/0 10/09/0 STORMWATER POLLUTION BAM 2691:3 2.00 0.00 2.00 0.00 3 3 PREVENTION 5 Component =INSPECTION Comments = User BAM Date 10/08/03 Component = Condition = Comments = 080664 User THJ Date 03/16/04 03116/0 03125/0 STORMWATER POLLUTION BAM 1679:2 2.00 0,00 2.00 0.00 -4 4 PREVENTION 6 Component =DRAIN Comments = WET User THJ Date 03/25/04 Component = DRAIN Comments = DRY " 081806 User Date 04/20/05 06/07/0 04/20/0 STORMWATER POLLUTION BAM 76065 1.00 16.97 0.00 0.00 4 5 PREVENTION TRAINING 7 Component = Condition = Comments =SEVERAL 083298 User CMC Date 03/21/05 03/2110 03/2910 STORMWATER POLLUTION BAM 45200 2,00 0.00 2.00 0,00 4 5 PREVENTION 1 Component =INSPECTION Equipment # _ "SW/DRAINS" and Status = "COMP" and Type <> "EQP" and Type <> "OTHR" Guilford Mills Fuquay „ F W ATF, 7 r~ Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources 12/13/2002 Alan W. Klimek, P.E. Director Division of Water Quality CERTIFIED MAIL RETURN RECEIPT REQUESTED ' Jimmy Summers'`'''\ Guilford Mills, Inc PO Box 26969 Greensboro NC 27419 SUBJECT: NOTICE OF VIOLATION AND REVOCATION FOR NON PAYMENT cp PERMIT NUMBER NCG170140 �\ Guilford Mills Incorporated -Wake r' Wake COUNTY Dear Permittee: Payment of the required annual administering and compliance monitoring fee of $80.00 for this year has not been received for the subject permit. This fee is required by Title 15 North Carolina Administrative Code 2H.0105, under the authority of North Carolina General Statutes 143-215.3(a)(1), (1a) and (1b). Because this fee was not fully paid within 30 days after being billed, this letter initiates action to revoke the subject permit, pursuant to 15 ncac 2H.0105(b) (2) (k) (4), and G.S. 143-215.1 (b) (3). Effective 60 days from receipt of this notice, subject permit is hereby revoked unless the required Annual Administering and Compliance Monitoring Fee is received within that time. Discharges without a permit are subject to the enforcement authority of the Division of Water Quality. Your payment should be sent to: N.C. Department of Environment and Natural Resources Division of Water Quality Budget Office 1617 Mail Service Center Raleigh, NC 27699-1617 If you are dissatisfied with this decision, you have the right to request an administrative hearing within Thirty (30) days following recipt of this notice, identifying the specific issues to be contended. This request must be in the form of a written petition conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North Carolina, 27611-7447. Unless such request for hearing is made or payments received, revocation shall be final and binding. If you have any questions, please contact: Mr. Ken Schuster, Raleigh Water Quality Regional Supervisor, (919) 571-4700. Sincerely, Alan W. Klimek, P.E. cc: Supevisor, Water Quality Permits and Engineering Unit Raleigh Regional Office County Health Department P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled / 10% post -consumer paper W State of North Carolina Department of Environment and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary Kerr T. Stevens, Director July 28. 1999 JIMMY SUMMERS GUILFORD MILLS INC.-FUQUAY-VARINA PLANT P.O. BOX 26969 GREENSBORO, NC 27419 Dear Permittee: 7"L •, NCDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES Subject: Reissue - NPDES Stormwater Permit Guilford Mills Inc.-Fuquay-Varina Plant COC Number NCG 170140 Wake County In response to your renewal application for continued coverage under general permit NCG 170000. the Division of Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6. 1983. The following information is included with your permit package: * A copy of general Stormwater permit NCG170000 * A Stormwater Pollution Prevention Plan (SPPP) Certification Form. Completion of this form is required to certify that you have developed and implemented the SPPP as per the conditions of the permit. This form must be completed and returned to the Division within 30 days of receipt of this letter. DO NOT SEND the SPPP with the signed form. * Five copies of the Analytical Monitoring form and five copies of the Qualitative Monitoring form * A copy of a Technical Bulletin for the general permit which outlines changes in the permit, key requirements. and addresses frequently asked questions • A Certificate of Coverage Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package please contact Tony Evans of the Central Office Stormwater and General Permits Unit at (919) 733-5083, ext. 584 Sincerely, Ley for Kerr T. Stevens cc: Central Files Stormwater and General permits Unit Files Raleigh Regional Office 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone 919-733-5083 Fax 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG170000 CERTIFICATE OF COVERAGE No. NCG170140 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute t43-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, GUILFORD MILLS INC.-FUQUAY-VARINA PLANT is hereby authorized to discharge stormwater from a facility located at GUILFORD MILLS INC.-FUQUAY-VARINA PLANT 200 DICKENS RD FUQUAY VARINA WAKE COUNTY to receiving waters designated as a UT of Basal Creek in the Neuse River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, 11, Ill, IV, V, and VI of General Permit No. NCG170000 as attached. This certificate of coverage shall become effective August 1, 1999. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day July 28, 1999. for Kerr 1'. Stevens, Director Division of Water Quality By Authority of the Environmental Management Commission State of North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary A. Preston Howard, Jr., P.E., Director April7, 1995 Jimmy Summers Guilford Mills Inc. P.O. Box 26969 Greensboro, NC 27419 I F."A 1�FEE HNR Subject: General Permit No. NCG 170000 Guilford Mills Inc. COC NCG170140 Wake County Dear Jimmy Summers In accordance with your application for discharge permit received on March 2, 1995, we are forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. Please take notice that this certificate of coverage is not transferable except after notice to the Division of Environmental Management. The Division of Environmental Management may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any question concerning this permit, please contact MR. ANTONIO EVANS at telephone number 919/733-5083. Sincerely, riv !�,vi: fbit A. Preston Howard, Jr. P.E. cc: --Raleigh Regional Office P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-7015 FAX 919-733-2496 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DIVISION OF ENVIRONMENTAL MANAGEMENT GENERAL PERMIT NO. NCG170000 CERTIFICATE OF COVERAGE No. NCG170140 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Guilford Mills, Inc. is hereby authorized to discharge stormwater from a facility located at Guilford Mills, Inc. 200 Dickens Road Fuquay-Varina, NC Wake County to receiving waters designated as an unnamed tributary to Basal Creek in the Neuse River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV of General Permit No. NCG170000 as attached. This certificate of coverage shall become effective April 7, 1995. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day April 7, 1995. A. Preston Howard, Jr., P.E., Director Division of Environmental Management By Authority of the Environmental Management Commission APEX B MI. 5255 W NE 695 .696 50' HOLLY SPRINGS 2.1 MI. (APEX) Q; 1) IIOI �� i� •.� 1 '(�Q�✓ �h 1 \ �� 3V—i �� / � 1��` � 1 m I -. ry �j• .`«6 '� \ Y (♦ r 11I3 BM �Jj- / i•l 438a Tower -------------- 1.+��-II _I_ I,��I —1� . �♦ ��=r �� JAI" 1P. I L43a. _ . , II I`IP i' I � \�• . J.�♦ ice\.'' �. _ �/ 1399 Y-� �. Im 1.1 `�'✓ 1 .. �, er'no faldi ens' / )� a COU _ 71 Go Cree4��✓��_i�` C o n <61 _r - /r• •..1 w I�Ovr r _ 9 10 •moo'. �� '-� � /' � -! .�1� —. o •:s f. � �i _ ✓ tiWi ..•ui� I Imo104. , t✓^ \�� C �i.. ` I y� r �1 . T'`I¢Bo- �I c -77 1 / yT \ �`� pI• r \ ( .. V '/•I 1 r ` C_ l 1__ 'aGFrN 11' \_ _ <6T- MOS Id _/�' 11 � - �� A ��/ �, . � � d � � � i - i� •J. - • � �, - n i i 1103 1.