NCG120056_COMPLETE FILE - HISTORICAL_20140128

h
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
NCGW IaDO5 h
DOC TYPE
/HISTORICAL FILE
DOC DATE
El ���y l�� nU
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG120000
Date submitted December 27, 2013
CERTIFICATE OF COVERAGE NO. NCG120056
FACILITY NAME: Upper Piedmont Regional Landfill
COUNTY: Person
PERSON COLLECTING SAMPLES: G. Duhon
LABORATORY: Pace Analytical Lab Cert. # 67
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' January (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
®Other: WS-IV, NSW
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
n No discharge this period?Z
Outfall No.
Date Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Chemical Oxygen Demand
Fecal Coliform
Total Suspended Solids
Benchmarks =__>
-
-
120 mg/L
1000 count per 100 mL
100 mg/L or 50 mg/L
003
01/14/14
0.6
Not Analyzed
99
Not Analyzed
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
' See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -
numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX".
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012
Page 1 of 2

q, W REPUBLIC
Q%13 SERVICES
January 28, 2014
Mr. John Holley, PE Sent via Electronic Transmission
Regional Engineer
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral and Land Resources
Land Quality Section
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Re: January 2014 DMR
Upper Piedmont Environmental Landfill
9650 Oxford Road, Rougemont, NC 27572
NCG120056
Dear Mr. Holley,
On behalf of the Upper Piedmont Regional MSW Landfill, Republic Services is transmitting a
Discharge Monitoring Report in response to the Tier II activities required for fecal coliform at
Outfall 003 at the referenced site. This is the second consecutive monthly sample for fecal
coliform at Outfall 003 that is below the benchmark value.
Based on the analytical results from the past two months and the information previously
provided by letter dated December 27, 2013 (copy attached), Republic Services requests the
cessation of monthly sampling for fecal coliform from Outfall 003 on a monthly basis. -
Thank you in advance for your consideration of this request. I can be reached at [phone]
with any questions.
Sincere y,
,/ G. -
Matt Einsmann, P.E.
Republic Services of NC, LLC
Cc: Mr. Greg Duhon, Upper Piedmont Environmental (electronic copy)
Mr. Bradley Bennett, DEMLR Stormwater Permitting (hard copies)
1220 Commerce St SW
Conover, NC 28613
828.695-2055 • Fax [phone]
www.republicservices.com

Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
0 No discharge this period?2
Date Sample.:F44-hour
rainfallOutfall
No.:
Collectedamount
Non polar O&G/TPH by
-
Total5uspended3
mo/dd/yr) ;;
3
:Inches -.:-.;`?
EPA-?1664 (SGT-HEM
.15mg/L
3006 LorSO,mg/L
003
12/09/13
0.5
<5.0
14.7
Footnotes from Part A also apply to this Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS: - - - - -
• A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS.- SEE PERMIT PART II SECTION B: -
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS.. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK. EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALP. YES-.❑ NO El.,
IF YES, HAVE YOU CONTACTEDTHE:DWQ REGIONAL OFFICE? YES .❑ NO ❑ - - -
REGIONAL OFFICE CONTACT NAME: - -
Mail an oriainal and one copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files - - - -
1617 Mail Service Center_
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:.
"I certify, under penalty of law, that this document and all -attachments -were prepared under my direction or supervision In accordance with -a system designed to
assure that qualified personnel properlygather and evaluate the information submitted. Based on my inquiry ofthe.person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is; to the best of my. knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false.information, including the possibility of fines and imprisonment foreknowing violations.
(Signature of Permittee)
Permit Date: 11/1/2012-10/31/2017
6 J� 2oi4
(Date)
SWU-248, last revised 10/25/2012
_Page 2 of 2 . -

aceAnalytical
miwPa�a'aAe.arn
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 1 of 1
Laboratory. Report.
Mt. Greg Duhon -
- - - Report Date: 12/23/2013
.. Upper Piedmont Environmental.
Date Received: 12/09/2013 _
9650 Oxford Rd.
Rougemont, NC 27572
Project: TANK A/OUTFALL 3
....
Pace Project No.: 92182405
-
Sample: TANKA '_ Lab ID:
92182406001 Collected: 12/09/1313:50 Matrix: Water
Parameters Results ..Units.
. .Report Limit.. "'Analyzed .. Qualifiers -
Cyanide 0.0069 mg/L
- - - 0.0050 12120/1310:43 -
Sample: OUTFALL3 - Lab ID:
92182405002 Collected: 12109/1313:45 Matrix: Water -
Parameters Results. -
Units Report Limit- Analyzed Qualifiers
Total Petroleum Hydrocarbons 'ND mg/L
- . 5.0 12/1111312:52 '
Fecal Coliforms 224 CFU/100
mL 1.0 .12/09/13 16:13
Total Suspended Solids - 14.7 mg/L
2.5 12/13/13 11:37
Chemical Oxygen Demand 36.0 mg)L.
25.0 12Y23/1311 :45
by:
Reviewed
Tabilha M Dacaf
[e-mail]
-
Raleigh Certification IDs
- -
6701 Conference Drive Raleigh, NC 27607 -
North Carolina Bioassay Certification #: 16 - -
North Carolina Wastewater Certification #: 67 _
North Carolina Drinking Water Certification #: 37731
Charlotte. Certification IDs -
9800 Kincey Ave: Ste 100, Huntersville, NC 28078 -
Flo-ridaINELAP Certification #: E87627 -
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84 -
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221 -
South Carolina Certification #: 99006001
-
- Asheville Certification lDs
2225 Riverside Dr., Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 -
South Carolina Certification #: 99030001 .
Massachusetts Certification V. M-NCO30 -
West Virginia Certification #: 356 - - - -
North Carolina Drinking Water Certification #: 37712
VirginiaNELAP Certification #: 460222 -
Page 1 of 3

V V�.1111 111C11V V..-
/ - F-RAL-CS-001-rev.01 Pece AshevIika Quality Omce k
Client Name' .w9p=.�'
Where Received: ❑ HUntersville ❑ Asheville Q Eden ,� Raleigh
Courior(Circlo): Fed'a UPS USPS Client Commercial Pace Other
Custody Seal on CoolcrlBox present: ❑ yeslff no Seals Intact:. es ❑ P4
Packing Material: ❑, Bubble Nhap Bubball�gJ age Nonne Other - -
Circle ThennometorUsed IR Guit SNi'122065167Typa of lee: We Blue None (]Samples on ice, cooing Process lla' begun.
IR Gim Bock U SN 122d6537,�,
Tomp Correctwn.Fictor Add/ ubtr, t
Corrected Cooler Tells C Biological Tissue is Frozen: ro. NIP
. Dateond lnitla $o person rxamiPin9
P� contents;
1 emp should be above freezing to VC, Comments:
Chain of. Custody Present:
Yes No ONIA 1.
Cliain of Custody Filled Out
Yu .DNo ONIA 2. . .
Chain of Custody Relinquished:
Yu ONo,-. OeuA 3.
Simples -Name &SIgnaturecirs COO: -
Yes ONO ..OWA. 4.
Samples Anived within Hold Time:
es ON. bWA 6.
Short Hold Time Adalysis:(<72hr)i
Yes ON.OWA 6. v C V I
Rush Turn Around Time Requested:
. OYes.BFlo OWA 7.
Sufficient Volume:
I 4Y.s ON. ONIA 6.
Cos sect Containers Used: _
/0�ros ONO' ONIA 9.
-Pare Containers Used:
Yes ONO ONIA
Containers In.tact: '
Y. ONO ONIA 10.' _
Filtered volume received for Dissolved tests
Ores DNo NrA 11.
Sample Labels match COC;
Yee O o ONVA 12. . .
.-Includes date/timell DIAnaiysisMatrix:
All conlalners no preservation have bean chocked.
ryes ONO CWA 13.
All containers needing preseration am found to be in
Dyes -ONO CNIA ."
/
compliance vith EPA recommendation.
nl ( �~
eza.,llons: VCA, eolitorm, TOO, OZG, WFDRO (w+tar)
es ONO Initial when completed
Samples checked for dechlorinatlom
Ores DNo A 14.
Hcadences in V0A Vials. >6mni :.
OYe: ON. NIA 15.
OYes ONO ZWA 16.
1"rip Blnnk:Present: -
Trip Blank Custody Seals Present
DYes DNo t)NIA
7L #(if 'rchaseased)
Pace Trip Blankof I purchased):
:_---
Field Data ReguIred?
Client Notification] Resolution:. Person Contacted: Daten ime:'
Comments/ Resolution: ..
SCURF Review: f11' ,Date: — Place label here
SRF Review: Date: `t t OR
Plote: Vihenever,them is a discrepancy affecting North Carolina compliance
_..._�amnles..a.copioLtNsSotl aLb,sentlolho Nedh Carolina DEHNR Handwrite project number
_—Co:nfureino.NP�aLi�uLor hold InenrreGj,p aseryeil a ou�iTe rys"------(if—no��hUallable)--"—
incorrect,cor
Page 2 of 3

Semi-annual Stormwater Discharge Monitoring Report
for. North.Carolina Division of Water Quality General Permit No. NCG120000
Date submitted December 27: 2013
CERTIFICATE OF COVERAGE NO. NCG120056
FACILITY NAME: Upper Piedmont Regional Landfill
COUNTY: Person
PERSON COLLECTING SAMPLES: G. Duhon
LABORATORY: Pace Analytical Lab Cert. # 67
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2013
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec .,
or. ® Monthly' D<—cE +ems (month)
DISCHARGING TO.CLASS ❑ORW ❑HQW . ❑Trout-❑PNA
❑Zero -flow : []WaterSupply ❑SA
®Other: WS-IV, NSW
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
U
No discharge this period?`
Date sample
�24 hour rainfall
•'
Outfall'No.
-
•- i
Collected
,
......amount;':
'�
Chemical Oxygen Demand.:
§,Fecal Coliform
--
Total Suspended solids
mo/dtl/yr)
_ <,_,.=
,:, Inches'
Benchmarks -=>::.'
.
_
120 mg/L .y
_...
o 1000 count;per 100mL
_...224
,100 mg/LSor50 mg/L
...
003
12/09/13
- 0.5 '...
:..:..: 36.0 ....
-
.... -14.7
' Monthly sampling (instead of semi,annual) must begin with the second consecutive benchmark exceedance for the same parameter at.the same outfall.
' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit text, Table 3, identifying the especially sensitive. receiving .water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -
numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L.. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2012-10/31/2017 - SWU-248, last revised 10/25/2012
' Page 1 of 2

Semi-annual Storrs water Discharge Monitoring Report
for North Carolina Division of Water.Quality General Permit No..NCG120000
Date submitted December 27; 2013
CERTIFICATE OF COVERAGE NO. NCG120056 SAMPLE COLLECTION YEAR _2013
FACILITY NAME:: Upper Piedmont Regional. Landfill SAMPLE PERIOD ❑ Jan -June `❑ July -Dec -
COUNTY: Person of ® Monthly'
(month)
PERSON COLLECTING SAMPLES: G. Duhon DISCHARGING TO CLASS ❑ORW . ❑HQW . ❑Trout .❑PNA
LABORATORY: Pace Analytical . Lab Cert. # 67 ❑Zero -flow.' ❑Water Supply [:]SA
Comments on sample collection or analysis: ®Other: WS-IV, NSW .
PLEASE REMEMBER -TO SIGN ON THE REVERSE
Part A: Stormwater Benchmarks and Monitoring Results
1 Monthly
❑ No discharge this period?z.
!: • k
Date Sample ; 24 hour rairifa11
Outfall No.Collected' amount,' .. _
a. Chemical Oxygen Demand ; Fecal Coll orm Total Suspended Solids `
.(mo/dd/yr) -.:`..!Inches.
Benchmarks =' 120 mg%L ;,' ' 1000;count per 100ymL :100'mg/L or 5o mg/L
12/09/13 0.5 i 36.0 ...224 - :.. :..14.7 -
sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requirement.
"See General Permit text, Table 3, identifying the especially sensitive.receiving water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect; ND, or other similar non -
numerical format. When results are below the applicable limits, they must he reported In the format, "<XX ms/L"; where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L.. Convereely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. :See General Permit text.
Permit Date: 11/1/W12-10/31/2017 SWU. 248, last revised 10/25/2012
. Page 1 of 2 .

Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
Footnotes from Part A also apply to this Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tfer 2, or Tier 3 responses. See General Permit text.
FOR PARTAAND PARTB MONITORING RESULTS: -- - - - - - -
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART -II SECTION B:.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS.. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BE NCH MAR K.EXCEEDENCES FOR. THE SAME PARAMETER AT.ANY ONE OUTFALL?. YES.,Q NO Q,. ..
- IF YES, HAVE YOU CONTACTED THE:DWQ REGIONAL OFFICE? YES .0 NO Q
REGIONAL OFFICE CONTACT NAME: - - -
Mail an original and one copy of this DMR including all "No Discharge"resorts within 30 days of receipt of the lab results for at end of monitoring Period
in the case of "No Discharge" reports) to: .
Division of Water Quality - - - - - - - - - - - - -
Attn: DWQ Central Files -
1617Mail Service Center
:. - .;. -.. :... :... .:.:... -
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the.pers000r persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is; to the best of my knowledge and belief, true, accurate, and complete. I
am aware tthatt there are significant penalties for submitting false.information, including the possibility of fines and imprisonment forknowing violations:'.'. -
(Signature of Permittee) - - (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012
- .Page 2 of 2 .

Parnell, David
From: Einsmann, Matt [[e-mail][
Sent: Friday, February 21, 2014 8:41 AM
To: Parnell, David
Cc: Duhon, Greg
Subject: Upper Piedmont
Attachments: December 2013.pdf; Transmittal Letter - January 2014 DMR.pdf
Dave
I received your voice mail message with information about our Representative Outfall request and our
Fecal Coliform sample results. I have attached the December 2013 and January 2014 DMR per your
request. You will see on the January report that there is an updated summary of the analytical results
from our outfalls. Outfall 003 has had 2 consecutive months with fecal coliform below the threshold
value (224 in December and 99 in January). I will forward results from February sampling when they
are available.
We have not performed any remedial measures at Outfall 003. However, we have changed our
sampling technique so that we collect a water sample from a higher elevation within the water
column. Under the old technique, we collected a sample at the bottom of the water column (i.e., near
the floor of the stream). Now, we are collecting the sample higher in the water column.
From your message, I understand that you will not render an answer to our requests until you review
the February results. We look forward to receiving your answers.
Matt Einsmann, PE
Environmental Manager
Republic Services
5111 Chin Page Road
Durham, NC 27703
phone [phone]
fax [phone]
cell 919-672-2837

Paco Analytical Services, Inc.
aceAnalytleal •
6701 Conference Drive
Raleigh, NC 27607
mm:pacalabs.mm
(919)834.49a4
Page 1 of 1
Laboratory Report
- Mr. Greg Duhon
- -
ReportDate:
12/23/2013
Upper Piedmont Environmental.
Date Received:
12/09/2013
9650 Oxford Rd. .
Rougemont; NC 27572
Project: TANKA/OUTFALL 3 :. .....
..: . ...... - ..:..
...
Pam Project No.: 92182405.
.Sample: TANK
Lab to:. 92182405001 Collected:
12/09/1313:50
Matrix: Water
Parameters
Results :'.Units. -. .Report Limit.
Analyzed
-Qualifiers
- -.
Cyanide -
0.0069 mg/L 0.0050
1220/1310:43
-.
Sample: OUTFALL 3
Lebo: 92182405002 Collected:
12/09/13 13:45
Matrix: Water
Parameters
- Results. Units Report Limit :
Analyzed
Qualifiers
Total Petroleum H drobarbons
NO m /L - - 5 0
12/11/1312:52
y 9
Fecal Coliforms - . - 224 CFU/100 mL
Total Suspended Solids 14t7 mg/L
Chemical Oxygen Demand . 36.0 mg/L
1.0 12/09/13 16:13
2.5 1D13/13 11:37 -
. 25.6 1223/13 11:45 --
�.
Reviewed by: ¢JUwf""
Tabitha M Dacal
[e-mail]
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Bioassay Certification #: 16
North Carolina Wastewater Certification #: 67
North Carolina Drinking Water Certification #: 37731
Charlotte Certification IDs
9800 Kincey Ave: Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
- North Carolina Field Services Certification #: 5342
West Virginia Certificatlon #: 357 -
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification A: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 356 -
North Carolina Drinking Water Certification #: 37712
VirginiaAfELAP Certification #: 460222
Page 1 of 3

I VvLrV111CI 0""re
F-RAL-CS-001-revA1 I .Pace Asheville Qualitl
Client Name:.'vgP=-<
Where Received: 0 Huntersville Asheville D. Eden ,R� Raleigh
Courier (Circle): . Fed Ex UPS USPS Client Commercial Pace Other
_ - Custody Seal on Cooler/Box Present: yes .no Seals intace. es Q no - -
Packing Material: El. Bubble Wrep ❑ Bubhlgpag� None Other__
_Circle Thermometer Used: IR Gun SNi12206fi387Type of ice: N/e Blue New Q.Sampleson (ce,cOo:lrgprOcesshas begun. .
IR Gun BackU SN:1220653, -
Temp Correction. Factor Add I ubtrr, t ' . C
''Brolp .DateandI Itlalso persona IrIing
Corrected Cooler Telimp: C gleal Tissue is Frozen: fa n N!A con.ents;-
Iemp should be above freezing to VC Comments: y.
Pace Trip Blank lot M (If purchased):_.___
Client Notification/ Resolution:. 'Field Data Required? Y ! N
Person Contacted: Datefnme:' __
Comments/ Resolution:
SCURF Review: ini .Date: _ -i Place label here -
SRF Review; Date: } L OR
Hole: %`ihenever.there is a discrepancy affecting North CarolinaoomPllanoe -
__.�amples;atop;o;.NLsto1lLL�ll be sent to the North Carolina DEHNR Handtvrlte project number
__-_—.- „iflcal'w '� AulAr ^^ln tnrnrtegl p aservailva oTf-Cernp (it-n01i raVallabl9)—'—'—
incorrect containers) -
Page 2 of 3

RelitI)y� etl (signature)
Fleceive I by (siqqWT
y"/ ne
Date
Dated%
Time
mquished 6y(signalure)
Reeeived by eaWre)
~—A""
Date
Time
me
Relinquished by(signalum)
Received by (signature)
Date
Time
Necelpl Gee m.s j�.. -yl
Cot 2'C ❑Tempi_"C
Res. Chlonnei .
❑Absent ❑Present ❑nla
Acid presew.'c2?
❑Yes ONO ONO
Base pros ON, >12?
❑ Yes ❑ No C No
Page 3 of 3

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
NCGj* UQ Jr-
DOC TYPE
HITS FQRICAL FILE
DOC DATEU�y
YYYYMMDD

aceAnalyticala
vmwpacelaes.cnm
Laboratory Report
Mr. Greg Duhon
Upper Piedmont Environmental
9650 Oxford Rd.
Rougemont, NC 27572
Project SAMPLING 1/14
Pace Project No 92186294
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 1 of 1
Report Date: 01/28/2014
Date Received: 01/14/2014
Sample:
TANK A
Lab ID:
92186294001 Collected:
01/14114 12'.50
Maldx: Water
Parameters
Results
Units Report Limit
Analyzed
Qualifiers
Cyanide
0.0064 mg/L
D0050
0112611411:13
Mt
Sample: OUTFALL 3 Lab ID: 92186294002 Collected: 01/14/1413:45 Matrx: Water
Parameters Results Units Report Limit Analyzed Qualifiers
Fecal Colifonns 99.0 CFU/100 mL 1.0 01114/14 15:35
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
q �
Reviewed by. '_)aJJ t-` 1 Ia
Tabfha M Dacal
[e-mail]
Raleigh Certification IDs
6701 Conference Drive Raleigh. NC 27607
North Carolina Wastewater Certification it: 67
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 288D4
Florida/NELAP Certification if. E87648
Massachusetts Certification #-. M-NCO30
North Carolina Drinking Water Certification if: 37712
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
Page 1 of 3

Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches;
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
-
15 mg/L
100 mg/L or SO mg/L
6.0 — 9.0 SU
003
01/14/14
0.6
Not Analyzed
Not Analyzed
Not Analyzed
Footnotes from Part A also apply to this Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
- Mail an oriainal and one copy of this DMR, including all "No Discharae" reports. within 30 days of receipt of the lab results for at end of monitorna period
In the case of "No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/ I __/C a
(Signature of Permittee)
Zvi .SA-J Z, ,;f
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012
Page 2 of 2

1!2ceAnalytrcal
www.pacelabs.com
6701 Conference Drive. Raleigh. NC 27607
r'(0`91 KM 4W, fax [phone]
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Page 3 of 3

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Where Received: Huntersvilie Asheville �. Eden Raleigh
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Page 2 of 3

qF REPUBLIC
ZMA SERVICES
December 27, 2013
Mr. John Holley, PF
Regional Engineer
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral and Land Resources
Land Quality Section
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Re: Request to Cease Sampling under Tier II Requirements
Upper Piedmont Environmental Landfill
9650 Oxford Road, Rougemont, NC 27572
NCG120056
Dear Mr. Holley,
On behalf of the Upper Piedmont Regional MS W Landfill, Republic Services is requesting to
cease sampling for fecal coliform from Outfall 003 on a monthly basis in accordance with the
Tier II requirements under General Permit NCG120000. This request is made following an
inspection of the site by Mr. David Parnell with the Land Quality Section on December 17, 2013.
During the site inspection, Mr. Parnell observed the stormwater basin upstream of Outfall 003
and confirmed that there was no industrial activity occurring in the drainage area leading to
Outfall 003. A summary of the analytical results from the site's outfalls from 2010 is attached
for reference. In addition, a site map depicting the outfalls is attached.
While unconfirmed, the source of the elevated fecal coliform results is likely caused by wildlife
activity (both birds and animals) in the area surrounding Outfall 003. It is our opinion that the
activities associated with the landfill are not causing the elevated results, and request that the site
be allowed to cease the Tier II requirements.
Thank you in advance for your consideration of this request. I can be reached at [phone]
with any questions.
Sincerely,
�v
Matt E'insmann, P.E.
—
Republic Services of NC, LLC
Cc: Mr. Greg Duhon, Upper Piedmont Environmental
Mr. Bradley Bennett, DEMLR Stormwater Permitting
1220 Commerce St SW
Conover, NC 28613
828.695-2055 • Fax [phone]
www.repubhcservices.com

STORMWATER ANALYTICAL RESULTS
UPPER PIEDMONT ENVIRONMENTAL LANDFILL
NCG120056
Outfall No.
Industrial Activity
Associated with
Drainage Basin
Activity
Status
Date
COO
(mg/1-1
Fecal Conform
(CFU/100 mL(
T55
(mg/L)
Oil and Grease
(mg/L(
TPH
(mg/q
1
landfill
Inactive
6/30/2010
NO
NO
NO
NO
NA
5/27/2011
<30
14
111
6.4
NA
9/23/20j1
18.2
182
68
5.4
NA
5/23/2012
14.8
4
6.7
<5.0
NA
10/29/2012
NO
11
11.1
NO
NA
6/3/2013
<25.0
20.0
20.5
NA
<5.0
10/7/2013
<25.0
80.0
29.6
NA
<5:0
2
Landfill
Active
6/30/2010
NO
NO
NO
ND
NA
5/27/2011
13.7
128
63.5
5.8
NA
9/23/2011
54.1
5,000
99
<5
NA
5/23/2012
NO
ND
N0.
NO
NA
10/29/2012
NO
191
8.1
NO
NA
6/3/2013
47.0
6,000
95
NA
<5.0
10/7/2013
28.0
58.0
18.1
NA
<5.0
3
Borrow Area
Inactive
6 30/2010
NO
NO
ND
NO
NA
5/27/2011
11.4
11
11.4
5.9
NA
9/23/2011
12.6
30
6
5
NA
5/23/2012
11.8
30
4A
6.4
NA
10/29/2012
NO
44
ND
NO
NA
6/3/2013
<25.0
Z500
5.7
NA
<5.0
10/7/2013
46.0
61000
255
NA
15.0
11 013
No Discharge
12/9/2013
360
224.0
14.7
NA
c5.0
4
Borrow Area
Active
6/30/2010
Out(ali
Not Constructed
5/27/2011
39.9
100
19.2
<5
NA
9/23/2011
18.2
>61000
46.7
5.4
NA
5/23/2012
26A
95
57.6
6.4
NA
10/29/2.012
NO
28
4
ND
NA
6/3/2013
33.0
3,000
5.7
NA
15.0
10/7/2013
<25.0
16.0
5.8
NA
<5.0
Threshold Value
120
11000
100
30
15
NO - Not Detected Above Laboratory Reporting Limit
NA = Not Analyzed (Note: Sample analysis changed from O&G to 'PH with issuance of new General Permit NCG320ODO, effective November 1, 2012.(
gold Values indicate results above the Threshold Value
Page 1 of 1 12/27/2013

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Parnell, David
From: Einsmann, Matt [[e-mail]]
Sent: Tuesday, January 28, 2014 3:32 PM
To: Parnell, David
Cc: Duhon, Greg; Einsmann, Matt
Subject: Upper Piedmont Landfill (NCG120056)
Attachments: Transmittal Letter - January 2014 DMR,pdf
Dave
I am transmitting the January 2014 DMR for the referenced site. As shown on the attached letter, this
is the second consecutive monthly sample for fecal coliform at Outfall 003 that is below the
benchmark value.
Based on the analytical results and information previously provided to DENR, we request the
cessation of monthly sampling for fecal coliform at Outfall 003.
Matt Einsmann, PE
Environmental Manager
Republic Services
5111 Chin Page Road
Durham, NC 27703
phone [phone]
fax [phone]
cell 919-672-2837
L «' )1
2_ -

STORMWATER ANALYTICAL RESULTS
UPPER PIEDMONT ENVIRONMENTAL LANDFILL
NCG120056
Outfall No.
Industrial Activity
Associated with
Drainage Basin
Activity
Status
Date
COD
(mg/L(
Fecal Coliform
(CFU/100 mL(
TSS
(mg/LI
Oil and Grease
(mg/L(
TPR
(mgJLl
1
Landfill
Inactive
6/30/2010
ND
NO
ND
NO
NA
5/27/2011
110
14
111
6A
NA
9/23/2011
18 2
182
68
5.4
NA
5/23/2012
14,8
4
6J
<5.0
NA
10/29/2012
NO
11
11.1
NO
NA
6/3/2013
<25.0
20.0
20.5
1 NA
a5.0
1O/7/2013
125.0
80.0
19.6
NA
<5.0
2
Landfill
Active
6/30/2010
NO
NO
NO
NO
NA
5/27/2011
13.1
128
63.5
5.9
NA
9/23/2011
54.1
5,000
99
<5
NA
5/23/2012
NO
NO
NO
NO
NA
10/29/2012
NO
191
8.1
NO
NA
6/3/2013
47.0
6,000
9.5
NA
<5.0
10/7/2013
28.0
58.0
18.1
NA
'SO
3
Borrow Area
Inactive2012
6/30/2010
NO
NO
NO
ND
NA
2011
11.4
11
11A
5.9
NA
2011
12.6
30
6
<5
NA
11.8
30
4.1
6.4
NA
/2012
NO
44
NO
NO
NA
2013
<250
2,500
5.7
NA
<5.0
2013
46.0
6,000
25.5
NA
<5.0
4
Borrow Area
Active
2010
OuHall
Not Constructed
2011
16/3/20113
39.9
100
19.2
<5
NA
2011
18.2
>6,000
46.7
5A
NA
2012
2G.4
95
S7b
6.4
NA
/2012
NO
28
4
NO
NA
2013
33.0
3,000
5.7
NA
'SO
/2013
<25-0
16.0
5.8
NA
<5,0
Threshold Value120
1,000
100
30
15
ND - Not Detected Above Laboratory Reporting Limit
NA- Not Analyzed (Note: Sample analysis changed from O&G to TPH with issuance of new General Permit NCG120000, effective November 1, 2012.)
Sold Values indicate resL its above th9 Threshold Value
Pagr 1 of 1
10/31/)013

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j • It
ewREPUBLIC
ZkOl SERVICES
December 27. 2013
Mr. John I lollcy, P1
Regional Engineer
North Carolina Department of Environment and Natural Resources
Division of Energy. Mineral and band Resources
Land Quality Section
Raleigh Regional Oftice
1628 Mail Service Center
Raleigh, NC 27699-1628
12e: Request to Cease Sampling under Tier II Requirements
Upper Piedmont Environmental Landfill
9650 Oxford Road, Rougemont, NC 27572
NC G 120056
Dear Mr. I Tolley,
On behalfofthe Upper Piedmont Regional MSW Landfill, Republic Services is requesting to
cease sampling for Iccal colilorm front Outfall 003 on a monthly basis in accordance with the
Pier II requirements under General Permit N('6120000. 'I'his request is made following an
inspection of the site by Mr. David Parnell with the band Quality Section on December 17, 2013.
During the site inspection, Mr. Parnell observed the stormwater basin upstream ol'Outfall 00;
and conlinned that there was no industrial activity occurring in the drainage area leading to
Outfall 003. n summary of the analytical results from the site's outfalls from 2010 is attached
for reference. In addition, a site map depicting the outfalls is attached.
While unconlinned, the source ofthe elevated fecal colifonn results is likely caused by wildlife
activity (both birds and animals) in the area surrounding Outfall 003. It is our opinion that the
activities associated with the landfill are not causing the elevated results, and request that the site
be allowed to cease the Tier II requirements.
Thank you in advance for your consideration of this request. I can be reached at [phone]
with any questions.
Sirieef�cly, .,
Malt Ilinsmann, P.H.
Republic Services ofNC', I.LC'
Cc: Mr. Greg Duhon. Upper Piedmont Environmental
Mr. Bradley Bennett, DEMLR Stornnvaler Permitting
1220 Commerce St SW
Conover, NC 28613
828.695-2055 • Fax [phone]
www.republicservices.com

"1 16
STORMWATER ANALYTICAL RESULTS
UPPER PIEDMONT ENVIRONMENTAL LANDFILL
NCG120056
Outfall No.
Industrial Activity
Associated with
Drainage Basin
Activity
Status
Date
COO
(mg/L)
Fecal Coliform
(CFU/300 mL)
TSS
(mg/L)
Oil and Grease
(mg/L)
TPH
(mg/L)
1
Landfill
Inactive
6/30/2010
NO
NO
NC
NO
NA
5/27/2011
<10
14
111
6A
NA
9/23/2011
18.2
182
68
SA
NA
5/23/2012
14.8
4
6.7
<5-0
NA
10/29/2012
ND
11
11,1
NO
NA
6/3/2013
<25.0
20.0
20.5
NA
<5,0
10/7/2013
<25,0
BOLD
19.6
NA
<5.0
2
Landfill
Active
6/30/2010
NO
NO
NO
NO
NA
5/27/2011
13.7
128
63.5
5.8
NA
9/23/2011
541
5,000
99
<5
NA
5/23/2012
NO
NO
NO
NO
NA
10/29/2012
NO
191
81
ND
NA
6/3/2013
47.0
6,000
9.5
NA
<5-0
10/7/2013
28.0
58.0
18,1
NA
60
3
Borrow At(,,)
Inactive
6/30/2010
ND
NO
NO
NO
NA
5/27/2011
11-4
11
11 d
5.9
NA
9/23/2011
12.6
30
6
NA
5/23/2012
11A
30
4.1
6.4
NA
10/29/2012
NO
44
NO
NO
NA
6/3/2013
<25.0
2,500
5.7
NA
<5.0
10/7/2013
46.0
1 6,000
25.5
NA
<5-0
11/30/2013
No Discharge
12/9/2013
36.0
224.0
14.7
4
Borrow Area
Active
6/10/2010
Outfall
Not Constructed
5/27/2011
39.9
100
19.2
<5
NA
9/23/2011
18.2
>6,000
46.7
SA
NA
5/23/2012
26A
95
57.6
0A
NA
10/29/2012
NO
28
4
NO
NA
6/3/2013
33.0
3,000
5.7
NA
<5.0
10/7/2013
<25.0
16-0
5-8
NA
<5.0
Threshold Value
120
1,000
100
30
15
NO Not Detected Above Laboratory Reporting Limit
NA Not Analyted (Note Sample analysis changed from O&G to TPH wuh issuance of new General Permit NCG120000, effective November 1, 2012J
Bold Values indicate results above the Threshold Value
Page 1 of 1 12/27/2013

4

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s .W
w REPUBLIC
ZO SERVICES
November 1, 2013
Mr. David Parnell
lnvironmentaf Senior Specialist
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral and [,and Resources
Land Quality Section
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Re: Request for Representative Outfall Status
Upper Piedmont Environmental Landfill
9650 Oxford Road, Rougemont, NC 27572
NCG 120056
Dear Mr. Parnell,
20v;
On behalf of the Upper Piedmont Regional MSW Landfill, Republic Services is requesting
Representative Outfall Status for the stormwater outfalls at the referenced site. This request is
being made after consultation with Mr. Bradley Bennett and Mr. Ken Pickle with the NC DENR
Stormwater Permitting Unit.
As shown on the attached site map, Sediment Basin No. 2 receives stormwater runoff from the
active portions of the municipal solid waste (MSW) landfill and Sediment Basin No. 1 receives
stormwater runoff from the inactive (but not permanently closed) portions of the MSW landfill.
As such, the stormwater discharges from these two control measures are substantially identical.
Likewise, Sediment Basin No. 4 receives stormwater runoff from the active borrow area that is
excavated for soil cover material and Sediment Basin No. 3 receives stormwater runoff from the
inactive borrow area. As such, the stormwater discharges from these two control measures are
substantially identical.
If granted representative status, the facility will perform the analytical monitoring requirements
in accordance with Section B of General Permit NCG 120000 at Outfall 2 and Outfall 4. which
receive stormwater runoff from active portions of the site.
In addition to this request for representative outfall status, we would like to discuss the analytical
results for fecal coliform. As shown on the attached summary of analytical data, fecal coliform
concentrations exceed the Threshold Value at differing outfalls at differing sample times. In
fact, the analytical data do not show any correlation between fecal coliform and any other
analytical results (e.g., fecal coliform results at Outfall 3 are 30 and 2.500 when TSS results at
1220 Commerce St SW
Conover, NC 28613
828.695-2055 • Fax [phone]
www.republicservices.com

t
Mr. David Parnell
November I. 2013
Outfall 3 are 6 and 5.7, respectively, for the same two sampling events). Further, the fecal
coliform concentrations at Outfall 3 have exceeded the Threshold Value for two consecutive
events, which would trigger Tier 11 actions. As stated above, Sediment Basin No. 3 receives
stormwater runoff from the inactive borrow area. As such, it is our opinion that the fecal
coliform values at this outfall are not associated with the landfill activities and should not be
considered an exceedance.
We would welcome a site visit in support of the request for representative outfall status and
deem it appropriate to evaluate any potential sources of fecal coliform at the time of your visit.
'Ihank you in advance for your consideration of this request. I can be reached at [phone]
with any questions.
Sincerely,
att Einsmann, P.E.
Republic Services of NC, LLC
Cc: Mr. Greg Duhon, Upper Piedmont Environmental

9� k

I 'm
NCDENR
ioa,�i��risi
-
Division of Water Quality, / Surface Water Protection
National Pollutant Discharge Elimination System
REPRESENTATIVE OUTFALL STATUS (ROS)
REQUEST FORM
If a facility is required to sample multiple discharge locations with very similar stormwater discharges, the
permittee may petition the Director for Representative Outfall Status (ROS). DWQ may grant Representative
Outfall Status if stormwater discharges from a single outfall are representative of discharges from multiple
outfalls. Approved ROS will reduce the number of outfalls where analytical sampling requirements apply.
If Representative Outfall Status is granted, ALL outfalls are still subject to the qualitative monitoring
requirements of the facility's permit —unless otherwise allowed by the permit (such as NCGO20000) and DWQ
approval. The approval letter from DWQ must be kept on site with the facility's Stormwater Pollution
Prevention Plan. The facility must notify DWQ in writing if any changes affect representative status.
For questions, please contact the DWQ Regional Office for your area (see page 3).
(Please print or type)
1) Enter the permit number to which this ROS request applies:
Individual Permit 1 I (or) Certificate of Coverage l�
N C S:_ L 1 _]AN C G 1 2_ 1 0 �5_L l
2) Facility Information:
Owner/Facility Name: Upper Piedmont Environmental Landfill
Facility Contact Mr. Greg Duhon
Street Address 9650 Oxford Road
City Rougemont State: NC ZIP Code 27572
County Person E-mail Address [e-mail]
Telephone No. 336 _364-3699 Fax: [phone]
3) List the representative outfall(s) information (attach additional sheets if necessary):
Outfall(s) 2 is representative of Outfall(s)
1
Outfalls' drainage areas have the same or similar activities?
x Yes
i No
Outfalls' drainage areas contain the same or similar materials?
x Yes
r1 No
Outfalls have similar monitoring results?
x Yes
i i No (i No data*
Outfall(s) 4 is representative of Outfall(s)
3
Outfalls' drainage areas have the same or similar activities?
x Yes
No
Outfalls' drainage areas contain the same or similar materials?
x Yes
No
Outfalls have similar monitoring results?
x Yes
No No data*
Outfall(s) is representative of Outfall(s)
Outfalls' drainage areas have the same or similar activities?
i Yes
No
Outfalls' drainage areas contain the same or similar materials?
: Yes
iNo
Outfalls have similar monitoring results?
L Yes
I No i i No data*
*Non-compliance with analytical monitoring prior to this request may prevent ROS approval. Specific
circumstances will be considered by the Regional Office responsible for review.
Page 1 of 3
SWU-ROS-2009 Last revised 12/30/2009

w k

Representative Outfall Status Request
4) Detailed explanation about why the outfalls above should be granted Representative Status:
(Or, attach a letter or narrative to discuss this information.) For example, describe how activities and/or
materials are similar.
Sediment Basin No 1 and Sediment Basin No. 2 receive stormwater runoff from the active portions of the
municipal solid waste (MSW) landfill. As such, the stormwater discharges from these two control measures
are substantially identical
Sediment Basin No. 3 and Sediment Basin No. 4 receive stormwater runoff from borrow areas that are
excavated for soil cover material and the stormwater discharges from these two control measures are
substantially identical
5) Certification:
North Carolina General Statute 143-215.6 B(i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record,
report, plan, or other document filed or required to be maintained under this Article or a rule Implementing this
Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case
under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device
or method required to be operated or maintained under this Article or rules of the [Environmental Managernentl
Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed
ten thousand dollars ($10,000).
I hereby request Representative Outfall Status for my NPDES Permit. I understand that ALL outfalls are still
subject to the qualitative monitoring requirements of the permit, unless otherwise allowed by the permit
and regional office approval. I must notify DWQ in writing if any changes to the facility or its operations take
place after ROS is granted that may affect this status. If ROS no longer applies, I understand I must resume
monitoring of all outfalls as specified in my NPDES permit.
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
Printed Name of Person Signing: Matt Einsmarm P.E
Title: Environmental Manager
r
(Signoture of Applicant) (Dote Signed)
j Please note: This application for Representative Outfall Status is subject to approval by the
(I NCDENR Regional Office. The Regional Office may inspect your facility for compliance with the
conditions of the permit prior to that approval.
Final Checklist for ROS Request
This application should include the following items:
x This completed form.
x Letter or narrative elaborating on the reasons why specified outfalls should be granted representative
status, unless all information can be included in Question 4.
x Two (2) copies of a site map of the facility with the location of all outfalls clearly marked, including the
drainage areas, industrial activities, and raw materials/finished products within each drainage area.
x Summary of results from monitoring conducted at the outfalls listed in Question 3.
Any other supporting documentation.
Page 2 of 3
SWUROS 2009
Last iev;5etl 12i30/2009

I,,

Representative Outfall Status Request
Mail the entire package to:
NC DENR Division of Water Quality
Surface Water Protection Section
at the appropriate Regional Office (See map and addresses below)
Notes
The submission of this document does not guarantee Representative Outfall Status (ROS) will be granted as
requested. Analytical monitoring as per your current permit must be continued, at all outfalls, until written
approval of this request is granted by DWQ. Non-compliance with analytical monitoring prior to this request
may prevent ROS approval. Specific circumstances will be considered by the Regional Office responsible for
review.
For questions, please contact the DWQ Regional Office for your area.
Asheville 1
2090 U.S. Highway 70
Swannanoa, NC 28778
Phone [phone]
FAX [phone]
Fayetteville Regional Office
Systel Building,
225 Green St., Suite 714
Fayetteville, NC 28301-5094
Phone [phone]
FAX [phone]
Mooresville Regional Office
610 East Center Ave.
Mooresville. NC 28115
Phone [phone]
FAX [phone]
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Phone [phone]
FAX [phone]
Washington Regional Office
943 Washington Square Mali
Washington, NC 27889
Phone [phone]
FAX [phone]
Wilmington Regional Office
127 Cardinal Drive Extension
Wilmington, NC 28405
Phone [phone]
FAX [phone]
Winston-Salem Regional Office
585 Waughtown Street
Winston-Salem, NC 27107
Phone [phone]
Water Quality Main FAX [phone]
Central Office
1617 Mail Service Center
Raleigh, NC 27699-1617
Phone [phone]
FAX [phone]
Pac,c c! 3
(WIU-POS-2( 19
Last 12:3n�20O11

.P , .

REPUBLIC
SECES
November 1, 2013
Mr. David Parnell
Environmental Senior Specialist
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral and Land Resources
Land Quality Section
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Re: Request for Representative Outfall Status
Upper Piedmont Environmental Landfill
9650 Oxford Road, Rougemont, NC 27572
NIX:120056
Dear Mr. Parnell,
On behalf of the Upper Piedmont Regional MSW Landfill, Republic Services is requesting
Representative Outfall Status for the stormwater outfalls at the referenced site. This request is
being made after consultation with Mr. Bradley Bennett and Mr. Ken Pickle with the NC DENR
Stormwater Permitting Unit.
As shown on the attached site map, Sediment Basin No. 2 receives stormwater runoff from the
active portions of the municipal solid waste (MSW) landfill and Sediment Basin No. I receives
stormwater runoff from the inactive (but not permanently closed) portions of the MSW landfill.
As such, the stormwater discharges from these two control measures are substantially identical.
Likewise, Sediment Basin No. 4 receives stormwater runoff from the active borrow area that is
excavated for soil cover material and Sediment Basin No. 3 receives stormwater runoff from the
inactive borrow area. As such, the stormwater discharges front these two control measures are
substantially identical.
If granted representative status, the facility will perform the analytical monitoring requirements
in accordance with Section 13 of General Permit NCG 120000 at Outfall xand Outfall 4, which
receive stormwater runoff from active portions of the site. I/
In addition to this request for representative outfall status, we would like to discuss the analytical
results for fecal coliform. As shown on the attached summary of analytical data, fecal coliform
concentrations exceed the "threshold Value at differing outfalls at differing sample times. In
fact_ the analytical data do not show any correlation between fecal coliform and any other
analytical results (e.g., fecal coliform results at Outfall 3 are 30 and 2,500 when TSS results at
1220 Commerce St SW
Conover, NC 28613
828.695-2055 • Fax [phone]
www.republicservices.com

Mr. David Parnell
November I, 2013
Outtall 3 are 6 and 5.7, respectively, for the same two sampling; events). Further, the fecal
coliform concentrations at Outfall 3 have exceeded the Threshold Value for two consecutive
events, which would trigger Tier 11 actions. As stated above, Sediment Basin No. 3 receives
stormwater runoff from the inactive borrow area. As such, it is our opinion that the fecal
coliform values at this outfall are not associated with the landfill activities and should not be
considered an exceedance.
We would welcome a site visit in support of the request for representative outfall status and
deem it appropriate to evaluate any potential sources of fecal coliform at the time of your visit.
Thank you in advance for your consideration of this request. I can be reached at [phone]
with any questions.
Sincerely,
Matt Einstnanm, P.B.
Republic Services of NC, LLC
Cc: Mr. Greg Duhon, Upper Piedmont Environmental

�
�jA D R v l
Division of Water Quality / Surface Water Protection
1_
National Pollutant Discharge. Elimination SVstem
NCDENR
RITRFSt'N't'A 1'IVIC OU'I'FALL STATUS (ROS)
REQUEST' FORM
If a facility is required to sample multiple discharge locations with very similar stormwater discharges, the
permittee may petition the Director for Representative Outfall Status (ROS). DWQ may grant Representative
Outfall Status if stormwater discharges from a single outfall are representative of discharges from multiple
outfalls. Approved ROS will reduce the number of outfalls where analytical sampling requirements apply.
If Representative Outfall Status is granted, ALL outfalls are still subject to the qualitative monitoring
requirements of the facility's permit —unless otherwise allowed by the permit (such as NCG020000) and DWQ
approval. The approval letter from DWQ must be kept on site with the facility's Stormwater Pollution
Prevention Plan. The facility must notify DWQ in writing if any changes affect representative status.
For questions, please contact the DWQ Regional Office for your area (see page 3).
(Please print or type)
1) Enter the permit number to which this ROS request applies:
N Individual Permitt (or) Certificate
le of Coverage
L-[C LS I (I_ N 1 C i G _i_l i 2d 0.. 0 1 57
-6]
2) Facility Information:
Owner/Facility Name: Upyer Piedmont Environmental Landfill
Facility Contact Mr. Greg Quhon
Street Address 9650 Oxford Road
City Roueemont
County Person _
Telephone No. 336 _364-3699
State: NC ZIP Code 27572
E-mail Address gduhon reRublicservices.com
Fax:336___ 364-4799
3) List the representative outfalls) information (attach additional sheets if necessary):
Outfall(s) 2 is representative of Outfall(s) _ _ _ 1
Outfalls' drainage areas have the same or similar activities? x Yes No
Outfalls' drainage areas contain the same or similar materials? x Yes j No
Outfalls have similar monitoring results? x Yes No t No data*
Outfall(s) 3 is representative of Outfall(s) 4
Outfalls' drainage areas have the same or similar activities? x Yes No
Outfalls' drainage areas contain the same or similar materials? x Yes c No
Outtalls have similar monitoring results? x Yes No i No data*
Outfall(s) is representative of Outfall(s)
Outfalls' drainage areas have the same or similar activities?
Outfalls' drainage areas contain the same or similar materials?
Outfalls have similar monitoring results?
i Yes i No
Yes t No
-. Yes i- No No data*
*Non-compliance with analytical monitoring prior to this request may prevent ROS approval. Specific
circumstances will be considered by the Regional Office responsible for review.
Page 1 of 3
SWU ROS-:.309 Last - evised 12'30Y2009

Representative Outfall Status Request
4) Detailed explanation about why the outfalls above should be granted Representative Status:
(Or, attach a letter or narrative to discuss this information.) For example, describe how activities and/or
materials are similar.
Sediment Basin No. 1 and Sediment Basin No. 2 receive stortriwater runoff from the active portions of the
municipal solid waste (MSW) landfill. As such, the stormwaler discharges from these two control measures
are substantially identical
Sediment Basin No. 3 and Sediment Basin No. 4 receive stormwater runoff bon borrow areas that are
excavated for soil cover material and the stormwaler discharges from these two control measures are
substantially identical
S) Certification:
North Carolina General Statute 143-215.6 B(i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record,
report, plan, or other document filed or required to be maintained under this Article or a rule implementing this
Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case
under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device
or method required to be operated or maintained under this Article or rules of the (Environmental Managementl
Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may Include a fine not to exceed
ten thousand dollars ($10,000).
I hereby request Representative Outfall Status for my NPDES Permit. I understand that ALL outfalls are still
subject to the qualitative monitoring requirements of the permit, unless otherwise allowed by the permit
and regional office approval. I must notify DWQ in writing if any changes to the facility or its operations take
place after ROS is granted that may affect this status. If ROS no longer applies, I understand I must resume
monitoring of all outfalls as specified in my NPDES permit.
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
Printed Name of Person Signing: Matt Einsmam .E
Title: Fnvironmental Manager
(Signature of Applicant)
(Date Signed)
Please note: This application for Representative Outfoll Status is subject to approval by the
NCDENR Regional Office. The Regional Office may inspect your facility for compliance with the
j conditions of the permit prior to that approval.
Final Checklist for ROS Request
This application should include the following items:
x This cornpleted form.
x Letter or narrative elaborating on the reasons why specified outfalls should be granted representative
status, unless all information can be included in Question 4.
x Two (2) copies of a site map of the facility with the location of all outfalls clearly marked, including the
drainage areas, industrial activities, and raw materials/finished products within each drainage area.
x Summary of results from monitoring conducted at the outfalls listed in Question 3.
Any other supporting documentation.
Page 2 of 3
$WU RMS 2009 Lasl,evned 12.'tT2009

Representative Outfall Status Request
Mail the entire package to:
NC DENR Division of Water Quality
Surface Water Protection Section
at the appropriate Regional Office (See map and addresses below)
Notes
The submission of this document does not guarantee Representative Outfall Status (ROS) will be granted as
requested. Analytical monitoring as per your current permit must be continued, at all outfalls, until written
approval of this request is granted by DWQ. Non-compliance with analytical monitoring prior to this request
may prevent ROS approval. Specific circumstances will be considered by the Regional Office responsible for
review.
rFor questions, please contact the DWQ Regional Office for your area.
Asheville I
2090 U.S. Highway 70
Swannanoa, NC 28778
Phone [phone]
FAX [phone]
Fayetteville Regional Office
Systel Building,
225 Green St., Suite 714
Fayetteville, NC 28301-5094
Phone [phone]
FAX [phone]
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115
Phone [phone]
FAX [phone]
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Phone [phone]
FAX [phone]
Washington Regional Office
943 Washington Square Mall
Washington, NC 27889
Phone [phone]
FAX [phone]
Wilmington Regional Office
127 Cardinal Drive Extension
Wilmington, NC 28405
Phone [phone]
FAX [phone]
Winston-Salem Regional Office
585 Waughtown Street
Winston-Salem, NC 27107
Phone [phone]
Water Quality Main FAX [phone]
Central Office
1617 Mail Service Center
Raleigh, NC 27699-1617
Phone [phone]
FAX [phone]
Pane 3 cf 3
4WU-ROS-2ep9 last rov'sed 711/3!1+20n9

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STORMWATER ANALYTICAL RESULTS
UPPER PIEDMONT ENVIRONMENTAL LANDFILL
NCG120056
Outfall No.
Industrial Activity
Associated with
Drainage Basin
Activity
Status
Date
COD
(mg/L)
Fecal Coliform
(CFU/100 ml.)
TSS
(mg/L)
Oil and Grease
(mg/L)
TPH
(mg/L)
1
Landfill
Inactive
6/30/2010
NO
NO
NO
NO
NA
5/27/2011
<10
14
111
6.4
NA
9/23/2011
18.2
182
68
5.4
NA
5/23/2012
14.8
4
6.7
<SO
NA
10/29/2012
NO
11
11.1
NO
NA
6/3/2013
<25.0
20.0
20.5
NA
<5.0
10/7/2013
<25.0
80.0
19.6
NA
<5.0
2
landfill
Active
6/30/2010
NO
NO
NO
ND
NA
5/27/2011
13.7
128
63.5
5.8
NA
9/23/2011
54.1
5,000
99
<5
NA
5/23/2012
NO
NO
NO
NO
NA
10/29/2012
NO
191
8.1
NO
NA
6/3/2013
47.0
6,000
9.5
NA
<5.0
10/7/2013
28.0
58.0
18.1
NA
<5.0
3
Borrow Area
Inactive
6/30/2010
NO
NO
ND
NO
NA
5/27/2011
11.4
11
11.4
5.9
NA
12.6
30
6
<5
NA
11.8
30
4.1
6.4
NA
E6/33/2013
NO
44
NO
NO
NA
<25.0
2,500
5.7
NA
<5.0
46.0
6,000
25.5
NA
<5.0
4
Borrow Area
Active
6/30/2010
Outfall
Not Constructed
'
5/27/2011
39.9
100
19.2
<5
NA
9/23/2011
18.2
>6,000
46.7
5.4
NA
5/23/2012
26A
95
57.6
6.4
NA
1O/29/2012
NO
28
4
NO
NA
6/3/2013
33.0
3,000
5.7
NA
<5.0
10/7/2013
<25.0
16.0
5.8
NA
<5.0
Threshold Value
120
1.000
100
30
IS
NO - Not Detected Above Laboratory Reporting Limit
NA - Not Analyzed (Note: Sample analysis changed from O&G to TPH with issuance of new General Permit NCG120000, effective November 1, 2012.)
Bold Values indicate results above the Threshold Value
Ate► � ��- �'
bus-(
' Page l of 1
10/31/2013

Parnell, David
From: Pickle, Ken
Sent: Monday, October 21, 2013 2:12 PM
To: Parnell, David
Cc: Bennett, Bradley; Holley, John
Subject: Republic Services, Rougemont landfill .
�> ck -W Hi Dave,
I have two topics to alert you about.
1. Heads Up: Republic Services has a landfill in Rougemont, Person County. They have a little bit of data showing
a fecal coliform issue (Tier 2) from one of their four stormwater outfalls. I advised Matt Einsmann to contact
you on two aspects:
a. Representative outfall status for the two fill areas, and for the two borrow pit areas.
b. Relief from fecal coliform monthly monitoring at one of the outfalls.
c. Matt understands that he needs to request your inspection, and input on these two issues. He will be
preparing a data summary and argument for your consideration. If you don't mind, I'd like to stay in the
loop with you on this since Matt and I have some prior history of contact on the fecal question. Thanks.
2. Looks like we're trying to schedule a group gathering at a Raleigh Yardwaste Center forth week. Maybe
tomorrow (I can't go), or Wednesday (I can go.) John men i?Yn a yo WbZ-pnttO into this one....... FYI.
Ken
Ken Pickle
Environmental Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: ken. oickle(clncdenr.00v
Website: htto://i)ortal.ncdenr.org/web/Ir/stormwater
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**

Permit: NCG120056
SOC:
County: Person
Region: Raleigh
Compliance Inspection Report
Effective: 11/O1/12 Expiration: 10/31/17 Owner: Republic Services of North Carolina LLC
Effective: Expiration: Facility: Upper Piedmont Evironmental Landfill
US Hwy No 158
Contact Person: Steve Nichting
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Roxboro NC 27573
Title: Phone: [phone]
Certification: Phone:
Inspection Date: 12/1712013 Entry Time: 08:00 AM
Primary Inspector: Gabriele B Jones
Secondary Inspector(s):
Reason for Inspection: Routine
Permit Inspection Type: Landfill Stormwater Discharge COC
Facility Status: ❑ Compliant ❑ Not Compliant
Question Areas:
E Storm Water
(See attachment summary)
Exit Time: 09:00 AM
Phone:
Inspection Type: Compliance Evaluation
a-
3
Page: 1

Permit: NCG120056 Owner - Facility: Republic Services of North Carolina LLC
Inspection Date: 12/17/2013 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
Page:2

i
Permit: NCG120056 Owner - Facility: Republic Services of North Carolina LLC
Inspection Date: 12/17/2013 Inspection Type: Compliance Evaluation
Reason for Visit:
Routine
Stormwater Pollution Prevention Plan
Yes No
NA
NE
Does the site have a Stormwater Pollution Prevention Plan?
❑
❑
❑
❑
# Does the Plan include a General Location (USGS) map?
❑
❑
❑
❑
# Does the Plan include a "Narrative Description of Practices'?
❑
❑
❑
❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
❑
❑
❑
❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
❑
❑
❑
❑
# Has the facility evaluated feasible alternatives to current practices?
❑
❑
❑
❑
# Does the facility provide all necessary secondary containment?
❑
❑
❑
❑
# Does the Plan include a BMP summary?
❑
❑
❑
❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
❑
❑
❑
❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
❑
❑
❑
❑
# Does the facility provide and document Employee Training?
❑
❑
❑
❑
# Does the Plan include a list of Responsible Party(s)?
❑
❑
❑
❑
# Is the Plan reviewed and updated annually?
❑
❑
❑
❑
# Does the Plan include a Stormwater Facility Inspection Program?
❑
❑
❑
❑
Has the Stormwater Pollution Prevention Plan been implemented?
❑
❑
❑
❑
Comment:
Qualitative Monitoring
Yes
No
NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
❑
❑
❑
❑
Comment:
Analytical Monitoring
Yes
No
NA
NE
Has the facility conducted its Analytical monitoring?
❑
❑
❑
❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
❑
❑
❑
❑
Comment:
Permit and Outfalls
Yes
No
NA
NE
# Is a copy of the Permit and the Certificate of Coverage available at the site?
❑
❑
❑
❑
# Were all outfalis observed during the inspection?
❑
❑
❑
❑
# If the facility has representative outfall status, is it properly documented by the Division?
❑
❑
❑
❑
# Has the facility evaluated all illicit (non stormwater) discharges?
❑
❑
❑
❑
Comment:
Page: 3

14,
,,
REPUBLIC
SERVICES OF NC, LLC
August 27, 2007
North Carolina Division of Water Quality
Raleigh Regional Office
1628 Mail Service Center
Raleigh, North Carolina 27699
Attention: Vicki Webb and Autumn Hoban
RE: Upper Piedmont Regional Solid Waste Landfill
Response to Compliance Evaluation Inspection
Permit NCG120056
Dear Ms. Webb and Ms. Hoban,
Page 1 of 2
1 1
I�
I
5 ��r�G1iREGlU1',i.1.OF�10E
We received your letter on August 10, 2007, regarding your Compliance Evaluation Inspection of our
Upper Piedmont Landfill. Your letter requests a response within 15 days to identify the non-stormwater
discharge flowing continuously at Stormwater Discharge Outfall # I. Your letter also requests that we
review Part VI, (3.) - Allowable non-stormwater discharges. Please consider this letter as our response to
your requests.
Upon receipt of your letter, our site manager performed an inspection around and upgradient of Sediment
Basin # 1 to determine if there were any non-stormwater flows entering the basin. No flows into the basin
were identified.
Our basins are designed with a riser pipe, which has perforated holes within 3-inches of the base as shown
on Drawings I and 2 (attached). These holes, by design, will allow discharges during dry periods. Most
of the water contained within our sediment basins is expected to be a result of stormwater-related events,
although some groundwater recharge to the pond may also occur. The overflows, as mentioned in your
inspection summary, are designed only for use during heavy storm events when capacity within the
sediment basin is near peak. The overflow is generally set 2 feet below the perimeter berm to prevent
overtopping of the berm. To be clear, it is the holes within the riser pipe that perform most of the basin
dewatering. This allows stormwater to be released slowly over time, preventing quick flushes during
storm events.
After reviewing, Part VI, (3.), we are confident that our discharge is directly related to stormwater and/or
groundwater recharge to the basin and is not a non-stormwater discharge.
It was unclear from your letter what the purpose of your field and analytical sampling was and to what
conclusion you were leading based on the results. Your results indicated that the level of manganese
(Mn) at our site was present but below stream standards, yet downstream the level of Mn exceeded the
stream standard. You also mention that iron (Fe) was present and a layer of sheen was present at the
downstream location. Your report also mentions that dissolved oxygen was low at 2.8 (at Sediment Basin
# 1) and 0.96 (downstream location). Your statement that, "The origin of the metals, and the cause(s) of
the harm to the stream would require further sampling and data analysis," concerns us and we would like
further clarification on the potential impacts of these results.

Page 2 of 2
In response to these statements and to protect our interests, we contracted with a third party consulting
firm, Golder Associates NC, Inc. (Golder), to perform sampling from the outfall of Sediment Basin #1
and attempt to collect a sample from the bridge crossing at Range Road and Clayton Road. In addition,
Golder was contracted to collect a water sample from inside sediment basin # I as well as a soil sample
from an upgradient location to Sediment Basin # 1. Each of the water samples were to be analyzed for the
metals that were detected during your sampling, as well as similar field parameters. Results were
examined to help determine potential downstream constituent concentrations that may be attributable to
the site and/or naturally occurring conditions.
Golder's report is attached to this letter for your reference. In this report you will note that due to dry
conditions, no flowing water was observed in Cub Creek at the time of their sampling and therefore no
sample could be obtained. However, some of the results for the surface water samples that Golder
obtained from the site were different than those collected during your site visit. In particular, the
dissolved oxygen readings were significantly different and more typical of surface water values. Only
one constituent of concern (Mn) was detected above the applicable surface water standard in the Sediment
Basin # I outfall sample during the Golder sampling event. Based on the evaluations in the Golder report,
the Mn concentration in the outfall sample may be biased high given the (naturally occurring)
concentrations of Mn detected in the soil sample collected on site and the turbidity noted for the outfall
sample. Moreover, the concentrations noted for surface water samples collected from the site are much
lower than those noted in the Cub Creek sample collected in June and it is possible that another off site
source may be contributing to the elevated Mn and Fe concentrations noted in Cub Creek.
We appreciate this opportunity to provide additional information in support of demonstrating our
continued regulatory compliance. Should you have questions or need additional information please call
me directly at 828-464-2414 x-307 or Rachel Kirkman (Golder) at 336-852-4903.
Sincerely,
Ra me
nd Hdffiman, PE
Republic Services of NC, LLC
Area Engineer
Attachments: Drawing # I & #2
Golder Associates NC, Inc. Report
Cc: Drew Isenhour
Steve Nichting
Scott McCallister
Rachel Kirkman, P.G.

S
REINFORCED PRECAST CONC.
OR SOLID ALUMINUM
OVERFLOW
WATER LEVEL ELEV�
AT OVERFLOW
STONE FILTER MATERIAL
NOTES: 1. SEDIMENT BASIN SHALL
OF SILT ON A YEARLY
TOP OF OVERFLOW SILT ACCUMULATION RE
STRUCTURE WHICHEVER OCCURS F
2. ALL FILL MATERIAL SFU
TO 95% STD. PROCTOF
15' MIN, 3. OVERFLOW STRUCTURE
CARRY BOTH NORMAL
WIDTH EMERGENCY FL O
2' MIN.
MAX 3
sees 1F
CONCRETE BASE
BE CLEANED
3ASIS, OR WHEN
,CHES 2 FEET,
L BE COMPACTED
DENSITY
3 SIZEDTO
.OW AND
W.
CONCRETE. HEADWALL
MIN. SLOP, 3
RCP OR SOLID
ALUMINUM
CARRIER PIPE
INLET 1 j
INVERT
CUT—OFF TRENCH
2' DEEP
ANTI —SEEPAGE COLLARS
(TYPICAL 2 PLACES)
F1011,110
OUTLET
PROTECTION
20' MIN.
OUTLET INVERT
(WARIES)
SILT FENCE

Z3 REMOVABLE TOP
TRASH RACK —
1'
PIPE RISER FILTER
HEIGHT VARIES FABRIC
STONE FILTER MATERIAL
BASIN
NO.
NO. OF 1' .
DIA HOLES
NO. OF HOLES
PER ROW
N0. OF
ROWS
1
125
25
5
3
120
24
5
18"
4
CONCRETE BASE ----
(SEE TABLE FOR VOLUME)
DIA. VARIES
i
hmw;n ) i-A Z
i 2� MIN
1' DIA. HOLES SPACED !EQUALLY
(SEE CHART THIS DETAIL)
REINFORCED PRECAST CONC.
OR SOLID ALUMINUM
OVERFLOW
0 00 0
0 0 0.0 0
00000
0 0 0 0 0
00000
i_ a Y II I I=1 I I
1 I All" 011:14
III=111 II
III -II
/ CARRIER PIPE
DIAMETER VARIES
COMPACTED SUBBASE

Golder Associates NC, Inc.
4900 Koger Boulevard Suite 140
Greensboro, NC 27407
Telephone [phone]
Fax [phone]
August 27, 2007
Republic Services of NC, LLC
Upper Piedmont Environmental
9650 Oxford Road
Rougemont, North Carolina 27572
336-364-3699
Attention: Mr. Steve Nichting
General Manager
Project No. 053-6621007.400
Re: Surface Water and Soil Sampling Report
Upper Piedmont Regional Landfill, Permit No. 73-04
Person County, North Carolina
Dear Steve:
As requested, Golder Associates NC, Inc. (Golder) is submitting the analytical results for surface
water and soil samples collected at Upper Piedmont Regional Landfill on August 20, 2007.
Surface water samples were taken from Sediment Basin # 1 and its outfall. An attempt to collect
a sample from Cub Creek was made; however, the stream had no flowing water at the time of
sampling. A soil sample was also collected on site upgradient of Sediment Basin #1 from
approximately 6 inches below ground surface. Samples were collected in pre -preserved bottles
and stored immediately in a pre -chilled cooler. Field parameters including pH, specific
conductance, turbidity, temperature, dissolved oxygen and oxidation reduction potential were
collected for both water samples using a field -calibrated Horiba water quality meter. The
samples were shipped to Environmental Conservation Laboratories (ENCO) of Cary, North
Carolina under chain -of -custody control to be analyzed for aluminum, barium, calcium, iron,
magnesium, manganese and sodium. These parameters were selected based on the fact that they
were detected previously in the pond discharge and Cub Creek samples collected on June 16,
2007, by personnel from the North Carolina Division of Water Quality (DWQ).
As presented, all of the analyzed parameters except barium were detected in the two surface
water samples. In general, the concentrations of detected constituents were similar to previous
results with the following exceptions. Barium was not detected during the August event for
either the pond or discharge sample. Reported aluminum and iron concentrations were lower for
the discharge sample during this event than those reported for the June event. Manganese
concentrations were slightly higher for the discharge sample and are above the applicable surface
water standard. However, the results may be biased high due to potential leaching of manganese
from sediments as high turbidity was noted for the August sample. Dissolved oxygen

Surface Water and Soil Sampling Report August 27 2007
Attn: Steve Nichtine -2- 0536621007.400
concentrations were also significantly different during this sampling event. The concentrations
detected in the pond and its discharge were 8.9 and 10.1 milligrams per liter (mg/L),
respectively, as compared to 2.8 mg/L reported for the discharge during the June sampling event.
The results of soil sampling indicate that all selected analytes are present in the soils at the site
and are assumed to be naturally occurring. Concentrations in the soils are generally similar to or
greater than those detected in the surface water samples. The exceptions to this are calcium,
magnesium and sodium, which were detected at lower concentrations in the soil sample or not at
all in the case of sodium.
Although no sample could be obtained from Cub Creek during the August sampling event, the
following observations can be made. The concentrations of iron and manganese detected during
the June sampling event in Cub Creek were considerably higher than those detected on site.
Therefore, it is possible that there may be another off site source contributing to the increased
concentrations of iron and manganese noted downstream of the site. There were no metals of
concern detected at concentrations above their respective surface water standards, with the
exception of manganese in the discharge sample, during the August 2007 sampling event. The
concentration of manganese is still considerably lower than that detected downstream during the
June event. It should be noted that due to the significant difference in dissolved oxygen
concentrations detected between the June and August sampling events, the dissolved oxygen
readings from June should be considered suspect and documentation of field meter calibration
should be requested from the DWQ. The dissolved oxygen concentrations detected during the
August sampling event are more typical of surface water values. Soil sampling results indicate
that in general the parameters detected in surface water could be attributable in part to naturally
occurring concentrations in the soil. Specifically, the two metals that were detected above their
respective standards in surface water samples were detected at similar or higher concentrations in
the soil sample.
If you have any questions regarding the attached data or information contained in this letter,
please contact the undersigned at336-852-4903.
Sincerely,
GOLDER ASSOCIATES NC, INC.
David Y. "Dusty" Reedy, P.G.
Project Hydrogeologist
Attachments: Summary Tables (2)
Laboratory Certificate -of -Analysis
Field Data Forms
Rachel P. Kirkman, P.G.
Senior Project Geologist
C: Ray Hoffman, P.E., Republic Services of NC, LLC, 1220 Commerce Street, SW,
Conover, North Carolina 28613
Terri C. Phillips. P.G., Golder Associates Inc., tphillips agolder.com (electronic)

Summery of Detected Comtitueeb in Svefare Water Samples for Upper Pirdmaet Ledfdl
Perimeter
Sam Im Date
Be rlin Limit
Unit;
Svrbre Water Standard
food Pond Discharge Cub Creek So Bridge
Alumivum
6/I6R007
50
ug/L
No Standard
710 1W
MM0O1
310
166 141 no
Ban.
6/16R007
10
ug/
ION)
eb 22 44
8R0R007
1.30
ND ND na
Calcium
N16R00]
IN
uglL
No Standard
7900 69W
V20R007
I50
u,,L
7020 7010
Imo
6/]6 W]
50
.,,L
1000-
990 320
9/20R007
6.I0
376 529
Magnesium
Wl4u7007
IN
ug/L
No Standard
na 3700 2800
8/20R007
23.0
4970 4750 rte
Manganese
&16R007
I0
uS/L
200
ua 79 1600
B MM7
0.320
135 211 va
Su,ium
6/16R007
IN
ugh
No StendW
v 9700 5400
3/20R00]
160
12" I1700
Dissolved Oxygen(field)
N162007
m
mg/L
,renter than 5^
2.8 096
8ROR00]
0.1
99 t0.1 va
Notes
1. ug/L - micm,rsms per It.,
2. mgfL = milligrams per liter
3. W16/07 samples were collected by NCDE RDWQ pmemmel.
4. Standards listed an, the Water Supply Surface Water Standards as defincd in 15A NCAC 2B except as voted. Cub Creek has a W S-1 V claenfimm.n.
5.' - Amon Lrrel from for Freshwater Aquatic Life
6. •• - Standard for Freshwater Aquauc Life
]. Shaded values are ahwe Surface Wow Standards (or below the randard in the cue of Dissolved Oxygen).
8.na not available
9. ND -not detected m stated reporting limit
10. Thw. no Flowing water in Cub Creek dunng the SRO/07 t uppling event.
Golder Associates
Upper Ptedeuont Landfill Pogo I of 1 0536661007 400

Summer, or Delrned Cmslime in soil g.mple ror U,,, Piedmont LandOa
Parameter
Sam tin Dam
Reporling Limit
Units
Sail Sam de
Aluminum
6/16/3007
car
mgfKg
nor
8/20/2007
35,9
m./K.
13"
Danner
6/161200)
mL
gfKg
na
8/20/2007
017
ma/K.
730
Calcium
6116/2007
on
mgfKg
na
8120R007
848
mull:.
531
Tina
6/I6/2007
o a
mp/Kg
8R0/2001
1).90
molK.
23900
Magnesium
6/16/2007
mgXg
8/20/200]
Taal
m.lK.
68
garese
6116/2009
mgSnO/2009
0,961
mWK.21)
Fldniu.
611612007
a a
mglKg
820Y100]
Rl
moX.
ND
\blef
I. mg/Kg = milligrams per Kilogram
2. na - not available
3. ND - not detected at stated reponing limit
Golder Associates
Upper Picdmunt Lundlill Page I of 1 0536661007 400

Environmental Conservation Laboratories, Inc.
10775 central Port Drive
Orlando FL, 32824
Phone: [phone] FAX: [phone]
Wednesday, August 22, 2007
Golder Associates, Inc. (G0007)
Attn: Rachel Kirkman
The Wingate Building 4900 Koger Blvd., Suite 140
Greensboro, NC 27407
RE: Laboratory Results for
Project Number: 0536621007, Project Name/Desc: Upper Piedmont LF
ENCO Workorder: A704680
Dear Rachel Kirkman,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, August 21, 2007.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Orlando. Data
from outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
3� M
David Camacho For Ronald Wambles
Project Manager
Enclosure(s)
The total number of pages in this report, including this page is 11

CllentlD: Dptfall .. • , I t Lab ID:'.A704680-01 `- Sampled: 08/20/07 09:S0' ' - Received; O8/ri/07 09:10
Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
.............................................................................................................. ........... ..... .. ......
EPA 6020 02/16/08 08/21/07 ]0:08 8/22/2007 09:13
Client ID: Pond _ Lab ID: A704680.02 "Sampled: '08/20/07'09:55 Received: 08/21/07 09:30
Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
EPA 6020 02/16/O8 08/21/07 10:08 8/22/2007 04:21
Client ID:. So)I SamPie I I Lab ID: `A704680 03 - ' Sampled: 08/20/07 10:10 , Received: 0B121/07. 09:10
Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
................................................................................................................ ................... ...
EPA 6020 02/16/08 OB/21/07 11:58 8/22/2007 07:59
EPA 6020 02/16/08 08/21/07 11:58 8/22/2007 08:02
EPA 6020 02/16/08 08/21/07 11:58 8/22/2007 08:11
Client ID:Field Blank":.. Lab ID: A704680-04 .. ..Sampled: 08/20/0710:15. , Remlved:`OB/33/07r 09:10'
Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
EPA 6020 02/16/66 OB/21/07 10:08 8/22/2007 03:31
Page 2 of 12

.- r •t
t 4,�
SAMPLE DETECTION SUMMARY
Pent ID:
Outtall
..:,
:, Lab ID:
A704680-01
-•'
-
Analyte
Results
Flag
MRL
Units
Method
Notes
Aluminum
191
100
u9/L
EPA 6020
Calcium
7010
1000
ug/L
EPA 6020
Iron
529
50.0
ug/L
EPA 6020
Magnesium
4750
1000
ug/L
EPA 6020
Manganese
211
10.0
ug/L
EPA 6020
Sodium
11700
1000
ug/L
EPA 6020
lient 10:
Pond
: o ;
Lab ID:
A704680-02
Analyte
Results
Flag
MRL
Units
Method
Notes
............................................................................
Aluminum
lbfi
..............
100
ug/L ........
ug/L
EPA.60 ... _ _
EPA 6020
_ ... _. _.........
Calcium
7020
1000
ug/L
EPA 6020
Iron
376
50.0
ug/L
EPA 6020
Magnesium
4970
1000
ug/L
EPA 6020
Manganese
135
10.0
ug/L
EPA 6020
Sodium
12000
1000
ug/L
EPA 6020
ientID:
Soil Sample •, ,
'- ...
. Lab ID:
A704680-03 ..
._. ,
.:
Analyte
Results
Flag
MRL
Units
Method
Notes
Aluminum
13000
326
mg/kg dry
EPA 6020
Barium
73.0
10.9
mg/kg dry
EPA 6020
Calcium
531
109
mg/kg dry
EPA 6020
Iron
23900
163
mg/kg dry
EPA 6020
Magnesium
675
109
mg/kg dry
EPA 6020
Manganese
217
2.72
mg/kg dry
EPA 6020
lent ID:.
Field Blank
.,.
tab ID: ,,
A704680-04-
Analyte
Results
Flag
MRL
Units
Method
Notes
......................................
Aluminum
.. ..... ............. ............
38.2
.....
I
........
100 00
........_
ug/L ug/L
_ .. .. .....
E EPA 6020
..........._.
Sodium
222
I
1000
ug/L
EPA 6020
Page 3 of 12

1�.
Description: Outfall Lab Sample ID: A704680-01 Received: 08/21/07 09:10
Matrix: Surface Water Sampled: 08/20/07 09:50 Work Order: A704680
Project: Upper Piedmont LF Sampled By: Dusty Reedy
Metals by EPA 6000/7000 Series Methods
_.._.. _..___.. _.. _....... ...........
"- ENCO O-/ancb cerefed ara4te [NC 424]
Analyte [CAS Numberl
Results Fja9
tJAU
PE
j U
MU
]i=
Method
Analned
ill Notes
Aluminum [7429-90-5]
141
ug/L
1
31.0
100
71
EPA 6020
08/22/0704:13
JMA
Barium [7440-393]-
1.30 a
ug/L
1
1.30
100
71121015
EPA 6020
08/22/0704: 13
JMA
Cakium [7440-70-2]'
7010
ug/L
1
150
1000
71121015
EPA 6020
08/22/0704:13
JMA
Iron [7439-89-6]'
529
411.
1
6.M
50.0
71121015
EPA 6020
08/22/0704:13
JMA
Magnesium [7439-95-41'
4750
Li
1
23.0
1000
71121015
EPA 6020
08/22/0704:13
JMA
Manganese [7439-96-5]'
211
ug/L
1
0.320
10.0
71121015
EPA 6020
0812210704:13
JMA
Sodium [7440-23-5]'
11700
ug/L
1
16.0
1000
71121015
EPA W20
08122/0704: 13
JMA
This report relates only to Me sample as received by Me IatMm[ory, and may only be reproduced in full.
Page 4 d( 12

Www.encolabs.com
Description: Pond Lab Sample ID: A704680-02 Received: 08/21/07 09:10
Matrix: Surface Water Sampled: 08/20/07 09:55 Work Order: A704680
Project: Upper Piedmont LF Sampled By: Dusty Reedy
Metals by EPA 6000/7000 Series Methods
"- ENCO Q'ianobW tNW anaryre (NC 424)
Analyte [CAS Numbed
Results tlaq
UJIM
P.E.
Hu
HBl
Bath
Method
Analwed
gy Notes
Aluminum [7429-90-5] •
166
ug/L
1
31.0
l00
71-21015
EPA 6020
08/22/07 04:21
3MA
aarium [7410.39.3] •
1.30 u
ug/L
1
1.30
l00
71-21015
EPA W20
OB/22/07 04:21
3MA
Calcium [7440-70-2] •
7020
ug/L
1
150
1000
7H21015
EPA 6020
OB/22/07 04'.21
31,1A
Imn [7439-89-61•
376
ug/L
1
6.70
500
7H21015
EPA 6020
08/22/0704:21
3MA
MaOnesium 17439.95-4) •
4970
ug/L
1
23.0
1000
7H21015
EPA 6020
08/22/07 04:21
31,1A
Manganese [7439-96-51•
135
ug/L
1
0.320
100
7H21015
EPA 6020
08/22/0704:21
3m
Sodium [7440-n-5]•
12000
ug/L
1
16.0
1000
7H21015
EPA 6020
08/22/0704:21
3MA
This report relates only to the sample as received dy the Ialroodory, and may only de reproduced in full.
Page 5 of 12

Description: Soil Sample 1
Matrix: Soil
Project: Upper Piedmont LF
Lab Sample ID: A704680-03
Sampled: 08/20/07 10:10
Sampled By: DUSty Reedy
Received: 08/21/07 09:10
Work Order: A704680
9/a Solids: 92.0
Metals by EPA 6000/7000 Series Methods
._..._._....__ .............. ....... _._....._.............................................. ................ ...._.__............
"- ENCO Orbndb mtWarralytePVC 4141
Analyte [[AS Numherl
Results I[aq
U=
DE
K"
MU
111=
Method
BBalyied
BY NO[es
Aluminum [7429-90-5]'
13000
mg/kg dry
30
35.9
326
7H2O031
EPA 6020
08/22/0708'. 11
3MA
Barium [7440.39-3] •
73.0
m9/k9 dry
1
0. 174
10.9
7H2O031
EPA 6020
08/22/07 07:54
3MA
Calcium 1740-70-21
531
mg/kg dry
1
8.48
109
7H2O031
EPA 6020
08/22/0707:54
)MA
Imn [7439-89-6] •
23900
mWkg dry
30
17.9
163
7H2O031
EPA 6020
08/22/07 0&11
3MA
Magnesium [7439-95-41•
675
mg/kg dry
1
14.1
109
7112O031
EPA 6020
08/22/0707:54
3MA
Mangano [7439-96.5]'
217
mg/kg dry
2.5
0361
2.72
7112O031
EPA 6020
08/22/0708.02
3MA
Sodium [7440-23.51`
14.1 ❑
0p/kg dry
1
14.1
109
7112O031
EPA 6020
08/22/0707:54
319A
This report relates only m he samye as receives try the lad B Ory, aW may onty x reproduced in full.
Page 6 of 12

Description: Field Blank
Lab Sample ID: A704680-04 Received: 08/21/07 09:10
Matrix: Surface Water
Sampled: 08/20/07 10:15 Work Order: A704680
Project: Upper Piedmont LF
Sampled By: Dusty Reedy
Metals by EPA 6000/7000 Series Methods
• - ENCO CrOnob certified anaW (NC 4241
Analvte [CAS Numberl
Results
Ehu
undA
RE
till
MU
@pall
Method
Analued
@y Notes
Aluminum [7429-90-5]
38.2
I
ug/L
1
31.0
100
71-121015
EPA 6020
08/22/0703:31
)MA
Barium 17440-39-3]
1.30
U
Ill
1
1.30
100
7H21015
EPA W20
08/22/0703:31
JMA
Calcium (74Q.70.2)•
150
u
ug/L
1
150
1000
7H21015
EPA 6020
08/22/0703:31
JMA
Iron [7439-896]'
6.70
u
ug/L
1
6X
50.0
7H21015
EPA 6020
00/22/0703:31
JMA
Magnesium (7439-95-4)'
23,0
a
ug/L
1
230
1000
7H21015
EPA 6020
08/22/070331
JMA
Manganese [7439 96 5]'
0.320
U
ug/L
1
0.320
10.0
71-121015
EPA 6020
08/22/0703:31
JMA
Sodium 17440-23-5)•
222
1
ug/L
1
16.0
1000
7H21015
EPA 6020
08122/0703:31
JMA
This report tell only W the Sample a5 receiveJ try 1M Iavoratory, and may only W reproduced in lull.
Page 7 of 12

Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 7H20031 - EPA 30508
Blank (7H20032-BLK1) Prepared: 08/21/2007 11:58 Analyzed: 08/22/2007 05:31
Spike Soume %REC RPD IAMI ,WResult Flao MRC ''Unllts Level Result %REC> Limits 7 = RPD Limit'li6tai
Barium
0,160
U
IO'D
rWkg onAt
Caldum
7,80
U
IN
mglkg wet
Iron
0.550
U
5.00
mg/kg met
Magnesium
13.0
U
100
.91 "a
Manganese
0.429
1
IN
mg/kg we
Sodium
13.0
U
100
mg/kg wet
.............
LCS (71120031-851)
............
Prepared: 08/2112007 11:58 Analyzed: 08122/2007 05:37
......
l
Spike ,Source
%REC
RPD
Analyte
Result
Fliq
MRL'
Units
Level Result' %REC'
'Umits RPD
Limit
Ili
Xurminum
983
1010
mg/kg ea
IN 99
85-115
Barium
51.3
10.0
mcii wet
50.0 103
85-115
Caldurn
2520
IN
mg/kg wd
2500 lot
85-115
Iron
101
5100
mg/kg wet
IN 101
85-115
Magnesium
2450
IN
mg/kg wel,
2500 98
as-Ils
Manganese
53,1
1.00
mg/kg aut
Soo 106
85-115
Sodium
2430
IN
mg/kg set
25W 97
85-115
Matrix Spike (7112001
Prepared: 08/21/2007 11:58 Analyzed: 08/22/2007 05:54
Source: A7014332-01
Spike Source
"%RECk
RPD,,
Analyte
Result
Flap
kkL
Units
M Le'Result, %REC �i
Llaens RPD
Limit
ililotel;
Aluminum
282
12.9
mg/kg dry
129 230 40
85-115
QM-07
Bari
67,7
12.9
mg/kg dry
64.5 0,207 U 105
85-115
Calcium
35I0
129
mg/kg dry
3230 385 97
85-115
Iron
225
6,45
mWkg dry
129 129 74
85-115
QM-07
Magnesium
3180
129
mg/kg dry
3230 16.8 U 98
85-115
Manganese
690
129
mg/kg dry
64.5 1.01 105
85-115
Sodium
3130
129
Vkg Or,
3230 16.8 U 97
85-115
Mabix Spike Dup (7H20031-MSD1)
Source: A704332-01
Prepared: 08/21/2007 11:58 Analyzed: 08122/2007 06:02
Samurn
70S
12.9
mWkg dry
64S
0,207 U
IN
85-115
4
20
Calcium
3620
129
mg/kg dry
3230
385
IN
85-115
3
20
Iron
233
645
mg/kg dry
129
129
so
85-115
3
20 QM-07
Magnesium
3270
129
mg/kg iny
3230
16.8 U
lot
85-115
3
20
Manganese
71.0
1.29
nogi di,
64.5
1.01
108
85-115
3
20
Sodium
3230
129
mgi day
3230
1618 U
IN
85-115
3
20
Post Spike (71120031-PS1) Prepared: 08/2112007 12:00 Analyzed: 08/22/2007 06: 10
Source: A704332-01
Spike SourOB, %REC RPD
Result Flag " MRL Units:Level' Result- %REC Limits' RPD Until, Notes
Page 8 of 12

r I.
OVAL
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 7H2O031 - EPA 30508
Post Spike (7H20031-PSI) Continued prepared: 08/21/2007 12:00 Analyzed: 08/22/2007 06:10
Source: A704332-01
F,Spike= v i Source , i %REC' _ `RPD
Analy[e q 'Result 'Flab' `MRL =Units :, ..Level rResult " %REC Limits' " RPD Limit - Notes
Barium
52.0
10.0
ug/L
49.0 -1.80 110 75-125
Calcium
2740
100
ug/L
2450 292 100 75-125
Iron
192
B00
ug/L
98.0 98.3 95 75-125
Magnesium
2430
100
ug/L
24K -5.70 99 75-125
Manganese
53.1
1.00
ug/L
49.0 O.765 107 75.125
Sodium
2420
100
ug/L
2450 -0,886 99 75.125
...............................................................................................................................
Batch 7H21015 - EPA 3005A
.......
Blank (7H21015-BLKl)
Prepared: 08/21/2007 10:08 Analyzed: 08/22/2007 03:17
.
Spike 'Source = %REC - ..
=RPD ...
Analyte;
Result = <fla9
MRL `"'
Units
"'Level Result ` %REC omits - RPD '`
Limit -'Notes
Aluminum
31.0
U
I00
ug/L
Barum
130
U
100
ug/L
Calcium
150
U
1000
ug/L
Iron
6.70
U
50.0
ug/L
Magnesium
23.0
u
1000
ug/L
Manganese
0.320
U
10.0
ug/L
Sedum
16.0
0
1000
ug/L
......................................................................................................................................
LCS (7H21015-BSI)
Prepared: 08/21/2007 10:08 Analyzed: 08/22/2007 03:23
'
Spike .Source t "'" b %REC,
RPD `
Ani " `
:Bevil
Flao
.MRL
:� •Urines^
-' level Result ' "%REC LimitsRDD
.Limit Nntea
Barium
523
100
u9/1-
500 105 85-115
Calcium
253M
1000
ug/L
25000 101 85-115
Iron
1020
50.0
ug/L
Iwo IO2 85-115
Magnesium
252M
1000
ug/L
25M 101 85-115
Manganese
520
10.0
ug/L
500 IN 85.115
Sodium
253W
1000
uy/L
250M 101 85-115
.........................................................................................................................
Matrix Spike (7H23015-M51)
.... ..... .. ..
Prepared: 08/2112007 10:08 Analyzed: 08/22/2007 03:39
Source: A704680-04
-
.,,Spike r Source :. %REC ..., ,..'..RPD
Analyte, ,.
Result" 'Flab
Mild.
Units
.Level ,Result ', -%REC Limits° "RPD ""Limit Notes ,.
Baru.
488
100
ug/L
500
1,30U
98
85-115
Cali
253M
1000
ug/L
25000
150 U
I01
85-115
Imn
IB10
50.0
ug/L
IWO
670❑
IN
85-115
Magnesium
253N
1000
ug/L
29000
23.0 U
101
85-115
Manganese
525
10.0
ug/L
500
0.320 U
105
85-I15
Sodium
21800
1000
ug/L
25000
222
98
85-115
......................................................................................................................................
Matrix Spike Cup (7H21015-MSD1)
Prepared: 08/21/2007
10:08 Analyzed: OB/22/2007 03:48
Source: A704680-04
Page 9 of 12

Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 7H21015 - EPA 3005A
Matrix Spike Dup (7H21015-MSD1) Continued
Prepared: 08/2112007 10:08 Analyzed: 08122/2007 03:48
Source: A704680-04
Spike %
n Source
%REC
RPD
A"�l
Result Flag,'
MRL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
A.rn,num
1070
100
og/l.
low
38,2
103
95-115
02
20
Barium
512
IN
u 11-
500
1.30 U
102
85-115
5
20
Calcium
254M
1000
ug/L
25000
150 U
101
85-115
0,05
20
Iron
1080
50.0
og/L
1000
6,70 U
ice
85-IIS
4
20
Magnesium
255M
1000
ug/L
25000
23.0U
102
85-115
0.7
20
Manganm
524
10.0
og/L
500
0.320 U
105
85-115
0.1
20
Sodom
249M
1000
g/L
25000
222
99
as-ils
0.3
20
................... —
Post Spike (7H21015-PS1)
.......................
Prepared:
08/21/2007
......... .
10:08 Analyzed: 08/22/2007 03:56
. . ............. —
Source: A704680-04
1
11
r,
Spike
Soumoe�
,%REC
1 -
RPD,
An'alyte
Result Flag
MRL
Units
"Level
Result.,%'R'
'E'C.-
i, Limits
RPD
Umit Notes
Numnum
108
10.0
4L
98.0
3.74
106
75-125
Barium
47.1
10.0
ug/L
49.0
-3.33
103
75-125
carourn
2480
IN
og/L
24M
5.53
101
75425
Iron
101
5,00
ug/L
98.0
0.392
103
75-125
MNnm,r.
2460
IN
4L
24W
-12.4
101
75-125
Mangano
510
IN
ug/L
49.0
-0.019
104
75-125
Sodurn
............
2480
IN
4/L
.......
2450
21.7
. . . . .
IN
. ---
75-125
...................
Page 10 of 12

J
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
Page I I of 12

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
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I
GOLDER ASSOCIATES INC.
QUALITY ASSURANCE & QUALITY CONTROL
LABORATORY DATA REVIEW alt=es
Page 1 of 4
Project Nante: Liver Piedmont Landfill (Non -Routine Surface Water Samples)
Project Reference Number: 053-6621007.100
Sampling Event Dote: August 20, 2007
Review Dane: August 22, 2007 /nitiaLs: DR
Report #: A704680
Person(s) performing the review are to initial each item on this form as acknowledgement of data acceptance,
or as acknowledgement of a review issue. In the case of the latter, a brief explanation should follow the
applicable item.
Golder Associates Inc. has reviewed the laboratory certificates of analysis, chain -of -custody form, and laboratory
provided sample group quality assurance and quality control data for the above referenced sample group to identify
potential bias or inaccuracy, in general accordance with the following United States Environmental Protection
Agency documents:
Region III Modifications to Functional Guidelines for Organic Data Review Multi -Media, Multi -
Concentration, September 1994;
Region III Modifications to the Laboratory Data Validation Functional Guidelines for Evaluating Inorganic
Analyses, April 1993; and
Laboratory Data Validation Functional Guidelines for Evaluating Inorganic Analyses, July 1998.
ANALYTE LIST(S)
Aluminum, Barium, Calcium, Iron, Magnesium, Manganese, and Sodium
1.0 CHAIN OF CUSTODY (COC) REVIEW
DR COC was properly signed by all parties.
DR Correct project name and number are on the form.
DR Sample receipt condition at laboratory was acceptable.
DR Each sample and blank submitted for analysis appears in the report.
Notes:
2.0 SAMPLE HOLDING TIMES
DR Holding times for extraction and/or analysis were met for each analytical
Method (see lab manual for holding times).
Notes:

GOLDER ASSOCIATES INC.
QUALITY ASSURANCE & QUALITY CONTROL
LABORATORY DATA REVIEW
Pagc 2 of 4
3.0 LABORATORY QUALITY CONTROL REVIEW
DR Laboratory analyzed at least one internal blank for each method, where applicable.
DR Laboratory blank is interference -free.
7H20031-BLKI
Alumimmn reported at 1.38 mg/kg "1"
Manganese reported at 0.429 mg/kg "I"
NA Surrogate recoveries are provided for each analytical method, where applicable.
NA Surrogate recoveries for each method are within the acceptable limits (i.e., at least
50% of the surrogates were within range).
DR MS/MSD/LCS data results are provided for each analytical method.
DR MS/MSD/LCS recoveries for each method are within the acceptable limits (i.e., at least I of
the 3 were within range).
7H20031-BLKI
Aluminum MS/MSD out of range
Iron MS/MSD out of range
Notes:
4.0 ANALYTE LISTS/METHODS
DR The proper number of constituents are present for each analyte list as identified above
(including detects where applicable).
DR Proper analytical methods were used for analysis.
Notes:
5.0 DATA REPORTING
DR All analytical reporting associated with the event was performed by the contracted lab.
DR Trip, field and/or equipment, and laboratory blank results have all been reported. All
detects for blanks are listed below by constituent. All laboratory method blanks, if any,
have been `flagged' with a'B' where detected in other samples as appropriate and a
laboratory narrative was provided. If the sample was flagged by the laboratory and is not
within 5X of the concentration in the blank (or I OX for commonly detected laboratory

GOLDER ASSOCIATES INC.
QUALITY ASSURANCE & QUALITY CONTROL - nA
LABORATORY DATA REVIEW = - Golder
Page 3 of 4 - ' A .,,, dates
contaminants -acetone, methylene chloride and phthalates), list below with explanation if
flags should be removed. If Flags need to be added for samples, also list below.
Field Blank:
Aluminum reported at 38.2 ug/L "I"
Sodium reported at 222 ug/L "I"
7H20031-BLKI
Aluminum reported at 1.38 mg/kg "F'
Manganese reported at 0.429 mg/kg "I"
Outfall:
Aluminum (141 ug/L): add `B" flag
Pond.
Aluminum: (166 ug/L): add "B"flag
DR It is clear from the laboratory report that samples have or have not been diluted during
analysis, and if the samples have been diluted, the result is reported as a multiple of the
dilution (e.g., a sample diluted I Ox resulting in an analytical detection of 1.0 should be
reported as 10). Those that have been diluted are listed below with the dilution factor.
Soil Sample 1:
Aluminum has dilution factor of 30
Iron has dilution factor of 30
Manganese has dilution factor of 2.5
DR The report provides the reporting limit for each constituent.
DR The results were reported at or below their proper reporting limits (e.g., MDLs, MRLs,
PQLs, etc.). Those that are not reported correctly are listed below (by constituent) with the
proper reporting limit listed beside them. State if the reporting limit error is due to
dilutions.
DR No inorganic and organic constituents were reported above their respective NC 21, Drinking
Water Standards in wells, surface points, or field/equipment/trip blanks.
Outfall:
Iron (529 ug/L): NC 2L = 300 ug/L
Manganese (211 ug/L): NC 2L = 50 ug/L
Pond.
Iron (376 ug/L): NC 2L = 300 ug/L
Manganese (135 ug/L): NC 2L = 50 ug/L

GOLDER ASSOCIATES INC.
QUALITY ASSURANCE & QUALITY CONTROL
LABORATORY DATA REVIEW (91
Page 4 of 4 ....,.a
DR For sites with historical data, no inorganic and organic constituents were detected in a well
or surface water point at concentrations outside of their historical range (more than 5X
previous concentrations or first-time detections).
DR Other report issues/Communications with laboratory/etc.:
Notes: Report provides "I" flags instead of "J" flags because that's the way it is reported in
Florida. Requested revised report 8-24-07.

� �
�c..��
DATE:8/20/07
SURFACE WATER SAMPLING LOG
Project Name: Upper Piedmont Landfill Project No./Phase No.: 0536621007.100
Sample ID: Pond Sampler(s): Dusty Reedy
Sampling Location: Pond located near GW-2
Equipment: Horiba U-22 Water Quality Meter
Temp.
Time
9:55
(aC)
27.32
PH
Salinity
(S.U.)
7.45
(%)
---
Cond.
TDS
(rnskm)
0.127
(mg L)
---
Turb.
ORP
(NTU)
27.5
(mvolts)
101
Dis. OZ
(mg/L)
8.9
SAMPLE LOCATION
Comments (sample methodology, weather conditions, color, silt, etc.): Pond level was very low
compared to previous visits to the site.
Signature: Date: Zo-o7
il_r, QA QC Sign Off: �Gu uIZ ��Cw Date: �{ ,1

DATE:8/20/07
SURFACE WATER SAMPLING LOG
Project Name: Upper Piedmont Landfill Project No./Phase No.: 0536621007.100
Sample ID: Outfall Sampler(s): Dusty Reedy
Sampling Location: Discharge of pond located near GW-2
Equipment: Horiba U-22 Water Quality Meter
Temp.
Time
9:50
(OC)
26.61
PH
Salinity
(S.U.)
6.48
(%)
---
Cond.
TDS
(mS/cm)
0.124
(mgL)
---
Turb.
ORP
(T,TU)
242.0
(mvolts)
124
Dis. 02
(mom)
10.1
SAMPLE LOCATION
L a ti dAH!/
O (' W. Z
CI . Oval-& 11
Comments (sample methodology, weather conditions, color, silt, etc.): Turbidity is biased hid due to
sediment stirred up when instrument was placed into the shallow water.
Signature: //�/,.�f�(t,¢rGa- Date: $-2-ov-07
QA/QC Sign Off: Date: LI-0-7

v-.V1
W4211 .'
FMAMMIS'"
DATE:8/20/07
SURFACE WATER SAMPLING LOG
Project Name: Upper Piedmont Landfill Project No./Phase No.: 0536621007.100
Sample ID: Cub Creek Sampler(s): Dusty Reedy
Sampling Location: Sample taken from pool of water north of bridge
Equipment: Horiba U-22 Water Ouality Meter
Temp.
Time
9:05
CC)
23.76
PH
Salinity
(S.U.)
5.73
(%)
---
Cond.
TDS
(MS/CM)
0.188
(mgL)
---
Turb.
ORP
(NTU)
8.0
(mvolts)
179
Dis. 02
(mom)
3.3
CD
SAMPLE LOCATION
1?4'3 e led
IZ7
Comments (sample methodology, weather conditions, color, silt, etc.): Stream was not flowing with standing
Pools of water north and south of the br4m N D c.. tx(y u l S . "FIe S C "ec;i2 . -
Signature: C,.�/��v.�
QA/QC Sign Off: b-y l
Date: F-Lo-o'7
Date: � -.4�-I—e'l

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Coleen Sullins, Director
Division of Water Quality
August 7, 2007
Name Mr. Steve Nichting
Facility Name Upper Pied mont-Rebublic Landfill
Address 9650 Oxford Rd
City, State, Zip Rougemont, NC 27572
SUBJECT: Compliance Evaluation Inspection
Facility Name Upper Piedmont — Republic Landfill
Permit Number NCG120056
County Person
Dear Mr. Nichting:
On June 16, 2007, Vicki Webb and Autumn Hoban, of the Division of Water Quality, Raleigh Regional Office, performed
an inspection of the subject facility. The following items should be addressed:
1.) Identify the non-stormwater discharge that is flowing continuously at Stormwater Discharge Outfall #1 and report
the findings to the Division of Water Quality within 15 days of receipt of this inspection letter. Please review Part VI,
(3.) Allowable non-stormwater discharges.
As part of the inspection, sampling was conducted in the unnamed tributary to Cub Creek at the entry location of the water
flow from Stormwater Outfall #1. Samples were also collected in Cub Creek at the Range Rd/Clayton Rd Bridge. All lab
results are attached and the observations are noted in the Summary Comments of this inspection report. It is our goal to
insure the quality of the surface waters of this State.
Please review the attached report. If you or your staff have any questions, do not hesitate to contact Vicki Webb
or Autumn Hoban at 919-791-4200.
Sincerely,
Vicki Webb Autumn Hoban
Enclosures
cc: Central files
RRO/DWQ Stormwater Compliance Files
Stormwater Permitting Unit
Danny Smith, NPS and Compliance Oversight
Mary Whaley, Solid Waste Unit
127 Cardinal Drive Extension, Wilmington, North Carolina 28405-3845
Phone: [phone] / Fax: [phone] / Internet: h2o.enr.state.nc.us
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper
One
NorthCarolina
Naturally

0
Permit: NCG120056
SOC:
County: Person
Region: Raleigh
Compliance Inspection Report
Effective: 09/01/02 Expiration: 08/31/07 Owner: Republic Services Of NC LLC
Effective: Expiration: Facility: Upper Piedmont Evironmental Landfill
US Hwy No 158
Contact Person: Steve Nichting
Title:
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 06/15/2007 Entry Time: 01:00 PM
Primary Inspector: Autumn Hoban
Secondary Inspector(s):
Vicki Webb
E.Shannon Langley
Reason for Inspection: Routine
Permit Inspection Type: Landfill Stormwater Discharge COC
Facility Status: ■ Compliant ❑ Not Compliant
Question Areas:
M Storm Water
(See attachment summary)
Roxboro NC 27573
Phone:[phone]
Certification:
Exit Time: 03:00 PM
Phone:
Phone:
Phone:
Phone:
Inspection Type: Compliance Evaluation
Page: 1

Permit: NCG120056 Owner - Facility: Republic services Of NC LLC
Inspection Date: 06/15/2007 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
This facility accepts industrial wastes: oil and petroleum contaminated soils (less than or equal to 3000 PPM), as well as,
water and wastewater sludges.
There is currently no requirement for the SWP3 at landfill sites.
The NCG 120000 and the NCG010000 permits were on -site as required.
Some vehicle maintenance is performed on -site. A Contractor performs maintenance as needed, but none was being the
conducted the day of the inspection, and no signs of spent or spilled fluids were observed.
The qualitative and analytical monitoring records were reviewed and the facility is in compliance with the monitoring
requirements of the permit.
There were three stormwater outfalls observed the day of the inspection. The #2 and #3 Stormwater Outfalls were dry
and the stormwater pond levels for #2 and #3 were below the overflow. The #1 Stormwater Outfall (By cell #3) has a
continous flow of water discharging into the un-named tributary on -site that connects to Cub Creek. The stormwater pond
connected to this outfall was not overflowing the day of the inspection and has been below the overflow level due the lack
of rainfall received this year. The discharge appears to be a non-stormwater discharge.
Grab samples were taken where the #1 Stormwater Discharge flows into the un-named tributary of Cub Creek. The
sample results are attached. The facility should idenflfy the origin of the continous discharge, as it did not appear to be
stormwater from the stormwater pond, and promptly report the findings to the Division of Water Quality. Sample results
indicated Mn, Fe, and At were present, but not at levels exceeding stream standards. The Dissolved Oxygen was low at
2.8.
It should be noted that results from grab samples taken in Cub Creek at the nearby Range Rd/Clayton Rd Bridge also
indicated the presence of Mn, and the level did exceed the stream standard. Fe was present and a layer of sheen was
present on the surface of the water at this location. The Dissolved Oxygen was extremely low at 0.96. The sheen had
the appearance of Iron Bacteria and/or Organic Decomposition. The origin of the metals, and the cause of "impaired-state—
¢f,the stream" would require further sampling and data analysis.
%1 Yt, 1'd
Page: 2

Permit: NCG120056 Owner - Facility: Republic Services Of NC LLC
Inspection Date: 06/15/2007 Inspection Type: Compliance Evaluation
Reason for Visit: Routine
Stormwater Pollution Prevention Plan Yes No NA NE
Does the site have a Stormwater Pollution Prevention Plan?
❑ ❑ ■ ❑
# Does the Plan include a General Location (USGS) map?
❑ ❑ ■ ❑
# Does the Plan include a "Narrative Description of Practices"?
❑ ❑ ■ ❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
❑ ❑ ■ ❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
❑ ❑ ■ ❑
# Has the facility evaluated feasible alternatives to current practices?
❑ ❑ ■ ❑
# Does the facility provide all necessary secondary containment?
❑ ❑ ■ ❑
# Does the Plan include a BMP summary?
❑ ❑ ■ ❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
❑ ❑ ■ ❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
❑ ❑ ■ ❑
# Does the facility provide and document Employee Training?
❑ ❑ _■ ❑
# Does the Plan include a list of Responsible Party(s)?
❑ ❑ ❑
# Is the Plan reviewed and updated annually?
❑
❑ ■ ❑
# Does the Plan include a Stormwater Facility Inspection Program?
❑ ❑ ■ ❑
Has the Stormwater Pollution Prevention Plan been implemented?
❑ ❑ ■ ❑
Comment: The SWP3 Plan is not a requirement for this permit.
Qualitative Monitoring
Yes No NA NE
Has the facility conducted its Qualitative Monitoring semi-annually?
■ ❑ ❑ ❑
Comment:
Analytical Monitoring
Yes No NA NE
Has the facility conducted its Analytical monitoring?
■ ❑ ❑ ❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
❑ ❑ ❑ ■
Comment:
Permit and Outfalls
Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site?
■ ❑ ❑ ❑
# Were all outfalls observed during the inspection?
■ ❑ ❑ ❑
# If the facility has representative outfall status, is it properly documented by the Division?
■ ❑ Cl ❑
# Has the facility evaluated all illicit (non Stormwater) discharges?
❑ ■ ❑ ❑
Page: 3

Permit: NCG120056 Owner - Facility: Republic Services Of NC LLC
Inspection Date: 06115/2007 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Comment: The #1 Stormwater Outfall continuously discharges a clear stream of
water, with some sheen present. The stormwater pond connected to this outfall was not
overflowing the day of the inspection and has been below the overflow level due to the
lack of rainfall received this year. The discharge appears to be a non-stormwater
discharge. The facility should make an effort to identify what the source of this
discharge is and promptly report the results of their findings to the Division of Water
Quality.
Page: 4

_.RD
RROSP
..egion:
RRO
collector
V WEBB
Sample Matrix:
Surfacewatar
Loc. Type:
RIVERISTREAM
Sample Depth
UN RD
' Sample ID:
AS18293
PO Number if
7W4668
OF wA%9
VisitlD
Q� Qy
Collect Date:
>_ r
Collect Time::
06/15/2007
12:30
ti
t7
Date Received:
06111812007
Time Received:
LabWOrks LoginlD
08:05
MMA
/
!
Date Reported:
0711&2007
Emergency YesJNo
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
B1-Countable membranes with 120 dies; Estimated
82- Counts from all fitters were zero.
B3- Countable membranes with more than 60 or 80 colonies; Estimated
B<-Fillers have counts of both '60 or 80 and < 20; Estimated
B5-Too many colonies were present; too numerous to count (TNTC)
J2- Reported value failed to meal QC criteria for either precision or acaaar-y; Estimated
J3-The sample matrix interfered Min Ore ability to make any accurate determination; Estimated
J6-The lab analysis was from an unpraserved or improparty chemically Preserved sample; Estimated
NI -The component has been tenatively identified based on mass spectral library search and has an estimated value
LAB
N&Estimated concentration is < PQL and >MDL
NE -No established PQL
P-EJevated PQL due to matrix interference andlor sample dilution
Q1-Holding time exceeded prior to receipt at lab.
02- Holding time exceeded following receipt by lab
PQL- Practical Quentitation Limit -subject to change due to instrument sensitivity
D- Samples analyzed for this compound but not d,,ja W
XI- Sample not analyzed for this compound
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 11

Locatic: !D: - CUBCREEKRANGERD
Loc. Descr.: CUB CREEK RANGE RDICLAYTON RD
Visit ID
NC DWWQ Laboratory Section 12esufts
Name POL
collect Date: 0611512007
Co0ec1 Tana- 12:30
�� �POtaaaa � fecalp � �
wurysvuam
Approved By Mate
Meew4 Refinen/e
24
'C
DSAUNDERS
MMATHIS
WET
61IM7
620107
Gmeae eM O01n egWE
MethM RNmervx
EPA1664A
10
10
U„IB
Milli.
MIBRAHIM
MOVERMAN
MET
61IM7
62IN7
7440-22<
Ag by ICpMS
M.ffiw Reimence
EPA 2002
5.0
5.0
U
UWL,
JJURGEVICH
ESTAFFORD
7429-945
AI Dy ICP
M26007
MWO7
Metho4 Refinenra
EPA 200.7
160
LIA
DSTANLEYI
ESTAFFORD "
7440-38-2
A8 by ICPMS
622f07
7r3107
Methm Referm/a
EPA 200.8
5.0
SO
U
JJURGEVICH
ESTAFFORD
7440.30-3
Ba by ICP
62607
7r107
Metho4 RNmenco
EPA 200.7
10
44
uwL
DSTANLEYI
ESTAFFORD
7440i1-7
BB by ICP
62607
7/4107
'
McNW Rmmence
EPA 200.7
5.0
5.D
U
OyL
DSTANLEYI
ESTAFFORD
7440-70.2
Ce by ICP
WD07
7307
Me0m4 Rammlce
EPA2003
0.10
89
rrlglL
D IT LEY
ESTAFFORD
7440-48-4
Cop x uy ICPMS
�`"07
7r1N7
Meaw6 RNmervs
EPA 2f10.8
U
OA
D IANLEYI
ESTAFFORD
744047,3
Cr by ICPMS
�=7
MM
McNo4 Reimerve
EPA 200.8
10
10
U
LO&
JJURGEVICH
ESTAFFORD
7440-50-8
CUMICPMS
62W7 -
7rM7
Melho4 RNmerice
EPA 200.8
2.0
2-0
U
uglL
JJURGEVICH
ESTAFFORD
7440-48i
Fa by ICP
62607
7/107
Ma0w0 RNmence
EPA 200.7
50
3200
LIA
DSTANLF'1
ESTAFFORD
7439-97.6
Hg 245.1
6/22)07
71=7
Me0w0 Retmmcn
EPA 248.1
02
D.ZO
U
OgIL
PGAUTHIER
ESTAFFORD
7439-95-4
Mg OY ICP
820'07
73N7
Memw Refineelx
EPA 200.7
0.10 �
28
MO&
DSTANLEYI
ESTAFFORD
7439-96-5
Mn by ICPAIS
625/07
M107
Metio Refer
EPA 200.8
10
1800
LIA
DSTANLEYI
ESTAFFORD
7439-98-7
Mo by ICPAI$
6QM7
7rf1o7
MeewC ReM1marre
EPA 200.8
10
10
U
lqh,
JJURGEVICH
ESTAFFORD
7440.23d
Na hY ICP
627M7
7/107
MeMotl RNmarve
EPA 200.7
0"10
5-4
I glL
DSTANLEY
ESTAFFORD
625A7
7r107
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 )919) 733.3908 Page 2 of 11

LocaLon',il: CUBCREEKRANGERD
NC In WQ Laboratory Section Results Sample ID ABI828:
Loc. Deacr.: CUB CREEK RANGE RD/CLAYTON RD Collect Date: 0611512007
Visit ID Collect Time:: 12:30
Name
r440-02-0
NI by ICPMS
_..._
.ei ybuudtu
Approved Fly !Date —
McUioC Reference
EPA 200.8
0
10
U
Wt.
JJURGEVICH
ESTAFFORD
7439-92-1
Pb by ICPMS
6¢rv07
7c 17
Melno4 Reference
EPA 200.8
10
10
U
LVL
JJURGEVICH
ESTAFFORD
7440-36-0
Sb by ICPMS
626U7
7f"7
Method ftelerenca
EPA 200.8
0
10
U
�L
JJURGEVICH
ESTAFFORD -
7782-09-2
Sa by ICPMS
627M7
7r3,D7
MathoE Reference
EPA 200.8
5.0
SD
U
oglL
JJURGEVICH
ESTAFFORD
7440.31-5
Sn by ICPMS
626117
MV07
Method Reference
EPA 200.8
10
10
U
JJURGEVICH
_
ESTAFFORD
7440-28-0
TftalOum (Tn ICPMS
6r27g7
773107
Me
Method Reg..
200.8
10
10
U
U91L
ESTAFFORD
ESTAFFORD
7440.32 6
TI (71Mrdtan) by ICP
626007
71M7.
MeReference
EPA 200.7
10
10
U
11�
DSTANLEYMelted
ESTAFFORD
7440-02-2
V by ICP
62=7
MM7
R Meth
oO e/erence
EPA 200.7
25
25
U
W4
DSTANLEY
ESTAFFORD
7440-66-6
Zn by 1CP
6rz6N7
7r3N7
McNed Retcence
EPA 2003
0
10
U
�
DSTANLEVI
ESTAFFORD
VOL
622f07
7r 7
75-78-1
Eyoj,,dML merle
.
1.0
Not ddedlad
uWL
MMW Rete..
FPA50301W48260
ATERRY
WELLING
`y 74-87-3
py0lmtdhane
6""7
OrLet07
Mehod Reference
EPA50301i2q/826p
.050
0'�
pa
Wti
ATERRV
RKELLING
75-01-4
Vinyl Chlpye
61IM7
628417
O50��
tyyL
Method Reference
EPA5030I624(8260
ATERRY
RKEWNG
74-83-9
1Wotrp01e01Hne
611&07
612M7
0.50
Net detected
MOtL
Mehod Refvence
EPA5030fR4tg260
ATERRY
RKELLING
75-00-3
C1110tpe1bgrM
6118107
62aN7
0.50
Not defected
lf�rL
MafhoO Reference
EPA5030U24B260
ATERRY
RKELLING
75-69-4
Tfkhk Bfarmledlerle
611 M7
628107
0.50
NoltlOtectad
Mallod Reference
EPA503(y6p4/9280
WO-
ATERRV
RKELLING
75-35-0
1,1-LAcr5oronn,,e
-
N18f07
ISUM7
0.25
IJlrt deterred
McBgd Relerenra
EPA503062q/8200
WrL
ATERRY
RKELLING
75-09-2
Metttyklte Gllaflde
N18N7
62M7
0
�
�
Meead Relerafce
EPA5030424/8260
ATERRY
RKELLING
'156£0.5
b8f19-1,2-0Iddrypyjlyq
rvIM7
8r18107
0.25
Nol detected
WrL
edrod erence
Reference
EPA503dfi2q/8260
ATERRY
WELLING
N18107
6/29107
Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
Page 3 of 11

Location.J: CUSCREEKRANGERD W q)WQ Laboratory Sectw' n Re` lifts
Loc. Descr.: CUB CREEK RANGE RDICLAYTON RD
Visit ID
Analyte Name - PQL
Collect Date.
Collect Tenet:
0611512007
12:30
Mclhod Re..r
EPA50300624/9260
w�
nicnnr
RKELLING
75-34-3 1.1-0IClll0toethW5
b18/07
608W
MeewC Retmenu
EPA5030I62!/8260
0.25 Not detected
qyL
- ATERRV
RKELLING
156-59-4 ya-1,2-0Idtlomedlene
b18A77
6/ 8,07
Met6e4 Reference
EPA503(L524Ifp60
0.25 Nye
MWL
ATERRY
WELLING
74-97-5 BfOme(111e1en1pelgee
611&07
602M7
Meewe Retmenes
EPA503(IU419260
025 Not deemed
UWL
ATERRY
WELLING
Mee Reference EPA50301624/6260
McMW Retwr
EPA50301624WW
Method Re .m
EPA5030524AQW
1-Trlct"Udhele
Meew4 Rele .
EPA5030�4/FI 0
b1807 W=7
ATERRY RKEE
'bl&07 6211107
6/1&07 628007
bl&07 62be7
61IM7 628,07
Me Rdereooe EPA50301624/9260 +- n1cnnr HKELLING
5623-5 Caltm Teeedtltldde b16D7 612M7
0.25 Not detected Ug1L ATERRY RKELLING
Meew4 Rebrence EPA5030r2V8260
Me6 Reference EPA5030024MM
MA
6/18107 6r2=7
6118107 6R11107
Me1ho6 Reterenm
EPA503N624/8260
n, cnnt
HKELLING
78-87-5
1,2-0Ictlbroproperle
btM7
0Caw
Meows Relmence
EPA5030624/9260
0.25
Not dete0ted
'
LIWL
ATERRY
RKELLING
79-0tb
TdctdoMo
b1=7
62e,07
R.le
Metno4 taranra
EPA5030162U8260
0.25
Nat detected
t1g2
ATERRY
RKELLING
75-27-4
Blompoldllor1x11et1erle
6/lW7
6/2af07
McMM Relwerwo
EPA50301624/8260
0.25
Not detected
UOrL
ATERRY
RKELLING
1W61-01-5
cts-1,3-Dk111omplopene
6Ma07
62=7
Me1no4 Rofcewe
EPA503p,624182fip
025
Not de0eme0
UBIE
ATERRY
RKELLING
b1607 6/28107
Metl1o4 Raleranre EPA50301624/8260
n,cnnr HKELLING
b1807 62a107
7soas 1,1 d-Tdwaosvl 0.25 Not detected
uplL ATERRY RKELLING
Meew4 Ralttare EPA5030524/8260
6118,07 628,407
Laboramry Sectloou- 1623 Mail SG"loe Center, Raleigh, NC 27699.1623 (919( 733J908 Page 4 of 11

Location ID: CUBCREEKRANGERD XC `' Q Laboratory Section 12esufts
Loc. Descr.: CUB CREEK RANGE RDICLAYTON RD
Visit ID
# Analyta Name PCIL
Resuk pualifier Unks
Tohfena
Sample ID
Collect Date:
Collect Time::
AB18282
06/1612007
12:30
WIM7
McMoe Reference
EPA5030624/8260
0.25
Nd detached
uWL
ATERI
6/1 W7
McOwtl Reference
EPA50301fi2418260
0.25
WIL
- ATERI
'DB)1,2-016romoeplene
6118107
Method Reference
EPA503052d/8260
0.25
Not detached
UWL
ATERI
&IBM7
M<MOC Referwe
EPA503062V8260
0.25
Nd detefded
LIWL
ATERF
110toberizme
WI M7
McMca Re/erence
EPA503652418260
0.25
Nat defarSed
'
WrL
ATERF
tlylhen>Mloo
61118f07
Method Referenm
EPA5030162418260
0.25
Not defiled
UWL
ATERF
omofOfin
6118f07
McMoe Reterence
EPA5030r2418260
1.0
LIWL
ATERF
P-Xybne
&IW7
WMad Reference
EPA5030/624f8260
0.50
ed
WIL
ATERF
Rolle
6118N7
McMoo Reference
EPA503OW418M
0.25
Nd detected
LWL
ATERR
,2,2-TBC3WorO8MarlB
6118N7
Method Referece
EPA50301621/8260
0.25
Not detectedLIWL
ATERR
.1.2-Tetradtloroadlane
6flW7
McNoe Refererrr.
EPA5030Ti21/8260
0.25
����
uWL
ATERR
;ylene
W W7
McMoO Reference
EPA503dfi21/8260
0.25
dtlletled
uWL
ATERR
,3-Trk3Jorgaoperlo
6118t07
McMOG Reference
EPA503ry62d18260
0.25
�
LIWL
ATERR'
XWA
W IV07
McMoO Relerenm
EPA50;p1624I8260
0.25
d�e�
tlp4
ATERR'
mOkerlmrM
6118(07
MBMOE Reluenca
EPA5030fi24B260
0.25
Oe0ot0a0
OWL
ATERR'
rOPYIh'enaena
61IM7
McMOE Reference
EPA503042418260
0.25
'�
ATERR`
ttlefolehMflp
N18f07
McMotl Refererre
EPA503016241g260
0.25
Not delected
LIWIL
ATERRI
6118N7
APProved By Mate
RKELLING
WW7
RKELLING
62M7
RKELLING
628f07
RKELLING
6 11107
RKEWNG
6R8N7
RKEWNG
62W7
WELLING
628107
RKEWNG
62M7
RKELLING
WM7
RKELLING
W=7
RKEWNG
628107
RKELLING
628f07
RKELLING
WaM7
WELLING
628107
RKELLING
6128107
RKELLING
628/07
RKEWNG
628107
RKELLING
6/28,07
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
Page 5 of 11

NC (D WQ La6oratory Section IZesufts
Looaion lD: CUBCREEKRANGERD
Lx. Descr.: CUB CREEK RANGE RDICLAYTON RD
Viva ID
Collect Date:
Collect Tune::
D611512007
12:30
POL Result Ouall0er Units A1WysUDate Approved By (Date
10867-8
Metta4 Relerenm
1,3,5 eT Refere erte
Me0we Reference
EPA503110626/8260
EPA50301624/8260
0.25
Notdetec7ed
-
uglL
6/18N7
ATERRY
6118107
NAtLLING
6128N7
RKELLING
6r2m7
98-06-6
M-glnylyavglp
0.25
Not detected
ugfL
ATERRY
RKELLING
Memo) Rebreno
EPA503Oa26/8260
6/18N7
95�3-6
1,2,4•Tnateltlyamm ne
612a107
0.25
Not detached
uyL
ATERRY
RKELLING
Me1Md Reference
EPA503N626/8260
135-98-e
eapglaylpe�yle
61l&07
(WW7
0.25
Not detected
U91L
ATERRY
RKELLING
MM RUerence
EPA503W624/6260
543-73-1
tiF.DtC111atpppnyerM (1.3)
b18107
6Raf07
0.25
Not detected
u9fL
ATERRY •.
RKELLING
Memos Reference
EPA5030524R260
106�48-7
PUIUMMI)IMens(1,4)
b18107
612a107
025
Not detected
1q/L
ATERRY
RKELLING
Memos Reference
EPA5O1pr826/8260
95-50.1
Odlfttlaraperlayy (1,2)
b1IIN7
WM7
0.25
Not detected
W4
ATERRY
RKELLING
MemoA Releren4
EPA503(Yfi2018260
99$7-6
p4 mprapyltpwalp
&18107
6r28107
0.25
Not detected
LIWL
ATERRY
RKEWNG
Me0wd Reference
EPA503O626/8260
104-51-8
a-Dunf Br�efle
b1=7
WM7
025
Not defamed
uglL
ATERRY
RKELLING '
Mamotl Reference
EPA5030W26/8260
96 1z e
12�1�Re
b18N7
6R8107
2.0
Not detected
uyL
ATERRY
RKELLING
Memos Reference
EPA5030r521/8260
120.82-1
1,2,4-Tdmyoropeaarlo
b18107
6/2M7
0.50
Not defamed
up/L
ATERRY
RKELLING
Me0aE Re..EPA5030/6211826p
91-20.3
Nalininalene
6/1 b07
6128IU7
0.50
Not detected
091L
ATERRY
RKELLING
Me11wG Refarenm
EPA5030624/$26a
87-68-3
Flelmtlllofoeutemara
b1b07
&2a107
0'50
Not detected
uyL
ATERRY
RKELLING
M.a Reference
EPA5030r524a260
87fi1-fi
1A2 IrKrdoropenzsne
6/1 b07
W8107
1.0
NaL deteLmtl
uplL
ATERRY
RKELLING
Memod Reference
EPA503b6261$260
2 �
bIM7
6r26107
- X1
uWL
ATERRY
RKELLING
MemeC Releralce
EPA503052U8260
WW7 6478107
Me0ntl Reference G. LUFT/80150
e una
6M8r07 6a8A7
TMmnym0y10uonne 0.63 N7 UOIL - ATERRY RKELLING
Mae RGaence EPA503016248260
61IM7 6/2807
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733,3908 Page 6 of 11

Loca:iori ID: CUBCREEKRANGERD NC L YVQ Laboratory Section 12esufts
Loc. Descr.: CUB CREEK RANGE RDICLAYTON RD
Vied ID
Analyte Name
POL
es
Roh 011alf0er
nits U
Volatile Organics In IIgWA
MenwU Rwbr EPA503016248260
_��
UWL
Chlorinated Pesticides In UgtM
Med Reler EPA 606
_mom
ug/L
AleWor
0.15
Net detected
MBNod Reference EPA 608
NdM
Memad
0.025
of deOBttod
�
Relmenre EPA fi09
%tra21ns
-
MGNod Relerenm EPA 609
3
Not detected
r+OfL
0.025
Not detected
vp1L
M-MW Reference EPA 60e
iHC Bete
0.025
Net detected
Me16oe Relererice EPq fi09
IHC_Detta
0.025
detecOBd
LIWL
Method Reference EPA 609
IltCri�rer i (Llrtdalle)
0.025
Net detected
Malloe Relmence EPA 60e
2dordana, Teci0—
0.5
Not defected
uWL
Maihud Refeence EPA 608
Not detected
�
Malloe Reference EPA 608
1d0rdefle, ti&rllrl8
0.02
Not detected
�L
Medad Reference EPA 608
Mordants
0.025
Not ��y�
Method Rolerenca EPA 609
0.2
Not detected
uyL
Mence
cMW ReferEPA609
Idoroberl
0.6
Not detected
�L
McNeJ Reference EPA 60e
R.t.
0.05
Not defected
MaMod Reference EPA 60a
11prd1El0f111
0.025
Net detected
MedwE Reference EPA 606
pA
0.025
Not deter
Memotl Reference EPA 608
Collect Date. 061IS12007
Collect Time:: 12:30
6'18007
JHAYES
6125/07
JHAYES
62507
JHAYES
WSW
JHAYES
62W7
JHAYES
62507
JHAYES
62507
JHAYES
625t17
JHAYES
625M7
JHAYES
625/07
JHAYES
625107
JHAYES
625/07
JHAYES
625107
JHAYES
62507
JHAYES
625W
JHAYES
62&07
JHAYES
625N7
JHAYES
62&07
Approved By
RKELLING
62 07
RKELLING
7/16/07
RKELLING
7/lW7
RKELLING
7/1W7
RKELLING
7/16/07
RKELLING
7/16I07
RKELLING
711 &07
RKELLING
7/1 &07
RKELLING
7n6r07
RKELLING
711 &07
RKELLING
7/16N7
RKELLING
7/1&07
RKELLING
7/1607
RKELLING
711 6107
RKELLING
7/16I07
RKELLING
7n6/07
RKELLING
7/16107
RKELLING
711 &07
Laboratory Sectiom> 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
Page 7 of 11

Location ID: CUSCREEKRANGERD NC D WQ Laboratory Section Results
Loc. Deacr.: CUB CREEK RANGE RDICIAYTON RD
Visit ID
Collect Date:
Collect Tene::
06115f2007
12:30
Reautt Qualifier Unite AnalysVDate Approved By /pate
Me0w4 Ralpence
EPA 608
- -
nnCLLlrylj
72-54-8 130D4,4'
625N7
7116107
0.025 Net detected W2
Me0w4 Reference
EPA 608
JHAYES
RKEWNG
3424-ffiE f3DE 2,1'
62507
7M6N7
et 0.04 Ndefected
W2 JHAYES
Me0w4 Refpexa
EPA 608
RKELLING
62507 7MW
1,4e0w4 Ralpmce
EPA 608
NtLLING
769-02fi
ODT 44'
52S07
7/16107
0.03
-
Not defected
JHAYES
RKEWNG
Metnoa Reipenre
EPA 608
50.29-3
DDi 4,4'
WSW
7116107
0.025
Not detected
W2
JHAYES
RKELLING
Metho4 Reference
EPA 608
60-57-1
pleltlrin
62507
7/16107
0.025
Netdetncted
LIWL
JHAYES
WELLING
M.0 RaMenco
EPA 608
959-98.e
Flw..•xa..f
Ef1507
7/16107
0.1125
- Not detected
W/L
JHAYES
RKELLING
Me6wE Referenm
EPA 609
33213-659
EndmJ6r111
625N7
7/16N7
Net detected
u01L
JHAYES
RKELLING
Me0ro4 Retperex
EPA 6080.025
-
1031117-6
B10osutlan etiolate
625N7
7AM7
0.025
Net detected
OC/L
JHAYES
RKELLING
Me0g4 Re..
EPA 608
7z-20-6
FJMM
625,07
7MM7
0.025
Not detected
Wk.
JHAYES
RKELLING
Mail" Reference
EPA 608
7421-93i
EMMe AN
625107
7116107
0.025
Not detected
uyL
JHAYES
RKEWNG
McOpE wfw
EPA 608Retpenre
53494-70.5
FJ1dM Ketale
625M7
7116r07
0.03
Net detached
W1L
JHAYES
RKEWNG
McNo4 Relpenca
EPA 608
2593-15-9
Elheaole
625107
7M6107
0.06
Not detachetl
DpIL
JHAYES
RKELLING
McNo4 ftefpenre
EPA 608
76��
fi2507
711607
Not detached
uD1L
JHAYES
RKELLING
McOnd
hil Relpenre
EPA 6080.025
1024-57-3
Iteptaddor apoldde
W25'07
711fi107
0.025
Not detected
uGtL
JHAYES
RKELLING
-
_.MeNo4 Rtlpenm
EPA 608
118-74-1
FimmdBprphe0mrle(pp6t)
W507
7/16107
0.015
- Nett
W1L
JHAYES
RKEWNG
Metlp4 Rtlerara
EPA 608
121-75-5
ttafaddarl
625107
7n6r07
0.2
Netdetected
W/L
JHAYES
RKEWNG
t1oNo4 Refeence
EPA E08
612507 7116107
Laboratory Section» 1623 Mail Sarvica Center, Raleigh, NC 27699-1623 [phone] Page 8 of 11

Locaiion ID:
CUBCREEKRANGERD
NC IDWWQ La6oratory section Wsufts
Sample ID
AB1828,
'
Loc. Descr.:
CUB CREEK RANGE RD/CLAYTON RD
Collect Dale:
06115/2007
Visit ID
Collect Time:
12:30
CASs Anatyte Name
POL
Result Qualifier
Units
7243-5
McOttixp r444
0.1
Not detected
-Method Reference
EPA 608
W'
2385-85-5
Mlrelc
0.03
tiw
Method Reference
EPA GallNot
39765-80-5
Tmrm N r dyor
0.02
Not detected
UW
Method ftalarmm
EPA 608
2688048-8
Olrydit h,,
0.05
Not detected
ugr
Method Relerenm
EPA 606
52645-53-1
M6red Pearled -In
Me0iod Referer[m
EPA 608
1.2
Not detected
1918-16-7
Prapedllor(EC)
0.3
Not detected
LionMa0rod
Reference
EPA 608
117-18-0
TealaDerle
Method ReferenceEPA
608
0.01
Not debcted
Ito
1582-09-e
TrMrselln
Method Refer
EPA608
0.035
Not detected
12674-11-72
Aroctor 1016
Method Relerencc
EPA 608 '
1
Not detected
�
11104-28-2
!-odor 1221
Ralarenm
EPA 608
1
Not detected
OWL
11141-16-5
ArorJor 1232
Method Referanm
EPA 608
1
Not detected
uyL
53469-21-9
Arodor 1242
Method Relarenre
EPA608
1
Not detected
�
12672-29$
NOcI-r 1248
Method Reterenm
EPA 608
1
Not detected
uWL
11097-69-1
Amctor 125{
Method Reference
EPA 6M
1
Not deected
uplL
11096-82-5
groctfy 1260
Me01od Relarence
EPA 608
1
Not deterded
uWL
37324-23-5
Arodor 1262
Medwd Reference
EPA 608
1
Not deected
Milk
8001-35-2
Tolalpfrerle
Method Relevance
EPA 608
3
Not detected
uplL
Uniden011ed postal by GdECD
Method Retttenm
EPA608
3
uWL
625'07
JHAYI
625I07
JHAYI
625w
JHAYI
625N7
JHAYE
fi25107
JHAYE
6125107
JHAYE
625107
JHAYE
62507
JHAYE
WSW
JHAYE
WW07
JHAYE
625107
JHAYE
W&U7
JHAYE:
625107
JHAYE:
625107
JHAYE;
625A7
JHAYE;
625M7
JHAYE:
625M7
JHAYE'.
625/07
Approved By
RKELLING
7/16107
WELLING
7116107
RKELLING
7/16107
RKELLING
7/16A]7
RKELLING
7n6/07
RKELLING
7n6107
RKELLING
7/16I07
RKELLING
7nem7
RKELLING
7/1607
RKELLING,
7n6107
RKELLING
711607
RKELLING
7n6107
RKELLING
7/16107
RKELLING
7/16N7
RKELLING
7/i6N7
RKELLING
7/16107
RKELLING
U16M7
RKELLING
7/16/07
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 9 of 11

M
Location ID: CUBCREEKRANGERD
Loc. Descr.: CUB CREEK RANGE RDICLAYTON RD
Visit ID
NC IDWQ Laboratory Section Resuhs
Collect Date:
Collect Time::
t1611612007
12:30
Analyte Name POL Result Ouallfier Units Analyst/Date Approved
APP
No4 Reference
EPA 61/
-
-ACLUNU
786-19.6
Gerbppletretli0rl
7112107
7/16107
0.8 Not detected
WfL
EPHIWPS
RKELLING
McNo4 Reference
EPA 611
LZEMPyd(os(FPD)
]112107
71IM72921-88-2
Metnm Reference
EPA 614
0.4 Net detected
WIL
EPHILLIPS
RKELLING
78-0e-8
pEF ( d merpina)
7112/07
7n6M7
0.4 Not deterred
WIL
EPHILLIPS
hotl R
MeegO Rnlermre
EPA fit/
RKELLING
7/12J07 7/16)07
Metllo4 Reference
EPA 614
-
UWL
EPHILLIPS
RKELLING
333-41-5
D{azLtoll
7I12M
7116N7
0.4
Not detected
oGIL
EPHILLIPS
RKELLING
Me01c4 Reference
EPA fill
62-7}7
DkJyorws(FPD)
7112007
7116107
2.1
Net detected
DGIL
EPHILLIPS
RKELLING
Method Relererlce
EPA 61/
60.61-6
D4nedloate
7112107
7MM7
04
Not detected
UGIL
EPHILLIPS
RKELLING
Mahan Rnlarence
EPA 61/
298.04-0
DlsWluln
7/IM7
7JIM7
0.8
Not elected
11gIL
EPHILLIPS
RKELLING
Metnen Rnierence
EPA 614
2497-06-6
Dlb=xan Z41IR e
711Se7
7/1607
1
Net detected
WfL
EPHILLIPS
WELLING
Melhan Reference
EPA 614
249717b
DLvdlaton SWtnl4de
]112J07
7M6,07
NE
Net detected
WIL
EPHILLIPS
RKELLING
McNe4 Relnrenre
EPA 614
2104-64-6
EPN
]/12/07
7/16/07
0.4
Not detected
rIWL
EPHILLIPS
RKELLING
Merton Refaeire
EPA614
'
56}12-2
Elftlon
]112N7
M6m7
0.4
Net detected
IIyL
EPHILLIPS
RKELLING
Meuan RNerence
EPA 614
13194-08-4
EtfropIOP
7112/07
7MW7
CA
Not detected
Wit-
EPHILLIPS
RKELLING
Meton Relnrare
EPA 611
55-38-9
renown
7/12107
71IM7
0.4
Net detach9d
1IgIL
EPHILLIPS
RKELLING
Melnen Relnenca
EPA 611
115-90-2
Fenudidtldon
7/t2A7
]n6N7
22 •
Not dye<Sed
l
ugL
EPHILLIPS
RKELLING
MBIno4 Reference
EPAfi11
34 7
Me (FPD)
7/12A17
71IM77786
0.4
Not defected
uglL
EPHILLIPS
RKELLING
Methf
Melno4 Releranca
EPA 61a
6923-22-0
ManpootoPfge
7/12107
71IM7
1
Net detected
I1gfL
EPHILLIPS
RKELLING
McNoO Reierence
EPA fit/
7/121r/7 ]/16/07
Laboratory Section» 1623 Mail Service Carrier, Raleigh, NC 27699-1623 [phone] Page 10 of 11

Lora(ion 10: CUBCREEKRANGERD NC L' • Q Laboratory Section q?Ssu t$
Loc. Descr.: CUB CREEK RANGE RDICLAYTON RD
Visit ID
Analyte Name
PpL
Resu lt pualifier Units
Wed
2.7t�
Me1no4 Referencc EPA 614
��
0.4
Not defxted
Metlro Reference EPA614
lah„ Parafton
0.4
14o1 detBCOBd
MetlwO Reference EPA 61!
1loon,
0.4
Nor de(eceed
McNod Relmenm EPA 611
Onr1el
. 0.4
Not detecsed
Me0n0 Releren<x EPA 614
DPP
0.4
Not XaCbd
M.MW Reference EPA 614
vlr,rin.
Madd pealsm by GC/Fpp u'•
Method Reference EPA 614
sm. late &490lg Meng del. by GCI
McMW Refers EPA We
Collect Date: OWIS12007
Collect Time. 12:30
7112107
EPHIL
7/12W
EPHIL
7112107
EPHIL
7/12/07
EPHILI
7/12107
EPHILI
7112A7
EPHILI
7/12/07
EPHILI
7/12W
JHAYE
WSM7
Approved
RKELLII
7/16107
RKELLII
7/16107
RKELLII
7116 7
RKELLII
7/1=7
RKELLII
7n6M7
RKELLII,
7A6107
RKELLII,
7M M7
RKELLII,
7n W7
RKELLII,
711=7
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
Page 11 of 11

COUNTY tX5ot CG+
RfVER BASIN:
'Ra�Pa Li
REPOR770 ) Regtuual OtBce
Other
_VjCOLLECTOR(S) : `�
Fatinaled HOD Range:
Seed: Chlorinated:
iWwn N/In tm Code Date Begio (yy/nn✓dc
u ly �I V rat 1 �. • F cY���&o& t j 5
DOD 310 "9(L
COD High 340 -wL
COD Low 335 ng/L
Colilorn' MF 1" 31616 /l000l
Colif—: MF Toml 31504 /100rol
Colifomr tribe FeW 31615 /100n1
CPISan: Feel Slrep 31673 /100nd
Reidue: ToW SW rowl-
Volriile SOS n9/1-
Fixed 510 tug/1-
Residue: Suspended 530 mg/L
Volnilc 535 n4/L
Fixed 540 -9fL
pH 403 armor
Acidity to pH 4.5 436 uig/L
Acidiy to pH 9.3 435 -w/L
AlkAinity to pH 8.3 415 mg/L
Allalinity m PH 4.5 410 owl.
TOC 680 owl
Tmbidiry 76 NTU
Colif000 Tomt Tube 1/100 nls
COMMENTS:
DIVISION OF WATER QUALITY
Chemistry tabontery Report/Water Qua6ly �j��Jy�' f�1�////�%/�//(//�
PRI` IORrTY SAWI F TYPE ) ( / 6/ V
AMBIENT
QA
�TR13AM El
EFFLUENT
COMPLIANCE
CHAIN OF CUSTODY
LAIC INFLUENT
ElEMERGENCY
VISITm
ESTUARY
Station Incatlom
IV r rr ! �� ;/
f1
Remarim:
D A-4.
Dale Fab (yy/mtddd)
Time Begin
TLne Eud
Depth - DM, DB, DBM
Value Type - A. tt, L
O
��l�s�a��i�L,
Chloride 940 mg/L
Chl e: Tri 32217 ug/L -
CM a: Car 32209 ug/L
Pheo hylin a 32213 ug/L
Coles T= 80 c u.
Colo[ (pH) 83 H- c.u.
Color: H76 82 e,u
Cyatude 720 -9(L
Fluoride 951 -9 -
Fomuldehyde 71880 nWL
Grove and Oils 556 uig/L
Hardness Taa1900 u9/1,
Specific Cad. 95 uoA d.
MBAS 38260 nWL
PheooB 32730 ug/L
Sulfite 995 -19fL
Sullido 745 -911-
Boon
Tannin & Lig in ug/L
Hwvaleid Clumdom U911.
Binrbaute nWL
Carbonate ng/L
Tout Dissolved Solids -9 L
S'AT = Iti. 5 ;JA 'i= 11.S I e n /'I -
-
NH3 as N 610 Pig/L
T104 an N 625 - mg1
NO2 plus NO3 to N 630 ng/l,
P: ToW a P 665 uiWL
PO4 as P 70507 m9/1,
P: Dissohed a P 666 nWL
K.PPtassiuro nWL
Cd-Cadmion 1027 ug/L
CrLlvontium:Total 1034 owl
V
Cu Copper 1042 ug/L
Ni-Niels l 1067 ug/L
P& Lead 1051 ug/L
Zp Zine 1092 ug/L
V-Vamdiun ug/L
Ag- Sihc 1077 u�L
N-Almtdmun 1105 ug/L
Buylliun 1012 ug/L
Ca-Calcium916 nWL
Co- Cobalt 1037 ug/L
Fe-Imm 1045 ue/L
Mo-Molybd� ug/L
-/
Sb-Aniao ug/L
V
Sn-Tin ug/L
Tt-Thallium up/L
Ti-Titanium ug/L
Hg-1631 nyI-
Lab Niunber /
Date Received:
Time Received:
Received By
Data Relea4 d
Due Reported:
Ca Poslte-T, S, B I Sample Type
Li-Lithimn 1132 WJL
-Mg- Magncsimn 927 ng/I.
Mn-Murg.. 1055 W/L
-
Na- Sodium 929 n9/1.
Arsenic.Tout 1002 W/L
S' Seleni= 1147 ug/L
Hg- Maauy 71900 ug/L
B.Herinm ugfL
OTx ddorvie Penicidm
Or�nophosphorus Perricidn
C
Arid Herbicides
B--(Nernnl&gcid EM.,table Org..
TPH Diesel Range
to Orguiio (VOA boale rcgd)
TPH Grsolirc Range
TPHBTEX G.I. Range
Aifthytoptod—
Tanpcurne on emival (°C)'

NC DENR/DWQ Laboratory
Report to: _RALIEGH Sample Anomaly Report (SAR)
Lab Number:
AB18283
Sample ID:
1
station Location:
CAB CREEK
County: PERSON/GRANVIL
Region: RA 4R6pf
NEAR SR1727
LE
AND PEED RD
Sample Type:
STREAM
Priority: N/A
Collector: V.WEBB/A.HOBAN
Date collected: 6/15/07
Date received: 6/18/07
Date analyzed: 6/19/07
Affected Parameter(s):
GREASE AND OILS
Analytical Area (check one):
®WCH []METALS
[]NUT ❑MICRO
The following anomalies occurred (check all that apply):
❑Samples
❑Improper container used
[]VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑Holding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
[]Sample exhibits gross non -homogeneity
❑Sample not chemically preserved properly
❑pH out of range (record pH):
❑Improper chemical
[]Residual chlorine present in sample
❑Color interference
[]Heavy emulsion formed during extraction
[]Sample bottle broken in lab - no reportable results
®Other (specify):Cooler Failure.
❑VOA ❑SVGA
❑PEST
❑Quality Control
❑Instrument failure - no reportable results
❑Analyst error - no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
[]Spike recovery
[]None added
❑Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑Intemal standards
[]Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
approval
[-]Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume
Comments: Sample received on 6/18/07 at 8:45 a.m, it was stored in the Nut/ wet them cooler, the temperature at this time was < 6
degree Celsius until) 1:00 am 6/19/07 started malfunction ,at 8:00 a.m(6/19/07) the thsca .,,.t,.. was reading 12.0 degree Celsius
44V,A 0 M C}t-1 A.%
Corrective Action:.Sample transferred to the semivolatile cooler untill the time of the analysis 9:00 a.m on 6/19/07.
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:J8
❑Other (explain):
Notification Required? ❑ Yes ® No
Person Contacted: Date:
Form completed by: a di Ibrahi /J» Date: 6/19/2007
Lead Chemist Review (initial):
BBIOCH EM
❑METALS
❑PEST_
❑VOA
Branch Head Review (initial; 6/Z/ / C t
QA/QC Review (initi (Q �0a
QATOo 11S\L bOMWY 4AR
❑SVGA
Logged into database by (initial):
IORa/01db,

I.M. Descr.: REPUBLIC LANDFILL
Location to: REPUBLICLANDFILL
County: PERSON ��F WA7FRO
River Basin
Report To RROSP ' \
Collector
Region: RRO
Sample Matrba: Surfacewater - --
Loc. Type: RIVER/STREAM
U
Sample Depth 1 .-;:
Sample Qualifiers and Comments
Sample ID:
AB18285
PO Numbers
TW4570
VishlD
Coiled Date:
06115/2007
Coiled Time
15:15
Date Received:
0611IMM7
Time Received:
08:05
Labworks LoginlD
MMA
Date Reported:
07/16/2007
Emergency Yes/No
COC Yes/No
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.ctwglab.org under Staff Access
A -Value reported is the average of two or more determinations
Bl-Countable membranes with <20 colonies; Estimated
B2- Counts from all fitters were zero.
B3- Countable membranes with more than 60 or 80 colonies; Estimated
Bd-Filters have counts of both >60 or 80 and < 20; Estimated
B5-Too many colonies were present; too numerous to count (TNTC)
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated
J3-The sample mamx interfered with the ability to make any accurate determination; Estimated
J6-The lab analysis was from an unpreserved or improperly Chemically preserved sample; Estimated
N 1-The component has been tentatively identified based cn mass spectral library search and has an estimated value
LAB
N3-Estimated concentration is < POL and >MDL
NE -No established POL
P-Elevated POL due to matrix interference and/or sample dilution
O1-Hording time exceeded prior to receipt at lab.
O2- Holding time exceeded following receipt by lab
PQL- Practical Ouantitabon Limit -subject to change due to instrument sensitivity
U- Samples analyzed for this compound but not detected
XI- Sample not analyzed for this compound
Laboratory Section >> 1623 Yell Service Canter, Raleigh, NC 27699-1623 (919) 733-3W8 Page 1 of 11

Location 10:
Loc. Descr-.
Visit ID
REPUBLICLANDFILL
REPUBLIC LANDFILL
NC 1O WQ Laboratory Section 12esufts
Name POL
Collect Date: 06/152007
Collect Time:: 15:15
Sarllple tenlparaarre et retnla by lam
___...._.
.,,.,
wwryseuale
APProved By IDate
McNoe Raferenra
24
'C
DSAUNDERS
MMATHIS
WET
WIM7
62010
Grease and On 61 liquid
Method RHcrence
EPA1664A
10
10
U,J8
n1pIL
MIBRAHIM
MOVERMAN
MET
6/19/07
IW1107
7440-22-0
AG by ICPMS
McNca Reference
EPA 2008
5.0
5.0
U
ILIA
JJURGEVICH
ESTAFFORD
7429-90-5
N by 1CP
626117
713107
McNo4 Reference
EPA 200.]
UWL
DSTANLEYI
ESTAFFORD
7440-38-2
As by ICPMS
6r1207
7M)7
Metho4 Reference
EPA 200.8
5.0
5.0
U
U9IL
JJURGEVICH
ESTAFFORD
7440-38-3
Be by ICP
6r26117
713N7
Me0w4 Re1ermre
EPA 200.7
0
�
uWL
DSTANLEVI
ESTAFFORD
7440-01-7
Ba by ICP
6126,07
7r=7
McNo4 Reference
EPA 200.7
5.0
5.0
U
UWL
DSTANLEYI
ESTAFFORD
7440-70-2
Ce by ICP
WM7
7r 7
Metho4 Rafaenca
EPA 200.7
0.10
_ 7.9
mg/L
USANLLY
ESTAFFORD
7440-48-0
(,ppal(py ICPMS
&25M7
7r=7
Mallo4 Reference
EPA 200.8
50
50
U
u04
DSTANLEYI
ESTAFFORD
744047-3
Cr by ICPMS
628107
73 7
McIhoE Referenm
EPA 200.8
0
10
ll
rrO1L
JJURGEVICH
ESTAFFORD
7440-50-8
Cu by ICPMS
606W
7W7
Method Reference
EPA 200.8
2.0
20
U
W2
JJURGEVICH
ESTAFFORD
7440-08-0
FB by ICP
626107
7/3/07
Method Refinenre
EPA 200.7
B90
UOfL
OSTANLEY1
ESTAFFORD
7439-97b
H9 245.1
622/07
7r3107
Me1ho0 Reference
EPA 215.t
0.2
020
U
ILIA
PGALfTHIER
ESTAFFORD
7439-954
Mp by ICP
620/07
7/=7
Mathoe Reference
EPA 200.7
0.10
3.1
mg/L
DSTANLEY1
ESTAFFORD
7439 -96-5
Mn hY ICPMS
62507
7r3107
Metho4 Reference
EPA 200.8
10
7g
ugfL
USANLEYI
ESTAFFORD
7439- 98-7
Mo by ICPMS
WZU7
7r 7
Methotl Relereilce
EPA 200.8
10
10
U
UWL
JJURGEVICH
ESTAFFORD
7440 -23-0
Na by ICP
627M7
713107
Method Reference
EPA 200.7
0.10
9.7
n191L
DSTANLEY
ESTAFFORD
6r25107
7r W7
Laboratory SecOon» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-39N
Page 2 of 11

Location ID: REPUBLICLANDFILL NC (L)WQ Laboratory Section Resufts Sample ID AB182a
Lot. Dascr.: 'REPUBLIC LANDFILL
Collect Date: 0611572007
Visa ID
Collect Time:: 15:15
Analyte Name POL Resuh puallfier Units ArlaystfDate Approved By [Date
McNOC Refererts
EPA 200.8
7439-92-1
Po b11ICPY
Y2"7
7/ 7S
10
10
U
UWL.
JJURGEVICH
ESTAFFORD
MBNOE Relerarn
EPA 200.8
7440-36-0
Sb by ICPMS
6/26;07
7/J107
10
10
U
u01L
JJURGEVICH
ESTAFFORD
Meaa4 Relarenco
EPA 200.8
Haze
Se
fi27107
7/JN7s-z
5.0
so
u
1Q&
JJURGEVICH
ESTAFFORD
MefhoA Relererrs
EPA 200 8
7440-31-5
Sn by ICPMS
b26107
7rW7
10
10
U
WfL
JJURGEVICH
ESTAFFORD
Mefnoa Reference
EPA 200.8
_
74d0-26
Thaw=(TI) I(PMS
6127N7
7/J/a7
10
10
U
UWL
ESTAFFORD
ESTAFFORD
Mefno4 Rat..
EPA200.8
744o�2a
II (mm�tUM) M ICP
fY2b0]
7/dr07
10
10
u
tplL
DSTANLEVt
ESTAFFORD
Meaw4 Referents
EPA 200.7
7440{2-2
V by ICP
b22M7
7/.L07
25
�
U
u01L
DSTANLEY
ESTAFFORD
Molho4 Reference
EPA 200.7
744or>6�
znbylCP
b2b07
7/JI07
10
to
u
u61L
DSTANLEYI
ESTAFFORD
Mefnaa Rafermce
EPA 200.7
VOL
fi22.07
7W7
75-76-1
Dkhk,,dlm,n,omeyhe
a
1.0
Not detected
11p1L
ATERRY
RKEWNG
Malhaa Reference
EPg5030/62//8260
74-87-3
UdoroRrodtene
b18,07
6/181a7
0.50
Nat defected
u01L
ATERRY
WELLING
Metlwtl Referent"
EPA5036'fi2//8260
75-01
Vlfryl ullorbp
6/1807
6/28107
0.50
Not detected
UWL
ATERRY
WELLING
McMW Rek ema
EPA5030824MW
6018N7
6f28N7
74-83-9
&atrionledterle
0_50
Not detected
upfL
ATERRY
RKEWNG
McMo4 Referents
EPA5030/624/8260
75-00-3
Cflloroethahe
d18107
6R8107
0.50
Not detected
ug/L
ATERRY
WELLING
McOwa Relarance
EPA503062//8260
75E9-4
TdtllbroMpromanans
6184)]
erletp7
0.50
Not detected
uglL
ATERRY
RKEWNG
MalloO Refmmce
EPA5031Y624/8260
75-35e
1,1-0Itltloroath r,
-
6/18,07
6/1e107
0.25
Not defected
Mp1L
ATERRY
WELLING
Neawe Ralerenca
EPA5038062//8260
75-09-2
Me zwierie CJda/lde
611 W7
6/L1907
10
Not detected
u01L.
ATERRY
WELLING
ReMence
EPA50;i0re2Ve28a
156-60-5
bane-1,2-043Ynoefterle
d18N7
6/28107
0.25
Not delerled
W1L
ATERRY
WELLINGMearo4
Relaerrc4
EPA503(L6241g260 -
b18,07
6/2eg7
Laboratory Sectftm» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone] Page 3 of 11

Location ID REPUBUCLANDFILL NC IO WQ Laboratory sectW- n 12esults Sample lD AB18281
Loc. Descr.: REPUBLIC LANDFILL Collect Date: 061152007
MAU ID Collect Tme::
16:16
CAS # Analyte Name
1634.04-4
�yl Ten -Butyl E1har
PqL
Result qualifier
Units
Arm s
y tlDate
APProvr
Meinod Relaence
EPA5030424/8260
0.25
W�L
ATERRY
RKEU
75-34-3
1,1-0kte0rpedtarte
WIt110]
fY2fl/0]
AbNod Raerence
EPASO3W6241926p
0.25
Not Oelected
OPIL
ATERRY
RKELI
156-59d
ds-1,2-0Idtlpo re
6/1 B107
628m7
Mahn Raaence
EPA5030621/8260
0.25
NOI detected
ug(L
ATERRY
RKELL
74-97-5
BIOmpCttl0fpRledlBlle
6'1&117
628107
McOwd Raaenw
EPA50305241e260
0.25
Npl defect60
LIWL
ATERRY
RKELL
67-fib-3
Cftloratam
61IM7
WM7
Mehod Reference
EPA603W41e260
0.25
Net Detected
UWL
ATERRY
RKELL
590-20-7
2�{ fll0repr 1e
IVIM7
W=7
Mallod Re/aenre
EPA5030�6pd/826p
0.25
Not detected
rrg1L
ATERRY
RKELL
107-06-2
1,2-0Ititlorpeplerle
W18107
0213417
Method Raerenm
EPA503ry6p41826p
0.25
F1ot delecta0
OGfL
ATERRY
RKELL
71-55E
1,1,1-TrIWOfoetlmnp
6v18,107
6/28A7
Mehod Raxence
EPA503062V826p
0.25
Not data,
OgfL
ATERRY
RKELL]
563-58-G
1.1-DltldOrnprnpenp
WM7
6f28M7
Method Retaenre
EPA503W624/826p
025
toot detected
LIWL
ATERRY
RKELLI
56-T}5
Carbon Tettactactlde
&111107
628I07
Methotl Reference
EPA50301624/8260
0.25
Net detected
UWL
ATERRY
RKEW
71<3-2
BBflmne
0.25
61IM7
(WW7
R M
elnod etaence
EPA503N624/ 826p
Not defected
ttg0.,
ATERRY
RKELLI
74-953
Dlbrmtctrledrsne
61IM7
626I07
Method Raerarce
FPA507d624/826p
1.0
Not rfefeceed
UWL
ATERRY
RKELW
78-67-5
1,2-0ItlJompmperre
6Vt6107
82W7
Method Reference
EPA5030I624B260
0.25
Not detected
UWL
ATERRY
RKELLII
79-01-6
Tddygp le
6116107
fir2aA7
eowd
MRUaaue
EPA5030624/826p
0.25
Not detect
L UW
ATERRY
RKELLII
75-27<
Bmmpoltlllorp11ep16ro
611 W07
628M7
Method ReMa
EPA50306241e260
0.25
1401 detected
�
ATERRY
RKELLII
61-01-5
—1,3-L.-M opropen6
61IM7
6r2M7
Method Retaence
EPA5030162d18260
0.25
Not defected
�
ATERRY
RKEWt
61-02{>
pens-1,3-Dltldnropropyb
6119107
628g7
Method Reference
EPA5030624/82fi0
0.25
Note
UWL
ATERRY
RKELLIh
79-00-5
1,1,2-TrfOtlprpEpt9rN
N1BA7
628107
Mallod Re..W62V826p
EPA503
0.25
Not detertetl
uyL
ATERRY
RKELLih
UIM7
62M7
By
Laboratory Section» 1623 Nall Service Center, Raleigh, NC 27699.1623 (919) 733,3908
Page 4 of 11

NC iDWQ Laboratory Section ResuCts
SatnPle iD
AS18285
:
Location IDREPUBLICLANDFILL
Loc. Descr.: REPUBLIC LANDFILL
Collect Date:
D61152007
Viisn ID
Collect Tune::
15:15
CAS # AnaMe
Name
PDL
108-W3
TaWerte
Result pualifier
Units
A�IysUDate
Approved By /Date
McOwe Ralaronce
EPA503&R4B260
0.25
Nor detected
uglL
ATERRY
RKELLING
142-28-9
1if� uproperle
&1&07
628,07
Rwdde
EPA503aW4M 60
0.25
Not detected
uyL
ATERRY
WELLING
12448-1
OWrompct6ptaeyhe�
&19,07
62=7
0.25
Nat detetiad
uOIL
Metnoe Rd,..
EPA503662//8260
ATERRY
RKELLING
106-93-4
(EDS)1,2{y0rptppp�
611M7
6281a7
MMoO Relmence
EPA5030162118260
0.25
Not detected
yOIL
ATERRY
RKEWNG
t27-16-4
Tetredduoatltetq
611&07
628107
MaBwE Reference
EPA503062i7a26p
025
Not detected
ttgn.
ATERRY
RKELLING
108-90-7
&I&D7
62aM7
MarIw4 Refinence
EPA5030r52N82fi0
0.25
Nor defecled
IVL
ATERRY
RKELLING
100<1<
Edty6l8f1Ly1e
IWIM7
y1M7
Me11w4 Refmmce
EPA503&62N826p
0.25
Not dMWesd
U91L
ATERRY
RKEWNG
75252
Bt0111a(pRr1
&1=7
W8107
Relmer¢e
EPASOj&62/g288
7.0
Not detected
W1L
ATERRY
WELLINGMe01oe
108-38-3
Il�p-XyI6I18
WIM7
628107
Methoe Relmenra
EPg5030.6p4/8260
0.50
Nd delecteO
ug/L
ATERRY
RKELLING
100-02-5
$(yfene
61tM7
W0,07
Rd.EPA503ry62//g260
0.25
Not detected
uyL
ATERRY
WELLING
79-34-5
1,1,2,2-TeaarJyafDeNaro
&18A17
62ero7
Metfrod Retarmm
EPA503&62/!ffifi0
0.25
Not ta'hed
LIWL
ATERRY
RKELLING
630.20E
1,1,1,2-T�erlYptoeDrerle
W8107
6211107
Matfaa Relmence
EPA5030e2//826p
0.25
Not deteceed
�
ATERRY
RKEWNG
9517E
o-Xylero
61IM7
6QW7
MethoE Relarerce
EPA5030/621/8260
0.25
Not detected
uD4
ATERRY
RKEWNG
96-18-4
1,2,3Tdrtdorapropigne
&1&D]
626107
Ralarence
EPA503d624/8260
0.25
Not detected
uplL
ATERRY
WELLING
98$2E
leapropylhertmne
6118007
62=7
Refinerice
EPA5030b26/a260
0.25
Nor detected
LIWL
ATERRY
WELLING
1
611 a,D7
WW7
MeewO Relmarre
EPA5030524t8260
0.25
- Not detected
LIWL
ATERRY
RKEWNG
103-65-1
fFPTombgmyle
_
&IM7
y28g7
McNoO RNmence
EPA50.TOr1724l8260
0.25
Not detected
t19IL
ATERRY
RKEWNG
95<9-8
21Y�l
&18107
628107
MWRero
McMotl etmenre
EPA5030b2lI8260
0.25
Not depecled
11gIL
ATERRY
RKEWNG
6/1&717
612=7
Lahorat0ry Saodon>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 5 of t 1

Location ID. REPUBLICLANDFILL NC E1WQ La6oratory,S'ection Resufts SW ple lD AB1828E
Loc. Descc: REPUBLIC LANDFILL Collect Date: 0611512007
Visit ID Collect Time:: 15:15
91
C
Name
McMW Reference
EPA503062418260
.3.5-TMlMhylpen]erb
Me W Refererica
>Izerb
EPA5030624/8260
WMW Refer.
EPA5030,524/8260
,2.4-Tdrttr✓rhylbsmerle
MC W Referoce
EPA5036'624/8260
L eMn Reference
EPA5030Ti2418260
-Dkliarohenayp (1,3)
Me11ioG Ralererlm
EPA5030W4we0
DlU1Ipt lbg1211 ('1,4)
Mer11oe Reference
EPAS036624/8260
Dldlbribml2nrte(1.2)
Madh Re..
lsopr6pyllpbteoe
EPA50301624/8260
Mett,ocl RWerence
nZarle
EPA503GW4/8260
M.O Reteence
r�
EPA503OW4/8260
M,,Mo Reference
EPA503052418260
:4-Tdtlduobottmta
M.mw Reference
plttllalerle
EPA503&624/826o
McNod Reference
EPA503016241MM
tab
Meffiw Reference
EPA5030/624mw
,3-Trlrhlor0beR2erle
MeO Reference
EPA5030624/8260
hot0e01y1 very) BRle7
Me w Referenm
EPA$03ry624WW
i-(m In UgUid
KAOMW Reference
Ca. LUFTM15B
Mallo Reference EPA5030L24/8260
MI
&1807
ATERI
611&07
ATERI
&I&07
ATERI
&1&U7
ATERI
r9IM7
ATERF
&IM7
ATERF
&1&07
ATERF
&I&U7
ATERR
61IB/07
ATERR
&1atu
ATERR
&I&07
ATERR
&18107
ATERR'
611B107
ATERR'
&1=7
ATERR`
13918107
ATERRI
&1&07
ATERR)
ISO M
ATERR)
6/18/07
Approved By
RKELLING
62&U7
RKELLING
626/07
RKELLING
62&07
RKELLING
62flf07
RKELLING
628N7
RKELLING
62&07
RKELLING
628/0]
RKELLING
628/0]
RKELLING
628I07
RKELLING
WM7
RKELLING
628,U7
RKELLING
WW7
WELLING
6261D7
RKELLING
62M7
RKELLING
62a/07
RKELLING
6/16107
RKELLING
6r26107
RKELLING
6/2&07
Laboratory Sectlon» 1623 Mall Service Center, Ralelgb, NC 77699-1623 [phone]
Page 6 of 11

Lorseon lD:
REPUBUCLANDFILL
NC IDNQQ Laboratory Section IZesufts
Sample ID
BB18285
Loc. Deacr.:
REPUBLIC LANDFILL
Collect Date:
06/1512007
VIM ID
CWect Tenet:
15:15
CAS # Analyte Name
PQL
Result Qualifier
Units
AnatysUDate
VolatileOrgaldra le 0Q1M
Approved By (Date
Meeln4 Rafera
EPA50301624/8260
— —
ATERRV
RKEWNG
PES
W M7
6rze107
Chlorinated PaWkides In U4dd
Melhoe Reference
EPA608
_TM-F_
LIWL
JHAYES
WELLING
15972.60-8
Aladdor
WSW
7n6007
'
Metlwe Reface¢¢
EPA 606
0.15
Not Ww�W
�Ugk
JHAVES
RKELLING
309-00.2
AIdrN
62507
WIM7
Melhoo Reference
EPA 608
0.025
Na deteCmd
�UWL
JHAYES
RKELLING
1912-24-9
Atrabrle
WW7
7116107
Mallo4 Ralermce
EPA 608
3
1401 detected
twL
JHAYES
RKELLING
319-84$
BHG-Alphg
6125107
7/18107
0.025
Not defxfed
UWL
McNOO Reference
EPA 608
JHAYES
RKELLING
319-85-7
BF1C-Beta
W&7
7/16U7
Moapa RNerare
EPA 609
0.025
Not defected
LIWL
JHAYES
RKEWNG
319-86.8
BHC_papa
WSM7
7/16107
Method Reference
EPA 6088
0.025
Not defeOetl
LIWL
JHAYES
RKELLING
58-89-9
BHC(Wldane)
62607
7n6107
McMW Reference
EPA 609
OD25
Na d�eged
W2
JHAYES
WELLING
57-74-9
CNofdane. Tetilrlkal
6r2.W7
WIM7
Relererve
EPA 608
0.5
Nd detected
uOIL
MAYES
WELLING
5103-71-9
CldOfdelle, Alpha
62607
7116107
Ralmence
EPA 608
0.02
Not deteoed
LIWL
JHAYES
WELLING
5103-74-2
Chlondane%Gomm,
6r2&U7
7/1607
MelM4 Reference
EPA fi08
0.02
Not detected
ugfL
JHAYES
RKEWNG
373448-3
Chlordane
W25M7
7n607
McNoe Reference
EPA 608
0.025
Naf detecMd
u{yL
JHAYES
RKELUNG
2675-7743
17601I1eb
GRW7
711W7
M.MW Reference
EPA 608
02
Not defected
uplL
JHAYES
WELLING
510.15$
6rt607
7ner07
Method Reference
EPA 608
0.6
� defer
MD/L
JHAYES
RKEWNG
2921-88-2
Cltlorpydhn
WSW
7/16M7
th MCod Refer.
EPA 608
0.05
Not defected
uOIL
JHAVES
RKELLING
1897-05-6
Cfl�orlp
625N7
7116107
Refeence
EPA 608
0.025
Not detected
tg(L
JHAYES
WELLING
1861-32-1
DCPA
62W7
7n6o7
Metlwa Reference
EPA 608
0.025
Not Keted
UWL
JHAYES
WELLING
_-.
- 625g7
7n6107
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-39M Page 7 of 11

Location ID:
REPUBLICLANDFILL
NC (DWWQ Laboratory Section 12esufts
Sample ID
ABI82S.1
Loc. Deem-
REPUBLIC LANDFILL
Collect Date:
06/15/2007
Vwt ID
Coltect Tune::
15:15
Rama PDL
53-19-0
DDD 2,4'
'-'...._.
�•„r
w Wlpuuale
Approved By /Date
0.05
00/L
Memoe Reference
EPA 608
JHAYES
RKELLING
72-54-8
DDD 4,4'
625107
7/16107
0.025
Moldelected
LIWL
Meew4 Reference
EPA 608
JHAYES
RKELLING
3424-82{
DDE 2,4'
625107
7/1W7
0.04
Nal detected
110/L
MeewA Relearn
EPA 608
JHAYES
RKELLING
72-55.9
DDE 4.4
62so7
7/16/07
0.025
Nol delec0ad
�
MemoO Relearn
EPA 608
JHAYES
RKELLING
789-02E
DDT 2,4'
625107
7n6/07
0.03
Not deleUed
UWL
Memo. Reference
EPA 60e
JHAYES
RKEWNG
50-293
DDT 4,4'
625/07
7/16107
Memo) Refeence
EPA 608
0.025
���
UWL
JHAYES
RKELLING
60-57-1
Dlaldfyl
fi251W
MW7
0.025
Not tacted
uofL
McOwd Reference
EPA 608
JHAYES
RKELLING
959-9B-e
EndOmdfeR I
rd25/07
7/16N7
Memoe Reference
EPA 608
0.025
Not deteceed
Ofl-
JHAYES
RKELLING
33213-65.9
EfIdOSlifaR ll
WSM7
7/16/07
Method Reference
EPA 609
o.o2s
Not detected
�
JHAYES
RKELLING
1031-07-8
Endo 1.11 aldete
62JW
7/1 W7
m Mece Reference
EPA 608
0.025
�
UIYL
JHAYES
RKELLING
72-20.8
Etldfin
625M7
7/16107
MWoo Refemce
EPA 608
0.025
Not detected
UWL
JHAYES
RKELLING
7421-93-0
Erddn Aldelryde
fi25W
7/16/07
Me0w4 Relearn
EPA 608
0.025
JHAYES
RKELLING
53494-70-5
FsNln KetOrla
625Sd7
7n607
MemoE Reference
EPA 608
OM
Not detected
LIWL
JHAVES
RKELLING
2593-15-9
Etllaaole
6/25M7
7/1W7
Memotl Refeence
EPA 608
0.06
Not detected
ugh--
JHAYES
RKELLING
76-44-8
liepfedllof
fi2Sffi7
71IM7
Mamoe Refeence
EPA 608
0.025
Nol detected
UWL
JHAYES
RKELLING
1024-57-3
tiep�ctllq epeedde
62SM7
7/16U7
Memoo Rofeenm
EPA 608
0.025
Nei delecled
ugfL
JHAYES
RKELLING
118-74-1
HelmdJorobenyeRe(pe8�
6125/07
7/16N7
MetlwC Refeence
EPA 608
0.015
NI#determtl
LIWL
JHAYES
RKELLING
121-75-5
Mall
6261J7
7116A17
Mattw
cUlon Releenca
EPA 608
0.2
Not dBl Ud
LIWIL
JHAYES
RKELLING
625107
7/16M7
Laboratory Section» 1623 Mall Service Center, Raleigh. NC 27699-1623 [phone]
Page 8 0/ 11

Location ID: REPUBLICLANDFILL NC (VWQ Laboratory section 12esufts
Loc. Descr.: REPUBLIC LANDFILL
vait ID
Analyte Name
G5d— for 4,4'
MaN Ralerare EPA 608
w
Me Reference EPA 608
Units
Collect Date:
Collect Tenet:
06/1612007
15:15
62507 7/16/07
WSW View
By (Date
Meepd Raference
EPA 608
'r`^nrca
RKELLING
26880�8-0
&25/07
7/16107
Method Rafarerea
EPA 608
0.05
Nol deteCOsd
LIWL
JHAYES
RKELLING
52645-531
MhEQ peRMOpIR
WSW
7n6107
Malhod Re..
EPA 608
12
Not detected
WIL
JHAYES
RKELLING
7918-76-7
Plppfo
WSW
7/16A17
fE
Methad RR
aNeference
EPA 608
0.3
Not deMOUlad
UVIL
JHAYES
RKELLING
117-18-0
Tealaene
62507
7/1607
M.Reference
EPA 608
0.01
Not detected
LIWL
JHAYES
RKELLING
t582-09-8
TdBualln
62507
7116/07
Melhad Reference
EPA 608
0.035
Not Oetacked
JHAYES
RKELLING
12674-71-12
Alodor 1016
62507
7116/07
Metlrod Refrarlm
EPA 608
1.
Na omectea
W/L
JHAYES
RKELLING
11104-28-2
Amdor 1221
62507
7I16007
Mehod Reference
EPA 608
1
Geltecteo
Wti
JHAYES
WELLING
62597 7/1607
McNoO Reterenm EPA 608
M9/L
JHAYES
RKELLING
53469-21-9
Ng10r 1242
W507
7/1607
Method Referents EPA608
1
���
nprL
JHAYES
RKELLING
12fi72-29di
Aloctor 1248
7/1607
cNcd MRelmente EPA 608
1
Not625/07
0D/L
JHAYES
RKELLING
11097-69-1
grglor 1254
fi25/07
7116ro7
MBNoO Relererlu EPA 608
t
Not
0D/L
JHAYES
RKELLING
11096-82-5
AlprJor 1260
7/16/07
McNlxl Reference EPA 608
1
Not detected62W7
WIL
JHAYES
RKELLING
37324135
Af0ctor 1262
62SM7
7116107 _
I
Not defected.
W/L
JHAYES
RKELLING
McNo Releranca EPA 606
8001-35-2
Tot aphene
62507
711607
Metlnd Reference EPA 608
3
WdetecteA
WIL
JHAYES
RKELLING
WSW
7/1607
(f16de100led DeBlM by GCIECD
lftmW Reference EPA 608
4
WfL
JHAYES
RKELLING
62507 711607
Lahontory Section" 1623 Ua6 Service Center, Raleigh, NC 27699-1623 (919) 733-3W8
Page 9 of 11

NC 1DWWQ Laboratory Section Results
location ID'. REPUBLICLANDFILL
I.M. Deacc: REPUBLIC LANDFILL
Visit ID
Collect Date: 06/15/2007
Collect Time:: 15:15
CAS # Ana,Y. Name
PQL
Result Qualifier
Units
Analyst/Date
based I'estlrldes L47dd
1
Approw
McMaE rence
EPA fit! Refe
TITLE
u4/L
EPHILLIP$
RKELI
786-19-6
CafbophenMon
—EPA
7/12A17
7/16 07
0.8
Not �
Mathotl Reference
�
EPHILLIPS
RKELL
2921-88-2
Chlorpynfioe (FPD)
'
7/11m7
]1eo7
0.4
detected
Metfwd Refererce EPA fiId
u0/L
EPHILLIPS
RKELL
78-48-8
DEF (01dd�ed fl7erplos)
7112107
7116/07
0.4
MethM Reference EPA 614
EPHILLIPS
RKELL
298-03-3
Deffleton
0.9
7112)07
]/t610]
Re Meth
od ference U
EPA6
�
EPHILLIPS
RKELL
333-41-5
pfayrgn
7112/07
7/1607
0.4
Metiwo Rekrenca EPA 674
LIWL
EPHILLIPS
RKELLI
62-73-7
Dkflldws (FPD)
7/12107
7/16107
2.1
Nor dfllaUed
Method Reference EPA614
uWL
EPHILLIPS
RKELLI
60.57-5
Dlrtlealoam
7/12/07
7/16107
EPA 611 Re Mc
Mo4 lerence
04
�
EPHILLIPS
RKELLI
298-04d
DISMoron
7112A7
7/16M7
08
e6wd eference
EPA fi16 R M
�
EPHIILIPS
RKELLI
2497-06-5
Dlsflfo60r1 $td(p1e
7/12107
7116107
1
od eMence
EPA 610 R Meh
09/L
EPHILLIPS
RKELLII
2497-07-6
Dlsutfotm StMmdde
7n2i07
M6107
NE
Nor detected
Mfahod RNerenm EPA 614
uWL
EPHILLIPS
RKELLII
!104{W-5
EPN
7112/07
7/1607
0.4
Not debited
Method aferen¢
EPA 614 R
LIWL
EPHILLIPS
RKELLIf
563-12-2
Eldon
7112,07
MM7
0.4
�
Method Reference EPA 616
UgrL
EPHILLIPS
RKELLII
194-484
E1hglfop
7/12M7
711607
MMnod
O.d
Ncl6eeacfeO
11pIL
Reference EPA 614
EPHILLIPS
RKELLIr
5538-9
Famj1100
7/12107
]116/07
Mehod Refererxx EPA fiId
04
Not detecead
upfL
EPHILLIPS
RKELLIN
115-90-2
FeftaldNlhlOn
7/12107
7/t6/07
Mehod
2.2
Naaereraed
uWL
Reference EPA 614
-
EPHILLIP$
RKELLIN
786-34-7
McMrfpboe (FPO)
7/12/07
7/i6M7
04
Not detected
Method Relerenro EPA 611
77DfL
EPHILLIP$
RKELLIN
323-22-0
blerlppplppfpe
t
7112/07
7/16/07
Mehod Refermrn EPA 614
Not dete0led
EPHILLIPS
RKELLIN
7/12107
7/1 M7
Laboratory Sectlon» 1823 Mail Service Center, Ra"h, NC 27699.1623 (919) 733,3908
Page 10 of 11

Location ID:
Loc. Deacr.:
V*R ID
REPUBLICLANDFILL
REPUBLIC LANDFILL
NC 1O WQ Laboratory section Results
Celled Date: 0611512007
Collect Time:: 15:15
CAS =
Ana" Name
PpL
Result Qualifier
Units
300-76-5
NabA
Analy511Date
APPtD�ad By [Date
2 7
Not datal:tad
LIWL
McMoa Referents EPA 611
EPHILLIP$
WELLING
55-38-2
cmr Peraollen
7/12/07
7/1 OW
McMm Refelerice EPA 6/1
0.4
Not Aetecaed
�
EPHILLIP$
RKELLING
298-00-0
MB9ryl PB1sttllerl
7/12f0]
]nb07
Mefl ERefe we. EPA 611
0.4
� detected
U91L
EPHILLIPS
WELLING
298-02-2
PHpate
7/1207
7MM7
Method Relnenre EPA 611
o.b
Not tfeeadee
�
EPHILLIPS
WELLING
2.-3
Ronne!
7112/07
7/1M7
Mealoe Reference EPA 611
0.4
Not atechad
UgIL
EPHILLIP$
KE
RLLING
3689-24-5
$IMOtapP
7112107
7/16M7
Refeence EPA 611
0.4
Not detectedMetlwo
LIWL
EPHILLIPS
WELLING
13071-79-9
Tefblfioe
-
7/12/07
7/1607
Memoe Relerenoe EPA 61/
0.4
Not dateciald
UO[L
EPHILLIPS
WELLING
7112107
7/16107
Un1�arffed Pam by G(hPD
Me Refemnce EPA 614
1
U9fL
EPHILLIPS
RKELLING
7/12)07
7/1607
Laboratory Sectlon» 1623 Mall Service Center, Raleigh, NC 27GM1623 (919) 733-39o8 Page 11 o1 11

COUNTY �.L J Cl-/
RIVER BAMN: (:1, n
REPORTTOJ� vR7T1\
eglon.l Once
Other
COLLECTOR(S)
Estimated BOD Range:
Seed: Chlorin.led:
itathm#fL tlon Code(1 4 ro legei y/mm
C�/V
BOD 310
COD High 34f
COD Low 335
31615
505
510
Find 540 np/L
atits
off 4.5 436,
IH 8.3 435
76
CONME4TS:
D"ION OF WATER QUALITY
Chemistry lAbontory Report / W.ter Qu.lRy
El
PRIORITY
AI.MIENT QA
COMPLIMCE CHAINOFCUSTODY
EMERGENCY VISIT ID
�J
SAW1 a TYPE
IN—J/IJ/
STREAM EFFLUENT
LAKE INFLUENT
El ESTUARY
Station Location:iia4(
T7ll
a
(v Qlet r r ,
L. A
rmtsddd) Time Begin Time End De i 0� 0 I I� o 3. /5 `I 8�O p[h-DM, DB, DBM Value Type. A, H,L
Chi a: Ti 32217
CM .: Car 32209
Pheophytin a 32213
Cola: Tme g0
Cola: (PH) 83
Cola: PH T6 82
Cyanide 720
Fluoride 951
Fdmtldehyde 71880
Greare and Oils 556
Rardrteas Taw 900
1..b Number
Date Rr ived
Time Received :
Received By
Data Released
Date Reported :
Compostte-T, S, B I Sample Type

Report to: NEUSE
NC DENR/DWQ Laboratory
Sample Anomaly Report (SAR)
Lab Number:
AB18285
Station Location:
SW#1
REPUBLIC
LANDFILL CUB
CREEK
OUTFALL
Sample Type:
STREAM
Date collected: 6/15/07
Affected Parameter(s):
GREASE. AND 0
Sample ID: 3
County: PERSON Region: ____NEwE
Ra/c (� - /0"1
Priority: N/A Collector: V.WEBB/A.HOBAN
Date received: 6/18/07 Date analyzed: 6/19/07
Analytical Area (check one):
®"'CH ❑METALS
❑NUT ❑MICRO
The following anomalies occurred (check all that apply):
)per container used
vials with headspace
le samples with headspace
les not received, but listed on fieldsheet
les received, but not listed on fieldsheet
beled as to tests, preservatives, etc.
ng time expired
'rior to receipt in lab
after receipt in lab
icient quantity for analysis
e exhibits gross non -homogeneity
e not chemically preserved properly
H out of range (record pH):
nproper chemical
tal chlorine present in sample
interference
emulsion formed during extraction
e bottle broken in lab - no reportable results
®Other (specify):Cooler Failure.
❑VOA ❑SVOA
[]PEST
Control
rumen failure — no reportable results
dyst error — no reportable results
added
'cry outside acceptance limits
IJSptxe recovery
❑None added
❑Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑Internal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
approval
❑Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume .
Comments: Sample received on 6/18/07 at 8:45 a.m, it was stored in the Nut/ wet them cooler, the temperature at this time was <6
degree Celsius untill 1:00 am 6/19/07 started malfunction ,at 8:00 a.m(6/19/07) the then —ter was reading 12.0 degree Celsius
+Arvn.mrhe.
Corrective Action:.Sample transferred to the semlvolatile cooler until) the time of the analysts 9:00 a.m on 6/19/07.
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:J8
❑Other (explain):
Notification Required? ❑ Yes ® No
Person Contacted: Date:
Form completed by: a di Ibrahin 'MT Date: 6/19/2007
Lead Chemist Review (initial):
KBIOCHEM _I`�O
❑METALS
❑PEST_
❑VOA
,ranch Head Review (initial): _ 1 O
QA/QC Review (initial � %n/p'7
QAWOMSUw Mtory\SAA
❑SVOA
Logged into database by (initial):

Water Quality Monitoring Field Meter Calibration Sheet
sampling Location:
a
Meters) Make/Model:
Meter(s) Serial #/ ID:
Date
Time
Initlals
Yylmm/dd
24hr Winm
Pro -Sampling Calibration
:00 01"
l)U
Post -Sampling Check
C'J-04 _, S
.(,0
W
M iscellaneous(Dos not apply to YSI 85
or Accumet Meters)
Battery Ranges = Surveyor: (ntemal-
Dissolved Oxvaen (rne
Y/N
Y/N
.2 7.SV, e><temal- 11-13V, Quanta: 4.0 I.5V
L)
Barometric'
D.O. Table Pressure
amp. °C % Saturation Value mmH
_. 9r t s _
' B.P. - 760 - 2.5 (AMDO); A = local altitude above sea level In feet
On D.O. Table, move one block right for every 55 tt. of altitude above sea level
r (PS/cm at 250C
Calibrated
Corrected D.Q. ° Initial Maier Meter
Attitude(ft.) I from Table
Dry Air 1.4 I Conductivity Standard e
Zero (a) 100 n000n0Calibration Check
o0o /47soor mn00n 000/10 000/
Inlhal Meter Calibrated ° Initial Maier a
Reading Meter Reading Readinn Calibrated Initial Meter 3105(ii Olaf'
I within t l00' 7 Y/ N r v7nl
NOTE Quanta reads in mS/cm, move decimal 3 places right for pS/cm,
3 Dry Air Calibrations are conducted for 48 Hydrolabs only.
4 Dry Air Checks (confirrnetim of zero In dry air) are conducted for YSI 85 5 Quanta meters,
5 Condo. standards are used to calibrate Duarte 5 4a Hydrolab Meters and to check
YSI 85.
s Does not apply to YSI 85 (leave blank).
1 For YSI 85, 'Initial Meter Reading'should be within m 2.
.: Bias!
r 1lo0::::'....
:: 8.to 11:.'.
�100:.:90
to 110
N 1,000
.�..A00 to 1;100
oao
06
47,800 :::::..
42,840 to 52,360' .
Initial Meter I Calibrated Meter Initial Meter I Calibrated Meier Slope Meter Reading Beetling Reading Reading Efficiancye Reading
Y/
Within t 0.2 ? ) Y / N Y
Slope efficiency does not apply to Hydrolab or Quanta.
Keep original on file for 5 years
FMC-12n2110tle

i /:
i

�.�� 1'1 ..r• CAI � �j ,� � V � C 1 . J y���-,, fig
f a Y t
' f'CII''� � ;yi 1r ,•� � C: a �: a � @,
RIM
466 41� >
*.