WQ0034513_Residual Annual Report 2019_20200213

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submital an
application?*
r Yes r No
Annual Report 2019
Year*
Date Paper Copy 2/13/2020
Received:*
Project Number* WQ0034513
Email Notifications
...................................................................................................
Does this need O Yes
review by the a No
hydrogeologist? *
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
.......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Rob Willcox
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0034513
Applicant\Permittee * Brunswick County
Facility Name * Brunswick County RLAP
Phone Number*
3363399128
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Class B Annual Report Submittal
Please attach all information required or requested for this submittal to be review here.
Application Forms Engineering Rans, Specifications, Calculations, Etc.)
2019 CLASS B ANNUAL REPORT - Brunswick
24.92MB
County-WQ0034513-signed.pdf
Upload only 1 PDF document. NL@iple documents must be combined into one PDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/11/2020

2019 ANNUAL REPORT
BRUNSWICK COUNTY PUBLIC UTILITIES
RESIDUALS LAND APPLICATION PROGRAM
NON -DISCHARGE PERMIT #WQ0034513
Prepared For:
Brunswick County
Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
Compiled By:
Willcox & Mahe Soil Solutions, PLLC
7231 B Summerfield Road
Summerfield, North Carolina 27358
February 2020

willcox&mate
SOIL SOLUTIONS
February 1, 2020
N.C. Department of Environmental Quality
Division of Water Resources — Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attention: Information Processing Unit
Reference: 2019 LAND APPLICATION ANNUAL REPORT
Brunswick County Public Utilities
Non -Discharge Permit No. WQ0034513
WMSS Project No. 15-04 Phase: 09
Non -Discharge Branch:
Willcox & Mahe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Brunswick County
Public Utilities (Brunswick County). WMSS compiled this report using data gathered during
the compliance year by Brunswick County and BioGreen Services, Inc. This data includes: 1)
land application certification forms, 2) annual residual sampling summary forms, 3) annual
pathogen and vector attraction reduction forms, 4) annual field summary forms and metals
field loading summary forms, 5) lab sheets, and 6) soil analysis reports.
Brunswick County land applied a total of 205.3 dry tons of biosolids under Permit No.
WQ0034513 during the 2019 calendar year (Carolina Shores W WTP-2.12 dry tons, Northeast
Brunswick Regional W WTP-34.32 dry tons, Ocean Isle Beach W WTP-20.82 dry tons, Sea
Trail WWTF-6.19 dry tons, and Shallotte WWTP-141.85 dry tons).
If there is any further information required or questions regarding this annual report please do
not hesitate to contact Mr. Donald Dixon, Deputy Director of Wastewater Operations with
Brunswick County at [phone] or Rob Willcox with WMSS for further assistance.
Sincerely,
Willcox & M�aab�e�Sooil Solutions, PLLCC
7,� t %' 6� � �wl -z sX
Martin Mahe 9PN/ Rob Willcox, L.S.S.
Agronomist/Partner Soil ScientistTartner
Enclosures
Shared\WMSS ProjectM2015115-04 Brunswick Count&hase 09 - 2019 Annual Report\Class M2019 CLASS BANNUAL REPORT -8n nswick
County.doc
Willcox & Mabe Soil SolUtions, PLLC/7231B Summerfield Road / Summerfield, NC 2735E / Rob336.339.9128 or
Martin 336.312.1396 /www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
Annual Land Application Certification Forms
(Form ACF)
II Annual Residual Sampling Summary Forms
(Form RSSF)
Annual Pathogen and Vector Attraction Reduction Forms
(503 Rules)
(Form PVRF 503)
IV Annual Land Application Field Summary Forms and Annual
Metals Field Loading Summary Forms
(Form FSF and MFLSF)
V Lab Sheets
VI Soil Analysis Reports

Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
RESIDUALS LAND APPLICATION PROGRAM
CLASS B RESIDUALS
PERMIT NO. WQ0034513
CAROLINA SHORES WWTP
NPDES PERMIT NO. NC0044873
NORTHEAST BRUNSWICK REGIONAL WWTP
NPDES PERMIT NO. NC0086819
OCEAN ISLE BEACH WWTP
PERMIT NO. WQ0006085
SEA TRAIL WWTF
PERMIT NO. WQ0012748
SHALLOTTE WWTP
PERMIT NO. WQ0000798
Mr. Donald Dixon, Deputy Director of Wastewater Operations
Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
[phone]
2019 Carolina Shores WWTP Dry Tons - 2.12
2019 Northeast Brunswick Regional WWTP Dry Tons - 34.32
2019 Ocean Isle Beach WWTP Dry Tons - 20.82
2019 Sea Trail WWTF Dry Tons - 6.19
2019 Shallotte WWTP Dry Tons - 141.85
Total Dry Tons 205.3
2019 Carolina Shores WWTP Dry Metric Tons - 1.92
2019 Northeast Brunswick Regional WWTP Dry Metric Tons - 31.13
2019 Ocean Isle Beach WWTP Dry Metric Tons - 18.88
2019 Sea Trail WWTF Dry Metric Tons - 5.61
2019 Shallotte WWTP Dry Metric Tons - 128.66
Total Dry Metric Tons 186.2

Brunswick County 2019 Summary (Class B - Permit No. WQ0034513)
Northeast-B
Ocean Isle-B
Carolina Shares-B
Sea Trail-B
Shallotte-B (Liquid)
(Gallons)
Shallotte-B (Cake)
(Cubic Yards)
January
36,000
February
221,000
79,500
March
153,000
52,000
April
May
66,000
50,500
June
July
32,500
August
September
October
689,000
40
November
169,000
December
7GalTom
153,000
390,000
281,500
135,000
689,000
40
34.32
20.82
2.12
6.19
140.21
1.64

SECTION I
ANNUAL LAND APPLICATION CERTIFICATION FORMS
(Form ACF)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034513 County:
Facility Name (as shown on permit):
Land Application Operator:
Brunswick
Brunswick Can
Year: 2019
Bio-Green Services, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes❑ No -If No, skip PartA, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv: Carolina Shores WWTP
Total number of application fields in the permit: 1 23
Total number of fields utilized for land application during the year:1 2
Total amount of dry tons applied during the year for all application sites: 1 2.12
Total number of acres utilizes for land application during the year: 1 21.7
Part B - Annual Comoiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .l 1 I 1 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon - Deputy Director ����� I
Perm'ifteeName and Title (type or print) 7 Signature of Permiittee 1Date
Signature- reparer* Carolina Shores Date Signature of Land Afplier Date
(if different from Pennittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00034513 County: Brunswick Year:
Facility Name (as shown on permit): Brunswick Countv
2019
Land Application Operator: Bio-Green Services, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes[] No -If No, skip Part A, and Part B and proceed to PartC. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary: Northeast Brunswick Reeional WWTP
Total number of application fields in the permit: 23 V
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 34.32
Total number of acres utilized for land application during the year: 23.0
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T.] I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in
the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon - Deputy Director �� N—t— t, I -3t-Z0
Permittee Name and Title (type or print) Signature of Permittee Date
Signature reparer*Northeast Brunswick Reg. W WTP Date Signature of Land lier Date
(if different from Penmittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DFNR FnRM Arr P ,)1,)n m

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00034513 County: Brunswick Year: 2019
Facility Name (as shown on permit): Brunswick County
Land Application Operator: Bio-Green Services, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes[] No -If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary: Ocean Isle Beach WWTP
Total number of application fields in the permit: 23
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites:1 20.82
Total number of acres utilizes for land application during the year: 1 23.5
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 1 SA NCAC 02T. I I I l were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of tines and imprisonment for knowing violations."
Donald B. Dixon - Deputy Director
� I —31- 2n
Permittee Name and Title(typeor print) Signature of Permittee Date
Signature of parer' Ocean Isle Beach WWTP Date Signature of Land Appl Date
(if different from Permittee) (if different from Permittee and Preparer)
x Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) nFNR Fnpm nrr rt')ivnnFl

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00034513 County:
Facility Name (as shown on permit):
Brunswick
Brunswick
Year: 2019
Land Application Operator: Bio-Green Services, Inc. Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes[] No -If No, skip Part A, and Part Band proceed to Part C. Also, If residuals were
336-940-4544
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary: Sea Trail W WTP
Total number of application fields in the permit: 23
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 6.19
Total number of acres utilizes for land application during the year: 21.7
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon - Deputy Director y (- 3 } -Zo
Permittee Name and Title (type or print) Signature of Permittee Date
l %AVi as " 0 /M 12—es� 2--11-
Signature eparer*Sea Trail WWTP Date Signature ofLand�Cpplier� Date
(if different from Permittee) (if different from Penmittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DFNR FDRM ACT f17/7rnfil

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00034513 County: Brunswick Year: 2019
Facility Name (as shown on permit):
Land Application Operator:
Brunswick
Bio-Green Services, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
21 Yes❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Shallotte WWTP
Total number of application fields in the pennit:1 23
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 1 141.85
Total number of acres utilizes for land application during the year: 80.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I 111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon - Deputy Director_
Permittee Name and Title (type or print) Signature of Permittee Date
- /- z-Jl-ZD
Shallotte W WTP Date Signature of Land Ap6fier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF i12/20061

6m Cl)a I I
ANNUAL RESIDUAL SAMPLING SUMMARY FORMS
(Form RSSF)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - R
WQ Permit Number: W00034513 Laboratory:
Facility Name: Brunswick County
Residual Source WQ # or NCO044873
NPDES #:
WWTP Name: Carolina Shores WWTP
Residual Analvsis Data
1) Environmental Chemists, Inc.
2)
3)
4)
5)
Parameter
(mg/kg)
Cone.
Limit
(mg/kg)'
Sample or Composite Date
01/02/19
Percent Solids (%)
NA
0.28
Arsenic
75
40.00
Cadmium
85
79.60
Chromium
NA
0.558
Copper
1 4,300
0.635
Lead
840
0.558
Mercury
57
0.019
Molybdenum
75
35.70
Nickel
420
0.558
Selenium
100
35.70
Zinc
7,500
1.77
Total Phosphorus
NA
105
TKN
NA
298
Ammonia -Nitrogen
NA
12.59
Nitrate and Nitrite
NA
1.20
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties
for submitting information, inc uding the possibility of fines and imprisonment for knowing violations."
s
Signature of Pr r * Date
*Preparer is defined m 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0034513
Laboratory: 1)
Facility Name:
Brunswick County
2)
Residual Source
NC0044873
3)
NPDCS # or WQ#:
4)
WWTPName:
Carolina Shores WWTP
g)
Residual Analvsis Data
Environmental Chemists, Inc.
Sample or Composite Date
tt
MM
-------------
-------------
-------------
-------------
-------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of PreDate
'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - D
WQ Permit Number: W00034468
Facility Name: Brunswick County
Residual Source WQ # or NCO086819
NPDES #:
W WTP Name: Northeast Brunswick Regional W WTP
Residual Analysis Data
Laboratory: 1)
2)
3)
4)
5)
Environmental Chemists, Inc.
Parameter
(mg/kg)
Cone.
Limit
(m /k gy
Sample or Composite Date
01/02/19
Percent Solids (%)
NA
5.38
Arsenic
75
10.9
Cadmium
85
10.9
Chromium
NA
29.9
Copper
4,300
1 140.0
Lead
840
10.9
Mercury
57
0.558
Molybdenum
75
10.9
Nickel
420
19.7
Selenium
100
10.9
Zinc
7,500
807.0
Total Phosphorus
NA
35,100
TKN
NA
94,600
Ammonia -Nitrogen
NA
43,100
Nitrate and Nitrite
NA
369.0
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, iip cludin the possibility of fines and imprisonment for knowing violations."
tgnaNr3 a of Prepn[er * Date
*Preparer is defined in 40 CFR Pan 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: W00034468 Laboratory:
Facility Name: Brunswick County
Residual Source NC0086819
NPDES # or WQN:
W WTP Name: Northeast Brunswick Regional W WTP
Residual Analvsis Data
1) Environmental Chemists, Inc.
2)
3)
4)
5)
MMMMMMMIMMMMMM
-------------
-------------
-------------
---------
"I certify, certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
11,494 /-?i-ao
�bignalure of Pr r* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - 8 (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00034513 Laboratory:
Facility Name: Brunswick County
Residual Source WQ N or
NPDES 4:
WWTP Name:
Residual Analvsis Data
W00006085
Ocean Isle Beach WWTP
2)
3)
4)
5)
Environmental Chemists, Inc.
Parameter
(mg/kg)
Cone.
Limit
(mg/kg)'
Sample or Composite Date
01/02/19
Percent Solids (%)
NA
1.28
Arsenic
75
39.80
Cadmium
85
39.80
Chromium
NA
39.80
Copper
4,300
1 70.90
Lead
840
39.80
Mercury
57
1.48
Molybdenum
75
39.80
Nickel
420
39.80
Selenium
100
39.80
Zinc
7,500
274.00
Total Phosphorus
NA
20,100
TKN
NA
61,800
Ammonia -Nitrogen
NA
5,030
Nitrate and Nitrite
NA
733.00
Jim
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for submittin false information, including the possibility of fines and imprisonment for knowing violations."
i
Signature of Pr er* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
DEN FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: W00034513 Laboratory:
Facility Name: Brunswick County
Residual Source W00006085
NPDES # or WQ#:
WWTP Name: Ocean Isle Beach W WTP
Residual Analvsis Data
1) Environmental Chemists, Inc.
2)
3)
4)
5)
-------------
-------------
-------------
-------------
-------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Prep Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM RSSF- B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00034513 Laboratory:
Facility Name: Brunswick County
Residual Source WQ p or W00012748
NPDES 4:
WWTPName: Sea Trail WWTF
Residual Analvsis Data
1) Environmental Chemists, Inc.
2)
3)
4)
5)
Parameter
(mg/kg)
Cone.
Limit
(mg/kg)'
Sample or Composite Date
01/02/19
Percent Solids (%)
NA
1.10
Arsenic
75
47.30
Cadmium
85
47.30
Chromium
NA
47.30
Copper
4,300
249.00
Lead
840
1 47.30
Mercury
57
1.82
Molybdenum
75
47.30
Nickel
420
47.30
Selenium
100
47.30
Zinc
7,500
648
Total Phosphorus
NA
30,700
TKN
NA
77,200
Ammonia -Nitrogen
NA
2,530
Nitrate and Nitrite
NA
821
Yor surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for submittin information, me] ding the possibility of fines and imprisonment for knowing violations."
�� A��-ao
'Signature of PrepafFr * Date
•Preparer is defined in 40 CFR Pan 503.9(r) and 15A NCAC 2T .I 102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: W00034513
Facility Name: Brunswick County
Residual Source
NPDES # or WQ#:
W WTP Name:
Residual Analvsis Data
W00012748
Sea Trail WWTF
Laboratory: 1) Environmental Chemists, Inc.
2)
3)
4)
5)
'------
Parameter
r •
MMME
-------------
-------------
-------------
-------------
-------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of pre - Date Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - 8 (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF- B
WQ Permit Number: W00034513 Laboratory:
Facility Name: Brunswick County
Residual Source WQ # or
NPDES #:
W WTP Name:
Residual Analvsis Data
W00000798
Shallotte WWTP
I) WaypointAnalytical
2)
3)
4)
5)
Parameter
(mg/kg)
Cone.
Limit
(m )a
Sample or Com osite Date
09/19/19
Percent Solids (%)
NA
4.88
Arsenic
75
8.55
Cadmium
85
318
Chromium
NA
37.30
Copper
4,300
1
180
Lead
840
47.30
Mercury
57
0.204
Molybdenum
75
12.80
Nickel
420
15.60
Selenium
too
10.00
Zinc
7,500
588
Total Phosphorus
NA
7,470
TKN
NA
39,800
Ammonia -Nitrogen
NA
5,100
Nitrate and Nitrite
NA
100.00
For surface disposal facilities the cerhn8 concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for subm'' 'a information ingluding the possibility of fines and imprisonment for knowing violations."
//ems(/
Signature of PyD er * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORNI RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: W00034513
Facility Name: Brunswick County
Residual Source
NPDES # or W Q#:
WWTP Name:
Residual Analvsis Data
W00000798
Shallotte WWTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
,--®---
�
------
-------------
-------------
-------------
-------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Pr er* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF- B (12/2006)

SECTION III
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS
(503 RULES)
(Form PVRF 503)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Brunswick County WQ Permit Number: W00034513
WWTP Name: Carolina Shores WWTP NPDES Number: NCO044873
Monitoring Period: From 1/l/2019 To 12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative Derformed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Altemative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 El
Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"
Lime Stabilization (]
Air Drying❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
...........
If applicable to alternative performed (Class A or Class B) complete the following monitoring
data:
Parameter
Allowable Level in
Sludge
g
Pathogen Density
Number o
Excee-
deuces
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech-ni que
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliforr
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
AIt. 1 (VS reduction)
❑
jAlt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O, uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
jAlt. 6 (Alk. Stabilization
0
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
jAlt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Ray Gambill - President (BioGreen)
Preparer Name and Title (type or print)
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Brunswick County WQ Permit Number: _
WWTP Name: Northeast Brunswick Regional WWTP NPDES Number: _
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
W00034468
NCO086819
Class A:
Alternative 1 ❑
Alternative 2 ❑
1 Alternative 3 ❑
Alternative 4 ❑
1 Alternative 5 ❑
I Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
I Heat Drying ❑
Heat Treatment ❑
Thermophilic El
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 El
Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization p
Air Drying❑
Composting ❑
lAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFK 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
JAIL 3 (30-day bench) ❑
JAIt. 4 (Spec. O, uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
jAlt. 6 (Alk. Stabilization❑
jAlt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
JAIL 10 (Incorporation)
❑
INo vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
Cl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Tim Webb - Wastewater Superintendent
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature o reparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DFNR PnRM PVRF i;m YI7/7nnri

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Brunswick County
W WTP Name: Ocean Isle W WTP
Monitoring Period: From I/l/2019
_ WQ Permit Number: W00034513
_ NPDES Number: W00006085
To 12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 977
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thennopl>ilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative I El
Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"
Lime Stabilization 0
Air Drying❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in
Sludge
PathogenDensity
y
um er o
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6[h power
per gram of
total solids
MPN
CFu
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
jAlt. 3 (30-day bench) ❑
JAIL 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
jAlt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
JAIt. 10 (Incorporation)
❑
INo vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
C] "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Gambill - President (BioGreen)
PrepQparer Name and
Title (type or print)
-.iCl nn.,,� 0 ,
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
2-
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
FacilityName: Brunswick County
WWTPName: Sea Trail WWTF
Monitoring Period: From 1/1/2019 To
WQ Permit Number: W00034513
NPDES Number: W00012748
12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative I ❑
Alternative 2 ❑
Alternative 3 ❑
Altemative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thennopl- lic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative I El
Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring
data:
Parameter
Allowable Level in
Sludge
g
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech-ni que
Minimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MI,N
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
JAIL 3 (30-day bench) ❑
jAlt. 4 (Spec. O, uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
jAlt. 6 (Alk. Stabilization
0
jAlt 7 (Drying - Stable) ❑
I Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
JAIL 10 (Incorporation)
❑
INo vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Ray Gambill - President (BioGreen)
Preparer Name and Title (type or print)
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
L�11 2c)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name:
WWTP Name:
Brunswick County
Shallotte WWTP
Monitoring Period:
From 1/1/2019
WQ Permit Number: W00034513
NPDES Number: W00000798
To 12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed -
Class A:
Alternative 1 ❑
Alternative 2 ElAlternative
3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
1 Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
I Pasteurization ❑
Class B:
Alternative 1 El
I Alternative 2 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying[]
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in
Sludge
Pathogen Density
Number of
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximuml
Units
Fecal Coliform
2 x ] 0 to the
6th power
per gram of
total solids
MPN
CFU
15,464
19 437
28,696
Colonies/
Gram
0
Annual
Grab
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.] (VS reduction)
El
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
JAlt. 4 (Spec. OZ uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
JAIt. 6 (Alk. Stabilization
❑
jAlt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
JAIL 10 (Incorporation)
❑
INo vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Tim Webb - Wastewater Superintendent
Preparer Name and Title (type or print)
Signature o rf� eparer*
Land Applier Name and Title (if applicable)(type or print)
1; Za2b
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
r)FNR rnRM D%/RF Sm W)Mrinal

SECTION IV
ANNUAL LAND APPLICATON FIELD SUMMARY FORMS
ANNUAL METALS LOADING SUMMARY FORMS
(Form FSF and MFLSF)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit #: W00034513 Annual Dry Tons Applied: 34.49
Owner: Clyde Galloway Operator:
Site #: NC-BR-CG Field #: 6
Clyde Galloway
Acres Utilized: 11.5
Predominant Soil Series: Goldsboro-GoA
Acres Permitted: 11.5
o r�
o ❑
Qo
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons
Per Acre
Residual Sources
(Summarize)
)
ite
Cond.
Dry'
Wet,
Moist
Inches
Precip.
past 24
Iir.s.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo-
nia-
Ni-
tro en
B
Ni-trate
and
Nitrite
PAN I
PAN 2
Must Select
Crop 1 Crop
P or p
2
Gal.
CuNd.
:
Report
Totals
in Gal.
Crop 1
Crop 2
Jan-19
36,000
3,130
0.28
0.0366
Carolina Shores WWTP
G/D
<0.5"
S
0.5
0.3
298
13
1
#######
0.00681
Ryegrass
1
Feb-19
79,500
6,913
0.28
0.0807
Carolina ShoresWWTP
G/D
<0.5"
S
0.5
1 0.3
298
1 13
1
#######
0.01503
Ryegrass
2
Mar-19
84,500
7,348
5.38
1.6485
qE Brunswick Regional WWTG/D
<0.5"
S
0.5
0.3
94,600
43,100
369
123.202
#######
Bermuda
3
Feb-19
221,000
19,217
1.28
1.0257
Ocean Isle Beach WWTP
G/D
<0.5"
S
0.5
0.3
61,800
5,030
733
#######
41.6023
Ryegrass
4
Mar-19
52,000
4,522
1.10
0.2074
Sea Trail WWTF
G/D
<0.5"
S
0.5
0.3
77,200
2,530
821
10.1578
#######
Bermuda
5
0
0.0000
0
0
6
0
0.0000
0
0
1
7
0
0.0000
0
0
8
0
1 0.0000
0
0
9
0
0.0000
0
0
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
41,130
:'i::::i:::::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.1466
0.1559
0.2000
0.7105
0.1373
0.0056
0.1456
0.1663
0.1456
3.4920
169.717
133.360 141.6241
Date
lbs/ac
Current Cumulative lbs/ac
0.3425 0.3601 7.4562 1.1607 0.5325 0.0250 0.432 0.6285 0.4598 26.1293
0.1959 0.2042 7.2562 0.4502 0.3952 0.0194 0.2860 0.4622 0.3142 22,6373
36 34 1338 267 15 374 89 2498
224 50
Prior Years Cumulative lbs/ac
Permitted C.P. L. R.***
Permit PAN Limit lst/2n d Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
-%:� A. Z- / / - ZC *Application Method: S - Surface, IN - Injection, INC - Incorporation
SigndtTre of Eand Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Brunswick County
Permit #:
WQ0034513
Operator:
Clyde Galloway Owner:
Acres Used:
11.5 Acres Permitted: 11.5
Total Dry Tons Applied (Annual):
Predominant Soil Series:
34.49
Goldsboro-GOA
Clyde Galloway
Site #: NC-BR-CG Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kz, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
1
1/2/19r1/2/19
a
I12119
q
1/2/19
s
I/2/19
6
e
9
0
11
1z
%Solids
0.28
0.28
5.38
1.28
1.1
Arsenic
40
40
10.9
39.8
47.3
Cadmiuml
79.6
79.6
10.9
1 39.8
47.3
Cliromiuml
0.558
0.558
29.9
39.8
47.3
Copper
0.635
0.635
140
70.9
249
Lead
0.558
0.558
10.9
39.8
47.3
Mercury
0.019
0.019
0.558
1.48
1.82
Molyb-
denum
denum
35.7
35.7
10.9
39.8
47.3
Nickel
0.558
0.558
19.7
39.8
47.3
Selenium
35.7
35.7
10.9
39.8
47.3
Zinc
2
2
807
274
648
Total
Phos-
phorus
105
105
35,100
20,100
30,700
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
11
2
3
q
5
6
7
6
9
10
11
12
O
� w
a O
y
o
0.0366
0.0807
1.6485
1.0257
0.2074
Arsenic
0.0029
0.0065
0.0359
0.0816
0.0196
0
0
0
0
0
0
0
0.1466
Cadmium
0.0058
0.0128
0.0359
0.0816
0.0196
0
0
0
0
0
0
0
0.1559
Chromiud
0.00004
0.00009
0.0986
0.0816
0.0196
0
0
0
0
0
0
0
0.2
Copper
0.00005
0.0001
0.4616
0.1454
0.1033
0
0
0
0
0
0
0
0.7105
Lead
0.00004
0.00009
0.0359
0.0816
0.0196
0
0
0
0
0
0
0
0.1373
Mercury
0,00000
0.00000
0.0018
0.003
0.0008
0
0
0
0
0
0
0
0.0056
Molyb-
0.0026
0.0058
0.0359
0.0816
0.0196
0
0
0
0
0
0
0
0.1456
denum
enum
Nickel
0.00004
0.00009
0.065
0.0816
0.0196
0
0
0
0
0
0
0
0.1663
Selenium
0.0026
0.0058
0.0359
0.0816
0.0196
0
0
0
0
0
0
0
0.1456
Zinc
0.0001
0.0003
2.6607
0.5621
0.2688
0
0
0
0
0
0
0
3.492
Total
Phos-
0.0077
0.0169
115.72
41.233
12.734
0
0
0
0
0
0
0
169.72
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applies' Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
Owner:
Clyde Galloway
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Brunswick County Permit #: WO0034513 Annual Dry Tons Applied: 15.37
Site #: NC-BR-CG Field #:
Operator: Clyde Galloway
8 Acres Utilized:
Predominant Soil Series: Goldsboro-GoA
11.5 Acres Permitted: 11.5
0
o s
„ co
o
Specify
Totals
Per
Acre
o
/o
Solid
s
Dry Tons
Per Acre
Residual Sources
(Summarize)
itC
Cond.
Dry,
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo-
nia-
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 C
P orro P
2
*
Gal.
Cu.Yd.
Report
Totals
n Gal.
Crop 1
Crop 2
0
0.0000
0
0
1
0
0.0000
1
0
0
2
Mar-19
68500
5,957
5.38
1.3363
EBmnswickRegional WWII
G/D
<0.51'
S
0.5
0.3
94,600
43,100
369
99.874
#######
Bermuda
3
0
0.0000
0
0
4
0
0.0000
0
0
5
0
0.0000
0
0
6
0
0.0000
0
0
1
7
0
0.0000
0
0
8
0
1 0.0000
0
1 0
1 9
0
0.0000
1
0
0
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
5,957
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0291
0,0291
0.0799
0.3742
0.0291
0. 0015
0.0291
0.0527
0.0291
2.1568
93.8083
99.874
0
Date
lbs/ac
:::
Current Cumulative Ibs/ac
0.1905 0.1997 1.3306 0.9319 0.2212 0.0053 0.189 0.2537 0.2844 7.5559::
0.1613 0.1706 1.2507 0.5577 0.1921 0. 1038 0.160 1 0.2011 0.2553 5.3991
36 34 1 1338 267 15 374 89 2498
224
Prior Years Cumulative Ibs/ac
Permitted C. P. L. R.***
Permit PAN Limit l st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
� Z-// - ZQ *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signatur f Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
* *** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied (Annual): 15.37
Permit #: WQ0034513 Predominant Soil Series: Goldsboro-GoA
Operator: Clyde Galloway Owner: Clyde Galloway
Acres Used: 11.5 Acres Permitted: 11.5 Site #: NC-BR-CG Field #: 8
Residual Analysis Data (Heavy Metals and Total Phosphorus use m¢/ke. % Solids use Raw Percent #l:
� t
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
J
9
5
6
]
8
9
W-1
11i
12
� O
o
1.3363
Arsenic
0
1 0
0.0291
0
0
0
0
0
0
0
0
0
0.0291
Cadmium
0
0
0.0291
0
0
0
0
0
0
0
0
0
0.0291
Chromiurr
0
0
0.0799
0
0
0
0
0
0
0
0
0
0.0799
Copper
0
0
0.3742
0
0
0
0
0
0
0
0
0
0.3742
Lead
0
0
0.0291
0
0
0
0
0
0
0
0
0
0.0291
Mercury
0
0
0.0015
0
0
0
0
0
0
0
0
0
0.0015
Molyb-
denum
denurn
0
0
0.0291
0
0
0
0
0
0
0
0
0
0.0291
Nickel
1 0
0
0.0527
0
0
0
0
0
0
0
0
0
0.0527
Selenium
0
0
0.0291
0
0
0
0
0
0
0
0
1 0 1
0.0291
Zinc
0
0
2.1568
0
0
0
0
0
0
1 0
0
0
2.1568
Total
Phos-
0
0
93.808
0
0
0
0
0
0
0
0On
93.808
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
gnatu�d ter Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit #: W00034513
Owner: Pearly Vereen Operator: Pearly Vereen
Site #: NC-BR-PV
Field #:
Acres Utilized: 12.0
Annual Dry Tons Applied: 9.02
Predominant Soil Series: Lynchburg-Ly
Acres Permitted: 12
o
„ ❑
o
S eci
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual Sources
(Summarize)
lte
Cond.
Dry,
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
till-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo-
nia-
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must
Must Select
I or Crop
P P
2
*
Gal.
Cu.Yd.
s
Report
Totals
in Gal.
Crop 1
Crop 2
0
0.0000
0
0
I
0
0.0000
0
0
2
0
1 0.0000
0
0
3
0
0.0000
0
0
4
0
0.0000
0
0
5
0
0.0000
0
0
6
0
0.0000
0
0
7
0
0.0000
0
0
8
0
0.0000
1
0
0
9
0
0.0000
0
0
N
Nov-19
169,000
14,083
1.28
0.7517
can Isle Beach W W"
G/D
<0.5"
S
0.5
0.3
61,800
5,030
3
00.4879
#######
Ryegrass
I1
0
0.0000
11
j30.2183
0
0
12
TOTALS:
14,083
:::::::::::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
PAN I
PAN 2
Lime A
lied
Annuallbs/acre
0.0598
0.0598
0.0598
0.1066
0.0598
0.0022
0.0598
0.0598
0.0598
0.4119
30,4879
0
Date
lbs/ac
urrent Cumulative Ibs/ac
0.0778 1 0.0861 0.1641 0.2158 0.1641 0.0050 0.080 0.1311 0.1311 0.8105
OOI80 0.0263 0.10.1043 0.0200.0713 0.0713 0.3986
36 34 267 374 89
2498?ermitted
:;.. ,: ..._ .. ::::" ]06 50
'rior Years Cumulative Ibs/
C. P. L. R.
'ermitPAN Limit Ist/2ndCrop
i certify, under penalty of taw, that this document was prepared under my direction or supervision in accordance with a system
lesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Lati Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorvoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loadin¢ Rate
** * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1.
DENR FORM FSF(5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied (Annual): 9.02
Permit #: W00034513 Predominant Soil Series: Lynchburg-Ly
Operator: Pearly Vereen Owner; Pearly Vereen
Acres Used: 12 Acres Permitted: 12 Site #: NC-BR-PV Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
. •:o
©
©
o
o
to
o
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
o
©
o
0
0
1
�0000000000
t l •:
O
I t •;
�0000000000
t t • :Ott
• ;
�ii u0000000000
t t•:
0
t 1•
••
0000000000
t l ..
0
t t.•
�0000000000
t t•:
0
t 1•
�0000000000
I t t
Ott
t
•
000000000'
0
1 t•:
0
t 1•
�0000000000
t t •:
O
t l •;
�0000000000
t t•.
0
I t•;
®0000000000
t , .
0
t ,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit #: WQ0034513
Owner: Joyce Brown Operator: Harvey Bell
Site #: NC-BR-HB Field #:
Acres Utilized: 10.2
Annual Dry Tons Applied: 4.58
Predominant Soil Series: Goldsboro-GoA
Acres Permitted: 10.2
$ y
„ ❑
Specify
T
Totals
Per
Acre
°fo
Solid
s
Dry Tons
per Acre
Residual Sources
(Summarize)
ite Cond.
Dry'
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TIN
Ammo-
nia-
Ni-
trogen
Ni-trate
and
Nitrite
PAN I
PAN 2
Must Select
Crop 1 Crop
P or p
2
Gal
Cu.Yd.
Report
Totals
in Gal.
Cro 1
P
Cro 2
P
0
0.0000
0
0
1
0
0.0000
0
1 0
2
0
0.0000
0
0
3
0
0.0000
0
0
4
May-19
66,000
6,471
0.28
0.0756
Carolina Shores WWTF
G/D
<0.5"
S
0.5
0.3
298
13
1
0.0141
#######
Bermuda
5
May-19
50,500
4,951
1.10
0.2271
Sea Trail WWTF
G/D
<0.5"
S
0.5
0.3
77,200
2,530
821
11.1221
#######
Bermuda
6
Jul-19
32,500
3,186
1.1
0.1462
Sea Trail WWTF
GID
<0.5"
S
0.5
0.3
77,200
2,530
821
7.15777
#######
Bermuda
7
0
0.0000
0
0
8
0
1 0.0000
1
0
0
9
0
0.0000
0
0
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS: 1
14,608
=aij?I.:..
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0414
0.0473
0.0354
0.1860
0.0354
0.0014
0.0407
0.0354
0.0407
0.4841
22.9365
18.2939
0
Date
Ibs/ac
Current Cumulative Ibs/ac
0.4932 0.3773 12.2944 1.0195 0.6444 0.0367 0.523 0.5884 0.5207 26.7756:::::::::::::::::::::::::::::::::::
0.4518 0.3300 12.2590 0.8335 0.6090 0.0353 0.4820 0.5530 0.4800 26.2915...::�:;
36 34 1338 267 15 1 1 374 1 89 1 2498
.:.:..............:..:..:.....:..:..:..:......:..:..:.....:..:.....:.....:......:..:..:..:........:..:.....`:::i::i:::....................
299 50
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
✓� - g,,., %S-� 2. // -^ Za *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature o Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Brunswick County Total Dry Tons Applied (Annual): 4.58
W00034513 Predominant Soil Series: Goldsboro-GoA
Harvey Bell Owner: Joyce Brown
10.2 Acres Permitted: 10.2 Site #: NC-BR-HB Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use ma/ke. % Solids use Raw Percent #):
Sample
or Com-
posite
Date
-L
2J
211
4
10, /02/19
s
01/02/19
]
01/02/19
a V y
s
o
z
% Solids
0.28
1.1
1.1
Arsenic
40
47.3
47.3
Cadmiuml
1
79.6
47.3
47.3
Chromium
0.558
47.3
47.3
Copper
0.635
249
249
Lead
0.558
47.3
47.3
Mercury
0.019
1.82
1.82
Molyb-
enum
denumd
35.7
47.3
47.3
Nickel
0.558
47.3
47.3
Selenium
35.7
47.3
47.3
Zinc
2
648
648
Total
Phos-
phorus
105
30,700
30,700
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
-31
41]
-51
6
]
8
9
10
11
12
0
O
C a C7
y
m
o'
0.0756
0.2271
0.1462
Arsenic
0
0
0
0
0.0060
0.0215
0.0138
0
0
0
0
0
0.0414
Cadmium
0
0
0
0
0.0120
0.0215
0.0138
0
0
0
0
0
0.6473
hromiu
0
0
0
0
0.0001
0.0215
0.0138
0
0
0
0
0
0.0354
Copper
0
0
0
0
0.0001
0.1131
0.0728
0
0
0
0
0
0.1860
Lead
0
0
0
0
0.0001
0.0215
0.0138
0
0
0
0
0
0.0354
Mercury
0
0
0
0
0.0000
0.0008
0.0005
0
0
0
0
0
0.0014
Molyb-
denum
0
0
0
0
0.0054
0.0215
0.0138
0
0
0
0
0
0.0407
Nickel
0
0
0
0
0.0001
0.0215
0.0138
0
0
0
0
0
0.0354
Selenium
0
0
0
0
0.0054
0.0215
0.0138
0
0_1
0
0
0
0.0407
Zinc
0
0
0
1 0
0.0003
0.2943
0.1895
0
0
0
0
0
Total
Phos-
0
0
0
0
0.0159
13.944
8.9767
0
0
0
0
D
A2236
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Brunswick County
Owner: Harry Hart
Site #: NC-CO-HH Field #:
Operator:
Permit#: WQ00345I3
Harry Hart
Acres Utilized: 12.3
Annual Dry Tons Applied: 1.64
Predominant Soil Series: Rains-Ra
Acres Permitted: 12.3
$ Yc
„ ❑
Specify
Totals
Per
Acre
%
Solid
s
Acre
Sources
(Summarize)
Site
Cond .
Dry,
Wet,
Moist
Inches
.
past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo-
ma_
Ni
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 Crop
P or p
2
Gal -Residual
Report
Totals
in Gal.
Crop 1
Crop 2
0
0.0000
0
0
1
0
0.0000
0
0
2
0
0.0000
0
0
3
0
0,0000
0
0
4
0
0.0000
0
0
5
0
0.0000
0
0
6
0
0.0000
0
0
1
7
0
0.0000
0
0
8
0
0.0000
0
0
9
Oct-19
40 1
3.252
4.88
0.1337
Shallotte WWTP
G/D
<0.5"PH
0.5
0.2
39,800
5,100
100
2.56444
#######
Pines
to
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
3.252
::::::::::::::i
As
Cd
Cr
Cu
PbMo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
plied
Annuallbs/acre
0.0023
0.0009
0.0100
0.0481
0.0126
0.0034
0.0042
0.0027
0.1572
1.99748
2.56444
0
Date
Ibs/acCurrent
Cumulative lbs/ac
0.0023 0.0009 0.0100 0.0481 0.0I26 0.003 0.0042 0.0027 0.1572
0.0000 0.0000 0.0000 1 0,0000 0.0000 0.0000 0.000 1 0.0000 1 0.0000 0.0000
36 34 1338 267 IS 374 89 2498
70
Prior Years Cumulative Ibs/ac 1
Permitted C.P. L. R.
Permit PAN Limit Ist/2nd Crop
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
yy 2 // *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signatur of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column an the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County
Permit#: WQ0034513
Operator: Harry Hart Owner:
Acres Used: 12.3 Acres Permitted: 12.3
Total Dry Tons Applied (Annual): 1.64
Predominant Soil Series: Rains-Ra
Harry Hart
Site #: NC-CO-HH Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosnhorus use me/ktr. % Solids use Raw Percent #1:
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
1
�000000000
1 1 1
00
1 1 1
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
z--i/- 20
Signature of Land Apo ler Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit #: W00034513 Annual Dry Tons Applied: 140.21
Owner: Harry Hart Operator: Harty Hart
Site #: NC-CO-HH Field #: 7 Acres Utilized: 68.1
Predominant Soil Series: Rains-Ra
Acres Permitted: 68.1
0 IS
„ a
A
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
de
Cond.
Dry,
Wet,
Moist
Inches
Precip.
past 24
Hrs.
A li
PP
cation
Meth-
oil*** *
Vola-
tili-
zation
Rate
Miner-
ali-
zation
Rate
TI{hl
Ammo-
nia-
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
P P
2
G�•
Cu.Yd.
'>:
Report
Totals
in Gal.
Crop 1
Crop 2
0
0.0000
0
0
I
0
1 0.0000
0
0
2
0
0.0000
0
0
3
0
0.0000
0
0
4
0
0.0000
0
0
5
0
0.0000
0
0
6
0
0.0000
1
0
0
7
0
0.0000
0
0
8
0
1 0.0000
0 1
0
9
Oct-19
689,000
10,117
4.88
2.0589
Shallone WWTP
G/D
<0.5"
S
0.5
0.2
39,800
5,100
100
39.489
#######
Rye
IO
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
10,117
:::::::::::::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0352
0.0131
0.1536
0,7412 1
0.1948
0.0008
0.0527
0.0642
0.0412
2.4213
30.76
39.489
0
Date
Ibs/ac
Current Cumulative Ibs/ac
0.0352 0.0131 0.1536 0.7412 0.1948 0.0008 0.053 0.0642 0.0412 2.4213
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.000 0.0000 1 0.0000 0.0000
36 34 1338 267 15 374 89 2498:
106
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit I st/2nd Crop
**1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Al . -=r Z--// -2Ci *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
*** * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied (Annual): 140.21
Permit #: WQ0034513 Predominant Soil Series: Rains-Ra
Operator: Harry Hart Owner: Harry Hart
Acres Used: 68.1 Acres Permitted: 68.1 Site #: NC-CO-HH Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use me/ke. % Solids use Raw Percent #):
Annual Heavy Metal FieldLoadings (Calculated in Ibs/acre):
I :
�000000000
I I
00
I t
�000000000
I I
00
I I
000000000
I .
00
t
...
000000000�00�.
�000000000
i ..:
00
t®":
�000000000
I l t l:
00
I I I l
�000000000
I l . -
00
I l .
�000000000
I I'
00
I I'
®000000000�00�
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

SECTION V
LAB SHEETS

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2019
Carolina Shores WWTP Permit No. W00034513
Mineralization Rate 0.30 0.28 % Solids
6.92 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(MWKg x 0.002)
Nitrogen (TKN)
0.030
298.000
0.596
Phosphorus
0.011
105.000
0.210
Potassium
0.023
228.000
0.456
PAN (injected)*
0.010
99.413
0.199
PAN (surface)*
0.009
93.118
0.186
Ammonia Nitrogen
0.001
12.590
0.025
Calcium
0.077
765.000
1.530
Calcium Carbonate Eq.
---
---
---
Magnesium
-
91.300
0.183
Sodium
-
413.000
0.826
Sulfur
---
---
---
Nitrate N / Nitrite N
---
1.200
0.002
Barium
---
--
--
Chloride
---
---
Iron
---
---
---
Aluminum
---
10.50
0.021
Arsenic
---
40.00
0.080
Cadmium
79.60
0.159
Chromium
0.558
0.001
Copper
---
0.635
0.001
Lead
---
0.538
0.001
Mercury
0.019
0.000
Molybdenum
---
35.70
0.071
Nickel
---
0.558
0.001
Selenium
---
35.70
0.071
Zinc
---
1.77
0.004
Envirochem: 2019-00096
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.20
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

4xyN Environmental Chemists, Inc.
6 q q k 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Date of Report:
Feb 05, 2019
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer ID:
08100011
Attention: Brian Blanton
Report #:
2019-00096
Project ID: Carolina Shores
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
19-00246 Site: Sludge
1/2/2019 8:48 AM Solid/Sludge
Aaron Hewett
Test Method Results Date
Chlordane (TCLP)
SW B46 Method 8081 B/3510
<0.02 mg/L
01/10/2019
Endrin(TCLP)
SW 846 Method8081B/3510
<0.0005mg/L
01110/2019
Heptachlor (TCLP)
SW 846 Method 0081 B1351 0
<0.0005mg/L
01/10/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081813510
<0.0005 mg/L
01/10/2019
Lindane (TCLP)
SW 846 Method 8081B1a510
<0.0005 mg/L
01/10/2019
Methoxychlor(TCLP)
SW 846 Method 8081 B13510
<0.0005mg/L
01/10/2019
Toxaphene (TCLP)
SW 846 Method 8081B13610
<0.05 mg/L
01110/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method B27013510
<0.050 mg/L
01/1212019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270MIO
<0.050 mg/L
01/12/2019
2,4,6-Trichlorophenol(TCLP)
SW846method 8270/3510
<0.050mg/L
01/12/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/12/2019
Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/12/2019
Hexachloro-1,3-butadiene(TCLP)
SW 846 method 827013510
<0.050mg/L
01/12/2019
Hexachlorobenzene(TCLP)
SW 846 method 827013510
<0.050mg/L
01/12/2019
Hexachloroethane(TCLP)
SW 846 method 827013510
<0.050mg/L
01/12/2019
m + p-Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/12/2019
Nitrobenzene (TCLP)
SW 846 method 6270/3610
<0,050 mg/L
01/12/2019
o-Cresol (TCLP)
SW 846 method 827=510
<0.050 mg/L
01112/2019
Pentachlorophenol(TCLP)
SW 845 method 8270/3510
<0.250mg/L
01/12/2019
Pyridine (TCLP)
SW 846 method 827013510
<0.050 mg/L
01112/2019
2,4,5-TP
SW846 Method 81 51A
<0.003mg/L
01/10/2019
2,4-D
SW846 Method 8151A
<0.003mg/L
01/1012019
1,1-Dichloroethylene (TCLP)
SW046 Method 826015030
<0.01 mg/L
01/11/2019
1,2-Dichloroethane(TCLP)
SW846 Method 82601503D
<0.01mg/L
01/11/2019
Benzene (TCLP)
SW846 Method 8260/5030
<0.01 rng/L
01/11/2019
Carbon Tetrachloride (TCLP)
SW846 Method 626015030
<0.01 mg/L
01/11/2019
RePon #Y.: 2019-00090
Page i of 4

Environmental Chemists, Inc.
8 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, M nnteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL $ CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Date of Report: Feb 05, 2019
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer ID: 08100011
Attention: Brian Blanton
Report #: 2019-00096
Project ID: Carolina Shores
Chlorobenzene(TCLP) SW846 Method826015030
<0.01mg/L
01/11/2019
Chloroform (TCLP) SW846 Method826015030
<0.01 mg/L
01/11/2019
Methyl ethyl ketone (TCLP) SW846 Method 8260/5030
<0.05 mg/L
01/11/2019
Tetrachloroethylene (TCLP) SW846 Method 82601503D
<0.01 mg/L
01/11/2019
Trichloroethylene (TCLP) SW846 Method B26015030
<0.01 mg/L
01/11/2019
Vinyl Chloride (TCLP) SW846 Method8260/5030
<0.01 mg/L
01/11/2019
RCI
Cyanide
EPA335.4
<0.05mg/kg
01/17/2019
Sulfide
SM 4500 S o
0.23 mg/kg
01/16/2019
Ignitability
SW 846 method 1010
>210 OF
01/14/2019
Sludge Residuals
Aluminum
EPA200.7
10.5mg/kg
01/06/2019
Calcium
EPA200.7
765mg/kg
01/16/2019
Chromium
EPA200.7
<0.558mg/kg
01106/2019
Copper
EPA200.7
0.635mg/kg
01/06/2019
Lead
EPA200.7
<0.558mg/kg
01/06/2019
Magnesium
EPA200.7
91.3mg/kg
01/16/2019
Nickel
EPA200.7
<0.558mg/kg
01/06/2019
Potassium
EPA200.7
228mg/kg
01/16/2019
Sodium
EPA200.7
413mg/kg
01/16/2019
Zinc
EPA200.7
1.77mg/kg
01/06/2019
Total Kjeldahl Nitrogen (TKN)
EPA351.2
298 mg/kg
01112/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
1.20 mg/kg
01/24/2019
Total Solids (%)
SM 2540 B
0.28 %
01/0312019
pH
SM4500HB
6.92units
01/17/2019
Ammonia Nitrogen
SM4500NH3 C
12.59mg/kg
01/2112019
Total Phosphorus
SM 4500 P F
105 mg/kg
01/10/2019
Mercury
SW8467471B
<0.019mg/kg
01/09/2019
TCLP Metals
Arsenic
EPA200.7
<1.0mg/L
01/1712019
Report #.: 2019-00096
Page 2 of 4

Environmental Chemists, Inc.
4
® g 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
-"� 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Date of Report: Feb 05, 2019
Post Office Box 249
Customer PO #:
Bolivia
NC 28422
Customer ID: 08100011
Attention:
Brian Blanton
Report M 2019-00096
Project ID: Carolina Shores
Barium
EPA200.7
<1.0mg/L
01/17/2019
Cadmium
EPA200.7
<1.0mg/L
01/17/2019
Chromium
EPA200.7
<1.0mg/L
01/17/2019
Lead
EPA200.7
<1.0mg/L
01/17/2019
Selenium
EPA200.7
<1.0mg/L
01/17/2019
Silver
EPA200.7
<1.0mg/L
01/17/2019
Mercury
EPA245.1
<0.0002mg/L
01/19/2019
Lab ID
Sample ID:
Collect DatelTime Matrix Sampled by
19-00246A
Site: Sludge
1/2/2019 8:48 AM Solid/Sludge Aaron Hewett
Test
Method
Results Date Analyzed
Arsenic
EPA200.7
<40.Omg/kg
01/28/2019
Cadmium
EPA200.7
<79.6mg/kg
01/2812019
Molybdenum
EPA200.7
<35.7mg/kg
02/03/2019
Selenium
EPA2007
<35.7mg/kg
01/3012019
Lab ID
Sample ID:
Collect Date/Time Matrix Sampled by
19-00247
Site: Effluent
112/2019 9:29 AM Water Aaron Hewett
Test
Method
Results Date Analyzed
LLMercury
EPA1631e
1.49ng/L
01/11/2019
Lab ID
Sample ID:
Collect Date/Time Matrix Sampled by
19-00248
Site: Field Blank
1/2/2019 9:29 AM Water Aaron Hewett
Test
Method
Results Date
Analvzed
LL Mercury EPA 1631E <0.500 ng/L 01/11/2019
Report #:: 2019-00096 Page 3 of 4

Environmental Chemists, Inc.
4
M(3.
6602 Windmill Way, Wilmington, NC 28405 > 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Date of Report: Feb 05, 2019
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer ID: 08100011
Attention: Brian Blanton
Report#: 2019-00096
Project ID: Carolina Shores
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-00249 Site: Effluent
1/2/2019 8:40 AM Water Aaron Hewett
Test Method
Results Date Analyzed
Nitrite Nitrogen EPA 353s
0.03 mg/L
01/03/2019
Total Phosphorus SM4500PF
1.74mg/L
01/10/2019
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA351.2
0.8 mg/L
01/12/2019
Nitrate+Nitrite-Nitrogen EPA353.2
8.59mg/L
01/16/2019
Total Nitrogen Total Nitrogen
9.4mg1L
01/25/2019
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
,f
Reviewed by: s' Xx.L\a R' I `L�t
Q
CLm
teport #:2019-00096 Page 4 of 4

Mercury (CVAFS)
Client: Environmental Chemist, Inc. Laboratory ID: UA07016-027
Description: 19-00247 Matrix: Aqueous
Dale Sampled:0110212019 0929
Dale Received:0110712019
crap we¢ooa Analytical method Dilution Analysis Date Analyst Prep Date Batch
1 1531E 1 01111/20191751 TJW 01/10/2019 1236 94490
CAS Analytical
Parameter Number Method Result O LOO Units Run
Mercury(CVAFS) 7439-97.6 1631E 1,49 0.500 nglL 1
Lw umn in vuarnamon a= Delecled in the method blank E= Duantitatlon of compound exceeded die calibration range
ND = Not defected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4M
H= Out of holding time W= Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (8e3) 791-9700 Fax [phone] w ahealylab.com
Page 31 of 47

Mercury (CVAFS)
Client: Environmental Chemist, Inc. Laboratory ID: UA07016-028
Description: 19.00248 Matrix: Aqueous
Date Sampled:0110212019 0929
Dale Received: 01/07/2019
Kun Prep metnoa Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 01/11120191757 TJW 01110120191236 94490
CAS Analytical
Parameter Number Method Result 0 LOO Units Run
Mercury(CVAFS) 7439-97-6 1631E NO 0.500 nglL 1
L00 = Limit of Oui n nation 8 = Decocted in the method Wank E = Ouantitatlon of compound exceeded the calibration range
NO = Not detected at or above Ne L00 N = Raixw ry Ia out of cdieda P = The RPD between two GC columns exceeds 40%
H = Out al holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] svww shealylab.com
Page 32 of 47

Sample Collection and Chain of Custody
Sample Type: I = Ialluent. K = Eft en w =WellNU =n!M n>r
p Collection a o
Sample Identification r 8 `_ o
DATE TIlHE TEMP
I,
C,Audl;.,� Strews 1 d4 I 1 1 -
Wilmington, NC 28405
Phone: [phone]
Fax (910) 392,4424
PRESERVATION
44 C� O ANALYSIS REQUESTED
p rLc I
^r:�uc.'111�� 11��JJ`�•'IA�"�GI
��,2-Ir�
I
I��h��Y�
I
I
I
li �iilv{�..,Tic..
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e�y,
G
G
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I
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I
I
I
I
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a--; o�
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ipi
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NOTICE — DECHLORINATION : Samples for Ammonia, TKN, Cyanide, Phenol, and Bacteria must be dechlorinated
(0.2ppmor less in the Feld at the time of collection. See reverse side for instructions.
Transfer Relinquished By: Date/Time Received By: Date/Time
trs�`
Temperature When Received:? Accepted: ejec .ed: Resample Reque t d:
Delivered By: G b {mac Received By. " � Date: r - 2 Time:
Comments: ____ _-

fin; ve" S COP
Wts r pa
Brunswick Count
Lime Stabilization Ph Test Results
Hauler:1310-GREED Services, Inc,
Sludge Source: C tArdyl; N"VItP
Permnit & o Q Li T B 7 3 Approximate Gallons: --� 2. S & a)
Initial Ph Test
Date-31-2.01,& Time. O 9 LIn Operator
o _
Ph Temp 19 e S
Temaperature Corrected Ph
2 Hour Ph Test
Date 1- i 1 Time _ � � �'l2 Operator_ i� '}� e <-V W -
a,
Ph Temp
Temperature Corrected Ph .1--1 -7
gg 24 Hour Ph 'hest
Date Time ®�1 �� Operator
Play CQ Temp
Temperature Corrected'Ph

��`�u�►1s coP�
D ODD
h 7 0
esT (
L - p
1-4 . L-1

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( -V :::- -\ S -F 0
Tl--,e I Q-3b
H

Brunswick County
Lime Stabilization Ph Test Results
Hauler: BIO-GREEN Services, Inc.
Sludge Source: C IR t) L l ,J cu 5 b t!) 1hD1 q WWTP
Permit #: N C OO ►-{ 4 A 7 3 Approximate Gallons: 3 Soe�
Initial Ph Test
Date S -;, Time IJQ L-10 Operator V VAjjje4.
Ph (1, . S' 11
Temperature Corrected Ph
o,
Temp Lq
1 I S `)
2 Hour Ph Test
Date O Iq Time l t-{ n Operator_
U.�
Ph 7, , t ( Temp
Temperature Corrected Ph 1 '�, , 9
24 Dour Ph Test
Date 5-3-'1-0l' Time Q !� C) Operator_ ►�
Ph 11,0-3 Temp '4�-(� �]
temperature Corrected Ph Z, . 0 'Z

�� ve4'v5 co PLI
Brunswick County
Lime Stabilization Ph Test Results
Hauler: BIO-GREEN Services, Inc.
Sludge Source: C yA vL o L „i r f7 ►n-L WWTP
Permit #: f1 G Qn H H � 7 7-� Approximate Gallons: 16 Doa
Initial Ph 'Pest
.Date S -), '�,C� i 9 Time, O C1 `3 D Operator P o
Ph I-), , S 9 Temp__ O
Tff mperature Corrected Ph 1 I , S G
2 Dour Ph Test
.Date Time 1130 Operator e�
Ph -7 Temp y 2,
Temperature Corrected Ph I `)-. , SS
24 Hour Ph Test
Hate 9 -a,0 9 Time Q a Operator iq LjtLv4-
Ph �,. 1 Temp ')\3 �1
temperature Corrected Ph

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2019
NE Brunswick Regional WWTP Permit No. WQ0034468
Mineralization Rate 0.30 5.38 % Solids
8.45 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
9.460
94,600.000
189.200
Phosphorus
3.510
35,100.000
70.200
Potassium
0.989
9,890.000
19.780
PAN (injected)*
5.892
58,919.000
117.838
PAN (surface)*
3.737
37,369.000
74.738
Ammonia Nitrogen
4.310
43,100.000
86.200
Calcium
1.490
14,900.000
29.800
Calcium Carbonate Eq.
---
---
---
Magnesium
—
4,420.000
8.840
Sodium
---
1,150.000
2.300
Sulfur
---
__
Nitrate N / Nitrite N
---
369.000
0.738
Barium
Chloride
---
---
---
---
---
---
SAR
0.49
Iron
---
---
---
Ceiling Concen.
Aluminum
---
5,300.00
10.600
(Mg/Kg)
Arsenic
---
10.90
0.022
75
Cadmium
---
10.90
0.022
85
Chromium
29.90
0.060
---
Copper
---
140.00
0.280
4,300
Lead
---
10.90
0.022
840
Mercury
---
0.558
0.001
57
Molybdenum
---
10.90
0.022
75
Nickel
---
19.70
0.039
420
Selenium
---
10.90
0.022
100
Zinc
---
807.00
1.614
7,500
Envirochem: 2019-00064
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = %PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.

Environmental Chemists, Inc.
1 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab 910.3914424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
M 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities Date of Report: Jan 31, 2019
Post Office Box 249 Customer PO #•
Bolivia NC 28422 Customer ID: 08100011
Attention: Donald Dixon Report #: 2019-00064
Project ID: NEBR
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-00166 Site: Sludge 1/2/2019 12:00 PM Solid/Sludge Randy Bumgamer
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA200.7
5300mg/kg
01/05/2019
Arsenic
EPA200.7
<10.9mg/kg
01/06/2019
Cadmium
EPA200.7
<10.9mg/kg
01/06/2019
Calcium
EPA200.7
14900mg/kg
01/16/2019
Chromium
EPA200.7
29.9mg/kg
01/06/2019
Copper
EPA200.7
140mglkg
01/06/2019
Lead
EPA 200.7
<10.9 mg/kg
01/06/2019
Magnesium
EPA200.7
4420mg/kg
01/1612019
Molybdenum
EPA200.7
<10.9mg/kg
01/11/2019
Nickel
EPA200.7
19.7mg/kg
01/06/2019
Potassium
EPA200.7
9890mg/kg
01/16/2019
Selenium
EPA200.7
<10.9mg/kg
01/06/2019
Sodium
EPA200.7
1150mg/kg
01/16/2019
Zinc
EPA200.7
807mg/kg
01/05/2019
Total Kjeldahl Nitrogen (TKN)
EPA351.2
94600mg/kg
01/29/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
369mg/kg
01/18/2019
Total Solids (%)
SM 2540 B
5.38 %
01 /03/2019
pH
SM 4500 H a
8.45 units
01/17/2019
Ammonia Nitrogen
SM4500NH3 C
43100mg/kg
01/21/2019
Total Phosphorus
SM4500PF
35100mg/kg
01/10/2019
Mercury
SW04674718
0.5580mg/kg
01/12/2019
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis
Reviewed by:
Report1x: 2019-00064 Page 1 of 1

ENVIRONMENTAL CHEMISTS9 INC
Sample Collection and Chain of Custody
Sample Tvoe: I = Influent. E = Effluent. W =WeII. ST =Stream- Rn =Snil- Si.= ,Cl..duo ntho.••
6602 Windmill Way
Wilmington, NC 28405
Phone: [phone]
Fax [phone]
N... /9- acts L/
a PRESERVATION ---�
Collection
Sample Identification o pa n `_ a` a
Ep U m li L e s p ANALYSIS REQUESTED
eL s r S
Z DATE TIME TEMP U '" V
NEBR SLUDGE
ObI {B(lo
5L
C
X
%Solids, TCLP
RCI
7 t
G
NEBR SLUDGE
—
S C
C
P
X
Metals:
Ag,As,Cd,Cr,Cu,Pb,Mo,Ni
Zn,Se,H
1 -L 19
260
�j�
Q
G
NEBR SLUDGE
`
SL
C
G
X
Nutrients-NH3, Total N, P
t
l
C
P
G
C
P
G
C
P
G
C
P
G
P
G
RC
P
G
P
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
-
2.
lL�li y -i2,'y
Temperature when Received: t 7 Accepted: / eje ted:_ Resample Requested:
Delivered By: Received By: tin �� 'F S L Date:1 - l� Time: L

Environmental Chemists, Inc.
enviroche-m6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
(smi 710 Bowsertown Road, Manteo, NC 27954 • 252.473-5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Post Office Box 249
Bolivia NC 28422
Attention: Brian Blanton
Revised Report:
Sep 17, 2019
Original Report Date:
Mar 08. 2019
Report #:
2019-02687
Customer ID:
08100011
Project ID: NEBR
Lab ID
Sample ID:
Collect Date/Time Matrix
Sampled by
19-06825
Site: NEBR Sludge
2/18/2019 7:55 AM Solid/Sludge
Richard Brower
Test
Method Results
Date
Sulfide
SM 4500 S D
1.56 mg/kg
02126/2019
Chlordane (TCLP)
SW 846 Method 8081813510
<0.02 mglL
02121/2019
Endrin (TCLP)
SW 846 Method 8081813510
<0.0005 mg/L
02/2112019
Heptachlor (TCLP)
SW 846 Method 808113/3510
<0.0005 mg/L
02/21/2019
Heptachlor epoxide (TCLP)
SW 040 Method 80018/3510
<0.0005 mg/L
02121/2019
Lindane (TCLP)
SW B46 Method 8061813510
<0.0005 mg/L
02/21/2019
Methoxychlor (TCLP)
SW 846 Method 008113/3610
<0.0005 mg1L
02/21/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
02/21/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 027013510
<0.05 mg/L
02/22/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
02/22/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 827013510
<0.05 mg/L
02/22/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method8270/3510
<0.05 mg/L
02/2212019
Cresol (TCLP)
SW 846 method 8270/3510
6.91 mg/L
02/22/2019
Hexachloro-1,3-butadiene (TCLP)
SW B46 method 8270/3510
<0.05 mg/L
02/22/2019
Hexachlorobenzene (TCLP)
SW B46 method 8270/3510
<0.05 mg/L
02/22/2019
Hexachloroethane (TCLP)
SW 046 method 8270/3510
<0.05 mg/L
02/22/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
6.91 mg/L
02/22/2019
Nitrobenzene (TCLP)
SW 846 method 827013510
<0.05 mg/L
02/22/2019
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
02/22/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.25 mg/L
02/22/2019
Pyndine (TCLP)
SW 846 method 8270/3510
<0.05 mg/L
02/22/2019
2,4,5-TP(TCLP)
SW846 Method8151A
<0.0003mg/L
02/2012019
2,4-D (TCLP)
SW846 Method 8151A
<0.0003 mg/L
02/20/2019
1,1-Dichloroethviene(TCLP)
SW846 Method026015030
<0.01mg/L
02/22/2019
1,2-Dichloroethane(TCLP)
SW846 Method8260/5030
<0.01mg/L
02/22/2019
Benzene (TCLP)
SW846 Method826015030
<0.01mg/L
02/22/2019
Report #:: 2019-02687
Page 1 of 2

Environmental Chemists, Inc.
enviroe 7em 6602 Windmill Wa)q Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
m'Ml 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL R CONSULTING CHEMISTS info( environmentalchemists.com
Brunswick County Public Utilities Revised Report: Sep 17, 2019
Post Office Box 249 Original Report Date: Mar 08, 2019
Bolivia NC 28422 Report #: 2019-02687
Attention: Brian Blanton Customer ID: 08100011
Project ID: NEBR
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/22/2019
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/22/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/22/2019
Methyl ethyl ketone (TCLP)
SW846 Method 826015030
<0.05 mg/L
02/22/2019
Tetrachloroethylene (TCLP)
SW846 Method 826015030
<0.01 mg/L
02/22/2019
Trichloroethylene (TCLP)
SW848 Method 826015030
<0,01 mg/L
02/22/2019
Vinyl Chloride (TCLP)
SW848 Method 8260/5030
<0.01 mg/L
02/22/2019
TCLP - Extraction
TCLP -Extraction
RCI
Cyanide
EPA335.4
0.079mg/kg
02/25/2019
Flash Point
SW 846 method 1010
>190 °F
03/0412019
pH
SW 646 Method 9045D
8.17 units
02/20/2019
TCLP Metals
Arsenic
EPA 200.7
<1.0mg/L
02/26/2019
Barium
EPA 200.7
<1.Omg/L
02/26/2019
Cadmium
EPA 200.7
<1.0mg/L
02/26/2019
Chromium
EPA 200.7
<1.0mg/L
02126/2019
Lead
EPA 200.7
<1.0 mg/L
02126/2019
Selenium
EPA 200.7
<1.0mg/L
02/27/2019
Silver
EPA 200.7
<1.0 mg/L
02/27/2019
Mercury
EPA245.1
<0.0002mg/L
0311712019
Comment:
Reviewed by:
Report #.: 2019-02687 Page 2 of 2

O02 Windmill Way Wilmington, NC 28
FF Ct 9O-392.=3 FAX 910 3 2„4420
Analytical & Consulling Chemists NCDENR: DWO C.F.RTIFICATION It 9e NCDHHS: DLS CERTIFICATION 8 37729 Info(ipenvironmentalchemists.com
Cni I FCTlnM Arun rUAIM nc rncTnnv
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ADDRESS: (� oY c _i i5v .,i r�e ^
NAME: Nc Fj p 4y a�SJ�•,�. f�e WW
NAME: i r, r_� a 1
REPORY NO: J — 2
PO NO:
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PHONEIFAX:
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Sampled Ov:
seam a roc. _ I..e...._. e _ roe..__. .
Sample Identification
Collection
E g
A
E° u
u°
a
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u a
c
E
c
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'z
PRESERVATION
'— — —
ANALYSIS REQUESTED
Date
Time
Temp
z
3
0
0
0
0
c
J.') grl � --f ,
Lva^e
J'
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SC
C
P 1
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GC
G
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G
G
C
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C
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Relinquished By:
Dete/Time
Received By:
- Datefrimo
x.
Temperature when Received: __- Accepted: -_ __- —Rejected: Resampie Reque Led:___
Delivered By: n r_A,—_Receiv d B °-L"�c.._QR--- 1 1 I�'I Time:
Y y�----- �- --- Date:-s3U15

Brunswick County
Lime Stabilization Ply Test Results
Hauler: BI®-GREEN Services, Inc.
Sludge Source: / 10Aeac2��r . ;r k. Pc, ions � TP
Permit #:1VC 00 ,FC, q / J Approximate Gallons: _
Initial Pin Test
Date 3 - / 8-/ 9 Time Operator i c�i yowPv
Ph /2,53 Temp
Temperature Corrected Ph _ Z 2. GS ' G
2 Hour Pin Test
Date 3—/ --1 �l Time %7/3 Operator Paoicly ):?uMC?arnev
v
Ph /2,2-/ Temp /8. '(-
Temperature Corrected Ph / 2,3) oG
24 Hour Ph Test
Date 3 —I C1— l Time Operator rr olv m a rn ey
Ph / 2 , IS Temp
Temperature Corrected Ph / 2 , 3 06�

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2019
Ocean Isle Beach WWTP Permit No. W00034513
Mineralization Rate 0.30 1.28 % Solids
6.1 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
6.180
61,800.000
123.600
Phosphorus
2.010
20,100.000
40.200
Potassium
0.427
4,270.000
8.540
PAN (injected)*
2.279
22,794.000
45.588
PAN (surface)*
2.028
20,279,000
40.558
Ammonia Nitrogen
0.503
5,030.000
10.060
Calcium
0.622
6,220.000
12.440
Calcium Carbonate Eq.
--
---
---
Magnesium
---
2,560,000
5.120
Sodium
--
8,670L00
17.340
Sulfur
---
--
--
Nitrate N / Nitrite N
---
733.000
1.466
Barium
---
---
---
Chloride
---
—
_--
Iron
---
Aluminum
—
1,100.00
2.200
Arsenic
---
39.80
0.080
Cadmium
---
39M
0.080
Chromium
39.80
0.080
Copper
---
70.90
0.142
Lead
39M
0.080
Mercury
---
1.480
0.003
Molybdenum
---
39.80
0.080
Nickel
---
39.80
0.080
Selenium
---
39.80
0.080
Zinc
---
274.00
0.548
Envirochem: 2019-00094
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
2.63
Ceiling Caucen.
75
85
4,300
840
57
75
420
100
7,500

Rr Environmental Chemists Inc.
y 8 0 - ° 8 -• 6602 Windmill Way, Wilmington, NC 28405 .. 910.392.0223 Lab • 910.392,4424 Pax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Pax
M 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Pax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Date of Report: Jan 29, 2019
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer ID: 08100011
Attention:
Report #: 2019-00094
Project ID: Ocean Isle Beach
Lab ID Sample ID: OIB
Collect DatelTime Matrix Sampled by
19-00241 Site: OIB WWTP
1/2/2019
7:56 AM Solid/Sludge Scott Leonard
Test
Method
Results
Date Analyzed
Chlordane (TCLP)
SW 646 Method 8081BI3510
<0.02 mg/L
01/1012019
Endrin(TCLP)
SW 846 Method8081B13510
<0.0005mg/L
01/1012019
Heptachlor (TCLP)
SW846 Method 8081813510
<0.0005 mg/L
01/10/2019
Heptachlor epoxide (TCLP)
SW 846 Method 80SIBI3510
<0.0005 mg/L
01/10/2019
Lindane(TCLP)
SW848Method 80818/3510
<O.DO05mg/L
01/10/2019
Methoxychlor (TCLP)
SW846 Method 80SIBI3510
<0.0005 mg/L
01/10/2019
Toxaphene (TCLP)
SW 846 Method 0081B13510
<0.05 mg/L
01110/2019
1,4-Dichlorobenzene(TCLP)
SW 846 method 8270/3510
<0.050mg/L
01/12/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/12/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/12/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg1L
01/12/2019
Cresol (TCLP)
SW846 Method827o/3510
<0.050mg/L
01112/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/1212019
Hexachlorobenzene(TCLP)
SW 846 method 8270/3510
<0.050mg/L
01/12/2019
Hexachloroethane (TCLP)
SW 846 method 82701351a
<0.050 mg/L
01/12/2019
m + p-Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/12/2019
Nitrobenzene (TCLP)
SW 646 method 827013510
<0.050 mg/L
0111212019
o-Cresol(TCLP)
SW 846 method 827=51 0
<0.050mg/L
01/12/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
01/12/2019
Pyridine (TCLP)
SW 846 method8270/3510
<0.050mg/L
01/12/2019
2,4,5-TP
SW846 Method 8151A
<0.003mg/L
01/10/2019
2,4-D
SW846 Method 8151A
<0.003 mg/L
01/1012019
1,1-Dichloroethylene (TCLP)
SW846 Method0260/5030
<0.01 mg/L
01/11/2019
1,2-Dichloroethane (TCLP)
SW846 Method826015030
<0.01 mg/L
01/1112019
Benzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
01/11/2019
Carbon Tetrachloride (TCLP)
SW846 Method8260/5030
<0.01 mg/L
01111/2019
Reportit; 2019-00094
Page 1 of 3

alk
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab m 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347 5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Post Office Box 249
Bolivia NC 28422
Attention:
Date of Report: Jan 29, 2019
Customer PO #:
Customer ID: 08100011
Report #: 2019-00094
Project ID: Ocean Isle Beach
Chlorobenzene(TCLP)
SW846 Method826015030
<0.01mglL
01111/2019
Chloroform (TCLP)
SW046 Method 8260/5030
<0.01 mg/L
01/11/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
01/11/2019
Tetrachloroethylene(TCLP)
SW846 Method826015030
<0.01mg/L
01/11/2019
Trichloroethylene (TCLP)
SW846 Method826015030
<0.01 mg/L
01/11/2019
Vinyl Chloride (TCLP)
SW846 Method 82601503D
<0.01 mg/L
01/11/2019
RCI
Cyanide
EPA335.4
<0.05mg/kg
01/17/2019
Sulfide
SM 4500 S D
1.09 mg/kg
01/16/2019
Ignitability
SW 846 method 1010
>215 OF
01/11/2019
Sludge Residuals
Aluminum
EPA200.7
1100mg/kg
01/05/2019
Arsenic
EPA200.7
<39.8mg/kg
01/06/2019
Cadmium
EPA200.7
<39.8mg/kg
01/06/2019
Calcium
EPA200.7
6220mg/kg
01/16/2019
Chromium
EPA200.7
<39.8mg/kg
01/06/2019
Copper
EPA200.7
70.9mg/kg
01/0612019
Lead
EPA 200 7
<39.8 mg/kg
01/06/2019
Magnesium
EPA200.7
2560mg/kg
01/16/2019
Molybdenum
EPA200.7
<39.8mg/kg
01111/2019
Nickel
EPA200.7
<39.8mg/kg
01/06/2019
Potassium
EPA200.7
4270mg/kg
01/16/2019
Selenium
EPA200,7
<39.8mg/kg
01/06/2019
Sodium
EPA200.7
8670mg/kg
01/16/2019
Zinc
EPA200.7
274mg/kg
01/05/2019
Total Kjeldahl Nitrogen (TKN)
EPA 351.2
61800 mg/kg
0111212019
Nitrate+Nitrite-Nitrogen
EPA353.2
733mg/kg
01/18/2019
Total Solids (%)
SM 2540 B
1.28 %
01/03/2019
pH
SM4500HB
6.10units
01/17/2019
Ammonia Nitrogen
SM 4500 NH3 C
5030 mg/kg
01/21/2019
Report #:: 2019-00094
Page 2 of 3

Environmental Chemists, Inc.
�tiat� V�a
Si � ' �:
�$ 8 8; 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 lab • 910.392.4424 Fax,ai�f`.'`. i'4;e "` 1 'Ma,, 710 Bowserfown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
a �' 255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(a-)environmentalchemists.com
Brunswick County Public Utilities Date of Report: Jan 29, 2019
Post Office Box 249 Customer PO #:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report #: 2019-00094
Project ID: Ocean Isle Beach
Total Phosphorus SM4500 P F 20100 mg/kg 01/10/2019
Mercury SW8467471B <1.48mg/kg 01/09/2019
TCLP Metals
Arsenic
EPA200.7
<1.0mg/L
01/12/2019
Barium
EPA200.7
<1.0mg/L
01/12/2019
Cadmium
EPA200.7
<1.0mg/L
01/1212019
Chromium
EPA200.7
<1.0mg/L
01/12/2019
Lead
EPA200.7
<1.0mg/L
01/12/2019
Selenium
EPA200.7
<1.0mg/L
01/12/2019
Silver
EPA 200.7
<1.0 mg/L
01/12/2019
Mercury
EPA245.1
<0.0002mg/L
01/19/2019
Lab ID
Sample ID: OIB
Collect Daterrime
Matrix Sampled by
19-00242
Site: Influent
1/2/2019 7:54 AM
Water Scott Leonard
Test
Method
Results Date Analyzed
Total Phosphorus
SM4500PF
4.26mg/L
01/10/2019
Lab ID
Sample ID: OIB
Collect Date/Time
Matrix Sampled by
19-00243
Site: Effluent
1/2/2019 7:48 AM
Water Scott Leonard
Test
Method
Results Date Analyzed
Nitrite Nitrogen
EPA353.2
0.05 mg/L
01/03/2019
Total Phosphorus
SM4500 P F
1.42 mg/L
01/10/2019
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA351.2
1.7 mg/L
01112/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
3.18mg/L
01/16/2019
Total Nitrogen
Total Nitrogen
4.9mg/L
01/21/2019
Comment: Sludge residuals,
except pH, reported on a dry weight basis,
pH reported on an as received basis.
Reviewed by: �,QJQ,
pjP)'
Report #:: 2019-00094 Page 3 of 3

ENVIRONMENTAL 4CHEMISTS, INC 6602 Windmill Way
M
Wilmington, NC 28405
Sample Collection and Chain of Custody PLone: [phone]
a v
w Collection 4!
ample Identification e 6 a a w;
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DATE TIME TEMP
s " °
PRESERVATION —
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c O 0 AtVnLYSLS REQUESTED
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1
G
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Brunswick County
Lune Stabilization Ph Test Results
Hauler. 810-GREEN Services, Inc.
Sludge Source: _ _Zic __ � nn�WTp
Permit: M JA - _------ Approximate Gallons: o�c4
Initial Pb Test
Date.2^ (--71q Time _1
Ph ---j-- Tr tnp .
temperature Corrected Ph
2 Hour Ph Teat
Time .1'�)3p_. Operator...j_�_..
'temmpp.,.- Tap
'emp Corrected Ph_
24 Hour Ph Test
I ate. 2� ., Time _j-&5
smp Corrected Ph
Operator
A.

Brunswick County
Lime Stabilization Ph Tog Results
"Ruler: BIO-GREEN Swims, Inc.
Sludge Source: � — - �QP/ICX� — —WWTP
;Permit #: ���Q(oQ�S - Approximate C*Hon&: _qZ�
Initial Ph Test
Date 1jA.11t_ Time I(1 Operator , ;!�4, _
remperature CorrecW Ph
2 Hour Ph Teat
)ate 1l -lf -J� rime J_g 3_5.
'emp Corrected Ph
'06
or__�_� _
Hour Ph Test ----------
I ate A-5-«, Time
A
T=p _
:mp Corrected Ph. I I k

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 2, 2019
Sea Trail WWTF Permit No. W00034513
Mineralintion Rate 0.30 1.10 % Solids
7.17 pH
Parameter
I %
Mg/Kg Dry Weight
(% x 1Q000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (THIN)
7.720
77,200.000
154.400
Phosphorus
3.070
30,700.000
61.400
Potassium
0.286
2,860.000
5.720
PAN (injected)*
2.575
25,752.000
51.504
PAN (surface)*
2.449
24,487.000
48.974
Ammonia Nitrogen
0.253
2,530.000
5.060
Calcium
2.150
21,500.000
43.000
Calcium Carbonate Eq.
---
--
Magnesium
---
6,030.000
12.060
Sodium
—
5,900.000
11.800
Sulfur
---
---
--
Nitrate N / Nitrite N
—
821.000
1.642
Barium
---
Chloride
---
---
---
Iron
---
Aluminum
---
5,620.00
11.240
Arsenic
---
47.30
0.095
Cadmium
---
47.30
0.095
Chromium
47.30
0.095
Copper
---
249.00
0.498
Lead
47.30
0.095
Mercury
---
L820
0.004
Molybdenum
47.30
0.095
Nickel
47.30
0.095
Selenium
---
47.30
0.095
Zinc
648.00
1.296
Envirochem: 2U 19-00095
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits
for calculation purposes.
SAR
0.96
Ceiling Coneen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
so
710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Post Office Box 249
Bolivia NC 28422
Attention: Brian Blanton
Date of Report: Jan 29, 2019
Customer PO #:
Customer ID: 08100011
Report #: 2019-00095
Project ID: Sea Trail
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-00245 Site: Sludge
1/2/2019
8:28 AM Solid/Sludge Clint Humphrey
Test
Method
Results
Date Analyzed
Chlordane (TCLP)
SW846 Method8081W510
<0.02mg/L
01/10/2019
Endrin (TCLP)
SW846 Method 8081B/3510
<0.0005 mg/L
01/10/2019
Heptachlor (TCLP)
SW 846 Method 8081 B/351 0
<0.0005mg/L
01/10/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081 B1351 0
<0.0005 mg/L
01/10/2019
Lindane(TCLP)
SW 646 Method 8081 B/351 0
<0.0005mg/L
01/1012019
Methoxychlor (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
01/10/2019
Taxaphene (TCLP)
SW 846 Method 80819/3510
<0.05 mg/L
01110/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/12/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/12/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01112/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/12/2019
Cresol (TCLP)
SW 846 method 627013510
<0.050 mg/L
01/12/2019
Hexachloro-1,3-butadiene(TCLP)
SW 846 method 827013510
<0.050mg/L
01/12/2019
Hexachlorobenzene (TCLP)
SW 846 method 627013510
40.050 mg/L
01/12/2019
Hexachloroethane(TCLP)
SW 846 method 827013510
<0.050mg/L
01/12/2019
m + p-Cresol (TCLP)
SW 846 method 827013510
<0,050 mg/L
01/12/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050mg/L
01/12/2019
o-Cresol (TCLP)
SW 846 method 827013510
<0.050 mg/L
01/12/2019
Pentachlorophenol (TCLP)
SW 846 method 827013510
<0.250mg/L
01/12/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
01/12/2019
2,4,5-TP
SW846 Method8151A
<0.003mg/L
01/10/2019
2,4-D
SW846 Method 6151A
<0.003 mg/L
01/10/2019
1,1-Dichloroethylene(TCLP)
SW846 Method8260/5030
<0.01mg/L
01/1112019
1,2-Dichloroethane (TCLP)
SW046 Method 8260/5030
<0.01 mg/L
0111112019
Benzene (TCLP)
SW846 Method0260/5030
<0.01mg/L
01/11/2019
Carbon Tetrachloride (TCLP)
SW846 Method8260/5030
<0.01mg/L
01/11/2019
Report #.: 201 g-00095 Page 1 or 3

Environmental Chemists, Inc.
qw�s
6602 Windmill Way, Wilmington, NC 28�405 . 910.392.0223 Lab • 910.392.4424 Fax
w710 Bowserton Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities
Date of Report: Jan 29, 2019
Post Office Box 249
Customer PO #:
Bolivia NC 28422
Customer ID: 06100011
Attention: Brian Blanton
Report #: 2019-00095
Project ID: Sea Trail
Chlorobenzene (TCLP) SW846 Method 8260/5030
<0.01 mg/L
01/11/2019
Chloroform (TCLP) SW846 Method$26015030
<0.01 mg/L
01/11/2019
Methyl ethyl ketone (TCLP) SW846 Method826015030
<0.05mg/L
01/11/2019
Tetrachloroethylene(TCLP) SW846 Method826015030
<0.01mg/L
0111112019
Tdchloroethylene (TCLP) SW846 Method 8260/5030
<0.01 mg/L
01/11/2019
Vinyl Chloride (TCLP) SW846 Method 8260/5030
<0.01 mg/L
0111112019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
0110812019
Sulfide
SM 4500 S D
<0.1 mg/kg
01/16/2019
Ignitability
SW 845 method 1010
>205 °F
01/11/2019
Sludge Residuals
Aluminum
EPA200.7
5620mg/kg
01/0512019
Arsenic
EPA200.7
<47.3mg/kg
01/06/2019
Cadmium
EPA200.7
<47.3mg/kg
01/06/2019
Calcium
EPA200.7
21500mg/kg
01/16/2019
Chromium
EPA200.7
<47.3mg/kg
01/06/2019
Copper
EPA 200.7
249 mg/kg
01106/2019
Lead
EPA 200.7
<47.3 mg/kg
01/06/2019
Magnesium
EPA200.7
6030mg/kg
01/16/2019
Molybdenum
EPA200-7
<47.3mg/kg
01/11/2019
Nickel
EPA200.7
<47.3mg/kg
01/06/2019
Potassium
EPA200.7
2860mg/kg
01/16/2019
Selenium
EPA200.7
<47.3mg/kg
01/06/2019
Sodium
EPA200.7
5900mg/kg
01/16/2019
Zinc
EPA200.7
648mglkg
01105/2019
Total Kjeldahl Nitrogen (TKN)
EPA351.2
77200mg/kg
01/12/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
821 mg/kg
01/18/2019
Total Solids (%)
SM 2540 B
1.10 %
01/0312019
pH
SM4500 H B
7.17 units
01117/2019
Ammonia Nitrogen
SM4500NH3 C
2530mg/kg
01/21/2019
ReportV 2019-00095
Page of

Environmental Chemists, Inc.
6602 Windnull Nay, Wilmington, NC 28405 = 910.392.0223 Lab ® 910.392.4424 Fax
E' ISN, 710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 A 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS in fo(`u environmentalchemisls.corn
Brunswick County Public Utilities
Post Office Box 249
Bolivia NC 28422
Attention: Brian Blanton
Total Phosphorus
Mercury
TCLP Metals
Date of Report: Jan 29, 2019
Customer PO #:
Customer ID: 08100011
Report #: 2019-00095
Project ID: Sea Trail
SM 4500 P F 30700 mg/kg
SW8467471E <1.82 mg/kg
01/10/2019
01109/2019
Arsenic
EPA200.7
<1.0mg/L
01/17/2019
Barium
EPA 2007
<1.0mg/L
01/17/2019
Cadmium
EPA200.7
<1.0mg/L
01/17/2019
Chromium
EPA2un7
<1.0mg/L
01/17/2019
Lead
EPA 200.7
<1.0 mg/L
01117/2019
Selenium
EPA200.7
<1.0mg/L
01117/2019
Silver
EPA 200.7
<1.0mg/L
01/17/2019
Mercury
EPA 2451
<0.0002mg/L
01/19/2019
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis
{E
Reviewed by: I� 11 0, ClAjGC
Y
Report #:: 2019-00095 Page 3 of 3

Analytical 6 Consulgng Chemists
ENVIRONMENTAL CHEMISTS, INC
f4CDENR: DWO CERTIFICATION t 94 NCDHHS: DLS CERTIFICATION S 37M
COLLECTION AND CHAIN OF CUSTODY
W2 Windmill Way Wilmington, NC 2&
OFFICE: 910.392-M3 FAX [phone]:
info®envlronmentalchwW sts.com
-+
- I ^t,.wC c-
-- - - �i G y J
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONEIFAX:
COPY TO:
emah:
Cbmninsi fAv 1 .._ .. ... n . ad CAHbf C NbC. 4 _ � _ — ... .. ,.- .-.
Sample identification
ollec ' n
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ma
---
PRESERVATION
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ANALYSIS REQUESTED
Date
Time
Temp
i
ox
c
0
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
G
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By.
DateTme
Received pY;
DateTme
I emperature wnen rieceivea:
Delivered Sv: _ c" � c
Time: L 3'� r�—
TURNAROUND:

N
i, li y. per'
a` Brunswick County
]Lime Stabilization Ph Test Results
Hauler: SIO-GREE 14 Services, Inc.
h1
+� ludge Source: ! z4Tj?AIL
Permit #: t�4- tZ -1 4 B
ii
A
Gallons:
Initial PI. Test
Date Time �perat(
Ph _ Temp 4
Temperature Corrected Ph 12.1
2 Hour Ph Test
Date- 3 - Tyme
Ph Temp
Temperature Corrected Ph _ 1
Date 3-12-2ot9 'time
Ph 12.
Temperature Corrected Ph
24 Hour
Temp
Test
Operator�C'

Brunswick County
Lime Stab Lion ph Test Results
Hailer. BIO-GREEN Service, Iine.
Sludge Source: " ,
W WTP
Approximate Gallons:
PP
Initial Ph Test
Date - t4 Time p
r Operator
Ph a 2
— •�� Temp_
Temperature Corrected Ph i 2 •� i
2 Hour Ph Test
Date 3v 19 Time 2 Operator
Temp
Temperature Corrected Ph
'I. oS
24 Hour Ph Test
Date 5-i- ►`� Time l:Z,,o Operator C
Ph 12.. a<j Temp 23 ' u
Temperature Corrected Ph 'L• p3
i

Brunswick County
Lime Stabilization Ph Vest Results
Hauler: BIO-GREEN Services, Inc.
Sludge Source:
Permit #: --L4jS,. 6o 12-14A ApproAmate Gallons: _ tt ,pp0
Initial Ph Test
Date -3D-111 Time Operator C ,1
Ph L2. k2j Temp 22%
Temperature Corrected Ph 12.0-1
2 Hour Ph Test
Date_A- 30-� Time Operator--C-- k ,
Ph 12• t9 Temp 22.C.
Temperature Corrected Ph l2• 13
24 Hour Ph Test
Date S- t _ Time ( P „_ Operator C
Ph l L. 2 1 . Temp Lls.I
Temperature Corrected Ph 12 • t

Sludge Source:
D.0 U u.e
Brunswick County
Lime Stabilization Ph Test Results
Hauler: BIO-GREEN Services, Inc.
EM
Permit #: Id Q 00 / 2 746 Approximate Gallons:
Initial Ph Test
DateI—Jo,-9-0-6-Time qa 3o_,, Operator
�� C
Ph �2. v3 Temp C'
Temperature Corrected Ph
2.16
2 Hour Ph Test
Date42oi1 Time
Operator
Ph _ i (• a'l
Temp
Temperature Corrected Ph %2 . o2
24 Hour Ph Test
Date g 7641 Time _ S I Operator C
Ph_ 9 .1(e Temp 2Q.9 �"�'
Temperature Corrected Ph _ 1 .. OiL

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: September 19, 2019
Shallotte WWTP
Mineralization Rate 0.20
Parameter
Carbonate
N / Nitrite N
4.88 % Solids
6.6 pH
% Mg/Kg I
(% x
3.980
0.747
0.054
1.214
0.510
4.310
Permit No. WO0034513
Weight Pounds/Dry Ton
000) I (Me/K2 x 0.002)
5,100.000
43,100.000
692.000
100.000
8.55
37.30
180.00
47.30
0.204
12.80
15.60
10.00
588.00
Waypoint 19-263-0046
79.600
14.940
1.082
24.280
19.180
10.200
86.200
5.640
1.384
0.200
39.200
0.017
0.006
0.075
0.360
0.095
0.000
1.176
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N +Nitrate N +Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.19
Ceiling Concen.
(mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

I V jyAtfe'\)
Waypoint
ANALYTICAL
10/1/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-263-0046
Client Project Description: Brunswick Co.
Shallotte. NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypoi ntana lytica l.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 9/20/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama 440750 Louisiana #04015
Mississippi California #29D4
Kentucky #90047 Tennessee #TN02027
VANELAP #460181
NC 4415
EPA #TND0012
Texas #T304704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 7

YB�
Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Client: EMA Resources Inc CASE NARRATIVE
Project: Brunswick Co.
Lab Report Number: 19-263-0046
Date: 10/1 /2019
Metals Analysis Method 6010D
Sample 95106
Analyte: Aluminum
QC Batch No: L455238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L455238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L455238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L455238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Phosphorus
QC Batch No: L455238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95105 (Shallotte WWTP Lagoon #1)
Analyte: Aluminum
QC Batch No: 1-455940/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Copper
QC Batch No: 1-455940/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L455940IL454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
Page 2 of 7

Waypointm G)
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213,2440
www.waypointanalytical.com
QC Batch No: L455940IL454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: 1-455940/1-454923
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: 1-455940/1-455479
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: 1-455940/1-455479
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 7

e
M
Waypoi nt. 2 Whitten Road, Memphis, TN 38193
Main 901.213.2400 0Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Brunswick Co. Report Date : 10/01/2019
755 Yadkinville Rd Information : Shallotte, NC Received : 09/20/2019
Mocksville , NC 27028
Danyale Love
Report Number :19-263-0046
REPORT OFANAL YSIS
Project
Manager
Lab No : 95105
Matrix:
Solids
Sample ID : Shallotte WWTP Lagoon #1
Sampled:
9/191201910:00
Test
Results
Units
MDL
MQL
DF
Date l Time
By
Analytical
Analyzed
Method
% Moisture
95.1
%
0.010
1
09/20/19 16:59
ADM
SW-DRYWF
Ammonia Nitrogen
5100
mg/Kg - dry
510
1
10/01/19 09:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<100
mg/Kg - dry
100
100
1
10/01/19 14:34
ZBD
4500NO3F-2011
Organic N
34700
mg/Kg - dry
1470
1
10/01/19 09:00
CALCULATION -
pH
6.6
S.U.
1
09/30/19 06:58
JSL
9045D
Total Solids
4.88
%
0.010
0.010
1
09/20/19 16:59
ADM
254OG-2011
Total Volatile Solids
28.2
%
0.010
0.010
1
09/20/19 16:59
ADM
254OG-2011
Total Kjeldahl Nitrogen
39800
mg/Kg -dry
1470
1
10/01/19 16:01
CLP 4500NORGD-2011
Phosphorus
7470
mg/Kg - dry
52.4
102
1
09/26/19 18:51
JTR
6010D
Aluminum
19600
mg/Kg - dry
41.4
102
1
09/26/19 18:51
JTR
6010D
Arsenic
<8.55
mg/Kg - dry
8.55
10.2
1
09/26/19 18:51
JTR
6010D
Cadmium
3.18
mg/Kg - dry
1.01
2.04
1
09/26/19 18:51
JTR
6010D
Calcium
43100
mg/Kg - dry
343
510
1
09/26/19 18:51
JTR
6010D
Chromium
37.3
mg/Kg - dry
3.88
5.10
1
09/26/19 18:51
JTR
6010D
Copper
180
mg/Kg - dry
2.96
5.10
1
09/26/19 18:51
JTR
6010D
Iron
23100
mg/Kg - dry
86.5
102
1
09/26/19 18:51
JTR
6010D
Lead
47.3
mg/Kg - dry
3.04
6.12
1
09/26/19 18:51
JTR
6010D
Magnesium
2820
mg/Kg - dry
45.3
102
1
09/26/19 18:51
JTR
6010D
Manganese
110
mg/Kg - dry
3.73
10.2
1
09/26/19 18:51
JTR
6010D
Mercury
0.2043
mg/Kg - dry
0.0698
0.316
1
09/23/1914:08
TJS
7471A
Molybdenum
12.8
mg/Kg - dry
2.65
5.10
1
09/26/19 18:51
JTR
6010D
Nickel
15.6
mg/Kg - dry
3.37
5.10
1
09/26/19 18:51
JTR
6010D
Potassium
541
mg/Kg - dry
60.8
102
1
09/23/19 21:35
BKN
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation
Limit
Page 4 of 7

B
WaYpo i
2790 Whitten Road, Memphis, TN 38133
■ ■t,
Ma
Main
901.213.2400 0Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins
Project
Brunswick Co.
Report Date : 10/01/2019
755 Yadkinville Rd
Information : Shallotte, NC
Received : 09/20/2019
Mocksville , NC 27028
Report Number :19-263-0046
REPORTOFANALYSIS
Dany\gale Love
Project Manager
Lab No : 95105
Matrix: Solids
Sample ID : Shallotte WWTP Lagoon #1
Sampled: 9/19/2019 10:00
Test
Results
Units MDL
MQL DF Date/Time By Analytical
Analyzed Method
Selenium
<10.0
mg/Kg - dry 10.0
10.2 1 09/26/19 18:51 JTR 6010D
Sodium
692
mg/Kg - dry 158
510 1 09/26/19 18:51 TFR 6010D
Zinc
588
mg/Kg - dry 22.0
25.5 1 09/26/19 18:51 JTR 6010D
Sulfur
12000
mg/Kg - dry 99.8
102 1 09/26/19 18:51 JTR 6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00 1 09/26/19 18:51 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 5 of 7

279D Whitten Road, Memphis,
Waypoi nt ,
Main 901.213.2400 °Fax [phone].2440
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number. 19-263-0046
Shipping Method
Fed Ex O US Postal O Lab
O UPS 0 Client 0 Courier
O Other:
Thermometer ID:
70
Shipping container/cooler uncompromised?
0 Yes
Q No
Number of coolers received
r —1
Custody seals intact on shipping container/cooler?
O Yes
O No
0 Not Required
Custody seals intact on sample bottles?
O Yes
O No
I> Not Required
Chain of Custody (COC) present?
Yes
O No
COC agrees with sample label(s)?
Yes
O No
COC properly completed
Yes
O No
Samples in proper containers?
0 Yes
Q No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
40 Yes
O No
Cooler temperature in compliance?
0 Yes
O No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
O No
Water - Sample containers properly preserved
O Yes
O No
N/A
Water - VOA vials free of headspace
0 Yes
O No
N/A
Trip Blanks received with VOAs
O Yes
O No
N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
O No
N/A
F High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
7 Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
O Yes
No
Comments:
Signature: Kristina A. McAdams Date & Time: 9/20/2019 10:37:29
Page 6 of 7

Client Name/Address
Client Project Manager/Contact
Billing Information
For laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location(City/state)
RUSH -Additipnal charges apply
Met dof5hipment
Matrix Key
,(1
�dA`1•or-r� /k
s-
Special Detection Limit(s)
Date Results Needed
Fed Ex OUPS ❑USPS
Courier Client Drop Off
W
W - Wastewater GIN -Groundwater
DW- Drinking Water 5-Soli/Solid O - Oil
P-Product M-Mist
Other
Project Number
Project Manager Phone N
Project Manager Email
Purchase Order Number
Site/Facility ID #
336-399-3646
[e-mail]
o
co
Z
(n
A Cool 4 SBC NaM03(Mlom Only)
0
.0
a
a cool ceC
Wa oint
ANALYTICAL
o
r
O
E
o
E
E
m
O
U)
c H1504 pH2
D None Required
2790 Whimn Road
sa
w
N
Q
E NaOH P11110
F HNWPH2
Memphis. IN 38133
Unless noted, all containers
o
°1
=
`o
M
Z
CU
T
1/^-�
U
G HCtpH2
[phone]
per Table ll of AD CfRPart
_
a
0)
Y
�-
O
U
H H3PO4 pHa
135.
E
-`
t
H
Z
iJ..
1 Cool a 6C NAZR03
Dale
Time
Sample Identification
Required
Analysis
/ Preservati
Comments/Notes
A
S/fRtcsroc--'
o:ov
L
G
Metals:Al,As,Ca, Cd,Cr,Cu, Fe, Pb
M n, M g, M o, H g, N i, S e, N a, P, S, K, Z n
6
IIIIII IIIII IIII IIIIII IIIIIIIIII IIII IIIIII III IIIIII IIIII IIII
IIII
W46245
zo 9
EIAAReeOCeS Inc 10.37:07
Brunsvrick Co.
For Laboratory Use Only
Sampled by(Name- Print)
J�oq �lk�-r�Kc-2
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Seals
Lab Comments
( YJ
l.% N
Relinq e R
Y
D e Time
Received by: (SIGNATURE )
Date Time
p
:W
Blan Coolef Temp
Relinqui ed by: (SIGNATURE)
Date Time
Received by: tSfGNATURE)
Date Time
L
Relinquished by: (SIGNATURE)
Date Time
Receive hy: ISIGNATURE)
Date
Time
</ I�
L
I-
C.

aceAnafyticalo ANALYTICAL REPORT
Nadonal Cehler PorTesdng&Innoatlon I �e1
October 10, 2019
I z
EMA Resources
Sample Delivery Group:
Samples Received:
Project Number:
Description:
L1145056
10/01/2019
Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksvllle, NC 27028
Entire Report Reviewed By:
_ Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced except In full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National Is performed per guidance provided In laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0069. Where sampling conducted by the customer, results relate to the accuracy of the Information provided.
and as the samples are received,
Tc
i a55
4Cn
5Sr
� 6
[QC
'GI
�I -AI
� gSc
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
EMA Resources L1145056 10OA9 ilia 1of21

TABLE OF CONTENTS ONELAB.NATIONWIDE
Cp: covor Page
1
Tc: Table of Contents
2
`V
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr. Sample Results
5
3S5
SHALLOTTE L1145056-01
5
rCn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Chemistry by Method 9034-90306
g
Wet Chemistry by Method 9045D
9
6QC
Wet Chemistry by Method D93/1010A
10
171-1
Mercury by Method 7470A
11
GI
Metals (ICP) by Method 6010D
12
1
71
Volatile Organic Compounds (GC/MS) by Method 8260D
13
° i
Chlorinated Acid Herbicides (GC) by Method 8151A
15
��Sc
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
Al: Accreditations & Locations
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATEITIME:
PAGE:
EMA Resources L1145056
10/1011911.18
2 of 21

SAMPLE SUMMARY ONELAB.NATIONWIDE.
SHALLOTTE L1145056-01 Waste
Collected by
Brent Collins
Collected date/time
09130/1908,00
Received dateltime
10/01I1909:00
El
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
ETC
Preparation by Method 1311
WG1357064
1
10/03/1915:27
10/0311915:27
IDW
Mt. Juliet. TN
Preparation by Method 1311
WG1357693
1
1010411915:03
10/04/1915:03
CGD
Mt. Juliet. TN
Wet Chemistry by Method 9012 B
WG1358978
1
10/OBA9 20:42
10109/1910,11
SDL
Mt. Juliet. TN
Wet Chemistry by Method 9034-9030B
WG1357109
1
10/OBA911:05
1010811911:05
MJA
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WGI355716
1
10/01/19 21:00
10/02A9 22,00
JIC
Mt. Juliet, TN
4Cn
Wet Chemistry by Method D93AO10A
WGI358323
1
10/08/1911:32
1010811911:32
MJA
Mt. Juliet, TN
Mercury by Method 7470A
WG1357917
1
10/05/1909:17
10107/1914:08
ABL
Mt. Juliet, TN
sSr
Metals(ICP) by Method 6010D
WG1357811
1
1010511915:12
10/07/1910:39
CCE
Mt. Juliet, TN
Volatile Organic Compounds (GC1MS) by Method 8260D
WG1358312
1
10/07A918i28
10/0711918,28
ACG
ML Juliet, TN
Chlorinated Acid Herbicides (Gq by Method 8151A
WG1358141
1
10/05/1916.41
10/06A913,04
LEL
ML Juliet, TN
sQC
Pesticides (GC) by Method 80818
WG1359164
1
10/08/1917:48
10/09/191102
LEL
ML Juliet, TN
Semi Volatile Organic Compounds(GC/MS) by Method 8270E
WG1357823
i
10107/1906:35
10/07/1920:24
AO
ML Juliet, TN
TGI
'AI
9Sc
ACCOUNT;
PROJECT:
SDG;
DATE/TIME:
PAGE:
EMA Resources
L1145056
10110/1911.18
3 of21

CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the RP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples ZTc
have been corrected for the dilution factor used In the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been Identified by the laboratory, and no information or data have been
knowingly withheld that would affectthe quality of the data.
rSr
6Qc
[GI
Justin Carr
Project Manager yAl
Project Narrative e5C
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/90306.
ACCOUNT: PROJECT: SDG: DATEMME: PAGE
EMA Resources L1145056 todo/19 ilia 4of21

SHALLOTTE
SAMPLE RESULTS - 01
ONE LAB. NATIONWIDE.
Collected date/time: 09/30/19 08:00
L1145056
Preparation by Method 1311
Result
Qualifier
Prep Batch
Analyte Analyte
dale / time
TCLP Extraction
10/3/2019 3273I PM WG1357064
TCLP ZHE Extraction -
10/4120193:03:57 PM WG1357693
Fluid 1
10/3/20193:27:31PM WG1357064
aSs
Initial pH 6.91
10/3/20193:27:31 PM WG1357064
Final pH 4.91
10IN2019 3:27:31 PM WG1357064
4Cn
Wet Chemistry by Method 9012 B
Result
Qualifier
RDL Dilution Analysis
Batch
Analyte mg/kg
mg/kg date/time
Reactive Cyanide ND
0.250 1 10/09/20191091
WG1358978
sQC
Wet Chemistry by Method 9034-9030B
'C'I
Result
Qualifier
RDL Dilution Analysis
Batch
Analyte mg/kg
mg/kg date/time
Reactive Sulfide 54.6
25.0 1 10/W201911:05
WG1357109
A�
Wet Chemistry by Method 9045D
eSc
Result
Qualifier
Dilution Analysis Batch
Analyte su
date/time
Corrosivity bypH 6.77
TS
1 10/02/201922:00 WG1355716
Sample Narrative:
-
L1145055-01 WG1355716: 6.77 at 22.7C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyze Deg. F date /time
Ignitability DNI at 170 1 101081201911:32 WG13583Z3
Mercury by Method 7470A
Result
Qualifier RDL
Limit
Dilution Analysis Batch
Analyte mgll
mg/I
mg8
date/time
Mercury ND
0.0100
0.20
1 16107/20191008 WG1357917
Metals (ICP) by Method 6010D
Result
Analyze
mgll
Arsenic
ND
Barium
0.101
Cadmium
ND
Chromium
ND
Lead
ND
Selenium
ND
Silver
ND
Qualifier RDL
limit
mg)1
----. .. ---
mgll .
0.100
5 _
0.100
100
0.100
1
0.100
5
0.100
5
0.100
1
0.100
5
Volatile Organic Compounds (GC/MS) by Method 8260D
Dilution Analysis
Batch
date /time
1 10/071201910:39
WG1357811
1 10/07/20191039
WG1357911
1 10107/201910:39
WG1357811
1 10107/201910:39
WG1357811
1 101071201910:39
WG1357811
1 101071201910:39
WG1357811
1 10/071201910:39
WG1357811
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg8
mg/1
mgA
date/time
Benzene
ND
0.0500
0.50
1 10107/201918:28
M1358312
Carbon tetrachloride
ND
0.0500
0.50
1 101071201918:28
WG1358312
Chlorobenzene
ND
0.0500
100
1 10107/201918:28
WG1358312
Chloroform
ND
0.250
6
1 10/07I201918:28
WGI358312
ACCOUNT: PROJECT: SDG: DATE/11ME: PAGE
EMA Resources L1145056 10110/191178 5 of 21

SHALLOTTE SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 09/30/19 08:00 L1145056
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
RDL
Limit
Dilution
Analysis
Batch
Analyte
mgA
mgA
mgll
date/time
1,2-Dichloroelhane
ND
0.0500
0.50
1
10/071201918:28
WG1358312
1,1-Dichloroethene
ND
0.0500
0.70
1
10107201918:28
WG1358312
2-Butanone(MEK)
ND
0:500
200
1
101071201918:28
WG1358312
Tetrachlomethene
ND
0.0500
0.70
1
10/071201918:28
WG1358312
Tdchloroethene
ND
0.0500
0.50
1
101071201918:28
WG1358312
Vinyl chloride
ND
0.0500
0.20
1
10/07/201918:28
WG1358312
(S)Toluene-d8
95.0
80.0-120
10107120191828
WG1358312
(S) "tomoBuorobenzene
104
77.0-126
10107201918:28
WG1358312
(5) 1.2-Dichloroethone-d4
112
70.0-130
10107201918.28
WG1358312
Chlorinated Acid Herbicides (GC) by Method
8151A
Result
Qualifier
RDL
Limit
Dilution
Analysis
Batch
Analyte
_ -_ -
mgA
mgA
mgA
date/time
2,4,5-TP (Silvex(
- -
ND
-
J4
-
0.00200
- -
1
---
1
_ 10/O6I2019_ 13:04
- -- ---
WG1358141
2,4-D
ND
J4
0.00200
10
1
10106/201913:04
WG1358141
(5)Z4-DichlorophenylAcelicAcid
127
14.0-158
101061201913:04
WG1358141
Pesticides (GC) by Method
8081B
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mgll
mgA
mgA
date/time
Chlordane
ND
0.00500
003
1
10109201911:02
WG1359164
Endrin
ND
0.00500
0.02
1
10/091201911:02
WG1359164
Heptachlor
ND
0.00500
0.0080
1
10/09/201911:02
WG1359164
Lindane
ND
0.00500
0.40
1
10109/201911:02
WG1359164
Methoxychlor
ND
0.00500
10
T
10/09/201911:02
WG1359164
Toxaphene
ND
0,0100
0.50
1
10/091201911:02
WG1359164
(S) Decachlorobipheny/
96.3
10.0-128
101091201911i02
WG1359164
(S)Tetrochloro-m-xylene
90.8
10.0-127
101091201911:02
WG1359164
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mgA
mgA
mgA
date/lime
1,4-Dichlorobenzene
ND
0.100
7.50
1
10/071201920,24
WG1357823
2,4-Dinitrotoluene
ND
0.100
0.13
1
10/07/201920:24
WG1357823
Hexachlorobenzene
ND
0.100
0:13
1
101071201920:24
WG1357823
Hexachlorc-13-butadlene
ND
0.100
0.50
1
10107201920:24
WG1357823
Hexachloroethane
NO
0.100
3
1
101071201920:24
WG1357823
Nitrobenzene
ND
0.100
2
1
101071201920:24
WG1357823
Pyridine
ND
J4 0.100
5
1
10/0712019 20:24
WG1357823
3&4-Methyl Phenol
ND
0.100
400
1
10/07/201920:24
WG1357823
2-Methylphenol
ND
0.100
200
1
10107/201920:24
WG1357823
Pentachloraphenol
ND
0.100
100
1
10107/201920:24
WG1357823
2,4,5-Trichlorophenol
ND
0.100
400
1
10107201920.24
WG1357823
2,4.6-Tdchlomphenol
ND
0.100
2
1
10107120192024
WG1357823
(5)2-Fluorophenol
36.6
10.0-120
101071201920.24
WG1357923
IS)Phenol-6
213
10.0-120
10107120192024
WG1357823
(5) Arltra4,enzene-d5
54.4
10.0-127
10107120192024.
WG1357823
(5))2-F/uorob/phenyl
70.0
10.0-130
10107120192024
WG1357823
(5)2,4,6-Trlbromophenol
88.0
10.0-155
10/07201920:24
WG1357823
(5)p-Terphenyl-M
68.6
10.0-128
10107201920:24
WG1357823
ACCOUNT: PROJECT: SDG: DATWTIME: PAGE:
EMA Resources L1145056 10A011911d8 6of 21

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GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below Is designed to better explain the various terms used in your report of analytical results from the Laboratory. This Is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer- Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
No
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) -Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate: used to evaluate analytical efficiency by measuring recovery, Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or If concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target %recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful OC Sample analysis will target all analyzes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be Included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier Is provided within the Glossary and Definitions page and
potentially a discussion of possible Implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The Information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncerinty
(Radjo hem
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the Included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This Is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number forthe analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy,
J5 The sample matrix Interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
TB Sample(s) received past1too close to holding time expiration.
H
zTc
3C8
�Cn
5
Sr
sOC
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ACCOUNT: PROJECT: SDG: DATEMME: PAGE
EMA Resources L1145056 10/10/1911:18 19 of 21

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. 4
Pace National is the only environmental laboratory accrediled/certlged to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our Industry. The most significant benefit to our one location design Is the design ofaur laboratory campus. The model Is condudve to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
' Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
Manama
40660
Nebraska
NC-05-15-05
Alaska _
17-026
Nevada
TN-03-2002-34
Arizona
AZO612 _ _
New Hampshire
2975
Arkansas _
88-0469
New Jersey—NEIAP
7N002
California
2932
New Mexico
Ne
Colorado
TN00003
New York
11742
Connecticut
PH•0197
--
North Carolina
-
Env375
Florida
E87487
North Carolina'
_
DW21704
Georgia
NELAP
North Carolina'
41
Georgia' _
_ 923 _ _
North Dakota
R-140
Idaho
TN00003 _
_
Ohfo—VAP
_ _
CLOO69
Illinois
200008 _
Oklahoma
_
9915
Indiana
C-TNoil
_ Oregon
TN200002
Iowa
364
Pennsylvania
_
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky"
90010
South Carolina
_
84004
Kentucky'
16
South Dakota
nya
Louisiana
A130792
Tennessee "
2006
Louisiana'
_ LA180010
Texas
_
TIO470424548-15
Maine
TN0002
Texas,_
_
LABO152
Maryland
324
Utah
TN00003
Massachusetts
M-TN003 _
Vermont
_
VT2006
Michigan _
9958
Virginia
466132
Minnesota
_ 047-999-395
Washington
C847
Mississippi
_ TNO0003
West Virginia
233
Missouri
340
Wisconsin
_
9980939910
Mantana
CERT0006
Wyoming
A2lA
Third Party Federal Accreditations
A21A— ISO 17D25 146WI AIHA4AP,tLC EMLAP 100789
A21A— ISO 17025' 1461.02 DOD --_ 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Cryplo TN00003
' Drinking Water 2 Underground Storage Tanks 'AquatkToxicity'ChemicaVMicrobialogical,Mold'Wastewater We Accreditation not applicable
IOUs Locations
Pace National has sixty-four client support centers that provide sample pickup
our main office. Pace National performs all testing at our central laboratory.
tTt WA
MT NO
OR
T ID SO
WY
T NV T NE
UT T CO
CA
TAZ NM
L
],
HI I
.m
sampling supplies. If you would like assistance from one of our support offices, please contact
hIN
T WI NY
NII T
A T PA
T IL rN,, OH
VAT -
K6 h1O ` ICY �-
D� AR SC
MS .AZ T(3
LA. I 1jj
Fl
N1E
ACCOUNT: PROJECT: SDG: DATEMME: PAGE
EMA Resources L1145056 10/10/19 ills 20 of 21

e- i -
Billing Information:
EMA Resources
755 Yadkinville Road
MOCksville, NC 27028
Mr. Brent Collins Pres
755 Yadkinville RoadMocksville, NC 27028 Chk
P
Gain of Custody Pagc_nf_
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Nrk.✓om.w nrma a.nwR
tW65LebanonRd
Moum Mon. rN 37122
Phom 615a5e.5asR
PMre: OW 767-9a59T I�
P,.: cts-psesas9 Q '
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Report to:
Mr. Brent Collins
Email To: brent.mllim0emaresourcesinc.com
Project
Description: Sludge
City/State
SPsI 1 1G
Collected: q�bVtpJL
Please Circle:
PT MCT ET
Phone: [phone]
Fax: [phone]
Client Project#
Lab Project11
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Tab: - 8�.32
Acctnum: EMARES
Template:T11413
Prelogin: P731244
PM: 807-Justin Carr
PB:
Shipped Via: FedEX Ground
aem.rLs Samplevllab onNl
Collected by (pnn[):
^
~� C.a11aAf
site/Facili 10g
dY
P.O. g
Collected by (signature):
Immediate) Y
Pecked on Ice N_ Y
Rush? (Lab MUST Be Notified) Quote If y
a-
_ Same Day _ flue Day a
_NW Da 5D Rad On —
y �( Date Results Needed Z
_Two Day _10Day(Rad Only)
_Three Day Nu. -
v
Sample ID
Comp/Grab
Me[rix +
Depth
Date
T(me
of
J
ntrs '
V
rL
SA4 fit,4-d-
C
SS
L I
9/30 /9
Y:ooeN
2 1
X
—I
p
I
I
• Matrix: emarks: ---
SS-5011 AIR-Alr F- Filter H
GW- Grountlwater e- Bioassay P _Temp
W- Waste Water RAD SCREEN: <0.5 mR/hr
DW- Drinking Waqter Flow_ Other
OT-Other 135.f. gL Samples returned via:
— _ _ Tracking g I �(�
UPS FedEx Courier g
Sam a Recei c the k ist
COC seal Preeenc/Intact: _NP z N
CDC Signed/Accurate: —Y —N
Bottles arrive intact: —Y —N
Correct bottles urea: _Y _N
Suf Eicienc voluree sent: —Y —N
` J
Relinquished by:(Signature) Date: —
Time: Received by: (Signature) Trip Blank Received: Yes/
94,0119 /Z-Vrpn HCL/MeoH
If A 11 clR,
VOA zero Headapace: Y _N
Preservation eorrece/Cheeks 1: x N
re/tLr: y—N
RRn Screen c0.5 re
Relinqu shed by: (Signature) Date: Time: Received by: (Signature) TBR
Temp: °(: 9ottics Rece a: If
1_ �A¢
Relinquished by: (Signature) Date: Time: R. ed for la my Sat ' ure i //) Date: Tim ' Hold:
V� '<,J/r0
preservation required by login: Oate/Time
Condit -
NCF OK

Shallotte WWTP
WQ0034468
Class B - 2019
i>i[;�I�i;�i[[if
F�C�I C0�1�OTIIt's
i€i`ICt
09/19/19
16,049
4.2054
09/19/19
28,696
4.4578
09/19/19
23,333
4.3680
09/19/19
15,464
4.1893
09/19/19
17,143
4.2341
09/19/19
18,293
4.2623
09/19/19
20,115
4.3035
Total 30.0205
Average 4.2886
€ Fecal Coliform Colonies /gram
Geometric Mean 19'437
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.
Geometric Mean of Less than 1,000 meets a portion of Class A - Alternative 5 Pathogen
Reduction requirement.

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 1
Report Date: 9/30/2019
Date Sample Rcvd: 9/19/2019
Meritech Work Order #
09191938 Sample: Shallotte Lagoon #1 Grab
9/19/19
Parameters
Result Analysis Date Reporting
Limit
Method
% Total Solids
24.3 % 9/20/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
16049 col/g dry wt 9/19/19
130 col/g drywt
SM 9222D
Meritech Work Order #
09191939 Sample: Shallotte Lagoon #2 Grab
9/19/19
Parameters
Result Analysis Date Reporting
Limit
Method
%Total Solids
11.5 % 9/20/19 0-100
%
SM 2540B
Fecal Coliform (Sludge)
28696 col/g dry wt 9/19/19
130 col/g dry wt
SM 9222D
Meritech Work Order #
09191940 Sample: Shallotte Lagoon #3 Grab
9/19/19
Parameters
Result Analysis Date Reporting
Limit
Method
% Total Solids
15.0 % 9/20/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
23333 col/g dry wt 9/19/19
130 col/g drywt
SM 9222D
Meritech Work Order #
09191941 Sample: Shallotte Lagoon #4 Grab
9/19/19
Parameters
Result Analysis Date Reporting
Limit
Method
% Total Solids
19.4 % 9/20/19 0-100
%
SM 2540B
Fecal Coliform (Sludge)
15464 col/g dry wt 9/19/19
130 col/g dry wt
SM 9222D
Meritech Work Order # 09191942 Sample: Shallotte Lagoon #5 Grab 9/19/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 21.0 % 9/20/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 17143 col/g dry wt 9/19/19 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 2
Report Date: 9/30/2019
Date Sample Rcvd: 9/19/2019
Meritech Work Order # 09191943 Sample: Shallotte Lagoon #6 Grab
Parameters Result Analysis Date ReoortingUmlt
%Total Solids 16.4 % 9/20/19 0-100 %
Fecal Coliform (Sludge) 18293 col/g dry wt 9/19/19 130 col/g dry wt
Meritech Work Order # 09191944 Sample: Shallotte Lagoon #7 Grab
Parameters Result Analysis Date Reporting Limit
%Total Solids 17.4 % 9/20/19 0-100 %
Fecal Coliform (Sludge) 20115 col/g dry wt 9/19/19 130 col/g dry wt
9/19/19
Method
SM 2540B
SM 9222D
9/19/19
Method
SM 2540B
SM 9222D
I hereby certify' that I have reviewed and approve these data.
Laba atoryRepresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

s9_=ors Chain of Custody Record (COC)
NPDES#:
Client:_ EMA Resources Inc. Phone:_336-751-1441
Address:_ 755 Yadkinville Rd Fax: [phone]
Moeksville NC 27028 Email:= [e-mail]
Project:
P.O.#:
Attention:_ Brent Collins Turn Around rime*
How would you like your report sent? 'RUSH work needs prior approval.
Circle all that apply: Emai preferred), Fax, Mail 5td soda s) 3-s Da s za.asurs
ME R ITEC H I N C•
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Pe nTa ' a p g pr' tJ: o 1 Z
Lab Use Only
Start
Tim
e me
End
Date Time
comp?
Groh?
#of
Cont.
Test(s)
Required
Yes es/N
No
pH ?
Cl OK?
sti
9i/5
Z
3
Y
5
l.t
7
v
V
Temperature Upon
Receipt:
Method of
"' Dechlorination <0.5 p m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. •*•
Q ,
Shipment:
Comments:
Compositor #
UPS
Jug#
Fed Ex
Hand Delivery
re here a ults fg regulatory purposes? Yes No 15
Relinqu" D te: Time:
x 9/gmjq S'cea.,
Report results in: mg/L [, mg/kg E ug/L [ �
Received by: Date: Time:
g%iy/�y
Other
Relin uished 9tQ%9/19 Time:/£:SJSOM
Received by: Date: Time:
Relinquished by: Date: Time:
Rec ed
9

% Volatile Solids IN 0.04
%Total Solids IN 0.1
% Fractional Volatile Solids IN 0.400
% Volatile Solids OUT 1.7
%Total Solids OUT 6.77
% Fractional Volatile Solids OUT 0.251
Volatile Solids
As a decimal
Volatile Solids In 0.400
Volatile Solids Out 0.251
Volatile Solids Reduction 49.7

EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date:
Reported:
For:
Comments:
Analytical Results
09/19/2019
09/20/2019
Shalotte WWTP
i.a-7ALYTIZ.'aL
r�
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190919-17-01
% Volatile Solids
IN
0.04
% SM25400
09/19/2019
WC
190919-17-01
Percent Solids
IN
<0.1
% SM25408-2011
09/19/2019
WC
190919-17-02
% Volatile Solids
OUT
1.70
% SM2540G
09/19/2019
WC
190919-17-02
Percent Solids
OUT
6.77
% SM2540e-2011
09/19/2019
WC
Respectfully submitted,
,-w%(L JT7)�.,
Dena Myers
NC Cart #440.
NCDW Cerl #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3

Condition of Receipt
Sample Number 190919-17-01 Temp on Arrival:
Parameter Schedule: Percent Solids
Parameter Schedule:
Sample Number 190919-17-02 Temp on Arrival:
Parameter Schedule:
Received on Ice
Received on Ice
Received on Ice
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

Client: _
L—
3G17PSVILLEANALYTIGL
Address: .',s,� Zi'✓1l UE a
R
122COW SUOI • P.O.rlox228
SgtoAlle, NC 28697
7} �
�(+1 C:.5 auC a28
(7e4)9724697
Contact Person: KN� Phone # .1 .5i_lvie FAX#
Chain of
Custody Record
PD # A Requisitioned by: Dare)
W to
cueWmar
Semple ID*
L IDY
Time Sampled
(GraOOnM
vela Sampled
(Gmb Ony)
g
s
Mail.
Puaneien «qudwl ror milYmr
�a. !1 of
;,.
��T�« say
Relinquished by:
Received by: /�G� 9T^
Relinquished by:
Received by:
Composite Sampling #i:
Time begin am, pm Date _/ /
Time and am, pm Date / !_
Composite Sampling #2:
Time begin am, pm Dale _J_J_
Time end am, pm Date _/_J_
Time %%S arl Oateqn/&,/f Sampled by: o
Time aT Date4���9 Transported by:/ 0
Time am, pm Date ___J_J_ Holding limes met:
Time am, pm Date _J_J_ l/
Compliance work:
Non-compliance work;
Lab Comments: Samples Transported On Ice:
Inluals:
iL
n
�m
N O
W N
V
o fi
n
n
cv
00
00
N
U
Z
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Q
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SOIL ANALYSIS REPORTS

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY20-SL010138
Client:
Bic Green Services Inc
Advisor:
Predictive
Nc 235 Grey Water Rd
U I.-.
Supply,NC 28462
Soil Report Mehlich-3
Extraction
-_/
Sampled County : Brunswick
Links to Helpful Information
Client ID:
503667
Advisor ID:
Sampled: Received: 10/16/2019 Completed: 10/25/2019
Farm: Brunswick
Sample ID: BRPV2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., E 0.8
60-80 0
0
0 0
0
0
0
0
Note: 12
2-Bermuda hay/past., M 0.0
180-220 0
0
0 0
0
0
0
0
Note: 12
Test Results [units - WIV in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mg/drna]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.61 0.93 10.4 80 2.0 5.6 158 141
61 13
55
50
47 47
405
405
110
0.3
3
Sample ID: BRAH1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean 1.3
0 0
30
0 0
10
0
0
0
Note: 3
2-Soybean 0.0
0 0
30
0 0
$
0
0
0
Note:3 Note:
Test Results [units -WIV in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-1
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.37 1.15 6.1 65 2.2 5.1 98 60
50 10
55
20
22 22
104
104
54
0.1
2
Sample ID: BRAH2
Recommendations: Lime
Nutrients (lb/acre)
I More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean 1.1
0 0
40
0 0
10
0
0
0
Note: 3
2-Soybean 0.0
0 0
40
0 0
$
0
0
0
Note:3 Note:
Test Results [units -WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mgldnr :
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.19 1.15 6.2 68 2.0 5.2 209 50
50 14
74
25
25 25
157
157
96
0.1
2
North Carolina
]�d.xne 1iu+[ FurJ Q'nnu>aoo
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: w .ncagr.gov/agronomil
Report No.
FY20-SL010138
Page 2 of 4
Sample ID: !
Recommendations:
Lime
Nutrients (lb/acre)
More
Os
Crop
(tons/acre)
N PzOS
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
0.8
120- 160 0
70
0
0
0
0
0
0
Note: 3
2-Com,grain
0.0
120-160 0
70
0
0
0
0
0
0
Note:3
Test Results [units - WIV in
91cm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
1.08 1.29 6.8
73 1.8 5.5
579 32
56 15
40
73
61
61
637
637
295
0.1
1
Sample ID: BRCG2
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
0.4
120 - 160 0
50
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
50
0
0
0
0
0
0
Note: 3
Test Results [units - WIV in
g/cm3; CEC and Na in
meg1100 cm3; NO3-N in mg1dm3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-Ali
Mn-AI2
Zn-I
Zn-AI
Cu-1
Na
ESP
SS-1 NO3-N
0.81 1.23 5.9
76 1.4 5.8
462 43
53 19
43
96
75
75
389
389
136
0.1
2
Sample ID: BRCG3
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
1.0
120 - 160 0
100
0
0
0
0
0
0
Note: 3
2- Corn, grain
0.0
120 - 160 0
100
0
0
0
0
0
0
Note: 3
Test Results [units - WIV in
glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WfV CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-1
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
1.08 1.33 5.7
67 1.8 5.3
440 19
52 14
38
84
67
67
469
469
180
0.1
2
Sample ID: BRCG4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain
1.2
120- 160 0
100
0
0
0
0
0
0
Note: 3
2 -Corn, grain
0.0
120 - 160 0
100
0
0
0
0
0
0
Note: 3
Test Results [units -WIV in
glcm3; CEC and Na in meq1100 cm3; NO3-N in mg/drrl3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
1.02 1.23 4.5
56 2.0 5.1
185 18
39 15
31
25
32
32
135
135
75
0.1
2

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomit
ReportNo.
FY20-SL010138
Page 3 of 4
Sample ID: §
Recommendations: Lime
Nutrients (lb/acre)
More
'GROG 8
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain 1.2
120- 160 0
100
0
0
0
0
0
0
Note: 3
2-Corn, grain 0.0
120-160 0
100
0
0
0
0
0
0
Note:3
Test Results [units - W/V in
glcnt3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]:
soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.76 1.24 4.5
55 2.0 5.1 308 22
37 16
37
21
30
30
139
139
77
0.1
2
Sample ID: BRHB1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., E 1.6
60-80 0
100
0
0
0
0
0
0
Note: 12
2-Bermuda hay/past., M 0.0
180-220 0
190
0
0
0
0
0
0
Note: 12
Test Results [units - W/V in
glcm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.56 1.13 10.4
73 2.8 5.2 1183 19
61 10
70
72
60
60
1562
1562
547
0.1
1
Sample ID: BRCC1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., E 1.4
60-80 0
100
0
0
0
0
0
0
Note: 12
2-Bermuda hay/past., M 0.0
180-220 0
190
0
0
0
0
0
0
Note: 12
Test Results [units - WIV in
g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg1dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS-1 NO3-N
0.97 1.23 4.2
48 2.2 4.9 180 18
33 13
36
21
30
30
129
129
72
0.1
2
Sample ID: NCRA1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., E 0.5
60-80 0
50
0
0
0
0
0
0
Note: 12
2- Bermuda hay/past., M 0.0
180-220 0
130
0
0
0
0
0
0
Note: 12
Test Results [units - WIV in
g/cm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP
SS -I NO3-N
0.41 1.01 1&5
87 2.1 5.8 171 44
56 30
42
856
531
531
398
398
300
0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
ReportNo. FY20-SLO10138
Page 4 of 4
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report
Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM°/
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
M-0
manganese index
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www-ncagr.gov/aoronomi/oboart4.htmYifsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/v
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, AG and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
zn-1
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.goWaoronomi/uvrsthtm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY20-SL012901
Client: Bio Green Services Inc Advisor:
Heavy Metals Nc 235 Grey Water Rd
Supply, NC 28462
Soil Report Mehlich-3Extraction
Sampled County :Brunswick
Links to Helpful Information
Client ID: 503667 Advisor ID:
Sampled: 09/20/2019 Received: 11/01/2019 Completed: 11/05/2019 Farts: Burnswick
Agronomist's Comments:
This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a
soil test extractant, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium
(Cr)- 0.2 ppm, lead (Pb)- 4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007). Note elevated zinc (Zn)in the sample.Although the above metals here are
not believed to pose a concern for plant growth, continue to monitor these and note where elevated above background levels. Note any lime and fertilizer recommendations.
Where soil test phosphorus P is very high (P-I > 100), crops will not respond to additional P applied. Ja athi Kamalakanthan 11/5/2019
Sample ID: BRHB1
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Bermuda hay/past., E 1.9 60-80 0 100 0 0 0 0 0 0
Note: 12
2-Bermuda hay/past., M 0.0 180-220 0 190 0 0 0 0 0 0
Note: 12
Test Results [units - W/Vin g/crr?; CEC and Na in meg1100 cm3; NO3-N in mgldm): Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.66 1.12 9.8 68 3.2 5.1 1079 18 58 9 59 56 51 51 1384 1384 480 0.1 1
Heavy Metals (parts per million): Arsenic, 0.2 Cadmium, 0.1 Nickel, 1.0 Chromium, 0.4 Lead, 5.0 Selenium, 0.1
North Carolina
inl�.ic:r im+: I ia�.il Unurr.+snrn
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SL012901
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report
Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-1
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 Ito per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability Index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
M-O
N
mineral -organic soil class
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit wwwncaoroov/aoronomi/oboart4.htmf9fsrnd information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertifizer.
P2O5
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-1
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-Al I, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncaqr. cov/agronomi/uyrsLhtm

Page 1 of 1
Report Number: 19-284-0611 �
Account Number:46245
Waypoint.
Send To: EMA Resources Inc ANALYTICAL
755 Yadkinville Road "Every acre... Every year."ra
Mocksville NC 27028
SOIL ANALYSIS REPORT
Date Received: 10/11/2019 Date Of Analysis: 10/14/2019 Date Of Report: 10/14/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Grower: Harry Hart
Analytical Methodist): Mehllch 3 SMP Buffer pH Loss On Ignition Water pH
NC = North Carolina Fertility Index Value
HM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
oI
Soil
Class
It
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
M 9
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
PH
Buffer
Index
H
meg1100g
meq/100g
6 Front
19710
1.4
106
84 H
NC=70
43 VL
NC=22
126 H
813 M
15
VL
5.6
6.77
1.6
6.9
MIN
6 Back
19711
1.6
121
68 H
NC=57
36 VL
NC=18
123 H
706 M
11
VL
5.4
6.74
1.9
6.6
MIN
7 A
19713
1.6
118
129 VH
NC=107
84 L
NC=43
172 H
1024 M
20
VL
5.8
6.77
1.6
8.5
MIN
7 B
19714
1-6
116
101 VH
NC = 84
72 L
N(
253 H
983 M
21
VL
6.1
6.81
1.2
8.5
MIN
Pines
19715
1.7
127
14 L
NC=12
j
17 VL
NC=9
34 L
134 VL
16
L
4.3
6.72
2.1
3.2
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Aluminum (AI)
Sample ID
Field ID
K
e/
Mg
%
Ca
%
Na
e/
H
%
NOaN
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm
Rate
SS
mslcm
Rate
ppm
6 Front
1.6
15.2
58.9
0.9
23.2
20 M
NC=42
4.0 H
NC=100.0
6 L
NC=38
0.7 L 1
NC=35.0
0.3
VL
0.27
VL
699
6 Back
1.4
15.5
1 53.5
0.7
28.8
18 M
NC=37
2.0 L
NC=50.0
6 L
NC=38
0.7 L
NC=35.0
0.4
L
0.2
VL
820
7A
2.5
16.9
60.2
1.0
18.6
34 H
NC=71
6.0 H
NC=150.0
9 L
NC=56
1.8 H
NC=90.0
0.4
L
0.4
VL
1002
7 B
2.2
24.8
57.8
1 1.1
1 14.1
37 VH
NC=77
3.7 H
NC=92.5
4 L
NC=25
1.0 M
NC=50.0
0.4
L
0.36
VL
926
Pines
1.4
8.9
20.9 1
2.2 1
65.6
16 M
NC=33
0.9 VL
NC=22.5
1 VL
NC=6
0.2 VL
NC=10.0
0.2
VL
0.1
VL
943
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of urirty days after testing. p me G
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: PAWr° Easy'
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by. waypomtAnalNlcal Vlrglyds, Inc.
Pauric McGroary

Brunswick County Class B biosolids land applied by BioGreen Services, Inc. (BioGreen) during the
2019 calendar year were lime stabilized to meet Pathogen and Vector Attraction Reduction
monitoring with the exception of Shallotte. Therefore, lime additions for soil pH adjustment are
being made to fields through the addition of lime stabilized biosolids.