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HomeMy WebLinkAboutWQ0041482_Application_20200214Initial Review INITIAL REVIEW Reviewer Thornburg, Nathaniel Is this submital an application?* r Yes r No Is this a complete application?* Complete App Date r Yes r No 02/13/2020 Project Number* WQ0041482 Applicant/Permittee City of Kinston Applicant/Permittee Post Office Box 339; Kinston, NC 28502 Address Is the owner in BIMS? r Yes r No Owner Type Facility Name County Municipal City of Kinston DCAR Lenoir Fee Category Major Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need O Yes review by the r No hydrogeologist? * Regional Office Washington Is the facility in BIMS? r Yes r No Fee Amount $1,310 CO Reviewer Erick Saunders: eads\egsaunders Admin Reviewer Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notification Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submitted Form Project Contact Information Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues. ....................................................................................................................................................................................................................................................................................................................................................................................................... Name * Rob Willcox Email Address* rob@willcoxmabesoil.com Project Information Submittal Type* r New Permit Application r Renewal c Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number WQ0041482 currently has project Applicant\Permittee * City of Kinston Phone Number* 3363399128 Applicant/Permittee Post Office Box 339; Kinston, NC 28502 Address* Facility Name * City of Kinston DCAR r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. City of Kinston - New Permit Application for Distribution of Class A Residuals Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) 19-07 City of Kinston Distribution of Class A 14.14MB Residuals Application Package-signed.pdf upload only 1 PDF document. NiLRiple docurrents rust be corrbined into one PDF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper --polka*-ion is required, be advised, applications accepted' far pre -review until both the paper and eIect-c-,i_ co1)ies nave been received. The paper copy shall include the following: o Application Form o All relevant attachments (calcs, soils report, specs, etc.) o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) MallinE address: ❑iuision of Water Resources1 Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center 1 Aft: Nathaniel Thornburg, 91° Floor, Cfice #942W ----------------------------------------------------------- ----------------------------------------- Raleih, NC 27699-1617 512 N. Salisbury St. Far questions or problems contact Tessa Monday attessa.monday@ncdenr.Qov or 919.707.3560. * W By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/11/2020 APPLICATION FOR NEW PERMIT DISTRIBUTION OF CLASS A RESIDUALS CITY OF KINSTON JOHNNIE MOSLEY REGIONAL WRF Willcox & Mabe Soil Solutions, PLLC Project No. 19-07 Prepared for: City of Kinston P.O. Box 339 Kinston, North Carolina 28502 Prepared by: Willcox & Mabe Soil Solutions, PLLC 7231 B Summerfield Road Summerfield, North Carolina 27358 willcox&mabe 8 0 1 L SOLUTIONS January 2020 willcoX&'l abe SOIL SOLUTIONS February 11, 2020 NCDEQ/DWR Water Quality Permitting Section Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Non -Discharge Permitting Unit Reference: Application for New Permit Distribution of Class A Residuals City of Kinston — Johnnie Mosley Regional WRF Willcox & Mabe Soil Solutions, PLLC Project No. 19-07, Phase: 01 Non -Discharge Permitting Unit: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting the enclosed application for a new permit for Distribution of Class A Residuals for the City of Kinston (Kinston) on behalf of Kinston. The application package includes information for obtaining a Distribution of Class A Residuals Permit in the name of Kinston to add one source, the Johnnie Mosley Regional WRF — 4,000 Dry Tons per year. If there is any further information required or questions regarding this application please do not hesitate to contact Kinston, Mr. Kenneth Stevens, Jr. at (252) 939-3306 or WMSS at 336-339-9128 for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe Agronomist cc: City of Kinston Rob Willcox, L.S.S. Licensed Soil Scientist Shared\WMSS Projects\2019\19-07 City of Kinston\Class A Permit Application Info\19-07 City of Kinston Distribution of Class A Residuals Application Package.doc Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, INC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willcoxmabesoil.com TABLE OF CONTENTS APPENDIX TITLE DISTRIBUTION OF CLASS A RESIDUALS APPLICATION FORM (FORM: DCAR 06-16) II FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION) III FORM DCAR 06-16 (ITEM H. - OPERATION AND MAINTENANCE PLAN) IV RESIDUALS SOURCE CERTIFICATION APPLICATION FORM • JOHNNIE MOSLEY REGIONAL WRF (FORM: RSC 06-16) APPENDIX I DISTRIBUTION OF CLASS A RESIDUALS APPLICATION FORM (DCAR 06-16) DWR State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 —DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website General —This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16); ® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The project name should be consistent on the plans, specifications, etc. ® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) (ENCLOSED) ® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395 Minor (residuals permitted for distribution <3,000 dry tons/year) $810 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) (ATTACHED) 0 List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Page I of 3 D. Program Information (All Application Packages) (APPENDIX II) 0 Provide a narrative explaining the following: ® How the materials will be handled and transported from where the residuals were produced to where it will be treated. How the residuals will be processed/treated (attach process flow diagram). ® How leachate collection will be handled. ® Where the residuals will be stored until processed. ® How the final product will be distributed (packaging, bulk, etc.) What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals Ioading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: Name and address of the person who prepared the residual that is sold or given away. A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ® Information on all applicable setbacks in accordance with 15A NCAC 02T A 108(b). ® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) (N/A) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T .1104(a)(2)(B), including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) (N/A) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). G. Environmental Assessments (Maybe Required— See 15A NCAC I C .0300) (N/A) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) (APPENDIX III) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. Submit the O&M Plan in accordance with 15A NCAC 02T .I I10 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 DWR State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: City of Kinston Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State Z Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Kenneth R. Stevens Title: WRF Sgperintendent/ORC Applicant's mailing address: Post Office Box 339 City: Kinston State: N.C.. Zip: 28502 Telephone number: (252) 939-3375 Email Address: Kermeth.stevens@ci.kinstonnc.us 2. Consultant's name: Rob Willcox License Number (for P.E.): N/A Affiliation: ❑ On Staff ® Retained (Firm: Willcox & Mahe Soil Solutions, PLLCI Consultant's mailing address: 7231B Summerfield Road City: Summerfield State: N.C.. Zip: 27358 Telephone number: (336) 339-9128 Email Address: rob@willcoxmabesoil.com 3. Fee submitted: 1.3 L0.00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ® new, ❑ modified, ❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: Date of most -recently issued permit: Date of most -recently certified Attachment A (if different than the permit): III. FACILITY INFORMATION: I. Name of residuals processing facility: Johnnie Mosley Regional WRF City: Kinston State: N.C.. Zip: 28501 Coordinates: Latitude: 35017' 19" Longitude: 77030' 55" Datum: NAD 83 Level of accuracy: nearest second Method of measurement: MAP County where facility is located: Lenoir 2. Facility contact (person familiar with residuals preparation): Name: Swindell Flowers Title: Residuals Coordinator Mailing address: 2101 Becton Farm Road City: Kinston State: N.C.. Zip: 29501 Telephone number. 2( 52) 939-3248 E-mail address: swindell.flowers@ci.kinston.nc.us FORM: DCAR 06-16 Page 1 of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 180 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); pellets will be managed by land application contractor Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added per 1.0 dry ton of residuals (dry ton) 3. Approximate amounts of the residuals received and processed at the facility: 2 900 dry tons per year. 4. " Approximate amounts of the final product (processed residuals) to be distributed: 2 900 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Attached 6. Does the facility have a stormwater management plan? ® Yes; ❑ No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Under Roof V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. W_ Residuals Source Certification APPENDIX IV FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) (N/A) attest that this application for nos Deen reviewer! Dy me ana is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. 0 Yes 0 No, Explain; I, Kenneth R. Stevens Jr. WRF Su erintendent / ORC (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for City of Kinston — Distribution of Class A Residuals (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: l��� Date: FORM: DCAR 06-16 Page 3 of 3 APPENDIX II FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION) FORM DCAR 06-16 (ITEM D. PROGRAM INFORMATION) D. Program Information (City of Kinston Class A Biosolids) The project objective is to produce Class A Biosolids at the City of Kinston Johnnie Mosley Regional Water Reclamation Facility (WRF). The existing biosolids handling system (belt filter press, lime stabilization) produces Class B Biosolids. The Kinston WWTF biosolids treatment system has been upgraded to replace the lime stabilization process with a new low temperature, thermal drying system to treat the dewatered sludge from the existing belt filter press. The lime stabilization system will be removed from the site. The biosolids produced with the Dryer will meet Class A requirements: Requirement to meet Pollutant Limits: NCAC 02T .1106 (a) and (c) [Section 503.13, Table 1 Ceiling Limits and Table 3 Pollutant concentrations]: these are met by the current treatment plant; the Dryer project will have no impact on the pollutants (ceiling levels are dry basis) Vector Attraction Reduction: NCAC 02T .1107 (a) (7) [Section 503.33 (a) (7)] "percent solids of sewage sludge that does not contain Unstabilized solids generated in a primary wastewater treatment process shall be equal to or greater than75 percent based on the moisture content and total solids prior to mixing with other materials" Pathogen Reduction Requirements: NCAC 02T .1106 (b) (3) Pathogen Reduction Requirement: Dryer will meet the Item (F) Process to Further Reduce Pathogens — Heat Drying (condition description): (F) Process to Further Reduce Pathogens - Heat Drying. The biological biosolids shall be dried by direct or indirect contact with hot gases to reduce the moisture content of the biological biosolids to 10 percent or lower. During the process, either the temperature of the biological biosolids particles exceeds 80 degrees Celsius or the wet bulb temperature of the gas in contact with the biological biosolids as they leave the dryer exceeds 80 degrees Celsius. • How the materials will be handled and transported from where the biosolids were produced to where it will be treated. Wastewater Treatment Process NPDES Permit No. NC0024336 The Johnnie Mosley Regional WRF plant is permitted by the NC DEQ Division of Water Resources NPDES Permit Number NC0024336. The plant is a fully D. Program Information (City of Kinston Class A Biosolids) Page 2 automated treatment facility considered state of the art. Its primary goal is to remove nutrients that causes oxygen depletion in the Neuse River. New modifications have been added to improve water quality and meet future discharge limits. These new modifications include computers that monitor and control all aspects of treatment for more efficient operations. Other modifications include denitrification filters and ultraviolet disinfection (UV). Denitrification Filter The denitrification filter is a deep sand filter bed. As water passes through the filter, particulate matter is trapped into the sand. The cleaner water is then discharged to the disinfection process. An added benefit to this system is that we can add a food source for the remaining bacteria that will cause them to use the chemical oxygen found in the nitrates of the effluent water. Once the chemical oxygen has been used, only pure nitrogen remains which bubbles off harmlessly into the air, thus preventing more nitrogen from entering into the Neuse River. Ultraviolet Disinfection The final treatment process is the disinfection of the plant effluent. The old disinfection process used gaseous chlorine to kill pathogenic organisms. This is a proven and very effective method of disinfection. The problem is that Chlorine has also been proven to be toxic to aquatic life, and will combine with other organic material to form compounds that have been shown to cause cancer. Because of this, more chemicals are added to remove any remaining chlorine after the disinfection process has been completed. The new plant has the ability to use ultra -violet light (UV). UV is a non -chemical process that prevents the bacteria from reproducing instead of actually killing the bacteria. This saves on chemical costs and prevents further damage to the environment. Dewatering and Biosolids Treatment Biosolids are aerobically stabilized followed by dewatering with Belt Filter Press. Prior to the new dryer operations, the sludge cake was chemically treated with lime mixing to generate Class B biosolids. This Dryer project will upgrade biosolids treatment to Class A. Dryer Operations The thermal drying system will use hot air convection at low temperature (150/175°F) (65/80°C) in a belt dryer. This system will treat the existing mechanically dewatered biosolids from the existing WRF. The Dryer will be capable of processing 10 dry tons per day (DTPD) of biosolids with an initial dry solid content of 16 percent. The final product will have a concentration of at least 90% dry solids. The new Dryer facility will be designed to run 24 hours per day seven days per week with capability of processing the design waste quantity in 24 hours. D. Program Information (City of Kinston Class A Biosolids) Page 3 Proof of Concept Testing was performed in January 2016 with a Pilot Dryer unit located at the Johnnie Mosley Regional WRF treating the existing mechanically dewatered biosolids. The testing confirmed that the Dryer unit can produce Class A Biosolids. Information on that testing is included in this Application. The new Dryer system will include the dryer unit and material handling. A new receiving hopper (8.5 cubic yard capacity) will be installed outside under the existing discharge conveyor from the existing Belt Filter Press. These dewatered biosolids will be pumped from the new hopper into the Dryer feed system. The feed system extruder spreads biosolids onto an upper belt which conveys solids to a lower belt that discharges the dried biosolids by conveyor to a new hopper. Dryer belt will be controlled (temperature, air flow) to attain proper dryness. The dried Class A Biosolids dried product will be stored inside the sludge building available for marketing and distribution. • How the biosolids will be processed/treated (attach process flow diagram). Reference previous response (flow diagram attached) • How leachate collection will be handled. Leachate will not be generated • Where the biosolids will be stored until processed. Class A Biosolids will be stored within the covered sludge storage building • How the final product will be distributed (packaging, bulk, etc.) Class A Biosolids will be land applied, not distributed • What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of biosolids loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. Product Information Labels and Application Information Sheets are Attached. Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. D. Program Information (City of Kinston Class A Biosolids) Page 4 Product Information Labels and Application Information Sheets are Attached Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: • Name and address of the person who prepared the residual that is sold or given away. • A statement that application of the biosolids to the land shall be in accordance with the instructions on the label or information sheet. • A statement that the biosolids shall not be applied to any site that is flooded, frozen or snow-covered. • A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored biosolids into any surface waters. • Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b). • A statement that the biosolids shall be applied at agronomic or recommended rates for intended uses. Product Information Labels and Application Information Sheets are Attached CITY OF KINSTON — CLASS A BIOSOLIDS PRODUCT LWORMATION LABEL Produced By: Preparer: City of Kinston Swindell Flowers, Land Application ORC Johnnie Mosley Regional WRF City of Kinston 2101 Becton Faun Road Kinston, North Carolina 28501 For information on this product contact City of Kinston Swindell Flowers, Land Application ORC (252) 939-3248 The Class A Biosolids (Johnnie Mosley Regional WRF) is generated by treatment of municipal wastewater. The generated biosolids are stable and contain a high nitrogen value for their application as a nitrogen fertilizer. The Johnnie Mosley Regional WRF is permitted for land application to farmland in accordance with Permit No. WQ00XXX. Provisions for Application Application of the Johnnie Mosley Regional WRF Biosolids are prohibited except in accordance with the provisions specified in the Application Information Sheet. Application must conform to standards identified in Permit WQOOV=and include but are not limited to: Setback Description Setback (feet) Liquid Cake Private or public water supply sources 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where the bottom intersects the SHWT) 25 0 Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 City of Kinston Class A Biosolids Product Information Label Application Information Sheet 1. Johnnie Mosley Regional WRF - Class A Biosolids are intended for use as a nitrogen fertilizer. Applications of Johnnie Mosley Regional WRF - Class A Biosolids should be made in accordance with approved application standards and WQOOXXXX permit conditions. 2. Johnnie Mosley Regional WRF - Class A Biosolids shall not be applied to flooded, frozen, or snow covered areas. 3. Application and storage of Johnnie Mosley Regional WRF - Class A Biosolids must be conducted in such a way as to prevent runoff from the application or storage site to any surface water. 4. Applications and loading rates of Johnnie Mosley Regional WRF - Class A Biosolids shall be applied at rates that comply with realistic yield expectations based on the soil series and crops found at: http://nutrients.soil.nesu.edu/yields/. 5. Johnnie Mosley Regional WRF - Class A Biosolids- shall not be applied if the land fails to assimilate the material or the application causes the contravention of surface water or groundwater standards. 6. Johnnie Mosley Regional WRF - Class A Biosolids shall not be applied within the 100- year flood elevation, unless the residuals are injected or incorporated within a 24-hour period following a residuals land application event. 7. Johnnie Mosley Regional WRF - Class A Biosolids shall not be applied during a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. 8. Johnnie Mosley Regional WRF - Class A Biosolids shall not be applied if the slope is greater than 10% for surface applied material, or if the slope is greater than 18% for injected or incorporated material. 9. Johnnie Mosley Regional WRF - Class A Biosolids shall not be applied if the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement. 10. Johnnie Mosley Regional WRF - Class A Biosolids shall not be applied if the vertical separation between the seasonal high water table and the depth of biosolids application is less than one foot.. 11. Johnnie Mosley Regional WRF - Class A Biosolids shall not be applied if the vertical separation of bedrock and the depth of residuals application is less than one foot. Contact City of Kinston for a copy of the most recent biosolids analysis and loading rates. City of Kinston Class A Biosolids Product Information Label CITY OF KINSTON CLASS A BIOSOLIDS RECEIPT FORM I (printed name) have received pounds / wet tons / cubic yards of the City of Kinston Class A Biosolids, a copy of the City of Kinston Class A product information label, and a copy of the most recent analysis of the product (if requested). I have read these documents and agree to adhere to the directions specified on the Application Information Sheet and the Product Information Label. Signature of Receiver Date of Receipt Address of Receiver City of Kinston Class A Biosolids Product Information Label APPENDIX III FORM DCAR 06-16 (ITEM H. - OPERATION AND MAINTENANCE PLAN) CITY OF KINSTON NON -DISCHARGE PERMIT NO. WQOOXXXXX OPERATIONS AND MAINTENANCE PLAN CLASS A BIOSOLIDS I. Purpose To put into place a plan that implements the requirements of North Carolina Department of Environmental Quality — Division of Water Resources (NCDEQ-DWR) Permit No. WQOOXXXXX for the City of Kinston. Requirements are included for the City of Kinston Class A Biosolids. Class A source(s) are listed within the permit. II. Operational Functions The operational functions of this program involve hauling Class A Biosolids from the respective WRF to land application sites which meet NCDEQ-DWR and EPA regulatory requirements. Class A Biosolids will be land applied at or below agronomic rates. City of Kinston will also account for any nutrient sources the landowner/lessee has applied. Biosolids will be land applied as a cake / pellet material utilizing tractor trailer, tractor and cake spreaders. Class A Biosolids will be spread evenly and at consistent rates. Class A Biosolids will be land applied on fields that are used for hay production, grazing, or row crop production harvested for animal feed. In the case where Class A Biosolids are land applied on fields utilized for grazing, applications rates will be reduced by 25% in accordance with USDA-NRCS 590 Nutrient Management Standards. Grazed fields will be determined by City of Kinston Operations Manager on site, or the appropriate personnel. The City of Kinston Class A Biosolids will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQOOXXXXX to include: o Toxicity Characteristics Leaching Procedure (TCLP), o Reactivity, Ignitability and Corrosivity, 0 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis, o Pathogen and Vector Attraction Reduction requirements, and o Any other applicable Permit conditions. III. Maintenance Schedules City of Kinston will follow the maintenance schedule as recommended by the manufacturer for the equipment utilized to complete the job within the limits of the permit. IV. Safety Measures City of Kinston continuously operates in a safety conscious manner. Employees participate in regular safety training that is designed to help employees recognize safety issues and take steps to prevent potential accidents from occurring. City of Kinston employees have the authority to stop operations if they think any aspect of the operation is going to lead to the cause of an environmental or personal accident. CITY OF KINSTON NON -DISCHARGE PERMIT NO. WQOOXXXXX OPERATIONS AND MAINTENANCE PLAN CLASS A BIOSOLIDS V. Spill Response Plan • Halt the source of the spill: Such as a ruptured line or valve, or damaged transportation unit. • Contain spill: Use straw bales to form a barrier. Straw or hay bales can be obtained from several sources for this purpose. Soil near the site can also be used to form a barrier for containment. • Clean up: Use Class A Biosolids application equipment to recover as much of the material as possible. After the application equipment has recovered as much material as possible, it will be land applied as per the management plan. A temporary sump pit may be dug in the containment area and spilled material washed into it to enhance recovery. • Final Clean up: The ultimate goal will be to restore the spill area to its original condition if possible. • Notification: As soon as possible after a spill occurs notify: o City of Kinston Johnnie Mosley Regional WRF (252) 939-3375 o Department of Environmental Quality Division of Water Resources Washington Regional Office (252) 946-6481 Management of clean-up efforts: The field superintendent shall take immediate charge of the clean-up activities. Additional labor will be requested from City of Kinston as needed. VI. Spill Prevention Plan The spill prevention plan requires that all equipment used to transport City of Kinston Class A Biosolids be subject to periodic safety inspections. Tires, brakes, lights, and turn signals will be inspected for proper working order. Each truck will be equipped with safety flares and appropriate signs to be used in the event of a breakdown. Any deficiencies observed during the safety inspections will result in the vehicle being removed from service and the responsible party for transport will be notified so that these deficiencies can be corrected and documented. Drivers and management personnel associated with the transport of the City of Kinston Class A Biosolids will be instructed in the spill prevention plan and will be required to attend training sessions. Drivers will be trained in defensive driving techniques in order to minimize road hazards. A driver who observes a road hazard will be required to report the hazards. As part of the spill prevention plan, drivers will be required to inspect the safety equipment of their vehicles on a daily basis. Any deficiency in safety equipment will be noted for corrective action. Drivers will be trained in the procedures to be taken in the event CITY OF KINSTON NON -DISCHARGE PERMIT NO. WQOOXXXXX OPERATIONS AND MAINTENANCE PLAN CLASS A BIOSOLIDS of a spill that occurs during the transport of City of Kinston Class A Biosolids. These procedures are discussed in the spill control, containment, and cleanup plan. VII. Spill Control, Containment, and Cleanup Plan Spills that occur during transport of the City of Kinston Class A Biosolids will occur at the generation point and the land application sites, respectively. These spills will not involve an environmental hazard or an over the road hazard and, therefore, will be handled accordingly. Spills that occur over -the -road will be subject to the contingencies contained in the spill control, containment, and cleanup plan. The following personnel will be involved in the spill control, containment, and cleanup. The responsible party for the transport will respond to the spill site and make an assessment of the spill and determine the containment procedures to be initiated and the equipment to be used to clean up the spill. The responsible party for the transport will be responsible for the direction of the cleanup team. In the event of a spill, the driver of the truck, if he has not sustained a debilitating injury, will and report the spill. The responsible party for transport will notify the appropriate authorities and will also notify the appropriate DWR Regional Office. The driver will set up safety flares and signs to wam motorists of the hazard. The responsible party for transport will mobilize the necessary equipment and personnel to the site, and will initiate the containment procedures. The site will be cleaned up according to the contingency plan. City of Kinston Class A Biosolids cleaned up from the site will be applied in accordance with the permit. VIII. Reporting Within 24 hours of a spill the field superintendent or appropriate representative shall present a written report detailing the cause of the spill and all action taken in response to the spill. City of Kinston will notify the appropriate Regional Office as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence IX. Inspection Plan Inspections for the land application of Class A Biosolids will be conducted at a minimum of daily at the land application site during land application events. Inspections will consist of inspecting the current field(s) that are being applied on, as well as inspecting random fields that have previously received Class A Biosolids applications. Inspections will be performed by City of Kinston personnel or appropriate representative on a CITY OF KINSTON NON -DISCHARGE PERMIT NO. WQOOXXXXX OPERATIONS AND MAINTENANCE PLAN CLASS A BIOSOLIDS rotational basis to ensure that all employees are familiar with the inspection processes. At a minimum, these inspections will consist of the following: • Verify that a biosolids analysis has been collected prior to land application activities being performed and that it meets the criteria for land application. • Verify that pathogen and vector attraction reduction data has been collected for the source to be land applied and that it meets the criteria for land application. • Verify the crop that is planted or is to be planted on the respective field(s). • Confirm that the correct amount of Class A Biosolids are being land applied. • Confirm that transport and application vehicles have a copy of the spill control plan. • Confirm that a copy of the permit and the operations and maintenance plan are maintained at the land application sites during land application activities. • Check that the field has been properly flagged and that buffers are adhered to. • Confirm that records are turned in at the end of each business day. Inspections will also be conducted by the City of Kinston ORC for the Johnnie Mosley Regional WRF or designated representative. X Sampling and Monitoring Plan • Sampling Procedures Accurate sampling is essential for valid laboratory test results. All samples collected at the respective Wastewater Treatment Plant (WWTP) are grab samples, which are samples taken at selected intervals to represent conditions at a given location at a particular point in time. Grab samples of biosolids are stored in a manner that will not alter sample characteristics. Proper preservatives are used for specific parameters. The samples are kept under refrigeration at 4° C until delivered to laboratory for analysis. • Sampling Log Sampling' information is recorded on a chain of custody (COC) form by City of Kinston personnel or their designated representative provided by the respective laboratory that is performing the required testing required by the permit. Log book entries include, at a minimum: o Purpose of sampling o Location of sampling point o Type of sample (grab or composite) o Name of person collecting samples o Type of Biosolids sampled (undigested, post -digestion, post -storage) CITY OF KINSTON NON -DISCHARGE PERMIT NO. WQOOXXXXX OPERATIONS AND MAINTENANCE PLAN CLASS A BIOSOLIDS o Number and volume of sample(s) collected o Description of sampling point o Date and time of collection The respective WWTP's Class A Biosolids will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQOOOXXXt to include: o Toxicity Characteristics Leaching Procedure (TCLP), o Reactivity, Ignitability and Corrosivity, 0 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis, o Pathogen and Vector Attraction Reduction requirements, o Any other applicable Permit conditions. Pollutant concentrations for Class A Biosolids shall not exceed the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis): Parameter Ceiling Concentration (milligrams per kilogram) Monthly Average Concentration (milligrams per kilogram) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 Class A Biosolids shall be analyzed to demonstrate it is non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed prior to land application of Class A Biosolids. CITY OF KINSTON NON -DISCHARGE PERMIT NO. WQOOXXXXX OPERATIONS AND MAINTENANCE PLAN CLASS A BIOSOLIDS TCLP analysis of Class A Biosolids shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5 Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane(3.0) 2,4,5-Trichlorophenol(400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor(10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) An analysis shall be conducted on the Class A Biosolids based on conditions set forth in Permit No. WQOOXXXXX. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) CITY OF KINSTON NON -DISCHARGE PERMIT NO. WQOOXXXXX OPERATIONS AND MAINTENANCE PLAN CLASS A BIOSOLIDS Pathogen Reduction: Per 15A NCAC 02T.1106 For DistributionlLand Application of Class A or Equivalent. A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids AND Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). JK heat drying Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107 M Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Biosolids. Shared\WMSS Projects\2019\19-07 City of Kinston\Class A Permit Application Info\City of Kinston Class A O&M Plan - Nov. 2019.doc APPENDIX IV RESIDUALS SOURCE CERTIFICATION APPLICATION FORM JOHNNIE MOSLEY REGIONAL WRF (FORM: RSC 06-16) • JOHNNIE MOSLEY REGIONAL WRF (FORM: RSC 06-16) (ATTACHMENTS) o VICINITY MAP o PROCESS FLOW DIAGRAM AND/OR NARRATIVE o QUANTITATIVE JUSTIFICATION o SAMPLING PLAN o ANALY TICAL DWR State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 06-16): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Mao Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page l of 1 ci 0 4i O U E c a Q L W N d L L H1 a W m q 0 F G1 e fi c U w a s z z fi L a V •� O q O U a m N O z a •Ti � w � O n x °o m QI 0 U w 7 N � o Z r%� U State of North Carolina IDepartment of Environmental Quality � Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Johnnie Mosley Regional WRF 2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private. Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: _). 3. Facility contact person and title: Swindell Flowers. Land Application ORC Complete mailing address: 2101 Becton Farm Road City: Kinston State: N.C. Zip: 28501 Telephone number: (M) 939-3248 E-mail address: swindel].flowers@ci.kinston.nc.us 4. Facility physical address: 2101 Becton Farm Road City: Kinston State: N.C.. Zip: 28501 Coordinates: Latitude: 35' 17' 17" Longitude: 77°30' 48" Datum: NAD83 Level of accuracy: nearest second Method of measurement: MAP 5. Purpose of the facility: 0 treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and % domestic) ❑ other (explain: _ ). 6. Does the facility have an approved pretreatment program: 0 Yes ❑ No 7. Facility permitted/design flow: 11_85 MOD and facility average daily flow: 5 MGD 8. Average amount of residuals being generated at this facility 1 100 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Type and volume of residuals storage (i.e., outside of residuals treatment units): 4 sheltered concrete pads II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 0 40 CFR Part503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: 0 Biological ❑ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes C9 no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: SGS North America. Inc and Date of analysis: 11/12/19 Passed corrosivity test: ® yes [] no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: _ OF (> 140°F) Passed reactivity test: ® yes ❑no. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500) TCLP Parameter Limit (m9/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 <0.10 Hexachlorobenzene 0.13 <0.0069 Barium 100.0 <2.0 Hexachloro-1,3-Butadiene 0.5 <0.0050 Benzene 0.5 <0.0031 Hexachloroethane 3.0 <0.016 Cadmium 1.0 <0.050 Lead 5.0 <0.050 Carbon Tetrachloride 0.5 <0.0036 Lindane 0.4 <0.000022 Chlordane 0.03 <0.00038 Mercury 0.2 <0.0050 Chlorobenzene 100.0 <0.0020 Methoxychlor 10.0 <0.000050 Chloroform 6.0 <0.0030 Methyl Ethyl Ketone 200.0 0.918 Chromium 5.0 <0.10 Nitrobenzene 2.0 <0.0093 m-Cresol 200.0 0.0510 Pentachlorophenol 100.0 <0.050 o-Cresol 200.0 <0.0056 Pyridine 5.0 <0.020 p-Cresol 200.0 0.0510 Selenium 1.0 <0.10 Cresol 200.0 0.0510 Silver 5.0 <0.10 2,4-D 10.0 <0.017 Tetrachloroethylene 0.7 <0.0022 1,4-Dichlorobenzene 7.5 <0.0026 Toxaphene 0.5 <0.0021 1,2-Dichloroethane 0.5 0.0127 Trichloroethylene 0.5 <0.0035 1,1-Dichloroethylene 0.7 <0.0032 2,4,5-Trichlorophenol 400.0 <0.0074 2,4-Dinitrotoluene 0.13 <0,0081 2,4,6-Trichlorophenol 2.0 <0.0075 Endrin 0.02 <0.000021 2,4,5-TP (Silvex) 1.0 <0.0013 Heptachlor and its Hydroxide 0.008 <0.000026 Vinyl Chloride 0.2 <0.0041 FORM: RSC 06- l6 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105., a. For Distribution/Laud Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Environment 1. Inc. and Date of analysis: 12/06/19 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 2.7 Cadmium 85 39 0.74 Copper 4,300 1,500 151 Lead 840 300 16 Mercury 57 17 0.37 Molybdenum 75 n/a <5.0 Nickel 420 420 12 Selenium 100 100 <5.0 Zinc 7,500 2,800 638 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: — Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but <25 30 200 210 ❑ >_ 25 but < 50 34 220 240 ❑ >_ 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ >_ 100 but < 125 53 360 390 ❑ >_ 125 62 450 420 Result (mg/kg) FORM: RSC 06- l6 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 89.14 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Environment 1. Inc. and Date of analysis: 12/06/19 Parameter Result (mg/kg) Aluminum 25,794 Ammonia -Nitrogen 1,045 Calcium 18,213 Magnesium 9,608 Nitrate -Nitrite Nitrogen 14.96 pH (Standard Unit) 5.8 Phosphorus 55,020 Potassium 9,153 Sodium 4,167 Total Kjeldahl Nitrogen 59,040 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 5.85 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): 0 default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (151) Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (mg1kt) Surface 17,396 29,250 Injection/Incorporation N/A N/A 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106 specify how residuals will meet the pathogen reduction requirements: a. For Distribudon/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ Asalmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D)] -No Prior Testing for Enteric Virus/Viable Helminth Ova. M Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, M heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For LandADplicationofClass B: ❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T. 1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal.• ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11.7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item 1I.8. below [15A NCAC 02T.1106(a)(2)1. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. M Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] -Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 • JOHNNIE MOSLEY REGIONAL WRF (FORM: RSC 06-16) (ATTACHMENTS) o VICINITY MAP o PROCESS FLOW DIAGRAM AND/OR NARRATIVE o QUANTITATIVE JUSTIFICATION o SAMPLING PLAN o ANALYTICAL i k I o 1 � T WT 1 y c r5 ,5 rd ' �. � m .ram ?r �, i � • xkd 1{ail ` = �• Faulkne_.r�-.,R�.d i� 4:'�- -.ram - R • � ;.y¢ pasII�HP�annog • + 1c i a f �Cv�.,. ,. ' Its` O .x • ;�, o ti I� Oal' `.. j x .. 'fir ar _ •.1 ` •J� h_ 9 DRYER INFORMATION Narrative The project objective is to produce Class A Biosolids at the City of Kinston Johnnie Mosley WRF. The existing biosolids handling system (belt filter press, lime stabilization) produces Class B Biosolids. The City of Kinston Johnnie Mosley WRIT biosolids treatment system will be upgraded to replace the lime stabilization process with a new low temperature, thermal drying system to treat the dewatered sludge from the existing belt filter press. The lime stabilization system will be removed from the site. The biosolids produced with the Dryer will meet Class A requirements: Requirement to meet Pollutant Limits: NCAC 02T .1106 (a) and (c) [Section 503.13, Table 1 Ceiling Limits and Table 3 Pollutant concentrations]: these are met by the current treatment plant; the Dryer project will have no impact on the pollutants (ceiling levels are dry basis) Vector Attraction Reduction: NCAC 02T .1107 (a) (7) [Section 503.33 (a) (7)] "percent solids of sewage sludge that does not contain Unstabilized solids generated in a primary wastewater treatment process shall be equal to or greater than75 percent based on the moisture content and total solids prior to mixing with other materials" Pathogen Reduction Requirements: NCAC 02T .1106 (b) (3) Pathogen Reduction Requirement: Dryer will meet the Item (F) Process to Further Reduce Pathogens — Heat Drying (condition description): (F) Process to Further Reduce Pathogens - Heat Drying. The biological residuals shall be dried by direct or indirect contact with hot gases to reduce the moisture content of the biological residuals to 10 percent or lower. During the process, either the temperature of the biological residuals particles exceeds 80 degrees Celsius or the wet bulb temperature of the gas in contact with the biological residuals as they leave the dryer exceeds 80 degrees Celsius. Wastewater Treatment Process NCO024336 The Kinston Regional Water Reclamation Facility plant is permitted by the NC DEQ Division of Water Resources NPDES Permit Number NC0024336. The plant is a fully automated treatment facility considered state of the art. Its primary goal is to remove nutrients that causes oxygen depletion in the Neuse River. New modifications have been added to improve water quality and meet future discharge limits. These new modifications include computers that monitor and control all aspects of treatment for more efficient operations. Other modifications include denitrifrcation filters and ultraviolet disinfection (UV). Denitrification Filter The denitrification filter is a deep sand filter bed. As water passes through the filter, particulate matter is trapped into the sand. The cleaner water is then discharged to the disinfection process. An added benefit to this system is that we can add a food source for the remaining bacteria that will cause them to use the chemical oxygen found in the nitrates of the effluent water. Once the chemical oxygen has been used, only pure nitrogen remains which bubbles off harmlessly into the air, thus preventing more nitrogen from entering into the Neuse River. Ultraviolet Disinfection The final treatment process is the disinfection of the plant effluent. The old disinfection process used gaseous chlorine to kill pathogenic organisms. This is a proven and very effective method of disinfection. The problem is that Chlorine has also been proven to be toxic to aquatic life, and will combine with other organic material to form compounds that have been shown to cause cancer. Because of this, more chemicals are added to remove any remaining chlorine after the disinfection process has been completed. The new plant has the ability to use ultra -violet light (UV). UV is a non -chemical process that prevents the bacteria from reproducing instead of actually killing the bacteria. This saves on chemical costs and prevents further damage to the environment. Dewatering and Biosolids Treatment Biosolids are aerobically stabilized followed by dewatering with Belt Filter Press. The sludge cake is chemically treated with lime mixing to generate Class B biosolids. This Dryer project will upgrade biosolids treatment to Class A. Dryer Operations The thermal drying system will use hot air convection at low temperature (150/175°F) (65/80°C) in abelt dryer. This system will treat the existing mechanically dewatered biosolids from the existing WRF. The Dryer will be capable of processing 10 dry tons per day (DTPD) of biosolids with an initial dry solid content of 16 percent. The final product will have a concentration of at least 90% dry solids. The new Dryer facility will be designed to run 24 hours per day seven days per week with capability of processing the design waste quantity in 24 hours. Proof of Concept Testing was performed in January 2016 with a Pilot Dryer unit located at the City of Kinston Johnnie Mosley WRF treating the existing mechanically dewatered biosolids. The testing confirmed that the Dryer unit can produce Class A Biosolids. Information on that testing is included as an Attachment to this Notebook. The new Dryer system will include the dryer unit and material handling. A new receiving hopper (8.5 cubic yard capacity) will be installed outside under the existing discharge conveyor from the existing Belt Filter Press. These dewatered biosolids will be pumped from the new hopper into the Dryer feed system. The feed system extruder spreads biosolids onto an upper belt which conveys solids to a lower belt that discharges the dried biosolids by conveyor to a new hopper. Dryer belt will be controlled (temperature, air flow) to attain proper dryness. The dried Class A Biosolids dried product will be stored inside the sludge building available for customers. The Class A Biosolids (when pathogen requirements are met) may be applied to a lawn, home garden, or public contact use site or sold or given away in a bag or other container for application to the land. The procedures and records for this will be maintained by a contractor to the City of Kinston. III City of Kinston (NC) 526.030.08 Operation and Maintenance Manual - Drawings Appendix 8 - Drawings suet Document No: 523.030.08 Issue Date Prepared by: Checked by: Approved by: A 15/04/2019 R. Mampel N. Prats I. Arafto Copyright: We reserve all rights in this document and in the information contained therein. Reproduction, use or disclosure to third partners without express authority is strictly forbidden. Copyright © SUEZ WATER TECHNOLOGIES AND SOLUTIONS SPAIN, S.L. SUEZ Water Technologies and S011itlons Drying Technologies B.U. — Avda. Hnos Bou sin P.B. 490 E-12080 Castellon (SPAIN) T lernm e <-,, 1: +�?Gi-i B3 i4lail .!�!!in p:��:haologies.wts@suer.com City ofKinston (NC) 526^0J0^U8 OpesdnnandMaintonanooManua|—Drawinga CONTENTS ^���v��� �N8^�� PLANT GENERAL ARRANGEMENT .................................... ..... ............................ .................... ............ 3 DRYER GENERAL ARRANGEMENT ............................ .............................................. 4 PUMPS SKID GENERAL ARRANGEMENT .,.......~,.—^_~.^..~.^^,°^.^°—.,.^~^'—. 5 COOLING TOWER GENERAL ARRANGEMENT ............ .......................................................................... 0 SOLEPLATE PLAN .............. ............................................... ...................................................................... 7 P&DDRYER ........... --- ................................................................................................. 8 P&V}WATER PUMPS SKID ..................... ................... ....................... .......... 8 P&DCOOLING TOWER ................. ................................................................................. ....................... O |!!!|§ § ] | |-!' ; Wit §|�: [ . |Amp � | §� § ■ . LIM "I L11 :w ml Lwc ate_ [ , / ( i � � i i i � i i \ � ; . �L Sa k § k� Oil _ ` \ / § § § � \ � ` E § ! � ) % | ! ¥ U .tell, [==: A Q i v ]6 RR MR (Atsas3 fi a� r: FIR [Pel 9KI NNI [S.0] —d V O� 0 Y alo q q U $Y 3tlG OS_ a� W'IEI[ [.AIE 6;EL] Alp WW Od' Edl L q'p a& Co b� n� .ma+g� [slrcl 11-ll] 466Z99d � � � |!!!|! f , .� `|..■, ! MN »wGd 61 in 09- li Iola- Eta- a- Z_ 4""'! In Imel- me- F ------ 7- I JP. ima- Hil | |\|H §! } | \ Milo; ) /• /. Gil # | I . Ii-Ix ^ ' d /| | j a �: . .f! M. �) � |•-} .! |a ! � | � !> E * , !!! ; ° � � �■ �� ! . � | �! �- ƒ UIEIG } ! f`~ y . (`® � | §� ] ` ] | ! \� �} { JOHNNIE MOSLEY REGIONAL WRF (QUANTITATIVE JUSTIFICATION) • Class B — Land Application 0 2016—1,066.90 DT 0 2017-1,156.33 DT 0 2018 — 95.51 • Class A Permit Request for increased future volumes of 4,000 Dry Tons / Year Sampling and Monitoring Plan Sampling Procedures Accurate sampling is essential for valid laboratory test results. All samples collected at the respective Wastewater Treatment Plant (WWTP) are grab samples, which are samples taken at selected intervals to represent conditions at a given location at a particular point in time. Grab samples of biosolids are stored in a manner that will not alter sample characteristics. Proper preservatives are used for specific parameters. The samples are kept under refrigeration at 4° C until delivered to laboratory for analysis. Sampling Log Sampling information is recorded on a chain of custody (COC) form by City of Kinston personnel or their designated representative provided by the respective laboratory that is performing the required testing required by the permit. Log book entries include, at a minimum: • Purpose of sampling • Location of sampling point • Type of sample (grab or composite) • Name of person collecting samples • Type of residuals sampled (undigested, post -digestion, post -storage) • Number and volume of sample(s) collected • Description of sampling point • Date and time of collection The respective W WTP's Class A Biosolids will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQOOOXXXX to include: • Toxicity Characteristics Leaching Procedure (TCLP), • Reactivity, Ignitability and Corrosivity, • 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis, • Pathogen and Vector Attraction Reduction requirements, • Any other applicable Permit conditions. Pollutant concentrations in the Class A Biosolids shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs): Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 The respective W WTP's Class A Biosolids shall be analyzed to demonstrate it is non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed annually. TCLP shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol(100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) 0.008) Toxaphene (0.5) Chloroform (6.0) Hexachlor(o153)-butadiene Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol(200.0) Lead (5.0) 2,4,6-Trichlorophenol(2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) An analysis shall be conducted on the respective W WTP's C1assA Biosolids based on conditions (monitoring frequencies) set forth in Permit No. WQOOOXXXX. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) The respective W WTP's Class A Biosolids shall be analyzed to demonstrate compliance with Pathogen Reduction and Vector Attraction Reduction requirements based on conditions (monitoring frequencies) set forth in Permit No. WQ0011431. The current Pathogen Reduction Alternatives and Vector Attraction Reduction Options utilized are as follows: Pathogen Reduction: Per 15A NCAC 02T.1106 For Distribution/Land Application of Class A or Equivalent. A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids AND 0 Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). 19 heat drying Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107 M Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. Willcox & Mahe Soil Solutions, PLLC RESIDUAL PAN CALCULATION Johnnie Mosley Regional WRF TKN= 59,040 mg/kg NH3= 1,045 mg/kg NO3-NO2-N= 14.96 mg/kg Min Rate= 0.30 PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2J * 0.002 0.30 57,995 523 14.96 PAN= 35.87 LBS/DT PAN= 17,936 mg/kg Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine the amount of PAN/DT remaining. 2ND YEAR RESIDUAL PAN PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002 0.15 57,995 17,399 PAN= 12.18 LBS/DT remaining from I st year application 3RD YEAR RESIDUAL PAN PAN= [min. rate (2nd year org. - N 3rd year min. - N] * 0.002 0.08 40,597 6,089 PAN= 5.52 LBS/DT remaining from 1st year application 4TH YEAR RESIDUAL PAN PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002 0.05 34,507 2,761 PAN= 3.17 LBS/DT remaining from I st year application 5TH YEAR RESIDUAL PAN PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002 0.03 31,746 1,587 PAN= 1.75 LBS/DT remaining from 1st year application Residual PAN from years 2 thru 5 after the initial application = 11,314 mg/kg Five -Year Maximum Adjusted PAN = 29,250 mg/kg Kinston SAR SAR Calculation Na mg/I Ca mg/I Mg mg/I 3714.4638 16235.0682 8564.5712 Na Ca Mg SAR 161.498 811. 553 713.714 5.85 Na mil eq Ca mil eq Mg mil eq 161.498 811.753 713.714 Enter Enter .% TS 89.14 Data Na mg/kg 4167 Ca mg/kg 18213 Mg mg/kg 9608 Job Name: Johnnie Mosley Regional WRF Page 2 CITY OF KINSTON NCDEQ - CLASS A LAND APPLICATION BIOSOLIDS ANALYSIS Residual Type: Biosolids Date Sampled: November 12, 2019 City of Kinston Pellets Permit No. New Mineralization Rate 0.3 89.14 % Solids 5.8 pH Parameter % Mg/Kg Dry Weight Pounds/Dry Ton (*/* x 10.0001 (Me/Ke x 0.002) :a (TKN) 5.904 59,040.000 118.080 orus 5.502 55,020.000 110.040 am 0.915 9,153.000 18.306 n'ected)* 1.846 18,458.460 36.917 urfaee)* 1.794 17,935.960 35.872 tiaNitrogen 0,105 1,045.000 2.090 n 1.821 18,213.000 36.426 a Carbonate Eq. -- __- dum -- 9,608.000 19.216 --- 4,167.000 8,334 - N / Nitrite N --- 14.960 0.030 um --- 25,794,00 51.588 --- 2.700 0.005 im --- 0.740 0.001 um.-- --- --- --- 151.00 0,302 --- 16.000 0.032 y --- 0.370 0.001 count --- 5.000 0.010 --- 12.00 0.024 m --- 5.000 0.010 --- 638.00 1.276 Environment 1 582 S *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. SAR 5.85 Ceiling Concen. (M ) 75 85 4,300 840 57 75 4Z0 100 7,500 WP0Il6�liu M % hmpuVad N.C. KINSTON REGIONAL. PLANT EMILY ELMORE PUBLIC UTILITIES P.O. SOX 339 KINSTON ,NC 28502 Dried Analysis Method PARAMETERS Biosolids Date Analyst Code PH, Units 5.8 11/13/19 TMR 4500HB-11 Aluminum, (dry wt. basis), mg/kg 25794 11/27/19 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 2.7 11/27/19 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 18213 11/27/19 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 0.74 11/27/19 MTM 3113E-04 Copper (dry wt. basis), mg/kg 151 11/27/19 LFJ EPA200.7 Lead (dry weight basis), mg/kg 16 11/26/19 1vr M 3113B-04 Magnesium (dry wt. basis), mg/kg 9608 11/27/19 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.37 11/25/19 NAB EPA7471B Nickel (dry wt. basis), mg/kg 12 11/27/19 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 9153 11/27/19 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 12/04/19 MTM 3113B-04 Sodium (dry wt. basis), mg/kg 4167 11/27/19 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 638 11/27/19 LFJ EPA200.7 Total Solids, % 89.14 11/12/19 KDS 254OG-11 TKN (dry wt.), mg/kg c 59040 11/14/19 TLH 351.2 112-93 Ammonia Nitrogen (dry wt.),mg/kg c 1045 11/13/19 DTL 350.1 112-93 Phosphorus, T. (dry wt.), mg/kg c 55020 11/14/19 AKS 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 14.96 11/14/19 DTL 353.2 R2.93 Molybdenum (dry wt. basis), mg/kg <5.0 12/04/19 LFJ EPA200.7 FAX (252) 756-0633 ID#: 582 S DATE COLLECTED: 11/12/19 DATE REPORTED : 12/06/19 REVIEWED BY: c Uncerti=ied data. DWR does not offer non -aqueous certification for this analytical procedure. r Ci - 0 a o - z O ari < Z�— < Z U O Z t m g J w w W O W LL ('J Y 2 �aI O m ¢ z O z� oo2i iFr w Y w w ¢ w O= =, U 0171 z \ ¢ O ¢ m U 0 v S1S31/SH313WVHVd a s u¢ u a SIMON d'IO.L C7 a saplalgiaH d'IJ.L u a s wl wad d-[,)l w C7 a IONS/lOA d'IJ.L S - < 40d w w w _ a -OAj +1 uluowwv F < NNI _ < Slnlaly a a Hd z SU NIVINOO.O= 00 cF o w 0 C7 " u' NOLL03t1001V Z U O 0o'3EWLM3MR >- > w w N0110311001b' On 80 O171173071 I/bw'3NIHOlH0 ltl101 s ¢ ¢ w n W tj o p" F1 E C fn Z W 0yaU — ^ �� F Z n U< O sou u n RbEN Oriz The results set forth herein are provided by SGS North America Inc. Technical Report for Environment 1, Inc Kinston Regional Plant: Kinston, NC 582S SGS Job Number: FA70002 Sampling Date: 11/12/19 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@envirorunentlinc.com Deedee Woolard Total number of pages in report: 13 e-Hnrdeopy 2. Attiomnfed Report ,• P AC`%rE0 � zt1in Test results contained within this data package meet the requirements Brice, M.S. General Manager of the National Environmental Laboratory Accreditation program and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 certifications; FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022). SC(96038000 DoD ELANANAB L2229), AZ(AZ0806), CA(2937). TXCr104704404). PA(68-03573), VA(460177), AK, All, IA, RY, MA, MS, ND, NH, NV, OR, OR, UT, WA, WV This report shall not be reproduced. except in its entirely, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • Id: 407-425-6700 • fax: 407-425-0707 SGS is the ,ale authority for authorizing edits a wudiiieatinn. to :his docunn.!t! Please ,h.oe yum idea, about Q'n Unauthorized madific8tion of this item! is strictly pn+hihu yl, how we of ,c'ee you better m: SGS Review standard terms at:hrtp://www.sgS.convcngcnns.md-condiliona Ei1S.US.Cu-"m,rrCn eirt sgs.ro,n 1 of 13 FArua02 Table of Contents -1- Section1: Sample Summary................................................................................................... Section2: Summary of Hits.................................................................................................... Section3: Sample Results........................................................................................................ 3.? : FA70002-1: DRIED BIOSOLIDS................................................................................ Section4: Misc. Forms............................................................................................................ 4.1: Chain of Custody........................................................................................................... Sections: 3 4 5 6 11 12 SGS 2 of 1 FA7W SGS North America Inc. Sample Summary Environment 1, Inc Kinston Regional Plant; Kinston, NC Project No: 582S Job No: FA70002 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA70002-1 11/12/19 08:00 CC 11/16/19 SO Solid DRIED BIOSOLIDS Soil samples reported on a dry weight basis unless o0herwise indicated on result page. I Summary of Hits Page I of I Job Number: FA70002 Account: Environment 1, Inc Project: Kinston Regional Plant; Kinston, NC Collected: 11/12/19 Lab Sample ID Client Sample to Result/ Analyte Qua[ RL NIDL Units Method FA70002-I DRIED BIOSOLIDS 2-Butanone (ME%) 0.918 0.050 0.020 mg/I SW846 8260B 1,2-Dichloroethane 0.0127 0.010 0.0031 mg/I SW846 8260B 3&4-Methylphenol 0.0510 0.050 0.0098 mg/I SW846 8270D q�,S"' 4 of 13 adG FA70002 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample to: DRIED BIOSOLIDS Lab Sample to: FA70002-1 Date Sampled: 11/12/19 Matrix: SO - Solid Date Received: 11/16/19 Method: SW846 8260B SW846 1311 Percent Solids: n/a Project: Kinston Regional Plant; Kinston, NC File to DF Analyzed By Prep Date Prep Batch Analytical Batch Run 01 5E19189.D 10 11/21/19 19:04 SO 11/19/1912:30 OP77780 V5E867 Run #2 Purge Volume tun #1 5.0 ml tun #2 VOA TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 71-43-2 Benzene ND D018 0.50 0.010 0.0031 mg/1 78-93-3 2-Butanone (MEK) 0.918 D035 200 0.050 0.020 mg/I 56-23-5 Carbon Tetrachloride NO D019 0.50 0.010 0.0036 mg/1 108-90-7 Chlorobenzene ND D021 100 0,010 0.0020 mg/1 67-66-3 Chloroform ND D022 6.0 0,010 0.0030 mg/I 106-46-7 1,4-Diclilorobenzene ND D027 7.5 0.010 0.0026 mg/1 107-06-2 1,2-Dichloroethane 0.0127 D028 0.50 0.010 0.0031 mg/I 75-35-4 1,1-Dichloroethylene ND D029 0.70 0.010 0.0032 mg/I 127-18-4 Tetmcldoroethylene ND D039 0.70 0,010 0.0022 mg/1 79-01-6 Trichloroedtylene NO D040 0.50 0.010 0.0035 mg/I 75-01-4 Vinyl Chloride ND D043 0.20 0.010 0.0041 mg/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dibromofluoromethane 97% 83-I18% 17060-07-0 1,2-Dichloroelhane-D4 100% 79-125% 2037-26-5 Toluene-D8 105% 85-112% 460-00-4 4-Bromofluorobenzene 108% 83-118% ND = Not detected MDL = Method Detection Limit I = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �fl...,v.,.. 6 of 13 Favoaoz SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: DRIED BIOSOLIDS Lab Sample ID: FA70002-1 Date Sampled: 11/12/19 Matrix: SO - Solid Date Received: 11/16/19 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: Kinston Regional Plant; Kinston, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 91007426.1) 1 11/25/19 17:59 MV 11/23/19 08:00 OP77840 S91272 Run #2 a X068230.1) 1 12/02/19 15:35 MV 11/23/19 08:00 OP77840 SX2805 Initial Volume Final Volume _ Run #1 100 ml 1.0 ml Run #2 100 ml 1.0 ml ABN TCLP List CAS No. Compound TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q 95-48-7 2-Melhylphenol ND D023 200 0.050 0.0056 mg/I 3&4-Methylphenol 0.0510 D024 200 0.050 0.0098 mg/I 87-86-5 Pentachlorophenol ND D037 100 0.25 0.050 mg/I 95-95-4 2,4,5-Trichlorophenol NO D041 400 0.050 0.0074 mg/l 88-06-2 2,4,6-Trichloropbenol ND D042 2.0 0.050 0.0075 mg/I 106-46-7 IA-Dichlorobenzeue NO D027 7.5 0.050 0.0050 mg/I 121-14-2 2,4-Dinitrotoluene NO D030 0.13 0.050 0.0081 mg/I 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/1 87-68-3 Hexachlorobutadiene NO D033 0.50 0.050 0.0050 mg/I 67-72-1 Hexachloroethane NO D034 3.0 0.050 0.016 mg/1 98-95-3 Nitrobenzene b - NO D036 2.0 0.050 0.0093 mg/I 110-86-1 Pyridine NO D038 5.0 0.10 0.020 mg/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 367-12-4 2-Fluorophenol 15% 15% 14-67% 4165-62-2 Phenol-d5 11% 11% 10-50% 118-79-6 2,4,6-Tribromophenol 31% c 26% 33-118% 4165-60-0 Nitrobenzene-d5 46% 39% 42-108% 321-60-8 2-Fluorobiphenyl 36% c 36% 40-106% 1718-51-0 Terphenyl-d14 37% c 39% 39-121% (a) Confirmation run for surrogate recoveries. (b) Associated CCV outside of control limits high, sample was ND. (c) Outside control limits due to matrix Interference. NO = Not detected MDL = Method Detection Limit ] = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found In associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound I of i3 FA7000? SGS North America Inc. Report of Analysis at Sample ID: DRIED BIOSOLIDS Sample ID: FA70002-1 rix: SO - Solid hod: SW846 8151A SW846 3510C ect: Kinston Regional Plant; Kinston, NC File ID DF Analyzed By #1 CC005246.1) 1 11/25/1912:37 RS #2 Initial Volume Final Volume on #1 10.0 ml 5.0 ml on #2 Page 1 of I Date Sampled: 11/12/19 Date Received: 11/16/19 Percent Solids: n/a Prep Date Prep Batch Analytical Batch 11/23/19 10:30 OP77842 GCC1558 Herbicide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 94-75-7 2,4-1) ND D016 10 0.050 0.017 mg/I 93-72-1 2,4,5-TP (Silvex) ND D017 1.0 0.0050 0.0013 mg/l CAS No. Surrogate Recoveries Run# I Run# 2 Limits 19719.28.9 2,4-DCAA 78% 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound aua 8 of 13 FA70=2 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample to: DRIED BIOSOLIDS Lab Sample ID: FA70002-1 Date Sampled: 11/12/19 Matrix: SO - Solid Date Received: 11/16/19 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Kinston Regional Plant; Kinston, NC i File to DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 KK95847.D 1 11/25/19 17:04 WH 11/23/19 08:00 OP77841 GKK3056 Run #2 Initial Volume Final Volume Run #1. 100 ml 5.0 ml Run #2 Pesticide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) a ND D013 0.40 0.00010 0.000022 mg/I 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/I 72-20-8 Endrin 3 NO D012 0.020 0.00020 0.000021 mg/I 76-44-8 Heptachlor a ND D031 0.00800.00010 0.000026 mg/I 1024-57-3 Heptachlor epoxide a ND D031 0.0080 0.00010 0.000020 mg/1 72-43-5 Methoxychlor ND D014 10 0.00020 0.000050 mg/l 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 877-09-8 Tetmchloro-m-xylene 76% 42-127% 2051-24-3 Decacldorobiphenyl 51% 27-127% (a) Associated CCV outside of control limits high, sample was NO. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/I1) B = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound SGS9 of 13 FA70WZ SGS North America Inc. Report of Analysis Page I of I ;lient Sample ID: DRIED BIOSOLIDS .ab Sample ID: FA70002-1 Date Sampled: 11/12/19 4atrix: SO - Solid Date Received: 11/16/19 Percent Solids: n/a 'roject: Kinston Regional Plant; Kinston, NC Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/I 1 11/20/19 11/21/19 LM SW846 6010D 1 SW840 3010A 3 Barium < 2.0 D005 100 2.0 mg/I 1 11/20/19 11/21/19 LM SW846 6010D 1 SW846 3010A 3 Cadmium < 0.050 D006 1.0 0.050 mg/I 1 11/20/19 11/21/19 LM SW840 6010D 1 SW846 3010A 3 Chromium < 0.10 D007 5.0 0.10 mg/I 1 11/20/19 11/21/19 LM SW846 6010D 1 SW846 3010A 3 Lead < 0.050 D008 5.0 0.050 mg/I 1 11/20/19 11/21/19 LM SWB46 6010D 1 SW846 3010A 3 Mercury < 0.0050 D009 0.20 0.0050 mg/I 1 11/21/19 11/21/19 4C SW846 7470A 2 SW846 7470A 4 Selenium < 0.10 D010 1.0 0.10 mg/I 1 11/20/19 11/21/19 LM SW846 60101) 1 SW846 3010A 3 Silver < 0.10 D011 5.0 0.10 mg/I 1 11/20/19 11/21/19 LM SW84G 6010D 1 SW846 3010A 3 (1) Instrument QC Batch: MA16349 (2) Instrument QC Batch: MA16351 (3) Prep QC Batch: MP36445 (4) Prep QC Batch: MP36454 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/l/11) 10 of 13 vn 1:.a W cq7aaoz l �N Orlando, FL Section 4 IrNm Ed Misc. Forms Custody Documents and Oilier Forms Includes the following where applicable: • Chain of Custody 11 of 13 FA70002 En.troament 1, [nc. �,A76COZ CHAIN OF CUSTODY RECORD P.O. Box 7085, I190akmont Dr. �/�r11 P_ of Box 1 - --_ RM •8 [M.. a ... .. •. BOX 339I, • • i F -1 1 Iiiiiiiiii- ��M=11111 DURINGSHIPM rr ---.■■ ..■.■....■..■.. MA PtF.15E'. tratruc6or51m wmdelin9 tole imm on Ne r2versa 5iGt. 1a{�� i'araOsamP'o In the blPcci!vli eGwe1eech pgmPlelet taNestedl N_ 0 371355 FA70002. Chain of Custody Page 1 of 2 SGS Sample Receipt Summary Job Number. FA70002 Client: ENVA Protect: 582S Date I Time Ri csived: 111161201910:40:00 AM DOIIvery Method: FX Alrblli We: Them 10: IR 1; Therm OF: -0L8; 0 of Coolers: 1 Cooler Temps (Raw Measured) °Co Cooler 1: (8.5); Cooler Temps (Corrected) °C: Cooler 1: (5.7); Cooler Information Y or N Sample Information V or N NiA 1. Custody Seals Present I'm ❑ 1. Sample labels present on bottles 2. Custody Seals intact ❑ 2. Samples preserved property 3. Temp Where achieved Fi] [] 3. Sufficient volume/containers recvd for enelysis: [� 4. Cooler temp veMceion IR Gun 4. Condition of sample Walit S. Cooler media list3@ey S. Sample raced within HT Cl n S. DateaTmes/lOs on CDC match Sample Label W Q Trip Blank Information V or N NIA 7. VCCs have headspace (] ❑ 2 1. Trip Blank present I cooler 0 El pp B. Bodies recelved for unspecified tests p 2. Trip Blank listed on COC r ❑ 6.j 9. Composlting Instructions dear L] W or S NIA 10. Vos Soil Kits/dam received past 48hm? ❑ C ,G] 3. Type Of TS Received - d iI-% Solids Jar recelved? [, ❑ ;� 12. Residual CNodne Present? ! _' [ M isc. Information Nu. or En nm, 25 tcra.n 5-Gram _ Number of 5035 Field Iota: _ Number of Lab Shared Metals: Teat Sees to phi 0.3 230315 pH 10.12 219813A Other. (Specify) ReaiWel Qrbrkle Tqi Snip Lnl:. Cam�a Oa@: 111152019 /P.a0U8 Redevcec -- -_ SMAI Rev. Wteonen TecMldarr: PEr138i Date: FA70002: Chain of Custody Page 2 of 2 SGS!at FA Orlando, FL The resultS Set forth hercin arc provided by SGS North America Inc. Technical Report for Environment 1, Inc Kinston Regional Plant; Kinston, NC 582S SGS Job Number: FA71534 Sampling Date: 01/09/20 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentlinc.com ATTN: Deedee Woolard Total number of pages in report: 9 e-Hardeopy 2.0 A« tarnated Repar7 Q PCCRFO .ice � rr I iTNI i t 4� '7BORA.10Pi Test results contained within this data package meet the requirements C itlm Brice, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(F.30327), n.(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZO806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, All, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SGS is the sine nudturity for am hol A11L cd its or uludilieat ions to this docwncm. Picric Sparc your idcaa abaul c Unauthorized lnadi licaOo l Of this report is Strict lv Pruhihited. hots tee can serve aon hcucr at: __SG' 9 Review standard hrruu ae Imp://tctvw.n„Sxnm/rnhernts-and-conditions E4tS.US.CuslomerCareGas.s.' . unn 1 of FA71534 Table A Contents -I- Section1: Sample Summary................................................................................................... Section2: Summary of Hits.................................................................................................... ........................ ........................................... .................................... , rs. t: FA71534-1: DRIED BIOSOLIDS................................................................................ Section4: Misc. Forms............................................................................................................ 4.1: Chain of Custody........................................................................................................... Sections: 3 4 5 7 8 0 m 0 2 of FA7153,1 SGS North America Inc. Sample Summary Environment 1, Inc Kinston Regional Plant; Kinston, NC Project No: 582S Job No: FA71534 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA71534-1 01/09/20 11:20 CC 01/11/20 SO Solid DRIED BIOSOLIDS Soil samples reported on a dry weight basis unless otherwise indicated on result page. R ����,,0 OR 3of9 FA]15&1 Summary of Hits Page 1 of I Job Number: FA71534 Account: Environment 1, Inc Project: Kinston Regional Plant; Kinston, NC Collected: 01/09/20 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA71534-1 DRIED BIOSOLIDS Corrosivity as pH 6.3 so SW846 CHAP? Ignitability (Flashpoint) a > 200 Deg. F SW846 1010A MOD (a) Not ignitable. FAn534 Scs Orlando, FL Sample Results Report of Analysis Section 3 5 of ZIGS PA71534 SGS North America Inc. Report of Analysis Client Sample ID: DRIED BIOSOLIDS Lab Sample ID: FA71534-1 Date Sampled: 01/09/20 Matrix: SO - Solid Date Received: 01/11/20 Percent Solids: n/a a Project: Kinston Regional Plant; Kinston, NC General Chemistry Analyte Result Corrosivity as pH 6.3 Cyanide Reactivity < 1.5 Ignitability (Flashpoint) b > 200 Sulfide Reactivity <50 (a) All results reported on a wet weight basis. (b) Not ignitable. RL = Reporting Limit Page 1 of 1 RL Units DF Analyzed By Method so 1 01/21/20 13:20 BW SW846 CHAP7 1.5 mg/kg 1 01/17/20 09:41 AC SW846 CHAP7 Deg. F 1 01/16/2010:54 Bw SW8461010A MOD 50 mg/kg 1 01/18/20 13:09 BW SW846 CHAP? a qe(z•, 6 of FA71534 -SGS�_ Orlando, FL Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 0 s v 7 of9 FAl153J Environmenil,Ine. CHAIN OF CUSTODYRRCORD jg7j5 jy P.O. Box 7085. 114 Oakmont Dr. '`/% Greenville, INC 27958 ° 1 °f 1 ..i Ph • .. I: i. . • • . ................ monsoon monsoon e • a •, .m KINSTON REGIONAL PLANT PUBLIC UTILUIES P.O. BOX 339 e 1 > 11 son El MEMO ■ I 1 1 ■■■■.........■..... MINE IM MINN e PLEASE HAD Instructions for completlnp this form on the inverse side. Samplermmphcea"C"Iorcomposkommpleora"G"for FORM ns iJ1(lZ0 012rah sample In the blocks above for each pammetermquested. N2 376108 111 FA71534: Chain of Custody Page 1 of 2 e FA71539 SGS Sample Receipt Summary Job Number: FA71534 Client: ENV. 1 Date 1 Time Received: 1/111202012:00:00 PM Delivery Method: FX Project: 582 S Airbill We: Therm ID: IR 1; Therm CF: -0.8; # of Coolers: 1 Cooler Temps (Raw Measured) °C; Cooler is (5.7); Cooler Temps (Connected) °C: Cooler 1: (4:9); Cooler Information Y or N Samole Information Y or N N/A 1. Custody Seals Present 2 ❑ 1. Sample labels present on bottles 2 ❑ 2. Custody Seals Intact 2 Cl 2. Samples preserved properly 2 ❑ 3. Temp criteria achieved 2 ❑ 3. Sufficientvolume/containers rectal for analysis: 2 ❑ 4. Cooler temp verification IR Gun 4. Condition of sample Intact S. Cooler media Ice(Beat 5. Sample recvd within HT 2 ❑ 6. Dalea/rimesADs on CDC match Sample Label 2 Cl Trio Blank Information Y or N NIA 7. VOCS have headspece ❑ ❑ 2 1. Trip Blank present/ cooler ❑ ❑ 2 8. Borges received for unspecified tests ❑ 2 2. Trip Blank listed on CDC ❑ ❑ 2 9. Composlting instructions clear ❑ ❑ 2 W or S NIA 10. Voa Soil Kits/Jars received past 48hm? ❑ ❑ 2 11. %Solids Jar received? El El 3. Type Of T8 Received ❑ ❑ ® 72. Residual Chlorine Present? ❑ ❑ 2 Misc. Information Numberof Encores: 25-Gram 5-Gram Number of5035 Field Kit& Number of Lab Filtered Metals: Test Strip Lot#s: pH 0-3 230315 pH 10-12 219813A Other. (Specify) Residual Chlorine Test Strip Lot#: Comments ant°s1 m, D. p524111 Technician: PETERH Date: 1/112we 02012:00:00 P Reviewer. s Date: FA71534: Chain of Custody Page 2 of 2 0 9 of FA71534 Johnnie Mosley Regional WRF WQOOXXXXX Class A - 2019 bate !Fecal Coltfosm 1utPi?1 er atxL Lo g. 12/16/19 490 2.6902 12/16/19 480 2.6812 12/16/19 840 2.9243 12/16/19 480 2.6812 12/16/19 850 2.9294 12/16/19 860 2.9345 12/16/19 840 2.9243 Total 19.7652 Average 2.8236 Geometric Mean Fecal Coliform MPN /gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen Reduction requirement. Enw,u oIMEW Flo kwpumbd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 KINSTON REGIONAL PLANT EMILY ELMORE PUBLIC UTILITIES P.O. BOX 339 KINSTON ,NC 28502 Sample Sample Sample PARAMETERS #1 #2 #3 Total Solids, % 91.59 93.13 92.90 Fecal Coliform (MPN ), /gram Solids 490 480 840 Drinking Water ID: 37715 Weetewater ID, 10 PHONE (252) 756-620- FAX (252) 756-0633 ID#: 582 T DATE COLLECTED: 12/16/19 DATE REPORTED 11222/18/19 REVIEWED BY: /v Sample Sample Analysis Method #4 #5 Date Analyst Code 93.03 91.81 1Z/16/19 JMS 2540G-11 480 850 12/16/19 KDS 9221E-06 - a_ 4 �Dri.king Water IDt'�77735 Waetevater IDi 10 114 OAKMONT DRIVE GREENVILLE. N.C. 27858 KINSTON REGIONAL PLANT EMILY ELMORE PUBLIC UTILITIES P.O. BOX 339 KINSTON ,NC 28502 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 582 T DATE COLLECTED: 12/16/19 DATE REPORTED : 12/18/19 REVIEWED BY:// Sample Sample Analysis Method PARAMETERS #6 #7 Date Analyst Code Total Solids, % 90.28 92.81 12/16/19 JMS 254OG-11 Fecal Coliform (MPN), /gram Solids 860 840 12/16/19 I(DS 9221E-06 I h x. o � W C0 C7 h uzNr'i � o z Z 8 0 o O S d p w !.7iJ 2 3 } 0- Lu off[ LL IL trg�� g U' p ZI p } W Z m O Z Fr U ?i I3 � � Cl ~z �i a S1S3US8313MM U 7 1 1 N. 0 0'^ V1 F � Q O p w d IueaJlo3 w C SPIIoS Molt % M N E fit] z y SH3NIV.NOOdON 0 Rq O � w m NOI.L'l3l'IOOltl 0 Oo'3HfIVU3dVS1 x N011I/BW' 3 '3NIHOlHO -IV HO l q/6W I80 HOiV ltl101 C •j „�� Z ¢ ¢ �n i '4 •o o � F o v�i •" w W u� W N v� N' N ChO��"� F r > > 0. 0 a a a s a a 't3y�� w >, o a o o WU Ha - tJ la 0 .. ¢ 01 'T O cc M OI Z `o i 7 vi n u E 0