NCG020167_MONITORING INFO_20190118

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV CCo o a C ( �j !
DOC TYPE
❑HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ �ol -1 o I )
WYYMMDD

H RA RISON
January 14, 2019
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources JAN � 8 2019
Attn: DWR Central Files CEN- t1HL FlL o
1617 Mail Service Center �'t"�R S ECT10tq
Raleigh, North Carolina 27699-1617
RE: Annual Summary Discharge Monitoring Report DMR
NCG020'167
Harrison Fletcher Quarry
Fletcher, NC
Buncombe County
To Whom It May Concern:
Please find accompanying this letter, one original and one copy of the Discharge
Monitoring Report DMR for the above referenced location.
If you have any questions or need more information, please contact me at Harrison
Construction Company Division of APAC Atlantic Inc. P.O. Box 449 Franklin, NC 28744 or
call me at (865)-279-6374.
Sincerely,
Jeffrey Arnette
Environmental Compliance
P.O. Box 449 (28744) . 136 Rock Quarry Road . Franklin, NC 28734 • Tel: [phone] • Fax: [phone]
A Division of APAC-Atlantic, Inc.
An Equal opportunity Employer

ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) — WASTEWATER
SUBMIT TO CENtTiRA ,L,:O`FFICE*
General Permit No. NCG020000
Calendar Year a0 ( Y
*Report ALL WASTEWATER monitoring.data on'this,form.(include"No,Flow'/'No:Discharge" and Limit Violations) from
the previous calendar year to,the DEQ!byrMARCH 1•of each year.
Certificate of Coverage No. NCG02
FacilityName: FL 'SC-H+ SZ QUA?Zi
County: —as)Naoms3f-�
Phone Number: &4 I,Y ) 5 2A'& 55 Total no. of outfalls monitored
Certified Laboratory [,f Lab # 4 Q
Lab #
Wastewater (WW) Discharge Outfall No. r I
Is this an Industrial sand mine (See 40 CFR §436 Subpart D)?
Yes ❑
No [�
Does this outfall discharge WW to SA waters?
Yes ❑
No [f
Does this outfall discharge WW to SIB or PNA waters?
Yes ❑
No
Does this outfall discharge WW to HQW or ORW waters?
Yes ❑
No d
If so, what Is the 7010 flow rate? or Tidally influenced waters,
7Q10 not available ❑
Does this outfall discharge WW to Trout jr) designated waters?
Yes ❑
No R(
Were there any limit violations in the calendar year?
Yes ❑
No ff
Outfall No.
(
Daily Flow
Rate, cfs
pH,
SU
TSS,
mgll
SS,
mill
!lapplkable
Discharge
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Fecal
Coliform,
col/1 00 ml
SA
•
Effluent
L•rinitations
Mo. Ave ! Oaily Max.
HQWor.ORW
60%,of
7Q10•
lndlc:faNOFLOW.
if applicable' ,
Treshwaaler,
6.0-8 0
sanweler
.6:8-8:5
Industrial SM}�
25145• �
„Haw orORW •
"20130
,.lioworo,,y
,�QTrorPNA
:101,15 .
HOW,ORW,
:SA^SB PNA;
or
a
0:110 2 '
-'
-
' No,Limit
ClrclePleter
Qiiellty.SUedard.
, l��!srappues:
251r10 •
,NIA : ,
Waterquallly
St. ter,
NIA
NlaterQue!!!y
Standardapp:les
N/A
Date Sample
Collected,
r
u
,
3 '3o f I q
C2/:Z9
6. 3<
a. 5
e o.-
< V o
nr
7
-7 3 I$
-0176
5
C .5
C0.1
41.0
A/
7
10 It if
2 a
6.4
3.0
<0
a.l
/V /i
7
1 X 1141it
0 1'7
&.4
4,2.5
e-.1
i •o
IVIA
Permit Date 101112015 - 9130/2020
Last Revised 10-2-2015

Certificate of Coverage No. N0002 FC�U]®0
CERTIFICATION
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Required by 40 CFR §122.22]
Signature
Date 1 V4 1 q
Mail Annual Summary Wastewater DMR to the NCDEQ Central Office:
Note the address is correct — Central Files is housed in DWR (not DEMLR)
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files Telephone [phone]
Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at:
[phone]
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) — WASTEWATER
SUBMIT TO CENTRAL OFFICE*
General Permit No. NCG020000
Calendar Year Q 0 I Y
'Report ALL WASTEWATER monitoring data an this form (include "No-Fiow"1"No Discharge" and Limit Violations) from
the previous calendar year to the DEQ by MARCH i of each year.
Certificate of Coverage No. NCG02 U©©M
Facility Name:-_FLtGj-(,tj iZ QUARR`�
County: __a�)Nd01%A 3f �- _
Phone Number: &2)5'aYS45.5 Total no. of outfalls monitored i
Certified Laboratory t >- Lab # _ _ 40
Lab #
Wastewater (WW) Discharge Outfall No. ___ I
Is this an industrial sand mine (See 40 CFR §436 Subpart D)?
Yes ❑
No EJ
Does this outfall discharge WW to SA waters?
Yes ❑
No R1
Does this outfall discharge WW to SI3 or PNA waters?
Yes ❑
No [✓f
Does this outfall discharge WW to HQW or ORW waters?
Yes ❑
No d
If so, what is the 7Q10 flow rate? or Tidally influenced
waters,
7Q10 not available ❑
Does this outfall discharge WW to Trout (Tr) designated waters?
Yes ❑
No 2
Were there any limit violations in the calendar year?
Yes ❑
No Z
Outfall No.
Daily Flow
Rate, cfs
pH,
SU
TSS,
mgll
SS,
mill
nappllcable
Discharge
Turbidity,
NTU
Upstream
(U)Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Fecal
Coiiform,
co11100 ml
SA
Effluent
Limitations
Mo. Ave l Daily Max
HQW or DRW
50% of
7Q10
lndfcafe NO FLOW
ifappllcehla-
freshwater
6A-9.0
saltwater
;8'$•.+�
InduslrlaI Sind
25145
HOW'orORW
20130
HQW orORW
and 7ror PHA
10115
HQW, ORW,
$asB;PNA,
or an Trout
y
0•1/0•2
No Limit
clrclaWater
Mimi* Standard
aat�applles:
/ !s fn� jl1
(
N/A
WattrQntllty
Standard applies
NIA
waterau$ll
Standard applies
NIA
_
Date Sample
Collected,molddl r
y
r
z
>;
yn�
Via, I�
:��'
Mill
3 30 1
1 s
(a• 3
a.5
40.1
c 1.0
w L87
7 131 IS
•OI
5<
2.5
<O.I
N A
7
In It if
3.6
<0-1
a.I
N1 A
7
Permit Date 10/1/2015 — 913012020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 [d©®[Z
CERTIFICATION
" I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Required by 40 CFR § 122.22]
Signature
Date I 14 14
Mail Annual Summary Wastewater DMR to the NCDEQ Central Office:
Note the address is correct - Central Files is housed in DWR (not DFMLR)
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files Telephone [phone]
Questions? Contact DEMLR Stormwater Permitting Staff In the Central Office at:
[phone]
Permit Date 10111205 — 9/30/2020
Last Revised 10-2-2015

W
-; ANNUAL SUMMARY DMR - STORMWATER
11 SEND TO CENTRAL OFFICE
STORMWA TER DISCHARGE OUTFALLS (SDO)
GENERAL PERMIT NO. NCG020000
*Report ALL STORAVVi1TER Monitoring Data on this form (including No Flow and No Discharge and Permit Limit Violations) by r11.4RCH I of each year.
CERTIFICATE OF COVERAGE NO. NCG020167
FACILITY NAME: APAC-Atlantic, Inc
PERSON COLLECTING SAMPLES
CERTIFIED LABORATORYPace Analytical
Part A: Stormwater Monitoring Reauirements
Lab # 040
Lab #
SAMPLE COLLECTION YEAR: 2018
COUNTY Henderson
PHONE NO. (_828)684-6701
ADD TO LISTSERVE? YES ® NO ❑ EMAIL:
Outfall
No.
Date Sample
Collected
(moldd/ y r OR
NO FLONV)t
In Tier 2
Monthly
�
Monitoring?
g.
(yln)
# of Months in
Tier 2
Sampling z
Total Flow
(MG)
Total Suspended
Solids
(mg/1)
Turbidity
(NTU)
Settleable
Solids (mlh)
Total
Rainfall
(in)
Event
Duration
(minutes)
-
-
-
-
-
1001,4
See Footnote"
0.13
SDO-2
5/16/18
No
N/A
0.22
463
452
0.8
3.93
600+
SDO-2
10/26/18
No
NIA
NIA
34.5
47.3
<0.1
1.82
600
`i
' If "NO FLOW" or "NO DISCHARGE. Inter "NO FLOW" or "NO DISCHARGE" for each outfall here and the Date Range. I,' {C`�
2 Per NCG02: Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmarr ange
3 If a value is in excess of the benchmark, or outside the benchmark range (for pI-I), you must implement the Tier 1 or Tier 2 responses in the General Permit.
a TSS benchmark values are 100 mg/l except in ORW, H WQ, trout, and PNA waters where they are 50 mg/l.
51he discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs designated
as trout waters: 25 NTU for all lakes and reservoirs, and all salt waters, 50 NTU for all other streams and surface waters. Turbidity may be monitored at the SDO.
Alternatively, the permitter may choose to monitor turbidity in the receiving water. directly upstream and downstream of the SDO.
Permit Date: 1/]/2010-12/31/2014 Last Revised 02-02-11
Page 1 of 2

f
Part B: VeClicle Maintenance Activity Moni oring Require ents for facilities using > 55 gal of new motor oil/month on average
Outfall
No.
Date Sample
Collected
(mo/ddlyr OR
NO FLOW}
In Tier 2
Monthly
Monitoring?
(y1n )
4 of Months
in Tier 2
SamplingZ
New Motor
Oil Usage
al/month
Total Flow
(MG)
TPH using method
1664A SGT-HEM
m I
Total Suspended
Solids
m
pH
(Standard
Units
Total
Rainfall
in
Event
Duration
minutes
-
-
153
l OW, a
6-93
HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES
AT ANYONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO ED
HAVE YOU CONTACTED THE REGION? YES [:]No ❑
WHO AT THE REGION HAVE YOU SPOKEN WITH?
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and c plete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing
viol io st" 1 /, 7
(Signature of Permittee)
Permit Date: 1/l/2010-12/31/2014
ate
Last Revised 02-02-1 1
Page 2 of 2

L_.ANINUAL SUMMARY DMR - WASTEWATER
SEND TO CENTRAL OFFICE*
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All I#'astewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Iliolcrtions) by M4RCH I of each year. If
you have limit violations, you must also have turned in a Limit Violation DMR to your local Regional Office within 30 days of receiving sample results from a lab_
CERTIFICATE OF COVERAGE NO. NCG020000
FACILITY NAME: APAC-Atlantic, Inc.
PERSON COLLECTING SAMPLES: _Dan March
CERTIFIED LABORATORY:_PaceAnalytical Lab #1_040
Lab #
LIMIT VIOLATIONS? YES ❑ NO
Part A: Wastewater Monitoring Renuirements
SAMPLE COLLECTION YEAR: 2018
COUNTY: Henderson
PHONE NO. (_828)_684-6701
ADD TO LISTSERVE? YES ®NO❑ EMAIL: [e-mail]
INDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS;? ❑
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids'
Turbidity3
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/11,
NTUZ_'
ml/i2
Standard'
col/m12''
M W I
03/30/18
<5
3.2
<0.1
7.3
M W 1
05/ 16/ 18
5.0
7.5
<0.1
7.61
iM W 1
08/02/ 18
6.4
6.4
<0.1
7.2
M W I
10/26118
7.2
7.2
<0.1
6.5
' All mines must monitor WW discharges forTSS. Only industrial sand mine discharges are subject to TSS limits.
'- If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
'The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exeeed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively. the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
a Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: 1 / 1 /2010-12/3 l /2014 Last Revised 02-02-1 1
Page 1 of 2

Part A (oAtinued: Wastewater Nlanitorine Requirements
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids
Turbidity'
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/I',2
NTU2,3
m1/12
Standard'
col/ml'•'
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
1 am/(w-
,�re thaq t�F►�g are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Permit Date: I/l/2010-12/31/2014
11 /66�
(D te)
Last Revised 02-02-1 1
Page 2 of 2

1. ANNUAL SUMMARY DMR -WASTEWATER
SEND TO CENTRAL OFFICE*
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH I of each year. If
You have limit violations, you must also have turned in a Limit Violation DMR to your local Regional Office within 30 days of receiving sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG020000
FACILITY NAb1E: APAC-Atlantic, Inc.
PERSON COLLECTING SAMPLES: Dan March
CERTIFIED LABORATORY:_Pace Analytical
LIMIT VIOLATIONS? ITS ❑ NO
Part A: Wastewater Monitorina Requirements
av161
_ Lab # _040
Lab #
SAMPLE COLLECTION YEAR: _2017
COUNTY: Henderson
PHONE NO. (_828)_684-6701
ADD TO LISTSERVE? YES ®NO❑ EMAIL: [e-mail]
INDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS''? ❑
Outfall'No.
Date Sample,
Collected
Total Flow
Total Suspended
Solids
Turbidity3
Settleable Solids
pH
Fecal Cofiforms
-
mm/dd/yr.
MG
mg/ll•z
NTU23
mI/lz
Standard'
'col/mll.4
03/30/17
5.4
7.3
<0.1
7.4
N1 W 1
06/30/ 17
4.5
1.6
<0.1
7.3
NI N\' 1
11 /07/ 17
7.0
5.5
<0.1
7.6
NlWl
Q3
Did not
discharge.
--
--
--
—
RECEIVE
J N 11 201E
t i !iL t'ILf~�
All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
z If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
a Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
Permit Date: 1/l/2010-12/31/2014 Last Revised 02-02-11
Page 1 of 2

fart A Continued: Wastewater Monitoring Requirements
rr f.i—r, -.
ss
Outfall 1Vo.'
- o 'y
4r' h ",r^ �^
Date Sample
u r
,Collectedly.
•; - -�s-,
-r �.j�x?'S "" r ..r
'Total Flow
r
y., r _ s'
�
Total''SusperidedTurbidity'
5alidsi��
i`Y�r... � �t __
.-4 ki - n
J ''
ri
Settleable Solids
c�, i4'+G� 1.� i'
-� •3r
II' W
" n._-i'-h
.c "v '� a
C
h
Fecal Coliforin
-J ` � �. n,..'_
Yr,
!1�IG-,
_
mg/l_
1�Tii.
-►.r'nl/i
~Standard
'col/ml �.
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those,Arsons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am a ale tVat9tqe are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) (Da e)
Permit Date: 1/1/2010-12/3112014 Last Revised 02-02-11
Page 2 of 2

r ! ANNUAL SUMMARY DMR - STORMWATER
11 SENT) TO CENTRAL OFFICE * I
STORMWA TER DISCHARGE OUTFALLS (SDO)
GENERAL PERMIT NO. NCG020000
`Report .4LL STORMfVATER Monitoring Data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH I ofeach year.
CERTIFICATE OF COVERAGE NO. NCG020167
FACILITY NAME: APAC-Atlantic, Inc
PERSON COLLECTING SAMPLES
CERTIFIED LABORATORYPace Analytical Lab # _
Lab #
Part A: Stormw•ater Monitoring Requirements
040
SAMPLE COLLECTION YEAR: 2017
COUNTY Henderson
PHONE NO. (_828)684-6701
ADD TO LISTSERVE? YES ® NO ❑ EMAIL:
Outfall
No.
Date Sample
Collected
(mo/dd/yr OR
NO FLOIAJ t
In Tier 2
Monthly
Monitoring?
(y/n)
# of Months in
Tier 2
Sampling2
Total Flow.
(MG) =
Total Suspended
Solids
(mg/1)
Turbidity
� � y
(NTU} .
Settleable
Solids (ml/l)
Total
Rainfall
(in)
Event
.Duration
(mintites)
-
-
-
-
100"
See Footnote••$
0.1.3
SDO-1
11/07/17
No
N/A
0.22
24.8
28.3
<0.1
1.2
480
SDO-1
Jan -June
No
NIA
NIA
N/A
N/A
NIA
N/A
N/A
NO FLOW
During
First
Semi
Annual
Period
.
J
11 1 1 7018
CEN 1 FCL7,L
IP f P`T G�
V � R -E
If "NO FLOW" or "NO DISCHARGE. Enter "NO FLOW" or "NO DISCHARGE" for each outfall here and the Date Range.
z Per NCG02: Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range
s If a value is in excess of the benchmark, or outside the benchmark range (for pH), you must implement the Tier I or Tier 2 responses in the General Permit.
a TSS benchmark values are 100 mg./l except in ORW, I-1WQ, trout, and PNA waters where they are 50 mg/l.
'The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTIJ for freshwater streams, lakes, and reservoirs designated
as trout waters; 25 NTU for all lakes and reservoirs. and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the SDO.
Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the SDO.
Permit Date: I/l/2010-12/31/2014 Last Revised 02-02-11
Page 1 of 2

Part B: Vehicle Maintenance Activity Moni oring Require ents for facilities using > 55 gal of new motor oil/month on average
--Outfall
No�.
-
� .
' Date Sanple
Collected
inolddl OR
�� r
.NO FILON)
� .y , ".
ra In Tier 2
ti Monthly, ,
MflnitorinQ?'
b
(y/n).
x '
^# of Mdnths '
'.
.�, rn Trer.,Z'
Sampling
N 1;F � yY •.'7
' New Mbtor
s
:coil Usage, .
6 riionth�
,�;
'Total Flow
t
- (MG) t
f
'}4 •N �- i
TPH trsin ►ttethod
g
I664A SCT=HEM
v �' - T -
Tool Sus, ericled..
�, ., p,,'
Solids
rii}
r,,-.r a -,
1? H
�(Stasidard
Units
., r .r
Total`
=' Raiahil
rn
�, �,
Event
�- -
Duration'
minutes '`
o s
3 n
raw 3 a
3
r r.
HAS YOUR FACILITY HAD l OR MORE BENCHMARK E\CEEDENCES
AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES ❑ NO
HAVE YOU CONfACI•ED TIIE REGION:' YES ❑ No ❑
WIIO AT TIE REGION HAVE YOU SPOKEN WITII?
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality T ��
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and copplete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing
vi
(Signature of Permittee)
Permit Date: 1/l/2010-1213112014
w rfi�-,
(Dat )
Last Revised 02-02-11
Page 2 of 2

or ..4ft
January 8, 2018
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Annual Summary Wastewater DMR
NCG020167
Harrison Fletcher Quarry
Fletcher, NC
Henderson County
To Whom It May Concern:
JAN 1p N
TION
INFORMA ONPROCESSING UNIT
Please find accompanying this letter, one original and one copy of the Annual
Summary Wastewater DMR for the above referenced location.
If you have any questions or need more information, please contact me at Harrison
Construction Company Division of APAC Atlantic Inc. P.O. Box 449 Franklin, NC 28744 or
call me at (865)-279-6374.
Sincerely,
ereyy nette
Environmental Compliance
P.O. Box 449 (28744) + 136 Rock Quarry Road • Franklin, NC 28734 • Tel: [phone] . Fax: [phone]
A Division of APAC-Atlantic, Inc.
An Equal Opportunity Employer

E-1
•
•
ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) — WASTEWATER
SUBMIT TO CENTRAL OFFICE*
General Permit No. NCG020000
Calendar Year a 01 -?
'Report ALL WASTEWATER monitoring data on this form (include "Noflow"Y`No Discharge" and Limit Violations) from
the previous calendar year to the DEQ. by MARCH 1 of each year,
Certificate of Coverage No. N0002
Facility Name: l- L- F--TC. M eT, Q t, ARTt `!
County: I-LS NDCSCS01-3
Phone Number: d kt 5-o0- 5455 Total no. of outfalls monitored
Certified Laboratory PN.r. a. Lab # 40
Lab #
Wastewater (WW) Discharge Outfall No. I
Is this an industrial sand mine (See 40 CFR §436 Subpart D)?
Yes ❑
No Z'
Does this outfall discharge WW to SA waters?
Yes ❑
No d
Does this outfall discharge WW to SB or PNA waters?
Yes ❑
No [�
Does this outfall discharge WW to HQW or ORW waters?
Yes ❑
No
If so, what Is the 7010 flow rate? or Tidally influenced
waters,
7Q10 not available ❑
Does this outfall discharge WW to Trout jr) designated waters?
Yes ❑
No Z
Were there any limit violations in the calendar year?
Yes ❑
Nov
Outfall No.
Daily Flow
Rate, cfs
pH,
SU
TSS,
mgll
SS,
mlll
HappikabN
Discharge
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Fecal
Coliform,
coI1100 ml
SA
Effluent
Limitations
Mo. Ave fDaily Mar_
Haw or ORW
50ORW,% of
7Q10
-
IndkateNOFf_OW
if applicable101.15
freshwater.
6.0-9.b
saltwater
6. g'a• 5
Industrial Sand
-25145
t♦Qw.,ORW
2�130
Hdw or ORw
andTrarPNA
HOW,
s. S,C"
aranyTrout
0:110.2
No Limit
ClrcleWater
O that app ;ard
50125/10
NIA
WaterOuallty
Standard applies
NIA
Water Quality
Standard applies
lA
Date Sample
Collected
molddl r
gin
. �E3.r}YrK.z'�a7
i`;* +t..r�
is�ri�a
a?kt'�
'.fi.-w
i5+,_�. �:St.iC.�3�
h'L+d:'I;ti�:i4h ,_„„-�. �
���t„•.�. 7{
0•
9
<1•
40.
!.
N
Ar A
llaQI-7
40,1
Do
IN A
Permit Date 10/1/2015 - 9/3012020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 0 1❑©❑7
CERTIFICATION
" I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Roquired by 40 CFR § 122,22]
Signature
Date I
Mail Annual Summary Wastewater DMR to the NCDEQ Central Office:
Note the address is correct - Central Files is housed in DWR (not DEMLR)
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
10 Raleigh, NC 27699.1617
[A
Central Files Telephone [phone]
Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at;
[phone]
Permit Date 1011/2015 - 9/3012020
Last Revised 10-2-2015

Oldcastid'
Industrial Minerals
January 4, 2017
Department of Environment and Natural Resources
Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: APAC-Atlantic, Inc. — Fletcher Quarry
269 Fanning Bridge Road
Fletcher, NC 28732
Certificate of Coverage: NCG020167
Dear Sirs:
RECEIVED
.JAN 17 2017
CENTRAL F71LES
DVL'R SECTION
Attached is the annual 2016 stormwater discharge monitoring report for APAC-Atlantic, Inc. — Fletcher Quarry.
Table 1 summarizes the stormwater discharge quality parameters. Also attached are the supporting analytical
and sampling documentation.
The samples were collected on March 6, 2016, during a 'Representative Storm Event' from the outfall of the
detention pond that collects stormwater from roads and aggregate stone storage areas at the facility. The total
precipitation during the storm event was 0.82 inches. Based on an impervious drainage area of'273,840 square
Feet, the maximum total flow through the SDO-00I detention pond is 0.140 MG.
The stormwater discharge complies with the turbidity and total suspended solids benchmarks.
The stormwater pond has been re -configured so that it rarely discharges. The overflow discharge line was raised
several inches. Consequently, the pond did not discharge during the second semi-annual period from .tune to
December 2016.
Please contact Dan March of Pisgah Environmental Services at 828-768-3335 or via c-mail at Pisgah -
air c vt.edu if you have questions or comments concerning this report.
Sincerely,
APAC-Atlantic, Inc.
fck Owen
Plant Manager
Attachments: Discharge Monitoring Report
Analytical Report
Sampling Chain -of -Custody
639 Fanning Bridge Road • P.O. Box 218 • Fletcher, NC 28732
[phone] • [phone] fax

Table: 1. APAC-Atlantic, Inc. — First Semi -Annual Discharge Monitoring Summary — March 6, 2016,
Discharge Characteristics
Units
Results
March 5 2015'
Benchmark
Limit
Settleable Solids
m TIL
<0.1
0.1
Total Suspended Solids
m L
5.9
100
H
pH
8.3
>6.0; < 9.0
Turbidity
NTU
6.4
50
Total Rainfall
Inches
0.83
NIA
Event Duration
minutes
360
NIA
Total Flow
MG
0.140
NIA
' Pace Analytical Laboratories report.
APAC-Atlantic — Stormwater Discharge Monitoring

ANNUAL SUMMARY DMR - STORMWATER I
II SEND TO CENTRAL OFFICE * 11
STORMWATER DISCHARGE OUTFALLS (SDO)
GENERAL PERMIT NO. NCG020000
*Report ALL STORABI ATER Monitoring Data on this form (including No Flow and No Discharge and Permit Limit Violations) by .LIRCHJgf each year.
CERTIFICATE OF COVERAGE NO. NCG020167
FACILITY NAME: APAC-Atlantic, Inc
PERSON COLLECTING SAMPLES
CERTIFIED LABORATORYPace Analytical Lab # 040
Lab #
Part A: Stormwater Monitoring Requirements
SAMPLE COLLECTION YEAR: 2016_t
COUNTY Henderson I
PHONE NO. [phone]
ADD TO LISTSERVE? YES E NO ❑ EMAIL:
Outfall
No.
Date Sample
Collected
(mo/ddlyr OR
NO FLOW)'
In Tier 2
Monthly
�
Monitoring.
(y/n)
# of Months in
Tier 2
Sampling Z
Total Flow
(MG)
Total Suspended
Solids
(mg/1)
Turbidity
(NTU)
Settleable
Solids (mlll)
W,1
Rainfa I
(in)
Event
Duration
minutes)
-
-
-
-
-
1003,4
See Footnote','
0.13
SDO-1
March 6, 2016
No
NIA
0.140
5.9
6.4
<0.1
0.83
360
SDO-1
.Ian -June
No
N/A
N/A
NIA
N/A
NIA
NIA
NIA
NO FLOW
During
Second
Semi
Annual
Period
1\
PEE
TWTT-20i7
r'
-AtT0 n I .-
C
WR 11;E
�nJ
If`NO FLOW" or "NO DISCHARGE, linter "NO FLOW" or "NO DISCIiARGE" for each outfall here and the Date Range.
Z Per NCG02: Tier 2 Monthly sampling shall be done until 3 consecutive samples are below the benchmark or within the benchmark range
s If a value is in excess of the benchmark, or outside the benchmark range (for pl-1), you must implement the Tier 1 or Tier 2 responses in the General Permit.
TSS benchmark values are 100 mg/l except in ORW, I -I WQ, trout. and PNA waters where they are 50 mg/l.
'The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU fir freshwater streams, lakes, and reservoirs designated
as trout waters: 25 NTU for all lakes and reservoirs. and all salt waters: 50 NTU for all other streams and surface waters. Turbidity may be monitored at the SDO.
Alternatively, the permittee may choose to monitor turbidity in the receiving water. directly upstream and downstream of the SDO.
Permit Date: l71/2010-12/31/2014 Last Revised 02-02-11
Page I of 2

Part B: Vehicle Maintenance Activitv Monitoring Requirements for facilities using > 55 gal of new motor oil/month on average
Outfall
No.
Date Sample
Collected
(moldd/yr OR
NO FLOW)
In Tier 2
Monthly
Monitoring?
(yfn)
# of Months
in Tier 2
Sampling
New Motor
Oil Usage
at/month
Total Flow
(MG)
TPH using method
I664A SGT-HEM
m 11
Total Suspended
Solids
m /l
pH
(Standard
Units
Total
Rainfall
in
Event
Duration
minutes
_
_
153
1003'4
6_93
HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES
AT ANY ONE OUTFALL (INCLUDING VEHICLE MAINTENANCE)? YES [:IN 0
HAVE YOU CONTACTED THE REGION? YES [:]No ❑
WHO AT THE REGION HAVE YOU SPOKEN WITH?
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANYINFORMATION REPORTED:
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and comiDlete. Lam aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing
violati
�a C 4;
(Signature of Permittee) ( ate
Permit Date: 171/2010-12/31/2014 Last Revised 02-02-11
Page 2 of 2

aceAnalytical
www.pacelebs.com
� C C- o 3olG�
April 08, 2016 -
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: APAC 507010
Pace Project No.: 92292738
RECEIVED
JAN 17 2017
CENTRAL FILES
DWR SECTION
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. March:
Enclosed are the analytical results for sample(s) received by the laboratory on April 06, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
ptCREO�
TNI }
t�e4 Alt�Y
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 1 of 11

aceAnalyfical
www.pscelabs.com
Project: APAC 507010
Pace Project No.: 92292738
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
Asheville Certification Ids
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #; 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 11

Pace Analytical Services, Inc.
Riverside
aceMalytical ®
Asheville,
lle, NC 28804
WWW..paceh3b com
[phone]
ANALYTICAL RESULTS
Project: APAC 507010
Pace Project No.: 92292738
Sample: SDO1 Lab ID: 92292738001 Collected: 04/06/16 11:30 Received: 04/06/16 16:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 6.4 NTU 1.0 1 04/0711613:40
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 5.9 mg1L 2.5 1 04/07/16 17:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/08/2016 01:01 PM without the written consent or Pace Analytical Services, Inc., Page 4 of 11

m
aceAnalytical
www.pacelebs.com
QUALITY CONTROL DATA
Project: APAC 507010
Pace Project No.: 92292738
QC Batch: WET144068 Analysis Method: EPA 180.1
QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92292738001, 92292738002
METHOD BLANK: 1703916 Matrix: Water
Associated Lab Samples: 92292738001. 92292738002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 1.0 04107/1613:40
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 1703917
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Turbidity NTU 10 9.9 99 90-110
SAMPLE DUPLICATE: 1703918
92292736001 Dup
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 2.5 2.5 1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/08/2016 01:01 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11

e
aceAnalytical
�
www.pwolabs.com
QUALITY CONTROL DATA
Project: APAC 507010
Pace Project No.: 92292738
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 26804
[phone]
QC Batch: WET/44098
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92292738001, 92292738002
METHOD BLANK: 1704678
Matrix: Water
Associated Lab Samples: 92292738001, 92292738002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2,5 04/07/16 17:35
LABORATORY CONTROL SAMPLE:
1704679
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% ReC Limits Qualifiers
Total Suspended Solids
mg/L
250 258
103 90-110
SAMPLE DUPLICATE: 1704680
92292736001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
16.2
12.8 23 J(D6)
SAMPLE DUPLICATE: 1704681
92292587003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/08/2016 01:01 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11

0
aceAnalytical
~v..pacelabs.com
QUALIFIERS
Project: APAC 507010
Pace Project No.: 92292738
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration,
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory
control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/08/2016 01:01 PM without the written Consent of Pace Analytical Services, Inc.. Page 8 of 11

aoAnalytkal
www.pecelahs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: APAC 507010
Pace Project No.: 92292738
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92292738001
SD01
EPA 180.1
WET/44068
92292738002
MWO1
EPA 180A
WET/44068
92292738001
SDO1
SM 2540D
WET14409B
92292738002
MW01
SM 2540D
WET/44098
Date: 04/08/2016 01:01 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyfical Services, Inc..
Analytical
Batch
Page 9 of 11

9
I
Document Name:
Document Revised: 18FES2016
o
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
8CL'�illrilyf1C31
F-CHR-CS-003-rev.18
Pace Huntersville Quality Office
Page 2 of 2 for Internal Use ONt
•„ � � � • - Client fame: _ �O# • 9229
Project #: 2738
Courier; El Fed Ex ❑UPS ❑LISPS • ••._ Client
❑ Commercial ❑Pace ❑Other: 92
2r9r2738 j r rlj� I Jf f
Custody Seal Present? ❑Yes �No Seals Intact? Yes ❑No 7
Date/Initials Verson Examining Contents;
Packing IVlaterial: /❑Bubble Wrap ❑Bubble Bags None// ❑Other:
Thermometer: ❑ 1/RGun #5 SN: 15527198 ❑ Type of Ice; ON' et ❑Blue ❑None ❑Samples on Ice, cooling process has beg
Correction Factor: GVC Cooler Temp Corrected (°C): Biological Tissue Frozen? ❑Yes ❑No �j N/A
Temp should be above freezing to 6°C
USDA Regulated Soil (❑ N/A, water sample)
Did samples oyiginate in a quarantine zone within the United States: CA, NY, di -SC rn SC (check maps)? Did samples originate from a foreign source (inteally,
nYes o including Hav,,ali and Puerto Rico)? [{Yes VlNu
COMMENTS:
Chain ofCustod Present?
Des
[:]No
❑N/A
1.
Chain of Custody Filled Out?
es
_, No
❑
❑ N/A
2,
Chain of Custody Relinquished?
/
❑Yes
❑No
©N/A
3,
Sampler Name and/or Signature on COC?
41es
[-]No
❑DI/A
d.
Samples Arrived within Hold Time?
es
ON.
❑N/A
'S.
Short Hold Time Analysis (02 hr)?
ocs
❑No--�❑N/A
6. f 6�' -
Rush Turn Around Time Requested?
❑Yes
[ZN
N/A
7.
Sufficient Volume?
Y
❑Plo
❑N/A
S.
Correct Containers Used?
Ycss ❑No
❑N/A
9,
-Pace Containers Used?
12Z
❑No
❑N/A
Containers Intact?
F7rYes
❑No
❑N/A
10.
Filtered Volume Received for Dissolved Tests?
❑Yes
-❑Plo
N/A
11. Note ifsediment is visible in the dissolved container
Sample Labels Match COC?
EaYes
❑No
❑N/A
12.
-Includes Date/Time/ID/Anal sls Matrix:
All containers needing acid/base preservation have been
checked?
[]Yes13.
❑Pia
N/A
All containers needing preservation are found to be.in
compliance with EPA recommendation?
(FIN03, H2SO4, HCI<2, N@0H >9 Sulfide, NaOH>12 Cyanide)
❑Yes
OftN/A.
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLHg
❑Yes
❑No
j
Samples checked for dechlorination
Oyes
❑No '
M
14,
Headspace in VOA Vials (>5-6mm)?
❑Yes
._[]No
&A
15.
Trip Blank Present?
❑Yes
ONO
16.
Trip Blank Custody Seals Present?
Oyes
.❑Na
N/A
�'
-
Pace Trip Blank Lot# (if purchased):
'
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Resolution:
Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review;;Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a,,copy'of this form will be sent to the
out ofbold, incorrect preservative, out-hftemp, incorrecrcontainersl
Field Data Required? [-]Yes ❑No
161
i Carolina DEHNR
Office 0-•
Page 10 of 11

►r"?
-PaceAnalXical -
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -or -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page: of
Sectio A Section B ASection C
Requlrcd Infomlatiow Required Project Info aeon; Invoice informatian:
Company: Report To:A ARenlion:
a
2 045465
,
Addr
a U L
Gepy To:
Company Name:
R GULATCIRY AGENCY
` , LL
�/
Address'
7,kN9DES I— GROUNDWATER r DRINKING WATER
UST f RCRA f OTHER
Em To
urchase Order No.:
�o
l { L
It A
Pho e:
Fax: Project
Name:
Pum ProlCcl
Site Location
STATE:
Requested Due DatoITAT: Project
Number. `
l
Paw ProW s.
Requested
Analysis
Filtered
(YIN)
.
Section D Matrix Codes
z
z
RegvlrydC animfixirralmn NIATR1k r CODE
s
COLLECTED
Preservatives
Drinking Water DIN
0
zz
Waler WT
Waste Water WW
0POWE
m
rrte
COMPOSITE
NDIGnAa
w
Product P
UN
J
Z
soillsofrd SL
0N
r
SAMPLE ID Nape L
U
Of
w
WP
(A•Z, 0.9 f ;) Air AR
w
p
w
¢
n.
a
-a
ao
t
Sample IOs MUST BE UNIQUE Tissue TS
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ADDITIONAL COMMENTS
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DATE
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ACCEPTED BY I AFFILIATION
DATE
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-Impon.'uh Neic: By srgrtng this leer you.— aocepLmg Yace's NI! I :1U clzy payment terms and agreeing io Iola charges of 1.5% per month b—w?iffi rims eat pa,i urchin j*tays, F-ALL-I.}-ULUrev.Uf , l b-May-LUU f

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCGO20000
` Date submitted _March 1, 2016_
CERTIFICATE OF COVERAGE NO. NCG020000 SAMPLE COLLECTION YEAR 2015
FACILITY NAME _APAC — Fletcher Quarry�� SAMPLE PERIOD ®Jan -June ®July -Dec
COUNTY He
PERSON COLLECTING SAMPLES _Dan March
LABORATORY —Pace Analytical Lab Cert. # 40
Comments on sample collection or analysis:
or ❑ Monthly' month'
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
kelceIVED ❑Zero -flow ❑Water Supply ❑SA
MAR 0 7 2016 ❑Other
CENTP,AL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3
°wR sFCrroN
Part A: Stormwater Benchmarks and Monitoring Results
❑ No discharge this period?'
Outfall No.
Date Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH'
Standard units
Turbidity
Benchmarks =__>
-
-
100 mg/L or 50 mg/0
6.0 — 9.0
50 mg/L
SDO1
03/05
0.23
290
7.6
630
SDOi
04/06
0.36
102
7.2
34.5
SDO1
05/27
0.53
52.3
7.3
101
SDO1
06
Did not
discharge.
SDO1
07
SDO1
08
SD01
09
SDOI
10
SDO1
11
SD03
11/18
0.28
6.4
7.8
2.6
SDO1
12/16
0.33
6.9
7.2
3.9
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
Name (P nt name)
Aza,c17 /11.e r/6m
Tifle (Print title)
r� 3
(Sign re) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part 13: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy Of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signatu a of Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

aceAnalytical
wwwpacelabs.com
I
December 19, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: APAC 507010
Pace Project No.: 92280320
Dear Mr. March:
Pate Analytical Services, Inc.
2225 Riverside Dr.
Asheville, Nc 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
www.pace)abs.com
Project: APAC 507010
Pace Project No.: 92280320
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #; 356
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

A
aceAnalytical
www.pacefebs.com
SAMPLE ANALYTE COUNT
Project: APAC 507010
Pace Project No.: 92280320
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92280320001 SD01 EPA 180.1 BRJ 1 PASI-A
SM 2540D SAM 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc -
Page 3 of 10

aceAnalytical
www.pacefabs.com
ANALYTICAL RESULTS
Project: APAC 507010
Pace Project No.: 92280320
Paco Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sampte: SD01 Lab ID: 92280320001 Collected: 12/16/15 17:10 Received: 12/17/15 11:33 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 3.9 NTU 1.0 1 12/18/15 06:11
25401) Total Suspended Solids Analytical Method: SM 25400
Total Suspended Solids 6.9 mg1L 2.9 1 12/18/15 10A3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2015 06:17 AM without the written consent of Pace Analybeal Services, Inc.. Page 4 of 10

aceAnalytfica!
www.pacelabs,com
Project: APAC 507010
Pace Project No.: 92280320
QC Batch: WETI42054
QC Batch Method: EPA 180.1
Associated Lab Samples: 9228032CO01
METHOD BLANK: 1632422
Associated Lab Samples: 92280320001
Parameter
Units
Turbidity
NTU
LABORATORY CONTROL. SAMPLE: 1632423
Parameter
Units
Turbidity
NTU
QUALITY CONTROL DATA
Analysis Method: EPA 180.1
Analysis Description: 180.1 Turbidity
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 1.0 12/18/15 06:11
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82 B)254-7176
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
10 9.8 98 90-110
SAMPLE DUPLICATE: 1632424
92280321001
Dup
Parameter
Units
Result
Result
Turbidity
NTU
4.9
4.9
SAMPLE DUPLICATE: 1632425
92280422003
Dup
Parameter
Units
Result
Result
Turbidity
NTU
3.5
3.5
RPD Qualifiers
1
RPD Qualifiers
1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2015 06:17 AM without the written consent of Pace Analytical Services, Inc., Page 5 of 10

aceAnalXical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: APAC 507010
Pace Project No.: 92280320
QC Batch: WET142060 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92280320001
METHOD BLANK: 1632475
Associated Lab Samples: 92280320001
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE: 1632476
Parameter Units
Total Suspended Solids mglL
Pace analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 12/18/15 10:38
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 246 98 90-110
SAMPLE DUPLICATE: 1632477
92280196003 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 5.2 5.0
SAMPLE DUPLICATE: 1632478
92280201005 Dup
Parameter Units Result Result
Total Suspended Solids mglL ND ND
RPD Qualifiers
4
RPD Qualifiers
Results presented on this page are in the units Indicated by the "Unite" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12119/2015 06:17 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 10

aceAnalytical
www.pacefabs.ccm
QUALIFIERS
Project: APAC 507010
Pace Project No.: 92280320
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
OUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
X-1-Zil:Ltt91A149
PASI-A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2015 06:17 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

0
Y aceAnalytical
www.we)abs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: APAC 507010
Pace Project No.: 92280320
Lab ID
Sample ID
QC Batch Method
QC Batch
92280320001
92280320001
SD01
SDO1
EPA 180.1
SM 2540D
WET142054
WETI42060
Date: 12/19/2015 06:17AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„
Pace Analytical Services, Inc.
2225 Riverside Or,
Asheville, NC 288C4
[phone]
Analytical Method
Analytical
Batch
Page 8 of 10

o CHAIN -OF -CUSTODY ! Analytical Request Document
1 Analytical
The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fieldS must be completed accurately. o
,Face
-- ---
j�
Page: ` of j 0
Section A� \ Section B Section C
1 tCD
a__
Required C112 nlormation: Required Project Information; Invoice Information:
Company: !j I 11 9 Report To: 'I A Aron' 'iorr.
_
7 j,
,
Addrecad ;�
Copy To: r n ] I
Company Name:
REGULATORY AGENCY
t -
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Address:
—
NPDES GROUND WATER � DRINKING WATER
��j�'
;— us ; RCRA - OTHER
-
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Order No.:
p—
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Ratomnce:
Phone: t J>
Fax:
Project Name: 1
sue ProjectSite
Location
1
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STATE_
Roquestod Due DalerTAT:
Project Number: D
Paco Profile p:
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
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RoqulroOCfiont Information M.a"rRix r CODE
{
COLLECTED
Preservatives
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Dnnking Water DW
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Wdu Water WW
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ADDITIONAL COMMENTS
RELINQUISHED BY! AFFILIAT16N
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TIME
ACCEPTED BY t AFFILIATION
DATE
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SAMPLER NAME AND SIGNATURE !t
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SIGNATURE of SAMPLER: ��v�
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uocument +Name: Sariiple•Condition Upon Document Revised:'Noveriiber 06, 2015,
aceAn�iCal Receipt (SCUR Page 1 of 2``
Knenv.ryccoJa s.��, Document No.: issuing Authorities:
n F-ASV-CS-003-rev.1'5 Pace Asheville QuaI4 Office
Client Name: 1`5rkQ Page 2 of 2 is for Internal Use Only
Courier (Circle): Fed Ex UPS USPS <Client Commercial Pace Other
Custody Seal on Cooler/Box Present: E3 yes Quo eals intact: [3 yes [] no
Packing Material: Bub te_WA a� Bubble Bags LI No Other
Thermometer Used: Gun#5 - 155271998 Type of Ice: Wet Blue None omples on ice, cooling process has begun
_IR Gun #4.SN:140290365-----_—.._._ er:-•--_.._._r __ _..._.- -- -- -- --- - - - - -, - - -._... - -- -- — --
Temp Correction Factor: Add / Subtract 010 C
Corrected Cooler Tem 5-1-7 C
p"
Biological Tissue is Frozen: Yes No NIA
Date and Initials f perso ex
mining
Temp should be above freezing to VC
Comments:
contents;
Chain of Custody Present:
es
❑No
❑NIA
1.
Chain of Custody Filled Out:
es
❑No
❑NIA
2.
Chain of Custody Relinquished:
es
No
❑NIA
3.
Sampler fame &;signature on COC:
es
No
❑NIA
4,
Samples Arrived within Hold,Time:
es: ❑No
0i4m
5.
Short Hold Time Analisis <72hr :
s' ❑No ''dl%lm
6. '
Flush Turn Around Time Requested:
❑Yes
o
❑NIA
7.
Sufficient Volume:
❑ s
❑No
❑NIA
8.
Correct Containers Used:
a
❑No
❑NIA
9.
-Pace Containers Used:
C9Ye
ONO
❑N/A
Containers Intact:
Yes
❑No
❑NIA
10.
Filtered volume received for Dissolved tests
Dyes
No
❑ MIA
11.
Sample Labels match COC:
❑Y
❑No
❑NIA
12.
-includes date/time/ID/Anal sls Matrix:
All containers needing preservation have been chocked.
1114
ON.
❑NIA
13.
All containers needing preservation are found to be In
es
❑No
❑NIA
compliance with EPA recommendation.
exceptions: VOA, oollform, TOC, O&G, Wl-DRO (water)
❑Yes
t
Samples checked for dechlorinatic^:
❑` —
1`�":^
— =.,
' ^
_
Headspace in VOA Vials (>6mm):
Dyes
❑No
A
15.
Trip Blank Present:
[]Yes
❑No
A
.
Trip Blank Custody Seals Present
❑Yes
❑No
IA
Pace —Trip Blank Lot # (if purchased):_
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
preservative, out of temp, incorrect containers)
Field Data Required?
r)ateffime:
Wo":9226020—
Y / N
Page 10 of 10

i
ace Analytical
wnm.pacelabs.com
November 21, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: APAC 507010
Pace Project No.: 92276708
Dear Mr. March:
Pace Analytical Services, Inc.
2225 Riverside Or,
Asheville, NC 28804
(B28)254-7175
Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2015•
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
pCCgF����
i
TNI
{9eORACp
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyticai Services, Inc..
Page 1 of 10

l
aceAnalytical
wrwr.pacelabs.tom
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
CERTIFICATIONS
Project: APAC 507010
Pace Project No.: 92276708
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #; 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: EB7046
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except 0 Full,
without the written consent of Pace Analytical Services, Inc., Page 2 of 10

laneAnalyficalo
wwwpacelabs.com
SAMPLE ANALYTE COUNT
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92276708001 MW-1 EPA 180.1
BRJ
1
PASI-A
SM 2540D
MJP
1
PASI-A
92276708002 SDO-3 EPA 180.1
BRJ
1
PASI-A
SM 2540D
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

�IaneAnalytical"
www.pacetabs.com
ANALYTICAL RESULTS
Pace Analytic at Services, Inc,
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: APAC 507010
Pace Project No.: 92276708
Sample: MW-1
Lab ID: 9227670BOOl Collected:
11/18/15 10:05
Received:
11/18115 15:49 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
Dan March
1
11/20/15 11:07
Collected Date
11118M5
1
11/20/15 11:07
Collected Time
10:05
1
11/20/15 11:07
Field pH
7.7 Sid. Units
0.10
1
11/20/15 11:07
180A Turbidity
Analytical Method: EPA 180.1
Turbidity
3.7 NTU
1.0
1
11/20/15 06:03
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
4.3 mg1L
2.9
1
11/20/15 01:56
Sample: SDO-3
Lab ID: 92276708002 Collected: 11118115 10:10
Received:
11/18/15 15:49 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
Dan March
1
11/20/15 11:08
Collected Date
11/18/15
1
11/20/15 11:08
Collected Time
10:10
1
11/20115 11:08
Field pH
7.8 Std. Units
0.10
1
11120115 11:08
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
2.6 NTU
1.0
1
11/20/15 06:03
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.4 mglL
2.7
1
11/20/15 01:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/2112015 05:51 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 10

aceAnalyfical
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l
QUALITY CONTROL DATA
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QC Batch: WETl41519
Analysis Method:
EPA 180.1
QC Batch Method: EPA 180.1
Analysis Description:
180.1 Turbidity
Associated Lab Samples: 92276708001, 92276708002
METHOD BLANK: 1611533
Matrix: Water
Associated Lab Samples: 92276708001, 92276708002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Turbidity
NTU
ND 1.0 11/20/1506:03
LABORATORY CONTROL SAMPLE:
1611534
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Turbidity
NTU
10 10.1
101 90-110
SAMPLE DUPLICATE: 1611535
92276658001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Turbidity
NTU
1.0 .97J
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not 5e reproduced, except in full,
Date: 11/21 /2015 05:51 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: WET141517
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92276708001, 92276708002
METHOD BLANK: 1611498
Matrix: Water
Associated Lab Samples: 92276708001, 92276708002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 11/20/15 01:56
LABORATORY CONTROL SAMPLE:
1611499
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 238
95 90.110
SAMPLE DUPLICATE: 1611500
92276803001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
213
203 5
SAMPLE DUPLICATE: 1611501
92276711004 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
ND
ND
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/21/2015 05:51 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 10

aceAnalytical
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QUALIFIERS
Project: APAC 507010
Pace Project No.: 92276708
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pate AnolyRital Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21/2015 05:51 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

I
eAnalytical
—pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: APAC 507010
Pace Project No.: 92276708
Lab ID Sample ID QC Batch Method QC Batch
92276708001
MW-1
FLD/
92276708002
SDO-3
FLDI
92276708001
MW-1
EPA 180.1
WET141519
92276708002
SDO-3
EPA 180.1
WET141519
92276708001
MWA
SM 2540D
WET141517
92276708002
SDO-3
SM 2540D
WET141517
Date: 11/21/2015 05:51 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28844
(82B)254-7176
Analytical
Analytical Method Batch
Page 8 of 10

CHAIN -OF -CUSTODY 1 Analytical Request Document o
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 16
//!;7
Page: f
Section A f1t Section 6 n Section C
f 9
Required Cpen'Apformafttioon; Required Project InfofmatiOn: r Invoice Information:
Company: i `: r Report Tv:r ��� RttenJOn:
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1
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Address��,.`/p
Copy To:
Company Name:
REGULATORY AGENCY
'
Address:
} NPDES GROUND WATER - DRfNKING WATER
l UST RCRA OTHER
Em To: r i -
•�C' �� F I F,
PurchaOrder No.:
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STATE:
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Requested Due Date/TAT:
Project Number: �j "� `
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Requested
Analysis
Filtered
{Y/N)
Section D Matrix Codes
--
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e
COLLECTED
Preservatives
>
Drinking Water OW
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Water WT
Waste Water WW
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Sample IDs MUST BE UNIQUE Tissue TS
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RELINQUISHED BY 1 AFFILI ON
DATE
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DATE
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SIGNATURE of SAMPLER;' ATE Signed >
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'Important Now By signing this form you are accepting Pace's NET 30 day payment terms and agreeing W laic charges of 1.5% per month for any inL 1 F-ALL-4-020rev.07, 15-May-2007

.11
2ceAnalXlcale
Document Name: Sample Condition Upon
Document Revised: November 06, 2015
.
Receipt SCUR
Pa e 1 of 2*
Document No.:
Issuing Authorities:
F-ASV-CS-003-revA5
Pace Asheville Quality Office
Client Name:. % Page 2 of 2 is for Internal Use Only
Courier (Circle): Fed Ex UPS USPS C Client) Commercial Pace Other
Custody Seal on Cooler/Box Present: ❑ yes no�eals intacE: yes [] no
Packing Material: _Bubbi�e Vllrap—[Bubble Bags -2 Non R Other
Thermometer Us d: 1R Gunft5 155271998__ Type of Ice: Wet Blue None OlSernpies on ice, cooling process has begun
_-]R Gun.44.SNA40290365..__.-----Other:-.-_.. _ ...._----. __ __.__ ._.__....._ ___ --_. _ __... ..._----.-_•--•-—•—•------.__... _. _ __ ---
ITemp Correction Factor: Add / Subtract (")_' 0 C
Corrected Cooler Temp.: 1� . I C Biological Tissue is Frozen: Yes No NIA
Date and Initials of pers n ea amining
Temp should be above freezing to 6°C Comments;
contents: 1
Chain of Custody Present Des ❑No ❑wA
1.
Chain of Custody Filled Out: ©es ❑No ❑NIA
2.
Chain of Custody Relinquished: es ©No ❑NIA
3.
Sampler Name•& Signature on COC: ©es J3 No ❑NIA
4.
Samples Arrived within Hold Time: 0 es ❑No. •❑NIA
5.
Short Hold Time Analysis (<72hr): EaY s ` ❑No "❑NIA
6, T fL
Rush Turn Around Time Requested: Dyes ONO ❑NIA
7.
Sufficient Volume: 137es ON, ©N/A
8.
Correct Containers Used: es ON, ❑NIA
9.
-Pace Containers Used: os (hll ❑NIA
Containers Intact: CIA', ON, ❑NI ,'10.
Filtered volume received for Dissolved tests ❑yes ONo ' NIA
11.
Sample Labels match COC: ❑v s ❑No ©NIA
12.
-Includes datellime/1D/Analysis Matrix:
All containers needing preservation have been checked. pYes_❑No ❑NIA
13,
All containers needing preservation are found to be In El e" s ❑No ❑NIA
compliance with EPA recommendation.
exceptions: VOA, collfurn, TOO, OSG, WI-DRO (water) ©Yes ©NO
Samples checked for dechlorination: ❑Yes ❑No ❑qN
14.
Headspace in VOA Vials (>6mm): Dyes ONO NIA
5.
Trip Blank Present: Oyes ❑No
,NI.16.
Dyes ❑No 4CJN1A
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (ifpurchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution -
SCURF Review:
Data;
Date/Time:
SRF Review:1 IDate: ItIA111 '�
Note: Whenever there is ii discrepancy affectinqAofth Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office (i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
s
Field Data Required? Y / N
WO#:92276708
92276708
Page 10 of 10

r
ace Analytical
www.pacelabs.com
June 04, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
Dear Mr. March:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 27, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
2��P pCCRE�,��O
7NI J
9BORp�O�I/
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Page 1 of 10

I
e Analytical
—pacefabs.com
Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28904
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
Page 2 of 10

f
ace Analytical
wimpacelabs.com
SAMPLE ANALYTE COUNT
Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26604
(62a)254-7176
Analytos
Lab ID Sample ID Method Analysts Reported Laboratory
92251675001 SD01 EPA 180.1 JTJ 1 PAS I -A
SM 2540D WRC 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

aceAnalytical
_pacelabs.mm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
Sample: S001 Lab ID: 92251675001 Collected: 05/27/15 13:10 Received: 05/27/15 16:34 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 101 NTU 5.0 5 05/28/1514:20
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 52.3 mglL 8.3 1 06/03/15 17:01
Date: 06/04/2015 013:01 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 4 of 10

aceAnalytrcal
wtna.pscelabs.com
Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
QC Batch: WET137736
QC Batch Method: EPA 180.1
Associated Lab Samples: 92251675001
METHOD BLANK: 1469621
Associated Lab Samples: 92251675001
Parameter
Units
Turbidity
NTU
LABORATORY CONTROL SAMPLE: 1469622
Parameter
Units
Turbidity
NTU
QUALITY CONTROL DATA
Analysis Method: EPA 180.1
Analysis Description: 180.1 Turbidity
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 1.0 05/2811514:20
Spike LCS LCS
Conc. Result % Rec
10 9.8 98
SAMPLE DUPLICATE: 1469623
92251678001
Dup
Parameter
Units
Result
Result
Turbidity
NTU
3A
3A
SAMPLE DUPLICATE: 1469624
92251675001
Dup
Parameter
Units
Result
Result
Turbidity
NTU
101
102
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
% Rec
Limits Qualifiers
90-110
RPD Qualifiers
1
RPD Qualifiers
1
Results presented on this page are In the units Indicated by the" Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06104/2015 08:01 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

0
aceAnalyllcal
www.pacelabs.com
QUALITY CONTROL DATA
Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
QC Batch: WETl37855 Analysis Method: SM 25401)
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92251675001
METHOD BLANK: 1474289
Associated Lab Samples: 92251675001
Parameter
Units
Total Suspended Solids
mg1L
LABORATORY CONTROL SAMPLE: 1474290
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1474291
Parameter
Units
Total Suspended Solids
mglL
SAMPLE DUPLICATE: 1474292
Parameter
Total Suspended Solids
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 06103/1516:57
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 242 97 90-110
92251596001 Dup
Result Result RPD Qualifiers
NO ND
92251690001 Dup
Units Result Result
mg1L 9.0 8.6
RPD Qualifiers
5
Results presented an this page are in the units Indicated by the"Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2015 08:01 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 10

NI
eAnalytical
xnwvpacerahs.com
QUALIFIERS
Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDt_ - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit,
Paco Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a I of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/0412015 08:01 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnalytical
wwwpacefabs,com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: APAC Fletcher Quarry 507010
Pace Project No.: 92251675
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92251675001
92251675001
SD01
SD01
EPA 180.1
SM 2540D
WET137736
WET137855
Date: 06/04/2015 08:01 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 8 of 10

' !;P_AnaIvricaI
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
www.parelabt.cam
Cn
`e
Page: of M
5 Ion A Section B Section G
ReCL
g. Client InIbm% i Required Pira)ecLlnform Son:
F
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Report Attention:
�� Q _ -i^a
9 6 5 0
n o. �� f 1
Canrya �`Y�
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AddIS: 2-
copy To:
Company Name:
REGULATORY AGENCY
Address:
NPDES GROUND WATER :— DRINKING WATER
— ST j RCRA - OTHER
Email To:
Purchase Order No.: f
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Requested
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Filtered
(Y!N)
Section D Matrix Codes
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Raqutred Client lntermatien MATRIX r c00e
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Preservatives
Y
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Drinking Water DIN
O
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Water WT
Waste wamr VIMcos<aosrm
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ADDITIONAL COMMENTS
RELINQUISHED BV I FFILIATION
DATE,
TIME
ACCEPTED BY ! AFFILIATION
DATE
TIME1
SAMPLE CONDITIONS
19,71
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SAMPLER NAME AND SIGNATURE`„ {
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PRINT Name of SAMPLER-
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SIGNATURE of SAMPLER:
(A'TE S!lYYy:
C a
U
n : Dy sG'wv — loan yov .,ra acccP-0 Yaws Ne I as day paymcnl temps and agroctng to iato crarges or 1.59E per month for arty Nveices Mt paiC r ith. 30 days.. • s i--ALL-0-020rev.07, 1 5-May-2007

Document Name: Sample Condition Upon
Document Revised: May 15, 2015
aceAnalytical n
Receipt (SCUR)
Page 1 of 2'
Document No.;
Issuing Authorities:
vw.epac000s.cam
F-ASV-CS-003-rev.14
Pace Asheville duality Office
Client Name: r /] Page 2 of 2 is for Internal Use Only
�N
Courier (Circle): Fed Ex UPS USP Client, Commercial Pace Other
Custody Seal on Cooler)Box Present: ❑ yes ,-no SS als intact: yes [� no
Packing Material; Bbbp
Ifp Bubble Bags L� Non ther
Thermometer Use . l Gun03-�130265 G�� Type of Ic : Wet ue None amples on Ice, cooling process has begun
IR Gun #4 SN:14029036 t- 1M rr
Tema Correction Factor: Add ! Subtract
Corrected Cooler Temp.: 01? C
v Biological Tissue is Frozen: Yes No NIA
Date and Initials o pers n ex mini g
contents: 5 7.7 /S
Temp should be above freezing to VC
Comments:
Chain of Custody Present;
os No ❑NIA
1.
Chain of Custody Filled Out:
es iqo' ❑NIA
2.
Chain of Custody Relinquished:
M-r---ZlNo ❑NiA
3.
Sampler Name & Signature on COC:
es • No ❑WA
4.
Sam les Arrived within Hold Time:
M4,LDNO ❑NIA
5.
Short Hold Time Analysis (<72hr):
es ONO', - NIA
6.
Rush Turn Around Time Requested:
Dyes Na ❑WA
7.
Sufficient Volume:
os No ❑NIA
S.
Correct Containers Used:
w ❑No ❑N1A
9.
-mace Containers Used:
es No 0H/A
Containers Intact:
es ❑No ❑NIA
Filtered volume received for Dissolved tests
OyeVdN. PKA
11,
Sample Labels match COC:
grYas ©tllo ©NIA
12.
-Includes dateltime/1D/Anal sis Matrix:
/
All 'containers needing preservation have been checked,
es ❑No ❑NIA
13.
All containers needing preservation are found to be In
compliance with EPA recommendation.
es ❑No NIA
exceptions: VOA, coliform, TOG, C&G, WI•DRO (water)
DYes Q o
Samples checked for dechlorination:
IJYes ONO r 1A
A4.
Headspace in VOA Vials (>6mm):
11Yes ©No 174A
15.
Trip Blank Present;
❑Yes ONO21A
16.
Trip Blank Custody Seals Present
Dyes ❑No
Pace Trip Blank Lot # (if purchased):
Client Notificatlonl Resolution: Field Data Required? Y 1 N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:
Date:
SRF Review:[ 4r� IDate: 1 >1-2��
Note: Whenever there is a discrepancy affecting Nortg Carolina
compliance samples, a copy of this form wlll be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
WO# : 9225fl6'T5
HIM 6UIEII NMI911
Page 10 of 10

t
s
aceAnalytical
www.Patelabs.com
April 13, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: APAC-Atlantic 507010
Pace Project No.: 92244067
Dear Mr. March:
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 06, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
,,�.
Chris Derouen
[e-mail]
Project Manager
Enclosures
pCCRE�'TFO
s=
�TNI
lgeO`AE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
www.pacelabs.com
Project: APAC-Atlantic 507010
Pace Project No.: 92244067
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

i
aceAnalytfical
wm.paceWs.com
SAMPLE ANALYTE COUNT
Project: APAC-Atlantic 507010
Pace Project No.: 92244067
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92244067001 SDO-1 EPA 180.1 MAB 1 PASI-A
SM 2540D WRC 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuii,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

aceAinaiytical
www.welabs.com
ANALYTICAL RESULTS
Project: APAC-Atlantic 507010
Pace Project No.: 92244057
Pace Analytical Services, Inc,
2225 Riverside Or.
Asheville, NC 28804
[phone]
Sample: SDO-1 Lab lD: 92244067001 Collected: 04/06/15 14:40 Received: 04/06/15 15:16 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 34.5 NTU 1.0 1 04/07115 15:30
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 102 mg1L 12.5 1 04/07/15 19:30
Date: 04113/2015 08:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 10

acmnalytical
www.pacelabs,com
Project: APAC-Atlantic 507010
Pace Project No.: 92244067
QC Batch: WETI36666
QC Batch Method: EPA 180.1
Associated Lab Samples: 92244067001
METHOD BLANK: 1427949
Associated Lab Samples: 92244067001
Parameter
Units
Turbidity
NTU
LABORATORY CONTROL SAMPLE; 1427950
Parameter
Units
Turbidity
NTU
SAMPLE DUPLICATE: 1427951
Parameter
Turbidity
QUALITY CONTROL DATA
Analysis Method: EPA 180,1
Analysis Description: 180.1 Turbidity
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 1.0 04/0711515:30
Qualifiers
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
10 9.9 99 90-110
92244067001 Dup
Units Result Result
NTU 34.5 34.8
RPD Qualifiers
1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resuh,
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 04/13/2015 08:43 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

acmnaiytical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: APAC-Atlantic 507010
Pace Project No.: 92244067
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QC Batch: WETI36676
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92244067001
METHOD BLANK: 1428746
Matrix: Water
Associated Lab Samples: 92244067001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 04/07/15 19:24
LABORATORY CONTROL SAMPLE: 1428747
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 256
102 90-110
SAMPLE DUPLICATE: 1428748
92243921001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
363
354 2
SAMPLE DUPLICATE: 1428749
92244154002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
8.2
8.2 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/13/2015 08:43 AM without the written consent of Pace Analytical Services, Inc- Page 6 of 10

0
aceAnalytfrcal
ww6V.pace16b5.c0m
QUALIFIERS
Project: APAC-Atlantic 507010
Pace Project No.: 92244067
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chtoroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/13/2015 08:43 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
Project: APAC-Atlantic 507010
Pace Project No.: 92244067
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92244067001 SDO-1 EPA 180.1 WET136666
92244067001 SDO-1 SM 2540D WET136676
Date: 04113/2015 08:43 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 10

0
/ Face jT1' thH1-
,� e,rr,�n «m
CHAIN -OF -CUSTODY [ Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
\
Sectioq Section B F r Section C
Required Clie Information: Roquired Projec formalion:
Page: of
g
Q 8 D
.11 Invoice Informa6DA:
C"n,"nyl Rep" To: '�' I i� � Attention:
P� 1" VJ YC
v
AddresL,Y
CoTo:
Copy
Company Name:
REGULATORY AGENCY
%y� � (� - �
Address:
—
NPDES i GROUNDWATER r- DRINKING WATER
i UST RCRA OTHER
Email To: 1
Purchase Order No.:
D
Pace arose
Rererence:
Rq¢ne: f F
Project Name: l I. 3 j { !
a� i I :�TI�"
Pace Profect
n�.vlagac
Site Location
STATE:
r
Requested Due DateITAT:
Project Number. ]�
Pam Profilo a:
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
—
Z
RequIrodCliont Information MATRIX J CDC
o
2
COLLECTED
Preservatives
Drinking Water OW
g
U
z
o
Water N!T
Wasto WateW r W
B
b
cs
CO�I,?OSITE
ComROWLE
U
Product p
m
START
ENUGRAB
w
Z
Soillsofid SL
g
p
}
_
SAMPLE ID oil OL
�?
w
0
ipe
(A.Z. 0-9 i: ) Air AR
u'Q
w
Q
�
z
�
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,.
.6
Sample IDs MUST BE UNIQUE Tissue TS
0
U
a
Fd-
z
ro
N
Other OT
X
w
w
{
¢
LL
O
a�
c
O
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c
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N
m
—
y
DATE
TIME
DATE
TIME
m
#
a
2
2
T
Z
Z
O
-q
IX
Pace Project NoJ Lab I.D.
-
3
r
4
5
6
7
8
9
10
11
12
ADDITIONAL COMMENTS
RELINgUISHEO BY I AFFILIA-RN
a 1
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
9
SAMPLER NAME AND SIGNATURE
U
Cl) O',GNAL , S
o PRINT Name of SAMPLER: / 4
az
c
v `
m
DATE Signed !
. � ,
o SIGNATURE of SAMPLE - v I�nMrDDmi• q ! , �,`�
c
a
~
" _
c u
U m
co
S
y
•Isnponant NOLC: By vgn ng this farm you aro acmatng Palls NET 30 day oaymont tarns and agroorrg 10 lata chu6e5 of 1.5% per month fw any invoices no, paid within 30 aays. F-ALL-0-020rev.07. 15-May-Zvu l

11
01
to Ol" abed v
Document Name: Sample Condition Upon
Document Revised: June 10, 2014
ace Analytical
Receipt SCUR
Page 1 of 2
Document No.:
Issuing Authorities:
F-ASV-CS-003-rev.14
Pace Asheville Quality Office
Client Name:
1
Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Other
Custody Seal on CoolerlBax Present: yes noo Seals intact: [] yes no
Packing Material: Bubble Wrap Bubble Bags E N��Wt
Other
Thermo er-USed- lR Gun#3-130265963 Type of iceBlue None Samples on ice, cooling process has begun
IR G/ #4 5N:140290365 Other:
Tdmp-Cerrectiori-Factor. Add ! Subtract 0.0 C
Corrected Cooler Temp.: t"i c
Temp should be above freezing to 6°C
Biological Tissue is Frozen: Yes No NrA
Comments:
Date and Initials contents: f pe{r�son exE I`g�
(�
Chain of Custody Present:
Yes ❑No
❑NIA
1.
Chain of Custody Filled Out:
1244. ❑No
❑NIA
2.
Chaim of Custody Relinquished:
dye- ❑No
❑NIA
3,
Sam ler Name & Signature on COC:
EfYeVONo
❑NIA
4"
Samples Arrived within Hold Time:
Ye ❑No
❑NIA
5.
Short Hold Time Analysis (<72hr):
Yes DNo
NIA
6.
Rush Turn Around Time Requested:
Dyes No
❑NIA
7.
Sufficient Volume:
es qNo
❑NIA
8"
Correct Containers Used:
-Pace Containers Used:
D es ON.
❑ eY� No
❑NIA
❑NIA
9.
Containers Intact:
q. es ON
❑NIA
10.
Filtered volume received for Dissolved tests
Dyes 0 No
Dt�
11.
Sample Labels match COC:
-Includes dateltimellDlAna! sis Matrix:
es ❑No
❑NIA
12.
• • •
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation,
exceptions: VOA, coliform, TM O&G, Wt•DRO (water)
Yes ©No ONIA
L. 4/V DNo ❑NIA
Oyes M-o
13,
Samples checked for dechlorination:
❑Yes ❑No
NIA
44.
Headspace in VOA Vials ( >6mm):
❑Yes ❑No
NIA
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased):
❑Yes ❑No
❑vas ❑No
D IA
D !A
Client Notification! Resolution: Field Data Required? Y I N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:
Date:
SRF Review: & Date: 12t15
Note: Whenever there is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
WO#:92244067
11111H11111 I 111HH11
92244067

aceAnalytical
[ ..pacelabs.com
March 12, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: APAC 507010 3/5/15
Pace Project No.: 92239951
Dear Mr. March:
Pace Analytical Servlc@S, Inc.
2225 Riverside Dr.
Ashevi1e, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 05, 2015, The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
www.pacotabs.com
Project: APAC 507010 315115
Pace Project No.: 92239951
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

e
aceAnalylical
w wvpacelabs,com
SAMPLE ANALYTE COUNT
Project: APAC 507010 315115
Pace Project No.: 92239951
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92239951001 SDO.1 EPA 180.1 1 1 PASI-A
SM 2540D WRC 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

0
aceAnalytical
wwwpacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
(82B)254-7176
Project: APAC 507010 315115
Pace Project No.: 92239951
Sample: SDO-1 Lab ID: 92239951001 Collected: 03/05/15 14:15 Received: 03105/15 15:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 530 NTU 20.0 20 03/0611510:30
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 290 mglL 25.0 1 03/11/15 19A2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Tull,
Date: 03/12/2015 08:18 AM without the written consent of Pace Analytical Services, Inc„ Page 4 of 10

aceAnalytical
wwwpacelahs,com
1
QUALITY CONTROL DATA
Project: APAC 507010 315115
Pace Project No.: 92239951
QC Batch: WETI36059 Analysis Method: EPA 180.1
QC Batch Method: EPA 180A Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92239951001
METHOD BLANK: 1404584 Matrix: Water
Associated Lab Samples: 92239951001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 1.0 03/0611510:30
LABORATORY CONTROL SAMPLE: 1404585
Parameter Units
Turbidity NTU
SAMPLE DUPLICATE: 1404586
Parameter Units
Turbidity NTU
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
10 10.1 101 90-110
92240020002 Dup
Result Result RPD Qualifiers
3.1 3.1 2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/12/2015 08:18 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnalytical
www.pacelabs,com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Ashevi4le, NC 28804
[phone]
Project: APAC 507010 3015
Pace Project No.: 92239951
QC Batch: WET136146
Analysis Method: SM 2540D
QC Batch Method: SM 25400
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92239951001
METHOD BLANK: 1407858
Matrix: Water
Associated Lab Samples: 92239951001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 03/11/15 19:36
LABORATORY CONTROL SAMPLE: 1407859
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 270 108 90-110
SAMPLE DUPLICATE: 1407860
92239896002 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg1L
ND 26.0
SAMPLE DUPLICATE: 1407861
92239935001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg[L
86.0 94.0 9 D6
Results presented on this page are In the units Indlcated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03112/2015 08:18 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 10

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: APAC 507010 315115
Pace Project No.: 92239951
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detecticn Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW845 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260,
N-N itrosod iphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/12/2015 08:18 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

6
acMnalytrcal
wwwpacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: APAC 507010 315115
Pace Project No.: 92239951
Pace Analytical Services, Inc.
2225 Riverside Dr.
AsheWle, NC 28804
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92239951001
92239951001
SDO-1
SDO-1
EPA 180.1
SM 2540D
WET136059
WET136146
Date: 03/12/2015 08:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 8 of 10

,Q CHAIN -OF -CUSTODY 1 Analytical Request Document
FaceARalAiCal The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed am ratefy.
-- --------.---
Page: r of m
d
Sectio Section B Section C
!
1
, S I 8 3
Requir d CI' t information: Required Prej 3Son: Invoice Information:
'
Compel:`` xr,! Report To: C Attention:
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Copy To:
Company Name:
RE ULATORY AGENCY
7 LLC r
Addre:
ss
NPOES ! GROUND WATER ;� DRINKING WATER
_ UST I RCRA - OTHER
T4.5 J
�d
Purchase Order No.-
Pace Ouoto
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Raforonca:
P ne: Fax:
Project Name:
Site Location •, r n
ManagerManagerPace gecjefi
11,�I 11�I
STATE:
Requested Due Date1TAT:
Project Number: ^Q
Pace Prof,= M
Requested
Analysis
Filtered
(YIN)
-
section D Matrix Codes
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RoclulmdClient lnfonna5an MATRIX 0 cone
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Preservatives
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Drinking Water DW
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Waste Water WW
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ADDITIONAL COMMENTS
BY I AFfReAICON
DATE
TIME
ACCEPTED BY I AFFILIATION
D`AJTE
TIME
CONDITIONS
�tREutiOTSMED
C
,aSA,MPLE
SAMPLER NAME AND SIGNATURE
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PRINT Name of SAMPLER:
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SIGNATURE of SAMPLER: D
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'Important Note: By sig.-dng Nis form yom are =*pbng Paces NET 30 day payment lams and agreeing to lave charges of 1.5% per month far any inmates not paid within k days.` ( r F-ALL-Q-420rev.07, 15-May2007

aceAnalytical'
Document Name: Sample Condition Upon
Receipt SOUR
Document Revised: June 10, 2014
Page 1 of 2
Document No.:
Issuing Authorities:
F-ASV-CS-003-rev.14
Pace Asheville Qua;ity Office
Client Name: Pr'Sgj a tj
Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Other
Custody Seal on Cooler/Box Present: ❑ yes Q , o / Seals intact: �s ' no
Packing Material: Bubble Wrap Ej Bubble Bags `;1Y 0ne Other
Thermometer Used: IR Gun#3.130265963 Type of Ice: et Blue None mples on ice, cooling process has begun
IR un #4 SN:140290365 tither.
Temp Correction Factor: Add I Subtract C
Corrected Cooler Temp.:C
Temp should be above freezing to VC
Biological Tissue Is Frozen: Yes No Nr Date and Initials of parson examining
contents: 6„S L& 5
Comments:
Chain of Custody Present:
%T49 ONO
ONIA
1.
Chain of Custody Filled Out:
ITYe- ON--
❑NIA
2.
Chain of Custody Relinquished:
t Yas ON-
❑NIA
3.
Sampler Name & Signature on COC:
1
Dyes Duo
ONIA
4.
Samples Arrived within Hold Time:
E Yes ❑No
❑NIA
5.
Short Hold Time Analysis (<72hr):
fires ONo
❑NIA
6. d 6 r ( r
Rush Turn Around Time Requested:
❑Yes ®No
ONIA
7.
Sufficient Volume:
b-Y'.� ON.
ONIA
8.
Correct Containers Used:
-Pace Containers Used:
0Yes ❑No
8 es ONO
ONIA
❑NIA
9.
Containers Intact:
Yes ON-
ONIA
10.
Filtered volume received for Dissolved tests
0 Yes ON.
ONIA
11.
Sample Labels match COC: ©rise ON. ❑NIA
-Includes date/time/ID/Analysis Matrix: Gt. j
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compllance with EPA recommendation.
exceptions: VOA, colriorm, TOC, O&G, WI-DRO (water)
GaY4 ONO
B es ONO
CKes ONO
ONIA
ONIA
13.
Samples checked for dechlorination:
OYes ❑No
UWA
14.
Headspace in VOA Vials >6mm):
❑Yes ONO
12514-1A
15,
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased):
❑Yes ©No
❑Yes Ono
ILIA
EK/A
16,
Client Notification! Resolution: Field Data Required? Y I N
Person Contacted: Date[Time:
Comments/ Resolution:
SCURF Review:
Date:
SRF Review:1 �� joate: 1 r G
Note: Whenever there is a discrepancy affecting N&A Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Codification Office ( i.e out of hold, incorrect
preservative, cut of temp, incorrect containers)
`WO#:92239951
119119 BIIII�IBI BIII �I
Page 10 of 10

ANNUAL SUMMARY DMR - WASTEWATER I
II SEND TO CENTRAL OFFICE* II
PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All Wastewater discharge monitoring data on this form (including No Flow and Mo Discharge and Permit Limit Violations) by NbIRCH / of each year. if
you have limit violations, you must also have turned in a Limit Violation DMR to your local Regional Office within 30 da}>s of receiving sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG020000 SAMPLE COLLECTION YEAR: 2015
FACILITY NAME: APAC-Atlantic, Inc. COUNTY: Henderson
PERSON COLLECTING SAMPLES: Dan March PHONE NO. (_828)_684-6701
CERTIFIED LABORATORY:_ Pace Analytical Lab # 40 ADD TO LISTSF.RVE? YES ®NO❑ EMAIL: [e-mail]
Lab #
LIMIT VIOLATIONS? YES ❑ NO ® DUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS4? ❑
Part A: Wastewater Monitoring Reouirements
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids
'Turbidity'
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/l'-2
NTU,-'
mill,
Standard,
col/mlx,a
MW1
03/31/15
6.7
5.4
<0.1
8.3
MW1
05/07/15
4.7
<3.0
<0.1
8.0
MWI
No Flow Q3
.e.
MW1
11/18/15
3.7
4.3
<0.1
7.7
I
CF-NTRAL
CWR SECTIO
All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters_ Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms.
LJ
Permit Date: 1/1/2010-12/31/2014 Last Revised 02-02-1 1
Page 1 of 2

Part A Continued: Wastewater Monitoring Requirements
Outfall No.
Date Sample
CollectedI
Total Flow
Total Suspended
Solids'
Turbiditys
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
i1IG
mg/1',Z
NTU'3
ml/12
Standard'
col/m12"
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTI FICATION FOR ANY INFORMA TION REPORTED:
"l certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibili of fi s and imprisonment for knowing violations."
(Signajafe of Permittee) ( ate)
Permit hate: I/l/2010-12/31/2014 Last Revised 02-02-11
Page 2 of 2

acmnalytical
www.pacelabs.cam
November 21, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: APAC 507010
Pace Project No.: 92276708
Dear Mr. March:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28844
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
p[CRF�/��O
s �TNI
`RB�RAt�
REPORT OF LABORATORY ANALYSIS
This repert shall not be reproduced, except in fuii,
without the written consent of Pace Analytical Services, Inc -
Page 1 of 10

laceAnalytical
www.pacelabs com
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

rl-"Iacie AnalyticaI
www.pace)abs.com
SAMPLE ANALYTE COUNT
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID Sample ID Method
Analysts
Anatytes
Reported
Laboratory
92276708001 MW-1 EPA 180.1
BRJ
1
PASI-A
SM 2540D
MJP
1
PASI-A
92276708002 SDO-3 EPA 180.1
BRJ
1
PASI-A
SM 2540D
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

aceAnalytical
ww,xpacelabs.com
ANALYTICAL RESULTS
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-1
Lab ID: 92276708001 Collected: 11/18/15 10:05
Received: 11/18/15 15:49 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
Dan March
1
11/20/15 11:07
Collected Date
11/18115
1
11/20/15 11:07
Collected Time
10:05
1
11/20/15 11:07
Field pH
7.7 Std. Units
0.10
1
11/20/15 11:07
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
3.7 NTU
1.0
1
11/20/15 06:03
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
4.3 mg1L
2.9
1
11/20/15 01:56
Sample: SDO-3
Parameters
Lab ID: 92276708002 Collected: 11/18/15 10:10
Results Units Report Limit DF
Received: 11/18/15 15:49 Matrix: Water
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
Dan March
1
11/20/15 11:08
Collected Date
11118115
1
11/20/15 11:08
Collected Time
10A0
1
11/20/15 11:08
Field pH
7.8 Std. Units
0.10
1
11/20/15 11:08
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
2.6 NTU
1.0
1
11/20/15 06:03
2S40D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.4 mg1L
2.7
1
11/20/15 01:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/21/2015 05:51 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 10

� aceAnalytical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
OC Batch: WET141519
Analysis Method:
EPA 180A
QC Batch Method: EPA 180.1
Analysis Description:
180.1 Turbidity
Associated Lab Samples: 92276708001, 92276708002
METHOD BLANK: 1611533
Matrix:
Water
Associated Lab Samples: 92276708001, 92276708002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Turbidity
NTU
ND
1.0 11/20/1506:03
LABORATORY CONTROL SAMPLE:
1611534
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Turbidity
NTU
10
10.1
101 90-110
SAMPLE DUPLICATE: 1611535
92276658001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Turbidity
NTU
1.0
.97J
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented 10 the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/21/2015 05:51 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

� an Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: APAC 507010
Pace Project No.: 92276708
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: WET141517
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92276708001, 92276708002
METHOD BLANK: 1611498
Matrix:
Water
Associated Lab Samples: 92276708001, 92276708002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5 11/20/15 01:56
LABORATORY CONTROL SAMPLE:
1611499
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250
238
95 90-110
SAMPLE DUPLICATE: 1611500
92276803001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
213
203 5
SAMPLE DUPLICATE: 1611501
92276711004
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/2112015 05:51 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 10

acmnalytrcal
www.pacelabs.com
QUALIFIERS
Project: APAC 507010
Pace Project No.: 92276708
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N- Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21/2015 05:51 AM without the written consent of Pace Analytical Services, Inc- Page 7 of 10

aceAnalytical
f,
www.pacelabs.com
1
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: APAC 507010
Pace Project No.: 92276708
Lab ID
Sample ID
QC Batch Method
QC Batch
92276708001
MW-1
FLD/
92276708002
SDO-3
FLDI
92276708001
141W-1
EPA 180.1
WET141519
92276703002
SDO-3
EPA 180.1
WET141519
92276708001
MW-1
SM 2540D
WET141517
92276708002
SDO.3
SM 2540D
WET141517
Date: 11/21/2015 05:51 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Ashevilte, NC 28804
[phone]
Analytical Method
Analytical
Batch
Page 8 010

CHAIN -OF -CUSTODY ( Analytical Request Document
AnalyticalThe Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must de completed accurately.
0
0
rn
........--._......,..
Section A i'\ Section 6 Section C
Page: i at � rye
! t CIL
Required Ct.en)t n:orma:ion: Required Project Information: A A Invoice Information:
Company: t; / r A 1 Report To: � { / �/ 5 A 1 , ij Attention:
l
i l� F'Ck { t �rf 4n�
�
Address ' .. E
Copy To:
Company Name:
REGULATORY AGENCY
/
Address:
� is NPDES GROUND WATER _ DRINKING WATER
-i�S>
Y
UST RCRA OTHER
Em3'' To: r /
i ..�C' A V l F
Putclmse Order No.:
Z.%
Paw Quote
Rcterence:
Phdne:
ct Name: ' /
Pace Project
Site Location
f%
STATE:
Requested Due Data/TAT:
Project Number: ^"\
Pace Praara n:
Requested
Analysis
Filtered
(YIN)
Section D matrix Codes
a
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RaqulrodcuentInrcrr,ation MATRIX r enoe
;
COLLECTED
Preservatives
5-1
Drinking Water OW
o
Water WT
Waste Water WW
3
v
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COMPOSnE
srA-
COMPOWE
errwc�no
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Sample IDs MUST Be UNICILIE Tissue TS
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5
6
7
8
9
10
11
12
ADDITIONAL COMMENTS
RELIMDU,SHED BY! AFFI7 ON
A r[
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
r
TIME
SAMPLE CONDITIONS
(� SAMPLER NAME AND SIGNATURE }!
U
a
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S
• PRINT Name of SAMPLER: �� `?' I �L�'� (° j f
Q
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v
StGNATURE of SAMPLER: ATE Signed
��t._ r 7 /� �
x -`
G
a
y
4
�.� M,DD�Y�_
N
-Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late char9cs of 1.5% per month for any invoices not paid -i:4n 30 6ys. L 1 F-ALL-0-020rev.07, 15-May-2007

Document dame: Sample Condition Upon
Document Revised: November 06, 2015
�-2ct'Anaricale
Receipt (SCUR)
Pagel of 2""
Document No.:
issuing Authorities:
F-ASV-CS-003- rev, 15
Pace Asheville Quality Office
Client Name:. v Page 2 of 2 is for Internal Use Only
Courier (Circle): Fed Ex UPS USPS Client commercial Pace Other
Custody Seal on Cooler/Box Present: yes no�eals intacE: [� yes [] no
Packing Material: �l_-e-Wrayp—���Bubble sags •� Non E Other
Thermometer Us d: IR Gun# 5271998_a Type of Ice:( Wet Blue None0 Samples on ice, cooling process has begun
--IR.Gun#4.SN:140290365...._..._..._____Ofher. - - -...--................ ....-. _ _ ...._............. _.__...__.....-..-- - ._..._.,__._._........._ -........_................-------
Temp Correction Factor: Add 1 Subtract C
Corrected Cooler Tomp.: I C Biological Tissue is Frozen: Yes No NIA
Date and Init als of pers n e amining
Temp should be above freezing to 6°C Comments:
contents: 1
Chain of Custody Present: 0 es ❑No ❑NIA
1.
Chain of Custody Filled Out, ❑Yes ❑No ❑N1A
2.
Chain of Custody Relinquished: es ON. ❑NIA
3.
Sampler Name& Signature on COG: Des No ❑NIA
4.
Samples Arrived within Hold Time: O es ON. 0141A
5.
Short Hold Time Analysis <72hr : DY sW ❑No "ON1A
6. I'd fL
Rush Turn Around Time Requested: Dyes No ❑NIA
7.
Sufficient Volume: Gw"' ON, ❑NIA
8.
Correct Containers Used: [;[ es ON, ❑NIA
9.
-Pace Containers Used: EX,, ptao ❑NIA
Containers Intact: Cyr s ❑No ❑NI ,
`10.
Filtered volume received for Dissolved tests ❑Yes QNo NIA
11.
Sample Labels match COC: ❑Y s ❑No ❑NIA
12.
-Includes dateltime/]D/Analysis Matrix:
All containers needing preservatlan have been checked, ©Yes ❑No ❑NIA
13,
All containers needing preservation are found to be in [ 4:ONo ❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, o&G, Wl-DRO (water) ❑Yes ENO
Samples checked for dechlorinatian: Dyes ❑No 1❑�11K
14.
Headspace in VOA Vials ( >6mm): ❑Yes ❑No NL
5.
Trip Blank Present: ©Yes ©No t JN1A
16,
❑Yes ONO 45IA
Trip Blank Custody Seals Present
Pace Trip Blank Lot # if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Revi
Date:
DatefTime:
SRF Review:[_ :: [Date: 1, / �
Note: Whenever there is a -discrepancy affectin h Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( Le out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y 1 N
woa:e227e70e
1111119011111 IN Hill
92276708
1
r
3
Page 10 of 10

{
ace Analytical
www.pace)abs.com
May 13, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: Apac 507010
Pace Project No.: 92248812
Dear Mr. March:
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 07, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
PCCRF��r�G
TNI
��B�RASfl
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
vnwr,pacelahs.com
Project: Apac 507010
Pace Project No.: 92248812
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asnev0e, NC 28804
[phone]
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 2 of 10

m
ace Analytical
WWW..Pacelabs, corn
SAMPLE ANALYTE COUNT
Project: Apac 507010
Pace Project No.: 92248812
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92248812001 MW-01 EPA 180A TEP 1 PASI-A
SM 2540D 1/VRC 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

aceAnalytical
www'mcelabs.cam
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Apac 507010
Pace Project No.: 92248812
Sample: MW-01 Lab lD: 92248812001 Collected: 05/07/15 11:10 Received: 06/07/15 12:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 4.7 NTU 1.0 1 05/08/1512:55
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 3.0 1 05/12/15 18:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2015 03:42 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 10

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Apac 507010
Pace Project No.: 92248812
QC Batch: WET137332 Analysis Method: EPA 180.1
QC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92246812001
METHOD BLANK: 1454127 Matrix: Water
Associated Lab Samples: 92248812001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 1.0 05/0811512:55
LABORATORY CONTROL SAMPLE: 1454128
Parameter Units
Turbidity NTU
SAMPLE DUPLICATE: 1454129
Parameter Units
Turbidity NTU
Spike LCS
Conc, Result
10 10
92248919001 Dup
Result Result
ND 1.0
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
LCS % Rec.
% Rec Limits Qualifiers
100 90-110
RPD Qualifiers
Results presented on this gage are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05113/2015 03:42 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnalytical
www.pacafabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
QUALITY CONTROL DATA
Project: Apac 507010
Pace Project No.: 92248812
QC Batch: WET137406 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92248812001
METHOD BLANK: 1457017
Associated Lab Samples: 92248812001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE:
145701B
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1457019
Parameter
Units
Total Suspended Solids
mg1L
Matrix: water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 05/12/161828
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 252 101 90-110
922486800D1 Dup
Result Result RPD Qualifiers
ND 5.4
SAMPLE DUPLICATE: 1457020
92248771001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L ND ND
RPD Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0511312015 03:42 PM without the written consent of Pace Analytical Services, Inc- Page 6 Of 10

aceAnalytical
mw.pacelabs.com
QUALIFIERS
Project: Apac 507010
Pace Project No.: 92248812
91MIJ :lll1111W -",
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anaiytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2015 03:42 PM without the written consent of Pace Analytcai Services, Inc- Page 7 of 10

_I
eAnalytical
—pacefabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Apac 507010
Pace Project No.: 92248812
Lab ID
Sample ID
QC Batch Method
QC Batch
92248812001
92248812001
MW-01
MW-01
EPA 180.1
SM 2540D
WET137332
WET137406
Date: 05/13/2015 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Analytical Method
Analytical
Batch
Page 8 of 10

o�
.=Face Analytical'
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be Completed accurately.
Pago: of It a
Section Section 13 Section C
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1 0 �• � � 3
Required fe Information: Required Pr ' formalien: Invoice Information:
Company. Report To: AtteriGon:
`; l
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Copy To:
Company Name:
REGULATORY AGENCY
Address:
NPDES i GROUNDWATER - DRINKING WATER
UST :` RCRA OTHER
Esmj ttz _
PurctmaseOrder
Pace Quote
..
J1tt..]] J
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Project Name:
Paw Pr ct
Site Location
Manager.
STATE:
Requested Due Datai TAT:
Project Number.
Paco ?rofde z:
Requesters
Analysis
Filtered
(Y/N)
Soction D Matrix Codes
2z
RcquireaClient Inromwton _M.A,Tkix f C-OOF
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COLLECTED -
Preservatives
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ADDITIONAL COMMENTS
REL ]SHED BY t AFFI TION
DATE
TIME
ACCEPTED BY 1 AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
r
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_ SAMPLER NAME AND SIGNATURE
U
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SIGNATURE of SAMPL
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'rmponant Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to Mato charges of 1.5% per month for any invoices not paid mthin 30 days. / F-ALL-0-020rev.07. 15-May-2007 I

Document Name: Sample Condition Upon .
Document Revised: June 10, 2014
aceAnalyticalo
Receipt SCUR '
Page 1 of 2
Document No,:
Issuing Authorities:
/ P""o
F-ASV-CS-003-rev.14
Pace Asheville Quality Office
Client Name. Is G
Courier (Circle): Fed Ex UPS USPS CI e t Commercial Pace . Other
Custody Seaton Coofer/Box Present: yes no Seals intact: ❑ yes n no
Packing Material: 0 Bub6p- Bubble Bags None n Other 1r
Thermometer Used. Gun#3 •130265963 Type of ice: wet, Blue None Samples on Ice, cooling process has begun
IR Gun #4 SN:144290365 Other:
Temp Correction Factor: Add / SubtraCtU C
Corrected Cooler Temp.: L1 C
Biological Tissue is Frpzen: Yes Ito NIA
Dato and Initials of persop ex ninl�
l (�
Temp should be above freezing to 6°C
Comments:
contents:
Chain of Custody Present:
8 os o
❑NIA
1.
Chain of Custody Fillet! Out:
os_12N.
❑NIA
2.
Chain of Custody Relinquished:
©Yes o
❑NIA
3.
Sampler Name & Si nature on COC:
ETY. ON.
❑NIA
4.
Sam fes Arrived within Hold Time:
Yes No
❑NIA
5.
Short Hold Time Analysis (<72hr):
Yes DNo
PNIA
6.
Rush Turn Around Time Requested:
Dyes P o
©NIA
7.
Sufficient Volume:
Yes ONO
❑NIA
8.
Correct Containers Used:
Yeess ❑No
❑NIA
9.
-Pace Containers Used:
No
❑NIA
Containers Intact:
Yes ❑No
❑NIA
10.
Filtered volume received for Dissolved tests
Oyes - Pro
0 NIA
11,
Sample labels match COC:
Yos ONO
❑NIA
12.
-Includes date/time/1D/Anal sis Matrix:
All containers needing preservation have been checked.
es C]No
❑NIA
13.
All containers needing preservation are found to be in
lJXes L7Na
❑N/A
compliance with EPA recommendation.
exceptions: VOA, c6form, TOG, 0&G, Wi-DRO (water)
Dyes 12
Samples checked for dechlorination:
❑Yes ONO
a IA
14.
Headspace in VOA Vials ( >6mm):
Dyes ONO
IA
15.
Trip Blank Present:
Dyes ONO
NIA
Jr.
Trip Blank Custody Seals Present
Dyes ONO
IA
Pace Trip Blank lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review
Date/Time:
SRF Review:) joate: 31 /5
Note: Whenever there is a discrepancy affecting flofth Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( Le out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y , 1 N
[Wo 2248812 1
1922 681aaiiouii�n�o0u I

� f
aceAnalytical
wnnv.pacelabs.em
April 01, 2015
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
RE: Project: MW-1
Pace Project No.: 92243404
Dear Mr. March:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 31, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
=��Q accR�o�14 0
r
�TNI
CgBoL AI�l
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

T
aceAnalytical
—pacefabs.com
I
Project: MW-1
Pace Project No.: 92243404
Asheville Certification 1Ds
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #- 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 10

Pace Analytical Services, Inc.
aceAnalytical 2225 Riverside Dr.
' Asheville, NC 28804
www.pacefabs.ccm [phone]
SAMPLE ANALYTE COUNT
Project: MW-1
Pace Project No.: 92243404
Anatytes
Lab ID Sample ID Method Analysts Reported Laboratory
92243404001 MW-1 EPA 180.1 MLS 1 PASI-A
SM 2540D WRC 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fug,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 10

Pace Analytical Services, Inc.
�+O �7 /+� ® 2225 Riverside or.
aci AI laly itiGl Asheville, NC 28804
www,pacelabs-cam
[phone]
ANALYTICAL RESULTS
Project: MW-1
Pace Project No.: 92243404
Sample: MWA Lab ID: 92243404001 Collected: 03/31/1509:10 Received: 03/3111513:28 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
100.1 Turbidity Analytical Method: EPA 180.1
Turbidity 5.4 NTU 1.0 1 04/01/15 09:50
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 6.7 mglL 2.6 1 03/31/15 19:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04101 /2015 04:26 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 10

aceAnalytical"
WWW.Pacelabs.cam
QUALITY CONTROL DATA
Project: MW-1
Pace Project No.: 92243404
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: WET136553
Analysis Method:
EPA 180.1
QC Batch Method: EPA 180.1
Analysis Description:
180.1 Turbidity
Associated Lab Samples: 92243404001
METHOD BLANK: 1423939
Matrix: Water
Associated Lab Samples: 92243404001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Turbidity
NTU
ND 1.0 04/01/15 09:50
LABORATORY CONTROL SAMPLE: 1423940
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Turbidity
NTU
10 9.9
99 90-110
SAMPLE DUPLICATE: 1423941
92243307001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Turbidity
NTU
33.2 32.9 1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01/2015 04:26 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

ace Analytical
www,pacelabs.com
QUALITY CONTROL DATA
Project: MW-1
Pace Project No.: 92243404
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: WET136542
Analysis Method:
SM 2540D
QC Batch Method: SM 25400
Analysis Description:
2540D Total Suspended
Solids
Associated Lab Samples: 92243404001
METHOD BLANK: 1423828
Matrix: Water
Associated Lab Samples: 92243404001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Total Suspended Solids
mg/L
ND
2.5 03/31/15 18:56
LABORATORY CONTROL SAMPLE: 1423829
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 250
100
90-110
SAMPLE DUPLICATE: 1423830
92242659001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Total Suspended Solids
mg1L
ND
ND
SAMPLE DUPLICATE: 1423831
92243266001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Total Suspended Solids
mg/L
25.8 28.2
9 J(1)6)
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2015 04:26 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 10

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: MW-i
Pace Project No.: 92243404
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 6260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration,
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
J(06) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory
control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01/2015 04:26 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnalytical
www.pacerabs.cw
, I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MW-1
Pace Project No.: 92243404
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92243404001 MW-1 EPA 1 BOA WET136553
92243404001 MW-1 SM 2540D WET136542
Date: 04/01/2015 04:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 10

CHAIN -OF -CUSTODY ! Analytical Request Document
PaceAnalytical The Chain of -Custody is a LEGAL DOCUMENT- All relevant fields must be completed accurately. o
• waw,pdrela6s.cGm
c Se`�nn A Section 8 � Section C
ry
Page: ofno
RequlrkCkcnt Information: Required Project Information: � / invoice Information:
ReportTo:i f, ! Atten[ron:
18 181 'S 3�i
Ef ,�
1 f
_
AQer;�/-Y ! ! ,�V A ` I
Copy To:
Company Name:
REGULATORY AGENCY
�s
Address:
NPDES I GROUND WATER 7 DRINKING WATER
—
s T RGRA OTHER
Email To: I
Purchase Order No.:
Pax Ouo;a
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Phan .
7
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Project Name:
Pace Prgecc
Site Location
r
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Proje:I Number.
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Re-
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{YI
Section D Matrix Codes
2
RegolredClicrq Inbrmatim - MATRIX I CODE
o
COLLECTED
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i
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a
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$
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SAMPLE ID Oil OL
w
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p
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Sample IDS MUST BE UNIQUE Tissue TS
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Other OT
U
x
Z
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a
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p'
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DATE
TIME
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TIME
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ADDITIONAL COMMENTS
I11SHED BY! AFFIrLIA71�N
DATE
A TED BY 1 AFFILIATION
DATE
TIME
CONDITIONS)
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SAMPLER NAME AND SIGNATURE I
U
o
ORIGINAL
—
PRINT Name of SAMPLE
`
SIGNATURE of SAMPLE - / ,{ DATE Signed S; `
IiMM(DD/YYr
F
X -
U
N
i 1s Ai /f _
-Irnpo.tant NOW By syning this loon you are accepting Pacc s NET 30 day payment teantt and agreoing la iaW chatgOS or I.S% per month for any mveiCOS net paid wi&n S0 J : ` --%I_ / I F-ALL-0-02Crev,07, 15-May-2007

N
Document Name: Sample Condition Upon
Document Revised: June 10, 2014
�t"c?Ce/Inalytical'
Receipt SCUR
Page 1 of 2
Document No.:
Issuing Authorities:
rvww p.ncalnhs.com
F-ASV-CS-003-rev.14
Pace Asheville Quality Office
Client Name: P;sc i q
Courier (Circle): Fed Ex UPS USPS CIien" Commercial Pace Other
Custody Seal on CooterlBox Present: ❑ yes -n.�o/Seals intact: ❑ yes ❑ no
Packing Material: Bubble Wrap Bubble Bags LJ None Other
Thermom x d Gun#3-130265963 Type of Ice: Wet Blue None Q'Santples on ice, cooling process has begun
IR G�n SN:140290365 Other:
Temp C rrection-Fac Pon: Add I Subtract 0- O C
Corrected Cooler Temp.: 3. ] T C
Temp should be above freezing to 6°C
Biological Tissue Is Frozen: Yes No NIA
Comments:
Dato and Inrtials of person oxa Ining-
Contents: (LOP, 3
Chain of Custody Present:
Yes
❑No
❑NlIA
1.
Chain of Custody Filled Out:
es
❑No
. CI NIA
2.
Chain of Custody Relinquished: •
Q es 0No
❑NIA
3.
Sampler Name & Signature on COC:
E es ONO
❑NIA
4.
Samples Arrived within Hold Time:
❑ e
ON.
❑NIA
5.
Short Hold Time Analysts (<72hr):
Yes ONO
❑NIA
6.
Rush Turn Around Time Requested:
Dyes
EYNo
❑NIA
7.
Sufficient Volume:
MYes ONO
❑NIA
8.
Correct Containers Used:
-Pace Containers Used:
CKes
2j'e
©No
DNo
❑NIA
ONrA
9.
Containers Intact:
❑ es
ONO
❑NIA,
10'.
Filtered volume received for Dissolved tests
❑Yes_OND
EfNIA
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
Yes
ONO
❑NIA
12.
Ali containers needing preservalion have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, Wt-DRO (water)
J3Yes
es
❑Yes
ONO ONIA
❑No ONIA
/
❑N6
13.
Samples checked for dechlorinafton:
Dyes
ONO
14.
Headspace in VOA Vials ( >6mm):
❑Yes
ONO
qNIA
15,
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # ifpurchased):_
❑Yes ONO
❑Yes ONO
2 A
16.
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time-
Comments/ Resolution:
SCURF Review: Bate: IWO:9 : 92243404
SRF Review: Date: L::::]
I I jjI`
Note: Whenever there is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North i I I 11111 4� 111 iii I
Carolina DEHNR Certification Office ( i.e out of hold, incorrect 92243404
preservative, out of temp, incorrect containers)
Page 10 of 10

d ANNUAL SUMMARY DMR - WASTEWATER. !
` SEND TO CENTRAL OFFICE*
�CGI O �Q ( (� PROCESS MINE/DEWATERING WASTEWATER
GENERAL PERMIT NO. NCG020000
* Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH I of each year. If
you have limit violations, you must also have turned in a Limit Violation DMR to your local Regional Office within 30 days of receivine sample results from a lab.
CERTIFICATE OF COVERAGE NO. NCG020000 SAMPLE COLLECTION YEAR: _2014
FACILITY NAME: APAC-Atlantic, Inc. COUNTY: Henderson
PERSON COLLECTING SAMPLES: Dan March PHONE NO. (_828)_684-6701
CERTIFIED LABORATORY: Pace Analytical Lab #_PIV TO LISTSERVE? YES ® NO❑ EMAIL:
Lab #
LIMIT VIOLATIONS? YES ❑ NO
Part A: Wastewater Monitoring Requirements
N 0 V 0 5 14NDUSTRIAL SAND'? ❑ DISCHARGING TO SA WATERS49 ❑
CENTRAL FILES
M%A Ifn e-. ram .... _. _ . .
Outfall No.
Date SampIle
Collected
Total Flow
Total Suspended
Solids
Turbidity
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/1`,
NTU'-1
ml/lz
Standard'
col/ml'•'
M WI
02/18/14
4.5
4.5
<0.1
8.7
MWI
04/11/14
5.3
2.6
<0.1
8.3
M W 1
07/10/14
5.6
6.3
<0.1
8.3
M W l
10/09/14
12.6
15.7
<0.1
8.3
All mines must monitor W W discharges for TSS. Only industrial sand mine discharges are subject to TSS limits.
z If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term.
3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs
designated as trout waters: 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the
Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge.
' Only facilities discharging to SA waters are required to monitor for Fecal Coliforms.
.`
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cod
a'1111C
Pen -nit Date: 1/1/2010-12/31/2014
Last Revised 02-02-1 1
Page I of 2

Part A Continued: Wastewater Monitorine Reauirements
Outfall No.
Date Sample
Collected
Total Flow
Total Suspended
Solids'
Turbidity'
Settleable Solids
pH
Fecal Coliforms
-
mm/dd/yr
MG
mg/11,2
NTU2j
ml/lz
Standard
col/m12.4
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGiV THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature oflle-rmittee)
// - .1 ozy
(Date)
Permit Date: 1/1/2010-12/31/2014
Last Revised 02-02-1 1
Page 2 of 2

Y
aceAnalXical
vnrw.pecelaGs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82a)254-7176
ANALYTICAL RESULTS
Project: APAC 507010
Pace Project No.: 92190216
Sample: MW-1 Lab ID: 92190216001 Collected: 02/18/14 16:10 Received: 02/19/14 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 4.5 NTU 1.0 1 02/20/14 01:00
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 4.5 mg1L 2.7 1 02/25/14 15:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2014 02:01 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11

aceAnalyfrcal
www.pecelatu.mm
ANALYTICAL RESULTS
Project: Water 4111
Pace Project No.: 9217231
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW1 Lab ID: 9217231001 Collected: 04/11/14 10:00 Received: 04/11/14 13:17 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 2.6 NTU 1.0 1 0411611414:00
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 5.3 mg1L 1.1 1 04/16/14 19:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in foil,
Date: 04121 /2014 10:05 AM without the written consent of Pace Anatyttcal Services, Inc..
Page 5 of 9

aceAnalytical
www.pacelabs com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: APAC 7/10/2014
Pace Project No.: 92208939
Sample: SW-1 Lab ID: 92208939001 Collected: 07/10/14 15:10 Received: 07/11/14 11:11 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 166 NTU 10.0 10 07/11/1419:41
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 82.0 mg1L 8.3 1 07/17/14 17:30
Sample: MWA Lab ID: 92208939002 Collected: 07/10114 15:20 Received: 07/11/14 11:11 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
180.1 Turbidity Analytical Method: EPA 180.1
Turbidity 6.3 NTU 1.0 1 07/11/14 19:41
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 5.6 mg1L 2.6 1 07/17/14 17:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2014 05:13 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 10

aceAnalytical6
* waAc6abs com
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28864
[phone]
ANALYTICAL RESULTS
Project: MW-110/09/14
Pace Project No.: 92220906
Sample: MW-1 tab ID: 92220906001 Collected: 10/09/14 14:40 Received: 10/10/14 12:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
Dan March
1
10/14/14 08:39
Collected Date
10110/14
1
10/14/14 08:39
Collected Time
14:40
1
10/14/14 08:39
Field pH
8.3 Std. Units
0.10 1
10/14/14 08:39
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
15.7 NTU
1.0 1
10/10/14 16:00
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
12.6 mg1L
3.7 1
10/13/14 15:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/1412014 03:58 PM without the written consent of Pace Analytical Services, Inc..
Page 4 of 10

October 24, 2014
Department of Environment and Natural Resources
Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re:' APAC-Atlantic, Inc.
General Permit No. NCG020000
Dear Sirs:
Attached is the 2014 mine dewatering wastewater discharge monitoring report (i.e., four quarters)
for APAC-Atlantic, Inc. of Fletcher, NC.
Attached are the supporting analytical and sampling documentation. All sampled parameters are
within permit limits.
Please contact Dan March of Pisgah Environmental Services at 828-768-3335 or via e-mail at
Pis ah-air(@vt.edu if you have questions or comments concerting this report.
Sincerely,
APAC-Atlantic, Inc.
Greg Davis
Operations Manager
Attachment: Discharge Monitoring Report
Analytical Reports (4)
CC: Dan March, Pisgah Environmental Services
639 Fanning Bridge Road - P.O. Box 218 • Fletcher, NC 28732
[phone] - [phone] fax

Oldcastier
Industrial Minerals
October 24, 2014
Department of Environment and Natural Resources
Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: APAC-Atlantic, Inc.
General Permit No. NCG020000
Dear Sirs:
Attached is the 2014 mine dewatering wastewater discharge monitoring report (i.e., four quarters)
for APAC-Atlantic, Inc. of Fletcher, NC.
Attached are the supporting analytical and sampling documentation. All sampled parameters are
within permit limits.
Please contact Dan March of Pisgah Environmental Services at 828-768-3335 or via e-mail at
Pisgah -air c vt.edu if you have questions or comments concerning this report.
Sincerely,
APAC-Atlantic, Inc.
Greg Davis
Operations Manager
Attachment: Discharge Monitoring Report
Analytical Reports (4)
CC: Dan March, Pisgah Environmental Services
639 Fanning Bridge Road • P.O. Box 218 • Fletcher, NC 28732
[phone] • [phone] fax

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H

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
February 7, 2005
Bobby G Stevens
Fletcher Limestone Co Inc
PO Box 218
Fletcher, NC 28732
Subject: NPDES Stormwater Permit Coverage Renewal
Fletcher Limestone Co Incorporated
COC Number NCG020167
Henderson County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG020000 the Division of Water
Quality (DWQ) is forwarding herewith the reissued stormwater general permit. Please review the new permit to familiarize
yourself with the changes in the reissued permit. The general permit authorizes discharges of stormwater and some types of
wastewater. You must meet the provisions of the permit for the types of discharges present at your facility. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1981
The following information is included with your permit package:
• A new Certificate of Coverage
A copy of General Stormwater Permit NCG020000
• ' A copy of a Technical Bulletin for the general permit
• Five copies of Discharge Monitoring Report (DMR) Forms - wastewater and stormwater
Five copies of Qualitative Monitoring Report Form
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require modification
or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other
permits which may be required by DENR or relieve the permittee from responsibility for compliance with any other applicable
federal, state, or local law, rule, standard, ordinance, order, judgment, or decree.
If you have any questions regarding this permit package please contact Bethany Georgoulias of the Central Office Stormwater
Permitting Unit at [phone], ext.529.
Sincerely,
b"') 4L��� y
for Alan W. Klimek, P.
cc: Central Files
Stormwater & General Permits Unit Files
Asheville Regional Office
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617
Intemet: h2o.enr.state.nc.uslsulstormwater.html 512 N. Salisbury St. Raleigh, NC 27604
E D E `V' E i! 1'1 E
1
E E B 2 1 2005 0
WATER QUALITY SECTION
ASHEVILLE REGIONAI.OFFICE
NOnehCarolina
Nalituilly
Phone [phone] Customer Service
FAX [phone]
An Equal OpportunitylAffirmative Action Employer — 50% Recycled110% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES.
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG020000
CERTIFICATE OF COVERAGE No. NCG020167
STORMWATER AND PROCESS WASTEWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and
the Federal Water Pollution Control Act, as amended,
Fletcher Limestone Co Inc
is hereby authorized to discharge stormwater and to operate treatment systems and discharges associated
with mine dewatering wastewater and process wastewater from a facility located at
Fletcher Limestone Co Incorporated
639 Fanning Bridge Rd
Fletcher
Henderson County
to receiving waters designated as Kimsey Creek, a class C stream in the French Broad River Basin in
accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II,
III, IV, V, and VI of General Permit No. NCG020000 as attached.
This certificate of coverage shall become effective February 7, 2005.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day February 7, 2005
for Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

� I�x R �c�10L aIr t (a Ine
Manufacturers of bright white Calcium Carbonate
i y Alp E:
t q�
01

g�g ;
r
Tucked away in the mountains of the
southwestern part of North Carolina,
there is a small, elegant town called
°•''r:"'; - Fletcher. Fletcher is south
Asheville
_. and only a short distance from the
�rV ,
historic Grove Park -Inn and Biltmore
Estates. Just.b ne eath Fletcher's
surfs lies a deposit of white marble.
Geologically known as part of the
Murphy Marble Belt, which is a seam of
marble that runs from Alabama through
Georgia to North Carolina, this band
of marble received it's name because
of the exposure into the Murphy, North
Carolina region. The Fletcher deposit is
very unique for the color and location.
Glacier Stone
is a division of Fletcher Limestone
Company, Inc. and sits on
approximately 122 acres of scenic
landscaped mountain property.
Glacier Stone is a manufacturer
of coarse, medium and fine white
inert ground calcium carbonate
(CaCO3). These products are used
as fillers and extenders to make
other products such as rubber
or latex compounds stronger
and more cost efficient. Plastics,
paints, glass, carpet, cultured
marble and vinyl are just a few of
the products consumers use daily
which incorporate ground calcium
carbonate (GCC).
Glacier Stone currently has the
following product sizes available:
Glacier White 3 micron
Glacier White 6 micron
Glacier White U micron
Glacier White 22 micron
Glacier Stone is in the process of
installing a screening plant that will
enable us to produce another line
of products to be used in decorative
cement finish applications. It is
anticipated that these products will
be available in mid 2005.
ti►
Al

4W 0
Our History
Since the mid-1800's, the Fletcher marble deposit has been a valuable source of material
for a multitude of applications in both commercial and decorative markets. During these
times, the crude means of excavating were primitive at best. State-of-the-art equipment
consisted of a sure-footed mule hooked to a wooden cart and a man with a strong back
armed with a metal pick and shovel.
Fletcher Limestone was first incorporated in 1948. In the late 1970's, Bob Stevens, a
monument company owner from Mount Airy, North Carolina, purchased stock in Fletcher
Limestone Company, Inc. In the early 1980's, Bob and t
company. By 1999, Bob purchased the shares of his pE
Bob's main business philosophy has always been
"If it is not a good and fair deal for all involved, it
is not going to be a lasting business and therefore
not worth putting your time, effort and money into."
Today, Fletcher Limestone is a family operation.
Bob is semi -retired but comes to the quarry often.
His daughter, Barbara, is the Chief Financial Officer.
Barbara's husband, John Brooks, is the Chief
Operations Officer and Bob's son, Mark, is the
Assistant Executive Officer of the company.
Bob Stevens envisioned the untapped potential of
Fletcher Limestone, and has now made that
vision a reality by diversifying into different
markets. It is our goal to make Fletcher
Limestone a leader in the ground
calcium carbonate markets. Bob
believes that this endeavor
will be excellent for all
involved.
Our goal is simple
mane a consistent quality product that
will improve the value of the customers
product — and have that product there
when it is needed. We achieve this
goal with well -trained, dedicated and
experienced employees.

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