NCG020854_COMPLETE FILE - HISTORICAL_20170131

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
�v �� Pao Jam/
DOC TYPE
PYHISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ I e 13
YYYYM M D D

e
aceAnalytical
wwrpxaleosoxn
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
June 21, 2016 / D a 135- �� �
N CT /� U (0
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: 2016 SW 6/16116
Pace Project No.: 92301709
Dear Glenn Amey:
, mA 3 .k "I
SIR
Enclosed are the analytical results for sample(s) received by the laboratory on June 16, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Collin Mummert, Charah Inc
4Ih
REPORT OF LABORATORY ANALYSIS
This report shall not loe reproduced, except in full.
without the written consent of Pace Analytical Services, Inc..
Page 1 of 17

ace Analytical*
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f
Project: 2016 SW 6/16/16
Pace Project No.: 92301709
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VrginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Page 2 of 17

aceAnalytical
xwwPsrr.'aasmm
SAMPLE ANALYTE COUNT
Project: 2016 SW 6116/16
Pace Project No.: 92301709
Pace Analytical Services. Inc,
2225 Riverside Or,
Asheville, NC 28804
18281254-7176
Lab ID
Sample ID
Method
Analysts
Analytts
Reported
Laboratory
92301709001
SED 4
SM 2540D
CRP
1
PASI-E
SM 2540F
CHM
I
PASI-E
EPA 180.1
DMN
1
PASI-A
92301709002
SED 3
SM 2540D
CRP
I
PASI-E
SM 2540F
CHM
i
PASI-E
EPA 180.1
DMN
1
PASI-A
92301709003
SED 1
SM 2540D
CRP
1
PASI-E
SM 2540F
CHM
1
PASI-E
EPA 180.1
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in roll.
without the written consent of Pam Analytical Services, Inc Page 3 of 17

aceAnalytical e
.pemretm.
SUMMARY OF DETECTION
Pace Analytical Services, Inc.
2225 Rwerslde Dr,
Asheville, NC 28804
[phone]
Project:
2016 SW 6116/16
Pace Project No.:
92301709
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92301709001
SED 4
SM 2540D
Total Suspended Solids
61.8
mglL
7.6
06/20116 15:58
EPA 180.1
Turbidity
58.2
NTU
1.0
06/17/16 23:14
92301709002
SED 1
SM 2540D
Total Suspended Solids
23.9
mglL
4.4
0620M6 15:58
EPA 180.1
Turbidity
19.0
NTU
1.0
08/17116 23:14
92301709003
SED 1
SM 2540D
Total Suspended Solids
8.8
mg/L
2.5
06/20/16 15:58
EPA 180.1
Turbidity
6.9
NTU
1.0
06/17/16 23:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services. Inc,.
Page 4 of 17

s
ace Analytical
xwwpacalabs oom
PROJECT NARRATIVE
Project: 2016 SW 6/16/16
Pace Project No: 92301709
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Dale: June 21, 2016
Pace Analytical services, Inc.
2225 Riverside Or
Asheville, NC 28804
[phone]
General Information:
3 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold limes with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All anatyles were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wnaen consent of Pace Analytical services, Inc.. Page 5 of 17

s
aceAnalXical
PROJECT NARRATIVE
Project: 2016 SW 6/16116
Pace Project No.: 92301709
Method: SM 2540F
Description: 2540F Total Settleable Solids
Client: Charah
Date: June 21, 2016
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NC 28804
(e29)254-717e
General Information:
3 samples were analyzed for SM 2540F Al samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold limes with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analyses were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within GC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
REPORT OF LABORATORY ANALYSIS
This report shall riot be ep oduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 17

aceAna1j cal
PROJECT NARRATIVE
Project: 2016 SW 6/16116
Pace Project No.: 92301709
Method:
EPA 180.1
Description:
180.1 Turbidity
Client:
Charah
Date:
June 21, 2016
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
(828)254-717e
General Information:
3 samples were analyzed for EPA 180.1. Al samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached al the end of this report.
Hold Time:
The samples were analyzed within the method required hold limes with any exceptions noted below.
Method Blank:
All anatyles were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within DC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not Ee reproduced. except in full,
without the written consent of Pace Analytical Services. Inc.. Page 7 of 17

Pace Analytical Somiees, Inc.
a Riverside Dr
aceAnaVical Ashevihevi .
Asheville. NC 28609
wawPorasscam [phone]
ANALYTICAL RESULTS
Project: 2016 SW 6/16/16
Pace Project No.: 92301709
Sample: SED 4
Lab ID: 92301709001 Collected: 06/16/16
09:00
Received: 06/16/16 14:35 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Dual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
61.8 mg/L
7.6
1
06/20/16 15:58
2540F Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
ND ni
0.10
1
06/17/1609:05
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
68.2 NTU
1.0
1
06/17/1623:14
REPORT OF LABORATORY ANALYSIS
This report shall not oa reproduced, except in lull,
Dale: 06/21/2016 10:53 AM without the wnden consent of Pace Analytical Services, Inc.. Page 8 of 17
0

i
Pace Analytical Services, Inc.
• 2225 Riversiee Dr.
aceAnalytical Asheville NC 2BB04
ewsrpa vleeacom [phone]
ANALYTICAL RESULTS
Project: 2016 SW 6116116
Pace Project No.: 92301709
Sample: SED 3
Parameters
Lab ID: 92301709002 Collected: 06116/1609:00
Results Units Report Limit OF
Received: 06/1611614:35 Matrix: Water
Prepared Analyzed CAS No. Dual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
23.9 mg/L
4.4 1
06/20/16 15:58
254OF Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
NO mUUhr
0.10 1
06/17/16 09:05
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
19.0 NTU
1.0 1
06/1711623:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21/2016 10:53 AM without the written consent of Pace Analytical Services, Inc, Page 9 of 17

aceAnalytical
e.wpxalessoom
ANALYTICAL RESULTS
Project: 2016 SW 6/16/16
Pace Project No.: 92301709
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: SED 1
Lab ID: 92301709003 Collected: 06/16/16 09:00
Received: 06/16/16 14:35 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
8.8 mg/L
2.5 1
06/20/16 15:58
2640F Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
ND mUUhr
0.10 1
06/17/16 09:05
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
6.9 NTU
1.0 1
06/17/1623:14
Date: 06/21/2016 10:53 AM
REPORT OF LABORATORY ANALYSIS
This report shell not he reproduced, except in lull,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 17

aceAnalytical.
wawpecNaascam
QUALITY CONTROL DATA
Project: 2016 SW 6/16/16
Pace Project No.: 92301709
QC Batch: EDEN/23188 Analysis Method: SM 2540D
OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 923017C9001, 92301709002, 92301709003
METHOD BLANK: 1759839 Matrix: Water
Associated Lab Samples: 92301709001. 92301709002. 92301709003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL NO 2.5 06120/16 15:56
Pace Analytical services, Inc.
2225 Riverside Dr
Asheville, NC 28804
(B28)254 7176
LABORATORY CONTROL SAMPLE:
1759840
Spike LCS LCS
%Rec
Parameter
Units
Conic. Result %Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 258 103
9C-110
SAMPLE DUPLICATE: 1759841
92301706001 Dup
Parameter
Units
Result Result RPD
Qualifiers
Total Suspended Solids
mg/L
26.7 27.5
3
Results presented on this page ere In Me units Indicated by Me "Unite' column except where an Imamate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not to, reproduced, except in full,
Date: 06121/2016 10:53 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 17

aceAnalAcale
rnawpecowscom
QUALITY CONTROL DATA
Project: 2016 SW 6116/16
Pace Project No.: 92301709
QC Batch: EDEN123166 Analysis Method: SM 254OF
QC Batch Method: SM 254OF Analysis Description: 254OF Total Satiable Solids
Associated Lab Samples: 92301709001, 92301709002, 92301709003
METHOD BLANK: 1758042 Matrix: Water
Associated Lab Samples: 92301709001, 92301709002, 92301709003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Settleable Solids mUUhr NO 0.10 06117/1609:05
SAMPLE DUPLICATE: 1758043
92301709001 Cup
Parameter Units Result Result RPD Qualifiers
Total Settleable Solids mUUhr ND ND
Pace Analytical Services, Inc.
2225 Riverside D,.
Asheville, NC 28804
[phone]
Results prevented on this page are In Me units Indicated by the "Units" column except shun an altemas unit Is presented to the right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21/2016 10:53 AM without the written consent of Pace Analytical Services, Inc..
Page 12 of 17

aceAnalytical
wwpeulebstam
QUALITY CONTROL DATA
Project: 2016 SW 6/16/16
Pace Project NO.: 92301709
OC Batch: WET/45610 Analysis Method: EPA 180.1
QC Batch Method: EPA 180.1 Analysis Description: 180.1 "1"urbidity
Associated Lab Samples: 92301709001, 92301709002, 92301709003
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 1758931
Matrix: Water
Associated Lab Samples: 92301709001, 92301709002, 92301709003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Turbidity
NTU
ND
1.0
06/17/1623:14
LABORATORY CONTROL SAMPLE:
1758932
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
%Rec Limits Qualifiers
Turbidity
NTU
10
10.0
100 90-110
SAMPLE DUPLICATE: 1758933
92301709001 Dup
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 58.2 58.7 1
Itti presented on this page are In Na unite indicated by the "Units' column except when an aeemale unit Is presented to the tight of the insult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 06121/201610:53 AM without the written consent of Pace Analytical services, Inc, Page 13 of 17

(�IaceAnalytical'
.peoNaGsmm
QUALIFIERS
Project. 2016 SW 6116/16
Pace Project No.: 92301709
DEFINITIONS
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville. NC 281304
[phone]
DF - Dilution Factor. if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
POL- Practical Ouantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2.Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
OUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-E Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21/2015 10:53 AM without the written consent of Pace Analytical Services. Inc.. Page 14 of 17

aceAnalytical
arwpawfadawm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 2016 SW 6/16/16
Pace Project No.: 92301709
Pace Analytical Services. Inc.
2225 Riverside Ur
Asheville, NC 28804
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92301709001
SED 4
SM 2540D
EDEN123188
92301709002
SED 3
SM 2540D
EDEN123188
92301709003
SED 1
SM 2540D
EDEN/23188
92301709001
SED 4
SM 254OF
EDEN1231643
92301709002
SED 3
SM 2540F
EDEN/23166
92301709003
SED i
SM 2540F
EDEN/23166
92301709001
SED 4
EPA 180.1
WET/45610
92301709002
SED 3
EPA 180.1
WET/45610
92301709003
SED1
EPA 180.1
WET/45610
Date: 06121/2016 10:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Analytical
Batch
Page 15 of 17

/, �:P,aceArulyfical
Document Name:
Document No.:
Document Revised: May 24, 2016
Issuing
Client IName: ! � project g wo# : 92301709
Courier: EJFed I 1"t' I UPS ❑LISPS Client II II� III I I II I I I I II �II
❑Commercial []pace ❑Dthec_
,�// 92301709
Custody Seal Present? []Yes No Seals Intact? []Yes �rvo
Daic/Initlab Pttian Examinln� Contanu:
Packing Material: ❑Bubble Wrap ❑Bubble Bags one []Other
Thermometer: T1505 Type of Ice: own ❑Nua one ❑:ampler on ice, tooling process has b un
Correction Factor: O.O'C Cooler Temp Corrected (IC); i` lologiral Tissues Fr oxen? ❑Yes QNo N/A
Temp should be abovefree to VC
USDA Regulated Sall N/A, water sample)
Did samples a ate In a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Imemat
[]Yes0 Including Hawail and Puerto Ricci? OYes LdKo
Lommersts/Oletrepasicy:. _
Chain of Custody Present?
n
ND
N/A
1.
Samples Arrivedwlthln Hold 7lme?
ONO
ONJA
Z.
Short Hold Time An - Is O2 hr.?
❑Yes
N/A.
3.
Rush Turn Around Time Requested?
OYes
o
MNJA
4.
Suffklam volume?
Yes
No
N/A
5.
Correct Containers Used?
.-OYn
❑No
❑N/A
6.
-Pace Containers Used?
Yes
ONO
ONIA
Containers Intact?
Yee
CINO
N A
7.
Samples Field Filtered?
❑Yes
❑No
N/A
B.
Note B sediment lsvlsible In the dissolved container
Sample labels Match C-OCP
,Ox,
ONO
❑N/A
9.
V
�
-Induces Date/Time/ID/Analysis Matrix:
All containers needing add/base preservation have been
10.
ehadeed7
❑Yes
ONO
/A
All contalners needing preservation we found to be In
compliance with EPArecommendatlon?
waarrxa
(HNOs, H,SO., HCI<2; NaOH >9 Sulfide, NaOH>12 Cyenlde) ❑Yes
ONO
N/A
N
Eaceptlonc VOA, Collform, TOC, Oil and Grease,
e,wwu
DRO/8015 (water) DOC,LLHg
❑Yes
❑No
Q(N/A
Samples checked for deehiodra0on7
Yet
ONO
1A
11.
Mead ace In VOA Vials >S-6mm 1
Yo
13NO
A
12.
Trip Blank Present?
❑Yes
ONO
QwlA
13.
Trip Blank Custody Saab Present?
❑Yo
ONO
❑Ff/A
Pace Trip Blank lot a (if purchased):
/
[LENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Ample
Discrepancy:
Date/lime:
Field Data Requlred? ❑Yes ONO
Project Manager SCURF Review: /// Date:
Project Manager SRF Review: Date:
Note: Whenever there Is a dbmpanry affecting North Carolina complunce samples, a copy of this fort, Me be sent to the North
Out of hold, Incorrect preservative, out of tamp, incorrect mmalnars)
Mee Ile.
Page 16 of 17

aceAnalytica!'
4wia.p�celeDa.csm
i 6701 Conference Ddve, Raleigh, NC 27607
ph; (919) 9344984, to; (919) 6306997
NCWW Cem167, NCOW CwW7731
Report Results To
Chain of Custody W.O.#
Company: /',(na.r:.L.. Sne
Address: W7I �(Lntr.i, IE'&,y vty2d
/Z.d eat is J[ 17531
Attn: 4t..v.'.r �Vr�GAt'�5./41-
Phone: 3NX -Y iR- 62 s )
Fax:e" M, j+,04 a rLiZe- Mrn1.. rYYI
Sampled by (signature):
Bill To:
Project Reference: ZU7( 5/u4MLJ44 r
�icw a rein a
Project Number:
Purchase Order k:
❑ Standard Report Delivery
❑ Rush Report Delivery (wlsurcharge)
**Flush Dto)edi are sublKI m paw spa W by
the laboraxrry
Requested Due Cale:
;elDtgtildr by(agrtalura)
R IIJIV
D a
'fi
3
9 hod by (signature)
R b1' (eigroture)
Dodd
Time
ielhquishad by(el9natura)
Reoeived by (signature)
Date
Tana
Receipt Condl6one(La I
❑ 41M ❑Temp
Res. Chlodrw:
❑Abwm ❑Present ❑nda
Add preserv. <27
❑ Vas ❑ No ❑ Na
Bess preaerv. s127
❑ yes ❑ No ❑ n/a
Page 17 of 17

e
aceAnalytical
swwpsobesavn
June 30, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Stormwater 6/28
Pace Project No.: 92303136
Dear Glenn Amey:
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 28, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Collin Mummert, Charah Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 16

(�IaceAnalyfical'
ewwpxNabs.
Project: Slormwater 6128
Pace Project No: 92303136
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FlondalNELAP Cerlificalion If: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
vrginiaA/ELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia(VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
2225 Riverside Di
Asheville, NC 2BB04
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 2 of 16

aceAnalytical0
• nipeodittmm
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville. NC 28804
(828)254J116
Project:
Pace Project No.:
Stormwaler 6/28
92303136
Analyses
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92303136001
BASIN 2
SM 25400
CHM
1
PASI-E
SM 2540F
CHM
1
PASI-E
EPA 180.1
MLS
1
PASI-A
92303136002
BASIN 4
SM 2540D
CHM
1
PASI-E
SM 2540F
CHM
1
PASI-E
EPA 180.1
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This mpo t shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc.. Page 3 of 16

aceAnalyticala
sww:ps[MSDamm
SUMMARY OF DETECTION
Pace Analytical Services, Inc.
2225 Riverside or
Asheville, NC 28804
[phone]
Project:
Stormwater 6l28
Pace Project No.:
92303136
Lab Sample ID
Client Sample ID
Method
Parameters
Result Units
Report Limit
Analyzed Qualifiers
92303136001
BASIN 2
SM 2540D
Total Suspended Solids
15.3 mglL
33
06129/l6 14:08
EPA 180.1
Turbidity
13.4 NTU
1.0
06/30/16 10:42
92303136002
BASIN 4
EPA 180.1
Turbidity
5.4 NTU
1.0
06/'30116 10:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in lull.
without the written consent of Pace Analytical Services. Inc,.
Page 4 of 16

aceAnalytical'
m ,sicelaasmm
PROJECT NARRATIVE
Project: Slormwaler 6/28
Pace Project No.: 92303136
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Date: June 30. 2016
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
(828)254-717e
General Information:
2 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below,
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below,
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPOs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services. Inc_ Page 5 of 16

aceAnalytical
•wwpxalab&ixvn
PROJECT NARRATIVE
Project: Stormwater 6l28
Pace Project No,: 92303136
Method:
SM 2540F
Description:
2540F Total Settleable Solids
Client:
Charah
Data:
June 30, 2016
Pace Analytical services. Inc.
2225 Riverside Or
Asheville, NC 2BB04
(e2e)254-e176
General Information:
2 samples were analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc_ Page 6 of 16

aceAnalytical
awwpsalabcmn
PROJECT NARRATIVE
Project: Stormwater 6/28
Pace Project 1 92303136
Method:
EPA 180.1
Description:
180,1 Turbidity
Client:
Charah
Date:
June 30, 2016
Pace Analytical Services. Inc.
2225 Riverside Or.
Asheville, i 288D4
[phone]
General Information:
2 samples were analyzed for EPA 180.1. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody andlor the sample condition upon receipt fomt (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analyles were below the report limit in the method blank, where applicable. with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 7 of 16

IceAnalyficale
wwapaosl ascwn
ANALYTICAL RESULTS
Pace Analytical Samices, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
Project: Stormwaler 6128
Pace Project No.: 92303136
Sample: BASIN 2
Lab ID: 92303136001 Collected: 06/28/16 12:00
Received: 06/28/16 14:15 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 25401)
Total Suspended Solids
15.3 mg/L
3,3
1
06/29/16 14:08
2540E Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
ND mL/L/hr
0.10
1
06/29/16 12:35
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
13.4 NTU
1.0
1
0613011610:42
Date: 06/30/2016 11:01 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, eacepl in lull,
without the written consent of Pace Analytical Servicea, Inc..
Page 8 of 16

Pace Analytical Services, Inc.
• 2225 Riverside Dr.
ace Analytical Asheville. NC 26804
ewwpaoxaas out" [phone]
ANALYTICAL RESULTS
Project: Stormwater 6/28
Pace Project No.: 92303136
Sample: BASIN 4
Lab ID: 92303136002 Collected:
06/28116 12:20
Received: 06/28/16 14:15 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
ND mg/L
2.5
1
06/291% 14:08
2540F Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
ND mlJUhr
0.10
1
06/29/16 12:35
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
5.4 NTU
1.0
1
06/30/1610:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull.
Date: 06/30/201611:01 AM without the written consent at Pace Analytical Services, Inc.. Page 9 of 16

(�IaceAnalytlll
0- pecrebxmn
QUALITY CONTROL DATA
Project: Stormwater 6/28
Pace Project No.: 92303136
QC Batch: EDEN123295 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description. 2540D Total Suspended Solids
Associated Lab Samples: 92303136001, 92303136002
METHOD BLANK: 1768700 Matrix: Water
Associated Lab Samples: 92303136001, 92303136002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL NO 2.5 06/29116 13:59
LABORATORY CONTROL SAMPLE: 1768701
Pace Analytical Services, Inc.
2225 Riverside D,.
Asheville, NC 28504
(82e)254-7176
Spike LCS LCS
%Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 258 103
90-110
SAMPLE DUPLICATE: 1769669
92302994002 Cup
Parameter
Units
Result Result RPD
Qualifiers
Total Suspended Solids
mg/L
NO NO
SAMPLE DUPLICATE: 1769670
92303054001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 53.3 52.6 1
Results presented on this page +rt In the ..its Indicated by the "Units' column except where an alternate unit is presented to the ri or the rtsull.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull.
Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 16

IceAnayical"
wwwpecelab ldern
QUALITY CONTROL DATA
Project: Stormwater 6/28
Pace Project No.: 92303136
OC Batch: EDEN23292 Analysis Method: SM 2540F
QC Batch Method: SM 254OF Analysis Description: 2540F Total Sellable Solids
Associated Lab Samples: 92303136001, 92303136002
METHOD BLANK: 1768594 Matrix: Water
Associated Lab Samples: 92303136001, 92303136002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Settleable Solids mL/L/hr NO 0.10 06/29116 12:35
SAMPLE DUPLICATE: 1768595
Parameter
Total Settleable Solids
92303138001 Cup
Units Result Result
mL/L/hr ND NO
RPD Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Results presented on thus page am in Me units Indicated by the "Units" column except wlrm an al emate unit Is presented to toe right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2016 11:01 AM without the written consent of Pace Analytical Services, Inc..
Page 11 of 16

aceAnalyicala
wawpaalaGsavn
QUALITY CONTROL DATA
Project: Stormwater 6/28
Pace Project No.: 92303136
QC Batch: WET145945 Analysis Method: EPA 180.1
QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92303136001. 92303136002
METHOD BLANK. 1769908 Matrix: Water
Associated Lab Samples: 92303136001. 92303136002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 1.0 06130/1610:42
Pace Analytical services, Inc.
2225 Riverside 0,
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
1769909
Spike
LCS LCS
% Rae
Parameter
Units
Cone.
Result %Rec
Limits Qualifiers
Turbidity
NTU
10
10 100
90-110
SAMPLE DUPLICATE: 1769910
92303136001
Dup
Parameter
Units
Result
Result RPD
Qualifiers
Turbidity
NTU
13.4
13.2
2
Results presentee on this papa are In the units InNoted by the "units" column except e4rtre an alternate unit Is presented to the right Of the result.
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 0613MO16 11:01 AM wilhout the wriden consent of Pace Analytical Services, Inc.. Page 12 of 16

aceAnalytical
awwpaceiabs.
QUALIFIERS
Project: Stormwater 6/28
Pace Project No.: 92303136
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NC 2BB04
(B28)254-7176
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate `y recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
CUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyi ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-E Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2016 11:01 AM without Me written consent of Pace Analytical Services. Inc- Page 13 of 16

aceAnalytical
.lasewaeacom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Projecl: Stormwaler6/28
Pace Project No.: 92303136
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 2BB04
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92303136001
BASIN 2
SM 2540D
EDEN/23295
92303136002
BASIN 4
SM 25400
EDEN/23295
92303136001
BASIN 2
SM 2540F
EDEN/23292
92303136002
BASIN 4
SM 2540F
EDEN/23292
92303136001
BASIN 2
EPA 180.1
WET/45945
92303136002
BASIN 4
EPA 180.1
WET/45945
Date: 0613012016 11:01 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reprcouced, except in full,
without the written consent of Pace Analytical Services, Inc.
Analytical
Batch
Page 14 of 16

��eAna/yticaf�
Document Name:
Document No.:
Document Revised: May 24, 2016
Page 1 of 2
Issuing Authority:
Osnn'1 n(l (nr Inr.rnal , lrn tt„„
Client Name: _ WO# : 92303136
Courier:
4eVY _ Protect N_
Fed Ex �,;J❑�USPS^ Cllant II�III III II IIIIII�I �II
❑Commercial []Pace ❑Other.^ IIIIIII111
36
Custody Seal Present? []Yes VNO Seals Intact? ❑Yes [7No
Data/initials Person GamlMn/ [pnbnK Z� IV
Packing Material: []Bubble Wrap []Bubble Bags ONin❑other:_
Thermanoter: T1505 Type if jPwet ❑Blue ❑None ❑Samplason ice, cooling process�h,a{sbegun
Correction Factor: 0.O'C Cooler Temp Corrected ('CI: �," Biological Tissue Frozen? []Yes []NO aN/A
Temp should be above fr ezing to VC
USDA Regulated Soli ( N/A, water sample)
Old samples Y1dginate In r� quarantine zone within the United States: CA, NY, or SC (check maps)? Old samplesodglnatehoma foreignsource(inte allonalty,
r rivo. ih. In,cludine Newell and Puerto RICO r IYes WINo
-CpmmenU Dlwe nc : -
Chain of Custody Present?
No
ON/A
1.
Samples Arrived within Hold Time?
dyes
dyes
No
ONIA
2.
Short Hold Time Analysis J47Z hr.)?
Yes
ON.
N/A
3..
I V Y YIJ.
Rush Tom Around Time Requested?
QYes
ONO
N/A
4.
,
Sufficient Volume?
9LYU
ONO
ONJA
S.
Correct Containers Used?
[7fYes
❑No
❑N/A
6.
-Pace Containers Used?
Yes
EJNo
,N/A
Containers intact?
Yet
. No
N/A
7.
Samples Field Filtered?
ONO
/A
8.
Noted sediment is visible In the dissolved container
Sample Labels Match CDC?
JYes
( Yes
ONO
❑N/A
9.
-Includes Date/nme/10/Anal is Matrix:
All containers needing add/base preservation have been
10.
wue,e
checked?
Yes
ONO
❑NIA
All containers needing preservation are found to be In
Mania
compliance with EPA recommendation?
1
(HNOs, HtSO,, HCk1; NaOrl 95ulfide, NaOH>32 Cyanldej
i[1Yes
0
ONO
❑N/A
Awa"U
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRo 8015 (waterl DOCLLHg
Yet
ONO
ONIA.
«,wlnnee.rwr
Samples checked for dechlorinatlon7
PJY.s
ONO
ONtA.
11.
Heads ace In VOA Vials >54mm ?
nYdS
ONO
N/A
32.
Trip Blank Present?
DYes
ONO
N/A
13.
Trip Blank CUstodi Seals Present?
❑Yes
ONO
eN/A
Pace Trip Blank Lot If(If urchawd):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Date/Time:
Dale:
Real Data Required? []Yes []No
Pro)ect Manager SRF Reviver: Dote:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, acopy of this form wia be sent to the North Car6rna YHNR Certification Office (i.e.
Out of hold, Inwrrect preservative, out of temp, inrorrzct contalnars)
Page 15 of 16

aceAnalytical '
` wnr.pecelahe.rom
j 6701 Canfwence Drive, Raleigh, NC Z7607
ph: (919)1114-4964, tax: (919) 6348497
NCWW Car1W, NCDW CertV 731
Report Results To:
Company:
Address:/Vi /L VA"fcliY�p
Atin:�arir.r �iu-Cci¢
Phone: �i-43ff— fl s/
Fax: C�✓fCCkr�e 1 . tort
Sampled by (signature):
Chain ®f Custody W.O.M
BIII To:
Project Reference:
:5He-)4w raz> -- An t.rS 1 5
Project Number:
Purchase Order M
❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
"Ru6n pro" me 6ugect to prbr approval by
e4labor"
Requested Due Data:
(o TSS , $c.rlic�blG $n1y15, Ti�i.lr ty
g,�,� z G •a Sw � is .so
r.� /6 L� TS, SGI-Hco-blt $nriJS� Trbi.li%y
Rel4pulal by(pignsh-)
by
D a
Retnittaflill by (signature)
Received by (signature)
Da
Time
Rthqulathed by(slgnawre)
Reoaivad by(eignalunt)
Date
Time
Hecalpt 1„pnc(�Mq fLff LiT Unry)
❑ at2°C ❑Te): J 'C
Fin. Chlorine:
❑Absent ❑Preeem ❑n/a
Acid praserv. c27
❑ Yes ❑ No ❑ n/s
Base preWN. W7
❑ Yes ❑ No ❑ rve
Page 16 of 16

lceAnalytical
~,xicaie0.v rom
May 25, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Stormwater Sed 7 5119
Pace Project No.: 92298375
Dear Glenn Amey:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Collin Mummert, Charah Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 1 of 15

(�Iaceftljftal'
wwwpacdet>mm
CERTIFICATIONS
Project: Stornrwater Sed 7 5/19
Pace Project No.: 92298375
Eden Certification We
205 East Meadow Road Suite A. Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738 UrginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 15

W Analytical
awwpecelsearom
SAMPLE ANALYTE COUNT
Project: Slorm ater Sed 7 5119
Pace Project No.: 92298375
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 20804
[phone]
Analytts
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92298376001 SED 7 SW SM 2130B
DWJ
1
PASI-E
SM 2540D
CRP
1
PASI-E
SM 2540F
CHM
1
PASI-E
REPORT OF LABORATORY ANALYSIS
This report shall not lee reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 3 of 15

aceAnalytical e
.Pscel4btms
SUMMARY OF DETECTION
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stormwaler Sed 7 5119
Pace Project No.: 92298375
Lab Sample ID Client Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
92298375001 SED 7 SW
SM 2130B Turbidity 20.7 NTU 0.50 05/20/16 14:15
SM 2540D Total Suspended Solids 22.4 mg/L 4.3 05/23/16 16:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pecs Analytical Services, Inc.. Page 4 of 15

aceAnalytii l e
rmw Mosel s.wm
PROJECT NARRATIVE
Project: Slormwater Sed 7 5/19
Pace Project No.: 92298375
Method:
SM 2130B
Description:
2130B Turbidity EDN
Client:
Charah
Date:
May 25, 2016
Pace Analytical services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
General Information:
1 sample was analyzed for SM 2130B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below
Surrogates:
All surrogates were within OC limits with any exceptions noted below.
Method Blank:
All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 5 of 15

laceAnalytical"
wvwpnMabxovn
PROJECT NARRATIVE
Project: Stormwater Sed 7 5r19
Pace Project No.: 92298375
Method:
SM 2540D
Description:
2540D Total Suspended Solids
Client:
Charah
Dale:
May 25, 2016
Pace Analytical services. Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody andror the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below,
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within GC limits with any exceptions noted below.
Surrogates:
All surrogates were within DC limits with any exceptions noted below.
Method Blank:
All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below,
DC Batch: EDEN122904
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID'. 1740343)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc. Page 6 of 15

aceAnalytical e
w.m2pmebbs.oxn
PROJECT NARRATIVE
Project: Stormwater Sed 7 5f19
Pace Project No.: 92298375
Method:
SM 2540F
Description:
2540F Total Settleable Solids
Client:
Charah
Date:
May 25, 2016
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28004
(e28)254-7176
General Information:
1 sample was analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody andfor the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below,
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
This data package has been reviewed far quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 15

aceAnalXical o
.pnoWnui on,
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Slormwater Sed 7 5/19
Pace Project No.: 92298375
Sample: SED 7 SW
Lab ID: 92298375001 Collected:
05119116
13:00
Received: 05/19116 15:55 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared Analyzed CAS No. Qual
21308 Turbidity EDN
Analytical Method: SM 21306
Turbidity
20.7 NTU
0,50
1
05/20/1614:15
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
22.4 mg/L
4.3
1
05/23116 16:09
2640F Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
NO mUL/hr
0.10
1
05/20/16 13:00
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date. 05125/2016 08:39 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 15

aceAnalytical
wwpacsiabaw+n
QUALITY CONTROL DATA
Project: Stornmvater Sed 7 5/19
Pace Project No.: 92298375
QC Batch: EDEN/22896 Analysis Method: SM 2130B
OC Batch Method: SM 2130B Analysis Description: 2130B Turbidity EDN
Associated Lab Samples: 92298375001
METHOD BLANK: 1739099
Matrix: Water
Associated Lab Samples: 92298375001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Turbidity
NTU
ND
0.50
05/20/1614:15
SAMPLE DUPLICATE: 1739100
92298350001
Cup
Parameter
Units
Result
Result
RPD Qualifiers
Turbidity
NTU
1.5
1.5
1
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
Results presented on Mls page am In the units Indicated by the "Unita' column except wimre an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/251201608:39 AM without Me written consent of Pace Analytical Services, Inc -
Page 9 of 15

aceAnalytical a
ewwpseslabi
QUALITY CONTROL DATA
Pace Analytical Semicos, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stormwaler Sed 7 5119
Pace Project No.: 92298375
OC Batch: EDENI22904
Analysis Method:
SM 2540D
OC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92298375001
METHOD BLANK: 1740340
Matrix: Water
Associated Lab Samples: 92298375001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5 05/23/16 16:07
LABORATORY CONTROL SAMPLE: 1740341
Spike LCS
LCS %Red
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Total Suspended Solids
mglL
250 266
106 90-110
SAMPLE DUPLICATE: 1740342
92298380003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
283
271 4
SAMPLE DUPLICATE: 1740343
92298421001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
29.7
27.2 9 06
Results presented on this page are in the units Indicates by the "Units' column except where an enemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 05/25/2016 08:39 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15

JceAnalytiiicaf'
wawpac"Woom
Project: Slormwaler Sed 7 5/19
Pace Project No.: 92298375
QC Batch: EDEN/22891
QC Batch Method: SM 254OF
Associated Lab Samples: 92298375001
METHOD BLANK: 1738918
Associated Lab Samples: 92298375001
Parameter Units
Total Settleable Solids mL/L/hr
SAMPLE DUPLICATE: 1738919
Parameter Units
Total Settleable Solids muuhr
QUALITY CONTROL DATA
Analysis Method: SM 2540F
Analysis Description: 2540F Total Settable Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 05/201l613:00
92298375001 Dup
Result Result RPD Qualifiers
NO ND
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
Results presented on thes page are In Me units Indicated by the "Units" column except where an alternate unit Is presented to the hired of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not the reproduced, except in full,
Dale: 05/25/2016 08:39 AM without Me written =.sent of Pace Analytical Services, Inc.
Page 11 of 15

aceAnalytical
awwpsciibb.cam
QUALIFIERS
Project: Stormwater Sed 7 5119
Pace Project No.: 92298375
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit,
MDL- Adjusted Method Detection Limit.
POL - Practical Ouantitation Limit,
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
CUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroelhylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited, Contact your Pace PM for the current list of accredited analyles.
TNI - The NELAC Institute.
LABORATORIES
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale', 05125/2016 08:39 AM without the written consent of Pace Analytical Services, Inc,. Page 12 of 15

aceAnalytical
• Peos'ebamn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater Sed 7 5/19
Pace Project No.: 92298375
Paco Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 20504
(828)254J176
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92298375001
SED 7 SW
SM 21308
EDEN/22896
92298375001
SED 7 SW
SM 2540D
EDEN122904
92298375001
SED 7 SW
SM 2540F
EDEN/22891
Date: 05125/2016 08:39 AM
REPORT OF LABORATORY ANALYSIS
This report shall not ce reproduced, except In full,
without the wriden Consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 13 of 15

ouuaumnt Name:
Docurnerit No.:
a}sjplp C nJit(unjlfj o'n�client Narne:
&
7
71 Commercial3'. E]e
Vvcyj11C11rPine 1 of 2V'vu•V•V
Issuing Authority:
Pace Raleigh Qaiillty ❑fflae
WO#:92298375
1111111111111111111111
92298315
CustodySeal Present? ❑Yes ONO Seals Intact? Yes �No
,❑,.__,,!! Date/Initials Person Eeeminln{CommIt ��� (�
Packing Material:1 []Bubble Wrap ❑Bubble Bags CONone ❑Other:_
Thermometer: LU IRSN: 122065397 ❑IR SN: 122065371 po of ice: gJWel ❑Blue ❑11one []Samples on Ice, cooling process It sbegun
Correction Factor: 0.O'C Cooler Temp Corrected('C): —I). Blologlcal Tissue Froten? []Yes ❑110 E]N/A
Temp should be above f ee2ing to 6'C
USDA Regulated Soll ( N/A, watei sample)
Didsarrpiwriginate in aquarantme zone within the United States: CA, NY, or SC(check maps)? DI -]yet
ham a/Orelgnsource (Int�e`Jatlpmlly,
tniludlno Haeralland Puerto Ricol?❑YCi (/]Na
tJres LJJ.Q
COMMENTS:'
Chain of Custody Present?
Yes
❑llo
NA
1.
_
Chain of Custody Filled Out?
( Yea
No
N/A
2.
Chain of Custody Relinquished?
Yes
EINd
N/a.
3.
Sampler Name end/or Sl nature on COC?
QNO
N/A
4.
Samples Arrivedsvlthln Had Time?
Yes
ONO
. N/A.
5.
90V T W0
Short Hold Time Analysis <72 hf?.
of
❑No
N A
6.,
Rush Turn Around Time Requested?
'/es
No
Sufficient Volume?
VJYCS
Q, No
NIA
8.
Correct Containers Used?
r s
❑NO
❑NIA
9.
-Pace Containers Used?
L—dY/
Nu
N A
..
Containers intact?
Idyi,
ONO
N A
10.
Filtered Volume Received for Dissolved Tests?
Yes
❑No
/A
11.
Nola If sediment Is vislblo in the dissolved container
Sample Labels Match COC?
Arcs
oNo
❑N/A
22.
-Includes Date imo/ID/Anil sh Malrlx:
All containers needing acid/base preservatlon have been
1���fff
13.
checked?
(Yes
❑No
❑rv/A
All containers needing preservation are found to be In
compliance with EPA recommendation?
(HNOs, HAD, HCI<2; NaOH >9Sulfide, NaOH>12 Cyanide)
o
[]No❑N/A
Exceptions: VOA, Colffarm,TOC, Oil and Grease,
DRO/8015 hvater) DOC,LLIi
es
[]No
CINLA.
Samples checked lordechlorinallon
Yes
No
N/A
14.
. Headspace in VOA Vials(>S-6mm1i
13yes
ONO
M
15.
-
TrlpBlankPresenl?
❑Yes
❑No
/A
16.
Trip Blank Custody Seals Present?
[]Yes[]NON/A
Pace Trip Blank lot N(if urchascd):
CLIENT NOTIFICATION/RESOLUTION Field Data Required? Dyes ONO
Person Contacted: Date/Time:
Comments/Reno IUtlon:
Pr,i Manager SCURF Review: Dale: .2n
Project Manager SRF Review: �%— Date:
Note: Whenever there is a discrepancy arfecting North Carolina, compliance samples,a copy of this Torm Will be sent to the North CarqflnA DEHNR Cenificatlun Onice(I.e.
Out of hoio, Intoned preservANe, out of temp, incorrect comaln en1
Page 14 or 15

aceAnalytical'
xwre.peeele6a.eom
' 6701 Conference Drive, Raleigh, NC 276D7
' ph: (919), e34-0954, tax: [phone]
NCWW CarDW, NCOW CerL437731
Chain of Custody
Report Results To:
Company:.L_Ha�h. r->♦r .
Address: it 7//-(eewle Fiuft�ra>I /2.1.
Phone: 9z-Y,5X- Sall
Sampled by (signature):
BIII To:
W.O. #
Project Reference:
Project Number:
Purchase Order N:
❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
"Ruch pmjerm are wbjecl to prior approval by
the laboratory
Requested Due Dale:
N.�1'fi �oh5stx �} c A> ♦ }it is F a � fr{ } Z t :y- 'Siy, ♦4 T.r a r:TC 1. 7 ^ .
2hs t r�',:>+.a fi._e?.x<:7,.,'3,i,�Lvii�`,�:k�.ij�.e:�7Si'("."GMR,r4..'>;"�w{..n. ,vds �.,:4t _ ..,s...,..t�s..� tiiev' e ;!;• .. iF'�e �... J•.ts'4,�`�
J
3
L• Zc:
■rwry,::83
0
"aysj
MINIM
Rdinquishod by (signature)
7
ved by s n
u i
16"-
Time
mhed by (signature)
R ad by (signature)
e
Time
RNinquished try (signature)
Recelved by (signature)
Date
Time
Recelpt Conditions( Orty)
❑ a:rc ❑ renili . J >C
Res. Chlorine.
❑Absem ❑Present Own
Acid preserv. <27
❑ Yes ❑ No ❑ Na
Rase preserv. >127
❑ Yes ❑ No ❑ Na
Page 15 of 15

aceAnalytical
.peulebs mm
May 11, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Basid 6 SW 5/5/16
Pace Project No.: 92296568
RECEIVE®
JAN S t Z017
CENTRAL FILES
DWR SECTION
Pace Analytical services, Inc.
2225 Riverside Dr
Asheville, NC 20804
[phone]
Dear Glenn Amey:
Enclosed are the analytical results for sample(s) received by the laboratory on May 05, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
4--
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc'. Collin Mummert, Charah Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 15

IaceAnalytical(�'
war..posiaEsmn
Project: Basid 6 SW 5/5/16
Pace Project No.: 92295568
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 633
VrginiaA/ELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This repel shall not Ge reproduced, except in full,
without the wnnon consent of Pace Analytical Services. Inca
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 15

aceAnalj&cal
.pavela•cwm
SAMPLE ANALYTE COUNT
Project: Basid 6 SW 515116
Pace Project No: 92296568
Pace Analytical Services, Inc.
2225 Riverside D,
Asheville, NC 28804
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92296568001 Sod 6 SM 21308 KCE 1 PASI-E
SM 2540D DWJ 1 PASI-E
SM 254OF KCE 1 PASI-E
REPORT OF LABORATORY ANALYSIS
This report shall not t a reproduced, except in lull,
without the written consent of Paco Analytical Services, Inc_ Page 3 of 15

aceAnalytical
ewxpecelebxmm
SUMMARY OF DETECTION
Pace Analytical Sorvlces, Inc.
2225 Riverside Or
Asheville, NC 25804
(82a)254-7176
Project:
Pace Project No.:
Basid 6 SW 5/5116
92296568
Lao Sample ID
Client Sample ID
Method
Parameters
Result Units Report Limit
Analyzed Qualifiers
92296568001
Sed 6
SM 2130B
Turbidity
34.5 NTU 0.50
05/06/16 11:00
SM 2540D
Total Suspended Solids
14.1 mg/L 2.5
05/06/16 12:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 15

aceAnalytical'
wxwpecelabs win
PROJECT NARRATIVE
Project: Basid 6 SW 515/16
Pace Project No: 92296568
Method:
SM 2130B
Description:
2130E Turbidity EON
Client:
Charah
Date:
May 11. 2016
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NO 28804
[phone]
General Information:
1 sample was analyzed for SM 2130B, All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report,
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc Page 5 of 15

aceAnaljftal
esrw paafebsmm
PROJECT NARRATIVE
Project: Basid 6 SW 5/5/16
Pace Project No.: 92296568
Method:
SM 2540D
Description:
2540D Total Suspended Solids
Client:
Charah
Date:
May 11. 2016
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NO 28804
[phone]
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold limes with any exceptions noted below.
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below,
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analyzes were below the report limit in the method blank, where applicable, with any exceptions rioted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: EDEN/22744
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1727831)
• Total Suspended Solids
• DUP (Lab ID: 1727832)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 15

aceAnalytical
u.w.pechalis W.
PROJECT NARRATIVE
Project: Basid 6 SW 5/5116
Pace Project No.: 92296568
Method:
SM 2540F
Description:
2540F Total Settleable Solids
Client:
Charah
Date:
May 11, 2016
Pace Analytical Services, Inc.
222$ Riverside Or
Asheville, NO 28804
[phone]
General Information:
1 sample was analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were whin method requirements with any exceptions noted below
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All anatytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments
This data package has been reviewed for quality and completeness and is approved for release,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wniten consent of Pace Analytical Services, Inc.. Page 7 of 15

Pace Analytical Services, Inc.
• 2225 Riverside Dr
aceAnalXieal Asheville NC 28804
swwprwbbs. [phone]
ANALYTICAL RESULTS
Project: Basid 6 SW 515116
Pace Project No.: 92296568
Sample: Sod 6
Parameters
Lab ID: 92296568001 Collected: 05105/16 12:00
Results Units Report Limit DF
Received: 05/05/16 16:15 Matrix: Water
Prepared Analyzed CAS No. Dual
2130B Turbidity EDN
Analytical Method SM 2130B
Turbidity,
34.5 NTU
050
1
05/O6/1611:00
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
14.1 mg/L
2.5
1
05/06/16 12:44
2540F Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
ND mUUhr
0.10
1
05106/16 11:30
REPORT OF LABORATORY ANALYSIS
This report shall not W reproduced, except in full,
Date: 05/11/2016 10:18 AM without the written consent a1 Pace Analytical Services, Inc. Page 8 of 15

aceAnalytical
QUALITY CONTROL DATA
Project: Basid 6 SW 515/16
Pace Project No.; 92296568
OC Batch: EDEN122739 Analysis Method: SM 21308
OC Batch Method: SM 2130B Analysis Description: 2130E Turbidity EDN
Associated Lab Samples: 92296568001
METHOD BLANK: 1727811
Associated Lab Samples: 92296568001
Parameter
Turbidity
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
NTU NO 050 05/0611611:00
SAMPLE DUPLICATE: 1727812
92296260001 Dup
Parameter Units Result Result
Turbidity NTU 4.5 4.4
RPD Qualifiers
0
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Results presented on Mile page en In Me units Indicated by the "Units' column except where en alternate unit le prdsenti d to the right pl the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/11/2016 10:18 AM without the written consent of Pace Analytical Services, Inc .
Page 9 of 15

(�IaceAnalyfical*
swxpecgw&cxm
Project: Basid 6 SW 5/5/16
Pace Project No: 92296568
QC Batch: EDEN/22744
OC Batch Method: SM 2540D
Associated Lab Samples: 92296568001
METHOD BLANK: 1727829
Associated Lab Samples: 92296568001
Parameter Units
Total Suspended Solids mg/L
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2,5 05/06/1612:38
Pace Analytical services, Inc.
2225 Riverside Dr
Asheville. NC 2B8D4
[phone]
LABORATORY CONTROL SAMPLE: 1727830
Spike LCS LCS %Rec
Parameter Units Conic Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 228 91 90-110
SAMPLE DUPLICATE: 1727831
92296282001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 99.0 114 14 D6
SAMPLE DUPLICATE: 1727832
92296535001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 56.5 47.5 17 D6
Results presented on this page an in the units Indicated by the "Units" column except Mien, an ahemate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 05111/201610: 18 AM without the written consent of Pace Analytical Services.Inc. Page 10 of 15

aceAnalytical
tnxpamfahsmm
QUALITY CONTROL DATA
Project: Basid 6 SW 5/5)16
Pace Project No.: 92296568
QC Batch: EDEN/22738 Analysis Method: SM 2540F
OC Batch Method: SM 254OF Analysis Description: 254OF Total Settable Solids
Associated Lab Samples: 92296568001
METHOD BLANK: 1727809 Matrix: Water
Associated Lab Samples: 92296568001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Settleable Solids mUUhr NO 0.10 05/06/16 11:30
SAMPLE DUPLICATE: 1727810
92296568001 Cup
Parameter Units Result Result RPO Qualifiers
Total Settleable Solids mUUhr NO NO
Pace Analytical Services, Inc.
2225 Riverside 0,
Asheville, NC 28804
[phone]
Results presented on this page am In the unite Indicated by Me "Units' column except where an altemate unit is presented to the Might or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 05/11/2016 10:18 AM without the written consent of Pace Analytical Services, Inc..
Page 11 of 16

al"Analyticals
.pacelabs can
QUALIFIERS
Project: Basid 6 SW 5/5116
Pace Project No.: 92296568
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
(82B)254-7176
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantilalion Limit.
RL- Reporting Limit,
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene. and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyle is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyles.
TNI - i he NELAC Institute.
LABORATORIES
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05111/2016 10:18 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 15

aceAnalytical
swwpecelabt.
Project: Basid 6 SW 5/5/16
Pace Project No.: 92296568
Lab ID
Sample ID
92296568001
Sod 6
92296568001
Sod 6
92296568001
Sod 6
Date: 05/11/2016 10:18 AM
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method
SM 213013
SM 2540D
SM 2540F
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NC 28804
(82B)254.7176
QC Batch Analytical Method
EDEN/22739
EDEN/22744
EDEN122738
REPORT OF LABORATORY ANALYSIS
This report shall not Its reproduced, except in full,
wilhcut the written consent of Pace Analytical Services, Inc.
Analytical
Batch
Page 13 of 15

uocument Name:
Document Revised: 26FE82016
Ida j it III •'" CllentName:
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Courier. Fed Ex V❑fU—Ptb— ❑LISPS Client
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Custody Seal Present? ❑Yes 6No Seals Intact? ❑Yes �No
Pace
Pace 2 of 2 for Internal Use ONI V
WO#:92296568
IIIIII IIIIII I III IIIfll
92296568
Date/Initials Person Examining ComaricaulfsH 1 iYo
Packing Material: ❑Bubble Wrap ❑Bubble Bags 41ione []Other. YYY---
Thermometer: IR SN: 122065387 ❑IR SN:122065371 Type tee: wet Blue Nane yp �j ❑ ❑ ❑Samples on fee, cooing process has begun
Correction Factor: 0.0'C Cooler Tamp CorrecTed ('C): a Z Biological Tissue Frozen? ❑Yes ONO mN/A
Temp should be above fre frig to 6'C r
USDA Regulated Sall ( 0 N/A, water sample)
Did samples glnate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inter atlonally,
[-Yes' I 1. ,_-,..�,__.._._ r... ri.
•ter u•�+
COMMENTS:
Chain of Custody Presents
Yes
CIND
EIN/A
1.
Chain of Custody Filled Out?
es
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2.
Chain of Custody Relinquished?
es
prvN
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3.
Sampler Name and/or Signature on COC7
ves
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O N/A
4.
Sam Ies Arrived within Hold Time?
Yes
EINO
N/A
S.
Short Hold Time Analysis (<72 hr ?
Y (
Yet
ONO
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Rush Tum Around Time Requested?
Dy.
No
N/A
7.
Sufficient Volume?
'm
r1No
❑N/A
8.
Correct Containers Used?
[]No
[]NIA
9.
-Pace Contalrleri Used?
/Yes
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❑N A
Containers Intact?
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10.
filtered Volume Received for Dissolved Tests?
❑yes
No
NA
11. Note if sediment is visible In the dissolved container
Sample labels Match COC?
]Yes
[]No
❑N/A
12.
-Includes DAte/Time/ID/Analysis ,Matrix:
All containers needing acid/base preservation have been
1/13
checked?
([JYes
QNo
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All containers needing preservation are found to be In
compliance with EPA recommendation?
(II1401, HrS0c, HO<Y NaOH>9 Sulfide, NaOH>12 Cyanide)
es
ONO
❑N/A
Exceptions; VOA, Collform, TOC, Oil and Grease,
7y,
0110/8015 1wateri DOCLLHS
s
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Yes
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N/A
24.
Heads ace In VOA vials (>S-6mm)?
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• 15.
Trip Blank Present? -
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Pace Trie Blank Lot A(if purchased):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Resolution:
Project Manager SCURF Review;
Date/Trse:
Date:
Project Manager SRF Review: 11 Date:
Note: Whenever therels a discrepancy affecting North Carolina compliance samples, a copy of this form will be ser
Out of hole, Incorrect Preservative, out of temp, Incorrect containers)
Field Data Required? ❑yes []No
Office II.e.
Page 14 of 15

- aceAnalytical'
` nwtv.pacslahccom
j 6701 CuntewCa Drive, Ralolgh, NC 27007
ph: (019) W-49M, lax: (910) e34fi497
NCWW Cert#67, NCDW CerW7791
Chain of Custody W.O.# `r:? r1(,
Report Results To:
Company: '..hats ",J:„ '
Address: 17 71 Mono"', e-e-Wtxzl /1,1 .
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Phone: ':fiZ•YSA-:fit _
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Bill To:
Project Reference: 131,5,e �
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Project Number:
Purchase Order #:
❑ Standard Report Delivery
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❑ 4 e2°C O Temp: °C
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❑ Yea ❑ No O nle
Base preserv. �124
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Page 15 of 15

1�
A7;-
NCDENR
North Carolina Department of Environment and Natural Resources
Pal McCrory Donald R. van der Vriart
Governor Secretary
June 5, 2015
Mr. Charles Price Cr nab T/5LA
Green Meadow, LLC l7�
12601 Plantside Drive
Louisville, Kentucky 40299
RE: Mining Permit No. 53-05
Colon Mine
Lee County
Cane Fear River Basin
Dear Mr. Price:
Your recent request to have the above referenced mining permit modified has been
approved. The modification is to redesign the erosion and sedimentation control measures
throughout the site and reduce the affected acreage to 314 acres as indicated on the Mine
Maps last revised December 31, 2014. The modification also includes changing the method
for reclaiming the mine by constructing structural fill using Coal Combustion Byproducts
(CCBs) in accordance with the provisions of the Coal Ash Management Act of 2014 and the
terms and conditions of Permit to Construct and Operate Colon Mine Site Structural Fill Permit
No. 5306-STRUC-2015 issued by the Division of Waste Management on June 5, 2015. A
copy of the modified permit is enclosed.
The conditions in the modified permit were based primarily upon the initial application.
Modifications were made as indicated by the modification request and as required to Insure
compliance with The Mining Act of 1971. The expiration date, mine name and permit number
shall remain the same as before the modification. I would like to draw your particular attention
to the following conditions where minor additions or changes were made: Operating Condition
Nos. 1B, 1C, 3C, 3D, 4B, 4C, 4D, 5, 10B and 12A and Reclamation Condition Nos. 1, 2A, 2E,
3. 4A and 4B.
G.S. 74-65 states that any actions taken under the Mining Act of 1971, such as the
issuance of mining permits, shall not be construed to supersede or otherwise affect or prevent
the enforcement of any zoning regulation or ordinance duly adopted by an incorporated city or
county or by any agency or department of the State of North Carolina, except insofar as a
provision of said regulation or ordinance is in direct conflict with the Mining Act of 1971. Thus,
the responsibility of compliance with any applicable zoning regulations lies with you.
As a reminder, your permitted acreage at this site is 371 acres and the amount of land
you are approved to disturb is 314 acres. Please note that the 21.15 acre area south of the
railroad cannot be released at this time and is still considered within the mine permit
boundary. This area can be released upon final stabilization of the disturbed areas.
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section • Land Quality Section
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http:/:/Iportal.ncdenr.org/web/Ir/
Mailing Address: 1612 Mail Service Center, Raleigh, North Carolina 27699-1612. 919-707.92001 FAX: [phone]
An Equal Opportunity 1 Affirmative Action Employer- 50% Recycled 110% Post Consumer Paper

Mr. Price
Page Two
Please review the modified permit and contact Ms. Judy Wehner, Assistant State Mining
Specialist, at [phone] should you have any questions concerning this matter.
S
TracDavis, PE, CPM
Dire r
Division of Energy, Mineral, and Land Resources
TED/jw
---- --Enclosures--_ -_-- —.----
cc: Mr. John Holley, PE, DEMLR Raleigh Regional Office Supervisor
Mr. Bradley Bennett, DEMLR Stormwater Permitting Supervisor
Ms. Janet Boyer, PE, DEMLR State Mining Specialist
Mr. Ed Mussler, PE, Division of Waste Management Permitting Supervisor
Mr. Jay Zimmerman, Director, Division of Water Resources
Mr, William Gerringer-Mine and Quarry Bureau, w/o enclosures

DEPARTMENT OF ENVIRONMENT
AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
LAND QUALITY SECTION
PERMIT
For the operation of a mining activity
in accordance with the provisions of G.S. 74-46 through 68, "The Mining
Act of 1971," Mining Permit Rule 15A NCAC 5 B, and other applicable
laws, rules and regulations
Permission is hereby granted to:
Green Meadow, LLC
Colon Mine
Lee County — Permit No. 53-05
for the operation of a
Clay Mine
Which shall provide that the usefulness, productivity, and scenic values of
all lands and waters affected by this mining operation will receive the
greatest practical degree of protection and restoration.
MINING PERMIT EXPIRATION DATE: December 12 2024

Page 2
In accordance with the application for this mining permit, which is hereby approved by the
Department of Environment and Natural Resources, hereinafter referred to as the Department,
and in conformity with the approved Reclamation Plan attached to and incorporated as part of
this permit, provisions must be made for the protection of the surrounding environment and for
reclamation of the land and water affected by the permitted mining operation. This permit is
expressly conditioned upon compliance with all the requirements of the approved Reclamation
Plan. However, completed performance of the approved Reclamation Plan is a separable
obligation, secured by the bond or other security on file with the Department, and may survive
the expiration, revocation, or suspension of this permit.
This permit is not transferable by the permittee with the following exception: If another
operator succeeds to the interest of the permittee in the permitted mining operation, by virtue
of a sale, lease, assignment or otherwise, the Department may release the permittee from the
duties imposed upon him by the conditions of his permit and by the Mining Act with reference
to the permitted operation, and transfer the permit to the successor operator, provided that
both operators have complied with the requirements of the Mining Act and that the successor
---- -- ----- — op�ra oragrees o assume tk�ulies_of_the:permittee with_reference_to-reclamation.of_tfie _
affected land and posts a suitable bond or other security.
In the event that the Department determines that the permittee or permittee's successor is not
complying with the Reclamation Plan or other terms and conditions of this permit, or is failing
to achieve the purposes and requirements of the Mining Act, the Department may give the
operator written notice of its intent to modify, revoke or suspend the permit, or its intent to
modify the Reclamation Plan as incorporated in the permit. The operator shall have right to a
hearing at the designated time and place on any proposed modification, revocation or
suspension by the Department. Alternatively and in addition to the above, the Department
may institute other enforcement procedures authorized by law.
Definitions
Whenever used or referred to in this permit, unless the context clearly indicates otherwise,
terms shall have the same meaning as supplied by the Mining Act, N.C.G.S. 74-49.
Modifications
November 4, 1988: This permit has been modified to change the company name from Sanford
Brick and Tile Corporation to Cherokee Sanford Group.
April 10, 1992: This permit has been modified to allow mining on 52 acres and on -site disposal
of petroleum contaminated soils as per the Mine Expansion Map Erosion and Sediment
Control Plan sated November 18, 1991.
July 21, 1992: This permit has been modified to allow crushed. brick to be substituted for #57
washed stone in the upstream faces of all rock check dams.

Page 3
February 13 1995: This Permit has been modified to increase the permitted acreage to
1093.18 acres and the affected acreage to 340 acres as indicated on the modification maps,
sheets 1-4 dated May 25. 1994 and sealed September 12, 1994.
August 2, 1996: This permit has been modified to change the corporate name from Cherokee
Sanford Group, Inc. to Cherokee Sanford Group, LLC,
October 24, 1997: This permit has been modified to revise the sediment and erosion control
plan as indicated on the Site Layout Mine Map dated September 22, 1997 and supplemental
information dated September 17, 1997 to more accurately reflect the field conditions, increase
the maximum depth of the mine map to 50 feet, allow the dewatering of the pit and allow two
lake areas to be left at the time of final reclamation.
September 22, 1999: This permit has been modified to add approximately 211.37 acres of
mine area that increases the affected acreage from 340.6 acres to 551.97 acres. This
modification includes expanding the mine area in three areas and the associated erosion and.
sP(iimeaLcontrol_measufes_as_indicated_on-the-General-Mineanformation-Map_dated June-21„
1999 and the Mine Modification Details Map last revised September 10, 1999, including the
supplemental information dated June 21, 1999 and August 25, 1999.
April 25, 2000: A partial release has been granted, reducing the permitted acreage at this site
by 5.01 undisturbed acres to 1088.17 acres.
December 12, 2014: A partial release has been granted, reducing the permitted acreage to
371 acres and the affected acreage at this site to 349 acres.
January 23, 2015: This permit has been transferred in its entirety from General Shale Brick,
Inc. to Green Meadow. LLC,
April 23, 2015: This permit has been modified to replace the flocculant currently permitted with
FLOC-1-11-8 and GT Clear, manufactured by Green Technologies, to improve settling efficiency
of suspended solids in the mine discharge water at this site provided these products are used
in accordance with the manufacturer's instructions as outlined in the letter and supplemental
information received by the Land Quality Section on April 10, 2015.
June 5, 2015: This permit has been modified to redesign the erosion and sedimentation
control measures throughout the site and reduce the affected acreage to 314 acres as
indicated on the Mine Maps last revised December 31, 2014. The modification also includes
changing the method for reclaiming the mine by constructing structural fill using Coal
Combustion Byproducts (CCBs) in accordance with the provisions of the Coal Ash
Management Act of 2014 and the terms and conditions of Permit to Construct and Operate
Colon Mine Site Structural Fill Permit No. 5306-STRUC-2015 issued by the Division of Waste
Management on June 5, 2015.
Expiration Date
This permit shall be effective from the date of its issuance until December 12, 2024

Page 4
Conditions
This permit shall be subject to the provisions of the Mining Act, N.C.G.S. 74-46, et. seq., and to
the following conditions and limitations:
OPERATING CONDITIONS:
A. Any wastewater processing or mine dewatering shall be in accordance with the
permitting requirements and rules promulgated by the N.C. Environmental
Management Commission. GS 74-51 (d) (3)
B. Any approvals or permits required to collect, handle, and properly dispose of any
water contacting Coal Combustion Byproducts (CCBs) shall be obtained prior to
any placement of CCBs within the mining permit boundary. GS 74-51 (d) (3)
C. Any stormwater runoff from the affected areas at the site shall be in accordance
-------- with- - -
an�applinable-permit.requirements.and.regulations.promulgated.byale
Environmental Management Commission. It shall be the permittee's
responsibility to contact the Stormwater Program to secure any necessary
stormwater permits, permit modifications, or other approval documents. The
terms and conditions of NPDES General Permit No. NCG020854 last revised
December 16, 2014 shall be followed. GS 74-51 (d) (3)
2. A. Any mining process producing air contamination emissions shall be subject to the
permitting requirements and rules promulgated by the N.C. Environmental
Management Commission and enforced by the Division of Air Quality. GS 74-51
(d) (3)
B. During mining operations, water trucks or other means that may be necessary
shall be utilized to prevent dust from leaving the permitted area. GS 74-51 (d) (3)
A. Sufficient buffer shall be maintained between any affected land and any adjoining
waterway or wetland to prevent sedimentation of that waterway or wetland from
erosion of the affected land and to preserve the integrity of the natural
watercourse or wetland. GS 74-51 (d) (2)
B. Any mining activity affecting waters of the State, water of the U. S., or wetlands
shall be in accordance with the requirements and regulations promulgated and
enforced by the N. C. Environmental Management Commission. GS 74-51 (d) (2)
C. Buffers shall be maintained as indicated on the Mine Maps last revised
December 31, 2014. GS 74-51 (d) (2)
D. No land disturbing activities shall be allowed within 50 feet of any wetland or
waterway until proof has been submitted to the Land Quality Section that all
necessary permits/certifications have been obtained from the US Army Corps of
Engineers and the Division of Water Resources. GS 74-51 (d) (2)

Page 5
A. Adequate mechanical barriers including but not limited to diversions, earthen
dikes, check dams, sediment retarding structures, rip rap pits, or ditches shall be
provided in the initial stages of any land disturbance and maintained to prevent
sediment from discharging onto adjacent surface areas or into any lake, wetland
or natural watercourse in proximity to the affected land. GS 74-51 (d) (6)
B. In order to improve settling efficiency of suspended solids in the mine discharge
water at this site, the operator shall use the flocculants FLOC-UL8 and GT Clear,
manufactured by Green Technologies, provided these products are used in
accordance with the manufacturer's instructions as outlined in the letter and
supplemental information received by the Land Quality Section on April 10, 2015,
GS 74-51 (d) (6)
C. All mining activities and any land disturbing activities conducted within the mining
permit boundary associated with the construction of the Coal Combustion
Byproducts (CCBs) structural fill, including the installation and maintenance of all
dsosiated-erosion-and-sediment-control-measures,-shall-be-conducted-as — —
indicated on the Mine Maps last revised December 31, 2014 and the
supplemental information received by the Land Quality Section on November 21,
2014, January 6, 2015 and March 17, 2015. GS 74-51 (d) (1-7)
D. No land disturbing activities and no structural fill placement shall occur into the
buffer or beyond the western mining permit boundary until an erosion and
sedimentation control plan has been submitted to and approved by the Land
Quality Section under the Sedimentation Pollution Control Act of 1973 and its
corresponding administrative rules and the associated construction stormwater
general permit has been issued. GS 74-51 (d) (7)
Groundwater monitoring and sampling prior to, during and post -disposal of Coal
Combustion Byproducts (CCBs) into the mined pits shall be implemented as outlined in
the Coal Ash Management Act and per the plan prepared for and approved by the
Division of Waste Management through Permit to Construct and Operate Colon Mine
Site Structural Fill Permit No. 5306-STRUC-2015 issued on June 5, 2015. GS 74-51 (d)
(2 and 3)
6. All affected area boundaries (314 acres) shall be permanently marked at the site on
100-foot intervals unless the line of sight allows for larger spacing intervals. GS 74-51
(d) (4)
The angle for graded slopes and fills shall be no greater than the angle which can be
retained by vegetative cover or other adequate erosion control measure, structure, or
device. In any event, exposed slopes or any excavated channels, the erosion of which
may cause off -site damage because of siltation, shall be planted or otherwise provided
with ground cover, devices or structures sufficient to restrain such erosion. GS 74-51 (d)
(4)

Page 6
8. The affected land shall be graded so as to prevent collection of pools of water that are,
or likely to become, noxious or foul. Necessary structures such as drainage ditches or
conduits shall be constructed or installed when required to prevent such conditions. GS
74-51 (d) (2)
9. Existing vegetation or vegetated earthen berms shall be maintained between the mine
and public thoroughfares whenever practical to screen the operation from the public. GS
74-51 (d) (4)
10. A. Sufficient buffer shall be maintained between any excavation and any mining
permit boundary or right-of-way to protect adjacent property. GS 74-51 (d) (4)
B. Buffers shall be maintained as indicated on the Mine Maps last revised
December 31, 2014. GS 74-51 (d) (4)
11. A physical barrier consisting of a fence or earthen berm, etc., shall be maintained
- --- arhund the-p-edmeter=of_any-highwall.-G.S-74_51_(d)_(4.)
12. A. The on -site disposal of Coal Combustion Byproducts (CCBs) as structural fill
within the mining permit boundary shall be conducted in accordance with the
Coal Ash Management Act and the Permit to Construct and Operate Colon Mine
Site Structural Fill Permit No. 5306-STRUC-2015 issued by the Division of Waste
Management on June 5, 2015, GS 74-51 (d) (7)
B. Notwithstanding the above condition, no on -site disposal of refuse or other solid
waste that is generated outside of the mining permit area shall be allowed within
the boundaries of the mining permit area unless authorization to conduct said
disposal has first been obtained from both the. Division of Waste Management
and the Land Quality Section, Department of Environment and Natural
Resources. The method of disposal shall be consistent with the approved
reclamation plan. GS 74-51 (d) (7)
C. Mining refuse defined by G.S. 74-49 (14) of The Mining Act of 1971 generated
on -site and directly associated with the mining activity may be disposed of in a
designated refuse area. All other waste products must be disposed of in a
disposal facility approved by the Division of Waste. Management. No petroleum
products, acids, solvents or their storage containers or any other material that
may be considered hazardous shall be disposed of within the permitted area. GS
74-51 (d) (7)
D. For the purposes of this permit, the Division of Energy, Mineral, and Land
Resources considers the following materials to be "mining refuse" (in addition to
those specifically listed under G.S. 74-49 (14) of the N.C. Mining Act of 1971):
GS 74-51 (d) (7)

Page 7
1. on -site generated land clearing debris
2. conveyor belts
3, wire cables
4. v-belts
5. steel reinforced air hoses
6. drill steel
E. If mining refuse is to be permanently disposed within the mining boundary, the
following information must be provided to and approved by the Division of Energy,
Mineral, and Land Resources prior to commencement of such disposal: GS 74-51
(d) (7)
1. the approximate boundaries and size of the refuse disposal area;
2. a list of refuse items to be disposed;
3. verification that a minimum of 4 feet of cover will be provided over the
refuse;
a verification-that-the-refuse_will be_disposed at teast_4_feet above_the
seasonally high water table; and
5. verification that a permanent vegetative groundcover will be established.
13. An annual Reclamation Report shall be submitted on a form supplied by the Department
by February 1 of each year until reclamation is completed and approved. GS 74-55
14. The operator shall notify the Department in writing of the desire to delete, modify or
otherwise change any part of the mining, reclamation, or erosion/sediment control plan
contained in the approved application for a mining permit and any approved revisions to
it. Approval to implement such changes must be obtained from the Department prior to
on -site implementation of the revisions. GS 74-52 (a)
15, The security, which was posted pursuant to N.C.G.S. 74-54 in the form of a
$500,000.00 blanket bond, is sufficient to cover the operation as indicated in the
approved application. This security must remain in force for this permit to be valid. The
total affected land shall not exceed the bonded acreage. GS 74-54
16. A. Authorized representatives of the Division of Archives and History shall be
granted access to the site to determine the presence of significant archaeological
resources. GS-74-50 (b3) (7)
B. Pursuant to N. C. G. S. 70 Article 3, "The Unmarked Human Burial and Human
Skeletal Remains Protection Act, " should the operator or any person in his
employ encounter human skeletal remains, immediate notification shall be
provided to the county medical examiner and the chief archaeologist, North
Carolina Division of Archives and History. GS-70-3

Page 8
APPROVED RECLAMATION PLAN
The Mining Permit incorporates this Reclamation Plan, the performance of which is a condition
on the continuing validity of that Mining Permit. Additionally, the Reclamation Plan is a
separable obligation of the permittee, which continues beyond the terms of the Mining Permit.
The approved plan provides:
Minimum Standards As Provided By G.S. 74-53
The final slopes in all excavations in soil, sand, gravel and other unconsolidated
materials shall be at such an angle as to minimize the possibility of slides and be
consistent with the future use of the land.
Provisions for safety to persons and to adjoining property must be provided in all
excavations in rock.
3. All overburden and spoil shall be left in a configuration which is in accordance with
accepted conservation practices and which is suitable for the proposed subsequent use
of the land.
4. No small pools of water shall be allowed to collect or remain on the mined area that are,
or likely to become noxious, odious or foul.
5. The revegetation plan shall conform to accepted and recommended agronomic and
reforestation practices as established by the North Carolina Agricultural Experiment
Station and the North Carolina Forest Service.
6. Permittee shall conduct reclamation activities pursuant to the Reclamation Plan herein
incorporated. These activities shall be conducted according to the time schedule
included in the plan, which shall to the extent feasible provide reclamation simultaneous
with mining operations and in any event, provide reclamation at the earliest practicable
time after completion or termination of mining on any segment of the permit area and
shall be completed within two years after completion or termination of mining.
RECLAMATION CONDITIONS:
Provided further, and subject to the reclamation schedule, the planned reclamation shall
be to backfill the mine excavation with Coal Combustion Byproducts (GCBs) in
accordance with the Coal Ash Management Act and Permit to Construct and Operate
Colon Mine Site Structural Fill Permit No. 5306-STRUC-2015 issued by the Division of
Waste Management on June 5, 2015. In addition, any disturbed areas shall be
regraded and revegetated as indicated on the Reclamation Plan, Sheet 02C-02, dated
December 31, 2014. GS 74-53
2. The specifications for surface gradient restoration to a surface suitable for planned
future use are as follows: GS 74-53

Page 9
A. All the final perimeter sideslopes shall be graded to a 3 horizontal to 1 vertical or
flatter slope.
B. Any settling ponds or sediment basins shall be backfilled and stabilized.
C. The processing, stockpile, and other disturbed areas neighboring the mine
excavation shall be leveled and smoothed.
D. Compacted surfaces shall be disced, subsoiled or otherwise prepared before
revegetation.
E. Materials not specifically approved within this mining permit shall not be
permanently disposed of at the mine site. On -site disposal of Coal Combustion
Byproducts (CCBs) and mining refuse shall be conducted in accordance with
Operating Condition Nos. 11A through 11E.
F. The affected land shall be graded to prevent the collection of noxious or foul
water.
3. Revegetation Plan:
After site preparation, all disturbed land areas shall be revegetated as per the Seeding
Plan submitted on the Erosion and Sedimentation Control Details, Sheet 3 of 3, last
revised December 31, 2014, GS 74-53
Whenever possible, disturbed areas should be vegetated with native warm season
grasses such as switch grass, Indian grass, bluestem and gamma grass. GS 74-51 (d)
(2)
In addition, the permittee shall consult with a professional wildlife biologist with the N.C.
Wildlife Resources Commission to enhance post -project wildlife habitat at the site. GS
74-51 (d) (2)
4. Reclamation Plan:
A. Reclamation shall be conducted simultaneously with mining to the extent
feasible. In any event, reclamation shall be initiated as soon as feasible after
completion or termination of mining of any mine segment under permit. GS 74-53

Page 10
B. Specific reclamation phases and schedules shall be followed as described in the
Reclamation Timeline, Section C, submitted with the supplemental information
received by the Land Quality Section on January 6,.2015 as follows: GS 74-53
Acres Estimated Completion
Phase 1 (Cells1 and 2) 38.1 November 2018
Phase 2 (Cells 3 and 4) 51.2 July 2021
Phase 3 (Cell 5) 29.4 November 2022
This permit, issued to Sanford Brick and Tile Company October 3, 1972, renewed
October 12, 1982, transferred to Cherokee Sanford Group Inc. November 4, 1988,
modified April 10, 1992 and July 21, 1992, renewed March 18, 1993, modified February
P ugust2--t996-October_2.4., _1.997 and_SepYember_22, 1.999;_renewed_March
22, 2004, modified April 6, 2005, renewed December 12, 2014. transferred to Green
Meadow, LLC January 23, 2015, and modified April 23, 2015. is hereby modified this 51h
day of June, 2015 pursuant to G.S. 74-52.
Tracy E. Davis, PE, CPM, Director
Division of Energy, Mineral, and Land Resources
By Authority of the Secretary
Of the Department of Environment and Natural Resources

0010
Genera! Shale
Building The American Dream*
February 20, 2015
NC Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
GENERAL SHALE BRICK, INC.
P.O. Box 3547, Johnson City, TN 37602 Ph. [phone] /FAX [phone]
www. generalshale. com
Certified: 7011 0110 0001 8214 3954
Subject: General Shale Brick, Inc.
2014 Stormwater Sampling Results
NCG020354 — Brickhaven No. 2 Mine
NCG020533 — Gulf Mine
NCG020442 — Beck Mine
NCG020854 — Colon Mine
Attached are our 2014 stormwater DMRs (original and copy) for the subject permits.
We recently transferred permit NCG020854 (Colon Mine) to Green Meadows LLC. The results
for this mine reflect our ownership in 2014.
Please call me at 423/952-4281 if you have questions concerning this information.
Thank you,
Steve Wyse, PE
Environmental Engineer
xc: Warren Paschal

VV
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
Mr. Charles E. Price
Green Meadow, LLC
12601 Plantside Drive
Louisville, NC 40299
Dear Mr. Price:
December 16, 2014
John E. Skvarla, III
Secretary
RECEIVED
DEC 2 2 2014
CENTRAL FILES
DWR SECTION
Subject: NPDES General Permit NCG020854
Green Meadow, LLC
Formerly General Shale Brick, Inc.
Certificate of Coverage NCG020854
Lee County
Division personnel received your request to revise your stormwater permit Certificate of
Coverage to accurately reflect your new company and/or facility name.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in
the General Permit remain unchanged and in full effect. This revised Certificate of Coverage is
issued under the requirements of North Carolina General Statutes 143-215.1 and the
Memorandum of Agreement between North Carolina and the U.S. Environmental Protection
Agency.
If you have any questions or need further information, please contact the Stormwater Permitting
Program at [phone].
Sincerely,
_/or Tracy E. D vis, P.E., CPM, Director
Division of Energy, Mineral and Land Resources
cc: Raleigh Regional Office
Stormwater Permitting Program Files
Cent al.Elle�
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section • Land Quality Section
1612 Mail Service Center, Raleigh, North Carolina 27699-1612. 919-707-9200 / FAX: [phone]
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http://portal.ncdenr.org/web/Ir/
An Equal Opportunity 1 Affirmative Action Employer— 50% Recycled 110% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL. AND LAND RESOURCES
GENERAL PERMIT NO. NCG020000
CERTIFICATE OF COVERAGE No. NCG020854
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Green Meadow, LLC
is hereby authorized to discharge stormwater from a facility located at:
Colon Mine
1604 Colon Road
Sanford
Lee County
to receiving waters designated as Roberts Creek, a class WS-fV water in the Cape Fear River
Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts 1, 11, 111, and IV of General Permit No. NCG020854 as attached.
This certificate of coverage shall become effective December 16, 2014.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day December 16; 2014.
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

Division of Energy, Mineral & Land Resources
�I
Land Quality Section/Stormwater Permitting
NCDENR
National Pollutant Discharge Elimination System
PERMIT NAME/OWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
Date Received
Year
I Month
I Da
Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
C� 1 S 2 0 0 0 0 I N 10* 10, 1 0 12 0 8 5 4
Permit status prior to requested change.
a. Permit issued to (company name):
b. Person legally responsible for permit:
c. Facility name (discharge):
d. Facility address:
e. Facility contact person:
General Shale Brick, Inc
Gregory A Bowles
First MI Last
Director of Real Estate, Environment & Geology
Title
3015 Bristol Highway
Permit Holder Mailing Address
Johnson City TN 37601
City State Zip
[phone] ( )
Phone Fax
Colon Mine
1604 Colon Road
Address
Sanford NC 27330
City Stale Zip
[phone] ext.
Larry Cockerill 243
First / MI / Last Phone
111. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ® Change in ownership of the facility
❑ Name change of the facility or owner
If other please explain:
b. Permit issued to (company name):
Green Meadow, LLC
c. Person legally responsible for permit:
Charles
E
Price
First
MI
Last
Managing Member
Title
VED
RECEIRECEIVED
12601 Plantside Drive
Permit Holder Mailing Address
DEC 15 2014
Louisville
KY
40299
City
State
Zip
DENR-LAND OJALITY
[phone]
cprice(rdcharah.com
STORMWATER PERMITTING
Phone
E-mail Address
d. Facility name (discharge):
Colon Mine
e. Facility address:
1604 Colon Road
Address
Sanford
NC
27330
City
State
Zip
f. Facility contact person:
Charles
E
Price
First
MI
Last
[phone]
cprice(@charah.com
Phone
E-mail Address
Revised Jan. 27, 2014

NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
IV. Permit contact information (if different from the person legally responsible for the+permit)
Permit contact: Charles E Price
First MI Last
Managing Member
Title
12601 Plantside Drive
Mailing Address
Louisville KY 40299
City . State Zip
(502) 245=1353 . cpriceacharah:com
Phone 'E-mail Address
V. Will the permitted Sacility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
VI Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
......:.................... :..........................................................................................
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
1, Gregory A. Bowles, attest that this application for a name/ownership change has been reviewed and is
accurate and complete to the best of my knowledge. 1 understand that if all required parts of this
application are not completed and that if all required supporting information is not included, this application
package will a returned as incomplete.V. l
l2- •ll.�:�
Signature Date
APPLICANT CERTIFICATION
I, Charles E. Price attest that this application for a nametownership change has been reviewed and is
accurate and complete to the.best of my knowledge. I understand that if all required parts of this
application are not completed and that if all required supporting information is not included, this application
package will be r trned as incomp te.
1z-lz-�y
Signature Date
PLEASE SEND THE:COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612

1372 FILED
0467 LEE COUNTY
MOLLIE A. MCINNIS
BK:01372 PG:0467 REGISTER OF DEEDS
FILED Nov 13, 2014
AT 01 A1:28 pm
BOOK 01372
START PAGE 0467
END PAGE 0476
Lt Cmmtr 11-13-2014
INSTRUMENT # 06088
NORTH CAROLINA
Real Estatc
Excix Tar $7.000.00
NORTH CAROLINA SPECIAL WARRANTY DEED
Excise Tax: $7,000.00
Parcel Identifier No. 9654-38-3247 (portion), 9654-58-2312, 9654-68-2373, 9655-81-9374 and 9655-62-2672 Verified by
County on the _ day of 12014 By:
Mail/Box to: Moore & Van Allen PLLC (MPH). 100 N. Tryon Street. Suite 4700, Charlotte, NC 28202
This instrument was prepared by:Bradshaw & Robinson. LLP, P.O. Box 607, Pittsboro, NC 27312 (without title examination)
Brief description for the Index: 410.56 acres, more or less. West Sanford Township, Lee County
THIS DEED made this 13th day of November 2014 (the "Effective Date'), by and between
GENERAL SHALE BRICK, INC.,
a Delaware corporation
3015 Bristol Highway
Johnson City, Tennessee 37601
GRANTEE
GREEN MEADOW, LLC,
a North Carolina limited liability company
12601 Plantside Drive
Louisville, Kentucky 40299
Enter in appropriate block for each Grantor and Grantee: name, mailing address, and, if appropriate, character of entity, e.g.
corporation or partnership.
The designation Grantor and Grantee as used herein shall include said parties, their heirs, successors, and assigns, and shall include
singular, plural, masculine, feminine or neuter as required by context.
W ITNESSETH, that the Grantor, for a valuable consideration paid by the Grantee, the receipt ofwhich is hereby acknowledged, has and
by these presents does grant, bargain, sell and convey unto the Grantee in fee simple, all that certain lot, parcel of land or condominium
unit situated in West Sanford Township, Lee County, North Carolina and more particularly described as follows (the "Property"):
Being all of that certain parcel or tract of land containing 410.56 acres, more or less, as shown on map or plat
entitled, "Recombination Survey of General Shale Brick, Inc. Property for Charah, Inc.," prepared by WNC
Professional Engineers & Surveyors recorded in Plat Slide 2014- li D Lee County Public Registry,
reference to which is hereby made for a more particular description.
Page 1 of 3

1372
0468
BK:01372 PG:0468
The Property was acquired by Grantor by instruments recorded in Book 584, Page 50, and in Book 1067, Page 682, Lee County
Registry. Grantor is the successor -by -merger to Cherokee Sanford Group, LLC, a Delaware limited liability company.
All or a portion of the Property does not include the primary residence of the Grantor.
Grantor hereby expressly conveys the Property subject to, and Grantor hereby expressly reserves from this conveyance, the Use
Restriction, and all other terms and conditions, and rights of the Grantor, pursuant to Exhibit A attached hereto and
incorporated herein by reference.
TO HAVE AND TO HOLD the aforesaid lot or parcel of land and all privileges and appurtenances thereto belonging to the Grantee in
fee simple.
And the Grantor covenants with the Grantee, that Grantor has done nothing to impair such title as Grantor received, and Grantor will
warrant and defend the title against the lawful claims of all persons claiming by, under or through Grantor, other than the following
exceptions:
1. Any defects in, interests in, objections to, exceptions to, or conditions, liens, encumbrances or other matters of record
relating to the title to the Property, whether evidenced by written instrument, or, if not evidenced by written
instrument, then any such matters that would be revealed by an accurate survey of the Property completed on the
Effective Date in accordance with exception #7, below.
2. Any encroachments upon or by the Property, any boundary disputes or conflicts regarding the boundaries of the
Property, any claims, rights -of -way, easements, restrictions and restrictive covenants upon or relating to the Property,
any encumbrances or other title defect(s), and the terms, provisions and conditions set forth in any instruments
evidencing or referring to any such defects, exceptions, conditions, liens, encumbrances, overlaps, encroachments or
boundary disputes or other matters.
3. All matters listed in Schedule i3 —Section 11 of the ALTA Commitment Form Commitment for Title Insurance issued
by Chicago Title Insurance Company as Commitment Number 14-12874CH (Revision 7, dated November 7, 2014),
which matters are incorporated herein by reference.
4. The lien of non -delinquent real property taxes and assessments, and any other non -delinquent impositions or exactions
of any governmental or quasi -governmental authority or body politic, or political subdivision, agency or department
thereof.
5. Any service, installation, connection, maintenance or construction charges due subsequent to the Effective Date.
6. The effect of any federal, state or municipal laws, rules, regulations or ordinances having applicability to the Property,
or any portion thereof, or the use or enjoyment of the same, whether now or hereafter in effect, including, but not
limited to, zoning, building, health, safety and environmental laws, rules and regulations, and notices of record relating
thereto.
7. Any defects in, interests in, objection to, exceptions to, or conditions, liens, encumbrances or other matters that would
have been disclosed on a current ALTA/ACSM Land Title Survey of the Property prepared as of the Effective Date in
accordance with the 2011 Minimum Standard Detail Requirements for ALTA/ACSM Land Title Surveys jointly
established and adopted by ALTA, ACSM and NSPS.
8. Any discrepancies, shortages in area, or state of facts which an inspection of the Property would disclose and which are
not shown by the public records.
9. Any creditors' rights exceptions customarily taken by title insurance companies.
[The remainder of this page is intentionally left blank; Grantor's signature is on the following page.]
Page 2 of 3

1372
0469
BK:01372 PG:0469
IN WITNESS WHEREOF, the Grantor has duly executed the foregoing as of the day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By:
Kevin H. Ham, Vice President
State of Tennessee -County of
I, the undersigned Notary Public of the County of .a and State aforesaid, certify that Kevin H. Ham
personally came before me this day and acknowledged that he is the Vice President of General Shale Brick, Inc., a Delaware
corporation, and that by authority duly given and as the act of such entity, he signed the foregoing instrument in its name on its behalf
as its act and deed. Witness my hand and Notarial stamp or seal, this _,J' day of November, 2014.
My Commission Expires: G - a9-10/(0
(Affix Seal)
�14`I,MY Cq
leg
Page 3 of 3
zia m,hcl COAtex— Notary Public
Notated or Typed Name

1372
0470 BK:01372 PG:0470
EXHIBIT A TO
NORTH CAROLINA SPECIAL WARRANTY DEED
THIS EXHIBIT A TO NORTH CAROLINA SPECIAL WARRANTY DEED (this "Agreement") is
entered into as of November 13, 2014 (the "Effective Date") by and between GENERAL SHALE BRICK, INC.,
a Delaware corporation (the "Grantor") and GREEN MEADOW, LLC, a North Carolina limited liability company
(the "Grantee"). Grantor and Grantee are sometimes referred to herein individually as a "Party" and collectively
as the "Parties."
WITNESSETH:
THAT, WHEREAS, the Parties entered into that certain Agreement for. Purchase and Sale of Property dated
November 12, 2014 (the "Contract"); and
WHEREAS, the Parties wish to provide record notice of certain terms of the Contract including, but not
limited to, matters regarding the Use Restriction.
NOW, THEREFORE, in consideration of ten dollars ($10.00), and for other good and valuable
consideration, the receipt and sufficiency of which are hereby acknowledged, Grantor and Grantee hereby agree as
follows:
SECTION 1. Declaration of Covenants. Grantor, with the joinder and the consent of the Grantee, hereby
declares that the Property shall be held, conveyed, encumbered, used, occupied and improved subject to the
following covenants, which shall encumber the title to the Property and shall be binding upon all persons now
having or hereafter acquiring any right, title, or interest in the Property, and their respective heirs, successors, and
assigns, and which shall inure to the benefit of the Grantor, its successors and assigns (the "Use Restriction"):
(a) Use Restriction. Prior to October 31, 2049, the Property shall not be used for the production,
manufacturing, storage, transportation or distribution of bricks, ceramic clay products or concrete masonry units.
This restriction on use shall run with the title to the Property and shall be enforceable by Grantee, its successors and
assigns. The Use Restriction shall expire and be null and void without further action of any Party on October 31,
2049 at 11:59 p.m. (local time).
SECTION 2. Environmental Release. Grantee, on behalf of itself and its members, managers and affiliates
and each of their respective successors and assigns (collectively, the "Releasors"), as of the Effective Date, hereby
waives, releases, and absolutely and forever discharges Grantor and its officers, directors, shareholders, subsidiaries,
affiliates, employees, agents and representatives, and their respective heirs, successors and assigns (collectively, the
"Releasees"), from any and all present or future rights, claims, actions, causes of action, demands, damages, liabilities,
attomeys' fees, costs, fines, penalties and expenses of every kind and nature whatsoever, now known or unknown, direct
or indirect, which any of the Releasors may have with respect to any of the Releasees, directly or indirectly arising from
or relating to (x) the presence or alleged presence of Hazardous Materials in, on, under, about, originating from or
relating to the Property if such Hazardous Materials were present at the Property on or prior to the Effective Date
including, without limitation, any such claims under or on account of any Environmental Law or this Agreement, (y)
any violation or alleged violation of any Environmental Law in connection with the Property that occurred or is alleged.
to have occurred on or prior to the Effective Date, and (z) the ownership, use, occupancy or operation of the Property
by Releasees on and prior to the Effective Date, including the use and/or operation of the Property for the mining of
clay or other mineral substances, and the conduct of any activities affecting the air, soil and/or water of the Property,
and activities related to the foregoing.

1372
0471
BK:01372 PG:0471
SECTION 3. Environmental Indemnity. From and after the Effective Date, Grantee shall indemnify,
defend and hold harmless Grantor and the other Releasees (individually, a "Grantor Indemnitee" and collectively,
"Grantor Indemnitees") from and against, and pay for (a) any and all actions, allegations, appeals, causes of action
(including removal and remedial actions), claims, demands, investigations, and lawsuits, of any kind, brought by
Grantee, a third party or any government entity against any Grantor Indemnitees based on, or arising or resulting from
(1) the actual or alleged presence of Hazardous Materials at, on, under or adjacent to the Property, to the extent such
Hazardous Material was first present or first alleged to be present at, on, under or adjacent to the Property on or after
the Effective Date, (2) any activity by Grantee, or any Person affiliated with Grantee, in connection with any actual,
proposed or threatened use, treatment, storage, holding, existence, disposition or other Release, generation, production,
manufacturing, processing, refining, control, management, abatement, removal, arrangement for disposal, handling,
transfer or transportation to or from the Property of any Hazardous Materials at any time located in, under, on or above
the Property, (3) the imposition, recording or filing or the threatened imposition, recording or filing of any
Environmental Lien encumbering the Property relating in any way to the activities conducted on, or operation or use
of, the Property on or after the Effective Date; (4) any actual or -threatened injury to, destruction of, or loss of natural
resources in any way connected with the Property arising on or after the Effective Date, including, but not limited to,
costs to investigate and assess such injury, destruction or loss relating in any way to the activities conducted on, or
operation or use of, the Property on or after the Effective Date; (5) any personal injury, wrongful death, or property or
other damage arising on or after the Effective Date under any statutory or common law or tort law theory, related to
environmental hazards on the Property, including, but not limited to, damages assessed for private or public nuisance
or for the conducting of an abnormally dangerous activity on the Property relating in any way to the activities conducted
on, or operation or use of, the Property on or after the Effective Date; and (6) any Environmental Claim relating in any
way to the Grantee's operation or use of the Property on or after the Effective Date (individually, a "Claim" and
collectively, "Claims'); and (b) any and all assessments, civil penalties, out-of-pocket costs and expenses (including
court costs and reasonable attorneys' fees) actually incurred by a Grantor Indemnitee (but excluding costs and expenses
of defending any Claim incurred by any such Grantor Indemnitee after Grantee has accepted and is diligently pursuing
defense of such Claim, unless such costs and expenses of defending such Claim are incurred with Grantee's prior written
consent), damages (including consequential and punitive damages awarded to any third -party), decrees, fines,
judgments, liabilities (including for strict liability), losses, obligations, orders and penalties (whether compensatory or
punitive) which may be assessed against or suffered or incurred by any Grantor Indemnitee based upon, or arising or
resulting from (i) any Claim that is (y) owed to Grantee, a third -party or any governmental entity, or (z) related to any
remedial actions to the Property required of Grantor under any applicable Environmental Law; or (ii) to the extent
arising out of, relating to or resulting from the Release or Threatened Release of Hazardous Materials from the Property
to, on, under, adjacent to, or otherwise affecting the real property owned by Grantor (including as successor in interest
to Cherokee Sanford Group, LLC, a Delaware limited liability company), or General Shale, Inc., on the date hereof (the
"Subject Property'), any remedial actions reasonably appropriate to enable clay to be mined from the Subject Property
or required to comply with applicable Environmental Law, including, without limitation, action to (x) test, identify,
investigate and monitor such Hazardous Materials or Release, and (y) clean-up, contain and remove such Hazardous
Materials (all of the foregoing, collectively, "Losses").
In the event that any Grantor Indemnitee receives written notice of the assertion of any Claim by any third -party or any
governmental entity with respect to which the Grantee is required to provide indemnification under this Agreement, the
Grantor Indemnitee shall provide Grantee with prompt written notice (a .'Claim Notice") of any Claim for which
indemnity is sought, which Claim Notice shall set forth in reasonable detail a statement of the pertinent facts known to
the Grantor Indemnitee concerning the Claim(s) that are the subject ofthe Claim Notice; provide d, however, that any
failure by a Grantor Indemnitee to give a timely, complete or accurate Claim Notice shall not affect the rights or
obligations of any party hereunder except and only to the extent that, as a result of such failure, Grantee's defense of
any such Claim was materially and adversely prejudiced. Grantee shall have the right, upon delivering written notice
(the "Defense Notice") to the Grantor Indemnitee within six (6) months after receipt from a Grantor Indemnitee of a
Claim Notice, to assume and conduct, at Grantee's sole cost and expense, the defense against those Claims identified
in the Claim Notice that are identified in the Defense Notice; provided, however, that (i) delivery by Grantee of a
Defense Notice shall constitute Grantee's irrevocable agreement that the Grantor Indemnitee(s) are entitled to
PAGE

1372 BK:01372 PG:0472
0472idemnification under this Agreement with respect to the Claims set forth in the Defense Notice, and (ii) Grantor shall
have the right to approve the defense counsel engaged by Grantee, such approval not to be unreasonably withheld,
conditioned or delayed (provided that Grantor hereby approves Moore & Van Allen PLLC). In the event that Grantee
shall fail to give a Defense Notice for any Claims identified in the Claims Notice within six (6) months after receipt
from a Grantor Indemnitee of such Claim Notice, then in any such event the Grantor Indemnitees shall have,the right
to conduct the defense of the Claims identified in the Claim Notice in good faith, provided that Grantor Indemnitees
shall be prohibited from compromising or settling any such Claims without the prior written consent of Grantee, which
consent shall not be unreasonably withheld, conditioned or delayed. In order to seek Grantee's consent, a Grantor
Indemnitee must provide to Grantee written notice detailing all of the terms, conditions and obligations of any proposed
settlement or compromise, including providing a copy of any proposed settlement agreement or other contractual
arrangement to be executed by parties to the proposed settlement or compromise (a "Grantor Indemnitee Settlement
Notice'). if Grantee does not provide to the respective Grantor Indemnitee(s) a written response to a Grantor
Indemnitee Settlement Notice within twenty (20) Business Days of Grantee's receipt of the Grantor Indemnitee
Settlement Notice (as provided in Section 18(b) herein), then Grantee's consent will be deemed given to the respective
Grantor Indemnitee. In the event the Grantee does timely deliver a Defense Notice and thereby elects to conduct the
defense of the Claims identified in the Defense Notice, the Grantor Indemnitees will cooperate with and make available
to the Grantee such assistance and materials as Grantee may reasonably request, all at the sole cost and expense of
Grantee. Regardless of which party defends such Claims, the other party hereto shall have the right at its own cost and
expense to participate in the defense assisted by counsel of its own choosing. Without the prior written consent of the
Grantor Indemnitees, which shall not be unreasonably withheld, conditioned or delayed, Grantee shall not approve the
entry of any judgment or enter into any settlement or compromise of any such Claims if (a) pursuant to.or as a result of
such judgment, settlement or compromise, such judgment, settlement or compromise would lead to liability or create
any financial or other obligation on the part of any Grantor Indemnitee for which the Grantor Indemnitee is not fully
indemnified and made whole hereunder, (b) the terms of such judgment, settlement or compromise do not provide for
a full and complete release of all such Claims in favor of each Grantor Indemnitee that is the subject of the Claim, and
(c) injunctive or other equitable relief will be imposed against any Grantor Indemnitee. In order to seek a Grantor
Indemnitee's consent, Grantee must provide to the Grantor Indemnitee written notice detailing all of the terms,
conditions and obligations of any proposed judgment, settlement or compromise, including, providing a copy of any
proposed settlement agreement or other contractual arrangement to be executed by parties to the proposed settlement
or compromise (a "Grantee Settlement Notice"). If a Grantor Indemnitee does not provide to Grantee a written
response to a Grantee Settlement Notice, within twenty (20) Business Days of the Grantor Indemnitee's receipt of the
Grantee Settlement Notice (as provided under Section 4 herein), then the Grantor Indemnitee's consent shall be deemed
given to the Grantee. Any judgment entered or settlement or compromise agreed upon as set forth in a Grantor
Indemnitee Settlement Noticethat is consented to by Grantee or a Grantee Settlement.Notice that is consented to by
Grantor, in the manner provided herein, shall be binding upon Grantee, and shall be conclusively deemed to be an
obligation with respect to which the Grantor Indemnitees are entitled to prompt indemnification hereunder, subject to
Grantee's right to appeal an appealable judgment or order.
For purposes of this Agreement, the term "Hazardous Materials" means chemicals, pollutants, contaminants, wastes,
toxic substances, hazardous substances, radioactive materials or genetically modified organisms, which are, have been
or become regulated by any federal, state or local government authority including, without limitation, (w) petroleum or
any fraction thereof, (x) asbestos, (y) any substance or material defined as a "hazardous substance" pursuant to § 101
of the Comprehensive Environmental Response, .Compensation, and Liability Act (42 U.S.C. § 9601), or (z) any
substance or material defined as a "hazardous chemical" pursuant to the federal Hazard Communication Standard (29
C.F.R. § 1910.1200); the term "Environmental Claim" means any claim, action, cause of action, investigation, or
notice (written or oral) by any person or entity alleging potential liability (including, without limitation, potential
liability for investigatory costs, cleanup costs, governmental response costs, natural resource damages, property
damages, personal injuries, or civil or criminal penalties) arising out of or resulting from (yy) the actual or alleged
presence or release into the environment of any Hazardous Materials at any location, whether or not owned or operated
by the Grantor, or (zz) circumstances forming the basis of any actual or alleged violation of any Environmental Law;
and the term "Environmental Law" means all federal, state, local, and foreign laws and regulations relating to pollution
or protection of human health or the environment (including, without limitation, ambient air, surface water, ground
PAGE

1372 BK:01372 PG:0473
0473
water, wetlands, land surface, subsurface strata, and indoor and outdoor workplace), including, without limitation, (yyy)
• laws and regulations relating to emissions, discharges, releases, or threatened releases of Hazardous Materials, and (zzz)
common law principles of tort liability. The terms "Release" and "Threatened Release" shall have the meanings
defined under Environmental Law. The term "Environmental Lien" means any mortgage, pledge, hypothecation,
assignment, deposit arrangement, encumbrance, lien (statutory or other), charge, or preference, priority or other security
interest or preferential arrangement arising pursuant to any Environmental Law or as a result of the presence, Release
or threatened Release or disposal of any Hazardous Materials. Grantee and Grantor agree that, in the event of any
Release or Threatened Release of Hazardous Materials in, at, on, under, about, originating from or relating to the
Property, or any Claims or Losses relating thereto, then (i) there shall be a presumption that such Hazardous Materials
were first introduced and first present in, at, on, under or about the Property after the Effective Date, and (ii) Grantee
shall bear the burden of proof if Grantee claims or asserts that such Hazardous Materials were present in, at, on, under
or about the Property on or prior to the Effective Date.
Grantee agrees that it shall not sell, assign or otherwise transfer any of the Property unless the purchaser, assignee or
transferee thereof, at or prior to such sale, assignment or transfer, agrees in writing (x) to be bound by and comply with
the terms of this Section 3 as if it were the Grantee hereunder, and (y) that Grantor is an intended beneficiary of such
writing. The immediately preceding sentence shall expire and be of no further force and effect at such time as none of
the following owns any portion of the Subject Property: (i) Grantor, (ii) Grantor's affiliates, (iii) any successor to all or
substantially all of the business of Grantor or its affiliates, and (iv) any direct or indirect subsidiary of Wienerberger AG.
SECTION 4. Notice. Any notice required or permitted to be given under this Agreement shall be in writing
and shall be deemed to have been given when deposited in Federal Express (or any other reputable national "next day"
delivery service) or in the United States mail via registered or certified mail, postage prepaid, return receipt requested,
and addressed as follows:
GRANTOR: General Shale Brick, Inc.
3015 Bristol Highway
Johnson City, Tennessee 37601
Ann: Real Estate Department
Phone: [phone]
and a copy (which shall
not constitute notice)
to: John A. Flaherty, Esq.
Dickstein Shapiro LLP
One Stamford Plaza
263 Tresser Blvd
Stamford, CT 06902
Phone: [phone]
GRANTEE: Green Meadows, LLC
12601 Plantside Drive
Louisville, KY 40299
Phone: [phone]
PAGE 4

1372
0474 and a copy (which shall BK:01372 PG:0474
not constitute notice)
to: Moore & Van Allen PLLC
100 N. Tryon Street, Suite 4700
Charlotte, North Carolina 28202-4003
Attention: Henry B. Ward, III
Phone: [phone]
Either Party may, from time to time, by notice as herein provided, designate a different address to which notices shall
be sent. Rejection or other refusal to accept or inability to deliver a notice required hereunder because of a changed
address of which no notice was given shall be deemed to be receipt of the notice. Grantee and Grantor agree that the
counsel for the Parties may deliver notice on behalf of the Parties.
SECTION 7. General Provisions.
(a) Applicable Law. This Agreement shall be governed by and construed in accordance with the
substantive laws of the State of North Carolina, without giving effect to its conflict of laws provisions.
(b) Entire Agreement. This Agreement and the Contract contain the entire understanding and
agreement by and between the Parties with respect to the Use Restriction, and all prior or contemporaneous oral or
written agreements regarding the Use Restriction, except for the Contract, are merged herein.
(c) Binding Effect. This Agreement shall be binding upon and shall inure to the benefit of the Parties,
and their respective heirs, successors and assigns.
(d) Severability. if any term or provision, or any portion thereof, of this Agreement, or the application
thereof to any person or circumstances shall, to any extent, be determined by a court of competent jurisdiction to
be invalid or unenforceable, then the remainder of this Agreement, or the application of such term or provision to
persons or circumstances, other than those as to which it is held invalid or unenforceable, shall not be affected
thereby, and each term and provision of this Agreement shall be valid and be enforced to the fullest extent permitted
by law.
(e) Captions and Headings. The captions and headings throughout this Agreement are for convenience
and reference only and the words set forth therein shall in no way be held to define or add to the interpretation,
construction or meaning of any provision of this Agreement.
(f) No Waiver. Failure of any Party to insist upon compliance of any provision of this Agreement
shall not constitute a waiver of the rights of such Party to subsequently insist upon compliance with that provision
or any other provision of this Agreement, nor in any way to affect the validity of all or any part of this Agreement.
(g) Amendment. No amendment to this Agreement shall be effective unless made in a writing signed
by the Parties, or their respective successors and assigns, and recorded on the Lee County Registry.
[The remainder of this page is intentionally left blank; signatures begin on the following page.]
PAGE 5

1372 BK:01372 PG:0475
0475
IN WITNESS WHEREOF, Grantor and Grantee have duly executed this Agreement as of the
day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By:
Kevin H. Ham, Vice President
State of Tennessee - County of / tJ?e ktin a r4� n
1, the undersigned Notary Public of the County of aj11a, &c giAD4 and State aforesaid,
certify that Kevin H. Ham personally came before me this day an�owledged that he is the Vice
President of General Shale Brick, Inc., a Delaware corporation, and that by authority duly given and
as the act of such entity, he signed the foregoing instrument in its name on its behalf as its act and deed.
Witness my hand and Notarial stamp or seal, this _L day of November, 2014.
My Commission Expires: 7'arnm5eCc 4-lelz- Notary Public
(o '129-a20/6p Notary's Printed or Typed Name
CA
TENNESSM
NOTARY
of this page is intentionally left blank; Grantee's signature is on the following page.]
EASEMENT AGREEMENT PAGE 6
AND DECLARATION OF COVENANTS

1372
0476
of
13K:01372 PG:O476
- County
GREEN MEADOW, LLC,
a North Carolina limited liability company
By: Cbarab, I ., its Member r
By:
Print Name: Charles E. Price
Title: President & CEO
I, the undersigned Notary Public of the County of �r., S,n,rti and State aforesaid, certify that
Charles E. Price personally came before me this day an ac owledged that he is the President & CEO of
Charah, Inc., the Member/Manager of Green Meadow, LLC, a North Carolina limited'liability company, and
that by authority duly given and as the act of such entity, he signed the foregoing instrument in its name on its
behalf as its act and deed. Witness my hand and Notarial stamp or seal, this 3 day
yoof,November, 2014.
My Commission Expires:
rJ !J Notary Public
���� Notary's Printed or Typed Name
(Affix Seal)
a ............
•5�r .
PAGE 7

©tF. Division of Energy, Mineral & Land Resources
Land Quality Section/Storniwater Permitting
National Pollutant Discharge Elimination System
NCDENR
"D N�o � PERMIT NAME/OWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
Date Received
Year Month
I Da
Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
N 1 G 1 S 10 1 2 1 0 0 0 0 I N 1 G 1 G 1 0 1 2 0 8 5 4
Permit status prior to requested change.
a. Permit issued to (company name): General Shale Brick, Inc.
b. Person legally responsible for permit-. Gregory A Bowles
First MI Last
Director of Real Estate, Environment & Geology
Tide
3015 Bristol Highway
Pennit Holder Mailing Address
Johnson City TN
37601
City State
Zip
[phone] (
)
Phone
Fax
c. Facility name (discharge):
Colon Mine
d. Facility address:
1604 Colon Road
Address
Sanford NC
27330
City State
Zip
e. Facility contact person:
[phone]
ext.Larry
Cockerill
243
First / MI / Last
Phone
111. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ® Change in ownership of the facility
❑ Name change of the facility or owner
!/other please explain
b. Permit issued to (company name):
Green Meadow, LLC
c. Person legally responsible for permit:
Charles
E
Price
First
MI
Last
Managing Member
Title
`�
RECEIVED
RC
12601 Plantside Drive
Pennit
Holder Mailing Address
DEC 15 20i4
Louisville
KY
40299
City
State
Zip
DENR-LAND QUALITY
[phone]
cprice o,charah.com
STORMWATER FERIVI!TTWG
Phone
E-mail Address
d. Facility name (discharge):
Colon Mine
e. Facility address:
1604 Colon Road
Address
Sanford
NC
27330
City
State
Zip
f. Facility contact person:
Charles
E
Price
First
MI
Last
[phone]
cprice(,charah.com
Phone
E-mail Address
Revised Jan. 27, 2014

NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
IV. Permit contact information (if different from the person legally responsible for the permit)
Permit contact:
Charles E Price
Firs[ MI Last
Managing Member
Title
12601 Plantside Drive
Mailing Address
Louisville KY 40299
City Stale Zip
[phone] cprice Q charah.com
Phone E-mail Address
V. Will the permitted facility continue to conduct the same industrial :activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
VI Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
I, Gregory A. Bowles, attest that this application for a name/ownership change has been reviewed and is
accurate and complete to the best of my knowledge. I understand that if all required parts of this
application are not completed and that if all required supporting information is not included, this application
package will a returned as incomplete. 1
4.
Signature Date
APPLICANT CERTIFICATION
1, Charles E. Price, attest that this application for a name/ownership change has been reviewed and is
accurate and complete to the best of nay knowledge. I understand that if all required parts of this
application are not completed and that if all required supporting information is not included, this application
package will be re rned as incolnp te.
Signature Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612

1372 FILED
0467 LEE COUNTY
MOLLIEA. MCINNIS
BK:01372 PG:0467 REGISTER OF DEEDS
FILED Nov 13, 2014
AT 01:41:28 pm
BOOK 01372
START PAGE 0467
END PAGE 0476
INSTRUMENT # 06088
Lee County 11-13-2014
NORM CAROLINA
Real E51:,,:
Excise Tar $7,000.00
NORTH CAROLINA SPECIAL WARRANTY DEED
Excise Tax: $7,000.00
Parcel Identifier No. 9654-38-3247 (portion), 9654-58-2312, 9654-68-2373, 9655-81-9374 and 9655-62-2672 Verified by
County on the _ day of , 2014 By:
Mail/Box to: Moore & Van Allen PLLC (MPH), 100 N. Tryon Street. Suite 4700, Charlotte, NC 28202
This instrument was prepared by: Bradshaw & Robinson, LLP, P.O. Box 607, Pittsboro, NC 27312 (without title examination)
Brief description for the Index: 410.56 acres, more or less. West Sanford Township, Lee County
THIS DEED made this 13th day of November, 2014 (the "Effective Date"), by and between
GRANTOR
GENERAL SHALE BRICK, INC.,
a Delaware corporation
3015 Bristol Highway
Johnson City, Tennessee 37601
GRANTEE
GREEN MEADOW, LLC,
a North Carolina limited liability company
12601 Plantside Drive
Louisville, Kentucky 40299
Enter in appropriate block for each Grantor and Grantee: name, mailing address, and, if appropriate, character of entity, e.g.
corporation or partnership.
The designation Grantor and Grantee as used herein shall include said parties, their heirs, successors, and assigns, and shall include
singular, plural, masculine, feminine or neuter as required by context.
W ITNESSETH, that the Grantor, for a valuable consideration paid by the Grantee, the receipt of which is hereby acknowledged, has and
by these presents does grant, bargain, sell and convey unto the Grantee in fee simple, all that certain lot, parcel of land or condominium
unit situated in West Sanford Township, Lee County, North Carolina and more particularly described as follows (the "Property"):
Being all of that certain parcel or tract of land containing 410.56 acres, more or less, as shown on map or plat
entitled, "Recombination Survey of General Shale Brick, Inc. Property for Charah, Inc.," prepared by WNC
Professional Engineers & Surveyors recorded in Plat Slide 2014- 110 Lee County Public Registry,
reference to which is hereby made for a more particular description.
Page I of 3

1372
0468
BK:01372 PG:0468
The Property was acquired by Grantor by instruments recorded in Book 584, Page 50, and in Book 1067, Page 682, Lee County
Registry. Grantor is the successor -by -merger to Cherokee Sanford Group, LLC, a Delaware limited liability company.
All or a portion of the Property does not include the primary residence of the Grantor.
Grantor hereby expressly conveys the Property subject to, and Grantor hereby expressly reserves from this conveyance, the Use
Restriction, and all other terms and conditions, and rights of the Grantor, pursuant to Exhibit A attached hereto and
incorporated herein by reference.
TO HAVE AND TO HOLD the aforesaid lot or parcel of land and all privileges and appurtenances thereto belonging to the Grantee in
fee simple.
And the Grantor covenants with the Grantee, that Grantor has done nothing to impair such title as Grantor received, and Grantor will
warrant and defend the title against the lawful claims of all persons claiming by, under or through Grantor, other than the following
exceptions:
1. Any defects in, interests in, objections to, exceptions to, or conditions, liens, encumbrances or other matters of record
relating to the title to the Property, whether evidenced by written instrument, or, if not evidenced by written
instrument, then any such matters that would be revealed by an accurate survey of the Property completed on the
Effective Date in accordance with exception 97, below.
2. Any encroachments upon or by the Property, any boundary disputes or conflicts regarding the boundaries of the
Property, any claims, rights -of -way, easements, restrictions and restrictive covenants upon or relating to the Property,
any encumbrances or other title defect(s), and the terms, provisions and conditions set forth in any instruments
evidencing or referring to any such defects, exceptions, conditions, liens, encumbrances, overlaps, encroachments or
boundary disputes or other matters.
3. All matters listed in Schedule B — Section 11 of the ALTA Commitment Form Commitment for Title Insurance issued
by Chicago Title Insurance Company as Commitment Number 14-12874CH (Revision 7, dated November 7, 2014),
which matters are incorporated herein by reference.
4. The lien of non -delinquent real property taxes and assessments, and any other non -delinquent impositions or exactions
of any governmental or quasi -governmental authority or body politic, or political subdivision, agency or department
thereof.
5. Any service, installation, connection, maintenance or construction charges due subsequent to the Effective Date.
6. The effect of any federal, state or municipal laws, rules, regulations or ordinances having applicability to the Property,
or any portion thereof, or the use or enjoyment of the same, whether now or hereafter in effect, including, but not
limited to, zoning, building, health, safety and environmental laws, rules and regulations, and notices of record relating
thereto.
7. Any defects in, interests in, objection to, exceptions to, or conditions, liens, encumbrances or other matters that would
have been disclosed on a current ALTA/ACSM Land Title Survey of the Property prepared as of the Effective Date in
accordance with the 2011 Minimum Standard Detail Requirements for ALTA/ACSM Land Title Surveys jointly
established and adopted by ALTA, ACSM and NSPS.
8. Any discrepancies, shortages in area, or state of facts which an inspection of the Property would disclose and which are
not shown by the public records.
9. Any creditors' rights exceptions customarily taken by title insurance companies.
IThe remainder of this page is intentionally left blank; Grantor's signature is on the following page.1
Page 2 of 3

1372
0469
BK:01372 PG:0469
IN WITNESS WHEREOF, the Grantor has duly executed the foregoing as of the day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By: '4Z4��
Kevin H. Ham, Vice President
State of Tennessee - County of lkmdAt 4r�G�011
I, the undersigned Notary Public of the County of and State aforesaid, certify that Kevin H. Ham
personally came before me this day and acknowledged that he is he is the of General Shale Brick, Inc., a Delaware
corporation, and that by authority duly given and as the act of such entity, he signed the foregoing instrument in its name on its behalf
as its act and deed. Witness my hand and Notarial stamp or seal, this -,'T- day of November, 2014.
My Commission Expires: l - .29 -.2016
(Affix Seal)
�%`��tttY1C
�,M
OF
TENNESW
s y NOTARY
:.N RUBUC
Page 3 of 3
Tit m-"V Ca,Qtex, Notary Public
Notated or Typed Name

1372
0470 BK:01372 PG:0470
EXHIBIT A TO
NORTH CAROLINA SPECIAL WARRANTY DEED
THIS EXHIBIT A TO NORTH CAROLINA SPECIAL WARRANTY DEED (this "Agreement") is
entered into as of November 13, 2014 (the "Effective Date") by and between GENERAL SHALE BRICK, INC.,
a Delaware corporation (the "Grantor") and GREEN MEADOW, LLC, a North Carolina limited liability company
(the "Grantee"). Grantor and Grantee are sometimes referred to herein individually as a "Party" and collectively
as the "Parties."
WITNESSETH:
THAT, WHEREAS, the Parties entered into that certain Agreement for Purchase and Sale of Property dated
November 12, 2014 (the "Contract"); and
WHEREAS, the Parties wish to provide record notice of certain terms of the Contract including, but not
limited to, matters regarding the Use Restriction.
NOW, THEREFORE, in consideration of ten dollars ($10.00), and for other good and valuable
consideration, the receipt and sufficiency of which are hereby acknowledged, Grantor and Grantee hereby agree as
follows:
SECTION 1. Declaration of Covenants. Grantor, with the joinder and the consent of the Grantee, hereby
declares that the Property shall be held, conveyed, encumbered, used, occupied and improved subject to the
following covenants, which shall encumber the title to the Property and shall be binding upon all persons now
having or hereafter acquiring any right, title, or interest in the Property, and their respective heirs, successors, and
assigns, and which shall inure to the benefit of the Grantor, its successors and assigns (the "Use Restriction"):
(a) Use Restriction. Prior to October 31, 2049, the Property shall not be used for the production,
manufacturing, storage, transportation or distribution of bricks, ceramic clay products or concrete masonry units.
This restriction on use shall run with the title to the Property and shall be enforceable by Grantee, its successors and
assigns. The Use Restriction shall expire and be null and void without further action of any Party on October 31,
2049 at 11:59 p.m. (local time).
SECTION 2. Environmental Release. Grantee, on behalf of itself and its members, managers and affiliates
and each of their respective successors and assigns (collectively, the "Releasors"), as of the Effective Date, hereby
waives, releases, and absolutely and forever discharges Grantor and its officers, directors, shareholders, subsidiaries,
affiliates, employees, agents and representatives, and their respective heirs, successors and assigns (collectively, the
"Releasees"), from any and all present or future rights, claims, actions, causes of action, demands, damages, liabilities,
attomeys' fees, costs, fines, penalties and expenses of every kind and nature whatsoever, now known or unknown, direct
or indirect, which any of the Releasors may have with respect to any of the Releasees, directly or indirectly arising from
or relating to (x) the presence or alleged presence of Hazardous Materials in, on, under, about, originating from or
relating to the Property if such Hazardous Materials were present at the Property on or prior to the Effective Date
including, without limitation, any such claims under or on account of any Environmental Law or this Agreement, (y)
any violation or alleged violation of any Environmental Law in connection with the Property that occurred or is alleged
to have occurred on or prior to the Effective Date, and (z) the ownership, use, occupancy or operation of the Property
by Releasees on and prior to the Effective Date, including the use and/or operation of the Property for the mining of
clay or other mineral substances, and the conduct of any activities affecting the air, soil and/or water of the Property,
and activities related to the foregoing.

1372
0471
BK:01372 PG:0471
SECTION 3. Environmental Indemnity. From and after the Effective Date, Grantee shall indemnify,
defend and hold harmless Grantor and the other Releasees (individually, a "Grantor Indemnitee" and collectively,
"Grantor Indemnitees") from and against, and pay for (a) any and all actions, allegations, appeals, causes of action
(including removal and remedial actions), claims, demands, investigations, and lawsuits, of any kind, brought by
Grantee, a third party or any government entity against any Grantor Indemnitees based on, or arising or resulting from
(1) the actual or alleged presence of Hazardous Materials at, on, under or adjacent to the Property, to the extent such
Hazardous Material was first present or first alleged to be present at, on, under or adjacent to the Property on or after
the Effective Date, (2) any activity by Grantee, or any Person affiliated with Grantee, in connection with any actual,
proposed or threatened use, treatment, storage, holding, existence, disposition or other Release, generation, production,
manufacturing, processing, refining, control, management, abatement, removal, arrangement for disposal, handling,
transfer or transportation to or from the Property of any Hazardous Materials at any time located in, under, on or above
the Property, (3) the imposition, recording or filing or the threatened imposition, recording or filing of any
Environmental Lien encumbering the Property relating in any way to the activities conducted on, or operation or use
of, the Property on or after the Effective Date; (4) any actual or threatened injury to, destruction of, or loss of natural
resources in any way connected with the Property arising on or after the Effective Date, including, but not limited to,
costs to investigate and assess such injury, destruction or loss relating in any way to the activities conducted on, or
operation or use of, the Property on or after the Effective Date; (5) any personal injury, wrongful death, or property or
other damage arising on or after the Effective Date under any statutory or common law or tort law theory, related to
environmental hazards on the Property, including, but not limited to, damages assessed for private or public nuisance
or for the conducting ofan abnormally dangerous activity on the Property relating in any way to the activities conducted
on, or operation or use of, the Property on or after the Effective Date; and (6) any Environmental Claim relating in any
way to the Grantee's operation or use of the Property on or after the Effective Date (individually, a "Claim" and
collectively, "Claims"); and (b) any and all assessments, civil penalties, out-of-pocket costs and expenses (including
court costs and reasonable attorneys' fees) actually incurred by a Grantor Indemnitee (but excluding costs and expenses
of defending any Claim incurred by any such Grantor Indemnitee after Grantee has accepted and is diligently pursuing
defense of such Claim, unless such costs and expenses of defending such Claim are incurred with Grantee's prior written
consent), damages (including consequential and punitive damages awarded to any third -party), decrees, fines,
judgments, liabilities (including for strict liability), losses, obligations, orders and penalties (whether compensatory or
punitive) which may be assessed against or suffered or incurred by any Grantor Indemnitee based upon, or arising or
resulting from (i) any Claim that is (y) owed to Grantee, a third -party or any governmental entity, or (z) related to any
remedial actions to the Property required of Grantor under any applicable Environmental Law; or (ii) to the extent
arising out of, relating to or resulting from the Release or Threatened Release of Hazardous Materials from the Property
to, on, under, adjacent to, or otherwise affecting the real property owned by Grantor (including as successor in interest
to Cherokee Sanford Group, LLC, a Delaware limited liability company), or General Shale, Inc., on the date hereof (the
"Subject Property"), any remedial actions reasonably appropriate to enable clay to be mined from the Subject Property
or required to comply with applicable Environmental Law, including, without limitation, action to (x) test, identify,
investigate and monitor such Hazardous Materials or Release, and (y) clean-up, contain and remove such Hazardous
Materials (all of the foregoing, collectively, "Losses").
In the event that any Grantor Indemnitee receives written notice of the assertion of any Claim by any third -party or any
governmental entity with respect to which the Grantee is required to provide indemnification under this Agreement, the
Grantor Indemnitee shall provide Grantee with prompt written notice (a "Claim Notice") of any Claim for which
indemnity is sought, which Claim Notice shall set forth in reasonable detail a statement of the pertinent facts known to
the Grantor Indemnitee concerning the Claim(s) that are the subject of the Claim Notice; provide d, however, that any
failure by a Grantor Indemnitee to give a timely, complete or accurate Claim Notice shall not affect the rights or
obligations of any party hereunder except and only to the extent that, as a result of such failure, Grantee's defense of
any such Claim was materially and adversely prejudiced. Grantee shall have the right, upon delivering written notice
(the "Defense Notice") to the Grantor Indemnitee within six (6) months after receipt from a Grantor Indemnitee of a
Claim Notice, to assume and conduct, at Grantee's sole cost and expense, the defense against those Claims identified
in the Claim Notice that are identified in the Defense Notice; provided, however, that (i) delivery by Grantee of a
Defense Notice shall constitute Grantee's irrevocable agreement that the Grantor Indemnitee(s) are entitled to
PAGE

1372 BK:01372 PG:0472
0472indemnification under this Agreement with respect to the Claims set forth in the Defense Notice, and (ii) Grantor shall
have the right to approve the defense counsel engaged by Grantee, such approval not to be unreasonably withheld,
conditioned or delayed (provided that Grantor hereby approves Moore & Van Allen PLLC). In the event that Grantee
shall fail to give a Defense Notice for any Claims identified in the Claims Notice within six (6) months after receipt
from a Grantor Indemnitee of such Claim Notice, then in any such event the Grantor Indemnitees shall have the right
to conduct the defense of the Claims identified in the Claim Notice in good faith, provided that Grantor Indemnitees
shall be prohibited from compromising or settling any such Claims without the prior written consent of Grantee, which
consent shall not be unreasonably withheld, conditioned or delayed. In order to seek Grantee's consent, a Grantor
Indemnitee must provide to Grantee written notice detailing all of the terms, conditions and obligations of any proposed
settlement or compromise, including providing a copy of any proposed settlement agreement or other contractual
arrangement to be executed by parties to the proposed settlement or compromise (a "Grantor Indemnitee Settlement
Notice"). If Grantee does not provide to the respective Grantor Indemnitee(s) a written response to a Grantor
Indemnitee Settlement Notice within twenty (20) Business Days of Grantee's receipt of the Grantor Indemnitee
Settlement Notice (as provided in Section 18(b) herein), then Grantee's consent will be deemed given to the respective
Grantor Indemnitee. In the event the Grantee does timely deliver a Defense Notice and thereby elects to conduct the
defense of the Claims identified in the Defense Notice, the Grantor Indemnitees will cooperate with and make available
to the Grantee such assistance and materials as Grantee may reasonably request, all at the sole cost and expense of
Grantee. Regardless of which party defends such Claims, the other party hereto shall have the right at its own cost and
expense to participate in the defense assisted by counsel of its own choosing. Without the prior written consent of the
Grantor Indemnitees, which shall not be unreasonably withheld, conditioned or delayed, Grantee shall not approve the
entry of anyjudgment or enter into any settlement or compromise of any such Claims if (a) pursuant to or as a result of
such judgment, settlement or compromise, such judgment, settlement or compromise would lead to liability or create
any financial or other obligation on the part of any Grantor Indemnitee for which the Grantor Indemnitee is not fully
indemnified and made whole hereunder, (b) the terms of such judgment, settlement or compromise do not provide for
a full and complete release of all such Claims in favor of each Grantor Indemnitee that is the subject of the Claim, and
(c) injunctive or other equitable relief will be imposed against any Grantor Indemnitee. In order to seek a Grantor
Indemnitee's consent, Grantee must provide to the Grantor Indemnitee written notice detailing all of the terms,
conditions and obligations of any proposed judgment, settlement or compromise, including providing a copy of any
proposed settlement agreement or other contractual arrangement to be executed by parties to the proposed settlement
or compromise (a "Grantee Settlement Notice"). If a Grantor Indemnitee does not provide to Grantee a written
response to a Grantee Settlement Notice, within twenty (20) Business Days of the Grantor Indemnitee's receipt of the
Grantee Settlement Notice (as provided under Section 4 herein), then the Grantor Indemnitee's consent shall be deemed
given to the Grantee. Any judgment entered or settlement or compromise agreed upon as set forth in a Grantor
Indemnitee Settlement Notice that is consented to by Grantee or a Grantee Settlement Notice that is consented to by
Grantor, in the manner provided herein, shall be binding upon Grantee, and shall be conclusively deemed to be an
obligation with respect to which the Grantor Indemnitees are entitled to prompt indemnification hereunder, subject to
Grantee's right to appeal an appealable judgment or order.
For purposes of this Agreement, the term "Hazardous Materials" means chemicals, pollutants, contaminants, wastes,
toxic substances, hazardous substances, radioactive materials or genetically modified organisms, which are, have been
or become regulated by any federal, state or local government authority including, without limitation, (w) petroleum or
any fraction thereof, (x) asbestos, (y) any substance or material defined as a "hazardous substance" pursuant to § 101
of the Comprehensive Environmental Response, Compensation, and Liability Act (42 U.S.C. § 9601), or (z) any
substance or material defined as a "hazardous chemical" pursuant to the federal Hazard Communication Standard (29
C.F.R. § 1910.1200); the term "Environmental Claim" means any claim, action, cause of action, investigation, or
notice (written or oral) by any person or entity alleging potential liability (including, without limitation, potential
liability for investigatory costs, cleanup costs, governmental response costs, natural resource damages, property
damages, personal injuries, or civil or criminal penalties) arising out of or resulting from (yy) the actual or alleged
presence or release into the environment of any Hazardous Materials at any location, whether or not owned or operated
by the Grantor, or (zz) circumstances forming the basis of any actual or alleged violation of any Environmental Law;
and the term "Environmental Law" means all federal, state, local, and foreign laws and regulations relatingto pollution
or protection of human health or the environment (including, without limitation, ambient air, surface water, ground
PAGE

1372 - BK:01372 PG:0473
0473
water, wetlands, land surface, subsurface strata, and indoor and outdoor workplace), including, without limitation, (yyy)
laws and regulations relating to emissions, discharges, releases, or threatened releases of Hazardous Materials, and (zzz)
common law principles of tort liability. The terms "Release" and "Threatened Release" shall have the meanings
defined under Environmental Law. The term "Environmental Lien" means any mortgage, pledge, hypothecation,
assignment, deposit arrangement, encumbrance, lien (statutory or other), charge, or preference, priority or other security
interest or preferential arrangement arising pursuant to any Environmental Law or as a result of the presence, Release
or threatened Release or disposal of any Hazardous Materials. Grantee and Grantor agree that, in the event of any
Release or Threatened Release of Hazardous Materials in, at, on, under, about, originating from or relating to the
Property, or any Claims or Losses relating thereto, then (i) there shall be a presumption that such Hazardous Materials
were first introduced and first present in, at, on, under or about the Property after the Effective Date, and (ii) Grantee
shall bear the burden of proof if Grantee claims or asserts that such Hazardous Materials were present in, at, on, under
or about the Property on or prior to the Effective Date.
Grantee agrees that it shall not sell, assign or otherwise transfer any of the Property unless the purchaser, assignee or
transferee thereof, at or prior to such sale, assignment or transfer, agrees in writing (x) to be bound by and comply with
the terms of this Section 3 as if it were the Grantee hereunder, and (y) that Grantor is an intended beneficiary of such
writing. The immediately preceding sentence shall expire and be of no further force and effect at such time as none of
the following owns any portion of the Subject Property: (i) Grantor, (ii) Grantor's affiliates, (iii) any successor to all or
substantially all of the business of Grantor or its affiliates, and (iv) any direct or indirect subsidiary of Wienerberger AG.
SECTION 4. Notice. Any notice required or permitted to be given under this Agreement shall be in writing
and shall be deemed to have been given when deposited in Federal Express (or any other reputable national "next day"
delivery service) or in the United States mail via registered or certified mail, postage prepaid, return receipt requested,
and addressed as follows:
GRANTOR: General Shale Brick, Inc.
3015 Bristol Highway
Johnson City, Tennessee 37601
Attn: Real Estate Department
Phone: [phone]
and a copy (which shall
not constitute notice)
to: John A. Flaherty, Esq.
Dickstein Shapiro LLP
One Stamford Plaza
263 Tresser Blvd
Stamford, CT 06902
Phone: [phone]
GRANTEE: Green Meadows, LLC
12601 Plantside Drive
Louisville, KY 40299
Phone: [phone]
PAGE

1372
0474 and a copy (which shall BK:01372 PG:0474
not constitute notice)
to: Moore & Van Allen PLLC
100 N. Tryon Street, Suite 4700
Charlotte, North Carolina 28202-4003
Attention: Henry B. Ward, III
Phone: [phone]
Either Party may, from time to time, by notice as herein provided, designate a different address to which notices shall
be sent. Rejection or other refusal to accept or inability to deliver a notice required hereunder because of a changed
address of which no notice was given shall be deemed to be receipt of the notice. Grantee and Grantor agree that the
counsel for the Parties may deliver notice on behalf of the Parties.
SECTION 7. General Provisions.
(a) Applicable Law. This Agreement shall be governed by and construed in accordance with the
substantive laws of the State of North Carolina, without giving effect to its conflict of laws provisions.
(b) Entire Agreement. This Agreement and the Contract contain the entire understanding and
agreement by and between the Parties with respect to the Use Restriction, and all prior or contemporaneous oral or
written agreements regarding the Use Restriction, except for the Contract, are merged herein.
(c) Binding Effect. This Agreement shall be binding upon and shall inure to the benefit of the Parties,
and their respective heirs, successors and assigns.
(d) Severability. If any term or provision, or any portion thereof, of this Agreement, or the application
thereof to any person or circumstances shall, to any extent, be determined by a court of competent jurisdiction to
be invalid or unenforceable, then the remainder of this Agreement, or the application of such term or provision to
persons or circumstances, other than those as to which it is held invalid or unenforceable, shall not be affected
thereby, and each term and provision of this Agreement shall be valid and be enforced to the fullest extent permitted
by law.
(e) Captions and Headings. The captions and headings throughout this Agreement are for convenience
and reference only and the words set forth therein shall in no way be held to define or add to the interpretation,
construction or meaning of any provision of this Agreement.
(t) No Waiver. Failure of any Party to insist upon compliance of any provision of this Agreement
shall not constitute a waiver of the rights of such Party to subsequently insist upon compliance with that provision
or any other provision of this Agreement, nor in any way to affect the validity of all or any part of this Agreement.
(g) Amendment. No amendment to this Agreement shall be effective unless made in a writing signed
by the Parties, or their respective successors and assigns, and recorded on the Lee County Registry.
[The remainder of this page is intentionally left blank; signatures begin on the following page.]
PAGES

1372. • BK:01372 PG:0475
0475
IN WITNESS WHEREOF, Grantor and Grantee have duly executed this Agreement as of the
day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By:
Kevin. Ham, Vice President
State of Tennessee - County of Li& %r r a {y n
I, the undersigned Notary Public of the County of and State aforesaid,
certify that Kevin H. Ham personally came before me this day and ace nowledged that he is the Vice
President of General Shale Brick, Inc., a Delaware corporation, and that by authority duly given and
as the act of such entity, he signed the foregoing instrument in its name on its behalf as its act and deed.
Witness my hand and Notarial stamp or seal, this L day of November, 2014.
,J.�
My Commission Expires: 7-4mm5eCIZVA°12- Notary Public
(o 'a9-o20/(0 Notary's Printed or Typed Name
-:,
CA
TENNESSM
y : NOTARY
PUBLIC
of this page is intentionally left blank; Grantee's signature is on the following page.]
EASEMENT AGREEMENT PAGE 6
AND DECLARATION OF COVENANTS

1372
0476
BK:01372 PG:0476
of
- County of
GREEN MEADOW, LLC,
a North Carolina limited liability company
By: Charah, In ., its Memberner
By: r/ J
Print Name: Charles E. Price
Title: President & CEO
r v
and State aforesaid, certify that
I, the undersigned Notary Public of the County of a�1 4, Charles E. Price personally came before me this day allya&howledged that he is the President & CEO of
Charah, Inc., the Member/Manager of Green Meadow, LLC, a North Carolina limited liability company, and
that by authority duly given and as the act of such entity, he signed the foregoing instrumentNovember, name on its
behalf as its act and deed. Witness my hand and Notarial stamp or seal, this�i_ day
of
My Commission Expires:
-/�0// ?
(Affix Seal)
;r
rJ
Notary's Printed or Typed Name
PAGE 7

��. Division of Energy, Mineral & Land Resources
Land Quality Section/Stormwater Permitting
NCDENR National Pollutant Discharge Elimination System
PERMIT NAME/OWNERSHIP CHANGE FORM
FOR AGENCV USE ONLY
Date Received
Year
Month
Da
I. Please enter the permit number for which the change is requested.
NPDES Permit
(or) Certificate of Coverage
N G S O
N 10, 10, 1 012 O 8 5 4
11. Permit status prior to requested change.
a. Permit issued to (company name):
General Shale Brick, Inc.
b. Person legally responsible for permit:
Gregory Bowles
First MI Last
Director of Environment
'fide
PO Box 3547
Permit Holder Mailing Address
Johnson City TN 37602
City State Zip
[phone] ( )
Phone Fax
c. Facility name (discharge):
Colon Mine
d. Facility address:
1604 Colon Road
Address
Sanford NC 27330
City State Zip
e. Facility contact person:
Warren Paschal [phone]
First / MI / Last Phone
111. Please provide the following for the requested
change (revised permit).
a. Request for change is a result of:
❑ Change in ownership of the facility
**No ownership change occurred**
❑ Name change of the facility or owner
/folherplease explain: Name listed on Contacts Summary is incorrect
b. Permit issued to (company name):
General Shale Brick, Inc.
c. Person legally responsible for permit:
Gregory Bowles
First MI Last
Director of Environment
o�d�D
'ripe
PO Box 3547
`
g ZW4
2
Pennit Holder Mailing Address
Nda�
Johnson City TN 37602
n grtfoth
City State Zip
�letmrs
(423 ) 282-4661
Phone F, nail Address
d. Facility name (discharge):
Colon Mine
e. Facility address:
1604 Colon Road
Address
Sanford NC 27330
City State Zip
f. Facility contact person:
Warren Paschal
First MI Iasi
(919 )774-6533 x-221
Phone I -mail Address
warreq p [e-mail]
IV. Permit from
contact information (if different
the person legally respons161e for the permit)
Revised Jan 27, 2014

Y'

NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
Permit contact Steve Wyse
First MI Last
Environmental Engineer
Title
PO Box 3547
Mailing Address
Johnson Citv TN 37602
City State Zip
[phone] [e-mail]
I'hone 17-mail Address
V. Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
x❑ Yes
❑ No (please explain)
VI. Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ovule e r ' I i o anon are
not sufficient for an ownership change **No ownership change occurred
.......................................................................................................................
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
I, , attest that this application for a name/ownership change has been reviewed and is accurate and
complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned a incomplete
A. 111^ </z-
Signature Gregory Bowles Date
APPLICANT CERTIFICATION
1, , attest that this application for a name/ownership change has been reviewed and is accurate and
complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as ii o . lete.
Signature Gregory Bowles Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Revised Jan. 27. 2014

0010
General Shale
Building The American Dreams
May 21, 2014
GENERAL SHALE BRICK, INC.
P.O. Box 3547, Johnson City, TN 37602 Ph. [phone] / FAX [phone]
www.generaishale.com
NC Division of Energy, Mineral, and Land Resources
Stormwater Permitting Program
Permit Contact Updates
1612 Mail Service Center
Raleigh, NC27699-1612
Subject: NPDES Permit Owner Name Correction
NCG020854
As I was completing our Industrial Stormwater Renewal contact forms online, I noticed that the
Owner Affiliation section was incorrect. Attached is the Permit Name/Ownership Change Form
to correct our records.
This change is not due to a change in ownership, we are simply trying to correct the record and
facilitate the online stormwater permit renewal. All other updates were completed online.
If you have questions about this material please call me at 423/952-4281.
Thank you,
A//////�
Steve Wyse, PE
Environmental Engineer

ANG-AWA
NC®ENR
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral, and Land Resources
Land Quality Section
Tracy E. Davis, PE, CPM Pat McCrory, Governor
Director John E. Skvada, III, Secretary
November 21, 2013
Mr. Gregory Bowles
General Shale, Inc.
P. 0. Box 3547
Johnson City, TN 37602
Subject: General Permit No. NCG020000
Colon Mine
COC NCG020854
Lee County
Dear Mr. Bowles:
In accordance with your application for a discharge permit received on October 3,
2013, we are forwarding herewith the subject certificate of coverage to discharge under the
subject state - NPDES general permit. This permit is issued pursuant to the requirements
of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between
North Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as
subsequently amended).
This certificate of coverage is not transferable. If the facility changes ownership or is
closed, the Division of Energy Mineral & Land Resources may require modification,
revocation or reissuance of the certificate of coverage.
This permit does not affect the legal obligation to obtain other permits which may
be required by the Division of Energy, Mining, and Land Resources, or any other federal,
state, or local authorities.
If you have any questions concerning this permit, please contact Larry Wade PE at
telephone number [phone].
Sin/ceerely, V�
for Tracy E. Davis, P.E.
cc: Raleigh Regional Office
Central Files
Stormwater Permitting Program Files
1612 Mail Service Center, Raleigh, North Carolina 27699-1612 • Telephone [phone] FAX: 919-733:2876
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: hito:lloortal.ncdenr.org/web/ Aland-ouality
An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG020000
CERTIFICATE OF COVERAGE No. NCGO20854
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
General Shale, Inc.
is hereby authorized to discharge stormwater from a facility located at
Colon Mine
1604 Colon Rd.
Sanford
Lee County
to receiving waters designated as Roberts Creek, a class WS-IV water in the Cape Fear River
Basin, in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts 1, 11, 111, IV, V, and VI of General Permit No. NCG020000 as
attached.
This certificate of coverage shall become effective November 21, 2013.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day November 21, 2013.
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

LOCATION MAP:
Latitude: 35932'05:3" N NCGO2O854 Facility
Longitude:-79!09'35.3" W
County: Lee General Shale, Inc. Location �—
Stream Class: Ws-R? Colon Mine
Receiving Stream: Ro.berts Creck �tL
Sub -basin: 03-06-07 (Cape Fear River Basin) /d Not to Scale

Wade, Larry
From: Parnell, David
Sent: Friday, November 08, 2013 10:15 AM
To: Wade, Larry
Subject: Stormwater Permits
Larry
It is permissible with RRO — DFMI.R — DLR —Stormwater, to go forward with approval of the following facility's
permits:
o N11G020855 R. M. Hayes Const —Stone Creek Sand and Gravel Mire
o NCG140431- Morgan Corp Roxboro Pugmill
• NCG020854 — General Shale, Colon Mine
Thanks,
Dave Parnell
Environmental Senior Specialist
North Carolina Department of Environment & Natural Resources
Division of Energy, Minerals, and Land Resources
Raleigh Regional Office
3800 Barrett Drive
Raleigh, NC 27609
0: [phone]
F: [phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law
and may be disclosed to third parties.
1

Wade, Larry '
From:
Wade, Larry
Sent:
Thursday, October 17, 2013 11:23 AM
To:
Parnell, David
Subject:
NCG020854 General Shale - Colon Mine
Attachments:
General NOI.pdf
Hello David,
Find attached the NO1 for the subject facility. ! am sending you a map through courier.
Please review these documents and let me know If you have any concerns, prior to issuing a permit for this facility.
If I do not receive a response from you within 30 days from the date of this email, I will proceed with issuing the permit
contingent upon central office review and approval.
If you have any questions, or require additional information please let me know.
Thanks,
Larry W. Wade PE Telephone: [phone]
Fax: [phone]
Stormwater Permitting Program
North Carolina Department of Environment & Natural Resources
Division of Energy Mineral and Land Resources
1612 Mail Service Physical Address - 512 N. Salisbury St. Room
9425
Raleigh, NC 27699-1612 Raleigh, NC 27604
************************This is a government E-mail address****************************
*********E-mails sent and received from this address can be disclosed to third parties************

'� Division of Water Quality /Surface Water Protection �r
NCDENR National Pollutant Discharge Elimination System
NC6
M«+m r.,.oux., ormr.ir.r or
a+.,nox.eHr..o N.a,nw neswnm
NCG020000
NOTICE OF INTENT
FOR AGENCY USE ONLY
Date Received
Year
Month
Do
13
16
Certificate of Coverage
b 514
Check At
I Amount
63314
100
Permit Assigned to
National Pollutant Discharge Elimination System application for coverage under General Permit
NCG020000:
STORMWATER DISCHARGES associated with activities classified as:
SIC (Standard Industrial Classification) Code - 14XX Mineral Mining Industry (except as specified below)
The following activities are also included:
Active or inactive mining operations (including borrow pits —except for NCDOT borrow pits) that discharge
stormwater contaminated with or that has come in contact with, any overburden, raw material, intermediate
products, finished products, byproducts or waste products located on the site of such operations;
Stormwater from vehicle maintenance activities at mining operations;
Overflow from facilities that recycle process wastewater; and/or
Mine dewatering (wastewater)
The following activities are specifically excluded from coverage under this General Permit:
Stormwater discharges associated with peat mining, coal mining, and metal mining;
Stormwater discharges from mining operations which are intermixed on site with stormwater from asphalt
operations and/or concrete operations;
Stormwater discharges associated with oil and gas extraction operations; and
Stormwater discharges associated with tourist gem mines
NCDOT borrow pits are covered under NCS000150
The following discharges are covered by NPDES general permit NCG520000 instead of NCG020000:
Point source discharges of stormwater and wastewater from in -stream sand mining operations (i.e., sand
dredging or dipping operations).
Please contact the NPDES Wastewater Point -Source Group for more information on coverage under this
permit.
Please print or tvpe all entries in this application form.
1) Mailing address of owner/operator (official address to which all permit correspondence will be mailed):
Legal Owner Name General Shale Inc.
(Attach the most recent Annual Report to the NO Secretary of State showing the current legal name of the corporation or entity.
Alternatively this permit can be given to an individual or government authority. This name must be the same name as appears on the
Division of Land Resources' Mining Permit.)
Signee's flame (as signed for in permit signature at bottom) Gregory Bowles
Street Address PO Box 3547
City Johnson City State TN ZIP Code 37602
Telephone No. 423 282-4661 Email greg.bowles(a)a)generalshale.com
Alternate Contact Name Steve Wvse Email (if different) steve.wysen.generalshale.com
Alternate Contact Telephone (if different) 423/952-4281 f 11 �(rJ j� f1CV7
OCT - 3 2013
Page 1 of 8
SW U-NCG02-NOI
oi.' Last revised <3/5/2012

NCG020000 N.O.I.
2) Location of facility producing discharge:
Facility Name Colon Mine
Facility Street Address 1604 Colon Road
Facility City Sanford State NC ZIP Code 27330
Facility County r eP _
Facility Contact
Telephone No.
Contact E-mail
Warren Paschal
919 774-5306 Fax:
war. [e-mail]
3) Physical Location Information:
Please provide a narrative description of how to get to the facility (use street names, state road numbers, and
distance and direction from a roadway intersection).Leaving Sanford, head north on Colon Road, turn
right on Brickyard Road at former brick plant, go 4/10 mile to mine entrance on left.
4) Latitude 35d 32' 5. 3" Longitude 79d 9' 35.3 "(degrees, minutes, seconds)
Permits:
5) This NPDES Permit Application applies to which of the following:
❑ New or Proposed Facility Date operation is to begin:
IN Existing Date began mining:
6) Standard Industrial Classification:
Provide the 4 digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility
SIC Code: 1 4 5 9
7) Provide a narrative description of the types of minerals mined at this facility
8) Is this mine an inactive mine site?
❑ No
Shale
N Yes If yes, do you posses an 'Inactive Renewal" from DEMLR and notified the DWO Regional Office or
have you certified to the DWO that the site has been stabilized? ® No ❑ Yes
9) Does this facility already have a valid Mining Permit from the Division of Energy, Mineral and Land Resource:
(DEMLR) [formerly DLR)?
❑ No
El Yes
If No, please indicate the status of the Mining Permit application:
If yes, please provide the Mining Permit number: 53-05 Please also provide a
copy of your DEMLR Mining Permit with this DWO application.
Note: DWO cannot issue a COC for the NCGO20000 General Permit until a Mining Permit is issued or
renewed by the DEMLR.
10) Does this facility have any other NPDES permits?
N No
❑ Yes If yes, list the permit numbers for all current NPDES permits for this facility:
Page 2 of 8
SWU-NCG02-NOI Last revised 9/5/2012

NCG020000 N.0.1.
11) Are you applying for a mining permit in the same location as a previously permitted mine?
IN No
❑ Yes If yes, specify permit number and name if known:
12) Does this facility have any Non -Discharge permits (ex: recycle permits)?
IS] No
❑ Yes If yes, list the permit numbers for all current Non -Discharge permits for this facility:
13) Does total area of this mine site include ready -mix and asphalt areas?
d No
❑ Yes
If yes, do they have D`A!O stormwater permits (if owned by the same company)? ❑ No
(provide permit number )
If not owned by the same company, who is the owner?
14) Will this mining operation precede development activities at this site?
❑ Yes
0 No
❑ Yes
15) Is this mine located within one of the 20 Coastal Counties and will it add more than 10,000 ft2 of impervious
surface?
® No
❑ Yes If yes, you may be required to apply for an additional state stormwater permit. Check with your
local Regional Office. See contact information and checklist below.
16) Is this mine located the Neuse, Tar -Pamlico, or Catawba River Basins, or the Randleman or Jordan
Water supply Watersheds?
® No
❑ Yes If yes, what size stream buffers are included or. site? ft. Please show buffers in site plans.
If yes, please include information and plans showing diffuse flow through buffers as required.
Discharge Points, Receiving Waters & Wetlands:
17) Receiving waters:
What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility stormwater
and/or wastewater discharges end up in? Roberts Creek
If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm
sewer system (e.g. City of Raleigh municipal storm sewer).
Receiving water classification (if known):
Note: Discharge of industrial wastewater to receiving waters classified as WS-II to WS-V, or SA, must
be approved by the Div. of Water Resources, or Div. of Marine Fisheries. If DWR or DMF does
not approve, coverage under NCG020000 cannot be granted. No new discharges of wastewater
are permitted in receiving waters classified as WS-1 or freshwater ORW. Wastewater
discharges to Saltwater ORW will not be approved under the NCG02 General Permit.
18) If your facility has wastewater discharges and they are to HWQ and/or PNA waters (Primary Nursery Areas)
waters, what is the proposed flow rate? (See
http://www ncdmf.neUmags/FNA maps/index.html, for map)
Page 3 of 8
SW U-NCG02-NOI Last revised 9/5/2012

NCG020000 N.O.I.
19) Discharge Points:
Number of discharge points (ditches, pipes, channels, etc. that convey discharges from the property):
Onsite: Stormwater: t Mine dewatering: Process Wastewater Overflow:
Offsite: Stormwater: — Mine dewatering: Process Wastewater Overflow:
Discharge points should be clearly marked on the submitted site plan.
Please provide short narrative description of discharges: Stormwater leaving the mine _
site vj3 a sediment basin.
a) is your mine dewatering and discharging? (Answer only if you are dewatering)
® No
❑ Yes If yes, where to? _ Surface Waters and/or Wetlands (on -site or off -site)
Other (on -site or off -site) Describe:
b) Are you dewatering but not discharging? (Answer only if you are dewatering)
® No
❑ Yes If Yes, please explain how you are dewatering, and where that water will be directed:
20) Will mining operations require dewatering near wetlands or impact any stream, groundwater, or wetlands?
M No
❑ Yes
Note: Wetlands must be CLEARLY DELINEATED on the site plan. Ivline dewatering activities that have
the potential to drain wetlands or otherwise impact surface water or groundwater MUST develop and
implement a Pumping Operation and Monitoring (O&M) Plan that has been approved by the
Division.
For sites that may drain wetlands — approval of a Pumping O&M plan may be required prior to
coverage under this general permit. The Pumping O&M Plan should be submitted to the
appropriate Regional Office and must be approved prior to operation.
The plan shall include, but is not limited to: (1) Groundwater monitoring strategies to demonstrate the
effect of pumping and to establish any pumping regime necessary to reduce impacts, and (2) Detailed
plans to maintain surrounding hydrology and respective monitoring to demonstrate compliance. See
checklist at end of document. Contact your local Regional Office for questions specific to your mine.
21) If you are dewatering, are there wetlands or surface waters within 400' of the mine pit perimeter?
❑ No
❑ Yes If yes, what distance are they from the mine pit perimeter?
22) Have you been required to obtain a 404/401 Certification permits?
® No
❑ Yes If yes, please briefly describe below (include information such a required mitigation, BMPs, setbacks,
and/or O&M plans for on or off -site wetlands or other pertinent information). Attach other sheets as necessary:
Page 4 of 8
SW U-NCG02-NOI Last revised 9/5/2012

NCG020000 N.O.I.
23) Have you been required to obtain a wetland delineation certified by the US Army Corps of Engineers?
M No ❑ Yes If yes, please attach to application submission.
Stormwater BMPs:
24) Does this facility employ any best management practices for stormwater control?
No IN Yes If yes, please briefly describe: Sediment and erosion control
25) Does this facility have a Stormwater Pollution Prevention Plan?
IS No ❑ Yes
If yes, when was it implemented?
26) Will vehicle maintenance activities occur at this facility?
® No ❑ Yes
Wastewater Treatment Facilities:
27) Will mine dewatering discharges occur?
® No
❑ Yes
28) Will discharges of overflows from process wastewater treatment systems occur?
® No
❑ Yes If yes,
a. Does this facility employ chemical additives to flocculate suspended solids? ❑ No ❑ Yes
If yes, please state the name, manufacturer and the quantity of average daily usage of the chemical additive
Note: Please see our website for a list of evaluated polyacrylamide (PAMS) products for use in North Carolina:
http://portal.ncdenr.org/web/wq/ws/su/npdessw
b. Does this facility overflow only during rainfall events exceeding the 10-yr, 24-hr rainfall event?
❑ No ❑ Yes
29) Are wastewater treatment facilities (including recycle systems) planned in the 100-year flood plain?
IN No
❑ Yes
30) Is your facility washing mined materials?
® No
❑ Yes If Yes, are you discharging this water?
Page 5 of 8
SWU-NCG02-NOI Last revised 9/5/2012

NCG020000 N.O.I.
Other:
31) Hazardous Waste:
a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility?
S1 No ❑ Yes
b) Is this facility a Smail Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of
hazardous waste?
❑ No ❑ Yes
c) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of
hazardous waste?
R7 No ❑ Yes
d) If you answered yes to questions b. or c., please provide the following information:
Type(s) of waste:
How is material stored:_
Where is material stored:
How many disposal shipments per year:
Name of transport / disposal vendor:
Vendor address:
32) Is your facility providing appropriate secondary containment for bulk storage of liquid materials? See permit
text for secondary containment requirements.
❑ No
LA Yes
33) Does your site have an active landfill within the mining permit boundary?
® No
❑ Yes If yes, specify type: ❑ LCID ❑ Other:
Final Checklist:
This application will be returned as incomplete unless all of the following items have been included and
initialed for. Please show that the following required information has been included by initialing in each
space below.
Fee of $100 made payable to NCDENR.
-7 Completed application and all supporting documents.
✓ Copy of the valid approved mining permit (MP) for the facility or indication of MP application status.
Copy of a county map or other general location map that shows the mining site and nearest major roads.
✓ Copy of USGS topographic map showing the mining site and surrounding areas, or other map that clearly
shows site location in relation to nearby streams, wetlands, and other waters, etc.
2 copies of large-scale (minimum 24" x 36") site plan with topographical lines with all outfalls, applicable
buffers and wetlands clearly delineated, and 100-year flood plain line if applicable.
A copy of your DEMLR mining permit.
A copy of your US Army Corps -approved wetland delineation if you marked "yes" to question 23 above.
-7 A line drawing of the water flow through the facility. A pictorial description of the nature and amount of any
sources of water and any collection and treatment measures.
— If mine site is in one of the 20 Coastal Counties:
• Applicant has checked with the appropriate regional office to verify the need for a Coastal State
Stormwater permit. Regional Office Contact:
Page 6 of 8
SWU-NCG02-NOI Last revised 9/5/2012

NCG020000 N.O.I.
• Applicant has included a detailed list of impervious surface areas and percentages, sub -drainage
areas and total drainage area.
If the mine is dewatering and near wetlands, or may otherwise impact surface waters or groundwater,
include the following and contact your local regional office about a Pumping O&M Plan (see below
for contact information). You may be required to provide an approved Pumping O&M plan priorto
NCG02 issuance.
_2 copies of detailed Full Size Plans (at least 24" x 36") delineating areas on the plans and listing
acrea a (including: wetlands, ditches, well -placements, pits, borrow areas, overburden storage,
stormwater controls/BMPs, vehicle maintenance areas, settling basins, product process (such as
screening, stockpiles, waste piles), total drainage area, impervious surface percentages (if slate sw
programs apply), applicable buffers, and access and/or haul roads).
__Pump dewatering size and information on its specifications.
____Well information (design, depths, maintenance).
_Physical monitoring for the wetlands areas.
_Settling pond sizing information, if applicable.
_Level spreader design, if applicable.
_Details about dewatering method.
_Cone of influence calculations.
_Description of measures to prevent erosion and flooding.
_Description & information about 401/404 permits that have been obtained.
_Copy of US Army Corps of Engineers wetland delineations or approved wetland delineation (if
applicable).
_I have contacted my local regional office about a Pumping O&M Plan.
Regional Office Contact: Date contacted:
-OR-
X I will not any impact nearby wetlands, surface waters or groundwater by dewatering.
Certification: North Carolina General Statute 143-215.6 b (i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other
document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false
statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly
renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the
[Environmental Management] Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to
exceed ten thousand dollars ($10,000).
33) Signatory Requirements (per 40 CFR 122.22)
All applications, reports, or information submitted to the Director shall be signed and certified.
a. All notices of intent to be covered under this General Permit shall be signed as follows:
(I) For a corporation: by a responsible corporate officer. For the purpose of this permit, a responsible corporate officer means: (a) a president,
secretary, treasurer or vice president of the corporation in charge of a principal business function, or any other person who performs similar
policy or decision making functions for the corporation, or (b) the manager of one or more manufacturing production or operating facilities
employing more than 250 persons or having gross annual sales or expenditures exceeding 25 million (in second quarter 1980 dollars), it
authority to sign documents has been assigned or delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or
(3) For a municipality, state, federal, or other public agency: by either a principal executive officer or ranking elected official.
I hereby request coverage under the referenced General Permit. I understand that coverage under this permit will
constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an individual
permit.
I agree to abide by the following as a part of coverage under this General Permit:
1. 1 agree to abide by the approved Mining Permit for this mining activity. (A copy of the valid mining
permit must be attached to this request.
Page 7 of 8
SWU-NCG02-NOI Last revised 9/5/2012

NCG020000 N.0.1.
2. 1 agree to not discharge any sanitary wastewater from this mining activity except under the
provisions of another NPDES permit specifically issued therefore.
3. 1 agree that bulk storage of petroleum products and other chemicals shall have adequate protection
so as to contain all spills on the site.
4. 1 agree that solid wastes will be disposed of in accordance with N.C. statutes and rules governing
solid waste disposal.
5. 1 agree that maintenance activities for vehicles and heavy equipment will be performed so as to not
result in contamination of the surface or ground waters.
I agree to abide by the provisions as listed above and recognize that the provisions are to be considered as
enforceable requirements of the General Permit.
1 certify that I am familiar with the information contained in this application and that to the best of my knowledge
and belief such information is true, complete, arid accurate.
Printed Name of Person Signing: Gregory Bowles
Title:
9/6 ' /c ?)
(Date Signed)
Notice of Intent must be accompanied by a check or money order for $100.00 made payable to NCDENR.
Mail the entire package to:
Stormwater and General Permits Unit
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Note
The submission of this document does not guarantee the issuance of an NPDES permit.
For questions, please contact the DWO Regional Office for your area.
DWO Regional Office Contact Information:
Asheville Office ......
[phone]
Fayetteville Office ...
[phone]
Mooresville Office ...
[phone]
Raleigh Office ........
[phone]
Washington Office ...(252)
946-6481
Wilmington Office ...
[phone]
Winston-Salem ......
[phone]
Central Office .........(919)
807-6300
Page 8 of 8
SW U-NCG02-NOI Last revised 9/5/2012

SOSID: 1155934
Date Filed: 7/31/2012 3:40:00 PM
Elaine F. Marshall
North Carolina Secretary of State
CD-470 r40) Business Corp®milon North Carolina Annual 2012 046 00762
11-22.10
Named Bu*wm Cempamlon: GENERAL SHALE INC.
Fiscal Yaer EroftV. 2 134 � io State of Intwrtoratlort: DELAWARE
Swatery of ate 0i Number.
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Rad4wedApwtCT. CORP SYSTEM
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county. Wake Ck' Raleigh-- Shas NC ZOcode:, 27601
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County. Wake Cyr Raleigh slste: NC apc(ide:27601
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Pdacipal Oilta Telsoona Number: ( 423) 262-4661
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PAY NCDENR*' DIV OF.' W4TER'
QUALITY
TO THE 1617 MAIL SERVICE"CENTER
ORDER RALEIGH' NC 27699 1617

1
DEPARTMENT OF ENVIRONMENT
AND NATURAL RESOURCES
DIVISION OF LAND RESOURCES
LAND QUALITY SECTION
PERMIT
For the operation of a mining activity
In accordance with the provisions of G.S. 74-46 through 68, " The Mining
Act of 1971," Mining Permit Rule 15A NCAC 5 B, and other applicable
laws, rules and regulations
Permission is hereby granted to:
Cherokee Sanford Group, LLC
Colon Mine
Lee County — Permit No. 53-05
for the operation of a
Clay Mine..
Which shall provide that the usefulness, productivity, and scenic values of
all lands and waters affected by this mining operation will receive the
greatest practical degree of protection and restoration.
MINING PERMIT EXPIRATION DATE: March 22, 2014

Page 2
In accordance with the application for this mining permit, which is hereby approved by the
Department of Environment and Natural Resources, hereinafter referred to as the Department,
and in conformity with the approved Reclamation Plan attached to and incorporated as part of
this permit, provisions must be made for the protection of the surrounding environment and for
reclamation of the land and water affected by the permitted mining operation. This permit is
expressly conditioned upon compliance with all the requirements of the approved Reclamation
Plan. However, completed performance of the approved Reclamation Plan is a separable
obligation, secured by the bond or other security on file with the Department, and may survive
the expiration, revocation, or suspension of this permit.
This permit is not transferable by the permittee with the following exception: If another
operator succeeds to the interest of the permittee in the permitted mining operation, by virtue
of a sale, imposed upon him by the conditions of his permit and by the Mining act with
reference to the permitted operation, and transfer the permit to the successor operator,
provided that both operators have complied with the requirements of the Mining.Act and that
the successor operator agrees to assume the duties of the permittee with reference to
reclamation of the affected land and posts a suitable bond or other security.
In the event that the Department determines that the permittee or permittee's successor is not
complying with the Reclamation Plan or other terms and conditions of this permit, or is failing
to achieve the purposes and requirements of the Mining Act, the Department may give the
operator written notice of its intent to modify, revoke or suspend the permit, or its intent to
modify the Reclamation Plan as incorporated in the permit. The operator shall have right to a
hearing at the designated time and place on any proposed modification, revocation or
suspension by the Department. Alternatively and in addition to the above, the Department
may institute other enforcement procedures authorized by law.
Definitions
Whenever used or referred to in this permit, unless the context clearly indicates otherwise,
terms shall have the same meaning as supplied by the Mining Act, N.C.G.S. 74-49.
Modifications
November 4, 1988: This permit has been modified to change the company name from Sanford
Brick and Tile Corporation to Cherokee Sanford Group.
April 10, 1992: This permit has been modified to allow mining on 52 acres and on -site disposal
of petroleum contaminated soils as per the Mine expansion Map Erosion and Sediment Control
Plan dated November 18, 1991.
July 21. 1992: This permit has been modified to allow crushed brick to be substituted for #57
washed stone on the upstream faces of all rock check dams.
February 13, 1995: This permit modified to increase the permitted acreage to 1093.18 acres
and the affected acreage to 340 acres as indicated on the mine modification maps, sheets 1-4
dated May 25, 1994 and sealed September 12, 1994.

Page 3
August 2, 1996: This permit has been modified to change the corporate name from Cherokee
Sanford Group, Inc. to Cherokee Sanford Group, LLC.
October 24, 1997: This permit has been modified to revise the sediment and erosion control
plan as indicated on the Site Layout Mine Map dated September 22, 1997 and supplemental
information dated September 17, 1997 to more accurately reflect the field conditions, increase
the maximum depth of the mine to 50 feet, allow the dewatering of the pit and allow two lake
areas to be left at the time of final reclamation.
September 22, 1999: This permit has been modified to add approximately 211.37 acres of
mine area that increases the affected acreage from 340.6 acres to 551.97 acres. This
modification includes expanding the mine area in three areas and the associated sediment and
erosion control measures as indicated on the General Mine Information Map dated June 21,
1999 and the Mine Modification Details Map last revised September 10, 1999, including the
supplemental information dated June 21, 1999 and August 25,:1.999.
April 25, 2000: A partial release has been granted, reducing the permitted acreage at this site
by 5.01 undisturbed acres to 1088.17 acres.
Expiration Date
This permit shall be effective from the date of its issuance until March 22, 2014.
Conditions
This permit shall be subject to the provisions of the Mining Act, N.C.G.S. 74-46, et. seq., and to
the following conditions and limitations:
OPERATING CONDITIONS:
A. Any wastewater processing or mine dewatering shall be in accordance with the
permitting requirements and rules promulgated by the N.C. Environmental
Management Commission.
B. Any stormwater runoff from the affected areas at the site shall be in accordance
with any applicable permit requirements and regulations promulgated by the
Environmental Management Commission. It shall be the permittee's responsibility
to contact the Water Quality Section, Division of Water Quality, to secure any
necessary stormwater permits or other approval documents.
2. A. Any mining process producing air contamination emissions shall be subject to the
permitting requirements and rules promulgated by the N.C. Environmental
Management Commission and enforced by the Division of Air Quality.
B. During mining operations, water trucks or other means that maybe necessary shall
be utilized to prevent dust from leaving the permitted area.

Page 4
3. A. Sufficient buffer (minimum 50 foot undisturbed except as noted below in Operating
Condition No. 3C) shall be maintained between any affected land and any adjoining
waterway or wetland to prevent sedimentation of that waterway or wetland from
erosion of the affected land and to preserve the integrity of the natural watercourse
or wetland.
B. Any mining activity affecting waters of the State, water of the U. S., or wetlands
shall be in accordance with the requirements and regulations promulgated and
enforced by the N. C. Environmental Management Commission.
C. Mining activities shall be allowed within 15 feet of Roberts Creek as indicated on
the mine maps, sheets 1 through 4, dated November 13, 2003 with the stipulation
that mining activities be conducted in such a manner as to ensure that all runoff
drains into the pit area. Immediately upon removal of material along the creek, a
100 foot buffer shall be established with hardwoods and shrubs:
4. A. Adequate mechanical barriers including but not limited to diversions, earthen dikes,
silt check dams, silt retarding structures, rip rap pits, or ditches shall be provided in
the initial stages of any land disturbance and maintained to prevent sediment from
discharging onto adjacent surface areas or into any lake, wetland or natural
watercourse in proximity to the affected land.
B. The upstream face of all check dams shall be lined with % inch to % inch crushed
brick with minimal fines.
C. Whenever possible, all drainage from the affected areas around the mine
excavations shall be diverted internal to said excavations.
D. Mining activities, including the installation and maintenance of the approved
sediment basins and associated diversion berms, shall be conducted as indicated
on the mine maps, Sheets 1 through 4, dated November 13, 2003 with the
following stipulation: immediately upon removal of the last mound of material along
the creek, a 100 foot buffer shall be established with hardwoods and shrubs.
E. Should the designed brick bat dams fail or stability problems develop in the
structure itself or at its abutments, said dams shall be redesigned and
reconstructed or replaced by other measures approved by the Department.
5. All affected acreage boundaries (551.97 acres) shall be permanently marked at the site
on 100-foot intervals unless the line of sight allows for larger spacing intervals.
6. The angle for graded slopes and fills shall be no greater than the angle which can be
retained by vegetative cover or other adequate erosion control measure, structure, or
device. In any event, exposed slopes or any excavated channels, the erosion of which
may cause off -site damage because of siltation, shall be planted or otherwise provided
with ground cover, devices or structures sufficient to restrain such erosion.

Page 5
The affected land shall be graded so as to prevent collection of pools of water that are,
or likely to become, noxious or foul. Necessary structures such as drainage ditches or
conduits shall be constructed or installed when required to prevent such conditions.
S. Existing vegetation or vegetated earthen berms shall be maintained between the mine
and public thoroughfares whenever practical to screen the operation from the public.
9. Sufficient buffer (minimum 50 foot undisturbed) shall be maintained between any
excavation and any mining permit boundary or right-of-way to protect adjacent property.
10. A physical barrier consisting of a fence or earthen berm, etc., shall be maintained
around the perimeter of any highwall.
11. A. No on -site disposal of refuse or other solid waste that is generated outside of the
mining permit area.shall be.allowed.within the boundaries of the mining permit
area unless authorization to conduct said disposal has first been obtained from
both the Division of Waste Management and the Land Quality Section,
Department of Environment and Natural Resources. The method of disposal
shall be consistent with the approved reclamation plan.
B. Mining refuse defined by G.S. 74-49 (14) of The Mining Act of 1971 generated
on -site and directly associated with the mining activity may be disposed of in a
designated refuse area. All other waste products must be disposed of in a
disposal facility approved by the Division of Waste Management. No petroleum
products, acids; solvents or their storage containers or any other material that
may be considered hazardous shall be disposed of within the permitted area.
C. For the purposes of this permit, the Division of Land Resources considers the
following materials to be "mining refuse" (in addition to those specifically listed
under G.S. 74-49 (14) of the N.C. Mining Act of 1971):
1. on -site generated land clearing debris
2. conveyor belts
3. wire cables
4. v-belts
5, steel reinforced air hoses
6. drill steel
D. If mining refuse is to be permanently disposed within the mining boundary, the
following information must be provided to and approved by the Division of Land
Resources prior to commencement of such disposal;:,:...,.
1. the approximate boundaries and size of the refuse disposal area;
2. a list of refuse items to be disposed;
3. verification that a minimum of 4 feet of cover will be provided over the
refuse;

Page 6
4. verification that the refuse will be disposed at least 4 feet above the
seasonally high water table; and
5. verification that a permanent vegetative groundcover will be established.
12. An annual Reclamation Report shall be submitted on a form supplied by the Department
by February 1 of each year until reclamation is completed and approved.
13. The operator shall notify the Department in writing of the desire to delete, modify or
otherwise change any part of the mining, reclamation, or erosion/sediment control plan
contained in the approved application for a mining permit and any approved revisions to
it. Approval to implement such changes must be obtained from the Department prior to
on -site implementation of the revisions.
14. The security, which was posted pursuant to N.C.G.S. 74-54 in the form of a $500,000.00
blanket bond, is sufficient to cover the operation as indicated in the, approved
application. This security must remain in force for this permit to be valid. The total
affected land shall not exceed the bonded acreage.
15. A. Authorized representatives of the Division of Archives and History shall be
granted access to the site to determine the presence of significant archaeological
resources.
B. Pursuant to N. C. G. S. 70 Article 3, "The Unmarked Human Burial and Human
Skeletal Remains Protection Act, " should the operator or any person in his
employ encounter human skeletal remains, immediate notification shall be
provided to the county medical examiner and the chief archaeologist, North
Carolina Division of Archives and History.

Page 7
APPROVED RECLAMATION PLAN
The Mining Permit incorporates this Reclamation Plan, the performance of which is a condition
on the continuing validity of that Mining Permit. Additionally, the Reclamation Plan is a
separable obligation of the permittee, which continues beyond the terms of the Mining Permit.
The approved plan provides:
Minimum Standards As Provided By G.S. 74-53
1. The final slopes in all excavations in soil, sand, gravel and other unconsolidated
materials shall be at such an angle as to minimize the possibility of slides and be
consistent with the future use of the land.
Z Provisions for safety to persons and to adjoining property must be provided in all
excavations in rock.
3. All overburden and spoil shall be left in a configuration which is in accordance with
accepted conservation practices and which is suitable for the proposed subsequent use
of the land.
4. No small pools of water shall be allowed to collect or remain on the mined area that are,
or likely to become noxious, odious or foul.
5. The revegetation plan shall conform to accepted and recommended agronomic and
reforestation practices as established by the North Carolina Agricultural Experiment
Station and the North Carolina Forest Service.
6. Permittee shall conduct reclamation activities pursuant to the Reclamation Plan herein
incorporated. These activities shall be conducted according to the time schedule
included in the plan, which shall to the extent feasible provide reclamation simultaneous
with mining operations and in any event, provide reclamation at the earliest practicable
time after completion or termination of mining on any segment of the permit area and
shall be completed within two years after completion or termination of mining.
RECLAMATION CONDITIONS:
Provided further, and subject to the Reclamation schedule, the planned reclamation
shall be t9:Tstore portions of the mine excavations to lake areas and to grade and
satisfactorily revegetate any other disturbed areas.
2. The specifications for surface gradient restoration to a surface suitable for planned
future use are as follows:

A.
B.
C.
D.
E.
The lake area shall be excavated to maintain a minimum water depth of four feet
measured from the low water table elevation.
The side slopes to the lake excavation shall be graded to a 3 horizontal to 1
vertical or flatter slope.
All remaining sideslopes shall be graded to a 2 horizontal to 1 vertical or flatter
slope.
Any settling ponds or sediment basins shall be backfilled and stabilized.
The processing, stockpile, and other disturbed areas neighboring the mine
excavation shall be leveled and smoothed.
F. Compacted surfaces shall. be disced, subsoiled or otherwise prepared before
......... ..
revegetation.
G. No contaminants shall be permanently disposed of at the mine site. On -site
disposal of waste shall be in accordance with Operating Condition 11.A through
D.
H. The affected land shall be graded to prevent the collection of noxious or foul
water.
Revegetation Plan:
After site preparation; all disturbed land areas shall be revegetated as per the
revegetation plan approved by T. Patrick Shillington, P.E. on June 16, 2004 or
by the following specifications:
Permanent Seed ino Saecifications
Dates Species Rate, Lbs/Acre
February 15—April 1 Kobe Lespedeza 10
50
Bahiagrass
Redtop 1
Winter rye (grain) 15
April 1 —July 31 Common Bermuda 50
August 1 — October 25 Lespedeza (unscarified) 30
40
German millet
October 25 — February 15 Rye (grain — temporary) 120

Page 9
Soil Amendments
Lime- 2000 Ibs/acre or follow recommendations from a soil test.
Fertilizer- 1000 Ibs/acre 8-8-8 or 10-10-10, or follow recommendations from a
soil test.
Mulch- All seeded areas shall be mulched using small grain straw at a rate
of 2000 Ibs/acre and anchored appropriately.
Whenever possible, disturbed areas should be vegetated with native warm season
grasses such as switch grass, Indian grass, bluestem and gamma grass.
In.addition, the permittee shall consult with a professional wildlife biologist with the N.C.
Wildlife Resources Commission to enhance post -project wildlife habitat at the site.
-f-?' Reclamation Plan:
Reclamation shall be conducted simultaneously with mining to the extent feasible. In
any event, reclamation shall be initiated as soon as feasible after completion or
termination of mining of any mine segment under permit. Final reclamation, including
revegetation, shall be completed within two years of completion or termination of mining.
This permit, issued to Sanford Brick and Tile Company October 3, 1972, renewed
October 12, 1982, transferred to Cherokee Sanford Group, Inc. November 4, 1988,
modified April 10, 1992 and July 21, 1992, renewed March 18, 1994, and modified
February 13, 1995, August 2, 1996, October 24, 1997, and September 22, 1999, is
hereby renewed this 22nd day of March, 2004 pursuant to GS 74-52.
I
-eJames D. Simons, Director
lo-k-Division of Land Resources
By Authority of the Secretary
Of the Department of Environment and Natural Resources