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Home My WebLink AboutWQ0034806_Residual Annual Report 2019_20200213Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submital an application?* r Yes r No Annual Report 2019 Year* Date Paper Copy 2/13/2020 Received:* Project Number* WQ0034806 Email Notifications ................................................................................................... Does this need O Yes review by the a No hydrogeologist? * Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by NJB Staff regarding electronic submittal, confirmation of receipt, and other issues. .................................................................................................................................................................................................................................................................................................................................................................................................... Name * Martin Mabe Email Address* martin@willcoxmabesoil.com Project Information ........................................................................................................................................................................ Submittal Type* f New Permit Application r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0034806 Applicant\Permittee * Wesley Wooten Facility Name * Coastal Farms and Residuals, LLC Phone Number* 336-312-1396 r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. One hard copy is being mailed. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) Coastal Farms 2019 Annual Report (NCDEQ).pdf 20.49MB upload only 1 RJF document. Maniple documents crust be combined into one RJF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contact the reviewer or Tessa Monday. If a paper application is required, be advised, applications accepted for pre -review until both the paper and electronic copies have been received. The paper copy shall include the following: o Application Form o All relevant attachments (caIcs, soils report, specs, etc. o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required} Mailine address: Division of Water Resources Division of Water Resources Non -Discharge Branch I Non -Discharge Branch ---- --- - --- - --- ------------ ------------------------------------i---------------------------------------------------------------------------- 1617 Mail -service Center Att: Nathaniel Thornburg, 9"' Floor, Office #942W ---- -NC �-- - -------------------------------------------- ------------------------------------------------ Raleih, 7699-1617 512 N. SaVisbury St For questions or problems contact Tessa Monday at tessa.monday@ncdenr.Qov or 919.707.3660. * W By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/10/2020 2019 ANNUAL REPORT LAND APPLICATION PROGRAM COASTAL FARMS AND RESIDUALS, LLC PERMIT #WQ0034806 Prepared For: Coastal Farms and Residuals, LLC 8155 Malpass Corner Road Currie, North Carolina 28435 Compiled By: Willcox & Mabe Soil Solutions, PLLC 7231B Summerfield Road Summerfield, North Carolina 27358 February 2020 willcox&mate SOIL SOLUTIONS February 10, 2020 NCDEQ-DWR Non -Discharge Compliance Unit 512 North Salisbury Street 90'Floor Office# 942X Raleigh, North Carolina 27604 Attention: Non -Discharge Compliance Unit Reference: 2019 LAND APPLICATION ANNUAL REPORT Coastal Farms and Residuals, LLC Permit No. W00034806 WMSS Project No. 15-19 Ph:01 Non -Discharge Compliance Unit: Willcox & Mahe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Coastal Farms and Residuals, LLC. WMSS compiled this report using data gathered during the compliance year by Coastal Farms and Residuals, LLC. This data includes: 1) certification form, 2) residuals analyses and pathogen / vector data, 3) application summaries and field loading rate reports, 4) soil analyses. If there is any further information required or questions regarding this annual report please do not hesitate to contact Coastal Farms and Residuals, LLC or WMSS for further assistance. Sincerely, Willc_ox�& Maabe Soil Solutions, PLLC Martin Mahe NC Land Application/Residuals Operator #22753 Enclosures Shared\WMSS Projects\2015\15-19 Coastal Residuals\2019 Annual Report\2019 ANNUAL REPORT- COASTAL FARMS.doc Willcox & Mabe Soil Solutions, PLLC / 7231 B Summertield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willcoxmabescil:mm TABLE OF CONTENTS SECTION NO. TITLE Certification Form II Residuals Analyses & Pathogen / Vector Attraction Data III 2019 Application Summary and Field Loading Rate Reports IV Soil Analysis CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: W00034806 County: Pender Year: 2019 Facility Name (as shown on permit): Coastal Farms and Residuals, LLC Land Application Operator: Mr. Wesley Wooten Phone: 910-283-5444 Land application of residuals as allowed by the permit occurred during the past calendar year? p Yes p No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary. Total number of application fields in thepermit: 12 Total number of fields utilized for land application during the year: 1 Total amount of dry tons applied during the year for all application sites: 668.67 Total number of acres utilized for land application during the year: 93.4 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. Hl Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Mr. Wesley W000ten, President Permittee Name and Title (type or print) !n 1/24/20 Signature f Permittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (12/2006) RESIDUAL ANALYSES TCLP ANALYSES IF REQUIRED AND PATHOGEN AND VECTOR ATTRACTION REDUCTION COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 23, 2019 Avendale W WTP 0.37 % Solids 6.71 off Permit No. W00030775 Parameter "-°/* ., 'Itifg/Kg Dry Weigh[ =. %x 10,Q00) Pounds/Dry Ton Nitrogen (TKN) 11.100 111,000.000 222.000 Phosphorus 2.440 24,400.000 48.800 Potassium 0.841 8,410.000 16.820 PAN (injected)* 5.739 57 390.000 114.780 PAN (surface)* 4.174 41 740.000 83.480 Ammonia Nitrogen 3.130 31,300.000 62.600 Calcium 3.190 31,900.000 63.800 Calcium Carbonate E . -- Magnesium 3,950.000 7.900 Sodium 15 200.000 30.400 Sulfur --- --- --- Nitrate N / Nitrite N --- 2,180.000 4.360 Barium Chloride --- --- --- Iron --- --- Aluminum --- 5,620.00 11.240 Arsenic 26.50 0.053 Cadmium --- 26.50 0.053 Chromium --- 26.500 0.053 Copper 462.00 0.924 Lead -- 26.50 0.053 Mercury 4.050 0.008 Molybdenum 26.50 0.053 Nickel 26.50 0.053 Selenium 26,50 0.053 Zinc --- 865.00 1.730 Environmental Chemistsp 2019-17953 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN SAR 1.30 Ceiling Concen. (MQ/Kg) 75 85 4,300 840 57 75 420 100 Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N+Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Tab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS is foriiuenvironmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Nov 01, 2019 ' 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: 'Welsley Wooten Report #: 2019-17953 Ltmmp Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45820 Site: Sludge 10/23/2019 3:00 PM Solid/Sludge wesley wooten Test Method Results Date Analyzec Sludge Residuals Aluminum EPA 200.7 5620mg/kg 10/28/2019 Arsenic EPA 200.7 <26.5 mg/kg 10/28/2019 Cadmium EPA 200.7 <26.5mg/kg 10/28/2019 Calcium EPA 200.7 31900 mg/kg 10/2812019 Chromium EPA 200.7 <26.5mg/kg 10/28/2019 Copper EPA 200.7 462mg/kg 10/2812019 Lead EPA 200.7 <26.5mg/kg 10/28/2019 Magnesium EPA200-7 3950mg/kg 10/28/2019 Molybdenum EPA 200.7 <26.5mg/kg 10/28/2019 Nickel EPA 200.7 <26.5 mg/kg 10/28/2019 Potassium EPA 200.7 8410mg/kg 10/28/2019 Selenium EPA 200.7 <26.5mg/kg 10/28/2019 Sodium EPA 200.7 15200mg/kg 10/28/2019 Zinc EPA 200.7 865mg/kg 10/28/2019 Nitrate+Nitrite-Nitrogen EPA353.2 2180mg/kg 10/29/2019 Total Solids (%) SM 2540 B 0.37 % 10/24/2019 pH SM 4500 H B 6.71 units 10/29/2019 Ammonia Nitrogen SM 4500 NH3 C 31300 mg/kg 10/27/2019 Total Kjeldahl Nitrogen (TKN) SM 4500 org B 111000 mg/kg 10/27/2019 Total Phosphorus SM4500PF 24400mglkg 10/30/2019 Mercury SW0467471B <4.05mg/kg 10/26/2019 Report # 2019-17953 Page 1 of 3 Environmental Chemists, Inca 4W. 6602 Windmill Wav, Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Pax 710 tiowsertown Road, Manteo, NC 27954 - 252.475.5702 Lab/Fox 255-.A Wilming ton Highm'aV, Jacksonville, NC 23540 o 910.3475543 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS inliNulelnvironmentalchemists.eom Lewis Farms ✓£ Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Date of Report: Nov 01, 2019 Customer PO #: Customer ID: 14020008 Report #: 2019-17953 Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45821 Site: 1 10/23/2019 3:05 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 0.33 % 10/24/2019 Fecal Density SM 9221 C E MPN 24 hr 503 23637MPN/g 10/24/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45822 Site:2 10/23/2019 3:06PM Solid/Sludge wesley wooten Test Method Results Date Analvzed Total Solids (%) SM 2540 a 0.39 % 10124/2019 Fecal Density SM92210EMPN 24hr503 35898MPN/g 10/24/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45823 Site: 3 10/23/2019 3:07 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 s 0.34 % 10/24/2019 Fecal Density SM92210EMPN 24hr503 38236MPN/g 10/24/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45824 Site: 4 10/23/2019 3:08 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 s 0.47 % 10/24/2019 Fecal Density SM 9221C E MPN 24 hr503 9575 MPN/g 10/24/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45825 Site: 5 10/23/2019 3:09 PM Solid/Sludge wesley wooten Test Method Results Date Analvzed Total Solids (%) SM 2540 s 0.49 % 10/24/2019 Fecal Density SM 9221C E MPN 24 hr sm 22449 MPN/g 10/24/2019 Report #:' 2019-17953 Page 2 of 3 Environmental Chemists, Inc. 1 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab - 910.392.4,124 Fax >5J 710 Bowsertown Road, Mmteo,. NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalebemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Nov 01, 2019 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2019-17953 Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45826 Site: 6 10/23/2019 3:10 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) sM2540 a 0.53 % 10/24/2019 Fecal Density SM 9221C E MPN 24 hr 503 14717 MPN/g .10/24/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45927 Site: 7 10/23/2019 3:11 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 s 0.21 % 10/24/2019 Fecal Density SM 9221C E MPN 24 hr 503 21429 MPN/g 10124/2019 Comment: Sludge residuals and Fecal Density reported on a dry weight basis. pH reported on an as received basis. - 1_I ^ Reviewed by: A Cky'lfoi I Report#r 2019-17953 Page 3 of 3 IV 4=0ENVIRONMENTAL CHEMISTS, INC OFFICE•9d0.392-0M ilmingto FAN 9128405 0-3 2- Analytical & Consulting Chemists NCDENR: DWO CERTERICATION 0 94 NCDHHS: US CERTIFICATION Y 37729 4424 COLLECTION AND CHAIN OF CIISTOOV CLIENT: l p PROJECT NAME: REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: E-MAIL: Sampled By: (i1%. SAMPLE TYPE: 1 = Influent E = Effluent W = Well ST = Stream SO = Soil SL = Slud Oth Sample Identification Collection E 8 8; e E 0 a(g E ` ce o t E " w 9m m g z PRESERVATION e, er. ANALYSIS REQUESTED D e Time Temp w i F a 4 $ o o w o f G G C P G G C p J s r G G Z 3 ac C P- G G G G 3'1 C P G G C P G G G C P G G 3� C P G G C P G G NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechimineted 10.2 ppm or leas) In the field M the time of wliecllon. See reverse for Instructions Transfer Relinquished BY: DateTme Received By.- Date/Time 1- 2. Temperature when Received: —T. C? Accepted: V Delivered By: Received ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTPName: AvendaleWWTP NPDESNumber: W00030775 Monitoring Period: From 1/1/2019 To 12/31/2019 Pathogen Reduction (15A: NCAC 02T .1106) - Please indicate level achieved and alternative nerfarmed: Class A• Alt. A time/tem ❑ ( P) Alt B Alk Treatment ❑ Alt. C ( ) (Prior Testing)❑ ....... ................... Alt.D (No Prior Test) ❑ Process to Further Reduce Patlio en s ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray❑ Gamma Ray ❑ Pasteurization Class B: JAIt. (1) Fecal Density❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air D iu ❑ Com ostiu ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ < If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Num er o Excee- enneqof Frequency Anal Analysis Sample Type na ica Tech- Minimu Geo. Mean Maxitnu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 9,575 21,608 38,236 MPN/g 0 Annual Grab SM92210E CFU ' 1000 mpn per gram of total solid (dry wei ht Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry Weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative Derformed: AR.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ I AT 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El JAIL 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the n vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Charles Bryan, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer*/ Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T 02/2006) COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Avendale WWTP iv& fdofi&M! 10/23/19 23,637 4.3736 10/23/19 35,898 4.5551 10/23/19 38,236 4.5825 10/23/19 9,575 3.9811 10/23/19 22,449 4.3512 10/23/19 14,717 4.1678 10/23/19 21,429 4.3310 Total 30.3423 Average 4.3346 Geometric Mean jjili**11121O. I Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 17, 2019 Carolina Beach W WTP Permit No. NC0023256 4.34 % Solids 6.9 pH Parameter % Mg/Kg Dry Weight (% x 10,0001 Pounds/DryTon at 0.002) Nitrogen (TKN) 5.080 50,800.000 101.600 Phosphorus 0.018 178.000 0.356 Potassium 0.150 1,500.000 3.000 PAN (injected)* 1.691 16,911.000 33.822 PAN (surface)* 1.587 15,866.000 31.732 Ammonia Nitrogen 0.209 2,090.000 4.180 Calcium 3.460 34,600.000 69.200 Calcium Carbonate E . --- Ma nesium --- 3,200.000 6.400 Sodium --- 3,870.000 7.740 Sulfur --- --- --- Nitrate N / Nitrite N --- 208.000 0.416 Barium --- --- --- Chloride --- --- --- Iron Aluminum --- 4,190.00 8.380 Arsenic 12.90 0.026 Cadmium 12.90 0.026 Chromium --- 21.500 0.043 Copper 631.00 1.262 Lead --- 30.20 0.060 Mercury 0.530 0.001 Molybdenum 12.90 0.026 Nickel 13.10 0.026 Selenium 12.90 0.026 Zinc - 906.00 1.812 Environmental Chemists # 2019-06163 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN SAR 1.11 Ceiling Concen. (Mg/Kg) 75 85 4,300 840 Surface Application: (Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N) N+Nitrite N=%PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. Environmental Chemists, once 6602 WindniiiI Way, Wilmin,tmt, W- 281.05 + 910.392,07ti I ab ^ 910392.4424 Fax 710 Bowsertown Road, fvlanteo, NC 27954 ^ 252.473.5702 Lab/Pax 255-A Wilmington Highway, Jacksonville, NC 28340 • 910.347.5843 Lab/Pax ANALYTICAL & CONSULTING CHEMISTS ----- info(eieavironmtnllilchcnlists.com _. Tow.... .__.____ _._.__.._._. Town of Carolina Beach _ .__-_. Date of Repoli: Juri 07, 2019 1121 North Lake Park Blvd Customer PO #: Carolina Beach NC 28428 Customer ID: 08100295 Attention: Lisa Courtney Report#: 2019-06163 Project ID: Sludge Lab ID Sample ID: Carolina Beach WWTP Collect Date/Time Matrix Sampled by 19-15519 Site: Sludge 4/17/2019 1:00 PM Solid/Sludge Client Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method B081B/3510 <0.005mg/L 04/23/2019 Endrin(TCLP) SW 846 Method8081BI3510 <0.00005mg/L 04/23/2019 Heptachlor (TCLP) SW 846 Method30813/3510 <0.00005mg/L 04/23/2019 Heptachlor epaxide (TCLP) SW 846 Method50813/3510 <0.00005mg/L 04/23/2019 Lindane (TCLP) SW 846 Method 80813135 10 <0.00005mg/L 04/2312019 Methoxychlor(TCLP) SW 848 Method 80815/3510 <0.00005mg/L 04123/2019 Toxaphene(TCLP) SW 846 Method 8081 B/351 0 <0.005mg/L 04/2312019 1,4-Dichlorobenzene(TCLP) SW 846 method 827013510 <0.050mg/L 04/1912019 2,4,5-Trichlorophenol(TCLP) SW 846 method827013510 <0.050mg/L 04/1912019 2,4,6-Trichlorophenol(TCLP) SW 846 method827013510 <0.050mg/L 04/19/2019 2,4-Dinitrotoluene(TCLP) SW 846 method 827013510 <0.050mg/L 04/19/2019 Cresol (TCLP) SW 846 method6270f0510 <0.050mg/L 04/19/2019 Hexachloro-1,3-butadiene(TCLP) SW 846 method 827013510 <0.050mg/L 04/19/2019 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 Hexachloroethane (TCLP) SW 846 method 827013510 <0.050 mg/L 04/19/2019 m + p-Crescl (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 a -Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 Pentachlorophenol (TCLP) SW846method 827013510 <0.250mg/L 04/19/2019 Pyridine (TCLP) SW 846 method 8270/3510 <0.050mg/L 04/19/2019 2,4,5-TP(TCLP) SW846 Method 8151A <0.0003mg/L 04/23/2019 2,4-D(TCLP) SW846 Method 8151A <0.0003mg/L 04/23/2019 1, 1 -Dichloroethylene (TCLP) SW846 Method 828015030 <0.01mg/L 04/30/2019 1,2-Dichloroethane(TCLP) SW846 Method 826015030 <0.01mg/L 04/30/2019 Benzene (TCLP) SW846Method 8280i5030 <0.01mg/L 04/30/2019 Carbon Tetrachloride (TCLP) SW846 Method 820015030 <0.01 mg/L 04130/2019 Report ;a. 2019-06163 ��, �mm� �p Page 1 of 4 �ar'trs�3'� tl^ Environmental Chemists, Inc. 6602 Windmill Way, YVilnunl,lon, NC 751(,5 r y:10 3920223 Lab s 910 397 4424 Fax 710 Bowsertown Pond klanteo NC 279,54 - 252,4"35702 Lab/l . 255-A Wilmington Flighway, Jacl.somille, NC 28540 a 9103475843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCa envi ontnertuddiemists.com ._ _.._..__.-._. ._.-__.__. Town of Carolina Beach --.... .._.....___ Date of Reports Jun 07, 2019 1121 North Lake Park Blvd Customer PO #: Carolina Beach NC 28428 Customer ID: 08100295 Attention: Lisa Courtney Report#: 2019-06163 Project -ID: Sludge Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/30/2019 Chloroform (TCLP) SW846 Method 826015030 <0.01 mg/L 04/30/2019 Methyl ethyl ketone (TCLP) SW846 Method 326015030 <0.05 mg/L 04/30/2019 Tetrachloroethylene (TCLP) SW846 Method 826015030 <0.01 mg/L 04/3012019 Trichloroethylene (TCLP) SW846 Method a26015030 <0.01 mg/L 04/30/2019 Vinyl Chloride (TCLP) SW846 Method 8260;503a <0.01 mg/L 04130/2019 RCI Cyanide EPA 335,4 0.082mg/kg 04/1812019 Sulfide SM 4500 S D 50.4 mg/kg 04/19/2019 Ignitability SW 846 method 1010 >210 °F 05/08/2019 pH SW 846 Method 90450 6.90 units 04/24/2019 Sludge Residuals Aluminum EPA200.7 4190mg/kg 04/22/2019 Arsenic EPA200.7 <12.9mg/kg 04/22/2019 Cadmium EPA200.7 <12.9mg/kg 04/22/2019 Calcium EPA200.7 34600mg/kg 04/22/2019 Chromium EPA 2007 21.5mg/kg 04/22/2019 Copper EPA200.7 631 mg/kg 04/22/2019 Lead EPA 200.7 30.2 mg/kg 04/22/2019 Magnesium EPA200.7 3200mg/kg 04/22/2019 Molybdenum EPA20o.7 <12.9mg/kg 04/22/2019 Nickel EPA200.7 13.1mg/kg 0412212019 Potassium EPA200.7 1500mg/kg 04/22/2019 Selenium EPA200.7 <12.9mg/kg 04/22/2019 Sodium EPA200.7 3870mg/kg 04/22/2019 Zinc EPA200.7 906mg/kg 04/22/2019 Nitrate+ N itrite-N itrogen EPA353.2 208mg/kg 05/02/2019 Total Solids (%) SM 2540 a 4.34 % 04/18/2019 Ammonia Nitrogen SM 4500 NH3 C 2090 mg/kg 04129/2019 Total Kjeldahl Nitrogen (TKN) SM4500oryB 50800mg/kg 04/29/2019 Report#" 2019-06163��~.We.��.�o, Paget of 4� @ �� 9 ° 0 4 • ,% 6602 Windmill Ww, WdnunghnL NC 2&105 r 91II n420223 Lab 910.3924424 Fax �rr _ r � 710 B �Arsertown Road, N7anteq, NrrC 27954 a 252.47? 1i02 La:,/Fax V°�9a�, ' ��` 255-.41h'ilmingtnn Hi&.vay. Jacksonville, NC 25540 9"I.0_347.5643 Lab/Fax ANALYTICAL & CONSULTINC CHEMISTS infohi;cnviromneniillchemists.com Town of Carolina Beach Date of Report: Jun 07, 2019 1121 North Lake Park Blvd Customer PO #: Carolina Beach NC 28428 Customer ID: 08100295 Attention: Lisa Courtney Report #: 2019-06163 Project ID: Sludge Total Phosphorus SM 4500 P P 178 mg/kg 05/01/2019 Mercury SWO4674718 <0.530mg/kg 04/2212019 TCLP Metals Arsenic EPA 2001 <1.O mglL 04123/2019 Barium EPA 200,7 <1.Omg/L 04/2312019 Cadmium EPA200.7 <I.Omg/L 04/23/2019 Chromium EPA200.7 <1.Omg/L 04/23/2019 Lead EPA 200.7 <1.0 mg/L 04/23/2019 Selenium EPA200.7 <1.0mg/L 04123/2019 Silver EPA200.8 <1 mg/L 04/2312019 Mercury EPA2451 <0.0002mg/L 04/22/2019 Lab ID Sample ID: Carolina Beach WWTP Collect Date/Time Matrix Sampled by 19-15520 Site: 1 4/17/2019 1:05 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 5.01 % 04/1812019 Fecal Density SM92210EMPN 24hr503 3394MPN/g 04/1812019 Lab ID Sample ID: Carolina Beach 1NWTP Collect Date/Time Matrix Sampled by 19-15521 Site:2 4/17/2019 1:06 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids(%) SM2540G 5.29% 04/18/2019 Fecal Density SM92210EMPN 24hf503 6617MPN/g 04/18/2019 Lab ID Sample ID: Carolina Beach WWTP Collect Date/Time Matrix Sampled by 19-15522 Site: 3 4/17/2019 1:07 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 5.24 % 04118/2019 Fecal Density SM 9221C E MPN 24 hr 503 6680 MPNIg 04/18/2019 Report A..201M6163 ��..•.��.+.�•��wa,�m.�.Mr.�m,.m•.e.o. Pan 3 of Environmental Chemists, Inc. "� 0 46602 �A mdn II 11 % 1Aglminglon, NC 28405 • 910397.0223 Lab • 910.392.4424 Fes ^ y i Cii.p 71(1 Bowser town Load, Vlantco, NC 2, c 2- � 'J59 25_ }73..57021_ab /Fr1x -'.,,-;,-. W 255-A Wilmington Highway Jacksonville, NC 28540 • 910347.S843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(eenvironmeulalchemists.cnm Town of Carolina Beach Date of ReportJun 07, 2019 1121 North Lake Park Blvd Customer PO #: Carolina Beach NC 28428 Customer ID: 08100295 Attention: Lisa Courtney Report #: 201B-06163 Project ID: Sludge Lab ID Sample ID: Carolina Beach WWTP Collect DatelTime Matrix Sampled by 19-15523 Site: 4 4/17/2019 1:08 PM Solid/Sludge Client Test Method Results Date Analvzed Total Solids (%) SM 2540 G 5.03 % 04/18/2019 Fecal Density SM 9221C E MPN 24 hr 503 6959 MPN/g 04118/2019 Lab ID Sample ID: Carolina Beach WWTP Collect Date/Time Matrix Sampled by 19-15524 Site: 5 4/17/2019 1:09 PM Solid/Sludge Client Test Method Results Date Ana Total Solids (%) SM 2540 G 4.52 % 04/18/2019 Fecal Density SM 9221 C E MPN 24 hr 503 11947MPN/g 04/18/2019 Lab ID Sample ID: Carolina Beach WWTP Collect Date/Time Matrix Sampled by 19-15525 Site: 6 4/17/2019 1:10 PM Solid/Sludge Client Test Method Results Date Total Solids (%) SM2540G 4.42% 04/18/2019 Fecal Density SM92210EMPN 24hr503 3847MPN/g 04/18/2019 Lab ID Sample ID: Carolina Beach WWTP Collect Date/Time Matrix Sampled by 19-15526 Site:7 4/17/2019 1:11 PM Solid/Sludge Client Test Total Solids (%) Fecal Density Comment: Reviewed by: Method SM 2540 G SM 9221 C E MPN 24 hr 503 Results 4.66 % 5151 MPN/g Date 04/18/2019 04/18/2019 Report:'.. 2019-06163w..e,.-.m.......e.:.�m,=..r,m..,�.s..,.�...�..n..�...n.,.._—__— _ ,........n,...,....�____-.aa�a 4nrn .ems ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTPName: CarolinaBeach WWTP NPDESNumber: NCO023256 Monitoring Period: From 1/1/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed: Class A: Alt. A (time/tern) ❑ TAIt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) Indicate "Process to Further Reduce Pathogens": Compost ❑T Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ , .:: Class B: I Alt. (1) Fecal Density El Alt. (2) Process to Si cautly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to S' cantly Reduce Pathogens": Lime Stabilization ❑ Air Dr ❑ Composting ❑ Aerobic Di estion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge 8 Pathogen Density um er o Excee- Frequency of Anal c s Y Sample p Type na y—u Tech- nialle inimu Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 3,394 5,894 11,947 MPN/g 0 Annual Grab SM92210E CFU 1000 mpn per gram of total solid (dry wei t Salmonella bacteria (in lieu of fecal colifonn) 3 Ma per 4 grams [oral solid (dry weight) Vector Attraction teduction (1m NC:AC UZU .1107) - Please indicate alternative nerformed: Att.l (VS reduction) 7TFAlt. 2 (40-day bench) ❑ JAR. 3 (30-day bench) ❑ Alt. 4 (Spec. 0, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Alk. Stabilization ❑ JAR 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) Ej jAlt. 10 (Incorporation) El jNo vector attraction reduction alternatives were erformed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note If you check this statement attach an explanation why you have not met one or both of the has been made under my system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." William Raymond, ORC Wesley Wooten, President Preparer Name and Title (ty e or print) land Applier Name and Title (if applicable)(type or print) Zi i �-?q-Z020 1/24/20 Si cure ofl epar Date Signature of and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Carolina Beach W WTP Date Fecal Coliform MPN per grain Log 04/17/19 3,394 3.5307 04/17/19 6,617 3.8207 04/17/19 6,680 3.8248 04/17/19 6,959 3.8425 04/17/19 11,947 4.0773 04/17/19 3,847 3.5851 04/17/19 5,151 3.7119 Total 26.3930 Average 3.7704 Geometric Mean 5,894 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 5, 2019 Morehead Citv 23.50 % Solids 6.63 off Permit No. NCO026611 Parameter % Mg/Kg DryWeight (% x 10,000) Pounds/DryToo (MMISgI 0.002 Nitrogen (TKN) 6.070 60,700.000 121.400 Phos horns 3.050 30,500.000 61.000 Potassium 0.552 5,520.000 11.040 PAN (injected)* 1.912 3,869.500 7.739 PAN (surface)* 1.848 3,777.000 7.554 Ammonia Nitrogen 0.127 1,270.000 2.540 Calcium 3.260 32,600.000 65.200 Calcium Carbonate E . -- Magnesium 0.538 5,380.000 10.760 Sodium 0.480 4,800.000 9.600 Sulfur Nitrate N / Nitrite N --- 18.000 0.036 Barium Chloride --- --- -- Iron --- --- --- Aluminum 12,500.00 25.000 Arsenic 9.86 0.020 Cadmium --- 3.52 0.007 Chromium --- 15.500 Copper 743.00 1,486 Lead --- 15.50 0.031 Mercury 0.739 0.001 Molybdenum - 4.38 0.009 Nickel 12.40 0.025 Selenium 5.69 0.011 Zinc --- 935.00 1.870 Environmental Chemists, Inc. 2019-03581 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN SAR 3.14 Ceiling Concen. (MPJK¢) 75 85 4,300 840 Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. 4��, r 1 4s k .. �F; ANALYTICAL & CONSULTING CHEMISTS Town Of Morehead City 706 Arendell Street Morehead City NC 28557 Attention: C Sutton Lab ID Sample ID: 19-09034 Site: class b sludge Test Environmental Chemists, Inc. ,e002 W)rdmill Wav, Wilm:ngl,nt. Nt- 24105 9C1.39' 0-129 Lab JIQ.392.4d24 Fi;� 710 13(n%ser ,�, n Road, elan' ^ - )i].-t'3_:Q Lab, Fax a. _-A 4^,'ibn,ng[un Highn ar, Ja..ia nx tl c, NC 28540 910.4 84l Lab; Fax Method i nli,�it. �• dctro i int:n,eleltemsti.ta�m Revised Report: Apr 29. 2019 Original Report Date: Apr 3. 2019 Report #: 2019-03581 Customer ID: 09020011 Project ID: Sludge Collect Date/Time Matrix Sampled by 3/5/2019 10:30 AM Solid/Sludge C. Sutton/N. Johnson Results . Date Analyzed CCE AOAC 1 005 <1 % 04/16/2019 Chlordane (TCLP) SW B45 Method 8081813510 <0.02 mg/L 03/06/2019 Endrin (TCLP) SW 846method BOB 1B13510 <0.0005mg/L 03/06/2019 Heptachlor (TCLP) SW 846 Method 5081 B1351 0 <0.0005mg/L 03/0612019 Heptachlor epoxide (TCLP) SW 846 Method80B1B/3510 <0.0005mg/L 03/06/2019 Llndene(TCLP) SW 846 Method 8081 B/3510 <0.0005mg/L 03/0612019 Methoxychlor (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 03/0612019 Toxaphene (TCLP) SW 846 Method 8081BI3510 <0.05 mg/L 03/0612019 1,4-Dichlorobenzene (TCLP) SW 846 method B27Oi3510 <0 050 mg/L 03/07/2019 2,4,5-Trichlorophenol (TCLP) SW 848method 0270;3510 <0.050 mg/L 03/07/2019 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/07/2019 2,4-Dinitrotoluene (TCLP) SW 846 method 8270,'3510 <0.050 mg/L 03/07/2019 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/07/2019 Hexachlom-1,3-butadiene(TCLP) SW 846 method027013510 <0.050mg/L 03/07/2019 Hexachlorobenzene (TCLP) SW 846 method B270/3510 <0.050 mg/L 03/0712019 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/07/2019 rn + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/07/2019 Nitrobenzene (TCLP) SW 846 method 827Oi3510 <0.050 mg/L 03107/2019 o-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 03/0712019 Pentachlorophenol (TCLP) SW 846 method 0270/3510 <0.250 mg/L 03/07/2019 Pyridine (TCLP) SW B46 method B27013510 <0.050 mg/L 0310712019 pH SW 846 Method 90450 6.63 units 03/20/2019 Paint Filter Test SW 846 Method 9095 A pass 03/18/2019 2,4,5-TP(TCLP) SWB46Method 8151A <0.003mg/L 03/11/2019 2,4-D(TCLP) SW846Method 8151A <0.003mg/L 03/1112019 1,1-Dichloroethylene(TCLP) SW846 Method 828015030 <0.01mg/L 03/13/2019 Report A:. 2019-03581 ��^•-,mum-�6 p Page 1 of 5 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc, 6 t 1 �%'ind InlII MAY. 1Vih idogton, 't 2t,10� n 91939 0173L b 910.3924424 Fax 'IU li,%,:ututctt P r Rtmteo NC.2795 t 252 47, vU tb Tax � A t"i I Inl gton Hilht a s, Jackson tlii, NC 2� 411 + 9 W.''4, .;84 Lab, Fax i n l �>4 gctn' I n n min Ittic hint i 51 a. cunt Town Of Morehead City 706 Arendell Street Morehead City NC 28557 Attention: C. Sutton Revised Report: Apr 29, 2019 Original Report Date: Apr 3. 2019 Report#: 2019-03581 Customer ID: 09020011 Project ID; Sludge 1,2-Dichloroethane(TCLP) SW846Method a250/5030 <0.01mg/L 03113/2019 Benzene (TCLP) SW846 Melhod 826015030 <0.01 mg/L 03113/2019 Carbon Tetrachloride (TCLP) SW846 Method B26015030 <0.01 mg/L 03/13/2019 Chlorobenzene (TCLP) Sw846 Method 826015030 <0.01 mg/L 0311312019 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/13/2019 Methyl ethyl ketone (TCLP) SW846 Method 826W5030 0.06mg/L 03/13/2019 Tetrachloroethylene(TCLP) SW846 Method 8260/5030 <0.01mg/L 03/13/2019 Trichloroethylene(TCLP) SW846 Method 826015030 <0,01mg/L 03/13/2019 Vinyl Chloride (TCLP) SW840 Method 8260/5030 <0.01 mg/L 03/13/2019 RCI Ignitability EPA 1030 <0.8 mm/sec 03/1812019 Cyanide EPA 3354 4.29mg/kg 03/13/2019 Sulfide SM 4500 S D 0.72 mg/kg 0311312019 Sludge Residuals Aluminum EPA 2007 12500mg/kg 03/08/2019 Arsenic EPA 2007 9.86mg/kg 03/0812019 Cadmium EPA 2007 <3.52mg/kg 03/08/2019 Calcium EPA 200,7 32600mg/kg 03/07/2019 Chromium EPA 2007 15.5mg/kg 03/08/2019 Copper EPA2007 743mg/kg 03/0812019 Lead EPA 200-7 15.5 mq/kg 03/08/2019 Magnesium EPA200.7 5380mg/kg 03/07/2019 Molybdenum EPA200.7 4.38mg/kg 03/08/2019 Nickel EPA200.7 12.4mg/kg 03/0812019 Potassium EPA 2007 5520mg/kg 03/07/2019 Selenium EPA 2007 5.69mg/kg 03/08/2019 Sodium EPA 2007 4800mg/kg 03/07/2019 Zinc EPA 200 7 935 mg/kg 0310812019 Nitrate+Nitrite-Nitrogen EPA353.2 18.0mg/kg 03/25/2019 Report d- 2019-03581 - _—.,........-.o...,.�...w.......�.t...,..,.>,..., Page 2 of 5 '7 ANALYTICAL & CONSULTING CHEMISTS Town Of Morehead City 706 Arendell Street Morehead City NC Attention: C. Sutton Total Solids (%) Ammonia Nitrogen Total Kjeldahl Nitrogen (TKN) Total Phosphorus Mercug Repeated to verify. TCLP Metals Arsenic Barium Cadmium Chromium Lead Selenium Silver Mercury Lab ID Sample ID: 19-09035 Site:1 Test Environmental Chemists, Irw. C602 Rrd:nill tvw 4Ltt.ui fuACYI0. 7ii;10'>3Lob 9103'L-1424Fa\ :'12 R. eai ;ull n Road, \tanieo, ^. C ?; 15a .. 4 0 L,tb F.a 25$_q Mm in;fun Hi,lghurMc. NC'�;40 • 910.347 841 Lab/Pa>. iaio�:<;ettvn;etmcttt:ilchrnusl: cum Revised Report: Apr 29, 2019 Original Report Date: Apr 3, 2019 28557 Report #: 2019-03581 Customer ID: 09020011 Project ID: Sludge SM 2540 a 23.5 % 03/06/2019 SNI 4500 NH3 c 1270 mg/kg 03/14/2019 SM 4500 Ofg a 60700 mglkg 03/11/2019 SM 4500 P F 30500 mg/kg 03/1912019 SW8457471B 0.7390mg/kg 03/17/2019 EPA 20C 7 <1.0 mg/L 03/18/2019 EPA 200.7 <1.0 mg/L 03/18/2019 EPA 200.7 <1.Omg/L 03/18/2019 EPA 200 7 <1.0 mg/L 03/18/2019 EPA 2007 <1.0 mg/L 03/18/2019 EPA 2007 <1.0mg/L 03118/2019 EPA 200 7 <1.0 mg/L 03/18/2019 EPA 245.1 <0.0002 mg/L 03/1012019 Collect Date/Time Matrix Sampled by 3/5/2019 10:40 AM Solid/Sludge C Sutton/N. Johnson Method Results Date Analvzec Total Solids (%) sM 2540 G 20.7 % 03/06/2019 Fecal Density SM92210EMPN24hr503 8209MPN/g 03/06/2019 Lab ID Sample ID: u Collect Date/Time Matrix Sampled by 19-09036 Site: 2 3/5/2019 10:42 AM Solid/Sludge C. Sutton/N. Johnson Test Method Results Date Analyzed Total Solids(%) SM2540G 20.7% 03/06/2019 Fecal Density SM 9221C E MPN 24 hr 503 6287 MPN/g 03/0612019 P.epart At 2019-03581 Page 0 of 5 Environmental Chemists, Inc. f'6014Ilid nitll k1 aV N'.; ngtrm, \'(_ 25405 - 910u- U 27 Lab 9 [0 302,=114 1`ar ,♦yy. 1 7I0 Prnvnertu, n Road, Menlo,), NC 27951 252 1" 3 5702 Lab/Fix ss' °i5�,a 4\'ibninnhm Hi�hurm', Jacksun� illu. hrC 2R5 F0 910,1475843 Lab,'Faa ANALYTICAL & CONSULTING CHEMISTS infeiukm imnmen:alchcmistseom Town Of Morehead City 706 Arendell Street Morehead City NC Attention: C. Sutton Lab ID Sample ID: 19-09037 Site:3 Test Total Solids (%) Fecal Density Lab ID Sample ID: 19-09038 Site:4 Test Total Solids (%) Fecal Density Revised Report: Apr 29. 2019 Original Report Date: Apr 3, 2019 28557 Report #: 2019-03581 Customer ID: 09020011 Project ID; Sludge Collect Date/Time Matrix Sampled by 3/5/2019 10:44 AM Solid/Sludge C. Sutton/N. Johnson Method Results Date Anal SM 2540 G 22.0 % 03/06/2019 SM 9221C E MPN 24 hr 503 4989 MPN/g 03/06/2019 Collect Date/Time Matrix Sampled by 3/5/2019 10:46 AM Solid/Sludge C. Sutton/N. Johnson Method Results Date Analyzed SM 2540 G SM 9221C E MPN 24 hr 503 22.4 % 0310612019 2051 MPN/g 03/06/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-09039 Site: 5 315/2019 10:48 AM Solid/Sludge C. Sutton/N, Johnson Test Method Results Date Analyzed Total Solids (%) sM 2540 G 20.1 % 03/06/2019 Fecal Density SM 9221C E MPN 24 hr 503 2435MPN/g 03/06/2019 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 19-09040 Site: 6 3/5/2019 10:30 AM Solid/Sludge C. Sutton/N. Johnson Test Method Results Date Analyzed Total Solids (%) SM 2540 G 22.6 % 03/06/2019 Fecal Density SM 9221C E MPN 24 hr 503 3499 MPN/g 03/06/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-09041 Site: 7 3/5/2019 %32 AM Solid/Sludge C. Sutton/N. Johnson Test Method Results Date Analyzed Total Solids (%) SM2540G 24.1 % 03/0612019 Fecal Density SM92210EMI N 24hr503 2037MPNIg 03/06/2019 Report 8 2019-03581 Page 4 of 5 ANALYTICAL & CONSULTING CHEMtIS16 Environmental Chemists, Ine. V-ol Windmill MI 4Vi61nt I r 14(: �S"0 1fL0 2022 Lab uW39 4421Fax 710 Sawe 0,m it [ u i l V. .i i nL 27954 251. t7-15702 Late; Fa% 25 A PVi l in in�ton H+lh. IJu l.a;1%IIle, NC'v-ln 911.47;844I-ahiFnx n lc,a e, ici runmen; alchem i;lsrant Town Of Morehead City Revised Report: Apr 29, 2019 706 Arendell Street Original Report Date: Apr 3, 2019 Morehead City NC 28557 Report#: 2019-03581 Attention: C. Sutton Customer ID: 09020011 Project ID: Sludge Comment: Sludge residuals reported on a dry weight basis. Revised to include calium carbonate equivalence. Reviewed by: I ReportP� 2019-0..581 Page 5 of 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 W WTP Name: Town of Morehead City NPDES Number: NCO026611 Monitoring Period: From 1/l/2019 To 12/3112019 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alterntive 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) in`Process to Furtber Reduce Pathogens": Compost El Heat Drying ❑ Heat Treatment ❑ Thenuo hilic ❑ Beta Ra ❑ L=Ginnma Ray ❑ Pasteurization ❑ Class B: I Alternative I O Alterative 2 ❑ If applicable to alternative performed (Class B only) indicate `Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Dtyio ❑ Com rosting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in SludgeMinimu Pathogen Density g y um er o Excee- dmges Frequency of Analysis Sample Type na ytica Tech - ninue Geo. Mean Maximu Units Coliform 2 x i 0 to the 6th power per gram of total solids MPN 2,037 3,681 8,209 MPNI g 0 Annual Grab sM 9221CL' CPU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal celiform) 3 MAN per 4 grams total solid (di y weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: AIM (VS reduction) ❑ Alt, 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ 1 Alt. 6 (Alk. Stabilization ❑ 1 Alt 7 (Drying -Stable) ❑ jAh. 8 (Drying - Unstable) ❑ AIt. 9 (Injection) ❑ Alt. 10 (Incorporation) E7 INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Rl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met" (Please [rote if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Chad Sutton, WWTP Superintendent Wesley Wooten, President PreparerNam and Ti a ype or print) Land Applier/Name and Title (if applicable)(type or print) 4/5/19 Signatur of Preparer* Date Signature of Lan Applies (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Morehead City WWTP Date Fecal Coliform MPN per gram Log 03/05/19 8,209 3.9143 03/05/19 6,287 3.7984 03/05/19 4,989 3.6980 03/05/19 2,051 3.3120 03/05/19 2,435 3.3865 03/05/19 3,499 3.5439 03/05/19 2,037 3.3090 Total 24.9621 Average 3.5660 Geometric Mean 3,681 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 10, 2019 Northwest Regional WRP Permit No. WQ0034367 1.50 % Solids 4.75 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds%Dry'I'on (Mg/Kg(Mg/Kg x 0.002) Nitrogen (TKN) 2.140 21,400.000 42.800 Phosphorus 0.001 6.500 0.013 Potassium 0.424 4 240.000 8.480 PAN (injected)* 0,886 8,862.000 17-724 PAN (surface)* 0.724 7,242,000 14.484 Ammonia Nitrogen 0.324 3,240.000 6.480 Calcium 1.330 13,300.000 26.600 Calcium Carbonate E . --- Magnesium 2,030.000 4.060 Sodium 8.130.000 16.260 Sulfur ___ ___ Nitrate N / Nitrite N --- 174.000 0.348 Barium Chloride ___ --- __ -- __ SAR 2.12 Iron -- --- - Ceiling Concen. Aluminum --- 9,730.00 19.460 M /K Arsenic 24.50 0.049 75 Cadmium --- 24.50 0.049 85 Chromium --- 24.500 --- -- Copper 103.00 0.206 4,300 Lead --- 24.50 0.049 840 Mercury 1.330 0.003 57 Molybdenum 24.50 0.049 75 Nickel 24.50 0.049 420 Selenium 24.50 0.049 100 Zinc 385.00 0.770 7500 11 Environmental Chemists # 2019-05822 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0,5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910) 389-8511 June 03, 2019 Mark Young Northwest RWRF 189 Mills Field Rd. Richlands, NC 28574 RE: NW Solids Enclosed are the results of analyses for samples received by our laboratory on 4/10/2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, c 'J (J Vi f r ' 44d Todd A. Roberts For Mark Young Northwest ORC C1i ONWASA Northwest RWRF Project: NW Solids 189 Mills Field Rd. Project Number: Reported; Richlands, NC 28574 Project Manager: Mark Young 06/03/2019 10:43 Sample Results Data Analyzed by: Environmental Chemists, Inc. Sample: NW Fecal # 1 N191531-01 (WW) 04/10/2019 09:20 Digestor Sludge Reporting Date Analyst Analyth Result Qual Limit Units Analyzed Initials Method -: Fecal Density', 1504 MPN/9 04/11/2017 ;GSM 9221C E MPN ,. 241r 503 ._. Total Solids (%) 1.33 % 04/11/2017 SM 2540 G Sample: NW Fecal # 2 N191531-02 (WW) 04/10/2019 09:21 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method Fecal Density < 1344 MPN/9 04/11p61 221C Y 4 503 ' Total Solids (%) 1.34 % 04/11/2017 SM 2540 G Sample: NW Fecal # 3 N191531-03 (WW) 04/10/2019 09:22 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method MPN/g 04/11/2017 SM 9221C E MPN 2ghr SQ3 Total Solids (%) 1.32 % 04/11/2017 SM 2510 G Sample: NW Fecal # 4 N191531-04 (WW) 04/10/2019 09:23 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed initials Method Fenl:Density 1527 MPN/9 04/1112017 SM 9227C E MPN Total Solids (%) 1.31 % 04/11/2017 SM 2540 G Sample: NW Fecal # 5 N191531-05 (WW) 04/10/2019 09:24 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed initials Method Feral DereiN z < 1056 MPN/g j 04/112017 SM 9221C E MPN ZlIX593 Total Solids (°/a) 0.97 04/11/2017 SM 2540 G The ronrenm ofMis me t apply fa Me mmpWs) analyzed in a tolz reWM dre chain Ofmx( document No dupGradm°fthis MX4 s aibn ,, errept in& mbmly. Page 2 of C® ONWASA Northwest RWRF Project: NW Solids 189 Mills Field Rd. Project Number: Reported: Richlands, NC 28574 Project Manager: Mark Young 06/03/2019 10:43 Sample Results (Continued) Data Analyzed by: Environmental Chemists, Inc. Sample: NW Fecal # 6 N191531-06 (WW) Digestor Sludge 04/10/2019 09:25 Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method Fecal Density A. - 1291 ak SM 9221C E MPN l 2jtw SP3 Total Solids (%) 1.55 % 04/1i�/2017 SM 2540 G Sample: NW Fecal # 7 N191531-07 (WW) 04/10/2019 09:26 Digestor Sludge Reporting Date Analyst Analyte Result Qual Unnit Units Analyzed Initials Method Fecat Density l 1600 MPN/9 041U_ Total Solids (0/6) 1.25 % 04/11/2017 SM 2540 G The contents Of thS&WtBPP1Y 0 the amPk(s) am&in as a� wffi Me ohwa of cmtody LYocvmnt ft dplk,� ofo,, �& k; 8/�, Wpt,�,& �,,Wy. Page 3 of 8 C� ONWASA Northwest RWRF Project: NW Solids 189 Mills Feld Rd. Project Number: Reported: Richlands, NC 28574 Project Manager: Mark Young 06/03/2019 10:43 Sample Results (Continued) Data Analyzed by: Environmental Chemists, Inc. Sample: NW Digestor A N191531-08 (SL) 04/10/2019 09:20 1lgestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method Aluminum 973n Ammonia-N 3240 mg/Kg 04/19/2019 SM 4500 NH3 C Arsenic - <24.5 mg/Kg 04/1912019 EPA 209J Calcium 13300 mg/Kg 01/19/2019 EPA 200.7 Cadmium <21.5 mg/Kg 0Q139/2019 EPA 200.7 Cyanide <0.025 0.025 m9/Kg 04/19/2019 EPA 335.4 Chromium <24.5 mg/Kg 04/12019 EPA 200.7 Copper 103 mg/Kg 09/19/2019 EPA 200.7 Mercury <0,0002 0.0002 mg/L 04/19/2019 EPA 245.1 Mercury <1.33 mg/Kg 04/19/2019 SW8967471B Ignitability NR deg F 04/19/2019 SW8161010 Potassium 4240 mg/Kg 04/19/2019 EPA 200.7 Magnesium 2030 mg/4 04/19/2019 EPA 200.7 Molybdenum < 24.5 mg/Kg 04/19/2019 EPA 200.7 Sodium 33 E0 mg/Kg 09f19/2019 EPA 200.7 Nickel < 24.5 mg/Kg 04/19/2019 EPA 200.7 Nitrate+,Nitrite-Nitrogen 174 mg/Kg 09/1912019 EPA 353.2 Lead < 24.5 mg/Kg 04/19/2019 EPA 200.7 PH 4.74 pH Unlls 04/19/2019 SM 4500 H B Selenium < 24.5 mg/Kg 09/19/2019 EPA 20000 .7 Sulfide NR ng/,K9 09/19f2019 SM 4500 S D Chlordane <0.005 0.005 mg/L 04/19/2019 SW8468081B/3510 Endrin <0.00005 Se-005 mg/L 0411W20,19 SW84680816f3510 Heptachlor <0.00005 5e-005 mg/L 04/19/2019 SW84680816/3510 Heptachlor epoxide -- < 0,00005 _ Se-005 mgL 09/19/2019 - SW89680818(3S10 Linda. <0.00005 Se-OOS mg/L 04/19/2019 SW8168081B/3510 Methoxychlor <0.00005 5e-005 mg/L 04(19/2019. SW8968081k33S10 Toxaphene < 0.005 0.005 mg/L 04/19/2019 SW846 80818/3510 _ 1,4-Dichlombenzen, <0.050 0,05 mg/L SW8468270/3510 2,4,5-Trichlorophenol <0.050 0.05 mg/L 04/19/2019 SW8468270/3510 2,4,6-Trichorophend <0.050 0.05 m9A 04/1912019 SW8468270/3510 2,4-Dinitrotoluene <0.050 0.05 mg/L 01/19/2019 SW8168270/3510 Cresol <0.050 0.05 M94 04/19(2019 SW8468270/3510 Hexachloro-1,3-butadiene <0.050 0.05 mg/L 04/19/2019 SW846 6270/3510 Hexachlorobenzene <0.050 0.05 TWL 09/19/2019 SW8468270/3SIO Hexachloroethane <0.050 0.05 mg/L 09/19/2019 SW8468270/3510 m+p-Cresol <0.050 0.05 mg/L 04p9/2019 5W8468270/3510 Nitrobenzene <0.050 0.05 mg/L 04/19/20119 SW8468270/3510 o-Gesal <0.050 00.5 m91L 04/19/20}9 SW8168279t35ID Pentachlorophenol <0.250 0.25 mg/L 04/19/2019 SW8468270/3510 Pyridine - < 0.050 0.05 mg/1- 04/19/2019 SW846 82700510 2,9,5-7P < 0.0003 0.0003 mg/L 04/19/2019 SW846 8151A 2,4-D <0.0003 0.0003 mg/L 09/19(2019 SW8968151A 1,1-DichloroeNylene <0.01 0.01 mg/L 04/19/2019 SW8468260/5030 themnzenm ofthis niiq,rappiy zo the sampie(s) aoi,4 din econianre with Me chain ofnrsrody document Ab dup/iraddl ofthu report is aibw ,, e¢epf o io, enf4ely. Page 4 of 8 C® ONWASA 4orthwest RWRF Project: NW Solids t89 Mills Field Rd. Project Number: Reported: tichlands, NC 28574 Project Manager: Mark Young 06/03/2019 10:43 Sample Results (Continued) Data Analyzed by: Environmental Chemists, Inc. Sample: NW Digestor A (Continued) N191531-08 (SQ 04/10/2019 09:20 Igestor Sludge Reporting Date Analyst Analyse Result Qual Limit Units Analyzed Initials Method 1,2-Dichicioethane <0.01 001 ..,,.n „°11,,.1- ,,..,.._..,.. Benzene <0.01 0.01 mg/L 04/19/2019 SW8468260/5030 Carbon Tetrachloride <0.01 0:01 mg/L 04MI2019, SW846826050 mg/L 04/19/2019 _ SW846 8260/5030 Chloroform <0.01 0.01 vig/L 04/1912019 SW846826015130 Methyl ethyl ketone <0.01 0.05 mg/L 04/19/2019 5W8168260/5030 Tetrachloroethylene <0.01 0.01 mg/L 04/19/2019 SW8468260/5030 TnchlorceNylene < 0.01 0.01 mg/L 04/19/2019 SW846 8260/5030 Vinyl Chloride <0.01 0.01 mg(L 04/1W2019 SWB46826_D/5030 Arsenic < 1.0 1 mg/L 04/19/2019 EPA 200.7 . Barium < SA 1 mg/L 04/19/2019 EPA 200.7 Cadmium < 1.0 1 mg/L 04/19/2019 EPA 200.7 Chromium < 1.0 1 mg/L 04/19/2019 EPA 200.7 Lead < 1.0 1 mg/L 04/19/2019 EPA 200.7 Selenium < 1.0 1 m9/1 01119(2019 EPA 200.7 Silver < 1.0 1 mg/L 04/19/2019 EPA 200.7 Total_Kjeldahl Nitrogen 21460 mg/Kg 04/19/2019 EPA 351.2 Phosphorus, total Sludge 6.5 mg/Kg 04/19/2019 SM 4500 P E Total Solitls (°/J 1.5 % 04/19/2019 SM 2549 G Zinc 385 mg/Kg 04/19/2019 EPA 200.7 The mntents afrbls My apply to the sampk(s) ane*y - a aMa rv/M Ne ohain ofcvsmCy document. NO Cuplir Wn ofmis ep dBa/kwed, except In in entirety. Page 5 of 8 6 ONWASA Northwest RWRF Project: NW Solids 189 Mills Feld Rd. Project Number: Reported: Richlands, NC 28574 Project Manager: Mark Young 06/03/2019 10:43 Notes and Definitions Dry Sample results reported on a dry weight basls. NO Analyte NOT DETECTED at or above the reporting limit Ilse roMentr olMis repwtapp/yro Mesampk(s)anwnayacM/n attvrdanre wM MedWn of[ust da=.t.. NO dUP/!mh'On of MlS rewrf Is allow ,, mtWm&wfir . Page 6 of 8 Environmental Chemists, Inc. iL 1 ' 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax ® 710 Bowsertown Road, Ivtanteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@envimnmentalchemistscom Onslow Water & Sewer Authority Date of Report: May 15, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2019-05822 -----._..- --. -- - - Project ID: Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-14622 Site: Digester 4/10/2019 9:20 AM Solid/Sludge Client Test Method Results Date Chlordane (TCLP) SW 846 Method 8081 B1351 0 <0.02 mg/L 04123/2019 Endrin (TCLP) SW846 Method 809113/3510 <0.0005 mg/L 04/23/2019 Heptachlor (TCLP) SW846 Method8081BI3510 <0.0005mg/L 04123/2019 Heptachlor epoxide (TCLP) SW846 Method 8081B/3510 <0.0005 mg/L 04/23/2019 Lindane (TCLP) SW846 Method 8081B/3510 <0.0005 mg/L 04/23/2019 Methoxychlor (TCLP) SW846 Method 80818/361a <0.0005 mg/L 04/23/2019 Toxaphene (TCLP) SW846 Method 8081RI3610 <0.05 mg/L 04/23/2019 1,4-Dichlorobenzene(TCLP) SW 846 method 8270/3510 <0.050mg/L 04/19/2019 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 2,4-Dinitrotoluene (TCLP) SW 840 method 827013510 <0,050 mg/L 04/19/2019 Cresol (TCLP) SW 846 method 82-10/351a <0.050 mg/L 0411912019 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 m + p-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 04/19/2019 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 04119/2019 o-Cresol (TCLP) SW Us method 827013510 <0.050 mg/L 04/1912019 Pentachlorophenol (TCLP) SW 846 method 827013510 <0.250 mg/L 04/19/2019 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/19/2019 2,4,5-TP (TCLP) SW046 Method 8151A <0.003 mg/L 04/23/2019 2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 04/23/2019 1,1-Dichloroethylene(TCLP) SW846 Method826015030 <0.01mg/L 04/22/2019 1,2-Dichloroethane(TCLP) SW846 Method8280/5030 <0.01mg/L 04/22/2019 Benzene (TCLP) SW846 Method8260/5030 <0.01 mg/L 04/22/2019 Carbon Tetrachloride (TCLP) SW846 Method8260/5030 <0.01 mg/L 04/22/2019 Report #-. 2019-05822 Page 1 of 4 Environmental Chemists, Inc. mo_ 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab > 910.392.4424 Fax 710 Sowsertown Road, Manteo, NC 279,94 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS into@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: May 15, 2019 228 Georgetown Road Customer PO M Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report M 2019-05822 -- ------------ ------Project ID: Chlorobenzene(TCLP) SW846 Method 826015030 <0.01mg/L 04/22/2019 Chloroform (TCLP) SW846 Method 826015030 <0.01 mg/L 04/22/2019 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05mg/L 04/22/2019 Tetrachloroethylene(TCLP) SW846 Method 626015030 <0.01mg/L 04/22/2019 Trichloroethylene (TCLP) SW046 Method 8260/5030 <0.01 mg/L 04/22/2019 Vinyl Chloride (TCLP) SW046 Method 8260/5030 <0.01 mg/L 04/22/2019 Sludge Residuals Aluminum EPA 200.7 9730mg/kg 04/1512019 Arsenic EPA200.7 <24.5mg/kg 04/15/2019 Cadmium EPA 200.7 <24.5mg/kg 04/15/2019 Calcium EPA 200.7 13300mg/kg 04/15/2019 Chromium EPA 200.7 <24.5mg/kg 04/15/2019 Copper EPA 200.7 103mg/kg 04116/2019 Lead EPA 200.7 <24.5 mg/kg 04/15/2019 Magnesium EPA200.7 2030mg/kg 04/15/2019 Molybdenum EPA 200.7 <24.5mg/kg 04/15/2019 Nickel EPA200.7 <24.5mg/kg 04/15/2019 Potassium EPA 200.7 4240mg/kg 04/16/2019 Selenium EPA 200.7 <24.5 mg/kg 04115/2019 Sodium EPA20o.7 8130mg/kg 04116/2019 Zinc EPA 200.7 385mg/kg 04/15/2019 Nitrate+ Nitrite-N itrogen EPA353.2 174mg/kg 05/02/2019 Total Solids (%) SM 2540 B 1.50 % 04/11/2019 pH SM 4500 H B 4.75 units 04115/2019 Ammonia Nitrogen SM4500NH3 C 3240mg/kg 04/16/2019 Total Kjeldahl Nitrogen (TKN) SM4600orgB 21400mg/kg 04115/2019 Total Phosphorus SM4500PF 6.50mg/kg 04/25/2019 Mercury SW8467471B <1.33mg/kg 04/12/2019 TCLP Metals Arsenic EPA 200.7 <1.Omg/L 04/23/2019 Report #:: 2018-05322 Page 2 of 4 Environmental Chemists, Inc. 4 / / 1 6602 Windmill Way, Wilmington, NC 28405 ^ 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M. 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info ,)environmentalchen»sts.com Onslow Water & Sewer Authority Date of Report: May 15, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2019-05822 Project l_D_ , Barium EPA 200.7 <1.0 mg/L 04/23/2019 Cadmium EPA200.7 <1.0mg/L 04/23/2019 Chromium EPA200.7 <1.0mg/L 04/23/2019 Lead EPA 200.7 <1.0 mg/L 04/23/2019 Selenium EPA200.7 <1.0mg/L 04/23/2019 Silver EPA200.8 <1 mg/L 04/23/2019 Mercury EPA245.1 <0.0002mg/L 04/22/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-14624 Site: 001 4/10/2019 9:20 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) Fecal Density SM 2540 G SM92210EMPN24hr503 1.33 % 1504MPN/g 04/11/2019 04/11/2019 Lab ID Sample ID: Collect Date[Time Matrix Sampled by 19-14625 Site: 002 4/10/2019 9:21 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids(%) SM2540G 1.34% 04/11/2019 Fecal Density SM92210EMPN 24hr503 <1344MPN/g 04111/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-14626 Site:003 4/10/2019 9:22 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 1.32 % 04111/2019 Fecal Density SM92210EMPN 24hr503 1516MPN/g 04/11/2019 Lab ID Sample ID: 19-14627 Site:004 Test Method Collect Date/Time 4/10/2019 9:23 AM Matrix Sampled by Solid/Sludge Client Results Date Total Solids (%) SM2540G 1.31 % 04/11/2019 Fecal Density SM 9221C E MPN 24 hr503 1527 MPN/g 04111/2019 capon 4:: 2019-05822 Page 3 of 4 Environmental Chemists, Inc. 8 6602 Windmill Way, Wilmington, NC 28405 < 910.392.0223 Lab ^ 910.392.4424 Fax _sM1i_ 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS iiifo@enviroiimentaiGheniists.com environmentaichenrists.com Onslow Water & Sewer Authority Date of Report: May 15, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2019-05822 Project ID_ Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-14628 Site: 005 4/10/2019 9:24 AM Solid/Sludge Client Test Total Solids (%) Fecal Density Method SM 2540 G SM 9221C EMPN 24 hr 503 Results & 97 % <1856 MPN/g Date Analyzec 04/11/2019 04/11/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-14629 Site: 006 4/10/2019 9:25 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM2540G 1.55% 04/11/2019 Fecal Density SM92210EMPN 24hr503 1291 MPN/q 04/11/2019 Lab ID Sample ID: 19-14630 Site:007 Test Total Solids (%) Fecal Density Collect Date/Time Matrix 4/10/2019 9:26 AM Solid/Sludge Method SM 2540 G SM 9221C E MPN 24 hr 503 Comment: Sludge residuals reported on a dry weight basis. K Reviewed by: -tI Ow oQ.Q,(,Q& Results Sampled by Client Date 1.25 % 04/11/2019 1600MPN/g 04/11/2019 Report 7t2019-05822 Page 4 of 4 ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 „r (910) 389-8511 ONWASA Work Order: N191531 (Continued) Analysis Due Expires Comments Sample ID: N191531-07 NW Fecal # 7 SL Sampled. 0411012019 09.26 SUBCONTRACT ORDER (Continued) recal Density Containers Supplied: 120 Sterile Na2S203 (A) 04/20/2019 04/10/2019 15:26 Sample ID: N191531-08 NW Digestor A SL Sampled. • 0411012019 09.20 Hg SW846 7471E 04/20/2019 04/SO/2019; W20 Cd 200.7 04/20/2019 04/10/2019 09:20 As 200.7 - - 04/20/2019 64/10/2019'09:20 r Mg 200.7 04/20/2019 04/10/2019 09:20 Al 200.7 04/20/2019 o4/10/2019'09:20' Ca 200.7 04/20/2019 04/10/2019 09:20 K 200.7 04/20/2019 04/10/2019 69:20 - - Ni 200.7 04/20/2019 04/10/2019 09:20 Na 200.7 04/20/2019"`04/10/2019'09:20 Mc 200.7 04/20/2019 04/10/2019 09:20 pH 04/20/2019 04/10/2019 09:37 Total Solids (%) 04/20/2019 04/17/2019 09:20 Cn- 335.4 04/20/2019 04/24/2019 09:20' Se 200.7 04/20/2019 04/24/2019 09:20 Sulfide colorimetric 04/20J2019' 04/24/2019' 09:20' Zn 200.7 04/20/2019 04/24/2019 09:20 Ammonia Nitrogen - 04/20/2019: 05/08/2019`09;20 Hg 245.1 04/20/2019 05/08/2019 09:20 Total Phosphorus 04/20/2019, 05/08/2019 '09:20 Total Kjeldahl Nitrogen (TKN) 04/20/2019 05/08/2019 09:20 SW'846 Mtd 8270/3510 04/10/2019 -05/08/2019^09:20 Ignitability 04/20/2019 05/08/2019 09:20 Nitrate+Nitrite-Nitrogen 04/20/2015 05108/2019-09:20 SW 846 8081B/3510 04/20/2019 05/08/2019 09:20 Cu 200.7 - - 04/20/2019, 10/07/2019 09:20 Cr 200.7 04/20/2019 10/07/2019 09:20 TCLP Metals 04/20/2019 10/07/2019 09 20 SW846 8260/5030 04/20/2019 10/07/2019 09:20 SW846 8151A _ 04/20/2019 10/07/2019 09:20 - Pb 200.7 04/20/2019 10/07/2019 09:20 Containers Supplied: P 4L (A) 1 I, Relinquished By Date Received By Date Receiving Temp: C Accepted: Rejected: Resample Requested: Delivered By: Received By: Date: Time: Page 2 of 2 0 U LL O ii LL Zw U I.L. z >z w ° Z= u O Z O Z 7 ° d E m N i j n O i w N I J H I z z 10 i Q I N I c � J U U V U U U U Z tip ti ti LL LLu°�. ti aaHio S. Z OIH1 `n O y QHOVN CONH W WVOSZH 1 10H 3NON �] HnewnN E OUPOI40 m V (V JO d) aulr uoO C+ C7 CD I� C7 (D c7 U C7 O 4eJg \ ausotlwoo N adAj aIdweS J U J U J U J (n J U1 J N J (A J U) E Q Q Q O /1 m w N a t �o U O JCZ J J J I V I A c N � w w ' d ik ik ik # Xk # a E m d `m a)w m w w w w w w w ` F _ AN m _ _ T m -em d ❑ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WWTP Name: Northwest Regional WRF WQ Permit Number: W00034806 NPDESNumber WQ0034367 Monitoring Period: From I1l/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: A �•�v rrior i est) U I Process to Furthe to alternative performed (Class A only) indicate "Process to Further ❑ Heat Dryin p Heat Treatment ❑ I- - I - I' ..-- ucucrLY m I air tG) rrocess to Signi. to alternative performed (Class Boni indicate "Process to Happlicableto a ternative performed (Class A or Class $) complete the following monttorin data Parameter Allowable Level Pathogen Density um er o n ica Excee- Frequency Sample in Sludge 'nilnu Geo. Mean Maxim Units of Analysis Type Tech- 2 x 10 to the 6th power MPN 1,291 1,510 1,856 MPN/g 0 Annual Grab SM9221CI per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry Wei ht salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform wei tit lector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: 11t.1 (VS reduction) ❑ Alt. Z (40-day bench) p Alt. 3 30-da bench lt. 5 14-Da Aerobic ( ❑ ( y ) ❑ It. 4 (Speer 02 uptake) ❑ ( Y ) ❑ Alt. 6 Alk. Stabilization Alt 7 (Drying -Stable) It. 8 (Drying -Unstable) ❑ It. 9 {Injection) p Alt 10 (Incorporation) +p No vector attractien reduction altematives were performed ❑ :ERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T .1I07 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the - �•• ••�� auauc unuer my alrection and supervision -in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Mark Young, ORC Wesley Wooten, President Prepare Name and and Tit] (ty r print) Land Applieer�Name and Ti a (if applicable)(type or print) Si nature of Pre / 12/13/19 p ate Signature of L d Applier (if applicable) Date *Preparer is de i d in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 07T (1919(inr) COASTAL FARMS AND RESIDUALS, LLC W00034806 Northwest Regional WRF 04/10/19 1,504 3.1772 04/10/19 1,344 3.1284 04/10/19 1,516 3.1807 04/10/19 1,527 3.1838 04/10/19 1,856 3.2686 04/10/19 1,291 3.1109 04/10/19 1,600 3.2041 Total 22.2538 Average 3.1791 Geometric Mean 151:0€s€i Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 24, 2019 Pluris Hampstead W WTF Permit No. W00037287 2.23 % Solids 5.95 pH ' "';11 .;Parameter ISIgIKg Dry Weight "%z10000) ', ' °PoundslDry Tan"- :,(M IK x0.002'". Nitrogen(TKN) 4.280 42,800.000 85.600 Phosphorus 1.920 19,200.000 38.400 Potassium 0.637 6,370.000 12.740 PAN (injected)* 1.667 16.674.400 33.349 PAN (surface)* 1.618 16,178.400 32.357 Ammonia Nitrogen 0.099 992.000 1.984 Calcium 1.050 10,500.000 21.000 Calcium Carbonate E . --- --- Magnesium 2,970.000 5.940 Sodium 6,500.000 13.000 Sulfur ___ ___ --- Nitrate N /Nitrite N --- 3,140.000 6.280 Barium Chloride - - --- -- --- -- --- SAR 2.15 Iron - -- -- Ceiling Coocen Aluminum --- 22,100.00 44.200 Arsenic - 12.30 0.025 75 Cadmium --- 12.30 0.025 85 Chromium --- 40.400 0.081 --- Copper 113.00 0.226 4,300 Lead --- 12.30 0.025 840 Mercury 0.81 0.002 57 Molybdenum 12.30 0.025 75 Nickel 19.40 0.039 420 Selenium 12.30 0.025 100 Zinc --- 293.00 0.586 71500 Environmental Chemists # 2019-17965 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. f 6602 Windmill Way, Wilinin ton, NC 28405 • 910.392.022 & Lab . 910.392.4.124 Fax 710 Hgwsertown Road, Mantco, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28W • 910.347.5943 Lab/Fax ANALYTICAL $ CONSULTING CHEMISTS ' in ro@anvimnmen otichemists.00m Plurls LLC. Date of Report: Nov 01, 2019 P. O, Box 856 ' Customer PO #: Sneads Ferry NC 28460 Customer ID: 09110001 Attention: Randy Hoffer Report #: 2019-17965 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45854 Site: Sludge 10/24/2019 9:37 AM Solid/Sludge King/Haisc Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 22100mg/kg 10/28/2019 Arsenic EPA200.7 <12,3mg/kg 10128/2019 Cadmium EPA200.7 <12.3mg/kg 10/2812019 Calcium EPA200-7 10500mg/kg 10/28/2019 Chromium EPA200.7 40.4mg/kg 10/28/2019 Copper EPA200.7 113 m/k 9 9 10l2812019 Lead EPA 2001 <12.3 mg/kg 10/28/2019 Magnesium EPA200,7 2970mg/kg 10/2812019 Molybdenum EPA200.7 <12.3 mglkg 10/2812019 Nickel EPA200.7 19.4mg/kg 10128/2019 Potassium EPA200.7 6370mg/kg 10/28/2019 Selenium EPA200.7 <12.3mg/kg 10/28l2019 Sodium EPA200.7 6500mg/kg 10/28/2019 Zinc EPA200.7 293mg/kg 10/2812019 Nitrate+Nitrite-Nitrogen EPA353.2 3140mg/kg 10/29/2019 Total Solids (4/0) SM 2640 B 2.23 % 10/24/2019 pH SM 4500 H B 5.95 units 10129/2019 Ammonia Nitrogen SM 4500 NH3 C 992 mg/kg 10/27/2019 Total Kjeldahl Nitrogen (TKN) SM45000rgB 42800mg/kg 10/2712019 Total Phosphorus SM4600 P F 19200 mg/kg 10/30/2019 Mercury SW8467471B <0.807mg/kg 10126/2019 Report #:: 2019-17965 Page 1 of 3 Environmental Chemists, Inc. t 1 s i 6602 Windmill Way. Wilmington, KC 28405 • 910.392.0223 Lab • 910,392.4424 Fax 710 Bowsertown Road, Nlanteo, NC 27954 • 252.473.5702 Lab/Fax 2.55-A Wilmington Highway, acksomille, NC 2854o • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS in I ow,envi ravne nta Ich emisU.wm Pluris LLC. P. 0. Box 856 Date of Report: Nov 01, 2019 Sneads Ferry NC 28460 Customer PO #: Attention: Randy Hoffer Customer ID: 09110001 Report #: 2019-17965 Project ID: Sludge Lab ID Sample ID: Collect Datelrime Matrix Sampled by 19-45855 Site: 001 10/24/2019 9:32 AM Solid/Sludge King/Halso Test Method Results Date Analyzed Total Solids (%) SM 2540 B Fecal Density 2.03 % 10/24/2019 SM 9221C E MPN 24 hr 503 Lab ID Sample ID: 8375 MPN/ 9 10/25/2019 Collect Date/Time Matrix Sampled by 19-45856 Site: 002 10/24/2019 9:33 AM Solid/Sludge King/Halso Test Method Results Date Analyzed Total Solids (%) SM2540e Fecal Density 2.14 °/. 10/24l2019 SM92210EMPN 24hr503 Lab ID Sample ID: 15421 MPN/ 9 10/25/2019 Collect Date/Time Matrix Sampled by 19-45857 Site: 003 10/24/2019 9:33 AM Solid/Sludge King/Halso Test Method Results Date Analyzed Total Solids (%) SM 2540 B Fecal Density 2.10 10124/2019 SM92210EMPN 24hr503 5239MPN/ 9 10/2512019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-45858 Site: 004 10/24/2019 9:34 AM Solid/Sludge King/Halso Test Method Results Date Analyzed Total Solids (°/9) SM 2540 B Fecal Density 2 42 t0/24/2019 SM92210EMPN 24hr503 3224MPN/ 9 10/25/2019 Lab ID Sample ID: Collect Date rime Matrix Sampled by 19-45859 Site: 005 10/24/2019 9:34 AM Solid/Sludge King/Halso Test Method Results Date Analyzed Total Solids (%) SM 2540 B Fecal Density 1.97 % 10/24/2019 SM 9221C E MPN 24 hr 503 6599 MPN/ 9 10l25/2019 Report 9: 2019-17965 Page 2 of 3 Environmental Chemists, Inc. / 1 6602 Windmill iNav, Wilmington, NC 28405 • 91.0.392,0223 Lab • 910.392.4424 Fax 710 Boo.serlown Road, Manton, NC27954 • 252: i73.5'i02 Lib/Fax 255-A Wiimington Highwa},. lacksunville, NC 28540 • 910.347.5843 Lab/ Fax ANALYTICAL 8 CONSULTING CHEMISTS inFo(nenvi ronmonlalollemists.com Pluris LLC. Date of Report: Nov 01, 2019 P. O. Box 856 Customer PO #: Sneads Ferry NC 28460 Customer ID: 09110001 Attention: Randy Hoffer Report #: 2019-17965 Project ID: Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 19-45860 Site: 006 10/24/2019 9:35 AM Solid/Sludge King/Halso Test Total Solids (%) Fecal Density Lab ID Sample ID: 19-45861 Site:007 Test Method SM 2540 B SM 9221C EMPN 24 hr 503 Method Collect Daterrime 10/24/2019 9:35 AM Results Date 2.18 % 10/2412019 5964 MPN/g 10/25/2019 Matrix Sampled by Solid/Sludge King/Halso Results Date Analvzed Total Solids (%) SM 2540 B 2 05 10/24/2019 Fecal Density SM 9221C E MPN 24 hr503 6342 MPN/ 9 10/25/2019 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported an an as received basis. Reviewed by: _ (osa, Repon #I'. 2019-17965 Page 3 of 3 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WWTPName: PlurisHampstead WWTF WQPerSNumber: WQ003 Monitoring Period: From IIV2019 NPDESNumber: WQ0037287 287 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Derformed: to alternative Eerformed (Class A ❑ Heat Drying ❑ ❑ Gamma Ray ❑ nicable to al Stabilization tr applicable to alternative performed (Class A or Parameter Allowable Level Patho€ in Sludge Minimun Geo. Me 2 x 10 to the MPN 3,224 6,598 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry au,vuo,m uduterial o mrly per 4 grams (in lieu of fecal I total solid (dry I (VS reduction) ❑ JAIL 2 ( 5 (14-Day Aerobic) ❑ Alt. 6 9 (Injection) El JAE10 Process to Further Redu( "Process to Further Reduce ess to Sigui. "Process to 15,421 Excee- Units -___ MPN/g Alt. 3 (30-day bench) C Alt 7 (Drying - Stable) C No vector attraction reduction Aerobic Digestion ❑ monitorin data: Frequency Sample na u ofAmtysis Type Tech. YP Annual Grab sM9221( ..-- -1..... ........ ... j El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the „ccu rrruuc unaer my uirection and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Randy Hoffer, ORC Wesley Wooten, President Preparer Name and Title a or print) Land Applrer Narlie and Title (if applicable)(type or print) /J / 49 11 /4/19 Sign ire of Pre D to Slgnatur of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) r1FNR re)ou DWOC Mr i4mmnnc. COASTAL FARMS AND RESIDUALS, LLC W00034806 Pluris Hampstead WWTF I iii€is i W400*0 tt1` MR........ ram ::::.:.:::::.:::::::::.::>::<:::::: 10/24/19 8,375 3.9230 10/24/19 15,421 4.1881 10/24/19 5,239 3.7192 10/24/19 3,224 3.5084 10/24/19 6,599 3.8195 10/24/19 5,964 3.7755 10/24/19 6,342 3.8022 Total 26.7360 Average 3.8194 Geometric Mean a: 9$ <`>`' I Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 29, 2019 Summerhouse 1.04 % Solids 6.73 DH Permit No. WQ0029945 Parameter % Mg/Kg Dry W eight Pounds/DryTon (% x 10,000) (Mg/Kg x 0.002) NitroRen(TKN) 4.630 46,300.000 1 92.600 BE�M��t ld2L• N / Nitrite N 77.000 37.900 1 0.076 Barium Chloride - - --- --- - - --- SAR 3.35 Iron - - --- - - Ceiling Concen. Aluminum --- 388.00 0.776 M K Arsenic 51.10 0.102 75 Cadmium --- 51.10 0.102 85 Chromium 119.000 --- -- Copper 155.00 0.310 4,300 Lead --- 51.10 0.102 840 Mercury 2.31 0.005 57 Molybdenum 51.10 0.102 75 Nickel 70.00 0.140 420 51.10 0.102 100 ,Zinc --- 3,830.00 7.660 1 7,500 p I 1 1 II Environmental Chemists M 2019.01584 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TICN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. rE�) zS t ��' t ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab s 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.3702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 s 910.347.5843 Lab/Fax info(denvironmentalchenri sts.com Onslow Water & Sewer Authority Date of Report: Feb 20, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report M 2019-01584 Project ID: Summerhouse Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04031 Site: Q190531-01 1/29/2019 9:10 AM Solid/Sludge Todd A Roberts Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 388mg/kg 02/06/2019 Arsenic EPA200.7 <51.1 mg/kg 02/09/2019 Cadmium EPA200.7 <51.1 mg/kg 02/09/2019 Calcium EPA200.7 38500mg/kg 02/03/2019 Chromium EPA200.7 119mg/kg 02/09/2019 Copper EPA200.7 155mg/kg 02/0912019 Lead EPA 200.7 <51.1 mg/kg 0210912019 Magnesium EPA200.7 3870mg/kg 02/03/2019 Molybdenum EPA200.7 <51.1 mg/kg 02/03/2019 Nickel EPA200.7 70.0mg/kg 02/09/2019 Potassium EPA200.7 6710mg/kg 02/03/2019 Selenium EPA200.7 <51.1 mg/kg 02/0912019 Sodium EPA 2003 5550 mg/kg 02/02/2019 Zinc EPA 2007 3830 mg/kg 02/04/2019 Total Kjeldahl Nitrogen (TKN) EPA 351.2 46300 mg/kg 02/07/2019 Nitrate+Nitrite-Nitrogen EPA353+2 37.9mg/kg 0211312019 Total Solids (%) SM 2540 B 1.04 % 01/30/2019 pH SM 4500 H B 6.73 units 02/13/2019 Ammonia Nitrogen SM 4500 NH3 C 1260 mg/kg 02/19/2019 Total Phosphorus SM 4500 P F 33200 mg/kg 02108/2019 Mercury SW8467471B <2.31 mg/kg 02/02/2019 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by: � it�n ry._� �� A n CA f\ '-�4 & OtAINA SA D'enamg Summer House WRF Twining Rose Lane Holly Ridge, NC 28445 Phone: 910.389.8511 Fax: na Project Manager: Todd A. Roberts ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910)389-8511 SUBCONTRACT ORDER Subcontracted Laboratory: Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax: (910) 392-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DL9 CERTIFICATION # 37729 Work Order: Q190531 Analysis Due Expires Comments Sample ID: Q190531-01 SH Digestor SL Sampled; 0112912019 09.10 Hg SW846 74718 Ni200.7 Na 200.7 Mo 200.7 Al 200.7 K 200.7 Cd 200.7 Ca 200.7 As 200.7 Mg 200.7 PH Total Solids (%) Se 200.7 Zn 200.7 Nitrate+Nitrite-Nitrogen Total Phosphorus Ammonia Nitrogen Total Kjeldahl Nitrogen (TKN) Pb 200.7 Cu 200.7 Cr 200.7 Containers Supplied: P 1 liter (A) 02/08/2019 01/29/2019 09:10 02/08/2019 01/29/2019 09:10 02/08/2019 01/29/2019 09:10 02/08/201901/29/200 09:10 02/08/2019 01/29/2019 09:10 02/08/2019-',01/29/2019 09:10 02/08/2019 01/29/2019 09:10 OV68/2019 .01/29/2019 09:10 02/08/2019 01/29/2019 09:10 02/08/2019' 01/29/2019 09:10': 02/08/2019 01/29/2019 09:27 02/08/2019 02/05/2019 09:10 02/08/2019 02/12/2019 09:10 02/08/2019 02/12/2019 09:10 02/08/2019 02/26/2019 09:10 02/08/2019 ``02/26/2019 09:10. 02/08/2019 02/26/2019 09:10 02/08/2019 02/26/2019 09:10 `. 02/08/2019 07/28/2019 09:10 02/08/2019 07/28/2019 .09:10 02/08/2019 07/28/2019 09:10 Sample ID: Q190531-02 SH Fecal # 1 SL Sampled. • 0112912019 09.11 Fecal Density ; 02/08/2019 01/29/2019 15:11 Total Solids (%) 02/08/2019 02/05/2019 09:11 Containers Supplied: f�{/ 120 Sterile Na2S203 (A) Sample ID: Q190531-03 SH Fecal # 2 SL Sampled,' 0112912019 09.12 Fecal Density 02/08/2019 01/29/2019 15:12 Total Solids (%) 02/08/2019 02/05/2019 09:12 -:77;;/w/ " / z Relinquished By Date eRR�By Date Receiving Temp i�}- C Accepted: .1 R��e',eqcrted: Resample Requested: Delivered By: �'m Received By: Dated Z�-/ Time: / Page 1 of 2 ONWASA Laboratory ,' 228 Georgetown Road SUBCONTRACT Jacksonville NC 28540 may" `""'" (910) 389-8511 ORDER + N (Continued) Work Order: Q190531 (Continued) Analysis Due Expires Comments Containers Supplied. 120 Sterile Na2S203 (A) Sample ID: Q190531-04 SH Fecal # 3 SL Sampled: 0112912019 09:13 Fecal Density , r 02/08/2019 01/29/2019 15:13 Total Solids (%) 02/08/2016 02/05/2019 09:13 9 zx�/ Containers Supplied.- 7 L 120 Sterile Na2S203 (A) Sample ID: Q190531-05 SH Fecal # 4 SL Sampled; 0112912019 09:14 Fecal Density 02/08/2019 01/29/2019 15:14 Total Solids (%) 02/08/2019 02/05/2019 09:14 /may Containers Supplied.• v/ 120 Sterile Na2S203 (A) Sample ID: Q190531-06 SH Fecal # 5 SL Sampled., 0112912019 09:15 Fecal Density 02/08/2019 01/29/2019 15:15 Total Solids (%) 02/08/2019 02/05/2019 09:15 Containers Supplied: L��/ 120 Sterile Na2S203 (A) Sample ID: Q190531-07 SH Fecal # 6 SL Sampled: 0112912019 09.16 Fecal Density 02/08/2019 01/29/2019: 15:16 Total Solids (%) 02/08/2019 02/05/2019 09:16 i Containers Supplied: 120 Sterile Na2S203 (A) Sample ID: Q190531-08 SH Fecal # 7 SL Sampled: 0112912019 09:17 Fecal Density 02/08/2019 01/29/2019 15:17 Total Solids (%) Containers Supplied: 02/08/2019 02/05/2019 09:17 120 Sterile Na2S203 (A) Relinquished By Date Received By Date Receiving Temp: C Accepted: Rejected: Resample Requested: Delivered By: Received Bv: n-.-. r__. Page 2 of 2 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab « 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info(ryenviromnen talchemists.com Onslow Water & Sewer Authority Date of Report: Feb 04, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2019-01652 Project ID: Summerhouse Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04212 Site: sludge #1 1/30/2019 8:39 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 1,13 % 01/3112019 Fecal Density SM 9221 C E MPN 24 hr 503 <1593MPN/g 01/31/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04214 Site: sludge #2 1/3012019 8:39 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 1.32 % 01/31/2019 Fecal Density SM92210EMPN 24hr503 <1364MPN/g 01/31/2019 Lab ID Sample ID: Collect Datefrime Matrix Sampled by 19-04215 Site: sludge #3 1/30/2019 8:39 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 G 1.40 % 01/31/2019 Fecal Density SM 9221 C E MPN 24 hr 503 <1286MPN/g 01/31/2019 Lab ID Sample ID: 19-04216 Site: sludge #4 Test Total Solids (%) Fecal Density Lab ID Sample ID: 19-04217 Site: sludge #5 Test Total Solids (%) Fecal Density Collect Date/Time 1/30/2019 8:39 AM Method SM 2540 G SM 9221C E MPN 24 hr 503 Collect Date/Time 1/30/2019 8:39 AM Method SM 2540 G SM 9221C E MPN 24 hr 503 Matrix Sampled by Solid/Sludge Client Results Date Analyzec 1A8% 01/31/2019 <1526MPN/g 01/31/2019 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 1.49 % 01 /3112019 <1209 MPN/g 01/31/2019 x Environmental Chemists, Inc. ANALYTICAL & CONSULTING CHEMISTS Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Attention: Todd Roberts Lab ID Sample ID: 19-04219 Site: sludge#6 Test Total Solids (%) Fecal Density Lab ID Sample ID: 19-04222 Site: sludge #7 Test Fecal Density 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax infotaenviroumen talchemists. com Date of Report: Feb 04, 2019 Customer PO #: Customer ID: 08100092 Report #: 2019-01652 Project ID: Summerhouse Collect Date/Time Matrix Sampled by 1/30/2019 8:39 AM Solid/Sludge Client Method Results Date Analvzed SM 2540 G SM MI EMPN 24 hr 503 1.35 % <1334 MPN/g Collect Date/Time Matrix 1130/2019 8:39 AM Solid/Sludge Method Results SM 9221 C E MPN 24 hr 503 Comment: Results reported on a dry weight basis. Reviewed by: p pj�AC1v 01/31/2019 01131 /2019 Sampled by Client Date Analvzed <1652 MPN/g 01/31/2019 RAn H&" 9MO.MF59 ONWASA za11�L Summer House WRF Twining Rose Lane Holly Ridge, NC 28445 Phone:910.389.8511 Fax: na Project Manager: Todd A. Roberts Work Order: Q190532 ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910)389-8511 SUBCONTRACT ORDER auOContractea LaooratOry: ' ('i yA r•tl z� Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax: (910) 392-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Analysis Due Expires Comments Sample ID: Q190532-01 SH Fecal # 1 SL Sampled., 0113012019 08:39 L fZ ( Z Fecal Density 02/09/2019 01/30/2019 14:39 Total Solids (%) 02/09/2019 02/06/2019 08:39 - Containers Supplied, 120 Sterile Na2S203 (A) Sample ID: Q190532-02 SH Fecal # 2 SL Sampled. • 0113012019 08.39 Fecal Density 02/09/2019 01/30/2019 14:39 Total Solids (°/a) 02/09/2019 02/06/2019 08:39 Containers Supplied. 120 Sterile Na2S203 (A) Sample ID: Q190532-03 SH Fecal # 3 SL Sampled. 0113012019 08.39 Fecal Density 02/09/2019 01/30/2019 14:39 Total Solids(%) 02/09/2019 02/06/2019 08:39 r Containers Supplied: IJ 120 Sterile Na2S203 (A) I Sample ID: Q190532-04 SH Fecal # 4 SL Sampled. • 0113012019 08.39 G�21(P Fecal Density 02/09/2019 01/30/2019 14:39 Total Solids (%) 02/09/2019 02/06/2019 08:39 Containers Supplied.• 120 Sterile Na2S203 (A) Sample ID: Q190532-05 SH Fecal # 5 SL Sampled. • 0113012019 08;39 Fecal Density 02/09/2019 01/30/2019 14:39 Total Solids(%) 02/09/2019 02/06/2019 08:39 Containers Supplied. r" � 120 Sterile Na2S203 (A) ,�� '• t �� s �) `� Sample ID: Q190532-06 SH Fecal # 6 SL Sampled, • 0113012019 08.39 Fecal Density 02/09/2019 01/30/2019 14:39 .r ,4 fry"r &.I2�ZkLaig Relinquished By ate Received By Date Receiving Temp: 0 C Accepted: --- Rej clIte/cl: Resample Requested: Delivered By: Received By: V� Date: 13D I`rf me: SO Page 1 of 2 a- ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910)389-8511 SUBCONTRACT ORDER (Continued) Work Order: Q190532 (Continued) Analysis Due Expires Comments Sample ID: Q190532-06 SH Fecal # 6 SL Sampled: 0113012019 08.39 Total Solids{%} 02/09/2019 ..102106/2019.08:39 Containers Supplied: 120 Sterile Na2S203 (A) Sample ID: Q190532-07 SH Fecal # 7 SL Sampled: 0113012019 08:39 Z74Z2-2 Fecal Density 02/09/2019 01/30/2019 14:39 Total Solids (%) 02/09/2019 02/06/20M, 68:39 Containers Supplied: 120 Sterile Na2S203 (A) Relinquished By ate Received By Date Receiving Temp: C Accepted: Rejected: Resample Requested: Delivered By: Received By: Date: Time: Page 2 of 2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTP Name: Summerhouse W WTP NPDES Number: WQ5029945 Monitoring Period: From 1/I/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt, A (tinichemp) ❑ I Alt B (AIk Treatment) ❑ I Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Beal Treatment ❑ Thermo Julie ❑ Beta Ray 01 Gamma Ray ❑ Pasteurization ❑ - Class B: JAII. (1) fecal Density El I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate"Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Dr ing ❑ Composting ❑ Aerobic Di cstion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g y um ero Excee- Frequency of Analysis Sample Type nay ica Tech - Minimun Geo. MeanMaximun Units Fecal Coliform 2xlOtothe 6tlr power per gram of total solids MPN 1,209 1,415 1,652 MPN/g 0 Annual Grab SM9221Cti CFU 1000 mpn per gram oftotal solid (dry Weight Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight Vector Attraction xeauction (15A NCAC 02T .1107) -Please indicate alternative nerformed: AILI (VS reduction) ❑ JAIL 2 (40-day bench) ❑ jAlt. 3 (30-day bench) ❑ JAR. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (AIk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) [] I Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ID CERTIFICATION STATEMENT (please check the appropriate statement) El "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the •-i nis aererm nation nas been mane under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are significant penalties for false certification including fine and imprisonment" Mike Lutz, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) we,�� 2/25/19 kl w 2/25/19 Signature of Preparer* Date Signature of La Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS & RESIDUALS, LLC WQ0034806 Summerhouse Date Fecal Coliform MPN per grain Log O1/30/19 1,593 3.2022 O1/30/19 1,364 3.1348 O1/30/19 1,286 3.1092 O1/30/19 1,526 3.1836 O1/30/19 1,209 3.0824 O1/30/19 1,334 3.1252 O1/30/19 1,652 3.2180 Total 22.0554 Average 3.1508 Geometric Mean 1415 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: June 13, 2019 Surf City W WTP Permit No. WQ0000795 3.71 % Solids 6.74 pH '. Parameter I % Mg/Kg Dry WeighT POnnds/Dry'fon I (%x 4.660 Ammonia Nitrogen 0.290 2,900.000 5.800 Calcium 3.860 38,600.000 77.200 N / Nitrite N --- 339.000 0 67R Barium --- --- SAR Chloride --- --- --- 1.38 Iron --- - --- Ceiling Concert. Aluminum --- 5,500.00 11.000 M /K Arsenic I9.40 0.039 75 Cadmium 19.40 0.039 85 Chromium --- 22.700 0.045 -- Copper 482.00 0.964 4,300 Lead --- 19.40 0.039 840 Mercury 1.080 0.002 57 Molybdenum -- 19.40 0.039 75 Nickel -- 19.40 0.039 420 Selenium --- 19.40 0.039 100 Zinc --- 3,560.00 7.120 7,500 II I I I I� Environmental Chemists N 2019-09596 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@cnvironmenlalchemists.com Town of Surf City Post Office Box 2475 Surf City NC 28445 Attention: Date of Report: Jul 17, 2019 Customer PO #: Customer ID: 08110024 Report #: 2019-09596 Project ID: Sludge Lab ID Sample ID: Surf City WWTP Collect Date/Time Matrix Sampled by 19-24598 Site: Sludge 6/13/2019 2:00 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 8081B/3510 <0.02 mg/L 06/20/2019 Endrin (TCLP) SW 846 Method 80813/3510 <0.0005 mg/L 06/20/2019 Heptachlor (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 06/20/2019 Heptachlor epoxide (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 06/20/2019 Lindane (TCLP) SW 846 Method 8081 B1351 0 <0.0005 mg/L 06/20/2019 Methoxychlor (TCLP) SW 846 Method 8081B13510 <0.0005 mg/L 06/20/2019 Toxaphene (TCLP) SW 846 Method 808119/3510 <0.05 mg/L 06/20/2019 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/20/2019 2,4,5-Trichlorophenol (TCLP) SW 846 method 6270/3510 <0.050 mg/L 06/20/2019 2,4,6-Trichlorophenol (TCLP) SW 846 method 6270/3510 <0.050 mg/L 06120/2019 2,4-Dinitrotoluene (TCLP) SW 846 method 6270/3510 <0.050 mg/L 06/20/2019 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 06/20/2019 Hexachloro-1,3-butadiene (TCLP) SW 846 method 827013510 <0.050 mg/L 06/20/2019 Hexachlorobenzene(TCLP) SW 846 method 827013510 <0.050mg/L 06/20/2019 Hexachloroethane (TCLP) SW 845 method 8270/3510 <0.050 mg/L 06/20/2019 m + p-Cresol (TCLP) SW 846 method 827a/3510 <0.050 mg/L 06/20/2019 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/20/2019 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/20/2019 Pentachlorophenol (TCLP) SW 846 method 827W510 <0.250 mglL 06/20/2019 Pyridine (TCLP) SW 646 method 827013510 <0.050 mg/L 06/20/2019 2,4,5-TP (TCLP) SW046 Method 8151A <0.003 mg/L 06/21/2019 2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 06121/2019 1,1-Dichloroethylene(TCLP) SW846 Method826016030 <0.01mg/L 06/19/2019 1,2-Dichloroethane(TCLP) SW846 Method8260/5030 <0.01mg/L 0611912019 Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 06/19/2019 Carbon Tetrachloride (TCLP) SW846 Method 8266/50a6 <0.01 mglL 06/19/2019 Report#:: 2019-09596 Page 1 of 4 Environmental Chemists, Inc. envir0` ` 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.57021-ab/Fax 255-A Wilmington f?ighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS iofoCalenvironnlentalchemists,com Town of Surf City Date of Report: Jul 17, 2019 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report M 2019-09596 Project ID: Sludge Chlorobenzene (TCLP) SW846 Method 8250/5030 <0.01 mg/L 06/19/2019 Chloroform (TCLP) SW846 Method8260/5030 <0.01mg/L 06/19/2019 Methyl ethyl ketone (TCLP) SW846 Method826015030 <0.05mg/L 06/19/2019 Tetrachloroethylene (TCLP) SW646 Method 6260/5030 <0.01 mg/L 06/19/2019 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 06/19/2019 Vinyl Chloride (TCLP) SW846 Method 826015030 <0.01 mg/L 06/19/2019 RCI Cyanide EPA335.4 <0.096mg/kg 0612812019 Sulfide SM 4500 S O 0.98 mg/kg 07/12/2019 Ignitability SW 046Method 1010 <70 OF 06/20/2019 Sludge Residuals Aluminum EPA200.7 5500mg/kg 06/18/2019 Arsenic EPA 200.7 <19.4 mg/kg 06/18/2019 Cadmium EPA 200.7 <19.4mg/kg 06/18/2019 Calcium EPA200.7 38600mg/kg 06/18/2019 Chromium EPA 200.7 22.7mg/kg 06118/2019 Copper EPA 200.7 482mg/kg 06/18/2019 Lead EPA 200.7 <19.4 mg/kg 0611812019 Magnesium EPA 200.7 2910mg/kg 06/18/2019 Molybdenum EPA 200.7 <19.4mg/kg 06/18/2019 Nickel EPA200.7 <19.4mg/kg 06/18/2019 Potassium EPA 200.7 2500mg/kg 06/18/2019 Selenium EPA 200.7 <19.4mg/kg 06/1812019 Sodium EPA 200.7 5420mg/kg 06/18/2019 Zinc EPA 200.7 3560 mg/kg 06/18/2019 Nitrate+Nitrite-Nitrogen EPA353.2 339mg/kg 06/2212019 Total Solids (%) SM2540e 3.71 % 06/17/2019 pH SM 4500 H n 6.74 units 07/02/2019 Ammonia Nitrogen sM4599NH3 c 2900mg/kg... 06/21/2019 Total Kjeldahl Nitrogen (TKN) SM4500org8 46600mg/kg 06125/2019 Report #:: 2019-09596 Page.2 of 4 Environmental Chemists, Inc. B B ! 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ^ 910.392.4424 Fax Isiq 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington fiigblmay, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoFi:emlironmen4rlehemists.com Town of Surf City Date of Report: Jul 17, 2019 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2019-09596 Project ID: Sludge Total Phosphorus SM4500PF 23900mg/kg 06/27/2019 Mercury Sw6467471B 1.08mg/kg 06/22/2019 TCLP Metals Arsenic EPA200.7 <1.0mg/L 06/21/2019 Barium EPA200.7 <1.0mg/L 06/21/2019 Cadmium EPA200.7 <1.0mg/L 06/21/2019 Chromium EPA200.7 <1.0mg/L 06/21/2019 Lead EPA200.7 <1.0mg/L 06/21/2019 Selenium EPA200.7 <1-0mg/L 06/21/2019 Silver EPA200.7 <1.0mg/L 06/21/2019 Mercury EPA245.1 <0.0002mg/L 06/22/2019 Lab ID Sample ID: Surf City VVWTP Collect DatelTime Matrix Sampled by 19-24599 Site: 91 6/13/2019 2:05 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM2540G 3.61 % 06/17/2019 Fecal Density SM 9221C E MPN 24 hr 503 96953 MPN/g 06/14/2019 Lab ID Sample ID: Surf City WWTP Collect Date/Time Matrix Sampled by 19-24600 Site: #2 6/13/2019 2:06 PM Solid/Sludge wesley woolen Test Method Results Date Analvzed Total Solids (%) SM 2540G Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Surf City WWTP Collect Date/Time 19-24601 Site: #3 6/13/2019 2:07 PM Test Total Solids (%) Fecal Density Method SM 2540 G SM 9221C EMPN 24 hr 503 3.74 % 06117/2019 64172MPN/g 06/14/2019 Matrix Sampled by Solid/Sludge wesley wooten Results Date Analyzed 3,63% 06/17/2019 66116 MPN/g 06/14/2019 Report#:: 2019-09596 Page 3 of 4 Environmental Chemists, Inc. ob,11 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 55-A Wilminton Highway, Jacksonville, NC 25540 910847.5R43 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infol"a;cnvironmentalchentislscont Town of Surf City Date of Report: Jul 17, 2019 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2019-09596 Project ID: Sludge Lab ID Sample ID: Surf City WWTP Collect Date/Time Matrix Sampled by 19-24602 Site: #4 6/13/2019 2:08 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.50 % 06/17/2019 Fecal Density SM 9221 C E MPN 24 hr 503 100000MPN/g 06/14/2019 Lab ID Sample ID: Surf City WWTP Collect Date/Time Matrix Sampled by 19-24603 Site: #5 6/13/2019 2:09 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.67 % 06/17/2019 Fecal Density SM 9221C E MPN 24 hr 503 147139 MPN/g 06/14/2019 Lab ID Sample ID: Surf City WWTP Collect Date/Time Matrix Sampled by 19-24604 Site: #6 6/13/2019 2:10 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 G 3.60 % 06/17/2019 Fecal Density SM 9221 C E MPN 24 hr 503 66667MPN/g 06/14/2019 Lab ID Sample ID: Surf City WWTP Collect Date/Time Matrix Sampled by 19-24605 Site: #7 6/13/2019 2:11 PM Solid/Sludge wesley wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 G 98.1 % 06/17/2019 Fecal Density SM 9221C E MPN 24 hr 503 1326MPN/g 06114/2019 Comment: Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: halLA, Report M. 2019-09596 Page 4 of 4 INC 6602WndmillWayWilmington, NC26405 tNVIRONMENTAL CHEMISTS °`ii 2•_ia.,i=-" f OFFICE: 91D.392-0223 FAX 910-392.4424 AnalyFcal B Consulting Chemists NCDENR: DWO CERTIFICATION X 94 NCDHHS: DLS CERTIFICATION # 3TT29 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: PROJECT NAME: S REPORT NO: °f _ �! S Yc ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: om np�eu oy: r s/ SAMPLE TYPE: 1 = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other; Collection = _ = e PRESERVATION Sample Identification a ° m E° 0o a 2 E g j o n i i o w ANALYSIS REQUESTED D e Time Tern a 7�a C P (l G G �J�Tie ff 2c� t C G P G C P G G 1 L l C P. l G G C P G G C P G G L' C P G G C P i G G C P G G Transfer Relinquished B Date/Time Received B Date(flme 2. I emperawre when Rece/ved: Accepted: Rejected: Resample Delivered Bv: Received Bv: n.re• Time: ND: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806 WWTPName: Surf CityWWTP NPDESNumber: W00000795 Monitoring Period: From 1/1/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achievers and alternativo norf"rmod. Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment)[] Alt. C (Prior Testing)❑ A1t.D (No Prim Test) ❑ Process to Further Reduce Patheeenas ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying -❑ Heat Treatment ❑ Thentlo hilic ❑ Beta Ray ❑ I Gamma Ray ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density v❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative per -formed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitorin data: Parameter Allowable Level in in Sludge Pathogen Density um er o Excee- Frequency 4 y of Analysis Sample p Type Analytical Tech - inimu Geo. Mean Maxim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids IMPN 1,326 47,368 147,139 MPN/g 0 Annual Grab SM922 (CE 1CFU 1000 mpn per gram oftotal solid (dry weight) Salmonella bacteria (in lieu of fecal colifonn) 3 MPN per 4 grams total solid (dry weight) v ocwr auracuon Reduction t1DA PICAw- 02 .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Ark Stabilization ❑ JAIt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El jAlt. 10 (Incorporation) El INo vector attraction reduction alternatives were performed ❑ l.L'1t llr ll,A L 1VN S A1ElYILN T(please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the --1 ms oerermmanon nos been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Smith, ORC Wesley Wooten, President Prepaarµerr Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) /" 1LjSjl9 W�N 12/6/19 Signature of Preparer* Date Signature of and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) LEWIS FARMS W00000455 Surf City WWTP l�at� E'ee��f�t3n Ivog..;5' 06/13/19 96,953 4.9866 06/13/19 64,172 4.8073 06/13/19 66,116 4.8203 06/13/19 100,000 5.0000 06/13/19 147,139 5.1E 06/13/19 66,667 4.8239 06/13/19 1,326 3.1225 Total 32.7284 Average 4.6755 Geometric Mean 6s!I Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 29, 2019 Swansboro 2.78 % Solids 6.02 PH Permit No. W 00034806 Parameter % Mg/Kg Dry Weight x 1Q000) Pounds/DryToa (M x 0.002) Nitrogen (TKN) 4.630 46,300.000 92.600 Phosphorus 0.053 526.000 1.052 Potassium 0.243 2,430.000 4.860 PAN (injected)* 1.537 15,369.000 30.738 PAN (surface)* 1.446 14,464.000 28.928 Ammonia Nitrogen 0.181 1,810.000 3.620 Calcium 3.260 32,600.000 65.200 Calcium Carbonate E . Magnesium 1,650.000 3.300 Sodium 3,360.000 6.720 Sulfur Nitrate N / Nitrite N --- 212.000 0.424 Barium --- --- --- Chloride --- --- --- Iron --- --- Aluminum --- 5,580.00 11.160 Arsenic 18.10 0.036 Cadmium --- 18.10 0.036 Chromium --- 18.200 Copper 297.00 0.594 Lead --- 18.10 0.0361 Mercury 0.94 0.002 Molybdenum 18.10 0.036 Nickel 18.10 0.036 Selenium 18.10 0.036 Zinc -- 3,780.00 7.560 Environmental Chemists # 2019-01578 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN SAR 3.82 Ceiling Concert. (Mg/Kl ) 75 85 4,300 840 Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 1� I Environmental Chemists, Inc. ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way, Wilmington, NC 28405 9 91.0.392.0223 Lab e 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5M2 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 m 010.347.5843 Lab/Fax in foriuenvi ro nn1 ental ch en1 i s t s. com Onslow Water & Sewer Authority Date of Report: Feb 20, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2019-01578 Project ID: Swansboro WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04025 Site: S190517-08 1/29/2019 9:30 AM Solid/Sludge Mike Luiz Test Method Results Date Analyze( Sludge Residuals Aluminum EPA 200.7 5580mg/kg 02/06/2019 Arsenic EPA 200.7 <18.1 mg/kg 02/09/2019 Cadmium EPA200.7 <18.1 mg/kg 02/09/2019 Calcium EPA 200.7 32600mg/kg 02/03/2019 Chromium EPA 200.7 18.2mg/kg 02/09/2019 Copper EPA 200.7 297 mg/kg 02/09/2019 Lead EPA 200,7 <18.1 mg/kg 02/09/2019 Magnesium EPA 200.7 1650 mg/kg 02/0312019 Molybdenum EPA 200.7 <18.1 mg/kg 02/03/2019 Nickel EPA 200.7 <18.1 mg/kg 02/09/2019 Potassium EPA 200.7 2430mg/kg 02/03/2019 Selenium EPA 2001 <18.1 mg/kg 02/09/2019 Sodium EPA 200.7 3360 mg/kg 02/02/2019 Zinc EPA 200.7 3780mg/kg 02/04/2019 Total Kjeldahl Nitrogen (TKN) EPA 351.2 46300 mg/kg 02/07/2019 N itrate+ N itrite-N itrogen EPA353.2 212mg/kg 02/13/2019 Total Solids (%) SM2540B 2.78% 01/30/2019 pH SM 4500 H B 6.02 units 02/04/2019 Ammonia Nitrogen SM 4500 NH3 C 1810 mg/kg 02/19/2019 Total Phosphorus SM 4500 P F 526 mg/kg 02/0712019 Mercury Sw8467471B <0.935mg/kg 02/02/2019 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by: _ �"a ENrn A L OOL Remrt#" 2019-0157R 0IVIUVA namg Lanoratory: Swansboro WWTF 228 Georgetown Road 3acksonville, NC 28540 Phone:910.389.8511 Fax: na Project Manager: Mike Lutz Work Order: S190517 ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910)389-8511 SUBCONTRACT ORDER �y Subcontracted Laboratory: 70 rs sr,. � .0 Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax: (910) 392-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 174naiysis Due Expires Comments Sample ID: S190517-01 Swan Fecal #1 WW Sampled., 0112912019 09.30 Fecal Density 02/08/2019 01/29/2019 15:30 Total Solids (%) 02/08/2019 02/05/2019 09:30 Containers Supplied:✓�(f 120 Sterile Na2S203 (A) Sample ID: S190517-02 Swan Fecal #2 WW Sampled.- 0112912019 09.30 Fecal Density 'Solids 02/08/2019 01/29/2019 15:30 Total (%) 02/08/2019 02/05/2019 09:30 Containers Supplied.g qqq 120 Sterile Na25203 (A) Sample ID: S190517-03 Swan Fecal #3 WW Sampled. • 0112912019 09.30 Fecal Density 02/08/2019 01/29/2019 15:30 Total Solids (%) 02/08/2019 02/05/2019 -09:30 Containers Supplied: 120 Sterile Na25203 (A) Sample ID: S190517-04 Swan Fecal #4 WW Sampled: 0112912019 09:30 Fecal Density 02/08/2019 01/29/2019 15:30 Total Solids(%) 02/08/2019 02/05/2019 '09:30- Containers Supplied.• 120 Sterile Na2S203 (A) �! Sample ID: S190517-05 Swan Fecal #5 WW Sampled., 0112912019 09.30 Fecal Density 02/08/2019 01/29/2019 15:30 Total Solids(%D) Containers Supplied. 02/08/2019 02/05/2019 09:30 / 120 Sterile Na25203 (A) Sample ID: S190517-06 Swan Fecal #6 WW Sampled; 0112912019 09.30 Fecal Density 02/08/2019 01/29/2019 15:30 / Lam/ ke?y lr Relinquished By Date ceiVed By Date Receiving Temp:.• !✓� C Accepted: vOi ezz/ Rej tt dy:.e Resample Requested: Delivered By: Received By: 'i /t Date: % Time:i's—r r .3� Page 1 of 2 ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910)389-8511 Work Order: S190517 (Continued) Analysis Due Expires Comments Sample ID: S190517-06 Swan Fecal #6 WW Sampled., 0112912019 09:30 SUBCONTRACT Total Solids (%) 02/08/2019 '' 02/05/2019 09:30 Wzz? Containers Supplied.• �/ 120 Sterile Na2S203 (A) ORDER (Continued) Sample ID: S190517-07 Swan Fecal #7 WW Sampled., 0112912019 09:30 Fecal Density 02/08/2019 01/29/2019 15:30 y Total Solids (%) 02/08/2019 02/05/2019 09:30 Containers Supplied.• 120 Sterile Na2S203 (A) Sample ID: S190517-08 Sboro Digestor A S[ Sampled. 0112912019 09.30 Cd 200.7 02/08/2019 01/29/2019 09:30 A[ 200.7 02/08/2019 01/29/2019 09:30 Na 200.7 02/08/2019 01/29/2019 09:30 As 200.7 02/08/2019 01/29/2019 09:30 Ni 200.7 02/08/2019 01/29/2019 09:30 Ca 200.7 02/08/2019 01/29/2019 09:30 Mo 200.7 02/08/2019 01/29/2019 09:30 Mg 200.7 02/08/2019 01/29/2019 09:30 K 200.7 02/08/2019 01/29/2619 09:30 �! Hg SW846 7471B 02/08/2019 01/29/2019 09:30 PH 02/08/2019 01/29/2019 09:47 Total Solids (%) 02/08/2019 02/05/2019. 09:30 Se 200.7 02/08/2019 02/12/2019 09:30 Zn 200.7 02/08/2019 02/12/2019 09:30 Ammonia Nitrogen 02/08/2019 02/26/2019 09:30 Total Phosphorus 02/08/2019 02/26/2019 09:30 Total Kjeldahl Nitrogen (TKN) 02/08/2019 02/26/2019 09:30 Nitrate+Nitrite-Nitrogen 02/08/2019 02/26/2019 09:30 Pb 200.7 02/08/2019 07/28/2019 09:30 Cu 200.7 02/08/2019 07/28/2019 09:30 Cr 200.7 02/08/2019 07/28/2019 09:30 Containers Supplied.- P 1 liter (A) Relinquished By Date Receiving Temp: C Received By Accepted: Rejected: Resample Requested: Delivered By: Received Date Time: Page 2 of 2 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0273 Lab m 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.4735702 Lab/Fax 255-A Wilmington I-Iighway; Jack-%onville, NC 28540 - 910.347.5843 Lab/Fax i n ro(aenvironmentalchemists.com Onslow Water & Sewer Authority Date of Report: Feb 20, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2019-01578 Project ID: Swansboro WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04018 Site: S190517-01 1/29/2019 9:30 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.87 % 01/3012019 Fecal Density SM 9221C E MPN 24 hr 503 11499 MPN/g 01/30/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04019 Site: S190517-02 1/29/2019 9:30 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) Fecal Density Lab ID Sample ID: 19-04020 Site: S190517-03 Test Total Solids (%) Fecal Density SM 2540 G SM 9221 C E MPN 24 hr 503 Collect Date/Time 1/29/2019 9:30 AM Method SM 2540 G SM 9221C EMPN 24 hr 503 2.79 % 01/30/2019 39427MPN/g 01/30/2019 Matrix Sampled by Solid/Sludge Mike Lutz Results Date Analvzed 2.71 % 01/30/2019 47971 MPN/g 01/30/2019 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04021 Site: S190517-04 1/29/2019 9:30 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.35 % 01/30/2019 Fecal Density SM 9221 C E MPN 24 hr 503 55320MPN/g 01/30/2019 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 19-04022 Site: S190517-05 1/29/2019 9:30 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM 2540 G 2.82 % 01130/2019 Fecal Density SM 9221 C E MPN 24 hr 503 24823MPN/g 01/30/2019 Re° ri #:. 2019-0157A , Environmental Chemists, Inc. 6602 ANindmill Way, Wilmington, NIC 28405 • 910.392.0223 Lab e 910 392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab /Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax in fotrd?environ in enlalchemists.com Onslow Water & Sewer Authority Date of Report: Feb 20, 2019 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2019-01578 Project ID: Swansboro WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-04023 Site: S190517-06 1/29/2019 9:30 AM Solid/Sludge Mike Lutz Test Total Solids (%) Fecal Density Lab ID Sample ID: 19-04024 Site:S190517-07 Test Total Solids (%) Fecal Density Method SM 2540 G SM 9221C EMPN 24 hr 503 Collect Date/Time 1/29/2019 9:30 AM Method SM 2540 G SM 9221C E MPN 24 hr 503 Results Date Analyzed 2,70 % 48149 MPN/g Matrix Sampled by Solid/Sludge Mike Lutz 01/30/2019 01130/2019 Results Date 2.76 % 01/30/2019 47102 MPN/g 01130Y2019 Rennrt k- 2n1n.m 5]a --- -- — —, •�•"Y•••"•• ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Fanm and Residuals, LLC WWTP Name: Swansboro WWTP Monitoring Period: From 1/1/2019 To WQ Permit Number: W00034806 NPDES Number: W00023261 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) [I Alt. C (Prior Testing)❑ AIt.D (No Prior Test) ❑ Process to Further Reduce PathoQen2s ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Beat Treatment ❑ Thennoplulic ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density 0 I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Di lug ❑ I Composting ❑ jAcrobic Digestion ❑ Anaerobic Digestion ❑ - If applicable to alternative performed (Class A or Class B) complete the following monitorin data: Parameter Allowable Level in Sludge Pathogen Density g y er oAnalytical F.umxcee- dennnq Frequency of Analysis Sample Type Tech - Minirnurr Geo. Mean Maximurr Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids I MPN 24,823 35,258 55,320 MPN/g 0 Annual Grab SM92210E CFU 1000 mpn per gram of total solid (dry wei ht Salmonella bacteria (in lieu of focal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIt. 4 (Spec. O, uptake) Alt. 5 (14-Day Aerobic) I_l Alt. 6 (Alk. Stabilization j] All 7 (Drying- Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) I] I Alt. 10 (Incorporation) 0 INo vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the my with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including tine and imprisonment." Mike Lutz, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 2/25/192/25/19 Signature of Preparer* Date Signature of Lay6 Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T,1102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS AND RESIDUALS, LLC W00034806 Swansboro Date Fecal Coliform MPN per gram Log 01/29/19 11,499 4.0607 01/29/19 39,427 4.5958 01/29/19 47,971 4.6810 01/29/19 55,320 4.7429 01/29/19 24,823 4.3949 01/29/19 48,149 4.6826 01/29/19 47,102 4.6730 Total 31.8308 Average 4.5473 Geometric Mean 35,258 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction requirement. COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 25, 2019 The Cape 2.06 %Solids 5.R3 nH Permit No. NC0057703 Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002) Nitrogen (TKN) 0.179 1,790.000 3.580 Phosphorus 2.100 21,000.000 42.000 Potassium 0.317 3,170.000 6.340 PAN (injected)* 0.977 9,770.395 19541 PAN surface)* 0.977 9,767.970 19.536 Ammonia Nitrogen 0.000 4.850 0.010 Calcium 4.080 40,800.000 81.600 Calcium Carbonate E . --- --- Magnesium --- 2,060.000 4.120 Sodium -- 6,310.000 12.620 Sulfur --- --- Nitrate N / Nitrite N --- 9,230.000 18.460 Barium --- - Chloride --- --- Iron _-- ___ Aluminum --- 5,530.00 11.060I Arsenic --- 9.56 0.019 Cadmium --- 9.56 0.019 Chromium --- 19.600 --- Copper --- 397.00 0.794 Lead --- 19.10 0.038 Mercury --- 0.971 0.002 Molybdenum --- 9.56 0.019 Nickel --- 11.40 0.023 Selenium 0.019 Zinc --- 4,710.00 9.420 Environmental Chemists, Inc. R 2019-19864 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN SAR Ceiling Concen. Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. 75 85 840 57 75 420 100 Environmental Chemists, Inc. i 0602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 7 7 CM. 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 L,ib/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@Qnvironmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Dec 18, 2019 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2019-19864 Project ID: sludge Lab ID Sample ID: Lewis / Farms Collect Date/Time Matrix Sampled by � 19-50421 Site: Sludge ITLf- e^Pe11/25/2019 4:00 PM Solid/Sludge Wooten Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 6530mg11kg 11/272019 Arsenic EPA2n0.7 <9.56mg/kg 11/27/2019 Cadmium EPA200.7 <9.56mg/kg 11/27/2019 Calcium EPA 200.7 40800 mg/kg 11/27/2019 Chromium EPA200.7 19.6mg/kg 11/27/2019 Copper EPA200.7 397mg/kg 11/27/2019 Lead EPA2oo.7 19.1 mg/kg 1127/2019 Magnesium EPA200.7 2060mg/kg 1127/2019 Molybdenum EPA200.7 <9.56mg/kg 11/27/2019 Nickel EPA200.7 11.4mg/kg 11/27/2019 Potassium EPA200.7 3170mg/kg 11/27/2019 Selenium EPA200.7 <9.56mg/kg 11/27/2019 Sodium EPA 2007 6310 mg/kg 11/27/2019 Zinc EPA200.7 4710mg/kg 1127/2019 Total Kjeldahl Nitrogen (TKN) EPA351.2 1790mg/kg 12/11/2019 Nitrate+Nitrite-Nitrogen EPA353.2 9230mg/kg 12/04/2019 Total Solids (%) SM 2540 s 2.06 % 11/26/2019 pH SM4500 H a 5.83 units 12/16/2019 Ammonia Nitrogen SM4500NH3 C <4.85mg/kg 12/02/2019 Total Phosphorus SM4500PF 21000mg/kg 12/05/2019 Mercury SW84674718 <0.971 mg/kg 11/30/2019 Repon #:: 2019-19864 Page i of 3 Environmental Chemists, Inc. envird - em 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax �- 710 6owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS inforenvironmentalehemists.com Lewis Farms & Liquid Waste, INC. 8155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Date of Report: Dec 18, 2019 Customer PO #: Customer ID: 14020008 Report #: 2019-19864 Project ID: sludge Lab ID Sample ID: Lewis Farms Collect DatelTime 19-50422 Site:1 11/25/2019 4:05 PM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Lewis Farms Collect Daterrime 19-50423 Site: 2 11/25/2019 4:06 PM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Matrix Sampled by Solid/Sludge Wooten Results Date Analyzed 2,25% 11/26/2019 14667MPN/g 11/26/2019 Matrix Sampled by Solid/Sludge Wooten Results Date Analvzed 2.40% 11/26/2019 20417MPN/g 11/26/2019 Lab ID Sample ID: Lewis Farms Collect Date/Time Matrix 19-50424 Site: 3 11/25/2019 4:07 PM Solid/Sludge Test Method Results Total Solids (%) Fecal Density Lab ID Sample ID: Lewis Farms 19-50425 Site:4 Test Total Solids (%) Fecal Density Lab ID Sample ID: Lewis Farms 19-50426 Site:5 Test Total Solids (%) Fecal Density SM 2540 B SM 9221C E MPN 24 hr 503 Collect Date/Time 11/26/2019 4:08 PM Method SM 2540 B SM 9221C EMPN 24 hr 503 Collect Date/Time 11/25/2019 4:09 PM Method SM 2540 B SM 9221C EMPN 24 hr503 Sampled by Wooten Date 2.07% 11/26/2019 11112MPN/g 11/26/2019 Matrix Sampled by Solid/Sludge Wooten Results Date Analvze< 2.28 % 11/2612019 14474MPN/g 11/26/2019 Matrix Sampled by Solid/Sludge Wooten Results Date Analyze( 2.21 % 11/26/2019 14933MPN/g 11/26/2019 Report #'.2019.19854 Page 2 of 3 Environmental Chemists, Inc. envir1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax (sM; 710 Bowsertown Road,Manteo, NC 27954 0 252.473,5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347:5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(ajenvironmentalchemists.com Lewis Farms 8 Liquid Waste, INC. Date of Report: Dec 18, 2019 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2019-19864 Project ID: sludge Lab ID Sample ID: Lewis Farms Collect Date/Time Matrix Sampled by 19-50427 Site: 6 11/25/2019 4:10 PM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2.38 % 11/26/2019 Fecal Density SM 9221C E MPN 24 hr503 71429 MPN/g 11/26/2019 Lab ID Sample ID: Lewis Farms Collect DatelTime Matrix Sampled by 19-50428 Site:7 11/25/2019 4:11 PM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2 26 11/26/2019 Fecal Density SM 9221 C E MPN 24 hr 503 9735MPN/g 11/26/2019 Comment: Sludge residuals and Fecal Density reported on a dry weight basis. pH reported on an as received basis, Reviewed by: klQt,1. hpl 11 1W, Report #r. 2019 19864 Pape 3 of 3 6602 NC 28405 ENVIRONMENTAL CHEMISTS, INC OFFICE:i910-3g -0223 ilmingto FAX 910-3 2- r Analytical & Consulting Chemists NCDENR: DWO CERTERCCATION If 94 NCDHHS: DLS CERTIFICATION # 37729 4424 COLLECTION AND CHAIN OF CUSTODY CLIENT- CAW 5 u^^j PROJECT NAME. REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: E-MAIL: Sampled By: tJ" SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification p Collection a ' m F m a 2 E `o s m E ao m r E Q W m m z PRESERVATION ANALYSIS REQUESTED Date Time Temp5 z = o i o �a li'i �f/., 7(/•'..."73 .s«-+i� G G t i D fLL / TS G G L o40 G G C P {OgLj G G s� Its G G y 's C P G G C e F)dU1 G G ' C P Sa�La G G C P G G C P G G NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorineleo (0.2 ppm or less) in the field at the time of eallectian. See reverse for instructions Transfer Relinquished By: Daterrime Received By: DateTme 1. 2. Temperature when Delivered By: Received TU Time: V*if ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: W00034806 WWTPName: The Cape WWTP NPDCSNumber: NCO057703 Monitoring Period: From 1/1/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .11061- Please indirnta favor A�h...aa —A .a+ +:.. : ..v...... vv u.au nllw 11g11,G 1J011 Vl IIIGYr Class A: Alt. A (tinge/tclu) ❑ Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ HeatDrying ❑ Heat Treatment ElThemrophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ ''_ ;'r i'. '#"-ji>='<.>'i»'.:'> `❑ ..: Class B: jAlt. (1) Fecal Density El I Alt. (2) Process to Significantly� Reduce Pathogens If applicable to altenrntive performed (Clnss B only indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Dryin ❑ Co m ostin ❑ JAerobic Di estion ❑ Anaerobic Digestion ❑'::#�;;::>::>'z>::::::::,:::>::..:::>,:::,:;s;:::;::e.;:;:.z<:,:�:::;::.::::•:.;:.:;.,.;,::;:;.::.: :y:.:.: Y... i::::.:.:F :v:. i h.: riii:i:v>:',\: n�:n::ii,i:.:.iiiiii: �i::;kyi:•i>:•'l.;:_:ii� v:;iji'i:i%tiv:::{{ fi:� ��i: If applicable to alternative erformed (Class A or Class B) complete the follolving monitoring data: Allowable Level Pathogen um er o Analytical Parameter en Density Frequency Sample e Excee- Tech - in Sludge inimu Geo. Mean Maximurr Units dencen of Analysis Type 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram oftotalsolid (dry 9,735 17,487 71,429 MPN/g 0 Annual Grab SM92210E wet ht) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform wei t Va,.+q.-e+rya w D-A.. nc♦ ..� ,, a -- V 1. t.� l.. e. vita .> io �/ - Haase marcate aternative erfor d Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ p me . Alt: 3 (31-day bench) ❑ Alt. 4 (Spec. Or uptake) ❑ Alt. 5 (14 Day Aerobic) El JAR. 6 (Alk. Stabillzation ❑ Alt 7 (Drying- Stable) El JAIL 8 (Drying- Unstable) ❑ Alt. 9 (Injection) l Alt. 10 (incorporation) 0 No vector attraction reduction alternatives were performed ❑ C1?WP11V1! A TTAAr CT A mnw.mw.m 1_ • -- ---- I va, v•cAalmrarnN is jjxuase caeca me appropriate statement) O "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) Y.,.�l llYllgrlV ll llnb YCCI: ruaue under my atrection unit supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Eric Youngs, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) ZpZU �d {/ 1l23/2020 Signature or�e>urer* ate Signature o and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS AND RESIDUALS, LLC W00034806 The Cape WWTP Ml'N er' ari 11/25/19 14,667 4.1663 11/25/19 20,417 4.3100 11/25/19 11,112 4.0458 11/25/19 14,474 4.1606 11/25/19 14,933 4.1741 11/25/19 71,429 4.8539 11/25/19 9,735 3.9883 Total 29.6991 Average 4.2427 Geometric Mean I� 17,487 :'; �� Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 23, 2019 Oak Island W WTP 1.62 % Solids 6.91 off Permit No. W00005790 Parameter % Mg/Kg Dry Weight (% x 10,00D -Pounds/Dry Ton M x 0.002 Nitrogen (TKN) 1.770 17,700.000 35.400 Phosphorus 0.815 8,150.000 16.300 Potassium 0.152 1,520.000 3.040 PAN (injected)* 0.644 6,441.800 12.884 PAN (surface)* 0.565 5,646.800 11.294 Ammonia Nitrogen 0.159 1,590,000 3.180 Calcium 1.770 17,700.000 35.400 Calcium Carbonate E . -- Magnesium 1,010.000 2.020 Sodium 2,220.000 4.440 Sulfur Nitrate N / Nitrite N -- 18.800 0.038 Barium Chloride --- Iron _ Aluminum --- 2,010.00 4.020 Arsenic 30.60 0.061 Cadmium --- 30.60 0.061 Chromium --- 30.600 0.061 Copper 107.00 0.214 Lead --- 30.60 0.061 Mercury 1.30 0.003 Molybdenum 30.60 0.061 Nickel 30.60 0.061 Selenium 30.60 0.061 Zinc --- 345.00 0.690 Environmental Chemists N 2019-01276 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN SAR Ceiling Concen. Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or <detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Line. II • 1 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 < 252-473.5702 Lab/Fax 255-A Wimington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalehemists-eom Town of Oak Island Date of Report: Feb 07, 2019 4601 East Oak Island Drive Customer PO #: Oak Island NC 28465 Customer ID: 11100035 Attention: David Kelly, II Report #: 2019-01276 Project ID: Fish Factory WWfP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 19-03269 Site: Sludge 1/23/2019 10:30 AM Solid/Sludge Kenneth Von Voigt Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 2010mg/kg 01/30/2019 Arsenic EPA 200.7 <30.6mglkg 01/30/2019 Cadmium EPA 200.7 <30.6mg/kg 01/28/2019 Calcium EPA 200.t 17700mg/kg 02/02/2019 Chromium EPA 200.7 <30.6mg/kg 01/28/2019 Copper EPA 200.7 107 mg/kg 01128/2019 Lead EPA 200.7 <30.6 mg/kg 01/28/2019 Magnesium EPA 200.7 1010mg/kg 02/02/2019 Molybdenum EPA 200.7 <30.6mg/kg 01/30/2019 Nickel EPA 200.7 <30.6mg/kg 01/28/2019 Potassium EPA20o7 1520mglkg 02/04/2019 Selenium EPA 200.7 <30.6mg/kg 01/28/2019 Sodium EPA 200.7 2220 mg/kg 02/02/2019 Zinc EPA 200.7 345mglkg 01/28/2019 Total Kieldahl Nitrogen (TKN) EPA 351.2 17700 mg/kg 02/05/2019 Nitrate+Nitrite-Nitrogen EPA353.2 <18.8mg/kg 02/06/2019 Total Solids (%) SM25408 1.62 % 0112412019 pH SM 4500 H e 5.91 units 02/04/2019 Ammonia Nitrogen SM 4500 NH3 C 1590 mglkg 02/06/2019 Total Phosphorus SM 4500 P F 8150 mg/kg 02/0612019 Mercury SW84674715 <1.30mg/kg 01/26/2019 Comment: `Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: kA' l�l � OYy.hl= p RepofU�:: 2019-01275 Page 1 of 1 ENVIRONMENTAL CHEMISTS, INC 6602Windmi ll Way Wilmington, NC 28405 NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 OFFICE: 910-392-0223 FAX 910-392.4424 Analytical & Consulting Chemists Prfl 1 L: `71 hl Akin ( LjAikl no nl ICT"', CLIENT: Town of Oak Island PROJECT NAME: Fish Factory WWTP v REPORT NO: J l ADDRESS: 4601 East Oak Island Drive CONTACT NAME: David Kelly, II (Director) PO NO: Oak Island, NC 28465 REPORT TO: Tray Bivins (tbivins@ci.oak-island.nc.us PHONEIFAX: 201.80411278.7438 Permit# WQ0005790 email:dkelly@ci.oak-is land. nc.us Sample Identification P Collection ' m w E° 0° J ° E " W ¢ E z .. .....1, -.. - ,•. PRESERVATION - v." -1 - a uuye valet ANALYSIS REQUESTED Date Time Temp W. =_ o' o _ 0 _ o w o g "Otn rc-'- fCnt �fJL1U� I- 23'!4 0'• io C P )-. "i X X Slo �k"erL- lzxw` G e .. i B@B 7 SS`Ni9�3 NH�9-TKN _ G G Effluent C P X —F-sc—a1-CoTiT37 rr--, G G 2/month Apr -October C P G G 1/month Nov -March C P G G C P G G Feb/June/October C P _ X X TDS, TOC, Chloride G G C P G G C P G G C P GtGtC LIMITS (daily): Boo 15 mg/L. NR3 6 mg/L, TSS 10 mg/L, Fecal 25 coloniesH 00 r01 Transfer 1. 2. , Rely ul-shad;By:, '; ! G- Date/Time Received By: D to/Time Delivered By:, Comments: By: ;ample Requested: Date: Z 41--?f Time: —TURNAROUND: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) FacilityName: Coastal Farms and Residuals, LLC W W TP Name: Oak Island W WTP Monitoring Period: From 19 To WQ Permit Number: WQ0034806 NPDES Number: W00005790 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) -Please indicate level achieved and alternative erformed Class A: Alt. A (time/tem) ❑ Alt B (Alk Treatment) ❑ P 'Alt. (Prior Testing)❑ :: A1t.D (No Prior Test) ❑ I Process to Further Reduce Patho-en s ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat D ino ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray ❑ I Gamma Ray ❑ Pasteurization Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to SjEjficantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization l7 Air D ing ❑ Corn ostin ❑ jAerobic Digestion ❑ Dig estion 1 If applicable table t o alternat' the performed ed Class A P ( or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density um er o Frequency Sample na tica y in Slud a g Minimu Geo. Mean Maximu Units Excee- Analysis Type Tech- 2 x 10 to the MPN —Auncesof 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams _7 (in lieu of fecal total solid (dry coliform) weight) �.. �...�..�� Loa I, l.tlt. vA 1 .11v i 1 - rreace inn rnre mrnrn arivn Alt.l (VS reduction) ❑ JAR. 2 (40-day bench) ❑ __._____ _________ ._r-A..,......... Alt. 3 (30-day bench) ❑ jAlt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization (] Alt 7 (Drying -Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ JAR. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ !`Lin TYvrl, A TYl .i '..A ADAl.n I JWJJ 01,MJLclY1lS1V r tprease cnectc the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." u ••t certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation wiry you have not met one or both of the made under my accordance designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer Name and Titleype or print) Gt/�r Signature of P parer* Land Applier Name and Title (if applicable)(type or print) 1/13/2020 Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) COASTAL FARMS AND RESIDUALS, LLC WQ 0034806 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Oak Island WWTP P.O.# Batch Size (gallons): 90000 +l• Lbs. or Gallons Used: Material Used For Stabilization: Lime E'EMEM Co ®®®� '®® ®®� '®® ®® •� '®® CO _ Q V d Cc O LL O N > a O N > a O N > a O N > a. O N > a O N > a O N > a O N > a N O N a O N > a 10 O N > a O N > a. O) O O N > a (O O O N > a Cl O O N > a O M O o N C [O O O C OI O O C N 0 C g f O N C g tp O N C N O C y N o N C g n N O C O nl O N C g t7 t7 Ci N C Ip I7 O N C O] nl O C g N V O C N V O C U m V M M n Ih ID co � M <r M M M N M M O co M N 00 N t\ N O N to N 'ITN N M N N N N O N M Cc f� CO —— O— I- 2019 APPLICATION SUMMARY Coastal Farms and Residuals, LLC Permit # WO0034806 2019 Field Application Summary FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC -I CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total Gallons NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93A0 CROP Com/Wheat Com/Wheat Com/Wheat Corn/Wheat Com/Wheat Cnm/Wheer CnmAvheat rnnJWhnar 0nm/W6.m r„ rrvhes, r.,..dw6ve. ne......a..m.,e l Source: ................................. - .............. _ I ,Avondale .................. 46,000 .Caralina Beach 1,020,000 Oak Island -... __......._............................ . Northwest. Regional 469,000 336,000 • .Pluris Hampstead 382,000 j .Summerhouse F................._._._........... 182,000 I S u r I City 757,500 Swan s6Oro 552,000 The Cape ................................ .............. I .......... .. 1,042,000 Total - - - - _ _ _ _ - - - 4,786,500 4,786,500 FIELD NO. AW-1 AW-2 AW-3 AWJ CPC-1 CPC-2 CB-1 NET ACRES 13.90 21.50 16.90 5.90 71.80 55.40 11.80 CROP Soybean/Wheat Soybean/Wheat Soybean/Wheat Com/Wheat Soybean/Wheat Soybean/Wheat So bean/li Morehead City Total CB-1 CFC-1 CFC-2 11.80 8190 72.80 AS-1 WC-1 Total 70.20 93.40 aswl/R a Bermuda/Rye 496 Wet Tons 496 496 FIELD APPLICATION SUMMARIES Coastal Farms and Residuals, LLC Permit # W00034806 2019 Field Application Summary SOURCE: Avendale FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC -I CPC-2 CB-1 CB-2 CFC-I CFC-2 AS-1 WC-1 Total NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons SITE Wooten Wooten Woolen Wooten Corben Packine Corben Packine CorbeOBrothers Corbett Brothers Cnrhett Farminn rnrhea Vnm'i— sinh,.— W rn'h.n January :............................... I February March ..........April......... ............................ May ..... .._...._... -......... 12,000 12,000 ' June 4,000 4,000 July August :............................... 12,000 12,000 1 September October 1 ............................... 8,000 8,000 November 10,000 10,000 December Total - - - _ - - - - - - - 46,000 46,000 Soybeans Com Wheat Rye Bermuda ------------ 46,000 46,000 Coastal Farms and Residuals, LLC Permit # W00034806 2019 Field Application Summary SOURCE: Town of Carolina Beach W WTP FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC -I CPC-2 C11-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 I1.80 15.00 81.90 72.80 70.20 93.40 Gallons SITE Woolen Wooten Wooten Wooten CorbetlPackine Corbett Packine CorbettBrothers Corbettemlhsrs Cnrhen Famine Cnrhen Famine cidh,vv W P—han January ................................ l February March ........... l 120,000 120,000 1— ' Aril 120,000 120,000 May ................ 120,000 120,000 June 1... ........... ................. 120,000 120,000 July ................................ 135,000 135,000 August ............................... 135,000 135,000 September ............................... 135,000 135,000 October :............................... 135,000 135,000 November December Total - - - - _ _ - - _ _ _ 1,020,000 1,020,000 Soybeans Corn Wheat Rye Bemmda ------------ 1,020,000 1,020,000 SOURCE: Morehead Citv WWTF FIELDNO. AW-I AW-2 AW-3 NET ACRES 13.90 21.50 16.90 SITE Wooten Wooten Wooten Coastal Farms and Residuals, LLC Permit 4 W00034806 2019 Field Application Summary AW-4 CPC -I CPC-2 CB-1 CB-2 CFC-I CFC-2 AS-1 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 Wooten Corbett Packing CorbettPackme Cmben Brothers Concru Brnrhera Cnrhee Fa,,,,t— WC-1 Total 93.40 Wet Tons January ..............I ........... .._. 2120 212 February - ................. March April ....... i........................ 83.0 83 May ............June I............ ......... l.... uly ................................ August t...................I......... _ 177.0 177 September r............................. October I............................... November December 24.0 24 Total - - - _ _ _ - - - - - 496 496 Soybeans Com Wheat Rye Bermuda ------------ 496 496 Coastal Farms and Residuals, LLC Permit # W00034806 2019 Field Application Summary SOURCE: Northwest Regional WWTF FIELDNO. AW-1 AW-2 AW-3 AW4 CPC-1 NET ACRES 13.90 21.50 16.90 23.40 68.80 SITE Wooten Wooten Wooten Wooten Corbett Pac January .............................. February .................. _..... _ March ............................. April ............................. May ............................. June ........... -- ... .......... July ............................. August ............................. September ........................... October November Total I - I - I - I - Soybeans Com Wheat Rye Bermuda CPC-2 CB-1 CB-2 CFC-1 55.40 11.80 15.00 81.90 lea Packing Corbett Brothers Corbett Brothers CorbettFan CFC-2 AS-1 WC-1 Total 72.80 70.20 93.40 Gallons Corbett Farming Sidbury W. Corbett 336,000 336,000 ------------ 336,000 336,000 336,000 336,000 336,000 336,000 Coastal Farms and Residuals, LLC Permit N W00034806 2019 Field Application Summary SOURCE: Town of Oak Island W WTP FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing, Corbea Brothers Corhem Brothers rnrMn aarn,ing rn.han nor,.d.,., enh...., January : ............................... February March :............................... 162,000 162,000 I April May ................................ ' June }................. _...... ..... - ' :.,,,,.,.,,,, ...... .......... 98,000 98,000 I August 1 ................. .............. 118,000 118,000 September ............................... - October ............................... 1 November 91,000 91,000 December Total - - - - - - - - - - - 469,000 469,000 Soybeans Corn Wheat Rye Bermuda ------------ 469,000 469,000 SOURCE: Pluris Hampstead WWTP FIELD NO. AW-1 AW-2 AW-3 NETACRES 13.90 21.50 16.90 SITE Wooten Wooten Wooten Coastal Farms and Residuals, LLC Permit # W00034806 2019 Field Application Summary AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-I CFC-2 AS-1 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 Wooten Corbett Packine Corbett Packine Corbett Brothers Corbett Brothers (7mhett Fnnninn Cnrhett Farmmv SIAh..... WC-1 Total 93.40 Gallons W r—h>n January :. 6,000 6,000.............................. February j.... ........ ................... 18,000 18,000 ' March ......... 54,000 54,000 ' April 36,000 36,000 May ..................... 66,000 66,000 June 13,000 13,000 ........... July --___ 18,000 18,000 j August 42,000 42,000 I September ............................... 49,000 49,000 October . } .............................. 36,000 36,000 :.November 44,000 44,000 December Total - - - _ _ _ - - - - - 382,000 382,000 Soybeans Corn Wheat Rye Bermuda ------------ ----------- .: III 382,000 Coastal Farms and Residuals, LLC Permit N W00034806 2019 Field Application Summary SOURCE: Summerhouse FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total NET ACRES 13.90 21.50 16,90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons SITE Wooten Wooten Wooten Wooten CorbettPackine CorbettPackine CorbettBrothers CorbettBrothers Cnrhett Farminn Cnrheu Farmh,u Sigh,,,,, W rn'h.a January .................. t............. , February } ............................... March ..... .......... ................ 65,000 65,000 I April May ,........... _................ June ....................... ....... :. July ............................. August September 26,000 26,000 October ................................ 26,000 26,000 November 13,000 13,000 I December 1 11,111 52,000 Total - - - _ _ - - - - - - 182,000 182,000 Soybeans Corn Wheat Rye Bermuda ------------ ----------- r r r 182,000 Coastal Farms and Residuals, LLC Permit # W00034806 2019 Field Application Summary SOURCE: Surf FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC -I CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 SITE Wooten Wooten Wooten Wooten Corbett Packine Corbett Packine Cmhou Rmthers Cnrhen Rrotherc Cnrherc Farmino r—h.0 cam... i— WC-1 Total 93.40 Gallons r.-we.. January ......................... —.. February March 1 ................ ............... 182,000 182,000 ' April May June I....._______...__ ..... 116,500 116,500 July I August 231,000 231,000 September October l............................... 228,000 228,000 November December Total - - - _ _ _ - - - - - 757,500Fi 757,500 Soybeans Cam Wheal Rye Bermuda ------------ 757,500 757,500 Coastal Farms and Residuals, LLC Permit # W 00034806 2019 Field Application Summary SOURCE: SWansboro FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Fanning Corbett Fanning Sidbury, W Corbett January ................................ February }... ........................ .... - March ............................... April }................ ...... ._..... - ..M ; .............aY ,,,.,,,..,, 276,000 276,000 June July I............................... August :............................... September October November ............................... December 276,000 276,000 Total - _ _ _ _ _ _ _ _ _ - 552,000 552,000 Soybeans Corn Wheat Rye Bermuda ------------ 552,000 552,000 Coastal Farms and Residuals, LLC Permit # W00034806 2019 Field Application Summary SOURCE: The Cape FIELD NO. AW-I AW-2 AW-3 AW-4 CPC -I CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 NET ACRES 13.90 21.50 16.90 23.40 68.80 95.40 11.80 15.00 81.90 72.80 70.20 SITE Wooten Wooten Wooten Wooten Corbett Packine Corbett Packina Cnnccu Rrorherc Cnrhrn Rmth— r—hnn Farminn rvM1ru P.—; .. cMd — WC-1 Total 93.40 Gallons I January :............................... 42,000 42,000 February } ............................... 51,000 51,000 March 39,000 39,000 t........._April 51,000 51,000 ,.........May .- .. 101,000 101,000 June 70,000 70,000 ' 1...... ..... JulY........... 100,000 100,000 August . ............................... 165,000 165,000 September ............................... 85,000 85,000 October ............................... 117,000 117,000 November 78,000 78,000 December 143,000 143,000 Total - - - _ _ _ _ _ _ _ - 1,042,000 1,042,000 Soybeans Corn Wheat Rye Beunuda ------------ 1,042,000 1,042,000 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding laboratory analysis. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number WD0034806 Facility Name Coastal Residuals NPDES # See Below W WTP Name See Below 2019 DATA RESIDUAL ANALYSIS DATA Laboratory 1 Environmental Chemist, Inc. 2 3 NPDES# W00030775 NC0023256 NCO026511 W00034367 W01005790 W00037287 W00029915 W00000795 W00023261 NC0057703 W WrP Name Avendala Carolina 9each Morehead City Narthwest Regions Oak Island W WTP Pluria Hampstead Summerhouse Surf City W WrP Swansbora The Cape Composited/Grab 10/23119 04117119 03105119 04110119 01123/19 10/24/19 01129h9 06113I79 01128/18 11125119 Percent Solids ------------ 0.37 4.34 23.5 1.5 1 1.62 2.23 1 1.04 1 3.71 2,78 1 2.06 ory Arsenic 26.60 12.90 9.86 24.50 30.60 12.30 51.10 19AO 18.10 9.56 Cadmium 26.50 12.90 3.52 24.50 30.60 12.30 51.10 19.40 18.10 9.56 Copper 462.00 631.00 743.00 103.00 107.00 113.00 155.00 482.00 297.00 397.00 Lead 26.50 30.20 15.50 24.50 30.60 12.30 51.10 19.40 18.10 19.10 Mercury 4.05 0.53 0.74 1.33 1.30 0.81 2.31 1.08 0.94 0.97 Molybdenum 26.50 12.90 4.38 24.50 30.60 12.30 51.10 19.40 18.10 9.56 Nickel 26.50 13.10 12.40 24.50 30.60 19.40 70.00 19.40 18.10 11.40 Selenium 26.50 12.90 5.69 24.50 30.60 12.30 51.10 19.40 18.10 9.56 Zinc 865.00 906.00 935.00 385.00 345.00 293.00 3.830.00 3,560.00 3,780.00 4,710.00 TKN 111,000.00 50,800.00 60,700.00 21,400.00 77,700.00 42,800,00 46,300.00 46,600.00 46,300.00 1,790.00 Ammonia-Nitmgen 31,300.00 2,090.00 1,270.00 3,240.00 1,590.00 992,00 1,260.00 2,900.00 1,810.00 4.85 Nitrate -Nitrogen 2,180.00 205.00 18.00 174.00 18.80 3,140.00 37.90 339.00 212.00 9,230.00 Total Phosphorus 1 24,400.00 178.00 30,500.00 6.50 8,150.00 19,200.00 1 33,200.00 1 23,9uluxu 526.00 21,000.00 X kaNll-z�- 1/24/20 (SIGNATURE PREPARER) DATE I certify, under enalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalfies for submitting false information, including the passibility of Ones and imprisonment for knowing violations. FIELD LOADING RATE REPORTS ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Coastal Farms and Residents WQPermitp W00034806 Field#: 1 Acres Utilized: 93.9 Land Owner. Wilber Corbett Annual DT's Applied: 668.67 Site B: WC Acres Permitted: 93.4 Operator: Allen Wooten Predominant Sell Series: Autryville-AuB Cation Exchange Capacity(mm 503): 4.2 Crop l Name: Bermuda Crop l Max. PAN: 196 Crop 2 Name: Ryegrass Crop 2 Max. PAN: 50 Application Method: S-Surface/I- Injected Volatilization Rate: Surface-0.5/ Injected or lacurporated-too Date WTs& Gals. mr Gi /Acre % TS DT/ Acre Residual Source Site Cond. Metals Ibs/ac Nutrients fibs/ae M As Cd Cu Pb H Mrs N4 Se Z. PAN PANE P Crop1 Crop2 TKN NH3 N2-N3 2019 46,000 493 0.37 0.01 AvnanleWeVTp D 0.000 0.000 0.007 0.000 0.000 0.000 0.000 0.000 0.013 0.68 0.19 0.37 Bermuda Ry m L69 0.48 0.03 2019 1,020,000 10,921 4.30 L98 Carolina Bnoh D 0.051 0.051 2.494 0.119 0,00E 0.051 0.05E 0.051 3.581 66.85 0.70 Bmmuaa 2aa.so 8.26 0.8E 2019 496 5 23.50 1.25 Morehead Ciw GAD 0.025 0.009 1.854 0.039 0.002 0.011 0.031 0.014 2.334 5.06 4.60 76.13 Bermuda Ry r n 15L50 3.17 0.04 2M9 336,000 3,597 1.50 0.23 Notthanr C/D 0.011 0.011 0.046 0.011 0.001 O.MI 0.011 0.011 0.173 3.99 0.00 Bermuda 9.63 1.46 0.08 2019 382,000 4,090 2.23 0J8 Plana Hammin D 0.009 0.009 0.086 0.009 0.001 0.009 0.015 0.009 0.223 10.42 2.26 14.60 Bermuda Ryegnn 32.56 0.75 2.39 2019 182,000 1,949 1.04 0.08 sammemome G/D 0.009 0.009 0.026 0,009 0.000 0.009 0.012 0.009 0.647 1.61 0.89 5.61 Bermuda Ry ry 7.83 0.21 0.01 2019 757,500 8,110 3.71 1.25 Bart Cityw Dry 0.049 0,049 1.210 0.049 0.003 0.049 0.049 0.049 8.934 41.03 59.98 m Beruda 116.94 7.28 0.85 2019 552,000 5,910 2.79 0.69 smmh. G/D ll 0.025 0.407 0.025 0.001 0.025 0.025 0.025 5.180 10.53 10.0 0.72 Bermad.111susemul 63.44 2AS 0,29 2019 1,042,000 11,156 2.06 0.96 The Cape GIB 0.018 0.018 0.761 0.037 0.002 0.018 10.022 0.018 9.028 13.09 5.64 40.25 Berman. 3.43 0.01 17.69 2019 469,000 5,021 1.62 0.34 tsd`ldamiw Dry 0.021 0.021 0.073 0.021 0.001 0,021 0.021 0.021 0.234 3.09 0.74 5.53 Bemuaa Ryetaae 12.0I 1.08 0.01 Total 4,78C"6 Aonanl lbs/acee Current Cumulative lbdacre Prior Years CunsiddWe Ruled.0.66 PermiHC.P.L.R•'• 0.218 0.20E 6.950 0.318 0.012 0.204 0.237 0.207 30.396 156.34 24.85 203.90 LimeA 0.88 0.83 27.0E 1.33 0.04 0.83 1.16 0.91 8336 196 50 Permit PAN Limt Ist/2nd CropDate Lbs/A O.fi3 20A6 1.01 0.03 0.63 0.92 0.70 5291 36 34 1}3B 267 15 a/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assum that qualified personnel properly gathered and evaluated the information submitted. I otn aware that there arc significant penalties for submitting false information, Including the possibility offines and imprisonment for knowing violations." X / /- ,%,, W4/20 *Application Method: S- Surface,IN - Injection, INC- Incorporation (Signabue oyadApplied) Date **Volatilization Rate:Surface - 0.5, InjectioNlncorpomtion-1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes application that was Injected or Incorporated WMSS, PLLC DENR FORM FSF(12/2006) Mod. SOIL ANALYSIS REPORTS It should also be noted that the Wilbur Corbett — Field WC-1 contained a pH of 5.6 and contained a recommendation of 0.3 tons of lime per acre recommendation. The current pH on these fields are not reflective of the liming amendments applied to the field in late December of 2019 (1 ton/acre), Coastal Farms and Residuals, LLC will continue to monitor this field in the future and make any necessary adjustments to pH as needed. //L44 Martin Mahe Agronomist Page 1 of 1 Report No: 20-014-1095 Account No: 08361 Advisor: Willcox & Matte Soil Solutions, PLLC 7231 B. Summerfield Rd Summerfield NC 27358 G Waypoint,. ANALYTICAL Client: Wilbur Corbett 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Farm: Date Received: 01/14/2020 Date of Report: 01/15/2020 Lab No Field ID Sample ID Soil Class HM% WN pH Ac P-1 K4 S-I Mn-1 Zn-I Zn-AI Cu-/ CEC BS% Ca% Mg% ESP Na SS -I NO3 N 19832 WC-1 MIN 0.9 5.6 0.7 98 56 12 44 93 93 65 3.0 76 51 14 2.6 0.1 Crop Recommendations., 1-Adjust pH to 6.0 Rec Uom Lime (tlacre) lb/acre 0.3 N P2O5 K2O S Mn 3 Mn-AI Zn Cu 49 B Mg 0 Last Crop Comment: Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WfV In g/cm3 North Carolina Division of Water Quality Certification #257. Analysis and fertility rewmmendafions shown on this report are perfonned in accordance within NCDA guidelines, Analysis prepared by: Waypoinl Analytical Virginia, Inc.