Loading...
HomeMy WebLinkAboutNCG020019_MONITORING INFO_20190212STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /v CC DOC TYPE. ❑HISTORICAL FILE i� MONITORING REPORTS DOC DATE ❑ � O� � � / a YYYYMMDD L ANNUAL ,SUMMARY M- WASTEWATER SEND TO CEIVTRAL OFFICE* RECEIVED 12 PROCESS MM/DEWATERING WASTEWATER $ 20d9 GENERAL PERMTT NO. NCG020000 CENTRAL FILES MLA", ..��— j * Report All Wastewater discharge monitoringdata on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH 1 of each y`eer: It you have limit violations _you must also have turned in a Limit Violation DMR to your local Regional Office within 30 days of receiving sample results from a lab. CERTIFICATE OF COVERAGE No NCG02 Q a 1 9 FACILITY NAME: COI m I g P, PERSON COLLECTING S AWLES- �r r c I�irres CERTIFIED LABORATORY: FAc—= ,xLLT ca.l Lab # f�7 Lab # L11 ITS VIOLATIONS? YES ❑ NO ❑ Part A: Wastewater Monitorhm Reauirements SAMPLE COLLECTION YEAR: COUNTY: rR4Mt; , A) PHONE NO. 9( 1 q ) LP — 3-7 ADD TO LISTERVE? YES El NO EMAIL: USt, r Bkmon►-t.�� INDUSTRIAL SAND'? KI DISCHARGING TO SA WATERS'? ❑ Outfall No. Date Sample Collected, 50090 Total Flow 00530 Total Suspended �. Solids 00400' Turbidlt3� 00545 Settleable Solids-,. 00400; p'S 31616 Fecal. Coliforme - mm/dd/yr MG aig/3 NTU ml/l Standard col/ml 63 0� �orF nj!✓ 1 nip 64,a a o 19 AID 71- M/91 arts j= 31.E /. AX -7 lie 'J-IJ r'a J 'a1A L2 001 .23,to 1.? WD 'Ali mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS bits. 2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term. 3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 1 t3 NTU for freshwater streams, lakes, and reservoirs designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt wafters; 50 N'TU for all other streams and surface waters. Turbidity may be monitored at the Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge. 4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms. I MAIA-11111 MnIA /` Last Revised 01-05-10 r- __. �.♦".Mrs � _� _I �'� • ----•tom-� - .. r. � }_ ,.t i __� .r -1 __- -w' •. •S _r.' .�,. i ' ` _ c .,.. * .: +" '1:" • i, , (� j Atli• a .. _ r t 1 ( aceAnalytical e www,p"Ahs.tom Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)8344984 Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92376380 Page 1 of 1 Report Date: 03/15/2018 Date Received: 03/09/2018 Sample: SITE 1 GP Lab ID: 92376380001 Collected: 03/07/18 15:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA 180.1 Turbidity 42.1 NTU 1.0 03113I18 03:59 H3 SM 2540D Total Suspended Solids 14.0 mg/L 2.0 03/13/18 19:45 D6 SM 254OF Total Settleable Solids ND mIJUhr 0.10 03/11/18 13:54 H3 EPA 9040 pH 6.9 Std. Units 0.10 03/12/18 12:25 H6 ANALYTE QUALIFIERS 06 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. H6 \Anaallysistinitiated outside of the 15 minute EPA required holding time. Reviewed by: - ' Terri Page (336)623-8921 terri.page@pacelabs.com Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NEL.AP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VrginiaNELAP Certification #: 460222 Page 1 of 4 document Name: Document Revised: February 7, 2018 Sampie Condltfan U an Reed t(SCUFt) Pa e i of 2 ��! • Document No.: Issufng Authotity: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Ht Client Name: -' adrG Courler: Ljted Ex OUPS IJSPS ❑ Commercial ❑Pate []Other:^ Custody Seal Present? ❑Yes [ko Seats intact? ❑Yes P�Qo WQ#9237s3— 9237 Datapnithls Person faumining ConUnts:��_ " Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑ other Bfologlcal Thsue Froxen7 Thermometer: Oyes ON" A VTIR Gun [D� Type of leer: Yet ❑glee []Nona Cooler Temp ('C): Q. Correction Factor: Add/Subtract (Y) d , Temp should be above freelfng to 6'C Confer Temp Corrected f'C): ❑Samples out of temp Criteria. Samples on lee, cadky proms has begun USDA Regulated Sall (kN/a watersamplef Did samples o f to n a quarantine cone within the United States: CA, NY, or SC (check maps)? Did samplas Wiginale from a ferelgn source (lnlem tfanaCy, f'Sv.� f : n t. ,Etta r,. .n, at n...,r., elmtr l- lv.. Wfun Cammena Dbtrr ant%: Chain of CusLadly present? RKU CINQ N/A 1 1. Samples Arrived wlthfn Hold rime? Ye tso I/A 2. Short Hold Time Analysts 01 hr.? Ne N/A 3. Rush Turn Around Time Re nested? es No N/A 4. Suf"clent Volume? Te Na N A $- Correct Containers Used? -Pica COAWhets Used? es ❑Na xo (]N/A r! A 6. COmainera intact? 1 Yes EIND [11YOL7. Dissolved ana Is: Samples Reid rlltered7 DY.1,No A 8. Sample Labels Match CDC? includes Date/nme/rD/Ana Is Matrlx: Yea 41% ON. ❑,J/A 4. Headspace In VOA Vlats {>S-6mm)7 Yu No rJ A 10, Trip Blank Present? trip Blank Custody Seals Present? ❑Yes UYes ❑No No N/A NIA 11. COMMENTS/SAMPLE DISCREPANCY 1 Field Data Requtrcd? ❑Yen ❑JJo Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: �� Date/Tfine: "Al Project Manager SCURF Revfaw: Date: 1 �� }_ r Project Manager SAF Revlaw; Date: r 1 Page 2 of 4 v ' ...-1'aceAaa44i al CHAIN -OF -CUSTODY I Analytical Request Document The CMi .o&Cusmdy ka s LEGAL DOCUMENT. AO rdamt 9dds must De rn PWW ecmmtdy. Sacdi A Section B Socuw C A-914.d Chem kd=00as P..q lmd Rgect k*X A on: W-im WA.T.6w- I:�.er. R.WT. 2056570 3ra++f it cr t-pY To: C—"-Y _ REGULATORY ACtNCY 1Si� l�C Z I S-Y9 Aet V (i I si r �S NPDES r GMUND WATER E- DMNKR4G WATER r UST f- RCRA r OTHER Ertl Tc �] ! Y te Vk&nf64'C .0 rnab: -�79y r (9 Y4(s-� 48 PmJee Nano site > ', S7AIE - Rapu-: d Due DaWTAT: Pe>)ea Mrraer. neo.e ":_ Reques&dMalyzEa - 9edion D M-&I- C-dft -ply Y Y MLLECTEo 1,f=r-w v S y ' Dm*rVWa Ow y➢y W> ., W.w u V e m COH`Orfif. Y PrCfuct P T C cop p c' yy ., Z •� i� V SAMPLE I0 �_ S W vYvoe ,°4,P (A,Z. 0.9I 1 Ad AR a Z F SOrtpM db MIST BE 11NIOUF. ?W 0 Dow OTS T u $~ o e N Z U a 4 tQ 'WINE� et { DATE Tax PAW Te1E O r ¢ ?rce Projtxt No./ LO. L s s T 9 10 tt 13 AODITIDNAL COMMENTS RElMOUCHED 8Y l AFFOJATION DATE TIME my AFF1WT'IOM DATE T= AM SPLE CONDRIDRS r ltrae4e - rvo d. Y SA►�LEH NAME AND SIGNATURE �Z^ �RI�I�a� /Rwr N} of SAMPLER: SIGNATURE of SAN:PLER: DATE WW" rc H N Twprae Nib- e'!>L N W'ella r• mpsi Paati {� ]0 eF PY+re MC esjwlq b bN dlrpee tS1L lW n'Anl1 Ix an1'in.der res NIG wOiit S7 asya h-.ALL•UO2(IfeV A7, 15-MOy-ZCP7 Document Document No.: 'Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Collform, TOC, Oil and Grease, ORO/8015 (water) DOC, LENS "Bottom half of box Is to list number of bottle Page 1 of 2 Issuing Aothorlty: WOE 92376380,. , L- . PM TWO F Due Dare° CLIENT: 91-Waday son ON oil I ONE ML SOMMOMMEN MINOR SEEMS pH Adjustment Log for Preserved Samples sample 10 1 Type of Presemdve pN upon nnipt Data preservation adjusted Time preservation adjusted Amount of Preservative added Lot e Note; Whenever there Is a dlsttepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina MUIR CerCfkatlon ONt s (I.e. Out of hold, Incorrect preservaave, out of temp, incorrect containers. Page 4 of 4 /ro? /�,FaceAnalytical ' amr-oacelahs-com CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section 8 Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: r Report 70: Attention: � / 2056570 tiV� ffJU:LJIti'! J.iukC�t"t^ �ftf CY{ Address: -y r,r' I' Copy To: Company Name: CO REGULATORY AGENCY I In R 4AIr.- f 014I'V M41,04 - 119 Address: V.I)- i:i C 1 f (r„ _ko a, Af j7 N P D E S f— GROUND WATER r DRINKING WATER j- UST r RCRA r OTHER Email To: e1/ , t Purchase Order No.: Pace Quote Reference: Phone: Faz: ProeCl f 9 -7 1 `t r� r/7 ' +F i Name: Pace Project I Site Location 1 fA tl9L 7e �i ' L 1 Manager: STATE: Requested Due DaterrAT: Project Number: Pace Profile a: Requested Analysis Filtered {YIN) Section D Matrix Codes COLLECTED 7 1 Required Client Information MATRIX t COOF Drinking Water UW O v Preservatives i J ` Water WT Wastewater WW m COMPOSITE COMPOSITE LD W Prod UCt p m START ENDIGRAR Z SoillSolid SL N q co SAMPLE ID Oil OL 1 F w Wipe WP (A-Z, 0-91;) Air AR p -" w 4 o_ z y _o Sample IDs MUST BE UNIQUE Tissue TS O a- 2 w H +� ou _ t Other OT U x w J z Ov a) p 21 �! m CL O O =O . N 2 ¢ a c z U m m Q t, t s m — < DATE TIME DATE TIME m � Z) 2 = = z z M O If Pace Project No./ Lab I.D. t 7,-4 P 1 07 P C; 2 3 -4 5 6 7 8 9 10 11 121 --- H-1 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE 'TIME _ f f ACCfr2D 8Y 1 AFFILIATION i DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE o m I c 0 a o r c PRINT Name of SAMPLER: E o} o v Z } z ' m ~ m — L) Ts a> E SIGNATURE of SAMPLER: DATE Signed (MMIDDIW}: in *Important Nola: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid wthin 30 days. F-ALL-0-020rev.07, 15-May-2007 Instructions for completing Chain of Custody (COC) I . Section A and B: Complete all Client information at top of shut: company name. address, phone, fax, contact (the person to contact if there are questions, and who will receive the final report.), e-mail address (if available), 1'0#, Project Name andlor Project Number as ynu would like; to see it appear on the report. 2. Section C: Invoice: Information: Billing information is included in this section. This infonnation should include the name and address of the person rc;ceiviDa the invoice. 3. Quote Reference should be completed if quotation was provided by face Analytical. Thu Project Manager, and Profile No. will be completed by Pace Analytical Services. 4. Site Location: A separate COC must be filled out for each day of sample collection. Record the two letter postal code: for the US state in which the samples were collected. 5. Regulatory Aeency: List the; program that is guiding the work to ensure proper regulations arc followed. 6. Section D: Complete a Sample Description in the "SAMPLE ID' section as you would like it to appear on the laboratory report. The following information should also be included: the sample matrix, sample type (G (grab) or C (composite). When collecting a composite, the start time and end time should be documented in the respective boxes. The collection time for a grab (G) sample should be entcrcd in the boxes marked `Composite End/Grab'), Sample temp at collection (if required by state), the total number of containers_ and preservative: used. Mark if the sample; was filtered in the field by marking Y or N in 'Filtered' row by the Analysis requested. S. Requested Analysis: List the required analysis and methods on the lines provided and place a check in the column for the: samples requiring the analysis. Additional comments should be referenced in the bottom left hand comer or include; attachments for extended lists of parameters. 9. The sampler should print their name in the space provided and sign their name followed by the date of the sampling event at the bottom of the COC in the spaces designated for `SAMPLE R NAME AND SIGNATURI '. 10. When relinquishing custody of the samples to a representative of the laboratory or other organization, indicate the Item Numbers of those samples being transferred; sign relinquished by, date and time, and include your affiliation. *Important Note: Standard Turnaround Time is 2 Weeks110 business days. Results will be delivered by end of business on the date due unless other arrangements have been made with )'our project manager. Special Project Requirements such as Low Level Detection Limits or level of QC reported must be included on the chain of custody in the Additional Comments section. c`eAnalytical www..pac9W&cam Pace Analytical Services, LLC 6701 Conference Drive Raleigh. NC 27607 (919)834-4984 Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92376380 Page 1 of 1 Report Date: 03115/2018 Date Received: 03/09/2018 Sample: SITE 1 GP Lab ID: 92376380001 Collected: 03/07118 15:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA 180.1 Turbidity 42.1 NTU 1.0 03/13/18 03:59 H3 SM 2540D Total Suspended Solids 14.0 mg/L 2.0 03/13/18 19:45 D6 SM 2540F Total Settleable Solids ND mL&ffir 0.10 03111/18 13:54 H3 EPA 9040 pH 6.9 Std. Units 0.10 03112/18 12:25 H6 ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. \'� Reviewed by: y Terri Page (336)623-8921 terri.page@paoelabs.com Asheville Certification IDa 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification # E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginialVELAP Certification #: 460222 North Carolina Drinking Water Certification M 37712 Page 1 of 4 a 0 Laboratory receiving samples: Ashev(jje0 Eden[] Greenwood ❑ Hunte�� • ,` Pit-n Client Name. ` `,r:4923763 ` proi j Courier. Fed Ex ❑UPS LIUSPS ent.. � �,•�� f ; ��� F is ` I h ❑ Commercial ❑Pace ❑otheri° 9 376360 r 1 r Cattm* Seal Present? []Yes (ko Seats fntad? []Yes Date/Inittall Pawn Examining Caaunts:�`�_ Paddng Material: ❑Bubble Wrap ❑Butsble Sags None ❑ other Biological Tlsule Frozen? Ther, bier, g 9 ,` ❑Yes ❑No A AIR Gun ID: ier ` 9Z TYPe a} foe: tYet Oak. ©MOM Confer Tamp ('C): O. D Carrecdon Fader, Add/Subtract ('Cj , � � Temp should be above freezing to WC Cooler Temp Corrected (%I: ❑Samples out of tamp craeda. Samples on Ice, mown ptocess has begun USDA Regulated sail OZ N/A, water sample) OW samples oagl�gte n a grarantlne zone within the UORed States: CA , NY, or SC (check maps)? old samptas adgtrute Irana }creign smote (Inter tionaCY, DYes indWLna HawaR and Puetta Ricoll FITu No Commence Discre ancY: Chain of Present? Ores ONO NA I. Samples Arrived whhln Hold Time? Y Io OWA 1. Short Hold Tine An <72. hr, ? es ON., A 7, Rusk Turn Around the Requested? rg to nW. 4. SufRcknr Vohanc? Na ONIA S. Correct Contalnan Used? -Pace Conwnert Usedt as []No 13HO [JN/A OHIA 6. Containers tntact7 OW& 7. Dissolved ana es field Flhsred? Y No A & ' Sample Labels Match COO -indudes oate/nmeAP/j Matti= Yes+ (7� Ono ❑n/A 9- Headspace in VOA Vlah (A-6mm)T Oyu 140 ! A_ ID, Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes ❑tfa No N/A N!A fl. COMMENR/SAMPLE DISCREPANCY ,e, r t'— I FWd Data Rayulred? ❑Yes ❑No 0s3 f/ r `pus a� �?';?L�j r Lot 10 of spilt containers: tLIENT NOTIFICATION/RESOLUTION Person contacted: Date/rmm Project Manager SCURF Revlaty Date. y I f 44 Project Manager SRF Review: Date: r 1 I Page 2 of 4 'Cr 0 :' ,.. •i"dCB,411d1ytiCc?!' CHAIN -OF -CUSTODY 1 Analytical Request Document �x a,.a+acc„:may b. you oocuu>:wr. n. fdcr„u fdtl. muu w mmq�ea .�.sco�,. 2056570 .t e . i. SwMw , on CL CYT ®e�©©■■■�i■■■ ■■■ eOWN ■��i■�ie�■■■■■■�i ■■■■■■■■■■■■i e ■■■■■■■■■e■�■■■■■■■■ ■■■■■■■■■■■■■ MEMO NONE e ■■■■■■■■■■■■■■■■ ■■■■■■■■n■■■■ e ■■■■■�■■■■�e■■■■■■■■■ ■■■■■■■■■■■■■ MEMO! MEMO! NONE e ■■■■■■�■■■e■■■■■■■■■ ■■■■■■■■■■■■■ e ■■■■■■■■■r■■■■■■■■ ■■■■■■■■■■■■■ MEMO! NONE m ■■i■■■■■■■r■■■■■■■■■■ ■■■■■■■■■■■■■ MEMO! MEMO! SOME m ■■■■■■■■m■■■■■■■■■■ ■■■■■■■■■■■■■ MEMO! � SOME •L ion .wdrlhw�n.•� rw>w ay.aruEr�ae.,ew*.�.r+e.na.a..:gawcmwd+57a.�mb+nrbabm=wn.ew..wp jF aomw.or.tsumr2onr Document Name: Document Ne.: 'Check mark top half of box If pH and/or dechlorination Is ved led and within the acceptance range for preservation samples. Smcepdanr. WDA, Colrfor% rOC, OII end Grease, ORQ/GGIS Iwatell OOC, L ft '•Bottom half of box Is to list number of bottle Document Revised: February 7.2018 Page 1 of 2 UNIUii0►130 soil iE� aii MENii► Ilk EMOMMEMOVEM's pom pH Ad)ustment Log for Preserved Samples Samoa to Two of Presatrathq pN "Pan renlpt Oath prewrvatlan adjusted Thne preservatloe adiusted Amount of Prawmafivt added Lot e Note: Vyhenemt there e a hlscrepaner aRnihsg North fStolrta compliance samplas, a ropy of thin form wi l be sent to the North Cetonna OEHNA Certlnrannn O9ke [La. Out of hold, kwweel preaemtNe, out of temp, btcerren mn.alnars. Page 4 of 4 "' - '. h ,./�face Analyfical- wong.oacelabs.earn CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody Is a LEGAL. DOCUMENT. All relevant folds must be compleied accurately, Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company. Report TO: Attentiom, 2056570 r Address; Copy TO: Company Name; REGULATORY AGENCY Address: V NPIDES F GROUND WATER F- DRINKING WATER r— UST F RCRA F- OTHER Email To: �urchdlse Order No.: Pace Quale Reference: Phone., Fax: Project Name: Pace Project Site Location I Manager I STATE: Requested Due Date/TAT: Project Number: Pace ProMs Requested Analysis Filtered (YIN) Section D Matrix Codes V 0. z Required Client Information MATRIX f CODE Drinking Water DW M 0 0 11 COLLECTED z 0 Preservatives i- Water WT Wastewater Ww L) to 00mPOSME COMPOSITE l'- Product P 9 START ENINGRAB Lu —1 Soll/Solid SL 0 -J to SAMPLE ID Oil Ol 6 Wipe W? (A.Z. 0-9 1.-) Air AR LU — :L Z to to H-r- 0 Sample lDs MUST BE UNIQUE TISSUe TS 0 0 Lu & 2 Xt Other OT 5 X W Lu 7- 0 'Fa LL 21 C5 a: U) 0 CL r- z 0 cc 4' d) ;E� r 5 a) DATE TIME DATE TIME U) 4 =) = Z: z z 2 0 ♦ -7, Pace Project No./ Lab I.D. I k 2 3 -4 7 10 17 121 1 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ,,ED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS I-) "fVV--e-- 'Y"?Ilf 1 (5-10 jP e- -e— SAMPLER NAME AND SIGNATURE C —Z PRINT Name of SAMPLER: 0 3�- �p >- DATE Signed SIGNATURE of SAMPLER: E 9 � Ir 3 — a — S W _J (MMMDrfY): 0 'Important Note: By signing thig term you Ons aCcOpurg Pam's NET 3D day payment lerms and agreeing to late charges of 1.5% per month for any Invokes not pa9d within 30 days. . F-ALL-Q-020rev,07, 15-May-2007 aceAnalytica! www.P8rC1Phs.cnm I Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NO 27549 Project: WADE MOORE EQUIPMENT C0 Pace Project No.: 92389780 Sample: SITE 1 GP Method Parameters SM 2130B Turbidity SM 2540D Total Suspended Solids SM 2540F Total Settleable Solids EPA 9040 P11 ANALYTE QUALIFIERS Laboratory Report Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)B34-49B4 Page 1 of 1 Report Date: 07/02/2018 Date Received: 06/26/2018 Lab ED, 92389780001 Collected: 06/26118 06:30 Matrix: Water Results units Report Limit Analyzed Qualifiers 5.7 NTU 0.50 06127/1813:30 6.2 mg1L 2.5 0612711816:53 ND mill-!hr 0A0 0612711813A0 7.6 Sid_ Units 0.10 06/29/18 15:12 H1,H6 Hi Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by:� pv— Terri Page (336)623-8921 terri.page @pacelehs.c0m Eden Certification 109 205 Fast Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 Virginia/VELAP Certification #: 460025 Page 1 of 4 �Y., acr�AflalL4rL:ir! --- iaboratary recatuing samples: AslievlRe U Eden❑ 0ofurnem Mime..: Dorument Fktviscdl Fei7tltary 7, 2019 SamplC C_^ ondftLosi ISpon Rarcl r 5Ct1R Pa a 1 ai 1 pacument No.: Issuing Aclftrity: F-CAA-CSd139-Rev.06 _ Pace CamPrias quality Qltice _ Greenwood 0 ' ClientN;snit•; �Cnur)m: F d -a {,JUPS uSPS CulranrlTial r e ,,,�,,(�� Valfwt- rrurndy Scai Presnat? [{Y•s Kko Seal, hitact? nVI., Peckhlg Maleilalt nw.bblo Wfill _�B,rE1F.lr. Rngs t Anne © 4311rET (Waglol Tissue Fro2en? Thcrrttnmc cr: ln; []Yes ©iVo �Sal>h ip f un rvr=c ul lrr•: iYn: [;_f alv� ( Ilnnr [dole, Ftmp f'Cj: Colloclirrn FartoL'.}d(f ,,"ttom� ( rensp slinuln �c above freP2ing to b'C Cnoler temp Cut rea eo {'C11 .--tiJ--1--- 057mD�s Mil Or tlmy tri[eria, SArnples as Irr, rrnussp pr ace rs ��•!!! lys i;C81rn WMA Regulates} Sail ,4jA, water samprtj t1'd taruolat rsti0,We in a v+aranrina aan, ithin isle. 11+11led 5IMPS: CA- r2Y, m Sr irherk maaat? Old Lammas wipinare from a (areldn tatwa (intecnallnna&:. Ye n (jp wOudinr llawall and Pucao pStal?QYcs }!o _ dhainofCvslad .Sanluies Arrivtd WOO rlold_rime? _? rr1 l-f:ln QIA 2. _ShurtHold Time ArWysh{1)2hr.1T _ 's na (Tl/A Rush Turn Around i )mt. Reques tq _ S%6,cicnl Volume? ,f�Ycr re f-)ssn_ P/A- O:irpctC01,10lertUsed? -Poce Containers used? dVj Qt>a ORIA {ram-,�i'ef Qf1n (�Nfn 6. comlincls lnrarl? �^ 7. UILSDived iRalY515: Sarnpl Cs FiCI[t nitefe5f? �Y rio YfA �. __ Sample IAheistlslctt CUL? Y@% f_ftlo cJnfs a, _ •Uldudes ilitt(IlmeflrlJAn;r]yns_ AIAEric: Ilcads�atc in VE2A V7uls n5•Gnlmf? P1'es :tn_ trip Rtank Prtt mrT _�-r UYes l_1:1a ( JNIA 1t. I Trlu Rlnrk t:ustudv Seals Presrnl? irr Nn lux ri 1lN nitNrSJSMiprF L={SCRF PAT'CY Flaki Data Rnqulrnd? [_]Y[s [_}ISa ___ Ln1 It) a(S !IS [t'11131ACrs; CLIP HT NO11F1CATIONlII[Snitl[tc:ls Person tnmacted: ��•_______�,_•�___,___ Ualn/Tlmc: __�•-. _ Prrrlcrt 0.SAnipt+SCURF pevlew: Prrrf ll �n[t Mtanoprr Sl}F Retriasv: J nxte: page 2 of 4 }', CHAIN -OF -CUSTODY I Anaiyticai Request Document P2CEitJk?��ilC3C C� V Tn. is a `�Gn[ OOCt1V!N-r. M rk4"4MC-kj a ,9 w w e e4 A,4r. 5asrian a 5c.don 9 srcelan G �+'� d 2056569 ac �a+Ko<+naeo'= a.a�drna rMc±c�urkvmaie�r. h„� Aw T. ""'°°e3 W. T R ►,,��. d ' S` CvyTp` R£C,lSLA'(WAGE4CY - r •y Ad NPOES r GRWND WATZ; 7- Ofa7G41'4G WATER r UST r RMA rc gm-4�&V-37 77p F O "a�""'s A'0�� Sim LaczUas SIAM A.q—wd Ow a*WrAr; Prgw r�nt+.0 P•,dL r. R�4txsted Artsiysc, F1t0erel EYnsl 1 � CoLLEMa 5. t4S4 rlqWwr OW vFa.r," ft:ar ring wean NYI fi /R SC'J.�OW t SAMPLEIU o a. ,.� :.. SxV,e L1UST OF. [fk:^_l.'E ri_:ua ,M � Oncr aT i o �FT un,'E Pacc Projrct tiC: Oat, r.0. S i�`Q. -� CY •.2.'.-�(dyP i '' I l! I l l € I l i i i l! I I z I' i i rlT I!I !I II 3 I I 1 I l l I l f I ! s 4 -T I 1! l f l I l ! i f l I I I I I I I ! I I ii liil'?I 1 I !!! l i { I S S a i t 111 i t I 1 i i i i i f i I I IE I S! A➢DrT,CK.,L'. wwt-LT5 Fuxawsm= eY i AFFILIATION MT= ! [ VE 4CCV711Z!,AjjL1AAaN DATE THE SAUVU COOL"ON5 yy Z I L$jR K"F dHA MNATURE oIr€Nat Par,T n— or S.AA,PLER: �. s:GNatt�(e, SAwTLER: Saq71'1d R's •zr:.-�.,n:.:rr.c,...._,�,..e.-r�++c:x.�..gs,U.nE'::-1cx«...,w-.:..,sn-r:w.wa..�n ari 5xcr wmru rn..,a+r.�!o.,.r �..-..n sirs r.�l.L-G20. �.C'. :�-+Aiv-29a7 Ununnenr Name: oocumant novlted; Febma Sample Candltlan [1 an Reecl I SCUft Pago 2 of 7 .PaCCNl31yl'Cc71 Uecutnent Nn.: lstuing Authorll y; 'Check mark top half of flax if pli nod/or dechlorination is verified and within the acceptance range for preservation samples. fxceptlunr. VOA, Coflorns, TOC., Oil and Grease, FJROIR015 (waltej 11UC, Wig #'got tom half of box Is to list number of battle is y ; b E E ppE F: E tr [ m E yL x a E pE E r3 eC 4 w mr o n g l7 l7 i� t7 a L7 O V ? U' � 7 A 4 w O �3 pfl Adjustment Log for Preserved Samples 5en+pleb type er Presarvaslve pnupenrerelpt pa e—re-e arratlan adjntted limp prafervaVun Amount of VleurvatWe totx ti aalnsred added NutC•. VJnrnr�m ll.ere' dlsuepsnry srlrRing rlunh for nlir a cainpli,rc.. nrnpG s,a mr Vnrl hrrs f nrM M5 l he s, V to the rlprlh Carallno oEH N:t Grt:Rcatlan OEnce li r. 7w of held, inrerrer,. pr tier,]I ,e, anto f te..,np. I n m r rerr ,,nta4rrn. Page 4 of 4 laceAnalyfical" - � www.pecefahs.rnm I Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: WADE MOORE EQUIPMENT CO Pace Project No.: 92389780 Pace Analyttcal Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 07/02/2018 Date Received: 06/26/2018 Sample: SITE 1 GP Lab lD: 92389780001 Collected: 06/26/18 06:30 Matrix: Water Melhod Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B Turgidity 5.7 NTU 0.50 06127/18 13:30 SM 2540D Total Suspended Solids 6.2 m9iL 2.5 06/27/18 16:53 SM 2540F Total Settleable Solids ND mlJLlhr 0.10 06/27/18 13:10 EPA9040 pH 7.6 Std. Units 0,10 06/29118 15:12 H1,H6 ANALYTE QUALIFIERS Hi Analysis conducted outside the EPA method holding time. H6 \Analysis initiated outside of the 15 minute EPA required holding lime. Reviewed by: Terri Page (336)623-8921 terri.page@pacelabs.com Eden Certification IDs 205 East Meadow Road Suite A. Eden, NO 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certifrration #: 37738 Virginia/VELAP Certification #: 460025 Page 1 of 4 Document rmamr.[ Document Revised: February 7, 2918 sansple Cond111on Upan Retelrrl 3CirR page 1 of 2 „• r G17�!lh3i}?;Lief Docbnteat Na.' Issuing Authority; r-CAR•CS.t733-rtev.pG Pact Careffnal Ckoality Office Labormory receiving samples: Asheviile t7j EdenFj Greenwood (J lit mom tourlor. _ f d C Ups ovsps L.•l�r © Cu,nnrrrripl f � ©Olher;_� r+ CuftndySCaSprefonl7 �[Yr.s P1n Sppfrinlacl? {]Yas [�No Parking Mata.daf: [11,10141c Ws -mu [_;Atttlhte Rags [Xane ❑ O[her C-r-DlMogfcjyes ©No DiN/Aat litfuo Frozen? 71rcr[name ar: Tzpx of hx: �tVr: (�Itlur 1-JNonc Cnnler Trnrp 1'Cl: r. >,�'? C/oirectlm Faclor_ Add uSNtPc 1•CI J Tenrp Should 6e att6vC Sretr]ng in 6'C Cool qr l amp Corructed ('Cy:-_ ( { 5ampkf Nrt of mmp c,hma. Sdrnp18 on Ice, f.nssrtg Process Ilat 4egun 1150A Aegsdmed 5 uif {( 4/A, wito tamplC{ OTd sanlptet odgiRalt ill a ltt+arintinr rrmc tvidtin the trrsissr33NIn: ('A, iiS'. It Si. lrirrCk mA(i417 Uid iampres orylrtote iroln a fDrtlgn saeum t;arxLAs[MnAFY, incluC:ng f"Wjill and Puerto RICO)? 07es lte Comments/olumpanccy: 0a101 Df CYflad -[)'fa jw 1. •�__- SanyNesArnvtdwllhin 110H riw? _- - Duo r'L1^ 2. 5hw(Hold TiMeAnalYtk <72ht.)2 �n J. _ Rush Turn aro_un_d limeRequesledt (Yas hu-,�-Nln _S0150enl Vnluurr.l _ J f}arr tefa �CJRJA 5. I:Crrect CuMaine, 3 Umd7 7 { {m 6. Hn I '41A I:nnlAiners lnsaCt7 _ _ _ _ 1st �Ho I 7. okt6r.il mgyfiy 5arnplxs Sirlo3 I4e_re,tL No :r/A v 11. _ ^ 53mplc tAhvh M.Hncc{1L1 Yu (]Ira Ufl/A 4. 117-� -InttodasUalrRi+nt11RlAnilysis _P.lal,+>,: Ilutdtp3ce in Vtln Vlalt {>S-Gnsna)7 (� [n f ): 4 Trrl+tilar+UTtseht7 ~-- -Qh'rl jrxr �jrrn { 44J4 lt. i Trlq gfa[lk Cultady Scats Pre:srntt Yse hn l7il iUMMENISJU%11'7r U+srrtFFANCk Fluldl!ta[a Requlmdl (-`}yes ❑Ira lntlOollplirctlnlainers: Ckit NT HQTI lIfgTl{SSif1lF plrllf4rJ j Person -�_�.� {lvf.✓- hate:\,j►Y- i Prnlart Rl:uragrtr SCt!{{f Revioe,; _ �_ project%tanager SHP Review: Poo 2 of A Cn w CD Co CL CHAIN -OF -CUSTODY I Analytical Request Document tna er mroY.r_ : a Scctlon A Sce=San B Saetlan G iiK ' � kCae�atTt_ upr,.ir.tl nTi tr.N:nsyn J.— vGv+nsa•` -�^ {'� A 56 569 r � To: F " .7d R %�Id•1l US* LWOM �+ C Q 5 1 v Tq rpm REGVUkYORY AGENCY tf15 IV Q 7 s ' F MOM i- 13ROVNO WAlTSic i OrZ NMr.. WATER r acsaA r crsaaER i c. �A 6nx Na, SiA M' ' R.qu.awd Ow p�(TA7; Prge� C►aEar °' t Raquesle¢ A=n Y% s Filtafrd (YIN) Sr7bn9 M�b:�[otics � ..' 4s i� y I�.gr.rrfas 4ivn+,ea; r.. J- , eye' a � COZLECTc6 amear.�yGws � i F i I WT w..:nv�aa Wray m warn cYaxr ww Eovs P 1w � ' ] SAMPLE 10 ,m y1.j, L-0i :� M AR U C ` 3.q� jD--WU8T 8F, UMQI._ rG— T$ F _ _ o a Z, s i t I I I i t i f i t l i � l i 1 1 Iillill 9 i FFF To i II I J i l! I I I I „ i l l i l i?Ifflll 12 I I I I I A9I/Ti16NAL CAMtlilEM73 £i/1rC.15NE7 BY RFF7uA:,PN f i nASE I T7l6 ALG 1Y1 U 6N DATE 'me. }A/tFLi cnnpt77flN5 11 1 i f I I i •� I ! ! I 1 � Ofi{G1S €AL SAMPLER NAME AND gGnArUFLG iytGrrANRt c1 SAiaPi.Est; �� rr� � sTi -r1—Y1-1 �i[.. w^, —lsr,rj: NETa 1,M-- '.--•11,---^ d+- F C'-1. �7-�l2Ckw�.�`i. 1.�l�Ty-��Gr nnrbMent Ndmr.; Oncurnent ROVISCO: Fabi Sanlpfe Condlden Upon Recelpt SCUAl Page S of 7 Pf7t C/ilh4ljdlC7i Uactone.nt Nn,; Issuing Author F-CAR-CS-Q33-Rev,06 (,.4 ; � 4�+t+w.E�Lm2 *Check mark tap halt of hnx if pH artll/ordechlorination is verlfled and wlthln the acceptance range for preservation sampfes, ExcepLlont: VOA, Cnlilarm, TQC, nil and Grracr, nRnl8o15 fwalctj UUc, twg "Ootturtt half of box is to Nst number of bottle 'ri Ti •- ,'F :i .n` r'i E o Y r . u X d a E l SI pE t K r+ L E F l F. " E �C- m E F s E = i Y Q C Q +i +[ O } T 7 l it � � � _� ...1__ �•_ � _w .�_._ _ ^- ._. ___ __ � _ - -_— 0urnlf+nld.7ncnr.catpre+nrvtfrvr,—I urlemo,nlmffC4c�nlalncn. page 4 of 4 e aceAnalytical. wwwpeoel b&=n Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: Site 1 GP Pace Project No.: 92401597 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)8344984 Page 1 of 1 Report Date: 10109/2018 Date Received: 10/01 /2018 Sample: Site 1 GP Lab ID: 92401597001 Collected: 09/29/18 11:30 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B-2011 Turbidity 113 NTU 1.0 10/02/18 14:34 H3 SM 2540D-2011 Total Suspended Solids 31.9 mg1L 6.4 10/04/18 19:28 SM 2540E-2011 Total Settleable Solids ND mUUhr 0.10 10/02/18 13:30 H3 EPA 9040C pH at 25 Degrees C 6.7 Std. Units 0.10 10/03/18 10:19 H3,H6 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. H6 \Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by: v� Terri Page (336)623-8921 tern. page@pa celabs. com Eden Certification IDS 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 Page 1 of 4 I /�'-{ty� 1 l Uboratory receiving samples: j Asheville ❑ Eden[:] Greenwood ❑ HuntersvlilioF' o.r-r-.n— "'--'••-'- -"'•^- - - - - - Wo# : 92401597 Client Name: u • \ ikd � Project Courier: Fed,Fx/V UPS USPS Cllent 1111111111111111111111 ❑ Commercial ❑Pace ❑Other, 92402597 Custody SailPretant? Dyes ONO Sealsintact? Dyes ©No Datl/tnitbis Person Eeamkdrg eonterwt / Packing Material: ❑Bubble Wrap [Bubble Bags ❑None © Other Thi; Fro" Thermanietar; d� � type of rce: Ower ❑aloe t---et,,lotoaltat LJr� ONO �ip/A I .- ❑None Document Name: Document Reldsed: February 7, 2018 �,,,r,,� Sample Condition U on Retal t SCUR Pa 1 of 2 r �11Q1r"�!' OocumtntNo.: IswfigAutharlty: FUR-CS-033-R�v.06 PacaGrdinastluall C>liEta pS Gun to: Cooler Temp I'CI: 0. r/ Correction Facto k p?Subtrast ('Cj Q . —[— Temp should be a bove freezing to 6'C Cooler Temp Corrected ('Cj: Z' O Samples out of temp criteria, Samples on ice. ending proms ��� /// hat begun USDA Regulated Solt (Fa MIA. waterumpie) Did samptes atgl to In aI uarantlne tone within the United States: CA, NY, or SC (check maps)? Did Lamples a4lnsto from a lordan source (Intemnionany, IlYes And rILna 14—an and Ruerru RJrnt7 F7Yes ComnNnt DIc[re Chain of CustodyPretend No N A 1. Samples Arrived within Hold Time? No HA 2- Short Hold Time Analysis <72 hr.)? „ No A 1. Rush Turn Around Tims Requested? as o0,111A a. SuRldenlVolume7 Ne NA S. Correct Containers Used? -Pace Containers used? es Oft (]N/A No NA G. Contatner7 Intact? a' Na N A ?. Dissohedana Is: Samples Field Filtered? es No A B. Sample libels MatchCOC7 -inctudes Date/Time/ID/Ana s Matrix: � ONa ❑N/A 9. Heads ale in VOA Vials a5-runm ? Yes No N A 10, trip Blank Present? TripBunk CustodySeals Present? Oyes e. ON. No N/A N/A 11, COMMENTS/SAMPiI DISCREPANCY -1- f-/i CLIENT NOTIFICATION/RESOLurnoN •—� W Lot ID of split containers: Person contacted: Oate/Tlme: Field Data Regsdred? Elves []No Project Manager SCURF Review; �/ Dare: //��''�� V r[ V Project Manager SRF Review: Dato: )0 1� Page 2 of 4 O7 a CHAIN -OF -CUSTODY 1 Analytical Request Document The Chefnb -Curwdy Is a LEGAL DOCUMENT- AN rekw&M tx*b ma = be cwnp KW scaaccy. ©e�er��n■Me _ - ■ciMMMII■n■■■■■■ Monsoon■■■■. ■■....■■■■■■■■■■ ■Mn■■■■■■■■o ■■..r.■■■■■■■... ■■■■■n■■■■nn ■■r.r�■■■■■o■■■■ Mongols no EMISSION ■■mmmmon■■■■o■■■ ■■■■■M■■n■■■ ® ■■m�rr.■■■■■o■■■■ n■■■■n■no■.■ ■■mmmmo■■■■s■nso ■on■o■■ns■■■ am ■o■ mmmo■■■■s■■■■ ■■s■■■■sso■■ Im ■ommmmo■■■■■■■s■ ■■n■os■o■■■■ EMISSIONS ■o■.onnno■■■ In ■■■r■��.jj��o■n�■■■■■■■ ■■n■■g■■■■■■ SIM, r 4 Document Name: Document Revised: February 7,1018 �,,,�d Sample Condition Up. A.te! t SCUR Page 1 of 2 • ' areAnary kJ1' Documanl No.: Issuing Authority: FCAR•CW33-Rev,06 Pace Carolinas Quality office 'Check mark top half of box If pH and/or dechlorfnation Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Caeform, Tor, OII and Grease, DRO/8015 iwaterl DOC, LLNg "Bottom half of box Is to list number of bottle Und : 9240159? PM: THP Due Dale: 10/11/18 CLIENT: 91-Wado Moor .r iiiiiiii►Qiii �1110i�ic�►���i�ONNo MEN Simmons Bosom is �►�iii i►�i � iiai�aii�ni� Image ammimmmmmommoss HOINVORk"11 IODINE nommenon sommommom He on 0 0 0010 0 MEESE on I LIN mol pH Adjustment tog for Preserver! Samples Sample to Type al preservatNe PH upon «ulpt Data preeervaden adfatted Time preservation adjusted Amount of prasernave added tat nom: wnenaVR roue rs a uscrepan[y umnma noon urauna compiurce samp:ee, a [opym rnn roan used w rena w cue owed wrmma uennn cenmsauun vnece p.e. out of hard, incorrect ofa$anative, out of temp, Incorrect contaEoees. Page 4 of 4 I aceAnalyficala www'mceleblmn Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: Site 1 GP Pace Project No.: 92401697 Pace Analytical Servlcea, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 101D912018 Date Received: 10/01/2018 Sample: Site 1 GP lab ID: 92401597001 Collected: 09/29/18 11:30 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130E-2011 Turbidity 113 NFU 1.0 10/02/18 14:34 H3 SM 254OD-2011 Total Suspended Solids 31.9 mglL 6.4 10/04/18 19:28 SM 254OF-2011 Total Settleable Solids ND mUUhr 0.10 10/02/18 13:30 H3 EPA 9040C pH at 25 Degrees C 6.7 Std. Units 0.10 10/03/18 10:19 H3,H6 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by: -AW Terri Page (336)623-8921 terri.page@pacelabs.com Eden Certification iDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 Page 1 of 4 i I Document Name: Document Revised: February 7, 20t8 A,,,�wi ' Sample Condition Upon Renl SCVR Page 1 of 2 Document No.: IssulnQ Authority: � • �"'4'r"�1 F•CAR-CS-033-Ray.t16 Pace Carolinas tludl Office Eaboratory recelving samples: Asheville ❑ EdenU Greenwood LJ HuntersvfllA Client Name: WO# : 92401597 Wfkd � Project Ij courier: Fed Ex UPS usps Client ❑ Commercial Pace Other. 92401597 Custody Sear Present? ❑Yes []No Seals Intact? []Yes QNo ['ate/W tl3th Person rxamktM Contsntsr�a- �' PaddngMaterial: []Bubble Wrap ❑Bubble Bags ©Kane ❑ Other 9lologlalTlssa$ F-roson? Thermometer: / Des []No Jai/A i .. �/`''f1` dfl S type of tor: Qwct ❑Blue ❑None '' 1 Lt Gun to: Cooler Temp I•Cl: _ O . y Correction Fan�A�d?Subtract VC) �t— Temp should be a bove freezing to WC Cooler Temp Corrected ('C): 1.0 ❑Samples outer temp crimda. Samples on ice, cooling preeess has begun USDA Regulated Soll ( N/A, watertample) Did samples orlglqato In a arantine zone within the United States: CA, NY, or SC (check mapsl? Did samples orlghsate hem a foreign source (sntsrnaslonally, f1Y�c f� LW,MMs Na,uan aM RrrmQbnl7 f'TVes � 1 Comment Oiscre Chafn of Custody Present? CIN. CJWA 1. Samples Arrived within Mold firm? No N A 1. Short NOW Time Ana h <72 hr.)? n Ne A Ruth Turn Around Time Requested? Yes GKQ n A _2- A. Suffidem Volume? n< n." 001A 5, Correct Containers Used? -Pace Containers used? RfyONO n171NO ❑N/A N A 6. Container! Intact? No M/A 7. Olssohred am Is: Samples Field Filtered? es No A d. Sample Labeh Match 0007 -Includes Date/Time/10 Ana Matrix: Ores CINa ❑N!A 9. Head ate in VGA Viais sS-8mm ? Dyes EINO MIA 10. Trip Blank Present? Trip Blank Custody Seals Present? cYet es I]rre No N/A N A 11. COMMENTS/lI MPU! DISCREPANCY Field Oats Required? ❑Yes ON* m- - q-b f-17 IIJt1 _Lot ID of split containers: _ CLRNT NOTIFiCAl"IRESOLU ON I� Person contacted: Date/Tlme: [ Project Manager SCURF Review: v Dalc / if Project Manager SRF Ravlevr. Date: lO �� M Page 2 of 4 ;; IT CHAIN -OF -CUSTODY / Analytical Request Document The CIIAT440=bWy Is a L6GAL DOCUMENT. At rW@vud fielft MLW be MuWWW amanidy. • NEWIMMMENEINSIM Emmons 0 nommosommism go sommoommonsm Im moommmmossommosso sommommossom 0 mommmmosommosomm MESONS son Is nommmmommosommon ■IMIMIMMIIIIMM 0 1 a moommmmolloolsoms assionsomons moommmmossommoson IMMENSENESS 1 woommmmossommonom ■sommommosms■ moommmmonsommossm ■onsisommosso RE sommmmassommosso mansommansom IN NEI z *Check mark top Ralf of box If pH and/or dechlorination is verified and wfthin the acceptance range for preservatlon samples. Fxceptlow VOA, CaAform, Tor, Off and Create, ORO/8015 Iwaterj OOC, LLHQ •'Bottom half of box Is to list number of bottle WOE# : 92401597 PM: THP Duo Dale: 10/11/18 CLIENT: 91-Wade Moor Emu on a No 0 son was 0 on MOMMM Begone jai ■aO���iia �uiiiii�ROiii C° `►��°a�Ci�■�°�iiiiii��Ci� PH Adjustment Log for Preserved Samples Sample0 rpm of pretemthm pH ppen receipt Date prawmatlen adjusted Tlme presemtlnn adfast•d Arnountefprawmtive .dded late . rrnenerer snare n a oesenpaney errean� norm ssrorma compuarce samp:es, ■ [opy Vr sms rwmsns a sen: [o [ne nu[n urprne usnnn urmrouon once li,e, Out of hold, 4rttrecl prnemt:ve, out of temp,lr,mrtecf connlnets. Page 4 of 4 ceAnalyticale www.peoekb&COM 1 i Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: TSS/SSITURBIDITYIPH Pace Analytical Services, LLC 6701 Conferenoe Drive Raleigh, NC 27607 (919)83"984 Page 1 of 1 Report Date: 12/31 /2018 Date Received: 12/28/2018 Pace Project No.: 92412355 Sample: GP SITE GP Lab ID: 92412355001 Collected: 12/28/18 08:30 Matrix: Water Method Parameters EPA 180.1 Rev 2.0 1993 Turbidity SM 2540D-2011 Total Suspended Solids SM 2540E-2011 Total Settleable Solids EPA 9040C ANALYTE QUAUFIERS pH at 25 Degrees C . Results Units 118 NTU 86.0 mg/L ND muuhr 6.4 Std. Units Report Limit Analyzed Qualifiers 1.0 12/29/18 12:55 2.5 12/31/18 12:33 0.10 12/29/18 13:02 0.10 1213l/18 13:19 H3 H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: \'� Terri Page (336)623-8921 terri.page@pacelabs.com Asheville, Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NEL.AP Certification #: E87648 Massachusetts Certification # M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaAfELAP Certification #: 460222 Page 1 of 4 r4 Document No.: Pace Carolinas Laboratory receiving samples: Asheville ❑ Eden0 Greenwood ❑ Huntersville ❑ Aaieighn Mechanircvlilnr) CrlentName: W0 "92412355 - ProJ� . MLIUSPS Courier: ©Fed Ea ©UPS ❑ Commerdaf CIPate QDther._� 1 924333 1 CustadySfal Present? QYes �t�o Sens intact? Des []No .....rmsW., ream Eaermnifi. Contra-t� Packing Material: CIRubbla Wrap []Rubble Rags 19<an a Other Rrdalrcal Tissruee FFrraren? Thermomater. DaGuam: rMTC.Qt- TYPeef- ®hues ❑tuue (]Yu ❑No !/A ©None Cooler Temp (Cl- 3.15 Correction Factor: Add/Subtract {'CJ Ci Coder Temp Corrected ('Cj: q Temp should be above heezhtg to 6'C QSamdesmnof team criteria. Samples an W, carom amen has begwn USDA Regulated Sall 1 `Q•F7/A. water sample) Dld samples ornate In a quarantine zone within the United States: CA, NY. or SC(rhed maps)? Odd simples originate horn a Foreign swuce (InwoltionsaY• r"lv— r INn r—lM Commanu panty: Chala W Cu1 fhesrot7 - E3WA 1• Samples,Anivtd wftMn Hold Timer &W DID WA L Short Hold Ttma Ana 42 hr.)? A 3. ' Rush Tum Around Time Requested? - QN9 OWA �. SuMentvodume7 ENM QFOD DWA 5 Carrots Carnainet Used? -Put Containers Used? En R& Qtte QN6 (]N/A QIYA 6. Contalatn rota? Mydir D19 • WA 7. OlssoMrd enn • Sam field Filtered? eOffe WA 9. Sample ubels Match COC7 Andudes Dste/rlm Matrbr. QfU ti . Qaa OWA 9, Heatispace In VGA Vials Dyes ONO /A 10. Trip Rink Present? Trf Riak rotadySexls Present? OYU (11, ❑No []no EXA 1124A U. COMMENt1/SAMPU MCREPANCY FheM Ran Regr N0 ❑Yet EINo I Lot ID or split conlalners: WENT NOMCAT7 RIMOLUMN Person contacted: Project Manager SCURF Ravlew: Project Meneger SRF Review: Dammme: Gate: I �- aI Dow i Page 2 of 4 CHAJN-OF-CUSTODYDocument I�o■rmmm■■■■■■■■■■ ■■■■■■ ■■S■■ �■�■■■■■��■■■■■■■■■■■■■■ ■■■■■■■■■r■■ i�■■�■���■■■■■■■■■■ ■■■■■■■■■r■■ SIMONSON i�■■�■���■�r■■■■■■■■■ ■■■■■■r■■M■■ i�r■�■���■■■■■■■■■■ ■■■■■■■■■■■■ i■i■�■■����r■■■■■■■■■ ■■■■■■■■■■■■ i■■■■■■■■���■�■■■■■■■■■■■ ■■■■■■■■■r■■ SIMONSON ��■■���■■r■■■■■■■■■ ■■■■■■■■■r■■ SIMONSON +o',+`,Tv-�=. ,,�i"4�E J;a� �'!`''•^!SifArr-g�'a �a::ti,`:'ytr� l.°v�':_; :r3�—� w:�:� ""' T4=� y :sY.'.G" s'4'z:,r=^:?;' =-¢� ". t -s. Dtxument Natnc Oocnment aevlsed: Fetuuary T, 2018 Sam a Condition U on Read t SCUa Page t of ] Document No.: Issuing Authoftty: F-CAH3•Rev.06 Pace Orofinas QualityOffice *Check mark top half of box If pH and/or dechlorination is verified and within the acceptance range for preservation samples, Eacepdow VOA, CoWmm, TM ail and fiteue, ago/001.5 (watru) DOC, Will; "Bottom half of box Is to list number of bottle ::...wc 924123.55 PM. j14p Cue Cale: 01/07/19 CLIENT: 91-Weds Moor pH Adjustment Log for Preserved Samples Sampk ID Type of Frunvadve pH uponrenlpt Date pres~Jim adjusted I Time pmemdu ad(usted Amount of P asemathte added Lot Nate: vfieneeer [hate It a disaepapcv affecdns Narth eatollru compllanco samples, a copy of Is form will be sentto the North Carolir-a UEHNg CtfVrkcaGon OlfK# p.e. Out of hold, Lnmtt t pfewrvattx, out of temp. Inmrrees cer"Lmrs. Page 4 of 4 ceAnalytical o ~ pwalebscom Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: TSS1SSffURBIDITYIPH Pace Project No.: 92412355 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date., 12/3112018 Date Received: 12128/2018 Sample: GP SITE GP Lab ID: 92412355001 Collected: 12/28/18 08:30 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA 180.1 Rev 2.0 1993 Turbidity 118 NTU 1.0 12/29/18 12:55 SM 254OD-2011 Total Suspended Solids 86.0 mg1L 2.5 12/31/18 12:33 SM 254OF-2011 Total Settleable Solids ND mUL1hr 0.10 12/29/18 13:02 EPA 9040C pH at 25 Degrees C 6.4 Std. Units 0.10 12131118 13:19 H3 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: \-� tk— Terri Page (336)623-8921 tem.page@pacelabs.com Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 Page 1 of 4 Document Nam@: Document Revised; February 7, 2019 Sam I@ Condltlon Upon Flocelptl SCUR Pa e 1 of 2 Document No.: ttstdng Auihonty: F-CAR-CS•033•Rev,06 PmeCardlriasQuality Office Laboratory receiving sampler: Asheville ❑ Eden[] Greenwood ❑ Huntenvllle ❑ Ralelghn—Methanle-111-17-1. Client Name: l : 92412355 1i111o# vro]I hAtIJS Courier: FedFx UPC S Client �4 � Cl Commercial []pace other I Custody Seel Present? []Yes W Sash Intact) QYes 924113151511111111111111 ❑Na ' ....varuu renal eaeminlna ConteAnr \Z� t�1 tin — Packing Material; ❑Bubbla Wrap t-�✓ ❑nubble Bass a ❑ Other Blofoglcat Thsue Frozen) Therrnemotsr, TYpeelleae j wat ❑Yes [:]No /A []Bluej]None ❑1RG,,M.. eht'[uU7 Cooler Temp ('C): "IS. 15 Correctlon Factor: Add/Subtract ('C) ! O \ Cooler Temp Corrected ('Cl: A Temp should be above freezing to b'C ❑SamNes out of temp aeala. Samples min. coding preen has began USDAReauhatadSon (DVA, water samplal Did tampks originate in a quarantine zone within the Untied Sista: CA NY, or SC ([heck maps)? tad samples allnate from a foreign soum (Werestlandy, f`4v.e T71Nn s r r . u. u,, a a..n. es n r lv.. nx COMMInrt Chaln of Qltody Present) No DIVA L Sampiss Araed within Hold nme7 Ne 0JqA L Short Nold Ttme Anal k l72 hr.)? E39W Oniq A 3, ' Rush Turn Around Time Re uasted7 u EK. A 4. Sufficient Volume? gfr ON. 0N/A S. Correct Containm Used) -Pare Containers Vied) En of ❑Na Ne []WA OnJA 6, Containers intact) No A 7. 011SOW aN : Samples Field Filtered? 0Y. ON. SK4 a, Sample libels Match COG -Indvdes Dat meA Ana Matrbc sa 4 [IN. ❑N/A 9. Heads InVOANaJs >S-6mm)7 es Na /A 10. trip Blank Present? Tri Blank Curtseah Present? ❑Yes OY. ON* ON. A 04A L7. COMMENTSjSAMPtE ("CAEPANCY Fleld eats Pieaudred) ❑Yos {]No } lot ID of spilt mntalners: , CUFNT NOTLf1CA710N/RiSMUTtON Person contacted: Project Manager SCURF RIVI4 Project Manager SRF Review; Date. Page 2 of 4 f CHAIN -OF -CUSTODY / Analytical Request Documeni The crsn•d-cuftdy Ia a LEGAL oocUMEW, As mdw m Roft mL= ba amnp wd mommm r. �nri■n - ........_ .... its _.- .._ -_' m. Ell aa©aIIIIIIII = � __�� �r ca�r!g[iYeb�ry.-�•".%C�a «"' ��.r+�:��':r,��—��.��..Y! �_ "�:•'L=�:.�Y�. �i�':e�:-�45.;-:2w �' f5'4�-z'F�:?�'S`=::�;r"�ar�i'rr r�.� ;s= .,a;,,� �.i%'`��r��."5"�`�'r•.� w 0 A Document Name: I DocumentAevlsad: February i, 7D1e Sam fs Condition Upon Racal t SCUA Pa e l oil Document No.. Issuing Authority: FCAR{5O33•Rev.06 Pace CarolinasCluail Oftke *Check mark top haB of box If pH and/or dechlorination Is"WON:99224123155 Ye rifled and within the acceptance range for preservation samples. Etcaptiotn: VOA, Collfotm, TOC, Oil and Grease, ORDIGOIS(water) GOC, LLHa te: 01/07/19 "Bottom half of box Is to list number of bottle 2? 7 Y 7 7 ? F �s .S A 3-1 pH Adjustment Log for Preserved Samples Ample to IW@ of pnsemativa pH upon rec 1pt Data preservation adiusttd Tlmt prntmd" rdlusted Amount d hatenytive added tot t r.�u: wrens.c.u.u•u.uuvcp.naY.i.v.u.�y nwu,�+.u...r uni,pu„aa.r..y,.,.. wrr ��.,....�,.��...w..,.a..,.F,...�...�.�.,.,.,. w,..,. �.���...,....,..�� ... Qvt oT pold, 4KurrM prtrerniMe, ovt of ttmp, Inrarren sgnnA+tn. Page 4 of 4 55'ceAna1Xib1* ' wwwpeceiabsobm Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92412485 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 01/04/2019 Date Received: 01/02/2019 Sample: SIT 1 GP Lab lD: 92412485001 Collected: 01/02/19 07:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B-2011 Turbidity 31.7 NTU 0.50 01/03/19 09:46 SM 2540D-2011 Total Suspended Solids 23.6 mg/L 2.6 01/03/19 13:45 SM 254OF-2011 Total Settleable Solids ND mULlhr 0.10 01/03/19 08:16 EPA 9040C pH at 25 Degrees C 7.6 Std. Units 0.10 01/03/19 09:22 H3 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: Kdsti Doss for Terri Page (336)623-8921 ten i.page@paoelabs.00m Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VrginiaNELAP Certification #: 460025 Page 1 of 4 D Document Name: Do cument Revised: February 7, 2018 Sample [unditlon Lip on Reu! t SCUR page 1 of 2 Document No*, Issuing Authority: F-CARCS-033-Rw.GS Pace Carolinas QWity OtRce Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ ME Client Name: Projectp: Wpat Courier, ❑Fed Ex UPS USP tent ❑Cemmuclal ❑Pace ❑Other:?,^ Custody Sul Present? Dyes �]+KQS�Sulslntaw Dyes ❑No WO#:92412485 1111111111111111111111 92412485 Oata/Inldak Penon Eamin]y [nnerntc�•� p Patddng Material: ❑Bubble Wrap ❑aubble Bags 43tMne ❑ Other Biologlal Tissue frozen? t Z J Thermometer: .❑None ❑Yes ❑No [519 Type o!!u:r j]91ue ❑tR Gun ID: CoolerTempl*Cl: r Correction Factor: Add/Subtract l'Cj Qr Temp should be above heetln6 W 6'C Cooler Temp Corrected I'el: r 3 ❑sampieseut of lemp crltetia. sample on tra, cooling process has begun USDA RqulatedSell (EMA,watersample) Old semplesarl[fr In a quarantine acne within the United States: Ck NY, or Sc [check maps)? DId samples orfs3mte lrcm a foreign sown lintamartlomily, ".. ��ku, .—d.-4&--e6-.tsTIN— turd Comments/D[stte ant . Chain of Custody Resent? es[]NO MINJA t. Samples Arrived wtthln Reid Time? i too EINIA 2. Short Hold Time AnalOf J<22hr,? CIYU N/A 3. RushTumAround Time Requested? es A 4. Sufficient Volume? No ONIA S. Correct Comalnea Used? -Pace Containers Used? -E Yru Ono ON. •❑NJA EIMM 6. Cuntafnersintaer7 Yes No aw. 7. Dissolved analysiss Sam Its Field Filtered? Yes e H A 8. Sampte labels Match COC? 4ndudes Oaie/rme OJAna sie Matrix: ❑Yea ONO ❑NIA 9. Kea df In VOA Vials >S-&nm 7 Yes to it/A 10, Trip Blank Present? Trip Blank Custody Seals Present? OYU o ONJA llnm 11. i COMMEMS/SAMPLE DISCREPANCY natal Data Repuhe6? ❑Yes ONO Lot ID of Spilt containers: _ WENT M017FICATIOP41RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Data: Protect Manager SRF Review: Date: Page 2 of 4 r t r .MOWN■■■■■�C� r� �.iiiiiiiiiiil© �tN�r������� Miiiiiiiiii® Jill rrrrrrrrrrrr� ...■■..■■■■.. [MINN m....■■■..�� ■■■.■.■■..■.� . = ' mom■■..um sons ■.■■■.■■■...NMI m' ©s �.■.■■.■■■■■■� ■■■■■■.■■..■NWWNW■ 111moommommommmmmon NOWINNIN .....■ 11111womuommmommo_IN .■■■■.■..■■.M■ Page 3 of 4 Document Hama: *Check mark top half of box If pH and/or dechlorination is verified and within the acceptance range for preservation samples. raceptlan: VOA, Callrorm, TOC, Oil and Greate, DROIR015 iwaterl Doc, t1Hg "Bottom half of box Is to list number of bottle f: February T, 2018 102 rArnlinatqualltyOlV(e 1 W0# : 9241 2485 PM: THP Due Date: 01/12/19 CLIENT: 91-Wade Moor ,,,, SEVEN 0 kin No ►►►0 r 10 ►►■■■■■■■■►►r■■■ ■►■ ■■ ■■■■►►■■■ a on M END Monsoon 0 \\ INI I� 1 0 In memo means on �r�■ ■► �0 ► ■► ■►►■■■■■■■■►�■■■ �� �� 0 monsoon ■on ►■■■■►►►■■►■■■►■■■■■ ■ ■►■■■ So00 Sam ►�■■ ilk ■ailk 000■■ ►■■■ .+a.t�a✓r' ��`atal�a=a' �nw==ww=w.w�=i==ww��rrrwatwa���sslt�wawrwatt� ��E�•�rr�•arr�•rdr�tt�:>_�.tt�tt���� t.v�e>—t�ttttttt� PH Adjustment Log for Preserved Samples Sample lP Type of Pwemtive pH upon nnlpt oate pretervatlnn adjusted Timepretarwtlon Idlusted Amount or Ptuervaim added tote a Pu P—V rP—M aamP'ai" ,.PPy m P.s. out of hard, tnmuect uroservall.e, out of temP.lnmrycs canuban. Page 4 of 4 laceAnalyficalo www.Pecelehs.C= Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92412485 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 t919fe34-4984 Page 1 of 1 Report Date: 01/04/2019 Date Received: 01 /02/2019 Sample: SIT 1 GP Lab ID: 92412485001 Collected: 01/02119 07.00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 213OB-2011 Turbidity 31.7 NTU 0.50 01/03/19 09:46 SM 2540D-2011 Total Suspended Solids 23.6 mg/L 2.6 01/03/19 13:45 SM 2540E-2011 Total Settleable Solids ND mUUhr 0.10 01103/19 08A6 EPA 9040C pH at 25 Degrees C 7.6 Std, Units 0,10 01/03/19 09:22 H3 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: Kristi Doss for Terri Page (336)623-8921 lerri.page@pacelabs.com Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification C 37738 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 Page 1 of 4 Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Client Name: MEMMUM vroject g: Courier: Fed Ea CJUPS USP ent ❑Cammerdal ❑Pare QOther. Custody SealPrasent7 ❑Yes 131�SealsIntact? []Yes QNO WO#:92412485 9i241448iiimiiirnu RaeeJlNtLb Perfon EasmNingCements:, -ki.� Packing Material: QBubble Wrap _ ©Bubble Bags 131111fna Q Other Biological Tissua Frozen? 7 Thermometer: [Yes ONO 'W QIRr.ID: 9005 Typeerlu: pafua []Mane CoalerTemp('C): e),Cz Correction Factor: Add/SubtractIT) Qr 1 Temp should be gbWa freezing to 6'C Cooler Temp Corrected ('C): QSam0as out of temp crlteda, Sampys an", enartng prords has begun USDARegulated Sol (e•TTfA,water sample) Did samples;l l In a quarantine cane within the United Sut4s: CA. NY, or SC (check maps)? Did sampl a aVtlmta from a raregn source (Intsmatlonsltr, I —)Yes INe Wfd dlne Ha—il aM Puertn Rirm17 My- Here CommengJDlscra Chain ofCustod Present? e, ao A I. Sam let Arrived within Hold came? / •io l71rqA 2. Shortstaid Time Anal sts c72 N. 7 es Elft QMYA 3. Rush Turn Around Time Requested? 171Yes efTro CIWA 4, Sufficient Volume? No N A S. Correct CantalnersUsed? -Pace ContelnersUsed? 45IN QLM ❑Na ON- ❑rl/A NIA 6, Contalnars Intact? Yes Q11. QN1. 7. Dissolved analysis: Samples Field Filtered? Yes a 177NIA S. Sample tabelsMatch COC7 -Includes Date sm4 O Ana tis Matrix: OYea ❑Ne ❑N/A 9. Handspxe In VOA Mats sS-6mm)7 Yes m ONIA 10. Trip Blank Present? Trip Blank Custody Seals Present? E]Yet Dyes Oro ❑ftJA 11A 11. COMMENT5JSAMKE oLSCREPANCY Meld Data Requhedl (]Yes CINo Lot ID of Split containers: CLUNT NOTIFICATIONfRESMUTItNI Person contacted: Project Manager SCURF Review: r =� Project Manager SRF Review; OateJFirne: -- Date: 1 ',_+I-----�_.�---��—`----• Date: I r� Page 2 of 4 c '�' ■rrrrrrrrr■rr� „1,,,1,11 NMI �'��rr�rrrrrrrrr .�A�.rr.rr.rrrrr�r� WIN rrrrr■ CiummmQUE WIN r..rrrurrrrn=0 ■rrri■ommmorr a �,>' , ; rr��■rrrrrrr■�ri� mmmmmrmrmmom � � . ■rr■ilir■�rr�rrr �a��rea ri■■�■�rr■�rrrr��ar© ■rrrrirrrrrrr�rr©€ ■mommmrrrrrrUEE WINm Ommommomm■irnMEN WINrr HE 11111mmummmummmmm.��� omrrirrrmm■®r 1 j�"11 Page 3 of 4 Document No.: *Check mark top half of box if pH and/or dechlorination is verified end within the acceptance range for preservation samples. Exceptions: VOA Coliform, TJC, 03 and Grease, MIMS (water) DOC, Wig "Bottom half of box Is to list number of bottle .--.—I IarollnAutuality j ^^•� t�ffrnllnat Quality Office WO# : 9241 PM: Ti�P 2485 CLIENT: Due Dale: 01/12/19 91-WBdo Moor : ■UNRO ■■\■ \\NONE■ ■■N 0 BE \ a\ \ \\\ \on a►■■ l►\\■a ■ DOE on ■■■■aD■■■ ©►■■ ►►►► ■■► on no NOON►►■■■ I�►\ ■■� \ ilk ►■■ \\ NOON ■■`� HER ii► \ \\\\ones\\� ■\ \\\\\NOON■ ■■ \\ \■■■ ii\■ ■\ \\ ■►\ ■1\\■■■■■■■■ �\ \■■� ■.■■■.... .0 ■. •..NOON■ ■■..■■■0 son IN 0 �rea�e���fer.asaaaa�rveaa►� �rr��tlJii�r aaatir�aea�aaaaraaa.�eae���er�sea�eele��ecrewewre..a�eee�eeee�eeeeeeeee.�a�>•a��eee�w�re �����gr��r�er��le��A_�eee�e����ei�r�e�eeee►.��rrree�r�ee� PH Adjustment Log for Preserved Samples Sample 10 Type of Pram ervative pH upon recalpt Oate p.eservadan edlusted Time pmmstioa edluned Amount of Praservalive added iota "Ole: who."* trove is a orr npa-cy al recuns "o fJrO— compn -- famptaf, a copy er .no.onn WJI rx fen[ of fm nurtn C.rw,ni ucnr,n fs,w�cauv, .„�av T .. Ovt of had. In=ma ormeMdoe, out d temp, incorrect ConpNen. Page 4 of 4 1QUALITY SAND, AT A QUALITY PRICE! WADE MOORE EQUIPMENT COMPANY, INC. P.O. Box 546 Louisburg, North Carolina 27549 Phone (919) 496.3794 Fax (919) 496.7898 January 15, 2019 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attached is the annual summary for 2018 with a copy of an early January test. Brandon Seiffert Sales Manager Wade Moore Equipment co. 0- ANNUAL.SUMMARY DAR - WASTEWATER L :1 SEND TO CENTRAL OFFICE PROCESS NU- E/DEWATERING WASTEWATER GENERAL PERMIT NO. NCG020000 !VIFD . MAR 0 8 2013 CCnl�;si * Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH I of each year. If you have limit_ violations, you must also have turned in a Limit Violation DMR to your local Regional Office wiihin 30 days of receiving sample results from a lab. _ CERTIFICATE OF COVERAGE NO. NCG02-D-Q-�- 9 SAIMYLE COLLECTION YEAR: Z O 1 '� FACILITY ?4AME: _ E 1� P:} - COUNTY: F* offi Ll vt PFRSO'_ti COLLECTLyG S-kM, PLES: rr; s PHONE NO. (9J qJ Uq {p - 3 -741,4 CERTIFIED LABORATORY: p&.« A,Ao�ky}ieo.1 Lab # ADD TO LISTERVE? YES ❑ NOR EMAIL: b ei G f o .Germ Lab # LMITS VIOLATIO?`S? YES ❑ NO ❑ MDUSTRIAL SAND"' Rr DLSCHARGING TO SA WATERS". ❑ Part A: Wastewater Monitoring Reuuirements Outfall No. I Date Sample Collected t 50050 Total Floe 00530 Total Suspended Salidsr 00400 Turbidity3 00545 Settleable Solids: 00400; pH 31616 j Fecal.Coliforms - rnm/dd/yr MG mg/? NTU mlA Standard collml f 5- 1- N/F - .%I ► I - ate- 1 k t` �. Z 0`1- Z7-- I� N F 9. 2 Iq.$ ND . 3 I i All mines must monitor IM discharges for TSS. Only industrial sand mine -discharges are subject to TSS limits, 2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit terra. 3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: I D'NTU for freshwater streams, lakes,, and reservoirs designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity maybe monitored at the Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge. 4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms_ n_ :• r.. . , r, ;�n, n_, �;z r�n7d Last Revised 01-05-10 ---- I _ram Fart A Continued: Wastewater Monitoring Requirements all No. Date Sample Collected` 50050 Total Flow . 00530 Total Suspended Solids! 00400 Turbidity3 00545 Settleable Solids 00400 pH 31616 Fecal Coliforms - msuldd/yr MG In ol,2NTU mJA2 Standard collm] R NT AIL ORIGINAL AND. ONE COPY OF THIS AN-TNUAL SUMMARY MiCLUDING .ALL "NO FLOW", "NO DISCHARGE" & LEYM VIOLATIONS) BY -MARCH ] OF EACH YEAR TO: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 LOU MUST SIG1Y THUS CERTIFICATION EOR_ANY EVFORAIATION REPOR TED: "I certify, under penalty of law, that this document and all attacbtnents were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the systems, or those persons directly responsible f6r gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of (Date) Permit Date: 1/ if201.0-12/31/2014 Last Revised 01-05-10 Page 2 of 2 I ' 1-,_�;aOAnalyticale www.nacefaf78,com . f Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: Wade Moore Equipment Pace Project No.: 92333284 Sample: SITE 1 GP Method Parameters SM 213QB 'Turbidity SM 2540D Total Suspended Solids SM 2540F Total Settleable Solids EPA 9040 pH Laboratory Report Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1' Report Date: 03/17/2017 Date Received: 03/14/2017 Lab ID: 92333284001 Collected: 03/14/17 07:00 Matrix: Water Results Units Report Limit Analyzed Qualifiers 0.81 TUTU 0.50 03/1511717:10 18.7 mg1L 2.5 03/1611713:00 ND mL1L1hr 0.10 03115/1715:30 7.0 Sid. Units 0.10 03/15117 17:08 H6 ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holdinq time. Reviewed by' v� Tern Page (336)623-8921 terri.page@paceiabs.com Eden Certification IDS 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025 Page 1 of 4 /�( fJ_ - eeere spec rlaeufrienr aevisenl xpt. 11, 'IIEiF�-I �� t"1GL'�i(lr?lyifCr?+_ SarnplC Cpnd{tion Uppn nCSeiplf SCUR _ Par[ 2 Uf 2 f11111 / Ilac urnen1LNu,: Issuing Aulhanty: —._?----•�--..-_�..-----_-�- .— V F,CAR'I�A-6O'JRr:v,e2 Pace Cluafily ort�cr. _,-- Laharatory reccivinp, samples; l� Asheville ❑ Edon Greenwood ( p�{�IahiXl MC[hanitsviliC CO, L[ [ HuntersvNfe t. ii,+,srift�1}; 11 Ghent Name; .Y::ll`' `ti:l• V 4•E: Preent Cmrrler: (_}I'ed Ex SUPS �II51'S •l.' r+ Cllcnt 333264 (_�fnnntse trial �Slar:r- j_(Othcr.—_. �,t :. 4 4l i„I ..v F4y,. T•� 'j � i Custedy Seal Present? IJYrs 'kilt) Seals In -I? __(yes % km ealr/lOdah Petsnn F.Mprelnby Cantlntc_ [�7 P_acklueMaterial: � ffiubhlcWrap (_-]nubble Rags Aril! Outher:��•, Thersnuniet c r [ �I0 Gun ID, !• � �; 7 T 111Rlue ❑lion* Elsamples of, lee, soli tzwoc-lids begun Corr m.liun Factor:/ pj.& C'outrr Tamp Catt4tttrd ('C): �— ,n flioroP.ical Tissue Frozen? ❑YeS (-(110 AN/A TCmp should be Ot)ove Vetting I WC -. U51)A Regulated Soi1([11'i N/A,watn "rnplPj l�f•� �,__ Did Sampl s ariglnale In a CRuaranhnr. rnn❑ vrtlfdn Site United Staws:6% NY, or Si: (check maps}? rnali nallf. — ClYr+s Jp — _ includingnawalf and Pwono Rita;? es a .. Commcntsiniscrcpanry: _. Samples Arriv¢d rrNhin hold time? i l� 1-qq1 J ff _ _2• - sltnrt itnld I Ime Anolysls 072 br.lt Sufficient Volume? _..—_ --• f_� S. Correct Contalnrls Used? �F'a[e Cantaln¢rs sJsedt i� )a LI 5amples Field Filtered? _ L� I-1 T C' 8, Note 11sedimem Is visible to the dl� ssph•cd canUlner Simple talents With RIC? ---• _ _-- _ - (-) ; � 7 -- -Includes hall•/l inl c/sU/An aiysis G 1 Reodsfrase: in VCTA Vials [>S rinu41 'rrs U. r! 1 10, Irip Blank rmscnt7 LI C.l l] --- llip Olank Cusls"dy Seals Prostrnl 7 _--.---. __._ - _yes WENT NOUTICATI014/11ESOEVIM14 Per Stan Cpntat Ip,4! CommentsJS�nrydr blstr epaner: Field Otu INqu lred7 Project Manager SCURF --- Revlrw; - -- - Date.: Project Manager SRF Dale:/ Ilusc: 4V7senr.:er lima is a dlsi r¢pancr ayec clog rlmsh Caro'Ina rnmpllln[c samples, a rope of this from w?s ba senl to the Norlh Carelloa DEIINA Lrsldkdlion nlflre (I,e. 1T,M1 ul Iwid, ine urrert OrC serratirr, nut of I¢mp, Inrnrserl ratiuiecrsY Page 2 of 4 0 M N [9 4 ! M r7� CHAIN F cal Request Document aCBAlt�fy'7Cd1 ra. a .ac cxr • , tErx 3oCrRREM. . y. �a..w,en w Sncsbn C s.euen c rpr: d I R..rrr d. wee...r: ..avw•� .r..a �....a- I...o ..dr..ee- Ir tuV>� "�'��• I i .er ILA. -- „°"•••p�. VoY �a-co r°0j•' 'pGAlZL2-- !}Lrlr i:E6vs.wTomrwcEucr (-P b Q NPOES i GF* a"7wA7Sk PRW"4.TCq ra.. ....c.o.... -, 5 •:� r* Ls- f- ,sst,. r or.lEA re: rw.• avr i..: r � lti. ' cJ U A•rx..•t. ccf=. _ ..3'�e •F i�� 4/ 7L?`3 �' t.•o.�,••...,� .,.,.. ter. l..c.ew, r. arE- R"..+ MatyW r'ke•e•'asi�`� s.msl9 11 } ! I I I I I cc� e'TEa I Presrr yrx i 1 I I SAMPLE M -,'r_a! ..el V I if CIO ��� � C �_ n � I � i � :+.'E I t1✓_ I tlu: I i ��41 � 1� I� f I = Ma.� LsC i.c. ne i C' 1 3-tie?! i I I s l l l l !! If iiIIVIII � I l k I I l i I I4l I l l s I l i I I 1 1 t l i l f l l l I k i I S I I k l i t I o I I I 11 11 ,5 I 1 1 1 I I l t I I I I 52 .:aorra..ace..IZWN I W w=MaoY,.trw,KW I DAM ,wee {� Ieor�o-�a.,AtrKyrno-, i o„F I swT s.MPtcoawrM.a I I i I i I I RRtlry..ti.eryWtlR: r Y� I �Et �t I '�,.+�*�.'i.wa.rrrt....-.kre r.r.•✓tYw.�.rs.re.p.r.n �r �..•.•x.. �+w.Y.-.U. �n o.e.m.L rwa. FtL'L^d2•JL.Di. 15-tis�-20�i J/ Sample Candllion Upun Racclpt! CURL 'r-CAA-QA,003-6__ev.0.2__ +a + *Check mark top half of box if pit and/or dechlorination Prof llw! is verified and withlo the acceptioce rat[ge for ' _preservalian samples.__._____ '•Bottum half of box is to list number of t)otlles k CLI 2 tip v :� i r i t cr � e 7 S •' v '71 J u a' 7 o y n �n Y. ri 7 z i3 7 Psge 2 0l 2 ! p t Due➢E;DaI a t 03/2CY117 i 91 r- n 7• t', [J [ a � E r' S p � � 1Y w � 5 .yy+ ,7�a� [1� � a�dr :� J✓' :i 7F r�i pH Adjustment Log for Preserved Samples pe of Prr.wvm!�, pltuponre[aipt Moe presenatlonadimted Umeprosomaeon adjusted ofpresp.mallre Lot Added Page 4 of 4 ceAnalytical www.P&CMabscom Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Pate Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)634-4984 Page 1 of 1, Report Date: 06/09/2017 Date Received: 06/05/2017 Project: SITEL GP Pace Project No.: 92342863 Sample: SITEL GP Lab ID: 92342863001 Collected: 06/05/17 06:45 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B Turbidity 3.9 NTU 0.50 06/06/17 15:05 SM 2540D Total Suspended Solids 6.2 mg1L 2.5 06/06/17 14A3 SM 2540F Total Settleable Solids ND mUUhr 0.10 06/06117 13:47 EPA9040 pH 6.9 Std, Units DAD 06/06/17 15:18 1-11,1-16 ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by: -'"""' Terri Page (336)623-8921 terTi.page@pacelabs.com Eden Certification tDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 Page 1 of 4 Document Name: ESP Twit Spec Document Revised: Sept. 21, 2016 sam le eandltMn Upon Recet t SCUR page- i of 2 ceMaWa1 • Document No.: Issuing Authority: F-CAR-QA-003•Rev.02 J Pace Quality office Laboratory receiving samples: Asheville Eden[] Greenwood Cj Huntersvilla ❑ Raleigh®�Mechanlre•atl f1 ----- � 9II 2342 13114I � I2 WO# • Client Name: C]�Iia Project Courier: Ex UPS USPS At 1111111 commercial []Pace []other: bII 863 J Custody Seal Present? Dyes [KIL seals Intact) Oyes du wtellnlnals Peron Fyamining rnntents: Packing Material: ❑Babble Wrap ❑Bubble Bags 9�ona ❑tither: Thermometer: �.( ®IR Gun il), �15.3492 _ Type of kek Afwet ❑glue QNane QSamples an ica, coding process has begun COrrectlan Factor:,-b Or Cooler TempCorrected ('Cl: 313 Biological Tissue Frozen? []Yes ❑No )KNJA Temp should be above freezing to 6'C USDA Regulated Solt [0 N/A, water sampfei Did $amp]gs prigmate Quarantine tone within the United States: CA, NY, or SC (check mapsl? Did samdes ariginata from a foreign source (Ntgratkmally, ❑Yes a inctudlna Hawaii and Puerto Ricci? Dyes jW90 CommentsJOlsuepan Chain of Custody present) 1. Samples Arrived within Hold Time? 2. Shan Hold Tlme Analysis 102 he.)? 3. Rush Turn Around Time Requested? 11 Cl El 1 4. volume? 5. —sufficient Correct Containers Used) -Pace Containers USedi 0 Ej 6. Containers Intact) U U 7. Samples Field Filtered? 8. Note It sediment is vhible in the dissolved Container Sample Labels Match 000 -includes Date/TimeAD/Analysis 9. Headspace In VOAVials (a5.6rnm ? Yet No N 10, Trip Olanit Present? Yes No N TripBlank CustodySeals Present? Yes Na N 11. CLIENT NOTIRCATION/RESOLU710N Person Contacted: I Comments/Sample Discrepancy: Review: Prefect Manager SRF Review: Field Data Required? UYts UNa Date/Time: Date: G Date: i Nate: Whenewr there is a discrepancy affecting North Carolina Compliance samples, a copy of th'nNem Will be sent to the Nonh Groans OEHNR Certification Office (i.e. Out of hold, intern preservative, out of letup, incorrect containers) Page 2 of 4 It 0 CHAIN -OF -CUSTODY 1 Ana"cal Request Document Tn Gr.at.®T .. LK.N DOC+srtM. AN ".r F. — r m.p.e.n.0a.9* ceAr>afytiu!' r� - .. 7E r� i - ■�©ems:=-mo I—w FMB --w--A .WTUs.—.— Aw .ALL-0420I OT, 7SMw200T V O Y S 5� a s = v � w 3' Wa 0 Q a A 1 3 m f a l a 1� N C » a m rfl rn A O in MOORE am mom NEEMEN MEMENEEMEMEN ............ ►N V 7 5 N co �w A aceAnalytical® wwwPetefatu.00m i Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92356255 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 09/26/2017 Date Received: 09/22/2017 Sample: SITE 1 GP Lab ID: 92356255001 Collected: 09/22117 06:30 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA 180.1 Turbidity 14.8 NTU 1.0 09/23/17 14:18 SM 2540D Total Suspended Solids 9.2 mglL 1.0 09/26/17 00:25 SM 2540F Total Settleable Solids ND mIJIJhr 0.10 09/23/17 14:53 EPA9040 pH 7.3 Std. Units 0.10 09/26/1711:00 H6 ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by: \� Terri Page (336)623-8921 terri.page@pacelabs.com Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 UrginiaNELAP Certification #: 460222 Page 1 of 4 --tahorataryrcce9vtrrg•sarnales- --- — -- -�~ •-- .-- w _ =. __----=--_----- —_ --- ---..— Asheville Eden GreenwoodHunters,�--`v_.._ ❑ ❑ ❑ f -'O# : 92356255 CffentNsme:� 1 �(�/{.aiv w /!/��� Projeri Courier: Fed Ex LjLrps LJUSPS ant ❑ Corrtmerdal []Pace ❑Other._ 1 92355255 —C++3tS�7Pl�iemT--�Yef-- -—Seairtrttatti—•-01'es — �r^.�--.,.�.� � _ DateJtaklak Person Eaminkta Cernartta: �� LG-'ri Packing Material: []nubble Wrap []Bubblegags ana J_] Other Biological TtssuaFrozen? �QgIW QNane []Yes ©No Q**— ~ ^-"•-eealer-Temp Com[Rcd ('C)r— • � OSrnplp out of trmp emerta. Sarnplu On la, Caoerea txocm her beaoe i@( vraterpmple} a quarantine lone wlthln the UnitW Statas: CA, NY, ar SC (check maps)? pW sanaler ortpeeate Irma a Porettn rOtrrte Pmenu _ ........ -.. _.. -._. _ ... ,. .. .• -•-'� Indudu Ha+.'7q Comma Ic Chain of Cup Present? No A L Samples dv thlnHoldTime? cr No kJA' 2. Short Hold Ti rm Ana 1i 107 hr.)? M4. A 3• R-hTwn A and Time uestad er o N JA �. Suffft ant Vol me? n He NJA 5. Correct Coma -Pace Con ners. Used? InerSUsed? Yes L11e, No ❑NJA ONo 0111A 6 Containers Intact? u 0 "'A Dfssohed an Is: Samples Ffeld Flhered? d No A e. Sample Labels 1ch COC? .-Inchrdes 1e/T1m[flD s Mat&' n Q❑ Na HfA' 4. Heads ace In OA Vials >S-6mm 7 ny. nuo NIA lA Trip Blank Pr Trip Wank Cus nt? d SCalf Present? []Yes es []Ho Nn NJ4 N A t1. UIENT NOnR TIONJRFSOLUTl0N PersContact on Comments/Sa4e Plsaepancy: I Date/Time: ..M Wra wequ—or tJrG 6,1no i Project Manes r SWRF Review: Gate: ! Project Mini SRF Review. Data liate: Whenever th Is a 69rnrpang aNecflrta North CAMIns campNance tampkf, a mPY Of this farm vAll he sent to the Honh CAMMU CUM CuuBoUM Office 11.0. pot of hold, Inm pressmthe, net of temp, tnmrrett containers) Page 2 of 4 CHAIN -OF -CUSTODY 1 Analytical Request Document CEAnalytical TTw Ch&H%tftdT d a LEGAL oxueh+T. AM r9*M% S&M mud n. oaran.d .marey. Baalan A ISCUM II Badwn C A.qupe pan.aa"Mma R.WAbr-d ggea.mvmariri V—rctorwar P,p,: a c "M'o . r opRf. 4tpT�Lf +JT (� " pEGULATORY AGENCY 'aOEGAlC. �75 4 WWATER Ens. io. . M1IGri ACtN't= . Cc7ri ° 'aW ddr ra.: «� S UST I RCRA OTHER r Pww 871a L=sdm It.ar..r Ow o. MTAT: NW*W IN✓i.. srATE —'j R*gtwstW An0f k. FBUMd fYAf! _ _ n v.pd MMds C.. ad nor., nlrr. r.emrr Fb1:� nr..aerwT. e.t f COLLECTED I 71 +i rs. .m 9 r�r?+nt � �n 0 .auuuo � 8 SAMPLE 1D a.vyM is vUTT ICE UNCLF to,w t/ U F i 6ATE 7I.IE MTL Td.F Y 1 ADOMNAL C*UULVTe ri.Lowunkeb ST I AEE1 A OMTE TWE rtA►Ea... Mod I MATE LWE BAMpLa CONCITION4 mod" A-1 &AMPLER NAME AMD SMUTURE ER7M N.m, r LkIPPLM $ p S F•ALL-04MOMV,06. f 2-0CI-M7 _ - Document Name: - - Document Revhed:July25,2017 �• Sample Londitlon Upon Recel t SCURIL : • . �. , Page 2 of 2 Document No.: �` ■■—■sss—��aa 3�ai311t r-CnR{5-033•Rev.o3 WO# 92356255 _Checkmarktof2lta jj�f-box 7pF�>3n`71CoL dj-ch1,itn—A1Din _`_77 Is verfflsdjand wethln the acceptance range for PM: THP Dug Date: 10/02/ 17 preservatmn samples. .BottomIIhalf of box is to list number of bottles CLIENT. 91—Wade Moor 11 ra man ■ �ii \ ■ IN BONDS I on s 11 ON DOE 0 USONk my I daemon m S some so 'a ONE one no In on 6169, on WN, 0 ONE so was Ilk Do- N I Sk IN MEN on p" Adjustment Log for Preserved Samples Semple lG Type el MewvaUrt PH W;an MMPt Vmpraumtlnnedlwted TIM Plutrvadon Artwlun alprcxrvetlre edlwtel edded lat 1� Page 4 of 4 r lacmnalytical' wx P&Ce18fM " Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92366931 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of T Report Date: 12/21/2017 Date Received: 12/13/2017 Samplo: SITE 1 GP Lab ID: 92366931001 Collected: 12113/17 13:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B Turbidity 20.8 NTU 0.50 12/14117 13:48 SM 2540D Total Suspended Solids 14.8 mg1L 2.6 12/18/17 15:43 SM 2540F Total Settleable Solids ND mUUhr 0,10 12/14/17 12:39 EPA9040 pH 7.8 Std. Units 0.10 12/14/17 14:16 H1,H6 ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by: Terri Page (336)623-8921 tern. pag a@pa celabs .com Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 Page 1 of 4 Document Name: Omment Revisad: July • Sam le Condttlon U on Reoei SCUR) PaSe 1 of 2 Document No.: Issuing Authorlti Ash )Ile 0 Eden❑ Greenwood ❑ HUntery WO# : 92366931 Client Name: 94 tfec Courier: []Fed UPS ETUSPS� O Qn�I ��� �■ Ir �� �I� ��� ❑ Commefdal ❑Pace ❑other:_ L92366931 Custody Seat Prese t? ❑Yes PAID Seals Intact? ❑Yes O r o ii Oateftnfl4lrPerson rramtatnjCentents• Paddry Matartal: ORubb)s Wrap []Bubble Bags [None ❑ Other Biological Tissue Frozen? Thermometer: ' \\ []Yes❑No RN/A ❑IRGun e- S' ` �Gret ❑Blw {Mona Typo of Ira: �7 �fasiedlnafer3or� LoolerlerppConected f_C}:_._.... .� � .. _--- -Terttp should he shove frcei4tgto 6'C--- .. _....._.. _.. . ❑Umples out of temp riReda. Sampler on ka, coding process 0%k* has "gun USDA Regulated So I ( RN/A, water sample) ' Did samples original in a quarantine zone within the United Sitter: CA, NY, or SC {tha() maps)? Dad sarMleseNabiate hen a foreign source lrqumslunsW, flu.. 1"9e.. s .d.,.w a.,..... qi.n»rlv.. MS 1.. ianmenu Phtre aY. plain of Custo Presents ru Nq N A 1. Sa esArdredwithin Hold Time? us No NA 2. Short Hold Time a sus 02 llr.t ela,, EINO ONIA 3. Rush,rum Aro Ttme Requested? nets No N A �. Sufflclentvolum 7 Na nNIA S. Correct Contain •Pace Cantaln %Usad7 n Used? 311, as 0Na ONO ❑NIA OWA 6. Containers Intad No N A 7. Dissolved ansirs : Samples Field R1lered? E5,1A a. Sample labels -Includes Dat tthCOCt me V&a Is Matrix: Yes ❑No ❑NIA 9. Heads stain VD Yals �5-6mm ? rn No NIA 10. TnP OIanl Prese Tri DIanl Cust I Seals Presents R. Mytj ❑No ONO NIA No, 11. CLIENT Pelson, Discrepancy: s Datemme: Field Date Requ:red7 IJs'as UNO Project Manager SCURF Review;Oats: -A `.1_? /.ITT I Pro)ect ManssaO SRFRevfaw: l A I. NOW whenmw thtri is a dlsuepancy Aff ct3ng North Urdinaa compliance sampks, a s»pY of IN' farm net be sent to the north Cafolm DEHNR Camm ation 011101 p.e. Out of hold, incanaa 1 WGIrvailve, out or temp, Intones conratneny i Page 2 of 4 Q O �S:cnon A S-1— a A—b" C M Memreae a Y*we PR MWnrsp.t CHAIN -OF -CUSTODY ! Analytical Requast Document T m LE CAL DOCU EW. Al n bWds R" ev —0aocftWI. 8-9— C M D, � 54-Io MWoet ,,� TCw REGULATDRYAOEMCY p 4 It N G. J I S41 K S L AJ � %� MPDES r cMOUfm W►TER r DMMKNG WATFM L,w TO Mcx PvsM .w orJ�w: o,•. {- V3T t• RCi 07n ER r dwttntua. JOi 7119Z Z�I d �tn .__— alb �x+eo Wind Or Y AT—T: — r7 D Wt?a C`e = Arwrbtis�Kw M�rPv COLLECTED P.Wq nMw +ftw Yrwr S z PM*Aur MIY naw.i v p � w TesSae Sl SAMPLE ID � L [+4L 54.•.4 - M s.,a.0.ULSTa°_MOLE T OT a M c � � oArr t.A� e.re Turt LD. - - -- �_er :-r=e��s-:-rr*ram-`:-•��Q�l % �Q f 1�fE.'♦ *.a' ;����►I�J®�ll�J'.:'ll WE MmsmE l i► lvi RAYPUR MAMA AM a1LTlAiVRE V PIMT Mr.r M i..M.suc _ 5 gyY L L L 10MATIRIt M a+rLH! OAR abase K i _ peemWm n �v.�+ � 4 vv r sp �� re•s n,.. KT!! r. nr++rr .r.w�w �r wr � uz �.w v w ..w... sr .r.n..n KJi[LDaiDwA7. 1S4h^xa.7 Document Name: Document Revised: Juty 25, 2017 ceArrarytira!' s,m le canditlon U cn ReceO" E�-OocomentNo: W0#� ; 92366931 f-CAR CSA33•Rev.0 w Ogheck m p hh@If of box ,if,PH and/or,dechlarinatlon PM: THP Due Date: 12/23/ 17 Is verified and ithln the acceptance range for preservations triples. CLIENT: 91—Wade Moor ••Bottom half ofbox Is to list number of bottles Rol 0 ONE E on so Nolen I 110 monling am mono somenom- Engine men on no on MM1G0MMM on SEEN as 0 SEEN= :1 Page 4 of 4 ANNUAL SUMMARY Dl -IR -WASTEWATER SEND TO CENTRAL OFFICE* PROCESS NIINE/DEWATERING WASTEWATER GENERAL PERMIT NO. NcG020000 *Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Permit Limit Violations) by MARCH 1 of each year. If you have limit violations, you must also have turned in a Limit Violation DM_ R to your local Regional Office_wiihin 30 dates of receiving sale results_ from a lab. CERTIFICATE OF COVERAGE NO. NCG02 D D j C) SA,A11PLE COLLECTION YEAR: 1 4� FACILITY NAME: Ekm ► t COUNTY: FRR niKLt r\1 PERSON COLLECTING SAMP S: ,_v r ax,rX s PHONE NO. iLi) CERTIFIED LABORATORY: ace Lab # ADD TO LISTERVE? YES ❑ NO® EMAIL: bt re�►�rynyW sel� ntoo�r�_ Lab # LUVHTS VIOLATIONS? YES /❑ NO ❑ INDUSTRIAL SAND'? E� DISCHARGING TO SA WATERS'? ❑ Part A: Wastewater Monitoring Requirements Outfail No. Date Sample t C9116cted 50050 Total Flow 00530 Total Suspended 1. Solids 00400' Turbidity . . 00545 . Settleable Solids , -00400 p$ 31616 Fecal. Colfforms - mm/dd/yr MG mg/I NTUW, mill Standard coVml ' 3 / (o. D S, N� ? J,:. 5 111J NO S r � CENTRAL FILES ' All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits. 2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term. 3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. 'Turbidity may be monitored at the Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge. 4 Only facilities discharging to SA waters are required to monitor for Fecal coliforms. Permit Date: 1/1/2410-12/31/2014 Last Revised 01-05-10 Pave 1 of 2 Part A Continued: Wastewater Monitorine Requirements Outfall No. Date Sample Collected' 50050 Total Flow .00530 Total Suspended Solidst 00400 Turbidity 00545 Settleable Solids 00400 pH 31616 Fecal Coliforms - mrn/dd/yr MG mg/11 NTU [no Standard col/ml-44 MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LOM VIOLATIONS) BY MARGIN J OF EAR YEAR Tom: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CER TIFICATION FOR ANY FIYFORMATION REPORTED "I certify, under penalty,of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that gii"ed.personnei properly gather and evaluate the information submitted. Based on 'my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aw that there ar sign' can ;penal ' s for submitting false information, including the�ossibility of fines and imprisonment for !mowing violations." erQJUJv201 (Signature d Permitted (Date) Ai Permit Date: 1/1120I0=12/31/2014 Last Revised 01-05-10 Page 2 of 2 aceAnalyfical wwwpK431obs.com Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: 934 FAST RIVER RD LOUISBURG NC Pace Project No.: 92289869 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 03/21 /2016 Date Received: 03/14/2016 Sample: SITE 1 GP GRAS Lab ID: 92289869001 Collected: 03/14/16 06:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B Turbidity 17.0 NTU 0.50 03/15/16 16:15 SM 2540D Total Suspended Solids 17.6 mg1L 2.5 03/17/16 10:58 SM 2540F Total Settleable Solids ND mL/Lfhr 0.10 03/15/16 13:30 EPA9040 pH 7.4 . Sid. Units 0.10 03/16/16 08:15 1-11,1-16 Sample: SITE 2 RP Lab ID: 92289869002 Collected: 03/14/16 06:20 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B Turbidity 5.4 NTU 0.50 03/15/16 16:15 SM 25400 Total Suspended Solids 6.0 mg1L 2.5 03/17116 10:59 SM 2540F Total Settleable Solids ND mL/L/hr 0.10 03/15/16 13:30 EPA9040 pH 6.7 Sid. Units 0.10 03/1611608:15 H1,H6 ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by: Terri Page terri.page@pacelabs.com Edon Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification M 37738 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 Page 1 of 5 aceAnaiytical www.paceialm.com r j 6701 Conference Drive, Raleigh, NC 27607 ph: {919) 834-084, Imr. (919) a34-M7 NCWW CerL#67, NCDW CeO37731 Chain of Custody w.a. VZ �J 1 ca-5 -f-- jet QuI r �./ V r l , '. Report Resu'V o; Company: j u4a �(} co Address: C) ao —s4j— �shukA tJc� a�sg Attn: Phone:—�`- Fax:— Sampled by (signature); all TO Projsct Reference: /VC a 7 5 Project !Number: Puruhase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (wlsurcharge) "Rush projects ara subject to prior approval by Me lahoratory Requested Due Date: /L---- —� 3 d_ 5' V ftel ed by (sign Receiver! 519nature) 3w Tune Rehnqui by (signature) Received by (signature) Time Res. Chlorine: ❑ Absent ❑ Present Cl n/a Acid preserv. c2? (] Yes ❑ No ❑ nla Base presarv. >12? ? ❑ Yes ❑ No j;1 n!a Page 2 of 5 Document Name: Document Revised: 26FEB2 016 dC£ifiFlaiy�lC21• Sample Condition Upon Recelpt(SCURj Page I of 2 / 'y+ Document No.: issuing Authority: i F-RAL-CS-001-rev.93 Pace Raleigh quality Office _ Page 2 of 2 for Internal Use ONLY Sample Condition Upon atent Name: fAAI �PmJeCt�) v - ijCourier:Fed Ex UP5 LISPS ❑ Commercial ❑Pate ❑Other: Custody Seal Present? [-]Yes �No seats intact? []Yes ONO Date/InWals Person EramfnIns' Conten Packing Material: ❑Bubble Wrap ❑Bubble Bags ANone, ( ❑other. Thermometer: iR SN:122065387 QIR SN: 12206S371 Type of fa: fLiWet ❑Blue []None ❑Samples on ice, cooling process rhas begun Correctlon Factor: .o'C Cooler Tamp Corrected ('C): Z , fj 8ialogical Th we Frozen? (3Yes []NO.' LdN/A Temp should be above fr sing to VCT USDA Regulated Soil (;N/A, water sample) Did sample; originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, nVnc Nn Inrli,dinn Havrali and stuprtn Rirni? rlYnc Mi COMMENTS: Chain of Custody Present? Yes No N/A 1. Chain of Custody Filled Out? Yes 0 No N/A 2. Chain of Custody Relinquished? Yes ©No N/A 3. Sam pier Name and/or Si nature on COC? Yes ONO CINJA 4. Sam piesArrived within HoIdTime? Yes E31do N/A S. Short H at d Tim e Ana lysis (472 hr)? Yes ❑No El N A Rush Turn Around Time Requested? yes UNo NIA 7. Sufficient Volume? Yes ONo QNJA 8. Correct Contalners Used? I/lYes []NO QN/A 9. -Pace Containers Used? V tx MN. A Containers Intact? LJyes ONO []N/A 10. Filtered Votume Received for Dissolved Tests? ❑yes []No N/A 11. Note if sediment is visible in the dissolved container, Sample Labels Match COC? YfYes ❑No []N/A 12. -includes Date me !p Ana sls Matrix: All containers needing acid/base preservation have been 13. checked? es ©No []N/A All containers needing preservation are found to be in compliance wit', EPA recommendation? (HNO.0 HrSO4, HCk2; NaOH >9 Sulfide, NaOH>12 Cyanldej ]Yes ❑No ❑N/A Exceptions: VOA, Collform, TM, Oil and Grease, DR0/8015 {water} DX,LLHZ Yes ❑No []N/A Samples checked for dechlorinatinn Yes ONO []N/A 14. -HeadsE2ce in VOA Vials (>5-6m2!? Oyes ❑No N/A 15. Yrip Blank Present? [[Yes []No N/A 16. Trip Blank Custody Seats Present? eras ONO N/A Pace Trip Lot S tIf purchased): CUEWT NOTIFICATIDN/RESOLLMON Field Data Required? []Yes []No Person Contacted: Date/Time: Comments/Resolution: Project Manager SCURF Review: Date: Project Manager SRF Review: _ Date: Nate: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification office (i.e. Out of hold, Incorrect pre servative, out of temp, Incurrect containersl Page 4 of 5 Document Name: Condition Upon Reci Document No.: . Document Revised: 26FE82016 Page 2 of 2 Issuing Authority: m a m 10 m 0 to a doM en m a. m C7 C7 l7 19 i'J M m [9 L7 L4 ' .J � O C a N N 0 0 $ In ca m Vi 1 I �- z 'r Client Sample 1D Sample Discrepancy pH Adjustment Log for Preserved samples sampie 1D Type of Preservative pH upon receipt Irate preservation adjusted Time preservation adjusted Amount of Preservative added Lot 125 ml Plastic Unp: BP4U 250 ml Plastic Unp: BP3U 500 ml Plastic Unp: BP2U I Liter Plastic Unp: BPI U 250 ml Plastic H2SO4: BP3S 250 ml Plastic HNO3: BP3N 250 ml Plastic ZN Acetate: 0113Z 250 ml Plastic NaOH: BP3C Wide mouthed glass Jar unp: WGFU 1 Liter Amber Unp: AG1U 1 Liter Amber NCI: AG1 H 250mi Amber Unp: AM 1 Liter Amber H2SO4: AGIS 250 ml Amber H2SO4: AMS 250 ml Amber NH4CL: AG3A 40 ml VOA HO: DG9H 40 ml VOA Na2S203: VG9T 40 ml VOA Unp: VG9U 40 mi VOA H3PO4: DG9P 5035 Kit: VOAK VPH 1 Gas Kit., VJGK 125 ml Sterile Plastic: SPST 250 ml Sterile Plastic: SP2T 250 mL Plastic (NH2)2SO4: BP3A 20 ml Scintilla#ion vials: VSGU Page 5 of 5 ' � m aneAnalytical 2 w wrpaceiahacom i Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92303562 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 {919)834-4984 Page 1 of 1 Report Date: 07/13/2016 Date Received: 06/3012016 Sample: SITE 1 GP Lab ID: 92303562001 Collected: 06/30116 10:50 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2540D Total Suspended Solids 23.9 mg1L 3.5 07/05/16 14:34 SM 254OF Total Settleable Solids ND mLIL/hr 0.10 07/01/16 11:30 EPA9040 pH 6.4 Std. Units 0.10 07/01/1612:50 H1,H6 EPA 180A Turbidity 26.5 NTU 1.0 07/01/16 22:30 ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. Reviewed by: 84 fJ Brittany Gibson for Terri Page terri.page@pacelabs.com Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Ftorida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification lDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 Page 1 of 3 ���� N L [Errprpll u on x.n I xa p. 3 d? Oouranl Np; Imm� AplMrin: 1#A4O�0pl�axM IIn RW QW: OKkil ' WOE : r�liil����i11 r"ccr•�r[.lwr �� �� o:.,! 1923g0j3562 �� IM1I � III � p a...dr l..InW.mr prn 4- rrl xn.cll C1[r. �]ra 11l.�IflP ruilYU.b rw+pr [.rY•q [nM .u,1,Abi p"'''[�'C' ....Ip wr..la pxpbbnwrvl pLutm axa 9 perM,:_ Thrmrn.n. T15D5 ryr.r pRw pxL. cpr,.[arp r..mrere cwr.T.xrce,[.dr fqr �,l px� OIW�rt�arMr•�r`�yy x.pxr KrWdwlrx... rrp...l p'[en pw Q*r• r.mR lxpaa lr llo.n groeC VSnI R.pd.4d dpx f [C} Kk rn. —."l Gd,r• aHpnxeb.xur.nMr. mravnrd.Ihr Wdt.d 311x.r fti xr, prx klr[.rxrxH Qrn W..,xrM rMb.r Wn. erw....r pm«1.rri.lx rs..,. wrdxW rrr..l.mYRr.. G!. urnd pww.17 • S.m .MrlwtlxNhM Held ryerli 7 sxr,nw lw.,w .nx.. w RnbTw •,oral ll�. w • a Suaknrr.VKum.l m w S Cpn.tl f<nhMaVrlr Ow EJW 6 Caxr.nxn xxpRl 1. swy.l lira r,wrm xp A x. xurl r.dm.nlxxxxrra v�p.rual ea+ulw II�x1a 1pMl.wulrrocl m pw pw+ / w mx.ura. r.dnlneh.. wr.mm�Mwe..r, Ip „�W <rc1AE1 f54r pxo pwA Al [RaptxlR MrdlN nrrrvrm..ry AMrrdmWln [rnplarw vM[pAnmrrmprrtl.tbnl �rw. Irr[1. Kx0. a]2 xNa yxxlyr. xppryll [F.+yY Ik [WA ..0 Iw.pao�YtY, CAlom�l0l,d W Guw DW 14 OOClI .�.'i•w s•mg.r sx....d yn.rrrdr..xyr> ' Wrrrprr MVM N.b.5 l 11 CIN, A U. T,bw,. na,rrp Qr. Co.. IL Irr Wn(ylrll'Irx rrerntl prr Orr wA p.n irp xWr.>olx KWr[Mrd + nRYrKdAIWIIpxdR[SdYrpx NW mbVl ,tr prr ON, wmon iawnaa: a�,rrM.jLrrgY v.r[repncY w.l.11 r.xyr fCM RW., OWN T rr.Ho Rrrxpr.xp R.Nr,.� Rrrr ___� wr: W.swwuw Y.dann•ra r,4xRr..n.� .wrx. rArrr..rmrwdR r.n.rl rr,..ww wm . dsa y, Oxrd.dd Ixmrnv nwhYw, rirl.! rPI1LYw�r. u.'rrrr4 P.p.l W 3 F l.[.r.d milliAI milli CY C I iI� r�o2'rtsnv:r•u,.r w+w�o .aumr.�w»a / aceAnalj cal www.pacelabs.com 6701 Conference Drive, Raleigh, NC 27607 ph: (919) 834-4984, fax: (919) 834-6497 NCWW Cert#67, NCDW Cert#37731 Chain of Custody W.O.* Report Results To: Bill To: yyf S Company: RQIDP_�-- Address: � � i L-k 7)�-5� Attn: l.tl� lj u Phone:�rj�1..1.��3 f Fax: Sampled by (signature): Project Reference: Project [Number: Purchase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) "Rush projects are subject to prior approval by the laboratory Requested Due Date: = �a�ys leescn P lto�n. ' � t: r a a4^S. S5ttaartT'�me .N EniDate�S„a EndTi IVIatnx os�� � �FfM1r1-Da4 FM�'Mc" s � im P�HH F!Sl'.es .. i - JI LE }�1�7/4i4rt7 1 �R1+ -. M-1 — tzL = k / 1 1.4 q. / t Relinquished by (signature) Recei`ved!by/(signat%i�e) ' !��l{Y�JI�EtII�A(VJf1� Date %. Time Relinquished by (signature) Received1N (signature) Date i Time Relinquished by (signature) Received by (signature) Date Time Receipt Conditions (Lab Use Only) ❑ 4t2°C ❑ Temp: °C Res. Chlorine: ❑ Absent ❑ Present ❑ n/a Acid preserv. <2? Yes ❑ No ❑ n/a Base preserv. >12? Yes 0 No ❑ n!a 1Y�IaceAnalytical rnnr.paCEraCs.GGrn i Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: SITE 1 GP Pace Project No.: 92313959 Pace Analytical Services, LLC 6701 Conference [hive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 10/04/2016 Date Received: 09/28/2016 Sample: SITE 1 GP Lab ID: 92313959001 Collected: 09/27/16 07:55 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers SM 2130B Turbidity 107 NTU 0.50 09/28/16 14:35 SM 25401) Total Suspended Solids 65.1 mg1L 4.9 09/29/16 13:14 SM 2540F Total Settleable Solids NO rnL/Llhr 0.10 09/28/16 15:30 EPA9040 pH 6.2 Std. Units 0.10 09/30/1611:45 1-13,1-16 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. \&`U Reviewed by: Terri Page terri.page@pacelabs.com Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 Virginia[VELAP Certification #: 460025 Page 1 of 3 fl U Document Name: Document Revised: May 24, 2016 Sample Condition Upon Recef SCU Page I of 7_ r- ' �`"�• Document No.: Issuing Authority. _._ F-RAC-(3.001-Rar.04 _ Pace Raleigh AualiryOffice Client Name: _ eject Courier LjFedlEx UPS USPS 00lent ❑ Commercial JDpace ❑Orhtr_ ustody Seal Present7 []Yes ONO Seals Intact? ❑Yes ONO D.e.lartitlak Person buminins -Waco f% Picking Material: ❑Bubble Wrap ❑Bubble Bags None ❑other: 'herinomeUr: T1505 Type ofky; owet cimue [_mono❑sampsasnnRe, coding wocasshasbegun :ormctlon Factor: 0.0'C Cooler Temp Corrected ('Cj: Z, Z Biological Tlssua Frozen? Oyes ❑No Q�/A emp should be above fr eIn' to 6'C SDA Regulated Sol (J N/A watersamplej Idsampte origlnateinaquaraminezone within the United States: CA, NY, orSC(checkmaps)? old mmpiespdgrnatefromafarelgnsource ftn�y ationaitg, 1Yes 7No IndudinattawaltandPuerto Alcol?MVes UNo Commerrtslfllscre lain of CrutadY Present? e. No WWA I. trclos Arrived within Hold TIme7 Yn NoE2111, 2, tort Hold Time Ana s (a2 hr.)? s o NIA 1 f jib 7umAroundTime Requested? Dyes RfNo [3NJA_ 4, _ sffklentVolume7 �ftes No CJNJA S, 10W CnWners used? 0. []NO NIA 6. PaceCantalnersUsed? _ 9fYes No A _ vste!nerslntact? Uv., nft ❑N A 7. Im FteldFgtered? QYes[]NO A 8. MotuIfWdlme(4isAsUetntho&sdYWconUiner Imple Labers Match CW. Oes ©No ❑NjA 9. -IncludesDate TlmejilTlAnalysls Matrlr.��� -� It containerspeeding add/base preservallon have been 10. r ietked? Yes [:]NO ❑N/A A contalners needing preservation are found to be in MOjN amptlance with EPA recommendation? Z, wroap.r ANO„ HAC. HCK2; NaOH 4Sulfide, NaOH>12 ryanlde] K ❑No DIVA eeepuons: VCSA Cohlorm, TOC, Oil and Grease, A0/8015twaterlDOC,LLH Z. No N A a_mplest_heck_edfor dernoAnation7 _ es No A 11. eadspace in VOA Vials p5.6mmj7 yes No A 12. rtp Blank present? Om❑Na NIA 13. rip Blank Custody Seals Present? ❑Yes []NO NIA, ace Trl Blank Lot fr IT urchasedj: CLICK NWIFICATIONIRESOWTION Person Contacted: DateflIrrm! Comments/Sample Distreps Rcy: PlddfradRequMA? UytS ❑Na Project Manager SCURF Review: Dam C�^I7 te: yr" Project Manager SRF Review, _ LJ - Da - t� V No:tr Whenever there Is a dlscrepauyaffecttngNorthCarollnacomplianresamples,acopYofthlsformwltbesent tothe North Carolina Di Out o! hold, Incorrect preservative, auto( tamp, In=recr containers) office Il.e. Page 2 of 3 aceAnalytical' rwr.y.alab�. (11� M1 Ctximmm vrke, ftva h, NC 27007 ph: (919) M 4W kX J919) W4-0497 NCWW OwW7, NCDW CertiOTni Chain of Custody PC,KP W.O,0 Report Resupa To: ©III To: cgrnq=y:11SIDE &Gq+ _I e: �QUrP eb Project Raterenc Address:- F a- I�JW Z44. _ �,u kt stnu,r a r, Pf*ct Nurrber: � rr Attn: uN Atwp-5, Purchase Order #: Ph": ��4 — 4,4�- 374 0 Standard Report Delivery Fsx: 3! - _r sa _ g��_ ❑ Rush RaW Delivery (wlsureharge) ••ALah wooer we wga+m car Wpmm W IM 1AWAlny Sampled by (Signature): Requested Due Date: fir° `�55 t kr�lCrr r R Shed ( s Date Tyne 11 41 x C r l TW (La� C r ❑ 4l?'C ❑Temp: 'C JJLXF` Rea ChWm: { a7e Tire ❑ Absent ❑ Presort ❑ nta Add pwwrv, t2? strjd by (s�nanee} Rene wed sign xe) NOy lkne ❑ Ws ❑ Na ❑ NO Base pregm,. -127 ❑ Ws ❑ No Q rda Page 3 of 3 aceAnalytical jwwwb&cam Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: GP Site 1 Pace Project No.: 92319224 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 . Page 1 of 1 Report Date: 11/15/2016 Date Received: 11/10/2016 Sample: GP Site 1 Lab ID: 92319224001 Collected: 11/10/16 07:00 Matrix: Method Parameters Results Units Report Limit Water Analyzed Qualifiers SM 21306 Turbidity 17.6 NTU 0.50 11/11/16 12A0 SM 2540D Total Suspended Solids 24.2 mg1L 2.9 11/11116 10:00 SM 254OF Total Settleable Solids ND mUUhr 0.10 11/11/16 08:30 EPA9040 pH 6.5 Std. Units 0,10 11/11/16 14:20 H1,H6 ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H6 Analysis initiated outside of the 15 minute EPA required holding time. \AA)� Reviewed by: Terri Page terri.page@pacelabs.com Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaA/EL.AP Certification #: 460025 Page 1 of 4 ?Gonferenoe eAnalXical www.pacefabs.com 67Drive, Raleigh, NC 27607 ph: (919) 834-4984, tax: (919) 894-8497 NCWW Certg67, NCDW Cert#37731 ChaIlIIl of Custody w.o.a_ WO#:92319224 92319224 Report Resul To: Company: LOL h W w Address: D, i3DX J Lout 7sc -s Attn: �i 1,1ba, iz'�Go2� Phone: 1 1- �t" -- 71? Fax: Sampled by (signature): Bill To: A 140F_fkOD }(sfhFrJT c i1 P0. BeX 5V-k LnL�tsl�u>�.. O C, a7s �g Project Reference: Project Number: Purchase Order #; ❑ Standard Report Delivery ❑ Rush Report Delivery (wlsurcharge) "Rush projects are subject to prior approval by the laboratory Requested Due Date: Sarnple:Descriptlon` ` , ll yy� k . 4t „ qy I•YQ. "Y�i J.. r1 +�"St s«.w 77r ({nbY' fit, �._ ; Start;Date°"q T G ' lk,;!StartlTiine 4., ; ;End Date;`f Il ;End71mer r'Gw; HMatrkfl WW.dW tiW s0i'sta� yAns ysesiRequestetl� ' �"�' }�' �f i`r ', ,#� `i ice; = tll "fir / ej ��mr�� .Yh{N Litj�Y[!7�l.z°i �L� ' ' T�1�? }�eSiiitX 1. A �1�u4 XC}..i:;q]K :f �i r1 �iFit7e .. ' Y tinh•'I GA s t1v II-dv..f � j� Q, a!`f s -� d U �Y11. `e r_ •V' �'3lAk�ss V,'N Nwi OEM`.' 1 N. l N I r \ /l�'.- �7,10O1,jti i�� i MIA11;/��t!l�/j"� mil` Me - WOM 14 4 P14riquished by (signature) R�T;,aWb�1%lTaureT Receipt Conditions (Leb Us Only) ❑ 4t2°C ❑ Temp: 'C Res. Chlorine: 0 Absent ❑ Present ❑ rtla Acid preserv. <2? ❑ Yes ❑ No ❑ n/a Base preserv.>127 ❑ Yes ❑ No ❑ Na Page 2 of 4 i UULUIIIC11t IVAllli••: VULUIIICtI• "V-Cu. 0Cr.. +, ... r.. Sample Condition Upon Recelpt{SCUR) Page 1 of 2 aceAnalyiica! Document No.: Issuing Authority: I F-CAR-CS-033-Rev.01 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ ?� Client Name: r t Jett tf: Courier: ]Fed Ex ❑UPS ❑LISPS ❑ Commercial ❑Pace []Other: Custody Seal Present? []Yes �5eals Intact? ❑Yes 0 Date/initials Person Examining Conten ' Packing Material: ❑Bubble Wrap []Bubble Bags ,Offone ❑Other: Thermometer: "//��� iR Gun ID: , (/ Type of Ice; et ❑Blue .❑None mples on ice, cooling process has be un Correctia Factor: Cooler Temp Corrected ('C): Biological Tissue Frozen? []Yes []NO N/A Temp should be above fire g to 6•C USDA Regulated Soil QI N/A, water sample) Did samples 90ginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source Including Hawaii and Puerto Rico)? ❑Yes liy, Chain of Custody Present? es QNG ❑N/A 1. Samples Arrived within Hold Time? es ❑No N/A 2. Short Hold Time Analysis (02 hr.)? []NO []NIA 3. Rush Turn Around Time Requested? []Yes -CfNo N/A 4. Sufficient Volume? es --ONO ❑N/A S. Correct Containers Used? -Pace Containers Used? EKes &fY,s (:]No [IN. ❑N/A N/A 6. Containers Intact? es []No N/A 7. Samples Field Filtered? (-]Yes []No j3WA 8. Note If sediment is visible In the dissolved container Sample Labels Match COO Yes []No ❑N/A 9. -Includes uate"imeilu nalysis Matrix. Headspace in VOAVlals (>5.6mm)? []Yes []NO ONfA lU. Trip Blank Present? ❑Yes []NO ONIA 11. Trip Blank Custody Seals Present? ❑Yes ❑No if/A CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? ❑Yes ❑No Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 3 of 4 w CO ro A O b_ 0 v m 0 efl d `m x 0 A � b Q rt O v 3 fD m � a e* o r 0 a m O ee n � FA � C m m Q m CL a fD a 3 3 m o a v to 4 CD 0 ac N F~+ O °D 90 V C1 47 A CU N r tteml3 � fa a = zzz zz ZA SP4U-125 mL Plastic Unpreserved (N/A) (Cl-) M. n 0 { 7C CL —Z SP3U-250 mL Plastic Unpreserved (H/A) =° y 1 fJl O m O = - 13PZU-500 mL Plastic Unpreserved (N/A) 1. O Q O- iv s = $P1U-1 liter Plastic Unpre ed (N/A) P mL P is H < 2) (0-) ,, $ O - Cr BP3N-250 mL plastic HNO3 (PH < 2) — n X SP3Z-250 mL Plastic ZN Acetate & NaOH (>9) Z e SPSC-250 mL Plastic NaOH (pH > 12) (C -) Q tDCD 0 Cr 3 D QQ toe WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) 0 3 AG1H-1 liter Amber HCI (pH < 2) O .tea p tD a n C) Q o 70 0 2 n AG3U-250 mL Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber H2SO4 (pH. < 2) CD AG3S-250 mL Amber H2SO4 (pH < 2) o ^ v Z `w 5 o m m o ~ AGM(DGMA 250 mL Amber NH4C1(N/A)(CI-) DG9H-40 mL VOA HCI (N/A) V o V. VG9T-40 mL VOA Na2S203 (N/A) ft VG9Lf-4Q mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) S V/GK (3 vials per kit)-VPH/Gas kit (N/A) ro c s SPST 125 mL Sterile Plastic (N/A— lab) tm C N C SP2T--250 mL Sterile Plastic (N/A —Lab) s o Q fI SP3A-250 mt. Plastic (NH2)2SO4 (9.3-9.7) r M Cubltainer C C VSGU-20 mL Scintillation vials (N/A) GN A w PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR) Please Mail Original And One Copy To Mailing Address Below GENERAL PERMIT NO. NCG0200(10 Part A: Facility Information D 4 (ail samples shall be reported within 3f0�ysfol owing monitoring period} Samples Collected In Quarter: 1 2 !3 Certificate Of Coverage No. NCG02 u( n�� unty of Facility Facility Name Name lof#Laboratory gcF Qwoi t 4-icaj Facility Contact t1 Ltl_ are5v CENT Sar-iC►cation #/01 Facility Contact Phone No. 3 79 p1j1R Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements ou"l : Number: Receiving Stream Name h .. :Date = ; S - to Col cctid -� L.501D. `00400 .. '.00530._ _.�� ._ I1fl1336 �- 00545:s_ = 'Doi Flaws H TolI&Sus tided Solids iifif Settlrabls Solids M1iGD.. _ =.funit..;::._. 1 u alo ee l�9 a l I go 19.7 j8.9 Nib �R2 Ro a" og d l i s .7 9 s AID 1 Measured continuously using a flow measuring device or estimated using manufacturer's pump curves and pump logs. Part C: Certification "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." n ) -L gnatuee of PermiUce) Part D: Mailing Address Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617 SWU-244-012005 PROCESSIMINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR) Please Mail Original And One Copy To Mailing Address Below GENERAL PERMIT NO. NCG020000 RECEIVED Part A: Facility Information FEB a;a ?ass Samples Collected In Quarter: 1 2 .dro) a (all samples shall be reported within 30 days following monitoring period) Ci~NTR FILES Certificate Of Coverage No. NCG02 County of Facility DWR — L.) N Facility Name i Name of Laboratory ' 4CE 4NA4 4i � a Facility Contact > . I1YZOtf2s`. Lab Certification # Facility Contact )Phone No. (_ql9 > �t . �3"7q Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements Number: : Receiving Stream Name Datr_ Sample Collected ,x Sii050 - .,.00400 00530_ 00S45�~;_. Daily Flaw` pH .. Tolal Suspended Soltd4 FurbWity Se}tleabie Solids - -.- � :'. . _. • model �` r ,_ � h'[Gll. =. uait.. ". _ 1,TUs�__� --=mi/l_.�_ .' u aZo ree dl� da l5 i .5 8 A1D 06 as IS ja. AID ND t Measured continuously using a flow measuring device or estimated using manufacturer's pump curves and pump lags. Part C: Certification "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of e' mittee) (Date) Part D: Mailing Address Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617 SWU-244-012005 ANNUAL SUMMARY DMR - WASTEWATER ` SEND TO CENTRAL OFFICE* PROCESS MINEMEWATERING WASTEWATER GENERAL PERMIT NO. NCG020000 7 EIVED EB `8 2016 CENTRAL FILES DWR SECTION * Report All Wastewater discharge monitoring data on this form (including No Flow and No Discharge and Pennit Limit Violations) by MARCH I of each _year. If you have limit violations, you must also have turned in a Limit Violation DVIR to your local Regional Office within 30 days of receiving sample results from a lab. CERTIFICATE OF COVERAGE NO NCG02 0 0 SAMPLE COLLECTION YEAR: e,36 is FACILITY NAME: Flerm 1-ne.�� t COUNTY: t)qN kL t fJ PERSON COLLECTING SAMP .ES: � tVn a al^ r �s PHONE NO. (9! ) 4 - q I � 1 1 9 CERTIFIED LABORATORY:. Ac L�-�c�_ _ [gab # _ :7 ADD TO LiSTSERVE? YES ❑ NO ENTAIL: bI VI n-ton d)W.7 e rn4)orf--CoM I.ab # LINI[T VIOLATIONS? l'E5 ❑ NO INDUSTRIAL SAND".) ® DISCHARGING TO SA WATERS'? ❑ Part A: Wastewater Monitoring Re uirements Outfall No. Date Sample Collected Total Flow Total Suspended Solids]Settleable Turbidity3 Solids pH Fecal Coliforms - mm/dd/yr MG mgA 1,2 NTU ' MIA2 1V a Standard 2 -r.a col/ml ' 03Mt 5 17.7 '7. NJ 7,0 O& e.� I 15 6, q 5.8 A10 ? 1 O a 1,5 14. . S a1 15 Y. 4 is a s a D , 9 r -oqla a 1 s s- 9.7 AI-D -7 0 t s All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits. z If an effluent iimit is exceeded. the permittee is required to institute monthly monitoring for that parameter for the remaining permit term, s The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs designated as trout waters; 25 NTU for all takes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the Stormwater Discharge Outfall. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge. d Only facilities discharging to SA waters arc required to monitor for Fecal Coliforms. Permit Date: l/l/2010-12/31/2014 Last Revised 01-21-1 1 Page 1 42 -J Part A Continued: Wastewater Monitoring Requirements Oulfall No. Date Sample Collected Total Flow 'Total Suspended Solids' Turbidity Settleable Solids pH Fecal Coliforms - mm/dd/vr MG mgfl NTU ml/l Standard col/ntl" MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW"'. "NO DISCHARGE" & LIMIT VIOLATIONS) BY MARCH 1 OF EACH YEAR TO: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 (919) 807-6379 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Rased on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I a mare that there are si ifican enalfor submittin � ' se information, including the possibility of lTj es and imprisonment for knowing violations." IL �_Jz UU-64-4— �Te ua 1�3 (Sign re of 1 tittee) X (Dale Permit Date: 1/1/2010-12/31/2014 Last Revised 0 1 -2 1 -1l Page 2 of 2 PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR) Please Mail Original And One Copy To Mailing Address Below GENERAL PERMIT NO. NCG020000 Part A. Facility Information Samples Collected In Quarter: 10 20 3 1 4 (ail samples shalt be reported withi3li{days foFi-�owfng cnrde 0")rnonitoring period) a! . Certificate Of Coverage No. NCGQ2 dd (�"y of Facility iz 14n1 k Li n1 Facility Name f F�� 4 Name of Laboratory RCYV4-L --f4c CAL, Facility Contact hirlibut IAJL YuaaLi' L•ab Certification # (0 7 Facility Contact Phone No. (919 ) 7 CENTRAL � L MAJR SEC-TION Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements :Date ' :-50t150=i `0098� r ,x-.�_ iiDSdS` u ': Ouilalt _ 4 ; . Number: Receiving Stream Name Sampie Collected �Daf1y Ftaw� " pH .. Total Suspended Solids Tuiiildity >Sotleable Solids•; :. - =:.unit.."::. NTU =s'_ w o reek 1� l rs 17. a �s _ 41 7 nIp �� 12,VSA fs L.a r sa N.a 1 Measured continuously using a flow measuring device or estimated using manufacturer's pump curves and pump lags. Part C: Certification "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." a aolep (Signature of a tte (Date) Part D: Mailing Address Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617 SWU-244-012005 PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR) a Please Mail Original And One Copy To Mailing Address Below larl GENERAL. PERMIT NO. NCG020000 Part A: Facility Information Samples Collected In Quarter 1 30 4 (all samples shall be reported within 30 days following monitoring period) (Orde Oaet Certificate Of Coverage No. NCG02 DD) 9 County of Facility Facility Name mY!t A i 1• Name of Laboratory Facility Contact W : k10 xr UU Ki o C UR Lab Certification # Facility Contact Phone No. Q iT- Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements rt� Q a 2p16 C-NTRP& FILES �Nr ��CTION iQ�IU K L i N Face 14na -tFG Lo'7 Date . ;. SOOSfl=. L00400 00530__ 7G'. �i00S45` x. �Dally Flow�� pH .:: Tott3t 5uspettdetl SalEds Ctaififctlty� - - �l5ettteable Sotids.' Outfall Receiving Stream Naine Sale Collected Ntimbe�_ s _ _rl Yit.- <mold -.r `_._ t4iG© _.. Wilt..' __.._. a r .�:NTI)s u a ree K U3 19 15 1 7 P I Measured continuously using a flow measuring device or estimated using manufacturer's pump curves and pump logs. Part C: Certification "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violation ' 2 5 (Signature nd ertt e) (Date) Part D: Mailing Address Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617 S W U-244-012005 1�a'neAnafytical'� www.pece71h'9'WM J i Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Project: WADE MOORE SAMPLING 03119M5 Pace Project No.: 92241941 Sample: SITE 01 GP �^ Laboratory Report Pace Analytical 3arvlcas, Inc. 6701 Conterenca Drlve Ralefgh, NC 27607 (919)834.4984 Page 1 of 1 Report Date: 03/3012015 Dale Received: 03/19/2015 tab ID: 92241941001 Collected: 03119115 10:50 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Turbidity 16.2 NTU 0.50 0312011512:53 Total Settleable Solids ND mI. Mr 0.10 03/20/15 12:50 Total Suspended Solids 24.7 mg1L 4.5 03/20/15 08:55 pl-I at 25 Degrees C 7.2 Sid. Units 1.0 03/27/15 10AD 11-16 Sample: SITE 02 RP Lab ID: 92241941002 Collected: 03/19/15 10:55 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Turbidity 7.8 NTU 0,50 0312011512:53 Total Settleable Solids ND mt.lLJhr 0.10 03120M5 12:50 Total Suspended`56Ik1s 7.a mg1L 5.0 03/20115 08:57 pH at 25 Degrees C 7.0 Std, Units 1.0 03127/15 10:40 H6 ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA recommended holding time. Reviewed oy: Sheila M McGlown shelia,mcglown@pacelabs.com Raleigh Cartification IDa 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Eden Certification iDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Ceftlficatton #: 37738 North Carolina Bioassay Certification 0: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Uastewater Certification #: 633 VlrglnlalVFLAP Cerilficatlon #: 460025 Page 1 of 3 acmnalytical www.pacelabs.com 6701 Conterenoe iJrlve, Reielgh, NC 276137 ph: (919) 834-4984, tax; (919) 834.6497 NCWW Cent#67, NCOW Cert#37791 Report Result To: V Campany: ( WWrc Address: .p, & •s Lou ccs4b Attn: L%:: Phone, �q_LNO• Xlg! �p-L Fax: _ I -06 - 9 d Sampled by (signature): Chain of Custody Bill 1 ! 1UG32� .. D. boxLJ 5 Project Reference: Project Number: Purchase Order #: ❑ Standard Report Delivery ED Rush Report Delivery (wlsurcharge) "Rush prolecta are sutilect to prior approvat by the laboratory Requested Due Date: Relinquished by (signature) Eli to Oa a ff Tame Relinquished by (signature) R d by (slgnatu) Qa Time �V 12; Lr� Relinquished by (signature) Received signature) Date Time Receipt Conditions (LabVsq Only) Cl 4t2°C 0 Temp: °C Res. Chlorine: Cp Absent ❑ Preseni [] nla Acid preserv, <27 G Yes ❑ No ❑ n/a Base preserv. >127 0 Yes 0 No fMOR of 3 Document Name. Satnplp Condltfi n..11�bn Dacumant Revlsed: Aprtl•04, 2013 h acsAnaiCal ' Receipt SC U,R r ??a page 1 of 2 •""'�"°"'" " Document No.- .:s IssulrtgAuthorities:. i-RAL-CS-' 1-rev: 2...'. `:...' Pace Asheville QU91fty Offlce ClientNerve: Whpre Recelv$d: HuntersAlle Ej Ashevilie p F-deh l�qlelg4 Caurfer (Circle): • Fed Ex UPS LISPS >;ile"I Commerclel Pecs .Other. Custody goal on Cooler113ox Present: ­ [] yes na. Seals lntact: i� yes ❑ no Packing Materiel: ElBubble Wrap Bub Ba a p NonkZ Pther Circle. Thermometer Used: 1.R Gun :122088: 8 a of Ice: Wet Blue No " l] semplas on Im coa$ng proasas heabegun iamp'Cortectiort factor'. Add 7 . extract C Rate""TI foals of ; on bxemining Corrected Cooler Tamp:: C .: Sio115gfcal Tlesua�.�s Fr6ien:' Yea'N NIA ctrUala Temp.`silauld be above freezing to. 4'4tr1t11et1ta:. Chilln:otCttstati':Preaent: :..,: • :. Yes-,E]ND- l3WA - �.... _ Chalnof Cusiaayi=Nled Oii4:...:.. alri�ot�uBtod Relln Ufshed:;... ea':�7No<..OWA' 3. •' .. . Sato 06N A Signature an COC; . eo4 G]Na';..IONiA •b.:, Savri' es tiirivedwrltisln hold Time:.. Ysa.: N ` C WA Sitor f Hold T rnO Anai Is' S.Tghr ; FEueh,Turn;AT u . d TIOt Re tig ed; QYea_. ©NfA Yee CiNd ©NIA Q: 60.rrt C Contall.lors.use d . Yea -PaCrr3 C'Dntal a ,ilet�d:... Y"'�r ©No ,ON1k. Flit'ered voluma reoeived-.for:l)lsbc4veti te$is [ Yes .[" w IVfn 11: . Sample Labels. m fch CQ ', ,; , . .. '.. Ya 'J 1146 QNIA . 12. -lnofudas:dateftlmelll)lArta! is IVlatrlx r All oontaln®r5 ileedlriB; P^��etvstlorj stave bean citedted: ag L7tJa []NIA 13.' . All e"v n,pro found to be. In vy� coinolancew4fi EPArecommendetlon. , ears bna: A,.: 1lfonn TOC,t)SG,WI.ORo No Saris' fes oho9k4§d for.dechlodnation, es ONo ©Wk 14, Haade soe In VOA Vlais >8min : OYes ©No IA 16. Trlp-1131brik Present: lOYas ONO 16. 1NrA Trip Slank'.custady Seals'Present ..[,]No Wl+rrA Pane 7rl :Blank Lot# If Grcltased : CAenfootlfldatloni-Resolutlon: 9oldDeteRequired? Y 'I N Person Contented; RtateMme: CommehrW Resolution: SCURF•lSRI= Place label here LOA - Revir3w:. Note: Whenever there a a dlnerepanoy affocting North Carolina compilanoe ' „t samples, a copy of this form All be sent to the North Carolina DFt9Nfi Cartlacatlan-QNEce (I.e out of bald, inoorreat pteaenrathre, out of tamp,�., . lncorrt3at cnnta4nere) l; S bf 3 ANNUAL SUMMARY DAR - WASTEWATER SEND TO CENTRAL OFFICE PROCESS NIINE/DEWATERING WASTEWATER GENERAL PERMIT NO. NCG020000 * ReportAll Wastewater discharge monitoring.data on this form (including No Flow and No Discharge and Permit Limit [violations} by MARCH 1 of each year. If ' { you have limit violations, you must also have turned in a Limit Violation DMR_ to your local Regional Office within 30 days of receiving sample results from a lab. T CERTIFICATE OF COVERAGE N . NCG02 0 © 1 1 SANTLE COLLECTION YEAR: FACILITY NAME: e i COUNTY: 1J LJ rU PERSON COLLECTING SAMPL S: ea a arri,s PHONE NO. Q( tR } q-QCQ_ 3 -79 11 CERTM ED LABORATORY: � C, Lab # ADD TO LISTERVE? YES ❑ NO❑ EMAIL: b'1 r nw rye ®wV4c ftore . g� Lab # LEYMS VIOLATIONS? YES ❑ NO Part A: Wastewater Monitoring Requirements INDUSTRIAL SAND"? Qr DISCHARGING TO'SA WATERS'? ❑ z Outfall No. Date Sample t Collected 50050 Total Flow 00530 Total Suspended Solids' 00400 Turbldity3 00545 Settleable So ltds . 00400; pH r' 31616 Fecal Coliforms mm/dd/yr MG mg/l NT1J ml/! Standard coUmlZ' Jc�.B rJD 1hL L A,,'7 a D A -o q-_ 1 nlp Fleo .SAS} 14D D M I e- 1hr 7,0 0'1- 4- 1 i./Io Flaw A6,r? NDn, LJLJW .S D?--a9-r a DOD t. t hr � ' All mines must monitor WW discharges for TSS. Only industrial sand mine discharges are subject to TSS limits. 2 If an effluent limit is exceeded, the permittee is required to institute monthly monitoring for that parameter for the remaining permit term. 3 The discharge shall not cause an instantaneous measurement of the turbidity of the receiving water to exceed: 10 NTU for freshwater streams, lakes, and reservoirs designated as trout waters; 25 NTU for all lakes and reservoirs, and all salt waters; 50 NTU for all other streams and surface waters. Turbidity may be monitored at the Stormwater Discharge Outfaii. Alternatively, the permittee may choose to monitor turbidity in the receiving water, directly upstream and downstream of the discharge. Only facilities discharging to SA waters are required to monitor for Fecal coliforms. "°ems Permit Date: 1/1/2010-12131/2014 Last Revised 01-05-10 Pagel of 2 Part A Continued: Wastewater Monitoring Requirements Outfal! No. Date Sample Collected' 50050 Total Flow 00530 Total Suspended Solids' 00400 Turbidity3 00545 Settleable Solids 00400 pH 31616 Fecal Coliforms - mm/dd/yr MG mg/l1a NTU M1/12 Standard2 collm!' MAI1?0'- IGfNAL AND ONE COPY OF THIS ANNUAL SL7TV IARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LD41T VIOLATIONS) BY MARCH-1- OF EACH YEAR TO: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YO U MUST SIGN THIS CERTIECATIONFOR ANY INFORMATION REPORTED: "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the lnformation, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that t re ar ign' ant pe a! 'es fa ubmitting false information, includ7(Date) ossibllity of ftges and imprisonment for !mowing violations." (Signs ` of Perkaittee) i Permit Date: 1/1!201042/31/2014 Last Revised 01-05-10 Page 2 of 2 wtiyw.pacafa65.com Laboratory Report Pace Analytical Services, Inc. 6701 Conference Drive Raleigh. NC 27607 (919)834-4984 Page 1 of 1 Wilbur Moore Report Date: 02118/2014 Wade Moore Equipment Company Date Received: 02/04/2014 PO sox 546 Louisburg, NC 27549 Project: WASTEWATER Pace Project Na.: 92188382 Sample: SITE 1 GP Lab ID: 92188382001 Collected: 02/04/14 07:45 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Turbidity 12.8 NTU 1.0 02/04/14 10.49 Total Settleable Solids ND mLlLlhr 0.10 02/05/14 10:00 pH at 25 Degrees C 7.2 Std. Units 1.0 02117/14 14:15 H6 Total Suspended Solids 12.8 ni 2.5 02106/14 20:54 Sample: SITE 2 RP Lab ID: 92188382002 Collected: 02/04114 08:15 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Turbidity 10 NTU 1.0 02/04/14 10:49 Total Settleable Solids ND mLlilhr 0 10 02105/14 10:00 pH at 25 Degrees C 7.0 Std. Units 1.0 02/17/14 14:15 1 Total Suspended Solids 5.9 mg/L 2.5 02/06/14 20:55 ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA recommended holding time. i Reviewed by: Nikitia Jones -Jackson nikitia.jones@pacelabs.conn Raleigh Certification IDs 6701 Conference Drive Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Bioassay Certification #;16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Cerfification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 Page 1 of 3 Z7I ce Analytical www.pafotabs.com 6701 Conference Drive, Raleigh, NC 27607 ph: (919) 834-4984, fax: (919) 834-6497 NCWW Cert#67, NCDW Cert#37731 Chain of Custody Report Resul To: �( fBill To: Company:D 1 ODJ ,} J1�iYr l tl�i� �Q;/mot !1� ice✓ Address: f o, �[JOX 5 4-V q >SbUrC AJC v�"7� �/ Attn: ` l l Phone: - 4 �-/� ' — Fax: 9 1 — 96 — -72 92 Sampled by (signature): W.O. # Project Reference: Project Number: Purchase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) "Rush projects are subject to prior approval by the laboratory Requested Due Date: Sample Description composuoor c'ab Start Date End Date Matrix W,Sal.®[W Analyses Requested Sam lea p Start Time End Time S,rf Svc Pry i ss 1uvb►� 7; 5' ' N. Sol A4 -rss 7g rbid; tt, Relinquished by (signature) Received by (signature) I Date The Relinquished by (signature) Received by (signature —) Date I Time °7I �W`�•G�l ?- �" �y �� O Relinquished by (signature) Received by (signature) Date Time Receipt Conditions (Lab Use Only) ❑ 4±20C ❑ Temp: oC P. Res. Chlorine: ❑ Absent ❑ Present ❑ n/a Acid preserv. <2? ❑ Yes ❑ No ❑ n/a Base preserv. >12? ❑ Yes ❑ No ❑ n/a Analytical www.pacelabs.com ive, Raleigh, NC 27607 ph: (919) 834-4984, fax: (919) 834-6497 NCWW Cert#67, NCDW Cert#37731 Chain of Custody Wa 4gZl��3-(2�4 Report Result o. }Bill To: Company: DD �+ !z MLbaL Q Ito Project Reference: Address: �`�- _LQIL'o w C ,N - xi Z-at�`sb rtJC ass L/ Project Number: - •_ AM, a Purchase Order#: Phone: / — 3 1a ❑ Standard Report Delivery `7❑ Rush Report Delivery (wlsufcharge) Fax: — r "Rush projects are subject to prior approval by the laboratory Sampled by (signature): Requested Due Date: ;r,Sample" Descrrptlon ', .'" .�. .cymP06k9O <�f t Start Date; jStart �Ti endcTme"$` �EriclrData� Matrix - w soa _OWN Arialjr&eslf t guested ;°• * s, ti. W �n f � - S,,f 50 P� �5-`' 7w-k c� Ww 7 • ,� _Itt., U f � e-+ SD I Pry `rss Turbrd, t � S: 15 V i� y4�li i . w { Y^ SRI Vt Relinquished by (signature) Re eived by ( nat ) , X Date 2 Time .D Relinquished by (signature) Received by (signature) D e Time X&�� y-ly 1130 Relinquished by (signature) RTcepfby (signature) Date Time Receipt Conditions (La?Only) © 4t20C ❑ Temp: °C Res. Chlorine: ❑ Absent ❑ Present ❑ n/a Acid preserv. <2? ❑ Yes ❑ No ❑ n/a Base preserv. >12? ❑ Yes 0 No 0 nla aceAnalytical www.pacelabs.com 6701 Conference Drive, Raleigh, NC 27607 ph: (919)834-4984,fax: (919)834-6497 NCWW Cert#67, NCDW Cert#37731 Chain ®f Custody W.o.# 2 Report Result o: Company: {� CO ) 00� Address: R0 B13. Sao — Uffiu 61011nc Nc- 1/154591 1:.R%%1il�lfFt� • gampled by (signature): Bill To: b. 3C).10 S °sb arc, AI C 49'1 S_ ff--/ Project Reference: Project Number: rcnase Urcier #: ❑ Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) "Rush projects are subject to prior approval by the laboratory Requested Due Date: ,Sample Descn�pi ono 't �s9�4 Qv ei� H� Start Gated �tCStartlime 19 50i9W6 ;>EntluTiine wwMpwlsw ,dw sai Aiialy§es fde+�uestU11 , . �f so) '7 �. 1 z+ .50 Af Tss 7urbr4,t 8; 15 i c. } .1 . J' M�1 Relinquished by (signature) Re ived by ( nat ] Date 2 Time D Relinquished by (signature) Received by (signature) D e Time Relinquished by (signature) R cei by (signature) Date Time Receipt Conditions (LabryJ�e _Only) ❑ 4t2°C ❑ Temp: L � L,Q °C Res. Chlorjne: ❑ Absent ❑ Present © n/a Acid preserv. <2? ❑ Yes ❑ No ❑ n/a Base preserv. >12? 0 Yes 0 No ❑ n/a I 17 ` ceAnalytical www.parelabs.com 6701 Conference Drive, Raleigh, NC 27607 ph: (919) 634-4984, fax: (919) 834-6497 NCWW Cert#67, NCDW Cert#37731 Report Result o: Company:(_113JA-More, & ov, D Address: E D DD j� '54P 11 i>o.0 ��un e- . N C- I'l 54-'1 Attn: JAL;Jlir~ VYk & !e� Phone: - / - 321 Fax: q 19 _ q� - 7 g 4� Sampled by (signature): Chain of Custody . W.O.# :� Bill To: k�QL 1KC-0-a eQ Lk 119 t), j 30,< 5 t A'sb LLrq,A/ C ,9°75 Project Reference: Project Number: Purchase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (w/surcharge) "Rush projects are subject to prior approval by the laboratory Requested Due Date: iS6implej'Descriptror� g$`,' r ��. Wom"poaie - ,'' t tpStartiDat6` t. "Stait�Time fndiNte��`' - ......, '" EndrTme i nmatiik)), Gw'suli;ew icAnalySeslReguestetl kt � ? At'� �` m'pie t i �,✓ P a- S�f s� PH r &5 Fai4 , � . - � 5 7 •� 5ej SDI A4 TSS -7—u rbid i twa- 8, 15 �r •i Nil n �r d +� Relinquished by (signature) Re ived by (shnat ) Date 2-1 d 14 Time q Relinquished by {signature} D e Time �R�eceiived Relinquished by (signature) R cei by (signature) Date Time Receipt Conditions (LatYjl�e Only) El4t2°C ❑ %mp: ' tQ °C Res. Chlorine: ❑ Absent ❑ Present ❑ n/a Acid preserv, <2? ❑ Yes ❑ No ❑ n/a Base preserv. >12? 0 Yes 0 No p n/a laceAnalyficalle fwwwpacareba.com Laboratory Report Wilbur Moore Wade Moore Equipment Company PO Box 546 Louisburg, NC 27549 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 1 of 1 Report Date: 08/11/2014 Date Received: 07/29/2014 Project: 07/29/14 SITE 1 & SITE 2 Pace Project No.: 92210949 Sample: SITE 1 Lab ID: 92210949001 Collected: 07/29/14 09:30 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Turbidity 20.7 NTU 1.0 07/30/14 18:05 Total Suspended Solids 22.2 m911- 6.1 07/30/14 16:26 Total Settleable Solids ND mL/Uhr 0,10 07/30/14 15:29 pH at 25 Degrees C 6.8 Std. Units 1.0 07/30/14 14:22 H6 Sample: SITE 2 Lab ID: 92210949002 Collected: 07/29/14 09:40 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Turbidity 14.3 NTU 1.0 07/30/14 18:05 Total Suspended Solids 10.8 mg/L 5.0 07/30/14 16:27 Total Settleable Solids ND mIJIJhr 0.10 07/30/14 15:29 pH at 25 Degrees C 6.8 Std. Units 1.0 07/30/14 14:22 H6 ANALYTE; QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA recommended holding time. Reviewed by:���z Sheila M McGlown sheila.mcglown@pacelabs.com Raleigh Certification IDs 6701 Conference Drive Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 Page 1 of 4 aceAnalyfical www.pacelabs.com 6701 Conference Drive, Raleigh, NC 27607 ph: (919) 834-4984, tax: (919) 834.6497 NCWW Cert#87, NCDW Cert#37731 Report Resui To: n Company: Address: isgC.0?,075 Attn: t 6'r re. Phone: � 41q- 3-79 Fax: 9j 9— to. ?8q�3 Sampled by (signature): Chain of Custody Wo#� f •ill �i r � • i Project Reference: Project Number: Purchase Order #: ❑ Standard Report Delivery ❑ Rush Report Delivery (wlsurcharge) —Rush projects are subject to prior approval by the laboratory Requested Due Date: Relinq by (signature , Received by (signal X �' Dais Time Relinquish y (signature) Ived by ( nature) Date Time Rellnquished by (signature) Received by (signature) Date Time Receipt Conditions (Lab Use Only) © 4±TC ❑ Temp: 'C Res. Chlorine: ❑ Absent ❑ Present 0 n/a Acid preserv. ¢27 ❑ Yes ❑ No ❑ nla Base preserv. >127 0 Yes 0 NoPQerVwf 4 Doeumant Name: Sample -Condition Upon Document Revised: April 04, 2013 _ .f �7C� EAI7al 1Cal m Receipt SCUR Pa e 1 of 2 ` Document No.: issuing Authorities:. F-RAL-CS-001-rev.02 i Pace Asheville Quality Office Client Name: L�OO (d YAOUY'� Where Received: Huntersvllle [] Asheville Eden ( Raleigh Courier (Circle): • Fed Ex UPS USPS Client Commercial Pace . Other Custody Seal on Cooler/Box Present: yes no Seals Intact: yes F1 no, Packing Material. 0 Bubble Wrap Bubble Bags fit None Other Circle Thermometer Used: IR Gun Suo 22065387T pe of Ice: et Blue None Samples on Ice, cooling process has begun IR Gun Back �1 Temp Correction Factor: Add! ubtract . Date and Initials of Person.examtning Corrected Cooler Temp.: C _C Biological Tissue is Frgien: Yes No NIA co a is !Pre ervat o check Temp, should be above freaOng to M Comments: Chain of CustodyPresent: Yas' ' No • ❑NIA. 'f.... _ _._ _...... _...... ... _ ... ....... .. . ._ Chain of Custody Fllled Out: Yes []No ❑N1A 2. Chain of Custody Relinquished: Rry.. ONo ❑NIA 3. Sam ler Name & Si neture on COC: Yes .CINo. ©wn 4.. Samples Arrived within Hold Time: OYes ❑No ❑wA b.'. Short Hold.Time Anal sis' <72hr : Yes ONO ❑tiA 6. Rush Turn Around Time Re uested: ❑Yes o 0WA 7. Suff(Cient.Volume: VYea DNo ❑WA 8. Correct Containers Used: Yes ©No ❑NIA 9. ' -Pace Contalners Upd; Yas ©Na ❑wA COnt1118rS Intact: Yes ©No ❑NIA 10. Filtered volume=received for Dissolved tests ❑Y09 ❑No gWA 11, Sample Labels match CDC: Yes QNo ONIA 12. -includes date/time/ID/Analysis Matrix: All containers needing•presorvatlon have been checked.as ©No ❑N!A 13. All containers needing preservation are found to be in rYes ONo ❑wA compliance with EPA recommendation, r" excaptlone: VOA,. eoliforrn, TOC, 0&G, WI-DRO (water) Xy., ONo Sam les checked for dechlorination: Yes ONo ©N/A 14. Headsp ace in VOA Vials >6mm : ❑Yes ONo wA 15. Trip Blank Present: ❑Yee []No/Olt 16. Trip Blank Custody Seals Present ❑Yes ONo LCNIA Pace Trip Blank Lot # if purchased): Client Notification/ Resolution: Field Date Required? Y 1 N Person Contacted: Date/Tlme: Comments! Resolution: SCURF ISRF Date: 'WO# + 9221®949 Review:, Note: Whenever there is a discrepancy affecting North Carolina compliance fll��lll�tl �I �I III II� samples, a copy of this form will be sent to the North Carolina DEHNR 92210949 Certification Off ce ( i.e out of hold, incorrect preservative, out of temp, (it no lanes avanaviv� incorrect containers) Page 3 of 4 Document Name: Sample Condition Upon. Document Revised: April 04, 2013 NC16/inalytal" Receipt (SCUR) Pa e 2 of 2 Document No.: issuing Authorities: F-RAL-CS-001=rev.02 Pace Asheville Quality Office a .r a is a r■ r a a a a ar r r r r r r r r r ■ t s • r r se■■■■■■tee■■■■e■�■■�■■■■■® ®■®■tee■■■■■■■■■ee■■■■■■■■�■■� Client Sample ID s Sam le Discre aric . H Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation Adjusted Time Preservation Adjusted AmRunt of Preservative added Lot# of Preservative Bottle Code Key 125 ml Plastic Unp: BP4U 250 ml Plastic Unp: BP31-1 500 mi Plastic Unp: BP21J 1 Liter.Plastic Unp: BP1 U 250 ml Plastic H2SO4: BP3S 250 i�il Plastic HNO3: BP3N 250 ml Plastic ZN Acetate. BP3Z 250 ml Plastic NaOH: BP3C Wide mouthed glass }ar unp: WGFU 1 Liter Amber Unp: AG1U 40 ml VOA H2SO4: DG9S 1 Liter Amber HCI: AG1H 5035 Kit: VOAK 500 ml Amber Unp: AG2U VPH 1 Gas Kit: V/GK 1 Liter Amber H2SO4: AG IS 125 ml Sterile Plastic: SPST 250 ml Amber H2804: AG3S 250 mi Sterile Plastic: SP2T 250 mi Amber NH4CL: AG3A 40 ml VOA HCl: DG9H 40 ml VOA Na2S2O3-. VG9T 40 ml VOA Unp: VG91J Page 4 of 4 PROCESSIMINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR) Please Mail Original And One Copy To Mailing Address Below GENERAL PERMIT NO. NCG020000 Part A: Facility Information Samples Collected In Quarter: 162Q-3Q 4Q (all samples shall be reported within 30 days following monitoring period) —tort, Ore) Certificate Of Coverage No. NCG02 a:p I ci County of Facility r AV t-'L I Nt Facility Name �l�rn�rcz ��' ;�- Name of Laboratory 1 'Rt-tsT Facility Contact �L1� �Y W. mc;c,-e_ Lab Certification N t�icJal'u, 04� 7 6LLOW 3 7 T3 j Facility Contact Phone No. `t 19 4-51, _ 3-79 4 Part B: Process Wastewater and Mire Dewatering Wastewater Monitoring Requirements Outfall Number Receiv ing Stream Name bate Sstnple Callecfed 50050_ °. -: 100400 00530 , ..00076,�:i . a; `. u_ 00545 Daily Flaw" pH Total Suspended Solids ,` Tuibldit y SefEleatile Solids molddl r -6IGD unit m NTUs mill }�;_,t-Qe - l- r i . D j �Z)C Sl. 7 G D. I FF 1 &2 - i - U S c>�� cite 7.�yo , ID 33. C D. r 1 Measured continuously using a now measuring device or estimated using manufacturer's pump curves and pump logs. Part C: Certification "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the ' ation submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there re significant penaltie for subim ing false information, including the possibility of times and imprisonment for knowing violations." / /A— n (Signature of Per ittee) (Date) Part D: Mailing Address Attn: Central Files, DFrNR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617 SWU-244-0121)05 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Permit No.: or Certificate of Coverage No.: N/C/GI FaciiityName: Wnj),c Mcu2f 6.Qk�nti�.�vT (t .. Ft-mtn , County: N u. i nl _ Phone No. � 19 - `i-Q lv _ 3 -7 Inspector: kdm�mtl ,_ L10 Mcc'L�2 Date of Inspection: Q,A.,,.Z t ,-2y'G' i l l l l l nil [3y this signature,/l certify that this report is accurate and complete to the best of my knowledge: U I y (Signature of Permittee or Designee) 1. Outfall Description Outfall No. i Structur (pipe itch, etc.) Receiving Stream: u r ee}'�__ Describe the industrial activities that occur within the outfall drainage area: 2. Color Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: -�3 1 Lxc -- L-49 k+ 3. Odor Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.) - - � C' NL - --- 4. Clarity Choose the number which best describes the clarity of the discharge where 1 is clear and 10 is very cloudy: 1 D2 3 4 5 S W U-242-020705 6 7 8 9 10 Page 1 5. Floating Solids Choose the number which best describes the amount of floating solids in the stormwater discharge where 1 is no solids and 10 is the surface covered with floating solids: f1� 2 3 4 5 6 7 8 9 10 6. Suspended Solids Choose the number which best describes the amount of suspended solids in.the stormwater discharge where 1 is no solids and 10 is extremely muddy- 1 ( 2/ 3 4 5 6 7 8 9 10 �/ r 7. Foam Is there any foam in the stormwater discharge? 8. Oil Sheen Is there an oil sheen in the stormwater discharge? Yes No Yes No \ 9. Deposition at Outfall Is there deposition of material (sediment, etc.) at or immediately below the outfall? Yes (No10. Erosion at Outfall---- Is there erosion at or immediately below the outfall? Yes Co l 1. Other Obvious Indicators of Stormwater Pollution List and describe l _l� Ie asn Note: Low clarity, high solids, and/or the presence of foam, oil sheen, deposition or erosion may be indicative of conditions that warrant further investigation and corrective action. Page 2 S W U-242-020705 �OF W A rF9 0 G O -r Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Permit No.: 1 bl U1_L111 or Certificate of Coverage No.: NIC/GI KIWI I�I I Facility Name: LtfRno_ M-c,,P — tPr ti T- County: EgaNKw N Phone No. 112 24g3r?`� Inspector: 1' w Date of Inspection: By this signature, I,9ertify thtat this rypprt}s accurate and complete to the best of my knowledge: (Signature of Perrnittee or Designee) 1. Outfall Description Outfall No. Structur '(pipe ditch, etc.) Receiving Stream: i F�i2 t U E-R Describe the industrial activities that occur within the outfall drainage area: Z. Color Describe the color of the discharge usin basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 'Tk-e_ - L(C & 3. Odor Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.) 4. Clarity Choose the number which best describes the clarity of the discharge where 1 is clear and 10 is very cloudy: 1 2 3 4 5 6 7 8 9 10 S WU-242.020705 Page 1 5. Floating Solids Choose the number which best describes the amount of floating solids in the stormwater discharge where I is no solids and 10 is the surface covered with floating solids: �1 ) 2 3 4 5 6 7 8 9 10 6. Suspended Solids Choose the number which best describes the amount of suspended solids in the stormwater discharge where 1 is no solids and 10 is extremely muddy: 1 { 2% 3 4 5 6 7 8 9 10 7. Foam Is there any foam in the stormwater discharge? Yes LNo 8. Oil Sheen Is there an oil sheen in the stormwater discharge? Yes Now` 9. Deposition at Outfall Is there deposition of material (sediment, etc.) at or immediately below the outfall? Yes CNo,) 10. Erosion at Outfall Is there erosion at or immediately below the outfall? Yes No 11. Other Obvious Indicators of Stormwater Pollution List and describe ' , 5 y Note: Low clarity, high solids, and/or the presence of foam, oil sheen, deposition or erosion maybe indicative of conditions that warrant further investigation and corrective action. L, Page 2 S W U-242-020705 0 Page 1 of 1 " F<.oTEST Laboratory Report _._._ Ln6 Locofio,,?'R' __...__..._ . __.11 L.vh Locaiio 'L" Lah LoalLron'1Y' NC/WW Cert.#: 067 NCIDW Cert.#: 37731 5 NCNM Cert.#: 103 NC1DW Cert.#: 37733 NCNVIN Cert.#: 075 NCIDW Cert.#: 37721 6701 Conference Dr, Raleigh, NC 27607 6300 Ramada or, Suite C2, Clemmons, NC 27012 6624 Gordon Rd, Unit G, Wilmiogton, NC 28411 Ph: (919) 834-4984 Fax: (919) 834-6497 Ph: (336) 766-7846 Fax; (336) 766-2514 Ph: (910) 763-9793 Fax: (910) 343.9688 „[,• aye :.fie5s'•;.�"Y:a.::.91 `F 4.C:E3A ... Project No.: Project ID: STORMWATER --- Prepared for --- WILBUR MOORE WADE MOORE EQUIPMENT COMPANY P. O. BOX 546 SHIP:934 EAST RIVER ROAD LOUISBURG, NC 27549 Report Date: 618/2009 Date Received: 6/112009 Work Order #: 0906-00012 Cust. Code: WA3794 CUSL P.O.#: No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 001 POND 1 6/112009 8:45 SW Grab 4 +1- 2 deg C Test Performed Method Results lab Loc Da�UZedTime Qualifier pH EPA 150.1 7.03 S.U. R 615109 9:29 Total Suspended Solids SM 2540D 20.0 mg1L R 613109 13:44 Settleable Solids EPA 160.5 <0.1 mUL R 611109 15:15 PH disclaimer Exceeds holding time. R 615109 10:51 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 002 POND 2 61112009 8:50 SW Grab 4 +1- 2 deg C Test Performed Method Results Lab Loc PU1atV Time Qualifier pH EPA 150.1 7.00 S.U. R 615109 9:29 Total Suspended Solids SM 2540D 11.0 mg/L R 613109 13:44 Settleable Solids EPA 160.5 <0.1 mUL R 611109 .15.15 pH disclaimer Exceeds holding time. R 615109 10:51 Reviewed by: Grirvrei for Tritest, 1 PROCESS/MINE DEWATERING WASTEWATER DISCHARGE MONITORING REPORT (DMR) IL Please Mail Original And One Copy To Mailing Address Below 777771 GENERAL PERMIT NO. NCG020000 Part A: Facility Information Samples Collected In Quarter: 1 � 2 3 D (all samples shall be reported within 30 days following monitoring period) et.doKl Certificate Of Coverage No. NCG02 CDC)i cl County of Facility _rRAn+KLf Facility Name p- 'nA Name of Laboratory `1 R1TE.=sT— Facility Contact Lj_ Obur W.T mc-cre- Lab Certification N 04-7 �61CLOW 3 7`13 j Facility Contact Phone No. 4( I )_ 4-9L- 3`79 L� Part B: Process Wastewater and Mine Dewatering Wastewater Monitoring Requirements _s50050 'OQd00.. OD530 ..y,• _.`u. D0076:''=� OOS45`:;._• Outfa- ll Receiving Stream Natfte � Sample Collected Daily Flowlk p1i . ,Total Suspended Solids � Turbidity ' Seixt,tleable Solids Ntiinber �4 _YFe%Y iLft;H_ fib, molddl r .� unit B i C09 i , rem - - r 03 —1 t42 Rk u F. o s v+^ d'►c 7,Do t7 33. = C �.1 I Measured continuously using a flow measuring device or estimated using manufacturer's pump curves and pump logs. Part C: Certification "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the ' ation submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there re significant penaltie for submt ing false information, including the possibility of fines and imprisonment for knowing violations.". I , / , , Part D: Mailing Address Attn: Central Files, DENR, N.C. Division of Water Quality, 1617 Mail Service Center, Raleigh, NC 27699-1617 i I rl ; d � JUN 182009 L 1 l" S WU-244-012005 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Permit No.: NLc4k —O/A O 0111-1 or Certificate of Coverage No.: NICIGI, FacilityName: blAyE Moab & uLj pmE-rjT 0-0.. F(Cm. rI 5ov County: in_NK� i N Phone No. Inspector: VW . rncon� Date of Inspection: Qw, ' l , ' loc j By this signatre,/I certify that this report is �U Ag (Signature of Permittee or Designee) 1. Outfall Description and complete to the best of my knowledge: Outfall No. i Structur ftill itch, etc.) Receiving Stream: �jLL a� Describe the industrial activities that occur within the outfall drainage area: 2. Color Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: _ _ -131 tee. — L tqk± 3. Odor Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.) K o N L 4. Clarity Choose the number which best describes the clarity of the discharge where I is clear and 10 is very cloudy: 1 3 4 5 6 7 8 9 10 Page 1 S W U-242-020705 5. Floating Solids Choose the number which best describes the amount of floating solids in the stormwater discharge where 1 is no solids and 10 is the surface covered with floating solids: 1 2 3 4 5 6 7 8 9 10 6. Suspended Solids Choose the number which best describes the amount of suspended solids in the stormwater discharge where I is no solids and 10 is extremely muddy: 3 4 5 6 7 8 9 10 7. Foam Is there any foam in the stormwater discharge? Yes No 8. Oil Sheen Is there an oil sheen in the stormwater discharge? Yes CNo 9. Deposition at Outfall Is there deposition of material (sediment, etc.) at or immediately below the outfall? Yes DNo 10. Erosion at Outfall Is there erosion at or immediately below the outfall? Yes No it. Other Obvious Indicators of Stormwater Pollution List and describe 1 it.e- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, deposition or erosion maybe indicative of conditions that warrant further investigation and corrective action. Page 2 SWU-242-020705 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Permit No.: or Certificate of Coverage No.: Facility Name: Ua p moogf_ a. — Amin S County: _TgAN KL4 N _ Phone No. R 1 .. Inspector: 1,J Date of Inspection: uv"e UCs By this signature, Igertify that this.rgpprt)s accurate and complete to the best of my knowledge: (Signature of Perm�ee or Designee) _ 1. Outfali Description OutfalI No. cA Structur (pipe ditch, etc.) Receiving Stream: ERR R►L'0 Describe the industrial activities that occur within the outfall drainage area: 2. Color Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: — Lt h 3. Odor Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.) �GNt✓ 4. Clarity Choose the number which best describes the clarity of the discharge where 1 is clear and 10 is very cloudy: 1 2 3 4 5 6 7 8 9 10 Page 1 5 WU-242-020705 5. Floating Solids Choose the number which best describes the amount of floating solids in the stormwater discharge where 1 is no solids and 10 is the surface covered with floating solids: O2 3 4 5 6 7 8 9 10 6. Suspended Solids Choose the number which best describes the amount of suspended solids in the stormwater discharge where 1 is no solids and 10 is extremely muddy: 1 0 3 4 5 6 7 8 9 10 7. Foam Is there any foam in the stormwater discharge? Yes CNo 8. Oil Sheen Is there an oil sheen in the stormwater discharge? Yes No 9. Deposition at Outfall Is there deposition of material (sediment, etc.) at or immediately below the outfall? Yes No 10. Erosion at Outfall Is there erosion at or immediately below the outfall? Yes No 11. Other Obvious Indicators of Stormwater Pollution ��. List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, deposition or erosion maybe indicative of conditions that warrant further investigation and corrective action. Page 2 SWU-242-020705 o Page 1 of 1 7FcD)OTEST Laboratory Report Lob Locobba 'R' �t Lo6 IocaGoa 'C' Lo6 Location '1V' NClWW Cert.#: 067 NClDW Cert.#: 37731 NC/WW Cert.#: 103 NCIDW Cert.#: 37733 NCNM Cert.#: 075 NCIDW Cert.#: 37721 I 6701 Conference Dr, Raleigh, NC 27607 6300 Ramada Or, Suite C2, Clemmons, NC 27 112 6624 Gordon Rd, Unit G, Wilmington, NC 28411 Ph: (919) 834-4984 Fax: (919) 834-6497 Ph: (336) 766-7846 Fax: (336) 766-2514 Ph: (910) 763-9793 Fax: (910) 343-9688 `�smrr�2rrs�s Project No.: Report Date: 6/812009 Project ID: STORMWATER Date Received: 611/2009 --- Prepared for --- WILBUR MOORE WADE MOORE EQUIPMENT COMPANY Work Order #: 0906-00012 P. 0. BOX 546 Gust. Code: WA3794 SHIP:934 EAST RIVER ROAD Cust. P.O.#: LOUISBURG, NC 27549 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 001 POND 1 611/2009 8:45 SW Grab 4 +1- 2 deg C Test Performed Method Results - - - I zed -:------ Lab Loc a� Time Qualifier pH EPA 150.1 7.03 S.U. R 615109 9:29 Total Suspended Solids SM 2540D 20.0 mg1L R 613/09 13:44 Settleable Solids EPA 160.5 <0.1 mUL R 611109 15:15 pH disclaimer Exceeds holding time. R 615109 10:51 No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition 002 POND 2 6/1/2009 8:50 SW Grab 4 +1- 2 deg C Test Performed Method Results -- --- ----- An ! zed -------- Lab Loc Dace Time Qualifier pH EPA 150.1 7.00 S.U. R 615109 9:29 Total Suspended Solids SM 2540D 11.0 mg/L R 613109 13:44 Settleable Solids EPA 160.5 <0.1 mLIL R 611109 15.15 pH disclaimer Exceeds holding time. R 615109 10:51 Reviewed by: v . for Tritest, 1